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Home My WebLink AboutWQ0034842_Residual Annual Report 2014_201502181. 2014 ANNUAL REPORT LAND APPLICATION PROGRAM TOWN OF MOREHEAD CITY PERMIT #WQ0034842 Prepared For: Town of Morehead City 706 Arendell Street Morehead City, North Carolina 28557 Compiled By: S&ME, Inc. 8646 West Market Street, Suite 105 Greensboro, North Carolina 27409 February 2015 RECEIVEDIDENDWR FEB 19 2015 WabrQuality Perm"fig Section February 17, 2015 S&ME NCDENR-DWR / Non -Discharge Permitting Unit 512 North Salisbury Street Raleigh, North Carolina 27604 Attention: Non -Discharge Permitting Unit Reference: 2014 LAND APPLICATION ANNUAL REPORT Town of Morehead City, North Carolina Permit No. WQ0034842 S&ME, Inc. Project No. 1584-13-023 Phase:03 S&ME, Inc. (S&ME) is submitting all monitoring and reporting requirements as specified in the above referenced permit for the Town of Morehead City, North Carolina (Morehead City) on behalf of Morehead City. S&ME compiled this report using data gathered during the compliance year from Morehead City. This data includes: 1) Class A Annual Distribution of -} Marketing / Surface Disposal Certification and Summary Form, 2) Annual Residual Sampling Summary Form, 3) Annual Pathogen and Vector Attraction Reduction Form (02T), and 4) Analytical Data. Morehead City distributed a total of 17.78 Dry Tons of residual solids during the 2014 calendar year. If there is any further information required or questions regarding this land application program please do not hesitate to contact Mr. Carl Dangerfield, WWTP Supervisor (252-726- 6237) for further assistance. Sincerely, S&ME, INC. Martin Mabe Project Manager/Agronomist N.C. Land Application/Residuals Operator #22753 Enclosure(s) cc: Town of Morehead City T:\Projects\2013\ENV\1584-13-023 Town of Morehead City\2014 Data\2014 ANNUAL REPORT.doc S&ME, INC. / 8646 W. Market Street, Suite 105 / Greensboro, NC 27409 / p 336.288.7180 f 336.288.8980 / www.smeinc.com Town of Morehead City 706 Arendell Street Morehead City, North Carolina 28557 252-726-6237 TOWN OF MOREHEAD CITY NPDES #NC0026611 NC PERMIT # WQ0034842. Mr. Carl Dangerf eld, WWTP Superintendent Town of Morehead City 706 Arendell Street Morehead City, NC 28557 2014 Morehead City WWTP Dry Tons 17.78 2014 Morehead City WWTP Dry Metric Tons 16.13 Total Dry Metric Tons 16.13 TABLE OF CONTENTS SECTION NO. TITLE Form DMSDF II Form RSSF III Form PVRF 2T and Form PVRF 503 IV Analytical Data FORM DMSDF CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: W00034842 FACILITY NAME: Town of Morehead City WWTP PHONE: 252-726-4503 COUNTY: Carteret OPERATOR: Carl Dangerfield - WWTP Superintendent FACILITY TYPE (please check one): ® Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) R1 Distribution and Marketing (complete Parts A, B, and C) .a.. -a., -9 yea M X. r i --4h, if Nn ckin nnrtc A. R_ C and certify form helow V►' U5 L--_ -- -- - - - Part A*: Part B*: Month Sources(s) (include NPDE5 # if applicable) Volume (d tons) Reci Tent Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January February March April May June JulyMorehead City NCO026611 2.96 2:96 Craven Ag Service 2.96 Fertilizer August September October November December Morehead City NCO026611 14.82 14.82 Baird Transport 14.82 Fertilizer Total from FORM DMSDF (sup) . ;>0°: :0,`,7. ', „0. Totals: Annual d tons _' �:' '_0;: a;., W 17:,7.8",.-" ' :,h' 1ti7 78;;,'; .:°t M 1`7 78w , a;_ Amendmen s used: * if mnre snace is reouired, attach additional information sheets (FORM DMSDF Bulking A ent s used: (supp)): Total Number of Form DMSDF (Supp) Part C: Facility was compliant during the past calendar year with all conditions of the land application permit R1 Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: L3 No -► R-No; Explain -in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I- certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �g3nature of Permittee 6 ZBif- Date Signature ofPreparer** (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date r DENR FORM DMSDF (1212006). FORM RSSF ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0034842 Laboratory: 1) " Environmental Chemists, Inc. Facility Name: Town of Morehead City 2) Residual Source WQ # or WQ0034842 3) NPDES #: 4) WWTP Name: Town of Morehead City WWTP .5) Rnairinal Analvcic Data Parameter _-_-__img�g) _.._..._ Conc. Limit m /k a Sample or Composite Date _�.___ .- -- —4f1-f-1"4— .. _. _.- ...... -..-.- Percent.Solids.(%o) NA -.- Arsenic 75 6.62 Cadmium 85 1.88 Copper 4,300 506 Chromium NA 9.72 Lead 840 8.1 Mercury 57 0.74 Molybdenum 75 1.88 Nickel 420 7.62 Selenium 100 4.59 Zinc 7,500 559 ~-1 ofaCPho§p-1►orus ��_ 5620 TKN NA 545 Ammonia -Nitro en NA 177 Nitrate and Nitrite NA 20.3 'ror surface aisposai taciunes me ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting fal"formation, including the possibility of fines and imprisonment for knowing violations." Z/W 0 Vgffatu a of Prep er bate *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) FORM PVRF 2T AND FORM PVRF 503 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Morehead City WQ Permit Number: WQ0034842 WWTP Name: Town of Morehead City WWTP NPDES Number: NCO02661 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) -Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) 0 1 Alt B (Alk Treatment) ® Alt. C (Prior Testing) 0 A1t.D (No Prio' Test) [3Process to Further Reduce Pathogengs If applicable to alternative performed (Class A only) indicate ."Process to Further Reduce Pathogens": Compost [j Heat Drying El Heat Treatment 0 Thermophilic 0 Beta Ray 13 Gamma Ray Pasteurization Class B: JAIt. (1) Fecal Density E3 Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens Lime Stabilization El Air Drying ® Composong ® Aerobic Digestion 0 Anaerobic Digestion 0::..................... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density Number of Frequency Sample Analytical Tech Parameter in Sludge MinimumGeo. Mean MaximumUnits - Excee- of Type Analysis d nces y ni ue 2 x 10 to the MPNf 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram! of total solid (dry` 1 1 1 MPN/g 0 Annual Grab 9221 C E weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate klternative performed: Alt.1 (VS reduction) El Alt.1(40-day bench) a Alt. 3 (30-day ben, h) E3 jAlt. 4 (Spec. 02 uptake) ll Alt. 5 (14-Day Aerobic) E3 Alt. 6 (Alk. Stabilization 0 jAlt 7 (Drying - Stable) [3 Alt. 8 (Drying - Unstable) 0 Alt. 9 (Injection) E3 Alt. 10 (Incorporation) ®No vector attraction reduction alternatives were performed 01 CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T 1107 have been met" "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) his determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Carl Dangerfield - WWTP Superintendent Pre arer Name and Title ie or print) ture of ep er* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Town of Morehead City WQ Permit Number: WQ0034842 WWTP Name: Town of Morehead City WWTP NPDES Number: NCO02661 Monitoring Period: , From 1/l/2014 To 14/1/2014 Pathoeen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative nerformed: Class A: Alternative 1 0 Alternative 2 ® Alternative 3 0 Alternative 4 E3 Alternative 5 0 Alternative 6 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 13 Heat Drying ® 1 Heat Treatment Thermophilic 0 Beta Ray C� Gamma gay(� Pasteurization 0 Class B: Alternative 10 Alternative 2 If applicable to alternative performed (Class B only) indicate "Process .to Significantly Reduce Pathogens": Lime Stabilization 0 Air Dryingo Com o' ® Aerobic Digestion D Anaerobic Digestion :::::::::::::::::::............................................... .. ..... . If applicable to alternative performed (Class A or Class B) complete toe :.....:.:..::.:.::.: following monitoring data: Parameter Allowable Level in Sludge Pathogen Density 3 Number o Excee- deuces Frequency of Analysis Sample Type Tech - ni ue MinimumGeo. Mean im Unity Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 1 1 1 { NON/g 0 Annual Grab 9221 C E Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) 1 Y ca:wr Z.LLl171CL1Un nCuuCuun I1411 R,r K - 1-M-9RE 1nOIC61TP.nn71nn nPrinrM&91- Alt.1 (VS -reduction) ® Alt. 2 (40-day bench) ® Alt. 3 (30-day bin ) ; [3 Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) ® Alt. 6 j(Alk. Stabilization R1 Alt 7 (Drying - Stable) ® JAIt. 8 (Drying - Unstable) El Alt. 9 (Injection) ® Alt. 10 (Incorporation) ® No vector attiactio# reduction alternatives were performed [3 CERTIFICATION STATEMENT (please check the appropriate stateent) C� "I certify, under penalty of law,.that the pathogen requi. ' e is in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 50333 have U.eei i met." ' "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have nint�e�n met." (Please note if you check this statement attach an ez lanation why you have not net o , e or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified :personnel properly gather and evaluate the information used to determine" that the pathogen and vector attraction reduction requirements have been met. I am aware that there are + significant penalties for false certification including fine and imprisonment " i Carl Dangerfield - WWTP Superintendent i Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) tgn ture of eparei* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 ( )26 i E DENR FORM PVRF 503 (12/2006) ANALYTICAL DATA TOWN OF MOREHEAD CITY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 1, 2014 Morehead City 70.40 % Solids 11.93 pH Permit No. WQ0034842 Parameter % Mg/Kg Dry Weight x 10,000 Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 0.055 545.000 1.090 Phosphorus 0.562 5,620.000 11.240 Potassium 0.267 2,670.000 5.340 PAN (injected)* 0.031 3,869.500 7.739 PAN (surface)* 0.022 3,777.000 7.554 Ammonia Nitrogen 0.018 177.000 0.354 Calcium 16.500 165,000.000 330.000 Calcium Carbonate E . --- --- --- Magnesium 0.328 3,280.000 6.560 Sodium 0.153 1,530.000 3.060 Sulfur --- --- Nitrate N / Nitrite N --- 20.300 0.041 Barium --- --- Chloride --- -- Iron --- --- Aluminum --- 7,670.00 15.340 Arsenic --- 6.62 0.013 Cadmium --- 1.88 0.004 Chromium --- 9.720 --- Copper --- 506.00 1.012 Lead --- 8.10 0.016 Mercury --- 0.74 0.001 Molybdenum --- 1.88 0.004 Nickel --- 7.62 0.015 Selenium --- 4.59 0.009 Zinc --- 559.00 1.118 Environmental Chemists, Inc. 2014-03786 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 (910) 392-0223 (Lab) (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: May 15, 2014 706 Arendell Street Customer PO #: Morehead City NC 28557 Report #: 2014-03786 Attention: C. Sutton Report to: C. Sutton Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-09186 Site: Sludge Class A 4/1/2014 10:20 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed 4 PAN calculation 219 mg/kg 05/15/2014 30% Mineralization rate for aerobically digested residuals. Chlordane SW 846 Method 808113/3510 <0.005 mg/L 04/06/2014 Endrin SW 846 Method 8081B/3510 <0.00005 mg/L 04/06/2014 Heptachlor SW 846 Method 808113/3510 <0.00005 mg/L 04/06/2014 Heptachlor epoxide SW846 Method 808113/3510 <0.00005 mg/L 04/06/2014 Lindane SW 846 Method 808113/3510 <0.00005 mg/L 04/06/2014 Methoxychlor SW 846 Method 808113/3510 <0.00005 mg/L 04/06/2014 Toxaphene SW 845 Method 8081B/3510 <0.005 mg/L 04/06/2014 1,4-Dichlorobenzene (TCLP) SW 646 method 8270/3510 <0.050 mg/L 04/02/2014 2,4,5-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 04/02/2014 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/02/2014 2,4=Dinitrotoluene (TCLP) SW 646 method 827013510 <0.050 mg/L 04/02/2014 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/02/2014 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/02/2014 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/02/2014 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/02/2014 m + p-Cresol (TCLP) SW 846 method 827013610 <0.050 mg/L 04/02/2014 Nitrobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 04/02/2014 o-Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 04/02/2014 Pentachlorophenol (TCLP) SW 846 method 627013510 <0.250 mg/L 04/02/2014 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/02/2014 Paint Filter Test SW 846 Method 9095 A pass '04/14/2014 2,4,5-TP SW846 Method 8151A <0.0003 mg/L 04/03/2014 2,4-D SW846 Method 8151A <0.0003 mg/L 04/03/2014 1,1-Dichloroethylene SW846 Method8250/5030 <0.01 mg/L 04/26/2014 1,2-Dichloroethane SW846 Method 8260/5030 <0.01 mg/L 04/26/2014 Benzene SW846 Method 8260/5030 <0.01 mg/L 04/26/2014 Carbon Tetrachloride SW846 Method 8260/5030 <0.01 mg/L 04/26/2014 Chlorobenzene SW846 Method 8260/5030 <0.01 mg/L 04/26/2014 Chloroform SW846 Method 8260/5030 <0.01 mg/L 04/26/2014 Methyl ethyl ketone SW846 Method 8260/5030 <0.05 mg/L 04/26/2014 Report #:: 2014-03786 Page 1 of 4 .q Environmental Chemists, Inc. 6602 Windmill Way - Wilmington, NC 28405 (910) 392-0223 (Lab) - (910) 392-4424 (Fax) 710 Bowsertown Road - Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: May 15, 2014 706 Arendell Street Customer PO #: Morehead City NC 28557 Report #: 2014-03786 Attention: C. Sutton Report to: C. Sutton Project ID: Sludge Tetrachloroethylene SW846 Method 8260/5030 <0.01 mg/L 04/26/2014 Trichloroethylene SW846 Method 8260/5030 <0.01 mg/L 04/26/2014 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 04/26/2014 RCI Ignitability EPA1030 <0.8 mm/sec 04/11/2014 Cyanide EPA 335.4 <0.099 mg/kg 04/22/2014 Sulfide SM 4500 S D <0.198 mg/kg 04/23/2014 Sludge Residuals Aluminum EPA 200.7 7670 mg/kg 04/07/2014 Arsenic EPA 200.7 6.62 mg/kg 04/04/2014 Cadmium EPA 200.7 <1.88 mg/kg 04/04/2014 Calcium EPA 200.7 165000 mg/kg 04/03/2014 Chromium EPA 200.7 9.72 mg/kg 04/04/2014 Copper EPA 200.7 506 mg/kg 04/07/2014 Lead EPA 200.7 8.10 mg/kg 04/04/2014 Magnesium EPA 200.7 3280 mg/kg 04/03/2014 Molybdenum EPA 200.7 <1.88 mg/kg 04/04/2014 Nickel EPA 200.7 7.62 mg/kg 04/04/2014 Potassium EPA 200.7 2670 mg/kg 04/03/2014 Selenium EPA 200.7 4.59 mg/kg 04/04/2014 Sodium EPA 200.7 1530 mg/kg 04/03/2014 Zinc EPA 200.7 559 mg/kg 04/07/2014 Ammonia Nitrogen EPA350.1 177 mg/kg 04/16/2014 Total Kjeldahl Nitrogen (TKN) EPA 351.2 545 mg/kg 04/28/2014 Nitrate+Nitrite-Nitrogen EPA353.2 20.3 mg/kg 04/21/2014 Total Solids (%) SM 2540 B 70.4 % 04/02/2014 Total Phosphorus SM 4500 P F 5620 mg/kg 04123/2014 pH SW 846 Method 9045D 11.93 units 04/07/2014 Mercury SWB46 7471E 0.7420 mg/kg 04/28/2014 TCLP Metals Arsenic EPA 200.7 0.100 mg/L 04/04/2014 Barium EPA 200.7 <0.100 mg/L 04/04/2014 Cadmium EPA 200.7 <0.100 mg/L 04/04/2014 Chromium EPA 200.7 <0.100 mg/L 04/04/2014 Lead EPA 200.7 <0.100 mg1L 04/04/2014 Selenium EPA 200.7 <0.100 mg/L 04/04/2014 Report #:: 2014-03786 Page 2 of 4 Environmental Chemists, Inc. 6602 Windmill Way •Wilmington, NC 28405 M (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94.,DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: May 15, 2014 706 Arendell Street Customer PO #: Morehead City NC 28557 Report #: 1 2014-03786 Attention: C. Sutton Report to. C. Sutton Project ID: Sludge Silver EPA 200.7 <0.100 mg/L 04/04/2014 Mercury EPA245.1 <0.0020 mg/L 04/13/2014 Lab ID Sample ID: Collect Datefrime Matrix Sampled by 14-09192 Site: 1 4/1/2014 10:20 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 70.6 % 04/02/2014 Fecal Density SM 9221 C E MPN 24 hr 503 <1 MPN/g . 04/02/2014 Lab ID Sample ID: Collect Datefrime Matrix Sampled by 14-09193 Site: 2 4/1/2014 10:20 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 68.8 % 04/02/2014 Fecal Density SM 9221C E MPN 24 hr 503 <1 MPN/g 04/02/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-09194 Site: 3 4/1/2014 10:20 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 76.9 % 04/02/2014 Fecal Density SM 9221 C E MPN 24 hr 503 <1 MPN/g 04/02/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-09195 Site: 4 4/1/2014 10:20 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 72.0 % 04/02/2014 Fecal Density SM 9221C E MPN 24 hr 503 <1 MPN/g 04/02/2014 Lab ID Sample ID: Collect Datefrime Matrix Sampled by 14-09196 Site: 5 4/1/2014 10:20 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 71.2 % 04/02/2014 Fecal Density SM 9221C E MPN 24 hr 503 <1 MPN/g 04/02/2014 Report #:: 2014-03786 Page 3 of 4 VInvir®nmental Chemists, Inc. r d s j 6602 Windmill Way o Wilmington, NC 28405 v (910) 392-0223 (Lab) e (910) 392-4424 (Fax) 710 Bowsertown Road Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: May 15, 2014 706 Arendell Street Customer PO #: Morehead City NC 28557 Report #: 2014-03786 Attention: C. Sutton Report to: C. Sutton Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-09197 Site: 6 4/1/2014 10:20 AM Solid/Sludge C.Sutton & C.Dangerfield Test Total Solids (%) Fecal Density Lab ID Sample ID: 14-09198 Site:7 Test Total Solids (%) Fecal Density Method SM 2540 B SM 9221C E MPN 24 hr 503 Results Date Analyzed 71.0 % 04/02/2014 <1 MPN/g 04/02/2014 Collect Date/Time Matrix Sampled by 4/1/2014 10:20 AM Solid/Sludge C.Sutton & C.Dangerfield Method Results Date Analyzed SM 2540 B SM 9221 C E MPN 24 hr 503 69.7 % 04/02/2014 <1 MPN/g 04/02/2014 Comment: Sludge residuals and Fecal density reported on a dry weight basis. pH, RCI and Paint Filter Test reported on an as received basis. Reviewed by: Report #:: 2014-03786 Page 4 of 4 gn'gpm "i" xl - Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWO CERTIFICATION'#94 NCDHHS: DLS CERTIFICATION #37729 6602 Windmill Way Wilmington, NC 28405 OFFICE., 910-392-0223 FAX 910-392-4424 lnfo@environmentalchemista.com COLLECTIONAND CHAIN OF CUSTODY .TENT: 111are,4e.J Cl PROJECT NAME: REPORT NO: )DRESS: CONTACT NAME: _ C. PO NO: -REPORT TO; PHONEIFAX: ICOPY TO: lemail: MpleCil Idy: C. -4V4,if-I ! L -- ldfta,"14 SAMPLE TYPE: I_= Influent, 1E = Effluent, W = Well, ST = Stream, SO = toll, SL = Sludge, Other: 'sample Identification Collection CL E a 2 PRESERVATION I ANALYSIS REQUESTED Date Time Temp lu 0 z 541H SL C r G C C9 e 4 Xc G G C -Ty— G G C 9 Fic, A7,w 4' G C 1D_ (Ci G C (p —re— G C (D 19 1 q rG) G b G C q G C (p) G Transfer Reknsu shed By: Date/Time Received B Date/Time w J'q s,27J nperature wnen eceiv _J- t�l Accepted: t/ —Rejected: F 4) Resample IR, , ) __ I 'livered By:_W 71 1 11 1 Becelved By: ate: TU mments., TU Time: 00 Il1+IP+t)RAIrTT NOTICE odh C,mAmDiv AM ofilfahrQ,aality (ii1iGDW( is stdcdly etd'bldn EPA.te:galalfonsfar sample Cdh=tiCM andptesesezHum Client Must pxy" the Fonaowimg Information 1_ SAMPLE IDENTIFICATION (Containef "on*cd.vvith mqm tedtcftW 2_ SAMPLE TYPE (Compass Grub, Watw. Sail. ctr-) 3. DATE COLLECTED 4. TU E VOLLECTED S. SAMPLE COLLECTOR i. 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Nany rI ical should get anyuorsinn Ordodws AD& nounyvvi& water aad seegme d'cA moat DeddoriwaiiraSamaies thatleoebreAcia PremvzUm 1_ Add4-5 grmules ofti nsuWateto abattlevvilh an acid pmenrifive_ 2_ After misingto dissolve lhetbiosdfate,PMwhalf of the sample into abntfic cuntining add as apme molive_ (AmmoniafTHNj._ ' 3 _ Then complet y fM bath bottles with fi wh sample_ Aaeegadardate oaed4 tine co11ecbdL =vgAe cdIedw. =dun gfpMperpm9wFa6,vm .A bem Mai=& E=h==n emoAde dY m &— + SU'e 0""C edledimsite mail Ret WCAC 2H O805 (a) �vti*&mtieel eottecfiu%ba"Mfm%°� m �� tai y ea9fl¢c rue i -.At arrzyfine ataboiala[yreaeives samples p1e � etirr�et annd aeeot a amtber sar•pte ifpoaile. if a ow smple oxmotbe :sea r4 fbe aodeal ==vh maybe aaa reabd em xvSF s s d=wttm " ot'tbeel aarltbeiaboaatacgmvstmtitythe Stabs-Lab�a�dlosgatbatR,em6radian(s}"Tbec,�nm�mst shda� ate ��44r �� ftpmwm fiw aawplena ' Rxt WCAC IH0t05 (a)(?) EYi}- Town of Morehead City WQ0034842 Morehead City WWTP . ......... ..... ....... ... ............ .......... .. ..... --- ....... ... ................ ... ........... ................ ......... ............. ........... .. . ....... ...... ............. ............... :............ ............ ........ . . ...... ....... . ......... . --'-p ::.g am::: . ......... 04/01/14 1 0.0000 04/01/14 1 0.0000 04/01/14 1 0.0000 04/01/14 1 0.0000 04/01/14 1 0.0000 04/01/14 1 0.0000 04/01/14 1 0.0000 Total 0.0000 Average 0.0000 Geometric Mean 1>>»>> Fecal Coliform MPN / gram Geometric Mean of Less than LOOO MPN/g meets Class A - Alternative I Pathogen for Reduction requirement. 12 I Town of Morehead City Daniel Williams, Public Utilities Director 706 Arendell Street Morehead City, NC 28557 252-726-6848, Permit #WQ0034842 A.,mi;� n�ro- a—ii imA Bio-Solids Analysis/Release of Liability CLASS A EXCEPTIONAL QUALITY (EQ) BIO-SOLIDS ANALYSIS Concentration Analysis Date Name Concentration (mg/kg) Dry Weight Pollutant Concentrations (Table 3,40 CFR 503.13) (monthly average) Ceiling Concentrations* (Table 1, 40 CFR503.13) (daily maximum) Total.Solids % 71.5% 04/02/2014 Feca((oliform (MPN),/gram Solids < 1 04/02/2014 Plant Available Nitrogen 219 mg/kg 05/15/2014 Phosphorus, Total [dry wt.) 5620 mg/kg 04/23/2014 Potassium, [dry wt.] 267o mg/kg 04/03/2014 Arsenic 6.62 41 mg/kg 75 mg/kg Agriwltural Lime Equivalent 3.11+/ac 06/18/2014 Cadmium <1.88 39 mg/kg 85 mg/kg Pathogen Reduction (40 CFR 503.32: Class A (Alternative Al) Thermally Treated Bio-Solids I Vector Attraction Reduction' (40 CFR 503.33): Motion 1) Alkaline Stabilization *Blo-Solids may not be land applied if any pollutant exceeds these values Copper 506 1500 mg/kg, 4300 mg/kg Lead 8.10 300 mg/kg 840 mg/kg Mercury 0.7420 17 mg/kg 57 mg/kg Molybdenum <1.88 n/a ' 75 mg/kg Nickel 1 7.62 1 420 mg/kg 420 mg/kg Selenium 1 4.59 1 100 mg/kg 100 mg/kg Zinc 1 559 2800 mg/kg 7500 mg/kg CERTIFICATION Ph Z ` �� Date of Transport ! I Certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. A. ame and OM 'al Title (type or print) B. Area Code and Telephone Number: ' 252-726-6237 C. ture* D. Date Signed: _ Recipient Name: Il S Irt' Address: 1 I N'''s'jV Telephone: Class A EQ iBio-Solids Amount Received: Intended Use: S' !Al Location of Land Application Site: Land Application Instructions: 1. The Class A EQ Bio-Solids Product shall be applied such that all applicable buffers, including a 10 foot buffer between any land application site and any public or private water supply source including wells, as well as any streams, rivers, lakes and drainage way, shall be maintained on any site. 2.. The Class A EQ Bio-Solids Product is prohibited on any site that' is flooded frozen or snow covered. i 3. Adequate procedures shall be provided to preventsurface runoff from carrying any disposed or stored classA EQ residuals product into any surface waters. 1, dw 4ffh'I / ("Recipient') understand that application of the Class A EQ Bio-Solids,product to the land is prohibited except in accordance with the instructions on this information form. I further understand that I am responsible for the i transporting of the Class A EQ Bio-Solids product which has been distributed to me. I am aware that by signing this form, I am releasing the Town of Morehead City of any'liabilities from improper land application and transporting of the Class A EQ Bio-Solids product. Signature I , �.j lsi Date J 0 Printed Name OP?VI LI M _. Town of Morehead City Daniel Williams, Public Utilities Director 706 Arendell Street Morehead City, NC 28557 252-726-6848, Permit #WQ0034842 Bio-Solids Analysis/Release of Liability CLASS A EXCEPTIONAL QUALITY (EQ) BIO-SOLIDS ANALYSIS Concentration Analysis Date Name Concentration (mg/kg) Dry Weight Pollutant Concentrations (Table 3, 40 CFR 503.13) (monthly average) Ceiling Concentrations* (Table 1, 40 CFR503,13) (daily maximum) Total Solids% 715% 04/02/2014 Fecal Col"iform (MPN),/gram Solids_ < 1 04/02/2014 Plant Available Nitrogen 219 mg/kg 0511512014 Phosphorus, Total [dry wt.] 5620 mg/kg 04/2$/2014 Potassium, [dry wt.] 2670 mg/kg 0410312014 Arsenic 6.62 41 mg/kg 75 mg/kg Agricultural Lime Equivalent 3.11 +/ac 06/18/2014 Cadmium <1.88 39 mg/kg 85 Mg/kg Pathogen Reduction (40 CFR 503.32: Class A (Altemative Al) Thermally Treated Bio-Solids Vector Attraction Reduction (40 CFR 50333): (Option 1) —Alkaline Stabilization `Bio-Solids may not be land applied if any pollutant exceeds these values Copper 505 1500 mg/kg 4300 mg/kg Lead 8.10 300 mg/kg 840 mg/kg Mercury 0.7420 17 mg/kg 57 mg/kg Molybdenum <1.88 n/a 75 mg/kg Nickel 1 7.62 420 mg/kg 420 mg/kg Selenium 4-59 100 mgAg 100 mg/kg Zinc 559 2800 mg/kg 7500 mg/kg CERTIFICATION Ph q=7 Date of Transport J Z zo I y I Certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to.assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. / A- Na a and Official Tide (type or print) (.��'/ �✓�7 v I cl k B. Area code and Telephone Number. 252 726.6237 C. Signa D. Date Signed: Recipient Name: �9 Address: Telephone: — �f3 �' Gass A EQ 80-Solids Amount Received: -`• Intended Use: r:j .oj9,C Location of Land Application Site: iStA In%yee Of,& -sib Land Application Instructions: 1. The Gass A EQ Bio Solids Product shall be applied such that all applicable buffers, including a 10--foot buffer'between any land application site and any public or private water supply source including wells, as well as any streams, rivers, lakes and drainage way, shall be maintained on any site. 2. The Class A EQ Bio Solids Product is prohibited on any site that is flooded frozen or snow covered. i 3. Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored class A EQ residuals product nto any surface waters. 1, ("Recipients) understand that application of the Class A EQ Bio-Solids product to the.land is _ ohi " d Acept in accordance with the instructions on this information form. i furthef understand that I am responsible for the transporting of the Class A EQ Bio-Solids product which has been distributed to me. 1 am aware that by signing this form, I am releasing the Town of Morehe Gty of any liabilities om improper land application and transporting of the Class A EQ Bio-Solids product. Date Signature —a Printed Name / s MHC Data Summary 2014.xis Summary Morehead City, NC Project: #26001 Date Cake (Ibs) Dry Solids (Ibs) Avg % Solids Lime Add'n (Ibs) Avg Lime Dose Biosolids pH (Cake Ibs) (Dried Ibs) 2hr 24hr January 2014 0 0 .0.0% 0 0.0% 0 0 0.00 0.00 January Totals: 0 0 0.0% 0 0.0% 0 0 February-2014-- - ------ 0-- - - - 0-- -- - - -0:0% ... - -- - 0-- --- ---0:0%-- --- ., ...0. - 0 - 0:00 0.00-- February Totals: 0 0 0.0% 0 0.0% 0 0 March 2014 03/18/14 9,458 1,562 16.5%' 543 3&0% 10,011 5,105 12.01 03/19/14 29,190 4,960 17.0% 980 20.0% 30,170 15,386 12.14 03/20/14 19,452 3,306 17.0% 662 20.0% 20,144 10,273 12.28 03/21/14 7,795 1,325 17.0% 281 22.0% 8,078 4,120 12.30 March Totals: -65-;895-- 11,1-53 13:5% 2,466-_. - 24.3°/a - -681403 34,884 April 2014 04/14/14 26,158 5,047 19.3% 803 15.9% 26,961 13,750 12.46 04/15/14 9,787 1,663 19.0% 293 17.6% 10,080 5,140 12.30 04/16/14 20,449 3,484 17.0% 668 19.2% 21,207 10,815 12.44 04/17/14 20,569 3,825 18.6% 647 16.9% 21,216 10,820 12.50 MHC Data Summary 2014.x1s Summary rehead City, NC April Totals: 76,963 14,019 18.5% May-W14 - - --------05/19/14 •-27;367 ---5;062 18.6% Uaicv 1-4 G0,001 4518 - _ 17.0% 05/22/14 14,561 2, 474 17.0% May Totals: 86,537 14,948 17.4% June Totals: 49,350 8,711 17.5% 2014 07/14/14 17,995 3,239. 18.0% 07/1.5/14 29,539 5,316 18.0% Project: #25001 (Ibs) Dose (.Cake Ibs) (Driedlh 2,411 17.4% 79,464 40,525 i DO-- -879--- - 19.5% ----17,794-- - _ 27,460 - _- _ , - 9-'0.75.. 14,004 1'2-36 12.40 656 26.5% - 15,216 7,455 12.40 3,455 23.8% 89,011 45,089 1,200 538 20.5% 18.8% 33,683 17,404 16,841 9,050 12.50 12:30 1,738 19.7% 51,087 25,891 856 26.4% 18,851 9,802 12.50 MHC Data Summary 2014.xis Summary City, NC Project: #25001 07/16/14 07/17/14 07/18/14 J.-I 39,146 267324 8,819 %lua► 7,044 4,474 1,587 I 18.0% 17.0% 18.0% I(Ibs) 1,437 799 306 Dose .20.4% 17.9% 19.3% (Cake Ibs) 40,583 27,123 9,125 (Dried Ibs) 21,103 2hr 12.23 14,103 12.50 4,471 12.33 .. July.T.otals:. _. 08/05/14 24,568 4,176 18.0% 813 19.5% 08/06/14 24,730 4,451 18.0% 8.16 18.3% 08/07/14 25,026 3,753 15.0% 754 20.1% 08/08/14 8,220 1,068 13.0% 384 36.0% 08/25/14 17,077 2,902 17.0% 624 21.5% 08/26/14 21,494 3,653 17.0% 738 20.2% 08/27/14 29,075 4,946 17.0%° 1,225 24.8% 08/28/14 30,820 5,238 17.0% 1,195 22.8% 08/29/14 12,733 1,909 15.00/- 480 25.1% August Totals:) 193,743 I 32,096 I 16.3% I 7,029 I 23.1 % 09/15/141 27,729 1 4,713 17. 09/16/14 25,348 4.309 117. 09/17/14 09/ 18/14 25,388 1 12,561 1 4,315 1 2-135 1 17. 17 703 1 3 17,701 9,027 22,232 12,449 29,075 15,119 31,709 16,448 13,213 6,870 199,241 1 107,686 423 14,500 1 ' 12.04 154 13,338 12.41 180 13,351 12.33 044 6,654 1 12:21 MHC Data Summary 2014.xis Summary Morehead City, NC Project: , #25001 Date Cake (Ibs) Dry Solids (lbs)(Ibs) Avg. % Solids Lime Add'n Avg Lime Dose Biosolids pH (Cake Ibs) (Dried Ibs) 2hr 24hr September Totals: 91,026 15,472 17.0% 2,785 18.7% 93,801 47,843 December- 2014_.-... .._ _...._._- _. _ .__.._...... 12/02/14 -12/03/14� 12/04/14 .- 5;848-- ----25;093_.,._- 25,130 -993- _ _ _-4;398-_...__ 4,246 '-17:0%----- __ _.17:5'/0 _._ -16.9% _ 1,050 984 23:9% 23.2% ---6;060 26,143 26,114 3,,636 10,457 9,139 12.17. - 12.20 12.29 December Totals: 56,071 9,637 17.1% 2,249 22.9% 58,317 23,232 nu w vaa cv JUJ I o./C15 Morehead City, NC #25001 Date: 03/18/14 Batch #1 Initial Cake Solids: Batch Weight: 16.5% 10,000 Lime Dose: 34.8% Time Biosolids (Ibs) % Solids Dry Weight Product Temp Lime Affn Sludge Feed (Ibs) Total Biosolids (Ibs) (Ibs) (F) (Ibs) Cake Dry Wet Dry 1:30 2M 10,011 9,244 21.9% 23.6% 2,192 2,192 161 156 543 9,548 1,562 10,011 2,105 2:30 8,482 25.7% 2,192 155 3:00 7,331 29.8% 2,192 154 3:30 6,657 33.0% 2,192 155 4:00 5,881 37.2% 2,192 164 4:30 4,720 46.5% 2,192 189 --�3,1'84v -__ 52.0% 2,192 184 543 9,548 1,562 10,011 2,105 wn w ✓ala GV IJUJ 1.7.RW - Morehead City, NC #25001 Cake Solids: 17.0% Lime -Dose: 19.8% Date: 03/19/14 Batch #1 Initial Batch Weight: 10,000 Time 8:00 8:30 Biosolids (Ibs) 10,021 9,665 % Solids 29.3% 30.2% Dry Weight (Ibs) 2,936 2,936 Product Temp (F) 138 112 Lime Add'n (lbs) 369 Sludge Feed (Ibs) Total Biosolids (Ibs) Cake 9,652 Dry 1,640 Wet 10,021 Dry 2,010 9:00 9,090 32.1% 2,936 167 9:30 8,109 36.0% 2,936 113 10:00 6,973 42.2% 2,936 119 10:30 6,094 47.9% 2,936 168 11:00 5,570 52.4% 2,936 11:10 11:30 5,218 3,205 54.0% 2,936 182 182 11:55' 12:30 10'098 9,149 28:3% 31.5% 2,858 .2,858 184 171. 310 9,788 1,663 10,098 1,973 1:00 .8,434 34.1% _ 2,858 167 1:30 7,373 39.0% '2,858 166 2:00 6,81.0 42.3% 2,858 185 2:30 5695 50.4% 2,858 191 3:05 5,309 54.0% 2,858 190 3:25 2,060 197 3:35 4:00 10,051 9;824 30.4% 32.6% 3,055 3,055 191 187 301 9,750 1,657 10,051 1,967 4:30 8,616 37.0% 3,055 186 5:00 7,994 40.0% 3,055 184 5:30 6,786 47.0% 3,055 191 6:00 6,131 52.0% 3,055 196 980 29,190' 4,960 30,170 51950 I rehead City, NC #25001 Date: 03/21/14 Batch #1 Time Biosolids % Solids (Ibs) 8:48 3,049 9:08 8,076 28.2% 9.36 7,754 29.6% 2 10:00 7,232 31.8% 2 10:30 6,455 35.7% 2 11:00 5,569 41.3% 2 11:30 5.122 44.8% 2 12:00 1 12:25 4,582 4.415 50.2% 59 no/ 2 1) MHC Data 20130321.xls Cake Solids: 17.0% Initial Batch Weight: 8,000 ight Product Temp Lime Add'n Sludge Feed (Ibs) (F) (Ibs) Cake Dry 143 i 141 281 7,795 1,325 141 141 142 155 ' 163 ' 182 183 281 7,795 1.325 Lime Dose: 21.2% TOWN OF MOREHEAD C1YT WWTP WQ0034842 pH Log 2014 Class "A" Biosolids Date Initial pH 2 Hour pH 24 Hour PH IOperator Initials Temp C Correction Factor PH Temp C Corr. Factor + Corrected H Time pH Time pH Time 3/20/2014 12.34 24 -.03 12.31 1215 12.33 1415 12.11 1215 CDD 40 Plus 0.45 39 Plus 0.42 4/14/2014 12-40 27 +.06 12.46 1330 12.46 1530 12.34 1330 CS 38 Plus 0.39 37 Plus 0.36 5/19/2014 12.73 21 -.12 12.61 1300 12.64 1500 12.5 1300 CS 36 Plus 0.33 35 Plus 0.30 6/25J2014 12.04 24 -.03 12.01 1100 12.09 1300 12.08 1100 CS/CDD 34 Plus 0.27 33 Plus 0.24 7/16/2014 12.20 28 -F.09 12.29 1100 1229 1300 12.23 1100 CS 32 Plus 0.21 31 Plus 0.18 8/5/2014 12.15 25 0 12.15 1130 12.08 1330 11.58 1130 CS 30 Plus 0.15 29 Plus 0.12 8/26/2014 12.13 25 0 12.13 1220 12.26 1420 12.05 1220 CDD/CS 28 Plus 0.09 27 Plus 0.06 9/15/2014 12.24 22 -.09 12.15 1245 12.22 1445 12.32 1245 CS 26 Plus 0.03 25 0.00 12/3/2014 12.12 25 0 12.12 1310 12.11 1510 11.92 1310 CS/CDD 24 Minus 0.03 23 Minus 0.06 22 Minus 0.09 21 Minus 0.12 20 Minus 0.15 19 Minus 0.18 18 Minus 0.21 17 Minus 0.24 16 Minus 0.27 15 Minus 0.30 14 Minus 0.33 13 Minus 0.36 12 Minus 0.39 * 2 HR and 24 HR Ph's are corrected 11 Minus 0.42 10 Minus 0.45