WQ0035595_Residual Annual Report 2014_20150302

GRANVILLE FARMS, INC.
2014 ANNUAL LAND APPLICATION OF
RESIDUAL BIO-SOLIDS REPORT
CLASS B PROGRAM
WQ0035595
Submitted by:
Soil Plus
208 Williams Street
Greenville, North Carolina 27858,
February 17, 2015

^' l ., " S
I
Cf �.
February 17, 2015
NCDENR-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2014 LAND APPLICATION ANNUAL REPORT
Granville Farms, Inc. "Class B" Program
NC Permit No.: WQ0035595
Soil Plus Project No. 200705.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for Granville Farms, Inc. Soil Plus compiled this
report using data gathered during the compliance year. This data includes (1) certification
form, (2) residual sampling, (3) field loading calculations, (4) pathogen and vector attraction
reduction documentation, (5) standard soil fertility nutrient analysis.
Granville Farms, Inc. conducted application events on permitted fields in Edgecombe &
Martin Counties during 2014. A total of 246.99 Dry Tons or 2,057,890 gallons of
permitted residual bio-solids were land applied to permitted fields.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact me or the Granville Farms, Inc. (919-690-8000) for further
assistance.
Respectfully,
C. Scott Carpenter, L.S.S.
North Carolina Nutrient Management Planner
Andy Smith, Granville Farms
Jason Smith, Granville Farms
208 Williams St.
Greenville, NC 27858
t(252) 917-4288
f [phone]
www.soilplus.net

'�91�aP
February 17, 2015
U.S. EPA
WWPD/WENF
U.S. EPA Region 7
11201 Renner Boulevard
Lenexa, Kansas 66219
Attention: Biosolids Center
Re: 2014 LAND APPLICATION ANNUAL. REPORT
Granville Farms "Class B" Program (Edgecombe County Farm)
NC Permit No.: WQ0035595
Soil Plus Project No. 200705.A10
Water Management Division:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit on behalf of Granville Farms, Inc. Soil Plus
compiled this report using data gathered during the compliance year. This data includes (1)
certification form, (2) residual sampling, (3) field loading calculations, (4) pathogen and
vector attraction reduction documentation, (5) standard soil fertility nutrient analysis.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact me or Granville Farms, Inc. (919-690-8000) for further
assistance.
Respectfully,
C. Scott Carpenter, L.S.S.
North Carolina Nutrient Management Planner_
Jason Smith, V.P. Granville Farms
208 Williams Street
Greenville,,NC 27858
t(252) 917-4288
f(800) 755-7153
www.soilplus.net

Granville Farms
2014 Annual Land
Application of
Residual Bio-Soilds
Report
WQ0035595
Edgecombe
County, NC
ANNUAL
CERTIFICATION FORM
Source Summary
Field Loading Summary
RESIDUAL SAMPLING
SUMMARY FORM
Ahoskie WWTP
Contentnea MSD WWTP
Neuse River WWTP
Town of Tarboro WW1?
Williamston WWTP
FIELD SUMMARY FORM
PATHOGEN & VECTOR
REDUCTION FORM
W
Ahoskie WWTP
Contentnea MSD VVWq?4
Neuse River WWTP
Town of Tarboro WWI?
Williamston WWTP
SOIL SAMPLES
JBS Farm
Eddie Brown Farm *5
© Copyright

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0035595 Granville Farms, Inc. Granville Farms Granville [phone]
Year: 2014
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 34
Total number of fields utilized for land application during the year: 15
Total amount of dry tons applied during the year for all application sites: 246.99
Total number of acres utilizes for land application during the year: 244.87
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality d❑ MQ
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
certified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilit
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilitie
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit.
r 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations."
Jason Smith, Vice President
a« 02-17-2015
Permittee Name and Title (type or print):
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Tuesday, February 17, 2015
Signature of Permittee
Signature of Land Applier Date
(if different from Permittee)

Source Summary
WWTP Volume Applied Dry Tons
Ahoskie WWT'P
747,500
93.51
Contentnea MSD V WTP
147,000
9.81
Neuse River WWTP
404,390
56.83
Stantonsburg WWTP
77,000
8.09
Town of Tarboro VAV IP
70,000
10.35
Williamston WWTP
612,000
68.39
Grand Total
2,U3-,S9U
246.99
Tuesday, February 17, 2015 Page 1 of 1

YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED
PERMITTED CROPS AND LOADING RATES
Acres
Volume
Crop 1 PAN Crop 2 PAN
Total P
Crop 1
PAN 1
Crop 2 PAN 2
Field
Used
Applied
Total DT
lbs/Ac. lbs/Ac.
lbs/Ac.
Crop 1 Name
PAN
Used
Crop 2 Name
PAN Used
Site# EB
1
10.19
136,000
15.20
50.00
59.07
Common
230
21.7%
Annual Ryegrass -
50
Bermudagrass
Pasture
2
16.21
231,200
25.84
53.43
63.12
Common
230
23.2%
Annual Ryegrass -
50
Bermudagrass
Pasture
3
12.88
130,000
16.26
42.34
63.39
Common
230
18.4%
Annual Ryegrass -
50
Bermudagrass
Pasture
4
8.74
129,200
14.44
55.38
65.42
Common
230
24.1%
Annual Ryegrass -
50
Bermudagrass
Pasture
5
7.89
115,600
12.92
54.89
64.84
Common
230
23.9%
Annual Ryegrass -
50
Bermudagrass
Pasture
Site# JBS
11
10.73
147,000
9.81
23.92
Common
207
Annual Ryegrass -
50 47.8%
Bermudagrass Hay
Hay
12
12.3
54,681
7.68
33.25
52.91
Wheat, Grain
116
28.7%
Sorghum, Grain
50
13
24.6
201,500
25.21
34.36
51.44
Wheat, Grain
125
27.5%
Soybeans, Manured,
50
Full Season
17
29.51
63,000
9.38
5.97
3.41
Corn, Grain
148
4.0%
Sorghum, Grain
50
2
12.83
130,585
18.35
76.13
121.14
Wheat, Grain
116
65.6%
Soybeans, Manured,
50
Full Season
Tuesday, February 17, 2015
Page 1 of
2

YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED
PERMITTED CROPS AND LOADING RATES
Acres
Volume
Crop 1 PAN Crop 2 PAN
Total P
Crop 1 PAN 1
Crop 2 PAN 2
Field
Used
Applied
Total DT lbs/Ac. lbs/Ac.
lbs/Ac.
Crop 1 Name
PAN Used
Crop 2 Name
PAN Used
211
31.7
416,000
52.04 55.05
82.41
Wheat, Grain
121 45.5%
Sorghum, Grain
50
22
16.49
77,000
8.09 2.90
21.69
Wheat, Grain
106 2.7%
Corn, Grain
50
3
17.9
97,357
13.68 40.68
64.74
Wheat, Grain
116 35.1%
Soybeans, Manured,
50
Full Season
32
10.4
7,000
0.97 2.08
2.31
Annual Ryegrass -
125 1.7%
Sorghum
50
Hay
6
22.5
121,767
17.11 40.48
64.41
Wheat, Grain
125 32.4%
Soybeans, Manured,
50
Full Season
Total 2,057,890 246.99
Tuesday, February 17, 2015 Page 2 of 2

r � i
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. W00035595 Facility Name Granville Farms, .Inc. Source Permit No. NCO088561 Source Name Ahoskie W VrP
Laboratory1 A&LEastem
Tabs, Inc.
Laboratory 2
Sample or CompositeDate 3/25/3014
Parameter (mg/Kg) Class A Clas B
Aluminum
N/A
N/A
30,400
Ammonia Nitrogen
N/A
N/A
6,670
Arsenic
41
75
4
Cadmium
39
85
2
Calcium
N/A
N/A
16,900
Copper
1,500
4,300
442
Lead
300
840
37
Magnesium
N/A
N/A
4,500
Mercury
17
57
0.8
Molybdenum
N/A
75
10
Nickel
420
420
24
Nitrate-Nitrite.Nitmgen
N/A
N/A
43
Percent Solids
N/A
N/A
3.00
pH (no units)
N/A
N/A
7.16
Phosphorus
N/A
N/A
25,100
Potassium
N/A
N/A
4,900
PAN (Inj./Inc.)
N/A
N/A
20,102
PAN (Surface)
N/A
N/A
16,767
Selenium
.100
100
5
Sodium
N/A
N/A
5,690
SAR
N/A
N/A
1.73
TKN
N/A
N/A
51,300
Zinc
2,800
7,500
1050
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel, properly gathered and evaluated the information submitted. I am awate that there are significant penalties for
submitting false information, including the ossibility of fines and imprisonment for knowing violations."
2//�/�
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102.(26)

FIELD LOADING ESTIMATES
Facility Ahoskie WW `P
Sampling Date
% Solids 3
Mineralization Rate 0.30
Gallons per DT 7,993.61
pH 7.16
Sodium Absorpotion 1.73 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 51,300 lbs./1,000 gal 12.84
Potassium lbs./1,000 gal
1.24
Ammonia Nitrogen (mg/Kg) 6,670.00 lbs./1,000 gal 1.67
Phosphorus lbs./1,000 gal
6.28
Nitrate -Nitrite (mg/Kg) 43.30 lbs./1,000 gal 0.01
Calcium lbs./1,000 gal
4.23
PLANT AVAILABLE NITROGEN SURFACE APPLIED
Calcium lbs./1,000 gal
1.13
PAN (mg/Kg) 16,767 lbs./1,000 gal 4.20
Manganese lbs./1,000 gal
0.08
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
2.01
PAN (mg/Kg) 20,102 lbs./1,000 gal 5.03
Molybdenum lbs./1,000 gal
0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
i
3rd Year
4th Year
i
5th Year
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
4.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
442.00
Copper lbs./1,000 gal
0.11
Lead (mg/Kg)
37.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.80
Mercury lbs./1,000 gal
0.00 '
Nickel (mg/Kg)
24.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
1050.00
Zinc lbs./1,000 gal
0.26
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Rem alIIing
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TI;TT
(-g/kg) (lbs/DT)
(-g/Kg)
TKN
(-g/kg) (lbs/DT)
(-g/Rg)
51,300
16,767
33.53
34,533
51,300
20,102 40.20
31,198
34,533
5,180
10.36
29,353
31,198
4,680 9.36
26,518
29,353
Z201
4.40
27,151
26,518
1,989 3.98
24,529
27,151
1,018
2.04
26,133
24,529
920 1.84
23,609
26,133
490
0.98
25,643
23,609
443 0.89
23,167
Equations
1st Yr. PAN (mg/Kg)=(MR x ('rKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 25,657 51.31 Total 28,133 56.27

Page: 1 of 2
Report Number: 14-087-0206
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
Lab Number: 98641
Sample Id: TA032514
.WWW:aleastern,com
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: 201201.A10-AHOSKIE WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/25/2014 12:30:00
Date Received: 03/28/2014 00:00
Date Reported: 04/03/2014
Total Solids *
3.00
30000
100.0
JM
03/28/2014 13:59
SM-2540G
Moisture "
97.00
100.0
JM
03/28/2014 13:59
SM-2540G
Total Kjeldahl Nitrogen
5.13
51300
10.0
JM
03/31/2014 09:00
SM-4500-NH3C-TKN
Total Phosphorus
2.51
25100
100
KM
03/31/2014 13:30
SW 6010C
Total Potassium
0.50
4960
100
KM
03/31/2014 13:30
SW 6010C
Total Sulfur
0.80
8030
100
KM
03/31/2014 13:30
SW 6010C
Total Calcium
1.69
16900
100
KM
03/31/2014 13:30
SW 6010C
Total Magnesium
0.45
4600
100
KM
03/31/2014 13:30
SW 6010C
Total Sodium
0.57
5690
100
KM
03/31/2014 13:30
SW 6010C
Total Iron
15000
100
KM
03/31/2014 13:30
SW 6010C
Total Aluminum
30400
100,
KM
03/31/2014 13:30
SW 6010C
Total Manganese
313
5
KM
03/31/2014 13:30
SW 6010C
Total Copper
442
5
KM
03/31/2014 13:30
SW 6010C
Total Zinc
1050
5
KM
03/31/2014 13:30
SW 6010C
Ammonia Nitrogen
0.67
6670
10.0
JM
03/31/2014 09:00
SM-4500-NH3C
Organic N
4.46
44630
10.0
03/31/2014 09:00
CALCULATION
Nitrate+Nitrite-N
43.3
2.00
JM
03/31/2014 09:00
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
03/31/2014 13:30
SW 6010C
All values are on a dry weight
basis except as noted by asterisk. Detection limit on all N series
is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced
in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-087-0206
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
y A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richniond, Virginia 23237 (804) 743-94ol Fax (04) 271-w6
wwwaleastem.com
Project: 201201.A10-AHOSKIE WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/25/2014 12:30:00
Lab Number: 98641 Date Received: 03/28/2014 00:00
Sample Id : TA032514 Date Reported: 04/03/2014
Total Chromium
52
5
KM
03/31/2014 13:30
SW 6010C
Total Nickel
24
5
KM
03/31/2014 13:30
SW 6010C
Total Lead
37
5
KM
03/31/2014 13:30
SW 6010C
Total Arsenic
4.0
3.0
KM
03/31/2014 13:30
SW 6010C
Total Mercury
0.8
0.4
KM
03/31/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
03/31/2014 13:30
SW 6010C
pH (Standard Units) "
7.16
2.00
JM
03/31/2014 09:00
SW-9045D
Total Molybdenum
10
5
KM
03/31/2014 13:30
SW 6010C
Soluble Phosphorus
0.11 1100
100
JM
04/01/2014 10:39
SOLUBLE P IN MANURE
Comments:
WATER SOLUBLE P, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Ourreports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

9 Microbac Laboratories, Inc. - Wilson Division
3809 Airport Drive NWicrobace T il: [phone]
r&,diflagte of Analysis Report Date: 29 Apr-2014
SCOTT CARPENTER
SOIL PLUS
208 WILLIAMS ST
GREENVILLE NC 27858
USA
Work Order:
2014-03-31-003
Date Received:
28-Mar-2014
Quote:
23-20140328-14
Sample Description:
Biosolids
Collection
SIDN
Client Marks
Analysis
Method
Date/Time:
Result
AA46175
Town of
Flash Point,Liquids
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
032714
AA46175
Town of
pH (Corrosivity)
Subcontracted
3/27/14
10:30
*See Attached
• Williamston TW .
032714
AA46175
Town of
Reactive Cyanide
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
032714
AA46175
Town of
Reactive Sulfide
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
032714
AA46175
Town of
TCLP,Full (Metals,
Subcontracted
3127/14
10:30
*See Attached
Williamston TW
VOC SVOC Pest @
032714
Herb)
AA46176
Town of Ahoskie A
Flash Point,Liquids
Subcontracted
3/27114
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
pH (Corrosivity)
Subcontracted
3/27114
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
Reactive Cyanide
Subcontracted
3/27114
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
Reactive Sulfide
Subcontracted
3/27/14
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
TCLP,Full (Metals,
Subcontracted
3/27/14
13:30
*See Attached
032714
VOC SVOC Pest @
Herb)
Reviewed and Approved by:Date: / 9 airy
Kim Hesse
For any feedback concerning our services, please contact James Nokes,lsenior Vice President, at [e-mail]
or Trevor Boyce, President, at [e-mail]
Chemical and Microbiological Analysis: Environmental — Agrochemical — Food — Pharmaceuticals
Page 1 of 1

® Microbac Laboratories, Inc.
1 Knoxville Division
505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www microbac.com
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[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY • CONSUMER PRODUCTS •WATER -AIR • WASTES FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
U Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson Date Received: 4/1/2014
3809 Airport Drive Cust #: R9024
Wilson, NC 27896 PO#.
Workorder: 1406051 Project: Soil Sampling
Analyte Result Units oil Qualifier Reporting Analyst Analyzed Method
j Limit
AA46176 Williamston Sampled: 03/27/2014 00:00
I
1406051.01 (Solid)
GCMS Volatiles
Analyzed By: Microbac Laboratories, Inc. - Chicagoland
I 1,1-Dichloroethene ND mg/L 10 H 0.050
jin 04/25/201413:34 1311/8260B
1,2-Dichioroethene ND mg/L 10 H 0.050 jin 04125/201413:34 1311/6260B
2-Butanone ND mg/L 10 H 0.10 jin 041251201413.34 1311/8260B
Benzene ND mg/L 10 H 0.050 jin 04125/201413:34 1311/8260B
r Carbon tetrachloride ND mg/L 10 H 0.050 jin 04/25/201413:34 1311/826oB
Chlorobenzene ND mg/L 10 H 0.050 jin 04/25/201413:34 1311/8260B
Chloroform ND mg/L 10 H 0.050 jin 04/25/201413:34 1311/8260B
Tetrachloroethene ND mg/L 10 H 0.050 jin 04125/201413:34 1311/8260B
Tdchloroethene ND mg1L 10 H 0.050 jin 04125/201413:34 1311/8280B
Vinyl chloride ND mg/L 10 H 0.020 jin 04/25/201413:34 1311/8280B
1,4-Dichlorobenzene ND mg/L 10 H 0.10 jin 04125/201413:34 1311/8260B
' Surrogate: 1,2-Dichloroethane-d4 74.5-132 H 106 % 04125/201413:34 131118260E
Surrogate: 4-Bromofluorobenzene 80-120 H 93.8 % 04/25/201413:34 131118260B
Surrogate: DlbromoBuoromethane 80-120 H 101 % 04/25/201413:34 131118260E
Surrogate., Toluene-0 80-120 H 101 % 04/26/201413:34 131118260E
Wet Chemistry
Analyzed By: Microbac Laboratories, Inc. - Chicagoland
- Reactive Cyanide ND mg/Kg 1 H 2.0 AGRIE 04/16/201413:00 Chapter 719014
Reactive Sulfide ND mg/Kg 1 H 2.0 EB 04/15/201409:15 Chapter7/9034
AA46176 Williamston Sampled: 03/27/2014 00:00
1406051-01RE1 (Solid)
TCLP Metals by 6000/7000 Series Methods
Analyzed By: Microbac Knoxville Division
Silver ND mg/L 1 0.00100 JNB 04116/201421:31 SW8486010B
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406051-02 (Solid)
Wet Chemistry
CThe data and Infonnatlon on this, and other accompanying documents, represent only the sempie(s) analyzed and Is rendered upon condition MEMBER
that R Is not to be reproduced wholly or In pert for advertising or other purposes without approval from the laboratory.
USDA-FPA•NIOSHTesdng Fcad Sanitagon Consufgng Chemical and MlemblologlcalAnalyses and Research
t1
Page 3 of 9
www.microbac.com [e-mail]

® Microbac Laboratories, Inc.
Knoxville Division
®®® 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Microbac Laboratories, Inc. -Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406051 Project Soil Sampling
Date Reported: 4/29/2014
Date Received: 4/1/2014
Cost #. R9024
PO#:
Analyse Result Units Dil Qualifier Reporting Limit Analyst Analyzed Method
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406061-02 (Solid)
Wet Chemistry
Analyzed BY: Microbac Knoxville Division
pH (Corrosivity) 7.3 pH Units 1 H4 SLN 04/09/201416:00 SW846 9045D
General Chemistry
Analyzed BY: Microbac Knoxville Division
Flash Point 121 °F 1 01 • 65 SDF 04/16/201417:27 SW8461010
TCLP Extraction Fluid 1 1 He JNB 04/11/201411:57 SW8461311
TCLP Metals by 6000/7000 Series Methods
Analyzed By: Microbac Knoxville Division
Arsenic
0.0431
mg/L
1
0.0150
JNB
04/11/2014 20:24
SW846 60108
Barium
0.151
mg/L
1
0.00400
JNB
04/11/2014 20:24
SW846 6010E
Cadmium
ND
mgf-
1
0.00750
JNB
04/11/2014 20:24
SW846 6010E
Chromium
ND
mg/L
1
0.00750
JNB
04/11/2014 20:24
SW046 6010E
Lead
ND
mg/L
1
0.0200
JNB
04/11/201420:24
SW84660108
Mercury
ND
mg/L
1
0.000200
JNB
04/15/201410:38
SW846 7470A
Selenium
0.0419
mg/L
1
0.0200
JNB
04/11/2014 20'.24
SW846 6010B
TCLP Semivolatiles by EPA Method 131118270C
Analyzed By: Microbac Knoxville Division
o-Cresol
ND
mg/L
1
0.0385
SLH
04116/201417:58
SW846 8270C
Pyridine
ND
mg1L
1
0.0192
SLH
04/16/201417.58
SW846 8270C
meta/para-Cresol
ND
mglL
1
0.0385
SLH
04/16/2014 17:58
SW846 8270C
Hexachloroethane
ND
mg/L
1
0.0192
SLH
04/16/201417:58
SW846 8270C
Nitrobenzene
ND
mg/L
1
0.0192
SLH
04/16/2014 17:58
SW846 0270C
Hexachlorobutadiene
ND
mg/L
1
0.0192
SLH
04/16/201417:68
SW846 8270C
2,4,6-Trichlorophenol
ND
mg1L
1
0.0192
SLH
04/16/201417:58
SW846 8270C
2,4,5 Trichlorophenol
ND
mg/L
1
0.0192
SLH
04/161201417:58
SW846 8270C
2,4-Dinitrotoluene
ND
mg/L
1
0.0192
SLH
04/161201417:58
SW846 8270C
Hexachlorobenzene
ND
mg/L
1
0.0192
SLH
041161201417:58
SW846 8270C
Pentachlorophenol
ND
mg/L
1
0.154
SLH
04/16/201417:58
SW846 8270C
1,4-Dichiorobenzene
ND
mg/L
1
0.0192
SLH
04/16/201417:58
SW846 8270C
Surrogate: 2-Fluorobiphenyl
10-108
59.0 %
04/16/201417:58
SW846 8270C
The data and Information on this, and other accompanying documents, represent only the somple(s) analyzed and is rendered upon condition
MEMBER
that it Is not to be reproduced wholly or In pad for advertising or other purposes without approval from the laboratory.
USDXEPA•NIOSH Testing
Food Sanitation Consulting
Chemiceland MleroblologicalAnalysee and Research
,r
Page 4 of 9
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Ynoxville Division
®®® 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY • CONSUMER PRODUCTS -WATER • AIR • WASTES; FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Microbac Laboratories, Inc. -Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406051 Project- Soil Sampling
Date Reported: 4129/2014
Date Received: 4/1/2014
Cost #: R9024
Pok
Analyte Result Units Oil Qualifier Reporting Analyst Analyzed Method
Limit
AA46176 Ahoskie Sampled: 63/27/2014 00:00
1406061-02 (Solid)
TCLP Semivolatiles by EPA Method 131118270C
Surrogate., 2-Fluorophenol
10-89.8
31.9 %
04/16/201417:58
SW846 8270C
Surrogate: Nltrobenzene•0
10-107
64.3 %
041161201417:58
SW846 8270C
Surrogate: Phenol-0
10-86.9
29.8 %
04/161201417:58
SW846 8270C
Surrogate., Terphenyl--04
10-111
74.3 %
04/16/201417:58
SW846 6270C
Surrogate.,Z4,6-Tribromophenol
10-126
31.1 %
04/16/201417:58
SW846 8270C
TCLP HERBICIDES
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
2,4-D
ND
ug/L
1
U,H1
20.0
ECL
04/171201420:00
SW8151A
2,4,5-TP (Silvex)
ND
ug/L
1
U, H1
2400
ECL
04/17/2014 20:00
SW8151A
Surrogate. 2,4-Dich/orophenylacetic acid
20-144
56.9 %
04/17/2014 20:00
SW8151A
TCLP Pesticides
Analyzed BY: Microbac Laboratories, Inc. - Ohio Valley
Endrin
ND
ug/L
1
U. H1
0.500
ECL
04117/201422:57
SW8081A
J Lindane
'ND
ug/L
1
U, H1
0.500
ECL
04/17/2014 22:57
SW8081A
Methoxychlor
ND
ug/L
1
U, H1
0.500
ECL
041171201422:57
SWBD81A
Toxaphene
ND
ug/L
1
U, H1
10.0
ECL
04/17/201422:57
SW8081A
-- Chlordane
ND
ug/L
1
U, H1
10.0
ECL
04/17/201422:57
SW8081A
Heptachlor
ND
ug/L
1
U, H1
0.500
ECL
04/17/201422:57
SW8081A
Heptachlor Epoxide
ND
ug1L
1
U, H1
0.500
ECL
04/17/2014 22:57
SW8081A
alpha Chlordane
ND
ug/L
1
U, H1
0.500
ECL
04/171201422:57
SW8081A
gamma Chlordane
ND
ug/L
1
U, H1
0.500
ECL
04/171201422:57
SW8081A
Surrogate:2,4,5,6-Tetrachloro-m-xylene
20-180
35.1 %
041171201422:57
SW8081A
Surrogate: Decachlorobiphenyl
25-140
28.5 %
04/17/2014 22:57
SW8081A
1
I' GCMS Volatiles
J
Analyzed By: Microbac Laboratories, Inc. - Chicagoland
_
1, 1 -Dichloroethene
ND
mg/L
10
H
0.050
jln
041241201413:13
1311/8260D
1,2-Dichloroethane
ND
mg/L
10
H
0.050
jln
04/241201413:13
131118260B
j 2-Butanone
0.22
mg/L
10
H
0.10
jln
041241201413:13
131118260B
Benzene
ND
mg/L
10
H
0.060
jln
04124/201413:13
1311/8280B
Carbon tetrachloride
ND
mg/L
10
H
0.050
jln
04124/201413:13
131118260B
The data and information on this, and other accompanying documents• represent only the sample(s) analyzed and is rendered upon condWon
MEMBER
that It Is not to be reproduced wholly or In pad for advertising or other purposes without approval from the laboratory.
USDA•EPA-MOSH Testing Food
Sanitation Consulting Chemical sod MicroblotoglcatAnelyeas and Research
Page 5 of 9
www.microbac.com
[e-mail]

I
Microbac Laboratories, Inc.
Knoxville Division
®®� 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Faw865.984.8616
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
V [e-mail]
CHEMISTRY • MICROBIOLOGY • FOOD SAFETY- CONSUMER PRODUCTS •WATER • AIR -WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4129/2014
Microbac Laboratories, Inc. - Wilson Date Received: 4/1/2014
3809 Airport Drive Cust #: R9024
Wilson, NC 27896 PO#:
Workorder: 1406051 Project: Soil Sampling
Reporting
Analyte Result Units Dil Qualifier Limit Analyst Analyzed Method
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406051-02 (Solid)
GCMS Volatiles
Chlorobenzene
ND
mg/L
10
H
0.050
jin 04/24/201413:13
131118260E
j Chloroform
ND
mg/L
10
H
0.050
jin 04/24/201413:13
131118260B
Tetrachloroethene
ND
mg/L
10
H
0.050
jin 04/24/201413:13
1311/8280B
Trichloroethene
ND
mg/L
10
H
0.050
jin 04/24/201413:13
1311/8260B
Vinyl chloride
ND
mg/L
10
H
0.020
jin 04/24/201413:13
131118260B
1,4-Dichlorobenzene
ND
mg/L
10
H
0.10
jin 04124/201413:13
131118260E
Surrogate: 1,2-Dichloroethane-d4
74.5-132
H
104 %
04/24/201413:13
131118960B
Surrogate: 4-Bromofluorobenzene
80-120
H
95.2 %
04124/201413:13
1311/8260B
Surrogate: Dibromofluoromethane
80-120
H
102 %
04124/201413:13
131118260E
Surrogate: Toluene-d8
80-120
H
100 %
04/24/201413:13
131118260B
Wet Chemistry
Analyzed By: Microbac Laboratories, Inc. - Chica4oland
^Reactive Cyanide
ND
mg/Kg
1
H
2.0
AGRIE 04/16/201413:06
Chapter7/9014
Reactive Sulfide
ND
mg/Kg
1
H
2.0
EB 04/15/2014 09:15
Chapter 7/9034
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406051-02RE1 (Solid)
TCLP Metals by 600017000 Series Methods
Analyzed By: Microbac Knoxville Division
Silver ND mg/L 1 0.00100 JNB 04/16/201421:37 SW84eeoioB
r
The data and Information an this, and other accompanying documents, represent only the sampte(s) analyzed and Is tendered upon condition MEMBER
that it Is not to be reproduced wholly or In pert for advertising or other purposes without approval from the laboratory.
USDA-EPA-MOSH Testing Food Sanitation Consulting Chemical and MlerobiotogieelAnelyses and Research
Page 6 of 9
www.microbac.com [e-mail]

#
Microbac Laboratories, Inc.
Knoxville Division
®®a 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Microbac Laboratories, Inc, -Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406051 Project: Soil Sampling
Certifications
Date Reported: 4/29/2014
Date Received: 4/1/2014
oust #: R9024
PC7k
Code
Description
Number
Expires
A2LA
A&A ISO/IEC 17025 Env. DoD Testing
3045.02
09/30/2014
A2LA
A2LA ISO/IEC 17025 Biological Testing
3045.01
09/30/2014
A2LAB-KNX
ISO 17025 KNX food
3131.01
05/31/2015
A2LAB-NSH
ISO 17025 NSH food
3131.02
06/30/2014
FL
State of Florida NELAC
E87966
06/30/2014
GA
Georgia Dept Natural Resources
980
04/13/2014
ILDPH
Illinois DOPH Micro analysis of drinking water
1755266
12/31/2016
ILEPA
Illinois EPA wastewater and solid waste analysis
200064
04/01/2015
INDEM
Indiana DEM support lab wastewater and solid waste
A305-9-292
12/31/2013
INDH
Indiana SDH Micro analysis of drinking water
M-45-8
12/31/2016
INSDH
Indiana SDH chemical analysis of drinking water
C-45-03
08/14/2016
KSDOH
Kansas Dept Health & Env. NELAP
E-10397
01/31/2015
KYEPP
Kentucky EPPC analysis Underground Storage Tanks
75
01/3112015
NCENV
NC Environmental
678
12/31/2013
NYDOH
New York State Department of Health Wadsworth
49179
04/01 /2015
NYDOH-1
New York State Department of Health Wadsworth
49386
04/01/2015
PADEP
Pennsylvania Department of Environmental Protect
68-04863
07/31/2014
PEDEP
Pennsylvania DEP Registration for Air analysis
68-04863
TN DW
North Carolina DENR NPDES effluent, surface water
TNNC597
12/31/2014
TN_DW
State of Tennessee
TN02017
04/30/2014
USDA
US Department of Agriculture
11/30/2013
USDAS
USDA Permit To Receive Soil
P330-12-00174
06/2012015
WADOE
Washington State Department of Ecology
C992
10/22/2014
WSDNR
Wisconsin DRN chemical analysis wastewater, solids
998036710
08/31/2014
The data and Inromlaiton on this, and other accompanying documents, represent only the sample(s) analyzed and Is rendered upon condition MEMBER
that h is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory.
USDA•EPA-MOSH Testing Food Sanitaft Consulting chemical and MlemblologicalAmetyses and Research i .L
Page 7 of 9
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Knoxville Division
q,505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 J Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY • MICROBIOLOGY FOOD SAFETY • CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson Date Received: 4/1/2014
3809 Airport Drive Cust M. R9024
Wilson, NC 27896 Pot
_I
Workorder: 1406051 Project Soil Sampling
j Notes
and Definitions
J
U
Not detected at.or above adjusted sample detection limit
R1
Duplicate RPD is outside of acceptance limits.
01
Fiashpoint temperature went up with each of the four tests. Even with vigorous shaking it appears volitile portion lessened
each time.
M5
Post digestion spike is outside of acceptance limits.
M3
Matrix spike recovery is outside of acceptance limits. The post digestion spike recovery Is acceptable.
M2
Matrix spike recovery is outside of acceptance limits, biased low.
He
Sample was analyzed past holding time.
H4 .
The test was performed outside of the EPA recommended holding time of 15 minutes.
H1
[Undefined]
i H
Analyte was prepared and/or analyzed outside of the analytical method holding -time
DET
Analyte DETECTED
ND
Analyte NOT DETECTED at or above the reporting limit
NR
i
Not Reported
dry
Sample results reported on a dry weight basis
RPD
Relative Percent Difference
I ,
The data and Information an this, and other accompanying documents, represent only the sample(s) analyzed and Is rendered upon condition MEMBER
that it Is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.
USDA-EPA•NIOSHTesfing Food Sanitation Consulting Chemical and MlcrobiologlcalAnelysesand Research
I
Page 8 of 9
L www.microbac.com [e-mail]
I

Microbac Laboratories, Inc.
Knoxville Division
S 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tti-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
w CHEMISTRY MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson Data Received: 4/1/2014
— 3809 Airport Drive oust #: R9024
Wilson, NC 27896 Pohl.
Workorder: 1406061 Project: Soil Sampling
Microbac Laboratories, Inc. - Knoxville
a�a ?HMV
Maraea Branner, Project Manager
Thank you for your business. For any feedback, please contact Ashley Morris, at [e-mail]. You may also contact Trevor Boyce,
! President, at [e-mail].
!. As regulatory limits change frequently, Microbac advises the recipient of this report to confirm such limits with the appropriate Federal, state, or local
1 authorities before acting in reliance on the regulatory limits provided.
The date and information an this, and other accompanying documents, represent oNy the sample(s) anaysed and Is rendereQ upon condltlon MEMBER
that h Is not to be reproduced wholly or In pad foradveNsing or other purposes without approval from the laboratory.
USDA-EPA-1,110SHTesting Food SeNlatlan Consulting Chemical and Microblologlcal Analyses and Research
Page 9 of 9
www.microbac.com [e-mail]

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Pcrmit N0. W00035595 Facility Name Granville farms, Inc. Snarce Permit No. WQ000104.9
Laboratory I hinvironment
1, Inc.
Laboratory 2
Sample orCompositeDatc 1/29/2014
Parameter (mg/Kg) Class A Clas li
Aluminum
N/A
N/A
18599
Ammonia Nitrogen
N/A
N/A
4,696
Arsenic 41
— -
75
2.5
Cadmium
39
Calcium
N/A
N/A
1s,342
Copper 1,500
4,300
343
Lead
300
T 840
! 21—
Magnesium
N/A
N/A
4,172
Mercury
17
57
0.49
Molybdenu
N/A
75
5
Nickel. 420
420
16
Nitrate-Nitri[e Nitrogen N/A T
_ N/A
317
PercentSollds! N/A
N/A
1.60
PH (no units)' N/A
^
N/A
Phosphorus N/A
N/A
9,461
Potassium N/A
N/A
6,514
PAN (Inj./Inc.) N/A
N/A
15,431
PAN (Surface) N/A
N/A
13,Us3
Sele in
100
100
5
Sodium
_--_--...
N/A
N/A
7,33+~
SAIL, NSA
N/A
— L6b
TKN N/A
N/A
39,+22
Zinc .` 2,800
�I_
7,500
9�i1
Snvre..Name Gnuuui.wK h1:1U y4'�C 1T
--r cerary, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

r
Facility Contentnea MSD WWTP
L- Sampling Date 1/28/2014
% Solids 1.6
i
Mineralization Rate 0.30
Gallons per DT 14,988.01
PH
FIELD LOADING ESTIMATES
Sodium Absorpotion 1.60 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 39,422 lbs./1,000 gal 5.26
Ammonia Nitrogen (mg/Kg) 4,696.00 lbs./1,000 gal 0.63
Nitrate -Nitrite (mg/Kg) 317.00 lbs./1,000 gal 0.04
PLANT AVAILABLE. NITROGEN SURFACE APPLIED
PAN (mg/Kg) 13,083 lbs./1,000 gal 1.75
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 15,431 lbs./1,000 gal 2.06
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Potassium lbs./1,000 gal .0.87
Phosphorus lbs./1,000 gal 1.26
Calcium lbs./1,000 gal 2.47
Magnesium lbs./1,000 gal 0.56
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
HEAVY METAL CONCENTRATION
HEAVY METAL LOADING
41
75
Arsenic (mg/Kg)
2.50
Arsenic lbs./1,000 gal
0.00
39
85
Cadmium (mg/Kg)
2.50
Cadmium lbs./1,000 gal
0.00
1,500
4,300
Copper (mg/Kg)
343.00
Copper lbs./1,000 gal
0.05
300
840
Lead (mg/Kg)
21.00
Lead lbs./1,000 gal
0.00
17
57
Mercury (mg/Kg)
0.49
Mercury lbs./1,000 gal
0.00
420
420
Nickel (mg/Kg)
16.00
Nickel lbs./1,000 gal
0.00
100
100
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
2,800
7,500
Zinc (mg/Kg)
920.00
Zinc lbs./1,000 gal
0.12
RESIDUAL NITROGEN CALCULATION
f 1 st Year
2nd Year
3rd Year
4th Year
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(-g/kg) (ms/DT)
(mg/Kg)
TKN
(-g/kg) (ms/DT)
(-g/Kg)
39,422
13,083
26.17
26,339
39,422
15,431 30.86
23,991
26,339
3,951
7.90
22,388
23,991
3,599 7.20
20,393
22,388
1,679
3.36
20,709
20,393
1,529 3.06
18,863
20,709
777
1.55
19,933
18,863
707 1.41
18,156
19,933
374
0.75
19,559
18,156
340 0.68
17,815
Equations
1st Yr. PAN (mg/Kg)=OM x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x W/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
i
Total 19,863 39.73
Total 21,607 43.21

PIO,BOX.7085,114 OAKMONT L? iV-E' -
GREENVILLF, N.C. 27835-7085
L_
C.M.S.D. (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON ,NC .28530
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Nitrogen, mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Nitrate Nitrogen(dry wt.), mg/kg
Nitrite Nitrogen(dry wt.), mg/kg
Phosphorus, T. (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
�;__ Wastewater�I�I
Sludge
Analysis
Method
Sample
Date Analyst
Code
18399
02/07/14 LFJ
EPA200.7
<2.5
03/04/14 MEL
311313-04
18542
02/07/14 LFJ
EPA200.7
2.5
03/09/14 MEL
3113B-04
343
02/07/14 LFJ
EPA200.7
28
02/07/14 LFJ
EPA200.7
21
03/03/14 MEL
311313-04
4172
02/07/14 LFJ
EPA200.7
0.49
02/11/14 ADD
245.1 R3-94
16
02/07/14 LFJ
EPA200.7
6514
02/07/14 LFJ
EPA200.7
<5.0
03/10/14 MEL
3113E-04
7334
02/07/14 ADD
3111B-99
920
02/07/14 ADD
3111B-99
39746
02/06114 SEJ
1.6
01/30/14 CMC
2540G-97
39422
02/03/14 ANO
351.2 R2-93
4696
01/30/14 ANO
350.1 R2-93
317
01/31/14 ANO
353.2 R2-93
6.50
01/31/14 AINTO
353.2 R2-93
9461
02/03/14 ALB
365.4 -74
<5.0
02/07/14 LFJ
EPA200.7
PHONE C252) 756-
FAX-(-252) 755-
ID#: 416
DATE COLLECTED: 01/28/14
DATE REPORTED : 03/11/14
REVIEWED BY:

-
May 06, 2014
Deedee Woolard
Environment 1, Inc.
114 Oakmont Dr
P.O. Box 7085
Greenville, NC 27858
TEL: [phone]
FAX: [phone]
RE: C.M.S.D.4/21
Dear Deedee Woolard:
Szonntit'Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls Ohio 44223
TEL: [phone] FAX. [phone]
Website: htty.1Asnv*se11ekcont
Order No.: 14042081
Summit Environmental Technologies, Inc. received 1 sample(s) on 4/22/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arkansas 88.0735, Califomia 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New -Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
OH2O0001, Pennsyhania 68-01335, Rhode island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-I 1-5, Region 8 8TMS-
L, USDAIAPHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia'00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Pagel of 5

Summit Environmental Technologies, Inc.
Workorder
V'A
1,J
LA U
3310 Win St.
Cuyahoga Falls, Ohio 44223
Sample Summary
TEL: [phone] FAX.• [phone]
WO#: 14042081
Website: hQ.1Atqviv.setIekcom
06-Mqv-14
CLIENT:
Environment 1, Inc.
Project:
C.M.S.D. 4/21
Lab Samplell) Client Sample ID Tag No Date Collected
Date Received Matrix
14042081-001
Sludge Sample
4/21/2014 8:50:00 AM
4/22/2014 9:45:00 AM Sludge
F Page 2 of 5

-
S whit Environmental Technologies, Inc.
"
t,.
ri
3310WinSt.
`6� argative
Case Narrative
¢a
i
r1 r' `t <. _ 5,
•, w
Cuyahoga Falls, Ohio 44223
wolk 14042081
4L
T ..
TEL. [phone] FAX., [phone]
Website: htlD://wwia.settekcom
Date: 5/6/2014
�— CLIENT:
Environment 1, Inc.
Project:
C.M.S.D.4/21
This report in its entirety consists of the documents Iisted below. All documents contain the Summit
Environmental Technologies, Inc: Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
-Control---Summary Reports and copies; of the Chain of Custody Documents supplied with'this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 3 of 5

i
Summit Environmental Technologies Inc.
Summit Environmental Technologies Inc.
WO#:
14042081
3310 Win St.
Cuyahoga Falls, Ohio 44223
Date Reported:
5/6/2014
TEL: [phone] FAX [phone]
Company:
Environment 1, Inc.
Website: httn✓iwunp.settekcon:
Address:
114 Oakmont Dr
Greenville NC 27858
Received:
4/22/2014
Project#:
C.M.S.D.4/21
TCLP Metals Analysis (6010)
Client ID#
Lab IID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge Sample
001
4121/2014 TCLP Arsenic(As)
0.50
NO mg/L
Sludge
EPA 6010 C
1
5.0
4/24/2014
WK
Sludge Sample
001
4/21/2014 TCLP Badum(Ba)
5.0
NO mg/L
Sludge
EPA 6010 C
1
100
4/24/2014
WK
Sludge Sample
001
4/21/2014 TCLP Cadmium(Cd)
0.10
NO mg/L
Sludge
EPA 6010 C
1
1.0
4/24/2014
WK
Sludge Sample
- 001
4/21/20i4 TCLP Chromium(Cr)
. 0.20
NO mg/L
Sludge
EPA 6010 C
1
5.0
4/24/2014
WK
Sludge Sample
001
4/21/2014 TCLP Lead(Pb)
0.50
NO mglL
Sludge
EPA 6010 C
1
5.0
4/24/2014
WK
Sludge Sample
001
4/21/2014 TCLP Selenium(Se)
0.50
NO mg/L
Sludge
EPA 6010 C
1
1.0
4/24/2014
WK
Sludge Sample
001
4/21/2014 TCLP Silver(Ag)
0.50
NO mg/L
Sludge
EPA 6010 C
1
5.0
4/24/2014
WK
TCLP Mercury Analysis (1311/7470)
Client -ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Sludge Sample 001 4/21/2014 TCLP Mercury 0.0020 NO mg/L Sludge EPA 7470 A 1 0.20 4/24/2014 ALJ
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected AnaIyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge Sample
001
4/21/2014 Chlordane, total
0.010
NO mg/L
Sludge
EPA 8081 B
1
0.030
4125/2014
JBN
Sludge Sample
001
4/21/2014 Toxaphene
0.10
NO mg/L
Sludge
EPA 8081 B
1
0.50
4/25/2014
JBN
Sludge Sample
001
4/21/2014 Endrin l 0.0020
NO mg/L
Sludge
EPA 8081 B
1
0.020
4/25/2014
JBN
Sludge Sample
001
4/21/2014 gamma-BHC
0.0020
NO mg/L
Sludge
EPA 8081 B
1
0.40
4/25/2014
JBN
Sludge Sample
001
4/21/2014 Heptachlor
0.0020
NO mg/L
Sludge
EPA 8081 -B
1
0.0080
4/25/2014
JBN
Sludge Sample
001
4/21/2014 Heptachlor epoxide
0.0020
NO mg/L
Sludge
EPA 8081 B
1
0.0080
4/25/2014
JBN
Sludge Sample
001 ,
4/21/2014 Methoxychlor
0.0020
NO mg/L
Sludge
EPA 8081 B
1
10
4/25/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge Sample
001
4/21/2014 1,1-Dichloroethene
0.1.0
NO mglL
Sludge
EPA 8260 B
1
0.70
515/2014
MES
Sludge Sample
001
4/21/2014 1,2-Dichloroethane
0.10
NO mg/L
Sludge
EPA 8260 B
1
0.50
515/2014
MES
Sludge Sample
001
4/21/2014 Benzene
0.10
NO mg/L
Sludge
EPA 8260 B
1
0.50
5/5/2014
MES
Sludge Sample
001
4/21/2014 Carbon tetrachloride
0.10
NO mg/L
Sludge
EPA 8260 B
1
0.50
5/5/2014
MES
Sludge Sample
001
412.1/2014 Chlorobenzene
0.10
NO mglL
Sludge
EPA 8260 B
1
100
5/5/2014
MES
Sludge Sample
001
4/21/2014 Chloroform
0.10
NO mg/L
Sludge
EPA 8260 B
1
6.0
5/5/2014
MES
Sludge Sample
001
4/21/2014 Tetrachloroethene
0.10
NO mg/L
Sludge
EPA 8260 B
1
0.70
5/512014
MES
Sludge Sample
001
4/21/2014 Trichloroethene
0.10
NO mg/L
Sludge
EPA 8260 B
1
0.50
5/5/2014
MES
Sludge Sample
001
4/21/2014 Vinyl chloride
0.20
NO mg/L
Sludge
EPA 8260 B
1
0.20
5/5/2014
MES
Sludge Sample
001
4/21/2014 MEK
2.0
NO mg/L
Sludge
EPA 8260 B
1
200
5/5/2014
MES
Page 4 of 5

Summit Environmental Technologies, Inc.
Wp#;
14042081
3310 Win St.
Czryahoga Falls, Ohio 44223
Date Reported:
5/6/2014
TEL: [phone] FAX: [phone]
Company:
Environment 1, Inc.
Website: httP.-Mv%vw.sette%Coni
Address:
114 Oakmont Dr
Greenville NC 27858
Received:
4/22/2014
Project#:
C.M.S.D.4/21
SVOC 8270 TCLP BNA List
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegL,vl
Run
Analyst
Sludge Sample
001
4/21/2014 1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
4/24/2014
AKE
Sludge Sample
001,
4/21/2014 2,4,5 Tdchlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
4/24/2014
AKE
Sludge Sample
001
4/21/2014 2,4,6-Tdchlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
4/2412014
AKE
Sludge Sample
001
4/21/2014 2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
4/24/2014
AKE
Sludge Sample
001
4/21/2014 Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
4/24/2014
AKE
Sludge Sample
001
4/21/2014 Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
4/24/2014
AKE
butadiene
Sludge Sample
001
4/21/2014 Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA-8270 C
1
0.13
4/24/2014
AKE
Sludge Sample
001
4/21/2014 Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
4/24/2014
AKE
Sludge Sample
001
4/21/2014 Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
4/24/2014
AKE
Sludge Sample
001
4121%2014 Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
4/24/2014
AKE
Sludge Sample
001
4/21/2014 Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
4/24/2014
AKE
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge Sample
001 4/2112014. 2,4-D
5.0 ND mg/L
Sludge
EPA 8321 A
1
10
4/25/2014
AMZ
Sludge Sample
001 4/21/2014 2,4,5-TP
0.50 ND mg/L
Sludge
EPA 8321 A
1
1.0
4/25/2014
AidIZ
Page 5 of 5
l

COMN OF ('J'S'l ODN , P% E
I H
I,W� ; Hj 11
(TIENT., -fit, 11
NAIT)GE, & WE'LLS AC
G f.. (I
"Mi"TRA SEWAGE DIS"r.
ms-. I'lUDGEN,
P,O. JIM 47-7
A i A
A
61411,71'ON ��C 285,M)
:,7,
I Q
xvq
41z� 77 V-1
91,
c

Environmpnt 1, Inc.
P.O. Box 7095, 114 Oakmont Dr.
Cyrop.nville. Nr.'2.795k
CHAIN OF CUSTODY RECORD
Page I of I
Phone-(252).756-6208 • Fax [phone]
CLIENT: 416 week: III
C.M.S.D. (SLUDGE & WELLS ACCT)
CONTE4 NTNIIE A METRO. SEWAGE DIST.
MS. RE, NFL, PRXDGIEN
P.O. BOX 477
IFTON.NC-28530
'GP
[phone]
COLLECTION0,
DISINFE.CTION
�j CHLORINE,'
UV
[NONL
:A
U
CHLORINE NEUTRALIZED AT COLLECTION .
pH CHECK (LAB)
-G-
G
G
G
G
CONTAINER TYPE, PIG
A
A
A
A
A
CHEMICAL PRESERVATION
A -NONE D-NAOH
B-HNC, E,HCL
C-HSO, F-' ZINC ACETATE/NAOH
G- NATHIOSULFATE
IL
�_
0)0
E I=
Ld 0
C) 0 �j Q
!;z
Lr
0.
9
i
U3
w
1—
U 0
0
a
U
E-,
:5
a,
U
P4
U
H
. U
H
U
E_
SAMPLE LOCATION
DATE
TIME
Sludge Sample
64m
CLASSIFICATION:
WASTEWATER (NPDES)
DRINKINGWATER
DWQ/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY MAINTAINED
DURING-SHIPMENT/DELIVERY
N
SAMPLES COLLECTED BY,
(Please Print)
SAMPLES RECEIVED IN LAB AT
RELINQUISHED BY (SIG.) (SAMPLER�)
DATE(TIME
RIICEI 8 (SIG.)
y
7z A DATEITIME
COMMENTS:
JAA
ELI��JSSHEAY (SP,
[RElb(NMISHED
D I ME
REC VED BY (SIG..
DAfFJTIME
DATE/TIME
RECEIVED BY (SIG.)
DATFJTIME
PLEASE READ Instructions for completing this form on the reverse side,
Sampler must place a "C" for composite sample or a "G" for "-' 272188
P_k __J, in +j_ kj_t�� k., inn m­k ­,­+_,4 N . i :j

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Pcrmit No. WQ0015595 Facility Name Granville Farms, Inc. Source Permit No. NC0029033
Laboratory 1
Laboratory 2
Sample or CompositeDate
Parameter (mg/Kg) Class A Clas B
City of
Raleigh Newe
City of
italclgll Nellie
City or
Raleigh Nc m
--T/ 13/2014
-2/ 17/2014
8/27/2014
Aluminum
N/A
N/A
I,3,800
15,229
17;323
Ammonia Nitrogen
N/A
N/A
4,841
36,182
_
47,359
Arsenic
Cadmium
�.._ 41.
39
75
- 85
-- 4.6
3.7
4.3
1.7
,4.4
- 4 5
Calcium
N/A
N/A
11,000
12,073
12,795
Copper
Lead
1,500
30.0
4,300
840
416.6
_ 24.8
384.2
-19.1
3.15.1
28
Magnesium
N/A
N/A
3,509 -
4,316
3,922
Mercury
17
I
57
1,56
1.82
0.37
Molybdenum
N/A
75
9.3
9.7
1.3.3
Nickel
420
420
19.3
22
24.6
Nitrate -Nitrite Nitrogen
N/A -
N/A
157
206
174
Percent Solids
N/A
N/A
3.78
2.96
3.37
PH (no units)
N/A
N/A
�N/A
7,38
7.95
9.18
- -- Phosphorus
N/A
56,369
53,446
42,348-
Potassium
N/A
- N/A
4,054
5,682�
6,188
PAN (Inj./Inc.)
N/A
N/A
16,879
48,996
50,293
~ PAN (Surface)
N/A
N/A
14,458
30,905
26,613
Selenium
Sodium
100
N/A
100
N/A
N/A
5
3,165
1.30
6.2
4,695
i.60
512
3,961
1.44
TKN
N/A
N/A
4.1,444
78,209
56,558
Zinc
1 2,800
7,500
705 2
507
1033.4
Source N-ame Neusc River WkV'IT
" I ccrdfy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gath -d and evaluated the information submitted. I am aware that there are significant penalties for
submitdn r alsc inform. n, mcl inin th possibility of fines and imprisonment for knowing violations"
iigutfture of preparer *I'- - Date
*Preparer is defined in 40 CPR Part 5039(r) and 15A NCAC 2T .1102 (26)

� . MA
Facility Neuse River WWI'P
L j Sampling Date 1/13/2014
% Solids 3.78
Mineralization Rate 0.3
Gallons per DT 6,344.13
PH 7.58
I:
FIELD LOADING ESTIMATES
Sodium Absorpotion 1.30 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 44,444 lbs./1,000 gal 14.01
i
Ammonia Nitrogen (mg/Kg) 4,841.27 lbs./1,000 gal 1.53
Nitrate -Nitrite (mg/Kg) 157.00 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 14,458 lbs./1,000 gal 4.56
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 16,879 lbs./1,000 gal 5.32
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Potassium lbs./1,000 gal
1.28
Phosphorus lbs./1,000 gal
17.77
Calcium lbs./1,000 gal
3.47
Magnesium lbs./1,000 gal
1.11
Manganese lbs./1,000 gal
0.21
Sulfur lbs./1,000 gal
0.12
Molybdenum lbs./1,000 gal
0.00
Class A Ceiling
Limits (mg/Kg)
Class B.Ceiling
Limits (mg/Kg)
HEAVY METAL CONCENTRATION
HEAVY METAL LOADING
Arsenic (mg/Kg)
4.60
Arsenic lbs./1,000 gal
0.00
41
75
1 C
39
85
Cadmium (mg/Kg)
3.70
Cadmium lbs./1,000 gal
0.00
I,
1,500
4,300
Copper (mg/Kg)
416.60
Copper lbs./1,000 gal
0.13
300
840
Lead (mg/Kg)
24.80
Lead lbs./1,000 gal
0.01
17
57
Mercury (rug/Kg)
1.56
Mercury lbs./1,000 gal
0.00
420
420
Nickel (mg/Kg)
19.30
Nickel lbs./1,000 gal
0.01
100
100
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
2,800
7,500
Zinc (mg/Kg).
705.20
Zinc lbs./1,000 gal
0.22
RESIDUAL NITROGEN CALCULATION
I
1 st Year
2nd Year
3rd Year
� l
4th Year
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Eg)
TKN
(mg/kg) (lbs/DT)
(mg/Rg)
44,444
14,458 28.92
29,986
44,444
16,879 33.76
27,565
29,986
4,498 9.00
25,488
27,565
4,135 8.27
23,430
25,488
1,912 3.82
23,576
23,430
1,757 3.51
21,673
23,576
884 1.77
22,692
21,673
813 1.63
20,860
22,692
425 0.85
22,267
20,860
391 0.78
20,469
Equations
1st Yr. PAN (mg/Kg)=(MR x CIXN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 22,177 44.35
Total 23,975 47.95

City of Raleigh Neuse River WIN Lab
WW Certification .# 511 EPA Lab Code NC01029
1Laboratory Report of Analysis
IISample Origination: Covered Aerobic Digeste
Date
m G C
Nam'...
U aZ
%
Z
mg/L
Z
mglkg
p
mg/L
+RI O s s
z z
mg/kg mg1L j mg/kg
M
0
Z
mg/L
M
0
Z
mgfkg
o
rn
mgll,
o
W
mg/kg I
Z eva
a
a s
N
mg/L,
Z
a°�.
ate '
N
• mg/kg ''
2.0
a 7
a v�; �
M
mg/L
Z .a
s
ELM
N
mglkg
1/1/2014
1/2/2014
3
113/2014
1/4/2014
1/5/2014
I
1/6/2014
1/7/2014
1/8/2014
'
1/9/2014
I
1/10/2014
1111 /2014
1/12/2014
1/13/2014 ,
CANIC13011314.
3.78;
1,680E44,444
2,131
56,369 183.001 4,841.27
5.940
157
14.591
386
541
14,459
638
16,879
1 /14/2014
1 /16/2014
j
1/16/2014
1/17/2014
1/18/2014
1/19/2014
11
1 /20/2014
1/21/2014
1 /22/2014
1 /23/2014
1/24/2014
1 /25/2014
1'
1/26/2014
1 /27/2014
1/28/2014
f
1/29/2014
'
1/30/2014
1/31/2014
Minimum
Maximum
Average
3.78
3.78
3.78
1,680;
1,680
1,680
44,444
44,444
44,444
2,1311
2,1311
2,131
56,3691 1831 4,841;
56,369 1831 4,841
56,369 183 4,841`
5.940
5.940
5.940
157 15
157 15
157 15
386
386
386
547
547
547.
14,459
14,459
14,459
6381
638
638
16,879
16,879
16,879
DA&d
Darrell Crews Date
Laboratory Supervisor

City of Raleigh Neuse River VVWTP Lab
WW Certification # 51/ EPA Lab Code NC01029
;Laboratory Report of Analysis i
(Sample Origination: Covered Aerobic Digester
Uwm
E
Uti
N>n�wCV
oc m
iLL
�
cC.R
m
�
��
dy
LL ..
m
U.
Date
%
%
%
%
SU
%
Count
counts/G
%
Count
counts/G
1/1/2014
1/2/2014
1/3/2014
1/4/2014
1 /5/2014
1/6/2014
1/7/2014
1/8/2014
1/9/2014
1/10/2014
1/11/2014
i
1 /12/2014
1/13/2014
CAD#1CB011314
CAD#lCB0122140725
76
3.78
61
51
7.58
3.70
<2.00
<54.05
1/14/2014
1 /15/2014
CAD#1 C B011314
CAD#1 CB0122140745
3.72
<2.00
<53.76
1/16/2014 •
CAD=13011314 '
CAD#1 CB0122140755
3:64
<2.00
<54.95
1/17/2014
CAD#1CB011314
CAD#1CB0123140725,
3.66
<2.00.
<54.64
1/18/2014 :
CAD#1 CB011314
CAD#1 CB0123140735
3.66
4.00
109.29
1/19/2014
CAM CB011314
CAD#1 CB0123140745
3.72
4.00
107.53
1/20/2014 '
CAD#1C6011314
CAD#1CB0127140735
3.58
<2.00
<55.87
1 /21 /2014
CAD#1 CB011314
CAD#1 CB0127140745
3.58
2.00
55.87
1/22/2014
CAD#1CB011314
CAD#1CB0127140755
3.64
<2.00
<54.95
1/23/2014
1/24/2014
11 /25/2014
I
1/26/2014
1 /27/2014
1/28/2014
1 /29/2014
1 /30/2014
1/31/2014
Minimum
1 3.781
61
51;
7.58
3.58
<2.00
<53.76
Maximum
1 3.781
61
51
7.581
3.721
4.001
109.29
Average
1 S.781
61
511
7.681
3.661,
<A41
<66.77
I - V
Darrell Crews ate
Laboratory Supervisor

City of'Raleigh Neuse River WWTP Lab
WW Certification # 51/ EPA Lab Code NC01029
Laboratory Report of Analysis
Sample Origination Covered Aerobic digester J
'},
G
PU
V
•�
C
R
d
'd
-
�
00
Date
mglkg
mglkg
mglkg
mglkg
mglkg
mg/kg
mg/kg
mg/kg
mglkg
mglkg
mg/kg
1/l/2014
_
1/2/2014
1/3/2014
1/4/2014
1/5/2014
1/6/2014
1/7/2014
1/8/2014
1/9/2014
1/10/2014
1111/20i 4
1/12/2014
1/13/2014
CAD#lCB011314
13,799.700
283.200
3.700
11,000.400
40.600
4.100
416.600
83,158.500
24.800
3,508.800
652.400
1/14/2014
1/15/2014
J
_
111612014
__
Y
111712014Yw�---
1/18/2014 .
1/19/2014
w
1/20/2014
--
1/21/2014
V22/2014
1/23/2014
--
1/24/2014--
1/2512014
1/26/2014
1/27/2014
1/2812014
1/29/2014
_
1/30/2014
1/31/2014
Minimum
13,799.700
283.200
3.700
11,000.400
40.600
4.100
416.600
83,158.500
24.800
3,508.800
652.400
Maximum
Average
503 Ceiling Cono
13,799.700
13,799.700
283.200
283.200
3.700
3.700
85
11,000.400
11,000.400
40.600
40.600
3000
4.100
4.100
416.600
416.600
43001
83,158.500
83,158.500
24.800
24.800
840
3,508.800
3,508.800
662.400
662.400
503 EQ _
39
1200
1500
_
300
503 %elling Cono
4.35
1.36
9.69
2.95
503 EQ
9.49
3.38
27.77
8.27
I
l�------�
Darrell Crews f�le
Laboratory SupervisOr
I
I
I

City of Raleigh Meuse River WWTP Lab
WW Certification # 51/ EPA Lab Code NC01029
Q
?
z
Date
mglkg
mglkg
mglkg
mglkg
mglkg
1/1/2014
1/2/2014
_ —
1/3/2014
1/4/2014
1/5/2014
1/6/2014
_
iR/2014
1/8/2014 M
_
1/9/2014
1/1012014
1111/2014
1/12/2014
1/13/2014 _
CAD#1CB011314
9.300
_
19.300
4,053.600
8.500
3,165.400
1/14/2014
1/15/2014
1/1612014
111 MO14
1/18/2014
-
1/19/2014
—
1/20/2014
1/21 /2014
--
1122/2014
1/23/2014
1124/2014
_
1/25/2014
1126/2014
112712014
1/28/2014
1/29/2014
1/30/2014
1/31/2014
Minimum
9.300
19.300
4,053.600
8.500
3,166.400
Maximum
9.300
19.300
4,063.600
8.500
3,165.400
Average
9.300
19.300
4,053.600
8.500
3,165.400
603 Ceiling Conc
75
420
503 EQ
17
420
% 503 Ceiling Conc
12.40
4.60
-
% 503 EQ
54.71
4.60
Darrell Crews Date
Laboratory Supervisor

Laboratory Report of Analysis
Sample Origination: Covered Aerobic Digester
c
9
B
_
Date
mglkg
mglkg
mglkg
mglkg
mg/kg
mg/kg
1/1/2014
1/2/2014
1/312414
_
_
1/4/2014
1/6/2014
1/6/2014
1/7/2014
1/8/2014
—
---
1/912014
1/10/2014
1/11/2014
1/12/2014
1/1312014
CAD#1 C8011314
40.900
52.200
705.200
4.600
5.000
1.56
1/14/2014
1/16/2014
1/16/2014
1/17/2014
1/18/2014
1/19/2014
1/20/2014
1/21/2014
—
1/22/2014
1/23/2014
1124/2Q14
1/25/2014
1/26/2014
1/27/2014
1/2812014
1/29/2014
1/30/2014
1/31/2014
Minimum
40.900
52.200
-705.2001
4.600
5.000
Maximum
40.900
62.200
705.200
4.600
5.000
A156
Average
40.900
62.200
705.200
4.600
6.000
603 Ceiling Conc
.7500
.75
100
57
503 EQ
2800
41
100
17
% 503 Ceiling Conc
9.40
6.13
5.00
2.73
% 603 EQ
25.19
11.22
5.00
9.15
Darrell Crews ate
Laboratory Suprvisor

i
Facility Neuse River W W I'P
I �
Sampling Date 2/17/2014
% Solids 2.96
FIELD LOADING ESTIMATES
Mineralization Rate 0.3
Gallons per DT 8,101.63
pH 7.95
Sodium Absorpotion 1.60 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 78,209 lbs./-1,000 gal 19.31
Potassium lbs./1,000 gal
1.40
Ammonia Nitrogen (mg/Kg) 36,182.43 lbs./1,000 gal 8.93
Phosphorus lbs./1,000 gal
13.19
Nitrate -Nitrite (mg/Kg) 206.00 lbs./1,000 gal 0.05
Calcium lbs./1,000 gal
2.98
PLANT AVAILABLE NITROGEN SURFACE APPLIED
Magnesium lbs./1,000 gal
1.07
PAN (mg/Kg) 30,905 lbs./1,000 gal 7.63
Manganese lbs./1,000 gal
0.16
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
PAN (mg/Kg) 48,996 lbs./1,000 gal 12.10
Molybdenum lbs./1,000 gal
0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1stYear
-� 2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
4.30
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.70
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
384.20
Copper lbs./1,000 gal
0.09
Lead (mg/Kg)
19.10
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
1.82
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
22.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
6.20
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
507.00
Zinc lbs./1,000 gal
0.13
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
T%N
(mg/kg) (Ibs/DT).
(.g/Kg)
TKN
(-g/kg) (ibs/DT)
(mg/Kg)
78,209
30,905
61.81
47,304
78,209
48,996 97.99
•29,213
47,304
7,096
14.19
40,208
29,213
4,382 8.76
24,831
40,208
3,016
6.03
37,193
24,831
1,862 3.72
22,968
37,193
11395
2.79
35,798
22,968
861 1.72
22,107
35,798
671
1.34
35,127
22,107
415 0.83
21,693
Equations
1st Yr. PAN (mg/Kg)=(MR x (THIN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/K& 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/K& 5th Yr. TKN x (MR/16)
Total 43,082 86.16
Total 56,516 113.03

City of Ralel-gh Neuse River WW Lab
WW Certification # 51/ EPA Lab Code NC01029
Laboratory Report of Analysis
Sample Origination: Covered Aerobic Digester
211/2014
2/3/2014
215/2014
2/11/2014
2113/2014
TT-
2119/2014
2/21/2014
2/25/2014
2127/2014
82
Darrell Crews --_
Laboratory Supervisor

City of Raleigh Neuse River WWTP Lab
WW Certification # 51 / EPA Lab Code NCO 1029
F
Laboratory Report of Analysis
Sample Origination: Covered Aerobir. Digester
6.1
M
m A
gy
7"Iy
-Z
);:[u
A�
q.,,I: ;t!:)4,,,,!q
j�jjtjqqit pV4rf
,1,,'�,";
1
a
t1nt,x.,:z
C&
--mounts/
dU0Vt:1
Vzt.
2/1/2014
';4
vi;
A
2/312OU
N'
2/5/2014
7 7 7 7
217/2014
r.
2/912014
j,
I
2/11/2014
211312014
Wl..412014,
.3:.
2115/2014
2117/2014
CAD#2CB021714
CAD#2CB0303140736
77
2.96
1 64,
47
7.95
2.76
<2.00
<72.46
<2. 001.1
2/19/2014
CAD#2CB021714
CAD#2CB0303140755
2.82
<2.00
<70.92
2120/2
V- 7t
i4l`
A U:. , ,
�2.
00 . j ,
2/21/2014
CAD#2CB021714
CAD#2CB0304140730
1
2.90
<2.00
<68.97
ru�-B0304140-
MPB52_1..7.1#
�'.,.�CADQC 74
2123/2014
CAD#2CB021714
CAD#2CB0304140750
2.84
<2.00
<70.42
2/2512014
2/2712014
2/2q12 P
iij-
III:-.4.f:.� 71.
it
Minimum
2.96
64
47
7.95
.2.681
<.001
<68.971
2 'S
Average
2.96
64
471
7-951
I el]Iz
____ 311012el�
-15arrDate
Laboratory Supervisor

City of Raleigh Neuse River WWTP Lab
WW Certification # 51/ EPA Lab Code NC01029
Laboratory Report of Analysis
Sample Origination Covered Aerobic Dineste
NO=;
-.•9
`fig90.5-21
g.
,9
2/112014
1 0,
213/2014
2/5/2014
21712OU
21.812014
2/912014
2110/2-014..:.*':'-
6�
2/11/2014
2/12120.14
2113/2014
ao
2/15/2014
M
2/17/2014
CAD#2CB021714
15,228.500
284.900
1.700
12,072.700
25.600
4.400
384.200
70,710.400
19.100,
4,315.500
649.500
2/1912014
2126/201'
212112014
2123/2014
2
212512014
2j 2640 4.-.'
-F
i6
2/2712014
Minimum
15,228.500
284.900
1.700
12,072.700
25.600
4.400
384.200
70,710.400
19.100
4,315.600
649.500
2§..flQ _0.
-.2 -900
, ".
-%�L-
-10-
X�
.0
V
Average
15,228.600
284.900
1.700
12,072.700
25.600
4.400
384.200
70,710.400
19.100
4,315.500
6.49.500
77
503 EQ
39
1200
1600
300
owm
r
--:
kmoofib
% 503 EQ
1 4.361
2.13
25.61
6.371
&1� �arreliw�cre�s��Date �
Laboratory Supervisor

City of Raleigh Neuse River WWTP Lab
WW Certification # 51 / EPA Lab Code NCOI 029
MM
�M
RN
...... . . . . . .
2/1/2014
2/3/2014
214/2014_
215/2014
217/2014
219/2014
2110/2014.* .
2/1112014
211312014
2/14/2014
H­
211512014
2 .1612014,
21171204
CAD#2CB021714
9.700
22.000
5,682.000
9.400
4,695.20D
go 8/2O
?JI 912014"
4.
2121/2014
,Z?J201
2123/2014
.244i2.014.:
?
2/2512014
212712014
2/28/2014---q':
75-
Zq
Minimum
9.700
22.000
5,682.000
9.400
4,695.200
Maximum:::_-Aw
....00
'�.-�Z 9 7
?2-OQQ
Average
9.700
22.000
5,682.000
9.400
4,695.200
503 Geilinj.Conc:'-,:'
0
.5
603 EQ
17
420
%_503.pe Tog
P,24
1% 503 EQ
�Si6l
5.24i
Darrell Crews Date
Laboratory Supervisor

Laboratory Report of Analysis
Sample Origination: Covered Aerobic Digester
Am
M',
M
--J
211/2014
gig
2/312014
215/2014
21712014
21912014
2111/2014
2/12/2 4-_,-j—,4t
2h3/2014
2114t201
j
2/1512014
2116/20
2/1712014
CAD#2CB021714
74.400
39.100
507.000
4.300
6.200
1.82
2119/2014
2121/2014
2/23/2014
2/242014"",t"
212512014
2/Z6t4Qzt4-
2127/2014
212
Y-
Minimum
74.400
39,100
507.000
4.300
6.200
11.82
—7 -40 41* 0
"39.100
607W0
Average
74.400
39.100
507.000
4.300
6.200.
1.82
503'C6Hl6g".C6na.:.-'
-- -75OD
'76
503 EQ
2800
41
100
17
sp-ppill h-j..Conc
% 503 EQ
18.111
10.49
6.20
10.73
'Pavv _V/060v
Darrell Crews Date
Laboratory Suprvisor

'.171:19'J1.I
l
- t FIELD LOADING ESTIMATES
Facility Neuse River W /IP
- Sampling Date 8/27/2014
% Solids 3.37
J Mineralization Rate 0.3
Gallons per DT 7,115.97
PH 9.18
Sodium Absorpotion 1.44 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
1 NITROGEN APPLICATION
C.�
NUTRIENT APPLICATION
TKN (mg/Kg) 56,558 lbs./1,000 gal 15.90
Potassium lbs./1,000 gal
1.74
Ammonia Nitrogen (mg/Kg) 47,359.05 lbs./1,000 gal 13.31
Phosphorus lbs./1,000 gal
11.90
Nitrate -Nitrite (mg/Kg) 174.00 lbs./1,000 gal 0.05
Calcium lbs./1,000 gal
3.60
_ PLANT AVAILABLE NITROGEN SURFACE APPLIED
Magnesium lbs./1,000 gal
1.10
PAN (mg/Kg) 26,613 lbs./1,000 gal 7.48
Manganese lbs./1,000 gal
0.22
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
6.84
PAN (mg/Kg) 50,293 lbs./1,000 gal 14.14
Molybdenum lbs./1,000 gal
0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
.39
85
1,500
4,300
300
840
17
57
420
100
k
2,800
1stYear
2nd Year
3rd Year
4th Year
5th Year
420
100
7,500
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
4.40
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
4.50
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
345.10
Copper lbs./1,000 gal
0.10
Lead (mg/Kg)
28.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.37
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
24.60
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
5.20
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
1033.40
Zinc lbs./1,000 gal
' 0.29
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (Ibs/DT)
(mg/Kg)
TKN
(-g/kg) (lbs/DT)
(-g/Kg)
56,558
26,613
53.23
29,945
56,558
50,293 100.59
6,265
29,945
4,492
8.98
25,453
6,265
940 1.88
5,325
25,453
1,909
3.82
23,544
5,325
399 0.80
4,926
23,544
883
1.77
22,661
4,926
185 . 0.37
4,741
4661
425
0.85
22,236
4,741
89 0.18
4,652
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 34,322 68.64
Total 51,906 103.81

City of Raleigh Neuse River WWTP Lab
WW Certification # 51/ EPA Lab Code NC01029
August 2014
Laboratory Report of Analysis
Sample Origination: =overed Aerobic Digester
Date
Class B Batch ID
# Fecal
Class B Fecal Grab
Times
Digester
g
Feed VS
Average
%
Class B
TS
%' /
V
Class B
VS
°�
Volatile
Cone
Reduction
%
v
Class B
pH
SU
'. Class B
TS Fecal
%
Class B
MPN
Count
~Class B
Fecal Col':
counts/G
Class B';
TS Fecal
% , :
• . Glass B
MP_N
mpn
Class B,.
Fecal Col
8/27/2014
CAD#4CB082714
CAD#4CB0902140733
77
3.37
56
62
9.18
3.26
<2.00
<61.35
8/28/2014 `
CAD#4CB082714
CAD#4CB0902140743
3.26
<2.00
<61.35
8/29/2014
CAD#4CB082714
CAD#4CB0902140753
3.38
<2.00
<59.17
8/30/2014
CAD#4CB082714
CAD#4CB0902140803
3.22
<2.00
<62.11
8/31/2014
CAD#4CB082714
CAD#4CB0903140735
3.88
<2.00
<51.55
9/1/2014
CAD#4CB082714
CAD#4CB0903140745
3.92
<2.00
<51.02
9/2/2014
CAD#4CB082714
CAD#4CB0903140755
4.10
<2.00
<48.78
9/3/2014
Maximum
77
3.37
56
62
9.18
4.10
<2.00
<62.11
Total
77
3.37
56
62
9.18
25.02
<14.00
<395.33
iAverage
77
3.37
56
62
9.18
3.57
<2.00
<56.48
Geo Mean
77
3.37
56
62
9.18
3.56
<2.00
<56.22

City of Raleigh Neuse River WW Lab
WW Certification # 51/ EPA Lab Code NCO1029
Laboratory Report of Analysis
iSample Origination: Covered Aerobic Digester
o
msw
Ro
v a z
N
F-
Y
Y.
`S.c
of
i-,;a
o
o=
F..a,
=
z
=
z
r+i
O
Z
r+i
O
z
00
0
N
d
Q t
CL
d
zQIt
a
d
Q'�
nN
d
Q � .;
s
Date
"/o :
mg/L
mg/kg
mg/L
mglkg
mg/L
mg/kg
mg/L
mg/kg
mg/L
mg/kg
mg[L
mg/kg
mg/L ,
mg/kg ,
8/1 /2014
8/2/2014
8/3/2014
8/4/2014 '
8/5/2014
8/6/2014
8!7/2014
8l8/2014
8/9/2014
8/10/2014
8/11 /2014
8/1212014
8/13/2014
8/1412014
8/15/2014
8116/2014
c
8/17/2014
_
8/18/2014
8/19/2014
8/20/2014
8/21 /2014
8/22/2014
8/23/2014
$/24/2014
8/25/2014
8l26/2014
8/27l2014
CAD#4C6082714
3.37
1,906
__
6,558
1,427
348
1,596.00
47,359.05
5.880
4
820,12
24,336
897
26,614
1,695
50,293
8/28/2014
8/29/2014
8/30/2014
8/31 /2014
Minimum
3.37
1,906
56,558
1,427
42,348
1,596
47.359
5.880
174
820
24,336
897
26,614
1,695
50,293
Maximum
3.37
1,906
56,558
1,427
42,348
1,596
47,359
5.880
174
820
24,3361
8971
26,614
1,695
50,293
Average
3.371
1,9061
56,558
1,427
42.348
1,596
47,359
5.880
174
820
24,336
897
26,614
1,695
50,293
Darrell Crews Date
Laboratory Supervisor

Laboratory Report of Analysis
Sample Origination: Covered Aerobic Digester
U
Date
mgikg
" mglkg
mgikg
mglkg-
mg/kg _
mg/kg.
8/1/2014
8/2/2014
8/3/2014
8/4/2014
-
8/5/2014
8/6/2014
8/7/2014
8/8/2014
8/9/2014
8/10/2014
8/11/2014
8/12/2014
8/13/2014
8/14/2014
8/15/2014
8/16/2014
8/17/2014
8/18/2014
8/1912014
8/20/2014
-
8/21/2014
8/22/2014
8/23/2014
8/24/2014
8/25/2014
8/26/2014
8/27/2014
CADil4CB082714
99.0W
43.500
1,033.400
4.400
5.200
0.37
8128/2014
_
8/29/2014
8/30/2014 .
8/31/2014
Minimum
99.000
43.500
1.033.400
4.400
5.200
0.37
Maximum
.99.000
43.500
1,033.400
. 4.400
'5.200
' - _ 0.37
Average
99.000
43.500
1,033.400
4.400
5.200
0.37
503 Ceiling Cone -
7500
7.5
100
57
503 EQ
2800
41
100
17
% 603 Ceiling Conc
_
13.78
,::":;`5.87
5.20
. '_: 0.66
% 503 EQ
36.91
10.73
5.20
2.20
Darrell Crews Date
Laboratory Suprvisor

City of Raleigh Neuse River WWTP Lab
WW Certification # 51/ EPA Lab Code NCO1029
U .
Date
mg/kg
mgikg `-
mg/kg :__
: - mg/kg- _
mg/kg
8/1/2014
8/2/2014
8/3/2014
8/4/2014
815/2014
8/6/2014
8/7/2014
8/8/2014
8l9/2014
8/10/2014
8/1112014
8/12/2014
8/13/2014
8/14/2014
8/15/2014
8/16/2014
8/1712014
8/18/2014
8/19/2014
8/20/2014
8/21/2014
8/22/2014
8/23/2014
8/24/2014
8/25/2014
8/26/2014
8/27/2014
CAD#4CB082714
13.300
24.600
6,187.500
15.400
3,961.300
8/28/2014
8/29/2014
8/30/2014
8/31/2014
Minimum
13.300
24.600
6,187.500
15.400
3,961.300
Maximum
13.300
24.600
6.187.500
15.400
3,961.300
Average
13.300
24.600
6,187.500
15.400
3,961.300
603 Ceiling Conc
= 75
420
503 EQ
17
420
%.503 Ceiling Con;
_
.17.73
.5.86
: -
% 503 EQ
78,24
5,86
44,vtUi 1�12,07 y
Darrell Crews Date
Laboratory Supervisor

City of Raleigh Neuse River WWTP Lab
WW Certification # 51/ EPA Lab Code NCO1029
Laboratory Report of Analysis
Sample Origination Covered Aerobic Digester
ca �
•o
a
•a,
•g
a
"-
d
Ir
i8
- .� .
Date
mg/kg
mglkg
mglkg
mg/kg
mglkg'
mg/kg
-mglkg .
mglkg
mglkg
_ mg/kg _
, mg/kg
8/1/2014
8/2/2014
8/3/2014
814/2014
8/5/2014
8/6/2014
8/7/2014
8/8/2014
8/9/2014
8/10/2014
8/11/2014
8/12/2014
8/13/2014
8/14/2014
8/15/2014
8/16/2014
8/1712014
8118/2014
8/19/2014
8/20/2014
8/21/2014
8/22/2014
-
8/23/2014
8/24/2014
8/25/2014
8/26/2014
8/27/2014
CAD#4CB082714
17,322.500
513.800
4.500
12,794.900
29.000
5.200
345.100
84,815.500
28.600
3,921.600
770.700
8/28/2014.
8/29/2014
8/30/2014
8/31/2014
Minimum
17,322.500
513.800
4.500
12,794.900
29.000
5.200
345.100
84,815.500
28.000
3,921.600
770.700
Maximum
17,322.500
513.800
4.500
12,794.900
29.000
5.200
345.100
84,815.500
28,000
3,921.600
. 770.700
Average
17,322.500
513.800
4.500
12,794.900
29.000
5.200
345.100
84,815.500
28.000
3,921.600
770.700
503 Ceiling Conc
85
_;
3000
-
A300
840
503 EQ
39
1200
1500
300
% 503 Ceiling Conc
5,29
_ . -. -
0.97
8.03
3.33
* 503 EQ
11.54
2.42
23.01
9.33
Darrell Crews Date
Laboratory Supervisor

RY,O)URA 6 OF C H ❑'1 C E
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Emily Fentress
City of Raleigh Neuse River WWTP
PO Box 590
Raleigh, NC 27602
Report Summary
Monday June 16, 2014
Report Number: L683721
Samples Received: 02/19/14
Client Project:
Description: TCLP Sampling
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have an
questions regarding this data package, please do not hesitate to caly
l.
Entire Report Reviewed By: 6� at4't4w.
T. Alan Harvill , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA.- 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN-•047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 10

OESC
I
Emily Fentress
City of Raleigh Neuse River WWTP
PO Box 590
Raleigh, NC 27602
Case Narrative
Monday June 16; 2014,
Report Number: L683721"
Samples Received: 02/19/14
Client Ptoject:
Descri tion: TCLP Sampling
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Other Comments
L683721-01 in CORR WG707879. The pH was taken using 2 times the
normal amount of water to suspend the sample due to hydroscopic
nature of the field sample.
Page 2 of 10

OESC
I
REPORT OF ANALYSIS
Emily Fentress
City of Raleigh Neuse River WWTP
PO BOX 590
Raleigh, NC 27602
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
June 16,2014
ESC Sample # : L683721-01
Date Received February 19, 2014
Description TCLP Sampling
Site ID
Sample ID DEWATERED PRIMARY
Project
Collected By Fentress
Collection Date 02/17/14 14:00
Parameter
Result Det. Limit
Units
Limit
Method
Date/Time By
Dil
Corrosivity Non-Corrosiv
9045D
02/26/14
1121 SDC
1
Ignitability See
Footnote
Deg. F
D93/101
02/25/14
1643 DR
1
Reactive CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B
02/23/14
1207
1
Reactive Sulf.(SW846 7.3.4.1)
BDL
25.
mg/kg
9034/90
02/22/14
1651 AS
1
TCLP Extraction
-
1311
02/20/14
0710 MVE
1
Mercury
BDL
0.0010
mg/1
0.20
7470A
02/20/14
2104 CCE
1
Arsenic
BDL
0.050
mg/l
5.0
6010B
02/22/14
0815 JDG
1
Barium
BDL
0.15
mg/l
100
6010B
02/22/14
0815 JDG
1
Cadmium
BDL
0.050
mg/l
1.0
6010B
02/22/14
0815 JDG
1
Chromium
BDL
0.050
mg/1
5.0
6010B
02/22/14
0815 JDG
1
Lead
BDL
0.050
mg/l
5.0
6010B
02/22/14
0815 JDG
1
Selenium
BDL
0.050
mg/l
1.0
6010B
02/22/14
0815 JDG
1
Silver
BDL
0.050
mg/l
5.0
6010B
02/22/14
0815 JDG
1
TCLP ZHE Extraction
-
1311
02/22/14
0709 MVE
1
TCLP Volatiles
Benzene
BDL
0.050
mg/1
0.50
8260B
02/22/14
1532 RB
1
Carbon tetrachloride
BDL
0.050
mg/l
0.50
8260B
02/22/14
1532 RB
1
Chlorobenzene
BDL
0.050
mg/l
100
8260B
02/22/14
1532 RB
1
Chloroform
BDL
0.25
mg/1
6.0
8260B
02/22/14
1532 RB
1
,1,2-Dichloroethane
BDL
0.050
mg/l
0.50
8260B
02/22/14
1532 RB
1
1,1-Dichloroethene
BDL
0.050
mg/1
0.70
8260B
02/22/14
1532 RB
1
2-Butanone (MEK)
BDL
0.50
mg/l
200
8260B
02/22/14
1532 RB
1
Tetrachloroethene
BDL
0.050
mg/l
0.70
8260B
02/22/14
1532 RB
1
Trichloroethene
BDL
0.050
mg/1
0.50
8260B
02/22/14
1532 RB
1
Vinyl chloride
BDL
0.050
mg/l
0.20
8260B
02/22/14
1532 RB
1
Surrogate Recovery
Toluene -dB
105.
% Rec.
114.
8260B
02/22/14
1532 RB
1
Dibromofluoromethane
ill.
% Rec.
125.
8260B
02/22/14
1532 RB
1
a,a,a-Trifluorotoluene
103.
% Rec.
114.
8260B
02/22/14
1532 RB
1
4-Bromofluorobenzene
93.4
% Rec.
128.
8260B
02/22/14
1532 RB
1
TCLP Pesticides
Chlordane
BDL
0.0050
mg/l
0.030
8081A
02/21/14
1547 CBB
1
Endrin
BDL
0.0050
mg/l
0.020
8081A
02/21/14
1547 CBB
1
Heptachlor
BDL
0.0050
mg/l
0.0080
8081A
02/21/14
1547 CBB
1
L683721-01 (IGNITABILITY) - did not ignite @ 170F
Page 3 of 10

12065 Lebanon Rd.
Mt. Juliet, TN 37122
E S C
[phone]
1-800-767-5859
Fax (615)
758-5859
L•A-8 S•C•!•E-N-C-E•5
Tax I.D.
62-0814289
-
Est. 1970
REPORT OF ANALYSIS
Emily Fentress
June
16,2014
City of Raleigh Neuse River WWTP
PO Box 590
Raleigh, NC 27602
ESC
Sample
# L683721-01
' Date Received February 19, 2014
Description TCLP Sampling
Site ID
Sample ID DEWATERED PRIMARY
Project
Collected By Fentress
Collection Date 02/17/14 14:00
Parameter
Result
Det. Limit
Units
Limit
Method
Date/Time By
Dil
Lindane
BDL
0.0050
mg/l
0.40
8081A
02/21/14
1547 CBB
1
Methoxychlor
BDL
0.0050
mg/1
10.
8081A
02/21/14
1547 CBB
1
Toxaphene
BDL
0.010
mg/l
0.50
8081A
02/21/14
1547 CBB
1
Surrogate Recovery
Decachlorobiphenyl
93.7
% Rec.
123.
8081A
02/21/14
1547 CBB
1
Tetrachloro-m-xylene
80.3
% Rec.
114.
8081A
02/21/14
1547 CBB
1
TCLP Herbicides
- 2,4,5-TP (Silvex)
BDL
0.0020
mg/1
1:0
8151A
02/25/14
2020 KLM
1
2,4-D
BDL
0.0020
mg/l
10.
8151A
02/25/14
2020 KLM
1
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
59.3
Rec.
8151A
02/25/14
2020 KLM
1
TCLP Semi-Volatiles
I 1,4-Dichlorobenzene
BDL
0.10
mg/l
7.5
8270D
02/23/14
0831 KMF
1
l 2,4-Dinitrotoluene
BDL
0.10
mg/l
0.13
8270D
02/23/14
0831 KMF
1
-' Hexachlorobenzene
BDL
0.10
mg/l
0.13
8270D
02/23/14
0831 KMF
1
Hexachloro-1,3-butadiene
BDL
0.10
mg/l
0.50
8270D
02/23/14
0831 KMF
1
Hexachloroethane
BDL
0.10
mg/l
3.0
8270D
02/23/14
0831 KMF
1
Nitrobenzene
BDL
0.10
mg/l
2.0
8270D
02/23/14
0831 KMF
1
Pyridine
BDL
0.10
mg/l
5.0
8270D
02/23/14
0831 KMF
1
�3&4-Methyl Phenol
0.11
0.10
mg/l
400
8270D
02/23/14
0831 KMF
1
-r 2-Methylphenol
BDL
0.10
mg/l
200
8270D
02/23/14
0831 KMF
1
Pentachlorophenol
BDL
0.10
mg/1
100
8270D
02/23/14
0831 KMF
1
2,4,5-Trichlorophenol
BDL
0.10
mg/1
400
8270D
02/23/14
0831 KMF
1
2,4,6-Trichlorophenol
BDL
0.10
mg/1
2.0
8270D
02/23/14
0831 KMF
1
Surrogate Recovery
2-Fluorophenol
26.4
o Rec.
87.0
8270D
02/23/14
0831 KMF
1
Phenol-d5
22.9
% Rec.
67.0
8270D
02/23/14
0831 KMF
1
Nitrobenzene-d5
58.3
% Rec.
120.
8270D
02/23/14
0831 KMF
1
2-Fluorobiphenyl
72.5
% Rec.
122.
8270D
02/23/14
0831 KMF
1
i 2,4,6-Tribromophenol
46.5
o Rec.
148.
8270D
02/23/14
0831 KMF
1
p-Terphenyl-dl4
82.8
% Rec.
149.
8270D
02/23/14
0831 KMF
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum Contaminant Level as established by the US EPA
L Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 02/26/14 16:54 Revised: 06/16/14 08:58
L683721-01 (IGNITABILITY) - did not ignite @ 170F
Page 4 of 10

OESC
I
REPORT OF ANALYSIS
Emily Fentress
City of Raleigh Neuse River WWTP
PO Box 590
Raleigh, NC 27602
June 16,2014
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
ESC Sample
# L683721-02
Date Received February 19,
2014
Description TCLP Sampling
Site ID
Sample ID CLASS A-RALEIGH PLUS
Project
Collected By Fentress
Collection Date 02/17/14 09:50
'
Parameter
Result Det. Limit
Units
Limit
Method
Date/Time By
Dil
Corrosivity
Non-Corrosiv
9045D
02/26/14
1121 SDC
1
Ignitability
See Footnote
Deg. F
D93/101
02/25/14
1643 DR
1
Reactive CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B
02/23/14
1209
1
Reactive Sulf.(SW846 7.3.4.1)
BDL
25.
mg/kg
9034/90
02/22/14
1651 AS
1
TCLP Extraction
-
1311
02/20/14
0710 MVE
1
Mercury
BDL
0.0010
mg/l
0.20
7470A
02/20/14
2127 CCE
1
Arsenic
BDL
0.050
mg/1
5.0
6010B
02/25/14
0023 WBD
1
Barium
0.60
0.15
mg/l
100
6010B
02/25/14
0023 WBD
1
Cadmium
BDL
0.050
mg/1
1.0
6010B
02/25/14
0023 WBD
1
Chromium
BDL
0.050
mg/1
5.0
6010B
02/25/14
0023 WBD
1
Lead
BDL
0.050
mg/1
5.0
6010B
02/25/14
0023 WBD
1
Selenium
BDL
0.050
mg/1
1.0
6010B
02/25/14
0023 WBD
1
Silver
BDL
0.050
mg/l
5.0
6010B
02/25/14
0023 WBD
1
TCLP ZHE Extraction
-
1311
02/22/14
0709 MVE
1
TCLP Volatiles
Benzene
BDL
0.050
mg/l
0.50
8260B
02/22/14
1549 RB
1
Carbon tetrachloride
BDL
0.050
mg/1
0.50
8260B
02/22/14
1549 RB
1
Chlorobenzene
BDL
0.050
mg/l
100
8260B
02/22/14
1549 RB
1
Chloroform
BDL
0.25
mg/1
6.0
8260B
02/22/14
1549 RB
1
1,2-Dichloroethane
BDL
0.050
mg/l
0.50
8260B
02/22/14
1549 RB
1
1,1-Dichloroethene
BDL
0.050
mg/1
0.70
8260B
02/22/14
1549 RB
1
2-Butanone (MEK)
BDL
0.50
mg/l
200
8260B
02/22/14
1549 RB
1
Tetrachloroethene
BDL
0.050
mg/1
0.70
8260B
02/22/14
1549 RB
1
Trichloroethene
BDL
0.050
mg/l
0.50
8260B
02/22/14
1549 RB
1
Vinyl chloride
BDL
0.050
mg/l
0.20
8260B
02/22/14
1549 RB
1
Surrogate Recovery
Toluene-d8
105.
% Rec.
114.
8260B
02/22/14
1549 RB
1
Dibromofluoromethane
108.
% Rec.
125.
8260B
02/22/14
1549 RB
1
a,a,a-Trifluorotoluene
104.
% Rec.
114.
8260B
02/22/14
1549 RB
1
4-Bromofluorobenzene
91.5
% Rec.
128.
8260B
02/22/14
1549 RB
1
TCLP Pesticides
Chlordane
BDL
0.0050
mg/1
0.030
8081A
02/21/14
1559 CBB
1
Endrin
BDL
0.0050
mg/1
0.020
8081A
02/21/14
1559 CBB
1
Heptachlor
BDL
0.0050
mg/l
0.0080
8081A
02/21/14
1559 CBB
1
L683721-02 (IGNITABILITY) - did not ignite @ 170F
Page 5 of 10

12065 Lebanon Rd.
Mt. Juliet, TN 37122
OESC
[phone]
1-800-767-5859
Fax (615)
758-5859
L•A•B S•G•!•E-N-C-E•S
Tax I.D.
62-0814289
Est. 1970
REPORT OF ANALYSIS
Emily Fentress
June
16,2014
City of Raleigh Neuse River WWTP
PO Box 590
Raleigh, NC 27602
ESC
Sample
# L683721-02
Date Received February 19, 2014
Description TCLP Sampling
Site
ID
Sample ID CLASS A-RALEIGH
PLUS
Project
Collected By Fentress
Collection Date 02/17/14 09:50
Parameter
Result
Det. Limit
Units
Limit
Method
Date/Time By
Dil
Lindane
BDL
0.0050
mg/l
0.40
8081A
02/21/14
1559 CBB
1
Methoxychlor
BDL
0.0050
mg/l
10.
8081A
02/21/14
1559 CBB
1
Toxaphene
BDL
0.010
mg/l
0.50
8081A
02/21/14
1559 CBB
1
Surrogate Recovery
Decachlorobiphenyl
86.0
% Rec.
123.
8081A
02/21/14
1559 CBB
1
Tetrachloro-m-xylene
79.2
% Rec.
114.
8081A
02/21/14
1559 CBB
1
TCLP Herbicides
2,4,5-TP (Silvex)
BDL
0.0020
mg/l
1.0
8151A
02/25/14
2034 KLM
1
2,4-D
BDL
0.0020
mg/l
10.
8151A
02/25/14
2034 KLM
1
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
77.4
% Rec.
8151A
02/25/14
2034 KLM
1
TCLP Semi-Volatiles
1,4-Dichlorobenzene
BDL
0.10
mg/l
7.5
8270D
02/23/14
0854 KMF
1
2,4-Dinitrotoluene
BDL
0.10
mg/l
0.13
8270D
02/23/14
0854 KMF
1
Hexachlorobenzene
BDL
0.10
mg/l
0.13
8270D
02/23/14
0854 KMF
1
Hexachloro-1,3-butadiene
BDL
0.10
mg/1
0.50
8270D
02/23/14
0854 KMF
1
Hexachloroethane
BDL
0.10
mg/l
3.0
8270D
02/23/14
0854 KMF
1
Nitrobenzene
BDL
0.10
mg/1
2.0
8270D
02/23/14
0854 KMF
1
Pyridine
BDL
0.10
mg/l
5.0
8270D
02/23/14
0854 KMF
1
3&4-Methyl Phenol
BDL
0.10
mg/1
400
8270D
02/23/14
0854 KMF
1
2-Methylphenol
BDL
0.10
mg/l
200
8270D
02/23/14
0854 KMF
1
Pentachlorophenol
BDL
0.10
mg/l
100
8270D
02/23/14
0854 KMF
1
2,4,5-Trichlorophenol
BDL
0.10
mg/l
400
8270D
02/23/14
0854 KMF
1
2,4,6-Trichlorophenol
BDL
0.10
mg/1
2.0
8270D
02/23/14
0854 KMF
1
Surrogate Recovery
2-Fluorophenol
35.2
% Rec.
87.0
8270D
02/23/14
0854 KMF
1
Phenol-d5
29.9
% Rec.
67.0
8270D
02/23/14
0854 KMF
1
Nitrobenzene-d5
68.5
% Rec.
120.
8270D
02/23/14
0854 KMF
1
2-Fluorobiphenyl
79.3
% Rec.
122.
8270D
02/23/14
0854 KMF
1
2,4,6-Tribromophenol
77.8
% Rec.
148.
8270D
02/23/14
0854 KMF
1
p-Terphenyl-dl4
84.9
% Rec.
149.
8270D
02/23/14
0854 KMF
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum Contaminant Level as'established by the US EPA
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 02/26/14 16:54 Revised: 06/16/14 08:58
L683721-02 (IGNITABILITY) - did not ignite @ 170F
Page 6 of 10

12065 Lebanon Rd.
Mt. Juliet, TN 37122
-
OESC
(615) 758-5B58
1-800-767-5859
Fax (615)
758-5859
L•A-8 S-G•1•E•N-G•E•S
Tax I.D.
62-0814289
_ m
Est. 1970
REPORT
OF ANALYSIS
Emily Fentress
June
16,2014
City of Raleigh Neuse River WWTP
PO Box 590
Raleigh, NC 27602
ESC
Sample
# L683721-03
Date Received February 19,
2014
Description TCLP Sampling
Site
ID
Sample ID CLASS B-CADlCB11314
Project
Collected By Fentress
Collection Date 02/17/14 09:30
.Parameter
Result Det. Limit
Units
Limit
Method
Date/Time
By
Dil
CorTosivity
Non-torrosiv
9045D
02/26/14
1121
SDC
1
Ignitability
See Footnote
Deg. F
D93/101
02/25/14
1643
DR
1
Reactive CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B
02/23/14
1210
1
Reactive Sulf.(SW846 7.3.4.1)
BDL
25.
mg/kg
9034/90
02/22/14
1651
AS
1
TCLP Extraction
-
1311
02/20/14
0710
MVE
1
Mercury
BDL
0.0010
mg/1
0.20
7470A
02/20/14
2107
CCE
1
Arsenic
BDL
0.050
mg/l
5.0
6010B
02/20/14
2349
ST
1
Barium
BDL
0.15
mg/l
100
6010B
02/20/14
2349
ST
1
Cadmium
BDL
0.050
mg/l
1.0
6010B
02/20/14
2349
ST
1
Chromium
BDL
0.050
mg/l
5.0
6010B
02/20/14
2349
ST
1
Lead
BDL
0.050
mg/1
5.0
6010B
02/20/14
2349
ST
1
Selenium
BDL
0.050
mg/1
1.0
6010B
02/20/14
2349
ST
1
Silver
BDL
0.050
mg/l
5.0
6010B
02/20/14
2349
ST
1
TCLP ZHE Extraction
-
1311
02/22/14
0709
MVE
1
TCLP Volatiles
Benzene
BDL
0.050
mg/l
0.50
8260B
02/22/14
1607
RB
1
Carbon tetrachloride
BDL
0.050
mg/l
0.50
8260B
02/22/14
1607
RB
1
Chlorobenzene
BDL
0.050
mg/1
100
8260B
02/22/14
1607
RB
1
Chloroform
BDL
0.25
mg/l
6.0
8260B
02/22/14
1607
RB
1
1,2-Dichloroethane
BDL
0.050
mg/l
0.50
8260B
02/22/14
1607
RB
1
1,1-Dichloroethene
BDL
0.050
mg/1
0.70
8260B
02/22/14
1607
RB
1
2-Butanone (MEK)
BDL
0.50
mg/l
200
8260B
02/22/14
1607
RB
1,
Tetrachloroethene
BDL
0.050
mg/1
0.70
8260B
02/22/14
1607
RB
1
Trichloroethene
BDL
0.050
mg/1
0.50
8260B
02/22/14
1607
RB
1
Vinyl chloride
BDL
0.050
mg/l
0.20
8260B
02/22/14
1607
RB
1
Surrogate Recovery
Toluene-d8
106.
% Rec.
114.
8260B
02/22/14
1607
RB
1
Dibromofluoromethane
106.
% Rec.
125.
8260B
02/22/14
1607
RB
1
a,a,a-Trifluorotoluene
99.3
% Rec.
114.
8260B
02/22/14
1607
RB
1
4-Bromofluorobenzene
90.7
% Rec.
128.
8260B
02/22/14
1607
RB
1
TCLP Pesticides
Chlordane
BDL
0.0050
mg/l
0.030
8081A
02/21/14
1612
CBB
1
Endrin
BDL
0.0050
mg/l
0.020
8081A
02/21/14
1612
CBB
1
Heptachlor
BDL
0.0050
mg/l
0.0080
8081A
02/21/14
1612
CBB
1
L683721-03 (IGNITABILITY) - did not ignite @ 170F
Page 7 of 10

OESC
t
REPORT OF ANALYSIS
Emily Fentress
City of Raleigh Neuse River WWTP
PO Box 590
Raleigh, NC 27602
Date Received February 19, 2014
Description TCLP Sampling
Sample ID CLASS B-CADlCB11314
Collected By Fentress
Collection Date 02/17/14 09:30
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
June 16,2014
ESC Sample # L683721-03
Site ID :
Project :
Parameter
Result
Det. Limit
Units
Limit
Method
Date/Time By
Dil
Lindane
BDL
0.0050
mg/l
0.40
8081A
02/21/14
1612 CBS
1
Methoxychlor
BDL
0.0050
mg/l
10.
8081A
02/21/14
1612 CBB
1
Toxaphene
BDL
0.010
mg/l
0.50
6081A
02/21/14
1612 CBB
1
Surrogate Recovery
Decachlorobiphenyl
92.0
% Rec.
123.
8081A
02/21/14
1612 CBB
1
Tetrachloro-m-xylene
81.1
% Rec.
114.
8081A
02/21/14
1612 CBB
1
TCLP Herbicides
2,4,5-TP (Silvex)
BDL
0.0020
mg/l
1.0
8151A
02/25/14
2048 KLM
1
2,4-D
BDL
0.0020
mg/l
10.
8151A
02/25/14
2048 KLM
1
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
100.
% Rec.
8151A
02/25/14
2048 KLM
1
TCLP Semi-Volatiles
1,4-Dichlorobenzene
BDL
0.10
mg/l
7.5
8270D
02/23/14
0918 KMF
1
2,4-Dinitrotoluene
BDL
0.10
mg/l
0.13
8270D
02/23/14
0918 KMF
1
Hexachlorobenzene
BDL
0.10
mg/l
0.13
8270D
02/23/14
0918 KMF
1
Hexachloro-1,3-butadiene
BDL
0.10
mg/l
0.50
8270D
02/23/14
0918 KMF
1
Hexachloroethane
BDL
0.10
mg/l
3.0
8270D
02/23/14
0918 KMF
1
Nitrobenzene
BDL
0.10
mg/l
2.0
8270D
02/23/14
0918 KMF
1
Pyridine
BDL
0.10
mg/l
5.0
8270D
02/23/14
0918 KMF
1
3&4-Methyl Phenol
BDL
0.10
mg/l
400
8270D
02/23/14
0918 KMF
1
2-Methylphenol
BDL
0.10
mg/l
200
8270D
02/23/14
0918 KMF
1
Pentachlorophenol
BDL
0.10
mg/l
100
8270D
02/23/14
0918 KMF
1
2,4,5-Trichlorophenol
BDL
0.10
mg/l
400
8270D
02/23/14
0918 KMF
1
2,4,6-Trichlorophenol
BDL
0.10
mg/l
2.0
8270D
02/23/14
0918 KMF
1
Surrogate Recovery
2-Fluorophenol
37.8
% Rec.
87.0
8270D
02/23/14
0918 KMF
1
Phenol-d5
29.3
% Rec.
67.0
8270D
02/23/14
0918 KMF
1
Nitrobenzene-d5
65.5
% Rec.
120.
8270D
02/23/14
0918 KMF
1
2-Fluorobiphenyl
78.5
% Rec.
122.
8270D
02/23/14
0918 KMF
1
2,4,6-Tribromophenol
70.5
% Rec.
148.
8270D
02/23/14
0918 KMF
1
p-Terphenyl-dl4
85.1
% Rec.
149.
8270D
02/23/14
0918 KMF
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum Contaminant Level as established by the US EPA
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 02/26/14 16:54 Revised: 06/16/14 08:58
L683721-03 (IGNITABILITY) - did not ignite @ 170F
Page 8 of 10

Attachment A
List
of Analytes with QC Qualifiers
Sample
Work
Sample
Number
Group
Type
Analyte
L683721-01
WG707374
SAMP
2,4,5-Trichlorophenol
WG707374
SAMP
.2,4,6-Trichlorophenol
WG707850
SAMP
2,4,5-TP (Silvex)
L683721-02
WG707374
SAMP
2,4,5-Trichlorophenol
WG707374
SAMP
2,4,6-Trichlorophenol
WG707850
SAMP
2,4,5-TP (Silvex)
WG707328
SAMP
Silver
L683721-03
WG707850
SAMP
2,4,5-TP (Silvex)
Run
ID Qualifier
R2887602 J3
R2887602 J3
R2888307 J3
R2887602 J3
R2887602 J3
R2888307 73
R2887681 O1J6J3
R2888307 J3
Page 9 of 10

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J3 The associated batch QC was outside the established quality control range
for precision.
J6 The sample matrix interfered with the ability to make any accurate
determination; spike value is low
01 (ESC) The analyte failed the method required serial dilution test and/or
subsequent post -spike criteria. These failures indicate matrix
interference.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
r-
I
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.,
Page 10 of 10

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
T WQ P=nitNo. WQ0035595 Facftj Name Gra vRk Faons, Iote Sowce PcamkNa. NCO0576M SaotnaName Stattt0nsbw8vM 1
0
0
0
m
t~ LC,
0
C 4
Labo,m" 1
LAorAwy2
Sample or Compos imcDate
Parametcr (mg/S.g) Mss A Cbs B
A&LRu=
abA lne
61312014
Alumimun
NIA
N/A
73 Go0
A,,.n.omi+ Niftagen
N/A
NIA
2j80
Arsenk
41
75
7
Cadmi¢m
39
85
2
Caleiacm
N/A
X/A
15500
Copper
1,50
4,300
.247
Lad
300
8"
to
Magnesium
K/A
N/A
2 M
17
57
mow4mum
N/A
75
3
Niekd
42O
420
t6
NitraesNimsIVotrogeo
NIA
N/A
S75
Pacmt Solids
N/A
N/A
232
pH (anumm)
NIA
NIA
7.0a
Phwphoz
NIA
N/A
Tx100
Potns "
N/A
N/A
1,406
PAN (%uj-A-c-)
N/A
NIA
203i
PAN (Sudace)
NIA
N/A
t, 6i
sclevilan
100
100
S
Sodinm
N/A
N/A
719
SAR
NIA
N/A
om
TM4
N/A
N/A
2X0
Zinc
2,800
7,140
426
'I certify, tmdcc penalty of law, dux ebn document was prepared under my direction or super&im in accordan=with a system desk-41 to
Assre that qualified personnel ProPedygatbrxed and evstnated the infwmation submitted. I am aware that tbz= are s4v ==penalces fvr
sub—im,g falseinfD=3i iom, indudimggthe pong aky of Sues and imprisonnft=focltttov+igg viohdons.'
is defined in 40 CPR Part 503.9(4 and 1SA NCAC 2T M02 (26)
Date
s

A AW4
- Facility Stantonsburg WWI'P
Sampling Date 6/3/2014
% Solids 2.52
Mineralization Rate 0.3
Gallons per DT 9,516.20
PH 7.08
FIELD LOADING ESTIMATES
Sodium Absorpotion 0.08 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 2,380 lbs./1,000 gal 0.50
Ammonia Nitrogen (mg/Kg) 2,380.00 lbs./1,000 gal 0.50
Nitrate -Nitrite (mg/Kg) 575.00 lbs./1,000 gal 0.12
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 1,765 lbs./1,000 gal 0.37
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 2,955 lbs./1,000 gal 0.62
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (rng/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
I
4th Year
5th Year
Potassium lbs./1,000 gal
0.61
Phosphorus lbs./1,000 gal
4.64
Calcium lbs./1,000 gal
33.21
Magnesium lbs./1,000 gal
0.59
Manganese lbs./1,000 gal
0.03
Sulfur lbs./1,000 gal
1.19
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
3.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
247.00
Copper lbs./1,000 gal
0.05
Lead (mg/Kg)
10.00
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
1.10
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
16.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
426.00
Zinc lbs./1,000 gal
0.09
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
TKN
PAN PAN
Nitrogen
TKN
PAN
PAN
Nitrogen
(mg/kg) (ms/DT)
(mg/Kg)
(mg/kg) (mS/DT)
(-g/Kg)
Z380
1,765 3.53
615
2,380
%955
5.91
-575
615
92 0.18
523
-575
-86
-0.17
-489
523
39 0.08
484
-489
-37
-0.07
-452
484
18 0.04
465
-452
-17
-0.03
-435
465
9 0.02
457
-435
-8
-0.02
-427
Equations
1 st Yr. PAN (mg/Kg)=(MR x CIYN-NH3)) + (VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x W/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 1,923 3.85
Total 2,807 5.61

Page: 1 of 2
Report Number: 14-155-0206
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
Lab Number: 55735
Sample Id : TS060314
A&L "Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237' [phone] Fax [phone]
Www,aleaitern.com
Project. TOWN OF STANTANSBURG
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 6/3/2014 11:00:00
Date Received: 06/04/2014 00:00
Date Reported: 06/10/2014
Total Solids "
2.52
25200
100.0
MW
06/05/2014 07:59
SM-2540G
Moisture "
97.48
100.0
MW
06/05/2014 07:59
SM-2540G
Total Kjeldahl Nitrogen
0.24
2380
10.0
JM
06/05/2014 08:24
SM-4500-NH3C-TKN
Total Phosphorus
2.21
22100
100
BW
06/05/2014 09:30
SW 6010C
Total Potassium
0.29
2900
100
BW
06/05/2014 09:30
SW 6010C
Total Sulfur
0.57
5650
100
BW
06/05/2014 09:30
SW 6010C
Total Calcium
15.80
158000
100
BW
06/05/2014 09:30
SW 6010C
Total Magnesium
0.28
2830
100
BW
06/05/2014 09:30
SW 6010C
Total Sodium
0.07
718
100
BW
06/05/2014 09:30
SW 6010C
Total Iron
22400
100
BW
06/05/2014 09:30
SW 6010C
Total Aluminum
17600
100
BW
06/05/2014 09:30
SW 6010C
Total Manganese
161
5
BW
06/05/2014 09:30
SW 6010C
Total Copper
247
5
BW
06/05/2014 09:30
SW 6010C
Total Zinc
426
5
BW
06/05/2014 09:30
SW 6010C
Ammonia Nitrogen
0.24
2380
10.0
JM
06/05/2014 08:24
SM-4500-NH3C
Organic N
0.00
0
1.0.0
06/05/2014 08:24
CALCULATION
Nitrate+Nitrite-N
575
2.00
JM
06/05/2014 08:25
SM-450ONO3F
Total Cadmium
<2.0
2.0
BW
06/05/2014 09:30
SW 6010C
All values are on a dry weight
basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential
use of our clients, and may not be reproduced in whole or part, nor may
any reference be made
to the work, the results, or the company in any advertising, news release, or other
public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-155-0206
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
Lab Number: 55735
Sample Id: TS060314
A&L Eastern Laboratories, Inc.
�- 7621 Whitepine Road Richmond, Virginia 23237` [phone] Fax [phone]
wwwaleastem.com
Project: TOWN OF STANTANSBURG
NC CERT#257
REPORT OF ANALYSIS
Total Chromium
23
5
BW
Total Nickel
16
5
BW
Total Lead
10
5
BW
Total Arsenic
3.0
3.0
BW
Total Mercury
1.1
0.4
JM
Total Selenium
<5.0
5.0
BW
pH (Standard Units)7.08
2.00
JM
Total Molybdenum
<5
5
BW
Soluble Phosphorus 0.02
200
100
JM
Comments:
WATER SOLUBLE P, SULFUR AND ORGANIC NITROGEN NOT FOR
COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca".
ALL OTHER
QC DATA IS ACCEPTABLE.
Date Sampled: 6/3/2014 11:00:00
Date Received: 06/04/2014 00:00
Date Reported: 06/10/2014
06/05/2014 09:30
SW 6010C
06/05/2014 09:30
SW 6010C
06/05/2014 09:30
SW 6010C
06/05/2014 09:30
SW 6010C
06/09/2014 10:30
SW-7471 B
06/05/2014 09:30
SW 6010C
06/05/2014 09:24
SW-9045D
06/05/2014 09:30
SW 6010C
06/06/2014 11:19
SOLUBLE P IN MANURE
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

CERTIFICATE OF ANALYSIS
SCOTT CARPENTER
SOIL PLUS
208 WILLIAMS ST
GREENVILLE NC 27858
USA
Microbac Laboratories, Inc. - Wilson Division
3809 Airport Drive NW
Wilson, NC 27896
Tel: [phone]
Report Date: 2014/06/23
Quote: 23-20140328-14
Work Order: 2014-06-03-023
Matrix: WW
Collection Date: 2014/06/03
Sample Submission Date: 2014/06/03
SIDN Client Marks Analvsis Name Method
AA50610 Town of Stantonsburg TS 060314 Flash Point - LiquidsSubcontracted
AA50610
Town of Stantonsburg TS 060314
pH (Corrosivity) Subcontracted
AA50610
Town of Stantonsburg TS 060314
Reactive Cyanide Subcontracted
AA50610
Town of Stantonsburg TS 060314
Reactive Sulfide . Subcontracted
AA50610
Town of Stantonsburg TS 060314
TCLP Full Metals V(Subcontracted
Comments:
Approved by:
Result Unit
*See Attached
*See Attached
*See Attached
*See Attached
*See Attached
Kim Hesse
For any feedback concerning our services, please contact James Nokes, Senior Vice President, at [e-mail]
or Trevor Boyce at [e-mail]
Environmental • Agrochemical • Food • Pharmaceuticals Page 1 of 1

1
Laboratory Report Number: L14060546
Kim Hesse
Microbac Laboratories
3809 Airport Drive
Wilson, NC 27896
Please find enclosed the analytical results for the samples you submitted to Microbac
Laboratories. Review and compilation of your report was completed by Microbac's Ohio
Valley Division (OVD). If you have any questions, comments, or require further assistance
regarding this report, please contact your service representative listed below.
Laboratory Contact:
Emily Yoak — Client Services Specialist
[phone]
[e-mail]
I certify that all test results meet all of the requirements of the accrediting authority listed below. All results for soil
samples are reported on a 'dry -weight' basis unless specified otherwise. Analytical results for water and wastes are
reported on a 'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is
available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of
Microbac Laboratories. The reported results are related only to the samples analyzed as received.
This report was certified on June 20 2014
David Vandenberg — Managing Director
State of Origin: IL
Accrediting Authority: Environmental Protection Agency ID:00152
QAPP: Microbac OVD
I \N ACCpgo y
� cF
Q
v E
U
S
Microbac Laboratories * Ohio Valley Division
158 Starlite Drive, Marietta, OH 45750 * T: [phone] F: [phone] * www.microbac.com
Page 1
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Lab Report #: L14060546
Lab Project #: 2941.016
Project Name: Wilson NC
Lab Contact: Emily Yoak
Record of Sample Receipt and Inspection
CommentsfDiscrepancies
This is the record of the shipment conditions and the inspection records for the samples received and reported as a sample delivery
group (SDG). All of the samples were inspected and observed to conform to our receipt policies, except as noted below.
The following discrepancies were noted:
Discrepancy
No chain of custody was received. CJR
Resolution
Coolers
Cooler # Temperature Temperature CDC # Airbill # Temp Required?
Gun
0019528 1 0.0 1Z2050150110117483 X
Inspection Checklist
#
Question
Result
1
Were shipping coolers sealed?
Yes
2
Were custody seals intact?
Yes
3
Were cooler temperatures in range of 0-6?
Yes
4
Was ice present?
Yes
5
Were COC's received/information complete/signed and dated?
No
6
Were sample containers intact and match COC?
Yes
7
Were sample labels intact and match COC?
Yes
8
Were the correct containers and volumes received?
Yes
9
Were samples received within EPA hold times?
Yes
10
Were correct preservatives used? (water only)
NA
11
Were pH ranges acceptable? (voa's excluded)
NA
12
Were VOA samples free of headspace (less than 6mm)?
NA
Microbac Laboratories a Ohio Valley Division
158 Starlite Drive, Marietta, OH 45750 • T: [phone] F: [phone]
www.microbac.com
Page 2
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Lab Report #: L14060546
Lab Project #: 2941.016
Project Name: Wilson NC
Lab Contact: Emily Yoak
Samples Received
Client ID
Laboratory ID
Date Collected
Date Received
AA50610
L14060546-01
06/031201411:30
06/05/2014 09:56
AA50611
L14060546-02
06/03/201413:30
06/05/2014 09:56
AA50610
L14060546-03
06/03/201411:30
06/05/2014 09:56
AA506U
L14060546-04
061031201413:30
06/05/2014 09:56
Microbac Laboratories • Ohio Valley Division
158 Starlite Drive, Marietta, OH 45750 • T. [phone] F: [phone]
www.microbac.com
Page 3
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Sample #: L14060546-01
Client ID: AA50610
Matrix: Sludge
Workgroup #: WG479732
Collect Date: 06/03/2014 11:30
Sample Tag:
Certificate of Analysis
PrePrep Method: N/A
Prep Method: SW7.34
Analytical Method: SW7.34
Analyst: EPT
Dilution: 1
Units: mg/kg
Analyte CAS #
Reactivity, Sulfide 18496-25-8
U Not detected at or above adjusted sample detection limit
Sample #: L14060546-01
Client ID: AA50610
Matrix: Sludge
Workgroup #: WG479540
Collect Date: 06/03/2014 11:30
Sample Tag:
PrePrep Method: N/A
Prep Method: 9045D
Analytical Method: 9045D
Analyst: ADG
Dilution: 1
Units: UNITS
Lab Report #: L14060546
Lab Project #: 2941.016
Project Name: Wilson NC
Lab Contact: Emily Yoak
Instrument: BURET
Prep Date: N/A
Cal Date:
Run Date: 06/1-1/2014 14:00
File ID: ET.1406111400-04
Resuk Qual RL MDL
U T3,00 100
Instrument: ORION-4STAR
Prep Date: N/A
Cal Date:
Run Date: 06/10/2014 12:30
File ID: OS140611-15253601
Ana"
CAS # Result Qua] RL
10-29-7 6.56 0.000
Corrosivity pH
Temperature At Determination (C)
7.90 0.000
MDL
0.000
0.000
Sample #:
L14060546-01
PrePrep Method:
N/A
Instrument: PRECISION
Client ID:
AA50610
Prep Method:
1010
Prep Date: N/A
Matrix:
Sludge
Analytical Method:
1010
Cal Date:
Workgroup #:
WG479906
Analyst:
RAH
Run Date: 06/12/2014 08:00
Collect Date:
06/03/2014 11:30
Dilution:
1
File ID: PR14061214114401
Sample Tag:
Units:
Degrees C
I Qual
MDL
Analyse
CAS #
Result
Ignitability
64.0
i >
ERL
0.000
0.000
> Result is greater than the associated numerical value.
Sample #:
L14060546-01
PrePrep Method:
N/A
Instrument: UV-120-1V 41
Client ID:
AA50610
Prep Method:
SW7.33
Prep Date: N/A
Matrix:
Sludge
Analytical Method:
SW7.33
Cal Date: 04/25/2014 14:31
Workgroup #:
WG480107
Analyst:
DLP
Run Date: 06/12/2014 15:00
Collect Date:
06/03/2014 11:30
Dilution:
1
File ID: 1V.1406121500-03
Sample Tag:
Units:
mg/kg
Page 1 of 3 Generated at Jun 20, 2014 09,44
Page 21
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Microbac
Certificate of Analysis
Sample #:
L14060546-01
PrePrep Method:
Client ID:
AA50610
Prep Method: 5030B/5030C/5035A
Matrix:
TCLP Leach
Analytical Method: 8260B
Workgroup #:
WG480217
Analyst: TMB
Collect Date:
06/03/2014 11:30
Dilution: 10
Sample Tag:
DL01
Units: ug/L
Lab Report#: L14060546
Lab Project #: 2941.016
Project Name: Wilson NC
Lab Contact: Emily Yoak
Instrument: HPMS8
Prep Date: N/A
Cal Date: 06/11/2014 19:24
Run Date: 06/13/2014 13:17
File ID: 8M398010
Analyte
Result
Qual
RL
MDL
EPA HW#
I Reg- Limit
Benzene
U
50.0
1.25
D018
500
Carbon tetrachloride
U
50.0
2.50
D019
500
Chlorobenzene
U
50.0
1.25
D021
100000
Chloroform
U
50.0
1.25
D022
6000
1.2-Dichloroethane
U
50.0
2.50
D028
500
1,1-Dichloroethene
U
50.0
5.00
D029
700
Methyl Ethyl Ketone
U
100
25.0
D035
200000
Tetrachloroethene
U
50.0
2.50
D039
700
Trichloroethene
U
50.0
2.50
D040
500
Vinyl chloride
U
100
2.50
D043
200
Surrogate
Recovery
Lower Limit
Upper Limit
Q
Dibromotluoromethane
92.1
86
U8
1,2-Dichloroethane-d4
95.7
8D
120
Toluene-d8
99.3
88
110
4-Bromofluorobenzene 100 86 U5
U Not detected at or above adjusted sample detection limit
Sample #:
L14060546-01
PrePrep Method:
Client ID:
AA50610
Prep Method: 3510C
Matrix:
TCLP Leach
Analytical Method: 8270C
Workgroup #:
WG479975
Analyst: JBK
Collect Date:
06/03/2014 11:30
Dilution: 1
Sample Tag:
01
Units: ug/L
Instrument: HPMS12
Prep Date: 06/11/2014 13:00
Cal Date: 05/22/2014 20:14
Run Date: 06/12/2014 18:35
File ID: 12M49365
Analyte
Result
Qual
RL
MDL
EPA HW#
I Reg. Limit
o-Cresol
U
50.0
25.0
D023
200000
m-,p-Cresol
U
50.0
25.0
D025
200000
1,4-Dichlorobenzene
U
50.0
25.0
D027
7500
2,4-Dinitrotoluene
U
50.0
25.0
D030
130
Hexachlorobenzene
U
50.0
25.0
D032
130
Hexachlorobutadiene
U
50.0
25.0
D033
500
Hexachloroethane
U
50.0
25.0
D034
3000
Page 1 of 7 Generated at Jun 20, 2014 09:44
Page 24
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Lab Report H: L14060546
Lab Project 4: 2941.016
Project Name: Wilson NC
Lab Contact: Emily Yoak
Certificate of Analysis
Analyte
Nitrobenzene
Pentachlorophenol
ResuR
Quai
RL
MDL
EPA HW#
Reg. Limit
U
50.0
25.0
D036
2000
U
250
125
D037
100000
Pyridine
U
250
125
D038
5000
2,4,5-Trichlorophenol
U
50.0
25.0
D041
400000
2,4,6-Trichlorophenol
U
50.0
25.0
D042
2000
Surrogate
Recovery
Lower Limit
Upper Limit
Q
2-Ruorophenol
31.4
21
100
Phenol-d5
21.6
10
94
Nitrobenzene-d5
63.2
35
114
2-Ruorobiphenyl
62.1
43
116
2,4,6-Tribromophenol
72.8
10
123
p-Terphenyl-d14
61.5
33
141
U Not detected at or above adjusted sample detection limit
Sample #: L14060546-01
PrePrep Method:
Instrument: HP15
Client ID: AA50610
Prep Method: 3510C
Prep Date: 06/11/2014 10:00
Matrix: TCLP Leach
Analytical Method: 8081A
Cal Date: 06/12/2014 18:50
Workgroup #: WG479872
Analyst: ECL
Run Date: 06/12/2014 21:37
Collect Date: 06/03/2014 11:30
Dilution: 1
File ID: 15G44608.R
Sample Tag: 01
Units: ug/L
Analyte
Result
Qual
RL
MDL
EPA HW#
Reg. Limit
Endrin
U
0.500
0.100
D012
20
Lindane
U
0.500
0.100
D013
400
Methoxychlor
U
0.500
0.100
D014
10000
Toxaphene
U
10.0
3.00
D015
500
Chlordane
U
10.0
3.00
D020
30
Heptachlor
U
0.500
0.100
D031
8
Heptachlor Epoxide
U
0.500
0.100
D031
8
alpha Chlordane
U
0.500
0.100
gamma Chlordane
U
0.500
0.100
Surrogate
Recovery
Lower Limit
Upper Limit
Q
2,4,5,6-Tetrachloro-m-xylene
41.3
20
180
Decachlorobiphenyl
32.1
25
140
U Not detected at or above adjusted sample detection limit
Page 2 of 7 Generated at Jun 20, 2014 09:44
Page 25
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Sample #: L14060546-01
Client ID: AA50610
Matrix: TCLP Leach
Workgroup #: WG480267
Collect Date: 06/03/2014 11:30
Sample Tag: 01
Analyte
Lab Report #: L14060546
Lab Project #: 2941.016
Project Name: Wilson NC
Lab Contact: Emily Yoak
Certificate of Analysis
PrePrep Method:
Instrument: HP17
Prep Method: METHOD
Prep Date: 06/11/2014 15:30
Analytical Method: 8151A
Cal Date: 06/13/2014 18:10
Analyst: ECL
Run Date: 06/14/2014 01:09
Dilution: 1
File ID: 17G17244.R
Units: ug/L
Result I Qual RL MDL
2,4-D U 20.0 5.00
2,4,5•TP (Silvex) U 2.00 0.500
surrogate Recovery Lower Limit I Upper Limit
2,4Dichioropherrylacetic acid 59.0 20 144
U Not detected at or above adjusted sample detection limit
Sample #: L14060546-01
PrePrep Method:
Client ID: AA50610
Prep Method: 3015
Matrix: TCLP Leach
Analytical Method: 6010B
Workgroup #: WG479811
Analyst: KHR
Collect Date: 06/03/2014 11:30
Dilution: 1
Sample Tag: 01
Units: mg/L
Analyte - -
Result Qual
Arsenic, TCLP
U
Barium, TCLP
0174
Cadmium, TCLP
U
Chromium, TCLP
U
Lead, TCLP
U
Selenium, TCLP
U
Silver, TCLP
U
U Not detected at or above adjusted sample detection Omit
Sample #: L14060546-01
PrePrep Method:
Client ID: AA50610
Prep Method: 7470A
Matrix: TCLP Leach
Analytical Method: 7470A
Workgroup #: WG479818
Analyst: JJS
Collect Date: 06/03/2014 11:30
Dilution: 1
Sample Tag: 01
Units: mg/L
Analyte
Result Qual
Mercury
U
U Not detected at or above adjusted sample detection limit
Pape 3 of 7
EPA HW#
Reg. Limit
D016
10000
D017
1000
Q
Instrument: PE-ICP2
Prep Date: 06/11/2014 11:24
Cal Date: 06/11/2014 08:49
Run Date: 06/11/2014 14:56
File ID: P2.061114.145651
RL
MDL
EPA HW#
Reg. Limit
1.00
0.500
D004
5
0.100
0.0500
D005
100
0.100
0.0500
D006
1
0.200
0.100
D007
5
1.00
0.500
D008
5
0.800
0.400
D010
1
0.100
0.0500
Dolt
5
Instrument: CVAAI
Prep Date: 06/11/2014 13:26
Cal Date: 06/11/2014 14:59
Run Date: 06/11/2014 15:42
File ID: M7.061114.154233
RL I MDL EPA HW# I Reg. Limit
0.00200 0.00100 D009 0.2
Generated at Jun 20, 2014 09:44
Page 26
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Lab Report #: L14060546
Lab Project #: 2941.016
Project Name: Wilson NC
Lab Contact: Emily yoak
Certificate of Analysis
Page 7 of 7
Generated at Jun 20, 2014 09:44
Page 30
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Microbac Laboratories Inc.
Ohio Valley Division Analyst List
June 20, 2014
001
- BIO-CHEM TESTING WVDEP 220
002
- REIC Consultants, Inc.
003
- Sturm Environmental
004
- MICROBAC PITTSBURGH
005
- ES LABORATORIES
006
- ALCOSAN LABORATORIES
007
- ALS LABORATORIES
008
- BENCHMARK LABORATORIES
O10
- MICROBAC CHICAGOLAND
ADC
- ANTHONY D. CANTER
ADG
- APRIL D. GREENE
ALS
- ADRIANE L. STEED
AWE
- ANDREW W. ESSIG
AZH
- AFTER HOURS
BAF
- BRICE A. FENTON
BJO
- BRIAN J. OGDEN
BKT
- BRENDAN TORRENCE
BLG
- BRENDA L. GREENWALT
BRG
- BRENDA R. GREGORY
CAA
- CASSIE A. AUGENSTEIN
CAF
- CHERYL A. FLOWERS
CEB
- CHAD E. BARNES
CJR
- COURTNEY J. REXROAD
CLC
- CHRYS L. CRAWFORD
CLS
- CARA L. STRICKLER
CLW
- CHARISSA L. WINTERS
CPD
- CHAD P. DAVIS
CSH
- CHRIS S. HILL
DAK
- DEAN A. K
DCM
- DAVID C. MERCKLE
DEV
- DAVID E. VANDENBERG
DIH
- DEANNA I. HESSON
DLB
- DAVID L. BUMGARNER
DLP
- DOROTHY L. PAYNE
DSM
- DAVID S. MOSSOR
ECL
- ERIC C. LAWSON
ENY
- EMILY N. YOAK
EPT
- ETHAN P. TIDD
ERP
- ERIN R. PORTER
FJB
- FRANCES J. BOLDEN
JBK
- JEREMY B. KINNEY
JDH
- JUSTIN D. HESSON
JDS
- JARED D. SMITH
JJS
- JOHN J. ST MARIE
JLL
- JOHN L. LENT
JMW
- JEANA M. WHITE
JTP
- JOSHUA T. PEMBERTON
JWR
- JOHN W. RICHARDS
JWS
- JACK W. SHEAVES
JYH
- JI Y. HU
KAJ
- KELLIE A. JOHNSON
KDW
- KATHRYN D. WELCH
KEB
- KATIE E. BARNES
KHR
- KIM H. RHODES
KRA
- KATHY R. ALBERTSON
KRB
- KAELY R. BECKER
KRP
- KATHY R. PARSONS
LEC
- LAURA E. CARPENTER
LKN
- LINDA K. NEDEFF
LLS
- LARRY L. STEPHENS
LSB
- LESLIE S. BUCINA
MBK
- MORGAN B. KNOWLTON
MDA
- MIKE D. ALBERTSON
MDC
- MIKE D. COCHRAN
MES
- MARY E. SCHILLING
MLB
- MEGAN L. BACHE
MMB
- MAREN M. BEERY
MRT
- MICHELLE R. TAYLOR
MSW
- MATT S. WILSON
PDM
- PIERCE D. MORRIS
PIT
- MICROBAC WARRENDALE
PSW
- PEGGY S. WEBB
QX -
QIN XU
RAH
- ROY A. HALSTEAD
REK
- BOB E. KYER
RLB
- BOB BUCHANAN
RM -
RAYMOND MALEKE
RNP
- RICK N. PETTY
RS -
ROSEMARY SCOTT
SAV
- SARAH A. VANDENBERG
SDC
- SHALYN D. CONLEY
SEP
- SUZANNE J. PAUGH
SLM
- STEPHANIE L. MOSSBURG
SLP
- SHERI L. PFALZGRAF
TLC
- TYLER L. CORDELL
TMB
- TIFFANY M. BAILEY
TMM
-.TAMMY M. MORRIS
TPA
- TYLER P. AMRINE
VC -
VICKI COLLIER
WJB
- WILL J. BEASLEY
WRR
- WESLEY R. RICHARDS
WTD
- WADE T. DELONG
XXX
- UNAVAILABLE OR SUBCONTRACT
WVDEP 060
Page 31
L1406O546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Microbac Laboratories Inc.
List of Valid Qualifiers
June 20, 2014
Qualkey: STD_ND=U
Qualifier Description
* Surrogate or spike compound out of range
+ Correlation coefficient for the MSA is less than 0.995
< Result is less than the associated numerical value.
> Result is greater than the associated numerical value.
A See the report narrative
B Analyte present in method blank
B1 Target analyte detected in method blank at or above the method reporting limit
B3 Target analyte detected in calibration blank at or above the method reporting limit
C Confirmed by GC/MS
CG Confluent growth
DL Surrogate or spike compound was diluted out
E Estimated concentration due to sample matrix interference
EDL . Elevated sample reporting limits, presence of non -target analytes
EMPC Estimated Maximum Possible Concentration
F, S Estimated result below quantitation limit; method of standard additions(MSA)
FL Free Liquid
H1 Sample analysis performed past holding time.
I Semiquantitative result (out of instrument calibration range)
J The analyte was positively identified, but the quantitation was below the RL
J,B Analyte detected in both the method blank and sample above the MDL.
J,H1 The analyte was positively identified, but the quantitation was below the RL. Sample analysis performed past holding time
J,P Estimate; columns don't agree to within 40%
J,S Estimated concentration; analyzed by method of standard addition (MSA)
L Sample reporting limits elevated due to matrix interference
L1 The associated blank spike (LCS) recovery was above the laboratory acceptance limits.
L2 The associated blank spike (LCS) recovery was below the laboratory acceptance limits.
M Matrix effect; the concentration is an estimate due to matrix effect
N Tentatively identified compound(TIC)
NA Not applicable
ND, L Not detected; sample reporting limit (RL) elevated due to interference
ND, S Not detected; analyzed by method of standard addition (MSA)
NF Not found by library search
NFL No free liquid
NI Non -ignitable
NR Analyte is not required to be analyzed
NS Not spiked
P Concentrations >40% difference between the two GC columns
Q One or more quality control criteria failed. See narrative.
QNS Quantity of sample not sufficient to perform analysis
RA Reanalysis confirms reported results
RE Reanalysis confirms sample matrix interference
s Analyzed by method of standard addition (MSA)
SMI Sample matrix interference on surrogate
SP Reported results are for spike compounds only
TIC Library Search Compound
TNTC Too numerous to count
U Not detected at or above adjusted sample detection limit
U,H1 Not detected; sample analysis performed past holding time.
UJ Undetected; the MDL and RL.are estimated due to quality control discrepancies.
W Post -digestion spike for furnace AA out of control limits
X Exceeds regulatory limit
X, S Exceeds regulatory limit;. method of standard additions (MSA)
Z Cannot be resolved from isomer - see below
\?icroli�4
Page 32
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Submission Form Wilson Division
3809 Airport Drive, Wilson, NC 27896
Phone: [phone]
M 1 C R O B A C` Fax: [phone]
www.rnicrobac.com
❑ GMP UGLP uISO u0tner
By (include company name, address, contact name, phone number & ema
Chock -here -if -you -want -confirmation -that -your samples were.receiyed.
Quote No.:
Report To (include company name, address, contact name, phone number & email address): Same as
`t,,�Y1:Y�
Send Report By:
❑ Email/PDF (email addresses) ❑ FaX (fax number)
❑ Report cc: - ❑ Other
Invoice To (include company name, a dress, contact name, phone number & email address): Same as above
15
tY ��G,ry J
I
I
Submission of this order form constitutes a binding contract for the requested analysis.
L14060546 / Revision: 0 / 39 total pages
❑ Mail
Turn -around -time:
Raw Data Required:" Y [IN
Controlled Substance: ElY ❑ N
"Additional charges apply
DEA Registration No.:
❑ Standard (10-15 workdays)
Sample Storage & Handling
Hazardous Information:
❑ Not Hazardous
ElRush (3-5workdays)•
❑ Emergency Rush (1-2 workdays)*
❑ Ambient
❑ Refrigerator (2 IC to 8 eC)
❑ Hazardous — MSDS Required
Suitable for disposal in a landfill w/o treatment
or
'must have prior approval from•Microbac WNC.
❑ Freezer (-10°C to -25 °C)
special packaging
Please refer to quote for surcharge Information.
❑ Freezer (-80°C)
I ElY ❑ N
SIDN &
Sample Type/
Customer
Analysis & Method
Reporting
Sample
WO
Material Name
Sample ID
Requested
Criteria
Collection
(internal
(This info. will be on the CoAlreport)
(LOD, specs,
air-Ifleft Clank
Time &
use only)
results will be
Date
reported as
(optional):
yh,� ti
nd)
� CL
A v � 1 c�
J• N
F} 0 1
4 Y
+
r
Microbac OVD
Additional Comments:
= Received: 06/0512014 09:56
By: COURTNEY REXRORD 221000055314
r
If data is to be used for regulatory compliance please indicate which regulatory agency.
Page 33
Generated: 06/20/2014 09:47

Microbac Laboratories Inc.
Internal Chain of Custody Report
Login: L14060546
Account: 2941
Project: 2941.016
Samples: 4
Due Date: 16-JUN-2014
Samplenum Container ID Products
L14060546-01 385306 REACTC REACTS
Bottle: 1
Seq.
I Purpose
I From
I To
I Date/Time
JAcceptlRelinquishlpH
1
LOGIN
COOLER
W1
10-JUN-2014 09:47
CLS
2
ANALYZ
W1
WET
11-JUN-2014 08:33
EPT
CLS
3
STORE
WET
A2
17-JUN-2014 09:05
CLS
BLR
Bottle: 2
Seq.
I Purpose
I From
I To
I Date/Time
lAcceptIRelinquishlpH
1
OGIN
OOLE
W1
10-JUN-2014 09:47
CLS
Bottle: 3
Seq.
I Purpose
I From I
To
I Date/Time
JAcceptlRelinquishlpH
1
OGIN
JCOOLE
W1
10-JM-2014 09:47
1 CLS
Samplenum
L14060546-01
Bottle: 1
Container ID Products
385307
Seq.
I Purpose
I From
I To
I Date Time
lAcceptIRelinquishl
pH
1
OGIN
COOLS
10-JUN-2014 09:47
1 CLS
Samplenum
L14060546-01
Bottle: 1
Container ID Products
385308 8081-TC 8151-TC 826-TC 827-TC TC-EX TC-ZHE
Seq. I
Purpose
From
I To
I Date/Time lAcceptIRelinquishlpH
1
LOGIN
COOLER
W1
10-JUN-2014 09:47
CLS
2
ANALYZ
W1
TCL
10-JUN-2014 11:36
BRG
CLS
3
STORE
TCL
A2
11-JUN-2014 07:41
BLG
BRG
Samplenum
L14060546-01
Bottle: 1
Container ID Products
385312 COR-PH
Seq.
I Purpose
From
I To
I Date/Time
lAcceptIRelinquishlpH
1
LOGIN
COOLER
W1
10-JUN-2014 09:53
CLS
2
ANALYZ
W1
WET
10-JUN-2014 12:24
ADG
BJO
3
STORE
WET
A2
10-JUN-2014 13:20
BJO
ADG
Al - Sample Archive (COLD)
A2 - Sample Archive (AMBIENT)
F1 - Volatiles Freezer in Login
V1 - Volatiles Refrigerator in Login
W1 - Walkin Cooler in Login
Li 4060546 / Revision: 0 / 39 total pages
Page 34
Generated: 06/20/2014 09:47

Microbac Laboratories Inc.
Internal Chain of Custody Report
Login: L14060546
Account: 2941
Project: 2941.016
Samples: 4
Due Date: 16-JUN-2014
Samplenum Container ID Products
L14060546-01 385313 FLASH
Bottle: 1
Seq.
I Purpose
I From
I To
I Date/Time
lAcceptIRelinquishlpH
1
LOGIN
OOLE
W1
10-JUN-2014 09:53
CLS
2
ANALYZ
W1
EXT
12-JUN-2014 08:36
RAH
CLS
3
STORE
EXT
A2
18-JUN-2014 08:10
CLS
JDH
Sample num Container ID Products
L14060546-02 385309 COR-PH FLASH REACTC REACTS
Bottle: 1
Seq.
I Purpose
I From
I To
I Date/Time
lAcceptIRelinquishl
pH
1
LOGIN
COOLER
W1
10-JUN-2014 09:47
CLS
2
ANALYZ
W1
WET
10-JUN-2014 12:24
ADG
BJO
3
STORE
WET
A2
10-JUN-2014 13:20
BJO
ADG
ALYZ
W1
WET
11-JUN-2014 08:33
EPT
CLS
5
ANALYZ
W1
EXT
12-JUN-2014 08:36
RAH
CLS
6
STORE
WET
A2
17-JUN-2014 09:05
CLS
BLR
7
STORE
EXT
A2
18-JUN-2014 08:10
CLS
JDH
Bottle: 2
Seq.
I Purpose
I From
I To
I Date/Time
lAcceptIRelinquishl
pH
1
OGIN
1COOLEJ
W1
10-J W-2014 09:47
CLS
Bottle: 3
Seq.
I Purpose
I From
I To
I Date/Time
lAcceptiRelinquishl
pH
1
OGIN
OOLE
W1
10-JUN-2014 09:47
1CLS
Samplenum Container ID Products
L14060546-02 385310
Bottle: 1
Seq.
I Purpose
I From
I To
I Date/Time
lAcceptIRelinquishlpH
1
OGIN
1COOLEJ
110-JUN-2614 09:47
1 CLS
Samplenum Container ID Products
L14060546-02 385311 8081-TC 8151-TC 826-TC 827-TC TC-EX TC-ZHE
Bottle: 1
Seq.
I Purpose
I From
I To
I Date/Time
lAcceptIRelinquishlpH
1
LOGIN
1COOLEJ
Wl
10-JUN-2014 09:47
CLS
2
ANALYZ
W1
I TCL
10-JUN-2014 11:36
BRG
CLS
3
STORE
I TCL
I A2
11-JUN-2014 07:41
BLG
BRG
Al - Sample Archive (COLD)
A2 - Sample Archive (AMBIENT)
F1 - Volatiles Freezer in Login
VI - Volatiles Refrigerator in Login
t
W1 - Walkin Cooler in Login
Page 35
L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

Microbac Laboratories Inc.
Internal Chain of Custody Report
Login: L14060546
Account: 2941
Project: 2941.016
Samples: 4
Due Date: 16-JUN-2014
Samplenum Container ID Products
L14060546-03 385906
Bottle: 1
Seq.
I Purpose
I From I
To
I Date/Time
lAcceptiRelinquishl
pH
1
OGIN
DOLE
W1
Ill-JUN-2014 10:58
1 CLS
Samplenum
L14060546-04
Bottle: 1
Container ID Products
385907 CN
Seq.
I Purpose
I From
I To
I Date/Time lAcceptIRelinquishlpH
1
OGIN
OOLE
W1
11-JUN-2014 10:58
1 CLS
Al - Sample Archive (COLD)
A2 - Sample Archive (AMBIENT)
Fl - Volatiles Freezer in Login
Vl - Volatiles Refrigerator in Login
W1 - Walkin Cooler in Login
L14060546 / Revision: 0 / 39 total pages
Page 36
Eic�•pl�ac
Generated: 06/20/2014 09:47

NELAP Addendum -May 22, 2014
Non-NELAP LIMS Product and Description
The following is a list of those tests that are not included in the Microbac — OVL NELAP Scope of
Accreditation:
Heat of Combustion (BTU)
Total Halide by Bomb Combustion (TX)
Particle Sizing - 200 Mesh (PS200)
Specific Gravity/Density (SPGRAV)
Total Residual Chlorine (CL-TRL)
Total Volatile Solids (all forms) (TVS)
Total Coliform Bacteria (all methods)
Fecal Coliform Bacteria (all methods)
Sulfite (S03)
Thiodiglycol (TDG-LCMS)
Acetate (HPLC-UV)
Formate (HPLC-UV)
Acetaldehyde (HPLC-UV)
Propionaldehyde (HPLC-UV)
Fluoroborate (ISE)
SOLID AND HAZARDOUS CHEMICALS
Nitrogen, Ammonia by Method 350.1
Chromium, Hexavalent, Leachable by SM3500 Cr-B 2009
Phenolics, Total by Method 420.1
NELAP Accreditation by Laboratory SOP
NONPOTABLE WATER
OVL HPLCO2/HPLC-UV
Nitroglycerin
_ Acetic acid
Butyric acid
Lactic acid
Propionic acid
Pyruvic acid
OVL MSS01/GC-MS
1,4-Phenylenediamine
1-Methylnaphthalene
1,4-Dioxane
Atrazine
Benzaldehyde
Biphenyl
Caprolactam
Page 37
_, L14060546 / Revision: 0 / 39 total pages Generated: 06/20/2014 09:47

F]
Hexamethylphosphoramide (HMPA)
Pentachlorobenzene
Pentachloroethane
NELAP Accreditation by Laboratory SOP
NONPOTABLE WATER
OVL MSV01/GC-MS
1, 1, 2-Trichloro-1,2,2-trifluoroethane
1,3-Butadiene
Cyclohexane
Cyclohexanone
Dimethyl disulfide
Dimethylsulfide
Ethyl-t-butylether (ETBE)
Isoprene
Methylacetate
Methylcyclohexane
T-amylmethylether (TAME)
Tetrahydrofuran (THF)
OVL RSKOI/GC-FID
Isobutane
n-Butane
Propane
Propylene
Propyne
OVL HPLC07/HPLC-MS-MS
Hexamethylphosphoramide (XMPA-LCMS)
SOLID AND HAZARDOUS CHEMICALS
OVL MSS01/GC-MS
1-Methyinaphthalene
Benzaldehyde
Biphenyl
Caprolactam
Pentachloroethane
NELAP Accreditation by Laboratory SOP
Page 38
L L14060546 / Revision: 0 / 39 total pages
Generated: 06/20/2014 09:47

SOLID AND HAZARDOUS CHEMICALS
OVL MSV0l/GC-MS
1.3-Butadiene
Cyclohexane
Cyclohexanone
Dimethyl disulfide
Dimethylsulflde
Ethyl-t-butylether (ETBE)
Isoprene
Methylacetate
Methylcyclohexane
n-Hexane
T-amylmethylether (TAME)
Page 39
L14060546 / Revision: 0 / 39 total pages
Generated: 06/20/2014 09:47

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0035595 Facility Name Granville Farms, Inc. Source Permit No. NC0020605 Source Name Town of'rarboro w wrp
Laboratory 1
Laboratory 2
Sample or CompositeDate
Parameter (mg/Kg) Clase A Clas Ii
Environmental
1, Inc.
Environmental
1, Inc.
Environmental
I, Inc,
Environmental
1, Inc.
1/10/2014
4/10/2014
7/3/2014
10/2/2014
Aluminum
N/A
N/A
64.046
48,412
53,393
64,734
Ammonia Nitrogen
N/A
N/A
1,210
1,792 -
2,145
1,043
Arsenic
41
75
3
3.9
10
14
Cadmium
39
85
0.7
0.6
0.7
0.6
Calcium
N/A
N/A
11,842
11,344
12,067
11.542
Copper
1,500
4,300
162
151
159
153
Lead
300
840
17
18
22
21
Magnesium
N/A
N/A
1,734
1,972
2,300
1,636
Mercury
17
57
0.16
0.24
0.19
0.22
Molybdenum
N/A
75
5
5
5
5
Nickel
420
420
8
8
10
9
Nitrate -Nitrite Nitrogen
N/A
N/A
8
4
4
11
Percent Solids
N/A
N/A
3.57
3.42
3.26
3.34
PH (no units)
N/A
N/A
6.50
6.00
5.90
5.90
Phosphorus
N/A
N/A
5,357
6,680
14,176
12,325
Potassium
N/A
N/A
2,399
2,967
3,129
2,182
PAN (Inj./Inc.)
N/A
N/A
9,386
9,334
5,033
11,119
PAN (Surface)
N/A
N/A
8,781
0.438
3,961
10,598
Selenium
100
100
5
5
5
5
Sodium
N/A
N/A
3,365
3,057
2,339
3,402
SAR
N/A
N/A
1.44
1.29
0.92
1.43
TKN
N/A
N/A
28,439
26,918
11,759
34,594
Zinc
2,800
7,500
621
1 454
560
573
"I certify, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, a lading the possibility of fines and Imprisonment for knowing violations."
Si aturc of preparcr * Date
*Prepater is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1101(26)

&- AGMAN FIELD LOADING ESTIMATES
Facility Tarboro WWTP
Sampling Date 1/10/2014
% Solids 3.57
Mineralization Rate 0.25
Gallons per DT 6,717.32
pH 6.5
Sodium Absorpotion 1.44 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 28,439 lbs./1,000 gal 8.47
Ammonia Nitrogen (mg/Kg) 1,210.00 lbs./1,000 gal 0.36
Nitrate -Nitrite (mg/Kg) 7.78 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 7,420 lbs./1,000 gal 2.21
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 8,025 lbs./1,000 gal 2.39
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Potassium lbs./1,000 gal 0.71
Phosphorus lbs./1,000 gal 1.59
Calcium lbs./1,000 gal 3.53
Calcium lbs./1,000 gal 0.52
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
HEAVY METAL CONCENTRATION
HEAVY METAL LOADING
41
75
Arsenic (mg/Kg)
3.00
Arsenic lbs./1,000 gal
0.00
39
85
Cadmium (mg/Kg)
0.70
Cadmium lbs./1,000 gal
0.00
1,500
4,300
Copper (mg/Kg)
162.00
Copper lbs./1,000 gal
0.05
300
840
Lead (mg/Kg)
17.00
Lead lbs./1,000 gal
0.01
17
57
Mercury (mg/Kg)
0.16
Mercury lbs./1,000 gal
0.00
420
420
Nickel (mg/Kg)
8.00
Nickel lbs./1,000 gal
0.00
100
100
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
2,800
7,500
Zinc (mg/Kg)
621.00
Zinc lbs./1,000 gal
0.18
RESIDUAL NITROGEN CALCULATION
1 St Year
2nd Year
3rd Year
4th Year
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen.
PAN PAN
Nitrogen
TEN
(mg/kg) (lbs/DT)
- (mg/Kg)
TEN
(mg/kg) (lbs/DT)
(mg/Kg)
28,439
7,420
14.84
21,019
28,439
8,025 16.05
20,414
21,019
Z627
5.25
18,392
20,414
2,552 5.10
17,862
18,392
1,149
2.30
17,242
17,862
1,116 2.23
16,746
17,242
539
1.08
16,703
16,746
523 1.05
16,223
16,703
261
0.52
16,442
16,223
253 0.51
15,969
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-N13))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/I6)
Total 11,997 23.99
Total 12,470 24.94

02/17/2014 12:04 2526414230
PUBLIC WORKS
PAGE 02/04
mWohmanq % WO
OBI
ID#: 305
TOWN OF TARBORO (9=0E)
MR. MICHAEL ALLEN
P.O. 80S 220 DATE COLLECTED: 01./10/14
TAgWORO ,NC 27886 DATE REPORTED 02/1.0/14
RLVIAWED BY:
Lagoon Activated Prim. Clar. Analysis Metbod
PARAMETERS Sludge Emuent Date Analyst Code
PH, units 6.5 01 /1,3114 TRD 450OR&OO
Total Cyanide, mg/1 0.007 <0.005 01/1.3/14 SEJ 4500CNE-99
Aluminfim, (dry wt. basis), mg/kg 64046 01/29/14 LFJ EPA200.7
Arsenic, ug/l <5.0 01/22/14 KE1, 31131344
Arsenic (dry wt. basis), mg/kg 3 01/30/14 MEL 311311-04
Calcium (dry wt. basis), mg/kg 11942 01/29/.14 LFJ EPA200.7
Cadmium, ug/l 1 <1.0 01117/14 MEL 3113R44
Cadmium (dry wt. basis), mg/kg 0.7 02/06/14 MEL 311311.04
Copper, ug/1 383 25 01/17/14 LFJ EPA200.7
Copper (dry wt, basis), mg/kg 162 01/29/14 LFJ EPA200,7
Total Chromium, jig/1 113 2S 01/17/14 ,LFJ EPA200.7
Chromium, T.(dry wt. baaia),mg/kg 51. 01/29/14 LFJ EPA200.7
Lead, ug/l 35 <5.0 01124/14 MEL 3113B44
Lead (dry weight basis), mg/leg 17 02/04/14 MEL 3.11.3B-04
.Magnesium (dry wt. basis), mg/kg 1734 01/29/14 LT.T EPA200.7
Meret:ry, ug/l 0.314 <0.2 01/17/14 ADD 245.1. R3-94
Mercury (dry wt. basis), rng/ltg 0.1.6 01/17/14 ADD 245.7 83-94
Nickel, ug/l 16 < 10 01/17/14 LFJ EPA200.7
Nielkel (dry wt. basis), mgAcg 8 01/29/14 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 2399 01/29114 LFJ EFA2,00.7
Selenium (dry wt. basis), mg/kg <5.0 02/03/14 MEL 303R-04
Salver, ug/l <5.0 <5.0 01/17/14 LI'J EPA200.7
Sodium (dry wt. basis), mg/kg 3365 01/28/14 ADD 311113--99
Zinc, z:gA 1121 40 01/31/14 ADT) 311113-99
Zinc (dry wt. basis), mg/kg 621 01/31/14 .ADD 311ID-99
Total Solids, % 3.57 0.25 01/13/14 HMB 2540G97
TKN (dry wt.), mg/kg 28439 01116/14 ANO 351.2 R2.93
.Ammonia Nitrogen (dry wt,),Mglkg 1210 01/14/14 ALB 350.1 112-93
Phosphorus, T. (dry wt.), mg/kg 5357 01/16/14 ALB 365.4 .74
Nitrate-Nitrito (dry wt.), mg/Itg 7.78 01/15/14 ANO 353.2 R2-93
Plant Available Nitrogen, mglkg 7420 01/22/14 SEJ
Molybdenum (dry wt. basis), mg/kg <5.0 01/29/14 LET EPA200.7

AGMAN FIELD LOADING ESTIMATES
Facility Tarboro WWI'P
Sampling Date 4/10/2014
% Solids 3.42
Mineralization Rate 0.25
Gallons per DT 7,011.93
pH 6
Sodium Absorpotion 1.29 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 26,918 lbs./1,000 gal 7.68
Ammonia Nitrogen (mg/Kg) 1,792.00 lbs./1,000 gal 0.51
Nitrate -Nitrite (mg/Kg) 3.82 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 7,181 lbs./1,000 gal 2.05
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) .8,077 lbs./1,000 gal 2.30
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Potassium lbs./1,000 gal 0.85
Phosphorus lbs./1,000 gal 1.91
Calcium lbs./1,000 gal 3.24
Calcium lbs./1,000 gal 0.56
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
HEAVY METAL CONCENTRATION
HEAVY METAL LOADING
41
75
Arsenic (mg/Kg)
3.90
Arsenic lbs./1,000 gal
0.00
39
85
Cadmium (mg/Kg)
0.60
Cadmium lbs./1,000 gal
0.00
1,500
4,300
Copper (mg/Kg)
151.00
Copper lbs./1,000 gal
0.04
300
840
Lead (mg/Kg)
18.00
Lead lbs./1,000 gal
0.01
17
57
Mercury (mg/Kg)
0.24
Mercury lbs./1,000 gal
0.00
420
420
Nickel (mg/Kg)
8.00
Nickel lbs./1,000 gal
0.00
100
100
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
2,800
7,500
Zinc (mg/Kg)
454.00
Zinc lbs./1,000 gal
0.13
RESIDUAL NITROGEN CALCULATION
1st Year
f
j 2nd Year
3rd Year
4th Year
i
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
118,941
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(-g/kg) (lbs/DT)
(mg/Rg)
26,918
7,181 14.36
19,737
26,918
8,077 16.15
18,841
19,737
2,467 4.93
17,270
2,355 . 4.71
16,486
17,270
1,079 2.16
16,190
16,486
1,030 2.06
15,455
16,190
506 1.01
15,684
15,455
483 0.97
14,972
15,684
245 0.49
15,439
14,972
234 0.47
14,738
Equations
1st Yr. PAN (mg/Kg)=W x (rKN-NH3))+(VRx NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x W12)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x W/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x W/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x W116)
Total 11,479 22.96 Total 12,180 24.36

05/20/2014 13:21 2526414230
PUBLIC WORKS
PAGE 03/04
J
EMWhMUM@Mq % 108
TOWN OF TARBORO (S =GR)
MR. MICiiAEL AZ+L=
P.O. SOX 220
TARBORO ,NC 27886
PARAMETERS
PH, Units
Total Cyanide, mgA -
.Aluminum, (dry wt. basis), mg/kg
Arsenic, ug/l
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium, ug/1
Cadmium (dry wt. basis), mg/kg
Copper, ugA
Copper, ug/l
Copper (dry wt. basis), mg/kg
Total Chromium, ug/l
Chromium, T.(dry wt. basis),mg/kg
Lead, ug11
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury, ug/1
Mercury (dry wt. haggis), mg/kg
Nickel, ug/l
Nickel (dry wt. bads), mg/kg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mg/kg
Silver, ug/l
Sodium (dry wt. basis), mg/kg
Zinc, ug/1
Zinc (dry wt. basis), mg/kg
Total Solids, %
TXN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phospboirus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mglkg
Lagoon
6.0
48412
3.9
1,1344
0.6
151
41
18
1972
0.24
8
2967
a 5.0
3057
454
3.42
26918
1792
6680
C 3.82
7178
4 5.0
1D#: 305
PATE COY-LECTED: 04/10/14
))�LTE $PORTED 45/19/16
REVIEWED BY:
Anaerobic Prue. Clar. Analysis . Method
Influent Effluent Date Analyst Code
04/14/14 TRB 4500HB-00
C 0.005 C 0.005 04/15/14 SW 4500CNE-99
04/29/1,4I,,F.T EPA200.7
C 3.0 04/29/14 MEL 3113.8-04
04/29/14 MEL 3113B-04
04/29/14 LFJ EPA200.7
8 L 1.0 04/22/14 MEL 31'13B-04
05/15/14 NM4 L 31138-04
1947 04/25/14 LET EPA200.7
8 05/02/14 LFJ EPA200.7
04/29/14 LFJ EPA200.7
432 <5.0 04/25/14 LFJ EPA200.7
04/29/1.4 LFJ EPA200.7
C 5.0 C 5.0 04/74114 MEL 3113E-04
04/30/14 MEL 31.,1,IB-04
04/29/14 LFd EPA200.7
4.7 ¢0.2 04/23/1.4 NnM 245.1 R3-94
04/15114 MTM 245.1 It,194
151 C 10 04/25/14 LFJ EPA200.7
04/29/1.4 LFJ EPA200.7
04/Z9/14 LFJ EPA200.7
05/14/14 MEL 3113E-04
15 <5.0 04/25/14 LET EPA200.7
05/02/14 M I f 3111B.99
6682 12 04/23/14 MTM 3111B.99
05/02/14 MTM 311111A9
5.45 04/15/14 MDT) 2540G97
04/21/14 ANO 351.2 R2-93
04/15/14 ALB 350.1 R2-93
04/21114 A,LD 365.4 -74
04/16/14 ANO 353.2 R2.93
04/22/14 SLY
04/29/14 3,4.FJ EPA200.7

ADMAN FIELD LOADING ESTIMATES
Facility Tarboro WWTP
Sampling Date 7/3/2014
% Solids 3.26
Mineralization Rate 0.25
Gallons per DT 7,356.08
pH 5.9
Sodium Absorpotion 0.92 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 11,759 lbs./1,000 gal 3.20
Ammonia Nitrogen (mg/Kg) 2,145.00 lbs./1,000 gal 0.58
Nitrate -Nitrite (mg/Kg) 3.83 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 3,480 lbs./1,000 gal 0.95
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 4,552 lbs./1,000 gal 1.24
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
1st Year
2nd Year
3rd Year
4th Year
i
5th Year
Potassium lbs./1,000 gal 0.85
Phosphorus lbs./1,000 gal 3.85
Calcium lbs./1,000 gal 3.28
Calcium lbs./1,000 gal 0.63
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
10.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.70
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
159.00
Copper lbs./1,000 gal
0.04
Lead (mg/Kg)
22.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.19
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
10.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
560.00
Zinc lbs./1,000 gal
0.15
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
TEN
PAN
PAN
Nitrogen
TKN
PAN PAN
Nitrogen
(mg/kg) (lbs/DT)
(mg/Kg)
(mg/kg) (lbs/DT)
(.ng/Rg)
11,759
3,480
6.96
8,279
11,759
4,552 9.10
7,207
8,279
1,035
2.07
7,244
7,207
901 1.80
6,306
7,244
453
0.91
6,792
6,306
394 0.79
5,912
6,792
212
0.42
6,579
5,912
185 0.37
5,727
6,579
103
0.21
6,476
5,727
89 0.18
5,637
Equations
1st Yr. PAN (mg/Kg)=(MR x (rKN-NI13))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 5,283 10.57 Total 6,122 12.24

08/05/2014 08:58 2526414230
Elow'OhMERN 19 bw
TOWN OF TARBORO (9LuDG1r)
MR. XICHARL ALLEN
P.O. BOX 220
TARBORO .NC 27886
p e'd
PUBLIC WORKS
PAGE 02/05
tD#: ` 305
DATE COLLECTED: 07/03/14
DATE REPORTED : 07/31/14
REVIEWED BY
Lagoon
Activated Prim. Clar.
Analysis
Method
PARAMETERS
Sludge Effluent,
Date Analyst Code
PH, Units
5.9
07/07/14 TRB
4500M-00
Total Cyanide, mg/l
0.007 <0,005
07/10114 SEJ
450OCNE-99
Aluminum, (dry wt. basis), mg/kg
53393
07/11/14 LFJ
EPA200.7
Arsenic, ug/1
7
07/14/14 MEL
3113B-04
Arsenic (dry wt. basis), mg/kg
10
07/22/14 CMF
311311-04
Calcium (dry wt. basis), mg/kg
12067
07/11/14 LFJ
EPA200.7
Cadmium, ugll
2 <1.0
07/16/14 MEL
3113B-04
Cadmium (dry wt, basis), mg/kg
0.7
07/16/14 MEL
3113E.04
Copper, ug/l
4" 15
07/11/14 LFJ
EPA200.7
Copper (dry wt, basis), mg/kg
159
07/11/14 LFJ
EPA200.7
Total Chromium, ug11
96 <5.0
07111114 LFJ
EPA200.7
Chromium, T-(dry wt. basis),img/kg
35
07/11/14 LFJ
ZPA200.7
Lead, ug/l
42 <5.0
07/11/14. MEL
3113B-04
Lead (dry weight basis), mg/kg
22
07/17/14 MEL
311313-04
Magnesium, (dry wt. basis), mg/kg
2300
07/11/14 LET
EPA200.7
Mercury, ug/l
0.24 C 0.2
07/09/14 MTM
245.1 R3.94
Mercury (dry wt. basis), mg/kg
0.19
07/24/14 MTX
245.1 R3-94
Nickel, ugA
20
07/14/14 Lk'J
EPA200.7
Nickel, ugli
<10
07/11/14 LI:T
EPA200.7
Nickel (dry wt. basis), mg/kg
< 10
07/11/14 - L)FJ
EPA200.7
Potassium (dry wt. basis), mg/kg
3129
07111/1.4 LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
07/15/14 MEL
3113E-04
Silver, ug/l
C 5.0
07/14/14 LF1
EPA200.7
Silver, ug/l
<5.0
07/11/14 LET
FXA200.7
Sodium (dry wt. basis), mg/kg
2339
07/22114 MTM
3111E-99
Zinc, ug/l
1435 53
07/11/14 LFJ
LTA200.7
Zinc (dry wt. basis), mg/kg
560
07/11114 LFJ -
EPA200.7 -
Total Solids, %
3.26
0.26
07/07/14 CNC
2540G-97
TKN (dry wt.), mg/kg
11759
07/10/14 ANO
351.2 R2-93
Ammonia Nitrogen (dry wt.),nm/kR
2145
07/08/14 ALD
350.1 112-93
Phosphon's, T. (dry wt.), mg/kg
14176
ALB
365.4 .74
Nitrate-Nftrite (dry wt.), mg/kg
<3,83
.07/10/14
07/09/14 ANO
353.2 I22--93
Plant Available Nitrogen, mg/kg
3476
07/15/14 SET

08/05/2014 08:50 2526414230
PUBLIC WORKS
PAGE 03/05
TOWN OF TxARBORO (SLUDGE)
MR- =CR&EL Ai LEN
P.4, SOX 220
TARBORO ,NC 27886
tD#: 305
DATE COLLECTED: 07/03/14
DAB'$ REPORTED : 07/31/14
REVIEWED 8Y: 4�
Lagoon Activated Prim. Clear. Analysis Method
PARAMETERS Sludge Effluent Date Analyst Code
Molybdenum (dry wt. basis), mg/kg <5,0 07/14/14 LFJ EPA200.7

AGM FIELD LOADING ESTIMATES
r --.
Facility Tarboro WWTP
i Sampling Date 10/2/2014
L, % Solids 3.34
Mineralization Rate 0.25
Gallons per DT 7,179.88
~ pH 5.9
Sodium Absorpotion 1.43 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 34,594 lbs./1,000 gal 9.64
Potassium lbs./1,000 gal
0.61
- Ammonia Nitrogen (mg/Kg) 1,043.00 lbs./1,000 gal 0.29
Phosphorus lbs./1,000 gal
3.43
Nitrate -Nitrite (mg/Kg) 10.70 lbs./1,000 gal 0.00
Calcium lbs./1,000 gal
3.22
- PLANT AVAILABLE NITROGEN SURFACE APPLIED
Calcium lbs./1,000 gal
0.46
PAN (mg/Kg) 8,920 lbs./1,000 gal 2.48
Manganese lbs./1,000 gal
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
PAN (mg/Kg) 9,441 lbs./1,000 gal 2.63
Molybdenum lbs./1,000 gal
0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39 -
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
14.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.60
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
153.00
Copper lbs./1,000 gal
0.04
Lead (mg/Kg)
21.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.22
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
9.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
573.00
Zinc lbs./1,000 gal
0.16
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Rem ainii
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TEN
(-g/kg) (lbs/DT)
(mg/Kg)
TEN
(-g/kg) (lbs/Df)
(-g/Kg)
34,594
8,920 17.84
25,674
34,594
9,441 18.88
25,153
25,674
3,209 6.42
22,465
25,153
3,144 6.29
22,008
22,465
1,404 2.81
21,061
22,008
1,376 2.75
20,633
21,061
658 1.32
20,403
20,633
645 1.29
19,988
20,403
319 0.64
20,084
19,988
312 0.62
19,676
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x W18)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x W/16)
Total 14,510 29,02 Total 14,918 29.84

11/06/2014 09:58 2526414230
PUBLIC WORKS
PAGE 03/14
TOWN OF 'T.ARBORO (1MMOE)
MR. MICaML ALLEN
P.O. BOX 220
TA OR0 ,IRC 27886
xD#; 305
DATE COY-LECTED: 10/02/14
DATE REPORTED : 10/30/14
RWIRWED BY:
Lagoon
Anaerobic Prim, Clar.
Analysis
Method
PARAMETERS
Influent k:muent
Date
Analyst
Code
PH, Units
5.9
10/07114
TRB
4500H"O
Total Cyanide, mg/1
<0.005 <0.005
10/03/14
SEJ
450OCN,E-99
Aluminum, (dry wt. basic), mg/kg
64734
10/14/14
LFJ
EPA200.7
Arsenic, ugll
150
10/10/14
MEL
31.1313-04
Arsenic (dry wt. basis), mg/kg
14
10/28/14
,MEL
3113E-04
Calcium (dry wt. basis), mg/kg
11542
10/14/14
LFJ
EPA200.7
Cadmiam, ugll
23 <1.0
10/16/14
MEL
3113B-04
Cadmimn . (airy wt. basis), mg/kg
0.6
10/22/14
MEL
311311-04
Copper, ug/1
4007 10
10/07/14
LFJ
EPA200.7
Copper (dry wt bads), mg/kg
153
10/14114
LFJ
EPA200.7
Total Chromium, ug/1
572 <5,0
10/07/14
LFJ
EPA200.7
Chromium, T.(dry wL basis),mg/kg
30
10/20/14
LFJ
EPA200.7
Lead, ug/l
683 <5,0'
10/15/14
MEL
3113B-04
Lead (dry weight basis), mg/kg
21
10/29/14
MEL
31'.(1"4
Magnesium (dry wt. basis), mg/kg
1636
10/14/14
J J
EPA200.7
Mercury, ug/l
11 <0.2
10/09/1.4
MTM
245.1 R3-94
Mercury (dry wt. basis), mglkg
0.22
10/0911.4
MUM
245.1 R3-94
Nickel, ug/1
294 <10
10/0711.4
LFJ
EPA200.7
Nickel (dry wt. basis), mg/kg
9
10/14/14
LF.T
EPA 200,7
Potassium (dry wt. basis), mg/kg
2182
10/14/14
LFT
EPA200.7 ,
Selenium, ug/l
23
10/23/14
1. L
3.113E-04
Selenium (dry wt. basis), mg/kg
<5.0
10/23/14
MEL
3113E-04
Silver, ug/1
42 <5.0
10/07/14
LFJ
EPA200.7
Sodium (dry wt. basis), mg/kg
3401
10/22/14
MT
311IB-99
Zinc, ug/l
19515 39
10/07/14
M.TM
31110-99
Zinc (dry wt. basis), mg/kg
573
10120/14
MZN
3111E-99
Total Solids, %a
3.34
5.55
10/02/14
CMC
-2540G47 - -
TKN (dry wt.), mg/kg
34594
10109/14
ANO
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
1043
10/09/14
ANO
350.1 R2-93
Phosphorus, T. (airy wt.), mg/kg
1Z325
10/09/14
AKS
165.4-74
Nitrate,Nitrite (dry wt.), mg/kg
10.70
10108/14
ANO
353.2 R2-93
Plant Available Nitrogen, mg/kg
13953
10/14/14
5EJ
Molybdenum (dry wt. basis), mg/kg,
<5.0
10/20/14
LFJ
EPA200.7

11/06/2014 09:58 2526414230 PUBLIC WORKS PAGE 06/14
SIa1 OW .Environmental rechnologtes, Inc.
3310 Win 5t.
F,r vlac�r�ntsr�rnl. rxcl caai.c��;:� :, lv summilt
0owkoga falls, Ohto 44223
F
•�! Artrrat,>r..a,+TEL: [phone]FAX,-[phone]
Websric; OyjL(,(jk1�w„rerrekcant
October 24, 2014
Deedee Woolard
Environment 1, Inc.
114 Oakmont Dr
P.O. Box 7085
Greenville, .NC 27858
TEL: [phone]
FAX: [phone]
RE; 305
Dear Deedee Woolard:
Order No.: 14100591
Summit Environmental Technologies, Inc. received 1 sarnple(s) on 10/3/2014 forthe analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative,
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel, free to call the laboratory
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St,
Cuyahoga Falls, Oltio 44223
MLA 0724.01, Nnbermt 41600, Arizona AZD788, Arkonses 83-0735, Calitomim 0725bCA Colorado, Comrecriwt PH-0105, belawnre, P1a*ion NEWC
Eg7688, Giorgi* E87683 rind 943, TWO OH00923, I inob 200061 and Rags, Indiana C-OH•13. Kamm L•-10347, K-Wcky (Undargmand Storage Tank)
3, Yantacky 90146. Lotriaana D4o61 mid LA1200M1, Maiao 2o12D15. Maryland 339, MaAurclnrsclts M•OPlio23, Minneacen 409711, hianlana CcRT0099,
New Hattiothire 2996, New Jetsay OPIDD6, New York 11777. NO& Carolina 39705 and 631, Ohio Wnking Warer4170, Ohio VAP CUM. Ok AO=
9940, Oregon OH20 001, Pennsylvania 63-01335, Rhode Island LA000317, Smith Carolina 92016001, Tennessee TN04018, Term TI D47044Wl I-5,
Region R BTMS-L, USD/VAPHIS P330-11.00244, Utah ORD092320114, Vermont VT-87688, Virginia 00440 and 1591. Wnshinsion C891, West
Virginia 248 and 9957C and H8768g, Wisconsin 399013o10
Page 1 of C
Page 9 of 9

11/06/2014 09:58 2526414230 PUBLIC WORKS PAGE 07/14
Summil Environmental Technologies. role,
'Workorder
vs,
rPn�vrSs►od�NTfaL'
trNd��aIR^1?�0.'3�,
3310 WIn St.
CuyahogaFallv,Ohio 44223
Sample Summary
?•�s;y-+'ca�L.�
ra .atoriA:;
TEL [phone] FAX; [phone]
WON: 14100$91
FYcbsite: h1fp;/hvxw setfek.conr
zQ_0�., j4
CLIENT:
Environment 1, ins,
^
Project.:
305
Lab S2mple[D
Client Sample ID
Tng No Date Collected
Date Received Matrix
14100591-001
SludSc Sample
I0=014 10:00:00 AM
10/3120149:45:00 AM Sludge
14100591-001
Sludge Sample
IOi2/2014 10;00;00 AM
108/2014 9;45:00 AM Sludge
Page 2 of 6
Page 2 of 9

11/06/2014 09:58 2526414230 PUBLIC WORKS PAGE 08/14
SOMMU Environmental Technologies, Inc.
TNIC.
3310lYln5t,Case Narrative
Ctvahoga Falls Ohio 44223 WOA: 14100591
MI., (330) 253•8211 FAX. [phone] Dom: 10124/2014
Wehstte; blip://w�wu.scllek enm
CLIENM Environment 1, Inc. .^
Project: 305
This report in its entirety consists ofthe documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter., Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM,,, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
original
Page 3 of 6
'age 3 of 9

11/06/2014
09:58
2526414230 PUBLIC WORKS
PAGE
09/14
Surnmir Holronmantal rectworogids, /nc.
WOI#: 14100591
$
3310 IYhr St.
�rrv�4nnur�;arrr,Lz�cxunen:+sr��,:v,�
Cuyahoga l:all%Ohio 44223 Date Reported: 10/24/2014
+�rar,
ttcar L.ai3,�rata,fnt
TEL. [phone] FAY. [phone]
Company: Environment
1, Inc.
-
lYebsire.; 1j11n(Ltetme.settek.com
Address: 114 Oakmont
Dr
Greenville NC 27858
Received: 10/3/2014
Project#: 305
TCLP Metals Analysis (6010)
Client W#
Lab M# Collected Analyse Rep LMt Result Units
Matrix Method DF
Ae9Lvl
Run
Analyst
Sludge Sample
001
1012/2014 TCLP Arsenic(AS) 0.50 NO mg/L
Sludge EPA 6010 C 1
5.0
10110/2014
WK
Sludge Sample
001
10/2/2014 TCLP Seaum(Ba) 6.0 NO mg/L
Sludge EPA 6010 C 1
100
10/10/2014
WK
Sludge Sample
001
101=014 TCLP Cadmlum(Cd) 0.10 NO mgk
Sludge EPA 6010 C 1
1.0
10/1012014
WK
Sludge Sample
001
101212014 TCLP Chromiumpo 0.20 ND mg/L
Sludge EPA 6010 C 1
5,0
1011012014
WK
Sludge Sample
001
1012/2014 TCLP Lead(Pb) 0.50 NO mg1(,
Sludge EPA 6010 C 1
5.0
10110/2014
WK
Sludge Sample
001
10/212014 TCLP Soleniurn(Se) 0.50 NO mg1L
Sludge EPA 6010 C 1
1.0
10/10/2014
WK
Sludge Sample
001
10/2/2014 TCLP Sllver(Ag) 0.50 NO mg/L
Sludge EPA 6010 C 1
6.0
1011012014
WK
TCLP Mercury Analysis (131117470)
Client ID#
Lab ID# Collected Analyse Rep Llmt Result Units
Matrix Method OF
RegLvl
Ron Analyst
lr Sludge Sample
001.
10/2/2014 TCLP Mercury 0.0020 NO mg/L
Sludge EPA 7470 A 1
0.20
10/10/2014
AW
SVOC SW-846: 8081-TCLP Pesticides
Client 11D# Lab 1,D# Collected Analyte Rep Lint Result units Matrix Method DF RegLvl stun Analyst
Sludge Sample
001
10/2/2014 Chlordane, total
0.010
NO mg1L
Sludge
' EPA 80818
1 0,030
10/14/2014
JSN
Sludge Sample
001
101212014 Toxaphene
0.10
NO mg/L
Sludge
EPAS081 E
1 0.50
10/14/2014
JBN
Sludge Sample
001
101212014 Endrin
0.0020
NO mg/L
Sludge
EPA a091 B
1 0.020
10114/2014
JBN
Sludge Sample
001
10/212014 gamma-BHC L
0.0020
ND mg/L
Sludge
EPA 8081 S
1 DAO
10114/2014
JBN
Sludge Sample
OD1
10/2/2014 Heptachlor
0,0020
ND mg1L
Sludge
EPA 8081 B
1 0,0080
1011412014
JBN
Sludge Sample
001
10/212014 Heptachlor epoxlde
0,0020
NO mg/L
Sludge
EPA 60815
1 0.0000
10/14/2014
JBN
Sludge Sample
001
101212014 Methoxyohlor
0.0020
NO mg/L
Sludge
EPA 6091 8
1 10
10/14/2014
JBN
VOC by GC/MS (826%,TCLP
Client ID#
.Lab ID# Collected Analyte
Rep Lint Result Units
Matrix
Method
DF
RegLvl
Ran
Analyst
Sludge Sample
001
10/212014 1,1-Dlchloroethene
0.10
NO mg/L
Sludge
EPA 8260 B
1
0.70
10/1312014
MO
Sludge Sample
001
10/212014 1,2-Dichlorcethane
0.10
NO mg/L
Sludge
EPA 8260 B
1
0.50
1011312014
MO
Sludge Sample
001
10/2/2014 Benzene
0.10
NO mg/L
Sludge
EPA 8260 B
1
0,50
10/1312014
MO
Sludge Sample
001
10/2/2014 Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 82$0 B
1
0.50
10/13/2014
MO
Sludge Sample
001
10/2/2014 Chiorobenzene
0.10
NO mg/L
Sludge
EPA 8260 B
1
100
10113/2014
MO
Sludge Sample
001
10/212014 Chloroform
0,10
NO mg1L
Sludge
EPA 8250 B
1
6.0
10113/2014
MO
Sludge Sample
001
10/2/2014 Tetrachloroethene
0.10
NO mg/L
Sludge
EPA 8260 B
1
0.70
10/13/2014
MO
Sludge Sample
001
10/2/2014 Trichlorcethene
0.10
NO mg/L
Sludge
EPA 8260 S
1
0.50
1011312014
MO
Sludge sample
001
10/212014 Vinyl chloride
0120
ND mg1L
Sludge
EPA $260 B
1
0.20
10/1312014
MO
Sludge Sample
001
101212D14 MEK
2.0
NO mglt.
Sludge
EPA SZOD B
1
200
10/13/2014
MO
P99V4 c#d9

11/06/2014 09:58 2526414230 PUBLIC WORKS PAGE 10/14
m1r Enviranmental Technologies. Inc. WO#:
3310 Win Sr.
IFiBYtpANdAEMIT.�t ��� !�ra0rngo . rvt; Cuyahoga Palk, Ohio 44223 Date Reported:
�rairi�3r„?� Lr�4v atn�:�r TEL: (330) aS3n41J1 Fi1.17 (330J 253-1489 Company:
Websile: htrn:thvivw.Setrek.Com Address:
SVOC 8270 TCLP BNA List
.14100591
10/24/2014
Environment 1, inc.
114 Oakmont Dr
Greenville NC 27858
Received: 10/3/2014
Project#: 30
CI!ient WN
Lab ID# Collected Analyse
Rep [,mt Result Units
Matrix
Method
DF
RegLvI
Run
Analyst
Sludge Sample
001
10/2/2014 1,4.01chlorobenxene
0.10
NO mg/L
Sludge
EPA 8270 C
1
7,5
10/1412014
AKE
Sludge Sample
001
10/2/2014 2,4,5-Trichlorophenol
0.26
NO mg/L
Sludge
EPA $270 C
1
400
10/14/2014
AKE
Sludge Sample
001
10/2/2014 2,4,64richlorophenol
0.25
ND mg1L
Sludge
EPA 8270 C
1
2.0
1011412014
AKE
Sludge Sample
001
10/2/2014 2.4-01nitrotoluene
0.10
NO mglL
Sludge
EPA 8270 C
1
0.13
10/14/2014
AKE
Sludge Semple
001
10/2/2014 Creeols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
IV14/2014
AKE
Sludge Sample
001
101212014 Hexq;Olato-u,
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.60
10/1412014
AKE
butediene
Sludge Sample
001
1012/2014 Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA $270 C
1
0.13
10/1412014
AKE
Sludge Sample
001
10/2r2014 Hexachloroethane
0.10
NO mgiL
Sludge
EPA 8270 C
1
3.0
10114/2014
AKE
Sludge Sample
001
10/2/9014 Nitrobenzene
0.10
NO mg/L
Sludge
EPA 8270 C
1
2.0
10/14/2014
AKE
Sludge Sample
001
IOIMO14 Pentaohlorophenol
0.26
NO, mgll.
Sludge
EPA 8270 C
1
100
10/1412014
AKE
Sludge Sample
001
10/2/2014 Pyridine
0.25
NO mg/L
Sludge
EPA 8270 C
1
5.0
1011412014
AKE
SVOC SW-846.- $321 Herbicides-TCLP
Client IN
Lab ID# Collected Analyte
Rep Lntt Result Units
Matrix
Method DF
RegLvl
Run Analyst
Sludge Sample
001 10/2/2014 2,4-D
5.0 ND mg/L
Sludge
EPA 8321 A 1
10
1011312014 AMZ
Sludge Sample
001 1002014 2AS-TP
0.50 NO mg1L
Sludge
EPA 8321 A 1
1.0
10/1312014 AMZ
P e5 aNQ

11/06/2014 09:58 2526414230 PUBLIC WORKS PAGE 11/14
Sammie F,r+vironn+arrral Techaalogles, Inc,
WO#: 14100591
3310 {Yh1 St.
ci -hoga Foils, 01d.44223
Datc Reported: 10/24/2014
TEL: (330)
253.8211 rAX: [phone]
Company: Environment 1, Inc.
iYebslre; [tttnl v,nv.settekcnm
Address: 114 Oakmont Dr
Greenville NC 27858
Received: 10/3/2014
Project#: 305
Clieut ID# Lab ID# Collected Analyte
Result Units
Matrix Method OF RL
Run ,Analyst
Sludge Sample 001 1012/2014 plashpoint (1407)
}140 °F
Sludge EPA 1010 1
1017/2014 TAH
Sludge Sample 001 10/21RO14 Cyanide, Reactive
NO ppm
Sludge EPA 8014 1 0.50
10/M014 TIR
Sludge Sample 001 1012=14 pH
7.3 s.u,
Sludge EPA 9046 D 1
10/812014 AYS
Sludge Sample 0D1 1012/2014 SUll1de, Reactive
30 ppm
Sludge EPA 9034 1 25
101712014 TIR
Pt ws d(e

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11/06/2014 09:58 2526414230 PUBLIC WORKS PAGE 14/14
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Page 9 of 9

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0035595 Facility dame Granville Itarms, Inc. Source Permit No. NC0020044 Source Name Williann;ton wwrp
Laboratory 1
Laboratory 2
Sample or CompositeDate
Parameter (mg/Kg) Class A Cias B
AM. Cistern
Labs, Inca
3/13/2014
Aluminum
N/A
N/A
21,100
Ammonia Nitrogen
N/A
N/A
7,460
Arsenic
41
75
6
Cadmium
39
85
2
Calcium
N/A
N/A
15,700
__._
Copper
],500
4,300
749
Lead
300
840
38
Magnesium
N/A
N/A
3,010
Mercury
17
57
0.4
Molybdenum
N/A
75
6
Nickel
420
420
25
Nitrate -Nitrite Nitrogen
N/A
N/A
60
Percent Solids
N/A
N/A
2.68
PH (no units)
N/A
N/A
7,23
Phosphorus
N/A
N/A
19,800
Potassium
N/A
N/A
3,830
PAN (Inj,/Inc,)
N/A
N/A
20.492
PAN (Surface)
N/A
N/A
16,762
Selenium
100
100
5
_ Sodium
N/A
N/A
5,250
SAR
N/A
N/A
1.64
TEN
N/A
N/A
50,700
Zinc
2,800
7,500
654
"I certify, tinder penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26)

.A',�.J����JC,i4�-\�
3 FIELD LOADING ESTIMATES
Facility Williamston WWII'
Sampling Date 3/13/2014
% Solids 2.68
Mineralization Rate 0.30
Gallons per DT 8,948.07
pH 7.23
Sodium Absorpotion 1.64 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 50,700 lbs./1,000 gal 11.33
Potassium lbs./1,000 gal
0.86
Ammonia Nitrogen (mg/Kg) 7,460.00 lbs./1,000 gal 1.67
Phosphorus lbs./1,000 gal
4.43
Nitrate -Nitrite (mg/Kg) 59.70 lbs./1,000 gal 0.01
Calcium lbs./1,000 gal
3.51
- PLANT AVAILABLE NITROGEN SURFACE APPLIED
Magnesium lbs./1,000 gal
0.67
i PAN (mg/Kg) 16,762 lbs./1,000 gal 3.75
Manganese lbs./1,000 gal
0.21
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
1.72
PAN (mg/Kg) 20,492 lbs./1,000 gal 4.58
Molybdenum lbs./1,000 gal
0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
I st Year
-- _ 2nd Year
3rd Year
4th Year
5th Year
1.
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
6.00
Arsenic lbs./1,000 gal
0.00 .
Cadmium {mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
749.00
Copper lbs./1,000 gal
0.17
Lead (mg/Kg)
38.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.40
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
25.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
654.00
Zinc lbs./1,000 gal
0.15
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TEN
(mg/kg) (lbs/DT)
(-19/g9)
TKN
(mg/kg) (lbs/DT)
(mg/]Kg)
50,700
16,762
33.52
33,938
50,700
20,492 40.98
30,208
33,938
5,091
10.18
28,848
30,208
4,531 9.06
25,677
28,848
2,164
4.33
26,684
25,677
1,926 3.85
23,751
26,684
1,001
2.00
25,683
23,751
891 1.78
22,861
25,683
482
0.96
25,202
22,861
429 0.86
22,432
-Dotal 253498 51.00
Total 28,268 56.54
Equations
1st Yr. PAN (mg/Kg)=(MR - (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MIL/16)

Page: 1 of 2
Report Number: 14-073-0211
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
Lab Number: 98394
Sample Id : TW031314
A&LEastern Laboratories, inc.
Whitepine Road Richmond, 9,( ) 1 Z
wwwaleastern.com
Project: 201206.A10-WILLIAMSTON WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/13/2014.13:00:00
Date Received: 03/14/2014 00:00
Date Reported: 03/25/2014
Total Solids *
2.68
26800
100.0
BW
03/14/2014 15:00
SM-254OG
Moisture *
97.32
100.0
BW
03/14/2014 15:00
SM-254OG
Total Kjeldahl Nitrogen
5.07
50700
10.0
JM
03/17/2014 09:15
SM-4500-NH3C-TKN
Total Phosphorus
1.98
19800
100
KM
03/17/2014 12:04
SW 6010C
Total Potassium
0.38
3830
100
KM
03/17/2014 12:04
SW 6010C
Total Sulfur
0.77
7690
100
KM
03/17/2014 12:04
SW 6010C
Total Calcium
1.57
15700
100
KM
03/17/2014 12:04
SW 6010C
Total Magnesium
0.30
3010
100
KM
03/17/2014 12:04
SW 6010C
Total Sodium
0.53
5250
100
KM
03/17/2014 12:04,
SW 6010C
Total Iron
27300
100
KM
03/17/2014 12:04
SW 6010C
Total Aluminum
21100
100
KM
03/17/2014 12:04
SW 6010C
Total Manganese
929
5
KM
03/17/2014 12:04
SW 6010C
Total Copper
749
5
KM
03/17/2014 12:04
SW 6010C
Total Zinc
654
5
KM
03/17/2014 12:04
SW 6010C
Ammonia Nitrogen
0.75
7460
10.0
JM
03/17/2014 08:44
SM-4500-NH3C
Organic N
4.32
43240
10.0
03/17/2014 08:44
CALCULATION
Nitrate+Nitrite-N
59.7
2.00
JM
03/17/2014 08:45
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
03/17/2014 12:04
SW 6010C
All values are on a dry weight
basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced
in whole or part, nor may
any reference be made
to the work, the results, or the company in any advertising, news release, or other
public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-073-0211
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
Lab Number: 98394
Sample Id: TW031314
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237' [phone] Fax [phone].
www,aleaitern.com
Project: 201206.A10-WILLIAMSTON WWTP
NC CERT#257
REPORT OF ANALYSIS
Total Chromium
51
5
KM
Total Nickel
25
5
KM
Total Lead
38
5
KM
Total Arsenic
6.0
3.0
KM
Total Mercury
<0.4
0.4
KM
Total Selenium
<5.0
5.0
KM
pH (Standard Units)
7.23
2.00
JM
Total Molybdenum
6
5
KM
Soluble Phosphorus
0.03 300
100
JM
Comments:
WATER SOLUBLE P, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "A[" AND "Mn".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Date Sampled: 3/13/2014 13:00:00
Date Received: 03/14/2014 00:00
Date Reported: 03/25/2014
03/17/2014 12:04
SW 6010C
03/17/2014 12:04
SW 6010C
03/17/2014 12:04
SW 6010C
03/17/2014 12:04
SW 6010C
03/17/2014 09:00
SW-7471 B
03/17/2014 12:04
SW 6010C
03/17/2014 08:44
SW-9045D
03/17/2014 12:04
SW 6010C
03/25/2014 08:39
SOLUBLE P IN MANURE
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Microbac Laboratories, Inc. - Wilson Division
3809 Airport Drive NW
Wilson, NC 27896
Tel: [phone]
Certl11991e Q Analysis Report Date: 29-Apr-2014
SCOTT CARPENTER
SOIL PLUS
208 WILLIAMS ST
GREENVILLE NC 27858
USA
Work Order: 2014-03-31-003
Date Received: 28-Mar-2014
Quote: 23-20140328-14
Sample Description: Biosolids
Collection
SIDN
Client Marks
Analysis
Method
Date/Time:
Result
AA46175
Town of
Flash Point,Liquids
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
032714
AA46175
Town of
pH (Corrosivity)
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW .
032714
AA46175
Town of
Reactive Cyanide
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
032714
AA46175
Town of
Reactive Sulfide
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
032714
AA46175
Town of
TCLP,Full (Metals,
Subcontracted
3127/14
10:30
*See Attached
Williamston TW
VOC SVOC Pest @
032714
Herb)
AA46176
Town of Ahoskie A
Flash Point,Liquids
Subcontracted
3/27114
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
pH (Corrosivity)
Subcontracted
3/27114
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
Reactive Cyanide
Subcontracted
3127/14
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
Reactive Sulfide
Subcontracted
3/27/14
13:30 -
*See Attached
032714
AA46176
Town of Ahoskie A
TCLP,Full (Metals,
Subcontracted
3/27/14
13:30
*See Attached
032714
VOC SVOC Pest @
Herb)
C
Reviewed and Approved by: Z'da' G Date:
Kim Hesse
i
vor any teeooacK concerning our services, please contact James Nokes,ISenior Vice President, [e-mail]
or Trevor Boyce, President, at [e-mail]
Chemical and Microbiological Analysis: Environmental — Agrochemical — Food — Pharmaceuticals
Page 1 of 1

® Microbac Laboratories, Inc.
Knoxville Division
® 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY • CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS - NUTRACEUTICALS
Kimberly Hesse
Microbac Laboratories, Inc. -Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406051
CERTIFICATE OF ANALYSIS
Project: Soil Sampling
Date Reported: 4/29/2014
Date Received: 4/1/2014
Cust #: R9024
PO#:
Analyse Result Units Dil Qualifier Limit ­ Analyst Analyzed Method
AA46175 Williamston Sampled: 03/27/2014 00:00
1406061-01 (Solid)
Wet Chemistry
Analyzed By: Microbac Knoxville Division
pH (Corrosivity) 6.0 pH Units 1 H4 SLN 041091201416:00 SW846 9045D
General Chemistry
Analyzed By: Microbac Knoxville Division
Flash Point 95 °F 1 65 SDF 04/16/201417:27 SW846 1010
TCLP Extraction Fluid 1 1 He JNB 041111201411:57 SW846 1311
TCLP Metals by 600017000 Series Methods
Analyzed By: Microbac Knoxville Division
Arsenic
0.0449
mg/L
1
0.0150
JNB
04/11/201420:18
SW8466010B
Barium
0.208
mg/L
1
0.00400
JNB
04/11/201420:18
SW84660108
Cadmium
ND
mg/L
1
0.00750
JNB
04/11/2014 20:16
SW846 6010E
Chromium
ND
mg/L
1
0.00750
JNB
04/11/2014 20:18
SW846 6010B
Lead
0.0248
mg/L
1
0.0200
JNB
04/11/201420:18
SW8466010B
Mercury
ND
Ing&
1
0.000200
JNB
04/151201410:36
SWB46 7470A
Selenium
0.0396
mg/L
1
0.0200
JNB
04111/201420:18
SWB466010B
TCLP Semivolatiles by EPA Method 131118270C
Analyzed Bv: Microbac Knoxville Division
o-Cresol
ND
mg/L
1
0.0400
SLH
04116/201417:28
SW846 8270C
Pyridine
ND
mg/L
1
0.0200
SLH
04/161201417:28
SW846 8270C
meta/para-Cresol
ND
mg/L
1 M2
0.0400
SLH
04/16/201417:28
SW846 8270C
Hexachloroethane
ND
M91L
1
0.0200
SLH
04/16/201417:28
SW846 8270C
Nitrobenzene
ND
mg/L
1
0.0200
SLH
04116/201417:2B
SW846 8270C
Hexachlorobutadiene
ND
mg/L
1
0.0200
SLH
04116/201417:28
SW846 8270C
2,4,6-Trichlorophenoi
ND
mglL
1
0.0200
SLH
04/16/201417:28
SW846 8270C
2,4,5 Tdchlorophenol
ND
mg/L
1
0.0200
SLH
04/16/201417:28
SW846 8270C
2,4-Dinitrotoluene
ND
mg/L
1
0.0200
SLH
04/161201417:28
SW846 8270C
Hexachlorobenzene
ND
mg/L
1
0.0200
SLH
04/16/201417:28
SW846 8270C
Pentachlorophenol
ND
mg/L
1
0.160
SLH
04/16/201417:28
SW846 8270C
1,4-Dichlorobenzene
ND
mg/L
1'
0.0200
SLH
04/16/201417:28
SWe46e27ac
The data and Information an this, and other accompanying documents, represent only the somple(s) analyzed and is rendered upon condition MEMBER
that g is not to be reproduced wholly or In pert for advertising at other purposes without approval from the laboratory,
USDA•EPXMDSHTesting Food Sanitation Consulting Chemical and MlcrdblologtcalAnalysesand Research
Page 1 of 9
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Knoxville Division
®®� 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY • MICROBIOLOGY FOOD SAFETY CONSUMER PRODUCTS -WATER • AIR . WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Microbac Laboratories, Inc. -Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406051 Project: Soil Sampling
Date Reported: 4/29/2014
Date Received: 4/1/2014
Cust #: R9024
PO#:
Analyte Result Units Dil Qualifier Reporting Analyst Analyzed Method
Limit
AA46175 Williamston Sampled: 03/27/2014 00:00
1406051-01 (Solid)
TCLP Semivolatiles by EPA Method 1311/8270C
Surrogate: 2-Fluorobiphenyl
10-108
77.1 %
04/16/201417:28
SW846 8270C
Surrogate: 2-Fluorophenol
10-89.8
43.1 %
04/16/201417:28
SW846 8270C
Surrogate: Nitrobenzene-0
10-107
83.8 %
04/16/201417.28
SW846 8270C
Surrogate: Phenol-d5
10-86.9
40.4 %
04/16/201417:28
SW846 8270C
Surrogate. Terphenyl--d14
10-111
90.2 %
04/16/201417:28
SW846 8270C
Surrogate: 2,4,6-Tdbromophenol
10-126
42.8%
04/161201417:28
SW846 8270C
TCLP HERBICIDES
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
2,4-D
ND
ug/L
1
U, H1
20.0
ECL
04/17/201419:34
SW8151A
2,4,5 TP (Silvex)
ND
ug/L
1
U. H1
2.00
ECL
04/17/201419:34
SW8151A
Surrogate: $4-Dichlorophenylaceticacid
20-144
43.6 %
04/17/201419:34
SW8151A
TCLP Pesticides
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
Endrin
ND
ug/L
1
U, H1
0.500
ECL
04117/201422:29
SW8081A
Lindane
ND
ug/L
1
U. H1
0.500
ECL
04/17/2014 22:29
SW8081A
Methoxychlor
ND
ug/L
1
U. H1
0.500
ECL
04/17/2014 22:29
SW8081A
Toxaphene
ND
ug/L
1
U, H1
10.0
ECL
04117/201422:29
SW8081A
Chlordane
ND
ug/L
1
U, H1
10.0
ECL
04/17/2014 22:29
SW8081A
Heptachlor
ND
ug/L
1
U, H1
0.600
ECL
04/17/2014 22:29
SW8081A
Heptachlor Epoxide
ND
ug/L
1
U, H1
0.500
ECL
04/17/2014 22:29
SW8081A
alpha Chlordane
ND
ug/L
1
U, H1
0.500
ECL
04/1712014 22:29
SW8081A
gamma Chlordane
ND
ug/L
1
U, H1
0.500
ECL
04/17/2014 22:29
SW8081A
Surrogate: 2,4,5.6-Tetrachloro-m Wene
20-180
37.2 %
04/17/201422:29
SW8081A
Surrogate: Decach/orobiphenyl
25-140
64.6 %
04117/201422:29
SIN8081A
The data and Information on this, and other accompanying documents, represent ontythe sample(s) analyzed and is rendered upon condition MEMBER
- that It Is not to be reproduced when or part for advertising or other purposes without approval from the laboratory.
USDA-EPA-NIOSH Testing Food Sanitatian Consulting Chemical and MicrobiologlralAnayses and Research.
Page 2 of 9
www.microbac.com [e-mail]
I

_ . ® Microbac Laboratories, Inc.
Knoxville Division
505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone].
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY • CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS - NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson Date Received: 4/1/2014
3809 Airport Drive oust#: R9024
Wilson, NC 27896 PO#:
Workorder: 1406051 Project: Soil Sampling
Analyse Result Units Dil Qualifier Limit Reporting Analyst Analyzed Method
t
AA46175 Williamston Sampled: 03/27/2014 00:00
1406051.01 (Solid)
GCMS Volatiles
Analvzed Bv: Microbac Laboratories. Inc. - Chicaaoland
1,1-Dichloroethene
ND
mg/L
10
H
0.050
jln
04/25/201413:34
131118280E
1,2-Dichloroethane
ND
mg/L
10
H
0.050
jln
04/25/201413:34
131118260E
2-Butanone <z— yl\v,K
ND
mg/L
10
H
0.10
jin
04/25/201413:34
1311/8260B
Benzene
ND
mg/L
10
H
0.050
jln
04/25/201413:34
1311/8260B
Carbon tetrachloride
ND
mg/L
10
H
0.050
jln
04/25/201413:34
1311/82609
Chlorobenzene
ND
mg/L
10
H
0.050
jln
04/25/201413:34
131118260E
Chloroform
ND
mg/L
10
H
0.050
jln
04/25/201413:34
1311/8260B
Tetrachloroethene
ND
mgtL
10
H
0.050
jln
04/251201413:34
1311/8260B
Trichloroethene
ND
mg/L
10
H
0.050
jln
04/25/201413:34
1311/826013
Vinyl chloride
ND
mg/L
10
H
0.020
jln
04/25/201413:34
131118260B
1,4-Dichlorobenzene
ND
mg/L
10
H
0.10
jin
04/251201413:34
1311/8260B
Surrogate: 1,2-Dichloroethane-d4
74.5-132
H
106 %
04/25/201413:34
131118260E
Surrogate: 4-Bromotiuorobenzene
80-120
H
93.8 %
04/25/201413:34
131118260B
Surrogate: Dibromofluoromethane
80-120
H
101 %
04/25/201413:34
131118260B
Surrogate: Toluene-d8
80-120
H
101 %
04/25/201413:34
131118260E
Wet Chemistry
Analyzed By: Microbac Laboratories, Inc. - Chicaaoland
Reactive Cyanide ND mg/Kg 1 H 2.0 AGRIE 04/16/201413:a0 Chapter7/9014
Reactive Sulfide ND mg/Kg 1 H 2.0 EB 04/15/2014 09:15 Chapter 7/9034
AA46176 Williamston Sampled: 03/27/2014 00:00
1406061-01RE1 (Solid)
TCLP Metals by 6000/7000 Series Methods
Analyzed By: Microbac Knoxville Division
Silver ND mg/L 1 0.00100 JNB 04/16/2014 21:31 SW846 6010B
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406051-02 (Solid)
Wet Chemistry
The data and Infannallon on this, and other accompanying documents, represent only the seinplais) analyzed and Is rendered upon condition MEMBER
that it is not to be reproduced wholly or In pert for advedlsing or other purposes without approval from the laboratory.
USDXEPA•NIOSH Testing Fcod Sanitation Consuldng Chemtcat and Mlaablologieal Analyses and Research
Page 3 of 9
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Yuoxvilte Division
®®� 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fa=8165.984.8616
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTS -WATER • AIR - WASTES - FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Microbac Laboratories, Inc. - Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406051 Project: Soil Sampling
Certifications
Date Reported: 4/29/2014
Date Received: 4/1/2014
oust #: R9024
PO#:
Code
Description
Number
Expires ._
A2LA
A2LA ISO/IEC 17025 Env. DoD Testing
3045.02
09/30/2014
A2LPL
A2LA ISO/IEC 17025 Biological Testing
3045.01
09/30/2014
A2LAB-KNX
ISO 17025 KNX food
3131.01
05/31/2015
A2LAB-NSH
ISO 17025 NSH food
3131.02
06/3012014
FL
State of Florida NELAC
E87966
06/30/2014
GA
Georgia Dept Natural Resources
980
04/13/2014
ILDPH
Illinois DOPH Micro analysis of drinking water
1755266
12/31/2016
ILEPA
Illinois EPA wastewater and solid waste analysis
200064
04/01/2015
INDEM
Indiana DEM support lab wastewater and solid waste
A305-9-292
12/31/2013
INDH
Indiana SDH Micro analysis of drinking water
M-45-8
12/31/2016
INSDH
Indiana SDH chemical analysis of drinking water
C-45-03
08/14/2016
KSDOH
Kansas Dept Health & Env. NELAP
E-10397
01/31/2015
KYEPP
Kentucky EPPC analysis Underground Storage Tanks
75
01/31/2015
NCEW
NC Environmental
678
12/31/2013
NYDOH
New York State Department of Health Wadsworth
49179
04/01/2015
NYDOH-1
New York State Department of Health Wadsworth
49386
04/01/2016
PADEP
Pennsylvania Department of Environmental Protect
68-04863
07/31/2014
PEDEP
Pennsylvania DEP Registration for Air analysis
68-04863
TN_DW
North Carolina DENR NPDES effluent, surface water
TNNC597
12/31/2014
TN DW
State of Tennessee
TN02017
04/30/2014
USDA
US Department of Agriculture
11/30/2013
USDAS
USDA Permit To Receive Soil
P330-12-00174
06/20/2015
WADOE
Washington State Department of Ecology
C992
10/22/2014
WSDNR
Wisconsin DRN chemical analysis wastewater, solids
998036710
08/31/2014
The data and information on this, and other eccompany(ng documents, represent only the sample(s) analyzed and Is rendeted upon condition MEMBER
that ti Is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory. ,
USDA-EPA-MOSH Testing Food Senhatlon ConsuNng Chem[cel and Mlaoblological Analyses and Research
Page 7 of 9
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® Microbac Laboratories, Inc.
Knoxville Division
Cr® 505 F. Broadway Avenue Maryville, TN 37804 965.977.1200 Fax:[phone]
ac
Tri-Cities, TN 423.926.6385 J Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson Date Received: 4/1/2014
3809 Airport Drive Cust #: R9024
Wilson, NC 27896 PO#:
Workorder: 1406051 Project: Soil Sampling
Notes and Definitions
U Not detected at or above adjusted sample detection limit
R1 Duplicate RPD is outside of acceptance limits.
01 Flashpoint temperature went up with each of the four tests. Even with vigorous shaking it appears volitile portion lessened
each time.
M5 Post digestion spike is outside of acceptance limits.
M3 Matrix spike recovery is outside of acceptance limits. The post digestion spike recovery is acceptable.
M2 Matrix spike recovery is outside of acceptance limits, biased low.
He Sample was analyzed past holding time.
H4 The test was performed outside of the EPA recommended holding time of 15 minutes.
H1 [Undefined]
H Analyte was prepared and/or analyzed outside of the analytical method holding time
DET Analyte DETECTED
ND Andlyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on a dry weight basis
RPD Relative Percent Difference
The data and Information an this, and other accompanying documents, represent only the semplets) analyzed and Is rendered upon condition MEMBER
that it Is not to be reproduced whally at in part for advertising or other purposes without approval from the labondary.
USDA-EPA•NIOSHTesWg Food Sanitation Consulting Chemical and NcroblologlcalAnsysesand Research i.
1<
Page B of 9
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Knoxville Division
® 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
wtxw.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY CONSUMER PRODUCTS •WATER • AIR - WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
_ Kimberly Hesse
Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson
Data Received: 4/1/2014
3809 Airport Drive
cost #: R9024
Wilson, NC 27896
Pam.
Workorder: 1406051 Project: Soil Sampling
Microbac Laboratories, Inc. - Knoxville
i
Maraea Branner, Project Manager
Thank you for your business. For any feedback, please contact Ashley Morris,
at ashleymorris@mlcrobaacom. You may also contact Trevor Boyce,
t President, at [e-mail].
F
'. As regulatory limits change frequently, Microbac advises the recipient of this report to confirm such limits with the appropriate Federal, state, or local
authorities before acting in reliance on the regulatory limits provided.
_ The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and Is rendered upon condition MEMBER
that It is not to be reproduced wholly or In part for advertising or other purposes without approval from the labaretary.
USDA-EPA-NIOSHTesthtg Food sanitation Consulting Chemical and MicrohlologlcalAnalysesand Research
Page 9 of 9
www.microbac.com [e-mail]

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# EB County Martin Crop 1 Common Bermudagrass Pasture
Facility Name Granville Farms, Inc. Field Name 1 SoilSeries Goldsboro Crop 1 Pan 230
IandOwmer Joseph Paul Bunting Acres Permited 10.19 Soil Abbrevation: GoA Crop 2 Annual Ryegrass - Pasture
Operator Eddie Brown Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization TKN Ammonia Nitrite
PAN
PAN Crop
05/09/2014 Gallons 61,200 2.68
10.19
0.67 6.84
Williamston WWTP
Dry 0
Surface
26.58
0.50
0.30 50,700
7,460.00 59.70
22.50
Crop 1
05/12/2014 Gallons 54,400 2.68
10.19
0.60 6.08
Williamston WW'IP
Dry 0
Surface
23.63
0.50
0.30 50,700
7,460.00 59.70
20.00
Crop 1
05/20/2014 Gallons 20,400 2.68
10.19
0.22 2.28
Williamston WWTP
Dry 0
Surface
8.86
0.50
0.30 50,700
7,460.00 59.70
7.50
Crop 1
Total Volume Applied 136,000
Total Dry Tons 15.20
Sum Total P
59.07
Total
50.00
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year 0.018 0.006
2.234
0.152
0.113 0.001
0.018
0.075
0.015
1.951
Lime (T/Ac.) Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year 8.021 4.008
34.461
10,157
18.131 0.802
10.027
10.067
10.019
28.827
Cumulative Total 8.039 4.014
36.695
10.309
18.244 0.803
10.045
10.142
10.034
30.778
Permitted CPLR 36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
JW14 1�q�c **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# EB County Martin Crop 1 Common Bermudagrass Pasture
Facility Name Granville Farms, Inc. Field Name 2 SoilSeries Goldsboro Crop 1 Pan 230
Landowner Joseph Paul Bunting Acres Permited 16.21 Soil Abbrevation: GoA Crop 2 Annual Ryegrass - Pasture
Operator Eddie Brown Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used DT/Ac.
Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia Nitrite
PAN
PAN Crop
05/13/2014
Gallons
61,200
2.68
16.21
0.42
6.84
Williamston WWTP
Dry
0
Surface
16.71
0.50
0.30
50,700
7,460.00
59.70
14.14
Crop 1
05/14/2014
Gallons
34,000
2.68
16.21
0.23
3.80
Williamston WWTP
Dry
0
Surface
9.28
0.50
0.30
50,700
7,460.00
59.70
7.96
Crop 1
05/15/2014
Gallons
47,600
2.68
16.21
0.33
5.32
Williamston WWTP
Dry
0
Surface
13.00
0.50
0.30
50,700
7,460.00
59.70
11.00
Crop 1
05/19/2014
Gallons
47,600
2.68
16.21
0.33
5.32
Williamston WWTP
Dry
0
Surface
13.00
0.50
0.30
50,700
7,460.00
59.70
11.00
Crop 1
05/20/2014
Gallons
40,800
2.68
16.21
0.28
4.56
Williamston WWTP
Dry
0
Surface
11.14
0.50
0.30
50,700
7,460.00
59.70
9.43
Crop 1
Total Volume Applied
231,200
Total Dry Tons 25.84
Sum'I'otal P 63.12
Total 53.43
Total
Reported in Gallons
Arsenic
Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc,
Crop 1
Crop 2
PAN
PAN
Current Year
0.019
0.006
2.388 0.163
0.121
0.001
0.019
0.080
0.016
2.085
(lbs./Ac.)
Lime ("I'/Ac.) Datc
(lbs./Ac.)
Prior Year
6.018
8.006
36.282 16.129
20.110
0.802
12.023
14.058
10.016
22.221
Cumulative Total
6.037
8.013
38.669 16.292
20.231
0.803
12.042
14.138
10.032
24.306
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# EB County Martin Crop 1 Common Bermudagrass Pasture
Facility Name Granville Farms, Inc. Field Name 3 SoilSeries Norfolk Crop I Pan 230
Landowner Nell B. Brown Acres Permited 12.88 Soil Abbrevation: NoA Crop 2 Annual Ryegrass - Pasture
Operator Eddie Brown Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia Nitrite
PAN
PAN Crop
05/21/2014
Gallons
26,000
3.00
12.88
0.25
3.25
Ahoskie WWTP
Dry
0
Surface
12.68
0.50
0.30
51,300
6,670.00
43.30
8.47
Crop 1
05/22/2014
Gallons
26,000
3.00
12.88
0.25
3.25
Ahoskie WWI'P
Dry
0
Surface
12.68
0.50
0.30
51,3W
6,670.00
43.30
8.47
Crop 1
05/23/2014
Gallons
39,000
3.00
12.88
0.38
4.88
Ahoskie WWTP
Dry
0
Surface
19.02
0.50
0.30
51,300
6,670.00
43.30
12.70
Crop 1
05/27/2014
Gallons
39,000
3.00
12.88
0.38
4.88
Ahoskie WWTP
Dry
0
Surface
19.02
0.50
0.30
51,300
6,670.00
43.30
12.70
Crop I
Total Volume Applied
130,000
Total Dry Tons 16.26
Sum Total P 63.39
Total 42.34
Total
Reported in Gallons
lrsenic
Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.020
0.010
2.232 0.263
0.187
0.004
0.051
0.121
0.025
5.303
(lbs./Ac.)
Lime T/Ac.) Date
(lbs./Ac.)
Prior Year
6.022
4.008
47.811 12.149
18.129
0.802
10.026
10.069
10.019
47.470
Cumulative Total
6.042
4.018
50.044 12.411
18.316
0.806
10.077
10.190
10.044
52.773
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Jmxls�c **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# EB County Martin Crop 1 Common Bermudagrass Pasture
Facility Name Granville Farms, Inc. Field Name 4 SoilSeries Norfolk Crop 1 Pan 230
Landowner John Lee Beach, Sr. Acres Permited 8.74 Soil Abbrevation: NoA Crop 2 Annual Ryegrass - Pasture
Operator Eddie Brown Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied %Solids Used
DT/Ac. Tons
Source
Condition Precip Method
P
Volatilization
Mineralization TEN Ammonia Nitrite
PAN
PAN Crop
05/07/2014 Gallons 68,000 2.68
8.74
0.87 7.60
Williamston W 717
Dry 0
Surface
34.43
0.50
0.30 50,700
7,460.00 59.70
29.15
Crop 1
05/08/2014 Gallons 61,200 2.68
8.74
0.78 6.84
Williamston WWTP
Dry 0
Surface
30.99
0.50
0.30 50,700
7,460.00 59.70
26.23
Crop 1
Total Volume Applied 129,200
Total Dry Tons 14.44
Sum Total P
65.42
Total
55.38
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
lead
Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year 0.020 0.007
2.475
0.169
0.126
0.001
0.020
0.083
0.017
2.161
Lime (T/Ac.) Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year 6.029 4.010
14.361
10.182
10.167
0.803
10.034
10.093
10.025
12.635
Cumulative Total 6.049 4.016
16.835
10.350
10.293
0.804
10.054
10.176
10.041
14.796
Permitted CPLR 36 34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# EB County Martin Crop 1 Common Bermudagrass Pasture
Facility Name Granville Farms, Inc. Field Name 5 SoilSeries Goldsboro Crop 1 Pan 230
LandOwner Nell B. Brown Acres Permited 7.89 Soil Abbrevation: GoA Crop 2 Annual Ryegrass - Pasture
Operator Eddie Brown Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop I
Crop 2
Date Measurement Applied % Solids Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization TKN Ammonia Nitrite
PAN
PAN Crop
05/05/2014 Gallons
54,400 2.68
7.89
0.77 6.08
Wilhamston WWTP
Dry 0
Surface
30.51
0.50
0.30 50,700
7,460.00 59.70
25.83
Crop 1
05/06/2014 Gallons
61,200 2.68
7.89
0.87 6.84
Williamston WWTP
Dry 0
Surface
34.33
0.50
0.30 50,700
7,460.00 59.70
29.06
Crop 1
Total Volume Applied
115,600
Total Dry Tons 12.92
Sum Total P
64.94
Total
54.89
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead
Mercury
Molvbdenum
Nickel Selenium
Zinc
Crop 1
PAN
Crop 2
PAN
Current Year
0.020 0.007
2.453
0.167
0.124
0.001
0.020
0.082
0.016
2.142
Lime (T/Ac. Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year
6.000 4.000
44.000
10.000
14.000
0.800
10.000
10.000
10.000
42.000
Cumulative Total
6.020 4.007
46.453
10.167
14.124
0.801
10.020
10.082
10.016
44.142
Permitted CPLR
36 34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Apphcadon Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQW35595 Site# JBS County Edgecombe Crop 1 Common Bermudagrass Hay
Facility Name Granville Farms, Inc. Field Name 11 SoilSeries Altavista-P Crop 1 Pan 207
LandOwner JBS Group, LLC Acres Permited 10.73 Soil Abbrevation: AaA Crop 2 Annual Ryegrass - Hay
Operator W3F Farmrs, Inc. Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement
Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization TKN Ammonia Nitrite PAN
PAN
Crop
01/09/2014 Gallons
70,000 1.60
10.73
0.44 4.67
Contenmea MSD WWTP
Moist 0
Surface
8.24
0.50
0.30 39,422
4,696.00 317.00
11.39
Crop 2
01/10/2014 Gallons
28,000 1.60
10.73
0.17 1.87
Contentnea MSD WWTP
Moist 0
Surface
3.29
0.50
0.30 39,422
4,696.00 317.00
4.56
Crop 2
01/14/2014 Gallons
49,000 1.60
10.73
0.30 3.27
Contenmea MSD WWI)
Moist 0
Surface
5.77
0.50
0.30 39,422
4,696.00 317.00
7.97
Crop 2
Total Volume Applied
147,000
Total Dry Tons 9.81
Sum Total P
17.30
Total
23.92
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
'Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.005 0.005
0.627
0.051
0.038 0.001
0.009
0.029
0.009
1.682
LimeT/Ac.) Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year
0.025 0.013
1.961
0.418
0.138 0.002
0.059
0.160
0.035
5.039
Cumulative Total
0.029 0.018
2.588
0.469
0.176 0.003
0.068
0.190
0.044
6.721
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# JBS County Edgecombe Crop 1 Wheat, Grain
Facility Name Grenville Fawns, Inc. Field Name 12 SoilSeries Dogue-P Crop 1 Pan 116
LandOwner JBS Group, LLC Acres Permited 12.30 Soil Abbrevation: DgA Crop 2 Sorghum, Grain
Operator WJF Farmrs, Inc. Crop 2 Pan 50
Volume Acres Dry
Date Measurement Applied %Solids Used DT/Ac. Tons
12/19/2014 Gallons 54,681 3.37 12.30 0.62 7.68
Source
Neuse River WWI?
Soil Application
Condition Precip Method
Moist 0 Surface
Total
P
52.91
Nitrate- Crop I
Volatilization Mineralization TKN Ammonia Nitrite PAN
0.50 0.3 56,558 47,359.05 174.00 33.25
Crop 2
PAN Crop
Crop 1
Total Volume Applied 54,681
Total Dry Tons 7.68
Sum Total P
52.91
Total 33.25
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year 0.005 0.006
0.431
0.036
0.035
0.000
0.017
0.031
0.006
1.291
LimeT/Ac.) (lbs./Ac.)
Date
(lbs./Ac.)
Prior Year 0.052 0.011
1.617
0.544
0.183
0.002
0.058
0.098
0.041
4.384
Cumulative Total 0.057 0.016
2.048
0.581
0.218
0.003
0.074
0.129
0.047
5.675
Permitted CPLR 36 34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
1�,Awx &M�L **Volatilization Rate: Surface - 0.5, Injection/Incotporation -1.0
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# JBS County Edgecombe Crop 1 Wheat, Grain
Facility Name Granville Farms, Inc. Field Name 13 SoilSeries Altavista-P Crop 1 Pan 125
Landowner JBS Group, LLC Acres Permited 24.60 Soil Abbrevation: AaA Crop 2 Soybeans, Manured, Full Season
Operator WJF Farmrs, Inc. Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied %Solids Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization
TRN Ammonia Nitrite
PAN
PAN Crop
12/08/2014 Gallons
32,500 3.00
24.60
0.17 4.07
Ahoskie WWTP
Moist
0 Surface
8.30
0.50
0.30
51,300
6,670.00
43.30
5.54
Crop 1
12/09/2014 Gallons
32,500 3.00
24.60
0.17 4.07
Ahoskie WW"
Moist
0 Surface
8.30
0.50
0.30
51,300
6,670.00
43.30
5.54
Crop 1
12/10/2014 Gallons
45,500 3.00
24.60
0.23 5.69
Ahoskie WWTP
Moist
0 Surface
11.62
0.50
0.30
51,300
6,670.00
43.30
7.76
Crop 1
12/11/2014 Gallons
84,500 3.00
24.60
0.43 10.57
Ahoskie WWTP
Moist
0 Surface
21.57
0.50
0.30
51,300
6,670.00
43.30
14.41
Crop 1
12/12/2014 Gallons
6,500 3.00
24.60
0.03 0.81
Ahoskie WWTP
Moist
0 Surface
1.66
0.50
0.30
51,300
6,670.00
43.30
1.11
Crop 1
Total Volume Applied
201,500
Total Dry Tons 25.21
Sum Total P
51.44
Total
34.36
Total
Reported in Gallons Arsenic
Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.016 0.008
1.812
0.213
0.152 0.003
0.041
0.098
0.020
4.304
Lime ('T/Ac.) Date
(lbs./Ac.)
(kbs./Ac.)
Prior Year
0.103 0.028
6.150
0.915
0.549 0.010
0.133
0.223
0.093
13.713
Cumulative Total
0.120 0.036
7.961
1.128
0.700 0.013
0.174
0.322
0.113
18.016
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# JBS County Edgecombe Crop 1 Com, Grain
Facility Name Granville Farms, Inc. Field Name 17 SoilSeries Altavista-P Crop 1 Pan 148
LandOwner JBS Group, LLC Acres Permited 29.51 Soil Abbrevation: AaA Crop 2 Sorghum, Grain
Operator WJF Farmrs, Inc. Crop 2 Pan 50
Volume Acres Dry
Date Measurement Applied % Solids Used DT/Ac. Tons
03/11/2014 Gallons 63,000 3.57 29.51 0.32 9.38
Source
Town of TarboroWWTP
Soil Application Total
Condition Precip Method P
Moist 0 ction/Incorpora 3.41
Nitrate- Crop 1
Volatilization Mineralization TKN Ammonia Nitrite PAN
1.00 0.30 28,439 1,210.00 7.78 5.97
Crop 2
PAN Crop
crop
Total Volume Applied 63,000
Total Dry Tons 9.38
Sum Total P 3.41
Total 5.97
Total
Reported in Gallons Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel Selenium
"Zinc
Crop 1
PAN
Crop 2
PAN
Current Year 0.002 0.000
0.103 0.032
0.011
0.000
0.003
0.005 0.003
0.395
LimeT/Ac.) Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year 0.043 0.017
3.525 0.549
0.280
0.005
0.087
0.256 0.051
9.425
Cumulative Total 0.045 0.018
3.628 0.582
0.291
0.005
0.090
0.261 0.054
9.820
Permitted CPLR 36 34
1338
267
15
374 89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. `I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
2 1 % 2015 ****C.P.L.R: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# 111S County Edgecombe Crop 1 Wheat, Grain
Facility Name Granville Farms, Inc. Field Name 2 SoilSeries Dogue-P Crop 1 Pan 116
LandOwner JBS Group, LLC Acres Permited 12.83 Soil Abbrevation: DgA Crop 2 Soybeans, Manured, Full Season
Operator WJF Fames, Inc. Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied % Solids Used DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization Mineralization
TEN Ammonia Nitrite
PAN
PAN Crop
12/02/2014 Gallons
30,474 3.37
12.83
0.33 4.28
Neuse River WWTP
Moist
0 Surface
28.27
0.50
0.3
56,558
47,359.05 174.00
17.77
Crop 1
12/03/2014 Gallons
18,367 3.37
12.83
0.20 2.58
Neuse River WWTP
Moist
0 Surface
17.04
0.50
0.3
56,558
47,359.05 174.00
10.71
Crop 1
12/04/2014 Gallons
36,509 3.37
12.83
0.40 5.13
Neuse River WWTP
Moist
0 Surface
33.87
0.50
0.3
56,558
47,359.05 174.00
21.28
Crop 1
12/12/2014 Gallons
45,235 3.37
12.83
0.50 6.36
Neuse River WWTP
Moist
0 Surface
41.96
0.50
0.3
56,558
47,359.05 174.00
26.37
Crop 1
Total Volume Applied
130,585
Total Dry Tons 18.35
Sum Total P
121.14
Total
76.13
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercun'
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.013 0.013
0.987
0.083
0.080 0.001
0.038
0.070
0.015
2.956
Lime /Ac. Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year
0.003 0.002
0.299
0.026
0.021 0.000
0.005
0.013
0.005
0.915
Cumulative Total
0.016 0.015
1.286
0.109
0.101 0.001
0.043
0.083
0.020
3.871
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# JBS County Edgecombe Crop 1 Wheat, Grain
Facility Name Granville Farms, Inc. Field Name 21 SoiLSeries Porstmouth Crop 1 Pan 121
1 AndOwner JBS Group, LLC Acres Permited 31.70 Soil Abbrevation: Pu Crop 2 Sorghum, Grain
Operator WJF Famtrs, Inc. Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement
Applied % Solids
Used DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization
TKN Ammonia Nitrite
PAN
PAN Crop
11/19/2014 Gallons
45,500 3.00
31.70
0.18 5.69
Ahoskie WWfP
Moist
0 Surface
9.01
0.50
0.30
51,300
6,670.00
43.30
6.02
Crop 1
11/21/2014 Gallons
65,000 3.00
31.70
0.26 8.13
Ahoskie WWIP
Moist
0 Surface
12.88
0.50
0.30
51,300
6,670.00
43.30
8.60
Crop 1
11/24/2014 Gallons
52,000 3.00
31.70
0.21 6.51
Ahoskie WWI'P
Moist
0 Surface
10.30
0.50
0.30
51,300
6,670.00
43.30
6.88
Crop 1
12/01/2014 Gallons
65,000 3.00
31.70
0.26 8.13
Ahoskie VAN P
Moist
0 Surface
12.88
0.50
0.30
51,300
6,670.00
43.30
8.60
Crop 1
12/02/2014 Gallons
58,500 3.00
31.70
0.23 7.32
Ahoskie WWTP
Moist
0 Surface
11.59
0.50
0.30
51,300
6,670.00
43.30
7.74
Crop 1
12/03/2014 Gallons
52,000 3.00
31.70
0.21 6.51
Ahoskie WWPP
Moist
0 Surface
10.30
0.50
0.30
51,300
6,670.00
43.30
6.88
Crop 1
12/04/2014 Gallons
32,500 3.00
31.70
0.13 4.07
Ahoskie WWl'P
Moist
0 Surface
6.44
0.50
0.30
51,300
6,670.00
43.30
4.30
Crop 1
12/05/2014 Gallons
45,500 3.00
31.70
0.18 5.69
Ahoskie WWTP
Moist
0 Surface
9.01
0.50
0.30
51,300
6,670.00
43.30
6.02
Crop I
Total Volume Applied
416,000
Total Dry Tons 52.04
Sum Total P
82.41
Total
55.05
Total
Reported in Gallons Arsenic
Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Scicnium
Zinc
Crop 1
PAN
Crop 2
PAN
Current Year
0.026 0.013
2.903
0.341
0.243 0.005
0.066
0.158
0.033
6.895
Limc (T/Ac.) Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year
0.057 0.008
1.992
0.510
0.206 0.003
0.049
0.094
0.037
4.516
Cumulative Total
0.083 0.021
4.894
0.852
0.449 0.008
0.115
0.252
0.069
11.411
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# JBS County Edgecombe Crop 1 Wheat, Grain
Facility Name Granville Farms, Inc. Field Name 22 SoilSeries Roanoke Crop 1 Pan 106
LandOwner JBS Group, LLC Acres Permited 16.49 Soil Abbrevation: Ro Crop 2 Com, Grain
Operator WJF Fames, Inc. Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip Method
P
Volatilization
Mineralization
TKN
Ammonia Nitrite
PAN
PAN Crop
08/18/2014
Gallons
14,000
2.52
16.49
0.09
1.47
Stantonsburg WWTP
Dry
0 ction/Incorpora
3.94
1.00
0.3
2,380
2,380.00
575.00
0.53
Crop 1
08/20/2014
Gallons
21,000
2.52
16.49
0.13
2.21
Stantonsburg WWTP
Dry
0 ction/Incorpora
5.92
1.00
0.3
2,380
2,380.00
575.00
0.79
Crop 1
08/21/2014
Gallons
28,000
2.52
16.49
0.18
2.94
Stantonsburg WWTP
Dry
0 ction/Incorpora
7.89
1.00
0.3
2,380
2,390.00
575.00
1.05
Crop 1
08/22/2014
Gallons
14,000
2.52
16.49
0.09
1.47
Stantonsburg WWTP
Dry
0 ction/Incorpora
3.94
1.00
0.3
2,380
2,380.00
575.00
0.53
Crop 1
Total Volume Applied
77,000
Total Dry Tons 8.09
Sum Total P 21.69
Total 2.90
Total
Reported in Gallons
Arsenic
Cadmium
Copper Chromium
Lead
Mercury
Molvbdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.003
0.002
0.242 0.023
0.010
0.001
0.005
0.016
0.005
0.418
(lbs./Ac.)
Lime (T/Ac.) Date
(Ibs./Ac.)
Prior Year
0.017
0.009
1.402 0.175
0.111
0.004
0.035
0.062
0.021
2.846
Cumulative Total
0.020
0.011
1.644 0.198
0.120
0.005
0.040
0.078
0.026
3.264
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# JBS County Edgecombe Crop 1 Wheat, Grain
Facility Name Granville Farms, Inc. Field Name 3 SoilSeries Dogue-P Crop 1 Pan 116
LandOwner JBS Group, LLC Acres Permited 17.90 Soil Abbrevation: DgA Crop 2 Soybeans, Manured, Full Season
Operator WJF Farmrs, Inc. Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Daw Measurement
Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization TKN Ammonia Nitrite
PAN
PAN Crop
12/15/2014 Gallons
65,443 3.37
17.90
0.51 9.20
Neuse
River WWTP
Moist 0
Surface
43.52
0.50
0.3 56,558
47,359.05 174.00
27.35
Crop 1
12/16/2014 Gallons
31,914 3.37
17.90
0.25 4.48
Neuse River WWTP
Moist 0
Surface
21.22
0.50
0.3 56,558
47,359.05 174.00
13.34
Crop 1
Total Volume Applied
97,357
Total Dry Tons 13.68
Sum Total P
64.74
Total
40.68
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.007 0.007
0.528
0.044
0.043
0.001
0.020
0.038
0.008
1.580
Lime (T/Ac.) Date
(]bs./Ac.)
(lbs./Ac.)
Prior Year
0.002 0.002
0.241
0.021
0.017
0.000
0.004
0.010
0.004
0.738
Cumulative Total
0.009 0.008
0.769
0.065
0.060
0.001
0.024
0.048
0.012
2.318
Permitted CPLR
36 34
1338
267
15
374
89
2498
" I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
�(, **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# JBS County Edgecombe Crop 1 Annual Ryegrass - Hay
Facility Name Granville Farms, Inc. Field Name 32 SoilSeries Altavista-P Crop 1 Pan 125
LandOwner JBS Group, LLC Acres Permited 10.40 Soil Abbrevation: AaA Crop 2 Sorghum
Operator WJF Farmrs, Inc. Crop 2 Pan 50
Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2
Date Measurement Applied %Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN
10/15/2014 Gallons 7,000 3.34 10.40 0.09 0.97 Town of Tarboro WWTP Dry 0 cdon/Incotpora 2.31 1.00 0.30 34,594 1,043.00 10.70 2.08
Total Volume Applied
7,000
Reported in Gallons
Arsenic
Cadmium
Current Year
0.003
0.000
Prior Year
0.037
0.023
Cumulative Total
0.039
0.023
Permitted CPLR
36
34
Total Dry Tone 0.97
Copper
Chromium
Lead
0.029
0.006
0.004
2.595
0.344
0.191
2.623
0.350
0.195
1338
267
Mercury Molybdenum
0.000 0.001
0.011 0.064
0.012 0.065
15
Sum Total P 2.31
Nickel
Selenium
Zinc
0.002
0.001
0.107
0.126
0.047
4.702
0.127
0.048
4.809
374
89
2498
Total 2.08
Crop 1
PAN
(lbs./Ac.)
Lime T/Ac.) Date
Crop
Crop
Total
Crop 2
PAN
(lbs./Ac.)
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
i� **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0035595 Site# JBS County Edgecombe Crop 1 Wheat, Grain
Facility Name Grenville Farms, Inc. Field Name 6 SoilSeries Altavista-P Crop 1 Pan 125
Landowner JBS Group, LLC Acres Permited 22.50 Soil Abbrevatiom AaA Crop 2 Soybeans, Manured, Full Season
Operator WJF Farmrs, Inc. Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization TKN
Ammonia Nitrite
PAN
PAN Crop
12/17/2014 Gallons 60,831 3.37
22.50
0.38 8.55
Neuse
River WWTP
Moist 0
Surface
32.18
0.50
0.3 56,558
47,359.05 174.00
20.22
Crop 1
12/18/2014 Gallons 60,936 3.37
22.50
0.38 8.56
Neuse
River WWTP
Moist 0
Surface
32.23
0.50
0.3 56,558
47,359.05 174.00
20.26
Crop 1
Total Volume Applied 121,767
Total DryTone 17.11
Sum Total P
64.41
Total
40.48
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year 0.007 0.007
0.525
0.044
0.043
0.001
0.020
0.037
0.008
1.572
Lime (T/Ac.) Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year 0.011 0.005
0.897
0.098
0.075
0.001
0,016
0.038
0.013
2.384
Cumulative Total 0.018 0.012
1.422
0.142
0.118
0.002
0.036
0.076
0.021
3.956
Permitted CPLR 36 34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number. WQ0035595
WWTP Name: Ahosi;ie WW TP NPDES Number. NCO088561
Monitoring Period: 01/01/2014 to 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and altetnative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
. Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 22,949 27,400 29,410 0 1 Grab Samples
Weight)
Analytical Technique SDI 9221 E
Vector Attraction Reduction Performed (40 CFR 503.33): At. 3 (30-day bench)
W "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met:' (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Stewart White, ORC
Prepares Name.and Title (type or print)
z��la�,�
Signature of Preparer* Date
Jason Smith, IT
Land Applier Name and Title (if applicable)(type or print) _
Ir3oZ3 02-13-2015
Signature of Land Applier (if applicable) Date
*Preparet is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Friday, February 13, 2015

Alk
PR0MPT-ACCURATE-,RF_Ll.A8LE-
-.EA-BOPLATORIES, INC
�N-N%lNV.PARLABS.00lNl
REPORT OF ANALYSES
Attn: SCOTT-CARPENTER
SOIL PLUS- P
208 WILLIAMS STREET D
GREENVILLE, NC 27858-
SAMPLE NUMBER-- 113320 SAMPLE ID- TA032514
DATE SAMPLED- 03/2,5/14
DATE RECEIVED- 03/28/14 SAMPLER- SC
TIME RECEIVED- 1000 DELIVERED BY- UPS
Page 1 of 1
ANAL'
ANALYSIS. METHOD DATE
DAY BENCH SCALE TEST VAR 03/3
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 0 3 /3
LABORATORY DIREC
P.O. Box 411483 - Charlotte
Phone: [phone] - Fa
ROJECT NAME:- MAR 14
ATE: 05/07/14

im R L-- A 00
Wd'd Aera�aom -Test
;- Percent - til" "VbIIL
'S
_T
T
26
OUT
004003
FS)'/R--.
FSVR-",'(,Vdn."Kleecky,
8%
F,SV R, -(M -a s 8 a 1-6 hce) 5 0/0i.,
IFS .(12LKldeqk)
II-.P
O; B 6z4 i i4s sit C harlotie�-,NTC -2,82 I" 1493
'(7 04 -588 -8333r�Lr(704)-588'-8335
-- --------

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number. WQ0035595
WWTP Name: Ahoslde VAVfP NPDES Number. NCO088561
Monitoring Period: 01/01/2014to 12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 22,949 27,400 29,410 0 1 Grab Samples
Weight)
Analytical Technique SM 9221 E
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-day bench)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107'have been met"
"I certify; under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
Q requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Stewart White, ORC Jason Smith, NT
Preparer Name and Title (type or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
02-13-2015
Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CPR Part 503.9(r) and 15ANCAC 2T .1102 (26)
Friday, February 13, 2015

ATSNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORD (503 Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number: WQ0035595
WV TP Name: Contentnea 11ISD WWrP NPDES Number: XVQ0001048
Monitoring Period: 01/01/2014 to 03/31/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed;
"Class A" Altemative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 380 1,047 3,451 0
Weight)1 Grab Samples
Analytical Technique SA! 9221 E
Vector Attraction Reduction Performed (40 CFR 503.33): Mt. 4 (Spec. 02 uptake)
a "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement m 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not nret one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment.''
Renee Smith
Preparer Name and Title (type or print)
Signature of Preparer*
Jason Smith, VP
Land Applier Name and Title (if applicable)(type or print)
Ir"la LI 02-16-2015
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Alonday, February 16, 2015

E
�TJAi.PATHOGEN ANTI) VECTOR ATTRACTION REDUCTION'FORM (02'T' mules)
Fality Name: Granville -Farms, lnc WQ Permit Number: NQ0035595
Wr-,,I PName: Contentnca AfSD WkUTP' NPDES Number: WQ6001048
Monit,cl.--mngPeriod: 01/01/2014 to 03/31/2014
Path"a.-wm,-n Reduction (15A NCAC 02T .11.06) - )Please Indicate level achieved and alternative performed:
"Class~. V' Alternative: Not Applicable
If appli.�ble to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class 331 Alternative: Alternative 1
If applij7%nle to alternative performed_("Class B" only) indicate "Process to Further Reduce Pathogens'-': Not Applicable
Fec,-U3Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
ColonnPer Gram of
Total :olids(Dry 380
ight) 1,047 3,451 0 1 Grab Samples
Axialyticf.-e Technique SIM 9221 E
Vect¢ysAttraction Reduction Performed (154 NCAC 02T .1107): Alt. 4 (Spec. 02 uptake)
❑ ill ce- r.*, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
req- an4'--meat in-15A NCAC 02T .1107 have been met."
'QI comfy, under penalty of late, that the pathogen -requirements in 15A NCAC 02T .1106 and the vector attraction_ reduction
requiVnientin 15A NCAC 02T .1107 have not been met.)) (Please note if you check this statement.attach an explanation why
you wave not met one or both of the requirements.)
"This de,1crmination has been made under my direction and supervision in accordance with the system. designed to ensure that
qualifiet3.personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I -am aware that there are, significant penalties for false certification including fine and
imprisonment"
Rcnec'Stnith
Preparer Na-me and Title (type or print)
Signature of Pieparer*
Jason Smith, VP
Land Applier Name and Title (if applicable) (type or print)
113WX 02-16-2015
Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part-503.9(r) and 15A NCAC 2T .1102' (26)
Monday, Febru.uy 10, 9015

till t�a�-`
, ,t � r
2.78,7 1�5-7085
C.M.S.D. (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
XS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON ,NC 28530
Sample
PARAMETERS #1
Total Residue, mgl[ 13960
Fecal Colil'orm (WN), /gram Solids 2364
Sample
#2
15920
879
ID#: 416 A
DATE
COLLECTED: 01/28/14
DATE
REPORTED
: 01/30/14
r
REVIEWED BY:
Sample Sample
Sample
Analysis
Method
#3 #4
#5
Date Analyst
Code
16360 11840
14200
01/28/14 MDD
2540E-97
1039 380
3451
01/28/14 MDD
9221E-06

C.M.S.D. (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON NC 28530
Sample Sample
PARAMETERS #6 #7
ID#: 416 A
DATE COLLECTED: 01/28/14
DATE REPORTED : 01/30/14
REVIEWED BY:
Analysis Method
Date Analyst Code
Total Residue, mg/l 13440 15480 01/28/14 MDD 2540B-97
Fecal Coliform (MPN), /grain Solids 967 504 01/28114 MDD 9221]E-06

Feel-u I)l vG(C.`hCn
J'a-! Q u O ` -C(
SPECIFIC OXYGEN UPTAKE RATE (SOUR)
FOR
AEROBICALLY STABILIZED SLUDGE
Analysis By:�L�f'�.��dYY�+� �1 Date:^y
Sample Point: 7j e'- P-V � - �U—.----
Sample Time: 3' I F7P-)
Air Temp (TA): -i° Sample Temp (T.�):_ Z20 Sample Site D0: _
I Time i Dissolved 02
J KInutes) f ___iimcq/L
(See Attached Graph)
Oxygen Consumption Rate (Slope), mg0 /L/min
=-(D0, mg/L) Timea ADO mq/L) Time..
Time-z — Time®
1-1
{ { I to-. i5-
{ L ( _,Llt��lni mg 07/L/min
I I {
I ( # Total Solids-,—
Specific Oxygen Uptake Rate, mg0Z/g/hr at 20? C
. (�Lllaioi = _ _m40-2,-/L/min 60 min j 20-TO
i ! •`(~ Total Solids, g/L hr
(20
60 min
X
�hr
mg0$/g/hr at 200'C

:3
TOME

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number: WQ0035595
WWTP Name: Neuse River WV VTP NPDES Number: NCO029033
Monitoring Period: 01/01/2014 to 01/31/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 54 66 109 0 1 Grab Samples
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 1 (VS reduction)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
ohn Gibson, W\,KfTP ORC
Jason Smith, VP
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Z� S
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February 3, 2015

City of Raleigh Neuse River VVWTP Lab
WW Certification # 51/ EPA Lab Code NC01029
;Laboratory Report of Analysis
(Sample Origination: covered aerobic Digester l
�
m
N -
R V N
gym"
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m '' H
to C9 ao
fy0 R
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`y m
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cu ¢'
0
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0
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2
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y v
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ca Z
0
d¢
U.
c6
d
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IE
F 0
U.
(t7
,
67.
U4
td'
ca
m
U.
Date
%
%
%
%
SU
%
Count
countslG
%
Count
counts/G
1/1/2014
1/2/2014
1 /3/2014
1 /4/2014
1 /512014
1/6/2014
1/7/2014
1/8/2014
1/9/2014
1/10/2014
1 /11 /2014
l
1 /12/2014
1/13/2014
CAD#1 CB01 1314
CAD#1CB0122140725
76
3.78
61
51
7.58
3.70
<2.00
<54.05
1/14/2014
1/15/2014
CAD#1CB011314
CAD#1CB0122140745
,
3.72
<2.00
<53.76
1/16/2014•
CAD#1CB011314
CAD#1CB0122140755
3.'64
<2.00
<54.95
1/17/2014
CAD#1CB011314
CAD#1CB0123140725
3.66
<2.00
<54.64
1/18/2014 -
CAD91 CB011314
CAD91 CB0123140735
3.66
4.00
109.29
1/19/2014
CAD#1 CB011314
CAD#1 CB0123140745
3.72
4.00
107.53
1 /20/2014 -
CAD#1 CB011314
CAD#1 CB0127140735
3.58
<2.00
<55.87
1 /21 /2014
CAD#1 CB011314
CAD#1 CB0127140745
3.58
2.00
55.87
1/22J2014
CAD#1013011314
CAD#1CB0127140755
3.64
<2.00
<64.95
1/23/2014
1/24/2014
;1 /25/2014
1 /26/2014
1 /27/2014
1/28/2014
1 /29/2014
1/30/2014
1/31/2014
Minimum
3.781
61
51;
7.581
3.58
<2.00
<53.76
Maximum1
3.78
61
611
7.58
3.721
4.001
109.29
Average1
3.781
611
511
7.581
3.661
<2A4
<66.77
D411 C�
Laboratory Supervisor

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number: WQ0035595
WWTP Name: Neuse River WNXrTP NPDES Number: NC0029033
Monitoring Period: 02/01/2014 to 07/31/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens"
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens":
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences
Colonies Per Gram of
Total Solids(Dry 70 74 89 0
Weight)
Technique 2%19221 E
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 1 (GCS reduction)
Not Applicable
Not Applicable
Frequency Sample Type
Grab Samples
"FV
I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both. of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
ohn Gibson, WWiTP ORC
Jason Smith, -\T
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February 3, 2015

City of Raleigh Neuse River WWTP Lab
WW Certification # 511 EPA Lab Code NC01 029
Laboratory Report of Analysis
Sample Origination: Covered Aerobic Digester
wi"
un
... ... .
0,01, f.
al
W, 11, "1 :"gu..
''PiA;
.
>
0
1111'..i. I. �; 1; ".
�. " * 'I -
to",
"g
'gl i:
.!--`.'CoU
n ts/G,:
U T
2/1/2014
2/2tgo
2/3/2014
TT
21512014
V
W/2014
77
219/2D14
A1_0/20
2/11/2014
2113/2014
Wf4/2Q
4-1
2115/2014
271�6120t
v4:t'
2117/2014
CAD#2GB021714
CAD#2CB0303140735
77
2.96
64
47
7.95
2.76
<2.00
<72.46
..I.'n.
.
.
63
2/19/2014
CAD#2CB021714
CAD#2CB0303140755
2.82
<2.00
<70.92
2/20�4QJ.
C� t3O3OM'4OgO5'-,
2/2112014
CAD#2CB021714
CAD#2CS03D4140730
2.90
<2.00
<68.97
2/22/2
9-862-1714�v"'
C' CAD92CS P30414014 0'
"A 1.!
2/23/2014
CAMCB021714
CAD#2CB0304140750
2.84
<2.00
<70.42
0
j'
2/26/2014
P,
?J2712014
Minimum
2.96
64
47
7.95
2.68
<2.00
<68.97
Max mu
'airr.
196
-1:':,:,..64
.
t ..
il*� —'47
' '
: �"'7 45
'90
�2 '.QO
Average
2.961
641-
47
7.95
2.80
<2.001
<7 1 .39
I L.'JI 14&' 311olz--o
-15arrell Crews Date
Laboratory Supervisor

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number: WQ0035595
WWTP Name: Neuse River VIVO NPDES Number: NCO029033
Monitoring Period: 08/01/2014 to 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
I" Class B "Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 49 55 62 0 1 Grab Samples
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 1 (ITS reduction)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
John Gibson, XXI XX/ l` ORC
Preparer Name and Title (type or print)
Sig afore of Preparer* Date
Jason Smith, G-P
Land Applier Name and Title (if applicable)(type or print)
2— n0 —'
Signature of Land Applier (if applicable) Date
*Preparer. is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February 3, 2015

City of Raleigh Neuse River VWWTP Lab
1NW Certification # 51/ EPA Lab Code NC01029
August 2014
-----_-_ __. - _._-_-_---___._----
Laboratory Report of Anaiysis
Sample Origination: .overed Aerobic Digester
Date
Class B Batch ID
# Fecal
Class B Fecal Grab
Times
Digester
Feed VS
Average
%
Class B
TS
%r /
V
Class B.
VS
%
Volatile '
Cone
Reduction
%
Class B
p H
SU
Class. B
TS Fecal
%
Class B :
M PN
Count
Class B
Fecai Col'
countslG
Class B .
. TS Fecal
%
• .Class B
MPN
mpn
Class B.
Fecal Col i
8/27/2014
CAD#4CB082714
CAD#4CB0902140733
77
3.37
56
62
9.18
3.26
<2.00
<61.35
812812014 `
CAD#4CB082714
CAD#4CB0902140743
3.26
<2.00
<61.35
8/29/2014
CAD#4CB082714
CAD#40B0902140753
3.38
<2.00
<59.17
8/3012014
CAD#4CB082714
CAD#4CB0902140803
3.22
<2.00
<62.11.
8/31/2014
CAD#4CB082714
CAD#4CB0903140735
3.88
<2.00
<51.55
9/1/2014
CAD#4CB082714
CAD#4CB0903140745
3.92
<2.00
<51.02
9/2/2014
CAD#4CB062714
CAD#4CB0903140755
4.10
<2.00
<48.78
9/3/2014
Maximum
77
3.37
56
62
9.18
4.10
<2.00
<62.11
Total
77
3.37
56
62
9.18
25.02
<14.00
<395.33
Average
77
3.37
56
62
9.18
3.57
<2.00
<56.48
Geo Mean
1 77
1 3.37
56
62
9.18
3.56
<2.00
<56.22

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number: WQ0035595
WWTP Name: Neuse River WkVTP NPDES Number: NCO029033
Monitoring Period: 01/01/2014 to 01/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens":
I "Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens":
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences
Colonies Per Gram of
Total Solids(Dry 54 66 109 0
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 1 (VS reduction)
Not Applicable
Not Applicable
Frequency Sample Type
Grab Samples
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and.the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.) .
"This determination has been made under my direction and supervision -in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
John Gibson, %YAV17P ORC
Jason Smith, Nil'
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
(
Signature of Preparer* Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February 3, 2015

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Granvffie Farms, Inc. WQ Permit Number: NVQ0035595
WWTP Name: Neuse River'%fWTP NPDES Number: NC0029033
Monitoring Period: 02/01/2014 to 07/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 70 74 89 0 1 Grab Sanples
Weight)
Analytical Technique SM 9221 E
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 1 (VS reduction)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
❑ requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
John Gibson, YXI TP ORC
Jason Smith, VP
Preparer Name and Title (type or rint) Land Applier Name and Title (if applicable)(type or print)
5 1
2-
Signature of Preparer* Date Signature of Land_Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February- 3, 2015

ANNUAL. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number: WQ0035595
WWTP Name: Neuse River W\VTP NPDES Number: NCO029033
Monitoring Period: 08/01/2014 to 12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens":
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens":
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences
Colonies Per Gram of
Total Solids(Dry 49 55 62 0
Weight)
Technique S-1 9221 E
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 1 (VS reduction)
Not Applicable
Not Applicable
Frequency Sample Type
Grab Samples
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
[� requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have. been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
John Gibson, WkX/TP ORC
Jason Smith, VP
Preparer Name and Title (type or rint) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparers` Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February- 3, 2015

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM( (503 Rules)
Facility Name: Granville Fauns, Irte. WQ permit Number: 1WQ0035595
WWxP Dianne: Stantonsbutg WWtg NPIDES Number: NCO057606
Monitoring Period: 01/01 /2014 to 12/31/2014
Pathogen Reduction (40 CPR 503.32) - Please Indicate level achieved aid alternative performed:
"Clues A" Alternative: Not Applicable
If applicable to alternative performed ("!;lass N' oily) indicate "process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative pe0ormed ("Class Ii" only) indicate "Process to Further Reduce Pathogens": Not.A,pphcable
Fecal Co1i£oxur Minimum+ Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
TotalSolids(Dxy 634,745 673,477 750,909 0 1 Grab Samples
Weight)
Analytical Technique Stile 9221 E
WctorAttraction Reduction Perfornled (40 CFR 503.33): Alt. 3 (30-day batch)
Iq certify, under penalty of law, that the pathogen requirements in 40 CPR 503.32. and the vector attraction reduction
requirement in 40 CPR 503.33 have been met."
"I cexdfy, under penalty of law, that the pathogen requirements in 40 CPR 503.32 and the vector attraction reduction
❑ requirement in 40 C`VX 503.33 have not been met" (Please note if you check this statement attacks arx explanadext why you have
not met one or both of the requirements.)
"This determination has been made wader: my direction and supervision in accordance with the system designed to ensure that
qualiAed peraoxwel property gather and evaluate the information used to determine that the pathogen and vector attraction '
xeduction xequiternt mts have been met. I am aware that there are significant penalties for Wee certification, including fine and
imptisonment."
Jason smith, NAP
Prepaeer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or jpictt)
02-1S-201S
Si re of Preparers' Date Signature of ]Land Appl er (if applicable) Date
't'Preparer is defined in 40 CPR Part 5039(r) and ISA,NCA.0 2T .1102 (M)
Sunday, Febwazy 15, 2015
Z 'd 01 'oN . 2inquo}ugS p utAol Ng:6Sl0Z '9l 'qaj

. -SOIL PLUS, _
TS 060314
114197
,0,6104114_ . .
r
07102114,_

SOIL. PLUS
MI
-. TS 060314
06/03/14
FECAL COLIFORM, GEOMETRIC:MEAN
SM 9221 E
!
a
a o
17,66.8
s a
2.51 %
a
702,665.50.
_1-141,97=
1"
'
2 =
18,265
2:63%
69.3.;709.04
3
16,186
.2.55%
634;744.77
4...
16,069:.-
2:53%
_".635,,147.09.
5
19,524
2.60%
750,908.60
6 .
16,372 .
2.57%
; : 637,041,68.
7
.16,846
2.52%.
668-1506.40

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Granville ixarrm, Inc. WQ Permit Number. WQ0035595
WVg7',ir Name: StantQnsbuxg W W1T NPDBS Number: NC0057606
Monitoring Period: 01/01/2014 to 12/31/2014
Pathogen Reduction (15A WCAC 02T .1106) - Please Indicate level acWeved and alternative perfoxmed;
"Class A" Alternative: Not Applicable
11'applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
R applicable Io sltecaat rve petfo rmed ("Class R" only) lodivate "Process to Futilhet Reduce Pathogens": Not Applicable
Fecal COWQXM Minimum Goo, Mean Maximum # of Exceedences Frequency Sample Type
Colonies Pet Gram of
Total Solids(Dty 634,745 673,477 750,909 0 1 Grab Samples
Weigh')
Analytical Technique SM 9221 B '
Vector Attraction Reduction Performed (15A NCAC OZT .1107): Alt_ 3 (30.day bench)
"I certify, under penalty of law, that the pathogen requirements in 15A NC&C 02T .1106 and the vector attraction xeductioo
21 xequi mmeat W 15,A. NCAtiC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
❑ xcquixewcxkt in 15,A, NCAC 02T .1107 have not been met.'► (Please note if you check this statement attach an explanation why
you have not met one or both of the xequixements.)
i°This determination has been made under my direction and supervision in accordance with the system designed to ensure that
rluvUed pexennnel pxopexly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction rerluiremente have been met. I am aware that them axe siguMcant penalties for false certification including Fme and
imprisonment."
Pxepaxex Name and Title (type or print)
Signs of Preparett' Date
Jason Smith, IT
Land Applier Name and Title (if applicable)(type or print)
0245-2015
Signature of Land,A.ppliex (if applicable Date
*Pxcpaxex is defused in 40 CPR Part 503.9(r) and 15AANCAC MUM (26)
Sunday, Vebowy 15, 2015
E 'd O101 'ON
2inquoluejg jo utAol ME:E I SM 9l 91d

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number. WQ0035595
WWTP Name: Town of Tarboro WWTP NPDES Number: NCO020605
Monitoring Period: 01 /01/2014 to 03/31/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A' Altemative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 9,091 38,446 109,091 0 1 Grab Samples
Weight)
Analytical Technique SM 9221 E
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 3 (30-day bench)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
F1 requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Michael Allen, ORC
Preparer Name and Title (type or print)
' Signature of Preparer* Date
Jason Smith VP
Land.Applier Name and Title (if applicable)(type or print)
2-12-2015
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC Z17.1102 (26)
Thursday, February 12, 2015

05/20/2014 13:21 2526414230 PUBLIC WORKS PAGE 02/04
LAGOON _ Fecal, Coliform
DATE
N- 2-1�!rni '01 ml
100 mi
�-q -1q ®po m ml , 0 f ml
0
721'727100 ml
ml ml
..
100 ml
a00f ml ,D1 mi
_?2 0 ml
wrrwww4o+wnv
�ii` �4j fC%o1 ml Of ml
`''i S,Y S 100 ml
vo I ml I mi
100 mi
mi .off ml
57� & 100MI
FECAL COLIFORM 2005

3 � _
RF70MPT liCGL RA"T'E. FiE4tAt3 L.E
,
WWVtC RARE..ABSCOM
-
t T �
30 ®ay bench Sca9e ��tended�Aerafi�an Tesfi
Percent Volat��e Soleds Reduction
3 -
< SOILSFLUS F
F.
T032594
_
#
- �03131114 -
-x,
� r
� "04J28J14
x � -
,.;Start End
`0 1976
0 9 924
r-
TS°log _
1.77°l0
1-7,'7%
01324
01225
r _
VS°lo
67.-:0,0°10
63% 67
-
a
IN
0 00,466
yQ.UT x
3
0323562
F,$VR {Mass Balance}
30.57%
FSVR Van Kleeck -
�
'13#70010
�:' r
FSVR Mass "'Balance},<15°fo :
NO _
ry
FSVR ;(van- Kteeck)-YES
a
s
t
}
i
t.
t
a
PO Bo�f411483sChartdtt 3241/483.� y
- i>h°ne(7Q4);588833$.�-FiY."�7t74)SS$8335 ki
� �
1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number. WQ0035595
WWTP Name: Town of Tarboro WWTP NPDES Number. NCO020605
Monitoring Period: 04/01/2014 to 06/30/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 36,364 57,065 90,909 0 1 Grab Samples
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 3 (30-day bench)
r "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requitement in 40 CFR 503.33 have not been met" (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Michael Allen, ORC
Preparer Name and Title (type or print)
Jason Smith VP
Land Applier Name and Title (if applicabie)(type or print)
�� �`�
� M � / � '2_J �S �i � 2-12-2015
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Thursday, February 12, 2015

05/20/2014 13:21 2526414230 PUBLIC WORKS PAGE 02/04
LAGOON - Fecal' Coliform
©SATE
�i-
z-rq fool ml , of ml
3(.34G 100 ml
y- -rq D p DOI^m1 ,Dlml
100 ml
±I-,L4 001 .q..ml ju ml
q0 qc" 100 ml
00 J ml
'7 Z� 100 mi
ml nl ml
„ o
N 5y4S 100 MI
.w�rr�w.rr-
N-���i� ml'01 ml
100 ml
�l_i4-►4 .�o� ml - SO/ ml
,�%� to _ ml
FECAL COLIFORM 2005

u
RAft
, A� P,
PROMPT-ACCU RATE -RE LtASLE
LABOR AV'rOPLIES, IMC
WWW.PARLABS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile SolidsReduction
.SAMPLE 10;
SAMPLE, C
;START DATE;
:ENb DATE.
Start: End:
TS
0.2511
0.2735
TS%
1.89%
1.90%
VS
0,1598
0.1647
VS%
63.64%
60.22%
yl N
0.003853
OUT
0.00389891
FSVR (Mass Balance)
--1,19%
FSVR (Van Kleeck)
13.51%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.Q. Box 411483 * Charlotte,'NC-28241.1483
Phone: [phone]-fiax,. (71T4) 588.8335

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number. WQ0035595 .
WWTP Name: Town of Tarboro WWTP NPDES Number: NCO020605
Monitoring Period: 07/01/2014 to 09/30/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens"
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens":
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences
Colonies Per Gram of
Total Solids(Dry 9,091 10,037 18,182 11
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (40 CFR 50333): Alt. 3 (30-dap bench)
Not Applicable
Not Applicable
Frequency Sample Type
Grab Samples
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 505.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Michael Allen, ORC
Preparer Name and Title (type or print)
r
Signature of Preparer* Date
Jason Smith VP
Land Applier Name and Title (if applicable)(type or print)
11"Im 2-12-2015
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Thursday, February 12, 2015

08/05/2014 08:58 2526414230 PUBLIC WORKS PAGE 05105
LAGOON -Fecal cal Coliform
DATE
1 mi , o I mi
100 mi
not . D I mi
100 mi
11 — mi m 01 mi
! 100 mi
7� ► —) �j , p0 j nil A D / mi
del100 mi
001 mi . p P mi,
0
®`1 100 mi
I mi 001 mi
0
100 mi
2 I — (1] 00 1 mi mi
0 mi
FECAL COLIFORM 2006

L
PROM PT•ACCU RATE- RELIA6 LE _
LABORATORIES' INC
WWW.PARLABS.CObf
REPORT OF ANALYSES
Attn: SCOTT CARPENTER
SOIL PLUS PROJECT NAME: SEP.14
208 WILLIAMS STREET DATE: 11/11/14
GREENVILLE,. NC 27858-
SAMPLE NUMBER- 116159 SAMPLE ID- T 093014 SAMPLE MATRIX --SO,
DATE SAMPLED- 09/30/14 -
DATE .RECEIVED- 10/01/14 SAMPLER- SC RECEIVED BY- DJ
TIME RECEIVED- 0950 DELIVERED BY- UPS °.TYPE SAMPLE -'.Grab
-Page 1 of 1
ANALYSIS -
ANALYSIS METHOD DATE TIME BY - RESULT UNITS
30 DAY BENCH SCALE TEST VAR 10/01/14 RE ATTACHED
LA130RATORY DIRECTOR
P.Q. Box 411483 • Charlotte, NC 28241-1483 .
Phone: (704) 5$8-8333 Fax: [phone]

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�, -,� � �. -- �: ,,, . - , ,,-�,;
�� "
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'rrrr:::::::::::: �� "I ----.,-l------',"',L'­ "-�--,
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- - �� . , I
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�, -� ". � .
.d � '' � . . � 11
. . ---� I -,.-,. , , I
-.,-l'- ,�

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number. WQ0035595
WWTP Name: Town of Tarboro W%= NPDES Number. NCO020605
Monitoring Period: 10/01%2014 to 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 9,091 10,037 18,182 0 1 Grab Samples
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 3 (30-day bench)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
[j- requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Michael Allen, ORC
Preparer Name and Title (type or print)
Jason Smith VP
Land Applier Name and Title (if applicable)(type or print)
Ile, _ � _ S` d lu&-MVL 2-12-2015
� �
Si�nature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Thursday, February 12, 2015

11/06/2014 09:58 2526414230 PUBLIC WORKS PAGE 02/14
LAGOON -Fecal Coliform
DATE
_ml ml
egaq j 00 ml
Mi
�0� la ,►y Mow mi ml
<9091 mi
mi . p ml
Cga�l 100 ml
D ����,,• ml ml
100 ml
OO1 mi © mi
�041 100 mi
, noj ml .�:. 2 L ml
a
100 mi
F Pao, ml
Q O
100 mi
FECAL, COLIFORM 2006

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number. WQ0035595
WWTP Name: Town of Tarboro WWI'P NPDES Number. NCO020605
Monitoring Period: 01/01/2014 to 03/31/2014
Pathogen Reduction (15A NCAC.02T .1106) -Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A' only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 9,091 38,446 109,091 0 1 Grab Samples
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-dap bench)
i certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T -1106 and the vector attraction reduction
F1 requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Mchael Allen, ORC
Preparer Name and Title (type or print)
Signature of Preparer* Date
Jason Smith VP
Land Applier Name and Title (if applicable)(type or print)
`dle S;�L 2-12-2015
Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Thursday, February 12, 2015

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Granville Fawns, Inc. WQ Permit Number. WQ0035595
WWTP Name: Town of Tarboro WWTP NPDES Number. NCO020605
Monitoring Period: 04/01 /2014 to 06/30/2014
Pathogen Reduction (15A NCAC OZT .1106) - Please Indicate level achieved and alternative performed:
"Class A' Altemative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 36,364 57,065 90,909 0 1 Grab Samples
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-day bench)
t°I certify, under penalty of law, that the pathogen requirements in 15ANCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
[1 requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met I am aware that there are significant penalties for false certification including fine and
imprisonment."
Michael Allen, ORC
Preparer Name and Title (type or print)
Signature of Preparer* Date
Jason Smith VP
Land Applier Name and Title (if applicable)(type or print)
S�L 2-12-2015
Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Thursday, February 12, 2015

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number. WQ0035595
WWTP Name: Town of Tarboro WWTP NPDES Number. NCO020605
Monitoring Period: 07/01/2014 to 09/30/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": NotApplicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Colifonn Minimum Gen. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 9,091 10,037 18,182 0 1 Grab Samples
Weight)
Analytical Technique SM 9221 E
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-dap bench)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC OZr .1106 and the vector attraction reduction
requirement in.15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
t� requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met I am aware that there are significant penalties for false certification including fine and
imprisonment."
Michael Allen, ORC
Preparer Name and Title (type or print)
Signature of Preparer* Date
Jason Smith VP
Land Applier Name and Title (if applicable)(type or print)
"'Ift% 2-12-2015
Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Thursday, Febnmary 12, 2015

ANNUAL PATHOGEN AND VECTOR ATTRACTION RIEDUCTION FORM (02T Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number: WQ0035595
WWTP Name: Town of Tarboro WWTP NPDES Number. NCO020605
Monitoring Period: 10/01/2014 to 12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Altemative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 9,091 10,037 18,182 0 1 Grab Samples
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-dap bench)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .U06 and the vector attraction reduction
dl requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
10 requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Michael Allen, ORC
Jason Smith VP
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
ZJ3��5j 2-12-2015
1
S' ature of Preparer* Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Thursday, February 12, 2015

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Granville Farms; Inc. WQ Permit Number: NVQ0035595
WWTP Name: Williamston W4V TP NPDES Number. NCO020044
Monitoring Period: 01/01 /2014 to 12/31 /2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A' Altemative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 81,211 149,178 366,879 0 1 Grab Samples
Weight)
Technique SM 9221 E
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 3 (30-day bench)
®"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
Cj requirement in 40 CFR 503.33 have not been met" (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment-"
Gene Reed, ORC
Preparer Name and Title (type or print)
Signature of Preparer* Date
Jason Smith, VP
Land Applier Name and Title (if applicable)(type or print)
2-12-2015
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Thursday, February 12, 2015

Yt_3 15LiXfC7t3, 7UAi`i!1!!UN_3 LIYi1tTt 4
:GREET V1 -LE N C �783�FAX.(252) ��ti-tz
756 Q633 -
ID#: 92 X
TOWN OF WILLIAMSTON
MR. GENE REED
P.O. BOX 506 DATE COLLECTED: 02/19/14
WILLIAMSTON ,NC 27892 DATE REPORTED : 02/24/14
- 3
Sample
PARAMETERS #1
Total Residue, mg/l - 19700
Total Solids; % 2.27
Fecal Coliform (i N), /gram Solids 116751
REVIEWED BY,
Sample
Sample
Sample
Sample
Analysis
Method
#2
#3
#4
#5
Date Analyst
Code
21533
20933
21233
13160
02/20/14 MDD
2540B-07
02/19/14 CMC
2540G97
366879
81211
108322
129771
02/19/14 MDD
9221E-06

'A N:I--- U KIVIU HI Vt-
:77
'063
TOWN OF WILLIANSTOW
MR. GENE REED
P.O. BOX 506
WILLIAMSTON NC 27892
ID#.- 92 X
DATE COLLECTED: 02/19/14
DATE REPORTED : 02/24/14
REVIEWED
Sample
Sample
Analysis
Method
PARAMETERS #6
#7
Date Analyst
Code
Total Residue, mg/l 15333
15933
02/20/14 MDD
2540B-97
Fecal Coliform WN), /gram Solids 215222
156224
02/19/14 AMD
9221E-06

PLLF;Z
PROM PT-ACCU RATE -RELIABLE
LABORATORIES, INC
1VNVNV.PARLABS.00M
REPORT OF ANALYSES
Attn: SCOTT CARPENTER
SOIL PLUS
208 WILLIAMS STREET
GREENVILLE, NC 27858-
SAMPLE NUMBER- 113174 SAMPLE ID- TW031314
DATE SAMPLED- 03/13/14
DATE RECEIVED- 03/14/14 SAMPLER- SC
TIME.RECEIVED- 1000 DELIVERED BY- UPS
Page 1 of 1
PROJECT NAME: MAR 14
DATE: 05/07/14
SAMPLE MATRIX- SO
TIME SAMPLED- 1300
RECEIVED BY- DJ -
TYPE SAMPLE- Grab
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 03/15/14 RE ATTACHED
LABORATORY DIRECTO)3.
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone],

��:._
. r..,

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Granville Farms, Inc. WQ Permit Number: WQ0035595
WW-1 Name: Williamston WWTP NPDES Number. NC0020044
Monitoring Period: 01 /01 /2014 to 12/31 /2014
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A' only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 81,211 149,178 366,879 0 1 Grab Samples
Weight)
Analytical Technique SM 9221 E
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt 3 (30-day bench)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Gene Reed, ORC
Preparer Name and Title (type or print)
Jason Smith, VP
Land Applier Name and Title (if applicable) (type or print)
J-0zilt 2-12-2015
Signature of Preparer* Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Thursday, February 12, 2015

(VCDAB�CS Agronomic Division Phone (919) 733,=2655
Website ' rn►ww ncagr:gov/agronomi/
Report No _ w FY15-SL019 '93
.prez4�, .,.
Client:
Granville Farms
Advisor: Scott Carpenter
4d M+f
._�
Predictive
PO Box 1396
8220 NC Hwy 96
Soil Plus LLC
208 Williams St.
Soil Report Mehlich-3
Extraction
Oxford, NC 27565
Greenville, NC 27858
`
Al. y '�
411110
Sampled Count Martin
Sampled: 11/15/2014 Received: 11/21/2014
completed: 01/09/2015
Farm: EB
Links to Helpful Information
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda hay/past., M 0.0
180-220 0
60
0 0
0
0
0 0
Note: 12
2 -Small Grain (SG) 0.0
80-100 0
10
0 0
0
0
0 0
Note: 3
Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
8-1 Mn-I
Mn-All Mn-Al2
Zn-1
Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.14 1.04
10.6 84 1.6 6.0 319 78
65 16
46 78
63 56
569
569
-525 0.1 1
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.0
180-220 0
70
0 0
0
0
0 0
Note: 12
2 -Small Grain (SG) 0.0
80-100 0
10
0 0
0
0
0 0
Note: 3
Test Results [units - WN in g/cnf; CEC and Na in meq/100 cd; NO3-N in mg/dd):
Soil Class:
Mineral
i
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.25 1.04
12.8 86 1.8 6.0 567 71
68 15
47 81
65 58
1159
1159
902 0.1 1
Sample ID: 3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop . (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M 1.7
180-220 0
180
25 0
0
0
0 0
Note: 12
2 -Small Grain (SG) 0.0
80-100 0
90
$ 0
0
0
0 0
Note: 3 Note:
Test Results [units - WN in g/cd; CEC and Na in meq/100 cO; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-I Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.76 1.16
4.9 48 2.6 4.8 335 25
37 8
145 81
66 59
416
416
320 0.1 2
wl ortll Carol lina:.
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA'&C$ Agronomic f)iv�sion ` -, Phone : [phone]
Website "www ncagr.gov/agronomy/
Report No.,, FY15-SL019193
Page 2 of 3
Sample ID: 4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M 0.5
180-220 0
10
0
0
0
0
0
0
Note: 12
2 -Small Grain (SG) 0.0
80-100 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/ddl:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
1.43 1.08 12.7 85 2.0 5.8 513 111
64 16
70
85
68
61
1130
1130
734
0.1
1
Sample ID: 5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past.,, M 0.3
180-220 0
10
0
0
0
0
0
0
Note: 12
2 -Small Grain (SG) 0.0
80-100 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/crrP; CEC and Na in meq/100 cd; NO3-N in mg/daft
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-1
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
1.49 1.09 12.7 85 1.9 5.9 492 112
65 16
57
78
64
57
1050
1050
716
0.1
1

NCDA&CS"Agronomic Division Phone (919).,33-2655
Webstte: www ncagr:gov%agronomi/ ,,
Report No, FY15=SL01.2157
Client:
Granville Farms, Inc.
Advisor:
Scott Carpenter
_"`'r•
Predictive
P.O. Box 1396
Oxford, NC 27565
Soil Plus LLC
208 Williams St.
Soil Report
Mehlich-3 Extraction
Greenville, NC 27858
Sampled County: Edgecombe
Sampled: 10/01/2014 Received:
10/28/2014
completed: 11/12/2014
Farm: JBS
Links to Helpful Information
Sample ID: 1
Recommendations:
Lime
Nutrients (lb/acre)
More -
Crop
(tons/acre)
N P206
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.9
80-100 0
90
25 25
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 -160 0
90
$ 25
0
0
0
0
Note: 3 Note:
Test Results [units - WN in g/cd; CEC and Na in meq/100 crTf; NO3-N in mg/drrt3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-1
Na ESP SS-1 NO3-N
0.41 1.41
3.3 52 1.6 5.2
230 24
41 7
25
89
63 70
101
101
83
0.1 3
Sample ID: 2
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P20S
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.8
80-100 0
90
25 0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 -160 0
90
$ 0
0
0
0
0
Note: 3 Note:
Test Results [units - WN in g/cd; CEC and Na in meq/100 crrr3; NO3-N in mg/dnr3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.41 1.41
3.2 52 1.5 5.3
240 23
42 6
30
92
65 72
102
102
81
0.1 3
Sample ID: 3
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P20e
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
1.2
80-100 70
100
0 0
0
0
2
0
Nofe: 3
2 -Corn, grain
0.0
120 - 160 70
100
0 0
0
0
$
0
Note: 3 Note:
Test Results [units - WN in g/crif; CEC and Na in meq/100 cm3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.86 1.15
4.7 59 1.9 5.0
27 19
45 12
30
41
35 42
40
40
16
0.1 2
orth Carolina,
ri►'�
Txi�rc�:iiii�t f'I€r�J`Cdaca+ni;��te."
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Sieve Troxler, Commissioner of Agriculture

NCDA&C$:Agronomic Droision Phone: `[phone] ;
Website: wvirw:ncagr:gov/agronomic :
Report
No
FY15-SL012157 "
Page 2 of 7
Sample ID: 4
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.4
80-100 110
110
0
0
10
6
2
0
Note: 3
2 -Corn, grain
0.0
120 - 160 110
110
0
0
0
$
$
0
Note: 3 Note:
Test Results [units - WN in g/cnf; CEC and Na in meq/100 cm3; NO3-N in mg/dO]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.36 1.29
3.9 72 1.1 5.6
13 15
60 10
27
22
23
30
23
23
22
0.1
3
Sample ID: 6
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.4
80-100 110
20
0
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 110
20
0
0
0
0
0
0
Note: 3
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrrp]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.22 1'.29
4.3 74 1.1 5.7
13 62
54 13
29
43
36
43
28
28
26
0.1
2
Sample ID: 7
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 - Small Grain (SG)
1.0
80-100 0
100
25
0
0
0
2
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
100
$
0
0
0
$
0
Note: 3 Note:
Test Results [units - WN in g/cO; CEC and Na in meq/100 crrr3; NO3-N in mg/dO]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.36 1.43
2.7 45 1.5 4.9
95 20
33 9
27
29
27
34
53
53
22
0.1
4
Sample ID: 8
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
1.2
80-100 0
110
25
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
110
$
0
0
0
0
0
Note: 3 Note:
Test Results [units - WN in g/cO; CEC and Na in meq/100 cm3; NO3-N In mg/dnf]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1
Na
ESP
SS-1 NO3-N
0.46 1.38
2,5 24 1.9 5.0
231 17
16 4
44
48
39
46
50
50
51
0.1
4

NCDA&C$AgronomcD
eieg/
Wbst
5=SL01"2157
Page 3 of 7
Sample ID: 9
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P206
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.4
80-100 10
50
0
0
0
0
2
0
Note: 3
2 -Corn, grain
0.0
120 - 160 10
50
0
0
0
0
$
0
Note: 3 Note:
Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
j
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.51 1.23
4.8 77 1.1 5.7
59 43
61 12
37
41
35
42
81
81
23
0.,1
2
Sample ID: 10
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P206
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.0
80-100 0
100 "
25
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
100
$
0
0
0
0
0
Note: 3 Note:
Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/drr]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.41 1.29
4.9 76 1.2 5.9
224 21
67 7
27
95
67
74
825
825
174
0.1
2
Sample ID: 11
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P206
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.9
80-100 , 0
70
25
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
70
$
0
0
0
0
0
Note: 3 Note:
Test Results [units - WN in g/cnf; CEC and Na in meq/100 cd; NO3-N in mg/drift
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS -I NO3-N
0.46 1.29
4.7 60 1.9 5.5
253 33
50 7
60
90
64
71
236
236
171
0.2
4
Sample ID: 12
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
"1 -Small Grain (SG)
0.6
80-100 0
50
25
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 -160. 0
50
$
0
0
0
0
0
Note: 3 Note:
Test Results [units - WN in 9/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN
CEC 'BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI -
Cu-I
Na
ESP
SS-1 NO3-N
0.46 1.22
4.5 69 1.4 5.5
123 42
55 9
63
60
46
53
225
225
82
0.2
4

NCDA8�C$ Agronomic Division Phone [phone]
- ; Website: www.ncagr.gov/agronoml/:...,
Report No
FY15-SL0.12157 ' .
Page 4 of 7
Sample ID: 13
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.0
80-100 0
80
0
0
$pH
0
0
0
Note: 3 Note:
2- Corn, grain
0.0
120 -160 0
80
0
0
0
0
0
Note: 3
Test Results [units - WN in g/crnf; CEC and Na in meq/100 cd; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-1
Na
ESP
SS-1 NO3-N
0.22 1.27 6.3
97 0.2 7.1
81 30
75 20
54
44
19
26
80
80
66
0.'1
2
Sample ID: 14
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
1.4
80-100 0
50
0
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
50
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/crr?; CEC and Na in megM00 cd; NO3-N In mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-Ali
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.86 1.16 5.2
55 2.4 5.1
221 44
41 9
50
61
47
54
167
167
70
0.2
4
Sample ID: 15
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Small Grain (SG)
0.0
80-100 0
50
0
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
50
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-1
Na
ESP
SS-1 NO3-N
0.46 1.23 6.0
87 0.8 6.4
195 46
72 10
40
59
39
46
217
217
187
0.1
2
Sample ID: 16
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.0
80-100 0
80
0
0
$pH
0
0
0
Note: 3 Note:
2 -Corn, grain
0.0
120 - 160 0
80
0
0
0
0
0
Note: 3
Test Results [units - WN in gled; CEC and Na in megM 00 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-1
Na
ESP
SS -I NO3-N
0.27 1.25 6.0
98 0.1 7.2
80 31
75 20
53
45
20
27
78
78
65
0.1
2

NobA&c6 A' 6 -26 56
9. onomi Division
e S ' www:ncagr.gov/agronomy/ m
WV b ito: www.ncacir. 0
R Nb':
Report FY,15" L01210"
Page 5 of 7
Sample ID: 17
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG) 0.4
80-100 0
70
25
20
0
0
0
0
Note: 3
2 -Corn, grain 0.0
120-160 0
70
$
20
0
0
0
0
Note: 3 Note:j
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/drift
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
. Mn-I
Mn-All
Mn-Al2
Zn-1
Zn-Al
Cu-1
Na
ESP
SS-1 NO3-N
0.27 1.29 &0 63 1.1 5.6 97 32
51 7
23
28
27
34
54
54
35
0.1
3
Sample ID: 18
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
I -Small Grain (SG) 1.2
80-100 0
110
25
0
0
0
0
0
Note: 3
2 -Corn, grain 0.0
120-160 0
110
$
0
0
0
0
0
Note: 3 Note:.1
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cd; NO3-N In mg/dd]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-Al
Cu-I
Na
ESP
SS-1 NO3-N
0.36 1.38 2.8 34 1.8 4.8 121 14
27 4
65
63
48
55
91
91
109
0.1
4
Sample ID: 19
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
I -Small Grain (SG) 0.6
80-100 0
80
25
0
0
0
0
0
Note: 3
2 -Com, grain 0.0
120-160 0
80
$
0
0
0
0
0
Note: 3 Note:
Test Results [units - WIV In g/crT?; CEC and Na in meqM 00 cd; NO3-N in mg/drr?]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-Al
Cu-I
Na
ESP
SS-1 NO3-N
0.56 1.26 3.9 66 1.3 5.5 145 27
55 8
34
66
50
57
102
102
66
0.1
3
Sample ID: 20
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
8
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG) 1.6
80-100 0
120
25
0
0
0
0
0
Note: 3
2 -Com, grain 0.0
120-160 0
120
$
0
0
0
0
0
Note: 3 Note., I
Test Results [units - W/V In g/cd; CEC and Na in meqM 00 cnrP; NO3-N in mg/drif ]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-Al
Cu-I
Na
ESP
SS-1 NO3-N
0.41 1.25 3.2 30 2.2 4.5 134 12
24 5
52
55
43
50
128
128
145
0.1
3

WWI 3
g 3-2656
we sle :www.ncagr.66vlagronomr,
Report
Page 6 of 7
Sample ID: 21
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P206
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
1.1
80-100 0
50
25
0
0
0
0
0
Note: 3
2 -Com, grain
0.0
120-160 0
50
$
0
0
0
0
0
Note: 3 Note:i
Test Results [units - WN in
g/cFTf ; CEC and Na in meq/1 00 cd; NO3-N
In mg/drif]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All
Mn-Al2
Zn-I
Zn-Al
Cu-I
Na
ESP
SS-1 NO3-N
0.81 1.21 4.7
55 2.1 5.4
295 44
43 8
68
85
61
68
313
313
240
0.2
4
Sample ID: 22
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P206
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.0
80-100 0
40
0
0
pH$
0
0
0
Note: 3 Note:$
2 -Corn, grain
0.0
120-160 .0
40
0
0
pH$
0
0
0
Note: 3 Note:j
Test Results [units - WN in g/crr?; CEC and Na in meq/1 00 crrP; NO3-N In mg/drr?]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-Al
Cu-I
Na
ESP
SS -I NO3-N
0.56 1.21 12.5
99 0.1 7.2
207 51
.91 6
63
67
32
39
205
205
145
0.2
2
Sample ID: 26
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P206
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.7
80-100 0
60
25
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120-160 0
60
$
0
0
0
0
0
Note: 3 Not@.A.
Test Results [units - WN in
g/crTf ; CEC and Na In meq/1 00 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-Al
Cu-I
Na
ESP
SS-1 NO3-N
0.76 1.24 4.5
63 1.6 5.5
192 38
51 9
37
61
47
54
229
229
109
0.1
2
Sample ID: 32
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P206
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
1.3
80-100 0
50
25
0
0
0
0
0
Note: 3
2 -Com, grain
0.0
120-160 0
50
$
0
0
0
0
0
Note: 3 Note:
Test Results [units - WN in
g/cnf ; CEC and Na in meq/1 00 cd; NO3-N In mg/drrP]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-Al
Cu-I
Na
ESP
SS-1 NO3-N
0.97 1.25 4.2
45 2.3 5.2
266 42
36 5
87
55
43
50
221
221
199
0.2
5