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WQ0036561_Residual Annual Report 2014_20141010
;tea .56 34 5(-% 4 Inc. City of Danville 2014 Annual Report Residuals Land Application Permit No. WQ0036561 Prepared By: EMA Resources, Inc. REDEIVED1DENR1DWR OCT 10 2014 Water Quality Phone 336*751.1441 — Fax 336.751.1442—'iffink, S-�,finr1 755 Yadkinville Rd — Mocksville, NC 27028 October 3, 2014 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2014 Annual Report — City of Danville, VA Treatment and Land Application of Residuals NCDENR Permit No. WQ0036561 Dear Sir or Madam: Enclosed is three copies of the 2014 Annual Report for the above referenced land application permit. During 2014 EMA Resources, Inc. land applied 972.23 dry tons of wastewater residuals to 323.8 acres of private farmland. Please contact me or Brent Collins — EMA Resources Inc., brent.collins&emaresourcesinc.com if you have any further questions regarding this report. Sincerely, Jerry >3. Shupe Jr. Project Manager Severn Trent Services 434-799-5137 Jerry. ShupegSTS ervices.com OCT 1 0 ,- Water Quaiity F-7mitttn€s Section ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0036561 County: Pittsylvania County, VA Year: _ Facility Name (as shown on permit): City of Danville, Northside WWTP Land Application Operator: EMA Resources Inc. Phone: Land application of residuals as allowed by the permit occurred during the past calendar year? 21 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Annlication Summarv: 2014 336-751-1441 Total number of application fields in thepermit: 38 Total number of fields utilized for land application during the year: 11 Total amount of dry tons applied during the year for all application sites: 972.23 Total number of acres utilizes for land application during the year: 323.8 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading Rates in 15A NCAC 02T. 1 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are d attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. { 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: I "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Barry Dunkley - Dir. of Wastewater Treatment OE Aff Pe ttee Name and Title (type or print) SignaPermittee Date i 6 - C5 9- I 1 't 9/15/2014 Sigb4ture reparer* V 0 Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) --j - - - �— l — (- _ - �� r—1 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: Facility Name: Residual Source WQ # or NPDES #: WWTP Name: Racirinal Analveic llata WQ0036561 City of Danville VA0060593 Northside WWTP Laboratory: 1) 2) 3) 4) 5) A&L Laboratories Parameter (mg/kg) Cone. Limit m k a Sample or Composite Date 3/24/14 5/8/14 5/19/14 6/2/14 Percent Solids (%) NA 6.67 8.24 5.46 6.14 Arsenic 75 30 27 6 6 Cadmium 85 3 3 3 3 Copper 4,300 435 436 480 470 Chromium NA 150 187 79 69 Lead 840 91 130 54 57 Mercury. 57 2.4 2.3 0.8 2.1 Molybdenum 75 19 20 28 25 Nickel 420 73 89 59 54 Selenium 100 5 5 5 5 Zinc 7,500 1560 1490 1840 1870 Total Phosphorus NA 19500 19700 23000 21800 TKN NA 34300 31100 40700 41400 Ammonia -Nitrogen NA 12300 8010 10400 10700 Nitrate and Nitrite NA 19.5 14.6 2 22.8 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." gnatu e f Preparer U Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0036561 Facility Name: City of Danville Residual Source VA0060593 NPDES # or WQ#: WWTP Name: Northside WWTP Rncidlnal Analveic nata Laboratory: 1) 2) 3) 4) 5) A&L Laboratories ParameterSample or Composite Date ---- Potassium ------------ ---------- ------------ ------------ ------------ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report racility Name: City of Danville Total Dry Tons Applied (Annual): 'ermit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: James Blackwell Owner: James Blackwell Predominant Soil Series: kcres Used: 24.9 Acres Permitted: 24.9 Site #: CS06 Field #: 39.54 Aesidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ample or 1 2 3 L4J _5j 6 L7 8j 9 10 11 12 Com- Avg. posite Date % Solids 6.63 Arsenic 17.25 admium 3 Copper 455.25 Chromium 121.25 Lead 83 Mercury 1.9 Molyb- 23 denum Nickel 68.75 Selenium 5 Zinc 1690 Total Phos- 21000 horus nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 11 L 2 L 3 4 5 6 7 8 9 10 11 12 DT/Ac./ c APP• Event 1.59 14 Arsenic 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.055 admium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 1.446 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.446 hromiu 0.385 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.385 Lead 0.264 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.264 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.073 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.073 denum Nickel 0.218 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.218 elenium 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 iMolyb- Zinc 5.367 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.367 Total Phos- 66.696 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 66.696 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". zl-�z 4�2�_ 9/4/2014 >ignature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville James Blackwell Operator: James Blackwell WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 33.54 Site #: Predominant Soil Series: CfB Crop 1 Name: Fescue Crop 1 Max. PAN: 216 Crop 2 Name: 1 Acres Utilized: 24.9 CS06 Acres Permitted: 24.9 Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: 0 .c 0 � O Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons oho Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wt,a Moist) Precip. Past 24 Hrs. inches Y � - coo b c * o � �'. : , w 4 � 9 � p * N' * �, * a TKN mg/kg Z =t � � e �. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( ) lbs/acre Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/10 143000 6.03 1.588 Northside WWTP Dry <.5" S 0.5 1 0.3 36875 10352.5 14.73 41.751 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... .......... FOTALS: 01 143000 :::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 41.751 0.000 Lime Applied Annuallbs/acre 0.055 0 0.055 36 0.010 0 0.010 34 1.446 0 1.446 1 1338 0.385 0 0.385 0.264 0 0.264 267 0.006 0 0.006 15 0.073 0 0.073 0.218 0 0.218 374 0.016 0 0.016 89 5.367 0 5.367 2498 66.696 :: Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop ........ ......... >: .::::::::» ...... .:::.. 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Z-e *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report 'Facility Name: City of Danville Total Dry Tons Applied (Annual): 37.75 'ermit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: James Blackwell Owner: James Blackwell Predominant Soil Series: RnB kcres Used: 26.6 Acres Permitted: 26.6 Site #: CS06 Field #: 2 Aesidual Analysis Data (Heave Metals and Total Phosphorus use mg/ke. % Solids use Raw Percent ft com- posite Date - Zinc •' 1 ___________ Total ' 111 Annual Heavy Total DT/Ac./ App. Event 1.42 Arsenic 0.049 admium 0.009 Conner 1.292 TTletal Field Loadings © © o o o ' 1 111 1 111 1 111 1 111 1 111 1 111 1 !11 1 111 1 111 1 111 1 111 1 1�• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • 1 1 11 ! I li ITItli I"iii� ME"11 M"111 liTlilili IVIiITli 1 111 1 111 1 ! 11 1 .. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 .. �� 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11! 1 • �� 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 � � � 1 1. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • �� 1` 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• i� 1 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 �� � •• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 � '• '�• • •; 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • '; "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. s am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 2:f-e42;�- 9/4/2014 signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Danville WQ Permit #: WQ0036561 Field #: 2 Acres Utilized: 26.6 Land Owner: James Blackwell Annual Dry Tons Applied: 37.75 Site #: CS06 Acres Permitted: 26.6 Operator: .lames Blackwell Predominant Soil Series: RnB Cation Exchange Capacity (non 503): 0 Crop 1 Name: Fescue Crop 1 Max. PAN: 162 Crop 2 Name: Crop 2 Max. PAN: � A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. wry' Wet, Moist) Precip. Past 24 Hrs. inches a � Ts '� 0 1; * 0 c w N :h � � * P- TKN mg/kg z =t � -3• mg/kg Nitrate and Nitrite mgtkg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 6/13 136500 6.63 1.419 Northside WWTP Dry <.5" S 0.5 1 0.3 36875 10352.5 14.73 37.306 NA Fescue 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): ......... .......... TOTALSI 01 136500 :::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 37.306 0.000 Lime Applied Annuallbs/acre 0.049 0.009 1.292 0.344 0.236 0.005 0.065 0.195 0.014 4.796 59.598 ...... .................. ............................ ........................... Date lbs/ac Prior Years Cumulative lbs/ac 0.1076 0.0288 23.0565 1.3401 0.7342 0.0186 0.1041 0.5048 0.0463 12.1702 Current Cumulative lbs/ac 0.157 0.037 24.348 1.684 0.970 0.024 0.169 0.700 0.060 16.966 Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit lst/2nd Crop e P 162 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report acility Name: City of Danville Total Dry Tons Applied (Annual): 'ermit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: James Blackwell Owner: James Blackwell Predominant Soil Series: licres Used: 20.7 Acres Permitted: 20.7 Site #: CS06 Field #: 80.87 FaB3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ample or Com- posite Date 11 Avg. 21 1314 L5J 6 L7 8 9 10 11 12 % Solids 1 6.63 Arsenic 17.25 admium 3 Copper 455.25 Chromium 121.25 Lead 83 Mercury 1.9 Molyb- den 23 Nickel 68.75 Selenium 5 Zinc 1690 Total Phos- horus 21000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 Copper® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ,hromium1 •� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 •� Lead 1 •� • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 •�' 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 � 1 :1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 :1 �-� IWM� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 +- •� 1 1' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• IJ� Total Phos- phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 9/4/2014 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Danville WQ Permit #: WQ0036561 Field #: 3 Acres Utilized: 20.7 Land Owner: James Blackwell annual Dry Tons Applied: 80.87 Site #: CS06 Acres Permitted: 20.7 Operator: James Blackwell Predominant Soil Series: FaB3 Cation Exchange Capacity (non 503): 0 Crop 1 Name: Fescue Crop 1 Max. PAN: 194 Crop 2 Name: Crop 2 Max. PAN: o QLiquid Volume applied (enter one) Solids/ Cu. Yds Gallons oho Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources DES #, W Q#, Fert., Animal Waste, etc) Cool W Moist) Precip. Past 24 Hrs. inches co � a o ° �, w * N TKN mg/kg o 0 w• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/16 162500 6.63 2.170 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.51 14.73 57.071 NA Fescue 6/17 130000 6.63 1.736 Northside WWTP Dry <.5" S 0. 0.3 36875 10352.5 14.73 45.657 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... .......... TOTALS: 0 292500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 102.727 0.000 Lime Applied Annuallbs/acre 0.135 0.023 3.557 0.947 0.649 0.015 0.180 0.537 0.039 13.206 164.094 :: Date Ibs/ac Prior Years Cumulative lbs/ac 0.2914 0.0819 54.8645 2.5035 1.5852 0.0329 0.2833 1.1329 0.0844 28.157 2000 Current Cumulative lbs/ac 0.426 0.105 58.422 3.451 2.234 0.048 0.463 1.670 0.123 41.363 Permitted C. P. L. R.**** 36 34 1 1338 1 1 267 15 1 1 374 89 2498 rmi PAN Limit 1 st/2nd Crop Pe t P 194 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Danville Total Dry Tons Applied (Annual): WQ0036561 Cation Exchange Capacity (non 503 only): James Blackwell Owner: James Blackwell Predominant Soil Series: 27 Acres Permitted: 27 Site #: CS06 Field #: 98.85 111 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- Iposite Date 1 Avg. 2 _3j L 4 5 j6 L_j 7 8 9 10 11 121 % Solids 6.63 Arsenic 17.25 Cadmium 3 Copper 455.25 lChromium 121.25 Lead 83 Mercury 1.9 Molyb- denum 23 Nickel 68.75 Selenium 5 Zinc 1690 ITotal Phos- horus 21000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 11 3.66 2 3 4 5 L.6j _7j 8 9 10 11 12 c Arsenic 0.126 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.126 Cadmium 0.022 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.022 Copper 3.333 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.333 Mromium 0.888 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.888 Lead 0.608 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.608 Mercury 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Molyb- denum 0.168 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.168 Nickel 0.503 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.503 Selenium 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Zinc 12.374 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 12.374 Total Phos- horus 153.762 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 153.762 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 9/4/2014 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Danville Land Owner: James Blackwell Operator: James Blackwell Crop I Name: Fescue WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 98.85 Site #: Predominant Soil Series: CfB Crop 1 Max. PAN: 216 Crop 2 Name: 4 Acres Utilized: 27 CS06 Acres Permitted: 27 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: o c Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources DES # W Q#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Y 410 cc _ �' o a; o z 2 �, - N' 0 :n w ?'_ * N * ?: 0 TKN mg/kg z Y o � o R. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 6/17 91000 6.63 0.932 Northside WWTP Dry <.5" S 0.5 1 0.3 36875 10352.5 14.73 24.502 NA Fescue 6/18 188500 6.63 1.930 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 50.755 NA Fescue 6/19 78000 6.63 0.799 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 21.002 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): "TOTALS: 01 3575oo ::.:::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 96.259 0.000 Lime Applied Annuallbs/acre 0.126 0.022 3.333 0.888 0.608 0.014 0.168 0.503 0.037 12.374 153.762 :;::: :: > : »»»:......... ........................... ............................ Date lbs/ac Prior Years Cumulative lbs/ac 0.1853 0.0484 34.2949 1.3808 0.8723 0.0169 0.1577 0.6553 0.0571 16.5146 2000 Current Cumulative lbs/ac 0.312 0.070 37.628 2.269 1.480 0.031 0.326 1.159 0.094 28.889 Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit lstJ2nd Crop 216 C°I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: City of Danville WQ0036561 Operator: John Neese/Jerry Friddle Owner: Acres Used: 20.6 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): James Blackwell Predominant Soil Series: 20.6 Site #: CS08 Field #: 71.87 CfB 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 Avg. 2 3 j L 4 5 6 7 8 9 j 0 Ill 1 12 % Solids 6.63 Arsenic 17.25 Cadmium 3 Copper 455.25 Ichromium 121.25 Lead 83 Mercury 1.9 Molyb- denum 23 Nickel 68.75 Selenium 5 Zinc 1690 ITotal Phos- horus 21000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 11 3.49 2 3 4 5 6 7j L8]9 LOJ Llj 12 y Arsenic 0.120 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.120 Cadmium 0.021 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Copper 3.177 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.177 Chromium 0.846 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.846 Lead 0.579 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.579 Mercury 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Molyb- enum 0.160 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.160 rd Nickel 0.480 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.480 Selenium 0.035 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.035 Zinc 11.793 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 11.793 Total Phos- horus 146.538 0.000 1 0.000 1 0.000 1 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 146.538 "I certify, under penalty of law, that this document was prepared under my airecnon or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 9/4/2014 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville James Blackwell Operator: John Neese/Jerry Friddle Crop 1 Name: Fescue Crop 1 Max. PAN: 216 Crop 2 Name: WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 71.87 Site #: CS08 Acres Utilized: 20.6 Acres Permitted: 20.6 Predominant Soil Series: CfB Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: .s~ � Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES # WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Moist) Precip. Past 24 Hrs. inches to cc �? �* a a * � o %`� �', .- * N 0 7y c, w ; m 0 TKN mg/kg z o ac o w• mg/kg Nitrate and Nitrite mg/kg PAN Applied pp ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/19 130000 6.63 1.745 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.51 14.73 45.878 NA Fescue 6/20 130000 6.63 1.745 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 45.878 NA Fescue 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... .......... TOTALS: 0I 260000 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 91.7561 0.000 Lime Applied Annuallbs/acre 0.120 0.021 3.177 0.846 0.579 0.013 0.160 0.480 0.035 11.793 146.538 :::::::::::::::::::: :: Date lbs/ac Prior Years Cumulative lbs/ac o 0 0 0 0 0 0 0 0 0 Current Cumulative lbs/ac 0.120 0.021 3.177 0.846 0.579 0.013 0.160 0.480 0.035 11.793 Permitted C. P. L. R.**** 36 1 34 1 1338 1 1 267 15 1 1 374 89 2498 Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 165.33 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: John Neese/Jerry Friddle Owner: James Blackwell Predominant Soil Series: CfB Acres Used: 26.8 Acres Permitted: 26.8 Site #: CS08 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or 1 2 _3j 4 5 6 7 8 9 101 11 12 Com- Avg. posite Date % Solids 6.63 Arsenic 17.25 Cadmium 3 Copper 455.25 IChromium 121.25 Lead 83 Mercury 1.9 Molyb- denum 23 Nickel 68.75 Selenium 5 Zinc 1690 Total Phos- 1 21000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5_ 6 7 8 1 91 10 11 12 DT/Ac./ 0 App. Event 6.17 Arsenic 0.213 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.213 Cadmium 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Copper 5.617 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.617 Chromium 1.496 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.496 Lead 1.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.024 Mercury 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Molyb- 0.284 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.284 denum Nickel 0.848 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.848 Selenium 0.062 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.062 Zinc 20.851 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 20.851 Total Phos- 259.098 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 259.098 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z-/ 9/4/2014 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville James Blackwell Operator: John Neese/Jerry Friddle WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 165.33 Site #: Predominant Soil Series: CfB Crop 1 Name: Fescue Crop 1 Max. PAN: 216 Crop 2 Name: Acres Utilized: CS08 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 26.8 26.8 0 Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonsJAc) Residual Sources (NPDES # WQ#, Fert., Animal Waste, etc) Soil Cond. W Moist) Precip. Past 24 Hrs. inches Y 4 b w « o 0 o * w' 0 � w * N' . 0 TKN mg/kg Z o mg/kg Nitrate and Nitrite mg/kg PAN Applied lbs/acre ( ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/28 201500 6.63 2.079 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 54.660 NA Fescue 6/29 240500 6.63 2.481 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 65.240 NA Fescue 6/30 156000 6.63 1.609 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 42.318 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... .......... TOTALS: 01 598000 - As Cd Cu Cr Pb Hg Mo Ni Se Zn P 162.2171 0.000 Lime Applied Annual lbs/acre 0.213 0.037 5.617 1.496 1.024 0.023 0.284 0.848 0.062 20.851 259.098 ::::::>:::.::: >:...: ...... ...................... Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0 Current Cumulative lbs/ac 0.213 0.037 5.617 1.496 1.024 0.023 0.284 0.848 0.062 20.851: Permitted C. P. L. R.**** 36 34 1 1338 1 1 267 1 15 1 1 374 1 89 2498 i e P rmit PAN Limit 1 st/2nd Crop 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report acility Name: City of Danville Total Dry Tons Applied (Annual): 109.63 'ermit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: James Blackwell Owner: James Blackwell Predominant Soil Series: FaB3 kcres Used: 28.3 Acres Permitted: 28.3 Site #: CS09 Field #: 9 Aesidual Analvsis Data (Heavy Metals and Total Phosphorus use m2/k2, % Solids use Raw Percent #): ;WWPT"-1 om- positeDate Total ' . • 111 WAnnual Heavy Total DT/Ac./ App. Event 11 3.87 Arsenic 0.134 admium 0.023 Copper 3.527 Chromium 0.939 Lead 0.643 Mercury 0.015 Molyb- denum 0178 Nickel Selenium Zinc 0.533 0.039 13.094 Total Metal Field Loadings (Calculated in lbs/acre): 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1111 1 111 1 111 1 111 1 111 1 • • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1' ' . . 1: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ! 111 (:► "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�f4- 9/4/2014 >ignature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville WQ Permit #: WQ0036561 Field #: 9 Acres Utilized: James Blackwell Annual Dry Tons Applied: 109.63 Site #: CS09 Acres Permitted: James Blackwell Crop 1 Name: Fescue Predominant Soil Series: Crop 1 Max. PAN: 194 Fa133 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 28.3 28.3 0 Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. We �' Moist Precip. Past 24 �• inches Y 4 ° r; 'd c ?, a. o.w' o o %e w w * N' 5 w'e `D N TKN mg/kg Z o GQ o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual g Application Crop 1 Crop 2 Crop 1 Crop 2 6/10 26000 6.63 0.254 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.51 14.73 6.679 NA Fescue 6/11 260000 6.63 2.540 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 66.791 NA Fescue 6/13 110500 6.63 1.080 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 28.386 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... ..... TOTALS: 01 396500 :::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 101.856 0.000 Lime Applied Annuallbs/acre 0.134 0.023 3.527 0.939 0.643 0.015 0.178 0.533 0.039 13.094 162.708 :::: ::::........... ::::: : Date lbs/ac Prior Years Cumulative lbs/ac o 0 0 0 0 0 0 0 0 0 2000 Current Cumulative lbs/ac 0.134 0.023 3.527 0.939 0.643 0.015 0.178 0.533 0.039 13.094 Permitted C. P. L. R.**** 36 34 1 > ;s 1 267 1 15 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop ::::::::::.......... :: ;..: _ :.. 194 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date * * * Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report +acility Name: 'ermit #: Operator: kcres Used: City of Danville Total Dry Tons Applied (Annual): WQ0036561 Cation Exchange Capacity (non 503 only): Marc Thomas Owner: Marc Thomas Predominant Soil Series: 9.8 Acres Permitted: 9.8 Site #: CS 10 Field #: 41.34 Clifford Aesidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ample or Com- posite Date 1 Avg. 2 L3J 1 41 L 5 j6 7 8 9 10 11 12 % Solids 6.63 Arsenic 17.25 admium ic 3 Copper 455.25 hromiu 121.25 Lead 83 Mercury 1.9 Molyb- denum 23 Nickel 68.75 Selenium 5 Zinc 1690 Total Phos- horus 21000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event L11 4.22 2 J [_3j 1 41 5 61 L7J8 9 110 11 J 12 14 Arsenic 1 0.146 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.146 admium 1 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Copper 3.840 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.840 hromium 1.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.023 Lead 0.700 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.700 Mercury 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Molyb- denum 0.194 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.194 Nickel 0.580 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.580 Selenium 0.042 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Zinc 14.257 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 14.257 Total Phos- horus 177.156 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 177.156 "I certifv. under Denaltv of law. that this document was Drenared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ze; �G;: �� 9/4/2014 >ignature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville Marc Thomas Marc Thomas Crop 1 Name: Fescue WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 41.34 Site #: Predominant Soil Series: Clifford Crop 1 Max. PAN: 216 Crop 2 Name: CS10 Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 9.8 9.8 0 S. Q 1�5., Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, FertAnimal Waste, etc) Soil Cond. (Dry, e ' Moist) Precip. Past 24 Hrs• inches a �' co a o o ?» 4 iU a «, �, 0 TKN mg/kg z Y El o �1 as o a Z$• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop ] Crop 2 Crop 1 Crop 2 6/2 149500 6.63 4.218 Northside WWTP Dry <.5" S 1 0.5 0.3 36875 10352.5 14.73 110.904 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... .......... TOTALS: 01 149500 ..:-:. As Cd Cu Cr Pb Hg Mo Ni Se Zn P 110.9041 0.000 Lime Applied Annuallbs/acre 0.146 0.025 3.840 1.023 0.700 0.016 0.194 0.580 0.042 14.257 177.156 :: :::::::::::::::::.:. :: Date lbs/ac Prior Years Cumulative lbs/ac 0.116 0.043 8.79 1.881 1.113 0.019 0.133 1.094 0.135 20.522 Current Cumulative lbs/ac 0.262 0.068 12.630 2.904 1.813 0.035 0.327 1.674 0.177 34.779 Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report acility Name: City of Danville Total Dry Tons Applied (Annual): 181.50 'ermit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: Marc Thomas Owner: Marc Thomas Predominant Soil Series: Clifford acres Used: 39.2 Acres Permitted: 39.2 Site #: CS10 Field #: 2 Aesidual Analvsis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft •• site �. te Yo Solids Arsenic Total • • • 111 - =Knnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 4.63 L2J 3 4j L5 J 6 7J L8 9 10 11 J 12 0 iA Arsenic 0.160 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.160 admium 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Copper 4.216 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.216 hromium 1.123 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.123 Lead 0.769 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.769 Mercury 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.018 Molyb- denum 0.213 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.213 Nickel 0.637 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.637 Selenium 0.046 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.046 Zinc 1 15.6491 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 15.649 Total Phos- 1194.4601 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 194.460 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 9/4/2014 >ignature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville WQ Permit #: WQ0036561 Field #: 2 Acres Utilized: Marc Thomas Annual Dry Tons Applied: 181.50 Site #: CS10 Acres Permitted: Marc Thomas Crop 1 Name: Fescue Predominant Soil Series: Crop 1 Max. PAN: 216 Clifford Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 39.2 39.2 0 S. o = ° q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources DES #, W #, ert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist) precip. Past 24 Hrs. inches Y co o ,"m 0.g o c 7y 2 - N' *P= 4 - * N *1K 0 TKN mg/kg Z Y El o 5 11 ? mg/kg Nitrate and Nitrite mg/kg PAN Applied (ibs/acre) Name of Crop Type Receiving Residual Application Crop 17 Crop 2 Crop 1 Crop 2 6/4 110500 6.63 0.779 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 20.493 NA Fescue 6/5 201500 6.63 1.421 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 37.370 NA Fescue 6/6 240500 6.63 1.696 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 44.603 NA Fescue 6/7 104000 6.63 0.733 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 19.288 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTAL&I 01 656500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 121 753 0.000 Lime Applied Annuallbs/acre 0.160 0.028 4.216 1.123 0.769 0.018 0.213 0.637 0.046 15.649 194.460 :::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0 2000 Current Cumulative lbs/ac 0.160 0.028 4.216 1.123 0.769 0.018 0.213 0.637 0.046 15.649 Permitted C. P. L. R.**** 36 34 1338 1 267 1 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Danville Total Dry Tons Applied (Annual): WQ0036561 Cation Exchange Capacity (non 503 only): Marc Thomas Owner: Marc Thomas Predominant Soil Series: 38.5 Acres Permitted: 38.5 Site #: CS10 Field #: Clifford 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- Iposite Date 11 Avg. __2j L3J 4 5 6 7 8 L9J 110]11 12 % Solids 6.63 Arsenic 17.25 Cadmium 3 Copper 455.25 Chromi 121.25 Lead 83 Mercury 1.9 Molyb- denum 23 Nickel 68.75 Selenium 5 Zinc 1690 Total Phos- horus 21000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ APP• Event 11 2.33 2 131 4 51 6 7 181 9 10 1111 121 Arsenic 0.081 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081 Cadmium 0.014 1 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Copper 2.125 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.125 Chromium 0.566 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.566 Lead 0.387 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.387 Mercury 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Molyb- dnum e 0.107 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.107 rt0Nickel .321 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.321 Selenium 0.023 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.023 Zinc 7.889 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.889 Total Phos- horus 98.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 98.028 "I certifv. under nenaltv of law. that this document was nrenared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 9/4/2014 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Danville Land Owner: Marc Thomas Operator: Marc Thomas Crop 1 Name: Fescue WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 89.86 Site #: Predominant Soil Series: Clifford Crop 1 Max. PAN: 216 Crop 2 Name: CS10 Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 38.5 38.5 C 11 (� Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, w Wet, Moist) Precip. Past 24 Hrs. inches Y ° d c �. 0. o. a o %`� * N * w 5, 7y m -, * N * TKN mg/kg Z Gt o 7 m' mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/2 84500 6.63 0.607 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 15.956 NA Fescue 6/3 143000 6.63 1.027 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 27.003 NA Fescue 6/4 19500 6.63 0.140 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 3.682 NA Fescue 6/7 78000 6.63 0.560 Northside WWTP Dry <.5" S 0.5 0.3 36875 10352.5 14.73 14.729 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): J .......... TOTALSI 01 325000 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 61.370 0.000 Lime Applied Annuallbs/acre 0.081 0.014 2.125 0.566 0.387 0.009 0.107 0.321 0.023 7.889 98.028 :: ................... .... ::::::.:.. Date lbs/ac Prior Years Cumulative lbs/ac 0.156 0.052 11.004 2.289 1.486 0.026 0.18 1.41 0.161 26.665 2000 Current Cumulative lbs/ac 0.237 0.066 13.129 2.855 1.873 0.035 0.287 1.731 0.184 34.554 Permitted C. P. L. R.**** 36 34 1338 267 15 1 374 1 89 2498 Permit PAN Limit lst/2nd Crop :::::::::::::::::::::: .. 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report 4 acility Name: 'ermit #: Operator: acres Used: City of Danville Total Dry Tons Applied (Annual): 55.69 WQ0036561 Cation Exchange Capacity (non 503 only): David Sartin Owner: David Sartin Predominant Soil Series: Toast 61.4 Acres Permitted: 61.4 Site #: CS14 Field #: 1 Aesidual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . Com- positeDate • ' 111 WKnnual Heavy Metal Field Loadings (Calculated in lbs/acre): •. © © © • ,, nnu I 1 V, R 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 AM 1 11• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 ,t• 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 t® t® I� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 � � 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� � Nickel 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11• Zinc 1•• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1.• Total ' • 1•� 1 111 1 111 1 111 1 111 1 111 1 Ilt 1 111 1 Itl 1 111 1 111 1 111 1• 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. - am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". >ignature of Land Applier 9/4/2014 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville WQ Permit #: WQ0036561 Field #: 1 Acres Utilized: David Sartin Annual Dry Tons Applied: 55.69 Site #: CS 14 Acres Permitted: David Sartin Crop 1 Name: Fescue Predominant Soil Series: Crop 1 Max. PAN: 129 Toast Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 61.4 61.4 0 o ct o Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied r PP per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip Past inches D c w a o c ;v m * *w -- %u P ; P. :� 0 TICN mg/kg Z Y o N 0 w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5/29 201500 6.63 0.907 Northside WWTP Dry <.5" S 0. 0.3 36875 10352.5 14.73 23.858 NA Fescue 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... .......... rOTA1,S: 01 201500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 23.858 0.000 Lime Applied Annuallbs/acre 0.031 0.005 0.826 0.220 0.151 0.003 0.042 0.125 0.009 3.066 38.094 :: Date Ibs/ac Prior Years Cumulative lbs/ac 0.104 0.018 5.238 0.927 0.864 0.015 0.116 0.801 0.079 14.966 2000 Current Cumulative lbs/ac 0.135 0.023 6.064 1.147 1.015 0.018 0.158 0.926 0.088 18.032 Permitted C. P. L. R.**** 36 34 1 1338 1 1 267 1 15 1 1 374 89 2498 Permit PAN Limit lst/2nd Crop ::::::: :: >:::...... ;: .:.:.::.:.::::. . > »: >.... 129 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9/4/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Page: 1 of 2 Report Number: 14-085-0209 Account Number: 79434 Submitted By: ROBERT CLIFTON Send To: SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE , VA 24540 Lab Number: 98590 Sample Id: B BASIN LTS L A &L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-8401 Fax (804) 271-W6 wwwakastern.com Project: B BASIN LTS REPORT OF ANALYSIS Date Sampled: 3/24/2014 13:30:00 Date Received: 03/26/2014 00:00 Date Reported: 03/31/2014 Total Solids 6.67 66700 100.0 JM 03/26/2014 13:45 SM-2540G Moisture " 93.33 100.0 JM 03/26/2014 13:45 SM-2540G Total Kjeldahl Nitrogen 3.43 34300 10.0 JM 03/27/2014 08:44 SM-4500-NH3C-TKN Total Phosphorus 1.95 19500 100 KM 03/27/2014 12:21 SW 6010C Total Potassium 0.25 2500 100 KM 03/27/2014 12:21 SW 6010C Total Sulfur 1.32 13200 100 KM 03/27/2014 12:21 SW 6010C Total Calcium 1.74 17400 100 KM 03/27/2014 12:21 SW 6010C Total Magnesium 0.42 4150 100 KM 03/27/2014 12:21 SW 6010C Total Sodium 0.94 9350 100 KM 03/27/2014 12:21 SW 6010C Total Iron 29000 100 KM 03/27/2014 12:21 SW 6010C Total Aluminum 31600 100 KM 03/27/2014 12:21 SW 6010C Total Manganese 827 5 KM 03/27/2014 12:21 SW 6010C Total Copper 435 5 KM 03/27/2014 12:21 SW 6010C Total Zinc 1560 5 KM 03/27/2014 12:21 SW 6010C Ammonia Nitrogen 1.23 12300 10.0 JM 03/27/2014 08:44 SM-4500-NH3C Organic N 2.20 22000 10.0 03/27/2014 08:44 CALCULATION Nitrate+Nitrite-N 19.5 2.00 JM 03/27/2014 08:45 SM-450ONO3F Total Cadmium 3.0 2.0 KM 03/27/2014 12:21 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-085-0209 Account Number: 79434 Submitted By: ROBERT CLIFTON Send To: SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE , VA 24540 Lab Number: 98590 Sample Id: B BASIN LTS L A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastern.com Project: B BASIN LTS REPORT OF ANALYSIS Date Sampled: 3/24/2014 13:30:00 Date Received: 03/26/2014 00:00 Date Reported: 03/31/2014 Total Chromium 150 5 KM 03/27/2014 12:21 SW 6010C Total Nickel 73 5 KM 03/27/2014 12:21 SW 6010C Total Lead 91 5 KM 03/27/2014 12:21 SW 6010C Total Arsenic 30.0 3.0 KM 03/27/2014 12:21 SW 6010C Total Mercury 2.4 0.4 KM 03/27/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 03/27/2014 12:21 SW 6010C Total Volatile Solids 45.28 452800 100.0 JM 03/26/2014 13:45 SM-2540G Total Molybdenum 19 5 KM 03/27/2014 12:21 SW 6010C Comments: NELAP ACCREDITED: VA NELAC LAB. # 460014. PA NELAC LAB # 68-03109, FL NELAC LAB # E871087, NJ NELAC LAB # VA011. RESULTS REPORTED MEET ALL REQUIREMENTS OF THE CURRENT NELAC STANDARDS. SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. CCE FOR COMPLIANCE IN VIRGINIA AND PENNSYLVANIA ONLY. FULL TCLP AND ICR TO FOLLOW FROM MEMPHIS QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLE TKANSMITTAT. s M!r~HAIi`T OF 1-W5-02os 3111CS 7621 Whit 11111111111111111111111111111111111 IIIIII I� IIIIII IIIIIIIII INI 79434 33- 6 2014 6446 SEVERN TPP,47 SERVICFS 13 03 51 8 BASIN LTS r r4ject, Submitted By/Charge To/ Colav To. Severn Trent Services, Danville WWTP 229 Northside Drive, Danville, VA 24540 Phone: 434-799-5137 / Fax: 434-799-5220 A&L Acct # 79434 VA Permit # VA0060593 Robert Clifton robert.cIifton@stservices.com) Sample Information Lab Number Collection Information Container Information Please Check desired Tests Sample ID (Lab Use Only) Type Date Time Number at Bottles Type Volume SLt SL2 503 Nitro en PH CCE Ag Cl Others Metals Series Sowse �tSff T C C.�1 L T+ '� U� _ Grab � + f � 1 0 — �3� � ✓ Glass � Plastic _ oz int -�qt � / 1i / ti/ / V � q� ! dTs Composite ✓ F — Grab _ Glass 6t — i T dab T EI Composite _ Plastic pint t cpt np5� l — Grab Glass -- 0z Cam osite _ —Plastic —pint _ Grab Glass — oz _ Plastic —pint 2*30 L1: Total Solids (Moisture) Total K,jeldahl Nitrogen, Phous sphorand Potassium L2: Basic Test Sl I plus Sulfur. Calcium, Magnesium,Sodium: Iron. Aluminum. "Aangariese, Copper And Zinc DS Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead. Nickel, Selenium. (Copper & Zinc included In SL2) itrogen SerieY: Total Kleldahl, Ammonium, Nitrate & Organic nitrogen CE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) -7r09 /,!S�711c Page: 1 of 2 Report Number: 14-129-0200 Account Number: 79434 Submitted By: ROBERT CLIFTON Send To: SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE , VA 24540 Lab Number: 55267 Sample Id: LTS B BASIN A� A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 www.aleastem.com Project: DANVILLE WWTP REPORT OF ANALYSIS Date Sampled. 5/8/2014 09:30:00 Date Received: 05/09/2014 00:00 Date Reported: 05/21/2014 Total Solids 8.24 82400 100.0 JM 05/09/2014 13:59 SM-254OG Moisture ` 91.76 100.0 JM 05/09/2014 13:59 SM-2540G Total Kjeldahl Nitrogen 3.11 31100 10.0 JM 05/12/2014 08:39 SM-4500-NH3C-TKN Total Phosphorus 1.97 19700 100 KM 05/12/2014 13:47 SW 6010C Total Potassium 0.23 2320 100 KM 05/12/2014 13:47 SW 6010C Total Sulfur 1.12 11200 100 KM 05/12/2014 13:47 SW 6010C Total Calcium 1.75 17500 100 KM 05/12/2014 13:47 SW 6010C Total Magnesium 0.40 4020 100 KM 05/12/2014 13:47 SW 6010C Total Sodium 0.74 7420 100 KM 05/12/2014 13:47 SW 6010C Total Iron 34300 100 KM 05/12/2014 13:47 SW 6010C Total Aluminum 29900 100 KM 05/12/2014 13:47 SW 6010C Total Manganese 870 5 KM 05/12/2014 13:47 SW 6010C Total Copper 436 5 KM 05/12/2014 13:47 SW 6010C Total Zinc 1490 5 KM 05/12/2014 13:47 SW 6010C Ammonia Nitrogen 0.80 8010 10.0 JM 05/12/2014 08:39 SM-4500-NH3C Organic N 2.31 23090 10.0 05/12/2014 08:39 CALCULATION Nitrate+Nitrite-N 14.6 2.00 JM 05/12/2014 08:40 SM-450ONO3F Total Cadmium 3.0 2.0 KM 05/12/2014 13:47 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-129-0200 Account Number: 79434 Submitted By: ROBERT CLIFTON Send To: SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE , VA 24540 Lab Number: 55267 Sample Id: LTS B BASIN www.aleastern.com A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Project: DANVILLE WWTP REPORT OF ANALYSIS Date Sampled: 5/8/2014 09:30:00 Date Received: 05/09/2014 00:00 Date Reported: 05/21/2014 Total Chromium 187 5 KM 05/12/2014 13:47 SW 6010C Total Nickel 89 5 KM 05/12/2014 13:47 SW 6010C Total Lead 130 5 KM 05/12/2014 13:47 SW 6010C Total Arsenic 27.0 3.0 KM 05/12/2014 13:47 SW 6010C Total Mercury 2.3 0.4 KM 05/14/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 05/12/2014 13:47 SW 6010C Total Volatile Solids 47.82 478200 100.0 JM 05/09/2014 13:59 SM-2540G Total Molybdenum 20 5 KM 05/12/2014 13:47 SW 6010C Alkalinity (as CaCO3) 43900 100 MW 05/20/2014 10:25 SM-2320 B Comments: NELAP ACCREDITED: VA NELAC LAB. # 460014. PA NELAC LAB # 68-03109, FL NELAC LAB # E871087, NJ NELAC LAB # VA011. RESULTS REPORTED MEET ALL REQUIREMENTS OF THE CURRENT NELAC STANDARDS. SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. CCE FOR COMPLIANCE IN VIRGINIA AND PENNSYLVANIA ONLY. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr", "Ni", AND "Pb". ALL OTHER QC DATA IS ACCEPTABLE. CUSTOMER REQUESTED ALKALINITY ADDED 5/19/14 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLE TRANS)' I"T1`AL FORNIt`C. IJA CIF A& L Ea- tern Laboratories 7621 Wltitepine Road R1�;))moiiJ ly'r\ 2323'% rt:j: fiC;:i-'13_a.t_l l Fax W4-271-b446 1 CusMn;er Intorm3bQn, Pfc,ar,t Lab t hur W Sample iC tLab Use Jnty1 TYPE' Grob 8- 4l�S t✓�i� Composite Grab i11NIlIIIIIIIIiIiIiIIIIIIINIIIiINllihll�llliill�>II1111181 200 M014 SEVERN TRENT SPIRVIC.ES 1205-36 DANVILLE WWTP Goseciian iniormebon 1 L)sle I Time / 42p1� Information Container Intormabon Number Type Vutim10e rt soft-1 Glass oz PlasticOz _pint q —_pint Elastic tozGlass jGlass _pint Plastic t Glass oz _mint Plash, t: -FMw Solids (Moisture) Total Kleldahl NiNogen. Phospitoi u, and Potas;aurn r And Zinc 2, Basic Tcst SI.I phu Sulfur, C:akiam, Magnn-sium,Slalluin_ Iran, Aluminum. Manganese, Cvppr 3 Metsia: Arsenic, Cadmium. Chromium, Mercury. MOtybdenum, Lead, Nickel. Selenium. (Copper & Zinc Included In SL2) trogre htrier: TuU] Kieldahi..Ammomun Nitrate & Orglnic N111LIgen :E: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) -OM Fo: Submitted By/Charge To/ Copy To: Severn Trent Services, Danville WW" 229 Northside Drive, Danville, VA 24E Phone: 434-799-5137 / Fax: 434-799-5 A&L Acct # 79434 VA Permit # VA0060593 Robert Clifton robert.cl ifton@stservices.com) 1 Pleasa Whedk Desired Testa sw Nlvwen CGE w Ct `%lSaatalttditse Sit ,I XIXIYI I I I IX or 0 Othe%5 o/a-r s Page: 1 of 2 Report Number: 16245 0207 A LI A&L Eastern Laboratories, Inc. Account Number: 46245 7621 ,Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Submitted By: BRENT COLLINS wwwaleastern.com Send To: EMA RESOURCES INC Project: DANVILLE 755 YADKINVILLE RD NC CERT#257 MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Lab Number: 55513 Sample Id : DANVILLE Date Sampled: 5/19/2014 10:15:00 Date Received: 05/22/2014 00:00 Date Reported: 05/28/2014 Total Solids * 5.46 54600 100.0 JM 05/23/2014 08:30 SM-2540G Moisture * 94.54 100.0 JM 05/23/2014 08:30 SM-2540G Total Kjeldahl Nitrogen 4.07 40700 10.0 JM 05/23/2014 08:30 SM-4500-NH3C-TKN Total Phosphorus 2.30 23000 100 KM 05/23/2014 10:35 SW 6010C Total Potassium 0.25 2540 100 KM 05/23/2014 10:35 SW 6010C Total Sulfur 1.62 16200 100 KM 05/23/2014 10:35 SW 6010C Total Calcium 2.04 20400 100 KM 05/23/2014 10:35 SW 6010C Total Magnesium 0.42 4190 100 KM 05/23/2014 10:35 SW 6010C Total Sodium 0.96 9630 100 KM 05/23/2014 10:35 SW 6010C Total Iron 33900 100 KM 05/23/2014 10:35 SW 6010C Total Aluminum 36100 100 KM 05/23/2014 10:35 SW 6010C Total Manganese 1000 5 KM 05/23/2014 10:35 SW 6010C Total Copper 480 5 KM 05/23/2014 10:35 SW 6010C Total Zinc 1840 5 KM 05/23/2014 10:35 SW 6010C Ammonia Nitrogen 1.04 10400 10.0 JM 05/23/2014 08:30 SM4500-NH3C Organic N 3.03 30300 10.0 05/23/2014 08:30 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 05/27/2014 08:15 SM-450ONO3F Total Cadmium 3.0 2.0 KM 05/23/2014 10:35 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-142-0207 �Y� Account Number: 46245 Submitted By: BRENT COLLINS www.aleastem.com Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 55513 Sample Id : DANVILLE A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Project: DANVILLE NC CERT#257 REPORT OF ANALYSIS Total Chromium 79 Total Nickel 59 Total Lead 54 Total Arsenic 6.0 Total Mercury 0.8 Total Selenium <5.0 pH (Standard Units) * 7.68 Total Volatile Solids 52.25 522500 Total Molybdenum 28 Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. Date Sampled: 5/19/2014 10:15:00 Date Received: 05/22/2014 00:00 Date Reported: 05/28/2014 5 KM 05/23/2014 10:35 SW 6010C 5 KM 05/23/2014 10:35 SW 6010C 5 KM 05/23/2014 10:35 SW 6010C 3.0 KM 05/23/2014 10:35 SW 6010C 0.4 KM 05/23/2014 09:00 SW-7471 B 5.0 KM 05/23/2014 10:35 SW 6010C 2.00 JM 05/23/2014 08:30 SW-9045D 100.0 JM 05/23/2014 08:30 SM-2540G 5 KM 05/23/2014 10:35 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt B10SOUDS SAMPLE TRAM SMITTAI FnPX flitT.xA MT f'11- r.,r A&L Eas ,I n j IjI (�j j� 7621 Whitepine Road Richmond VA 23237 T lllll��l�'II'IIIII�I'I�I"I�11III'III��II�I�II1NII'IIIII�IIRI 462�2D147 CUStomer Inir EMA RESOURCES INC A 1 111 12:55:49 DANVILLE'NO CERT#25, Submitied By EMA Resources Inc EMA Resources Inc 755 Yadkinville Rd 755 Yadkint ille Rd Mocksville, NC 27028 Mocksville, NC 27028 Project I Z)01,,; lit Sample Information Lab Number Collection information Container Information Sample ID (Lata Use Only) Type Date Tirne Number Type Volume 5L 1 of Bott;es bnv �(c 13 —Grab ( 1 _ Glass — oZ Composite Plastic __pint 9t Grab Glass — oz Composite _ Plastic —pint at _ Grab Glass — oz — Composite _ Plastic _mint at — Grab Glass — 0Z _ Composite _ Plastic —mint _ .t IAccount # Please Check Desired Tests SL2 503 503 Nrtrooen pH CCE Ag G voiatile Series Solids I Relinquished By: (Signature) Date Tyne Received By: f Signature) Date Time s/goh y /a txPr1 ! 2z 3 Test Package Details Special Instructions or Remarks SL1: total Sulids (Moisture) Tota) Kiel dattl IN Phosphorus and PotassIurn SL2: Rasic Tost SL I plus Sulfur. Calciurn, MaEmesiunr,Sodium: Iron. Aluminum. Manganese, Copper And Zinc 503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium. (Copper $ Zinc included in SL2) Nitrogen Series: Total Kjeldahl, Ammoniarn, Nitrate K Organic Nitrogen. - --- OCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) Others Page: 1 of 2 Report Number: 14-155-0212 Account Number: 79434 Submitted By: ROBERT CLIFTON Send To: SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE , VA 24540 ( A L . ._® 11111maleastern.com A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Project: DANVILLE WWTP REPORT OF ANALYSIS Date Sampled: 6/2/2014 17:30:00 Lab Number: 55741 Date Received: 06/04/2014 00:00 Sample Id: LTS-B BASIN Date Reported: 06/10/2014 Total Solids 6.14 61400 100.0 MW 06/05/2014 07:59 SM-2540G Moisture * 93.86 100.0 MW 06/05/2014 07:59 SM-2540G Total Kjeldahl Nitrogen 4.14 41400 10.0 JM 06/05/2014 08:24 SM-4500-NH3C-TKN Total Phosphorus 2.18 21800 100 BW 06/05/2014 09:30 SW 6010C Total Potassium 0.25 2540 100 BW 06/05/2014 09:30 SW 6010C Total Sulfur 1.51 15100 100 BW 06/05/2014 09:30 SW 6010C Total Calcium 1.93 19300 100 BW 06/05/2014 09:30 SW 6010C Total Magnesium 0.38 3810 100 BW 06/05/2014 09:30 SW 6010C Total Sodium 1.12 11200 100 BW 06/05/2014 09:30 SW 6010C Total Iron 29800 100 BW 06/05/2014 09:30 SW 6010C Total Aluminum 31300 100 BW 06/05/2014 09:30 SW 6010C Total Manganese 959 5 BW 06/05/2014 09:30 SW 6010C Total Copper 470 5 BW 06/05/2014 09:30 SW 6010C Total Zinc 1870 5 BW 06/05/2014 09:30 SW 6010C Ammonia Nitrogen 1.07 10700 10.0 JM 06/05/2014 08:24 SM-4500-NI3C Organic N 3.07 30700 10.0 06/05/2014 08:24 CALCULATION Nitrate+Nitrite-N 22.8 2.00 JM 06/05/2014 08:25 SM-450ONO3F Total Cadmium 3.0 2.0 BW 06/05/2014 09:30 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9�/W , Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ftei— to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 10212 Account Number: 79434 � A&L Eastern Laboratories, Inc. 9434 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Submitted By: ROBERT CLIFTON wwwaleastem.com Send To: SEVERN TRENT SERVICES Project: DANVILLE WWTP ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE , VA 24540 REPORT OF ANALYSIS Date Sampled: 6/2/2014 17:30:00 Lab Number: 55741 Date Received: 06/04/2014 00:00 Sample Id: LTS-B BASIN Date Reported: 06/10/2014 Total Chromium 69 5 BW 06/05/2014 09:30 SW 6010C Total Nickel 54 5 BW 06/05/2014 09:30 SW 6010C Total Lead 57 5 BW 06/05/2014 09:30 SW 6010C Total Arsenic 6.0 3.0 BW 06/05/2014 09:30 SW 6010C Total Mercury 2.1 0.4 JM 06/09/2014 10:30 SW-7471 B Total Selenium <5.0 5.0 BW 06/05/2014 09:30 SW 6010C Total Volatile Solids 53.26 532600 100.0 MW 06/05/2014 07:59 SM-2540G Total Molybdenum 25 5 BW 06/05/2014 09:30 SW 6010C Alkalinity (as CaCO3) 56800 100 MW 06/05/2014 08:35 SM-2320 B Comments: NELAP ACCREDITED: VA NELAC LAB. # 460014. PA NELAC LAB # 68-03109, FL NELAC LAB # E871087, NJ NELAC LAB # VA011. RESULTS REPORTED MEET ALL REQUIREMENTS OF THE CURRENT NELAC STANDARDS. ALKALINITY, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLE TRANSMIT]IAt, FORM/CHAIN OF A&L Eastern Laboratories 7e.'.1 'A'hilclillic Rudd ROMWild V,\ 23237 Tel: 804-743-9401 Fax. 904-271-64415 1 Customer Info: Submitted MCharae To/ Copy To: Severn Trent Services, Danville WW 229 Northside Drive, Danville, VA 24! Phone: 434-799-5137 ! Fax: 434-799-5 79434 14` A&L Acct # 79434 �IIIIIIIl111IlIIIII�1III�111iI1I1111I111I111II111111I111111 THE-N �ERVt�E 31 VA Permit # VA0060593 SEVERN E)ANVILLEVdWTP Robert Clifton robert.clifton@stservices-com ProjW. Sam le Information t..ab Number Collecti-on trttorrnaten Container Infarmation !'lease C'heuk Desired Tests Sample ID (Lab Use Only) Type Gate Wino Igfgottles� Number TypE ic!ume SLt i ) 5 - ! 503 Metals Nitrogen SPrles pH F CC_ AU Cl Volatile Solids Others Q / ,icy, Grab � jv�� (I� l�C r ! _ Glass X Plastic oz pint j( a -T ja (.� _ 0/an t l 1 Basin Composite + �`t�o �_q r n — Glass -- cz Grab Plastic _pint com osite t Grab — Glass oz _pint Plastic Composite _t I - _ Grab — Glass '— Dint Plastic —p Composite lime S lot Instructions orF'emrl8r+:5 Relinquished By: (S{ nature Gate Time Recelved L' : (Signature) Oats" 1 LlafL j-3 1 writ P 'a a Qetails SL1: ToW SoUds (Nioisture) rotal K,ie!dahl Nitrogen. PJxxphorus and Potassium �O -- SL2: B sie Test Cl.I plus Sulfur. Calcium, Magnrsium,Sodium. Iron, Aluminum, Mangaru>e, Copper And Z_im $03 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum. Lead, Nickel. Selenium. (Copper & Zinc included in SL2) - Nitrogen Srries: Total Kleldahl, Ammonium. N,trate & l)f9wiic Nitrogen. CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) 4/4/2014 SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE, VA, 24540 Ref: Analytical Testing Report Number: 14-085-0218 Project Description: B BASIN LTS/TCLP Dear ROBERT CLIFTON: A&L Eastern Laboratories received sample(s) on 3/26/2014 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in our laboratory in accordance with Standard Methods, The Solid Waste Manual SW-846, EPA Methods for Chemical Analysis of Water and Wastes and /or 40 CFR part 136. The EPA requires that water samples analyzed for pH, dissolved oxygen and total residual chlorine be analyzed in the field. Analyses and results reported which do not indicate "Field" for these parameters were analyzed outside the holding time as specified in Table II of 40 CFR Part 136.3. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, instrumentation maintenance and calibration were performed in accordance with guidelines established by the USEPA and NELAP. The results are shown on the attached analysis sheet(s). Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. — Alabama #40750 Arkansas #88-0650 Illinois #200015 Kentucky #90047 Kentucky UST #41 EM a Louisiana #04015 Florida #E87943 Mississippi Pennsylvania #68-3195 Oklahoma #9311 USDA #S-46279 Tennessee #02027 EPA #TN00012 Virginia #00106 NELAP #100456 California #05240CA Texas #T104704180-05-TX L _A&.L-Eastem—Laboratories: 1 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 27i-6"6 wwrwaleastern.com Sample Summary Table Report Number: 14-085-0218 Client Project Description: -1 B BASIN LTS/TCLP -� Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID j 98603 B BASIN LTS TCLP 03/24/2014 13:30 03/26/2014 6010B ETC _1 98603 B BASIN LTS TCLP 03/24/2014 13:30 03/26/2014 7470A ETC i 98603 B BASIN LTS TCLP 03/24/2014 13:30 03/26/2014 8081A ETC 98603 B BASIN LTS TCLP 03/24/2014 13:30 03/26/2014 8151A ETC 98603 B BASIN LTS TCLP 03/24/2014 13:30 03/26/2014 8260B ETC 98603 B BASIN LTS TCLP 03/24/2014 13:30 03/26/2014 8270C ETC i 98603 B BASIN LTS TCLP 03/24/2014 13:30 03/26/2014 SW-1311 ETC V i 98603 B BASIN LTS TCLP 03/24/2014 13:30 03/26/2014 SW-1311 (ZHE) ETC I J ETC: Environmental Testing and Consulting, Inc., Memphis, TN, Certification: #1354 I , Al wwwaleastern.com. 79434 SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE, VA 24540 Submitted By: ROBERT CLIFTON } Report Number :14-085-0218 I Lab No : 98603 Sample ID : B BASIN LTS Test TCLP Herbicide Extraction TCLP Metals Extraction TCLP PCB Extraction I I TCLP Pesticide Extraction TCLP SVOC Extraction I TCLP VOC ZHE Extraction Analytical Method: 6010B Prep Method: 3005A Test i TCLP Arsenic TCLP Barium 1 TCLP Cadmium JJJ TCLP Chromium TCLP Lead i J TCLP Selenium TCLP Silver 1 I .,,A&L,Eastern-:.Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 ROBERT CLIFTON Project B BASIN LTS/TCLP Information : REPORT OFANALYSIS Report Date : 04/04/2014 Received : 3/26/2014 t awc4 I►�` io'r Pauric McGroary Agronomist Matrix: TCLP Sampled: 3 / 24/ 2014 13:30 Results Units MQL DF Date / Time By Analytical Analyzed Method Combined Combined Combined Combined Combined Combined Prep Batch(es): L194456 Results Units MQL 1 03/31/14 14:54 SAI SW-1311 1 03/31/14 14:54 SA] SW-1311 1 03/31/14 14:54 SAI SW-1311 1 03/31/14 14:54 SAI SW-1311 1 03/31/14 14:54 SAI SW-1311 1 03/31/14 14:45 SAI SW-1311 (ZHE) Date/Time Prepped: 4/1/2014 10:00:00 DF Date / Time By Analytical Analyzed Batch <0.250 mg/L 0.250 1 04/01/14 21:36 BKN L194621 0.310 mg/L 0.250 1 04/01/14 21:36 BKN L194621 <0.050 mg/L 0.050 1 04/01/14 21:36 BKN L194621 <0.100 mg/L 0.100 1 04/01/14 21:36 BKN L194621 <0.100 mg/L 0.100 1 04/01/14 21:36 BKN L194621 <0.500 mg/L 0.500 1 04/01/14 21:36 BKN L194621 <0.050 mg/L 0.050 1 04/01/14 21:36 BKN L194621 -�r _I Qualifiers/ * Outside QC limit B Analyte detected in blank Definitions C GCMS Confirmation Analysis E Exceeds calibration range g GGA outside QC limits H Beyond holding time J Estimated Value M Minimum value NA Not on Scope of Accreditation NC Not confirmed - Q Surrogate Recovery T Sample exhibits toxicity U Unconfirmed 1 AFL i wwwaleastern:com, 79434 SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR J DANVILLE, VA 24540 Submitted By : ROBERT CLIFTON Report Number 14-085-0218 Lab No : 98603 Sample ID : B BASIN LTS Analytical Method: 7470A Prep Method: 7470A I Test _A &L _Eastern_ Laboratories. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271 ,6446, ROBERT CLIFTON Project B BASIN LTS/TCLP Information : REPORT OPANAL YSIS Prep Batch(es): L194563 Results Units MQL i TCLP Mercury <0.0010 mg/L 0.0010 Analytical Method: 8081A Prep Method: 3510C Prep Batch(es): L194505 Test Results Units MQL J TCLP Endrin TCLP gamma-BHC TCLP Methoxychlor TCLP Toxaphene TCLP Chlordane TCLP Heptachlor Epoxide TCLP Heptachlor Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Analytical Method: 8151A 1 Prep Method: 8151A Test Report Date : 04/04/2014 Received : 3/26/2014 Pauric McGroary Agronomist Matrix: TCLP Sampled: 3/ 2412014 13:30 Date/Time Prepped: 4/2/2014 09:00:00 DF Date / Time By Analytical Analyzed Batch 1 04/02/14 13:01 JRS L194624 Date/Time Prepped: 4/1/2014 14:50:00 DF Date / Time By Analytical Analyzed Batch <0.001600 mg/L 0.001600 10 04/02/14 18:37 VIC L194727 <0.001600 mg/L 0.001600 10 04/02/14 18:37 VIC L194727 <0.001600 mg/L 0.001600 10 04/02/14 18:37 VIC L194727 <0.01200 mg/L 0.01200 10 04/02/14 18:37 VIC L194727 <0.008000 mg/L 0.008000 10 04/02/14 18:37 VIC L194727 <0.001600 mg/L 0.001600 10 04/02/14 18:37 VIC L194727 <0.001600 mg/L 0.001600 10 04/.02/14 18:37 VIC L194727 62.13 Limits:36-116% 10 04/02/14 18:37 VIC L194727 52.17 Limits:25-123% 10 04/02/14 18:37 VIC L194727 Prep Batch(es): L194549 Results Units MQL Date/Time Prepped: 4/1/2014 17:40:00 DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0020 mg/L 0.0020 1 04/02/14 17:24 VIC L194826 TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0020 1 04/02/14 17:24 VIC L194826 Surrogate: DCAA 49.60 Limits: 20-120% 1 04/02/14 17:24 VIC L194826 Qualifiers/ * Outside QC limit B Analyte detected in blank Definitions C GCMS Confirmation Analysis E Exceeds calibration range g GGA outside QC limits H Beyond holding time i J Estimated Value M Minimum value NA Not on Scope of Accreditation NC Not confirmed Q Surrogate Recovery T Sample exhibits toxicity U Unconfirmed i� AFL {_ www.aleastern:com 79434 ' SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE, VA 24540 Submitted By: ROBERT CLIFTON { j Report Number:14-085-0218 Lab No : 98603 Sample ID : B BASIN LTS .J Analytical Method: 8260B Prep Method: 5030E Test A-L:Eastern-,Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804)' 271.896 y TCLP Benzene TCLP Carbon Tetrachloride TCLP Chlorobenzene - TCLP Chloroform TCLP 1,4-Dichlorobenzene j t TCLP 1,2-Dichloroethane TCLP 1,1-Dichloroethene iTCLP Methyl Ethyl Ketone (MEK) TCLP Tetrachloroethene TCLP Trichloroethene I TCLP Vinyl Chloride Surrogate: 4-Bromofl uorobenzene i Surrogate: Dibromofluoromethane I i Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 l Analytical Method: 8270C Prep Method: 3510C Test ROBERT CLIFTON Project B BASIN LTS/TCLP Information : REPORT OPANALYSIS Prep Batch(es): L194748 Results Units MQL Report Date : 04/04/2014 Received : 3/26/2014 pow« mF (fawr Pauric McGroary Agronomist Matrix: TCLP Sampled: 3/ 24/ 2014 13:30 Date/Time Prepped: 4/2/2014 10:51:00 DF Date I Time By Analytical Analyzed Batch <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 <0.200 mg/L 0.200 1 04/02/14 15:13 SEB L194750 <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 <0.0100 mg/L 0.0100 1 04/02/14 15:13 SEB L194750 89.8 Limits:71-137% 1 04/02/14 15:13 L194750 80.0 Limits:70-128% 1 04/02/14 15:13 L194750 83.0 Limits:63-136% 1 04/02/14 15:13 L194750 121 Limits:70-130% 1 04/02/14 15:13 L194750 Prep Batch(es): L194457 Date/Time Prepped: 4/1/2014 10:30:00 Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol TCLP 3&4 Methylphenol TCLP 2,4-Dinitrotoluene f <0.020 mg/L <0.040 mg/L <0.020 mg/L 0.020 0.040 0.020 1 04/01/14 19:36 NFP L194587 1 04/01/14 19:36 NFP L194587 1 04/01/14 19:36 NFP L194587 Qualifiers/ * Outside QC limit B Analyte detected in blank Definitions C GCMS Confirmation Analysis E Exceeds calibration range g GGA outside QC limits H Beyond holding time J I Estimated Value M Minimum value NA Not on Scope of Accreditation NC Not confirmed Q Surrogate Recovery T Sample exhibits toxicity U Unconfirmed 1 wwwaleastern:com' 79434 SEVERN TRENT SERVICES ROBERT CLIFfON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE, VA 24540 Submitted By: ROBERT CLIFfON Report Number : 14-085-0218 Lab No : 98603 j Sample ID: B BASIN LTS Analytical Method: 8270C h r Prep Method: 3510C Test A&L_,Eastern_ Laboratories.. 7621 Whitepine Road Richmond', Virginia 23237 (804) 743-9461 Fax (804) 271 �W6. ROBERT CLIFfON Project B BASIN LTS/TCLP Information : REPORT OFANALYSIS Prep Batch(es): L194457 Results Units MQL Report Date : 04/04/2014 Received : 3/26/2014 Pauric McGroary Agronomist Matrix: TCLP Sampled: 3/ 24/ 2014 13:30 Date/Time Prepped: 4/1/2014 10:30:00 DF Date / Time By Analytical Analyzed Batch TCLP Hexachlorobenzene <0.020 mg/L 0.020 1 04/01/14 19:36 NFP L194587 TCLP Hexachlorobutadiene <0.020 mg/L 0.020 1 04/01/14 19:36 NFP L194587 i TCLP Hexachloroethane <0.020 mg/L 0.020 1 04/01/14 19:36 NFP L194587 TCLP Nitrobenzene <0.020 mg/L 0.020 1 04/01/14 19:36 NFP L194587 TCLP Pentachlorophenol <0.040 mg/L 0.040 1 04/01/14 19:36 NFP L194587 TCLP Pyridine <0.020 mg/L 0.020 1 04/01/14 19:36 NFP L194587 TCLP 2,4,5-Trichlorophenol <0.020 mg/L 0.020 1 04/01/14 19:36 NFP L194587 TCLP 2,4,6-Trichlorophenol <0.020 mg/L 0.020 1 04/01/14 19:36 NFP L194587 i Surrogate: TCLP 2,4,6-Tribromophenol 50.5 Limits: 40-125% 1 04/01/14 19:36 NFP L194587 Surrogate: TCLP 2-Fluorobiphenyl 48.5 Limits: 38-107% 1 04/01/14 19:36 NFP L194587 i Surrogate: TCLP 2-Fluorophenol 20.0 Limits: 20-110% 1 04/01/14 19:36 NFP L194587 Surrogate: TCLP 4-Terphenyl-d14 51.5 Limits: 33-122% 1 04/01/14 19:36 NFP L194587 ? Surrogate: TCLP Nitrobenzene-d5 42.5 Limits: 29-110% 1 04/01/14 19:36 NFP L194587 Surrogate: TCLP Phenol-d6 14.3 Limits: 10-115% 1 04/01/14 19:36 NFP L194587 Qualifiers/ * Outside QC limit B Analyte detected in blank Definitions C GCMS Confirmation Analysis E Exceeds calibration range g GGA outside QC limits H Beyond holding time J Estimated Value M Minimum value NA Not on Scope of Accreditation NC Not confirmed A &L.rvEaste.m..Labo_ratories: 7621 Whitepine,Road Richmond,, Virginia 23237 (804) 743-94D1 Fax.(804) 271-6446, W W W.aleastemxom Cooler Receipt Form Customer Number: 79434 Customer Name: SEVERN TRENT SERVICES Report Number: 14-085-0218 Shipping Method 0 Fed Ex 0 UPS 0 US Postal Client 0 Lab 0 Courier 0 Other Shipping container/cooler uncompromised? 0 Yes 0 No Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Required Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) (— Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes IS No Comments: Any regulatory non-compliance issues will be recorded on non-compliance report. Signature: Brandi Watson Date & Time: 03/26/2014 13:57:00 i �u��om�:r tnto: SAMPLE Ti�"r�Sl�rr�-�'eT.. t �ViICHAIh1 O Submitted By/Charge To/ Colav To. Severn Trent Services Danville IAMITP ern Laboratories 229 Northside Drive Danville, VA 2 14-o85-0218 i Pic: Bt}4-?il-t+446 S 7� o�Z�2o,4 Phone: 434-799-5137 / Fax: 434-799-5 1350.00 nation A&L Acct # 79434 SEVEFN TRENT SERVICES B BASIN LTSfTCIP Charge Tt) VA Permit # VA0060593 Robert Clifton robert.clifton@stservices,comj Project Snm le Informabon Lob Number Collection Information Containarinformation Please (,hock Deslmd Tantn _ i ypa Date Tima Humber of Bottles TYPO Volume Sample IQ (Lab Use Only) 503 SLf SI-2 tiiatols hiitroge-1 volatile Sarin+ phi GCr A(f CI sows Mars b again �..i-j�' C� Grob l I ` �14 1 �i� I�aO ~ 415'IF ✓ Glass Plastic -^— cz - -p1ntVol �'-` Composite - � glrtT-�ti1� T 11`� _Grab ^ C7�e — oz Plastic ptnl rw " Com o t _ _ Grab _ Glass -- of Co Ile _ Plastic _pint — Grab Glass Plastic — oz ---pint — _ Relinquished By: (Signature) Date `rime Fteceiveu B 'Sl natucu Uuiv Time T/fY (D or,< Test ('�tcka e Q eiaAfi �� special Insttvctlone or Remarica A: Total Solids (Moisture) Total Kjeldahi Nitrogen, Phosphorus nrd Potassium p t L. L2: Basic Teat SLt plus Sulfur, Calcium, Mognosium,Sodium, Iron, Aluminum, Mmcgancsc, Copper And Zinc � F � r $03 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, NIL*el, Solanium. (Copper & Zinc Included In SI-2i Nitrogen Series: Total KIrldahl, Ammonium, Nitrate K Organic Nitrogen. GCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) �..Oq 1S7°G u 4540 220 _ a or n 4/14/2014 SEVERN TRENT SERVICES ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR DANVILLE, VA, 24540 Ref: Analytical Testing Report Number: 14-085-0219 Project Description: B BASIN LTS/ICR Dear ROBERT CLIFTON: A&L Eastern Laboratories received sample(s) on 3/26/2014 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in our laboratory in accordance with Standard Methods, The Solid Waste Manual SW-846, EPA Methods for Chemical Analysis of Water and Wastes and /or 40 CFR part 136. The EPA requires that water samples analyzed for pH, dissolved oxygen and total residual chlorine be analyzed in the field. Analyses and results reported which do not indicate "Field" for these parameters were analyzed outside the holding time as specified in Table II of 40 CFR Part 136.3. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, instrumentation maintenance and calibration were performed in accordance with guidelines established by the USEPA and NELAP. The results are shown on the attached analysis sheet(s). Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, s %d- 0 6°"- Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the 1 analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Alabama #40750 Louisiana #04015 Florida #E87943 California #05240CA Arkansas #88-0650 Mississippi Pennsylvania #68-3195 Texas #Tl04704180-05-TX 'i Illinois #200015 Oklahoma #9311 USDA #S-46279 Kentucky #90047 Tennessee 402027 EPA #TN00012 Kentucky UST #41 Virginia #00106 NELAP #100456 1 � x 1 RLA A&L stern-labor-afories _ 7621,Whitepin6,Road Richmond,Viiginia23237 (804)743-9401 Faz(804)271-6446 _1 wwwaleastemcom Sample Summary Table Report Number: 14-085-0219 Client Project Description: B BASIN LTS/ICR --J Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 1 98604 B BASIN LTS Solids 03/24/2014 13:30 03/26/2014 SW-1030 ETC `) 98604 B BASIN LTS Solids 03/24/2014 13:30 03/26/2014 SW-7.3.3 ETC 98604 B BASIN LTS Solids 03/24/2014 13:30 03/26/2014 SW-7.3.4 ETC -J 98604 B BASIN LTS Solids 03/24/2014 13:30 03/26/2014 SW-9045C ETC i ETC: Environmental Testing and Consulting, Inc., Memphis, TN, Certification: #1354 I 1 AFL J` wwwaleastern,com 79434 SEVERN TRENT SERVICES j ROBERT CLIFTON NORTHSIDE WWTP 229 NORTHSIDE DR G DANVILLE, VA 24540 J Submitted By : ROBERT CLIFTON j Report Number : 14-085-0219 Lab No : 98604 Sample ID: B BASIN LTS i Test i I Cyanide (Reactivity) Ignitability pH (Standard Units) J Sulfide (Reactivity) j f 1� �A&L _ Eastern_�,Laboratories. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-946t Fax (804)'271.6446. ROBERT CLIFTON Project B BASIN LTS/ICR Information : REPORT OFANALYSIS Results Units MQL Report Date : 04/14/2014 Received : 3/26/2014 Pauric McGroary Agronomist Matrix: Solids Sampled: 3/ 24/ 2014 13:30 DF Date / Time By Analytical Analyzed Method 0.272 mg/Kg 0.125 1 04/04/14 08:00 KM2 SW-7.3.3 >96 Degrees C 1 04/03/14 07:25 GHD SW-1030 6.9 S.U. 1 04/08/1413:30 TAW SW-9045C 251 mg/Kg 25.0 1 04/04/14 08:00 KM2 SW-7.3.4 Qualifiers/ * Outside QC limit Definitions C GCMS Confirmation Analysis i B Analyte detected in blank E Exceeds calibration range � L _A&L..:Ea:stern-.._Laboratories._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 74M401 Fax (804) 271-6446, wwwaleaste-m.com Cooler Receipt Form Customer Number: 79434 Customer Name: SEVERN TRENT SERVICES Report Number: 14-085-0219 Shipping Method 0 Fed Ex Is UPS 0 US Postal Client 0 Lab 0 Courier 0 Other] _ Shipping container/cooler uncompromised? 0 Yes 0 No Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Any regulatory non-compliance issues will be recorded on non-compliance report. Signature: jBrandi Watson Date & Time: 03/26/2014 14:01:30 7621 Whitq SAMPLE TRANSMITTAL i kIA/CIIAM OF! A&L Eastern Laboratories `I-6446 Z L___)Mtr rnr0. Submitted By/Charge To/ Copy To: Severn' Trent Services, Danville WWTP 229 Northside Drive, Danville, VA 24540 Phone: 434-799-5137 / Fax: 434-799-5220 111111 Jill 111111111111111111111111111111 19 Jill 11N A 8� L A ccfi # 79434 i Illlll lull ��� 0 -0 0 VA Permit # VA0060593 SE ERN VENT SERVICES 14:00:2a B BASIN LTSiICR I Robert Clifton robert.clifton@stservices.com) Project -- — — Sample Informatlon Lab Number Collection Information Container Information Please Check Desired Teats Type Date Time Number of Bottles Type Votume SL I SL2 503 Nletals Nitrogen Series pH CCE Ag CI Volatile Solids Others Sample ID (Lab Use only) Irj CI,�UU� _ Grab 3 �ayy1 12'� o _' ✓ Glass '�_' Plaattc -- olnt L?$ c o&Ile T 6330 �t Fir _ Grab Glass -- 0z [ nII« afa i t 1 — i Plastic —pint + !at"rc`x►�,* Z�QMP04118 at _.._� �...__.... _...._. _ _ Grab Glass -- oz Plastic _ —pint Com osite I ql Grab L class — oz Plastic ---pint cj_ —- Relinquished By: (Signature) Date Time Received (Signature) Date TImL 2 ; 30 Test Package Details Special Instructlone or Rema*s SLI I Total Solids (Moisture) Total Kjeldahl Nitrogen, Phosphorus and Potassium J .e SL2; Basic Teat SLI plus Sulfur, Calcium, Ma&7esium,8odium, Iron. Aluminum, Manganese, Copper And Zinc b t t 603 Metale: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium. (Copper & Zinc Included in SL2) Nitroken Series: Total K.icldahl. Ammonirun, Nitrate do Organic Nitrogen. CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime: Treated Sludge) 7 aC. rJ' I ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Danville WQ Permit Number: WQ0036561 WWTP Name: Northside WWTP NPDES Number: VA0060593 Monitoring Period: From 3/20/2014 To 3/20/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative uerformed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ra Y ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density 21 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ D' Anaerob is ig estion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- Frequency of Analysis Sample 'Type Analytical Tech-nique MinimumGeo. Mean aximu Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 71038 122912 270270 MPN/g 0 Quarterly G SM92210E- 2006 CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ ! CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if i you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine %/ that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jerry Shupe - Project Manager Pre arer Name and Title type or print) ' - � Si ature f Preparer* U Date Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) zu 4� 9/15/2014 Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Danville WQ Permit Number: WWTP Name: Northside WWTP NPDES Number: Monitoring Period: From 5/19/2014 To 5/19/2014 WQ0036561 VA0060593 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed: Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray E31 Gamma RayPasteurization Class B: Alt. (1) Fecal Density 0 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number oFrequency Excee- ences of Analysis Y Sample Type Analytical Tech-ni ue q inimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gam of total solids MPN 283 381 510 MPN/g 0 Quarterly G SM92210E- 2006 CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .11071- Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jerry Shupe - Project Manager Preparer Name and Title type or print) Sijjnture a Preparer* U Date Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) z�z 4;2� 9/15/2014 Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date .DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: _ WWTP Name: _ Monitoring Period: City of Danville Northside WWTP From 6/4/2014 To WQ Permit Number: WQ0036561 NPDES Number: VA0060593 6/4/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative Derformed: Class A: Alt. A (time/temp) [3Alt B (Alk Treatment) [3 Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑Gamma Ray teurization Pasteurization ❑ Class B: Alt. (1) Fecal Density 21 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ c Anaer obi Digestion estion ❑ g If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g Number o Excee- dences Frequency of Analysis Sample 'Type Analytical Tech-nique Minimum Geo. Mean klaximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 267 291 332 MPN/g 0 Quarterly G SM92210E- 2006 CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative Derformed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jerry Shupe - Project Manager Preparer Name and Title (type or print) —AV,1V,Z/5. Si ture Preparer* Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) I -/I "/i Z�Z 42�- 9/15/2014 Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WWTP Name: City of Danville Northside WWTP Monitoring Period: From 6/16/2014 To WQ Permit Number: WQ0036561 NPDES Number: VA0060593 6/16/2014 Pathoeen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative Derformed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) El Alt. C (Prior Testing) El A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ R Beta a Gamma Ray ❑ Y Pasteurization za i Class B: Alt. (1) Fecal Density 0 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ 1 Composting ❑ Aerobic Digestion ❑ D' e Ana gti erobic i son If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g � Number o Excee- dences Frequency of Analysis Sample Type Analytical Tech -pique Minimum Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 269 366 1242 MPN/g 0 Quarterly G SM92210E- 2006 CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 NON per 4 grams total solid (dry I weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative Derformed: Alt.1 (VS reduction) 21 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ j CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jerry Shupe - Project Manager Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 9/15/2014 Si6latureaPreparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Analytical Results EMA Resources, Inc. 755 Yadkinville Rd. Mocksville NC 27028 Entered 3/20/2014 - Reported: 4/29/2014 For: Danville Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst. 140320-9.1 % Solids 1 1.85 % SM264OB-1997 3120/14 CL 140320-9.1 Fecal Coliform MTF 1 270,270 MPN/g SM9221 CE-2006 3/20/14 CL 140320-9.1 'Geometric Mean 1 122,912 MPN/g dry wt. basis 3124/14 CL 140320-92 % Solids 2 1.87 % SM254OB-1997 3/20/14 CL 140320-9.2 Fecal Coliform MTF 2 90,909 MPN/g SM92210E-2006 3/20/14 CL 140320-9.3 % Solids 3 1.84 % SM254OB-1997 3/20/14 CL 140320-9.3 Fecal Coliform MTF 3 92,391 MPN/g SM92210E-20.06 3/20/14 CL 140320-9.4 % Solids 4 1.84 % SM254OB-1997 3/20/14 CL 140320-9.4 Fecal Coliform MTF 4 163,043 MPN/g SM92210E-2006 3120114 CL 140320-9.5 % Solids 5 1.83 % SM254OB-1997 3/20/14 CL 140320-9.5 Fecal Coliform MTF 5 120,219 MPN/g SM92210E-2006 3/20/14 CL 140320-9.6 % Solids 6 1.79 % SM254OB-1997 3/20/14 CL 140320-9.6 Fecal Coliform MTF 6 134,078 MPN/g SM92210E-2006 3/20114 CL 140320-9,7 %. Solids 7 1.83 % SM254OB-1997 3120/14 CL 140320-9.7 Fecal Coliform MTF 7 71,038 MPN/g SM92210E-2006 3/20/14 CL 140320-9.8 Bench 30 Day Bench 12.9 % EPA625R-92/0 3/20114 CL PQ. Box 228 • Statesville, North Carolina 28687. 7041872/4697 'EMA Resources, 'I'ne. 755 Vadk6ville. Rd-. Mocksville. NC. 27028` Entered 3120/2014 . Reported: ,4/29/2014 , For: f Date !.Sample ID Parameter Cust.ID Result Units Method Analyzed 'Analyst Respectfully,'.submifted,. -; Derta Myers NC Cert .440, NCDW- Cert.#37755, , -, EPA NC0090.9 . M Box 228.8t ites- ine,. Norih .CaroHm.2868.7.7.04/872/4G9,7 EMA Resources, Inc. 755 Yadkinville Rd. Mocksville NC 27028 Enteredt 3/20/2014 Reported: 4/29/2014 Sample ID:140320-9.8 Analytical"Results For: Danville PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30dayl' Total'Solids Volatile Solids % Volatile Solids Week 1 133 0:94 0.54406 Week Z 1.73 0.95 0.5511 Week 3 1.74 0.91 0.5220 Week 4 1.70 0.90 0.5283 Week 5 1.64 0:83 6.5059 Volatile Solid-s' Reduction: ,0.5406 - 0.5059 'X 100 =.12.9 % 0:5406 - (0.5406 X 0.5059) Respectfully submitted, Dena Myers Statesville Analytical, Inc: NC WW Cert.# 440NC DW Cert. #37755 P.O. Box 228 - 'Statesville, North Carolina 28687.704/872/4697 Client; /A Q�Sc+tx�rat•- - STATESVILLEANALYTICAL 122 Court Street P.O. Box 228 Statesville. NC 28687 Chain of Custody Recar�l: Addiess: .._- C6rttact Poison: Phone.#; 334-7V% iggl , FAX#, 33re•'Z'` ; P,O # Requisitioned by: (TRI8. Date} Ctistoitter ' 8ampie ID# . Cab -ID #� Tmq Samplod (Grati3Oniy} Datesampled' (Grab ohij! p ° . Matrix Barometers:requested toy analysis = - sludgo - w ww �. 4Jivi• -! U 7a 3� i�4 MCA�: it�?Qrp. `Relinquished by: � ,� Time 2 )0povam, pm. Date � idol :��1 SamDled bv: f� ,"Received by: Tale am, Nh Date l_/_ . Transported by: ..Relinquished,b Time am,."pm Date _/ I_ Holding,times met: b T ��. a atel L/ . :Received Y - :i , pm Compliance work: .Coi>�posite Sampling`#1• Time begin :"- am, pm •Date:—/` -.%_ Non-compliance work:; - Ti''me�'end am; pm Date, t a_ b comments: -'Coiliiposite Sampling #2: Time.begin .. am pm', Date._/ Time end = am, pm Date /=/, Analytical Results - EMA Resources, Inc. 755 Yadkinville Rd. Mocksville NC 27028 'Entered 5/19/2014 - Reported: 5/22/2014 For: Danville Date sample ID Parameter Cust ID Result Units Method Analyzed Analyst - 140519-4.1 % Solids 1 3.92 % SM254OB-1997 5119/14 HM ' 140519-4.1 Fecal Coliform MTF 1 <510 MPN/g SM92210E-2006 5/19/14 HM -14051:9-4.1 Geometric Mean 1 <381 MPN/g dry wt. basis 5/22/14 CL 14.0519-4.2 % Solids 2 4.86 % SM2540B-1997 5/19/14 HM : 140519-4.2 Fecal Coliform MTF 2 <412 MPN/g SM92210E-2006 5/19/14 HM 140519-4.3 % Solids 3 -5.67 % SM254013-1997 5/19/14 HM ,1405194.3 Fecal Coliform MTF ^, <353 MPN/g SM92210E-2006 5/19/14 HM 140519-4.4 %c Solids 4 5.10 % SM254OB-1997 5/19/14 HM 140519-4.4 Fecal Coliform MTF 4 <392 MPN/g SM92210E-2006 5/19/14 HM. 140519-4.5 %'Solids 5 4.98 % SM254OB-1997 5/19/14 HM ,14051.9-4.5 Fecal Coliform MTF 5 <402 MPN/g SM92210E-2006 5119114 HM 140519-4.6 % Solids .6 5.70 % SM254OB-1997 5/19/14 HM 140519-4.6 Fecal Coliform MTF 6 <351 MPN/g SM92210E 2006 5/19/14 HM 140519-4.7 % Solids 7 7.07 % SM254OB-1997 5/19/14 HM 140519-4.7 Fecal Coliform MTF 7 <283 MPN/g SM9221 CE2006 6/19114 HM PO. Box 228 - Statesville, North Carolina 28687 & 704187214697 EMA Resources, Inc. 755 Yadkinville Rd. --IMocksville NC 27028 Entered 5/19/2014 Reported: 5/22/2014 For: Date Sample ID Parameter Cust ID Result Units Method Analyzed. Analyst Respectfully submitted, i Dena Myers NC Cert #440, NCDW Cert #,37755, EPA NCO0909 P.O. Box 228 • Statesville, North Carolina 28687. 704/872/4697 Client:. r 43oJft P_3 _ - STAMVILLE ANALYTICAL 122 Court Street" • P.O. Box 228 Statesille NG 28687 Chaai Of -: Custody Record Address: ff�� a .y !'SQ tj10f - d L.-!i y _ ' contact Person'. n pa6lli� F,-,,hone # {{ FAX# PO # Requtsttioried by: (Time Date) 'Custbmer ' S4m IeID# p Lab-1D# Tlme Sampled (Grab Only) . Dafe.Sampted (Grab•Only) a �. Matrix parameters requested for analysis ow -w.: ww •' 7 Relinquished by: - - Time.` amp Date, .�/_/ - - Sampled.,:by - J Received by)�.� Time pm Date/ 6/ Transported by • Relinquished by: Time am; pm Date -1-1 Holding times met:.t Received t5y; _ -- Time arri; 'pm Date _I I Compliance work: Composite;Samuling#1 c . ` Tinge begin — pm Date 'l ! Non-compliance work: Time Time end 'am, pm Date /_/_ Lab:Comments: Composite Sampling #2: , -Tme--begin ":. ---,,am; pm, Date _�,/— - Time, end - : atn�: pm. - Date _. l._Z = : Analytical Results -EIVIA Resources, Inc. 755 Yadkinville Rd. Aocksville NC 27028 Entered 6/4/2014 : teported: 6/12/2014 ,or: Danville Sample ID Parameter Cust ID Result Units Method Date Analyzed AnalYst 140604.7.1 % Solids 1 6.66 % SM254OB-1997 614114 CL 140604-7.1 Fecal Coliform MTF 1 <300 MPN/g SM9221 CE-2006 614/14 CL 140604-7.1 Geometric Mean l 294 MPN/g dry wt.'basis 6/9/14 CL 140604-7.2 % Solids 2 6.58 % SM2540B-1997 614114 CL 40604-7.2 Fecal Coliform MTF 2 <304. MPN/g SM92210E-2006 614114 CL 140604-7.3 % Solids 3 7.44 %` SM254OB-1997 6/4114 CL 140604-7.3 Fecal Coliform MTF 3 <269 MPN/g SM92210E-2006 6/4/14 CL 140604-7.4 % Solids 4 6.91 % SM2540B-1997 6/4/14 CL 140604-7.4 Fecal Coliform.MTF4 <289 MPN/g SM92210E-2006 6/4/14 CL 140604-7.5 % Solids 5 6.03 % SM254OB-1997 6/4/14 CL 140604-7.5 Fecal Coliform MTF 5 332 MPN/g SM92210E-2006 6/4/14 CL 140604-7:6 %Solids - 6 7.49 ' °/a SM254.06-19$7 6/4/14 CL : 140604-7.6 Fecal Coliform MTF 6 <267 MPN/g SM9221 CE-2006 6/4114 CL Respectfully submitted,, Dena Myers NC Cert #440, NCDW Cert #37755,, - EPA NC00909' I P.O. Bcix 228 - Statesville, North Carolina 28687.704/872/4697 Client: FM At)arc • - STATESVILLE ANAUYTICAL 122 Court Street • `P.O. BOm228 Sta587tesville. NC.28 04) 8724607 lain of C .. Address: ,, y , ,I i 'Contact. Person: r -".E �/ 2_ ,. _ Custody:Record PO..# Requisitioned by:. ',(TimeI Date) y, 4VOL Customer. ,Sample,IdN Lab-1D d TimelSampled (GraE� Only), _ � Date.Sampied {Giati Only) � a. �` Matrix ParBmete�s requested #o[;analy$is s ua5a .:w i Rel'inquished.'by: "". Y; Time :Q : 4 m� UAW C,� I I_ ' am, p l . N 'Sampled tiy;: fD if Received,.hy: Time am, pm' Date % : /_ Transported by: Relinquished by: - Time am, pm. Dater_ r Holding times met: Recelveci,by: _Time Compliance work: CompoaiWSarnpling #1: Time begin • am; Pm Date Non -;compliance work: Time. end am, pm. Date _h/� Lab eommen'is: Composite Sampling_#2;. Time'begin am, .pm 'Date _7_l_ Time end Analytical Results _J --J;EMA Resources; Inc: -75a Yadkinville Rd. IMocksvil{e NO 2?02$ - iEntered "61512014. JReported:. 6/1=014 -or: Danvilie,replacement 6%4114 Safi*e ID Parameter Cust ID Result". Units Method Dat® Analyzed Analyst," 1.40605-27 % Solids 7 replacement- 6,65 %: SM25408-1997 615114 --A40605-27 Fecal Coliform MTF 7 replacement, . <301 MPN4 SM92210E-2006 '615114 _J 'Respectfully submitted, ,Dena Myers. _! NO Cert #440: NCD1N Cert #37755 . EPA' NC00909 CL cL P.O.-Box:228 wSiatesville,North Carolina L28687 - 704/872/4697 -_i —_J —J I .Client; iPA t5 r - b !° - STATESVILLEANALYTICAL 122 Couri Stree{ - P.C. box.228 Statesvil le. NC 28687 (704872-4697- Address:- .,:. 'Contact- Person: d�rrr C �l�,a Phone # FAX# -7. --1 Hq 3 .- 1- �'��tZ Clhain of Cu§#o ecord dy R . tt (Tme Datej. PO #, � - Requisitionetl by: Ciii. Customer - Sample IDii Cab•ID # Time;Sainpled - ° " (Grab;Only) " - - Date Sampled (Grab Onfy) n e . _ Matrix ted _ s regues ,_ _for analysis Parameter 94. w. ° . ww J®Adf �f _. "i✓..?"" •� d 1� 1> 4�,tV� - / . / /1) _ a hhi J_ wo^. L i° _A f,. n i dffv¢ . Fite. l Relinquished by: • _ Timedi�i5 ate.$' L / �' %/ �! . ''' , - _.-. - ,.,. Sampled _ +,yam - Received by: m. 1 �� _ : - �,. 1' Time I �ys ri am;#Date / /,if Transported by: r.,%. Relinquished by: Time, ,- A(, am, m- ate' / 5 % / Holding times Received by: F Time . �t am, pte ,met: Co' liance_work":, Composite Sampling"#i: Time. begin _am, pm Date ! /� Non=compliance .work. Time -end am, pm Date / = / .:,,' Lab Comments: Composite' Sam piing#2: Time begin. - aril, -,pm Date _./_/_ I Tme"end am, pm .Date �,A alytical Results 4 . EMA Resources; Inc. 755 Y0dkinville-.Rd.., j Mocksv'ille', NC 27A28- Entered, 6/1612014- Reported: 6/1912014, i � Fon. D4,+v; ' Sample ID' Parameter . Gust ID Result � Uniits. Method � Date Analyzed Anal ` 140616;3.1 %861ids. 1 7.26 % 8M2540B-1997 6/17114 H.M• ;140616-3:1 i ; ;:Fecal Coliform MTF 1 276�. MPN/g SM92210E 2006 6/1.7114 Hit 1140616-3.1 Geometric Mean 1. 366. MPN/g dry wt., basis 6/18/14 CL 14w6-12' %Solids 2 7.44 °! SM254OB-1997 61171.14 ' HM j 140616=3:2 Fecal Coiiform MTF 2 269 MPN/g SM92210E 2006 6117114, HM 14061673.3 % Solids 3' .6.49 % 8M2640BI-1997 6/17/14 HM 1406164,3 Fecal Conform MTF 3 308 MPN/g'. SM9221 CE 2006 -,6(17/14� HM 140616-3.4 :% Solids _ 4, 6,44 °lo . SM2540,13=1997 6l17/14 HM 140616=3.:4 Fecal Coliform MTF 4 1242 -MPNIg , SM0221'CE2006.. 6/17/14" .HM �140616-3.5 %:Solids 5 6.15 % SM254OB-1997 6/1,7/14 HM '140616°=3 5 FecaI Coliform:MTF 5` : ' . <325` `" MPN/g . , . . SM922,10E 2006. ' " fi(,17t t4` " HM ` 140616-3:6 •%,Solids' 6 _ 632 Dlo SM254013-1,997 6/17/14 NM 140616-3.6 Feca'I oliform MTF 6 - 298 MPN/g SM92210E-200& 6(.17/14 HM 140616-31 % Solids: 7 6.26 %o' SM2540B-1'997 611.7/14 . HMas 140616-3,7 Fecal Coliform MTF 7 319 MPN/g SM92210E-2006 6(17114 HNI_ P-0. Bog 229 • Statesville, NortkCardina'28687 . 7041872/4697 EMA Rasour-cesinc. 755 Yadkihville Rd. Mocksville NC 270,28 Entered 6/16/2014 Reported.,, 6/19/2014 For: Sample ID Parameter Cust"ID Date Result Units-, Method Analyzed Analyst Respectfully- §LibmOed, Dena, Myers NG.,Cert #440 NCDW Geri #37755, EPA NC00909- PO. Box 228 • Statesville, North Carolina 28687 704/872/4697 Client: STATESVILLE ANALYTICAL Address: `� `7�s } _ - 122 Court Street • P.O. Box 228 -1 Statesville, NC 28687 (7tk1) 8724697 Chain of Custody Record i6��vt i4 I F 1lYLp Contact Person: / /j Phone # FAX# �{ I Requisitioned by: (Time Dat®} PO #El F, j; i IL Customer Sample 10# Lab -ID # Time Sampled (Grab Only) Date Sampled (Grab Only} n �j Parameters requested foranalysis Sludg© watra , voa, t r '{J 4 tiL% " ° 4 may: c3 o Fe, i�- 0 a V1 V \V l , I I Relinquished by: Received by: Relinquished by: t Received by: (�i-.- "'~_ ` Composite Sampling-#1: Time begin am, pm Date / / l Time end am, pm Date Composite Sampling #2: l Time begin am, pmDate Time end am, pm Date __/__/_ Time t ,; C> am,O Date ' A` Time am, pm Date I^1 Time am, pm Date J� Time am pm Date L/ { k, { I.ab Comments. _1 Sampled by: ' Transported by: 19C Holding times met: Compliance -work: Non-compliance work: BASIN PROFILE B BASIN Sample Date 5/8/2014 Quarter 2nd Sludge Level 11 (Maximum Tank Level = 15 Feet) Basin Location Located closest to access road Catwalk I nr_atinnc B2, B4, 136: adjacent to access road 61, B3, 135: adjacent to A Basin side The RAS 1 & 2 twelve month average used to calculate % Volatile Reduction = 60.12% = 0.6012 as a decimal RAS 1 & 2 %TVS Data Oct-12 62.85% Feb-13 60.46% Jun-13 59.50% Nov-12 68.40% Mar-13 63.65% Jul-13 52.80% Dec-12 58.30% Apr-13 64.10% Aug-13 56.75% Jan-13 66.80% May-13 57.80% Sep-13 51.00% Observation B Basin was wasted into from October 1, 2012 thru September 30, 2013. RAS wasted to this basin during this time frame was used in the calculation. Profile of the sludge was taken from each catwalk of B Basin and composited. A Basin %Total Solids (%TS) = 8.24 as a A Basin %Total Volatile Solids (%TVS) = 47.82 = ##### decimal %Volatile Reduction; IN - OUT x 100 IN - (IN x OUT) IN = %TVS of the RAS average as a decimal OUT = %TVS of Basin sample as a decimal %Volatile Reduction: 0.6012 - 0.4782 x 100 0.6012 - (0.6012 x 0.4782) %Volatile Reduction = 39.2 > 38% required for land applicatioi I W1 of Report Number: 14-177-0554 Account Number: 46245 @9AL_, Send To: EMA RESOURCES INC wwwaleastern.com 755 YADKINVILLE RD MOCKSVILLE NC 27028 Date Received: 06/26/2014 - - (- -' A&L_Ea_sternlaboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Grower: JAMES BLACKWELL Farm ID: CS-06 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Analysis: 06/27/2014 Date Of Report: 06/27/2014 a.', .� .' �•$am . .. tea'.`.. Or a Ic Ma er - g n tt = . ° Ph" os`P h ru' .o s Potassirim< IVIa nesium 9-,,p Calcium" °'Sodium �H✓ " Acirli' tY Ie ID=� P'o FieId1D,.` La6.` ��:Number" ENRIlAehlich'3 - Reserve i°K_' ,'� Mg Ga Na 'Soil Buffer_H .'< /oR�ate,_` Ibs1A . `ppm Rate ppm Rate �-.� =ppm Rate`° .E` 'ppm Rate "pH Ir►tlex . meg1100g megl100g PPm�Rafe ppmRate, . 1 22354 3.7 M 115 55 H 188 VH 137 H 614 L 18• VL 5.6 6.78 1.5 6.2 NC=46 NC=96 2 22355 3.3 M 108 116 VH 59 L 156 H 621 M 16 VL 6.1 6.86 0.7 ;4NC=97 NC=30 3 22356 4.5 M 129 H 188 221 VH 86 L 885 M 25 VL 5.5 6.73 2.0 7.8 NC=73 NC=113 4 22357 4.6 M 126 184 H 273 VH 174 M 1337 M 25 VL 5.7 6.69 2.4 11.3 NC=70 NC=140 P scent Base.Saturation`,.:'"_ ` e _ _ i r e N t at Sulfur Zinc - Man" ariese' 9 , iron a Cope. ` pp BoKon j° '•Solutle $alas Chloride ' . F Aluminum",c SamplelD ield ID K . M g; ,Ga Na 3 Mn Fe Cu ;8 SS CI•;',.5 AI . .o o /o 0 /o;':. 0. ' •%: , .,;.< m a "e rii ate ;pP R m ~ -Rate f pP„pR m Rate. PRE Rate pp, m` _ -Rate: ms%cm Rate ' m ' • Rate Pp RP. m, .a., , z.,d PP ,.Rate, ppm ;R-t ,. . 1 10 L 4.6 H 52 VH 232 VH 1.6 H 0.5 L 0.11 VL 7.8 18.4 49.5 1.3 23.4 NC=21 NC=115.0 NC=325 NC=80.0 2 7 VL H 83 VH 153 VH 12.2 VH 0.5 L 0.08 VL 2.8 24.1 57.5 1.3 13.6 �7.7 NC=15 NC=192.5 NC=519 NC=610.0 3 L 7.1 H 101 VH 152 VH 13.6 VH 0.6 M 0.1 VL 7.3 9.2 56.7 1.4 25.9 �13 NC = 27 NC = 177.5 NC = 631 NC = 680.0 4 16 M 13.7 VH 277 VH 161 VH 14.3 VH M 0.19 VL 6.2 12.8 59.2 1.0 21.1 10.9 NC=33 NC=342.5 NC=1731 NC=715.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Ratingafter each value: VL e Low), L (Low), M (Medium), (pounds per acre), ms/cm milli -mhos per centimeter), me /100 maximum of thirty days after testing. (Very ) ( ) ( ) (p p ) ( P ) q g by. Pctw" XF 60,wr H (High), VH (Very High). ENR -Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = IbslA, Analysis prepared by: A8L Eastern laboratories, Inc. C.E.C. - Cation Exchange Capacity. Soluble Salts ms/cm x 640 = ppm. Pauric McGroary W1 of I _ - Report Number: 14-177-0556� Account Number: 46245 Send To: EMA RESOURCES INC WWwaleastern.com 755 YADKINVILLE RD MOCKSVILLE NC 27028 Date Received: 06/26/2014 Date Of Analvsis: 06/27/2014 A&L_Eastem Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Grower: NEESE/FREDDIE Farm ID: CS-8 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Resort: 06/27/2014 Organic Matter �, Phosphorus -., Potassl'um� _ Magnesiurri , . ; Calcium 'T _ Sotlium P _ = pH Acidity, . C.E C p� Sample ID FieldlD Lab Number' ENR` % Rate 1 Meriiich 3 • Reserve K Mg - Ca " Na' $oif- ,. Buffer. _ .Ibs/A Rate p 'in � m .. Rate. �PP . ppm . ` Rate m ,: Rate pP � p,P m . ., Rate pp m Rate H P. Index ;' me /100 q 9 me " /700 q %-. 1 22361 3.1 M 102 242 VH 122 M 173 H 817 M 23 VL 6.1 6.84 0.9 6.9 NC = 202 NC = 62 -Percent Base Saturation,., Nitrate, -- :Sulfur'. 'Zinc- _ .Manganese" :Iron` ` " Copper-` „ ' -Boron ` SolutileSattsChloride Aluminum.: Sample IDS," Field K Mg - Ca Na ,. , H NO3N ` . _ �S Zn - Mn Fe .. Cu B SS . CI .: = Al 7 ID ppm Rate ppm Rate ppm Rate ppm -, Rate 'ppm `Rate ppm Rate ppm Rate 'ms/cm Rate ppm Rate ppm 1 10 L 10.1 VH 26 H 145 VH 15.6 VH 0.6 M 0.1 VL 4.5 20.9 59.2 1.4 13.7 NC=21 NC=252.5 NC=163 NC=780.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: ?0,z. XF G0wr� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Analysis prepared by: A&L Eastern Laboratories, Inc. 1 C.E.C. - Cation Exchange Capacity. Soluble Salts ms/cm x 640 = ppm. Pauric McGroary s�&C'� ., OnOrTnc vivlslon rnvne: a i 733-zoos t / - —vdebs`iie: vvuvW:ncagr.goviagronontiu- _.. _ __ _..----� _.__ [ r«pyrt Nb:046z - Client: John Neese Advisor: EMA Resources Inc. Predictive tt 7327 Strawberry Ln Summerfield, NC 27358 755 Yadkinville Rd Mocksville, NC 27028 Mehlich-3 ExtractionaSOil Repo Sampled County: Caswell Sampled: Received: 07/09/2014 Completed: 07/17/2014 Farm: NC-CS-08 Links to Helpful Information Sample ID: 00002 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - WIV in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drrP]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 1.16 9.2 91 0.8 6.3 141 39 60 29 27 218 143 498 498 514 0.1 1 Sample ID: 00003 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrassfTim, 1 0.0 120-200 0 50 0 0 0 0 0 0 Note: 12 2- $pH Test Results [units - WIV in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.18 10.5 93 0.8 6.4 159 45 60 31 28 243 156 720 720 643 0.1 1 Forth- Carolina� Tobaad Trust FOnd tomiriissiont Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture ow 1 Of Report Number: 14-177-0558 A&L-Eastem- LaboratoriesAccount Number: 46245 9AFL _ 7627 Whitepine Road Richmond, Virginia 23237 (904) 743-9401 Fax.(804) 271-6446 Send To: EMA RESOURCES INC wwwaleasterncom Grower: 755 YADKINVILLE RD GLENN HODGES Farm ID: MOCKSVILLE NC 27028 CS-09 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Received: 06/26/2014 Date Of Analysis: 06/27/2014 Date Of Report: 06/27/2014 Organic Matter' Phosphorus u Potass mN- .yMa ne ium. g s Calcium -Sodium.';"' T H° P Acidi" uh( . E. Sample ID- Lab ENR % F,. Mehhch 3 Reserve , K Mg Ca Na 'Soil ` 'Field ID Number Rate ° Ibs1A ppm Rate ppm ,SRate 'ppm Rate ppm Rate ppm Rate ppm Rate pH3 <- Index :,wmeq/100g meq/100g ; j 9 22363 3.4 M 110 58 H 49 VL 73 M 586 M 26 L 5.3 6.76 1.7 5.5 NC = 48 1 'NC = 25 Percent'Basesaturation-Ni tiate Sulfur Zmc Manganese Iron Copper,"= Boron "Soluble—Salts—sChlor�de Aluminum , Sample ID" Ca Na', . H NO3N S Zn . , :; ; Mn. Fe •< :,Cu ' . Ba, ,, .. ,: SS ' CI AI Field ID :' .. %' _ %„ . .. % .' °/a ;' ppm _,Rate ppm Rate .ppm Rate ppm ° .Rate`a'PPm Rate PP..n!,.3-Rate, PRm= .Rate ins/cm :Rate PPmz , ,Rate ;ppm 9 12 L 3.7 H 22 H 131 VH 6.3 VH 0.4 L 0.06 VL 2.3 11.1 53.3 2.1 30.9 NC=25 NC=92.5 NC=138 NC=315.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. PW« mF 60wr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Soluble Salts ms/cm x 640 = ppm. Pauric McGroary Report Number: 14-177-0555 Account Number: 46245 Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE NC 27028 Date Received: 06/26/2014 AFL www.aleastem.com A&L-Eastem !.abolratodes 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Grower: MARC THOMAS CS-10 Farm ID: SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Analysis: 06/27/2014 Date Of Report: 06/27/2014 1 r.aOrganic Matter. �Pliosptiorus =Potassium -Magnesium CalaiuOn, pH Aci2lity � , , , v:: �Sodiuin tSampie ID "FieId,1D' '- 'Lab ENR Mehhch-3 - Reserve;Buffed., -°Number ;'�%-"`" . Rate , Ibs/A" P,p, m Rate Pp m Rate - 'm ,Rate Pp ; m 'Rate pP ip Rate Rp , PPn4 . Ratem pH "Index :'"megjl100g ,°ineg1100g`� 1 22358 2.8 M 99 30 L 65 L 168 VH 539 M 13 VL 6.2 0.6 4.9 NC = 25 NC = 33 2 22359 3.6 M 112 20 L 216 VH 128 M 1107 M 17 VL 5.7 6.78 1.5 7.3 NC=17 NC=110 5 22360 3.4 M 109 80 H 56 L 146 H 514 L 23 VL 5.2 6.72 2.1 6.1 NC=67 NC=29 :. Percent,Base Saturation., Nitrate r Sulfur. `Zinc Man anese 9 $,Iron; ,z Cap er° • ` RP Boron ,'• 1 Soiutite,$a)ts Chloride r Aluminum:'< 'Sample ID, F,ie1d1D. K.x. Mg '. Ca:" Na = H NO3N S Zn kMri Fe Cu °7° ' "` °�° ,ry 07°" "; %9, F" °7° m' '.:Rate, PP a ' m ;Rate PP_ . PP my .. Rate, PP m - Rate .PP m Rate m ,"•, Rate PP a m` Rate Pp, ms/cm`,A,Rate,' ppm Rate ppm 1 6 VL 3.2 M 84 VH 92 VH 1.3 M 0.5 L 0.1 VL 3.4 28.6 55.0 1.2 12.2 NC=12 NC=80.0 NC=525 NC=65.0 2 13 L 1.9 L 40 H 153 VH 1.4 M 0.6 M 0.32 VL 7.6 14.6 55.3 1.0 21.0 NC=27 NC=47.5 NC=250 NC=70.0 5 14 L H 273 VH 4.2 VH 0.6 M 0.09 VL 2.4 19.9 42.1 1.6 34.2 �7.7 �29H NC=29 NC=192.5 NC=181 NC=210.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pam« me G0„r H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Analysis prepared by: A&L Eastern Laboratories, Inc. v�j" C.E.C. - Cation Exchange Capacity. Soluble Salts ms/cm x 640 = ppm. Pauric McGroary 1 of Report Number: 14-177-0557 Account Number: 46245 Send To: EMA RESOURCES INC wWWaleaste.mtom 755 YADKINVILLE RD MOCKSVILLE NC 27028 Date Received: 06/26/2014 Date Of Analysis: 06/27/2014 A& - East_em L ab ora tones 7621Whitepine,Road Richmond, Vrginia23237 (804)743-9401 Fax(804)271-W6 Grower: DAVID SARTIN Farm ID: CS-14 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 06/27/2014 °Organic"Matter ,.Phos`iho�us- R, ,° :Potas§ium� " Ma nes'ium g Calcium Sodium•. , pH.'•'' Acidi Sa1n le ID P . ;Field ID.` = Labh Number ENR • �/, Rate."'" Mehl 3 Reserve K.. M 9 " Ca3 Na' Sotl Buffer H a Ibs/A Pp m .:Rate m?~ -Rate �pR. `m Rate PP- `pp m :Rate pp m Rate" 4m Rate pP :.p!I Indez.' me L100 Q 9 me; /100 q g 1 22362 2.4 L 91 248 VH 54 L 98 H 494 M 17 VL 5.5 6.81 1.2 4.7 NC = 207 NC = 28 ".RercenYBase 5atur'aton `., Nitrate _ Sulfur", Zmc Man anese 9 . Iron Co"` e� pP . wBoron Soluble.Salts °Chloride, `= Aluminum' p .,�� Mg� Ca: ` : Na ' H„ :. NO".N s ,,.5, .� ,.' : s •.,;°; Zn `� Mn Fe .: : Cu '�, �. B a ppni�-: Rate ppm .' Rate ppm, x Rate ppm; �` Rates ppin :Rate ',ppm xtiRate ppm��' "Rate.ms/cm, RaYe� ppm Rate ppm , 1 11 L 12.9 VH 118 VH 207 VH 4.6 VH 0.6 M 0.07 VL 2.9 17.4 52.6 1.6 25.8 NC = 23 NC = 322.5 NC = 738 NC = 230.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. : me Gr� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, y Porz. C.E.C. - Cation Exchange Capacity. Soluble Salts ms/cm x 640 = ppm. Analysis prepared by: A8L Eastern Laboratories, Inc. b Pauric McGroary