Loading...
HomeMy WebLinkAboutNCG030251_MONITORING INFO_20190122STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V DOC TYPE ❑HISTORICAL FILE 12K MONITORING REPORTS DOC DATE Z YYYYMMDD Stormwater Discharge- Monitoring Report for North Carolina Division of Energy, Mineral and and Resources General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCGO3� _.�S''' FACILITY NAME COUNTY T PERSON COLLECTING SAMPLE ,n, i 1 LABORATORY Q, v � 1' Ja s Lab Cert. 0 `�'}---- Comments on sampl llection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR SAMPLE PERIOD [] Jan -June �-J y-Dec or El Monthly' month RECEIVE TO CLASS QORW [�HQW []Trout [[PNA ❑Zero -flow []Water Supply [—].SA JAN 2 2 2019 M6ther - CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION No discharge this period?' Outfall No. Date Sample Collected 1 (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics-5H Urganics Benchmarks _ - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46S29 C0530 00400 01119 01051 01094 00552 78141 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. ' For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Section B, Table 1 to identify the especially sensitive receivingwaterclassifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 ,jo l eta.ihals-, 1!1.). Inc01001a10 I Solvent management plan into ills' Stalnnw ltrr Pnilt,lirlll I'rr vc'nl1 1) I'1a;3 rL:i;' `i() CI'•'llry, c)II'4 lli{ r++i�lltrl'rllr'ilt 1[)1 { If) lilUllil:If )I'}{; r bf, walvod11112 solvent in:111:11.jun1r_°nl plon Oiall include ,I list Ut III[• t0l;Ii Iflkil r'trl'•.11ill (Ul1WpU11111)� +.iyt'rI ind Illt, ollivr t'l,1IttvI1L-- Ilitod In MA kpvnor.,l )'! i_11t. [01 t4tj ,,A! 1;1t;iliiir?5 (!It'CIiIII F, I e'llipl ev tIII • fT0 li mIIitomIt, waivor, tIir rti'.(Io,isor Qi, ll --jpri I I w in] 1�-,Wtnl; CI;ttlIILAUGa AdtCnwr it, tlN.pll 0I)1111 Illy IIItItlily Ell 1N.- Itl•E4IM IW [Wr,.11M dircclty f,'l.Iluel•,ibll' lur t1l.,I1.1gIng Eurllt)11.111t.1' W1111 lilt' 11r•rltlil It,rllllt VI]III, I r';Ir 11rell IvIll Ill! I01,11 1tlxl( olI,.Ilnr',, { 110). t ( orllly ilutt 11) tile. 1)1'!,l Ili my knuwIo4I ,e anil I)lairl, Ill) dilloplul" r)i ( ol)(1-1111 rltt'd tuxit Ill p,Ifllr -, 11111.0 Ihr 51t1t-111W.11r1 ul ;Il t"Is will.. 11 .114' I-XIlQWl1 t() r.Illtt, ill jr ,t.) 111SLdII•h rltl i+lit WN I)Cr(ll 1'041 ;our lilirig till' I:l,t -Iltsr•hoig. • 1t antlt1r1111; r,`pol l I It111111'f r el Illy ll),It till , 1.11 illly 1', IlrY hll'I tlf'1)11U 1; Illy .Ill IN, 111 UV)!,)elfri of till- •.ulvt`111 11)•Irt.)r;t!r1lt'I)I 111:rIt im.II)lloll Ill till! i11111l14Vallt[ 111111tilltill 11;eVel)Itull Hall " r4dTII,• (t'iil;t 11.11110) 0�.-�y�v.� talc (frill tillrl 51f!l,.1111,1' �, wits: Results 1►tust he reported in tlttmerlcal format. Do not report 13riow 1. mit, 60L, : ('CIL, Ntt.ltjAvIt't:1, NI ), (te :)ttuv 5trnilar non rltllrlt:t Irol inrnliii. Wien result•, me let-,lokv il)r' apples ablC Ilmils, tgd in the format, pip wllt'rt' xX I� liho minion .1l valur' ni till dcit't null (lfrlll, ) CI)nrlitt{; 11E1H1, t'tr . it, -- Note: If yuu report a sueriplc value trj cxcess of the benehmarle, you )oust implement firer 1. Tier 1, ar her resf)nnsc>s See Generul P rmrt tc;xr. Part H. Vehicle Maintenance Area Monitoring Results: nnly for facilities averaging 55 gat of new oil per month, _ n Nu disc'haige this perrucl:) - -' --_� Illatu Sample Calieelled1 F24 huur rerinfall amount, Meta Motor Oil ur IN on -Polar 081G{ Total Total Suspended Outhlli Na, Imo/dcl/vrl I lrtches' Hydraulic Oil L's.rgc Pettofettrn Ilyctrocarbnns Solids tiel)elrmarlr. -- - - 15 ttng/L 100 mg/1_ or So tul,/1 ' — - -- - - 116529 l !•!r p11 Qi!';5Z TT rt3S :0 1 umrt;et2r I.UtiC ----�- - r Footnotes from Rm-1 A also apply to Pr&:rt A fflO e• l f ya!e report r: sarl7ple ueiue in c:.cess of the bcnrhmurk, you must implement Ter 1, Fier 2, or Tier 3 response,-. See General Permit text. 1'rrmti l7^t1 :11/iJJf11,; [}j/it/,lrZt SWt! 2,15,I.E•,l rcylUtt 11/1/711t1i I'.tpr 7 Ot � .—ItI AAP1(1 NAk{I I{ MONIII iWI\11G Vi Mf ,I — :,,'i3.YFi:lf:.il:lt[C r.yrj 111J1Nri ft;l rllii,"iIt1177 Bd� iIIP I:BICfllly. `',1 I'i IIIVIIITAi%C,- 11''.FCIIoN II.-- o• •' LXLI I I)AFJC1 5 114 11 IU:}tP; I OR I I if ',r,.MI I'AItA AL II1, At '11.11 "AMI Ott [ I At I 1111C.6,LII TIER Z RLQUjftE.lY71?NTS. ,1 I. 1'1 I{0.9i i r'f,Ij I 0 •rl t I iC1N !' • I W111 3 1IA'. Yc.11lld I A{'1111'i IIAI14 1 M M01IL lit IH,IIMAICK i XCLLI)T NCl S 1('rH I III, SA MI PARAMI. )LIf AT ANY ON! IN I I I Al I ' YES n NO I:] WYES, IIAV..'d;111itIN1AClli11III kt,'Mk.1t1tl_I;t{iNAI.+.fli1(1,i YESQNoE] 111 tAONAI :JI• -R 1• CON I ACI N't1 W Mail orI origintrr copy o fhis lllbT, int rtadinrl ali "flies gisthargq' rr��uarfsts riidiira w�1 ds 4�s,c�j rc>cc'_rpt ojthe lob results (orvt end ojmanutnring period in the case of '7Vta L�ischurae' re�rc�rts� Irs: DIVI•arin of Walt•I (Zu,dlty ftllll IMLI Lt:nlral I IIrl. 1 i J t Nr�. I rI ' i I V I I.[' t, ('I I t L't 1',.itt'q'It,MIMICt1f1111.1 '/0'19161 "I rr ruly, iiode 1 I;t=n,Illy u1 ld:v. tlt,tt LIrI-, dirrunuctit art:i :dl artadimrnr•. wr'rr IitvI1,),111) urttk•r Iity IIit"( line tit '.L111r'rvr,Wn In I:.: •,Vsicctt Lit-,hlfcnL,tl Itr +.•nlr' Llta! h!t,Ihlirll r, ['^.nn[[l't (}I Ultla ly f-',,ttlLct at to CV,Ikll,ite tI IL, r ful nw"rt In ,I If will rl•tl e:,t ,r-tj I H! IIIy 1HIIklr: yr trl lirt' fr: •r•,nn rlr (rrr prl i Why nk.1[ial;l' till• •.y .I [.,II, [>I =':T.r to r r[r•. [kU0 11� rr-0111r,il•h 1•11 1:•ttlt r11q; t Itf• s!1lnntt,t[utn, 111:• 1111u1 iliolirttt • U111111 It•rl 1'. Ire II1,. 1IV ,t [11 :rty knrtwloell [ .1titI It( -Irs'1, trttr. •Irrttr,ikr•, ,nul t f.ritrttlt'[t' i at:.tw.:rr• r;t :' 11u r. . r, 1„usf+I'.'nt itr ti trrl[•• 11.1 • ltlnnrL1Ir11 :.,{,r ilslrtrru,[lu,r: Inr lutlutl; III$ Im ".bully of LrII • :t,cl 1;uI1tnotinivnl Inr kncrwtnl; Ulnk.ttturt'r. ' 4igo�rlure of Pr:mrttt<�• is a• t'rtnllt I�.tk< it/1J:[lii l7�iJ3i/i^f?I _ -- 1WJ �. I.hd IUVL�cr[ 11,'.l�rll3:a_ En4ronmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this Joan, please visit hops:/Idcq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N/CI[t}I cD/--b I•:D1,3l:�l or Certificate of Coverage No.: N_/C/G/ CV 3 /0 {a/S/ l I Facility Narpg: `LAY �� / Chip t: ( 4 I r A' County: R Date of Inspection: Time of Inspection: Total Event Precipitation (inches): 1. o Phone No n i---- . All permits require qualitative monitoring to be performed during a "measurable storm event." I A "measurable storm event" is a storm event that results in an actual discharge from the permitted site I outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm I interval does not apply if the permittee is able to document that a shorter interval is representative for j local storm events during the sampling period, and the perminee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No.Structure (pipe, ditch, etc.): Receivine5tream: strial Activities that occur within the outrfall drainage area: Des/tribe the 1 R Page I of 2 SWU-242. Last modified 05.01/2018 2. Color: Describe the color of the d (light, medium dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): L e'11 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is n'oo solids and 5 is extremely muddy: d 1� 2 3 4 5 7. Is there any foam in the stormwater discharge? O Yes 0 No. 8. Is there an oil sheen in the stormwater discharge? OYes ® No. 9. Is there evidence of erosion or deposition at the out -fall? o Yes ® No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Pare 2 of 2 SWU-242. Last modified 06!01/2018 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis ARM Environmental Services, Inc. 11164 Downs Road Pineville, NC 28134 Attention: Tim McCorkle Project Name: Watts Water SW Lot Number:TL21101 Date Completed:01/07/2019 1 01/07/2019 10:58 AM Approved and released by: Lab Director - Greenville: Lucas Odom A413 -+� 4ccaeoirro 000cir The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (603) 791-9700 Fax (803) 791-9111 wNwu.shealylab,com Page I of 28 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENIR No: K9 NC Field Parameters No: 5639 Case Narrative ARM Environmental Services, Inc. Lot Number: TL21101 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. PesUPCBS by GC The closing continuing calibration verification (CCV) associated with sample TL21101-001, TL21106-001 did not meet acceptance criteria. Sample matrix is suspected to have contributed to this failure. The samples in this batch contributed to DDT and Methoxychlor being killed from the pest column. As such the samples are not being rerun for fear of killing the columns again. SVOCs by GUMS The laboratory control sample (LCS) for analytical batch 93936 marginally exceeded control limits for the following analytes: 2-Chloronapthalene. Shealy Environmental Services, Inc. 105 Vantage Point Drive West Columbia, Sr, 29172 (803) 791-9700 Fax (B03) 791-9111 www,shealylab,com Page 2 of 28 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary ARM Environmental Services, Inc. Lot Number: TL21101 Sample Number Sample ID Matrix Date Sampled Date Received 001 002 Aqueous 12/20120181130 12/21/2018 (1 sample) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 28 SHEALY ENVIRONMENTAL SERVICES, INC. Detection Summary ARM Environmental Services, Inc. Lot Number: TL21101 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 002 Aqueous TSS SIvE 2540D- 6.1 mg/L 5 001 002 Aqueous Lead 200.8 3.3 ug/L 9 001 002 Aqueous Zinc 200.8 79 ug/i_ 9 (3 detections) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 28 Client:ARM Environmental Services, Inc. Laboratory ID:TL21101-001 Description: 002 Matrix: Aqueous Date Sampled; 1212012018 1130 Date Received-.1212112018 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (TSS) SM 254OD-2011 1 12/27/2018 2207 KFE 93502 1 1 - HEM 116648 1 01/02/2019 1017 ARP 93808 CAS Analytical Parameter Number Method Result Q li Units Run TSS SM 2541 6.1 1.4 ni 1 Si - HEM (non -polar materiai) 1664B NO 4.3 1 1 Volatile Organic Compounds by Gi Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 624.1 624.1 1 12/22/2018 0648 STM 93178 Parameter CAS Number Analytical Method Result 0 Li Units Run Acrolein 107-02-8 624.1 NO 5.0 uglL 1 Acrylonitrile 107-13-1 624.1 ND 5.0 uglL 1 Benzene 71-43-2 624.1 ND 1.0 ug/L i Bromodichloromethane 75-27-4 624A ND 1.0 ug1L 1 Bromoform 75-25-2 624.1 ND 1.0 uglL 1 Bromomethane (Methyl bromide) 74-83-9 624.1 ND 2.0 ug/L 1 Carbon tetrachloride 56-23-5 624.1 ND 1.0 uglL 1 Chlorobenzene 108-90-7 624.1 NO 1.0 ug1L 1 Chloroethane 75-00-3 624.1 ND 2.0 uglL 1 2-Chloroethylvinylether 110-75-8 624.1 NO 5.0 ug/L 1 Chloroform 67-66-3 624.1 ND 1.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624.1 ND 2.0 ug/L 1 Dibromochloromethane 124-48-1 624.1 ND 1.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 624.1 ND 1.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 624.1 NO 1.0 uglL 1 1,4-Dichlorobenzene 106-46-7 624.1 ND 1.0 ug/L 1 Dichlorodifluoromethane 75-71-8 624A ND 2.0 uglL 1 1,1-Dichloroethane 75-34-3 624.1 ND 1.0 ug/L 1 1,2-Dichloroethane 107-06-2 624.1 ND 1.0 ug/L 1 1,1-Dichloroothene 75-35-4 624.1 ND 1.0 uglL 1 cis- 1,2-Dichlofoethene 156-59-2 624.1 ND 1.0 uglL 1 trans-1,2-Dichloroethene 156-60-5 624.1 ND 1.0 uglL 1 1,2-Dichlompropane 78-87-5 624.1 ND 1.0 ug/L 1 cis- 1,3-Dichioropropene 10061-01-5 624.1 ND 1.0 11 1 trans-1,3-DichIoropropene 10061-02-6 624.1 ND 1.0 Li 1 Ethylbenzene 100-41-4 624.1 ND 1.0 uglL 1 Methylene chloride 75-09-2 624.1 ND 1.0 ugR 1 1,1,2,2-Tetrachloroethane 79-34-5 624A ND 1.0 uglL 1 Tetrachloroethene 127-18-4 624.1 ND 1.0 uglL 1 Toluene 108-88-3 624.1 NO 1.0 ug/L 1 LOG = Limit of Quantitafion B - Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOG N = Recovery is out of criteria P = The RPD between two GC columns exceeds 4D % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www,shealylab.com Page 5 of 28 Client:ARM Environmental Services, Inc. Laboratory ID:TL21101-001 Description: 002 Matrix: Aqueous Date Sampled:1212012018 1130 Date Received:1212112018 Volatile Organic Compounds by GCIMS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 624.1 624.1 1 12/22/2018 0648 STM 93178 CAS Analytical Parameter Number Method Result Q LOQ Units Run 1,2,4-Trichlorobenzene 120-82-1 624.1 ND 1.0 ug1L 1 1, 1, 1 -Trichlo roethane 71.55-6 624.1 ND 1.0 ug1L 1 1,1,2-Trichloroethane 79.00-5 624.1 ND 1.0 ug1L 1 Trichloroethene 79.01-6 624.1 ND 1.0 uglL 1 Trichlorofluoromethane 75-69-4 624.1 ND 1.0 ug1L 1 Vinyl chloride 75-01-4 624.1 NO 1.0 ug1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 100 70-130 1,2-Dichloroethane-d4 91 70-130 Toluene-d8 102 70-130 Semivolatile Organic Comoounds by GC/MS Run Prep Method 1 625.1 Analytical Method Dilution Analysis Date Analyst 625.1 1 01/0512019 0030 JCG Prep Date Batch 12/2712018 1734 93463 CAS Analytical Parameter Number Method Result Q LOQ Units Run Acenaphthene 83-32-9 625.1 ND 1.6 ug1L 1 Acenaphthylene 208-96-8 625A ND 1.6 uglL 1 Anthracene 120-12-7 625.1 NO 1.6 ug1L 1 Benzidine 92-87-5 625.1 ND 8.0 uglL 1 Benzo(a)anth race ne 56-55-3 625.1 ND 1.5 uglL 1 Benzo(a)pyrene 50-32-8 625.1 ND 1.6 ug1L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 ug1L 1 Benzo(g,h,i)perylene 191-24-2 625A ND 1.6 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 ug1L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 uglL 1 Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 uglL i bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1.6 ug1L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 uglL 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 ug1L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 ug1L 1 2-Chloronaphthalene 91-58-7 625.1 ND 1.6 ug1L 1 2-Chlorophenol 95-57-8 625.1 ND 1.6 ug1L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 ug1L 1 Chrysene 218-01-9 625.1 ND 1.6 uglL 1 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 uglL 1 1,2-Dichlorobenzene 95-50-1 625.1 ND 1.6 ug1L 1 1,3-Dichlorobenzene 541-73-1 625.1 ND 1.6 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = QLantilation of compound exceeded the calibration range ND = Not cetected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shea3y Environmental Services, inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (8o3) 791-9111 www.shealylab.com Page 6 of 28 Client:ARM Environmental Services, Inc. Laboratory ID:TL21101-001 Description: 002 Matrix: Aqueous Date Sampled:1212012018 1130 Date Received:12/2112018 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625A 1 01/05/2019 0030 JCG 12/27/2018 1734 93463 CAS Analytical Parameter Number Method Result Q LOQ Units Run 1,4-Dichlorobenzene 106-46-7 625.1 ND 1.6 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 ug/L 1 2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 ug/L 1 Diethyl phthalate 84-66-2 625.1 ND 1.6 ug/L 1 Dimethyl phthalate 131-11-3 625.1 ND 1.6 ug/L 1 2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 ug/L 1 Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 ug1L 1 2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 ug/L 1 2,4-Dinitrotoluene 121-14-2 625.1 ND 3.2 ug/L 1 2,6-Dinitrotoluene 606-20-2 625.1 ND 3.2 ug/L 1 Di-n-octylphthalate 117-84-0 625.1 ND 1.6 ug/L i 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625A ND 8.0 uglL 1 Fluoranthene 206-44-0 625.1 ND 1.6 ug/L 1 Flttorene 86-73-7 625.1 ND 1.6 ug/L 1 Hexachlorobenzene 118-74-1 625.1 ND 1.6 ug/L 1 Hexachlorobutadiene 87-68-3 625.1 ND 1.6 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 ug/L 1 Hexachloroethane 67-72-1 625.1 ND 1.6 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 ug/L 1 Isophorone 78-59-1 625A ND 1.6 ug/L 1 Naphthalene 91-20-3 625.1 ND 1.6 ug/L 1 Nitrobenzene 98-95-3 625.1 ND 1.6 ug/L 1 2-Nitrophenol 88-75-5 625.1 ND 3.2 ug/L 1 4-Nitrophenol 100-02-7 625.1 ND 8.0 ug1L 1 N-Nitrosodimethylamine 62-75-9 625.1 ND 1.6 ug1L 1 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 1.6 ug/L 1 Pentachlorophenol 87-86-5 625.1 ND 8.0 ug/L 1 Phenanthrene 85-01-8 625.1 ND 1.6 ug/L 1 Phenol 108-95-2 625.1 ND 1.6 ug1L 1 Pyrene 129-00-0 625.1 N❑ 1.6 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not.deiected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 28 Client:ARM Environmental Services, Inc. Laboratory ID:TL21101-001 Description: 002 Matrix: Aqueous Date Sampled: 1212012018 1130 Date Received:1212112018 Run 1 Acceptance Surrogate Q °% Recovery Limits 2-Fluorobiphenyl 73 37-129 2-Fluorophenol 92 24-127 Nitrobenzene-d5 88 38-127 Phenol-d5 93 28-128 Terphenyl-dl4 108 10-148 2,4,6-Tribromophenol 89 41-144 Oraanochlorine Pesticides and PCBs Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608.3 3665A 608.3 10 01/04/2019 0615 CHG 12/27/2018 1405 93455 2 608.3 3665A 608.3 1 01/02120191353 CHG 12/27/2018 1405 93455 CAS Analytical Parameter Number Method Result Q LOQ Units Run Aldrin 309-00-2 608.3 ND 0.40 ug1L 1 Aroclor 1016 12674-11-2 608.3 ND 0.40 uglL 2 Arocior 1221 11104-28.2 608.3 ND 0.40 ug1L 2 Aroclor 1232 11141-16-5 608.3 ND 0.40 ug1L 2 Aroclor 1242 53469-21.9 608.3 ND 0.40 ug1L 2 Arocior 1248 12672-29.6 608.3 ND 0.40 ug1L 2 Arocior 1254 11097-69-1 608.3 ND 0.40 ug1L 2 Aroclor 1260 11096-82-5 608.3 ND 0.40 ug1L 2 gamma-BHC (Lindane) 58-89-9 608.3 ND 0.40 ug1L 1 alpha-BHC 319-84-6 608.3 ND 0.40 ug/L 1 beta-BHC 319-85-7 608.3 ND 0.40 uglL 1 delta-BHC 319-86-8 608.3 ND 0.40 ug1L 1 Chlordane 57-74-9 608.3 ND 4.0 ui 1 4,4'-DDD 72-54-8 608.3 ND 0.40 ug/L 1 4,4'-DDE 72-55-9 608.3 ND 0.40 uglL 1 4,4'-DDT 50-29-3 608.3 ND 0.40 u91L 1 Dieldrin 60-57-1 608.3 ND 0.40 uglL 1 Endosulfan 1 959-98-8 608.3 ND 0.40 u91L 1 Endosulfan 11 33213-65-9 608.3 ND 0.40 ug1L 1 Endosulfan sulfate 1031-07-8 608.3 ND 0.40 u91L 1 Endrin 72-20-8 608.3 ND 0.40 u91L 1 Endrin aldehyde 7421-93-4 608.3 ND 0.40 ug1L 1 Heptachlor 76-44-8 608.3 ND 0.40 ug1L 1 Heptachlor epoxide 1024-57-3 608.3 ND 0.40 ug1L 1 Toxaphene 8001-35-2 608.3 ND 4.0 ug1L 1 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits Decachlorobiphenyl 87 20-131 96 20-131 Tetrachloro-m-xylene 73 30-132 69 30-132 LOG = Limit of Quanttation 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOG N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 28 Client:ARM Environmental Services, Inc. Laboratory ID:TL21101.001 Description: 002 Matrix: Aqueous Date Sampled:1212012018 1130 Date Received:1212112018 ICP-MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 01/03/2019 0924 BNW 12/26/2018 1123 93289 CAS Analytical Parameter Number Method Result Q LOQ Units Run Copper 7440-50-8 200.8 ND 10 ug/L 1 Lead 7439-92-1 200.8 3.3 2.0 u91L 1 Zinc 7440.66-6 200.8 79 10 ug/L 1 LOQ = Limit of QuanttaSen B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO - Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 h H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com f Page 9 of 28 QC Summary Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheatylab.com Page 10 of 28 Inorganic non-metals - MB Sample ID: TQ93502-001 Matrix. Aqueous Batch:93502 Analytical Method: SM 254OD-2011 Parameter Result Q Dil LOQ Units Analysis Date TSS ND 1 1.0 ni 12/27/2018 2207 LOO = Limit of Quafttabon DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria J = Estimated result � LOQ and � DL + = RPD is out of criteria ND = Not detected at or above the LOO Note-. Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 11 of 28 Inorganic non-metals - LCS Sample ID: T093502-002 Matrix: Aqueous Batch:93502 Analytical Method: SM 254OD-2011 Spike Amount Result % Rec Parameter (mg/L) (mglL) Q Dil % Rec Limit Analysis Date TSS 250 250 1 100 90-110 12/2712018 2207 LOG = Limit of Guantilation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GG columns exceeds 40% N = Recovery is out of criteria J = Estimated result < LOO and ? DL + = RPD is out of criteria ND - Not detected at or above the LOG Note:, Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services. Inc. 106 Vantage Point Drive west Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 29 Inorganic non-metals - MB Sample ID: U093808-001 Matrix: Aqueous Batch:93808 Analytical Method: 1664B Parameter Result Q Dil LOCI Units Analysis Date SGT - HEM (non -polar material) ND 1 4.0 mgtL 01/02/2019 1017 LOO = Limit of QuanGtation DL = Detection Limit 1_00 = Limit of Detection P = The RPD between two GC columns exceeds 4D*A N = Recovery is out of criteria J = Estimated result < LOO and , DL t = RPD is out of criteria ND - Not detected at or above the LOO Note:. Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 13 of 28 Inorganic non-metals - !_CS Sample ID: UQ93808-002 Matrix: Aqueous Batch:93808 Analytical Method: 1664E Spike Amount Result % Rec Parameter _ (ni (mg1L) Q Dil % Rec Limit _Analysis Date SGT - HEM (non -polar material) 40 37 1 92 64-132 01102)2019 1017 LOQ = Limit of Quontitalion DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria J = Estimated result � LOD and a DL + = RPO is out of criteria NO = Not detected at or above the LOO Note= Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 14 of 28 Volatile Organic Compounds by GUMS - MB Sample ID: T093178-001 Matrix: Aqueous Batch: 93178 Prep Method: 624.1 Analytical Method: 624.1 Parameter Result Q Dil LOG Units Analysis Date Acrolein ND 1 5.0 ug/L 12/21/2018 2255 Acrylonitrile ND 1 5.0 ug/L 12/21/2018 2255 Benzene ND 1 1.0 ug/L 12/21/2018 2255 Bromodichloromethane ND 1 1.0 ug/L 12/21/2018 2255 Bromoform ND 1 1.0 ug/L 12/21/2018 2255 Bromomethane (Methyl bromide) ND 1 2.0 ug/L 12/21/2018 2255 Carbon tetrachloride ND 1 1.0 ug/L 12/21/2018 2255 Chlorobenzene ND 1 1.0 ug/L 12/21/2018 2255 Chloroethane ND 1 2.0 ug/L 12/21/2018 2255 2-Chloroelhylvinylether ND 1 5.0 u91L 12/21/2018 2255 Chloroform ND 1 1.0 ug/L 12/21/2018 2255 Chloromethane (Methyl chloride) ND 1 2.0 ug/L 12/21/2018 2255 Dibromochloromethane ND 1 1.0 ug/L 12/21/2018 2255 1,2-Dichlorobenzene ND 1 1.0 ug1L 12/21/2018 2255 1,3-Dichlorobenzene ND 1 1.0 ug1L 12121/2018 2255 1,4-Dichlorobenzene ND 1 1.0 ug1L 1212112018 2255 Dichlorodifluoromethane ND 1 2.0 ug1L 12/21/2018 2255 1,1-Dichloroethane ND 1 1.0 ug1L 12/21/2018 2255 1,2-Dichloroethane NO 1 1.0 ug/L 12/21/2018 2255 1,1-Dichloroethene ND 1 1.0 ug/L 12/21/2018 2255 cis-1,2-Dichloroethene ND 1 1.0 ug/L 12/21/2018 2255 trans-1,2-Dichloroethene ND 1 1.0 u9/L 12/21/2018 2255 1,2-Dichloropropane ND 1 1.0 uglL 12/21/2018 2255 cis- 1,3-Dichloropropene ND 1 1.0 ug/L 12/24/2018 2255 Vans-1,3-Dichloropropene ND 1 1.0 u91L 12/21/2018 2255 Ethylbenzene ND 1 1.0 ug/L 12/21/2018 2255 Methylene chloride ND 1 1.0 ug/L 12/21/2018 2255 1,1,2,2-Tetrachloroethane ND 1 1.0 ug/L 12/21/2018 2255 Tetrachloroethene ND 1 1.0 ug/L 12/21/2018 2255 Toluene ND 1 1.0 ug/L 12/21/2018 2255 1,2,4-Trichlorobenzene ND 1 1.0 ug/L 12/21/2018 2255 1,1,1-Trichloroethane ND 1 1.0 ug/L 12/21/2018 2255 1,1,2-Trichloroethane ND 1 1.0 ug/L 12/21/2018 2255 Trichloroethene ND 1 1.0 ug/L 42/21/2018 2255 Trichlorofluoromethane ND 1 1.0 ug/L 12/21/2018 2255 Vinyl chloride ND 1 1.0 ug/L 12/21/2018 2255 Surrogate Q % Rec Acceptance Limit Bromotluorobenzene 99 70-130 1,2-Dichloroethane-d4 88 70-130 Toluene -dB 101 70-130 LOD = Limit of Quantilation P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOO and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the LOD Note-, Calculations are performed before rounding to avoid round -off errors in calculated results Shealy (environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 15 of 28 Volatile Organic Compounds by GC/MS - LCS Sample ID: T093178-002 Matrix:. Aqueous Batch:93178 Prep Method: 624A Analytical Method: 624.1 Spike Amount Result % Rec Parameter (ug1L) (ug1L) Q Dil % Rec Limit Analysis Date Acrolein 200 180 1 91 60-140 12/21/2018 2124 Acrylonitrile 40 42 1 105 60-140 12/21/2018 2124 Benzene 20 20 1 100 65-135 12/21/2018 2124 Bromodichloromethane 20 19 1 93 65-135 12/21/2018 2124 Bromoform 20 20 1 99 70-130 12/21/2018 2124 Bromomethane (Methyl bromide) 20 20 1 99 15-185 12/21/2018 2124 Carbon tetrachloride 20 18 1 89 70-130 12/21/2018 2124 Chlorobenzene 20 20 1 101 65-135 12/21/2018 2124 Chloroethane 20 21 1 105 40-160 12/21/2018 2124 2-Chloroethylvinylether 20 19 1 94 1.225 12/21/2018 2124 Chloroform 20 19 1 96 70-135 12/21/2018 2124 Chloromethane (Methyl chloride) 20 19 1 94 1-205 12/21/2018 2124 Dibromochloromethane 20 19 1 94 53-149 12/21/2018 2124 1,2-Dichlorobenzene 20 21 1 106 65-135 12/21/2018 2124 1,3-Dichlorobenzene 20 21 1 105 70-130 12/21/2018 2124 1,4-Dichlorobenzene 20 21 1 106 65-135 12/21/2018 2124 Dichlorodifluoromethane 20 18 1 88 60-140 12/21/2018 2124 1,1-Dichloroethane 20 20 1 98 70-130 12/21/2018 2124 1,2-Dichloroethane 20 19 1 94 70-130 12/21/2018 2124 1,1-Dichloroethene 20 19 1 96 50-150 12/21/2018 2124 cis-1,2-Dichloroethene 20 20 1 102 70-130 12/21/2018 2124 trans-1,2-Dichloroethene 20 20 1 101 70-130 12/2112018 2124 1,2-Dichloropropane 20 18 1 90 35-165 12/2112018 2124 cis- 1, 3-Dich loropropene 20 17 1 86 25-175 12/21/2018 2124 trans-1,3-Dichloropropene 20 17 1 85 50-150 12/21/2018 2124 Ethylbenzene 20 20 1 102 60-140 12/2112018 2124 Methylene chloride 20 19 1 93 60-140 12/21/2018 2124 1,1,2,2-Tetrachloroethane 20 21 1 104 60-140 12/21/2018 2124 Tetra chloroethene 20 20 1 102 70-130 12/21/2018 2124 Toluene 20 20 1 101 70-130 12/21/2018 2124 1,2,4-Trcchoorobenzene 20 20 1 102 60-140 12/21/2018 2124 1,1,1-Trichloroethane 20 18 1 90 70-130 12/21/2018 2124 1,1,2-Trichloroethane 20 20 1 101 70-130 12/21/2018 2124 Trichloroethene 20 20 1 101 65-135 12/21/2018 2124 Trichlorofluoromethane 20 18 1 88 50-150 12/21/2018 2124 Vinyl chloride 20 18 1 92 5-195 12/21/2018 2124 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 96 70-130 1,2-Dichloroethane-d4 87 70-130 Toluene-d8 98 70-130 LOQ = Limit of Quantita8on OL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria J = Estimated result < LOG and > DL + = RPD is out of criteria ND = Not detected at or above the LOG Notez,Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 16 of28 Volatile Organic Compounds by GUMS - LCSD Sample ID: T093178-003 Matrix: Aqueous Batch: 93178 Prep Method: 624.1 Analytical Method: 624.1 Spike Amount Result % Rec % RPD Parameter (ug1L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Acrolein 200 180 1 88 3.0 60-140 20 12/22/2018 0540 Acrylonitrile 40 40 1 100 4.5 60-140 20 12/22/2018 0540 Benzene 20 20 1 102 2.0 65-135 20 12/22/2018 0540 Bromodichloromethane 20 18 1 92 0,98 65-135 20 12/22/2018 0540 Bromoform 20 18 1 90 10 70-130 20 12/22/2018 0540 Bromomethane (Methyl bromide) 20 20 1 98 1.8 15-185 20 12/22/2018 0540 Carbon tetrachloride 20 18 1 90 0.91 70-130 20 12/22/2018 0540 Chlorobenzene 20 20 1 99 1.7 65-135 20 12/22/2018 0540 Chloroethane 20 21 1 103 2.3 40-160 20 12/22/2018 0540 2-Chloroethylvinylether 20 19 1 94 0.15 1-225 20 12/22/2018 0540 Chloroform 20 19 1 95 1.5 70-135 20 12/22/2018 0540 Chloromethane (Methyl chloride) 20 18 1 92 2.0 1-205 20 12/22/2018 0540 D ibromochloro methane 20 18 1 90 4.4 53-149 20 12/2212018 0540 1,2-Dichlorobenzene 20 20 1 99 6.5 65-135 20 12/22/2018 0540 1,3-Dichlorobenzene 20 20 1 102 2.7 70-130 20 12/2212018 0540 1,4-Dichlorobenzene 20 19 1 97 9.0 65-135 20 12/22/2018 0540 Dichlorodifluorom ethane 20 17 1 83 6.4 60-140 20 12/22/2018 0540 1,1-1)ichloroethane 20 19 1 93 5.0 70-130 20 12/22/2018 0540 1,2-Dichloroethane 20 18 1 92 1.7 70-130 20 12/22/2018 0540 1,1-Dichloroethene 20 19 1 94 1.5 50-150 20 12/22/2018 0540 cis-1,2-Dichloroethene 20 20 1 101 1.1 70-130 20 12/22/2018 0540 trans-1 ,2-Dichloroethene 20 20 1 98 3.2 70-130 20 12/22/2018 0540 1,2-Dichloropropane 20 18 1 88 3.2 35-165 20 12/22/2018 0540 cis- 1,3-Dichloropropene 20 17 1 83 3.8 25-175 20 12/22/2018 0540 trans- 1, 3- Dichloro pro pene 20 16 1 78 9.3 50-150 20 12/22/2018 0540 Ethylbenzene 20 20 1 100 1.2 60-140 20 12/22/2018 0540 Methylene chloride 20 18 1 92 1.0 60-140 20 12/22/2018 0540 1,1,2,2-Tetrachloroethane 20 20 1 99 4.8 60-140 20 12/22/2048 0540 Tetrachloroethene 20 20 1 98 4.5 70-130 20 12/22/2018 0540 Toluene 20 20 1 101 0.60 70-130 20 12/22J2018 0540. 1,2,4-Trichlorobenzene 20 19 1 94 8.8 60-140 20 12/22/2018 0540 1,1,1-Trichloroethane 20 18 1 90 0.87 70-130 20 12/22/2018 0540 1,1,2-Trichloroethane 20 20 1 100 0.73 70-130 20 12/22/2018 0540 Trichloroethene 20 20 1 101 0.74 65-135 20 12/22/2018 0540 Trichlorofluoromethane 20 17 1 86 2.6 50-150 20 12/22/2018 0540 Vinyl chloride 20 19 1 94 2.3 5-195 20 12/22/2018 0540 Acceptance Surrogate 0 % Rec Limit Bromofluorobenzene 99 70-130 1,2-Dichloroethane-d4 90 70-130 Toluene-d8 98 70-130 LOG - Limit of Guantitaton P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOG and � DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the LOG Note%Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 17 of 28 Semivolatile Organic Compounds by GC/MS - MB Sample ID: T093463-001 Batch: 93463 Analytical Method: 625.1 Matrix: Aqueous Prep Method: 625.1 Prep Date: 12/27/2018 1734 Parameter Result Q Dil LOQ Units Analysis Date Acenaphthene ND 1 1.6 ug1L 01/0312019 1132 Acenaphthylene ND 1 1.6 uglL 01/03/2019 1132 Anthracene ND 1 1.6 ug1L 01/03/2019 1132 Benzidine NO 1 8.0 ug/L 01/03/2019 1132 Benzo(a)anthracene NO 1 1.6 ug/L 01/03/2019 1132 Benzo(a)pyrene ND 1 1.6 ug/L 01/03/2019 1132 Benzo(b)fluoranthene NO 1 1.6 ug1L 01/03/2019 1132 Benzo(g,h,i)perylene NO 1 1.6 ug1L 01/03/2019 1132 Benzo(k)fluoranlhene NO 1 1.6 uglL 01/03/2019 1132 4-Bromophenyl phenyl ether NO 1 1.6 ug1L 01/03/2019 1132 Butyl benzyl phthalate ND 1 1.6 ug1L 01/03/2019 1132 bis (2-Chloro-l-methylethyl) ether NO 1 1.6 ug/L 01/03/2019 1132 4-Chloro-3-methyl phenol NO 1 1.6 ug/L 01/03/2019 1132 bis(2-Chloroethoxy)methane NO 1 1.6 ug/L 01103/20191132 bis(2-Chloroethyl)ether NO 1 1.6 uglL 01/03/2019 1132 2-Chloronaphthalene NO 1 1.6 ug/L 01/03/2019 1132 2-Chlorophenol ND 1 1.6 ug/L 01/03/2019 1132 4-Chlorophenyl phenyl ether ND 1 1.6 ug/L 01/03/2019 1132 Chrysene ND 1 1.6 ug/L 01/03/2019 1132 Dibenzo(a,h)anthracene NO 1 1.6 ug/L 01/03/2019 1132 1,2-Dichlorobenzene NO 1 1.6 ug/L 01/03/2019 1132 1,3-Dichlorobenzene NO 1 1.6 ug/L 01/03/2019 1132 1,4-Dichlorobenzene ND 1 1.6 ug/L 01/03/2019 1132 3,3'- Dich lorobenzid ine ND 1 8.0 ug/L 01/03/2019 1132 2,4-Dichlorophenoi NO 1 1.6 ug/L 01/03/2019 1132 Diethyiphthalate ND 1 1.6 ug/L 01/03/2019 1132 Dimethyl phthalate ND 1 1.6 ug/L 01/03/2019 1132 2,4-Dimethylphenol NO 1 1.6 ug/L 01/03/2019 1132 Di-n-butyl phthalate NO 1 1.6 ug/L 01/03/2019 1132 4,6-Dinitro-2-methyl phenol NO 1 8.0 ug/L 01103120191132 2,4-Dinitrophenol ND 1 8.0 u1 01/03/2019 1132 2,4-Dinitrotoluene ND 1 3.2 ug/L 01/03/2019 1132 25-Dinitrotoluene ND 1 3.2 ug1L 01/03/2019 1132 Di-n-octylphthalate ND 1 1.6 ug/L 01/03/2019 1132 1,2-Diphenylhydrazine(as azobenzene) NO 1 1.6 ug/L 01/03/2019 1132 bis(2-Ethylhexyl)phthaiate ND 1 8.0 ug/L 01/03/2019 1132 Fluoranthene ND 1 1.6 ug/L 01/03/2019 1132 Fluorene ND 1 1.6 ug/L 01/03/2019 1132 Hexach lo robe nzene NO 1 1.6 ug/L 01/03/2019 l 132 Hexachlorobutadiene NO 1 1.6 ug/L 01/03/2019 1132 Hexachlorocyclopentadiene ND 1 8.0 uglL 01/03120191132 Hexachloroethane NO 1 1.6 ug/L 01/03/2019 1132 Indeno(1,2,3-c,d)pyrene NO 1 1.6 ug/L 01/03/2019 1132 Isophorone ND 1 1.6 ug/L 01/03/2019 1132 L00 = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40% N = Recovery is out of cnteria J = Estimated result < LOQ and > DL = RPD is out of criteria No = Not detected at or above the LOO Note: -Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 18 of 28 Semivolatile Organic Compounds by GC/MS - MB Sample ID: TQ93463-001 Matrix: Aqueous Batch: 93463 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 12/27/2018 1734 Parameter Result Q Dil LOQ Units Analysis Date Naphthalene ND 1 1.6 ug/L 01/03/2019 1132 Nitrobenzene ND 1 1.6 uglL 01/03/2019 1132 2-N itropheno l ND 1 3.2 uglL 01 /03/2019 1132 4-Nilrophenol ND 1 8.0 uglL 0110W2019 1132 N-Nitrosodimethylamine ND 1 1.6 uglL 01/0312019 1132 N-Nitrosodi-n-propyiamine ND 1 1.6 uglL 01103120191132 N-Nitrosodiphenylamine (Diphenylamine) ND 1 1.6 ug/L 01/03/2019 1132 Pentachlorophenol ND 1 8.0 uglL 01/03/2019 1132 Phenanthrene ND 1 1.6 uglL 01/03/2019 1132 Phenol ND 1 1.6 uglL 01/03/2019 1132 Pyrene ND 1 1.6 ug1L 01 /03/2019 1132 1,2,4-Trichlorobenzene ND 1 1.6 ug1L 01/03/2019 1132 2,4,6-Trichlorophenol ND 1 1.6 ug1L 01/03/2019 1132 Acceptance Surrogate Q % Rec Limit 2-Fluorobiphenyl 41 37-129 2-Fluorophenol 35 24-127 Nitrobenzene-d5 55 38-127 Phenol-d5 40 28-128 Te rphenyl-d 14 80 10-148 2,4,6-Tribromophenol N 38 41-144 LOO = Limit of Quantilation P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and y OL + = RPD is out of critena LOD = Limit of Detection NO = Not detected at or above the LOQ Note: -Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 19 of 28 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: T093463-002 Matrix: Aqueous Batch:93463 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 12/27/2018 1734 Spike Amount Result % Rec Parameter (uglL) (u91L) Q Dil % Rec Limit Analysis Date Acenaphthene 20 13 1 65 47-145 01/0312019 1329 Acenaphthylene 20 12 1 60 33-145 01/0312019 1329 Anthracene 20 17 1 86 27-133 01/0312019 1329 Benzidine 100 49 1 49 1-150 01/0312019 1329 Benzo(a)anthracene 20 19 1 93 33-143 01/03120191329 Senzo(a)pyrene 20 17 1 83 17-163 01103120191329 Benzo(b)fluoranthene 20 19 1 96 24-159 01103120191329 Benzo(g,h,i)perylene 20 20 1 98 1-219 01/0312019 1329 Benzo(k)fluoranthene 20 20 1 99 11-162 01/0312019 1329 4-Bromophenyl phenyl ether 20 16 1 80 53-127 01/0312019 1329 Butyl benzyl phthalate 20 21 1 106 1-152 01/0312019 1329 bis (2-Chloro-1-methylethyl) ether 20 16 1 79 36-166 01/0312019 1329 4-C h loro-3-m ethyl phenol 20 15 1 76 22-147 0110312019 1329 bis(2-Chloroethoxy)methane 20 13 1 65 33-184 01/0312019 1329 bis(2-Chloroelhyl)ether 20 19 1 94 12-158 01/0312019 1329 2-Chloronaphthalene 20 11 N 1 57 60-120 01/0312019 1329 2-Chiarophenol 20 13 1 63 23-134 01/0312019 1329 4-Chlorophenyl phenyl ether 20 13 1 67 25-158 01/03/2019 1329 Chrysene 20 19 1 95 17-168 01/0312019 1329 Dibenzo(a,h)anthracene 20 19 1 97 1-227 01/0312019 1329 1,2-Dichlorobenzene 20 12 1 58 32-129 01/0312019 1329 1,3-Dichlorobenzene 20 11 1 57 1-172 01103120191329 1,4-Dichlorobenzene 20 11 1 56 20-124 01/0312019 1329 3,3'-Dichlorobenzidine 20 17 1 84 1-262 01/0312019 1329 2,4-Dichlorophenol 20 14 1 68 39-135 01/0312019 1329 Diethyl phthalate 20 17 1 87 1-120 01/0312019 1329 Dimethyl phthalate 20 17 1 85 1-120 01/0312019 1329 2,4-Dimethylphenol 20 11 1 56 32-120 01/0312019 1329 Di-n-butyl phthalate 20 21 1 104 1-120 01/0312019 1329 4,6-Dinitro-2-methylphenoi 20 18 1 90 1-181 01103120191329 2,4-Dinitrophenol 40 24 1 59 1-191 01103120191329 2,4-Dinitrotoluene 20 18 1 89 39-139 01103120191329 2,6-Dinitrotoluene 20 16 1 79 50-158 01/0312019 1329 Di-n-octylphthalate 20 17 1 87 4-146 01103120191329 1,2-Diphenylhydrazine(as azobenzene) 20 21 1 103 1-150 01/0312019 1329 bis(2-Ethylhexyl)phthalate 20 22 1 108 8-158 01103120191329 Fiuoranthene 20 19 1 94 26-137 01/0312019 1329 Fluorene 20 14 1 71 59-121 01/0312019 1329 Hexachlorobenzene 20 18 1 88 1-152 0110120191329 Hexachlorobutadiene 20 11 1 55 24-120 01103120191329 Hexachlorocyclopentadiene 100 32 1 32 1-150 01103120191329 Hexachloroethane 20 13 1 63 40-120 01103120191329 Indeno(1,2,3-c,d)pyrene 20 19 1 97 1.171 01/03/2019 1329 Isophorone 20 16 1 80 21-196 01/0312019 1329 LOO = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 4D% N = Recovery is out of criteria J = Estimated result < LOQ and i OL + = RPD is out of criteria ND = Not detected at or above the LOQ Note: -Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 20 of 28 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: TQ93463-002 Matrix: Aqueous Batch:93463 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 12/27/2018 1734 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Naphthalene 20 14 1 68 21-133 01/03/20191329 Nitrobenzene 20 15 1 74 35-180 01/03/20191329 2-Nitrophenol 20 14 1 69 29-182 01/03/20191329 4-Nitrophenol 40 33 1 84 1-132 01/03/20191329 N-Nitrosodimethylamine 20 15 1 74 1-150 01/03120191329 N-N'itrosod'i-n-propylamine 20 18 1 89 1-230 01/03120191329 N-Nitrosodiphenylamine (Diphenylamine) 20 17 1 83 1-150 01/03/2019 1329 Pentachlorophenol 40 40 1 101 14-176 01103/20191329 Phenanthrene 20 17 1 86 54-120 01103/20191329 Phenol 20 13 1 64 5-120 01/03/20191329 Pyrene 20 19 1 97 52-120 01/03/20191329 1,2,4-Trichlorobenzene 20 12 1 60 44-142 01103/20191329 2,4,6-Trichlorophenol 20 14 1 68 37-144 01103120191329 Acceptance Surrogate Q % Rec Limit 2-Fluorobiphenyi 60 37-129 2-Fluorophenol 44 24-127 Nitrobenzene-d5 80 38-127 Phenol-d5 66 28-128 Terphenyl-d14 107 10-146 2,4,6-Tribromophenol 76 41-144 LOO = Limit of QuantiWon P - The RPD between two GC columns exceeds 40% N = Recovery is out of criteria DL = Detection Limit J - Estimated result - LOO and > DL = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the LOQ Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, tnc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791.9111 www,shealylab.com Page 21 of 28 Organochlorine Pesticides and PCBs - MB Sample ID: TQ93455-001 Matrix: Aqueous Batch: 93455 Prep Method: 608.3 Cleanup: 3655A Analytical Method: 608.3 Prep Date: 12/27/2018 1405 Parameter Result Q Dil LOCI Units Analysis Date Aldrin ND 1 0.040 ug/L 01/04/2019 0514 Aroclor 1016 ND 1 0.40 ug/L 01/02/2019 0000 Aroclor 1221 ND 1 0.40 ug/L 01/02/2019 0000 Aroclor 1232 ND 1 0.40 ug/L 01/02/2019 0000 Aroclor 1242 ND 1 0.40 ug1L 01/02/2019 0000 Aroclor 1248 ND 1 0.40 ug/L 01/02/2019 0000 Aroclor 1254 ND 1 0.40 ug/L 01/02/2019 0000 Aroclor 1260 ND 1 0A0 ug/L 01/02/2019 0000 gamma-BHC (Lindane) ND 1 0,040 ug/L 01/04/2019 0514 alpha-BHC ND 1 0,040 ug/L 01/04/2019 0514 beta-BHC ND 1 0.040 ug/L 01/04/2019 0514 delta-BHC ND 1 0.040 ug/L 01/04/2019 0514 Chlordane ND 1 0.40 ug/L 01/04/2019 0514 4,4'-DDD ND 1 0.040 ug1L 01/04/2019 0514 4,4'-DDE ND 1 0.040 ug1L 01/04/2019 0514 4,4'-DDT ND 1 0.040 ug/L 01/04/2019 0514 Dieldrin ND 1 0.040 ug/L 01/04/2019 0514 Endosulfan I ND 1 0.040 ug/L 01/04/2019 0514 Endosulfan II ND 1 0,040 ug/L 01/04/2019 0514 Endosulfan sulfate ND 1 0.040 ug1L 01/04/2019 0514 Endrin ND 1 0.040 ug/L 01/0412019 0514 Endrin aldehyde NO 1 0.040 ug/L 01/04/2019 0514 Heptachlor ND 1 0.040 ug1L 01/04/2019 0514 Heptachlor epoxide NO 1 0.040 ug1L 01/04/2019 0514 Toxaphene ND 1 0.40 ug/L 01/04/2019 0514 Acceptance Surrogate 0 % Rec Limit Decachlorobiphenyl 64 20-131 Tetrachloro-m-xylene 52 30-132 LOG = Limit of ouantitation P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria DL = Detection Limit J = Estimated result � LOO and n DL = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the LOG Note: -Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive west Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheatylab.com Page 22 of 28 Organochlorine Pesticides and PCBs - LCS Sample ID: T093455-002 Matrix: Aqueous Batch: 93455 Prep Method: 608.3 Cleanup: 3665A Analytical Method: 608.3 Prep Date: 1212712018 1405 Spike Amount Result % Rae Parameter (ug1L) (u91L) Q Dil %Rec Limit Analysis Date Aldrin 0,80 0,59 1 74 54-130 01104/2019 0529 gamma-BHC (Lindane) 0,80 0.63 1 79 43-130 01/04/2019 0529 alpha-BHC 0,80 0.59 1 74 49-130 01/04/2019 0529 beta-BHC 0,80 0.57 1 72 39-130 01/04/2019 0529 delta-BHC 0,80 0.64 1 81 51-130 01/04/2019 0529 4,4'-DDD 0,80 0.65 1 82 48-130 01/0412019 0529 4,4'-DDE 0,80 0.63 1 79 54-130 01/04/2019 0529 4,4'-DDT 0.80 0.72 1 90 58-130 01/04/2019 0529 Dieldrin 0.80 0.68 1 85 36-146 01/04/2019 0529 Endosulfan 1 0.80 0.63 1 78 57-141 01/04/2019 0529 Endosulfan 11 0.80 0.60 1 74 22-171 01/04/2019 0529 Endosulfan sulfate 0.80 0.60 1 75 38-132 01/04/2019 0529 Endrin 0.80 0,66 1 83 51-130 01/04/2019 0529 Endrin aldehyde 0.80 0.63 1 78 60-140 01/04/2019 0529 Heptachlor 0.80 0.59 1 74 43-130 01/04/2019 0529 Heptachlor epoxide 0.80 0,64 1 80 57-132 01/04/2019 0529 Acceptance Surrogate Q % Rec Limit Decachlorobiphenyl 66 20-131 Tetrachloro-m-xylene 60 •30-132 LOO = Limit of Quantitation P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria DL = Detecton Limit J = Estimated result < LOO and a DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the LOQ Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 23 of 28 ICP-MS - MB Sample ID: TQ93289-001 Matrix: Aqueous Batch:93289 Prep Method: 200.2 Analytical Method: 200.8 Prep Date: 12/26/2018 1123 Parameter Result Q Dil LOQ Units Analysis Date Copper NO 1 10 uglL 01/03/2019 0808 Lead NO 1 2.0 uglL 01/03/2019 0808 Zinc NO 1 10 uglL 01/03/2019 0808 LOD = Limit of Ouantitaton OL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOG and > DL + = RPD Is out of crito6a ND = Not detected at or above the LOG Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheaiytab.com Page 24 of 28 ICP-MS - LCS Sample ED: T093289-002 Matrix: Aqueous Batch: 93289 Prep Method: 200.2 Analytical Method: 200.8 Prep Date: 12/26/2018 1123 Spike Amount Result % Rec Parameter ^Copper (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 100 96 1 96 85-115 01/03/2019 0813 Lead 100 100 1 100 85-115 01/0312019 0813 Zinc 100 96 1 96 85-115 01/0312019 0813 LOq = Limit of Qua ntitaton DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria J = Estimated result , LOO and - DL * = RPD is out of criteria ND = Not detected at or above the LOD Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791.9111 www.shealylab.com Page 25 of 28 Chain of Custody and Miscellaneous Documents Shealy Environmental Services. Inc. 106 Vantage Point Drive west Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shcaiylab.com Page 26 of 28 �CD � v m � SHEALY ENVIRONMEWAL SERVICES, INC. o = ,�i3E�iLY Chain o1 Custody R9172 eeord A ,a;e r�o �lao i-a1 97oa� Fax�lvc. aai 7sumbia. SC ?911z T� 02 vmvr.sheaMab.com m m RepartraCan6r.Y T. rr�vrtr rYn. lF.mair C) 3 � ..is (ALgrsh 8� J narc �Yi:I� N ems' 1 1 Alsyru PsorAManaS �r 4a l4ArScr w* r DRrO %A sfA s ►•' jmi�ISfiT31J►BFiD�l6t�jl�flL�•rG9D7�J�13'JM�TP�l! � � K �� � � j� � � � `� t DtO 0 I ! i N O v W I I O r m ro i N a knot/ Mo by 3 fi�4S�rthOe by -5. fWCMZMW bV >(Ptbrta&aaars�rrroetadlhrra�odlydlxr. &errapretxep�ar J lush (*MOY) D Rehvn tc C5? at O DisprBr by C Rol -Hap% 0 Pa wb4 = SIB IrrM j Dare ►krs r. b Ore T" P FM 2. 0 J.i!f YY• ram/ yY A 1�jlltiTi� I !Dare :Tw.e 4. taba'e try6 I 2. 5 : All samplafare mialm d for four vmaks (ram nwalpr OAB LA ON1 v urleu^s other arransrernerrta are MSCa P-,vnvd on t r =w. Yes w r. Path DISTRWUMIN. 'AWME s rkLUV,rrerjn w MbaraArp P^ -Q&=Wek PW9,FeidtYlenr U,;,y Number 6 7 4 4 6 OmM No. PW—Lly—i TL21101 trp IF r CC RewA pmen!q (Spedryl Urn A till XOP AM - 'zl'!r—a-5 zswx ramo.�L� 'z: v,r„umanr rm:.noer: � nD• ass Eta nwr.C1BdJ 28rt cn 2 n Z C z ic Z r M C 0 M Z 0 SHEALY ENVIRONMENTAL SERVICES, INC. SbivrYb�wuVol :nner.dlS"-Vto-.roe. tit tul I i :.nneMNtfmncr.MF•'dlnlRf'•tA hM;:Li%vVUW:P :1:]a Sample Receipt Checklist (SR `) Client: - —Aj2 wi Cnnler Inspected hVidate: LKA 1 17..171 ]-or*: 7'L- Z Dt3 Mcans infrercipt %HNI ❑ C'liont 0 irYti Fcdlix Other. Yesl 0 No 1, Wae custody seals went On the cooler? Yesl D Nol 0 NA 2. If custody seals were Present. were they intact and unb ken? H Strip ID: j&jZ7 S Cldorine Strip ID: riginal teipperatura upon receipt! Derived (Carrected) ternperauna upon receipl: Lhu:'LohodTcmpc'rut Blank ❑APdris't Buldcs IR Cwn ID:Iit Vu d of coolmrt: Wet Ice L Ice Packs Lj M fee Ll Nolte Tested by:- id Snap -Cup ID: Cartuclian F'ecwr. "C (] Yes ❑ No ` 1+A 3" If remptxature of any cooler eatoeeded ti"0°C, was Praj pM was Notified by: phone! email ! face-to-face (circl t Manager Notified? one)" U Yes El No 1 ° I+A a. is the omnrnercial caurler's zki", Slip atrached to 1hi farm? Ycs ❑ No 5. Vl•c= propercmikaly pnxxxiurt:s frelinyuishcd-rcxriv ) followed'? YC5 U No G. Were sample IDs Iisted on the WC? Yesi ❑ Nu 7, Wert sample IUe listed rnt all sample containers? ? Yes ❑ Na 5. Was collection date & time listed on the COC7 Yrzj ❑ No 9. WuN wllut:lit►n date & time listrrl on all .ample otmtlti crs? Yes D No 10. Did all containcr label information (ID, da-.c, time) aV ae with the CiiC? Y"cz ❑ No I I- Were tests oo be performed listed on the COG? � � ❑ Vn 12. Did all urnples arrive in the proper con ainers foreach (unbrokcn, lids on. ctc•Xl — test and..+rtr in good condition Yes L" i No 13. Was adequate sample volume available? Yoe$ ❑ No 14. Were all samples received within ti the hniding time r atl hours, whichever comes tirsCl '' Yra yo 15. Were any samples containers missktWvAt s, (cir0c tv c) sumplcs Not listed on C.` 0 ' �_ Yes ❑ No /V 16. For VOA and RSK-175 sarnp4a, were bubbles prese any of the VOA vials? >'pea -size' (:'+v'orGmm in diameter) in Ye..1 Nn L J NA 17. Wm, all DROfinetaWnutrient samples received at a pl I nf <2? Yes =0 JZNA 18. Wcrc all cynni:dc samp3os received at a pH = 12 and st Ifid; srunples rcec4ed ul u pH:- 9? }��-� u va �" 1�fA 19' Were a applicable N11j� KK.cyam r�phennlafi25 (< chlorine'? ,5mg L) samples free o rest >a ❑ Yes ❑ No ry(NA f0] 20. Wete cllew reinwkVmquests (l.c, nxlueswd dilutions, correctly truttscribed frarn life COC intu Ilre wmmtatt sx VNISD designations, etc... on in LIh4S.' Yes 7-1 No 21. Wlms the Suotc number ligtczl on the container• label? If yes, t7u0re ample PrLnwrva Lion (h,7u,Y W vumplutod fur tiny samplc(s) incorrectly preserved 3r with headspace-) Sample(s) were received Ineormectly p in sample receiving with all- of Circle C4iv: H2504, HNO3, HCI, NaOH tisirq ir,ne of preservation 11"root= dtall unr prrscrvt lit a is r►trtlrtl, plt ate tt crvad and tvere aldjumed acwttlingly SR ,4 _ . c in tine comments below" ttmplu(s) _ _ were receive I with bubbles '�G mm in diameter. amples(s) _ _ wcrc mccivcd with TRC % djuslcd ucuordingly in stunplc rccritring with sodium dtiosulfate (Na_S�0.1) tuith Sh 4.5 mg�l" (ir419 i! "e) ar,d were ly in: 5R batalade labels applied by. d_ I I,+ Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 28 of 28 1 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date Submitted: August 6, 2018 CERTIFICATE OF COVERAGE NO. NCG030281 FACILITY NAME Tipper Tie, Inc. COUNTY Wake PERSON COLLECTING SAMPLES LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' July i _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flaw ❑Water Supply ®SA ❑Other RECEIVED, PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 AUG 0 9 2018 CENTRAL F,1 FILLS \w ® No discharge this period?z 11 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics' Benchmarks 100 mg/L or 50 mg/LQ 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg1L 1 mg/L ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 It, Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." &12e1-71 T 7Joca oi S N2mee (Print name) Title {Print title) 01 S- 6-18 (Signature) (Date) Note: Results must be reported in numerical format. Do not_repor_t Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported_ in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' .Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See Genera! Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this QMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) Permit Date: 11/1/2012-10/31/2017 8-6-/S (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 -- \ q V, Semi-annual Stormwater Discharge Monitoring Report For North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 01/31/18__ CERTIFICATE OF COVERAGE NO. NCG030251 FACILITY NAME Watts - Spindale COUNTY Rutherford PERSON COLLECTING SAMPLES Mark Kennard LABORATORY Lab Cert. # _ Comments on sample collection or analysis: No flow observed at the outfall Part A: Stormwater Benchmarks and Monitoring Results 5 M K COLLECTION YEAR 2017 REC��5 MPLE PERIOD ❑ Jan -June ®July -Dec FEB NIB or ❑Monthly-' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA CENTRAL FILES ❑Zero -flow ❑Water Supply ❑SA DWR SECTION ®Other c PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ® No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks ===> - - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 2-no discharge 12/05/18 _ 0.25 N/A N/A N/A N/A N/A N/A N/A -' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, lnches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AAND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 dot's of receipt of the lob results (or of end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are sigpif penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of IL)1� (D te) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual „Stormwater Discharge Monitoring Report For North Carolina Division of Water Quality General Permit No. NCG030000 CERTIFICATE OF COVERAGE NO. NCG030251 FACILITY NAME Mueller Steam Specialty COUNTY Robeson PERSON COLLECTING SAMPLES Date submitted 07/27117 SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ® Jan -June ❑July -Dec or ❑Monthly'.__ (month) / DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY TBL Lab Cert. # REUV Y Vi ❑Zero -flow ❑Water Supply ❑SA Comments on sample collection or analysis: No flow observed at ®Other Class C, SW outfalls #1 or #2 ��� � g 20i7 CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 OWR SECTION Part A: Stormwater Benchmarks and Monitoring Results ® No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks =__> - _ 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 "Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PqL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period: Outfall No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier .1, Tier 1, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge"' reports, within 30 days of receipt of the lab results or at end of monitoring eriod in the case of "No Discharge" reports) to: Division of Water Quality _ Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware that there are s' nificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ']1,-)1, (Signature of PerrNitte)e) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-anniez9 Stormwater Discharge Monitoring Report For North Carolina Division of Water Quality General Permit No. NCG030000 CERTIFICATE OF COVERAGE NO. NCG0302.51 FACILITY NAME Watts - Spindale COUNTY Rutherford PERSON COLLECTING SAMPLES Mark Kennard LABORATORY Lab Cert. # _ Date submitted 07127117 Comments on sample collection or analysis: No flow observed at the outfall Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ® Jan -June ❑July -Dec or ❑Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA RECen V Er) ❑Zero -flow ❑Water Supply ❑SA 15�Other c AUG 08 2017 t CENTRAL FILES DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ® No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/Tota1 Total Petroleum Hydrocarbons Toxic Organics Benchmarks =__> - - 100 mg/L or 50 mg/L' 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 2-no discharge 06/05/17 0.55 N/A N/A N/A N/A N/A N/A N/A 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 4 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfall No. Hate Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 1S mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 r * See Gener5l Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are ificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." >9 04L � � --�,n I I I (Signature of r 'ttee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report For North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 01/27/17 CERTIFICATE OF COVERAGE NO. NCG030251 FACILITY NAME Watts _Spindale COUNTY Rutherford PERSON COLLECTING SAMPLES Mark Kennard LABORATORY Lab Cert. # T Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD ❑ Jan -June ® July -Dec RECEIVED or ❑Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ����j ❑Zero -flow ❑Water Supply ❑SA CENTRAL FILES ®Other c _DWR OSECTION F#L E PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 U0r__--%V P Z No discharge this per,ad?2 Outfall No. Date Sample Collected` (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks - - 100 mg/L or 50 mg/L° 6.0 — 9.0 0,007 mg/L ' 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 12/29/16 0.29 N/A N/A N/A N/A N/A N/A N/A 2 12/29/16 0.29 N/A N/A N/A N/A N/A N/A N/A 3 12/29/16 0.29 N/A N/A N/A N/A N/A N/A N/A 4 12/29/16 0.29 N/A N/A N/A N/A N/A N/A N/A 5 12/29/16 0.29 N/A N/A N/A N/A N/A N/A N/A 6 12/29/16 0.29 N/A N/A N/A N/A N/A N/A N/A 7 12/29/16 0.29 N/A N/A N/A N/A N/A N/A N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition ar, found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or SO mg/L* 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART Ii SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART It SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original -and one copy of this DMR, including_ all "No Discharge" reports,_ within 30 days of receipt of the lab results for at end of monitoring_period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or . those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware that there are Og<fcant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." [Signature of (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 IIIWAEM A Watts Water Technologies Company February 16, 2016 815 Chestnut Street • North Andover, MA • 01845-6098 • Tel. (978)688-1811 •Fax: (978) 794.1846 BY CERTIFIED MAIL — RETURN RECEIPT REQUESTED Central Records Division of Energy, Mineral and Land Resources 1617 Mail Service Center Raleigh, NC 27699-1617 F?ECEI VED FEB 2 3 2016 CSIq7'R,4L FILES DWR SECTION Re: Dischart!e Monitoring Report and Notice of Comoliance Status Watts Regulator, 100 Watts Roa orth Carolina Certificate of Coverage Numbei NC603025 To Whom It May Concern: In accordance with certificate of coverage referenced above and requirements of general permit number NCG030000 ("General Permit"), please find enclosed discharge monitoring report ("DMR") for monitoring year 4, period 1, monthly monitoring (January 2016) regarding Watts Regulator ("Watts") facility at 100 Watts Road in Spindale, North Carolina ("Facility"). Consistent with the February 3, 2010 Approval of Representative Outfall Status, Watts obtained quantitative data for samples from outfalls 001, 002, 004 and 006.` Based on the enclosed results reflected in the January 2016 DMR, these outfalls remain in Tier III status. In addition to the required outfall sampling, Watts obtained samples for PH from outfalls 003, 005 and 007. Those data are also reflected on the enclosed DMR.z Upon receiving July 2015 sampling results, Watts engaged environmental consulting firm of Hart & Hickman ("H&H") to develop additional best management practices ("BMP") for the Facility. Given that all four of the monitored outfalls are in Tier III status, monthly monitoring data continues to be used to evaluate the effectiveness of these additional BMPs and the need for further improvements. Additional activities continued during the sampling period, and though the outfalls remain in Tier III status, analytical sampling shows overall continued improvement. As mentioned in previous correspondence, a meeting was requested with representatives of the Division of Energy, Mineral and Land Resources (DEMLR) to discuss results of a storm water compliance audit performed and Watts' efforts to implement additional BMPs at the Facility. On January 27, 2016, we were pleased to host Darlene Kucken from DEMLR Asheville Regional Office who reviewed the site stormwater program and toured the Facility. As part of the discussion, we reviewed data contained in documentation from H&H that was attached to recently submitted DMR reports, which included results of background sampling during the months of October and November 2015. In short, the data indicate that copper and zinc present in the Facility's storm water discharge likely originates from "non -industrial" sources — either the Facility's roof (which is not exposed to industrial operations) and the roadway adjacent to the Watts Regulator Company Since 1874 watts.com ,., Facility's storm water outfalls. The results also suggest that the Facility's additional BMPs will resolve previous exceedences of the lead benchmark. A follow-up letter dated February 3, 2016, was received from Darlene Kucken indicating the Facility is being relieved of Tier III monitoring requirements and is no longer required to perform monthly sampling of storm water outfalls. Accordingly, Watts will resume semi-annual sampling of storm water outfalls and submit the next DMR following conclusion of the January to June 2016 monitoring period. Letter from Ms. Kucken also requested Watts continue investigative sampling of roof drains, road runoff, and actual precipitation for three to four additional storm water sampling periods. Watts plans to obtain these samples on a monthly basis and submit them directly to Ms. Kucken. Finally, letter from Ms. Kucken asked that Watts provide documentation of how often the roof at the Facility will be whitened and research the potential for roof whiteners to contribute zinc to the Facility's storm water. Watts will work with H&H to evaluate existing literature on this issue. If research determines that roof whitening agents may be contributing zinc to storm water discharged from the Facility, Watts will investigate whether there are practicable steps that can be implemented to reduce that contribution and propose appropriate revisions to our storm water pollution prevention plan. Watts will provide Ms. Kucken with the results of this effort when the next DMR is submitted. In addition, at that time, Watts will plan to discuss possibility of making outfall 002 as the Facility's sole representative outfall for monitoring. Please contact me at (978) 689-6070 at your convenience if you have any questions. Sincerely, Howard H. Chu Director, Environment, Health and Safety Watts Water Technologies, Inc. Enclosures cc: Central Records, Division of Water Quality aceAnalytical www.paoolabs wn January 20, 2016 Mark Kennard Watts Water Technologies 815 Pickens Street Chesnee, SC 29323 RE: Project: Stormwater - January Pace Project No.: 92282687 Dear. Mark Kennard: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Enclosed are the analytical results for sample(s) received by the laboratory on January 12, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures PCpi lge0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 aceAnalytica! Huntersville, NC 28078 www.pacelahs.00m (704)875-9092 e CERTIFICATIONS Project: Stormwater - January Pace Project No.: 92282687 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia[VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 14 aceAnalytical www.pacelaba.wm ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater - January Pace Project No.: 92282687 Sample: OU- 001 Lab ID: 92282687001 Collected: 01/08/16 09:55 Received: 01/12/16 14:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 01/20/16 07:14 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 53.6 ug/L 5.0 1 0111311617:30 01114/1616:29 7440-50-8 Lead ND uglL 5.0 1 0111311617:30 01114/1616:29 7439-92-1 Zinc 36.0 ug/L 10,0 1 01/1311617:30 0111411616:29 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 5.2 1 01/13/16 09:35 REPORT OF LABORATORY ANALYSIS This report shall not t>e reproduced, except in full, Date: 01/20/2016 04:39 PM without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 aceAnalytical® www.pacelatrsam ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater - January Pace Project No.: 92282687 Sample: OU- 002 Lab ID: 92282687002 Collected: 01/08/16 10:10 Received: 01/12/16 14:30 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mg/L 5.0 1 01/20/16 07:14 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 24.8 ugIL 5.0 1 01/1311617:30 0111411616:32 7440-50-8 Lead 7.2 uglL 5.0 1 0111311617:30 01/1411616:32 7439-92-1 Zinc 22.0 ug/L 10.0 1 01/1311617:30 01/14/1616:32 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids NO mg/L 3.1 1 01/13/16 09:36 REPORT OF LABORATORY ANALYSIS This report shall not t)e reproduced, except in full, Date: 01/20/2016 04:39 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 14 aceAnalytical waw.p3cgleb&0w ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater - January Pace Project No.: 92282687 Sample: CU- 004 Lab ID: 92282687003 Collected: 01/08/16 10:15 Received: 01/12/16 14:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 01/20/16 07:15 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 65.5 ug/L 5.0 1 01/13/1617:00 01/14/1619:04 7440-50-8 Lead 5.8 ug/L 5.0 1 01/13/1617:00 01/1411619:04 7439-92-1 Zinc 109 ug/L 10.0 1 01/1311617:00 01/14/1619:04 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 7.2 mg/L 3.3 1 01/13/16 09:37 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/20/2016 04:39 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14 aceAnalytrcal WWW..pac"&Com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater - January Pace Project No.: 92282687 Sample: OU- 006 Lab ID: 92282687004 Collected: 01/08/16 10:22 Received: 01/12/16 14:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 01/20/16 07:15 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 47.2 ug/L 5.0 1 0111311617:00 01/1411619:13 7440-50-8 Lead ND ug/L 5.0 1 01/1311517:00 01/1411619A3 7439-92-1 Zinc 113 ug/L 10.0 1 01/1311617:00 0111411619:13 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 2.5 1 01/13/16 09:37 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 01/20/2016 04:39 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 14 aceAnalytrcal www.pacebbs.twm QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)8759092 Project: Stormwater- January Pace Project No.: 92282687 QC Batch: GCSV123846 Analysis Method: EPA 1664E QC Balch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92282687001, 92282687002, 92282687003, 92282687004 METHOD BLANK: 1650466 Matrix: Water Associated Lab Samples: 92282687001, 92282687002, 92282687003, 92282687004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mglL ND 5.0 01/20/16 07:11 LABORATORY CONTROL SAMPLE: 1650467 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 37.7 94 78-114 MATRIX SPIKE SAMPLE: 1650468 92282919001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL ND 40 38.3 96 78-114 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/20/2016 04:39 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 14 aceAnalytical www.pacelabs com Project: Stormwater - January Pace Project No.: 92282687 QC Batch: MPRP/20464 QC Batch Method: EPA 200.7 Associated Lab Samples: 92282687001. 92282687002 METHOD BLANK: 1646195 Associated Lab Samples: 92282687001, 92282687002 Parameter Units Copper uglL Lead ug/L Zinc uglL QUALITY CONTROL DATA Analysis Method: EPA200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 01/14/1614:53 ND 5.0 01/1411614:53 ND 10.0 01/14/1614:53 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1646196 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug/L 500 495 99 85-115 Lead uglL 500 472 94 85-115 Zinc uglL 500 456 91 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1646197 1646198 MS MSD 92282581001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug1L 21.8 500 500 533 538 102 103 70-130 1 Lead uglL ND 500 500 423 418 84 83 70-130 1 Zinc ug/t_ 3.9J 500 500 418 412 83 82 70-130 1 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1646199 1646200 MS MSD 92282660003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper uglL 357 500 500 860 880 100 104 70-130 2 Lead ug/L 17.5 500 500 457 460 88 89 70-130 1 Zinc uglL 718 500 500 1150 1160 86 88 70-130 1 Results presented on this page are in the units indicated by the -Units- column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/20/2016 04:39 PM without the written consent of Pace Analytical Services, Inc.. Page 8of14 aceAnalytical %,%w.pacelab&=n QUALITY CONTROL DATA Project: Stormwater - January Pace Project No.: 92282687 QC Batch: MPRP/20465 Analysis Method: EPA200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92282687003, 92282687004 METHOD BLANK: 1646201 Associated Lab Samples: 92282687003, 92282687004 Parameter Units Copper ug/L Lead ug/L Zinc ug/L Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 01/1411618:58 ND 5.0 01/1411618:58 ND 10.0 01/14/1618:58 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1646202 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 498 100 85-115 Lead ug/L 500 468 94 85-115 Zinc ug/L 500 452 90 85-115 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1646203 1646204 MS MSD 92282687003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 65.5 500 500 561 576 99 102 70-130 3 Lead ug/L 5.8 500 500 467 475 92 94 70-130 2 Zinc ug/L 109 500 500 549 558 88 90 70-130 2 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1646205 1646206 MS MSD 92282745010 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 29.1 500 500 543 542 103 102 70-130 0 Lead ug/L ND 500 500 405 409 81 82 70-130 1 Zinc ug/L 25.1 500 500 442 451 83 85 70-130 2 Results presented on this page are In the units indicated by the "Units" column except where an attemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/20/2016 04:39 PM without the written consent of Pace Analytical Services, Inc. Page 9 of 14 aceAnalytical www.pacelabs.corn QUALITY CONTROL DATA Project: Stormwater - January Pace Project No.: 92282687 QC Batch: WET142441 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92282687001, 92282687002, 92282687003, 92282687004 METHOD BLANK: 1645853 Matrix: Water Associated Lab Samples: 92282687001, 92282687002, 92282687003, 92282687004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 01/13/16 09:34 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1645854 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 228 91 90-110 SAMPLE DUPLICATE: 1645855 92282687001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1645856 92282592001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/20/2016 04:39 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 14 aceAnalj6cal wwwpacelaftmn QUALIFIERS Project: Stormwater - January Pace Project No.: 92282687 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 S - Surrogate i,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) , MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260, N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyzes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /20/2016 04:39 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14 aceAnalytical "W pacelabs com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater- January Pace Project No.: 92282687 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92282687001 OU- 001 EPA 1664B GCSVl23846 92282687002 OU- 002 EPA 1664B GCSV123846 92282687003 011,11- 004 EPA 1664B GCSV123846 92282687004 OU- 006 EPA 1664B GCSV123846 92282687001 011.11- 001 EPA 200.7 MPRPI20464 EPA 200.7 ICP118464 92282687002 0U- 002 EPA 200.7 MPRP120464 EPA 200.7 ICP118464 92282687003 011,11- 004 EPA 200.7 MPRP120465 EPA 200.7 ICP118465 92282687004 OU- 006 EPA 200.7 MPRP120465 EPA 200.7 1CP118465 92282687001 OU-001 SM 2540D WET142441 92282687002 OU-002 SM 2540D WET142441 92282687003 0U- 004 SM 2540D WET142441 92282687004 OU- 006 SM 2540❑ WET142441 Date: 01/20/2016 04:39 PM REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page12of14 /1 Document Name: Analytical' Sample Condition Upon Recel Document No.: . F-CHR-CS-003-rev.17 Document Revised: 260Cf2 Page 1- of 2 `. Issuing Authority: Pace Huntersvilie Quality Of A Client Name: Project M. i WO :92282687 Liu �-C'r': Te � ►. ,� j� . � � Courier: ❑Fed Ex S ❑LISPS ❑Client � 1111111111111111111M❑Commercial ❑Pace ❑Other: 192282687 Custody Seat on Cooler/Box Present? ❑Yes PNo Seals Intact? ❑Yes ❑No I Packing Material: ❑Bu le Wrap LJ ubble Bags ❑None ❑Other:_ Thermometer 1505 Used: Type of Ice: r Wet ❑Blue []None ❑ amples nn Ice, coolirig'process has begun Cooler Temp Corrected ('C): Blologlcal Tissue Fi:ozen?' _ [:]Yes No ❑N/a rll Temp should be above freezing to 6°C Correction Factor: 0.01C Date and Initials of Person Exam lning.Conterits: 17 USDA Regulated Soil { [] N/A, water sample) Did samples on to in a quarantine zone within the United States: CA, NY, ar SC (check maps)? Did samples originate from a foreign source (internationally, ❑Yes LJ No Including Hawaii and Puerto Rich)? ❑Yes ❑No - If Yes to either questlon, fill out a Regulated Sall Checklist and include with SCUR/COC paperworlt._•' COMMENTS: . Chain of Custody Present? By" No N/A I. Chain of Custody Filled Out? Q es [IN, ❑N A 2. Chain of Custody Relinquished? es ONO N/A 3, Sampler Name and/or Signature on COC? es QN, QN/A 4, Sam pies Arrived within Hold Time?- - - es- • ONO- '❑N/A- 5: - Short Hold Time Analysis (<72 hr)? Yes ©o N/A 6. Rush Turn Around Time Requested? Yes No ❑N/A 7. Sufficient Volume? es - NO ❑N/A 8. Correct Containers Used? Yes ❑No ❑N/A 9. -Pace Containers Used? es No' ❑N/q Containers intact? ' Yes OC4, ❑N/A 10. Filtered Volume Received for Dissolved Tests? QYes No ❑ A 11. Note if sediment is visible In the dissolved container­ Sample Labels Match COC? 13es ❑No [I NIA ,M .7 ... 12. -Includes Date me ID/Anal sls Matrix: All containers needing acid/base preservation have been // 13, checked? ©Yes ❑No ❑N/A All containers needing preservation are found to be in compliance with EPA recommendation? (HNOs, HrSOa, HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide) Yes ❑No ❑N/A Exceptions: VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC,LLHg pYes I]No ❑N/A Samples checked for dechlorizatlon QYes ONO ❑ /A 14. Headspace In VOA Vials (>5.6mm)7 Yes ONO NI 1S. " Trip Blank Present? []Yes ONO N/ , 16. Trip Blank Custody Seals Present? []Yes[]No/A Pace Trip Blank lot# ifpurchased): CLIENT NOTIFICATION/RESOLUTION -;Field Datoegytred?'- ❑Yes • ❑No i Person Contacted: Date/Time: Comments/Resolution: `,;;r,. Project Manager SCURF Review: Dale: 2L P (� Note: Whenever there is a discrepancy affbeting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DE HNR Certification Office (i.e. Out of hold, Incorrect preservative, out of temp, incorrect containers). Page 13 of 14 i� ,` PaceMalylics!' Section A Section B RCRLIled Gtient lnfnrma6— n.11 ;1 Prni I nfn..nal;­ CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All retevant.fields must be completed accurately. ° v Section C N lm Invoice Information: Pa e : 1 >)f 1 M Company: Watts Water Technolonies Report To: Mark Kennard Attention: MAi'L V_e.tie?jA;!D Address: 100Waits Rd Copy To: Companyblarw tjATrL Ijry—,e. ,• -, C3- Spindale, NC 28160 Address: R uato lA en Emma; l q r ¢ , r. to ,,_; 't+•[ Purchase Order #: Pace duple: C ' Phone: • ^ • -' j -Lft - r' jFax Project Name: Stormwatar - N•� Q-iL Pace Project Manager: nicote.gasiorowSki labs,com, - - State I Location Requested Duo Date: 5 r Project 0: Pace Profile #; 7136 tp -AIC ..Re uesled'Anat sis Filtered YIN G t 1 z MATRIX COOT_ COLLECTED z Preservatives }. ` Orin- wa . ow a u O w.ta WT 3 r u w..t. water vw P p° P SAMPLE ID u Od DL One Character per box. v+w� wP tiAct w ,o li START END n = m a jA•Z,0.9I,-j F w. ,w. Sample Ids must be unique T.�,,,° TB % W TDATETIME W, ro O jp �-• iYLLI `w a a, Z 9 w C m e a S DATE TIME d N = z V. z z z p r P ¢ rt,5� z OV -oo i11�5 i •, K X ��+ J 4 C)IJ 00 v! I =5 i _6- I .�+7 - 9 I '10 I ,'1 I `•ADDITIONAL` COGMFftffr r I'- 'RELINOOISHFDBYIAFFILIATION,' DATE 4- r •TIME' l� 7ACCEPTED BYfAFFi[lAT76N` '„DATE- i TIME.r SAMPLE CONDmONS, - }. 31 t>tw $AMPLER NAME AND SI6NA7U_RE .. • , E r m P T amp of SAMPLER' r NA-' A r�1i z o Z m z m z S A7 RE o AMPLER: DATE Signed: 7 o �- q u) c Semi-annual Stormwater Discharge Monitoring Report For North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 02/16/16 CERTIFICATE OF COVERAGE NO. NCG030251 SAMPLE COLLECTION YEAR 2016 FACILITY NAME Watts - Spindale SAMPLE PERIOD ❑ Jan -June ❑ July -Dec COUNTY Rutherford or ® Monthly' January (month) PERSON COLLECTING SAMPLES Mark Kennard DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY Pace Analytical Lab Cert. # 12 5342 37706 ❑Zero -flow [:]WaterSupply []SA Comments on sample collection or analysis: ®Other c Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --> ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks =__> - I - 100 mg/L or 50 mg/L4 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0,067 mg/L 15 mg/L 1 mg/L 1 01/08/16 0.14 <5.2 6.6 0.0536 <0.005 0.0360 <5.0 NA 2 01/08/16 0.14 <3.1 6.8 0.0248 0.0072 0.0220 <5.0 NA 3 01/08/16 0.14 N/A 6.3 N/A N/A N/A N/A NA 4 01/08/16 0.14 7.2 6.6 0.0655 0.0058 0.109 <5.0 NA 5 01/08/16 0.14 N/A 6.6 N/A N/A N/A N/A N/A 6 01/08/16 0.14 <2.5 1 6.6 0.0472 1 <0.005 0.1130 <5.0 NA 7 01/08/16 0.14 N/A 1 6.1 N/A I N/A N/A N/A N/A 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of,the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), i certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX_m L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No dischorge this period?Z Outfall No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B * See General Permit text, Table S, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Stanley Aiken — Regional Engineer at the Ashville Regional Office Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 da s of recei t of the lab results or at end of monitoring eriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there err<gnificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature -�J) S11 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report P For North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 12/29/15 CERTIFICATE OF COVERAGE NO. NCG030251 FACILITY NAME Watts - Spindale COUNTY Rutherford PERSON COLLECTING SAMPLES Mark Kennard LABORATORY Pace Analytical Lab Cert. # 12, 5342, 37706 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' November _ _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ®Other c PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organicss Benchmarks - - 100 mg/L or 50 mg/0 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 11/18/15 0.17 .0225 7.2 0.068 .0092 .0443 <5.0 NA 2 11/18/15 0.17 .0163 7.3 .0403 <0.005 0.0645 <5.0 NA 3 11/18/15 0.17 N/A 6.7 N/A N/A N/A N/A NA 4 11/18/15 0.17 .0308 6.5 0.142 <0.0207 0.220 <5.0 NA 5 11/18/15 0.17 N/A 6.3 N/A N/A N/A N/A N/A 6 11/18/15 0.17 <100mg/L 6.4 0.0674 <0.005 0.196 <5.0 NA 7 11/18/15 0.17 N/A 6.0 N/A N/A N/A N/A N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. G See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be Waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is im plementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. (vote: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part 8 * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART li SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART li SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER ATANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Stanley Aiken — Regional Engineer at the Ashville Regional Office Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date: 11/1/2012-10/31/2017 12 / 29 /15 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 CERTIFICATE OF COVERAGE NO. NCG FACILITY NAME Watts - Spindale COUNTY Rutherford PERSON COLLECTING SAMPLES Mark LABORATORY Pace Analytical Comments on sample collection or an Semi-annual Stormwater Discharge Monitoring Report "c. for North Carolina Division of Water Quality General Permit No. NCG03000000 Date submitted 11/23/15 030251 SAMPLE COLLECTION YEAR 2015 nu-py SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' October Kennard DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA Lab Cert. # 12, 5342, 37706 ®Zero -flow ❑Water Supply [:]SA alysis: ❑Other Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ®No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks ===> - - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 N/A N/A N/A N/A N/A N/A N/A N/A N/A 2 N/A N/A N/A N/A N/A N/A N/A N/A N/A 3 N/A N/A N/A N/A N/A N/A N/A N/A N/A 4 N/A N/A N/A N/A N/A N/A N/A N/A N/A 5 N/A N/A N/A N/A N/A N/A N/A N/A N/A 6 N/A N/A N/A N/A N/A N/A N/A N/A N/A 7 N/A N/A N/A N/A N/A N/A N/A N/A N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mp,/L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 -- 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B * See General Permit text, Table S, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Stanley Aiken — Regional Engineer at the Ashville Regional Office Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware that ther are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1►)70l1, (Signature 4fte nittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report For North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 11/04/15 CERTIFICATE OF COVERAGE NO. N00030251 FACILITY NAME Watts - Spindale COUNTY Rutherford PERSON COLLECTING SAMPLES Mark Kennard LABORATORY Pace Analytical Lab Cert. # 12, 5342, 37706 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 7, SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' September month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow ❑Water Supply ❑SA ®Other c PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 �l ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks =__> - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 09/24/15 3.43 5.0 6.4 0.0974 .0067 .0546 <5.0 NA 2 09/24/15 3.43 3.9 5.6 .0184 0.005 0.045 <5.0 NA 3 09/24/15 3.43 N/A 6.1 N/A N/A N/A N/A NA 4 09/24/15 3.43 <100mg/L 6.0 0.157 <0.005 0.11 <5.0 NA 5 09/24/15 3.43 N/A 6.3 N/A N/A N/A N/A N/A 6 09/24/15 3.43 <100mg/L 6.8 0.0726 <0.005 0.11 <5.0 I NA 7 09/24/15 3.43 N/A 6.1 N/A N/A N/A N/A N/A 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). *See notes in Attachment regarding regional and site pH readings relative to benchmark and monitoring results. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (70), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan," Mr. John Palotta Name (Print name) Vice President of Operations Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier1, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 ' * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Stanley Aiken — Regional Engineer at the Ashville Regional Office Mail an oriainal and one copy of this DMR, includina all "No Discharae" reports. within 30 days of receipt of the lab results for at end of monitorina period in the case of "No Discharge" reports] to: Division of Water Quality " Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date:11/1/2012-10/31/2017 4 Nov 2015 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 aceAnalytical www.pacefabs.wm October 05, 2015 Mark Kennard Watts Water Technologies 815 Pickens Street Chesnee, SC 29323 RE: Project: WATTS SPINDALE SW Pace Project No.: 92269627 Dear Mark Kennard: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 29, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 13 laneMalj6cal" Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacalabs.Wm (� (704 )875-9092 CERTIFICATIONS Project: WATTS SPINDALE SW Pace Project No.: 92269627 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #. 357 North Carolina Wastewater Certification #: 12 VirginiafVELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 13 aceAnalytical wwN:pecedabs.00m ANALYTICAL RESULTS Project: WATTS SPINDALE SW Pace Project No.: 92269627 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OU-001 Lab ID: 92269627001 Collected: 09/24/15 09:55 Received: 09/29/15 12:15 Matrix: Water Parameters Results Units Report Limit DP Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 10/02/15 08:54 200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA200.7 Copper 97.4 ug1L 5.0 1 09/30/15 18:30 10/05/15 01:03 7440-50-8 Lead 6.7 ug1L 5.0 1 09/30/15 18:30 10/05/15 01:03 7439-92-1 Zinc 54.6 ug/L 10.0 1 09/30/15 18:30 10/05/15 01:03 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 5.0 mg/L 2.5 1 09/30/15 03:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1010512015 04:33 PM without the written consent of Pace Analytical Services, Inc.. Page 3 of 13 aceAnalytical o www.paca►abs.cam ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: WATTS SPINDALE SW Pace Project No.: 92269627 Sample: OU-002 Lab ID: 92269627002 Collected: 09/24/15 10:05 Received: 09/29/15 12:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg1L 5.0 1 10/02/15 08:55 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 18.4 uglL 5.0 1 09/30/15 18:30 10/05/15 01:07 7440-50-8 Lead ND uglL 5.0 1 091301151&30 1010511501:07 7439-92-1 Zinc 45.0 ug/L 10.0 1 09/30/15 18:30 10/05/15 01:07 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.9 mg1L 3.6 1 09/30/15 03:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/05/2015 04:33 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 13 0 aceAnalytical WWW4 acaJabs.WM ANALYTICAL RESULTS Project: WATTS SPINDALE SW Pace Project No.: 92269627 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 011.1-004 Lab tD: 92269627003 Collected: 09/24/15 10:15 Received: 09/29/15 12:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Oual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg1L 5.0 1 10/02/15 08:55 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 157 uglL 5.0 1 09/30/15 18:30 10/05/15 01:10 7440-50-8 Lead ND uglL 5.0 1 09/30/15 18:30 10/05/15 01:10 7439.92-1 Zinc 110 uglL 10.0 1 09/30/15 18:30 10/05/15 01:10 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 2.5 1 09/30/15 03:53 Date: 10/05/2015 04:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 13 aceAnalytical www.pacefabs.cw ANALYTICAL RESULTS Project: WATTS SPINDALE SW Pace Project No.: 92269627 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OU-006 Parameters Lab ID: 92269627004 Collected: 09/24/15 10:25 Results Units Report Limit DF Received: 09/29/15 12:15 Matrix: Water Prepared Analyzed CAS No. Qual 1664 SGT HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 10/02/15 08:56 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 72.6 ug1L 5.0 1 09/30/15 18:30 10/05/15 01:13 7440-50-8 Lead ND ug/L 5.0 1 09/30/15 18:30 10/05/15 01A3 7439-92-1 Zinc 110 ug/L 10.0 1 09/30/15 18:30 10/05/15 01:13 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 2.9 ' 1 09/30/15 03:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/05/2015 04:33 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 13 (�55'cmnalyticalo www.pac*kb&cam QUALITY CONTROL DATA Project: WATTS SPINDALE SW Pace Project No.: 92269627 QC Batch: GCSV122776 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92269627001, 92269627002, 92269627003, 92269627004 METHOD BLANK: 157289E Matrix: Water Associated Lab Samples: 92269627001, 92269627002, 92269627003, 92269627004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 10/02/15 08:24 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1572899 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.8 99 64-132 MATRIX SPIKE SAMPLE: 1572900 92268758006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 16.5 82 64-132 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/05/2015 04:33 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 13 (�55'cie Analyfical *"..pacelabs.rx n QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: WATTS SPINDALE SW Pace Project No.: 92269627 QC Batch: MPRP119677 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92269627001, 92269627002, 92269627003, 92269627004 METHOD BLANK: 1571115 Matrix: Water Associated Lab Samples: 92269627001, 92269627002, 92269627003, 92269627004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper uglL ND 5.0 10/05/15 00:29 Lead uglL ND 5.0 10/05/15 00:29 Zinc ug/L ND 10.0 10/05/15 00:29 LABORATORY CONTROL SAMPLE: 1571116 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec limits Qualifiers Copper uglL 250 238 95 85-115 Lead uglL 250 232 93 85-115 ' Zinc uglL 250 226 90 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1571117 1571118 MS MSD 92269719002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug1L 50.2 250 250 313 302 105 101 70-130 4 Lead ug1L 9.0 250 250 252 242 97 93 70-130 4 Zinc ug1L 75.6 250 250 311 298 94 89 70-130 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1571119 1571120 MS MSD 92269439003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug1L ND 250 250 254 245 100 97 70-130 4 Lead ug1L ND 250 250 243 237 97 95 70-130 3 ,Zinc ug1L 0.012 250 250 249 243 95 93 70-130 2 mglL Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/05/2015 04:33 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 13 e 5ac ie A na ly tical wwwpacetabs.com QUALITY CONTROL DATA Project: WATTS SPINDALE SW Pace Project No.: 92269627 QC Batch: WET140482 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92269627001, 92269627002, 92269627003, 92269627004 METHOD BLANK: 1570311 Matrix: Water Associated Lab Samples: 92269627001, 92269627002, 92269627003, 92269627004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 09/30/15 03:51 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1570312 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 232 93 90-110 SAMPLE DUPLICATE: 1570313 92269560010 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1570314 Parameter Total Suspended Solids 92269740002 Dup Units Result Result mg/L ND ND RPD Qualifiers Results presented on this page are In the units indicated by the "units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuii, Date: 101OW2015 04:33 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 13 aceAnalytical wwwPocelabs.cam QUALIFIERS Project: WATTS SPINDALE SW Pace Project No.: 92269627 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MID L-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nilrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/05/2015 04:33 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13 acmnalytical o wwwpacelabs com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: WATTS SPINDALE SW 92269627 Analytical tab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92269627001 OU-001 EPA 1664B GCSV/22776 92269627002 OU-002 EPA 1664B GCSV/22776 92269627003 OU-004 EPA 1664B GCSV/22776 92269627004 OU-006 EPA 1664B GCSV/22776 92269627001 OU-001 EPA 200.7 MPRP119677 EPA 2007 ICP117720 92269627002 OU-002 EPA 200.7 MPRP/19677 EPA 200.7 ICP117720 92269627003 OU-004 EPA 200.7 MPRP/19677 EPA 200.7 ICP117720 92269627004 OU-006 EPA 200.7 MPRP/19677 EPA 2003 ICP117720 92269627001 OU-001 SM 2540D WET140482 92269627002 OU-002 SM 2540D WET/40482 92269627003 OU-004 SM 2540❑ WET/40482 92269627004 OU-006 SM 2540D WET/40482 Date: 10/05/2015 04:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 13 ?ce�j��� Sample Condition U on-Recei t SCUR Page 1 of 2' ,FYDoctiment Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Client Name: Cv 4•Page 2 of 2 Is for Internal Use Only Courier: ❑ FedE)❑ UP USP❑ ClierD Co merciC] Pace Other 0~tional a%_ f Custody Seal on Cooler/Box Present: ❑ [� yes /no Seals intact: ❑ yes -❑ no pajihlt�t 's`'c4 PX. ro'. iVame:•` Packing Material: ❑ Bubble Wrap r42 Bubble Bags❑ None❑ Other Thermometer Used: IR Gun , Type of Ice: et' tue ' None amples on Ice, cooling process has begun Temp Correction Factor TCorrection U Corrected Cooler Temp.: 'C Temp should be above freezing to 6•C Biological Tissue is Frozen: Yes No to Comments: Date and Initials of person examinln contents: Chain of Custodx Present; Yes No ❑N!A 1: Chain of Custody Fitted Out: 0 es. QN, ❑N!A 2. Chain of C I ustody Relinquished: es ❑N!A 3. Sampler blame & Signature on COC: as ❑ ❑NIA 4. Samples Arrived within Hold Time: 01ercjNay''"❑N! 5.. Short Hold Time Analysis <72hr : ❑Yes ❑ ►A 6. Rush Turn Around Time Requested: C]Yes o ❑NIA. 7. Sufficient Volume: es No ❑NIA 8: Correct Containers Used: -Pace Containers Used: E Yes ❑ s ❑ , ❑N/A ❑N/A 9. , Containers Intact: es ❑No ❑N/A 10. Filtered volume received for Dissolved tests ❑Yes JQKo ❑Nr 1. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: Yes ❑yo ❑N!A 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, coliform, TOC, O&G, W-DRO(wafer} es ❑N DOyes Mo. es ❑N erm s unu ❑N1A ❑N!A 13. Samples checked for dechlorination: ❑Yes ❑No ❑ /A 14. Heads pace In VOA Vials >6mm : ❑Yes ❑No N/A Trip Blank Present; Trip Blank Custody Seals Present Pace Trip Blank Lot # if purchased): ❑Yes ❑No ❑Yes ❑No N!A ❑NIA Client Notification/ Resolution: Field Data Required? Y / N Person Contacted: Dateffime: Comments/ Resolution: SCURF Review: 'm Date: _-ZrWO# : 92269627 SRF Review: Date: 5 Note: Whenever there is a discrepancy affecting North Carolina compliance 10119 samples, a copy of this form will be sent to the North Carolina DEHNR 92269627 ddB BBB IIII /III 111 ill/ 1 Certification Office ( i.e out of hold, Incorrect preservative, out of temp, r Incorrect containers) i CHAIN -OF -'CUSTODY 1 Analytical Request Document The CAain•of-Custody is a LEGAL DOCUMENT. All reiavant fialds nXim be completed accurately. .vnnr.PatehLssom Section A /��f^^ page Section B - Section C Required Dienj ! / lnformaion: Requred Project lnfonnaliom lnnivalniomwticn: fr'IJC,�Y�IL. . .iT1Cf�Up wur+.�, 4�{1fCi'. COM rrctC r0panT0:MARK VENNAQt7 Allanlon.MARie- i�x1AJAR& 7_' :anpamr: I, 4ddrass I O - Copy To: o:•�'4szo C Ll Cemp eJaF S a.%/rTZM Ir04 IJoLC, 61 REGULATORYAGENCY .`J''►FJVa)i1 / 1/C 'LL%tpl% /'� J•fCk+c: .C'• UNc.�c. a f.GaM Amress R� GO '•JSAr.1J �N4 ZQ' ('7. NPDES r` GROUNDWATER r DRINKING WATER r UST r- RCRA i— OTHER lYI O►" .KorT11C W' .c: a Plun2 Orcer No.: Pea Ouete ftf- : p Fax: A Pfejeel N me: Pace Prgeu Site Location STATF: _ • • . Raga tad Dui DatarTAT: -s f D Prcjeahlumper. Pea Prow+: .! '„ I - Requested'Anatysis Filtered (Y1N)-•:• . ^-. _ ' Section D Matrix Cede. Nneulrw Clore lnwrraeua MATRIX r CODE - s COLLECTEO Preservatives - S: '. •, .. Drinking Waar �7C[ 1(�% Wafer g $ t: Waste Water W W • Product .' p U sTnm Soi_ dOL �/ 8 rl m SAMPLE ID w>» ? m Sample (A-Z. oaI.-) ar - AR MUST BE UNiOUE 7« O pwp D I . a. Z 2 5 p V F ey I jDs 4 Uj DATE , "ME DARE TIME x = x z z M O VA U ¢ Pau PrD{act Not Lab I.D. �• O�' -� C7b ;Arr, • x ' kx k' x -A1fi1 z O L: + O aS 7 X X ?e x k )C . G q/2Y o= x 'A U s � t 6 7 a � a. `. "ITIONAL COMMENTS - ,•I REL1NQUtSNEDBYl AFFILIATION-{. ;•;'I, DATES•`^;-I1*,TiMSE ..'I. ,.,r, ACCEPTE0,8Yf AFFILIATION-',.yt- :1 o11TE---j, TIME- I SAMPLECONDmONS Tr SAMPLER NAIAE AND SIGNATURE - .: - cy co S PRWT Nam" of SAMPLER: C N J,4 q 2 1 "3 DATE 512ned (] (,/ SIGNATURE of SAMPLER: T 2 ( %S G ye y (ttIWwM: Lrmp N41e'. By z Wwg V 4 farm you acc&Wq Pant NET 30 eaf Pny~t lemu ono tgrverg to wa owrges a i s% Per —M for wry rnwaa ml Paid w m 30 CMA F-ALL4420rdv.07. 15-May-2007 \� WAr r T WATER TECHNOLOGIES November 4, 2015 BY CERTIFIED ARIL — RETURN RECEIPT REQUESTED Central Records Division of Energy, Mineral and Land Resources 1617 Mail Service Center Raleigh, NC 27699-1617 RECEIVED NOV 10 2015 CENTRAL FILES DWR SECTION" Re. Discharee Monitoring Report and Notice of Compliance Status for Watts Regulator Facility located at t 100 Watts Road; Spindale, North Carolina (Certificate of Coverage Number NCG030251) To Whom It May Concern: In accordance with the certificate of coverage referenced above and the requirements of general permit number NCG030000 (the "General Permit"), please find enclosed Watts Regulator's ("Watts") discharge monitoring report ("DMR") for monitoring year 3, period 2 monthly monitoring (September, 2015) regarding our facility located at 100 Watts Road in Spindale, North Carolina (the "Facility"). Consistent with the February 3, 2010 Approval of Representative Outfall Status, Watts obtained quantitative data for samples from outfalls 001, 002, 004 and 006. Based on the results reflected in the September 2015 DMR, these outfalls are in Tier III status. In addition to the required outfall sampling, Watts obtained samples for PH from outfalls 003, 005 and 007. Those data are also reflected on the enclosed DMR.' Upon receiving the results of the July 2015 sampling reflected in the enclosed DMR, Watts engaged the consulting firm of Hart & Hickman ("H&H") to develop additional best management practices ("BMP") for the Facility. Given that all four of the monitored outfalls are now in Tier III status, monthly monitoring data continues to be used to evaluate the effectiveness of these additional BMPs and the need for further improvements. Additional landscaping improvements have continued during the sampling period, and though the outfalls have moved into Tier Ill status, analytical results shown significant improvement. As mentioned in my previous correspondence, I would like to schedule a meeting with representatives of the Division of Energy, Mineral and Land Resources in order to discuss the results of a stormwater compliance audit performed by AECOM and Watts' efforts to implement additional BMPs at the Facility.. Please contact me at your earliest convenience at (978) 689- 6070 to arrange a time. Sincerely, Howard H. Chu Director, Environment, Health and Safety Watts Water Technologies, Inc. Enclosures cc: Central Records, Division of Water Quality ` As documented in the June 2015 DMR, the pH of precipitation in and around Spindale is commonly below the benchmark range in the General Permit. Watts will continue to collect "neat" precipitation samples, analyze those samples for pH, and include the summarized results in each DMR, in accordance with footnote 1 of Table 3 in the General Permit. Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 04% Date submitted 09/30/15 CERTIFICATE OF COVERAGE NO. NCG0302SI FACILITY NAME Watts - Sp_indale COUNTY Rutherford PERSON COLLECTING SAMPLES Mark Kennard LABORATORY_ Pace Analytical Lab Cert. # 12, 5342, 37706 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results L1 SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec cl or ® Monthly' August (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA� ®Zero -flow ❑Water Supply ❑SA� ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 —) ®No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organicss Benchmarks 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 N/A N/A N/A N/A N/A N/A N/A N/A N/A 2 N/A N/A N/A N/A N/A N/A N/A N/A N/A 3 N/A N/A N/A N/A N/A N/A N/A N/A N/A 4 N/A N/A N/A N/A N/A N/A N/A N/A N/A S N/A N/A N/A N/A N/A N/A N/A N/A N/A 6 N/A N/A N/A N/A N/A N/A N/A N/A N/A 7 N/A N/A N/A N/A N/A N/A N/A N/A N/A 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date; 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 putfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, lnches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cops! of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results !or at end of monitoring period in the case o "No Discharge" re orts to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4 V, (Signature of Permittee) Permit Date:11/1/2012-10/31/2017 9— 3J iS (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 IV WATT T WATER TECHNOLOGIES September 30, 2015 BY CERTIFIED MAIL — RETURN RECEIPT REQUESTED Central Records Division of Energy, Mineral and Land Resources 1617 Mail Service Center Raleigh, NC 27699-1617 RECEIVE® OCT 0 5 2015 CENTRAL FILES DWR SECTION Re: Discharge Monitoring Report and Notice of Compliance Status for Watts Regulator Facility located at 100 Watts Road; Spindale, North Carolina (Certificate of Coverage Number NCG030251) To Whom It May Concern: In accordance with the certificate of coverage referenced above and the requirements of general permit number NCG030000 (the "General Permit"), please find enclosed Watts Regulator's ("Watts") discharge monitoring report ("DMR") for monitoring year 3, period 2 monthly monitoring (August, 2015) regarding our facility located at 100 Watts Road in Spindale, North Carolina (the "Facility"), Consistent with the February 3, 2010 Approval of Representative Outfall Status, Watts attempted to sample for quantitative data from outfalls 001, 002, 004 and 006. Due to the lack of available qualifying rain events in August, we were unable to do so during August of 2015. Based on the results reflected in the July 2015 DMR, and no -flow in August 2015, these outfalls remain in Tier II status, and monthly monitoring of all four will continue. Watts continues to engage the consulting firm of Hart & Hickman ("H&H") in developing and evaluating additional best management practices ("BMP") for the Facility. Given that all four of the monitored outfalls are now in Tier II status, monthly monitoring data will be available to evaluate the effectiveness of these additional BMPs and the need for further improvements. As mentioned in my previous correspondence, in light of the results of AECOM's compliance audit, and the Facility's entry into Tier II status under the General Permit, I would like to schedule a meeting with representatives of the Division of Energy, Mineral and Land Resources in order to discuss these matters further. Please contact me at your earliest convenience at (978) 689-6070 to arrange -a time. Sincerely, 41z, Howard H. Chu Director, Environment, Health and Safety Watts Water Technologies, Inc. Enclosures cc: Central Records, Division of Water Quality 26396012v1 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 8/10/15 i� CERTIFICATE OF COVERAGE NO. NCG030251 FACILITY NAME Watts Regulator - 5 indale COUNTY Rutherford PERSON COLLECTING SAMPLES Ademola Bakenne LABORATORY Pace Analytical Lab Cert. # 12, 5342, 37706 Comments on sample collection or analysis: A Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ® ]an -June ❑ July -Dec or E] Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [:]WaterSupply ❑SAftw< ®Other C PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches3 Total Suspended Solids pH, standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =__> - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 06/27/15 0.21 137 4.2 1.19 0.203 0.379 <5.0 N/A 2 06/27/15 0.21 8.1 4.6 1.53 0.156 0.555 <5.0 N/A 3 06/27/15 0.21 N/A 4.9 N/A N/A N/A N/A N/A 4 06/27/15 0.21 5.4 6.1 0.254 0.007 0.268 <5.0 N/A 5 06/27/15 0.21 N/A 6.0 N/A N/A N/A N/A N/A 6 06/27/15 0.21 17.1 6.0 0.225 0.0205 0.242 1 <5.0 N/A 7 06/27/15 0.21 N/A 6.1 N/A N/A N/A I N/A N/A I Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/2S/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Mr. John Palotta Name (Print name) Vice President of Operations _ Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format,"<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part 13: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No dischorge this period ?2 Outfall No, Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. ti Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier I, Tier 2, or Tier 3 responses. See Genera! Permit text. FOR PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. + TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMIt including all "No Discharge" re orts within 30 days o recei # o the lab results or at end o mani#orin eriad in the case of "No Discharge" reports] to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR'ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware t here are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Si a)re of Permittee) {pate) Permit Date,11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 VIOWANM A Watts Water Technologies Company 815 Chestnut Street • North Andover, MA • 01845-5098 • Tel, (978) 688-1811 • Fax: (978) 794-1848 August 10, 2015 BY CERTIFIED MAIL — RETURN RECEIPT REQUESTED RECEIVED Central Records AUG 14 2015 Division of Energy, Mineral and Land Resources CENTRAL FILES 1617 Mail Service Center DWR SECTION Raleigh, NC 27699-1617 Re: Discharge Monitoring Report and Notice_ of Compliance Status Watts Regulator, 100 Watts Road, Spindale, North Carolina Certificate of Coverage Number NCG030251 To Whom It May Concern: In accordance with certificate of coverage referenced above and requirements of general permit number NCG030000 (the "General Permit"), please find enclosed discharge monitoring report ("DMR") for monitoring year 3, period I (January 1, 2015 to June 30, 2015) regarding Watts Regulator ("Watts") facility located at 100 Watts Road in Spindale, North Carolina (the "Facility"). Consistent with the February 3, 2010 Approval of Representative Outfall Status, Watts obtained quantitative data for samples from outfalls 001, 002, 004, and 006. Based on the results submitted with the DMR, these four outfalls are now in Tier II status and Watts will begin monthly monitoring accordingly. Watts also obtained samples for pH analysis from outfalls 003, 005, and 007. Those data are also reflected in the enclosed DMR.' Watts recently engaged the environmental consulting firm AECOM to conduct a stormwater compliance audit at our Facility. Though results of this audit continues to be under evaluation, Watts requested that AECOM revise the Facility's stormwater management plan ("SWPPP"), engaged Proctor Environmental Services, Inc., ("PES") to assist in implementing AECOM recommendations, and — upon receiving the results of the recent sampling reflected in the enclosed DMR — retained Hart & Hickman ("H&H") to develop additional best management practices ("BMP") for the Facility. Given that ail four of the monitored outfalls are now in Tier 11 status, monthly monitoring data will be available to evaluate effectiveness of these additional BMPs and the need for any further improvements. In light of the AECOM compliance audit results and entry under the General Permit into Tier II status by the Facility, I respectfully request a meeting with representatives of the Division of Energy, Mineral and Land Resources in order to discuss these matters further. As I will be on shown in the documents attached to the DMR, the pH of precipitation in and around Spindale is commonly below the benchmark ran,e in the General Permit. Watts will continue to collect "neat" precipitation samples, analyze those samples for pH, and include the results with its next DMR (for July 2015), in accordance with footnote 1 of Table 3 in the General Permit. Watts Regulator Company Since 1874 watts.com a previously -planned business trip to Asia Pacific during the weeks of August 17`h and 24`h, 1 am available to meet during the weeks of August 31" or September 71h. Please contact me at your earliest convenience by phone (978-689-6070) or e-mail (howard.chu@watts.com) to arrange a date and time. Sincerely, /Ij t/�_ Howard H. Chu Director, Environment, Health and Safety Watts Water Technologies, Inc. Enclosures cc: Central Records, Division of Water Quality pH Data Information Watts Regulator Site Spindale, North Carolina NC Division of Water Quality General Permit No. NCG030000 The following pH readings were recorded from the seven outfalls at the Watts facility in Spindale, North Carolina during the ,tune 2015 sampling event. These readings were taken at the laboratory, Pace Labs, from laboratory -provided sample bottles filled during the sampling event for the sole purpose of obtaining pH readings. A pH meter was not available at the site during the June 2015 stormwater sampling event. Outfall No. pH Reading 001 4.2 002 4.6 003 4.9 004 6.1 005 6.0 006 6.0 007 6.1 Due to the variable pH readings collected (ranging from 4.2 to 6.1) and that three readings (Outfalls 001, 002, and 003) were outside the NC stormwater benchmark range of 6.0 to 9.0, a literature search was conducted to determine if pH data could be found to verify historical regional precipitation pH readings. The National Atmospheric Deposition Program (NADP) monitors precipitation chemistry to measure atmospheric deposition and study its effects on the environment. Sites in the NADP precipitation chemistry network began operations in 1978 with the goal of providing data on the amounts, trends, and geographic distributions of acids, nutrients, and base cations in precipitation. Their website, http://nadp.sws.uiuc.edu/dataLsiLtes/map/?net=NTN, summarizes results from 250 sites located around the country. pH data collected from five nearby monitoring stations (Gatlinburg, TN, Franklin, NC, Mt. Mitchell, NC, Greenville, SC, and Salisbury, NC, located relative to the subject site as shown on the following map) are shown on the following graphs. Data indicate that pH readings ranging from approximately 4.5 to 5 have been typical in the area around Spindale for the past 30 or more years. In addition to the literature search, Watts has begun recording pH readings during precipitation events at the site using an on -site, calibrated pH meter. The following data was collected during an 0.49 inch precipitation event on July 25, 2015 from clean plastic bottles located at three areas of the site unaffected by structures or foliage. Sample No. Location PH Ring 1 North Central Fence 4.2 2 Northeast Fence, by Rain Gage 4.1 3 Southeastern, Gate A 4.0 Both the literature search and on -site pH readings indicate that the pH readings collected during the June 2015 are not unusual for this area of North Carolina. National Atmospheric Deposition Program http://nadp.sws.uiuc.edu/data/sites/map/?net=NTN The National Atmospheric Deposition Program (NADP) monitors precipitation chemistry. The program is a cooperative effort between many different group, including federal, state, tribal and local governmental agencies, educational institutions, private companies, and non -governmental agencies. In 1977, U.S. State Agricultural Experiment Stations (SAES) organized a project, later titled the National Atmospheric Deposition Program (NADP), to measure atmospheric deposition and study its effects on the environment. Sites in the NADP precipitation chemistry network began operations in 1978 with the goal of providing data on the amounts, trends, and geographic distributions of acids, nutrients, and base cations in precipitation. The network grew rapidly in the early 1980s. Much of this expansion was funded by the National Acid Precipitation Assessment Program (NAPAP), established in 1981 to improve understanding of the causes and effects of acidic precipitation. Reflecting the federal NAPAP role in the NADP, the network name was changed to NADP National Trends Network (NTN). The NTN network currently has 250 sites. Franklin. NC Site Data Trend for pH 5.3 5.2 5.1 5.0 • 4.9 i 4.8 4.7 4.6 4.5 4.4 National Atmospheric Deposition Program http://nadp.sws.uiuc-edu/data/sites/map/?net=NTN NTN Site NC25 0 Q p 4 ,. ♦ 1976 1978 1980 1982 1984 1986 1988 1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010 2012 2014 2016 Year Annual Criteria Met Annual ®� Criteria Not; Met s ® Trend line National Atmospheric Deposition Program http://nadp.sws.uiuc.edu/data/sites/map/?net=NTN Gatlinburg, TN Site Data Trend for PH oa �p National Atmospheric Deposition Program 5.3 5.2 5.1 5.0 4.9 4.8 4.7 4.6 4.5 4.4 4.3 NTN Site TN11 ' ? @ • � I i I I i � 1978 1980 1982 1984 1986. 1988 1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010 2012 2014 2016 Year 7 Annuat ®1 Criteria Met Annual ®a Criteria Not Met ® Trend fine National Atmospheric Deposition Program http://nadp.sws.uiuc.edu/data/sites/map/?net=NTN Mt Mitchell, NC Site Data Trend for pH 4� p� National Atmospheric Deposition Program 5.3 5.2 5.1 5.0 4.9 4.9 4.7 4.6 4.5 4.4 NTN Site NC45 «- __.. ._... - _ _— ............... r e --.... ♦ i i • 1 I i i 1984 1996 1988 1990 1992 1994 1996 1998 2000 2002 2004 2D06 2008 2010 2012 2014 2016 Annuat ®i Criteria Met Annuat Criteria Not Met Nil Trend tine National Atmospheric Deposition Program http://nadp.sws.uiuc.edu/data/sites/map/?net=NTN Greenville SC Site Data Trend for pH 0O ao National Atmospheric Deposition Program 4.56 4.54 4.52 4.50 4,48 4.46 G 4.44 4.42 4.40 4.38 4.36 4.34 1978 1980 NTN Site SC18 1982 o Year 1984 1986 1988 ®� Annual a Criteria Met Annual ®.I Criteria Not Met Trend tine j National Atmospheric Deposition Program http://hadp.sws.uiuc.edu/data/sites/map/?net=NTN Piedmont NC Station, near Salisbury Site Data Trend for pH vka °an National Atmospheric Deposition Program NTN Site NC34 5.4 5.2 5.0 4.8 4.6 4.4 4.2 • — Annuaif ®� Criteria Met Annual ®i Criteria Not 1 Met, — Trend line 1976 1978 1990 1982 1984 1986 1988 1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010 2012 2014 2016 V— alceAnalj#ical e wrr ,,pecelehS.0= July 10, 2015 Tom Proctor Proctor Environmental RE: Project: WATTS SPINDALE SW Pace Project No.: 92256587 Pace Analytical Services, Inc. 9800 Kircey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Tom: Enclosed are the analytical results for sample(s) received by the laboratory on June 30, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNi standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, V�, c, -- Cs r„ -J Liamm Carrubba fiamm.carrubba@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page i of 14 �;a'ne'AnaVicalo wew pacelebs.com Project: WATTS SPINDALE SW Pace Project No.: 92256587 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37705 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification M 37712 CERTIFICATIONS FloridalNELAP Certification #: E87627 Kentucky LIST Certification #: 84 West Virginia Certification M 357 urginivVELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #. 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 14 lane'Analyfical" xww.pacelaba.com SAMPLE ANALYTE COUNT Project: WATTS SPINDALE SW Pace Project No.: 92256587 Pace Analytical Services, Inc. 9800 Mncey Ave. Suite 500 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analysts Reported Laboratory 92256587001 OU - 001 EPA 1664E SMS 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 25400 MDW 1 PASI-A EPA 9040 MLS 1 PASI•A 92256587002 OU - 002 EPA 1664E JMS 1 PASI-C EPA200.7 JMW 3 PASI-A SM 2540D MDW 1 PASI-A EPA 9040 MLS 1 PASI-A 92256587003 OU - 004 EPA 1664B JMS 1 PASI-C EPA200.7 JMW 3 PASI-A SM 2540D MDW 1 PASI-A EPA 9040 MLS 1 PASI-A 92256587004 OU - 006 EPA 1664B JMS 1 PASI-C EPA200.7 JMW 3 PASI-A SM 2540D MDW 1 PASI-A EPA 9040 MLS 1 PASI-A 92256587005 OU - 003 EPA 9040 MLS 1 PASI-A 92256587006 OU-005 EPA9040 MLS 1 PASI-A 92256587007 OU - 007 EPA 9040 MLS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, without the written consent or Pate Analytical Services, Inc.. Page 3 of 14 acmnalytrcal WW'pecelafls.ww ANALYTICAL RESULTS Project: WATTS SPINDALE SW Pace Project No.: 92256587 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersvitle, NC 2807a (704)875-9092 Sample: OU - 001 Parameters Lab ID: 92256587001 Collected: 06/27/15 14:12 Results Units Report Limit OF Received: 06/30/15 09:30 Matrix: Water Prepared Analyzed CAS No, Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mg1L 5.0 1 07/09115 09:51 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200-7 Copper 1190 ug1L 5.0 1 07/01/15 17:35 07/03/15 06:25 7440-50-8 Lead 203 ug1L 5.0 1 07/01/15 17:35 07/03/15 06:25 7439-92-1 Zinc 379 ug1L 10.0 1 07/01/15 17:35 07/03115 06:25 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 137 mg1L 16.7 1 07/01/15 12:46 9040 pH Ana lylical Method: EPA 9040 pH 4.2 Std. Units 0.10 1 07/07/15 13:55 H6 Sample: OU - 002 Parameters Lab lD: 92256587002 Collected: 06/27115 14:22 Results Units Report Limit DF Received: 06/30/15 09:30 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oif and Grease NO mg1L 5.0 1 07/09/15 09:51 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 1530 ug1L 5.0 1 07101/15 17:35 07/03/15 06:28 7440-50-8 Lead 156 ug1L 5.0 1 07/01/15 17:35 07/03115 06:28 7439-92-1 Zinc 555 ug(L 10.0 1 07/01/15 17:35 07/03/15 0618 7440-66-6 25400 Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 8.1 mglL 2.5 1 07/01/15 12:46 9040 pH Analytical Method: EPA 9D40 pH 4.6 Std, Units 0.10 1 07/07/15 13:55 H6 Sample: OU - 004 Lab ID: 92256587003 Collected: M27/15 14:38 Received: 06/30/15 09:30 Matrix: Water Parameters Results Units Report Limit DF , Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mglL 5.0 1 07/09115 09:51 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 254 ug1L 5.0 1 07/01/15 17:35 07/03115 06:31 7440-50-8 Lead 7.0 ug1L 5.0 1 07/01115 17:35 07/03/15 06:31 7439-92-1 Zinc 268 ug1L 10.0 1 07/01/15 17:35 07/03/15 06731 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0711012015 10:59 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 14 lacieAnalj6caf" nww.P I0bs.CoM ANALYTICAL RESULTS Project: WATTS SPINDALE SW Pace Project No.: 92256587 Pace Analytical Services, Inc. 980D Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OU - 004 Lab ID: 92256587003 Collected: 06/27/15 14:38 Received: 06/30/15 09:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 5.4 mglL 2.5 1 07/01/15 12:48 9040 pH Analytical Method: EPA 9040 pH 6.1 Std. Units 0.10 1 07/07/15 13:55 H6 Sample: OU -Doe Lab ID: 92256587004 Collected: 06/27/15 14:50 Received: 06/30/15 09:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mglL 5.0 1 07/09/15 09:52 200.7 MET 1CP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 225 ug1L 5.0 1 07/01/15 17:35 07/03/15 06:34 7440-50-8 Lead 20.5 ug1L 5.0 1 07/01/15 17:35 07/03/15 06:34 7439.92-1 Zinc 242 uglL 10.0 1 07/01/15 17:35 07/03/15 06:34 7440-66-6 2540D Total Suspended Solids Analytical Method. SM 2540D Total Suspended Solids 17.1 mg1L 3.6 1 07/01/15 12:49 9040 pH Analytical Method: EPA 9040 pH 6.0 Sid. Units 0.10 1 07107/15 13:55 H6 Sample: OU -003 LabJD- 92256587005 Collected: 06/27/15 14:29 Received: 06/30/15 09:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 9040 pH Analytical Method: EPA 9040 pH 4.9 Sid. Units 0.1 D 1 07/07/15 13:55 H6 Sample: OU -005 Lab ID: 92256587006 Collected: 06/27/15 14:43 Received: 0613011509:30 Matrix: Water Parameters Results Units Report Limlt DF Prepared Analyzed CAS No. Quaff 9040 pH Anatytical Method: EPA 9040 pH 6.0 Sid. Units 0.10 1 07/07/15 13:55 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/1012015 10:59 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14 aceAnalXical VrtYV.f f 8C2�803. [Of+l i E I Project: WATTS SPINDALE SW Pace Project No.: 92256587 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite too Huntersville, NC 28076 (704)875-9092 Sample: OU - 007 i Lab ID: 92256587007 Collected: 051271115 14:58 Received: 06/30/15 09:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 9040 pH ; Analytical Method: EPA9040 pH ; 6.1 Std, Units 0.10 1 07/07/15 13:55 H6 Date: 07/101201510:59AM i REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, tnc.. Page 6 of 14 lane'Analyfical"' xwwpacefa6scom QUALITY CONTROL DATA Project: WATTS SPINDALE SW Pace Project No.: 92256587 QC Batch: GCSV/21883 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Late Samples: 922565870D1, 92256587002, 92256587003, 92256587004 METHOD BLANK: 1504908 Matrix: Water Associated Lab Samples: 92256587001, 92256587002, 92256587003, 92256587004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 07109l15 09:44 Pace Analytical Services, Inc. 9800 Vincey Ave. Suite 100 Huntersvilie. NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1504909 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 33.3 83 78-114 MATRIX SPIKE SAMPLE: 1504910 35195511005 Spike MS M5 % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mgfL <1A 40 38.1 94 78-114 Results presented on this page are in the units indicated by the "Units" column except where an attemale unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fun. Date: 07/10/2015 10:59 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 14 aceAnalytical Kww.Pacerabs.com QUALITY CONTROL DATA Project: WATTS SPINDALE SW Pace Project No.: 92256587 QC Batch: MPRP118891 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples., 92256587001, 92256587002, 92256587003, 92256587004 METHOD BLANK: 1499491 Matrix: Water Associated Lab Samples: 92256587001. 922565B7002, 92256587003, 92256587004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Capper ug1L ND 5.0 07/03/15 05:08 Lead ug1L ND 5.0 07/03/15 05:08 Zinc ug1L ND 10.0 07/03/15 05:08 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1499492 Spike LCS LCS %Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper uglL 500 488 98 85-115 Lead ug1L 500 479 96 85-115 Zinc ug1L 500 471 94 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1499493 MS 92256672009 Spike Parameter Units Result Conc. Copper ug1L ND 500 Lead ug1L ND 500 Zinc ug1L 0.046 500 mg1L 1499494 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD Qual 500 295 466 59 93 70-130 45 M1,R1 500 293 457 58 91 70-130 44 M1,R1 500 308 465 52 84 70.130 41 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1499495 1499496 MS MSD 92256444002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug1L 81.4 500 500 602 593 104 102 70-130 2 Lead ug/L 54.8 500 500 506 502 90 89 70-130 1 Zinc ug/L 57.2 500 500 528 526 94 94 70.130 0 Results presented on this page are in the unils Indicated by the -Unlls- column except where an alternate unit is presentetl to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in dull. Date: 07/10/2015 10:59 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 14 aceAnalytical xww.pacelabs.com QUALITY CONTROL DATA Project: WATTS SPINDALE SW Pace Project No.: 92256587 Pace Analytical Services, Inc. SsoO KlnceyAve. Suite too Huntersville, NC 28078 (704)875-9092 QC Batch: WET138518 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples:. 92256587001, 92256587002, 92256587003, 92256587004 METHOD BLANK: 1499098 Matrix: Water Associated Lab Samples: 92256587001, 92256587002, 92256587003, 92256587004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 07101/15 12:36 LABORATORY CONTROL SAMPLE: 1499099 Spike LCS LCS °% Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 240 96 90-110 SAMPLE DUPLICATE: 1499100 92256445010 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1499101 92256513006 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/10/2015 10:59 AM without the written consent of Pace Analyticat Services, Inc.. Page 9 of 14 aceAnalytical KS.wpacelabs com QUALITY CONTROL DATA Project: WATTS SPINDALE SW Pace Project No.: 92256587 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunletsville. NC 28078 (704)B75-9092 QC Batch: WET138635 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92256587001, 92256587002, 92256587003, 92256587004. 92256587005, 92256587006. 92256587007 SAMPLE DUPLICATE: 1502780 922SM7001 Dup Parameter Units Result Result RPD Qualifiers pH Sid. Units 4.2 4.3 1 H6 SAMPLE DUPLICATE: 1502781 92256690001 Dup Parameter Units Result Result RPD Qualifiers pH Sid. units 7.3 7.4 1 H6 Results presented on Ihls page are in the units indicated by the "Units- Column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 07/10/2015 10:59 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 14 aceAnalytical wwWvpacelabs.cam QUALIFIERS Project: WATTS SPINDALE SW Pace Project No.: 92256587 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc- 9800 Kincey Ave. Suite 100 Huntersville, NC 28075 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyle is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Get - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chlaroethylvinyl ether, Styrene, and Vinyl chloride, A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N- Nitrosod iphenyl a mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNl accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA recommended holding time- M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. RI RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07110/2015 10:59 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14 laceAnaiXicale rvusepacelahs.wm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: WATTS SPINDALE SW Pace Project No.: 92256587 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 922565870D1 OU - 001 EPA 1664B GCSV/21883 922565670D2 OU - 002 EPA 16646 GCSV/21883 92256587003 OU - 004 EPA 9664E GCSV/21883 92256587OD4 OU - 006 EPA 1664B GCSV121883 92256587001 QU-001 EPA200.7 MPRP118891 EPA200.7 92256587002 OU - 002 EPA200.7 tAPRP118891 EPA200.7 92256597003 OU - 004 EPA200.7 MPRP118891 EPA200.7 92256587004 OU - 006 EPA200.7 MPRPtIS891 EPA200.7 922565B7DO1 OU - 001 SM 2540D WET/38510 92256587002 OU - 002 SM 2540D WET138518 92256587003 OU - 004 SM 2540D WFT138518 92256587004 OU - 006 SM 2540D WET/38518 92256587001 OU - 001 EPA9040 WET138535 92256587002 OU - 002 EPA 9040 WET/38635 92256587003 OU - 004 EPA 9040 WET/38635 92256587004 OU - 006 EPA 9040 WET138535 92256587005 OU - 003 EPA 9040 W'cT/38635 92256587006 OU - DOS EPA 9040 WET138635 92256587007 OU - D07 EPA 9040 WET138635 Date: 07110/2015 10:59 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc - Analytical Batch ICP116955 ICP116955 I C P/ 16955 ICP/16955 Page 12 of 14 Document Name: document Revised: May 18, 2015 1?c�ak?lytl�i<• Sample Condition Upon Receipt (SCUR) Page 4 of 2' Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Client Name: ��C�;-��1,( Page 2 of 2 is for Internal Use Only Courier: ❑ ed >_ ❑ UPS❑ USPS❑ Client❑ Commercial❑ Pace Other Q 4 5 } Custody Seat on Cooler/Box Present: ❑ yes [3 no Seats intact: ❑ yes ❑ no Packing Material: ❑ Bubble V❑p ❑ ubble Bag ❑ None Other Wet Thermometer Used: IR Gun T1401 ype of Ice: Blue None Samples on Ice, cooling process has begun Temp Correction Factor • T1401 No Correction Corrected Cooler Temp.: / 'C Temp should be above freezing to 6'C Biological Tissue is Frozen: Yes No !!A Date and Inlflal of p son camining oa g contents: - 1_ Comments: Chain of Custody Present: OYes ONO ONIA 1. Chain of Custody Filled Out: ElYes ONO ONIA 2. Chain of Custody Relinquished: $Yes ONO ONIA 3. Sampler Name & Signature on COC: 6Yes ONO ❑NIA 4. Samples Arrived within Hold Time: (SYes ONO ❑N(A 5. Short Hold Time Analysis (<72hr): ❑Yes RNo ONIA 6. Rush Turn Around Time Requested: ❑Yes )SINo ©"IA 7, Sufficient Volume: ItYes ❑No ❑NIA 8. Correct Containers Used: -Pace Containers Used: NYes ONO &Yes ONO ONIA ONIA 9. Containers Intact: ((yes ©No ❑NIA 10, Filtered volume received for Dissolved tests ❑Yes 29No ❑NIA 11. Sample Labels match COC: ` tNYes ONo ONIA -Includes date/fimellD/Analysis Matrix: `` -T 12. All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions; VOA, coWorm, TOC, o$G, Vdl•DRO (water) MYes ONO tgYes ONO tKYes ONO ONIA ONIA 13. Samples checked for dechtorination: ❑Yes Zblo ONIA 14. Headspace in VOA Vials ( >6mm): ❑Yes ❑No ONIA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): - __ ❑Yes ONO ❑Yes ONO i?NIA SNIA 16. _..... .. _. _ Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: Date/Time: Comments/ Resolution: W`C!i J/ r nl hL.nl 1..�rc SCURF Review: �- Date: 1�-30- I� 92�5658? SRF Review: 1 ) Date: I C ?o • o Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, 92256$87 incorrect containers) Page 13 of 14 Pa'ceAnaly tical` vrr.Proflrbc.rarr SncVon A KnggMd CIM: nt[rM�Iilm CHAIN -OF -CUSTODY 1 Analytical Request Document Ile. Ch?m-cf.CvOody •. *LEGAL O'J VM:-fJ7. AI mrowrtf ddo rnue' be C.•nFtatgi ocnr Wy- � f � SettionB GectlonC R*gnQrd PN,Kt:ntaane0an: try.Y Ief&wdltrl. trFali% C. {�S W:Ltiij�t r� W�Jr'�. �a4ht Gl l..l�L l• . .� v '✓ L.� �� w +�� nctiizss ; i�1t _ CWY Fo' li Y T� �1 RE ULATORT AGENCY L:E'! } ,., � All �� WPaES a^RWNOW,%T;;R (kRINKINGWATER — usT - RCRA 4TT•IE3? nYa rQ !/• J'•' r_hra 0+rir Na: a+[ot��h Ratlronn;[ 6Gt hh ;" L� J • Fes. Fr•'Y`3N 7 J 1.• � • i � rtavpu.'W SJt+r Lo=alti0n OquJcWODut VmWTA1: Drdpa lum r. Pam Pr64 *^ RCQIl �4Let1+4J1AiY�+� �iRCrcfl ��� 64girr6 Kstrh:CopaS = � ? ' Rugan4CIVIt Irev fmWks $AT.IA r,; COLLFCTEC Preseryypven i Otinlemti+;el1[ Q�y ! . gClO'Jla7ar lYoda[r P n � Z a1M7rrE t r L•:/.b � •• ` SINUS oltl S. r ' q _ Y SAMPLED Q. n! A"Of � � G o c SA7S�r FJ'C.r — 1.14Vk9i:i ld ATt WeA.P5 A,$-r RE LNICIVE -49U4 'M CY_'tcr a! p 0 w S it, a F ; ti oG�yt X j a L O �^ 67 r ^-y LZ J � CATr Tn:E lurk T AfE x x i IS E .� j J Paco Pro ort Ne,! Lah LD. 1 r ... -� i 2 /h 7(14(^may :Q f&— cf 4 i Ix x ,/ V1CC s s �( 00 3 ! b S 7 itu a V,1104 I i iG 1 11 'JZ _ FF 1 ADOMONAL COMMUTO R4JNOOI:WIM BY 1AFFILK11011 18 A'AE ACCFMD BY) AFFUATtOh DATE 11M Wing eoumnollc f ! vo SAt/ViFR NA'r1E A M 514MATURE H ' f7i:rlT KnrSLO y:SA4SYLR S 4 �• 51tjYaTUF2 Y. ti.111Pi..5 N " 'Gres• g �p IKnWOn^i;l V7 �� �•7 � / v C 1? e .j, A •lryawri Sr', L': i, 1Frri%ss la prr;r'v is*-- i P-44,:NET'C bL-ra:Mrrs a"5',po-r01-,*'r-rF+i:ar F»iL!-Rr iOf;'�.07, 15, L,L'•• 'tiD: Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 8/27115 CERTIFICATE OF COVERAGE NO. NCG030251 FACILITY NAME Watts - Spindale COUNTY Rutherford PERSON COLLECTING SAMPLES Tom Proctor LABORATORYPace Analytical Lab Cert. it — 12, 5342, 37706 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' July _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑zero -flow ❑Water Supply ❑SA ®Other c PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period?Z Iac �r."Nan-PolarO&G/, r. ' Date Sample, 24hou[ rainfall 7 ;pH', t • t ; , 'Lead Total,7oici[ Outfall No T t a } - Collected amount; 76Laf Suspended Solids_ ,t ;,� a +- t:, ` r Standard uriitst Copper �' . ? "� + Zinc I Total'Pet[oleum !' 5 Organics _ `> r } Hydr&kbor �(mo/dd%yri r Inches}i ;> �Y'kr .�W ,=�s .' ,'i#'w""O „ a,.•'w` r" _'., :.rNl ., i' +_ Berahmarks =__» Gr = ` ' 10o mg/L;or 50'mg%L° ! :6.0 - 9.0 O:Oo7 mg/L=; ='0.03 mg/!= r '0.067-mgf L j =•iS'mg/L 1 mg/L 1 07/14/15 0.32 22.6 4.7 .876 .107 .310 <5.0 NA 2 07/14/15 0.32 75.5 6.0 1.370 0.173 0.449 <5.0 NA 3 07/14/15 0.32 N/A 5.8 N/A N/A N/A N/A NA 4 07/14/15 0.32 16.9 6.5 0.234 0.0125 0.204 <5.0 NA 5 07/14/15 0.32 N/A 6.4 N/A N/A N/A N/A N/A 6 07/14/15 0.32 18.4 6A 0.195 0.0198 0.282 <5.0 NA 7 07/14/15 0.32 N/A 6.4 N/A N/A N/A N/A N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. a For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). *See notes in Attachment regarding regional and site pH readings relative to benchmark and monitoring results. Permit Date: 11/i/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "[lased upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), l certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Mr. John Palotta - Name (Print name) Vice President of Operations Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part 6: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?2 T� UutfaN�No: _ ?. Date Sample Collected"' (mo%dd]yrl 24-hourralnfall;•I amount, T Incfies3� ,tNon-polar O&G/TPH by; EPA �166d {SGT-HEM) "1 "';.Total 5uspended,Sollds pH- Benchmarks -- => - . _ :15 meL . 100 mg/L of 50 mg/L* 6.0 = 9.0 5LI NA NA NA NA NA NA Footnotes from Part A also apply to this Part B Permit Date: 1I/I/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2of3 * See General Permit text, Table S, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART it SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ No ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results_(or at end of monitoring period in the case o "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there ar nificant penalties for submitting false information, including the possibility f fines and imprisonment for knowing violations. ""*�F Z7 J� 4— (Signature of a ittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 %%IWATM A Watts Water Technologies Company 815 Chestnut Street • North Andover, MA • 01845-6098 • Tel. (978) 688-1611 • Fax: (978) 794-1848 RECEIVED August 27, 2015 AUG 2 8 2015 Central Records — Division of Energy, Mineral and Land Resources CENTRAL FILES 1617 Mail Service Center DWR SECTION Raleigh, NC 27699-1617 Re: Discharge Monitoring Report (DMR) and Notice of Compliance Status Watts Regulator, 100 Watts Road; Spindale, North Carolina Certificate of Coverage Number NCG030251 To Whom It May Concern: In accordance with certificate of coverage referenced above and requirements of general permit number NCG030000 ("General Permit"), please find enclosed DMR for monitoring year 3, period 2, monthly monitoring (July, 2015) regarding Watts Regulator ("Watts") facility at 100 Watts Road in Spindale, North Carolina ("Facility"). Pursuant to February 3, 2010, Approval of Representative Outfall Status, Watts obtained quantitative data for samples at outfalls 001, 002, 004, and 006. Watts will continue monthly monitoring of these outfalls per the General Permit. In addition to required outfall sampling, Watts obtained "neat" samples at the Facility for pH. Consistent with footnote I of Table 3 in the General Permit, and the information enclosed with the Facility's previous DMR regarding natural pl-1 of precipitation in Spindale, on August 6, 2015, the Facility measured pH of three "neat" precipitation samples with the following results: At the Facility rain gauge — pH was 4.8; Within the north central portion of the Facility - pH was 4.7; and Adjacent to Gate A, within the southeast portion of the Facility — pH was 4.7. These results indicate the Facility pH benchmark should be in range of 4.7 or 4.8. Accordingly, pH measurements at outfalls 001 and 003 are within the appropriate applicable benchmark range. As requested in the August 10, 2015, cover letter for the January — June 2015 monitoring period DMR, [ would appreciate an opportunity to meet with representatives from the Division of Energy, Mineral, and Land Resources to discuss the results of a recent stormwater compliance audit at the Facility by AECOM and continuing efforts to implement additional stormwater best management practices ("BMP"). Please contact me at your earliest convenience by phone (978- 689-6070) or e-mail (howard.chu a watts.com) to arrange a date and time. Sincerely, / Q Howard H. Chu Director, Environment, Health and Safety Watts Water Technologies, Inc. Enclosures Watts Regulator Company Since 1874 watts.com aceAnalytical wwwpecelabs.cam July 28, 2015 One Time Client One Time Clients Private Small Jobs Huntersville, NC 28078 RE: Project: WATTS SPINDACE SW Pace Project No.: 92259490 Dear One Client: Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on July 15, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, �1, 0— -'`zb,---- Liamm Carrubba liamm.carrubba@pacelabs.com Project Manager Enclosures P, CR¢�� TNI REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 5aceAnalyticaI wwwpxelans.com Project: WATTS SPINDACE SW Pace Project No.: 92259490 Pace Analytical Services, Inc. 9800 IGncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #. 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 UrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 UrginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 14 aceAnalytical. www.pacelabs.com Project: WATTS SPINDACE SW Pace Project No.: 92259490 Lab ID Sample ID 92259490001 OU-001 92259490002 OU-002 92259490003 OU-004 92259490004 OU-006 92259490005 OU-003 92259490006 OU-005 92259490007 OU-007 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 1664E JMS 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D WRC 1 PASI-A EPA 9040 MLS 1 PASI-A EPA 1664B JMS 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D WRC 1 PASI-A EPA9040 MLS 1 PASI-A EPA 1664B JMS 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D WRC 1 PASI-A EPA 9040 MLS 1 PASI-A EPA 1664B JMS 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D WRC I PASI-A EPA 9040 MLS 1 PASI-A EPA 9040 MLS 1 PASI-A EPA9040 MLS 1 PASI-A EPA9040 MLS 1 PASI-A REPORT OF LABORATORY ANALYSIS This repots shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 aceAnalj4ical www.pacdabs.com ANALYTICAL RESULTS Project: WATTS SPINDACE SW Pace Project No.: 92259490 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OU-001 Lab ID: 92259490001 Collected: 07/14/15 08:51 Received: 07/15/15 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 07/21/15 14A5 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 876 ug1L 5.0 1 0712211519.00 0712711512:56 7440-50-8 Lead 107 ug/L 5.0 1 07/22/15 19:00 07/24/15 22:27 7439-92-1 Zinc 310 ug/L 10.0 1 07/22/15 19:00 07/24115 22:27 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 22.6 mg/L 5.0 1 07/21/15 22:36 D6 9040 pH Analytical Method: EPA 9040 pH 4.7 Std. Units 0.10 1 07/22/15 15:15 D6,H6 Sample: OU-002 Lab ID: 92259490002 Collected: 07114/15 08:55 Received: 07115/15 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 07/21/15 14:45 2D0.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 1370 ug1L 5.0 1 0712211519:00 0712711513:05 7440-50-8 Lead 173 ug1L 5.0 1 07/22/15 19:00 07/24/15 22:36 7439-92-1 Zinc 449 ug1L 10.0 1 07/22/15 19:00 07/24/15 22:36 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 75.5 mg1L 6.2 1 07/21/15 22:39 9040 pH Analytical Method: EPA 9040 pH 6.0 Std. Units 0.10 1 07/22/15 15:15 H6 Sample: OU-004 Lab ID: 92259490003 Collected: 07114N 5 09:02 Received: 07/15115 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 16645 Oil and Grease ND mg/L 5.0 1 07/21/15 14:45 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 234 ug/L 5.0 1 07/22/15 19:00 07/2711513:08 7440-50-8 Lead 12.5 ug/L 5.0 1 07/22/15 19:00 07124/15 22:39 7439-92-1 Zinc 204 ug1L 10.0 1 07/22/15 19.00 07124/15 22:39 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07128/2015 10:01 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 14 aceAnalytical www.pecelabs oo 1 ANALYTICAL RESULTS Project: WATTS SPINDACE SW Pace Project No.: 92259490 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 Sample: OU-004 'Lab lD: 92259490003 Collected: 07/14/15 09:02 Received: 07/15/15 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 16.9 mg/L 3.3 1 07/21/15 22:39 9040 pH Analytical Method: EPA 9040 pH 6.5 Std. Units 0.10 1 07/22/15 15:15 H6 Sample: Ott-006 Lab ID: 92259490004 Collected: 07/14/15 09:07 Received: 07/15/15 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 07/21/15 14:46 200.7 MET 1CP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 195 ug1L 5.0 1 07/2211519:00 07/27/1513:20 7440-50-8 Lead 19.8 ug1L 5.0 1 07/22/15 19:00 07/24/15 22:42 7439-92-1 Zinc 282 uglL 10.0 1 07t22115 19:00 07/24/15 22:42 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 18.4 mg1L 5.0 1 07/21/15 22:39 9040 pH Analytical Method: EPA 9040 pH 6.4 Std. Units 0.10 1 07/22/15 15:15 H6 Sample: OU-003 Lab ID: 92269490005 Collected: 07/14/15 09:12 Received: 07/15/15 09A5 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 9040 pH Analytical Method: EPA 9040 pH 5.8 Std. Units 0.10 1 07/22/15 15:15 1-16 Sample: OU-005 Lab ID: 92259490006 Collected: 07/14/15 09:20 Received: 07/15115 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 9040 pH Analytical Method: EPA 9040 pH 6.4 Std. Units 0.10 1 07/22/15 15:15 H6 Date:0712812015 10:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 14 aceAnalXical www.pacelabs.com ANALYTICAL RESULTS Pace Anatytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)87$-9092 Project: WATTS SPINDACE SW Pace Project No.: 92259490 Sample: OU-007 Lab ID: 92259490007 Collected: 07/14/15 09:24 Received: 07115115 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 9040 pH pH Date:0712MO15 10:01 AM Analytical Method: EPA 9040 6.4 Std. Units 0,10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 07122/15 15:15 Page 6 of 14 ace Analytical www.pacwabs.com QUALITY CONTROL DATA Project: WATTS SPINDACE SW Pace Project No.: 92259490 QC Batch: GCSV122022 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92259490001, 92259490002, 92259490003. 92259490004 METHOD BLANK: 1514532 Matrix: Water Associated Lab Samples: 92259490001, 92259490002, 92259490003, 92259490004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 5.0 07/21/15 14:41 LABORATORY CONTROL SAMPLE & LCSD: 1514533 Parameter Oil and Grease Units mg1L Pace Analytical Services, Inc. 9800 KinceyAve, Suite 100 Huntersville, NC 28078 (704)875-9092 1514534 Spike LCS LCSD LCS LCSD % Rec Max Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 40 36.2 35.9 90 90 78-114 1 30 Resutts presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/28/2015 10:01 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 14 laneA'nalytical' wwwpecefabs.com QUALITY CONTROL DATA Project: WATTS SPINDACE SW Pace Project No.: 92259490 QC Batch: MPRPI19060 Analysis Method: EPA 200.7 QC Batch Method: EPA200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92259490001. 92259490002, 92259490003, 92259490004 METHOD BLANK: 1515627 Matrix: Water Associated Lab Samples: 92259490001, 92259490002, 92259490003, 92259490004 Blank Reporting Parameter Units Result Limit Analyzed Copper ug1L ND 5.0 07/24/15 22:12 Lead ug1L ND 5.0 07/24/15 22:12 Zinc ug1L ND 10.0 07/24/15 22:12 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1515628 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 479 96 85-115 Lead ug/L 500 458 92 85-115 Zinc ug/L 500 459 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1515629 1515630 MS MSD 92259490001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 876 500 500 1380 1380 100 101 70-130 0 Lead ug/L 107 500 500 572 577 93 94 70-130 1 Zinc ug1L 310 500 500 774 779 93 94 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1515631 1515632 MS MSD 92259484001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 535 484 107 96 70-130 10 Lead ug/L ND 500 500 509 459 102 92 70-130 10 Zinc ug1L ND 500 500 511 462 102 92 70-130 10 Results presented an this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07128/2015 10:01 AM without the written consent of Pate Analytical Services, Inc.. Page 8 of 14 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: WATTS SPINDACE SW Pace Project No.: 92259490 QC Batch: WET138989 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92259490001, 92259490002, 92259490003, 92259490004 METHOD BLANK: 1515090 T Matrix: Water Associated Lab Samples: 92259490001, 92259490002, 92259490003, 92259494004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 07/21/15 22:36 LABORATORY CONTROL SAMPLE: 1515091 Spike LCS Parameter Units Conc. Result Total Suspended Solids mglL 250 266 SAMPLE DUPLICATE: 1515092 92259490001 ❑up Parameter Units Result Result Total Suspended Solids mglL 22.5 27.4 Pace Analytical Services, tnc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 106 90-110 RPD Qualifiers 19 D6 Results presented on this page are in the units indicated by the"Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/28/2015 10:01 AM without the written consent of pace Analytical Services, Inc.. Page 9 of 14 1ceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: WATTS SPINDACE SW Pace Project No.: 92259490 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 OC Batch: WET139011 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92259490001,92259490002,92259490003,92259490004,92259490005,92259490006,92259490007 SAMPLE DUPLICATE: 1515546 92259490001 Dup Parameter Units Result Result RPD Oualifiers PH Std. Units 4.7 4.5 3 D6,1-16 Results presented on this page are in the units indicated by the "Units- column except where an alternate unit Is presented to the right of the result. . REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/28/2015 10:01 AM without the written consent of pace Analytical Services, Inc.. Page 10 of 14 aceAnalytical www.pacelahs.com QUALIFIERS Project: WATTS SPINDACE SW Pace Project No.: 92259490 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL-Reporting Limit. Pace Analytical services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NG 28078 (704)875.9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA recommended holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/2812015 10:01 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14 aceAnalytical s wwwpacelabs.c= QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: WATTS SPINDACE SW Pace Project No.: 92259490 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92259490001 OU-001 EPA 1664E GCSV122022 92259490002 OU-002 EPA 1664E GCSV122022 92259490003 OU-004 EPA 1664E GCSV122022 92259490004 OU-006 EPA 1664E GCSV122022 92259490001 OU-001 EPA200.7 MPRP119060 EPA 200.7 92259490002 OU-002 EPA 200.7 MPRP119060 EPA 200.7 92259490003 01.1-004 EPA 200.7 MPRP119060 EPA200.7 92259490004 OU-006 EPA 200.7 MPRP119060 EPA 200.7 92259490001 OU-001 SM 25401) WET138989 92259490002 OU-002 SM 2540D WET138989 92259490003 OU-004 SM 2540D WET138989 92259490004 OU-006 SM 2540D WET138989 922594900011 OU-001 EPA 9040 WET139011 92259490002 OU-002 EPA 9040 WET139011 92259490003 OU-004 EPA 9040 WET139011 92259490004 OU-006 EPA 9040 WET139011 92259490006 OU-003 EPA 9040 WET139011 92259490006 OU-005 EPA 9040 WET139011 92259490007 OU-007 EPA 9040 WET139011 Date:.0712812015 10:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP117138 ICP117138 IC P117138 I C P117138 Page 12 of 14 / ✓�`7CQAraalytica! Sample Condition Upon Recell Document Number: F-CHR-CS-403-rev.16 Page 1 of 2k - Issuing Authority: Pace Huntersville Quality Office Client Name: Courier: ❑ Ox ❑ UPS❑ LISPS❑ Client❑��no f4 mercial❑ Pace Other Custody Seal on CoolerlBox Present: El yes Seals intact: ❑ yes Packing Material: ❑ Bubble VDp ❑ b e B s ❑ None❑ Other Thermometer Used: IR Gun T1401 Tvpo of Ice: /Wet Blue None Tema Correction Factor T1401 No Correction ' Page 2 of 2 is for Internal Use Only ❑ no Samples on ice, cooling process has begun V 'C Biological Tissue is Frozen: Yes N Biolo g � pate and Initlmining a f er a ta Corrected Cooler Temp.: contents: Temp should be above freezing to 6'C Comments: Ch:ain'of Cu . st6dy Present: Ye ONO ❑NIA 1, Chain of Custody ;gilled Out: 2<111 ONO ❑NIA 2. Chain of Custody Relinquished: s ©No ❑NIA 3, Sampler Name & Signature on COC: Y ❑No ❑NIA 4. Samples Arrived within Hold Time: Yes ❑No ❑NIA 5. Short Hold Time Analysis (<72hr): Dyes o NIA 6. Rush Turn Around Time Requested: ❑Y 0<0 ❑NIA 7. Sufficient Volume: dyx ONO ❑NIA 8. Correct Containers Used: ❑No ZY ❑NIA 9. -Pace Containers Used: ❑No ❑NIA Containers Intact: Yes ❑No DN/A, 10. Filtered volume received for Dissolved tests Dyes ❑No NIA 11. Sample Labels match COC: No ❑NIA 12, Cj -includes date/time![D/Anal sis Matrix: W All containers needing preservation have been checked. e ONO ❑wA 13. All containers needing preservation are found to be in ❑NIA compliance with EPA recommendation. compliance Z exceptions: VOA, co:itorm, TOC, O&G, Wl-DRO (water) ❑No Samples checked for dechlorination: Dyes No ❑tar 14. Headspace in VOA Vials ( >6mm): Dyes ONO Nly 15. Trip Blank Present: ©Yes ONO 12<1 ZNIA 16, Trip Blank Custody Seals Present ❑Yes ❑No Pace Trip'Blank Lot # if -purchased): ---- --- - — - - - -__------.--___---------.--T_.______ —_ —__-__-- Client Notification! Resolution: Field Data Required? Y ! N Person Contacted:'DatelTime: ��- _ �' �f j n Comments/Resolution: �_�,`�?,- Y�-�rt�(-�• ic.�_��s l•\i. SCURF Review: Date:` Place label here SRF Review: ��' Date: i JI i� Wp : 9225949Q Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form.will be sent to the North Carolina DEHNR �I I II I I��11 fII Certification Office ( I.e out of hold, Incorrect preservative, out of temp, I 11 11 II 11 incorrect containers) 92259490 Page 13 of 14 /,-s 2aceAna0cal' CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain•of-Custody i$ a LEGAL DOCUMENT, All relevant fields must be completed accurately. • wwrr.pacelass.com Section A Section B Section C Page; i of ff Required Client Information: Requirod Project Information: Invoice Information: Company+ 70: Attention: © 08 port £ctGfD.`. �V1y-r4I,VF1� T G � CL ` C a 1;4 Address; � �� r�i-.a 1 ` Copy S i Gf - To: Gall—L f/ Company Name: REGULATORY AGENCY l '1 r r�C t , �j �V t i 17 �,• Address: NPDES F- GROUND WATER ( DRINKING WATER UST RCRA r OTHER ' t TQj% r a Purchase V C 1 l� i�i r.' • �( �S.• ltri Order No.: Paco Quota Rolarorlw: `� F : 1' Prooct Name: Jr i f/¢ i Pape Proiact Site Location thr (1 %Y • {V ! i A4anagar. _w !7 & t Requested Due DateiTAT: Project Number: Paw Promo 0: Requested Analysis Filtered (YIN) Suction D Matrix Codes z Required Chant Informatan MATRIX J CODE o n COLLECTED Pmservarives >`- Drinking water nzrN Water WT WeWater U CO ComposnrE WART =JposrrE Cw.1 Produc! P SoilfSoGd SAMPLE ID oil OL wipe WP (A-Z, 0.91: ) Air AR v r- Z f t o Sample IDS MUST BE UNIQUE Tissue TS p L) a w as H I U Otner OT Lq a a U v_ �' O p = m` c r v — DATE TIME DATE TIME a 7 2 S X Z z O y- Pace Project NO.I Lab I.D. 1 OtA—. 00 1 141610 . 2 — 1 6 , l J� v �7 < 5 6 CO-- 003 1 ate I I I " i I I '7. -- Gas • E l yyC �y 9 10 11 112 ADDITIONAL COMMENTS REUN2= BX AFFILIATION DATE TIME CCEP7 BY FF LIATION DATE TIME SAMPLE CONDITIONS S 6� ORIGINALSAMPLER NAME AND SIGNATURE c oST Q a z ? PRINT Name of SAMPLER: �� �/j� y _ F tY " U a SIGNATURE of SAMPLER: DATE Signed IMM1DD": %� m ' mponenl Note. By signing this form you arc ace0;4ng Paw's NET 30 day payment terms and agreeing to lam charges of 1.5% pat month for any invoicps not paid wtnin 30 days. F-ALL-0-024rev.07. 15-Mav;1007 Semi-annual Stormwater Discharge Monitoring Report For North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 01/29/15 CERTIFICATE OF COVERAGE NO. NCG030251 FACILITY NAME Watts - Spindale COUNTY Rutherford PERSON COLLECTING SAMPLES Mark Kennard LABORATORY Pace Analytical Lab Cert. # 12, 5342, 37706 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' December (month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [:]WaterSupply ❑SA ®Other c 6" PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH*, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics$ Benchmarks =__> - - 100 mg/L or 50 mg/L4 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 12/22/15 1.31 <2.9 7.0 0.0500 <0.005 0.0732 <5.0 NA 2 12/22/15 1.31 <2.6 6.7 .0069 <0.005 0.0134 <5.0 NA 3 12/22/15 1.31 N/A 6.4 N/A N/A N/A N/A NA 4 12/22/15 1.31 <2.5 6.8 0.0448 <0.005 0.0797 <5.0 NA 5 12/22/15 1.31 N/A 6.9 N/A N/A N/A N/A N/A 6 12/22/15 1.31 <5.6 6.7 0.0161 1 <0.005 0.0669 <5.0 I NA 7 12/22/15 1.31 N/A 6.2 N/A N/A N/A N/A I N/A 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Stanley Aiken — Regional Engineer at the Ashville Regional Office Mail an original and one copy of this DMR includin all "No Discharge" reports, within 30 days of receipt oL the lab results or at end of monitoring eriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." I z5 a c, (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 %1kjWA1=M WATER TECHNOLOGIES January 29, 2016 BY CERTIFIED MAIL — RETURN RECEIPT REQUESTED Central Records Division of Energy, Mineral and Land Resources 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Discharge Monitoring Report and Notice of Compliance Status for Watts Water Technologies Facilitv located at 100 Watts Road, Spindale, North Carolina (Certificate of Coverage Number NCG030251) To Whom It May Concern: In accordance with the certificate of coverage referenced above and the requirements of general permit number NCG030000 (the "General Permit'), please find enclosed Watts Water Technologies ("Watts") discharge monitoring report ("DMR") for monitoring year 3, period 2 monthly monitoring (December 2015) regarding our facility located at 100 Watts Road in Spindale, North Carolina (the "Facility'). Consistent with the February 3, 2010 Approval of Representative Outfall Status, Watts obtained quantitative data for samples from outfalls 001, 002, 004 and 006. Based on the enclosed results reflected in the December 2015 DMR, these outfalls remain in Tier III status. In addition to the required outfall sampling, Watts obtained samples for PH from outfalls 003, 005 and 007. Those data are also reflected on the enclosed DMR.' Upon receiving the results of the July 2015 sampling, Watts engaged the consulting firm of Hart & Hickman ("H&H") to develop additional best management practices ("BMP") for the Facility. Given that all four of the monitored outfalls are in Tier III status, monthly monitoring data continues to be used to evaluate the effectiveness of these additional BMPs and the need for further improvements. Additional activities continued during the sampling period, and though the outfalls remain in Tier III status, analytical results continue to reflect improved analytical results. As mentioned in previous correspondence, a meeting was requested with representatives of the Division of Energy, Mineral and Land Resources to discuss results of a stormwater compliance audit performed and Watts' efforts to implement additional BMPs at the Facility. On January 27 h, we were pleased to host Darlene Kucken from the Asheville regional office who reviewed the site storm water program and toured the Facility. As part of the discussion, we reviewed data contained in documentation from H&H that was attached to recently submitted DMR reports, which included results of background ' As documented in the June 2015 DMR, the pH of precipitation in and around Spindale is commonly below the benchmark range in the General Permit. z Consistent with the February 3, 2010 Approval of Representative Outfall Status, the Facility did not sample outfalls 003, 005 or 007. sampling during the months of October and November 2015. In short, the data indicate copper and zinc present in the Facility's stormwater discharge likely originates from "non -industrial" sources — either the Facility's roof (which is not exposed to industrial operations) or the roadway adjacent to the Facility's stormwater outfalls. The results also suggest that the Facility's additional BMPs will resolve the recent results above the lead benchmark. These results confirm metals in the background samples with zinc and copper concentrations at similar levels to the outfall samples. Please contact me at (978) 689-6070 at your convenience if you have any questions. Sincerely, 141 " `' _ Howard H. Chu Director, Environment, Health and Safety Watts Water Technologies, Inc. Enclosures cc: Central Records, Division of Water Quality Semi-annual Stormwater Discharee Mo_nit_orin . Report for North Carolina Division of Water Quality General Permit No. NCG030000 CERTIFICATE OF COVERAGE NO. N00030 2 5 1 FAauTy NAME Waft-SWICUte COUNTY Rutherford PERSON COLLECTING SAMPLES iermftr VV W I URS LABORATORY Pace c8l Lab Cert. 0 Comments on sample collection or analysis: Date submitted 112116113 12.5342,37706 Part A. Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2014 SAMPLE PERIOD ❑ Jan -June ❑i♦ July -Dec or ❑ Monthly' _ , fmon[1 DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water supply ❑SA Mother C PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this periad e Outfali No. Date Sample , Collected" (mo/dd/yr) 24-hour rainfall amount, Inches' Total suspended Solids pH, standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons total Toxic Organics s genchmarks 1W mg/L or 50 mg/L 6.0 - 9.0 0.037 mg/L 0A3 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 /1'%r7 /1 A C, r I iaid i .s c-14,i, n V iS 002 - S µ �[ 4u r i r 004 S c - �vL r� ! Sc I Z 6F'1 006 Nv S� �c — 'e'v� m—f << ; J s�i sss /, 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the al] the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Mark Kennard Name (Print name) Environmental Health & Safety Title (Print title) /- 7 -/S (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection limit, BDL, cPQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX ma/L'. where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text Part 13: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. 0 No discharge this period?? Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 2664 (SGT-HEM) Total Suspended Solids pH Benchmarks Is mg/L 100 mg/L or 50 mg/L' 6.0 — 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B ' See General Permit text, Table 5, Identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:1111/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Nate: if you report a sample value In excess of the benchmark you must implement Tier 1, ner 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACIUTY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO pw IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mall an original and one co»v of this DMR. incluchl a!! "No Discharge" reoorts. wlthln 0 days of recelat of the lob results for at end of monitoring period In the case of "No Discharge" resorts! to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible forgathering the Information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and Imprisonment for knowing violations." (Signature of Permitteef /- 7 -/S (Date) Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 January 7, 2015 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Semi -Annual Discharge Monitoring Report Submittal for July - December 2014 Watts Regulator- Spindale Facility, 100 Watts Drive, Spindale, NC Storm Water Permit COC Number NCG030251 Dear Division of Water Quality, As required by the referenced Storm Water Permit Certificate of Coverage, please find enclosed the original and one copy of the semi-annual storm water Discharge Monitoring Report (DMR) for the referenced facility. This DMR is being submitted by URS Corporation on behalf of Watts Regulator as the following sample designated in Table 2 of the permit: Year 2 - Period 2 Sample #14 July 1, 2014 - December 30, 2014 Due to insufficient rainfall during sampling hours and insufficient dry periods between rainfalls, no sampling was completed during this period. Please call me at (704) 716-0737 if you have any questions or if you need any additional information. Sincerel , J ifer Wheat Environmental Scientist, URS, Corporation Enclosures URS Corporation — North Carolina 6000 Fairview Road, Suite 200 Charlotte, North Carolina 28210 (704) 522-0330 Phone (704) 522-0063 Fax RECEIVED JAN 12 ?01,9 CENTRAL FILES DWR SECTION Semi-annual Storm_water Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No, NCGO30000 Date submitted 112118113 CERTIFICATE OF COVERAGE NO. NCG03 0 2 5 1 FACILITY NAME watts - spindale COUNTY Rutherford PERSON COLLECTING SAMPLES Jennifer wheat 1 uRs LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2014 SAMPLE PERIOD ■❑ Jan -June ❑ July -Dec or ❑ Monthly' month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []zero -flow []Water Supply [—]SA NOther C PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 X No dischorge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids PH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic nrganlcss Benchmarks 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 002 004 006 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. -'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Mark Kennard Name (Print name) Environmental Health & Safety Title (Print title) w - (5ignature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?? Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, lnches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ==-a _ - 15 mg/L 100 mg/L or 50 mg/L' 6.0 - 9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B ' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: ■ A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART It SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALLTRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO FNI IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copy of this DMR, includina all "No Discharge" reports, within 30 days of receipt of the lob results for at end of monitoring period in the case of Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." WW4-1- X� (Signature of Permittee) Permit Date: 11/1/2012-10/31/2017 8 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 W_ Oj� August 26, 2014 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RECEIVED AUG 282014 CENTRAL FILES DWQIBOG Subject: Semi -Annual Discharge Monitoring Report Submittal for January — June 2014 Watts Regulator — Spindale Facility, 100 Watts Drive, Spindale, NC Storm Water Permit COC Number NCG030251 Dear Division of Water Quality, As required by the referenced Storm Water Permit Certificate of Coverage, please find enclosed the original and one copy of the semi-annual storm water Discharge Monitoring Report (DMR) for the referenced facility. This DMR is being submitted by URS Corporation on behalf of Watts Regulator as the following sample designated in Table 2 of the permit: Year 2 — Period 1 Sample #13 January 1, 2014 — June 30, 2014 The sampling for Year 2 -- Period 1 did not occur due to lack of rainfall during sampling hours. No sample was able to be taken and results therefor were not available. Additionally, a Request for Rescission was submitted to the State of North Carolina on June 6, 2014. A decision on the request has yet to be determined. With appropriate rainfall during the sampling hours of Year 2 — Period 2, sampling will occur to remain in compliance with the current stormwater permit. Please call me at (704) 716-0768 if you have any questions or if you need any additional information. Sincerely, Mike Fulkerson Sr. Environmental Scientist, URS Corporation Enclosures URS Corporation — North Carolina 6000 Fairview Road; Suite 200 Charlotte, North Carolina 28210 (704) 522-0330 Phone (704) 522-0063 Fax STOR111WATP-It DISCIIARGE OUTFALL (SDO) MONITORING REPORT GENLRAL PERM[T NO. NCG030000 SAfiMPLLS COLLECTED DURING CALENDAR YEAR: April 2011) CERTIFICATE OF COVERAGE NO. NCG030251 This monitoring report is ducat the Division no later than 30 clays from FACILITI' NAME Watts Reyulalor—Spindale Facility the date the facility receives the sampling results from the Ltburatory.) PLRSON COLLECTING SAN11'LLS Lanette Small — URS Corporation CER'TIFILD I.,AROI2ATOltY: Pace Analytical Services—Aslreyille Lab #40 113110Nl: NO. (828) 286-4115 Part A: Specific Monilorina Requirements Otntfall No. Date Sample Collected, mokldlyr 00530 (10400 01051 110556 78141 Total Suspended Solids, mg/L Jill, Standard units Lead, nigh, Oil and Grease, mg,/L Total Toxic Organics', mglL Benchmark - 100 Within 6.0-9.0 0.033 30 1 001 04/20/2010 NIA' NIA' 0.144 N/AZ NIA" 002 04/20/2010 NIA' Not Sam tled3 (1.068 NIA' NIA'" 003 Not Sam pled NIA" Not Sampled-' NIA- NIA" NIA" C�� a p. ..r r. Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark ranee for pH, you must implement "Pier I. or Tier 2 responses. See General Permit text. No chemicals on the Total "Toxic Organic (1-1-0) list are used at the facility, and none have been used during the past 3 years. Therefore. the Solvent Management t at the facility consists ol'a certification that the chemicals are not used at the facility. As a result, TTO monitoring is not required based on the waiver contained in the stormywater-n permit. 2 Per Tier 2 sampling analysis guidance received from Chuck Cranford of the NCDENR DWQ Regional Office during his site visit on Tuesday, November 17, 2009, only s lilple parameters affected by a Tier 2 response require monthly analysis. Per Tier 2 pl-! sampling guidance received from Chuck Cranford of the NCDENR DWQ Regional Office via email dated 12/14/2009, samples for pH will not be collected on a monthly basis. Samples for pH will only be collected during the semi-annual events along with "neat" rain samples for pH. S .' w—isy?���r.�.Kl�,;,•,�:7+.,:�.�1:..�µ.: _.-_ r_.r? . Y;��-t,,. Did this facility perform Vehicle i\4aintenance Activities using more than 55 gallons of new motor oi] per month? _yes X no #°' �- (if yes, complete Part B) Part B: Vehicle Maintenance Activity i lonitoring Requirements 3 Outfall Nu. Date Sample Collected, rnnolcidlvr 00556 00530 00400 s t I 11 LL= L Oil and Grease, m-,/L Total Suspended Solids, m g/L pill, Standard units New Minor bi IT- age' Annual avera.(fe a[/mn Benchmark - 30 1011 6.0-9.11 lu U ( f =P 3 Q 2010 _.I QUALIT�SF-CTION i Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for PH, you must implement Tier I or Tie 2 resp� 6n s�LE REGIONAi OFFICE ;r;r See General Permit text. y l STORM EVENT CHARACTERISTICS: flail Original and one-c(ijij" to: Division of Water Quality Date: 04/20/2010 (first event sampled) _ Attn: D1N'Q Central Files Total Event Precipitation (inches): 0.28 1617 Mail Service Centel - Date (list each additional event sampled this reporting period, and rainfall amount) Raleigh, North Carolina 27699-1617 Total Event Precipitation (inches): SWU-245-031308 Page 1 oC2 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EMPA Effluent Guidelines for the facility subject to the requirement to sample (for moral Cnishin; use the definition as found in 40 CFR 43,.1 I; for semiconductor manufacture use the definition as found in 40 C_FR 469.12: for electronic crystal manufacture use the definition as found in 40 CM 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention I'lan may so certify, and the requirement for TI'O monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilitics electing to employ the Tf0 monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry ol'the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics ("lTO), I certify that to the best of my knowledge and belief, no dumping of concentrtued toxic organics into the storntwater or areas which are exposed to rainfall or stormwaler runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management Plan included in the Storinwater Pollution Prevention Plan." Ken Ledoux Safety & Environmental Manager �_L 64� SaIvy— �5- (Signature) (Date) "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based tin my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 ant aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." clp� <I -t Z-/D (Signature ol-Pcrmittee) (Date) SWIJ-245-031308 Page 2 of 2 May 3, 2010 Division of Water Quality Attn: DWW1Q Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Tier 11 Response Monthly Disc harge,Monitoring Report Submittal for April 2010 Watts Regulator — Spindale Facility, 100 Watts Drive, Spindale, NC Storm Water Permit COC Number NCG030251 Dear Division of Water Quality, Based on the analytical results for the Year 1-Period I and Period 2 samples for pH and lead at Outfall 002 and pH at Outfall 003, the Watts Regulator-Spindale Facility proceeded to the Tier 2 response actions required by the North Carolina General Industrial Storm Water Permit NCG030000 under the referenced Storm Water Permit Certificate of Coverage for these outfalls. In addition. based on the analytical results for the Year 2-Period 1 and Period 2 samples for lead at Outfall 001 the facility proceeded to the Tier 2 response actions required at this outlali. Please find attached the original and one copy of the required April 2010 Discharge Monitoring Report (DMR) for the Tier 2 lead sampling at Outfalls 001 and 002. Based on Tier 2 pH sampling "uidance provided by Chuck Cranford via email received on 12/14/2009, pl-I sampling is only collected as normal during the semi-annual sampling events but not on a monthly basis as part of the Tier 2 sampling. The DMR also indicates NA for all other test parameters at these outfalls based on the Tier 2 sampling analysis guidance provided by Chuck Cranford of the NCDENR DWQ Regional office during his site visit on 'I'uesdav, November 17, 2009. and confirmed via email received 12/14/2009. This DMR is being submitted by URS Corporation on behalfof Watts Regulator. Please call me at (704) 716-0765 if'you have any questions or if you need any additional information. Sincerelv, Lanette Small Environmental Scientist. URS Corporation ItinCIOSures URS Corporation — North Carolina 6135 Park South Drive, Suite 300 Charlotte, North Carolina 28210 (704) 522-0330 Phone (704) 522-0063 Fax GENERAL PERMIT NO. NCG030000 CERTIFICATE? OF COVERAGE -NO. NCC030251 FACI Ll'I'Y NAME N1`atts_R gnktor-SpindaEe_Facility PERSON COLLECTING SAMPLES N/A CERTIFIED LABORATORY: NIA Part A: Specific Monitorint` Requirements STOICNINVATER DISCHARGE OUTFALL (SDO) MONITORING REPORT SAMPLES COLLECTED DURING CALENDAR YEAR: August 2010 '['his monitoring report is due at the Division no later than 30 days front the date the facility receives the sampling results from the laboratory.) PIIONE NO. (828) 286-4115 Outfitll No. Date Sample"Total Collected, m old dIy r 00530 00400 01051 00556 78 ,4'l Suspended Solids, mg/L pll, Standard units Lead, mg/L Oil and Crease, nig/L Total'l;oxic Organicsr, mg/I, Benchmark - 100 Wit hm 6.0-9.I1 0.033 30 1 001 Ariust 2010 N/A= N/A' No blow N/A- N/A' 002 1 August 2010 N/A" Not Sant fled No Flow NIA- N/AZ 003 August 2010 NIA'" Not Sampled' NIA' N/A" NIA- Nute: I f you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must -implement Tier- 1 or Tier 2 responses. � rI See General Permit teat. U ' No chemicals on the Total Toxic Organic (T'1-0) list are used at the facility, and none have been used during the past 3 years. Therefore, the Solvent Management Phtt) at the facility consists of a certification that the chemicals are not used at the facility. As a result, TTO monitoring is not required based on the waiver contained in the storiii'Mter permit. ` Per Tier 2 sampling analysis guidance received front Chuck Cranford of the NCDENR DWQ Regional Office during his site visit on "Tuesday, November 17, 2009,WMi ly sample �mrameters affected by a Tier 2 response require monthly analysis. Per Tier 2 pH sampling guidance received front Chuck Cranford of the NCDENR DWQ Regional Office via email dated 12/14/2009, samples for pH will not be collected o a monthly basis. Samples for pH will only be collected during the semi-annual events along with "neat' rain samples for pl-I. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes \ no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitorinp_ Requirements Outfall No. Date Sample Collected, mo/dd/yr 00556 00530 00400 Oil and Grease, m g/L Total Suspended Solids, mg/L pill, Standard units New Motor Oil Usage, Annual average gal/moI Benchmark - 30 100 6.0-9.0 - �t 1 Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier l or Tier 2 responses See General Permit text. STORM FVE'NT CIIARACTEIII S['ICS: Date: N/A (first event sampled) Total Event Precipitation (inches): N/A [)are (list each additional event sampled this reporting period, and rainfall antnunt) Total Event Precipitation (inches): Mail Original and one copy to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh. North Carolina 27699-1617 SWU-245-031308 Page l of 2 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, nuulufactLire semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the FPA Effluent GL1ideli11CS for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 4 33.1 1; for semlCondnetor 111anUfaClLlre L1Se the definition as fOLnld in 40 CFR 469. 12, for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Facilities that incorporate a solvent management plan into the Stonmrvater Pollution Prevention Plan nlay so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the 170 monitoring waiver, the discharger shall sign the following certification statement: "Based upon Illy inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the storniwatcr or areas which are exposed to rainfall or siormwater runoff has occurred since filing the last discharge monitoring report. l further certify that this facility is implementing the all tine provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Ken Ledoux Safety & Environmental Manager (Sign lure) (Date} w"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature. of Yermittee) (Date) SWU-245-03 t 308 Page 2 of 2 ff1'v 4pw a aA September 9, 2010 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Tier II Response Monthly Discharge Monitoring Report Submittal for August 2010 Watts Regulator — Spindale Facility, 100 Watts Drive, Spindale, NC Storm Water Permit COC Number NCG030251 Dear Division of Water Quality, Based on the analytical results for the Year 1-Period 1 and Period 2 sam pies for pH and lead at Outfall 002 and pH at Outfall 003, the Watts Regulator-Spindale Facility proceeded to the Tier 2 response actions required by the North Carolina General Industrial Storm Water Permit NCG030000 under the referenced Storm Water Permit Certificate of Coverage for these outfalls. In addition, based on the analytical results for the Year 2-Period 1 and Period 2 samples for lead at Outfall 001 the facility proceeded to the Tier 2 response actions required at this outf all. The sporadic and unpredictable nature of summertime thunderstorms in the Spindale, North Carolina, area has resulted in no available sampling opportunities during a representative storm event for the month. Please find attached the original and one copy of the required August 2010 Discharge Monitoring Report (DM R) for Outfalls 001, 002 and 003 indicati ng no flow for the Tier 2 lead sampling at Outfalls 001 and 002 and indicati ng not sampled for the Tier 2 pH sampling at Outfalls 002 and 003 based on Tier 2 pH sampling guidance provided by Chuck Cranford via email received on 12/14/2009. Per this guidance Mr. Cranford indicated that pH samples should be collected as normal during the semi-annual sampling events bu monthly basis as part of the Tier 2 sampling. The DMR also indicates NA for all other test parameters at ese o—u—Ta is based on the ier sampling analysis guidance provided by Chuck Cranford of the NCDENR DWQ Regional office during his site visit on Tuesday, November 17, 2009, and confirmed via email received 12/14/2009. This DMR is being submitted by URS Corporation on behalf of Watts Regulator. Please call me at (704) 716-0765 if you have any questions or if you need any additional information, Sincerely, .��rL;'fi.i_�.i 9 (-%Y - '•�"r'�L r�_ij �d-. Lanette Small Environmental Scientist, URS Corporation Enclosures URS Corporation — North Carolina 6135 Park South Drive, Suite 300 Charlotte, North Carolina 28210 (704) 522-0330 Phone (704) 522-0063 Fax - OCT -72010 U i GENERAL PERAIIT NO. NCG030000 CERTIFICATE Oh COVERAGE NO. NCG030251 FACILITY NAME 11'aus Rc�ulator—Snindale hacility PERSON COLLECTING SAMPLES N/A CERTIFIED LABORATOR)': N/A Part A: Specific Alooitorin g Re+ t iremenls S•I.ORi111YATER DISCHARGE OUTFALL (SDO) :MONITORING REPORT SAMPLES COLLECTED DURING CALENDAR TEAR: Jttly 2010 This nionitlu•inb r'cport is duc at the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) PIIONE NO. _(828) 286-41 I-S Outfall No. Date Sample Collected, mo/dd/yr 00530 00400 01051 00556 78141 Total Suspended Solids, nig/L 1)11, Standard unit+ Lead, nag/L Oil and Grease, mg/L Total Toxic Organicsl, nu4/L Benchmark - 100 11'ithin 6.0 — 9.0 0.033 30 1 001 July 2010 N/A N/A- No Flow N/A� N/A- 002 Jtily 2010 NIA' Not Sampled-' No Ploy NIA' N/A' 003 Juh, 2010 N/A.Not Sant fled Nh1' NIA' N/A' Note: Ifyou report a sampled value in excess of the benchmark value, or Outside the benchmark ran-c IOr pH, y'OLI Must II1lplCment Tier I Or -Tier 2 responses. i . See General Permit text. 1 No chertticals on the Total Toxic Organic (TTO) list are used at the facility, and none have been used during the past 3 years. "Therefore, the Solvent Mana+-entcn�Plan at the facility consists of a certification that the chemicals are not used at the facility. As a result, TTO rnonitorin" is not required !rased on the waiver contained in the stoint water vermit. Per Tier 2 sampling analysis guidance received from Chuck Cranford of the NICDENR D\VQ Regional Office during his site visit on Tuesday, November 17,260�, only sample )arameters affected by a Tier 2 response require monthly :analysis. — Per Tier 2 pH sampling guidance received from Chuck Cranford of the NCDLNR DWQ regional Office ice via email dated 12/14/2009. samples for pi -I will not be collected on a monthly basis. Samples for pH will only be collected during the semi-annual events along wills "neat" rain samples for pH. Did this facility perform Vehicle Nlaintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Nl01Lit0r•i1lg RNquirements Outfall No. Date Sample Collected, mo/dd/ yr 00.556 00530 00400 Oil and Grease, nig/L Total Suspended Solids, ni /L Jill, Standard units New Motor Oil Usage, Annual average gal/lno Benchmark - 30 100 6.0 — 9.0 - Note: Ifyou report a sampled value in excess of the benchmark value, or outside the benchmark ranee fbr pH, you Must intplentcnt Tier 1 or'Ticr ?responses. See General Permit text. STORM EVENT Cl1ARACTERISTICS: Date: N/A (first event sampled) TWA Eve11t Precipitation (inches): NIA Date (list each additional event sarnpled this reporting period, and rainfall anuutnt) Total Event Precipitation (inches): Mail Original and one copy to: Division of Water Quality Attn: D11'O Central Files 1617 Mail Service Center Raleigh, North Carolina 27099-1017 S%VU-245-031305 Page I of'' Total Toxic OI'ga111C5 saltll)ltll, i5 a])])11CalIlC 011l)' for those faCllttlC5 which perform metal finishing operations, MaIlUfaCWIT semiconductors, nlanulacture electronic Cl- s'S sls, ar manufacture cathode ray tubes. For ptn'poses of this permit the definition of Total Toxic Organics is that definition contained ill the EPA Efllucllt GUIdCliile5 for the facility subject to the requirement to sample (for metal finishing use the definition 115 fOtlIId i t 1 40 CFR 433.1 1; for setlllCOMIIICIOI' IllatlUfaCltlre use the defirlitiotl as found in 40 CFR 469.11 for electronic crystal mallufacture use the definition as found in 40 CFR 469.22: and for cathode ray tube mallufacture rise the definition FOliild ill 40 CFR 469.31). Facilities that incorporate a solvent num:[gentent plan into the StormH'ater I'ullutforl PrCVCmtion Plan may so certify, and the requirement for "1TT0 111011il06lh may be waived. The solvent ntana.-emcia plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electiii- to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: • "fused upon my inquiry of the person or persons directly responsible for managing compliance with the ])errnit nlorlitorimg requiremem for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no duulping of concentrated toxic organics into the stOn wvater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. l further certify that this facility is implementing the all the provisions of the solvent man, enlerlt plan included in the Stormwater Pollution Prevention Plan." Ken Ledous Safety & EmVil-011111e11[al Manager < L-,-N �/ �- L, &--� 7 (Signature (Date) "I certify, under penalty of law, that this document mid all aitachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly bather and evaluate the information submitted. Based on my inquiry of the person or persons who niffll.t(;e tltc system, or those persons directly responsible for gathering (lie information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of Fines and imprisonment for kttt►wint, violations." % D (Signatu fermi c)' (Uatc) SNVU-245-0 130S Page 2 of 2 i JLrly 29, 2010 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Tier 11 Response Monthly Discharge Nlonitoring Report Submittal for July 2010 Watts Regulator — Spindale Facility, 100 Watts Drive, Spindale, NC Storm Water Permit COC Number NCG030251 Dear Division of Water Quality. Based on the analytical results for the Year 1-Period I and Period 2 samples for pH and lead at Outfall 002 and pl-I at Outfall 003, the Watts Regulator-Spindale l'acility proceeded to the Tier 2 response actions required by the North Carolina General Industrial Storm Water Permit NCG030000 under the referenced Storm Water Permit Certificate of-Coverar-e for these outfalls. In addition, based on the analytical results for the Year 2-Period 1 and Period 2 samples for lead at Outfall 001 the facility proceeded to the Tier 2 response actions required at this oLutfall. The sporadic and unpredictable nature of SLIillmertime thunderstorms in the Spindale, North Carolina, area has resulted in no available sampling opportunities during a representative storm event for the month. Please find attached the original and one copy of the required July 2010 Discharge Monitorim, Report (DMR) for OLltfalls 001, 002 and 003 indicating no flow for the Tier 2 lead sampling at Outfalls 001 and 002 due to the lack of a representative storm event during reasonable operating flours for the month of March and indicating not sampled Ior the Tier 2 pl-I sampling at Outfalls 002 and 003 based on Tier 2 pFl sampling guidance provided by Chuck Cranford via email received on 12/1 1/2009. Per this guidance Mr. Cranford indicated that PH samples should be collected as normal during the semi-annual sampling events but not on a monthly basis as part of the Tier 2 sampling. -rile DMR also indicates NA for all other test parameters at these outfalls based on the Tier 2 sampling analysis guidance provided by Chuck Cranford of the NCDENR DWQ Regional office during his site visit on Tuesday. November 17, 2009, and confirmed via email received 12/14/2009. This DMR is being, submitted by URS Corporation on behalf of Watts Regulator. Please call me at (704) 716-0765 ifyou have any questions or ifyou need any additional information. Sincerely, I_anette Small Environmental Scientist, URS Corporation Enclosures URS Corporation — North Carolina 6135 Park South Drive, Suite 300 Charlotte, North Carolina 28210 (704) 522-0330 Phone (704) 522-0063 Fax