WQ0035749_Residual Annual Report 2014_20150330

2014 ANNUAL REPORT
LAND APPLICATION PROGRAM
NORTH CAROLINA DEPARTMENT OF TRANSPORTATION
PERMIT # WQ0035749
PREPARED BY:
ROBIN L. MAYCOCK
NORTH CAROLINA DEPARTMENT OF TRANSPORTATION
1558 MAIL SERVICE CENTER
RALEIGH, NC 27699-1558
FEBRUARY 2014 RECEIVEDIDENRID WR
MAP 30 2W5
Water Quality
Permitting Section

STATE OF NORTH CAROLINA
DEPARTMENT OF TRANSPORTATION
PAT MCCRORY
GOVERNOR
March 20, 2015
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
ANTHONY J. TATA
SECRETARY
Reference: NCDOT Land Application 2014 Annual Report
Permit No. WQ0035749, NC Department of Transportation
Land Application of Diamond Grinding and
Hydrodemolition Operation Slurry
Dear Mr. Hardee:
The North Carolina Department of Transportation (NCDOT) is submitting all monitoring
and reporting requirements as specified in Condition IV in Permit WQ0035749. Due to
adverse weather delays, an email requesting an extension on the March 1, 2015 deadline
was sent to Ed Hardee (DWR, Water Quality Permitting Section) on March 3, 2015. An
extension was granted until April 1, 2015, as referenced by the attached email. The
following hydrodemolition projects utilized the subject permit in calendar year 2014:
Mt. Misery Road over Highway 74, located in Leland, New Hanover County
College Road/West Market Street Bridge #8, New Hanover County
I-40 "Fortify" Bridges (Sunnybrook Rd, Crabtree Rd), Wake County
Wright Memorial Bridge #35 over Currituck Sound, Currituck County
The projects listed above are shown in the table below with correlating information on the
bridge name, project number, laboratory name, report number and the date sampled.
BRIDGE
PROJECT
LAB NAME
REPORT #
DATE
Mt. Misery Rd.
C203074
Environmental
2014-15971
10/14/2014
Chemists, Inc.
College Rd.
C203074
Environmental
2014-15972
12/26/2014
Chemists, Inc.
I-40 Bridges
C203166
ESC Lab Sciences
L693672
4/14/2014
Sunnybrook Rd.
A&L Eastern Labs, Inc.
14-101-0203
5/8/2014
Crabtree Rd.
14-101-0204 ,
4/10/2014
Wright
C203338
Microbac Labs, Inc. —
23-20140328-14
4/10/2014
Memorial
Wilson
(R41014)
Bridge #35
A&L Eastern Labs, Inc.
14-101-0215
4/10/2014

In summary, the total amount of hydrodemolition operation slurry (HOS) that was land
applied in 2014 was 607,000 gallons, as shown by project in the table below.
PROJECT/BRIDGE
TOTAL GALLONS
Mt. Misery Road
31,000
College Road
8,000
I-40 Bridges
132,000
Wright Memorial Bridge #35
436,000
TOTAL
607,000
The 2014 Annual Report is broken into two sections, Laboratory Analyses by Project, and
Land Application Logs by Project. If any further information is required or there are any
questions regarding this Annual Report, please .contact Ms. Robin Maycock at (919) 861-
3780 or by email at [e-mail].
Sincerely,
Michael L. Holder, PE
NCDOT Chief Engineer
Attachments: 2014 Annual Report
cc: Robin Maycock, L.S.S., L.A., NCDOT
Thomas C. Niver, P.G., NCDOT
Kenneth Pace, P.E., NCDOT

Maycock, Robin L
From:
Hardee, Ed
Sent:
Tuesday, March 03, 2015 1:36 PM
To:
Maycock, Robin L
Cc:
Mcdaniel, Chonticha
Subject:
RE: WQ#0035749
Robin,
With this email I am granting an extension for submittal of the 2014 Land Application Annual Report for permit
WQ0035749 until April 1, 2015. Include a copy of this email in the report.
Ed Hardee
Division of Water Resources
Water Quality Permitting Section, Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
Phone [phone]
DISCLAIMER: Email correspondence to and from this address is subject to the North
Carolina Public Records Law and may be disclosed to third parties unless the content is
exempt by statute or other regulation.
From: Maycock, Robin L
Sent: Tuesday, March 03, 2015 1:31 PM
To: Hardee, Ed
Cc: Mcdaniel, Chonticha
Subject: WQ#0035749
Ed:
Due to the adverse weather and other delays, I would like to request an extension on submittal of the 2014 Land
Application Annual Report for the NCDOT Programmatic Permit for Diamond Grinding and Hydrodemolition
Slurry. Please respond to confirm that this is possible. I think that two weeks should be enough time to get it reviewed
and signed internally.
Thanks!
Robin
Email correspondence to and from this sender is subject to the N.C. Public Records Law and may be disclosed to third parties.

TABLE OF CONTENTS
SECTION TITLE
LABORATORY ANALYSES of HYDRODEMOLITION OPERATION
SLURRY (HOS)
2014 LAND APPLICATION SUMMARY

SECTION I: LABORATORY ANALYSES OF HYDRODEMOLITION OPERATION SLURRY

Mt. Misery Road Bridge Report # 2014-15971

'Environmental Chemists, Inc.
a 6602 WmdmiA Way a Wilmington, NC 28405
[phone] (Lail) ® [phone] (Fax)
710 Bowsertown Road e Manteo, NC 27954
[phone]
ANALYTICAL & COMSULnNG
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Levels Farms & Liquid Waste, INC. Date of Report: Jan 21, 2015
8155 Malpass Comer Road Customer PO #:
Currie MC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report 4: 2014-15971
Project ID: Bridge Samples
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-38938 Site: Bridge #1 10/14/2014 12:00 PM Solid/Sludge Client
Tact Method Results Date Analyzed
CCE AOAC 1.005 0.1 % 01 /21 /2015
Total Solids (%) SM2540 B 1.02 % 01/02/2015
pH SM 4500 H B 12.2 units 01/09/2015
Comment:
Reviewed by:
Report#:: 2014-16971 Page I of t

W.WW ...uu..nn ■Woy -. nnarsyw.q .•v -. ' ;
neENVIRONMENTAL CHEM15T5, INC; OFFICE: 910-392.0223 FAX [phone]
Analytical Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION 9 37729 [e-mail] '
COLLECTION ARID CHAIN OF CUSTODY
CLIENT: ��; � �
PROJECT NAME:
REPORT NO: 1-1*941
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO-
email:
Sarn fed : SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identifq
Collection
m
c m
r
H a
°
to
°
„
..2r. E
o W
m 2
PRESERVATION
ANALYSIS REQUESTED
D to
Time
Temp
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G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
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Transfer
Relinquished B :
Date/Time
Received By:
Date/Time
Temperatuve when Received: Accepted: �
Delivered By: Received By:
Comments:
mesample
!,
Time: 1---

College Road Report # 2014-15972

n-viron, mental Chemlsts, In. c.
6602 Windmill Way ilmnington, NC 28405
[phone] (Lab) ® [phone] (Fax)
710 Bowsertown Road o lVantec), NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR. DWQ CERTIFICATE #94 DLS CERTIFICATE #37729
Lewis Fars & Liquid Waste, UNC.
8 155 Malpass Comer Road
Currie NC 28436
Attention: Wesley Wooten
Date of Report: Jan 21, 2015
Customer PO #:
Customer ID-. 14020008
Report #, 2014-15972
Project ID: Bridge Samples
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-38939 Site: Bridge #2
12/2612014 12:00 PM Solid/Sludge Client
Test Method Results Date Analyzed
CCE AOAC 1.006 0.1% 01/2-1/2015
Total Solids (%) SM 2540 8 20.9% 12/30/2014
pH SM 4600 H B 12.1 units 01/09/2015
Comment
Reviewed by:
ikeport*: 2014-15972 Page 1 of 1

i E N V I KU N M E N I AL G H L M l b I b! I N U OFFICE: 910.392-0223 FAX [phone]
Analytical & Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION #r 37729 [e-mail]
C®LLECTION AND CHAIN OF CUSTODY
CLIENT:
------------------LL----- -- -
PROJECT NAME:
REPORT NO:ADDRESS-
CONTACT CONTACT NAME:
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO:
email:
Ramnlad RV- SAMPLE TYPE: I = influent. E = Effluent. W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
- ^ —
Sample ��entiCatl®rD
Collection
m
°
L
E° t7
V
; ,..
„
s E
m
PRESERVATION
ANALYSIS REQUESTED
lea a
Time
Temps
i
s
�►
s
M
z
s
G
o
171
G
G
C
P—
G
G
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Transfer
Relinquished By.
Date/Time
Received By:
DateMme
1.
Temperature When Received: l ' AccepteU: sarnp1n F%W uv U.
Delivered By: Received By: l ®ate: / r Time: �
Comments: TU NA OUND:

1-40 Bridges — Sunnybrook and Crabtree Roads Report #L693672 (TCLP)

DATA SUMMARY & CALCULATION SHEET
Date Prepared - April 28, 2014 ItS&M E
"COOT Project No.1361-12-161A, Phase 09, Granite Construction
Comparison of laboratory reported metal concentrations in the hydrodemolition solids vs IHSB preliminary remedial goals
Sample ID = Fortify- Sunnybrook Bridge. Sample Collected on April 14, 2014. Sample Collected By= Rob Willcox with SBME, Inc.
Constituent
Basis
Lab Results
(Total Metals)
m
Lab
Method
Preliminary
Residential -Health
Based Soil
-Remediation Goal .
(PSRG)
Ik
PSRG Health Based
Adjusted Values'
m
Protection of
Groundwater PSRG
m
Lab Results
(SPLP Method)
u
HCAC 2L
Groundwater
Quality Standards
u IL
Arsenic
C
4A
6010E
0.61
30.5
5.8
0.32
10
Barium
N
37
6010B
3000
5000
580
94
580
Cadmium
N
<0.37
6010B
14
23.3
3.0
<5.0
2.0
Hexavalent Chromium'
CIM
6.6
7199
0.29
14.6
3.8
20
10
Lead'
1.8
6010B
400
400'
27D
4.0
15
Mercury
N
c 0.029
7471
2.0
3.3
1.0
< 0.20
1.0
Selenium
N
1.0
6010B
78
130.0
2.1
< 20
20
Saver
N
0.5
6010B
1 78
130.0
3.4
8.2
20
=concentration reported in the sample is greater than the lion -adjusted PSRG
= concentration reported in the sample is greater than the Protection of Groundwater Remedlal' Goal
Hexavalent Chromium* = Hexavalent chromium has the most restrictive goal for the different forms of chromium. Total chromium has also been
reported and is below PSRG Goals
Lead ' = The SRG is based on USEPA guidance on lead cleanup levels. The value cannot be adjusted
Preliminary PSRG Health Based Goal. Adiusted Values' (methodoloav taken from reference 2 below):
For carcinogens = PSRG Health Goal x 100in, where n = number of carcinogens present (for the above example n =2)
For non -carcinogens = PSRG Health Goal x 51n, where n = the humber of non -carcinogens present (for the above example n = 3)
Basis
C = The PSRG is based on the carcinogenic endpoint and corresponds to an'excess lifetime cancer risk of 1 in i,000,000
N = The PSRG is based on the non -carcinogen endpoint and corresponds to a hazard quotient of 0.2.
M = Contaminant is a mutagen
References:
1) Inactive Hazardous Site Branch, Preliminary Soil Remediation Goals (PSRG) Table, July 2013
2) Registered Environmental Consultant Program, Implementation Guidance, (November 2012 (Edited 12112112)
t+,UMlVonnWpWL1QuswwHWNCDOT%PhM02-W—WG Wk4Sn.M2M41nfumam\Crmt.cmv hnWrdnft Vn Vm NtMhb [NOUble-4-2sr4

a
OESC
1
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814209
Est. 1970
Rob Willcox
S6ME Inc. - Greensboro NC
3718 Old Battleground Road
Greensboro, NC 27410
Report Summary
Thursday April- 24, 2014
Report Number: L693672
Samples Received: 04/15/14
Client Project: 1588-10-027
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
JiM4Hunt , ESC Representative
Laboratory Certification Numbers
A2LA —1461-01, AIRA - 100789, AL - 40660, CA - 01157CA, CT-.PH-0197,
FL - E87487,. GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV3752DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-ii-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 20

12065 Lebanon Rd.
Mt. Juliet, TN 37122
OESC 1615) 758-5858
1-800-767-5859
Fax [phone]
L•A•B S•C•1•E•N•C•E•S
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Rob Willcox April 24, 2014
S&ME Inc. - Greensboro NC
371E Old Battleground Road
Greensboro, NC 27410
ESC Sample
# L693672-01
Date Received April 15,
2014
Description Fortify-Sunnybrook Bridge /
Crabtree
Bridge
Site ID :
RALEIGH,
NC
Sample ID SUNNYBROOK DEWATERING BOX
Project
1588-10-027
Collected By Rob Willcox
Collection Date 04/14/14 11:50
Parameter
Result
Det. Limit
Units
Limit
Method
Date/Time
By
Dil
Corrosivity
Corrosive
9045D
04/17/14
1536
MGM
1
Ignitability
See Footnote
Deg. F
D93/101
04/19/14
1505
AS
1
Reactive CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B
04/16/14
1354
ASK
1
Reactive Sulf.(SN846 7.3.4.1)
BDL
25.
mg/kg
9034/90
04/16/14
1315
JBG
1
TCLP Extraction
-
1311
04/17/14
0809
LJN
1
Mercury
BDL
0.010
mg/l
0.20
7470A
04/18/14
1437
CCE
10
Arsenic
BDL
0.45
mg/1
5.0
6010C
04/18/14
1842
ST
1
Barium
BDL
1.4
mg/l
100
6010C
04/18/14
1842
ST
1
Cadmium
BDL
0.45
mg/l
1.0
6010C
04/18/14
1842
ST
1
Chromium
BDL
0.45
mg/1
5.0
6010C
04/18/14
1842
ST
1
Lead
BDL
0.45
mg/l
5.0
6010C
04/18/14
1842
ST
1
Selenium
BDL
0.45
mg/l
1.0
6010C
04/18/14
1842
ST
1
Silver
BDL
0.45
mg/1
5.0
6010C
04/18/14
1842
ST
1
TCLP 2HE Extraction
-
1311
04/18/14
1501
MVE
1
TCLP Volatiles
Benzene
BDL
0.050
mg/l
0.50
8260B
04/19/14
2058
JC
1
Carbon tetrachloride
BDL
0.050
mg/1
0.50
8260B
04/19/14
2058
JC
1
Chlorobenzene
BDL
0.050
mg/1
100
8260B
04/19/14
2058
JC
1
Chloroform
BDL
0.25
mg/l
6.0
8260B
04/19/14
2058
JC
1
1,2-Dichloroethane
BDL
0.050
mg/l
0.50
8260B
04/19/14
2058
JC
1
1,1-Dichloroethene
BDL
0.050
mg/l
0.70
8260B
04/19/14
2058
JC
1
2-Butanone (MEK)
BDL
0.50
mg/l
200
8260B
04/19/14
2058
JC
1
Tetrachloroethene
BDL
0.050
mg/1
0.70
8260B
04/19/14
2058
JC
1
Trichloroethene
BDL
0.050
mg/1
0.50
8260B
04/21/14
1708
JC
1
Vinyl chloride
BDL
0.050
mg/1
0.20
8260B
04/19/14
2058
JC
1
Surrogate Recovery
Toluene-d8
97.8
% Rec.
114.
8260B
04/19/14
2058
JC
1
Dibromofluoromethane
94.8
% Rec.
125.
8260B
04/19/14
2058
JC
1
a,a,a-Trifluorotoluene
102.
% Rec.
114.
8260H
04/19/14
2058
JC
1
4-Bromofluorobenzene
99.6
% Rec.
128.
8260B
04/19/14
2058
JC
1
TCLP Pesticides
Chlordane
BDL
0.0050
mg/l
0.030
8081A
04/19/14
1506
CBB
1
Endrin
BDL
0.0050
mg/l
0.020
8081A
04/19/14
1506
CBB
1
Heptachlor
BDL
0.0050
mg/l
0.0080
8081A
04/19/14
1506
CBB
1
L693672-01 (IGNITABILITY) - Did Not Ignite 0 170 F
Page 2 of 20

u A
12065 Lebanon Rd.
Mt. Juliet, TN 37122
OESC
[phone]
1-800-767-5859
Fax [phone]
L•A•B 5•C•I•E•N•C•E•5
Tax I.D. 62-0814289
e
Est. 1970
REPORT OF ANALYSIS
Rob Willcox
April 24,
2014
S&ME Inc. - Greensboro NC
371E Old Battleground Road
Greensboro, NC 27410
ESC Sample
# L693672-01
Date Received April 15, 2014
Description Fortify-Sunnybrook
Bridge
/ Crabtree
Bridge
Site ID
RALEIGH, NC
Sample ID SUNNYBROOK DEWATERING BOX
Project
1588-10-027
Collected By Rob Willcox
Collection Date 04/14/14 11:50
Parameter Result
Det. Limit
Units
Limit Method
Date/Time By Dil
Lindane
BDL
0.0050
mg/l
0.40 8081A
04/19/14 1506 CBB 1
Methoxychlor
BDL
0.0050
mg/l
10. B081A
04/19/14 1506 CBB 1
Toxaphene
BDL
0.010
mg/l
0.50 8081A
04/19/14 1506 CBB 1
Surrogate Recovery
Decachlorobiphenyl
90.3
% Rec.
123. 8081A
04/19/14 1506 CBB 1
Tetrachloro-m-xylene
89.1
% Rec.
114. 8081A
04/19/14 1506 CBB 1
TCLP Herbicides
2,4,5-TP (Silvex)
2,4-D
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
TCLP Semi-Volatiles
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-dl4
BDL
0.0020
mg/l
1.0
8151A
04/18/14
2335 KLM 1
BDL
0.0020
mg/l
10.
8151A
04/18/14
2335 KLM 1
87.0
% Rec.
8151A
04/18/14
2335 KLM 1
BDL
0.10
mg/1
7.5
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/l
0.13
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/1
0.13
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/l
0.50
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/1
3.0
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/1
2.0
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/l
5.0
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/l
400
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/l
200
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/l
100
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/l
400
8270C
04/21/14
1731 KMF 1
BDL
0.10
mg/l
2.0
8270C
04/21/14
1731 KMF 1
41.3
% Rec.
87.0
8270C
04/21/14
1731 KMF 1
23.7
% Rec.
67.0
8270C
04/21/14
1731 KMF 1
60.0
% Rec.
120.
8270C
04/21/14
1731 KMF 1
79.2
8 Rec.
122.
8270C
04/21/14
1731 KMF 1
68.9
% Rec.
148.
8270C
04/21/14
1731 KMF 1
66.2
% Rec.
149.
8270C
04/21/14
1731 KMF 1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum Contaminant Level as established by the US EPA
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/24/14 17:34 Printed: 04/24/14 17:35
L693672-01 (IGNITABILITY) - Did Not Ignite @ 170 F
Page 3 of 20

OESC
1
REPORT OF ANALYSIS
Rob Willcox
S&ME Inc. - Greensboro NC
3718 Old Battleground Road
Greensboro, NC 27410
April 24,2014
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
ESC Sample #
L693672-02
Date Received
April 15, 2014
Description
Fortify-Sunnybrook Bridge /
Crabtree
Bridge
Site ID
RALEIGH, NC
Sample ID
SUNNYBROOK DEWATERING BOX
Project #
1588-10-027
Collected By
Rob Willcox
Collection Date
04/14/14 11:50
Parameter
Result
MDL
RDL
Units Qualifier Method
Date
Dil.
Arsenic
0.00032
0.00025
0.0010
mg/1 J
6020
04/21/14
1
SPLP Extraction
-
1312
04/20/14
1
Mercury
U
0.000049
0.00020
mg/l
7470A
04/22/14
1
Barium
0.094
0.0017
0.0050
mg/l
6010B
04/23/14
1
Cadmium
U
0.00070
0.0050
mg/l
6010B
04/23/14
1
Chromium
0.020
0.0014
0.010
mg/1
6010B
04/23/14
1
Lead
0.0040
0.0019
0.0050
mg/l JP1
6010B
04/23/14
1
Selenium
U
0.0074
0.020
mg/l
6010B
04/23/14
1
Silver
0.0082
0.0028
0.010
mg/l JP1
6010B
04/23/14
1
U = ND (Not Detected)
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit LOQ PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/24/14 17:34 Printed: 04/24/14 17:35
Page 4 of 20

REPORT OF ANALYSIS'
Rob Willcox
S&ME Inc. - Greensboro NC
3718 Old Battleground Road
Greensboro, NC 27410
April 24, 2014
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]'
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
ESC
Sample #
L693672-03
Date Received
April 15., 2014
Description
Fortify-Sunnybrook
Bridge /
Crabtree
Bridge
Site
ID
RALEIGH, NC
Sample ID
SUNNYBROOK DEWATERING BOX
Project
#
1588-10-027
Collected By
Rob Willcox
Collection Date
04/14/14 11:50
Parameter
Dry
Result
MDL
RDL
Units
Qualifier Method
Date
Dil.
Hexavalent Chromium
6.6
0.26
1.5
mg/kg
71199
04/24/14LI
ORP
-100
my
2580 B-2
04/17/14
1
pH
12.
su
9045D .
04/18/14
1
Total Solids
68.3
0.0333
2540 G-2
04/16/14
1
Mercury
U
0.0028
0.029
mg/kg
7471
04/17/14
1
Arsenic
4.4
0.32,
1.5
mg/kg
J6J3
6010B
04/22/14
1
Barium
37.
0.085
0.37
mg/kg
J6J3
6010B
04/22/14
1
Cadmium
U
0.035
0.37
mg/kg
J6J3
6010B
04/22/14
1
Chromium
14.
0.070
0.73
mg/kg
J6J3
6010B
04/22/14
1
Lead
1.8
0.095
0.37
mg/kg
J6J3
6010B
04/22/14
1
Selenium
1.0
0.37
1.5
mg/kg
JP1J6J3
6010B
04/22/14
1
Silver
0.50
0.14
0.73
mg/kg
JJ6J3
6010B
.04/22/14
1
Results listed are dry weight basis.
U = ND (Not Detected)
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = ReportedDetection Limit = LOQ = PQL = EQL ='TRRP MQL
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 04/24/14 17:34 Printed: 04/24/14 17:35
L693672-03.(PH) - [e-mail]
Page 5 of 20

REPORT OF ANALYSIS
Rob Willcox
SSME Inc. - Greensboro NC
3718 Old Battleground Road
Greensboro, NC 27410
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814209
Est. 1970
April 24, 2014
ESC Sample #
L693672-04
Date Received
April 15, 2014'
Description
Fortify-Sunnybrook
Bridge / Crabtree Bridge
Site ID
RALEIGH, NC
Sample ID
CRABTREE DEWATERING BOX
Project #
1588-10-027
Collected By
Rob Willcox
Collection Date :
04/14/i4 11:50
Parameter
Result Det. Limit Units
Method
Date Dil.
PH
12. su
9045D
04/18/14 1
Total Solids
85.4 0.100 %
2540 G-2011
04/16/14 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/24/14 17:34 Printed:, 04/24/14 17:35
L693672-04 (PH) - 12@21.1c
Page 6 of 20,

Attachment A
List of Analytes with QC Qualifiers
Sample
Work
Sample
Run
Number
Group
Type
Analyte
ID
Qualifier
L693672-01
WG716568
SAMP
2,4,5-TP (Silvex)
R2906008
J6
WG716555
SAMP
Mercury
R2905949
001J6J3
L693672-02
WG717129
SAMP
Arsenic
R2906969
J
WG717128
SAMP
Lead
R2907628
JP1
WG717128
SAMP
Silver
R2907628
JP1
L693672-03
WG717148
SAMP
Arsenic
R2907510
J6J3
NG717148
SAMP
Barium
R2907510
J6J3
WG71714B
SAMP
Cadmium
R2907510
J6J3
WG717148
SAMP
Chromium
R2907510
J6J3
WG717148
SAMP
Lead
R2907510
J6J3
WG71714B
SAMP
Selenium
R2907510
JP1J6J3
WG717148
SAMP
Silver
R2907510
JJ6J3
Page 7 of 20

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J (EPA) - Estimated value below the lowest calibration point. Confidence
correlates with concentration.
J3 The associated batch QC was outside the established quality control range
for precision.
J6 The sample matrix interfered with the ability to make any accurate
determination; spike value is low
O (ESC) Sample diluted due to matrix interferences that impaired the ability
to make an accurate analytical determination. The detection limit is
elevated in order to reflect the necessary dilution.
01 (ESC) The analyte failed the method required serial dilution test and/or
subsequent post -spike criteria. These failures indicate matrix
interference.
P1 RPD value not applicable for sample concentrations less than 5 times the
reporting limit.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 8 of 20

Summary of Remarks For Samples Printed
04/24/14 at 17:35:10
TSR Signing Reports: 350
R5 - Desired TAT
MDL/RDL
Sample: L693672-01 Account: SMEGBNC Received: 04/15/14 07:00 Due Date: 64/22/14 00:00 RPT Date: 04/24/14 17:34
Sample: L693672-02 Account: SMEGBNC Received: 04/15/14 07:00 Due Date: 04/22/14 00:00 RPT Date: 04/24/14 17:34
Rotate for MRCRAB
Sample: L693672-03 Account: SMEGBNC Received:. 04/15/14 07:00 Due Date: 04/22/14 00:00 RPT Date: 04/24/14 17:34
Rotate for MRCRA8
Sample: L693672-04 Account: SMEGBNC Received: 04/15/14 07:00 Due Date: 04/22/14 00:00 RPT Date: 04/24/14 17:34
Rotate for MRCRAB

OESCL•A•B S•C•I•E•N•C•E•S
S&ME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road
Greensboro, NC 27410
Quality Assurance Report
Level II
L693672
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814299
Est. 1970
April 24, 2014
Laboratory Blank
Analyte
Result
Units
Rec Limit
Batch .
Date Analyzed
Total Solids
< .1
t
WG716139
04/16/14
08:50
Reactive Sulf.(SW846 7.3.4.1)
< 25
mg/kg
WG716217
04/16/14
13:15
Reactive CN (SW846 7.3.3.2)
< .125
mg/kg
WG716218
04/16/14
13:50
Mercury
< .02
mg/kg
WG716168
04/17/14
09:17
Mercury
< .001
mg/l
WG716555
04/18/14
13:03
2,4,5-TP (Silvex)
< .002
mg/1
WG716568
04/18/14
14:42
2,4-D
< .002
mg/l
WG716568
04/18/14
14:42
2,4-Dichlorophenyl Acetic Acid
Rec.
86.30 22.9-153
WG716568
04/18/14
14:42
Arsenic
< .45
mg/1
WG716695
04/18/14
18:32
Barium
< 1.35
mg/1
WG716695
04/18/14
18:32
Cadmium
< .45
mg/l
WG716695
04/18/14
18:32
Chromium
< .45
mg/l
WG716695
04/16/14
18:32
Lead
< .45
mg/1
WG716695
04/18/14
18:32
Selenium
< .45
mg/1
WG716695
04/18/14
18:32
Silver
< .45
mg/1
WG716695
04/18/14
18:32
1,1-Dichloroethene
< .05
mg/1
WG716895
04/19/14
19:31
1,2-Dichloroethane
< .05
mg/l
WG716895
04/19/14
19:31
2-Butanone (MEK)
< .5
mg/l
WG716895
04/19/14
19:31
Benzene
< .05
mg/1
WG716895
04/19/14
19:31
Carbon tetrachloride
< .05
mg/1
WG716895
04/19/14
19:31
Chlorobenzene
< .05
mg/l
WG716895
04/19/14
19:31
Chloroform
< .25
mg/1
WG716895
04/19/14
19:31
Tetrachloroethene
< .05
mg/l
WG716895
04/19/14
19:31
Trichloroethene
< .05
mg/1
WG716895
04/19/14
19:31
Vinyl chloride
< .05
mg/1
WG716895
04/19/14
19:31
4-Bromofluorobenzene
% Rec.
102.0 71-126
WG716895
04/19/14
19:31
Dibromofluoromethane
€ Rec.
96.30 78.3-121
WG716895
04/19/14
19:31
Toluene-d8
% Rec.
98.10 88.5-111
WG716895
04/19/14
19:31
a,a,a-Trifluorotoluene
% Rec.
101.0 85-114
WG716895
04/19/14
19:31
Arsenic
< .001
mg/1
WG717129
04/21/14
22:43
Mercury
< .0002
mg/1
WG717021
04/22/14
08:32
Chlordane
< .005
mg/l
WG716622
04/19/14
13:02
Endrin
< .005
mg/l
WG716622
04/19/14
13:02
Lindane
< .005
mg/1
WG716622
04/19/14
13:02
Heptachlor
< .065
mg/1
WG716622
04/19/14
13:02
Methoxychlor
< .005
mg/l
WG716622
04/19/14
13:02
Toxaphene
< .01
mg/l
WG716622
04/19/14
13:02
Decachlorobiphenyl
& Rec.
123.0 10-156
WG716622
04/19/14
13:02
Tetrachloro-m-xylene
% Rec.
92.60 13.9-137
VIG716622
04/19/14
13:02
Performance of this Analyte
is outside of
established criteria.
For additional information,
please see Attachment A 'List
of Analytes with QC Qualifiers.'
Page 9 of 20

JOESC
L•A•B 5•C•1•E•N•C•E•S
SSME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road
Greensboro, NC 27410
Quality Assurance Report
Level II
L693672
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 24, 2014
Laboratory Blank
Analyte
Result -
Units % Rec
Limit
Batch
Date Analyzed
1,4-Dichlorobenzene
< .1
mg/l
WG716619
04/21/14 16:21
2,4,5-Trichlorophenol
< .1
mg/1
WG716619
04/21/14 16:21
2,4,6-Trichlorophenol
< .1
mg/l
WG716619
04/21/14 16:21
2,4-Dinitrotoluene
< .1
mg/l
WG716610
04/21/14 16:21
2-Methylphenol
< .1
mg/1
VIG716619
04/21/14 16:21
364-Methyl Phenol
< .1
mg/1
WG716619
64/21/14 16:21
Hexachloro-1,3-butadiene
< .1
mg/1
WG716619
04/21/14 16:21
Hexachlorobenzene
< .1
mg/l
WG716619
04/21/14 16:21
Hexachloroethane
< .1
mg/1
WG716619
04/21/14 16:21
Nitrobenzene
< .1
mg/l
VIG716619
04/21/14 16:21
Pentachlorophenol
< .1
mg/l
WG716619
04/21/14 16:21
Pyridine
< .1
mg/l
WG716619
04/21/14 16:21
2,4,6-Tribromophenol
% Rec. 76.60
11.2-130
WG716619
04/21/14 16:21
2-Fluorobiphenyl
% Rec. 89.30
29.5-131
WG716619
04/21/14 16:21
2-Fluorophenol
% Rec. 45.60
10-77.9
WG716619
04/21/14 16:21
Nitrobenzene-d5
% Rec. 69.70
21.6-123
W6716619
04/21/14 16:21
Phenol-d5
% Rec. 29.50
5-70.1
WG716619
04/21/14 16:21
p-Terphenyl-dl4
% Rec. 72.70
29.3-137
WG716619
04/21/14 16:21
Arsenic
< 1
mg/kg
WG717148
04/22/14 23:58
Barium
< .25
mg/kg
WG717148
04/22/14 23:58
Cadmium
< .25
mg/kg
WG717148
04/22/14 23:58
Chromium
< .5
mg/kg
WG717148
04/22/14 23:58
Lead
< .25
mg/kg
WG717148
04/22/14 23:58
Selenium
< 1
mg/kg
WG717148
04/22/14 23:58
Silver
< .5
mg/kg
WG717148
04/22/14 23:58
Barium
< .005
mg/1
WG717128
04/23/14 09:23
Cadmium
< .005
mg/1
WG717128
04/23/14 09:23
Chromium
< .01
mg/1
WG717128
04/23/14 09:23
Lead
< .005
mg/l
WG717128
04/23/14 09:23
Selenium
< .02
mg/l
WG717128
04/23/14 09:23
Silver
< .01
mg/1
WG717128
04/23/14 09:23
Hexavalent Chromium
< 1
mg/kg
WG717009
04/24/14 09.34
Duplicate
Analyte
Units
Result Duplicate RPD
Limit
Ref Samp Batch
Total Solids
%
83.3
82.3 1.30
5
L693609-03 VIG716139
Reactive Sulf.(SW846 7.3.4.1)
mg/kg
0.0
0.0 0.0
20
L693565-02 WG716217
Reactive CN (SW84'6 7.3.3.2)
mg/kg
0.0
0.0 0.0
20
L693565-02 WG716218
Mercury
mg/kg
0.200
0.196 3.00
20
L693780-10 WG716168
ORP
my
10.0
10.0 0.0
20
L693447-01 WG716432
ORP
my
70.0
70.0 0.0
20
L693544-05 WG716432
Corrosivity
0.0
0.0 0.0
10
L693224-01 WG716476
+ Performance of this Analyte
is outside of
established criteria.
For additional information,
please see Attachment A 'List of Analytes with
QC Qualifiers.'
Page 10 of 20

12065 Lebanon Rd.
Mt. Juliet, TN 37122
OESC [phone]
1-800-767-5859
Fax [phone]
L•A•B S•C•1•E•N•C•E•S
Tax I.D. 62-0814289
Est. 1970
S&ME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road Quality Assurance Report
Level II
Greensboro, NC 27410 April 24, 2014
L693672
Duplicate
Analyte
Units
Result
Duplicate
RPD
Limit
Ref Samp
Batch
pH
su
6.80
6.70
0.743
1
L693013-01
WG716687
pH
su
7.90
7.90
0.253
1
L694091-01
WG716687
Mercury
mg/1
0.0
-0.000209
45.0*
20
L693672-01
WG716555
Arsenic
mg/1
0.0
-0.0201
1630*
20
L693672-01
WG716695
Barium
mg/1
0.0,
0.318
1.00
20
L693672-01
WG716695
Cadmium
mg/1
0.0
0.00617
17.0
20
L693672-01
WG716695
Chromium
mg/1
0.0
0.159
2.00
20
L693672-01
NG716695
Lead
mg/1
0.0
-0.0237
45.0*
20
L693672-01
WG716695
Selenium
mg/l
0.0
-0.0470
248.4
20
L693672-01
WG716695
Silver
mg/l
0.0.
0.0165
23.0*
20
L693672-01
WG716695
Ignitability
Deg. F
0.00
0.00
0.00
10
L693730-01
WG716780
Arsenic
mg/l
0.0
0.000320
20.0
20
L693672-02
WG717129
Mercury
mg/l
0.0
0.0000214
9.00
20
L693672-02
WG717021
Arsenic
mg/kg
3.40
2.97
14.0
20
L693672-03
WG717148
Barium
mg/kg
25.0
24.7
2.00
20
L693672-03
WG717148
Cadmium
mg/kg
0.0
-0.132
16.0
20
L693672-03
WG717148
Chromium
mg/kg
10.0
9.88
4.00
20
L693672-03
WG717148
Lead
mg/kg,
1.20
1.25
3.00
20
L693672-03
WG717148
Selenium
mg/kg
0.0
0.676
108.*
20
L693672-03
WG717148
Silver
mg/kg,
0.0
0.33B
.7.00
20
L693672-03
WG717148
'Barium
mg/l
0.0920
0.0940
2.00
20
L693672-02
WG717128
Cadmium
mg/1
0:0
-0.0000285
1-78.*
20
L693672-02
WG717128
Chromium
mg/1
0.0190
0.0198
6.00
26
L693672-62
WG717i26
Lead
mg/1
0.0
0.00401
39.0*
20
L693672-02
WG717128
Selenium
mg/l
0.0 .0.00315
73.0*
20
L693672-02
WG717128
Silver
mg/1
0.0
0.00821
71.0*
20
L693672-02
WG717128
Hexavalent Chromium
mg/kg
4.50
4.50
0.443
20
L693672-03
WG717009
Laboratory
Control Sample
Analyte
Units
Known Val
Result
8 Rec
Limit
Batch
Total Solids
50
50.0
-100.
85-115
NG716139
Reactive Sulf.(SW846 7.3.4.1)
mg/,kg
100
85.0
85.0
70-130
WG716217
Reactive CN (SW846 7.3.3.2)
mg/kg
.1
D.105
105.
50=150
WG716218
Mercury
mg/kg
12.4
1.1.4
92.0
71.6-128
WG716168
* Performance of this Analyte
is outside of
established
criteria.
For additional information,
please see Attachment A 'List of Analytes with
QC Qualifiers.'
Page 11 of 20

S&ME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road
Greensboro, NC 27410
Quality Assurance Report
Level II
L693672
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 24, 2014
Laboratory
Control Sample
Analyte
Units
Known Val
Result
% Rec
Limit
Batch
ORP
mV
100
100.
100.
90-110
WG716432
Corrosivity
5.93
5.90
99.5
98.3-101.7
WG716476
PH
su
5.93
5.90
99.5
98.3-101.7
WG716687
Mercury
mg/l
.003
0.00309
103.
85-115
WG716555
Arsenic
mg/l
9
9.61
107.
80-120
WG716695
Barium
mg/1
9
9.94
110.
80-120
WG716695
Cadmium
mg/l
9
9.95
ill.
80-120
WG716695
Chromium
mg/1
9
9.92
110.
80-120
WG716695
Lead
mg/l
9
10.2
113.
80-120
WG716695
Selenium
mg/1
9
10.1
112.
80-120
WG716695
Silver
mg/l
9
9.65
107.
80-120
WG716695
2,4,5-TP (Silvex)
mg/l
.005
0.00360
72.1
57.6-129
WG716569
2,4-D
mg/l
.005
0.00324
64.9
43.9-115
WG716568
2,4-Dichlorophenyl Acetic Acid
74.20
22.9-153
WG716568
Ignitability
Deg. F 82
92.0
100.
93-107
WG71678O
1,1-Dichloroethene
mg/l
.025
0.0247
99.0
67.8-129
WG716895
1,2-Dichloroethane
mg/l
.025
0.0213
85.1
68.8-124
WG716895
2-Butanone (MEK)
mg/l
.125
0.127
101.
55-149
WG716895
Benzene
mg/1
.025
0.0238
95.4
74.8-121
WG716895
Carbon tetrachloride
mgll
.025
0.0245
98.0
70.2-123
WG716895
Chlorobenzene
mg/1
.025
0.0249
99.5
78.1-119
WG716895
Chloroform
mg/l
.025
0.0239
95.5
76-121
WG716895
Tetrachloroethene
mg/l
.025
0.0258
103.
72.6-126
WG716895
Trichloroethene
mg/1
.025
0.0237
94.7
77.7-118
WG716895
Vinyl chloride
mg/1
.025
0.0244
97.8
65.9-128
WG716895
4-Bromofluorobenzene
99.70
71-126
WG716895
Dibromofluoromethane
95.70
78.3-121
WG716095
Toluene-d8
90.30
08.5-111
WG716895
a,a,a-Trifluorotoluene
100.0
85-114
WG716895
Arsenic
mg/l
.05
0.0559
112.
85-115
WG717129
Mercury
mg/l
.003
0.00296
99.0
85-115
WG717O21
Endrin
mg/l
.0002
0.000167
83.5
50.1-131
WG716622
Lindane
mg/l
.0002
0.000169
84.5
54.7-125
VIG716622
Heptachlor
mg/1
.0002
0.000167
83.4
26.7-127
WG716622
Methoxychlor
mg/l
.0002
0.000147
73.6
48.2-144
WG716622
Decachlorobiphenyl
61.70
10-156
WG716622
Tetrachloro-m-xylene
63.90
13.9-137
41G716622
• Performance of this Analyte
is outside
of established
criteria.
.For additional information,
please see
Attachment A IList
of Analytes with
QC Qualifiers.'
Page 12 of 20

JOESC
L•A•B S•C•1•E•N•C•E•S
S&ME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road
Greensboro, NC 27410
Quality Assurance Report
Level II
L693672
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 24, 2014
Laboratory Control Sample
Analyte
Units
Known
Val
Result
% Rec
Limit
Batch
1,4-Dichlorobenzene
mg/1
.025
0.0190
76.0
21-89.4
WG716619
2,4,5-Trichlorophenol
mg/l
.025
0.0235
93.9
34.9-112
WG716619
2,4,6-Trichlorophenol
mg/1
.025
0.0239
95.5
29.8-107
WG716619
204-Dinitrotoluene
mg/1
.025
0.0224
89.6
31.2-105
WG716619
2-Methylphenol
mg/1
.025
0.0152
60.7
26.4-86.9
WG716619
3&4-Methyl Phenol
mg/l
.025
0.0160
64.1
27.9-92
WG716619
Hexachloro-1,3-butadiene
mg/l
.025
0.0236
94.3
16.1-104
WG716619
Hexachlorobenzene
mg/l
.025
0.0259
104.
38.5-116
WG716619
Hexachloroethane
mg/1
.025
0.0187
74.7
16.5-89.8
WG716619
Nitrobenzene
mg/1
.025
0.0231
92.3
31.4-106
WG716619
Pentachlorophenol
mg/1
.025
0.0172
66.7
10-97.4
WG716619
Pyridine
mg/1
.025
0.00950
38.0
13.5-58.9
WG716619
2,4,6-Tribromophenol
83.50
11.2-130
WG716619
2-Fluorobiphenyl
89.90
29.5-131
WG716619
2-Fluorophenol
43.10
10-77.9
WG716619
Nitrobenzene-d5
75.70
21.8-123
WG716619
Phenol-d5
29.50
5-70.1
WG716619
p-Terphenyl-dl4
83.20
29.3-137
WG716619
Arsenic
mg/kg
237
236.
99.0
83.1-117
WG717148
Barium
mg/kg
252
264.
105.
94.1-116
WG717148
Cadmium
mg/kg
191
200.
105.
83.2-117
WG717148
Chromium
mg/kg
128
140.
109.
81.3-118
WG717148
Lead
mg/kg
103
98.4
96.0
83.1-117
WG717148
Selenium
mg/kg
110
112.
101.
78.7-122
WG717148
Silver
mg/kg
47.3
48.8
103.
66.2-134
WG717148
Barium
mg/1
1
1.00
100.
80-120
WG717128
Cadmium
mg/l
1
0.964
96.0
80-120
WG717128
Chromium
mg/1
1
1.01
101.
80-120
WG717128
Lead
mg/l
1
0.991
99.0
80-120
WG717128
Selenium
mg/1
1
0.973
97.0
80-120
WG717128
Silver
mg/l
1
0.987
99.0
80-120
W6717120
Hexavalent Chromium
mg/kg
125
120.
96.0
90-110
WG717009
Laboratory
Control Sample Duplicate
Analyte
Units
Result
Ref
%Rec
Limit
RPD
Limit
Batch
Reactive Sulf.(SW846 7.3.4.1)
mg/kg
90.0
85.0
90.0
70-130
5.71
20
WG716217
Reactive CN (SW846 7.3.3.2)
mg/kg
0.105
0.105
105.
50-150
0.0
20
WG716218
ORE
mV
100.
100.
100.
90-110
0.0
20
WG716432
Corrosivity
5.90
5.90
99.0
98.3-101.7
0.0
10
WG719476
pH
su
5.90
5.90
99.0
99.3-101.7
0.0
20
WG716687
2,4,5-TP (Silvex)
mg/l
0.00298
0.00360
60.0
57.6-129
19.1
20.7
WG716568
2,4-D
mg/1
0.00284
0.00324
57.0
43.9-115
13.3
28
WG716568
* Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment
A 'List of
Analytes with
QC Qualifiers.'
Page 13 of 20

12065 Lebanon Rd.
Mt. Juliet, TN 37122
OESC [phone]
1-800-767-5859
Fax [phone]
L-A-® 9-C-I•E-N-C-E-5
Tax I.D. 62-0814269
•
Est. 1970
SSME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road Quality Assurance Report
Level II
Greensboro, NC 27410 April 24, 2014
L693672
Laboratory
Control Sample Duplicate
Analyte
Units
Result
Ref
%Rec
Limit
RPD
Limit
Batch
2,4-Dichlorophenyl Acetic Acid
60.80
22.9-153
Ignitability
Deg.
F 82.0
82.0
100.
93-107
0.00
20
VIG716780
1,1-Dichloroethene
mg/l
0.0249
0.0247
99.0
67.8-129
0.450
20
VIG716895
1,2-Dichloroethane
mg/l
0.0211
0.0213
.84.0
68.8-124
0.640
20
WG716895
2-Butanone (MEK)
mg/l
0.109
6.127
87.0
55-149
14.9
20
WG716895
Benzene
mg/l
0.0238
0.0238
95.0
74.8-121
0.110
20
WG716895
Carbon tetrachloride
mg/1
0.0244
0.0245
98.0
70.2-123
0.400
20
WG716895
Chlorobenzene
m4/1
0.0254
0.0249
102.
78.1-119
2.19
20
WG716895
Chloroform
mg/1
0.0235
0.0239
94.0
76-121
1.66
20
WG716895
Tetrachloroethene
mg/l
0.0250
0.0258
100.
72.6-126
3.20
20
WG716895
Trichloroethene
mg/l
0.0238
0.0237
95.0
77.7-118
0.590
20
WG716895
Vinyl chloride
mg/l
0.0242
0.0244
97.0
65.9-128
0.910
20
WG716895
4-Bromofluorobenzene
101.0
71-126
VIG716895
Dibromofluoromethane
95.30
78.3-121
WG716895
Toluene-d8
98.40
88.5-111
WG716895
a,a,a-Trifluorotoluene
99.40
85-114
WG716895
Arsenic
mg/l
0.0558
0.0559
112.
85-115
0.0
20
WG717129
Endrin
mg/l
0.000165
0.000167
82.0
50.1-131
1.42
29.1
WG716622
Lindane
mg/l
0.000173
0.000169
86.0
54.7-125
2.37
21.1
WG716622
Heptachlor
mg/1
0.000166
0.000167
83.0
20.7-127
0.510
30.5
WG716622
Methoxychlor
mg/l
0.000142
0.000147
71.0
48.2-144
3.61
27.8
WG716622
Decachlorobiphenyl
61.00
10-156
WG716622
Tetrachloro-m-xylene
63.90
13.9-137
WG716622
1,4-Dichlorobenzene
mg/l
0.0196
0.0190
78.0
21-89.4
3.33
32.6
WG716619
2,4,5-Trichlorophenol
mg/l
0.0244
0.0235
98.0
34.9-112
3.98
23.9
WG716619
2,4,6-Trichlorophenol
mg/l
0.0242
0.0239
97.0
29.8-107
1.31
24.1
WG716619
2,4-Dinitrotoluene
mg/1
0.0245
0.0224
98.6
31.2-105
9.03
22
WG716619
2-Methylphenol
mg/l
0.0152
0.0152
61.0
26.4-86.9
0.470
26.5
WG716619
364-Methyl Phenol
mg/1
0.0155
0.0160
62.0
27.9-92
3.45
27
WG716619
Hexachloro-1,3-butadiene
mg/1
0.0244
0.0236
96.0
16.1-104
3.65
31.2
WG716619
Hexachlorobenzene
mg/l
0.0271
0.0259
108.
38.5-116
4.27
20.1
WG716619
Hexachloroethane
mg/1
0.0202
0.0187
81.0
16.5-89.8
7.79
30.7
WG716619
Nitrobenzene
mg/l
0.0231
0.0231
92.0
31.4-106
0.0500
25.7
WG716619
Pentachlorophenol
mg/l
0.0170
0.0172
69.0
10-97.4
0.910
35.1
WG716619
Pyridine
mg/l
0.00997
0.00950
40.0
13.5-58.9
4.89
32.5
WG716619
2,4,6-Tribromophenol
88.50
11.2-130
WG716619
2-Fluorobiphenyl
94.30
29.5-131
WG716619
2-Fluorophenol
44.00
10-77.9
WG716619
Nitrobenzene-d5
74.60
21.8-123
WG716619
Phenol-d5
28.20
5-70.1
WG716619
p-Terphenyl-dl4
78.00
29.3-137
WG716619
Barium
mg/1
1.01
1.00
101.
80-120
1.00
20
lIG717128
Cadmium
mg/1
0.966
0.964
97.0
80-120
0.0
20
WG717128
Chromium
mg/l
1.01
1.01
101.
80-120
1.00
20
WG717128
Lead
mg/1
0.995
0.991
99.0
80-120
0.0
20
WG717128
Selenium
mg/1
0.973
0.973
97.0
80-120
0.0
20
WG717128
Silver
mg/1
0.988
0.987
99.0
80-120
0.0
20
WG717128
• Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment
A 'List of
Analytes with
QC Qualifiers.'
Page 14 of 20

12065 Lebanon Rd.
Mt. Juliet, TN 37122
OESC (6151 758-5858
1-800-767-5859
Fax [phone]
L•A•® S-C•I-E•N•C•E•S
Tax I.D. 62-0814289
o •
' Est. 1970
SSME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road Quality Assurance Report
Level II
Greensboro, NC 27410 April 24, 2014
L693672
Laboratory
Control Sample Duplicate
Analyte
Units
Result
Ref
%Rec
Limit RPD
Limit
Batch
Hexavalent Chromium
mg/kg
120.
120.
96.0
90-110 0.0
20
WG717009
Matrix Spike
Analyte
Units
MS Res
Ref Res
TV
% Rec
Limit
Ref Samp
Batch
Mercury
mg/kg
0.672
0.196
.5
95.0
80-120
L693780-10
VIG716168
Mercury
mg/l
0.000982-0.000209
.0003
33.0*
80-120
L693672-01
WG716555
Arsenic
mg/l
9.82
-0.0201
9
110.
75-125
L693672-01
WG716695
Barium
mg/l
10.2
0.318
9
110.
75-125
L693672-01
WG716695
Cadmium
mg/l
9.88
0.00617
9
110.
75-125
L693672-01
VIG716695
Chromium
mg/l
9.89
0.159
9
110.
75-125
L693672-01
WG716695
Lead
mg/l
9.95
-0.0237
9
110.
75-125
L693672-01
WG716695
Selenium
mg/l
10.5
-0.0470
9
120.
75-125
L693672-01
WG716695
Silver
mg/l
10.0
0.0165
9
110.
75-125
L693672-01
WG716695
2,4,5-TP (Silvex)
mg/l
0.0284
0.0
.05
57.0*
57.6-129
L693672-01
WG716568
2,4-D
mg/l
0.0283
0.0
.05
56.0
43.9-115
L693672-01
WG716568
2,4-Dichlorophenyl Acetic Acid
66.00
22.9-153
WG716568
1,1-Dichloroethene
mg/l
1.23
0.0
1.25
99.0
51.1-140
L693972-01
WG716895
1,2-Dichloroethane
mg/l
1.09
0.0
1.25
87.0
60-126
L693972-01
WG716895
2-Butanone (MEK)
mg/l
6.23
0.0
6.25
100.
22.4-138
L693972-01
WG716895
Benzene
mg/l
1.21
0.0
1.25
97.0
54.3-133
L693972-01
WG716895
Carbon tetrachloride
mg/l
1.22
0.0
1.25
97.0
55.7-134
L693972-01
WG716895
Chlorobenzene
mg/1
1.25
0.0
1.25,
100.
67-125
L693972-01
WG716895
Chloroform
mg/l
1.19
0.0
1.25
96.0
63-129
L693972-01
WG716895
Tetrachloroethene
mg/1
1.26
0.0
1.25
100.
53-139
L693972-01
WG716895
Trichloroethene
mg/1
1.19
0.0
1.25
95.0
44.1-149
L693972-01
WG716895
Vinyl chloride
mg/l
1.22
0.0
1.25
97.0
47.8-137
L693972-01
WG716895
4-Bromofluorobenzene
101.0
71-126
WG716895
Dibromofluoromethane
96.50
78.3-121
WG716895
Toluene-d8
97.80
88.5-111
WG716895
a,a,a-Trifluorotoluene
100.0
85-114
WG716895
1,1-Dichloroethene
mg/l
1.18
0.0
1.25
95.0
51.1-140
L694060-01
WG716895
1,2-Dichloroethane
mg/l
1.01
0.0
1.25
81.0
60-126
L694060-01
WG716895
2-Butanone (MEK)
mg/l
5.02
0.0535
6.25
79.6
22.4-138
L694060-01
WG716895
Benzene
mg/1
1.15
0.0
1.25
92.0
54.3-133
L694060-01
WG716895
Carbon tetrachloride
mg/l
1.17
0.0
1.25
93.0
55.7-134
L694060-01
TIG716895
Chlorobenzene
.mg/l
1.21
0.0
1.25
97.0
67-125
L694060-01
WG716895
Chloroform
mg/l
1.14
0.0
1.25
91.0
63-129
L694060-01
WG716895
Tetrachloroethene
mg/l
1.23
0.0
1.25
98.0
53-139
L694060-01
lIG716895
Trichloroethene
mg/l
1.15
0.0
1.25
92.0
44.1-149
L694060-01
WG716895
Vinyl chloride
mg/l
1.17
0.0
1.25
93.0
47.8-137
L694060-01
W6716895
4-Bromofluorobenzene
101.0
71-126
WG716895
Dibromofluoromethane
94.10
78.3-121
WG716895
Toluene-d8
97.60
88.5-111
lIG716895
a,a,a-Trifluorotoluene
100.0
85-114
WG716895
Mercury
mg/l
0.00285
0.0000214
.003
94.0
80-120
L693672-02
lIG717021
Endrin
mg/l
0.00182
0.0
.002
91.0
50.1-131
L693672-01
WG716622
* Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment
A 'List of Analytes
with QC
Qualifiers.'
Page 15 of 20

12065 Lebanon Rd.
Mt. Juliet, TN 37122
OESC [phone]
1-800-767-5859
Fax [phone]
L•A•B S•C•('E•N•C•E•S
Tax I.D. 62-0814289
Est. 1970
S&ME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road Quality Assurance Report
Level II
Greensboro, NC 27410 'April 24, 2014
L693672
Matrix
Spike
Analyte
Units
MS Res
Ref Res TV
Rec
Limit
Ref Samp
Batch
Lindane
mg/l
0.00106 0.0
.002
93.0
54.7-125
L693672-01
WG716622
Heptachlor
mg/l
0.00182 0.0
.002
91.0
20.7-127
L693672-01
WG716622
Methoxychlor
mg/1
0.00172 0.0
.002
86.0
48.2-144
L693672-01
41G716622
Decachlorobiphenyl
83.60
10-156
WG716622
Tetrachloro-m-xylene
78.70
13.9-137
WG716622
1,4-Dichlorobenzene
mg/l
0.170
0.0
.25
68.0
14-104
L693672-01
WG716619
2,4,5-Trichlorophenol
mg/l
0.243
0.0
.25
97.0
30.6-120
L693672-01
WG716619
2,4,6-Trichlorophenol
mg/1
0.241
0.0
.25
97.0
19.1-114
L693672-01
VIG716619
2,4-Dinitrotoluene
mg/l
0.214
0.0
.25
86.0
16.2-135
L693672-01
WG716619
2-Methylphenol
mg/l
0.141
0.0
.25
56.0
10-133
L693672-01
WG716619
3&4-Methyl Phenol
mg/l
0.156
0.0
.25
62.0
17.4-100
L693672-01
WG716619
Hexachloro-1,3-butadiene
mg/l
0.209
0.0
.25
84.0
15.7-109
L693672-01
WG716619
Hexachlorobenzene
mg/l
0.238
0.0
.25
95.0
31.9-135
L693672-01
WG716619
Hexachloroethane
mg/l
0.176
0.0
.25
70.0
10.4-105
L693672-01
41G716619
Nitrobenzene
mg/l
0.210
0.0
.25
84.0
23.1-121
L693672-01
WG716619
Pentachlorophenol
mg/l
0.162
0.0
.25
65.0
10-108
L693672-01
WG716619
Pyridine
mg/l
0.0838
0.0
.25
34.0
10-77.8
L693672-01
WG716619
2,4,6'Tribromophenol
83.80
11.2-130
WG716619
2-FLuorobiphenyl
82.50
29.5-131
WG716619
2-Fluorophenol
39.90
10-77.9
WG716619
Nitrobenzene-d5
66.50
21.8=123
WG716619
Phenol-d5
26.10
5-70.1
WG716619
p-Terphenyl-d14
69.10
29.3-137
WG716619
Arsenic
mg/kg
10.2
2.97
50
15.0*
75-125
L693672-03
41G717148
Barium
mg/kg
16.3
24.7
50
0.0*
75-125
L693672-03
WG717148
Cadmium
mg/kg
7.70
-0.132 50
15.0*
75-125
L693672-03
WG717148
Chromium
mg/kg
21.1
9.88
50
22.0*
75-125
L693672-03
WG7L7148
Lead
mg/kg
7.88
1.25
50
13.0*
75-125
L693672-03
WG717148
Selenium
mg/kg
9.53
0.676
50
18.0*
75=125
L693672-03
WG717148
Silver
mg/kg
15.8
0.338
50
31.0*
75-125
L693672-03
WG717148
Hexavalent Chromium
mg/kg
24.0
4.50
20
98.0
75-125
L693672-03
WG717009
Matrix Spike
Duplicate
Analyte
Units
MSD
Ref
%Rec
Limit
RPD Limit
Ref Samp
Batch
Mercury
mg/kg
0.728
0.672
106.
80-120
8.00 20
L693780-10
WG716168
Mercury
mg/l
0.000474
0.000982
22.7*
80-120
70:0* 20
L693672-01
WG716555
Arsenic
mg/1
9.69
9.82
108.
75-125
1.00 20
L69.3672-01
WG716695
Barium
mg/1
9.92
10.2
107.
75-125
3.00 20
L693672-01
WG716695
Cadmium
mg/l
9.56
9.00
106.
75-125
3.00 20
L693672-01
W6716695
Chromium
mg/1
9.68
9.89
106.
75-125
2.00 20
L693672-01
WG716695
Lead
mg/l
9.72
9.95
108.
75-125
2.00 20
L693672-01
WG716695
Selenium
mg/1
10.2
10.5
114.
75-125
3.00 20
L693672-01
WG716695
Silver
mg/l
9.74
10.0
108.
75-125
3.06 20
L693672-01
WG716695
2,4,5-TP (Silver.)
mg/l
0.0295
0.0284
59.0
57.6-129
3-80 20.7
L693672-01
WG716568
2,4-D
mg/l
0.0305
0.0283
61.0
43.9-115
7.64 28
L693672-01
WG716568
214-Dichlorophenyl Acetic Acid
63.90
22.9-153
WG716568
* Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment A 'List
of Analytes
with QC Qualifiers.'
Page 16 of 20

12065 Lebanon Rd.
Mt. Juliet, TN 37122
10ESC [phone]
1-800-767-5859
Fax [phone]
L'A•B S•C•I•E•N•C•E•S
Tax I.D. 62-0814289
row
Est. 1970 .
S&ME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road Quality Assurance Report
Level II
Greensboro, NC 27410 April 24, 2014
L693672
Analyte
Units
Matrix Spike
MSD Ref
Duplicate
%Rec
Limit
RPD
Limit
Ref Samp
Batch
1,1-Dichloroethene
mg/1
1.14
1.23
91.5
51.1-140
7.54
20.2
L693972-01
WG716895
1,2-Dichloroethane
mg/l
1.00
1.09
80.3
60-126
8.03
20
L693972-01
WG716895
2-Butanone (MEK)
mg/l
5.61
6.23
89.8
22.4-138
10.5
27
L693972-01
WG716895
Benzene
mg/l
1.13
1.21
90.1
54.3-133
7.01
20
L693972-01
WG716895
Carbon tetrachloride
mg/l
1.14
1.22
91.2
55.7-134
6.65
20
L693972-01
WG716895
Chlorobenzene
mg/l
1.19
1.25
95.3
67-125
5.00
20.3
L693972-01
WG716895
Chloroform
mg/l
1.12
1.19
89.7
63-129
6.24
20
L693972-01
WG716895
Tetrachloroethene
mg/1
1.21
1.26
97.0
53-139
3.93
20
L693972-01
WG716895
Trichloroethene
mg/l
1.12
1.19
90.0
44.1-149
5.42
20
L693972-01
WG716895
Vinyl chloride
mg/l
1.15
1.22
92.1
47.8-137
5.46
20
L693972-01
WG716895
4-Bromofluorobenzene
99.20
71-126
WG716895
Dibromofluoromethane
94.60
78.3-121
WG716895
Toluene-d0
97.20
88.5-111
WG716895
a,a,a-Trifluorotoluene
102.0
85-114
WG716895
1,1-Dichloroethene
mg/l
1.13
1.18
90.3
51.1-140
4.65
20.2
L694060-01
WG716895
1,2-Dichloroethane
mg/l
0.951
1.01
76.1
60-126
5.85
20
L694060-01
WG716895
2-Butanone (MEK)
mg/l
4.95
5.02
78.4
22.4-138
1.31
27
L694060-01
WG716895
Benzene
mg/l
1.08
1.15
86.6
54.3-133
6.17
20
L694060-01
VIG716895
Carbon tetrachloride
mg/l
1.09
1.17
87.2
55.7-134
6.86
20
L694060-01
WG716895
Chlorobenzene
mg/l
1.17
1.21
93.4
67-125
3.75
20.3
L694060-01
WG716895
Chloroform
mg/l
1.08
1.14
86.1
63-129
5.50
20
L694060-01
WG716895
Tetrachloroethene
mg/1
1.17
1.23
93.4
53-139
5.04'
20
L694060-01
WG716895
Trichloroethene
mg/l
1.09
1.15
87.6
44.1-149
4.94
20
L694060-01
WG716895
Vinyl chloride
mg/l
1.11
1.17
89.1
47.8-137
4.49
20
L694060-01
WG716895
4-Bromofluorobenzene
102.0
71-126
WG716895
Dibromofluoromethane
96.90
78.3-121
WG716895
Toluene -dB
98.10
88.5-111
WG716895
a,a,a-Trifluorotoluene
102.0
85-114
WG716895
Mercury
mg/l
0.00265
0.00285
67.5
80-120
7.00
20
L693672-02
WG717021
Endrin
mg/1
0.00186
0.00182
92.9
50.1-131
2.15
29.1
L693672-01
WG716622
Lindane
mg/l
0.00192
0.00186
96.2
54.7-125
3.41
21.1
L693672-01
WG716622
Heptachlor
mg/1
0.00184
0.06182
92.1
20.7-127
1.43
30.5
L693672-01
WG716622
Methoxychlor
mg/l
0.00176
0.00172
88.2
48.2-144
2.27
27.8
L693672-01
WG716622
Decachlorobiphenyl
84.70
10-156
WG716622
Tetrachloro-m-xylene
75.40
13.9-137
WG716622
1,4-Dichlorobenzene
mg/1
0.187
0.170
74.7
14-104
9.50
36.4
L693672-01
WG716619
2,4,5-Tzichlorophenol
mg/1
0.248
0.243
99.4
30.6-120
2.31
33.8
L693672-01
VIG716619
2,4,6-Trichlorophenol
mg/l
0.255
0.241
102.
19.1-114
5.26
29.9
L693672-01
WG716619
2,4-Dinitrotoluene
mg/l
0.231
0.214
92.4
16.2-135
7.61
20.6
L693672-01
WG716619
2-Methylphenol
mg/1
0.155
0.141
62.1
10-133
9.57
40
L693672-01
WG716619
364-Methyl Phenol
mg/l
0.171
0.156
68.4
17.4-100
9.16
27.7
L693672-01
WG716619
Hexachloro-1,3-butadiene
mg/l
0.221
0.209
88.5
15.7-109
5.70
37.6
L693672-01
WG716619
Rexachlorobenzene
mg/l
0.242
0.238
96.7
31.9-135
1.54
20
L693672-01
WG716619
Hexachloroethane
mg/l
0.191
0.176
76.4
10.4-105
8.29
40
L693672-01
WG716619
Nitrobenzene
mg/l
0.221
0.210
88.5
23.1-121
5.10
29
L693672-01
WG7-16619
Pentachlorophenol
mg%l
0.152
0.162
60.8
10-108
6.43
40
L693672-01
WG716619
Pyridine
mg/l
0.0921
0.0938
36.8
10-77.6
9.45
38.8
L693672-01
WG716619
2,4,6-Tribromophenol
80.60
11.2-130
WG716619
2-Fluorob'iphenyl
84.20
29.5-131
WG716619
2-Fluorophenol
48.30
10-77.9
WG716619
Nitrobenzene-d5
72.30
21.8-123
WG716619
Phenol-d5
27.90
5-70.1
WG716619
p-Terphenyl-dl4
73.00
29.3-137
WG716619
* Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment
A 'List
of Analytes
with QC Qualifiers.'
Page 17 of 20

OESC
I
S&ME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road
Greensboro, NC 27410
Quality Assurance Report
Level II
L693672
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 75B-5858
1-800-767-5859
Fax [phone]
Tax Z.D. 62-0814289
Est. 1970
April 24, 2014
Matrix. Spike Duplicate
Analyte
Units
MSD
Ref
BRec
Limit
RPD
Limit
Ref Samp
Batch
Arsenic
mg/kg
53.2
10.2
100.
75-125
136.*
20
L693672-03
WG717148
Barium
mg/kg
72.1
16.3
94.9
75-125
126.*
20
L693672-03
WG717148
Cadmium
mg/kg
46.5
7.70
93.2
75-125
143.*
20
L693672-03
WG717148
Chromium
mg/kg
58.2
21.1
96.6
75-125
94.0*
26
L693672-03
WG711148
Lead
mg/kg
47.5
7.88
92.6
75-125
143.*
20
L693672-03
WG717148
Selenium
mg/kg
51.8
9.53
102.
75-125
138.*
20
L693672-03
WG717148
Silver
mg/kg
50.9
15.8
101.
75-125
105.*
20
L693672-03
WG717148
Post
Spike
Serial Dilution
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 18 of 20

JOESC
L•A•B 5•C•I•E•N•C•E•S
SBME Inc. - Greensboro NC
Rob Willcox
3718 Old Battleground Road
Greensboro, NC 27410
Quality Assurance Report
Level II
L693672
Serial Dilution
Batch number /Run number / Sample number cross reference
NG716139: R2904984: L693672-03 04
WG716217: R2905140: L693672-01
WG716218: R2905371: L693672-01
WG716168: R2905464: L693672-03
WG716375: R2905507: L693672-01
WG716245: R2905570: L693672-03
WG716432: R2905604: L693672-03
WG716476: R2905622: L693672-01
WG716687: R2905913: L693672-03 04
WG716555: R2905949: L693672-01
WG716568: R2906008: L693672-01
DIG716695: R2906080: L693672-01
WG716626: R2906492: L693672-01
WG716898: R2906496: L693672-02
WG716780: R2906502: L693672-01
WG716895: R2906823 R2906886 R2908526: L693672-01
WG717129: R2906969: L693672-02
WG717021: R2907045: L693672-02
WG716622: R2907133:• L693672-01
WG716619: R2907188: L693672-01
WG717148: R2907510 R2908489: L693672-03
WG717128: R2907628: L693672-02
WG717009: R2909028: L693672-03
* * Calculations are performed prior to rounding of reported values.
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page. 19 of 20
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 24, 2014

OESC
I
S&ME Inc. - Greensboro NC
Rob Willcox
371E Old Battleground Road
Greensboro, NC 27410
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Quality Assurance Report
Level II
April 24, 2014
L693672
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The quality control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limits, every sample that is effected is flagged with the
appropriate qualifier in Appendix B of the analytic report.
Method Blank - an aliquot of reagent water carried through the
entire analytic process. The method blank results indicate if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytes above the reporting limit in the method blank are
qualified with the "B" qualifier.
Laboratory Control Sample - is a sample of known concentration
that is carried through the digestion/extraction and analysis
process. The percent recovery, expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control". If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J9" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate - is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has statistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a 11J5" or a "J6". The relative percent difference (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a "J3" qualifier.
Page 20 of 20

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1-40 Bridges — Sunnybrook and Crabtree Roads Report #14-106-0203 & 0204

Page: 1 of 1
Report Number: 14-106-0203 99.
A&L Eastem Laboratories, Inc.
Account Number: 45819
7621 Whittpine Rord Ruhmond, Yirginia ]DZJ7 (ee4)743A401 Par (e04)471bf16
Submitted By: ROB WILLCOX wwwAleastern.com
Send To: SBME (1588) Project: 1351-12-161A PHASE:09
MARTIN MABE GRANITE CONSTRUCTION
3718 OLD BATTLEGROUND RD
GREENSBORO , NC 27410-2314
REPORT OF ANALYSIS Date Sampled: 4/142014 11:50:00
Lab Number: 50004 Date Received: 04/16/2014 00:00
Sample Id : SUNNYBROOK Date Reported: 042212014
Total Solids63.64 636400 100.0 RD 04/16201415:00 SM-254OG
Moisture • 36.36 100.0 RD 04/162014 15:00 SM-254OG
pH (Standard Units)' 12.38 2.00 MW 04/17201409:24 SW-9045D
Comments:
NELAP ACCREDITED: VA NELAC LAB. # 460014. PA NELAC LAB # 68-03109. FL NELAC LAB # E871087, NJ NELAC LAB # VA011. RESULTS REPORTED
MEET ALL REQUIREMENTS OF THE CURRENT NELAC STANDARDS.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our /epon3 amf leffers are for Cho erGlumm aI01 Canflr/ett.af mt. Df ou Clients. ana may not be repraf/eCea m r.7io/e Of pan. flor nfar any rolerenCu bb mafl'
to the'-"Ie the felflltb.'V tffe confp:'ny el Fby aa%K fam' news fef me. or ofhe yfbllc announcements wdhouf obfaYunq Cut pnoi kW]ifen artlhonzaric-n.
Debbie Ho@

Page: 1 of 1
Report Number. 14-106-0204
Account Number: 45819
Submitted By: ROB WILLCOX
Send To: SBME (1588)
MARTIN MABE
3718 OLD BATTLEGROUND RD
GREENSBORO , NC 27410-2314
Lab Number: 50005
Sample Id: CRABTREE
Total Solids ' 63.99
Moisture ' 36.01
pH (Standard Units)12.38
Comments:
�YL A&L Eastem Laboratories, Inc.
7921Whit.pino Road Rih—.d.Vrgini,23237 (604(743-9401 Fa>,[phone]
wwwA]eastern.com
Project : 1351-12-161A PHASE:09
GRANITE CONSTRUCTION
REPORT OF ANALYSIS Date Sampled: 4/14/2014 00:00:00
Date Received: 04/16/2014 00:00
Date Reported: 0422/2014
639900 100.0 RD 04116/201415:00 SM-254OG
100.0 RD 04/16201415:00 SM-254OG
2.00 MW 04/172014 09:24 SW-9045D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Gtrrrapons arvt !e[tars am hr tha "dusl'o an, I arontrrWrn a! use of our cmrts. and may out be repraduced 11, Wrote rl pay na may ary retarancu be made
to the a;Yk. rile M"Us..v the cewy am, 41:myndeelhAkr9, oral reiunzeaulhanLanar.
Debbie Holt

ILM
111111llllllllllllllill� I�IIIIhIIIIIIIIIIIIIIRII1II0I �9�014'
0 16 201
Year Comomw Name _ 12:51 01
1351-12-161A PHASE 09
VIVITAL FORM/CHAIN OFCUSTODY Accounts
&L Eastern Laboratories5�
80-1-141-9401 hat: 804-27I-C-1 tG I nttlil:.uppnrtalrr>ulrastrm.rnm
ptomer Information
Charge To
Copy To
� B i'1J,'LCC v- SE (1,2C-FN5S 0je0
.S°M.E
d . 5
�2h'lc�rn S/JlliC. Co�'�
Project [1351-12- 161,4 10hw., d r? G, AAl17E 4 ' 5iRUcr?,6 Ao
Sample Information
Lab Number
Collection Information
Container Information
Please Check
Desired Tests
Sample ID
il-ab Use
Only)
Type
Date
Time
of Betttles
Type
Volume
SL1
SL2
NitrogenrespH
CCE
Ag
Cl
Volatile
Others
eta
Metals
Sanes
Solids
>Jq
_ Grab
*141
%rJ�D
_Glass
Plastic
c;,
— -)int
%U7AL-
�Q
Composite
�a 1
L D 5
A �l„L E
tf"' Jµss
Grab
Plastic
—gip pint
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%67J L
66 LID s
— Grab
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— oz
Com osite
_
— Plastic
—Pint
t
— Grab
Glass
F
o`
Plastic
—Pint
Com o_i A
Retin ulshed B (Signature)
Date
Time
Received BY: (Signature)
Date
Time
Test Package Details
Special Instructions or Remarks
St.i: 'Total Solid, (WiUnrel Total Kiddahl Nitrogen Phosohorus and Potassium
SL2: Raeic Tcst SLl rlirN Sullur, Ca1Cit11Ji. N1nW1CNianlaV,hllm. Iron, Aluminum, Mlan^_amaN, . U nrxa;�nd /ine
503 Metals: Arsenic, Cadmium Chromium, Mercury. Molybdenum. Lead, Nickel, Selenium.
(Copper & Zinc included in SL2)
Nilrrgeu Series:'fotal Kleldahl. Ammonium Mimic& i rutnic Nitrogen.
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)

Wright Memorial Bridge #35 Report# 23-20140328-14 (R41014)

Microbac0
Microbac Laboratories, Inc. -Wilson Division
3809 Airport Drive NW
Wilson, NC 27896
Tel: [phone]
Certificate of Analysis Report Date: 30-Apr-2014
�. • - 1,7111YIN ``'��t �'" Work Order: 2014-04-10-012
RPO,R?C;�O µ?;`,,.°: rl Date Received: 10-Apr-2014
SCOTT CARPENTER
SOIL PLUS
208 WILLIAMS ST
GREENVILLE NC 27858
USA
Quote: 23-20140328-14
Sample Description: WVV
Collection
SIDN
Client Marks
Analysis
Method
Date/Time:
Result
AA46970
R041014
Flash Point,Liquids
Subcontracted
4/10/14 12:00
*See Attached
AA46970
R041014
pH (Corrosivity)
Subcontracted
4/10/14 12:00
*See Attached
AA46970
R041014
Reactive Cyanide
Subcontracted
4/10/14 12:00
*See Attached
AA46970
R041014
Reactive Sulfide
Subcontracted
4/10/14 12:00
*See Attached
AA46970
R041014
TCLP Full Metals
Subcontracted
4/10/14 12:00
*See Attached
VOC SVOC Pest and
Herb
i
Reviewed and Approved by:Date:
Kim Hesse
For any feedback concerning our services, please contact James Nokes, Senior Vice President, at [e-mail]
or Trevor Boyce, President, at [e-mail]
Chemical and Microbiological Analysis: Environmental — Agrochemical — Food — Pharmaceuticals
Page 1 of 1

Microbac Laboratories, Inc.
Knoxville Division
. S - 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri Cities, TN 423.926.6385 1 Nasbville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTS -WATER - AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEU71CALS
CERTIFICATE OF ANALYSIS
Jeff Taylor
Microbac Laboratories, Inc. - Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406286 Project: Soil Sampling
Date Reported:
4/29/2014
Date Received:
4/11/2014
Cust #:
R9024
Po#:
2014-04-10-012
Analyte Result Units Oil Qualifier ReportingLimit Analyst Analyzed Method
AA46970 Sampled: 041101201412:00
1406286-01(Sludge)
General Chemistry
Analyzed BY: Microbac Knoxville Division
TCLP Extraction Fluid 0 1 JNB 04/16/2014 09:44 SW8461311
TCLP Metals by 6000/7000 Series Methods
Analyzed By: Microbac Knoxville Division
Arsenic
ND
mg/L
1
0.0150
JNB
04/221201418:31
SW846 8010E
Barlum
0.232
mg/L
1
0.00400
JNB
04/22/201418:31
SW846 6010E
Cadmium
ND
mg/L
1
0.00750
JNB
04/22/201418:31
SW846 6010B
Chromium
0.0249
►ng1L
1
0.00750
JNB
04/271201418:31
SW846 6010E
Lead
ND
mg/L
1
0.0200
JNB
04122/201418:31
SW846 6010B
Mercury
ND
mg/L
1
0.000200
JNB
04/171201416:41
SW846 7470A
Selenium
ND
mg/L
1
0.0200
JNB
04122/201418:31
SW846 6010E
Silver
ND
mg/L
1
0.00100
JNB
04/22/201418:31
SW846 6010B
TCLP Semivolatiles by EPA Method 131118270C
Analyzed By: Microbac Knoxville Division
Pyridine
ND
mg/L
1
0.0192
SLH
04/221201419:19
SW846 8270C
o-Cresol
ND
mg&
1
0.0385
SLH
04/22/201419:19
SW846 0270C
meta/para-Cresol
ND
mg/L
1
0.0385
SLH
04/22/201419:19
SW846 8270C
Hexachloroethane
ND
mg/L
1
0.0192
SLH
04/22/201419:19
SW846 8270C
Nitrobenzene
ND
mg/L
1
0.0192
SLH
04/221201419:19
SW846 8270C
Hexachlorobutadiene
ND
mg/L
1
0.0192
SLH
04/22/201419:19
SW846 8270C
2,4,6-Trichlorophenol
ND
mglL
1
0.0192
SLH
04/22/201419:19
SW846 8270C
2,4,5 Trichlorophenol
ND
mg/L
1
0.0192
SLH
04122/201419:19
SW846 6270C
2,4-Dinitrotoluene
ND
mg/L
1 Q3, R1
0.0192
SLH
04/22/201419:19
SW846 8270C
Hexachlorobenzene
ND
mg/L
1 R1
0.0192
SLH
04/22/201419:19
SW846 8270C
Pentachlorophenol
ND
mg/L
1 Q3, R1
0.154
SLH
04/22/201419:19
SW846 8270C
1,4-Dichlorobenzene
ND
mg/L
1
0.0192
SLH
04/22/201419:19
SW846 8270C
Surrogate:2-F/uoroblphenyl
10-112
65.6%
04/221201419:19
SW846 8270C
Surrogate:2-Fluomphenol
10-97
35.2%
04/22/201419:19
SW846 8270C
Surrogate: Nitrobenzene-db
10-107
70.0 %
04122/201419:19
SW846 8270C
Surrogate: Phenol-0
10-87
33.8 %
04/221201419:19
SW846 8270C
Sunvgate:7erphenyl-d14
10-130
80.1 %
04/22/201419:19
SW846 8270C
The data end Information on this, and other accompanying documents, represent only the sample(s) analyzed and Is rendered upon condition
MEMBER
that it Is not to be reproduced wholly or In part for advedlsing or other purposes wilhoul approval from the laboratory.
USDA•EPA-NIosH Testing Food sanitation consulting
Chemical and MluoblologloelAnalyses and Research
MR
Page 1 of 5
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Knoxville Division
e 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Pax:865.984.8616
Tri-Cities, TN 423:926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY - MICROBIOLOGY FOOD SAFETY • CONSUMER PRODUCTS -WATER - AIR • WASTES - FOOD - PHARMACEUTICALS - NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Jeff Taylor Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson Date Received: 4/1112014
3809 Airport Drive oust #: R9024
Wilson, NC 27896 PO#: 2014-04-10-012
Wnrknrders 1406285 Project: Soil Sampling
Analyse Result Units Dil Qualifier Reporting
g Analyst Analyzed Method
AA46970 Sampled: 041101201412:00
1406285.01 (Sludge)
TCLP Semivolatiles by EPA Method 1311/8270C
Surrogate: 2,4,6-Tdbromophenot 10-141 37.6 % 04/22/201419,.19 SW846 6270C
TCLP HERBICIDES
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
^2A.D 6.42 ug/L 1 1 20.0 JBK 04/21/201417.47 SW8151A
2,4,5-TP (Siivex) ND ug/L 1 U 2.00 JBK 04/211201417:47 SW8161A
Surrogate:2,4-DlchlorophenylaceNcacid 20-144 88.0% 04/21/201417:47 SW8151A
TCLP Pesticides
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
Endrin
ND
ug/L
1
U
0.500
ECL
04/18/2014 04:29
SW8081A
Undone
ND
ug/L
1
U
0.500
ECL
04/18/2014 04:29
SWB081A
Methoxychlor
ND
ug/L
1
U
0.500
ECL
04/18/2014 04:29
SW8081A
Toxaphene
ND
ug/L
1
U
10.0
ECL
04/18/2014 04:29
SW8081A
Chlordane
ND
uglL
1
U
10.0
ECL
04/18/2014 04:29
SW8081A
Heptachlor
ND
uglL
i
U
0.500
ECL
04/18/2014 04:29
SW8081A
Heptachlor Epoxide
ND
uglL
1
U
0.500
ECL
04/18/2014 04:29
SW8081A
.alpha Chlordane
ND
ug/L
i
U
0.500
ECL
04/18/2014 04:29
SW8081A
gamma Chlordane
ND
ug/L
1
U
0.500
ECL
04/18/2014 04:29
SW8081A
Surrogate: 2,4,5,6-Tetrach/oro-m-xy/ene
20-180
36.4 %
04/18/2014 04:29
SW8081A
Surrogate: Decachloroblphenyl
25-140
64.3 %
04/18/2014 04:29
SW8081A
GCMS Volatiles
Analyzed
BY: Microbac Laboratories, Inc. - Chicaroland
_
1,1-Dichloroethene
ND
M91L
10
0.050
jln
04/24/201414:13
1311/8260B
1,24Dichloroethane
ND
mg/L
10
0.050
jln
04/24/201414:13
1311/82608
2-Butanone
ND
mg/L
10
0.10
jin
04/24/201414:13
1311/8260B
Benzene
ND
mg/L
10
0.050
jin
04/24/201414:13
1311/8260B
Carbon tetrachloride
ND
mg/L
10
0.050
jin
04/24/201414:13
1311/8260B
Chlorobenzens
ND
mg/L
10
0.050
jin
04124/201414:13
131118260B
Chloroform
ND
mg/L
10
0.050
jin
041241201414:13
131118260B
Tetrachloroethene
ND
mglL
10
0.050
jin
04/241201414:13
1311/8260B
Tdchloroethene
ND
mg/L
10
0.050
jin
041241201414:13
131118260E
The data and Information an this, and other accompanying documents, represent only the sample(s) analimed and Is rendered upon CondWon
MEMBER
that N Is not to be reproduced wholly or In pad for advertising or other purposes without approval from the laboratory.
USDMIPA,NIDSH Testing Food sanitation consulting
chemical and MlaoblologicalMaryses and Resoarch
C�►�
Page 2 of 5
www.microbac.com [e-mail]

® Microbac Laboratories, Inc.
Knoxville Division
505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 NasbviUe, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTS -WATER - AIR • WASTES • FOOD - PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Jeff Taylor Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson Date Received: 4/11/2014
3809 Airport Drive Gust #: REIM
Wilson, NC 27896 PO#: 2014-04-10-012
Workorder: 1406285 Project: Soil Sampling
Analyte Result Units Dil Qualifier
ger Limit Analyst Analyzed Method
AA46970 Sampled: 04110/201412:00
1406285.01(Sludge)
GCMS Volatiles
Vinyl chloride ND
mg/L 10
0.020
jin 04/24/201414'13
131118260E
1,4-Dichlorobenzene ND
mg/L 10
0.10
jin 04124/201414:13
131118260B
Surrogate: 1,2-Dlchlomethane-0
74.5-132
104 %
041241201414:13
131118260B
Surrogate., 4-Bromofluorobenzene
80-120
93.1 %
04/24/201414:13
131118260B
Surrogate: Dlbromofluoromethane
80-120
91.5 %
04/24/201414:13
131118260E
Surrogate: Toluene-0
80-120
103 %
04124/201414:13
131118260B
The data and information on this, and other eccomparpMg documanls, roproserd onlythe semple(s) analyzed and Is rendered upon condition MEMBER
that a Is not to be reproduced whotty or In part for advedistng or etherpurposes without approval from the laborsiory.
UsDA.EPA.NioSHTesWg FoodeanitatlonConsuQing chemical and utcroblologlcalAnslysesand Research Lam: .
Page 3 of 5
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Knoxville Division
®S 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fam865.984.8616
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY • MICROBIOLOGY - FOOD SAFETY - CONSUMER PRODUCTS -WATER - AIR • WASTES - FOOD - PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Jeff Taylor
Microbic Laboratories, Inc. - Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406286 Project: Soil Sampling
Certifications
Date Reported:
4/29/2014
Date Received:
4/11/2014
Cust #:
R9024
PO#:
2014-04-10-012
Code
Description
Number
Expires
A2LA
A2LA ISO/IEC 17025 Env. DoD Testing
3045.02
09/30/2014
A2LA
A2LA ISO/IEC 17025 Biological Testing
3045.01
09/30/2014
A2LAB-KNX
ISO 17025 KNX food
3131.01
05/31/2015
A2LAB-NSH
ISO 17025 NSH food
3131.02
06/30/2014
FL
State of Florida NELAC
E87966
06/30/2014
GA
Georgia Dept Natural Resources
980
04/13/2014
ILDPH
Illinois DOPH Micro analysis of drinking water
1755266
12/31/2016
ILEPA
Illinois EPA wastewater and solid waste analysis
200064
04/01/2015
INDEM
Indiana DEM support lab wastewater and solid waste
A305-9-292
12/31/2013
INDH
Indiana SDH Micro analysis of drinking water
M-45-8
12/31/2016
INSDH
Indiana SDH chemical analysis of drinking water
C-45-03
08/14/2016
KSDOH
Kansas Dept Health & Env. NELAP
E-10397
01/31/2015
KYEPP
Kentucky EPPC analysis Underground Storage Tanks
75
01/31/2015
NCENV
NC Environmental
678
12/31/2013
NYDOH
New York State Department of Health Wadsworth
49179
04/01/2015
NYDOH-1
New York State Department of Health Wadsworth
49386
04/01/2015
PADEP
Pennsylvania Department of Environmental Protect
68-04863
07/31/2014
PEDEP
Pennsylvania DEP Registration forAir analysis
68-04863 .
TN_DW
North Carolina DENR NPDES effluent, surface water
TNNC597
12131/2014
TN_DW
State of Tennessee
TN02017
04/30/2014
USDA
US Department of Agriculture
11/30/2013
USDAS
USDA Permit To Receive Soil
P330-12-00174
06/20/2015
WADOE
Washington State Department of Ecology
C992
10/22/2014
WSDNR
Wisconsin DRN chemical analysis wastewater, solids
998036710
08/31/2014
The data and Information on this, and other aecompselring dosranents, rapresmd only the sample(®) analyzed and Is rendered upon condition MEMBER
that it Is not to be reproduced wholly or in part for adveNsing or other purposes without approval from the laboratory.
USDA.EPA-MOSH TesWtg Food Sanitation Conuftli Chamkal and MicrobiologicalAnatyses and Research Lli1r1.L
A
Page 4 of 6
www.microbac.com [e-mail]

® Microbac Laboratories, Inc.
Knoxville Division
• 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY - MICROBIOLOGY - FOOD SAFETY - CONSUMER PRODUCTS -WATER - AIR - WASTES - FOOD - PHARMACEUTICALS - NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Jeff Taylor
Microbac Laboratories, Inc. - Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406285 Project: Soil Sampling
Notes and Definitions
Date Reported:
4/29/2014
Date Received:
4/11/2014
Cost #:
R9024
PO#:
2014-04-10-012
U Not detected at or above adjusted sample detection rimit
R1 Duplicate RPD is outside of acceptance limits.
Q3 LCS recovery Is below acceptance limits. The reported value is estimated.
M3 Matrix spike recovery is outside of acceptance limits. The post digestion spike recovery is acceptable.
M2 Matrix spike recovery is outside of acceptance limits, biased low.
M1 Matrix spike recovery is outside of acceptance limits, biased high.
J The analyte was positively identified, but the quantitation was below the RL
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on a dry weight basis
RPD Relative Percent Difference
Microbac Laboratories, Inc. - Knoxville
Una
Maraea Branner, Project Manager
Thank you for your business. For any feedback, please contact Ashley Morris, at [e-mail]. You may also contact Trevor Boyce,
President, at bevorboyce@mlcrobaacom.
As regulatory. limits change frequently, Microbac advises the recipient of this report to confirm such limits with the appropriate Federal, state, or local
authorities before acting In reliance on the regulatory limits provided.
The data and Information on this, and other aeeompanytng documents, represent only the samples) analyzed and Is rendered upon condition MEMBER
that g is not to be reproduced wholly or In pad, for advedtstng or other purposes wilhout approval from the laboratory.
USOXEMNIOSH Testing Food SaNtegon Consuft Chemical and MlcroblologwAnalysee and Research
Page 5 of 6
www.microbaacom [e-mail]

1406285-01 sampled: 04/10/201412:0D
Microbac Laboratories, Inc`. - Wilson I
MI-I"O,l?d II � I�III�IIIIUI�III�IfI�I���IIIIIII
38
IIII�III�II IAIIII�I�III
252=�� 252-237-9341 Fax
www.microbac.com
Analysis Request Form — Intral-aboratory Chain of Custody
P.O.Mork Order # 4 - -10 - 01Z Date Ordered:
Subcontracted Company: Microbac / Knoxville Division
Address: 505 East Broadway Avenue
Maryville. TN 37804
Phone: [phone] Fax: [phone]
STRL Datefrime
Sample # Sampled Sam le Description Analysis Reauested
W6 -70 I-)O-ig Q l TC L. p
1
Check if RUSH service is requested. Tracking #: 5 1� f / 70 9-
Check if data is to be used for regulatory compliance , if yes, which agency:
Special Instructions: Please reference our Sample # on report. Report each
Sample # separately. Also, include entire sample description.
Send Reports to [e-mail] or fax [phone]
Invoices should be sent to Jeff Taylor: jeff.taylor _microbac.com
Number of Containers Shipped: S Page -L of -
Subcontracted by: RDate: V-jo-I V_
Sample Split by: Date:
Shipped by: A v le-y Date: _ /'/o- /V
Received by: RDate: -im - c r,4e,
Chemical and Microbiological Analysis:
Environmental*Agrochemical*Foods*Pharmaceuticals

Microbac Laboratories, Inc.
Knoxville/Nashville Divisions
COOLER INSPECTION FORM # 10001.1
Client Name: P ( Y'd bn r w i k k•r
Date/nme Received: / fiQ1
( a O
Work Order: U (PUS
No. of Samples:
Received By: V J
Checklist Completed By: -0-11
/
Carrier: FedExU UPSr6 ClIentU Field
Services(, Other(:
After -Hours Receipt?
Yes ❑
No
Er
Shipping container in good condition?
Yes !"
No
❑ Not Present ❑
Custody seals Intact on cooler?
Yes ❑
No
❑ Not Present'
Custody seals intact on samples?
Yes ❑
No
❑ Not Present JZ'
Chain of custody present?
Yes /El'
No
❑
Chain of custody includes proper client information?
Yes p"
No
❑
Chain of custody includes proper collection information and signatures? Yes A-
No
❑
Chain of custody includes dates and times of sample collection?
Yes
No
❑
Chain of custody includes proper sample descriptions?
Yes
No
❑
Chain of custody agrees with sample labels?
Yes M'
No
❑
Chain of custody identifies proper sample matrix?
Yes . M'
i
No
❑
Chain of custody identifies proper number of samples?
Yes Z
No
❑
Chain of custody includes required analysis?
Yes E'
No
❑
Chain of custody signed when relinquished and received?
in
Yes ,�
Yes
No
No
❑
❑
Samples are proper containers/bottles?
,O�
San7ple containers are intact?
Yes �0'
No
❑
Sufficient sample volume collected for requested analysis?
Yes ,2- ' No
❑
VOA vials for aqueous samples have zero headspace?
Yes ❑
No
❑ Not Present ICI--"
Samples received within holding times?
Yes
No
❑
Samples received on Ice?
Yes
No
❑
Sample properly preserved?
Yes
No
❑
Remarks:
If No, adjusted by? Date/rime:
ANY "NO" EVALUATION REQUIRES CLIENT NOTIFICATION (excluding After -Hours Receipt).
Comments:
Effective Date: 05/05/11 F:\shared files\Forms\Cooler Inspection Form #10001.1.pdf Page 1 of 1

Wright Memorial Bridge #35 Report# 14-101-0215

4
Page: 1 of 2
Report Number: 14-101-0215
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
LA A&L Eastern Laboratories, Inc..
7621 Whltapino Road Richmond, Virginia 23237 [phone] Fax [phone]
WWWaleastem.com
Project: 201007.1311-RALEIGH BRIDGE
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/10/2014 11:45:00
Lab Number: 98938 Date Received: 04/11/2014 00:00
Sample Id : R041014 Date Reported: 04/22/2014
Total Solids *
0.76
7600
100.0
JM
04/11/2014 14:50
SM-2540G
Moisture "
99.24
100.0
JM
04/11/2014 14:60
SM-254OG
Total Kjeldahl Nitrogen
0.40
3950
10.0
JM
04/16/2014 08:30
SM-4500-NH3C-TKN
Total Phosphorus
0.04
392
100
KM
04/16/2014 14:52
SW 6010C
Total Potassium
1.76
17600
100
KM
04/16/2014 14:52
SW 6010C
Total Sulfur
0.06
609
100
KM
04/16/2014 14:52
SW 6010C
Total Calcium
13.80
138000
100
KM
04/16/2014 14:52
SW 6010C
Total Magnesium
0.02
218
100
KM
04/16/2014 14:52
SW 6010C
Total Sodium
2.06
20600
100
KM
04/16/2014 14:52
SW 6010C
Total Iron
1210
100
KM
04/16/2014 14:52
SW 6010C
Total Aluminum
173000
100
KM
04/16/2014 14:52
SW 6010C
Total Manganese
13
5
KM
04/16/2014 14:52
SW 6010C
Total Copper
8
5
KM
04/16/2014 14:52
SW 6010C
Total Zinc
29
5
KM
04/16/2014 14:52
SW 6010C
Ammonia Nitrogen
0.40
3950
10.0
JM
04/16/2014 08:30
SM-4500-NH3C
Organic N
0.00
0
10.0
04/16/2014 08:30
CALCULATION
Nitrate+Nitrite-N
211
2.00
JM
04/16/2014 08:40
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
04/16/2014 14:52
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results; or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-101-0215
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
Lab Number: 98938
Sample Id: R041014
A&L Eastern Laboratories, Inc.
7621 Whltepine Road Richmond, Virginia 23237 [phone] Fax [phone]
vinarww.aleasterro9.com
Project: 201007.1311-RALEIGH BRIDGE
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 4/10/2014 11:45:00
Date Received: 04/11/2014 00:00
Date Reported: 04/22/2014
Total Chromium
12
5
KM
04/16/2014 14:52
SW 6010C
Total Nickel
6
5
KM
04/16/2014 14:52
SW 6010C
Total Lead
<5
5
KM
04/16/2014 14:52
SW 6010C
Total Arsenic
<3.0
3.0
KM
04/16/2014 14:52
SW 6010C
Total Mercury
<0.4
0.4
KM
04/16/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
04/16/2014 14:52
SW 6010C
pH (Standard Units) *
12.36
2.00
JM
04/16/2014 08:30
SW-9045D
Total Molybdenum
<5
5
KM
.04/16/2014 14:52
SW 6010C
Soluble Phosphorus
<0.01 <100
100
JM
04/16/2014 09:00
SOLUBLE P IN MANURE
Comments:
NELAP ACCREDITED: VA NELAC LAB. # 460014. PA NELAC LAB # 68-03109, FL NELAC LAB # E871087, NJ NELAC LAB # VA011. RESULTS REPORTED
MEET ALL REQUIREMENTS OF THE CURRENT NELAC STANDARDS. SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. CCE
FOR COMPLIANCE IN VIRGINIA AND PENNSYLVANIA ONLY.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

SECTION II: LAND APPLICATION SUMMARY

Mt. Misery Road

HYDRODEMOLITION OPERATION SLURRY / DIAMOND GRINDING SLURRY
LAND APPLICATION LOG
Project Name
(Source of HOS/DGS): Mt. Misery Road over Highway 74; Leland (New Hanover County)
Project Location: Mt. Misery Road over Highway 74 Bridge; - Latitude 3401612411' :Longitude 78003126"
Project Description: Hydrodemolition — IVS Hydro (Project# C203074)
Land Application -
Operator in Responsible Charge: Wesley Wooten — Lewis Farms & Liquid Waste, Inc.
Date of Land
Application
Location of Receiving Site
(Land Owner Name)
Receiving Site Address or
Latitude / Longitude
Quantity Applied
(Gallons or Dry Weight)
% Solids
413114
Corbett Field
Latitude: 34024'10"; Longitude: 77056'27"
4,000 Gallons
N/A
5/2/14
Corbett Field
Latitude: 34024'10"; Longitude: 77°56'27"
4,000 Gallons
N/A
5/10/14
Corbett Field
Latitude: 34024'10"; Longitude: 77°56'27"
3,000 Gallons
NIA
5129114
Corbett Field
Latitude: 34024'10"; Longitude: 77056'27"
4,000 Gallons
NIA
6/31/14
Corbett Field
Latitude: 34°24'10"; Longitude:_ 77056'27"
4,000 Gallons
N/A
-6/2/14
Corbett Field
Latitude: 34024'10"; Longitude: 77056'27"
4,000 Gallons
NIA
6/9/14
Corbett Field
Latitude: 34024'10"; Longitude: 77056'27"
4,000 Gallons
NIA
6116/14
Corbett Field
Latitude: 34°24'10"; Longitude: 77°56'27"
4,000 Gallons
N/A
Mt. Misery Road over Highway 74 Bridge Total
31,000 Gallons
T:\Projects\2010\ENV\1588-10-027 NC DOT\Phase 02 - Diamond Grindina Slurrv\2014 Annual Renort\Lewis Farms\Mt- Misery Road & Hiahwav 74v Aivn APPi i('ATIC)M i nr: 9MA rl—

HYDRODEMOLITION OPERATION SLURRY / DIAMOND GRINDING SLURRY
pH LOG
Project Name
(Source of HOSIDGS): Mt. Misery Road over Highway 74; Leland (New Hanover County)
Project Location: Mt. Misery Road over Highway 74 Bridge; - Latitude 34015'24"' :Longitude 7800312611
Project Description: Hydrodemolition — IVS Hydro (Project# C203074)
Land Application
Operator in Responsible Charge: Wesley Wooten — Lewis Farms & Liquid Waste, Inc.
Date pH Sample Collected
Date pH Analyzed / Reported
Lab or Field Sample
pH Measurement
Unit Sampled
(Truck, Frac Tank, Dewatering Box., etc.)
4/3/14
4/3/14
Field
12.0
Dewatering Box
5/2/14
5/2/14
Field
11.9
Dewatering Box
5/10/14
5/10/14
Field
11.8
Dewatering Box
5/29/14
5/29/14
Field
12.1
Dewatering Box
5/31/14
5/31/14
Field
12.2
Dewatering Box
6/2/14
6/2/14
Field
11.7
Dewatering Box
6/9/14
6/9/14
Field
12.1
Dewatering Box
6/16/14
6/16/14
Field
11.9
Dewatering Box
6/16/14 and 10/14/14
1/9/15 / 1/21/15
Lab
12.2
Dewatering Box
T:\ProjectM2010\ENV\1588-10-027 NC DOT\Phase 02 - Diamond Grinding Slurry\2014 Annual Report\Lewis Farms\Mt. Misery Road & Highway 74\pH LOG 2014.doc

College Road

HYDRODEMOLITION OPERATION SLURRY / DIAMOND GRINDING SLURRY
LAND APPLICATION LOG
Project Name
(Source of HOS/DGS): College Road and West Market Street Bridge — New Hanover County, Bridge #8
Project Location: College Road and West Market Street — Latitude 34014'46"; Longitude 72052'16"
Project Description: Hydrodemolition — IVS Hydro
Land Application
Operator in Responsible Charge: Wesley Wooten — Lewis Farms & Liquid Waste, Inc.
Date of Land
Application
Location of Receiving Site
(Land Owner Name)
Receiving Site Address or
Latitude / Longitude
Quantity Applied
(Gallons or Dry Weight)
% Solids
12/18/14
Corbett Field
Latitude: 34024'10"; Longitude: 77056'27"
8,000 Gallons
N/A
College Road & West Market Street Bridge Total
8,000 Gallons
T:\Projects\2010\ENV\l588-10-027 NC DOT\Phase 02 - Diamond Grinding Slurry\2014 Annual Report\Lewis Farms\College Road 8& W. Market\LAND APPLICATION LOG 2014.doc

HY®R®®EMOLITION OPERATION SLURRY / DIAMOND GRINDING SLURRY
pH LOG
Project Name
(Source of HOS/DGS): College Road and Nest Market Street Bridge — New Hanover County, Bridge #8
Project Location: College Road and West Market Street — Latitude 34014'4611; Longitude 72052116"
Project Description: Hydrodemolition — IVS Hydro
Land Application
Operator in Responsible Charge: Wesley Wooten — Lewis Farms & Liquid Waste, Inc.
Date pH Sample Collected
Date pH Analyzed / Reported
Lab or Field Sample
pH Measurement
Unit Sampled
(Truck, Frac Tank, Dewatering Box, etc.)
12/18/14
12/18/14
Field
11.9
Dewatering Box
T:\Projects\2010\ENW 588-10-027 NC DOT\Phase 02 - Diamond Grinding Slurry\2014 Annual Report\Lewis Farms\College Road & W. Market\pH LOG 2014.doc

1-40 Bridges (Sunnybrook/Crabtree Roads)

8:56 AM
1/15/15 Accrual Basis
1-40 Bridge Sludge
Atlantic OBX, Inc.
Bridge Sludge
1/2014 thru 12/2014
Source Name
Gallons
Ship Date
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/19/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/19/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/19/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/19/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/19/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/19/2014
Invoice
IVS Hyrdo:I-40 Bridge
4,000
5/19/2014
Invoice
IVS Hyrdo:I-40 Bridge
4,000
5/19/2014
Subtotal
32,000
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
5/28/2014
Subtotal
40,000
Invoice
IVS Hyrdo:1-40 Bridge
4,000
6/30/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
6/30/2014
Subtotal
8,000
Invoice
IVS Hyrdo:1-40 Bridge
4,000
8/29/2014
Invoice
IVS Hyrdo:1-40 Bridge
8,000
8/29/2014
Invoice
IVS Hyrdo:1-40 Bridge
8,000
8/29/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
8/29/2014
Subtotal
24,000
Invoice
IVS Hyrdo:1-40 Bridge
4,000
9/24/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
9/24/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
9/24/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
9/24/2014
Invoice
IVS Hyrdo:1-40 Bridge
4,000
9/24/2014
Invoice
IVS Hyrdo:1-40 Bridge
8,000
9/24/2014
Subtotal
28,000
Total
1-40 Bridge Sludge
132,000

ONTROt
Post Office Box 2560 Kitty Hawk, NC 27949
(252} 285-2030 (:?52) 449-6G©4
"'Ww.atlantiesewagexom
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Invoice
L1at i . inv ice'#`•,.
5/19/2014 19698
Service address; Terms ` Service Date T echn
1-40 Bridge, Raleigh, NC Net 15 5/19/2014
Descc�ption
Amour
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
419/14 with pH of 11.9.
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & SA on
4/10/14 with pH of 11.7
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
4111/14 with pH of 12.0
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
4/12/14 with pH of 11.8
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
4/13/14 with pH of 11.8
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
4/19/14 with pH of 11.7
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
4/29/14 with pH of 11.8
4000 gallons of slurry removed from bridge and disposed of in Edwards Field 'No. 8 & 8A on
4/30/14 with pH of 11.9
Biosolid Test Package & TCLP
Sales Tax
Total
Thank you for your business. We appreciate the opportunity to serve you. PaymentslCredits
IBalance Due

A ILAA�, 11C
GE
LSEW
r� # Y f 6"
t TRi 0
"r��.
���a�a rts.�vrGti�
Post Office Box 2560 Kitty Hawk, NC 27949
(252) 255i-2030
(: 52) 49-6604
\vww. atlanticsewage.com
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Invoice
Date 'Invoice
6/2/2014 19868
PO or VVO No.� Service Address Terms Service [late . Technician
1-40 Bridge, Raleigh, NC Net 15 5/28/2014�_
T-----�
Description I Amount
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
5/2/14 with pH of 11.7
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
5/14/14 with pH of 11.8
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
5/16/14 with pH of 12.0
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
5/17/14 with pH of 11.8
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
5/19/14 with pH of 11.7
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A, on
5/20/14 with pH of 11.8
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
5/21/14 with pH of 11.9
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
5/22/14 with pH of 11.8.
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
5/23/14 with pH of 11.9
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
5/28 with pH of 11.7
Sales Tax
Total
Thank you for your business. We appreciate the opportunity to serve you. 4 Payments/Credits
Balance Due

CONTROL
Post Office Box 2560 Kitty Hawk, NC 27949
d252k 255-2030 [phone]
w�t,%v. atlanticsewagexom
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Date
Invoice #
7/17/2014
20475
P,0 orWa Nd. ServiceAddress � Terms ServicL- Date Technician
1-40 Bridge, Raleigh, NC Net 15 6/30/2014
Description i Amount
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on i
6/26/14 with pH of 11.8 I
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
6/30/14 with pH of 11.6
Sales Tax
Total
Thank you for your business. We appreciate the opportunity to serve you. ( Payments/Credits
Balance Due

4.
NTR
Post Office Box 2560 Kitty Hawk, NC 27949
[phone] (:452)449-6604
wWw.atlanticsewagexom
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Invoice
Date
`
Invoice
9/4/20141
21117
hiclaw,'
e, k
Service dress ferms,''
'Pobi 0, "Tech
1-40 Bridge, Raleigh, NC Net 15 8/29/2014
moun,t
,,� -
D tIbn,.,: espr,p
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & BA on
8114/14 with pH of 11.9
8000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
8/20/14 with pH of 11.8 and 12.0
8000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
8/22/14 with pH of 12.0 and 11.8
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
8/29/14 with pH of 11.7
Sales Tax
Total
Thank you for your business. We appreciate the opportunity to serve you.! Payments/Credits
Balance Due
I

cONTRol
Post Office Box 2560 Kitty Hawk. NC 27949
[phone] [phone]
www.atlanticsewage.com
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Invoice
- Date ,i 4 =irav�aacg#f:K:`,
10/7/2014 21469
Ad
P® arWO 9�aervrce. "dross Tefrr�s RServrc
j 1-40 Bridge, Raleigh, NC j Net 15 1 9/24/2014 1
Description
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
9/16/2014 with pH of 11.8
4006'gailons"iaf slurry rerrioved from bridge "and disposed, of -in Edwards.'Field-No. 8; &,8A on
9/18/2014'with.pKof 11.6.
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8'& 8A on
11.9 with pH of 11.9
4000 gallons .of slurry removed from° bridge and disposed of-inEdwards Field --No. '8 & 8A an
9/20/2014 with --pH of.,11.6 :.
4000 gallons of slurry removed from bridge and disposed of in Edwards Field No. 8 & 8A on
9/23/2014 with pH of
8000 6allons�6f slurry, �emoved,;from.bridge and disposed of in,Edwards Field No. 8 & BA on;:
9124/2014' with pH of 11c;8 and 11 7 :: .'
Sales Tax
Total
Thank you for your business. We appreciate the opportunity to serve you. Payments/Credits
IBalance Due
Amount,

Wright Memorial Bridge #35

M
8:66 AM
Atlantic OBX, Inc.
1115/16 Accrual Basis
Bridge Sludge
Wright Memorial Bridge
1/2014 thru 12/2014
Sludge
Source Name
Gallons Ship Date
Invoice
IVS Hyrdo-Wright Memorial
4,000
1/28/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
1/28/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
1/28/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
1/28/2014
Invoice
'IVS Hyrdo-Wright Memorial
8,000
1/28/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
1/28/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
1/28/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
1/28/2014
Subtotal
52,000
Invoice
IVS Hyrdo-Wright Memorial
8,000
2/28/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
2/28/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
2/28/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
2/28/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
2/28/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
2/28/2014
Subtotal
44,000
Invoice
IVS Hyrdo-Wright Memorial
4,000
3/21/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
3/21/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
3/21/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
3/21/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
3/21/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
3/21/2014
Subtotal
40,000
Invoice
IVS Hyrdo-Wright Memorial
4,000
4/11/2014
Invoice
IVS Hyrdo-Wright Memorial
12,000
4/11/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
4/11/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
4/11/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
4/11/2014
Subtotal
32,000
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014

8:56 AM Atlantic OBX, Inc.
1/15/15 Accrual Basis
Bridge Sludge
Wright Memorial Bridge Sludge 1/2014 thru 1212014
Source Name
Gallons Ship Date
Invoice
IVS Hyrdo-Wright Memorial
8,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
10/31/2014
Subtotal
92,000
Invoice
IVS Hyrdo-Wright Memorial
8,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
16,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
16,000.
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
12,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
11/21/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
11/21/2014
Subtotal
116,000
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
8,000
12/19/2014
Invoice
IVS Hyrdo-Wright Memorial
4,000
12/19/2014
Subtotal
60,000
Project Total
Wright Memorial
436,000

COPliR01.
Post Office Box 2560 Kitty Hawk. Nas-s� ,349
04
fa5w4w5atlant es wage.com
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
. .�
invoice
;Date . :Invoice'#' G
2/6/2014 18364
------�-- �. . - � � ephnicianwvv �`;.
Service Address.:. .,Terms ... :y5eovii'ce`Date ..
Wright Memorial Bridge Net 15 1/28/2014
Description. .
4000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 213 on 114 with pH of 11.5
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 3 on 1/10 with pH of 11.5 & 12.0
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 3 on 1/13 with pH of 12.3 & 12.3
14000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
I No. 2B on 1/14 with pH of 12.3
18000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2B on 1117 with pH of 12.3 & 12.3
8000 t end of bridge and disposed of in Newbern Field
gallons of slurry removed from Eas
No. 3 on 1120 with pH of 11.8 & 11.6
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2A on 1121 with pH of 11.9 & 11.6
4000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 3 on 1/28 with pH of 11.8
Dare County Sales Tax
Total
Thank you for your business. We appreciate the opportunity to serve you.I Payments/Credits
Balance Due
KC

ATSL
VAN,
EIC
'(�`�,Y Q
ONTROL
,', gey,jTrR
r�rr"rya ur.�°rro�'�+s
Post Once Box 2560 Kitty Hawk, NC 27949
(2:52) 2r>5-2030
[phone]
www.atlanticsewagge.com
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Invoice
Date
Invoice #
3/10/2014
18685
PO or.WO No. Service Address, Terms Service Date Technician
Wright Memorial Bridge Net 15 i 2/28/2014 PC
Description Amount .:-
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 3 & 2A on 2/19/2014 with pH of 11.8 & 11.6
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2A on 2/21/2014 with pH of 12.3 & 12.5
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2A & 3 on 2/22/2014 with pH of 11.8 & 11.7
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2A on 2/25/2014 with pH of 12.8 & 12.0
4000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2A on 2/27/2014 with pH of 11.8
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 3 on 2/28/2014 with pH of 11.6 & 11.9
Sales Tax
Total
Thank you for your business. We appreciate the opportunity to serve you. Payments/Credits
a
Balance Due

r
C4'NTRO
Post Office Box 2560 Kitty Hawk. NC 2,7949
(2S2) 256-2030
�nvw.atlanticsewage.com
[phone]
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Invoice
bale
: "-In e,#.,.:
4/1/2014
18966
PO;ror WO;No Service.Address Terms Service Date 1`echmciain
Wright Memorial Bridge Net 15 3/21/2014 PC
' D scrtption Am',
4000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 3 on 3/3 with pH of 11.7
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Fields
No. 2A & 3 on 3/12 with pH of 11.8 & 11.6
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2A on 3/17 with pH of 11.8 & 11.6
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2A on 3/19 with pH of 11.8 & 11.6
4000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2A on 3/20 with pH of 11.6
8000 gallons of slurry removed from East end of bridge and disposed of in Newbern Field
No. 2A & 3 on 3/21 with pH of 11.7 & 11.9
Sales Tax
f-
Total
Thank you for your business. We appreciate the opportunity to serve you. i Payments/Credits
Balance Due

or
::.a... Invoice
Post Office Box 2560 Kitty Hawk, NC 27949
[phone] (2s2) 449.6604
MwW.atlanticse�vagexom
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Date'
' Invo„ice
4/22/2014
19243
P® or W0'No 8erv11ce Address Terms ;.Service Date Techntt:lan
Wright Memorial Bridge Net 15 4/11/2014 PC
De'sc'nptton' Amount
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 4/4 with pH of 11.9
12,000 gallons of slurry removed from West end of bridge and disposed of in Newbern
Fields No. 2A & 3 on 4/5 with pH of 11.6, 11.8 & 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2A on 4/9 with pH of 11.8
8000 gallons of slurry removed from West end of bridge and disposed of in Newbern Fields
No. 2A & 3 on 4110 with pH of 11.7 & 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 4/11 with pH of 11.9
I
i
Thank you for your business. We appreciate the opportunity to serve you.
i
Total
Payments/Credits $0.00 1
Balance Due

c0N,IRQL
Post Office Box 2560 Kitty Hawk, NC 2790
(:25 2} 2SS-2030 . f252> 449-6604
w -- atlnn icsewa a com
BILL, TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Invoice,
Dates
Irnvoice l" "
11/5/2014
21785
Poor Wo No �:Seev6 Address Terms " Seru ce Date Techrncian
Wright Memorial Bridge Net 15 10/31/2014 PC
Description Amount
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 10/4 with pH of 11.0
4000 gallons of slurry removed, from West end, of bridge,and disposed of in Newbern-Field I
No. 3 on 10/6 with pH of 11.0
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2 on 10/7 with pH of 10.0
4060'gallons of slurry removed from West°end of •bridge and disposed of in, Newbem Field
No. 3 on 10/8'with, pH of 11.5
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2 on 10/11 with pH of 11.6
4000- gallons of slurry, removed from West. end,of bridge and disposed of in Newbern Fieid
No. 2 on 10/13 with pH of 11.7
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field ;
No. 2 on 10/11 with pH of 11.5
4000 gallons of slurry removed from West end of•bridge and disposed, of in Newbern ;Field f
No. 2 on 1,0/13 with pH of 11.5
8000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2 on 10/14 with pH of 11.6 and 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbem Field "
No. 2A on,10/15 with pH of 11:4
4000 gallons of slurry. removed from West end of bridge and disposed of in Newbem Field j
No. 2 on 10/17 with pH of 11.2 I
4000 gallons of slurry removed from West end of bridge -and disposed of in Newbern:, Field
No. 2 on 10/18 with pH°of 11.2
4000 gallons of slurry removed from West end of bridge and disposed of in Newbem Field
No. 2 on 10/20 with pH of 11.3 ;
4000 gallons'of slurry removed from West end of bridge and disposed -of in Newbern Field
No: 2'on 10/21 with pH of 11.6 ' • f " +.
Total ' �.-..w_
Thank you for your business. We appreciate the opportunity to serve you.I Payments/Credits
Balance Due
Page 1

v
TLANTI
Invoice
CONTROL
t ars°r�° Date Invoice
Post Office Box 2560 Kitty Mawk, NC 27949
(252) 255_2030 (252) 449•66041 11/5/2014 21785.
Nv%V%v.atlanticsewa_ge.com
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
I�
PO.or 1a91®'No. Service Address - Terms Service Date _ Technician
Wright Memorial Bridge Net 15 3 10/31/2014 PC
Description �� Amount
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 10/22 with pH of 11.7
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 10/23 with pH of 11.7 t
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 10/24 with pH of 11.6
8000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field ;t
No. 3 on 10/28 with pH of 11.3 and 11.5
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field '
No. 3 on 10129 with pH of 11.6
f;
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Fieldi
No. 3 on 10/30 with pH of 11.3
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 10/31 with pH of 11.2
Sales Tax
Total
Thank you for your business. We appreciate the opportunity to serve you. I Payments/Credits
Balance Due
Page 2

ONTROL
Tic acavic
Post Office Box 2560 Kitty Hawk. NC 27949
(252) 7' 5-2030 (�52)449-6604
�v,,K:atlanticse%vage.com
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Invoice
nvolc6V
12/312014 21977
P6 or,woN
$6rvlce'Adre
7
.,Terms,
Service Date,
Technician:
Wright Memorial Bridge
Net 15
11/21/2014
PC
escn
AMQUnV
D` 1ptlow,'_
77 j,,,,
8000 gallons of slurry removed from West end of bridge and disposed of in Newbern, Field
No. 3 on 11/1 with pH of 11.6 and 11.6
16,000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 11/3 with pH of 11.3, 11.3, 11.8 and 11.6
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 11/4 with pH of 11.7
16,000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 11/5 with pH of 11.2, 11.6, 11.8, 11.6
8000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 11/6 with pH of 11.3 and 11.6
8000 gallons of slurry removed from West end of bridge and disposed of in Newbem Field
No. 3 on 1-1/7 with pH of 11.8 and 11.4
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2 on 11/8 with pH of 11.3
12,000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2 on 11110 with pH of 11.6, 11.8 and 11.9
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2 on 11/11 with pH of 11.6
8000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2A on 11112 with pH of 11.4 and 11.7
4000 gallons of slurry removed from West end of bridge and disposed of in Newbem Field
No. 2 on 11113 with pH of 11.7
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 11/15 with pH of 11.3
8000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2 on 11/17 with pH of 11.8 and 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 11/19 with pH of 11.8
Total
Thank you for your business. We appreciate the opportunity to serve you. I Payments/Credits
Balance Due
Page 1

a w
AT- I
NT L
�j{., L.' 14V24' L:i'
Post Office Box 2560 Kitty
Hawk, NC 27949
(25 2+s.5 2030
(2!52) 449-6604
�ti�vw,adl anticsewage.conl
BILL TO:
IVS Hydro, Inc.
P.O. Box 245
Waverly, WV 26184
Invoice
Date Invoice #
12/3/2014 ; 21977
PO ;or WO No. Service Address � �i Terms � i "� Service Cute . "Technician
Wright Memorial Bridge Net 15 11/21/2014 PC
,. IDeseriPtixsn ° _ � i . Amount . F
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 2 on 11/20 with pH of 11.3
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No.�2 on 11/21 with pH of 11.6
Sales Tax
Total
Thank you for your business. We appreciate the opportunity to serve you. r Payments/Credits
I Balance Due
Page 2

TDC
Post Office Box 2560 Kitty Hawk, NG 27949
[phone] (2�52).449-6604
. w%�,w.atlantiesevvage.com
BILL TO:
IVS Hydro, Inc,
P.O. Box 245
Waverly, WV 26184
Invoice
Date
110oice 47
12/26/2014
22187
PO;or0 N6. ServiceAddrei� TenS'PVice,Dater T6ch niclan°
Wright Memorial Bridge Net 15 12/19/2014 PC
7
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No.3 on 12/2 with pH of 11.4
4000gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No.3 on 12/ 3with pH of 11.3
8000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 12/4 with pH of 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No.3 on 12/5 with pH of 11.6
4000 gallons of slurry removed from West end of bridge and disposed of in Newbem Field
No3. on 12/9 with pH of 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No.3 on 12/11 with pH of 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No.3 on 12/12 with pH of 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 12/14 with pH of 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 12/ 15 with pH of 11.6
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No.3 on 12/ 16 with pH of 11.8
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No.3 on 12/17 with pH of 11.7
8000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No.3 on 12/ 18 with pH of 11.7
4000 gallons of slurry removed from West end of bridge and disposed of in Newbern Field
No. 3 on 12/ 19 with pH of 11.8
Sales Tax
TiDtal
Thank you for your business. We appreciate the opportunity to serve you. L payments/Credits
IBalance Due
nt._
AMiDU