NC0025534_Priority Pollutant Scan_20191112

Action History (UTC-05:00) Eastern Time (US & Canada)
Submit by Anonymous User 11/12/2019 10:13:39 AM (Supplemental Submittal)
Submit by Bennett, Bradley 11/12/2019 3:14:51 PM (Supplemental Info Submittal)
• Bennett, Bradley assigned the task to Bennett, Bradley 11/12/2019 3:13 PM
• The task was assigned to Thedford, Wren, Bennett, Bradley 11/12/2019 10:13 AM

Initial Review Information
Updated ID#:* IWORTANf:FEVIBAERSHOLLDVERFYand revise here ifnecessary.
NCOO25534
How should this project be handled?*
r File r Discard
Information Submitted on 11/12/2019
Submitter Information
Name: Garrett DeMoss
Vft is subrritting the inforrretion?
Email Address:* [e-mail]
Submittal Information
The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental
information associated with discharge monitoring reports (DMR). All DMR data is required to be submitted
electronically through the eDMR system and should not be submitted here. Division staff will reviewall
uploaded documents and will only maintain required information. Documents such as laboratory reports are not required
to be submitted and will not be maintained in the system.
Project Information:
Rease SUDDly the Dernit nun ber for this
Existing ID#* PerrritNurrber
NCOO25534
Exarrples: NCKxxxxxx or NO&xxxxx
Facility Name:* City of Hendersonville WWTP
County: Henderson
Please upload all files that need to be
submited. *
dick the upload button or drag and drop files here to attach docurrent
2019 PPA.pdf 822.52KB
Only pdf files are accepted.
Comments about the attachments:
Uploaded 2019 Priority Pollutant Analysis Report
* V By checking the box and signing box below, I certify that:
o I have given true, accurate, and complete information on this form;

• I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the
NC General Statutes (the "Uniform Electronic Transactions Act)
• I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes
(the "Uniform Electronic Transactions Act');
• I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written
signature; AND
• I intend to electronically sign and submit the Supplemental Information form."
Full Name: Garrett DeMoss
Signature:
Date Submitted: 11/12/2019

4G/'l/��q�W,, Pace Anay6ca13eMr8,LLC
lXi4/+ <7l® m5RivasiEe Br.
awvpamlahcmm Ialieui8e, NC 28W
(828)2 7176
ANALYTICAL RESULTS
Pro)oa V PEEE(PPA)1O 19
Pace Project No.: 92WM3
SBMPM: WWiP EFF(PPA) GRAB Lab IM 92448923001 CoIle : 10/W/191013 Receivetl: 1p 1914:211 Mab& Wathr
P..1am R oft UMs Report Lund BF Ptepa Anayzel CAS No. pual
HEM,Oland Grease
Ar-Wbool Motfa: EPA 1664E
Oil aM Grease
NO
mg)L
48
1
1WIW1918:29
1631E Memury,L. Level
Analyfia McBmd EPA1631E Pmpaalon MC :EPA1631E
Mo.,
1.78
M&
0.60
1 1W16f1915:30
t0A&1914:57 7439-97{
624 Volatile Organics
Anayoi Method:
EPA M4.1
Acrolein
ND
u9/L
5.0
1
1W17M9n:M 107-02
Ac lmrlrile
NO
ug/L
5.0
1
10M711922:09 107-13-1
Benzene
NO
rglL
1.0
1
1W171192209 71A3-3
f oEiMmomethane
NO
U91L
2.0
1
10A7A922-O9 7S274
Bromoiorm
NO
ug/L
20
1
1W17A922:09 75-252
BromometMne
NO
W&
2.0
1
1M7A922:09 74 9
Cation tefta Mlatle
NO
ug)L
2.0
1
1W1711922:09 56235
Cbiombei ene
NO
U91L
2.0
1
IW711922:M 108-90-7
Chlomethano
NO
ug/L
2.0
1
t0A7/192209 75 3
2- hloroeftivinyl ether
NO
ug/L
5.0
1
1W17MO22:N 110-75 o3
CMoro m
NO
ug/L
2.0
1
1W17A92 W 67E
Chloromothane
NO
u91L
2.0
1
IW71192209 7"72
Oibmmatlllomm U,om
NO
ug)L
2.0
1
1W17/192209 1244&1
1t-DkWomftne
NO
ugL
2.0
1
10117/19M:M 75- 3
1,2-D6 ome0rane
NO
ug/L
2.0
1
1W17M922:W 107Afi-2
1 to a
NO
U91L
2.0
1
1W17M92 7535-4
n1 1. iolilo
bans-1,2-OicblomeMene
NO
uglL
20
t
.0
tOM7/1922:09 156-60sv
1,243ic1Goo opane
NO
QWL
20
1
1W17/192 M 78 5
cs-1,3-DichloWapene
NO
uglL
2.0
1
10/17/1922:09 100614115
barml,3DichloroPropene
NO
Wg
20
1
10M7A9UW 100614125
ENylbenzeno
NO
W&
1.0
1
11Y17119MM 10041A
Methylene Wh a
NO
U91L
20
1
UUM19MM 75 2
1,1,2,2-Tehachlomethane
NO
u9)L
20
1
1W1711OMW 79
TetrarM ethene
NO
tg/L
20
1
10117A92209 127-11"
Toluene
N13
uga-
t.0
1
1W17A922:M 10888-3
1,1,1-TnrlJoroeMane
NO
IWL
2A
1
10117119MM 715
1,1,2-Tnchloroethaire
NO
u9)L
20
1
iW17A922:W 79
Toohloo er
NO
LWL
20
1
1W17/192 (Xl 794
Vnlyla.rde
S-w9ates
NO
W&
2.0
1
10M7/192209 75514
4Bromofluorobenzene(S)
96
%
70-130
1
1W17119MM 460-00d
ioluened8(S)
104
%
70-130
1
iW17/192209 M37-265
1,2�ane-0 (S)
95
%
70-130
1
1 W171" M 09 171 fi 17-0
4WA Phenolics, Total An810n1Meth : EPA420.4 Rev 1 01983 Preparation Me0m0 EPA4211A Rev 1 01993
Pherml NO m9)L 9.00 1 1W15M915:15 10/18M907:44 108-95-2
4600CNE Cyanitie, Total Anaygaal Me W: SM 4500CN-E-Ali Preparation MC : SM 45�011
Cyanide NO mg& U.0080 1 10A4/1915:18 I M&1910:58 57-125
REPORT OF LABORATORYANALYSIS
TNs repoM1aBall�be reProea-eR. evre(d in iu8,
Gate: 1022/201803:54 PM wmlmmrtmevmnm wnsent of Pe�Arelyli4i SeMt6,LLC. Page4o134

eAnalAca(
o..remr��
ANALYTICAL RESULTS
PX¢Aoatyt Senrzaa,t1L
222e mwmdo or.
AgheY , NC 2e
(628)25 7176
Project: NNYIPEW(PPA) 10d-19
Pace Pm dNe.: 92446923
Sample: WWfP EFF(WA) LLXG Lab ID: 92A4892= Wlect 10MM91013 Received: 1MW191420 Mahix: Water
B K
Parameters Results Units RWod Iim6 DF Prepared Anayretl CAS No. Dual
1631E Nercury,L. Level
W.q
1..1 1.71WKR FIBIF_ l9IJ
Anafyi Method:EPA1631E Pmparadon Me iod:F A1631E
ND nWL 050 1 1&1&1915W 1&1&1914:42 143 W-
REPORT OF LABORATORYA14ALYSIS
rtis report sn� rmtl»repmdured, erept lnmtl.
wN�adltrewM(en mnaeM MPx¢A�alyb'al Servirps. LLG
Page 5 of 34

/1^.. /�' PaceAnalytiralsmiw,LC
,_ aceAnal}41ca1 =5 � Dr.
Pslurille, NC 26m4
m
' (82d)25L7176
ANALYTICAL RESULTS
Pmjed: W P EFF(PPA)10819
Pace Project No.: 92M8923
Sample: W9v1PEFF("A) CAMP Lab ID: WW923003 GUlkd¢d: 10N8/1910:18 Remy : IGM191420 MaldxN3Yer
ParmneMa Reoda udta Report Lund DF Prepaid AraWW CAS No. Dual
200.7 MET IM Aoa"cal M¢8md: EPA200.7Rev 4A IW,I PMPaMW" Me od: EPA200.] Rev 4.41994
Alimony
NO
u98-
50
1
10116M9 MN
iM&192042 7440-360
Araedc
NO
u9IL
100
1
IW1&1910:%
1011911920A2 74 &2
B"Imun
NO
W&
1.0
1
IWIW1910.59
IM911920:42 744041-7
Cadmium
NO
u9/L
10
1
10I16r1910:59
1&19/1920:42 74404&9
Cok
9460
ug/L
IN
1
1MM910.59
1&19/1920:42 74 70-2
Gvomium
ND
o9/L
5.0
1
1MM910M
iM9/1920:42 7440-47-3
copper
17.8
ug&
5.0
1
1MW91059
1011M920A2 7440.5
Lead
ND
U9/L
5.0
1
1M&1910:59
lWl WI920:42 ]439-92-1
Magravum
2540
ug/L
100
1
IWI&191059
1011M920:42 7439554
mokol
50.7
ug/L
5.0
1
IM611910:59
1MM920:42 74 -o
Selenium
NO
u9/L
10.0
1
10/iM910:59
IMW192042 T/8249-2
Silver
NO
u9A-
5.0
1
10I1M910:59
IM91192DA2 744&224
Thallium
ND
ug)L
10.0
1
1011611910:59
10/19I1920A2 7446"
Hardness, Totl(SM 2 B)
34100
ug/L
662
1
1M&19 IQ-%
IWIWI920.42
L.
53.2
y3/L
100
1
t0ItM9 M0
10119/1920:42 7440£GB
9M.8 MET ICPMS
Ana"Mettmd:
EPA200.8 Prepamfi0n Method: EPA200.8
Copper
18-6
ug1L
10
1
iM&1905:30
1011M9 W.01 7440
Silver
ND
ug4-
050
1
10/15/1905:30
1MM90O01 1440224
245.1 Mercury
Analybr Melhod:
EPA2451 Rev 3.01994 P ,.tbn
Me oil: EM2451 Rev 1.11994
W.r
NO
u9A
020
1
IMIM912:10
10/22/1913A3 743497E
us NWv
Analyfip Method
EPA 625.1 Preparllan Mdhod
EPA625.1
Arn ph ne
ND
u9/L
5.0
1
101151191624
1011M916A6 8352-9
Acenaph&Woe
NO
ug/L
50
1
10MM91624
10/16/1916:46 208
ArMMa a
NO
u9/L
5.0
1
lM&191624
1011M916A6 120-12-7
Benadine
NO
u9/L
50()
1
1MM916:24
1011W1916-.6 92E7E
B¢n20(d)an6vaRvle
NO
u9IL
50
t
10/15191024
101I6H91646 S6b53
Bemo(a)pyrt a
NO
u91
5.0
1
1011M91624
1MM916:46 50-32E
6emo(b)Puoradhene
NO
1D2
5.0
1
1M&1916:24
1&1M918:46 205-99-2
Bemo(9.h.q,wne
NO
ug/L
50
1
10/1&191624
1011&1916:46 191-242
O o(k*omnt a
NO
u9/L
5M
1
101M916:24
10/16/1916:46 207-0&9
4Ammophenylphenyl ether
NO
o9/L
50
1
1MM91624
IMM916:46 101b
BuMher"pWaile
NO
u9/L
5.0
1
1M&1916.24
IGI M916:46 65-0&7
tia(2Chbroe8wxy)methan¢
NO
U91L
100
1
1011M916Z4
10MM916:46 111-91-1
M(2-Ght.thyl)ether
NO
ou&
5.0
1
10M&191624
1MM916:46 Ill i41
2Chloronaphthal¢n¢
NO
U91L
5.0
1
10119191624
10/1&1916:46 91-547
2Lhlorophenol -
NO
UWL
5.0
1
10/1"91624
1MM916:46 9&5]b
4CMorophenylphenyl ether
NO
ua
5.0
1
iM&191624
10/191916:46 700 72-3
Chry
NO
u91
5.0
1
1&1&191624
1M&1916:45 21"1-9
Dib¢n (a,h)ar racene
NO
UWL
5.0
1
1MM916:24
1M&1916:46 5&70-3
12-Oichb en.m
NO
o9IL
5.0
1
1MM916:24
iMM916A6 9550-1
1,&Dichbrobemene
ND
uWL
5.0
1
1MM916:24
iM M 916:46 541-]3-1
1.dUGtlombemene
ND
U91L
6.0
1
1011&1916:24
IMM91645 106-4&7
3,3'-Dichiomberrvdirg
NO
U91L
25.0
1
iMM916:24
i&1&1916:46 91-94-1
REPORT OF LABORATORY ANALYSIS
T MM" dull rmt be repmduoM, a opt in full,
Dale.AD22/201903:54PM w oot Mewm 00000muf P.Malykml6ek C. pwoof34

Paw Aaalybc9Sanires,=
aceAmlXicale m6I: a.
- Ashe4ae, Nc 26eoc
a. m
ANALYTICAL RESULTS
Pmlect WWiP EFF(PPA) 10A-19
Pam Project No.: 92448923
Sample: W P EFF (PPA) G P Lab ID: 9244992 3 GOHec : 1 WDW1910:18 R—Mi : 10/091191420 Ma : MW
Parameters
Results
UnBs
Re nLhdi
DF
Pmp wl AnaWy DASNo Quai
625 MSSV
Anarytigl Me0ro6: F3A625.1 Preparation Meffwtl:. EPA 625.1
2,4DiMompMwl
NO
l-WL
50
1
1WiW191624 lW1&1916:46 1200&2
D ffiylpWalate
NO
ug/L
50
1
iW1W1916:24 1W16/1916A6 840&2
2,4 .,m Ylphenal
NO
ug1L
10M
1
1Wl W1916:24 1011&1916A6 105b7-9
Dlmethyl"WaW
NO
ug&
&0
1
1WIM91624 iWt&191646 131-11-3
Oii butyl"alffi
NO
u9&
50
1
1011Wt916:24 tWi W1916:96 64-742
4,6-Dinitro2-methylphenol
NO
uglL
20.0
i
1W1&1916:24 lWt&1916:46 53452-1
2,4-Dlnilmphenai
NO
W&
50.0
1
MW191624 1W18i1916:46 51-2
2,4DinftUuene
NO
1191L
50
1
iWt&191624 IWt&191646 121-14-2
2,&Din&Mduerre
NO
u &
5.0
1
1W1&191624 iW1W1916:46 6W 2
DHtdAylphftM
NO
ug1L
50
1
10/1Yt916:24 1W1&1916:46 117�
1,2-Dphenylhyda
NO
ug/L
5.0
1
10MS1t916:24 1W1611916.46 122�7
bls(2-Mylhex])pt late
NO
ug/L
5.0
1
iW191916241Wi&191646117e1A
Flumar a
NO
09/L
5.0
1
tW1&191624 1MW1916:46 20644-0
Fluorene
NO
491L
5.0
1
1W1&191624 IMW1916:48 e&]34
Hex WM 1,3buladene
NO
u91L
5.0
1
1W1&191W24 10YIW191646 e7b&3
Hex Mmb mene
NO
ug1L
5.0
1
1MM91624 1011W1916:46 1W741
Hesachlomgd peM em
NO
ug&
10.0
1
MW191624 MM916:96 T2474
HexachlometM1ane
NO
ug1L
50
1
1WiW191624 IW16M916:46 6]-]2-1
Indeno(1,E,3 )pyre a
NO
W&
5.0
1
1W1&191624 lW1&1916:46 19339E
I.Pharaoe
NO
ug1L
10.0
1
10/1W191684 1WW1916M6 7&541
384M."phenol(.&p �1)
NO
uglL
Mo
1
1W15/191624 tWM916:46 15831-104 N2
Naphthalene
NO
uglL
5.0
1
10M91916:24 1WlW916:46 91-2&3
Nitrobenzene
NO
u91L
50
1
10/19191624 MM916: 9&953
2-NNophmol
NO
u90
5.0
1
iW191916:24 10/161t91&: 8&756
4MAWhenol
NO
uWL
50.0
1
1W19191624 10/1W1916'48 100412-7
N-9&0s im MyF im
NO
u &
50
1
iW15N916:24 10/1&1916'46 62-259
N-NNoso-0i+ mpylamim
NO
ug1L
5.0
1
1W15N91624 IWiW1916'48 621$4-7
N-NitrasoEiphenylamine
ND
ug1L
100
1
10O1 916:24 iW16N91&: 86366
2,2'-Oryds(t-cM1lompmpane)
ND
ug/L
5.0
1
IMW1916:24 IMM1916:46 10&60-1
P°nladrlae°pM1en°I
No
ug1L
10.0
1
1WW191624 10/1&191&: 87�
Phananlhnne
NO
u91L
5.0
1
iW19191624 1MWi91&: 8501-0
Pher
NO
W&
5.0
t
iW15/1916:24 MWO 16:46 106-95-2
Pyrene
ND
y31L
5.0
1
1WI91916:24 10/16/1916:46 129
1,2,4Tntllbrobellzene
NO
W&
50
1
10/1W1916:24 1W1&1916.-6120 -1
2,4,&Thp lomphend
NO
ug/L
100
1
1WiW1916:24 1W1&1916:46 880&2
Suimgalas
Ndrabenzene+l5 (S)
66
%
16120
1
1W191916:24 1WiW191646 41656&0
2-Huor ipherrA(S)
58
%
1&120
1
10119191624 1011W1916A6 321fi08
Teryheny 14(S)
34
%
11131
1
iW191916:24 IWW191646 1718 1-0
Phenol-06(8)
24
%
14120
1
1W1&191W24 1 WW916:4613127-863
2-Fluomphenol(S)
35
%
10-120
1
tW151191624 10/1&1916:46 367-124
2,4.&Tnbmmophenal(S)
99
%
1013]
1
1Wt9191624 10/1&1916.46 IW&
25405 Total DL Wee Solkis
M*Uwl We : SM 2540 Ml
Taal DffisoPoe6 SM.
241
mg&
25.0
1
10(1 W1905:21
REPORT OF LABORATORYANALYSIS
Tttls repartshell
mtbe repmauW, eiceznm
fu6,
Date: 1022Y20t903:54 PM
riNoutBrexilren
wmnne Pao:Aretya�Seruira, LLC.
Page7af34

P.Anay�,=
CBM2/yGCal p 2225 Rlversitle 0r
wavV+celNxsm A9iexlle. NC 28
(e28)25471M
ANALYTICAL RESULTS
Project Y P EFF(PPA) 10-&19
Pare ProjeC No.: 92448923
S MP1e: W WtP EFF (MAI COMP Lap 10: 92448923003 Cabe : 10MM910:18 Receivetl: 10ft M91420 M.— WA
Pammefere ReN111a Units Report Limo OF Preps M.Vy CAS No. Qual
To l Nitrogen Caloula0on
Tatal Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
3512 Top[ KIeMeM Nitrogen
Nitrogen, Ki Mahl, ToWl
3532 NNrogen, NO2R103 pm.
Nilrogeq NO2 plus NO3
3MI Phosphorus, Tow
Phosp .
Maly" McBwa:T NO3+NO2C ICWa
162 m9IL 0.52 1
102211914:15
A ytl MCMotl: FA 350.1 Rev 2.01993
NO mglL 0.10 1 10117/1917.19 ]864-41-7
Ara*tln Megmd:EPA351.2Rev2.01M PrepamSon McMotl:EMA 12Rev2.01993
39 mg/L 0.50 1 1&t7/1903:59 1&1&1906D2 TI27-37-9
An W.I Meilmrt: EPA353.2 Rev 2.01993
127 mWL 020 5 1& W91443
Am"We W: EPA395-1 %v2D 1993 Prepara5on McBgE: EPA 365.t Rev 2 01993
0.1 m9/L 0.050 1 10MD191945 MM911:14 T/2&14D
REPORT OF LABORATORY ANALYSIS
11gs revue snae na ee rePmoucm. �reptm tun.
Date: 1022/201903:54 PM wlgwtge written mnsent of Pero Anyypd 3salma, LLC.
Page 6 of 34

aceAnal.Wcal o
»anA�a+n
QUALIFIERS
Project ViVu PEFF(PPA)ITT19
Paca Projectble: 924 23
DEFINITIONS
PaceAnalytictl Services, LLC
zzza laws w
fishie ne, NG 28804
(92a)251-71T0
DF- Dilution Fail dhapmed, represents the fads' applied in the reported data due to diluron of the sample aliquot.
ND -Not Detectetl at or above adjustetl reporting IimR.
TNTC-Too Numerous To Count
J - afirromi concentration above the adjusted mefhr d distortion limit and below the adjusted reporting limit
MDL-Adjusted Methed DHecOoo Limit
PQL- Practical Quambtion Limn
RL- Reporting Limit -The sanest concentration vaWe that meets project Far,aremen6 for gwnMafrve data wgh known precision and
bias for a speche andirle in a spedfic matrix.
S-Smogate
12-D"ptrenylhydream decomposes to and carrot be separated from Ago ene mill, Method 8270. The result forest anakda, is
a sombhietl concentration.
Gansisk:m with EPA possible, asounded data are displayed ars have been used to wlwlate %mansi and RPD values-
LCS(D) - Laborasry CoMral Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
MP -Sample Dupfcam
RPD - Relative Percent DiBerence
NC -Not Calculable.
SG -Sill® Gel - Clean -Up
U- indicates the compound was analyzed W. but runt detected
Adtl preservation may not be appmpdate per 2 Chlmoethyl irryl other.
A separate vial preserved to a pH of4 is recwmwntlod in SLAW Chapmr4 for the ar lysk afAao4in antl Ace lonaile by EPA
behind BZ6o.
N-Nitmsptlipherrylamble decomposes and cannot be separated from Diphenylamine using Method! 8270- The result reported for
each analyte is a combined cony tration.
Pace Analyticalis TNIacaetliled Ca yom Pace PMfrontswrmntlistofacomsitetlanatytes.
TNI -The NELAC Instihrte.
I1`,90RAT0RIE3
PASTA Pare Anaytiwl Services-AshevAle
PASIL Paw Analyfical5ervices-Chadmle
PASI-M Pace Analytical Serrices- Minneapolis
Albi QUALIFIERS
M1 Matru spike recoveryexceetled QC lanits. Batrti acoeptetl based on laborathry corNol sample (LCS) recovery.
M6 ispike and Ma(rix spke dupfiwle remvs, not evaluated against control limits sonar sample: dinier.
N2 The lab does not hos NELAC l accreditation for this parameter but other acaedgalior5rcerlfiwtipns may apply. A
complete list of a ccretlitationslwtlifirations is available upon request
1`5 The EPA or methatl required sample preseenspn anthems this corpus, therefore acceptable recoveries may, not be
achieved in sample manic spikes
R1 RPD value was outside control limits.
03 Anaysis of 24tlomethyl vsyl ether was performed firm a sample thazwas ties preserved to pH<2 cosh 1131. Add
preservation is not alkrved tier this promisor by lfte test method! rotor NPDES compliance pet 40CFR part 136.
REPORT OF LABORATORY ANALYSIS
This repot stbll not be nepmduced, exr in roll,
Date: 10r2 1903:64 PM iMless NO w Nnr mnsem of Pam Analytial Services, TC,
Page 3l)of 34