HomeMy WebLinkAboutWQ0035576_Residual Annual Report 2014_20150216P9- 6-6-3 5 576
Broad
River
Water
Authority
Broad River Water Authority
2014 Annual Report
Land Application Program
NC Permit No. WQ0035576
fRECEIVEL)
FEB ]67015
INFOR'VIA /O ASROC ,SING UNIT
ANN UAL LAIN1) APYLIUATION CERTIFICATION FORM
NVQ Permit#: WQ0035576 County:
Facility Name (as shown on permit):
Land Application Operator:
Rutherford
Year: 2014
Broad River Water Authority
Southern Soil Builders, Inc. Phone: 336-957-89Q9
Land application of residuals as allowed by the permit occurred during the past calendar year?
[A'
Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
Total number of application fields in thepen-nit:
I - NA
Total number of fields utilized for land application during the year:
3
Total amount of dry tons applied during the year for all application sites:
592.79
Total number of acres utilizes for land application during the year:
90
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. Yes El No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
ermittee Name and Title (type or print) U
Signature of Permittee Date
a-6-ly
of LaaApplier
Date
(if different fro Pe itd.ee) (if different from Permittee and Preparer)
* Preparer is defin-0 in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0035576
Facility Name: Broad River Water Authority
Residual Source WQ # or WQ0035576
NPDES #:
WWTP Name: Broad River Water Authority
RPairinnl Analvcic Data
Laboratory: 1) A&L Eastern Labs.
2)
3)
4)
5)
ParameterConc.
(mg/kg)
S le or Composite Date
Now WR
'For
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
of Prey *
2.o \
Date
*Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (1212006)
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0035576 FACILITY NAME:, Broad River Water Authority
PHONE: 828-287-7776 COUNTY: Rutherford OPERATOR: Brad Joyner
FACILITY TYPE (please check one): D Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
& Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes &, No ® — * If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
July
August
September
October.
November
December
WQ0035576
0
592.79
592.79
Todd Hunnicutt
592.79
Soil Admendment
Total from FORM DMSDF (sup)
Totals:
Annual (dry tons):
0
592.79
592.79
_. ,..
592.79
Amendment(s) used:-Bulkin Agent(s) used: -
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) l
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit Of Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ® No o If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All'operation and maintenance requirements were compiled with or, in the case .of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the bestlof my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
a
ignature of Permittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signture of Prep er
(if different from ermi e)
z
Date
DENR FORM DMSDF (12/2006)
Page: 1 of 2
Report Number: 14-227-0207
Account Number: 46381
Send To: SOUTHERN SOIL BUILDERS
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER, NC 28669
Lab Number: 57063
Sample Id: BRWA
�L A &L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-W6
WWw.aleastem.com
Project: BRWA
NC CERT # 257
REPORT OF ANALYSIS
Date Sampled: 8/13/2014 12:05:00
Date Received: 08/15/2014 00:00
Date Reported: 08/21/2014
Total Solids *
32.86
328600
100.0
JM
08/15/2014 15:00
SM-2540G
Moisture *
67.14
100.0
JM
08/15/2014 15:00
SM-2540G
Total Kjeldahl Nitrogen
0.34
3440
10.0
TW
08/20/2014 08:35
SM-4500-NH3C-TKN
Total Phosphorus
0.10
981
100
KM
08/19/2014 13:04
SW 6010C
Total Potassium
0.24
2420
100
KM
08/19/2014 13:04
SW 6010C
Total Sulfur
0.25
2520
100
KM
08/19/2014 13:04
SW 6010C
Total Calcium
0.11
1130
100
KM
08/19/2014 13:04
SW 6010C
Total Magnesium
0.33
3280
100
KM
08/19/2014 13:04
SW 6010C
Total Sodium
<0.01
<100
100
KM
08/19/2014 13:04
SW 6010C
Total Iron
45300
100
KM
08/19/2014 13:04
SW 6010C
Total Aluminum
125000
100
KM
08/19/2014 13:04
SW 6010C
Total Manganese
593
5
KM
08/19/2014 13:04
SW 6010C
Total Copper
33
5
KM
08/19/2014 13:04
SW 6010C
Total Zinc
90
5
KM
08/19/2014 13:04
SW 6010C
Ammonia Nitrogen
0.02
243
10.0
MW
08/18/2014 09:09
SM-4500-NI3C
Organic N
0.32
3197
10.0
08/18/2014 09:09
CALCULATION
Nitrate+Nitrite-N
38.3
2.00
MW
08/18/2014 09:10
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
08/19/2014 13:04
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9
Our reports and letters are for the exclusive and confidential use of our chenis. and may not be reproduced in whole or part, nor may a. ry reference be made M�l
to the work, the results. or the company in any advertising, news release, or other public announcements mrithout obtaining our prior written. authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14-227-0207
Account Number: 46381
Send To: SOUTHERN SOIL BUILDERS
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER, NC 28669
Lab Number: 57063
Sample Id: BRWA
® A&L Eastern Laboratories Inc.
■ ■Y� 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
wwwaleastem.com
Project: BRWA
NC CERT # 257
REPORT OF ANALYSIS
Date Sampled: 8/13/2014 12:05:00
Date Received: 08/15/2014 00:00
Date Reported: 08/21/2014
Total Chromium
57
5
KM
08/19/2014 13:04
SW 6010C
Total Nickel
22
5
KM
08/19/2014 13:04
SW 6010C
Total Lead
18
5
KM
08/19/2014 13:04
SW 6010C
Total Arsenic
7.0
3.0
KM
08/19/2014 13:04
SW 6010C
Total Mercury
<0.4
0.4
KM
08/20/2014 08:50
SW-7471 B
Total Selenium
<5.0
5.0
KM
08/19/2014 13:04
SW 6010C
pH (Standard Units) *
6.18
2.00
TW
08/18/2014 09:49
SW-9045D
Total Molybdenum
<5
5
KM
08/19/2014 13:04
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr" AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exciusive and confidential use of our clients, and may not be reproduced ir, w,hoie or parr, nor t-oay any reference be made
to the work. the results, or the company in any advertising, news release. or other public announcements without obtaining our prior written authorization.
Debbie Holt
PAN
Mineralization
as decimal
ITotal dry
tons/yea
jAcres
Applied -on
90
Rate
0.4
TKN
3440
K
3 : -
F 342
NO3
38.3-1
NO2
0
% Solids
0.3286
592.79
PAN Surface
1448.5jmglkg 2.897 lbs/dry ton
1717.313 lbs total PAN
19.08125 lbs PAN/acre
PAN In-c'j U0 C O
1619.51mg/kg 3-239 lbs/dry ton
1920.047 1 ibs total PAN
21.333851lbs PAN/acre
Pry Tons/1000 gal.
1.-370262
1st year PAN
Surface lbs.
1717.31263
1st year PAN
Injected lbs.
1920.04681
lbs./acre
Surface
19.08125144
lbs./acre
Injected
21.33385344
MR(TKN-NH3)+ +.5(NH3)+NO3+NO2 =mg/kg
mg/kg x.002 =Ibs/dry ton
MR(-r,KN"NH3',i I I + NH3jl+N%ID',3+NO2
=Mgll,-
k
mg/kg x.002 =Ibs/dry ton
1000 X 8.34 X %solids X sp. gravity "=dry tons/1 000gal."
2000
SAR
Sodium Absorption Ratio
Na :'Sodium (Mg/L) Equivalent weight: 23
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
Milli Equivalent = Mg/L / Equivalent weight
Na(Mg/L) Ca M /L M M /L
32.86 1 371.3 1 1077.8
Lig KEA
I �icl (M_ Q
I Mg_LNI
1.4-28696
'18.565
89,81667
SAR:= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 0.194078 1 (Frorn Mg/L entered above)
SAR= 0.192907 (From ME entered below)
Na ME
Ca ME
Mgt
1.42
1 18.56
1 89.81
The amour
amount of E
Permitting c
Analytical Results
Southern Soil Builders
958 Hoots Road
Roaring River NC 28669
Entered 8/13/2014
Reported: 8/19/2014
For: BRWA
Sample ID
Parameter
Cust ID
Result
Units
Method
Date
Analyzed Analyst
140813-28.1
% Solids
1
28.7
%
SM2540B-1997
8/14/14
WL
140813-28.1
Fecal Coliform MTF
1
<7
MPN/g
SM92210E-2006
8/14/14
WL
140813-28.2
% Solids
2
29.8
%
SM2540B-1997
8/14/14
WL
140813-28.2
Fecal Coliform MTF
2
<6.7
MPN/g
SM9221 CE-2006
8/14/14
WL
140813-28.3
% Solids
3
30.5
%
SM2540B-1997
8/14/14
WL
140813-28.3
Fecal Coliform MTF
3
<6.6
MPN/g
SM9221 CE-2006
8/14/14
WL
140813-28.4
% Solids
4
29.5
%
SM2540B-1997
8/14/14
WL
140813-28.4
Fecal Coliform MTF
4
<6.8
MPN/g
SM9221 CE-2006
8/14/14
WL
140813-28.5
% Solids
5
28.6
%
SM2540B-1997
8/14/14
WL
140813-28.5
Fecal Coliform MTF
5
<7
MPN/g
SM92210E-2006
8/14/14
WL
140813-28.6
% Solids
6
31.3
%
SM2540B-1997
8/14/14
WL
140813-28.6
Fecal Coliform MTF
6
<6.4
MPN/g
SM92210E-2006
8/14/14
WL
140813-28.7
% Solids
7
29.8
%
SM2540B-1997
8/14/14
WL
140813-28.7
Fecal Coliform MTF
7
<6.7
MPN/g
SM9221 CE-2006
8/14/14
WL
Respectfully submitted,
U/-�A'/OL
Dena Myers
NC Cert #440,
NCDW Gert #37755,
EPA NCdO9O9
P.O. Box 228 • Statesville, North Carolina 28687 • 704/872/4697
Client:
AC'
STATESVILLE ANALYTICAL
122 Court Street • P.O. Box 228
Address: �j �y v� !
{J
-..�.i
Statesville, NC 28687
.(Z04)' 872-4697
% .� r / - _ - - - - - - - - - -- - - - - - - - - -
Contact Person: '7 (/'l (7`� Phone # [) 7 n FAX#
• - 4_(h ! 6�A-- 3 `-' — �J �7 I 3
CIS '� , E
� f f
Chain of
Custody Record
PO # u Requisitioned by: Crime Date)
Customer
Sample ID#
Lab -ID #
Time Sampled
Grab Onl
( y)
Date Sampled
(Grab Only)
a
a
o
Matrix
Parameters requested for analysis
Sludge
w
ww
�Q'
IF•
ag a�
�
-j
�
y
��(
t�
Relinquished by: �.
Time t "�
am, Date
/ j �/
Sampled by:�
( 1
Received by: (/f
2 y
Time `; :
�;
am,Imi Date
% /
Transported by:
Relinquished b :'"�
q Y
Time
am, pm Date
/
Holding times met:
Received by:
Time
an ; pm Date
/ /
Compliance work:
Composite Sampling #1:
Time begin am, pm Date / /
Non-compliance work:
Time end am, pm Date / /
Lab Comments:
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date /_/
Condition of Receipt
Sample ID 140813-28.1-28.7 Client Southern Soil Builders
Temp on Arrival
pH upon Arrival Parameter Schedule % solids
❑
HNO3
❑
HCl
❑
NaOH
❑
H2SO
❑
Na2S2O
❑
Dechlorinated
—' pH'upon Arrival - —. Parameter Schedule _-__Fecal
ColifoM MTF
❑
HNO3
❑
HCl
❑
NaOH
❑
H2SO
❑
Na2S2O
❑
Dechlorinated
❑ Chemicals in containers, client
❑ Chemicals upon receipt
❑ Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
Page 1 of 1
Analytical Results
Southern Soil Builders
958 Hoots Road
Roaring River NC 28669
Entered 8/13/2014
Reported; 8/27/2014
For: BRWA
Sample ID
Parameter
Cust ID
Result Units
Method
Date Anal st
Analyzed Y
140813-3T
Corrosivity
BRWA
See Attached
SW-846
8/22/14 PACE
140813-31
Ignitability
BRWA
See Attached
1010M
8/22/14 PACE
140813-31
Reactivity
BRWA
See Attached
SW-846
8/22/14 PACE
140813-31
TCLP
BRWA
See Attached
1311
8/22/14 PACE
Respectfully submitted,
Dena Myers
NC Cert#440,
NCDW Cert #37755,
EPA NC00909
P.O. Box 228 • Statesville, North Carolina 28687. 704/872/4697
Client: C f I
' `'�) 4' t3 • ✓ ° C4 r = a r
STATESVILLE ANALYTICAL
122 Court Street - P.O. Box 228
Statesville, NC 28687
-�' .
- (704 8--)- 72-4693-..
fi Address: g j °
Contact Person: r
a
Phone #
-�
FAX#
f) v V
Chain of
Custody Record
PO # Requisitioned by: (Time Date)
Customer
Sample ID#
Lab-ID
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
a
0
Matrix
Parameters requested for analysis
sludge
WWW
B R" j A
yy#�� , %}
' V j� J 1 �
l "�'
f' (; `�
,�
l i . �7 d 1�� rrSia), �`!) •ls_
/+'
Relinquished by:
Received by:
Relinquished by:
Received by:
Composite Sampling
Time begin
Time end
Composite Sampling
Time begin
Time end
�,1�
!� , r
_
#1-
am, pm Date / /
am, pm Date / /
#2:
am, pm Date
am, pm Date / /
de
Time
Time
Time
Time
Lab Comments:
am, pm)Date 26 / /1
am m Date / t r�'
am, pm Date / /
am, pm Date / /
Sampled by:
Transported by. jy
Holding times met:
Compliance work:
Non-compliance work:
s `
Condition of Receipt
Sample ID 140813-31 Client Southern Soil Builders
Temp on Arrival
pH upon Arrival
Parameter Schedule
Corrosivity
❑
HNO3
❑
HCl
❑
NaOH
❑
H2SO
❑
Na2S2O
❑
Dechlorinated
pH upon Arrival
Parameter Schedule
Ignitability
❑
HNO3
❑
HCl
❑
NaOH
❑
1i2SO
❑
Na2S2O
❑
Dechlorinated
pH upon Arrival
Parameter Schedule
Reactivity
❑
HNO3
❑
HCl
❑
NaOH
❑
112SO
❑
Na2S2O
❑
Dechlorinated
pH upon Arrival
Parameter Schedule
TCLP
❑
HNO3
❑
HCl
❑
NaOH
❑
112SO
❑
Na2S2O
❑
Dechlorinated
❑ Chemicals in containers, client
❑ Chemicals upon receipt
❑ Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers,, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
❑ Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals 'in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
❑ Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
❑ Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
Page 1 of I
aceAnalXical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: 08/13/14 140813-31
Pace Project No.: 92213461
Sample: 140813-31 Lab ID: 92213461001 Collected: 08/13/14 13:15 Received: 08/14/14 15:10 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 08/18/14 15:15
amma-BHC L' d
g ( m ane)
Chlordane (Technical)
ND ug/L
0.50 1
08/19/14 10:01
08/20/14 11:00
58-89-9
Endrin
ND ug/L
3.0 1
08/19/14 10:01
08/20/14 11:00
57-74-9
Heptachlor epoxide
ND ug/L
ND ug/L
0.50 1
0.50
08/19/14 10:01
08/20/14 11:00
72-20-8
Methoxychlor
ND ug/L
1
1000
08/19/14 10:01
08/20/14 11:00
1024-57-3
Toxaphene
1
08/19/14 10:01
08/20/14 11:00
72-43-5
Surrogates
ND ug/L
3.0 1
08/19/14 10:01
08/2011411:00
8001-35-2
Decachlorobiphenyi (S)
49 %
10-138 1
08/19/14 10:01
08/20/14 11:00
2051-24-3
Tetrachloro-m-xylene (S)
52 %
10-110 1
08/19/14 10:01
08/20/14 11:00
877-09-8
8082 GCS PCB
Analytical Method: EPA 8082 Preparation Method: EPA
3546
PCB-1016 (Aroclor 1016)
ND ug/kg
127 1
08/15/14 15:02
08/18/14 16:44
12674-11-2
PCB-1221 (Aroclor 1221)
ND ug/kg
127 1
08/15/14 15:02
08/18/14 16:44
11104-28-2
PCB-1232 (Aroclor 1232)
ND ug/kg
127 1
08/15/14 16:02
08/18/14 16:44
11141-16-5
PCB-1242 (Aroclor 1242)
ND ug/kg
127 1
08/15/14 15:02
08/18/14 16:44
53469-21-9
PCB-1248 (Aroclor 1248)
ND ug/kg
127 1
08/15/14 15:02
08/18/14 16:44
12672-29-6
PCB-12541 (Aroclor 1254)
ND Llg/kg
127 1
08/15/14 15:02
08/18/14 16:44
11097-69-1
PCB-1260 (Aroclor 1260)
ND ug/kg
127 1
08/15/14 15:02
08/18/14 16:44
11096-82-5
Surrogates
Decachlorobiphenyl (S)
51 %
21-132 1
08/15/14 15:02
08/18/14 16:44
2051-24-3
8151 Chlorinate Herbicide TCLP
Analytical Method: EPA 8161
Preparation Method: EPA 3510
2,4-D
ND mg/L
0.038 1
08/22/14 08:00
08/22/14 22:19
94-75-7
2,4,5-TP (Silvex)
Surrogates
ND mg/L
0.038 1
08/22/14 08:00
08/22/14 22:19
93-72-1
2,4-DCAA'(S)
98 %
42-142 1
08/22/14 08:00
08/22/14 22:19
19719-28-9
6010 MET'ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/15/14 16:30
Arsenic
ND mg/L
01050 1
08/18/14 19:05
08/19/14 11:26
7440-38-2
Barium
0.67 mg/L
0.25 1
08/18/14 19:05
08/19/14 11:26
7440-39-3
Cadmium
ND mg/L
0.0060 1
08/18/14 19:05
08/19/14 11:26
7440-43-9
Chromium
ND mg/L
0.025 1
08/18/14 19:05
08119/1411:26
7440-47-3
Lead
ND mg/L
0.025 1
08/18/14 19:05
08/19/14 11:26
7439-92-1
Selenium
ND mg/L
0.10 1
08/18/14 19:05
08/19/14 11:26
7782-49-2
Silver
ND mg/L
0.025 1
08/18/14 19:05
08/19/14 11:26
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA
1311; 08/15/14 16:30
Mercury
ND ug/L
0.20 1
08/18/14 20:00
08/21/14 14:08
7439-97-6
8270 MSSV TCLP Sep Funnel
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA
1311; 08/18/14 15:15
1,4-Dichlor'obenzene
ND ug/L
50.0 1
08/1911410:01
08/20/1412:54
106-46-7
2,4-Dinitrot'oluene
ND ug/L
50.0 1
08/19/14 10:01
08/20/14 12:54
121-14-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/27/2014 09:52 AM without the written consent of Pace Analytical Services, Inc..
Page 4 of 21
aceAnaljdical
www.pecolabs.com
ANALYTICAL RESULTS
Project: 08/13/ 14 140813-31
Pace Project No.: 92213461
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NO 28078
(704)875-9092
Sample: 140813-31 Lab ID: 92213461001 Collected: 08/13/14 13:15 Received: 08/14/14 15:10 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date:•.EPA 1311; 08/18/14 15:15
Hexachloro-1,3-'butadiene
ND ug/L
50.0
1
08/19/14 10:01
08/20/14 12:54
87-68-3
Hexachlorobenzene
ND ug/L
50.0
1
08/19/14 10:01
08/20/14 12:54
118-74-1
Hexachloroethane
ND ug/L
50.0
1
08/19/14 10:01
08/20/1412:64
67-72-1
2-Methyl phenoI(o-Cresol)
ND ug/L
50.0
1
08/19/14 10:01
08/20/14 12:54
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
50.0
1
08/19/14 10:01
08/20/14 12:54
Nitrobenzene
ND ug/L
50.0
1
08/19/14 10:01
08120/1412:54
98-95-3
Pentachlorophenol
ND ug/L
100
1
08/19/14 10:01
08/20/14 12:54
87-86-5
Pyridine
ND ug/L
50.0
1
08/19/14 10:01
08/20/14 12:54
110-86-1
2,4,5-Trichlorophenol
ND ug/L
50.0
1
08/19/14 10:01
08/20/14 12:54
95-95-4
2,4,6-Trichlorophenol
ND ug/L
50.0
1
08/19/14 10:01
08/20/14 12:54
88-06-2
Surrogates
Nitrobenzene-d5 (S)
25 %
12-102
1
08/19/14 10:01
08/20/14 12:54
4165-60-0
2-Fluorobiphenyl (S)
26 %
13-107
1
08/19/14 10:01
08/20/14 12:54
321-60-8
Terphenyl-d14 (S)
53 %
21-132
1
08/19/14 10:01
08/20/14 12:54
1718-51-0
Phenol-d6 (S)
9 %
10-110
1
08/19/14 10:01
08/20/14 12:54
13127-88-3 SO
2-Fluorophenol (S)
15 %
10-110
1
08/19/14 10:01
08/20/14 12:54
367-12-4
2,4,6-TrlI*omophenol (S)
32 %
27-108
1
08/19/14 10:01
08/20/14 12:54
118-79-6
8260 MSV TCLP
Analytical Method: EPA 8260 Leachate Method/Date:
EPA 1311; 08/19/14
11:34
Benzene
ND ug/L
192
38.5
08/20/14 21:25
71-43-2
2-Butanone (MEK)
ND ug/L
385
38.5
08/20/14 21:25
78-93-3
Carbon tetrachloride
ND ug/L
192
38.5
08/20/14 21:25
56-23-5
Chlorobenzene
ND ug/L
192
38.5
08/20/14 21:25
108-90-7
Chloroform
ND ug/L
192
38.5
08/20/14 21:25
67-66-3
1,4-Dichl6robenzene
ND ug/L
192
38.5
08/20/14 21:25
106-46-7
1,2-Dichloroethane
ND ug/L
192
38.5
08/20/14 21:25
107-06-2
1,1-Dichloroethene
ND ug/L
192
38.5
08/20/14 21:25
75-35-4
Tetrachloroethene
ND ug/L
192
38.5
08/20/14 21:25
127-18-4
Trichlorodthene
ND ug/L
192
38.5
08/20/14 21:25
79-01-6
Vinyl chloride
ND ug/L
192
38.5
08/20/14 21:25
'75-01-4
Surrogates
1„2-Dichloroethane-d4 (S)
103 %
70-130
38.5
08/20/14 21:25
17060-07-0 1g
Toluene-d8 (S)
94 %
67-135
38.5
08/20/14 21:25
2037-26-5
4-Bromofluorobenzene (S)
96 %
70-130
38.5
08/20/14 21:25
460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
73.9 %
0.10
1
08/15/14 14:51
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
08/27/14 03:40
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
3.8
1
08/18/14 19:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/2` 12014 09:62 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 21
aceAnalytkal
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ANALYTICAL RESULTS
Project: 08/13/14 140813-31
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Pace Project No.: 92213461
Sample: 140813.31 Lab ID: 92213461001 Collected: 08/13/14 13:15 Received: 08/14/14 15:10 Matrix: Solid
Resuits reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7358 Reactive Sulfide Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
Date: 08/27/2014 09:62 AM
ND mg/kg
38.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
08/18/14 15:00
Page 6 of 21
Analytical Results
Southern Soil Builders
958 Hoots Road
Roaring River, NC
28669�
Receive Date: 09/22/2014
Reported: 09/26/2014
For: BRWA
Comments:
Sample, Number Parameter Sample ID Result Unit Method Analyzed Analyst
140922-17-01 Corrosivity BRWA 5.0 SW-846 09/23/2014 Pace
Respectfully
submitted,
hO'P%-VVO-,
Dena Myers
NC Cert #440,
NCDW Lert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 1
Client:
d� P
' i � ' �J1
STATESVIILEANALYTICAL
122 Court Street • P.O. Box 228
Address: ' j
�!"
Statesville, NC 28687
(704) 872-4697
6 q
Contact Person:
e
Phone # 3-c`iS7 �, j, .j f
FAX# 5 3
Chain of.
Custody Record .
PO # Requisitioned by: (Time. Date)
Customer
Sample ID#
Lab -ID #
Time Sampled
( Grab Only)
y)
Date Sampled
(Grab Only).
a
o
Matrix
Parameters requested for analysis
Sludge
w
ww
t i
RL'L.i920 —
y
i7
)
!j C%U�.c
` /
G? �2 /�l
i
y�
.'C
U
!
itrr:s.�.4
Relinquished. by:
Time
1.0
am, pm Date // :.
Sampled by: F�
Received by:
Y
', -� -�.
;_ .. -- ' �. �
Time I
1�_ �?
.am,:p'� Date?
�' _'
/��.
—
Transported by:
Relinquished by:
Time
-am,.pm Date
Holding times met:
Received by:
Time
am, pm Date
—./_/_,,-�
Compliance work:
Composite Sampling #1:
Time begin
am, pm Date %
/
Non-compliance work:
Time end
am, pm Date
'Composite
Lab Comments:
Sampling #2
-lima begin
am, pm Date
'Time end
am, pm Date /
/
aceAnalXkal
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
(704)875-9092
Project: 140922-17
Pace Project No.: 92218545
Sample: 140922-17 Lab ID: 92218645001 Collected: 09/22/14 11:00 Received: 09/23/14 16:00 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters R I
esu is Units Report Limit DF Prepared Analyzed CAS No, Qual
9045 pH toll Analytical Method: EPA 9045
pH at 25 Degrees C 5.0 Std. Units 0.10 1 09/25/14 15:45 H1
Date: 09/26/2014 01:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 9
ANN UAL PATHOGEN AND VEUTOK ATTRACTION RED UUTION FORM (02T Rules)
Facility Name:
Broad River Water Authority
WWTP Name: Broad River Water Authority
Monitoring Period: From 1/l/2014 To
WQ Permit Number:
NPDES Number:
12/31/2014
WQ0035576
NCO181035
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) D
I Alt B (Alk Treatment) D
Alt. C (Prior Testing)
AID (No Prior Test)
Process to Further Reduce Pathogengs D
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 131
Heat Drying D
Heat Treatment D
Thermophilic D
Beta Ray D
Gamma Ray D
Pasteurization
Class B:
Alt. (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization D
Air Drying D
Composting D
Aerobic Digestion D
Anaerobic Digestion
g on C]
,
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Nurn er o
Excee-
c
Frequency'
of Analysis
Y
Sample
Type
Analytical
Tech -
niame
Minim
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
WN
CFu
1000 mpn per gram
of total solid (dry
weight)
6.4
6.73
7
MPN/g
0
7'
grab
sm9221e
Salmonella bacteria
(in lieu of fecal
coliform)
3 NTN per 4 grams
total solid (dry
weight)
vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed:
Alt.I (VS reduction) ®
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) D
I Alt. 4 (Spec. 02 uptake)
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ®
Alt 7 (Drying - Stable) D
JAIt. 8 (Drying - Unstable)
Alt. 9 (Injection) ®
Alt. 10 (Incorporation) ®
No vector attraction reduction alternatives were performed
CEKTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
D "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction,and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
5eft 6 04 -- � 0 �C.� Dennis Key Southern Soil Builders, Inc.
?re arer me and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
3i ture o r � ' gn f epa Date Signature of Land Applier (if applicable) Date
*Preparer is define n 40 CFR Part 503.9(r) and 15A NCAC '2T .1102 (26)
DENR FORM PVRF 02T (12/2006)