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HomeMy WebLinkAboutNCG030042_MONITORING INFO_20181205STORMWATER DIVISION CODING SHEET NCG PERMITS . PERMIT NO. V 03 �� a DOC TYPE ❑ HISTORICAL FILE Pr- MONITORING REPORTS DOC DATE ❑ o lg to � YYYYMMDD Rick Flickinger Manager -Equipment Reliability T 336-495-2625 M 336-465-1127 rick.flickinger@timken.com December 5, 2018 NC Dept. of Environmental, Health, and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Central Files Please find enclosed the following: O The original and one copy of the Semi -Annual Stormwater Discharge Monitoring Report O Two copies of the actual test results from Research & AnaIytical Laboratories, Inc. For this sampling period, all levels are below the benchmark thresholds. We completed the Tier 1 investigation after the Springtime sampling and were unable to determine any assignable root causes for the Zinc and Copper levels to exceed the threshold values at Outfall 001 and 003 respectively. If you need.any additional information, please do not hesitate to contact me at (336) 495-2625, or you may send inquiries to the following address: Rick Flickinger The Timken Company 3500 Timken Place Randleman, NC 27317 Sincerely, Rick Flickinge Manager -Equipment Reliability Stronger.Commitment. Stronger. Value. Stronger. Worldwide. Stronger. Together. I Stronger. By Design. The Timken Company Mail Code: ASB-01 4500 Mount Pleasant St. NW North Canton, OH 44720 ov Semi-annual StormwaterOchar a Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted _l z/S_ /Z0' e CERTIFICATE OF COVERAGE NO. NCG03 d f.a 4 'Z FACILITY NAME Tl mr cz&J_ AsF� 'L�U(Lu„ PI ArJ � COUNTY P PERSON COLLECTING SAMPLES LABORATORY'�' -: A- '- � 6 5 Lab Cert. # '3 " J-77 0 ) Comments on sample collection or analysis: Part A: Stormwater Benchmarks.and Monitoring Results SAMPLE COLLECTION YEAR z c ( 8 SAMPLE PERIOD ❑ Jan -June July -Dec RECEte/tzr) or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA DEC 13 20 jg ❑Zero -flow NWater Supply ❑SA CENTRAL FILEES ❑Other DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks ===> + - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L) 0.03 mg 0.067 mg/Lf 15 mg/L 1 mg/L 1[�,' I, Z /'�i L �f 4�noS !L -C�00S 1L oSLo !L "�M l_. — /C[7� V i f, E i 1 Z 1 �J 7� 5r %�/S �P� �P /%j' L C70 )L :CO.57" ✓;., 51 : C7i }J 1, rJ ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. S Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." 1' I cl-- L vc �_1 ro S L R- Name (Print name) rF?'� �/u !� � L—`�, — +� � V_ �Gh'1 �►�' l (fit :l..t i�- f5! t< 1 T� Title (Print title) I Z Z�I (Signature) ( ate) Note: Results must be reported.in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "_<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc -An mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit D- 1/1/2012-10/31/2017 SWU-245, last reviser' ''2-5/201-2 1 Page 2of3 "', Note: 10report a sample value in excess of the benchmark, you must irk Rent Tier 1, Tier 2, or Tier 3 responses. See General Permit text•..., .: FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copv of this DMR. includina all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorina period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 MDORESEA.RCh&ANA1YTiCA1 Report of Analysis LA ORAT®RiESFINC. 11/27/2018 t�ttlttflf�t., . ��., For: Timken �,�C► • Y��� 3500 Timken Place Randleman, NC 27317 : ° o inId NC #34 . u7 Z" ,. Attn: Rick Flickinger = NC #37701 Client Sample ID: Outfall 001 Lab Sample ID: 59064-01 Site: Timken Collection Date: 11/12/2018 10:35 Parameter Method Result Units Rep Limit Analyst Analysis_DatelTime Copper, Total EPA 2M7 <0.005 mg1L 0.005 JF 1111512018 Hydrocarbon O&G EPA 1664 Revision Milica Gel <5 mg/L 5 EE 11/1912018 Lead, Total EPA 200.7 50.005 mg1L 0.005 JF 11/15I2018 pH SM 4500 H+15-2000 6.91 Std. Units 11/12/2018 1035 Temperature (Thermometric) SM 2550B 10.4 °C 11/12/2018 1035 Total Suspended Solids (TSS) SM 2540 D-1997 <5 mg/L 5 AW 11/16/2018 Zinc, Total EPA 200.7 0,056 mg1L 0.01 JF 11/1612018 Client Sample ID: Outfall 003 Lab Sample ID: 59064-02 Site: Timken Collection bate: 11/12/2018 10:37 Parameter Method Result Units Rep Limit Analyst Analysis DatelTime Copper, Total EPA 200.7 <0.005 mg/L 0,005 JF 11/15/2018 Hydrocarbon O&G EPA 1664 Revision B/Silica Gel <5 mg/L 5 EE 11/19/2018 Lead, Total EPA 200.7 <0.005 mg/L 0.005 JF 11/15/2018 pH SM 4500 H+B-2000 7.15 Std. Units 11/12/2018 1037 Temperature (Thermometric) SM 25508 10.5 °C 11/12/2018 1037 l F Total Suspended Solids (TSS) SM 2540 D-1997 6.6 mg/L 5 AW 11/16/2018 Zinc, Total EPA 2007 .0.013 mglL 0.01 JF 11/15/2018 NA = not onolyzed P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: 336-996-2841 Fax: 336-996.0326? w,nweandaiabs.com Page t ral coa basie vid RESEARCh & ANA1yTfCA1 L-AboRATORIES� :INC. Analytical / Process Consultations Prone (336) 996-2841 CHAIN OF CUSTODY RECORD WATER I WASTEWATER misc. COMPANY '71 Cu m n+ JOB NO, WGj• a i z a� Co o' D' Q@ �� s ��� , J qi Q—N '� �• `r Q t� �� �� G1 +.`a O Q_ Ga 2P �O Ca �' c� UOGti V� ryv ti4 ryyo ry� ^� a" ti`� ." yP REQUESTED ANALYSIS STREETADDRESS 3500 70)(LE0 9(-AEG PROJECT F"qr- zacb S-t,: S A L..0 CITY, STATE, ZIP 3.36 _ �{`1S = Ze ZS rTLCi 1W .NC: Z73 SAMPLER NAME (PLEASE PRINT) I CK -LtC ti d CONTACT CC.ZI PHONE SAMPLER SIGNATURE SAMPLENUMBER (LAB USE pNLY� DATE TIME COMP GRAB TEMP .0 RFS 123 c�lOmAE pr�ovNxla WME (saw) SA E LOCATION f LD. 73 ✓ /�, CDC-- ' C:�-. f—F 0, PH _ LLry i'ti1r�l� i C� • Y � G r N G C. 5c3, 9 SS D c) OUT Fr'+ t— -7, ISM ^l:wl.Q Ja,� ` G �> of C_ C -To, Y` F � SS f RELINQUISHED BY DATEmME RECEIVED B REMARKS: SAMPLE TEMPERATURE AT RECEIPT 2 °C RELINQUI BY DATEMME ISM RI5CEIKD BY m nISE"ARCh 6 AN�A�y����4� A�riat �sis Re port .of y 0.. 6•��CN.�'TrrC+'•. For: Tirnkeri +. •� ' 3500 Timkkn Place :'� + • Randlern4h, 27317 ,� ""Co, o• cn ;NC .Co, -'NC Z� w Attn: Rick Flickinger NCMf 77M 5. . Client Sample ID: Outfall 001 Lab Sample ID: 59064-01 Site: Timken. Collection Date: 1111212018 10:35 - Parameter ; . , _ Method Result 'Units - Rep Limit Anal st ArialysisDatelTirhe - Copper, Total EPA 200,7 <0.005 rng1L 0.005 JF 1Ill 512018 Hydrocarbon O&G EPA 1664 Revision B/Silica Gel <5 mg/L 5 EE 11119/2018 Lead, Total EPA 200.7 <_0.005 mg/L 0.005 JF 11/1512018 pH SM 4500 H+13-2000 6,91 Std. Units 11112/2018 1035 Temperatu7e (Thermometric) SM 2550B 10.4 'C 11/12/2018 1035 Total Suspended Solids (TSS) SM 2540 D-1997 <5 mg/L 5 AW 11116/2016 Zinc, Total EPA 200.7 ao56 mglL 6.01 JF 1 ill 5/2018 Client Sample ID: Site: Outfall 003 - Timken Lai; Sample,]D: Collection Date: 59064<02 1*1/12/2018 10:37 Parameter - , ,Method Result units Rep Limit Analyst Analysis Date/Time Copper,'Total EPA 200.7 4005� mg1L 0.005 JF 11/15/2018' Hydrocarbon O&G EPA-1664 Revision'$/Silica Gel <5 rnglL 5 EE 11/19/2018 Lead, Total EPA.200.7 <0,005 mg/L 0,005 JF 11115/201 a PH SM 4500 H+B-2000 7.15 Std. Units 11/12/201'8 1037 temp&bture (Thermometric) SM 2550B 10.5 °C: 11/12/2018 037 . 1 Total Suspended Solids JSS) SM-2540 D-1997 6.6 mg/L 5 AW 11116/2618. 1 Zinc; Total EPA 200.7 .0.013 mglL 0A1 JF 11115/2018 i _ N.A = not analyzed I - P.C). 86X473 166 S15ori Street Kerneisville;-North CaToRn, 2 2284 Tel: 336-996-2BQ1 Fax:336-996-0326 www.randalabs.com��� Rage 1 i ra'._coa_basic_Od i • CHAIN `OF.CUSTQDX RECORD, '�AboRAT�RIES, TNC.. Analytical /`'•�P.rot�cess,Consultations �P,hone,(36)=9`�6=284.1 � WATER 1WASTEWATEi2 t, 'r 'MISC.- COMPANY.• JOS'NO. ' r,rn cy Cu Z� O, . STREET ADDR ESS. PROJECT - 3s00 7C:.lu S'i.,;. s C-C: c� 41 } CITY; STATE -ZIP 'u. • 3 3CA- f j Z5 SAMPLER NAME �eLEASE PRINT) [- oC[:'07AIJ' NC' �-73 I CIK • •-L:Lc A,) w z T' OpG t� CONTACT PHONE SAMPLER SIGNATURE Cc'2` a Op Ica Up C9 r lcsL;fi=c�:� k+N4c:,t� o x o Q• `� ti ryho 'Y �" .h '" .� �" ��Q REQUESTED:ANALYSIS' SAMPLE NUM[!ER DATE TIME; C09PGRU TEMP °C ass- c 1401 i- +rc+.ioY¢o`, snNitie wwrwx SAh ELOCAiIQNlI.D. (LABU5E0NLY� (zi fYaN) Isam� . 03 S` rl�zl� 3j 0VTFts L Coves i� C 50, CC F O h- RELIiJQUl5HED BY DATELfIh1E REGEiVED 6 r REMARKS: RELINQUISHED.By DATEMME' RECE D BY j ISM ! SAMPLE TEMPERATURE AT RECEIPT Lv + + June 20, 2018 NC Dept. of Environmental, Health, and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Central Files Please find enclosed the following: Rick Flickinger Manager -Equipment Reliability T 336-495-2625 M 336-465-1127 rick. Flickingerotim ken.com JUL 08 2018 CENTRAL FiLEZ DWR SECTION • The original and one copy of the Semi -Annual Stormwater Discharge Monitoring Report • Two copies of the actual test results from Research & Analytical Laboratories, Inc. For this sampling period, the Zinc level was just over the benchmark at Outfall 001 and the Copper level was over the benchmark threshold at Outfall 003. We are currently performing a Tier 1 investigation to detennine possible causes. If you need any additional information, please do not hesitate to contact the at (336) 495-2625, or you may send inquiries to the following address: Rick Flickinger The Timken Company 3500 Timken Place Randleman, NC 27317 Sincerely, Rick Flickinger Manager -Equipment Reliability Stronger. Commitment. Stronger. Value. Stronger. Worldwide, Stronger. Together. I Stronger,By Design, The Timken Company Mail Code: ASB-01 4500 Mount Pleasant St. NW North Canton, OH 44720 #1 Semi-annual StormwateiW. charge Monitoring Re 0V � for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted LtzllbB CERTIFICATE OF COVERAGE NO. NCG03 0 U -k 3 FACILITY NAME ' 1 /✓ V-E0 PL-PrA3 ►% COUNTY _ryN PERSON COLLECTING SAMPLES 61L LABORATORY'_R� A L.A& Lab Cert. # ' ,37 L j Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR zoo 6 SAMPLE PERIOD (Jan -June ❑ July -Dec or ❑ Monthly' _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flaw ®Watersupply - [:]SA ❑ Other 1 G iri Kr CFI\PL•EASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 > ❑ No discharge this period?2 Outfall No. "Date:Sample. Collected' (mo/dd/yr), 24°hour rainfall- amount, Inches' = Total Suspended Solids pH; Standard units pWR Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks =__> _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L L voV "IL ,ci3.� . ik'L 5 M CCU 3 G li i' L3 J 5" A7 L {o= �/!.� o%7- M97L <,LYcs -7 M9 JL- 5m >'L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). -A Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." ifc K +--Ik)46'n Name (Print name) MAKMCC(L ���2V_i�MCN'i F�C�.1R�Sl L 77r Title (Print title) 4j?,Yfi 6 (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX�, where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. r Permit 1/1/2012-10/31/2017 SWU-245, last revis 2512012 r Page 2 of 3 Note: 9report a sample value in excess of the benchmark, you must a Cent Tier 1, Tier 2, or Tier 3 responses. See General Permit tee�,,,� s FOR PART AAND PART MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCFEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME QUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE QUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy o} this DMR, including all "No Discharge" reports, within 30_days of receipt of the- lob results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false Information, including the possibility of fines and imprisonment for knowing violations." AV/ to (Signature of Permitte j (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwatela)charge„Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted T A `i;_ _ CERTIFICATE OF COVERAGE NO. NCG03 O v 2 FACILITY NAME i ieny-iE0 i�.5;t1�=b�lLo PLP1 i COUNTY _ _ `r am ' k Q[4 PERSON COLLECTING SAMPLES ' 4 , ��c�, E 2 LABORATORY'-k A LA5 Lab Cert. # 3 7 c3 j Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR zoI 6 SAMPLE PERIOD R Jan -June ❑ July -Dec or ❑ Monthly' {month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow kIWater Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES Z AND/OR 3 --> ❑ No discharge this period?' Outfall No. Date Sample 1 Collected (mo/dd/yr) 24=hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum hydrocarbons Total Toxic 5 Organics Benchmarks =__> _ - 100 mg/L or 50 mg/LQ 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L i mg/L 001 Ca 11 1 `� ..� '� 5r L , c Ot)6 M14L � :. ti.� •1 L .14 2- li � 57 rq — 00 3 C, 1f j i3 j + S. m' L- �_ �/is ttiz I- L �.c�ca� !� UY7M 4 4 �m IL 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 46912; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Ml�h) 6 6e(L — JQL)i0M(N% )A(31 L 771V Title (Print title) CP Z Y / 6 (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' putfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =_=> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit C?=~—N1.1/1/2012-10/31/2017 SWU-245, last revise" 12512012i►. 1 Page 2 of 3 Note: (:�.,,report a sample value in excess of the benchmark, you must i. aent Tier 1, Tier 2, or Tier 3 responses. See General Permit tex:_,� FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE QUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail on original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" resorts) to: Division of Water Quality Attm DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete, I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." •ZY (Signature of Permitte j (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 ., RESEARch & ANALyTiCA[ Q€ LAbORATORIES, INC. 0Cr� For: Timken 3500 Timken Place Randleman, NC 27317 Attn: Rick Flickinger Report of Analysis 5/19/2018 r 1!,/;Q i NC434 z:-Cn Z NC937701 i 9' 4JI1111111% Client Sample ID: Outfall 001 Lab Sample ID: 51858-01 Site: Timken Collection Date: 6/11/2018 16:20 Parameter Method Result Units Rep Limit Analyst Analysis Date/Time Copper, Total EPA 200.7 0.006 mg/L 0.005 KL 6/13/2018 Hydrocarbon O&G EPA 1664 Revision B/Silica Gel <5 mg/L 5 EE 6/13/2018 Lead, Total EPA 200.7 <0.005 mg/L 0.005 KL 6/13/2018 pH SM 4500 H+8-2000 6.99 Std. Units 6/11/2018 Total Suspended Solids (TSS) SM 2540 D-1997 <5 mg/L 5 AA 6/13/2018 Zinc, Total EPA 200.7 0.142 mg/L 0.01 KL BY13/2018 Client Sample ID: Outfall 003 Lab Sample ID: 51858-02 Site: Timken Collection Date: 6/11/2018 16:22 Parameter Method Result Units Rep Limit Analyst Analysis DatelTime Copper, Total EPA 200.7 0.012 mg/L 0.005 KL 6/13/2018 Hydrocarbon O&G EPA 1664 Revision B/Silica Gel <5 mg/L 5 EE 6/13/2018 Lead, Total EPA 200.7 <0.005 mg/L 0,005 KL 6/13/2018 pH SM 4500 H+8-2000 6.96 Std. Units 6/11/2018 Total Suspended Solids (TSS) SM 2540 D-1997 5.6 mg1L 5 AA 6/13/2018 Zinc, Total EPA 200.7 0.047 mg/L 0,01 KL 611 3i201 8 NA = not analyzed P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: 336-996-284i Fax: 336-996-0326 t+nrnv,randalabs.com Page 1 'al coa "'Id '.10 RF5EARch & ANA1yTICA1 I_AbORATORIES, INC. Analytical / Process Consultations Phone 13361 996-2841 CHAIN OF CUSTODY RECORD WA7ERl WASTE4JATER MISC, COMPANY r>sl«0 co A, p iVOY� JOB NO. cam, o z y° p o` ��1 e• �r ��'' U�¢ v � U U U o�^Q. U Q' ryvry ry ry 5 ftEQUESTEI]ANALYSIS STREET ADDRESS 3 �Ciu /,l Kt U J�l�ce PROJECT S i:CIA UI L3 wL✓ K� CIT-Y. STATE, ZIP itAWVLC-MAJ /UC 2 73! SAMPLER NAME (PLEASE PRINT) lCIL �1Clii CONTACT PHONE y(ICIC (=Llcj(-I Ai �C)'l 334-YS'S-24z SAMPLER SIGNATURE € _ SAMPLEHIFi1f3ER {IAS USEOHLYj BATE TIME t0>1P GARS TEN ,CCI PESm:,2 11ernn ws[F is EAMPL DCATBOH11.0, 5 " � (r j �! d;! ./ i• _ C"_i �7 i C?cJ T F � l.. Cc;9 P� IL L 11L G 1' !L za.1 ✓ 5 Uo:j CK� 4 LL CUPpCiL _ �1rUG C- (Z e Wsc- 1 5 j RED; jIsHe`oeY � 01�1`ME R IveoeY REMARKS: SAMPLE TEMPERATURE AT RECEIPT R NDUISH BY 4 1` 1i DATE/1MIAE N ECEI JJ RESEARCh & ANA[yTICA1 L LAbORATORIES� INC. 't" 1 14i `,1 Report of Analysis 6/19/2018 i�l<iiiflfr�l For: Timken�QG,,..�•C 3500 Timken Place Randleman, NC 27317 Z cc° 0: cn M NCn34 „ ,to • Zi Attn: Rick Flickinger 4 NC437701 ' p`Ap.1 �� f!+ Client Sample 1D: Outfall 001 Lab Sample ID: 51858-01 Site: Timken Collection Date: 6/11/2018 16:20 r— Parameter Method Result Units l Rep Limit Analyst Analysis Date/Timed Copper, Total — EPA 200.7 0.006 mglL 0.005 KL 6/13/2018 Hydrocarbon O&G EPA 1664 Revision B/Silica Gel <5 mg1L 5 EE 6/13/2018 Lead, Total EPA 200.7 <0.005 mc3/L 0.005 KL 6/13/2018 pH SM 4500 H+13-2000 6,99 Std. Units 6/11/2018 Total Suspended Solids (TSS) SM 2540 D-1997 <5 mg/L 5 AA 6/13/2018 Zinc, Total EPA 200.7 0.142 mg/L 0.01 KL 6/13/2018 Client Sample ID: Outfall 003 Lab Sample ID: 51858-02 Site: Timken Collection Date: 6/11/2018 16:22 Parameter Method Result Units Rep Limit Analyst Analysis DatelTime Copper, Total EPA 200.7 0.012 mg/L 0.005 KL— 611312018 Hydrocarbon 08G EPA 1664 Revision B/Silica Gel <5 mg/L 5 EE 6/13/2018 Lead, Total EPA 200.7 <0.005 mg/L 0.005 Kt_ 6/13/2018 pH SM 4500 H+B-2000 6.96 Std, Units 6111/2018 Total Suspended Solids (TSS) SM 2540 D-1997 5.6 mglL 5 AA 6/13/2018 Zinc, Total EPA 200.7 0.047 mg/L 0.01 KL 6/13/2018 NA = not analyzed e P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 lei: 336-996-2a41 Fax.: 336-996-0326 wwvv,randalabs .com Page i RESEARCh & ANAIygiCAL LAbORATORIES, INC. Analytical / Process Consultations Phone 13361 996-2EW CHAIN OF CUSTODY RECORD WATER f WASTEWATER misc. COh1PhNY Jon NO o z c c" ay�P° m=Ps ti0 g aTEM c'��a�a�a�'ca. P o � y_ ti ro ro �" y REQUESTEQANALYSIS STREET ADDRESS 3 �UV ill %I1Kt"-= d�r'}-C Sr PROJECT' t5 i��lti z.Uf k3 wl...i �� K'� CITY.STATE,TIP U�ciwC�LMR✓ iV� �73ti7ICIL SAT.SPLERNAME (PLEASEPAINT) CONTACT PHOtIE �ctc Flkcxi&A6cat 33(z-iy� 2Gz} SAMPLER SIGNATURE PLE MlA1EEl RUSEONLY DATE ME CCU Gw .G o�s� lvw M� is�wt sAIrPL OGAT�aNrcD. _ 621-1 L sg 9( 0 . 12 c r r5 zzzz ✓ c�o'3 61-,F �A- nEE Aj C, % S F1 _ I RELINOUISHEDBY DATITkIlll� ft , IVEOBY i �. REMARKS: SAMPLE TEMPERATURE AT RECEIPT 3. 2 °C R NOUISH BY J �' DATEITIME LI12�i$ ECEA �J i Rick Flickinger Manager -Equipment Reliability T 336-495-2625 M 336-465-1127 rick.flickinger@timken.com September 20, 2017 NC Dept. of Environmental, Health, and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Central Files Please find enclosed the following: • The original and one copy of the Semi -Annual Stonnwater Discharge Monitoring Report • Two copies of the actual test results from Research & Analytical Laboratories, Inc. For this sampling period, all levels are below the benchmark thresholds. If you need any additional information, please do not hesitate to contact me at (336) 495-2625, or you may send inquiries to the following address: Rick Flickinger The Timken Company 3500 Timken Place Randleman, NC 27317 Sincerely, Rick Flickinger Manager -Equipment Reliability Stronger. Commitment. Stronger.Value. Stronger. Worldwide. Stronger. Together. I Stronger.By Design_ The Timken Company Mail Code: ASB-01 4500 Mount Pleasant St. NW North Canton, OH 44720 Semi-annual Stormwaterschalrge Monitoring Report IR) for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03 0 C? t Z. FACILITY NAME r-EL-.9 -�VSM-[30rtn f2C COUNTY ';ZAr�Q,cP►# PERSON COLLECTING SAMPLES LABORATORY --i A L_ PrFaS Lab Cert. # NCG 3y 37 -7o/ Comments on sample collection or analysis: Part A: Stormwater Benchmarks.and Monitoring Results SAMPLE COLLECTION YEAR Z01-7 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly" (month} DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RECEIVED ❑Zero -flow [Water supply ❑SA ❑Other 5EP 2 G NP CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION ❑ No discharge this period?' Outfall No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ==_> _ - 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L ,,em s m 1�. S o�� I� �, :5 04 L �. oc> 3 �l ra i , S /X It a.- < L , b aS .� oat JL 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). t_ Permit Date: 11/1/2412-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible form anaging compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." i cK rL tckra)iLr t _ Name (Print name) Title (Print title) Qk___7=2 q -20� (Signature) (Date) Note: Results must be reported•in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/O where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 - 9.0 su Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit D 1.1/1/2012-10/31/2017 SWU-245, last revise 25/2012 Page 2 of 3 ', Note: 41,)report a sample value in excess of the benchmark, you must in Trent Tier 1, Tier 2, or Tier 3 responses. See General Permit text. _/ t p' FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case o "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm !7-?,0-1% (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Qcharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted y�z��za 17 CERTIFICATE OF COVERAGE NO. NCG03 0 Z FACILITY NAME —r'►+ K-952 -ISM -Goan P(L-A-nJ i COUNTY V,,o o, P 14 PERSON COLLECTING SAMPLES LABORATORY 'R-! A L_ Pt6_S Lab Cert. # A%G3y /37 70/ Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR Z017 SAMPLE PERIOD ❑ Jan -June R July -Dec or ❑ Monthly— _- lmonth) DISCHARGING TO CLASS ❑ORVII ❑HQW []Trout ❑PNA ❑Zero -flow [Dwatersupply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. 'iDate'Sample' Collected' (mo/dd/.yr). • '�`24'hour ra amount, 3 Inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non-Polar O&G/infall Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks ===> _ - 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L I4 r i yti s m 11, 5 (.')0(0JL. J� Stty L 044 roeIL 00 3 �1'(r I , S JAkd'ts L L , UCtS L t qa a1 in i� < 5- 1L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469,22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The Solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employthe TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." _ 2 , Gk EL cc..krn3¢Lj_IL Name (Print name) /r dA.-i4r,f, a - L Uui PMeAj REtta I&LI � Title (Print title) Q2,0- ,� 1 k(Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. !Vote: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yrj 24-hour rainfall amount, 3 Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM} Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 - 4.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Da' 1/1/2012-10/31/2017 SWU-245, last revised^.125/2012 Page 2 of 3 r Note: report a sample value in excess of the benchmark, you must in vent Tier 1, Tier 2, or Tier 3 responses. See General Permit text ~ , FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NOR IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "l certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my Knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm <7- ?,cl-17 (Date) Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 RESEARCh & ANA.1YTiCA1 LA oRAT06ES� INC. Report of Analysis 9/19/2017 For: Timken �.�G •••C�•",.� •��fi �: 3500 Timken Place `ter • Randleman, NC 27317 ilk:.`= a :o� Nca3a z Attn: Rick Flickinger r •;:•o/c37701 �•�= a, AP,� Client Sample ID: 001 Outfall Lab Sample ID: 39637-01 Site: Timken Collection Date: 9/6/2017 13:35 Parameter Method Result Units Rep Limit Ana! s# Analysis Datefrime Copper, Total EPA 200.7 0.006 mg/L 0,005 KL 9/11/2017 Lead, Total EPA 200.7 <0.005 mg/L 0.005 KL 9/11/2017 Oil & Grease EPA 1664 B <5 mg/L 5 AW 9/13/2017 pH SM 4500 H+8-2000 7.15 Std. Units 9/6/2017 Total Suspended Solids (TSS) SM 2540 13-1997 7.0 mg/L 5 AA 9111/2017 Zinc, Total EPA 200.7 0.044 mg/L 0.01 KL 911112017 Client Sample ID: 003 Outfall Lab Sample ID: 39637-02 Site: Timken Collection Date: 9/6/2017 13:38 Parameter Method Result Units Rep_ Limit Analyst alysis Date/Time, :An Copper, Total EPA 200.7 <0,005 mg/L 0.005 KL 9/11/2017 Lead, Total EPA 200.7 <0.005 mg/L 0.005 KL 9/11/2017 Oil & Grease EPA 1664 B <5 mg/L 5 AW 9/13/2017 pH SM 4500 H+B-2000 6.99 Std. Units 9/6/2017 Total Suspended Solids t i SS) SM 2540 D-1997 <5 mg/L 5 AA 9/11/2017 Zinc, Total EPA 200.7 <0.01 mg/L 0.01 KL 9/11/2017 NA = not onotyzed P.O. Boz 473 106 Short Street Kernersville, North Carolina 27284 Tel: 336-996-2841 Fax: 336-996-0326 www.randalabs.com Page 1 ral_coa basic_vid MiIIIMI RESEARCh & ANA[yT1CAL L4bORATORIES, INC. Analytical 1 Process Consultations Phone 13361 996-2841 CHAIN OF CUSTODY RECORD WATER f WASTEWATER M15C. COMPANY JOB NO, H 1 m O 9 `a y0• J V Q, �� _�° O pV O- �y lP m��` Y ` U a' a' a' REQUESTED ANALYSIS STREETAODRESS :~i)Ci '11f17 C'U LL-` PROJECT CITY, STATE, ZIP SAMPLER NAME (PLEASE PRINT) CONTACT PHONE SAMPLlwH SIGNATURE SAMPLENUMBER rLRB USE ONLY) DATE TUJE QY AA9 TEM ,LGIn KSuaan� a SAMPLE LOCATION MI. 01 1-1 : T1 n I 0v, L L _ .p �INc 00 L/TYgLL C- �� RELINC UISHEO BY DATQTIMIE RECEIVED BY REMARKS: i5w+v. SAMPLE TEMPERATURE AT RECEIPT 3 q °C RELINQUIS ED BY r 4-A "l JIDATEMME — f -, � RECEVED BY RIESEARCh&ANAtyTiCAI Report of Analysis LAbORATORiESF INC. 9/19/2017 F�, For: Timken Timken Place `4.�'�G =: �C `� k. Randleman, NC 27317 • O V NC ##343500 „ .ov Attn: Rick Flickinger NC ##37701 �: ► ► "441 jFD ANp�y �+iirrt�ta�+'t Client Sample ID: 001 Outfall Lab Sample ID: 39637-01 Site: Timken Collection Date: 9/6/2017 13:35 Parameter 'Method Result Units Rep Limit Analyst AnalysisDatelTime Copper, Total EPA 200.7 0A06 mg/L 0.005 KL 9/11/2017 Lead, Total EPA 200.7 <0.005 mg/L 0.005 KL 9/11/2017 Oil & Grease EPA 1664 B <5 mg/L 5 AW 9/13/2047 pH SM 4500 H+13-2000 7.15 Std. Units 9/6/2017 Total Suspended Solids (TSS) SM 2540 D-1997 7.0 mg/L 5 AA 9/1112017 Zinc, Total EPA 200.7 0,044 mg/L 0.01 KL 9/1112017 Client Sample ID: 003 Outfall Lab Sample ID: 39637-02 Site: Timken Collection Date: 9/6/2017 13:38 Parameter Method Result Units Rep -Limit Analyst Analysis Date/Time; Copper, Total EPA 200.7 <0.005 mg/L 0.005 KL 9/11/2017 Lead, Total EPA 200.7 <0,005 mg/L 0.005 KL 9/11/2017 Oil & Grease EPA 1664 B <5 mg1L 5 AW 9/1312017 pH SM 4500 H+13-2000 6.99 Std. Units 9/6/2017 Total Suspended Solids k7SS) SM 2540 D-1997 <5 mg/L 5 AA 9/11/2017 Zinc, Total EPA 200.7 <0.01 mg/L 0,01 KL 9/11/2017 NA = not analyzed P.O. Boz 473 106 Short Street Kemersville, North Carolina 27284 Tel: 336-996-2841 Fax: 336-996-0326 www.randalabsxonn Page 1 ral coa basic vtd RESEARCh & ANAIYACAL LAbORATORiES, INC. Analytical / Process Consultations Phone (3361 996-2841 CHAIN OF CUSTODY RECORD WATER I WASTEWATER I MISC. COMPANY JOBNO g a mVe., �Q yo" Q~ U QQ o`eUeUaU 4 ry ry ry �" 5 REQUESTED ANALYSIS STREET ADDRESS ' '0 52ni " eu C9zF PROJECT r1jLL J1 5 �, . t�q°TZ7L CITY, STATE, ZLP SAMPLER NAME (PLEASE PRINT) CONTACT PHONE rest F�IC.-Inxc'r'C Y95—zc,z:` SAMPLER&GNATURE SAMPUNUMSER W 9SEOHLYj DATE TWE WASTE 'C RLi ,t� � I—R, Y R! pawl SAMPLE LOCATiDRlLD. PM 1.5r b 9 P 6717 L � SING 1, li: _ i4 C,,. 9 c REUNCHISHED BY DATEfTM+IE _t� RECEIVED BY r REMARKS: � % SAMPLE TEMPERATURE ATRECE[P. �q °(; REUNQUIS F01 Y rr^S' fj .fjI, `c- nDkTyTIME I ]] , RECEIYEBBY `�'—\ OTION1 MT1 June 29, 2017 NC Dept. of Environmental, Health, and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Central Files Please find enclosed the following: Rick Flickinger Manager -Equipment Reliability T 336-495-2625 M 336-465-1127 rick.flickinger@timken.com • The original and one copy of the Semi -Annual Stonnwater Discharge Monitoring Report • Two copies of the actual test results frorn Research & Analytical Laboratories, Inc. For this sampling period, the Zinc level was just over the benchmark at Outfall 001 and the Copper level was just over the benchmark threshold at Outfall 003. We are currently performing a Tier 1 investigation to detennine possible causes. If you need any additional infonnation,_plcase do not hesitate to contact me at (336) 495-2625, or you may send inquiries to the following address: Rick Flickinger The Timken Company 3500 Timken Place Randleman, NC 27317 Sincerely, Rick Flickinger Manager -Equipment Reliability Stronger. Commitment, Stronger.Value. Stronger.Worrdwide. Stronger. Together. I Stronger.Sy Design. The Timken Company Mail Code: ASB-01 4500 Mount Pleasant St. NW North Canton, OH 44720 �- Semi-annual Stormwaterk:6char a Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 6�`_ Z `T- ) `7 CERTIFICATE OF COVERAGE NO. NCG03 © n � FACILITY NAME I l LrW - ipe&cyto COUNTY w00 L l PERSON COLLECTING SAMPLES moo(_ HOC- w04&lL LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A. Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 7 0 1 RECEs SAMPLE PERIOD 57 � Jan -June _ j July -Dec , L-0 or Monthly' month JUL 0 5 WSCHARGING TO CLASS ❑ORVV ❑HQW ❑Trout ❑PNA C E i•FFFZAL i it E5 ❑Zero -flow ®Water Supply ❑SA F)V'JR SECTION ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic organicss Benchmarks ===> _ - 100 mg/L or 50 mg/L 6.0 - 9.0 0:007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 L �XIL -c'OoSall , ensf k rk -7, 1 , 00q AVIL 1 ,00514 % a51.n J LS>M j' ' Monthly sampling (instead of semi-annual) must begih with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. S Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469,22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 PACP 'I of R Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) /n&1L- e QViI}I itit j-j ►R(R-I 1f7/ Title (Print title) Q��Q 1 z y/17 (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit 0.1/1/2012-10/31/2017 . 5WU-245, last revise?5/2012 Page 2 of 3 0 Note: *report a sample value in excess of the benchmark, you must i0cent Tier 1, Tier 2, or Tier 3 responses. See General Permit text. �Z FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCE£DENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" re orts� within_3dreceipt oLthe lab_ results (or at end o monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn-. DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm 6111117 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater L char e Monitoring Report 0J. for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted - Z 9-1 CERTIFICATE OF COVERAGE No. NCG03 4 0 q � FACILITY NAME / f4rN + orto c COUNTY _ �Av nQD Plf PERSON COLLECTING SAMPLES c+[_ rcic- k_jo4L2 LABORATORY Lab Cert. tt Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _ ZC9 I SAMPLE PERIOD Jan -June j July -Dec or Monthly'_ (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ®Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfall No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids PH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics 5 Benchmarks ===> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0:007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 4 i3f+ { L 7,' Jr o IL 'C g1Sol, .k 4 S,4, CJ U CQ 13 I �o. Y i. �, I uo4 t_ 1 ,005IM A. asl n 1 LSm I ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 P. E; M 1 of :z Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), i certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." 19L1c.iCl Name (Print name) /n1OOJIf66n- 6QuQW6,) PAR-1661 0_11 Title (Print title) agu GlZ r117 (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XXm L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period:' Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, - Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===y _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Dim 1/1/2012 10/31/2017 SWU-245, last reviser" 175/2012 ,mil Page 2 of 3 4 I y Nate: l;,�report a sample value in excess of the benchmark, you must in,r--dent Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART li SECTION B. • 2 FXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, _including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case af "No Discharge" reports: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FORANY INFORMATION REPORTED: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations," (Signature of Perm _�12 M 7 (Date) Permit Date, 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Paee 3 of 3 RESEARCh & ANA yTDCA1 Report of Analysis Qo . LABORATORIES? INC. 6/27/2017 �OQ t'bj 9 l l l tl'. For: Timken •`••`•*�G�'�rT�4����`L 3500 Timken Place Randleman, NC 27317 o NCp34 Z; Attn: Rick Flickinger =� NC tt37701 . e"', P// FD ANP4A�. '#tfIIAIYlll1- Client Sample ID: 001 Outfall Lab Sample ID: 35928-01 Site: Timken Collection Date: 6/13/2017 19:45 Parameter Method Result Units Rep Limit An^, alyst Analysis Daterrime Copper, Total EPA 200.7 0.006 mg/L 0.005 SK 6/16/2017 Hydrocarbon 0&G EPA 1664 Revision B/Silica <5 mg/L 5 JF 6/16/2017 Gel Lead, Total EPA 200.7 <0.005 mglL 0.005 SK 6/1612017 pH SM 4500 H+13-2000 7.45 Std, Units 6/13/2017 Total Suspended Solids (TSS) SM 2540 D-1997 <5 mg1L 5 AA 6/15/2017 Zinc, Total EPA 2003 0.075 mg/L 0.01 SK 6/16/2017 NA = not onolyzed P.O. Box 473 106 Short Street Kernersvitle, North Carolina 27284 Tel: 336-996-2841 Fax: 336-996-0326 www,randatabs.com Page 1 ral coa basic vld tL\ RESEARCb & ANAl yTICAI I-AbORATORlES, INC. Analytical / Process Consultations Phone (336) 99E-2641 CHAIN OF CUSTODY RECORD WATER! WASTEWATER I M15C. COMPANY JOB NO. " o o k � v O• �_ �6� ` F Q O of �c� F q, �V ° �3' v v v �� rY REQUESTED ANALYSIS STREETADDRESS �� 3 7 CX� %/�lI�L�A� sf L_!} Ge PROJECT s ^r ,u r- ZCI ( V7L-JZ s+ U CITY, STATE, ZIP �J —1) G Z.731 SAMP ER NAME (PLEASE PRINT) 1 C)C. FL c AX CA_ CONTACT PHONE I c FL ►cY-jN4vA 5 - 2�Z-S SAMPLER SIGNATURE J SAMPLE NUMBER (LAB USE ONLY) DATE TIME COPTORAB TEMP eC RES ,�ylt, fiE 19�C� i7aN� I A,n K Isnw, 5 PLELOCATIONII.D. -c� 7'y Oo L n,O t5i5 S RSHED BY�MI7 �`� RECEIVED BY �REMARKS:L9 SAMPLE TEMPERATURE AT RECEIPT °C RELIN HED bDAJEjfl REC ED 1 6 k%- f"— RESEARCh & ANA[yTiCAt a LA ORATORiES, INC. For: Timken 3500 Timken Place Randleman, NC 27317 Attn: Rick Flickinger Report of Analysis 6/27/2017 �tirrart'rrr4 •a �a;co NC434 z*tn,. NC 937701 dt +` �''9Tf'`�ED AN���• ``, ��br u n �++►+r Client Sample ID: OUtfall 003 Lab Sample ID: 35929-01 Site: Timken Collection Date: 6/13/2017 19:47 Parameter Method Result Units Rep Limit Analyst Analysis Date/Time Copper, Total EPA 200.7 0.009 mg/L 0.005 SK 6/16/2017 Hydrocarbon O&G EPA 1664 Revision BfSilica <5 mg1L 5 JF 6/16/2017 Gel Lead, Total EPA 200.7 <0.005 mg1L 0.005 SK 6/16/2017 pH SM 4500 H+B-2000 7,18 Std. Units 6/13/2017 Total Suspended Solids (1-SS) SM 2540 D-1997 6.4 mg1L 5 AA 6/15/2017 Zinc, Total EPA 200.7 0.051 mg/L 0.01 SK 6/16/2017 NA = not analyzed P.0, Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: 336-996-2841 Fax: 336-996-0326 www.randalabs.com Page 1 rat coa basic .1d RESEARCh & ANA1yTiCA1 LAbORATORiES, INC. Analytical 1 Process Consultations Phone (336) 996-2841 CHAIN OF CUSTODY RECORD WATER I WASTEWATER I MISC. COMPANY 74K&u CbAflr,v JOB NO. w 0 1P - ¢% ~ y v �� `b- moo' y~ �Q ; �O` n �� �• \y `a Q ° �C 0 0� F` L� Q• �Q Q Q Q°t tiv� ryry�o �" �" REQUESTED ANALYSIS ST'REETADDRESS Ut/nlGn� cE PROJECT -�7 5u� Zr+7 l,+tia4t1� CITY, STATE, Zip SAAIPLER NAME (PLEASE PRINT) CONTACT PHONE c C� rLtr'� (N4 crlL 9S Z�c 2 5 SAMP i SIGNATUF SAMPLE NUMBER (LAB USE ONLY) DATE TIME 'COUP Cm TEMP .0 FtES I ItiI rrno ur:[ ufEj SAMPLE (sows SAMPLE LOCATION I I.D. Sq Zj-DL 6113 7'v7 0 )?FLL hr C Pp en- vz c. <; s C 7 SS RELINQUISHEDJDT�IjE RECEI Y REMARKS: SAMPLE TEMPERATURE AT RECEIPT 0 C RELINQUISHED BY QAErTtIlE REC Y/ L� RESEARCh & ANA1YTICA1 LABORATORIES, INC. Report of Analysis 6/27/2017 For: Timken 4`4�,�,.••�C •• ,+it 3500 Timken Place`; Randleman, NC 27317 o.th NC #34 Z: - Attn: Rick Flickinger NC p37701 {�. CsF i�Ec-ro �C Client Sample ID: 001 Outfall Lab Sample ID: 35928-01 Site: Timken Collection Date: 6/13/2017 19:45 Parameter Method Result Units Rep Limit Analyst Analysis DatelTime Copper, Total EPA 200.7 0.006 mg/L 0.005 SK 6/16/2017 Hydrocarbon O&G EPA 1664 Revision B/Silica <5 mg/L 5 JF 6/16/2017 Gel Lead, Total EPA 200.7 <0.005 mglL 0.005 SK 6/16/2017 PH SM 4500 H+13-2000 7.45 Std. Units 6/13/2017 Total Suspended Solids (FSS) SM 25401a-1997 <5 mg1L 5 AA 6/15/2017 Zinc, Total EPA 200.7 0.075 mg/L 0.01 SK 6/1612017 NA = not onolyzed P.O. Box 473 tfl6 Short Street l{ernersville, North Carolina 27284 Tel: 336.996-2841 Fax: 336-996-0326 www.randalabs.com Page 1 WSEARCh & ANAlyfiCAl LABORATORIES, INC. Analytical / Process ConsulCabons Phone (336) 996-2841 CHAIN OF CUSTODY RECORD WATER 1 WASTEWATER I MISC. COMPANY JOB NO. _ u � 0 h v \qVI �0` �}��� ,h y � 6 �. o ¢ �C, ��J_�5 Q U C Q V ti ti y y �v v �• REQUESTED ANALYSIS STREET ADDRESS 35-UC? 7-/M c-V d L tJ C-e PROJECT Veicu6 :. ( �' CH &o CITY, STATE, ZIP LC-Yn •+�J -,1,7 G Z731 SAhMP ER NAME (PLEASE PRINT) ` z�i CONTACT PHONE I C tiCY N4n33� �- SAMPLEk 1CNAURE J SAMPLE NUMBER {LAB USE ONLY} DATE TIME OmpGflaB TEMPIC nes mnn� REBOVI u [rryNi HA x snw S PLELOCATIDNfI.D. (2a c� L C C)pprn RElf SHEDBY DA t ME RECEIVED BY REMARKS: SAMPLE TEMPERATURE AT RECEIPT ~' °C REL1N HED pA�F�11{f•f (� �1' `t REC ED RESEARCh & ANA1yTICAL LABORATORIES? INC. Report of Analysis 6/27/2017 till 9aIIIIloU For: Timken �.��G .-••••. !4•. 3500 Timken Place Randleman, NC 27317 y cc N6 tvcx3a 0.Ch �. S• Attn: Rick Flickinger �: NC 437701 i Client Sample ID: Outfall 003 Lab Sample ID: 35929-01 Site: Timken Collection Date: 6/13/2017 19:47 Parameter Method Result Units Rep Limit Analyst Analysis Dateffime Copper, Total EPA 200.7 0.009 mg/L 0,005 SK 6/16/2017 Hydrocarbon O&G EPA 1664 Revision B/Silica <5 mg1L 5 JF 6/16/2017 Gel Lead, Total EPA 200.7 <0.005 mg1L 0.005 SK 6/16/2017 PH SM 4500 H+13-2000 7.18 Std. Units 6/1312017 Total Suspended Solids (TSS) SM 2540 D-1997 6.4 mg1L 5 AA 6/15/2017 Zinc, Total EPA 200.7 0.051 mg/L 0.01 SK 6/16/2017 NA = not analyzed P.O. Boxa73 106 Short Street Kemersville, North Carolina 27284 Tel: 336-996-28a1� Fax: 336-996-0326 w%wi.randalabs.com Page 1 '8i C^sa �sS�C 1d RESEARCh & ANAIYTICAI LAbORATORiES, INC. Analytical / Process Consultations Phone (336) 996-2641 CHAIN OF CUSTODY RECORD WATER! WASTEWATER I MISC, COMPANY JOB NO. x o w o o , �ny1 Ci. y Z ~ �I �v � `vim �Q ; yq. ���' o�� "A:? o � �?`.o° ��PyO}�OG�aprGco`gdv���a`� ` Q Q q o� C F ¢. C7 Q' Q' Q' c z ti�ry4 l`70'L�o �" ^ �REQUESTED ANALYSIS STREETADDRESS vo /��a'�+*ti �' cc PROJECT 5?t Zc+"7 7Z,z w/i' "� CITY, STATE., ZIP C�m17� BUG Z�3 r SAMPLER NAME (PLEASE PRINT) k-k- FLLc.�r�c,if/C CONTACT 33FiONE C� t�'�IC�I Nor /� r Z.(,Z S SAMP SIGNATIJ SAMPLE NUMBER (LAB USEDt'ILYI BATE TIME CCYPGRA9 TEM 'C RES CI i.�,ai CIgp41N[ irnru SAun[ Isuwi SAMPLE LOCATION II,D. 7`v7 X �, G) 0 o0t Pt+LL H� C P _ -9) �uc- 7 Ss RELINQUISHED BY Z fDt3rTi�fj�E RECEI Y REMARKS: 3 SAMPLE TEMPERATURE AT RECEIPT °C RELINQUISHED 6Y AgrE 1� REC Y� /�� Semi-annual Stormwatelocharge Monitoring Report 7j ' for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted /0 S —1 CERTIFICATE OF COVERAGE NO. NCG03 0 O q Z FACILITY NAME r MKE: P — s a 1. COUNTY _ —A NQ6LPR PERSON COLLECTING SAMPLES r,�,,cK LABORATORY P{YE PNNLWiCAL Lab Cert. # 1 2— Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _ Z01 SAMPLE PERIOD ❑ Jan -June July -Dec or ❑ Monthly' _ fmonthj - DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow RLWatersupply []SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --> ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr), 24haur rainfaEl amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics s Benchmarks ==_> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 00 911cL ,7S m jt _7_,A 8 00SM r_ NO , oaf a03 G�Lq Igo I.7S A)G.�� ND N� oz(o L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. A See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may, so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." "_R\CY- Name (Print name) ( ni9QAQ-t- Ec ��Qm�ti� �C�IR �i�rry Title (Print title) - -- Q� �:2"/y-5-A, (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note. If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' putfal! No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Ikon -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit D �.1/1/2012-10/31/2017 SWU-245, last reviser' "-,25/2012 � • ) (, r Page 2 of 3 f Note:areport a sam le value in excess of the benchmark, ou must 0-.iient Tier 1 Tier 2, or Tier 3 res onses. See Genera! Permit text A Y A FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including al! "No Discharge" reports, within 30 days of receipt of the lab results Lor at end of monitoring period in the case of "No Discharge" reparts) to:^ Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of / t? -- 5 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 October 5, 2016 R 2@190WE n U 0U I.2 2016 CEO -WATER RESOURCES 401 & BUFFER PEFiMiTTWG NC Dept. of Environmental, Health, and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Central Files Please find enclosed the following: Rick Flickinger Manager -Equipment Reliability T 336-495-2625 M 336-465-1127 rick.Flickinger@timken.com ac;z,[EOdc OCT 1 0 2016 DID+iSION DF WATER RESOURCES • The original and one copy of the Semi -Annual Stormwater Discharge Monitoring Report • Two copies of the actual test results from Pace Analytical Services, Inc. For this sampling period, the Zinc levels have returned to normal levels and below the upper limit. Our investigation after the Spring Sampling was unable to identify any contributing factors to the prior sample's elevated levels. If you need any additional information, please do not hesitate to contact me at (336) 495-2625, or you may send inquiries to the following address: Rick Flickinger The Timken Company 3500 Timken Place Randleman, NC 27317 Sincerely, Rick Flickinger Manager -Equipment Reliability Stronger. Commitment. Stronger.Value. Stronger.Worldwlde. Stronger. Together. I Stronger. By Design. The Timken Company Mail Code: ASB-01 4500 Mount Pleasant St. NW North Canton, OH 44720 ----- - -w---� ._ ...� �- � , - .. '.i �� � � � or�� `. Jt3 i 1 ....i � 4: .. i4 s � i 4 P V Semi-annual Stormwater L�char a Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted S - I/ - /(o CERTIFICATE OF COVERAGE NO. NCG03 v 0 `i z- FACILITY NAME 7Tmy_LrN _ Aslt[ b,,+Go PLA#J T COUNTY !�RAN aa0 PERSON COLLECTING SAMPLES ick LABORATORY19kr3_ A00{,Y TiCXL Lab Cert. # I Z Comments on sample collection or analysis: Part A: Stormwater Benchmarks.and Monitoring Results SAMPLE COLLECTION YEAR Z 0 i �2 SAMPLE PERIOD Jan -June ❑ July -Dec �— - or ❑ Monthly'— (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA Zero -flow ❑ KWaterSupply ❑SA RECEIVED ❑Other MAY A 6 2916 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL FILES DWR SECTION ❑ No discharge this period?" Qutfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks =__> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 00 1 zz / o L 7,14 40107 4 ND -I L 003 `{{21 h 6 c0.s1 aoiP3w IL N� o 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible forma naging compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." �R1CR LC,K.I+3Ci 6rL Name (Print name) M 6C'IL - SQJ12A48VT 9G0I%j L,71' Title (Print title) "/ (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format,"<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ==_> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit D*1/1/2012-10/31/2017 ® SWU-245, last reviseo?5/2012 ,L Page 2 of 3 i Note: if,report a sample value in excess of the benchmark, you must im•ient Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and, one copy of this DMR, including all "No Discharge" reports within 30 days otrecept of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 May 23, 2016 NC Dept. of Environmental, Health, and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Central Files Please find enclosed the following: Rick Flickinger Manager -Equipment Reliability T 336-495-2625 M 336-465-1127 rick.flickinger@timken.com RECEIVED May 2 5 tots CENTRAL FILEs DWR SECTION • The original and one copy of the Semi -Annual Stormwater Discharge Monitoring Report • Two copies of the actual test results from Pace Analytical Services, Inc. For this sampling period, the Zinc levels were slightly elevated at the both outfall sampling locations. We are currently performing an investigation as to possible causes. If you need any additional information, please do not hesitate to contact me at (336) 495-2625, or you inay send inquiries to the following address: Rick Flickinger The Timken Company 3500 Timken Place Randleman, NC 27317 Sincerely, Rick Flickinger Manager -Equipment Reliability St longer. Commitment. Stronger_ Value. Stronger. Worldwide. Stronger. Together_ I Stronger. By Design, The Timken Company Mail Code: ASB-01 4500 Mount Pleasant St. NW North Canton, OH 44720 ' Semi-annual Stormwater Lcharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted / — f 9 -/ 5f CERTIFICATE OF COVERAGE N0. NCG03 0 0 Lk Z. FACILITY NAME-7-1rvIILEK) •- Asl{E{30rt O Q 1. W COUNTY "' DCX-P 14 PERSON COLLECTING SAMPLESF��tki+J4E�- LABORATORYPKC !JkL TlOk�- Lab Cert. # —Z Comments on sam le collection or anal sic• SAMPLE COLLECTION YEAR Z01 S 11 U-11 SAMPLE PERIOD ❑ Jan -June •®_July -Dec � RECEIVED or ❑ Monthly'_ �monthj � i"C V DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA NOV 2 3 2015 ❑zero -flow ®,Water Supply ❑SA—;< ❑Other P v CENTRAL PILES DVVR SECTION Part A: Stormwater Benchmarks,and Monitoring Results N o _ Nwe- DomM--LTL-_D PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --> ❑ No discharge this period?2 Outfall No. Date Sample' Collected' ' (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks ===> - - 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L C�C7 i v z7 11.5 --? CP , y t3 A), nl �S 0 U Z+ �j J i ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. s The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible forma nagingcompliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." "—RICY,- rL.ICKiAi4�s� Name (Print name) ftN44c- & - L QL)(Pryl(sr.Ji ECU R-siUT)( Title (Print title) 0-0 1 rr AS - (Signature) (mate) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XXmR/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period: Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 Su Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit D 1/1/2012-10/31/2017 SWU-245, last revise ?5/2012 R ,a Page 2 of 3 Note: !f report a sample value in excess of the benchmark, you must imp W client Tier 1, Tier 2, or Tier responses. See Genera! Permit text. FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO tQ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports. to: ^ Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm A 5- (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 2ce Analidical rrWWP&celabs.mrn November 12, 2015 Mr. Rick Flickinger Timken Company 3500 Timken Place Randleman, NC 27317 RE: Project: Timken - Fall 2015 Pace Project No.: 92273923 Dear Mr. Flickinger: Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 Enclosed are the analytical results for sample(s) received by the laboratory on October 29, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell taylor.ezell@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (336)623-8921 Page 1 of 11 I� aceAnalytical www.pacblabs.COrrl CERTIFICATIONS Project: Timken - Fall 2015 Pace Project No.: 92273923 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Flodda/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalytical' wwrpecelabs.com SAMPLE ANALYTE COUNT Project: Timken - Fall 2015 Pace Project No.: 92273923 Pace Analytical Services, Inc. 205 EaSt Meadow Road - SuiteA Eden, NC 27288 (336)623-8921 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92273923001 001 EPA1664B JMS 1 PAS I-C EPA200.7 CDF 3 PASI-A SM 2540D SAM 1 PASI-A 92273923002 003 EPA 1664E JMS 1 PASI-C EPA200.7 CDF 3 PASI-A SM 2540D SAM 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalytical www.p&cotabs.com ANALYTICAL RESULTS Project: Timken - Fall 2015 Pace Project No.: 92273923 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Sample: 001 Lab ID: 92273923001 Collected: 10128/15 11:00 Received: 10/29/15 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By Rick 1 11/12/15 13:53 Flickinger Collected Date 10/27/15 1 11/12/15 13:53 Field pH 6.48 Std. Units 0.10 1 11/12/15 43:53 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 11/10/15 09:27 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 2003 Copper NO ug1L 5.0 1 11/03/15 20:00 11/04/15 23:17 7440-50-8 Lead ND ug/L 5.0 1 11103/15 20:00 11/04/15 23:17 7439-92-1 Zinc 29.5 ug/L 10.0 1 11/03/15 20:00 11/04/15 23:17 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 7.0 mg/L 3.2 1 11/01/15 15:13 Sample: 003 Parameters Field Data Collected By Collected Date Field pH HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Date: 1111212015 01:54 PM Lab ID: 92273923002 Collected: 10/28/15 11:10 Received: 10/29/15 09:45 Matrix: Water Results Units Report Limit OF Prepared Analyzed CAS No. Oual Analytical Method: Rick 1 11/12/15 13:53 Flickinger 10/27/15 1 11/12/15 13:53 6.56 Std. Units 0,10 1 11/12/15 13:53 Analytical Method: EPA 1664B NO mg/L 5.0 1 11/10/1509:28 Analytical Method: EPA200.7 Preparation Method: EPA200.7 5.7 ug/L 5.0 1 11 /03/15 20:00 11/04/15 23:21 7440-50-8 NO ug/L 5.0 1 11/03/15 20:00 11/04/15 23:21 7439-92-1 16.5 ug/L 10.0 1 11/0311520:00 11/0411523:21 7440-66-6 Analytical Method: SM 2540D ND mg/L 3:3 i 11/01/1515:14 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalytrcal wwwpacabbs.min QUALITY CONTROL DATA Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (3361623-8921 Project: Timken - Fall 2015 Pace Project No.: 92273923 QC Batch: GCSV123160 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92273923001, 92273923002 METHOD BLANK: 1602426 Matrix: Water Associated Lab Samples: 92273923001. 92273923002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mglL ND 5.0 11/10/15 09:20 LABORATORY CONTROL- SAMPLE: 1602427 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mglL 40 34.9 87 78-114 MATRIX SPIKE SAMPLE: 1602428 92273805002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL ND 40 36.6 86 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2015 01:54 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalyticafo www.pxetabs.com QUALITY CONTROL DATA Project: Timken - Fall 2015 Pace Project No.: 92273923 QC Batch; MPRP/19949 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92273923001. 92273923002 METHOD BLANK: 1598071 Associated Lab Samples: 92273923001, 92273923002 Parameter Units Copper uglL Lead ug1L Zinc ug/L Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 11/04/15 22:38 ND 5.0 11/04/15 22:38 ND 10.0 11/04/15 2238 Qualifiers Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 LABORATORY CONTROL SAMPLE: 1598072 Spike LCS LCS %Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper uglL 500 518 104 85-115 Lead uglL 500 498 100 85-115 Zinc uglL 500 499 100 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1598073 1598074 MS MSD 92274192001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Copper uglL ND 500 500 509 512 102 102 70-130 1 Lead ug/L ND 500 500 502 498 100 100 70-130 1 Zinc ug/L 2.8J 500 500 521 521 104 104 70-130 0 Qual MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1598075 159B076 MS MSD 92273964001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Copper uglL ND 500 500 545 488 109 97 70-130 11 Lead ug/L ND 500 500 534 478 106 95 70-130 11 Zinc uglL 56.4 500 500 617 571 112 103 70-130 8 Results presented on this page are in the units indicated by the "units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /12/2015 01:54 PIN without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 aceAnalytical www.pocefabs.com QUALITY CONTROL DATA Project: Timken - Fall 2015 Pace Project No.: 92273923 QC Batch: WET/41157 Analysis Method: SM 25400 QC Batch Method: SM 2540D Analysis Description: 25400 Total Suspended Solids Associated Lab Samples: 92273923001, 92273923002 METHOD BLANK: 1596407 Matrix: Water Associated Lab Samples: 92273923001, 92273923002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 11/01/15 15:06 Pace Analytical Services, Inc. 205 East Meadow Road - SurteA Eden, NC 2728E (336)623-8921 LABORATORY CONTROL SAMPLE: 1596408 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 240 96 90-110 SAMPLE DUPLICATE: 1596409 92274207001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 173 179 3 SAMPLE DUPLICATE: 1596410 92273916001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND Results presented on this page are In the units In cleated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2015 01:54 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 LgC1 lytical rrnty. Aacsfabs. turn Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27288 (336)623-8921 QUALIFIERS Project: Timken - Fall 2015 Pace Project No.: 92273923 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Oiphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Chadotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2015 01:54 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical. www.PntelabS.=n QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: Timken - Fall 2015 Pace Project No.: 92273923 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92273923001 001 FLD! 92273923002 003 FLD/ 92273923001 001 EPA 1664B GCSV123160 92273923002 003 EPA 1664B GCSVI23160 92273923001 001 EPA 200.7 MPRP119949 EPA 200.7 92273923002 003 EPA 200.7 MPRP119949 EPA 200.7 92273923001 001 SM 2540D WETI41157 92273923002 003 SM 2540D WET141157 Date: 11/1212015 01:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ICP117986 ICP117986 Page 9 of 11 uccumen Sample Condition Upon Receipt SCUR u�`U111G1IPage 1 of 2* �- aC�Ark7lylr�71� Document Number: Issuing Authority: { _ F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Client Name: T ! M r I ti n ' Page 2 of 2 is for Intemal Use Only Courier: ❑ Fed E)❑ UPC] USP❑ Clier❑ Commerci;D Pace Other 0 tional .'. - Custody Seal on Cooler/Box Present: El yes C] no Seals intact: ❑ yes ❑ no prof. Name:' Packing Material: ❑ Bubble Wrap 0 Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1. 403 Type of Ice: Wet Blue None ❑Samples on ice, cooling process has begun Temn Correction Factor T142oNo Correction Corrected Cooler Temp ! 1 , `7 •C Biological Tissue is Frozen: Yes No/' WA 1 Date and Initials of person examining P rU�,2.`l contents: .A Temp should be above freezing to 6°C � Comments: Chain of Custody Present_ �� ClYes G]No ONIA 1. Chain of Custody Filled Out: ©Y s CBNo ONIA 2. %li; Chain of Custody Relinquished: i Oyes ❑Now❑w 3. Sampler Name & Signature an COC: ❑WrClNo ❑NIA 4. Samples Arrived within Hold Time: ❑Yea ONO ❑NIA 5. Short Hold Time Analysis <72hr): Oyes ONO ❑NIA 6. Rush Turn Around Time Requested: ❑Yes ONo ❑NIA 7. Sufficient Volume: i7Y s,❑No ❑NIA B. Correct Containers Used: dyes No ❑NIA 9. -Pace Containers Used: ElYes ❑No ❑NIA Containers Intact: ❑ es ❑No ❑NIA 10, _ Filtered volume received for Dissolved tests ❑Yes ❑No 0N11C 1. Sample Labels match COC: ❑Yes Chl ❑NIA 12. T i ^K a �a -� ` c r` (, ! L ey -Includes dateMmeAD/Ana sis Matrix: / 16 ' ? 7 I 1 j . U • `� An containers neecUM preservation have been checked. Yes []No ❑NrA 13. Ail containers needing preservation are found to be in 2Y es No ❑NIA compiiance with EPA recommendation- exceptions: VOA. c*om TOC, O&G• WWRO twater) ❑Yes ❑No / Samples checked for decNorination: ❑Yes ONO lac �• 14. IT 7 Headspac:e in VOA Vials (>Bmm): Oyes ONO 15_ Trip Blank Present: i ❑Yes ONO ZA 16. Trip Blank Custody Seats Present se []Yes ❑No Pace Trip Blanc Loi # (rf pur&msed': Client Notification) Resolution: Person Contacted: Comments/ Resolution: DateMcme: SCURF Review: Date V SRF Review: Date: L 5-1 Note, Whenever there is a discrepancy affeding North = compliance samples. a capy of this torrn uvf be sent to the HwO Carolina DEHNR Certification Office (ie out of hoA kKxued press native, out of tersp, insane[ containers} Field Data Required? Y I N WO#:92273923 II I II=73MII I II I �Ilul III Page 10 of 11 v'�? FaceAnalytical' 1".0acelahs.com CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed aoouratoiy. 0 7 Section A Section B Section C Pape: of Required Client Inlormation: Requirod Project Information: Invoice information- Company: Report Tor Altanti 2003367 ^� _ } ,+^� m Ct CK rL-kQ V_i eLL , �� ��tG�i�+';c� Address: 3 _'f11� ' Y-ti `r iY Copy To: Company Name: T! M Lr1J REGULATORY AGENCY rh' ire iQ: %;Nr11J r� C. 1-7 31l Address: '}W�NPDES I" GROUND WATER r" DRINKING WATER r UST 1" RCRA r OTHER Email To: purchase Order No.: peal 0-to i Rpinrnncw Phnne: as Project Name: ,,,� I I MIG O EAVLL 21iS' face Pr atnct fit:irtnil.*: A 7 LL ��E Site Location STATE' C' Requested Due DatefTAT: Project Numeer: 11ace Nrotiio x; rt f_ �L lfL Requested Analysis Filtered (YIN) Section D Matrix Codas ,� 5 ti ~ 7 RegRlrcd Giant Inlcrroob- MAIRI% ! CODF o• o � COLLECTED Presarvolivos N r Drinkimi Witter DW 0 Water W7 Waste Walcr UJW Product P K u to COMaoslrr, $TART Cnxs=aslle ENDIGRAR U w J 41 Soil#solid SL y ti SAMPLE ID wpe WP " N 4, [A•Z. 0-9 r ,-] Air AR to d a }- � � I I t ��J� ��Z✓ c� Sarnplo IDs MUST BE UNIQUE Tisxue TS Q U r M ry r. r `\ Other OT (n V w a LL W U 0 ~ { n DATE TIME onrl: TIME *k a z Z O y Y Pace Project Na.l Lab I.D. 2 CC ��C}U r`' � 7 C J J 4 1AI Is< 7f 5 ) 5- Q Z it I x s ,,0`` v �-% V �- Vy V�/ 7 s 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY t AFFILIATION DATE TIME ACCEPTED BY ! AFFILIATION DATE TIME 9AMPLH CONDITIONS L..GnS't51: 7�00 ~i t l_o I'n�i `� /��!✓ '�'. .r �ir.,��t rtr .�GI G'r Vr � 1•% � htC �%f -r 1) ORIGINAL SAMPLER NAME AND SIGNATURE U 9� PRINT Name of SAMPLER: y� rt C. jf~ n7 �1 ti r SIGNATURE of SAMPLER DATE 3ipned C� {MWODmjt Z 7 S 'ImTwnant Nam: By sipnmq Ink lorin YOU Artt aca.pwil PAcu's NEl 30 day prynwnt farms and aereein<,t to l.rtn chanty of 1.5% per .ontn tar my invoice. not l -thin 30 days, 4!-ALL-0.020rov.01, 18-stay-2007 Semi-annual Stormwater Le"Charge Monitoring Report • for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted - S CERTIFICATE OF COVERAGE NO. NCG03 v Oki Z FACILITY NAME _ lMK—, 0 jlJ 0,a COUNTY _28-20OL-PH PERSON COLLECTING SAMPLES LABORATORY VA,CA-a— Lab Cert. # Z Comments on Sample collection or analysis: Part A: Stormwater Benchmarks.and Monitoring Results SAMPLE COLLECTION YEAR _Z C t5 SAMPLE PERIOD [K Jan -June ❑ July -Dec or ❑ Monthly' (month) p DISCHARGING TO CLASS ❑ORW ❑HOW []Trout❑PNA f � �ErVEn ❑Zero -flow [Kwater Supply ❑5A= LJ [:]Other— � CUN 2 G z015 � ►vr PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 DwR SECTlpN L& ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, .Inches; Total Suspended Solids pH; Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons TotaelaT'exic Organics5 Benchmarks 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L UV L .�i21 -ZS `�� Z M L (S, 0047- Al O `.1 !I 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. ;The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469,22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible forma nagingcompliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) (Y1RUA4isE QQI()M&i 2CUA41L<IIt,! Title (Print title) (Signature) (Date) Note: Results must be,reported in numerical format. Do not report Below Detection Limit, BDL; <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. t Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) ' Total Suspended Solids pH Benchmarks --=> _ 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part 8 * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit D /1/2012-10/31/2017 SWU-245, last revised Page 2 of 3 Note: If report a sample value in excess of the benchmark, you must im0ent Tier 1, Tier 2, or Tier 3 responses. See General Permit text. 0 t FOR PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO [j IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy otthis DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 �PaceAnai ical' wwtv.Racelabs.cam CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. Ail relevant fields must be completed accurately, Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: q ry ,q fy Gompany; Report To: r Attention: E -RI L �- L, i -Y-1 A) Ci t-- 2 Jh 0 1 L Addl4:; O 7.O PL_ Copy To: Company Name: A] I m REGUTATORY'AGENCY ' i-QAAQ . N r- Z 73 j Addres �C�C) ; NPDES .GROUND WATER j DRINKING WATER r UOTHER LIST r RCRA j� Email To: j Purchase �trm Order No,; Pace Quote - tl �tir�� Reference Phone: Fax: Project . .. rr- 7 --Z4;ZS Name: 1 J C I,h Ler/ 201. Pace Project �s Manager: avn 1 )�. -Le U\ tjft Site Site Location STATE: , - Requested Due Data TAT:' Project Number: Pace Profile q. Requested.Analysis,Fiitered:(Y1N)'. - _• Section Matrix Codes a`z-' Required Chant Information MATRIX,f CODE .g COLLECTED Preservatives prinking Water DW (J Z11 O • ` Water WT Water WW � m CpMPO3 COMPOSITE: eOMPOSirE " 1� Product START ENacrne t~Vu Z Soil/Solld SL SAMPLE ID oil ,°p �_ w W +` e (A-Z,0-91,-) Airp AR p w .o. Z Sample IDs MUST BE UNIQUE Tissue TS O IL - F a) ^ N " '� ` I t U Ocher OT . XLLJ ' DATE TIME 'DATE TIME u) i X X z z O, „y � Pace Project Il Lab I.D. 1' a) — tlU 2 .4 _ t� ca j 6 Qc, -75 -3 za a. 9 10 11 12 - ..ADDITIONAL COMMENTS `' RELINQUISHED BYJ AFFILIATION 'DATE TIME 'ACCEPTED BY I AFFILIATION DATE, .TIME SAMPLE CONDITIONS Pcckse A 0o -ra_ 0-erf L7 -3 J i+ (tltlr"1v+�tJRIGII�AL SAMPLER NAME AND'SIGNATURE c 6 z o^ m c z m o C) z a z a } PRINT Name of SAMPLER: I F�,G i �iy � ' I" m `—' U m E DATE Signed a SIGNATURE of SAMPLER: (MMIDDIYY): 'Z J cn m I ul Im ortant Note: By signing this form YOU are accepting Pace's NET 30 day g g charges p y r y y • p g g y p g y payment terms and a reeln to lots cha es of f.5� per month for an mvaces n aid uritgin 30 days, F-ALL- �02Drev.07, 15-Ma -20 aceAnalytrcal r www.pacoh?bs.com I June 18, 2015 Mr. Rick Flickinger Timken Company 3500 Timken Place Randleman, NC 27317 RE: Project: TIMKEN SPRING WATER 2015 Pace Project No.: 92251159 Dear Mr. Flickinger: Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 2728E (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on May 22, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell taylor.ezell@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 Pace Analytical Services, Inc. aceAnalytical a 205 East Meadow Road -Suite A Eden, NC 27288 wwwpacelabs.mm (336)623-8921 CERTIFICATIONS Project: TIMKEN SPRING WATER 2015 Pace Project No.: 92251159 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloddalNELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shait not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalytical wwN pacelabs.com Project: TIMKEN SPRING WATER 2015 Pace Project No.: 92251159 Lab ID Sample ID 92251159001 001 92251159002 003 SAMPLE ANALYTE COUNT Method EPA 1664B EPA 200.7 SM 2540D EPA 1664B EPA 200.7 SM 2540D REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Analytes Analysts Reported laboratory CLW 1 PAS I-C JMW 3 PAS! -A WRC 1 PASI-A CLW 1 PAS I-C JMW 3 PASI-A WRC 1 PASI-A Page 3 of 11 - Mnalytkal f www.pacelabs.can ANALYTICAL RESULTS Pace Analytical Services, Inc. 205 East Meadow Road -Suite A Eden, NC 27288 (336)623-8921 Project: TIMKEN SPRING WATER 2015 Pace Project No.: 92251159 Sample: 001 Lab ID: 92251159001 Collected: 05/21/15 00:00 Received: 05122/15 09:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual Field Data Collected By Collected Date Field pH Field Temperature HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Analytical Method Rick 1 06/03/15 17:37 Flickinger 5121IM5 1 06/03/15 17:37 6.93 Std. Units 0.10 1 06/03/15 17:37 76 deg C 0.50 1 06103/15 17:37 Analytical Method: EPA 1664B ND mg/L 5.0 1 06/03/15 08:13 Analytical Method: EPA200.7 Preparation Method: EPA200.7 6.2 ug/L 5.0 1 05/27/15 15:00 05/29/15 02:12 7440-50-8 ND ug/L 5.0 1 05/27/15 15:00 05/29/45 02:12 7439-92-1 32.3 ug/L 10.0 1 05127/15 15:00 05/29/15 02:12 7440-66-6 Analytical Method: SM 2540D 9.2 mg1L 2.5 1 05/28/1515:15 Sample: 003 Lab ID: 92251159002 Collected: 05/21/15 00:00 Received: 05/22/15 09:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Collected Date Field pH Field Temperature HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Date: 06/18/2015 04:08 PM Analytical Method Rick 1 06/03/15 17:38 Flickinger 5121115 1 06103/15 17:38 7.20 Std. Units 0,10 1 06/03115 17:38 72.5 deg C. 0.50 1 06/03/15 17:38 Analytical Method: EPA 1664B ND mg/L 5.0 1 06/03/15 08:13 Analytical Method: EPA 200.7 Preparation Method: EPA200.7 5.1 ug/L 5.0 1 05/27/15 15:00 05/29/15 02:16 7440-50-8 ND ug/L 5.0 1 05/27/15 15:00 05/29/15 02:16 7439-92-1 10.6 ug/L 10.0 1 05/27/15 15:00 05/29/15 02:16 7440-66-6 Analytical Method: SM 2540D 4.6 mg/L 3.1 1 05128/1515:15 REPORT OF LABORATORY ANALYSIS This report shag not be reproduced, except in full, WOW the written consent of PaceAnalyticat Services, Inc.. Page 4 of 11 aOAnalytical wwtr. pacelabs.com i QUALITY CONTROL DATA Project: TIMKEN SPRING WATER 2015 Pace Project No.: 92251159 QC Batch: GCSV121523 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92251159001, 92251159002 METHOD BLANK: 1473399 Matrix: Water Associated Lab Samples: 92251159001, 92251159002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 5.0 06/03/15 08:06 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 LABORATORY CONTROL SAMPLE: 1473400 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 37.7 94 78-114 MATRIX SPIKE SAMPLE: 1473401 92251179001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 38.6 96 78-114 Results presented on this page are in ttia units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/18/2015 04:08 PM without the written consent of Pace Analytical Services, Inc- Page 5 of 11 aceAnalytical www.paceJabs.am I I QUALITY CONTROL DATA Project: TIMKEN SPRING WATER 2015 Pace Project No.: 92251159 QC Batch: MPRP118556 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92251159001, 92251159002 METHOD BLANK: 1468601 Associated Lab Samples: 92251159001, 92251159002 Parameter Units Copper uglL Lead ug/L Zinc uglL Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 05I29115 00:52 ND 5.0 05/29/15 00:52 ND 10.0 05/29/15 00:52 Qualifiers Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 LABORATORY CONTROL SAMPLE: 1468602 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper uglL 500 509 102 85-115 Lead uglL 500 481 96 85-115 Zinc uglL 500 460 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1468603 1468604 MS MSD 92254133003 Spike Spike MS MSD MS MSD % Rec Parameter units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper uglL 685 500 500 1210 1170 105 96 70-130 4 Lead uglL 9.8 500 500 516 468 101 92 70-130 10 Zinc uglL 949 500 500 1390 1360 88 82 70-130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1468605 1468606 MS MSD 92251497008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper uglL ND 500 500 554 508 111 101 70-130 9 Lead uglL 11.5 500 500 514 470 100 92 70-130 9 Zinc uglL 74,9 500 500 561 517 97 88 70-130 8 Results presented an this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date'.0611812015 04:08 PM without the written consent of PaceAnalytical Services, Inc.. Page 6 of 11 aCMnalyflcal www.pacelabs.00m QUALITY CONTROL DATA Project: TIMKEN SPRING WATER 2015 Pace Project No.: 92251159 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QC Batch: WET137738 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92251159001, 92251159002 METHOD BLANK: 1469739 Matrix: Water Associated Lab Samples: 92251159001, 92251159002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 05128/15 15:10 LABORATORY CONTROL SAMPLE: 1469740 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 262 105 90-110 SAMPLE DUPLICATE: 1469741 92251021001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1469742 92251044001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/18/2015 04:08 PM without the written consent of Pace Analytical Services, Inc- Page 7 of 11 __ i 6Analytrcal www.pacera6s.corn f ) QUALIFIERS Project: TIMKEN SPRING WATER 2015 Pace Project No.: 92251159 Fs1WM Ii_H@U,] Pace Analytical Services, Inc. 205 East Meadow Road - Suite Eden, NC 27288 (336)623-8921 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA.guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP -Sample Duplicate RP - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anaiytes. TNI - The NELAC Institute. LABORATORIES PAS I -A Pace Analytical Services - Asheville PAS I-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/18/2015 04:08 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical www.PaceJ2bS.WM QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: Pace Project No.: TIMKEN SPRING WATER 2015 92251159 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92251159001 001 FLD! 92251159002 003 FLD/ 92251159001 001 EPA 1664B GCSV121523 92251159002 003 EPA 1664E GCSV121523 92251159001 001 EPA 200.7 MPRP118556 EPA 200.7 ICP116646 92251159002 003 EPA 200.7 MPRP118556 EPA 200.7 ICP/16646 92251159001 001 SM 2540D WET137738 92251159002 D03 SM 2540D WETI37738 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/18/2015 04:08 PM without the written consent of Pace Analytical Services, inc.. Page 9 of 11 eeA1i<11ytrlN, Sample Condition Upon Receipt SCUR Page 1 of 2+ Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Client Name: t t-Page 2 of 2 is for Internal Use Only Courier: ❑ Fed Ex ❑ UPS LISPS❑ Client❑ Commercial❑ Pace Other Q"'tlni181a5kti: Custody Seal on Cooler/Box Present: ,0 yes ❑ no Seals intact: yes ❑ no Packing Material: ❑ Bubble VDp fQ't3ubble Bags ❑ None ❑ Other Thermometer Used: I Gun T1401 Type of Ice: lue None ❑ Samples on ice, cooling process has begun Temp Correction Factor T1401 No Correction J Corrected Cooler Temp.: -)•(�! -C Biological Tissue is Frozen: Yes No A Temp should be above freezing to VC Comments: Date and Initials of person examining a contents: � Chain of Custody Present: ryes ONO ❑NIA 1. Chain of Custody Filled Oul: - fes ONO ❑NIA 2. Chain of Custody Relinquished; Ayes ❑No ❑MIA 3. Sampler Name & Signature on COC: Ayes ❑No ❑NIA 4. Samples Arrived within Hold Time: pYe"s ONO ❑NIA 5. Short Hold Time Analysis <72hr : ❑Yes WWo ❑NIA 6. Rush Turn Around Time Requested: ❑Yes No ❑NIA 7. Sufficient Volume: ,oY ONO ❑WA S. Correct Containers Used: es ON, ❑WA -Pace Containers Used: lames ONO ❑NIA 9. Containers Intact_ Ades ❑No ❑NIA 10. Filtered volume received for Dissolved tests s ONO ❑NIA 11. Sample Labels match COC: es ❑No UNIA -Includes dalettimeAD/Anal sis Matrix: 4-1 12. An containers needxV preservation have been checked. oes 11t4o ©NIA All containers needing preservation are found to be in Rves ONO DIVA compliance %vrth EPA recommendation. C exceptions: VOA, cokbm% TOC, O&G, Wt-DRO (water) ❑Yes No 13. Samples checked for dechlorination: ❑Yes ONO ,9 A 14- Headspace in VOA lftals >Smm : ❑Yes ❑No BWA 15, Trip Blank Present: CIYes ❑No j2a Trip Blank Custody Seals Present Dyes ❑No,,,QtGiA Pace Trip Blank Lot # ifpurchased): - — - 16, Client Notification/ Resolution: Field Data Required? Y ! N Person Contacted: Dateliune: Comments/ Resolution: SCURF Review: Q'V Date: I 1-22 SRF Review Data• Note- Whenever there is a drurxepancy aliecting North Carorma compffame sarmrptes, a copy of thiis €arm vA be sent to the North Carolina DEHM Certibcation Ofte ( Le out of hoW. incorrect preservative, out of teaw, incorrect eontamers) t, W0t:92251159 1111111111111111111111 Page 10 of 11 -FraceAnalytrcal' CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain•of•Cusfady is a LEGAL DOCUMENT. All relevant holds must be completed accurately. www,pacerabs.Cem P-09o. of Section A Section B Section C I- r •r (^1 Requirod client Information; Requlmd Project Informaton; Invoice Wormation: Company,... • Report To: .7� Attention: _ 1 !f'"i`f '�' •° L.L }��Lc- tr�:G•�{` tC i-r LC.z cs%- , Address: i f - t"`4 Copy To: Company Name: 'I^•' - /J v REGULATORY AGENCY - 1 ^� r ^- �t X-NPDES f- GROUND WATER 7 DRINKING WATER �"' UST ;"' PORA i OTHER Emarf To: 1 4.1 ,,,,J Purchase Omar No.: PQCQQuoie Phone: _ � c ._ - -, • .- . 2.C:."L3 Fax: Project I�amC: �. r-. l�'ilC.i=r�+ ,] �r �.�. C.:�="Z:S: �: Porn Proledt ,�. Manager, .'iV 1L L�, i ••ir�ftVl ir� 'S LoostEan Srp'Et Requested Dub DateJTAT: Project Nurnw. Porn Proft 9: /�. Ly ` Requested Analysis Filtered (YIN) Section 0 Matrix Codes 2 RequimdCtent tnformadon MATRIX t CODE 3 COLLECTED Preservatives P 1 DrinNing Water ow Water WT wastevvater ww m C9��OSR� COWOsrTli Y V ` t� J Product P So1115Quo SL $TART E�Dreana w F w tom, % = . SAMPLE ID oil DL �; r� � .. �, r- j- w,pe wP (A-Z, 0-91:) Air AR w p m a w H t Sample 10s MUST BE UNIQUE Tissue TS O a w �' a • , • s S Other nT a ~ DATE TIME DATI; TIME r z Z z �.i IX Pace Pro oat No./ Lab I.D. 2 " .. t ; Z. f44 Es t Jf X S 4 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I APRUATION DATE TIME SAMPLE CONDITIONa �Jf�IGtE`!AL SAMPLER NAME AND SIGNATURE 6 ' e G PRINT Namo of SAMPLER: •� 1 C..,�. 1�'� iw'.- SIGNATURE of SAMPLER;n 11 DATE Slyned C Tt (MMIDD JZ I 'Imponam Note: By signing this form you are somplinp Pace's NET 30 day paymbnt terms and egrooing to lase cnargos or 1.5 R per month fof any Irrvolom maid +filhin 10 days. F-ALL-Q-020rov.07, 1$-May-20C7 Semi-annual Stormwater Aharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 2%'Zy — / `/ CERTIFICATE OF COVERAGE NO. NCG03 D d -2 SAMPLE COLLECTION YEAR Z k4 FACILITY NAME T/M(CCU) — Prsf- Gow Pi.lw r SAMPLE PERIOD ❑ Jan -June [,July -Dec COUNTY !�PL DQ(_ Of or ❑ Monthly' (month) PERSON COLLECTING SAMPLES �. LCY.,IiV ` DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY PW )4)&y neAL Lab Cert. # �_ ��+�1� !ED ❑Zero -flow Water Supply ❑SA Comments on sample collection or analysis: v i V ❑Other_ DEC 02 zfl14 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL. FILES Part A: Stormwater Benchmarks and Monitoring Results DWR SECTION IV d - JI,Jt.� i c�C�L�G7gn ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L (3 co i I N a -7. Z.Z. NJ ND 033 b o 14 . '7 .-7 in f If -7. 5 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensiti%4 receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). ; Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible form an aging compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that tot he best of my knowledge and belief, no dumping of concentrated toxic organics into the storm water or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." e-wl oc Cl I N4IL Name (Print name) Title (Print title) 6 /1--zo -t V (Signature) ( Date) Note:'Results must be reportedin numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other, similar non -numerical format.' When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. (Vote:' if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Disl/1/2012-10/31/2017 0 SWU-245, last revise 25/2012 Page 2 of 3 1 Note: if Joreport a sample value in excess of the benchmark, you must imorent Tier 1, Tier 2, or Tier 3 responses. See General Permit text# FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. + TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 3U daVs of receipt of the lab results or at end o monitorin period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 g aceAnalytical www.pacokbs.com November 12, 2014 Mr. Rick Flickinger Timken Company 3500 Timken Place Randleman, NC 27317 RE: Project: TIMILEN Pace Project No.: 92224251 Dear Mr. Flickinger: Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Liamm Carrubba liamm.carrubba@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without thew ritten consent of Pace Analytical Services, Inc.. Page 1 of 11 aoAnalytical w*w.pac@Mbs.wrn CERTIFICATIONS Project: TIMILEN Pace Project No.: 92224251 PaeeAnalyticaI Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Charlotte Certification IDs 9800 Kinsey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiafVELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia[VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Anaty ical Services, Inc.. Page 2 of 11 aceAnalidical www.pacelabs.corn SAMPLE ANALYTE COUNT Project: TIMILEN Pace Project No.: 92224251 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Anatytes Lab ID Sample ID Method Analysts Reported Laboratory 92224251001 001 EPA1664B CLW 1 PAS I-C EPA200.7 JMW 3 PASI-A SM 2540D MDW 1 PASI-A 92224251002 003 EPA 1664E CLW 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalytical mvwpacelaDs.mm ANALYTICAL RESULTS Project: TIMILEN Pace Project No.: 92224251 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Sample: 001 Lab ID: 92224251001 Collected: 11/01/1409:15 Received: 11/05/1413:25 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Analytical Method RF 1 11 /01114 09:15 7.22 Std. Units 0.10 1 11101/14 09:15 Analytical Method: EPA 1664B ND mg/L 5.0 1 11 /06114 07:51 Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 ND ug1L 5.0 1 11/06/14 15:05 11/10/14 20:05 7440-50-8 ND ug1L 5.0 1 11/06/14 15:05 11/10/14 20:05 7439-92-1 33.1 ug/L 10.0 1 11/06/14 15:05 11/1011420:05 7440-66-6 Analytical Method: SM 2540D ND mg/L 3.0 1 11/0711410:16 Sample: 003 Lab ID: 92224251002 Collected: 11/01/14 09:15 Received: 11/05/14 13:25 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By RF 1 11/01/14 09:15 Field pH 7.54 Std. Units 0.10 1 11/01/14 09:15 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 11/06/14 07:51 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND uglL 5.0 1 11/06/14 15:05 11110/1420:24 7440-50-8 Lead ND uglL 5.0 1 11/06/14 15:05 11/10/14 20:24 7439-92-1 Zinc 16.7 uglL 10.0 1 11/06/14 15:05 11/10/1420:24 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 7.7 mg/L 3.0 1 11/07/14 10716 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /12/2014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalytical wwwpacofabs.= QUALITY CONTROL DATA Project: TIMILEN Pace Project No.: 92224251 QC Batch: GCSVl19400 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92224251001, 92224251002 METHOD BLANK: 1323366 Associated Lab Samples: 92224251001, 92224251002 Parameter Units Oil and Grease mglL LABORATORY CONTROL SAMPLE: 1323367 Parameter Units Oil and Grease mglL Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336}623-8021 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11 /06114 07:37 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 37.1 93 78-114 MATRIX SPIKE SAMPLE: 1323368 92224149002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL ND 40 33.8 84 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalytical www.pacefabs.crnm QUALITY CONTROL DATA Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: TIMILEN Pace Project No.: 92224251 QC Batch: MPRP117285 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92224251001, 92224251002 METHOD BLANK: 1323877 Associated Lab Samples: 92224251001, 92224251002 Parameter Units Copper ug/L Lead ug/L Zinc ug/L Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 11/10/1419:59 ND 5.0 11/10/1419:59 ND 10.0 11/10/1419:59 Qualifiers LABORATORY CONTROL SAMPLE: 1323878 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug1L 500 492 98 85-115 Lead ug1L 500 491 98 85-115 Zinc ug1L 500 480 96 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1323879 1323880 MS MSD 92224251001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 511 510 101 101 70-130 0 Lead ug/L ND 500 500 498 498 99 99 70-130 0 Zinc ug/L 33.1 500 500 523 523 98 98 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1323881 1323882 MS MSD 92224290007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 47.3 500 500 560 552 102 101 70-130 1 Lead ug/L 13.7 500 500 498 490 97 95 70-130 1 Zinc uglL 329 500 500 810 802 96 95 70-130 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 e aceAnalytical www.pacaab3.corn QUALITY CONTROL DATA Project: TIMILEN Pace Project No.: 92224251 QC Batch: WETI34152 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92224251001. 92224251002 METHOD BLANK: 1324884 Matrix: Water Associated Lab Samples: 92224251001. 92224251002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 11/07/14 10:14 LABORATORY CONTROL SAMPLE: 1324885 Parameter Units Total Suspended Solids mglL SAMPLE DUPLICATE: 1324886 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1324887 Parameter Units Total Suspended Solids mg/L Spike LCS LCS Conc. Result % Rec 250 238 95 92224365001 Dup Result Result 356 364 92224606001 Dup Result Result 135 128 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 % Rec Limits Qualifiers 90-110 RPD Qualifiers 2 RPD Qualifiers 5 Results presented on this page are in the units Indicated by the -Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/1212014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnalytical www.pacelabs.wrn QUALIFIERS Project: TIMILEN Pace Project No.: 92224251 DEFINITIONS Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aoAnalytrcal www.pacalabs.00rn QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 205 East Meadow Road - SulteA Eden, NC 27288 (336)623-8921 Project: TIMILEN Pace Project No.: 92224251 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92224251001 001 FLD! 92224251002 003 FLD/ 92224251001 001 EPA 1664E GCSV119400 92224251002 003 EPA 1664B GCSV119400 92224251001 001 EPA 200.7 MPRP117285 EPA 200.7 92224251002 003 EPA 200.7 MPRP117285 EPA 200.7 92224251001 OD1 SM 2540D WET134152 92224251002 003 SM 2540D WET134152 I�i���It�],wZ7L�iY7ki•�,u. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Ana4ocal Services, Inc.. ICP115582 ICP115582 Page 9 of 11 -.�ceAr�tylical Condition UponrReceip, Document Number: F-CHR-CS-003-rev.15 CUR Pa e 1 of 2 Issuing Authority: Pace Huntersville Quality Office Client Name: rc Courier: Fed Ex ' UPS USPOther---- Custody ❑ ❑ S❑ Client❑ Commercial❑ Pace O tloflal Y...- il t.,. ''1.�d(B . 9 Seal on Cooler/Box Present: ❑ yes no Seats intact: El yes ❑ no �,� •-� Packing Material: ubble 1�p ❑ Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun' T1401 Type of Ice: iV Blue None Samples on ice; cooling process has begun Temp Correction Factor 71401 No Correction Corrected) Cooler Tem �• �C p•� Temp should be above freezing to 6°C Biological Tissue is Frozen: Yes No i Comments: Date and )Hill is Rf pars n exa Ir Ing contents: �t" �� �_ �t1 Chain of Custodx Preseni: ❑ es ❑No ❑WA 1. Chain of Custody Filled Out: E41es. []No ❑NIA 2. Chain of Custody Relinquished: (--]Yes E9 o ❑WA 3. Sampler Name & Signature on COO: es [---]No ❑NIA 4. Sam les Arrived within Hold Time: 14es ❑No ❑NrA 5. Short Hold Time Analysis <72hr : ❑Yes m 11 WA 6. Rush Turn Around Time Requested: ❑Yes Q o ❑NIA 7. Sufficient Volume: e es No ❑WA 8. Correct Containers Used: -Pace Containers Used: Yes No es UNo ❑WA ❑WA 9. Containers Intact: es ❑No ❑WA i0. Filtered volume received for Dissolved tests ❑Yes No 0 11. Sample Labels match COC: r 5 -Includes datellimeADlAnat sis Matrix: es ®a ❑WA V. _ AA g r s 5W P ,-- t r^lh4lS i (vif' eifi rtoeG;rigpreseryaEton !rave been ilfy6s Ufio AU containers needing preservation are found to be in ".No compliance with EPA recommendation. exceptions: VOA, coliform, TOC, o&G, VA-DRO (water) UYes ❑I4o UWA ❑Ntp 13: Ei5�2 tf _ /"LPf-�rEj 5 - S S 6. 6, e L� Samples checked for dechlorination: ❑Yes ❑No 0 rA 1 . Headspace in VOA Vials >8mm): ❑Yes []No 0 A Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased : OYes ❑No []Yes []No NfA Client Notification/ Resolution: Field Data Required? Y i N . - Person Contacted: Datelrrne: Commenlst Resolution: . SCURF Review: [.0 • Date: li SRF Review: iDate: •S_ We: Whenever there is a discrepancy affecting North Carolina oompdianoe samples, a copy of this form will be sent to the North Carosna DENIM Certification Office ( Le out of hold, incorrect preservative, out of tempo inoorrect containers) mace lacer Here f117 rem rh....... ,51 i Page 10 of 11 2ceAna6&ical- CHAIN-OF-CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately, ° m Suction A Section B Section C Paget of i Requlrod Client information: Rogtftred Project trdormaLon: Invoice Information: Company. Report ro: ILK = Ll L� l 1�+4 G rc Attenlion�R t ` - L C IC rNCB E' it 1790606 Aadr, jG0 ! to QL'Ac t5, �Tv Company Name: .J1oKe�') REGULATORY AGENCY ANL-ElIl19fJ A� Z `� Atltlre C Jti rn1 rn) NPDES i GROUND WATER ?— DRINKING WATER i UST F RCRA i OTHER EmaII To: (( � Purchase Order No.: Paea D�oEa S1' 1"311 'ii e�i rCJ�' Reference; Prone: • r Fax: � Pro;ecl Name: ,� _ _ f 1 /Yj I (. r� Poor Project Manager. L1 lZ r� U Site LOCpRIOn STATE• J�, �• Requatted Duo DaterTAT: Project Number. Paw Prardd a • �—t^r ,r-^, r^ i Requested Analysis Filtered (YIN) Section D Matrix Codes eq Rubcd Cpontln10 ban MAT t, 1000E s COLLECTED Preservatives P Drinking wager Dw water wT $ �; ww vduc F mCg AR&TE R pasaPwater w {� aL SoiVSoGSL SAMPLE ID Wipe wP x �' fL W w ' a \ {A z aT BE TAird AR Semple IDs MUST BE UNIQUE Tdave TS w p Q 5 aY F '0 v l 1 Othor OT L5 w O J� (CI► to ..� U y O ?+ W $~ �d qa 0 LL c y Z �3 A e5 d a i� — L N DATE TIME D47E TIME v+ 2 Z 2 Z Z g Pace Pro eGt No ! LobI.D. 6i� I 00 I C t+Ir 9: 5- 2 4 3- cot QU s O" - U2 ] �C r s 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TWE ACCEPTED BY! AFFILIATION DATE TIME SAMPLE CONDITIONS roc 1 f IiCj1Cv/lt!0 .9k� I �l SAMPLER NAME AND SIGNATURE U PR]NT Name Of SAMPLER: �i c.tc �E~tcKrrVG C-',;iGI N`-A SIGNATURE of SAMPLER: DATE Slgnod tMWDDNY): ii Lily •Importam: Note: fly sigring m,a fonm YCu arc *=v9 ng Paroh NET 30 day payment tame and agreeing to iste charges or 1.5% per month for any inwims net aid wm� 30 days. F-ALL-0-020rev.07.1 s-MayaaOr ft TIMKEN Where You Turn Richard Flickinger Manager- Equipment Reliability The Timken Company Mail Code: ASB-01 3500 Timken Place Randleman, NC 27317 United States Telephone: 336-495-2625 Facsimile: 336-495-2661 May 8, 2014 NC Dept. of Environment, Health, and Natural Resources Division of Water Quality aMail Service Center "uE�V � Raleigh, NC 27699-1617 E JUN 0 3 2014 Attention: Central Files CENTRAL FILES DWQIBOG Please find enclosed the following: • The original and one copy of the Semi -Annual Stormwater Discharge Monitoring Report • Two copies of the actual test results from Pace Analytical Services, Inc. If you need any additional information, please do not hesitate to contact me at (336) 495-2625, or you may send inquiries to the following address: Rick Flickinger The Timken Company 3500 Timken Place Randleman, NC 27317 Sincerely, Rick Flickinger Manager -Equipment Reliability cc: Josh Gaub — Corporate EH&S RECEIVED JUN 0 9 n !4 CENTRAL f ILES �'Mn. q Rrtn' dck.flickinge<@timken.com Semi-annual Stormwater Akharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted Zo I CERTIFICATE OF COVERAGE NO. NCG03 0 0 1 Z FACILITY NAME 7-/ oiy C0 — PtiS_k{L?YLD PLAN T COUNTY '_�000L.PH PERSON COLLECTING SAMPLES LABORATORY I�kC R,* -J1 I CetL_ Lab Cert. # 1 'Z Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 7- 0 I y SAMPLE PERIOD KJan-June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow 4Watersupply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --> No discharge this period?' Outfall No. -Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks ===> o.4 z I - 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 2S 1 C? , 4 0 { .y S. �I u l L '� O; as U g -7 1 S Cho 3 n; y p« z 2 1L, zo, 6 aS bq, .0 - s 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement fort otal toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." cK F-k- tc�_t 0 q c R- Name (Print name) ih At,)A <e2 - C Qu (pMk �-j �E1`�Ft131L li y Title (Print title) Qk J4 (Signature) (Date) Note: Results must be reported•in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 5o mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit D 1/1/2012-10/31/2017 SWU-245, last revised 25/2012 0, Page 2 of 3 Note: if *report a sample value in excess of the benchmark, you must im'Gent Tier 1, Tier 2, or Tier 3 responses. See General Permit text.�� FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO t, IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days ot receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." {Signature of Perm (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater L�charge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted _,:� —`i _ Z(:,Py CERTIFICATE OF COVERAGE NO. NCG03C) 0 `4? FACILITY NAME _ 'Ti�►�(�E� --_I�St�I:[(CD (�trAN r COUNTY vy ppLPii _ PERSON COLLECTING SAMPLESi LABORATORY_,NC- CNL- Lab Cert. #i 1 Z _ Comments on sample collection or analysis: Part A: Stormwater Benchmarks.and Monitoring Results SAMPLE COLLECTION YEAR Z 0 1 SAMPLE PERIOD XLJan-June ❑ July -Dec or ❑ Monthly' month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero-f'low KWaterSupply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --> ❑ No discharge this period?' Outfali No. Date Sample. Collected' _[mo%dd/yr): 24=hour:raihfall amount, Inches3 Total Suspended Solids pH, • Stan"dard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks =__> c�,ilz;51 - 10a mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L L� o y i 1 swt vo -7 003 d, 0" 26s r ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes.- For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible forma nagingcompliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) a (Signature) (Date) Note: Results must be reported.in numerical format. Do not report Below Detection Limit, BDL, <PQL, Nan -detect, ND, or other similar non -numerical format. When results are below the applicable limits, the must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: !f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected (mo/dd/yr) 24=hour rainfall amount, inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> . _ 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit DrO_"1" �1/1/2012-10/31/2017 SWU-245, last revised!'25/2012 �__J/ Q. Page 2 of 3 Nate: !f report a sample value in excess of the benchmark, you must irrmOtent Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results; (or at end of monitoring period in the case of "No Discharge" reportsto: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 IaceAnalyticalo (�mvw. pacelabs.com May 07, 2014 Mr. Rick Flickinger Timken Company 3500 Timken Place Randleman, NC 27317 RE: Project: TIMKEN Pace Project No.: 92199094 Dear Mr. Flickinger: Pace Analytical Services, Inc, 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on April 29, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Liamm Carrubba liamm.carrubba@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written Consent of Pace Analytical Services, Inc.. Page 1 of 11 aceAnalytical "".PacelaDa.wm Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 CERTIFICATIONS Project: TIMKFN Pace Project No.: 92199094 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDS 2225 Riverside Dr., Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fink, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 e acmnalytical mrw pacelab3.=n SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: TIMKEN Pace Project No.: 92199094 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92199094001 001-001 EPA1664B CLW 1 PASI-C EPA200.7 JMW 3 PASI-A SM 2540D ❑AS 1 PASI-A 92199094002 003-001 EPA 1664B CLW 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D DAS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalytical www.pxWabz.=n ANALYTICAL RESULTS Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: TIMKEN Pace Project No.: 92199094 Sample: 001-001 Lab ID: 92199094001 Collected: 04/25/14 13:45 Received: 04/29114 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By Rick 1 05/07/14 10:31 Flickinger Collected Date 4125114 1 05/07/14 10:31 Collected Time 13:45 1 05/07/14 10:31 Field pH 6.90 Sid. Units 0.10 1 05/07/14 10:31 HEM, Oil and Grease Analytical Method: EPA 16648 Oil and Grease NO mg/L 5.0 1 04/30/14 10:14 200.7 MET lCP Analyticat Method: EPA 200,7 Preparation Method: EPA 200.7 Copper 16.3 ug1L 5.0 1 04/30/14 16:00 05/05/14 21:29 7440-50-8 Lead ND ug/L 5.0 1 04/30/14 16:00 05/05/14 21:29 7439-92-1 Zinc 87.4 ug/L 10.0 1 04/30/14 16:00 05/05/14 21:29 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540❑ Total Suspended Solids 45.6 mglL 10.0 1 05/02/14 15:20 Sample: 003-001 Lab lD: 92199094002 Collected: 04/25/14 13:45 Received: 04/29/14 09A5 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By Rick 1 05/07/14 10:32 Flikinger Collected Date 4125114 1 05/07/14 10:32 Collected Time 13:45 1 05/07/14 10:32 Field pH 7.16 Sid. Units 0.10 1 05/07/14 10:32 HEM, Oil and Grease Analytical Method: EPA 16648 Oil and Grease NO mg/L 5.0 1 04/30/14 10:15 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 8.0 ug1L 5.0 1 04/30/14 16:00 05/05/14 21:32 7440-50-8 Lead ND ug1L 5.0 1 04/30/14 16:00 05105/14 21:32 7439-92-1 Zinc 19.7 ug1L 10.0 1 04/30/14 16:00 05105/14 21:32 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 26.3 mg/L 8.3 1 05/02/14 15:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/07/2014 10:34 AM without the wntten consent of Pace Analytical Services, I nc.. Page 4 of 11 aceAnalytical wwwpacelabs.cam QUALITY CONTROL DATA Project: TIMKEN Pace Project No.: 92199094 QC Batch: GCSV/17428 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92199094001, 92199094002 METHOD BLANK: 1188292 Matrix: Water Associated Lab Samples: 92199094001, 92199094002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 5.0 04/30/14 10:07 Pace Analytical Services, Inc. 205 East Meadow Road - Suite Eden, NC 27288 (336)623-8921 LABORATORY CONTROL SAMPLE: 1188293 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg[L 40 35.1 88 78-114 MATRIX SPIKE SAMPLE: 1188294 92199021001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 36.1 90 78-114 Date: 05/07/2014 10:34 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalyflcal. ~.pacelabs.=n QUALITY CONTROL DATA Project: TIMKEN Pace Project No.: 92199094 QC Batch: MPRP115826 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92199094001, 92199094002 METHOD BLANK: 1188623 Associated Lab Samples: 92199094001, 92199094002 Parameter Units Copper ug/L Lead ug/L Zinc ug/L Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 05/05/1419:50 ND 5.0 05/05/1419:50 ND 10.0 05/0511419:50 Qualifiers Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 LABORATORY CONTROL SAMPLE: 1188624 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper uglL 500 472 94 85-115 Lead ug/L 500 455 91 85-115 Zinc ugfL 500 451 90 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1188625 1188626 MS MSD 92199188003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 12.2 500 500 479 489 93 95 70-130 2 Lead ug/L 5.7 500 500 444 457 88 90 70-130 3 Zinc ug/L 175 500 500 606 622 86 89 70-130 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1188627 1188628 MS MSD 92198977001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 482 477 96 94 70-130 1 Lead ug1L ND 500 500 451 446 90 89 70-130 1 Zinc ug/L ND 500 500 456 449 90 89 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05t0712014 10:34 AM without thewritten consent of Pace Analytical Services, Inc.. Page 6 of 11 laceAnalyfical" rnm.paee)abs.corre QUALITY CONTROL DATA Project: TIMKEN Pace Project No.: 92199094 QC Batch: WET/30833 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92199094001. 92199094002 METHOD BLANK: 1190574 Matrix: Water Associated Lab Samples: 92199094001, 92199094002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 05/02114 15:18 LABORATORY CONTROL SAMPLE: 1190575 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1190576 Parameter Units Total Suspended Solids m91L SAMPLE DUPLICATE: 1190577 Parameter Units Total Suspended Solids mg1L Date: 05/07/2014 10:34 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 262 105 80-120 92199391001 Dup Result Result RP❑ Qualifiers 184 168 9 92199188002 Dup Result Result RPD Qualifiers 15.8 15.6 2 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 ace Analytical www pacerabs.mm QUALIFIERS Project: TIMKEN Pace Project No.: 92199094 DEFINITIONS Pace Analytical services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TN - The NE LAC Institute. LABORATORIES PASI-A PaceAnalyticalServices-Asheville PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report small not be reproduced, except in full, Date: 05/07/2014 10:34 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 laneAnalytrcaI www. pacelabs=M QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: TIMKEN Pace Project No.: 92199094 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92199094001 001-001 FLDI 92199094002 003-001 FLD/ 92199094001 001-001 EPA 1664B GCSV117428 92199094002 003-001 EPA 1664B GCSV117428 92199094001 001-001 EPA 200.7 MPRP115826 EPA 200.7 92199094002 003-001 EPA 200.7 MPRP115826 EPA 200.7 92199094001 001-001 SM 2540D WET130833 92199094002 003-001 SM 2540D WET130833 Date: 05/07/2014 10:34 AM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ICP114329 IGP114329 Page 9 of 11 _� ��ceAn��lylrcal • Sam le Condition Upon Recei Document Number: F-CHR-CS-003-rev.14 Page 1 of 2 Issuing Authority: Pace Huntersville Quality Office Client Named h Courier: 7"Fed Ex ❑ UPS❑ USPs❑ Client❑ Commercial[] Pace Other O rtlOrlal '�� Piaui a E3 Custody Seal on CoolerlBox Present: El yes no Seals intact: El yes ❑ no �o� NRwatel Packing Material: ❑ Bubble Wrap A Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1102 040 Type of Ice: et Blue None 7fSamples on ice, cooling process has begun Temp Correction Factor T1102: No Correction T1301: No Correction p : (�, �% C Corrected Cooler Tem • Biological Tissue is Frozen: Yes No g' Date and Initials of person examining contents:�r/%/dl Temp should be above freezing to WC Comments: Chain of Custodi Present: Oyes DNo ❑NIA 1. Chain of Custody Filled Out: Yes ❑No ❑NrA 2. Chain of Custody Relinquished: 2Yes ❑No ❑NrA 3. Sampler Name & Signature on COC: Yes ❑No ❑NrA 4. Samples Arrived within Hold Time: Yes ❑No ❑NIA 5. Short Hold Time Analysis (<72hr): ❑Yes jZrNo ❑NrA 6. Rush Turn Around Time Requested: ❑Yes KNo ❑NIA 7. Sufficient Volume: PdYes ❑No ❑NIA 8. Correct Containers Used: Yes ❑No ❑NIA g. -Pace Containers Used: V Yes ❑No ❑NrA Containers Intact: OYes ❑No ❑NIA 10. Filtered volume received for Dissolved tests ❑Yes ❑No 94A 11, Sample Labels match COC: P<1 ❑No ❑NIA 12'3'4'U -includes datehime/ID/Analysis Matrix: All containers needing preservation have been checked. ElYes ❑No NIA 13. All containers needing preservation are found to be in ( 't fi r compliance with EPA recommendation, /o yes ❑Na NIA exceptions: VOA, ooffonn, TOC, OBG, WI-DRO (vrater) es ❑No Samples checked for dechlorination: Oyes ❑No KNIA, 14. Headspace in VOA Vials ( >6mm): ❑yes ❑No dNIA 15. Trip Blank Present: ❑Yes ❑No NIA 1& Trip Blank Custody Seals Present ❑Yes ❑No I�ENIA Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Field Data Required? Y I H Person Contacted: Dateliime: Comments/ Resolution: SCURF Review:l W IDaw. SRF Review: pate: Note: Whenever there is a discrepancy affecting North Carolina cornpliance samples, a copy of thus form wig be sent to the North Carolina OEHNR Certification Office ( Le out of hold, :inc orrecl preservative, out of temp, incorrect containers) Page 10 of 11 CHAIN -OF -CUSTODY / Analytical Request Document FaeeAnalyfreal a The Chain -of -Custody is a LEGAL DOCUMENT. Aft relevant fields must be completed accurately, -0 Page: or Section A Section fa Section C l J -3 61 Required Client Information: Roqulred Project Information: Invoze Information: Company: Report To: Attention: .7 C Ic �L LG�f�yOrn f G� !✓ .'.Jj- .1 Address• SO1 �f n tt o ��� Copy To: Company Name: 7r� �� REGULATORY AGENCY R4�ND.a",r1) tiL Z7317 Address: .3,00�T�nt)CE a PL4CCO' 5e_NP ES FF GROUND WATER 7 DRINKING WATER r-- i'- UST I"' RCRA OTHER Email To: 1 PurC3"Iase 4`�c�•�5�c.�iPt r ��-+Ht1'flr� Order No.: Pace Ounfa Reference: Phone: '3-f{'y�-uyZ Fax: Project Name: . / •�//}7 r-e-N Paco Pmfect .Nenager: L)4MK C VLJ Slte Loaatlon STA rE: J� Requested Due DmerTAT: Project Number: ante Prchla p: !:� Requested Analysis Filtered (Y/N) Section D Matrix Cedes - z RegufredCliant Information MATRIX I CODE g 2 COLLECTED Preservatives J (� Drinking water Dw g ° z Water Y07 Waste water WW Product P 00mCOMPOSITE� � exoane � v �J SdVSOGd St. TZ OL SAMPLE �D wlpe " I- °a (A-Z. ,) Air AR O z f I y a /1 S! TS Sample IDe MUST BE UNIQUE Tissue TS a M Q7 N Ll Olhor X w OU v v C7 C - R Tl jj < n Q Z U O y Q - to GATE TIME DATE TIME # = T S 2 Z d� O M Pace Project Nod Lab I.D. 1 O L.,-rC X X X X 2 0 0 - C} o Z 4 X x s 0 - OU Z, I fi bo 5 7 B 9 10 11 J12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS FlG1.0 meftsutcea P 4 C)o SAMPLER NAME AND SIGNATURE U p mw{ u ORIGINAL PRINT Name of SAMPLER: fc1�- FL LGiLrN4�'Jt a .tee G V m °i ^ SIGNATURE of SAMPLER] ✓ L' Signed - 7t4.DATE (MWODIYY): ZS /oc '� ✓i 9mpertom Nplaf By signirg INS for III yeu dre aMepa-g Paces NE ISo day payment terms and agreeing to We charges of %.5% per month for eny mvoirm If gold -11- "11., F-ALL-0-020tev,07, 15•May-2007 aceAnalyilcal mvw. pacalaba.=n May 07, 2014 Mr. Rick Flickinger Timken Company 3500 Timken Place Randleman, NC 27317 RE: Project: TIMKEN Pace Project No.: 92199094 Dear Mr. Flickinger: Pace Analytical Services, Inc. 205 East Meadow Road - Suite Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on April 29, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, bra• � - Liamm Carrubba liamm.carrubba@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This reporl shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 aceAnaoical rmwpacalabs.corn Project: TIMKEN Pace Project No.: 92199094 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 FloddalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 Page 2 of 11 e aceAnalytical www;Welabs.cw SAMPLE ANALYTE COUNT Project: TIMKEN Pace Project No.: 92199094 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92199094001 001-001 EPA 1664B CLW 1 PAS I-C EPA 200.7 JMW 3 PASI-A SM 2540D OAS 1 PASI-A 92199094002 003-001 EPA 16648 CLW 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D OAS 1 PAS I -A REPORT OF LABORATORY ANALYSES This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, inc.. Page 3 of 11 Pace Analytical Services, Inc. e 205 East Meadow Road - Suite A aceAnalytical Edon, NC 27288 www.pecelabs.corn ANALYTICAL RESULTS Project: TIMKEN Pace Project No.: 92199094 Sample: 001-001 Lab ID: 92199094001 Collected: 04/25/14 13:45 Received: 04/29/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Collected Date Collected lime Field pH HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Analytical Method Rick 1 05/07/14 10:31 Flickinger 4125114 1 05/07/14 10:31 13:45 1 05/07/14 10:31 6.90 Std. Units 0.10 1 05/07/14 10:31 Analytical Method: EPA 1664E ND mg/L 5.0 1 04130/1410:14 Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 16.3 ug/L 5.0 1 04/30/14 16:00 05/05/14 21:29 7440-50-8 NO ug/L 5.0 1 04/30/14 16:00 05/05/14 21:29 7439-92-1 87.4 ug/L 10.0 1 04/30/14 16:00 05/05/14 21:29 7440-66-6 Analytical Method: SM 2540D 45.6 mg1L 10.0 1 05/02/14 15:20 Sample: 003-001 Lab ID: 92199094002 Collected: 04/25/14 13:45 Received: 04/29/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Collected Date Collected Time Field pH HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Date: 05/07/2014 10:34 AM Analytical Method: Rick 1 05/07/14 10:32 Flikinger 4125114 1 05/07/14 10:32 13:45 1 05/07/14 10:32 7.16 Std. Units 0.10 1 05/07/14 10:32 Analytical Method: EPA 1664E ND mg/L 5.0 1 04/30/14 10:15 Analytical Method: EPA 2001 Preparation Method: EPA200.7 8.0 ug/L 5.0 1 ND ug1L 5.0 1 19.7 ug/L 10.0 1 Analytical Method: SM 2540D 26.3 mg/L 8.3 1 04/30/14 16:00 05/05/14 21:32 7440-50-8 04/30/14 16:00 05/05/14 21:32 7439-92-1 04/30/14 16:00 05/05/14 21:32 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 05/02/14 15:20 Page 4 of 11 aceAnalytical www.pacelabs.oam QUALITY CONTROL DATA Project: TIMKEN Pace Project No.: 92199094 QC Balch: GCSV/17428 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92199094001, 92199094002 METHOD BLANK: 1188292 Matrix: Water Associated Lab Samples: 92199094001, 92199094002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L NO 5.0 04/30/14 10:07 Pate Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-6921 LABORATORY CONTROL SAMPLE: 1188293 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 35.1 88 78-114 MATRIX SPIKE SAMPLE: 1188294 92199021001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 36.1 90 78-114 Date: 05/07/2014 10:34 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 e aceAnalytical .pacelabs.mn ) QUALITY CONTROL DATA Project: TIMKEN Pace Project No.: 92199094 QC Batch: MPRP115826 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92199094001, 92199094002 METHOD BLANK: 1188623 Associated Lab Samples: 92199094001, 92199094002 Parameter Units Copper uglL Lead uglL Zinc ug/L Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 05/0511419:50 ND 5.0 05/0511419:50 ND 10.0 05/051141950 Qualifiers Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-9921 LABORATORY CONTROL SAMPLE: 1188624 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper uglL 500 472 94 85-115 Lead ug/L 500 455 91 85-115 Zinc ug1L 500 451 90 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1188625 1188626 MS MSD 92199188003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Copper uglL 12.2 500 500 479 489 93 95 70-130 2 Lead uglL 5.7 500 500 444 457 88 90 70-130 3 Zinc uglL 175 500 500 606 622 86 89 70-130 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1188627 1188628 MS MSD 92198977001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper uglL ND 500 500 482 477 96 94 70-130 1 Lead ug/L ND 500 500 451 446 90 89 70-130 1 Zinc ug1L ND 500 500 456 449 90 89 70-130 1 Date: 05/07/2014 10:34 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6of11 - ;a'ccie Analytical www pacelabs.com f f QUALITY CONTROL DATA Project: TIMKEN Pace Project No.: 92199094 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QC Batch: WET130833 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92199094001, 92199094002 METHOD BLANK: 1190574 Matrix: Water Associated Lab Samples: 92199094001, 92199094002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 05/02/14 15:18 LABORATORY CONTROL SAMPLE: 1190575 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 262 105 80-120 SAMPLE DUPLICATE: 1190576 92199391001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg(L 184 168 9 SAMPLE DUPLICATE: 1190577 Parameter Total Suspended Solids Date: 05/07/2014 10:34 AM 92199188002 Dup Units Result Result mg/L 15.8 15.6 RPD Qualifiers 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aCiMnalyfical www.px0abs.mn i QUALIFIERS Project: TIMKEN Pace Project No.: 92199094 DEFINITIONS Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/07/2014 10:34 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 11�;a'ne Analjdrcal . pacefabs. cam j QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 206 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: TIMKEN Pace Project No.: 92199094 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92199094001 001-001 FLD/ 92199094002 003-001 FLDI 92199094001 001-001 EPA 1664B GCSV117428 92199094002 003-001 EPA 1664B GCSV117428 92199094001 001-001 EPA 200.7 MPRP115826 EPA 200.7 ICP114329 92199094002 003-001 EPA 200.7 MPRP115826 EPA 200.7 ICP114329 92199094001 001-001 SM 2540D WET130833 92199094002 003-001 SM 2540D WET13O833 Date: 05/07/2014 10:34 AM REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, wRhout the written consent of Pace Analytical Services, Inc.. Page 9 of 11 I Sample Condition Upon Recei Document Number: F-CHR-CS-003-rev.14 Page 1 of 2 _ Issuing Authority: Pace Huntersville Quality Office Client Name: Courier: WFed Ex ❑ UPS{] USPsO Client[] Commercial❑ Pace Other �O $Orval. A .�MiW-' P[ojD a i]atel r Custody Seal on CoolerlBox Present: El yes no Seals intact: ❑ yes El no , � , Rroj�Nartte: - .:; Packing Material: ❑ Bubble Wrap 'Z Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1102 *QCType of Ice: et Blue None �65ampies on ice, cooling process has begun Temn Correction Factor T1102 No Correction T1301 • Nn Cnrrectinn Corrected Cooler Temp.. . 19.7 •C Biological Tissue is Frozen: Yes No g' Date and Initials of erson examining contents: Temp should be above freezing to 6°C Comments: Chain of Custody Present: FYes ON, ❑NfA 1. Chain of Custody Filled Out: PZ�Yes ONo ❑NIA 2. Chain of Custody Relinquished: Yes ONO ❑N(A 3. Sampler Name & Signature on COC: Yes CINo ❑NrA 4. Samples Arrived within Hold Time: Yes ONo ❑wA 5. Short Hold Time Analysis (<72hr): Dyes grNo ❑wA 6. Rush Turn Around Time Requested: Oyes dNNo ❑wA 7. Sufficient Volume. �Ye ON. ©WA 8. Correct Containers Used: ®Yes ❑Ho ©NIA 9. -Pace Containers Used. VYes ONO ©NrA Containers Intact: P2rYes ❑too FJN1A 10, Filtered volume received for Dissolved tests OYes ONo 11. Sample Labels rnatch COG: Des ONo C3N/A 12 r�4' { -Includes dateAimeADlAnatysis Matrix: All containers needwrg pmserva1iionhave -been checked. &es ©l+io NIA 13. AU containers needing .are found 'toibe'in / ft li�r 4 ,preservation compliance with EPA reoommendation. t�Yes ONo I�lA exce0ons: VOA, coklorm, TOC, G&G, W DRO (water) es (]No Sairoes checked far ded-Za iraation: 'DYes ONo 14. Headspace in VOA Vials ( >6mm): :Oyes Elmo17�N1A 1KIA 15. Trip 6W* Present- 10Yes 10.No ANIA 1•6. Trip Stank Custody Seals Present Oyes Otto 41A pace Trip Blank Lot 9 #1',purchased,): Client Notification/ Resolution: !Field Data'Regdired? Y ! N 'Person Contacted: -DatelTime: CommentsPResdlution: SaJF F iReviewlDate: 11 44- , SRF Review: Q ! Date': Note: 'Whenevertthereiis:a,discrepancy:affeclingiNorth,Cardlina,wMohance •samples,:a,oppy.of,this,,form, iillbe!sentstoitheiNorthrCardlinaiDFIcNR -Certification Offrcet(La-outoflhdld,lincorrectipreservative,rout df,temp, incorrect,containers) Page 10 of 11 11 sr? .FaceAnalytical' CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a ZEGAL DOCUMENT. All rolevant Aelca must oo Compleled accurately. o wsew, pasaiaas.eam Section A Section B Section C Page: p? M - - h 1^ 9 61 it -- - Required Client Information, Required Project Information: Invoice lnformalbr: Att Report eMinn: Reort T Company: -r'irrlKEn] f c.� ,Tt 1 c. �r�G c3lz_. '� c I� l'� �C-�+n'S>rR- ---- --�-- -- --.-- Address' dam._ J'+^ r J' Copy To, Company Name: % fyl iLE+t� / REGtII ATORYAOENEY _ _ ---- Q /OC. Z7 3 j Address: -jC�.) � Y NPD&J r'` GROUNDWATER 'r- DRINKING WATER (- UST r- RCRA OTHER Email Email ioL .�•i,�+xken s:. �, IJy Ci-' iCU't+� Purchase Order No.: woSuoin Roferonca: F'hane: 2.S Fax: Project Name: '7'1 Al � E-A1 PacoPrvlect Manager: I- +%A tK C 64 site Logatlon STATE: Requested Due DatotTAT: Proioet Number: aca Fro i e or — -Rgqupsted Analysis Filtered'(YIN)- Section D Matrix Codes Required Cl,m irm,, — MATRIX , CGQti C04LECTED Are¢ervavvaB N ZTFF J Ornking Water DIN v WaWT Waste, ProdeCWAlef PW 2 (� KC coNPOSiTE START COMPOTE SI ENVJCAAS ,, fi Sol VSolid St. g 0 >•f e► r.. ��! SAMPLE ID oanP up (A-Z.0-9l,-j Air AR p iy d Z i- h i a �rAJ� ` Sample IDs MUST P.k I1NIgUE Tissue O a z U N jlj OT Other or X w w G m 1111 c � v" m Q 1 ~ < rn DATE TIME DATE TIME � Z i Z Z Z Q --* Pace Pro jest Nol Lab I.D. i CCU f Ix ors Z ! 6 o 7 'Ov - 6 - - — is- - --- - - - - E �E I I I ADDITIONAL COMMENTS RELINQUISHED By I AFFILIATION DATE TIME ACCEPTgp BY l AFFILATION TIME SAMPLE CONDITIONS /� Y 1 (fN,--G 4w) �% r\1:�� 5 �� ��� _+r-�DATE fffllrl `7r --r ! - -- — - - Ff��� - - - - - ,- - t- — -- SAMPLER NAME AND SIGNATURE U 6 N PRINT Nome of SAMPLER: r-L L G jC I .�Crc'7L • E to a _ u SIGNATURE of SAMPLER DATE 9ignad - - - - MMfOD1YYj: lillw m KoWv Sy srn-urg this to ni y- are arsopilhg Pece's NE 19e day paymem terms and agreeing to late diargae d 1.5".5 ver monEh for any mvaires f -- vnlh- "o dais F-ALL-Q-026 e J.07. 15•May-2007