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HomeMy WebLinkAboutWQ0034806_Residual Annual Report 2014_20150204RECRVED 2014 ANNUAL REP6k*u 4 2015 LAND APPLICATION PRQyN COASTAL FARMS AND ANNOWXINNIT PERMIT OWQ0034806 Prepared For: Coastal Farms and Residuals, LLC 8155 Malpass Corner Road Currie, North Carolina 28435 Compiled By: S&ME, Inc. 8646 West Market Street, Suite 105 Greensboro, North Carolina 27409 February 2015 February 2, 2015 I I NCDENR-DWQ 512 North Salisbury Street Raleigh, North Carolina 27604 Attention: Information Processing Unit Reference: 2014 LAND APPLICATION ANNUAL REPORT Coastal Farms and Residuals, LLC Permit No. WQ0034806 S&ME, Inc. Project No. 1588-09-034 1 Non -Discharge Compliance Unit: S&ME, Inc. (S&ME) is submitting all monitoring and reporting requirements as specified in ' the above referenced permit on behalf of Coastal Farms and Residuals, LLC. S&ME compiled this report using data gathered during the compliance year by Coastal Farms and r Residuals, LLC. This data includes: 1) certification form, 2) residuals analyses and pathogen / 5 vector data, 3) application summaries and field loading rate reports, 4) soil analyses. If there is any further information required or questions regarding this annual report please do not hesitate to contact Coastal Farms and Residuals, LLC or S&ME for further assistance. Sincerely, S&ME, Inc. Martin Mabe �obWillcox, L.S.S. a NC Land Application/Residuals Operator Natural Resources Services Leader #22753 Enclosures T:\Projects\2009\ENV\1588-09-034 Coastal Residuals\2014 Annual Report\2014 ANNUAL REPORT.doc S&ME, INC. / 8646 W. Market Street, Suite 105 / Greensboro, NC 27409 / p 336.288.7180 f 336.288.8980 / www.smeinc.com TABLE OF CONTENTS SECTION NO. TITLE I Certification Form H Residuals Analyses & Pathogen / Vector Attraction Data III 2014 Application Summary and Field Loading Rate Reports IV Soil Analysis CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0034806 County: Pender Year: 2014 Facility Name (as shown on permit): Coastal Farms and Residuals, LLC Land Application Operator: Mr. Wesley Wooten Phone: 910-283-5444 Land application of residuals as allowed by the permit occurred during the past calendar year? ! ► Yes No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach.an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in thepermit: 13 Total number of fields utilized for land, application during the year: 1 Total amount of dry tons applied during the year for all application sites: 226.65 Total number of acres utilized' for land application during the year: 93.4 Part B - Annual Comoiance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. vi Yes =J No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and,three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T . I I05(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .11 l 1 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 1 I) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified' in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing viola _ons Mr. Wesley W000ten, President Permittee Name and Title (type or print) Signature of Permittee Date Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) RESIDUAL ANALYSES TCLP ANALYSES IF REQUIRED AND PATHOGEN AND VECTOR ATTRACTION REDUCTION Ll ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach ft fwm to tha corteapandirg hrboretmy enalyds. Pkeae now that your permit may contain additional pammetera to ba snaWed then (ham required to be su nnuffued on this form. Permit Number Effii;�: Facility Name siduals Laboratory ironmenta�Inq- t3 NPDES 9 ,WWTP Name 2014 DATA Arseft - 2.05 Cadmium 2.05 Comr 882 00 Lead Mercury 2820 OAS Mc um NidW 2.05 14.80 Selemlum 4.92 23nc TKN Ammonla•N an 1 000. 00 30 700.00 3 550.00 Ntb WN 4115.00 Total Phosohorus 7 o9o.o0 x 2 _2 S^ (SIGNATU OF PREPARER) DATE I certify, and r penally of law, that this document was prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: May 6, 2014 Carolina Beach WWTP Permit No. NCO023256 3.76 % Solids 6.8 nH Parameter I % JMg/KgDrXWeighf x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 3.070 30,700.000 61.400 Phosphorus 0.709 7,090.000 14.180 Potassium 0.219 2,190.000 4.380 PAN (injected)* 1.218 12,180.000 24.360 PAN surface)* 1.041 10,405.000 20.810 Ammonia Nitrogen 0.355 3,550.000 7.100 Calcium 3.620 36,200.000 72.400 Calcium Carbonate E . --- --- --- Magnesium --- 4,630.000 9.260 Sodium --- 4,760.000 9.520 Sulfur --- --- --- Nitrate N / Nitrite N --- 485.000 0.970 Barium --- --- --- SAR 1.21 Chloride --- --- --- Iron --- --- --- Ceiling Concen. /K Aluminum --- 4,390.00 8.780 Arsenic --- 2.05 0.004 75 Cadmium --- 2.05 0.004 85 Chromium --- 18.800 0.038 --- Copper --- 862.00 1.724 4,300 Lead --- 28.20 0.056 840 Mercury --- 0.48 0.001 57 Molybdenum --- 2.05 0.004 75 Nickel --- 14.80 0.030 420 Selenium -- 4.92 0.010 100 Zinc --- 1,000.00 2.000 7,500 Environmental Chemists # 2014-05216 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: ' (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) $M 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252)473-5702 CHEMISTS NCDENR.- DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town of Carolina Beach Date of Report: Jun 19, 2014 1121 North Lake Park Blvd Customer PO M Carolina Beach NC 28428 Customer ID: 08100295 Attention: Bill Raymond Report M 2014-05216 Project ID: Wastewater Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-12545 Site: SSB#2 6/6/2014 10:03 AM SolidlSludge Bill Raymond Test Method Results Date Analyzed Chlordane SW846 Method 8081B/3510 <0.005 mg/L 05/16/2014 Endrin SW 846 Method 8081 B/3510 <0.00005 mg/L 05/16/2014 Heptachlor SW 846 Method 8081 B1351 0 <0.00005 mg/L 05/16/2014 Heptachlor epoxide SW 846 Method 8081B/3510 <0.00005 mg/L 05/16/2014 Lindane SW 846 Method 8081B/3510 <0.00005 mg/L 05/16/2014 Methoxychlor SW 846 Method 80818/3510 <0.00005 mg/L 05/16/2014 Toxaphene SW 846 Method 8081 B1351 0 <0.005 mg/L 05/16/2014 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/16/2014 2,4,5-Trichlorophenol(TCLP) SW 846 method8270MIO <0.050 mg/L 05/15/2014 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/15/2014 2,4-Dinitrotoluene (TCLP) SW 846 method 827013510 <0.050 mg/L 05/15/2014 Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 05/15/2014 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270=10 <0.050 mg/L 05/16/2014 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050. mg/L 05/15/2014 Hexachloroethane (TCLP) SW846 method 827013510 <0.050 mg/L 05115/2014 m + p- Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05115/2014 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/15/2014 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/15/2014 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/15/2014 Pyridine (TCLP) SW846 method 827013510 <0.050 mg/L 05/15/2014 2,4,5-TP SW646 Method 8151A <0.0003 mg/L---- -05/1912014 - - 2,4-D SW846 Method 8151A <0.0003 mg/L 05/19/2014 1,1-Dichloroethylene SW846Method 8260/5030 <0.01 mg/L 05/16/2014 1,2-Dichloroethane SW846 Method 826015030 <0.01 mg/L 05/16/2014 Benzene SW846 Method 826015030 <0.01 mg/L 05/16/2014 Carbon Tetrachloride SW846 Method 8260/6030 <0.01 mg/L 05/16/2014 Report #:: 2014-05216 Page 1 of 3 I I Environmental Chemists, Inc. env 6602 Windmill Way •Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) ® 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 - ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town of Carolina Beach Date of Report: Jun 19, 2014 1121 North Lake Park Blvd Customer PO #: Carolina Beach NC 28428 Customer ID: 08100295 Attention: Bill Raymond Report #: 2014-05216 Project ID: Wastewater Chlorobenzene SW846 Method 8260/6030 <0.01 mg/L 06/16/2014 Chloroform SW846 Method 8260/5030 <0.01 mg/L 06/16/2014 Methyl ethyl ketone SW846 Method 826015030 <0.05 mg/L 06/16/2014 Tetrachloroethylene SW846 Method 8260/5030 <0.01 mg/L 05/16/2014 Trichloroethylene SW846 Method 8260/5030 <0.01 mg/L 05/1612014 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 05/16/2014 RCI Cyanide EPA 335.4 <0.124 mg/kg 05/20/2014 pH SM 4500 H B 6.80 units 05/15/2014 Sulfide SM 4500 S o <0.249 mg/kg 05/20/2014 lgnitability SW 846 method 1010 >212 °F 05/08/2014 Sludge Residuals Aluminum EPA200.7 4390 mg/kg 05/16/2014 Arsenic EPA200.7 <2.05mg/kg 05113/2014 Cadmium EPA200.7 <2.05mg/kg 05/13/2014 Calcium EPA200.7 36200mg/kg 05/14/2014 Chromium EPA200.7 18.8 mg/kg 06/13/2014 Copper EPA 200.7 862 mg/kg 05/13/2014 Lead EPA200.7 28.2 mg/kg 05/13/2014 Magnesium EPA200.7 4630mg/kg 05/14/2014 Molybdenum EPA200.7 <2.05mg/kg 05/13/2014 Nickel EPA200.7 14.8mg/kg 06/13/2014 Potassium EPA200.7 2190 mg/kg 05/14/2014 Selenium EPA200.7 4.92mg/kg 05/13/2014 Sodium EPA200.7 4760mg/kg 05/14/2014 Zinc EPA200.7 1000mg/kg 05/13/2014 Ammonia Nitrogen EPA350.1 3550mg/kg 05/12/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 30700mg/kg 05/14/2014 Nitrate+Nitrite-Nitrogen EPA353.2 485mg/kg 05/14/2014 Report#r 2014-05216 Page 2 of 3 Environmental Chemists, Inc. 7envirochem 6602 Windmill Way - Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DI.S CERTIFICATE #37729 Town of Carolina Beach 1121 North Lake Park Blvd Carolina Beach NC 28428 Attention: Bill Raymond Date of Report: Jun 19, 2014 Customer PO #: Customer ID: 08100295 Report #: 2014-05216 Project ID: Wastewater - Total Solids (%) SM2540 B 3.76 % 05/07/2014 Total Phosphorus SM 4500 P F 7090 mg/kg 05/21 /2014 Mercury SWW7471B 0.4840mg/kg 06/07/2014 TCLP Metals Arsenic EPA 200.7 <0.100mg/L 05/15/2014 Barium EPA 200.7 <0.100 mg/L 05/15/2014 Cadmium EPA 200.7 <0.100 mg/L 05/15/2014 Chromium EPA 200.7 <0.100mg/L 05/15/2014 Lead EPA 200.7 <0.100 mg/L 05/15/2014 Selenium EPA 200.7 <0.100mg/L 05/15/2014 Silver EPA200.7 <0.100mg/L 05/15/2014 Mercury EPA245.1 <0.0020mg/L 05/14/2014 Comment: Sludge residual results reported on a dry weight basis. Reviewed by: Report*: 2014-05216 Page 3 of 3 Anaiytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLI=CTION AND CHAIN OP CUSTODY . 6692 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 Info@environmentalchemists.com CLIENT: (TttT1.1 O WU j"ZOC PROJECT NAME: V)OG�t G`!�1 t`•M t'.11; REPORT NO: ADDRESS: O S •� CONTACT NAME: ,% C f�nc PO NO: -7 Z 7 VOLMUM-ReCICL, NC 1. 20 REPORT TO: IiG&CdI.Cr C UVAV�ek.O M PRONE/PAX: qt0% IJR-1%'7Oi-7000 COPY TO: - email: b ll Yx µow caolir4y-Of Ramnlprl Rv- t 112-ri\i AffkA SAMPLE TYPE: I = Influent. E = Effluent, W = Well, ST = Stream. SO = Soil. SL = Sludge. Other: 'Sample Identification Collection M.y 5 N w w a E' G 0 ;, c t9 c U V z e .5 o LU a M -� z PRESERVATION ANALYSIS REQUESTED Date Time Temp Z N o o c SSl3 2 rrlo-I 1 UO3 1:7 i/ Ia ll� a# )( 1, cfi0.1 5 G c P sy G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished -By: Date/Time Received By: Dateffime /aji 1Lisa GIs-t41 loll z. 116 l�{l 4 : a o Temperature when Received: Accepted: ejec e : rcesampie rcequestea. I Delivered By: Received By. Q� �� Date: 5-CGIV Time: /S o Comments: TURNAROUND: LEWIS FARMS WQ0000455 Carolina Beach WWTP . . . ..... .. ............................ ........... . ......... .............. . ...... ................. ..... . . .. ..... .... 04/15/14 6,389 3.8054 04/15/14 3,602 3.5565 04/23/14 219,513 5.3415 04/23/14 415,585 5.6187 04/23/14 241,936 5.3837 04/23/14 240,642 5.3814 04/23/14 415,585 5.6187 Total 1 34.7058 Average 1 4.9580 Geometric Mean Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. I Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab),• (910)392-4424(Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DI.S CERTIFICATE #37729 Town of Carolina Beach Date of Report: Apr 21, 2014 1121 North Lake Park Blvd Customer PO #: Carolina Beach NC 28428 Report #: 2014-04382 Attention: Bill Raymond Report to: Bill Raymond A Project ID: Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-10545 Site: Basin #1 4/15/2014 10:17 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (°!°) sM 2540 B 3.60 % 04/16/2014 Fecal Density SM 9221C E MPN 24 hr503 6389 MPN/g 04116/2014 Lab ID Sample ID: �i Collect Date/Titne Matrix Sampled by 14-10546 Site: Basin #2 4/15/2014, 10:17 AM Solid/Sludge Client Test Method Results Date Analyzed I Total Solids (%) - sM 2540 B 3.61 % - 04/16/2014 Fecal Density SM 9221C E MPN 24 hr.903 3602 MPN/g 04/16/2014 Comment: Results reported on a dry weight basis. Reviewed by: / N),'0 , NQ'InAt Report #:: 2014-04382 Page 1 of 1 � .NC PRIM ON 07 I'lTo. Date Temp. .5a.1p lit �rl -c ..-CRI( Fe-ca jd P. P I. G mm it No eml dQChkM Pm. A, V. r Environmental Chemists, Inc. • 'chem 6602 Windmill Way •Wilmington, NC 28405 (910)392-0223(Lab) • (910) 392-4424 (Fax) sM 710 Bowsertown Road a Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town of Carolina Beach, Date of Report: Apr 28, 2014 1121 North Lake Park Blvd Customer PO #: Carolina Beach NC 28428 Report #: 2014-04734 Attention: Bill Raymond Report to: Bill Raymond Project ID: Wastewater Treatment- Pollutant Scan Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-11387 Site: Sludge #1 4/23/2014 11:58 AM Solid/Sludge Bill Raymond - Test Method Results Date Analyzed Total Solids (°to) SM 2540 B 4.10 % 04/24/2014 Fecal Density SM 9221C E: MPN 24 hr 503 219513 MPN/g 04/24/2014 Lab ID Sample ID: Collect DateITime Matrix Sampled by j 14-11388 Site--- Sludge #2 4/23/2014 11:58 AM Solid/Sludge Bill Raymond Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.85 % 04/24/2014 Fecal Density SM 9221 C E MPN 24 hr 503 415585 MPN/g 04/24/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-11389 Site: Sludge #3 4/23/2014 11:58 AM Solid/Sludge Bill Raymond Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.72 % 04/24/2014 Fecal Density SM 9221C E MPN 24 hr 503 241936 MPN/g 04/2412014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-11,390 Site: Sludge #4 4/23/2014 11:58 AM Solid/Sludge Bill Raymond, Test Method Results Date Analyzed Total Solids (%) SM 2640 B 3.74 % 04/24/2014 Fecal Density SM 9221C E MPN 24 hr 503 240642 MPN/g '04/24/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-11391 Site: Sludge #5 4/23/2014 11:58 AM -Solid/Sludge Bill Raymond Test Method Results Date Analyzed j, Total Solids (%) SM 2640 B 3.85 % 04/2412014 Fecal Density SM 9221C E MPN 24 hr 603 415585 MPN/g 04/24/2014 - Report #:: 2014-04734 Page 1 of 2 envirochem ANALYTICAL & CONSULTING CHEMISTS Town of Carolina Beach 1121 North Lake Park Blvd Carolina Beach NC 28428 Attention: Bill Raymond Environmental Chemists, Inc. 6602 Windmill Way o Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Date of Report: Apr 28, 2014 Customer PO #: Report #: 2014-04734 Report to: Bill Raymond Project ID: Wastewater Treatment - Pollutant Scan Comment: Results reported on a dry weight basis. Reviewed by: 4 I I7 Page 2 of 2 Report#:: 201404734 »sw� t.srs'ars a EN l:; _•t�ilUTLC. 1FM[ST;.IC�► ���': < • •�,'.Chemises 11COENR:•DWWQ`CERTIFICATIdtilr' . OFFICE: T110 392-0223 FAX �10 392�f424 �;g' �.94'NCaliHS: DL•S`G.ERTlFICATgN * 37729 COLLECTION•AND'CHAIN OF CUSTODY CLIENT: Ct f-0 1'CQC• PROJECT NAME:' S �,4ift?Q tt�i`} ' REPORT NO• 1 T -% ADDRESS,y:� s• Oic)00 CONTACT NAME: [: •• PO NO. K3 `?x�c�,, C E24 ZQ ;.' REPORTTO:1`i PHONEIFAX: (gt0)4N-Z9Ib Z . CQPYT0:.:•;2--1.:Mti iL S SarrpletiBy � .•:n. .ILI .:•�-.;:' C�•p�:q�W SAiMF l:E TYPE I = IMluent, E:= Ef(IW it, W = Well, ST = Stream, SO = Soi! ;SL = `Sludge, O&r: Collection: :: -` PRESERVATION _ t- .. Wy .: .zO ''•'�m yp Date Timie Tern J: :t . . REQUESTEDO ANAYSISAIl B (m_ • o xo. �4,O. _ ; O �4,r• ., V J..�•.', • O i =i. N 2 t ' �: �. z' _ _' a 4 sluff e SL ;c 13] ,/ --' x -QCa 1 ' :Co G G:=: _ - c 5 L P. 43.1)q l i d. S�N :� # y13 SL c G �' i 13RI C. P' G G :.: G .t P :} r' G ::h `4 C. � :•' No o�c +�o+3iaWK Z1C� ;. G.. -'^^� • M. ryifl{df• P. hMld.ilidBlGi�fli •..- .. ' 7ranahr' .t *:� .y 1. 11N� be dlCI7{Ofl{IKb l02 PPm, ).liill.iiwstts:ti�arca�f.cMioe. s•�':.+�es. for issOructioss. : Reli` uistiei! B DafialTime' �ad Da,om- e ;—'j T*aWmaWm when Received: Z3 :l �P�= jetted _ Dalivsr�d By: —�i CGY�r1Ar1�'• F% elired B s i�I y Date: .`i'1 t-i�i 14 Tiw.®• ANNUAL PATHOGEN AND VECTOR ATTRACTION R { DUCTION FORM (02T Bales) Facility Name: Coastal Farms and Residuals, LLC wQ permit Number- WQ0034806 WI'VTP Name! Town of Carolina Beach WWTP NPIDES Number: NCO023256 ------ Monitoring Period: From 1 /1 /2014 TO 12/31 /2014 Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternative pt l'1'avmed'. C.lass A.: Alt. Ei (Bane/temp) 0 Alt B (All; Treatment) Alt. C (Prior Testing) M A1t.D (114o Prior Test) Process to Further Reduce Pathogengs 0 rf annlioahlp fn enlf-prn anvil TZ0,1 i'ahrmpil dd'`lne% A nnIVA ieaalietate to-Furalter Reduce Patlaexiens": Compost at Drying ® - beat Treatment 13 Thermophilic El Beta Ray Gamma Ray ® Pasteurization 0 Class 9: JAlt_ (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens 0 If applit:blale to alternative peaforined (Class B onl3) indicate `T ocess to Ssgnifica fitly Reduce 1'uthogepp": Lime Stabilization ® Air Drying ® CoTj)osting CI jAcrobic Digestion 13 nae o c .D' a ti ti r bi i s o A � If nianlicalele to alternaf i er nerf'ormed (Class A or Class R) cesm nlete the folloWinE mordtorine data: Parameter Allowable Level Sludge Pathogen Density NUMber o Excc- donee Frequency of Analysis Sample Type Ana ytrca Tech- ni h- auc Minima Geo. Dean Vlaximn Units 2 x 10 to the 2 MPN 6111 power CFU Fecal Coliforrit per gram of total solids 1000 mpn per grata of total solid (dry. 3,602 90,777 415,585 id1PN/9 0 Annual Grab SM 9221C weight) Salmonella bacteria 3 MPN per 4 ,b77ratns (in lieu of fecal total solid (dry coliform) weight) ector Attraction Red®rction (1SA NCAC 02T .11I0 71- Pleaseitbdiente aide` not ve ne'rfiDrmeal: AltJ ( S reduction) " Alt. 2 (40-day bench) ® Alt. 3 (30-day bench) ® Alt. 4 (Spec. O, uptalcc) (� Alt., 5 (14-Day Aerobic), Alt. 6 (Alit. Stabilization ® Alt 7 (Drying - Stable) 0 JAIL 8 (Drying -Unstable) Alt. 9 (Injection) [3 Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed [� CERTIFICATION STATEI Il1'l' (pleases checic the appropriate statement) R1 "I certify, sander penalty of law, that the pathogen requirements in f Si) NCAC 02T .1106 and the vector attractiatr reduction requirement in 15A, NCAC 02T _1107 have been ineLl' El "I certify, under penalty of law, that the pathogen requirements in ISA. NCAC 02T .1106 and the vector attraction reduction requirement in ISA NCAC 027'.1107 have not been met." (Please mote if you check this statement attach an explanation why you have not abet cite or both of tiler requirements.) "This determination has been trade tinder my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I arts aware that there are significant pettalties f"or false certification including dart' -and imprisonment.', William J.Raymond, ORC Wesley Wooten, Manager Preparer Name and Title (type or print) Land Appli - Na ie • ,id T' e (if applicable)(type or print) i Ol -2 n •Z��.� 02� IS Signature repay _4 Date Sign4tuK. of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) l DENR FORM PVRF 02T (1212006) COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: July 28, 2014 MOTSU - North Wharf Permit No. NCO029122 2.39 % Solids 6.26 nH Parameter 1. % lMg/KgDryWeightl x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 0.667 6,670.000 13.34.0 Phosphorus 0.097 967.000 1.934 Potassium 0.099 992.000 1.984 PAN injected)* 0.211 2,114.200 4.228 PAN surface)* 0.205 2,049.200 4.098 Ammonia Nitrogen 0.013 130.000 0.260 Calcium 0.191 1,910.000 3.820 Calcium Carbonate E . --- --- --- Magnesium --- 849.000 1.698 Sodium --- 242.000 0.484 Sulfur --- --- Nitrate N / Nitrite N --- 22.200 0.044 Barium --- --- SAR Chloride --- --- 0.18 Iron --- --- --- Ceilin ' Concen. g Aluminum -- 13,100.00 26.200 (Mg/Kg) Arsenic --- 3.77 0.008 75 Cadmium --- 3.77 0.008 85 Chromium --- 20.300 0.041 --- Copper --- 23.90 0.048 4,300 Lead --- 13.20 0.026 840 Mercury --- 0.13 0.000 57 Molybdenum --- 3.77 0.008 75 Nickel --- 11.20 0.022 420 Selenium --- 3.77 0.008 100 Zinc - 53.60 0.107 7,500 Environmental Chemists # 2014-08955 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. COSTAL FARMS AND RESIDUALS, LLC WQ003480600.455 MOTSU . ............. .......... ............. .... ... ... ... . ::e ........ .. l: .. : ........................... . . . ..................... 07/28/14 662,651 5.8213 07/28/14 758,621 5.8800 07/28/14 160,772 5.2062 07/28/14 130,549 5.1158 07/28/14 281,691 5.4498 07/28/14 357,143 5.5528 07/28/14 412,699 5.6156 Total 1 38.6415 —] Average 1 5.5202 Geometric Mean Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen for Reduction requirement. 4 ' Environmental Chemists, Inc. envirochem6602 Windmill Way • Wilmington, NC 28405 -= (910)392-0223(Lab) • (910)392-4424(Fax) SM 710 Bowsertown Road a Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 -' CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Lewis Farms & Liquid Waste, INC. Date of Report: Aug 15, 2014 8155 Malpass Corner Road Customer PO #; Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2014-08955 Project ID: MOTSU-North Wharf Lagoon Lab ID Sample ID: 14-22162 Site: Sludge Test Collect DatelTime 7/28/2014 11:05 AM Method Matrix Sampled by Solid/Sludge Jay Baker Results Date Analyzed Sludge Residuals Aluminum EPA200.7 131.00 mg/kg 08/04/2014 Arsenic EPA200.7 <3.77 mglkg 07/31/2014 Cadmium EPA200.7 <3.77 mg/kg 07/31/2014 Calcium EPA200.7 1910.mg/kg 07/31/2014 Chromium EPA200.7 20.3 mg/kg 07/31/2014 Copper EPA2o0.7 23.9 mg/kg 07/31/2014 Lead EPA200.7 13.2 mg/kg 07/31/2014 Magnesium EPA200.7 849 mg/kg 07/31/2014 Molybdenum EPA 200.7 <3.77 mg/kg 08/05/2014 Nickel EPA200.7 11.2 mg/kg 07/31/2014 Potassium EPA200.7 992 mg/kg 07/31/2014 Selenium EPA200.7 <3.77 mg/kg 07/31/2014 Sodium EPA200.7 242 mg/kg 07/31/2014 Zinc EPA200.7 53.6 mg/kg 07/31/2014 Ammonia Nitrogen �l EPA350.1 130mg/kg 07/31/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 6670 mg/kg 08/07/2014 Nitrate+Nitrite-Nitrogen EPA353.2 22.2 mg/kg 08/01/2014 Total Solids (%) SM 2540 B 2.39 % 07/30/2014 pH SM4500 H 8 6.26 units 08/01/2014 - Total Phosphorus SM 4500 P F 967 mg/kg 08/07/2014 Mercury SW8467471B <0.126mg/kg 08/14/2014 Report #:: 2014-08955 Page 1 of 3 Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Lewis Farms & Liquid Waste, INC. Date of Report: Aug 15, 2014 8155 Malpass Corner Road Customer PO M t Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2014-08955 Project ID: MOTSU-North Wharf Lagoon LabID Sample ID: Collect Date/Time Matrix Sampled by 14-22163 Site: 1 7/28/2014 11:06 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Total Solids {%) SM 2540 8 3.32 % 07/30/2014 Fecal Density SM 9221C EMPN 24 hr 503 662651 MPN/g 07/29/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-22164 Site: 2 7/28/2014 11:06 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.45 % . 07/30/2014 Fecal Density SM92210EMPN 24hr503 758621 MPN/g 07/29/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14 22165 Site: 3 7/28/2614 11:07 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Total Solids (%) sM 2540 B 3.11 % 07/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 160772 MPN/g 07/29/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-22166 Site: 4 7/28/2014 11:07 AM Solid/Sludge Jay Baker t Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.83 % 07/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 130549 MPN/g 07/2912014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-22167 Site: 5 7/28/2014 11:07 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed r_ 1 Total Solids (%) SM 2540 B 2.84 % 07/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 281691 MPN/g 07/29/2014 Report #:: 2014-08955 f • 1 Page 2 of 3 _a F77Environmental Chemists, Inc. Lienvirochem 6602 WindmillWay • Wilmington, NC 28405 (910)392-0223(Lab) • (910) 392-4424 (Fax) SM 710 Bbwsertown ].load a Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE 494. DIS CERTIFICATE 437729 Lewis Farms & Liquid Waste, INC. Date of Report: Aug 15, 2014 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2014-08955 Project ID: MOTSU-North Wharf Lagoon Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-22168 Site: 6 7/28/2014 11:08 AM Solid/Sludge Jay Baker i Test Method Results Date Analyzed Total Solids (%) SM 2540 s 1.96 % 07/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 357143 MPN/g 07/29/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-22169 Site: 7 7/28/2014 11:08 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Total Solids (%) SM 2540 a 3.15 % 07/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 412699 MPN/g 07/29/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report #:: 2014-08955 Page 3 of 3 ..r Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLFCTION AND CHAIN OF rtISTC)DY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com CLIENT: f..r; J PROJECT NAME: 1*0>7-5q- 1JjtC 4jC..•X REPORT NO: iY- Pqs ADDRESS: CONTACT NAME: ++� PO NO: REPORT TO: Sl+ PHONEIFAX: COPY TO: sr : a. /Vf -457/� email: Samnled Bv: t/ ZZ SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludae. Other: Sample Identification Collection 4 d S y No .c E `o c ;, a (7 �o va c _o` �+ u E O W m g gz PRESERVATION ANALYSIS REQUESTED ate Time Temp i i s o = 0 = 0 z o w a ff f /a C P • ,� 114UXI C P / / f L K• C P b G G aa� C P G G Lug G G tNs} L�L� G G eJ Ly�l G G C P G G C P G G C P G G Transfer Relinquished By: Daterrime Received By: Date/Time 1. 2. e Temperature when Received:- 3 — Accepted: - Rejected: Resample Re a ed: Delivered By: r✓! Received By: Date: Time: Comments: TURNAROUND: Lb( AQ { ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) l r, 1 Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806 WWTP Name: MOTSU - ^ NPDES Number: NCO029122 Monitoring Period: From 1/l/2014 To 12/31/2014 Pathoeven Reduction (15A NCAC 02T .1106) - Please indicate level nehieverl and alternative nerfnrmoA- Class A: All. A (time/temp) 0 1 Alt B (Alk Treatment) [I Alt. C (Prior Testing) E3 A1t.D (No Prior Test) ES I I Process to Further Reduce Pathogengs 014 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 1I I Heat Drying 0 Heat Treatment ® Theiinophilic Beta Ray 01 Gamma Ray 0 Pasteurization Class B: I Alt. (1) Fecal Density R1 Alt. (2) Process to Significantly Reduce Pathogens El If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying 0 Composting Aerobic Digestion 0 Anaerobic Digestio n on If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er oFrequency Excee- dences of Analysis Sample Type Analytical Tech - ni ue , Minimum Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram oftotal solid (dry weight) 130,549 331,299 758,621 MPN/g 0 Annual Grab SM 9221 Salmonella'bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) Vector Attraction Keduction 05A NUAC 02T .1107) - Please indicate alternative performed:, Alt. ] (VS reduction) ® Alt. 2 (40-day bench) ® Alt. 3 (30-day bench) ® Alt. 4 (Spec. OZ uptake) El Alt. 5 (14-Day Aerobic) [3 Alt. 6 (Alk. Stabilization E3 jAlt 7 (Drying - Stable) ®Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ® Alt. 10 (Incorporation) R1 INo vector attraction reduction alternatives were performed E3 CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T..1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my ,direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information, used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Wesley Wooten, Manager Preparer N e and Ti lei print) o Land Applier Name and Title (if applicable)(type or print) Signature o reparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21'^".1102 (26) 1 DENR FORM PVRF 02T (12/2006) COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: February 27, 2014 North Topsail WWTF Permit No. W00005849 2.86 % Solids 7.03 nH Parameter % Mg/Kg Dry Weight % x 10,000) Pounds/Dry Ton M /K x 0.002 Nitrogen (TKN) 1.790 17,900.000 35.800 Phosphorus 1.450 14,500.000 29.000 Potassium 0.493 4,930.000 9.860 PAN (injected)* 0.552 5,524.260 11.049 PAN surface)* 0.548 5,475.360 10.951 Ammonia Nitrogen 0.010 97.800 0.196 Calcium 2.870 28,700.000 57.400 Calcium Carbonate E . --- --- --- Magnesium --- 3,060.000 6.120 Sodium --- 5,240.000 10.480 Sulfur --- ___ Nitrate N / Nitrite N --- 85.800 0.172 Barium --- --- SAR 1.33 Chloride --- --- Iron --- --- --- Ceiling Concen. ' (Mg/Kg) Aluminum --- 45,500.00 91.000 Arsenic --- 3.91 0.008 75 Cadmium --- 3.22 0.006 85 Chromium --- 26.700 --- --- Copper --- 248.00 0.496 4,300 Lead --- 7.41 0.015 840 Mercury --- 0.52 0.001 57 Molybdenum --- 3.22 0.006 75 Nickel --- 20.20 0.040 420 Selenium -- 4.65 0.009 100 Zinc =-- 3,100.00 6.200 7,500 Environment 1 # 2014-02332 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. r COASTAL FARMS AND RESIDUALS, LLC WQ0034806 North Topsail WWTF ........................... .. 02/27/14 29,963 4.4766 02/27/14 38,462 4.5850 02/27/14 176,679 5.2472 02/27/14 17,858 4.2518 02/27/14 38,063 4.5805 02/27/14 59,441 4.7741 02/27/14 107,914 5.0331 Total 1 32.9483 Average 4.7069 Geometric Mean € 3p€€'€€ Fecal Coliform MPN /gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. rop'". Environmental Chemists, Inc. -7- L —7 envirochem6602 Windmill Way • Wilmington, NC 28405 i (910)392-0223(Lab) (910)392-4424(Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Pluris LLC. (Utility Partners LLC.) Date of Report: Apr 09, 2014 P. O. Box 856 Customer PO #: t Sneads Ferry NC 28460 Report #: 2014-02332 Attention: Randy Hoffer Report to: Randy Hoffer Project ID: Sludge + i Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-05703 Site: Sludge 2/27/2014 11:40 AM Solid/Sludge Pete Peterson Test Method Results Date Analyzed Sludge Residuals ' Aluminum EPA200.7 45500 Mg/kg 03/13/2014 I Cadmium EPA200.7 <3.22 mg/kg 03/1012014 Calcium EPA200.7 28700 mg/kg 03/12/2014 Chromium EPA200.7 26.7 mg/kg 03/10/2014 Copper EPA200.7 248 mg/kg 03/10/2014 i Magnesium EPA200.7 3060 mg/kg 03/12/2014 Molybdenum EPA200.7 <3.22 mg/kg 03/10/2014 Nickel EPA200.7 20.2 mg/kg 03/10/2014 Potassium EPA200.7 4930mg/kg 03/12/2014 Selenium EPA200.7 4.65mg/kg 03/14/2014 Sodium EPA200.7 5240mg/kg 03/12-/2014 Zinc EPA 200.7 3100 mg/kg 03/12/2014 } Arsenic EPA200.8 3.91 mg/kg 3/17/2014 s1 Ammonia Nitrogen EPA 350.1 97.8 mg/kg 03/04/2014 Total Kjeldahl Nitrogen (TKN) EPA $51.2 17900 mg/kg 03/26/2014 I P i Nitrate+Nitrite-Nitrogen EPA 353.2 85.8 mg/kg 03/11/2014 Total Solids (%) sM 2540 B 2.86 % 02/28/2014 pH SM4500 H B 7.03 units 03/11/2014 Total Phosphorus SM450D P F 14500 mg/kg 04/03/2014 Mercury SWM7471B 0.5240 mg/kg 02/28/2014 5�' Lab ID Sample ID: Collect DatelTime Matrix Sampled by 14-05703A Site: Sludge 2/27/2014 11:40 AM Solid/Sludge Pete Peterson Test . Method Results Date Analyzed Lead EPA200.7 7.41 mg/kg 04/08/2014 Report #:: 2014-02332 Page 1 of 3 Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) - (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL &CONSULTING (252) 473-5702- CHEMISTS NCDENR- DWQ CERTIFICATE #94. DL5 CERTIFICATE #37729 Pluris LLC. (Utility Partners LLC.) Date of Report: Apr 09, 2014 P. O. Box 856 Customer PO #: Sneads Ferry NC 28460 Report#: 2014-02332 Attention: Randy Hoffer Report to: Randy Hoffer Project ID: Sludge Lab ID Sample ID: 1 Collect Date/Time Matrix Sampled by 14-05710 Site: 2/27/2014 11:40 AM Solid/Sludge Pete Peterson Test Method Results Date Analyzed Total Solids (%) SM 2540 6 2.67 % 02/28/2014 Fecal Density SM 9221C E MPN 24 hr503 29963 MPN/g 02/2812014 Lab 1D t ,._r Test Sample ID: 2 Collect Date/Time Matrix " Sampled by C*#_. --_. _ 7/77111A4A _.14.An A1111 Method Results Date Analyzed I Total Solids (%) SM2540 a 2.86 % 02/2-8/2014 Fecal Density SMD2210EMPN 24hr503 38462MPN/g 02/28/2014 Lab ID Sample 1D: 3 CollectDatelTime Matrix Sampled by 14-05712 Site: 2/27/2014 11:40 AM Solid/Sludge Pete Peterson Test Method Results Date Analyzed Total Solids {%) SM 2540 s 2.83 % 02/28/2014 Fecal Density SM 9221C E MPN 24 hr503 176679 MPN/g 02/28/2014 Lab ID Sample ID: 4 Collect Date/Time Matrix Sampled by 14-05713 Site: 2/27/2014 11:40 AM Solid/Sludge Pete Peterson } I Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.80 % 02/28/2014' Fecal Density SM 9221C E MPN 24 hr 503 17858 MPN/g 02/28/2014 Lab ID Sample ID: 5 Collect Date/Time Matrix Sampled by 14-05714 Site: 2/27/2014 .11:40 AM Solid/Sludge Pete Peterson Test Method � Results Date Analyzed S Total Solids % ( ) SM 2540 s o 2.89 /0 02/28/2014 Fecal Density SM 9221C E MPN 24 hr 503 38063 MPN/g 02/28/2014 i l Report #:: 2014-02332 I � 1 i � Page 2 of 3 f 1. T Environmental Chemists, Inc. envirochem 6602 WindmillWay. • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) sna 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 i Pluris LLC. (Utility Partners LLC.) Date of Report: Apr 09, 2014 P. O. Box 856 Customer PO #: i Sneads Ferry NC 28460 Report #: 2014-02332 Attention: Randy Hoffer Report to: Randy Hoffer Project ID: Sludge Lab ID Sample ID: 6- Collect Date/Time Matrix Sampled by 14-05715 Site: 2/27/2014 11:40 AM Solid/Sludge Pete Peterson Test Method Results Date Analyzed Total Solids (%) SM 2540 a 2.86 % 02/28/2014 Fecal Density SM 9221c a MPN 24 hr 503 59441 MPN/g 02/28/2014 Lab ID Sample ID: 7 Collect Date/Time Matrix Sampled by 14�15716 Siite: 21277-2-0a4- 11;40-AM-Solid/Sludge - Pete-Reterson- �I Test Method Results Date Analyzed a j Total Solids (%) SM 2540 s' 2.78 % 02/28/2014 Fecal Density SM 9221C E MPN 24 hr 503 107914 MPN/g 02/28/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: y Report #:: 2014-02332 Page 3 of 3 a I , Analytical & Consulting Chemists . ENVIRONMENTAL CHEMISTS, ING NCDENR: DWQ CERTERICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 6602 Windmill Way Wilmington, NU 204u0 OFFICE: 910-392-0223 FAX 910-392-4424 COLLECTION AND CHAIN OF CUSTODY CLIENTc_Pluris PROJECT NAME: —Groundwater Lowering REPORT NO: Ic ADDRESS: CONTACT NAME: C(� Get _PO NO: REPORT TO: PHONE/FAX: 71 COPY TO: E-MAIL: __a ••1 ...-uL.11 e7 - e#­ Cn = _qr%u 4;1 _ = studae. Other: Sample Identification Collection MM ANALYSIS REQUESTED Fwam bIVA Snow, monolog r L4 ArrAfAM 0 VAP IF, PASS 7AF O1111101111"T WAM W, 'A �sM w gm "AF �T��W WA 4� W ��� paterrime Temperat Delivered Comment 1 I ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806 WWTP Name: North Topsail WWTF NPDES Number: WQ0005849 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed: Class A: Alt A (time/temp) ❑ Alt B (Alk Treatment) ElAlt. C (Prior Testing) ❑ AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) Indicate "Process to Further Reduce Pathogens-: Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ra ❑ Gamma Pay ❑ Pasteurization ❑ Class B: JAIL (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com ostin g ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ - If applicable to alternative performed (Class A or Class B) complete the Ilowing monitoring data: Parameter Allowable Level in Sludge in Pathogen Density Number o Excee- deuces Frequency of Analysis y Sample Type a ytica Tech - ni ue Minimu Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 17,858 50,921 176,679 MPN/g 0 Annual Grab SM 9221 Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative Derformed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench). ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) (] No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) t] "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Randy Hoffer, ORC Wesley Wooten, Manager Preparer a and Title (type or print) Land Appli N e d T' le (if applicable)(type or print) 1 ao>s of 24 iS Signatur f Preparer* Date Signatu e o Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) DENR FORM PVRF 02T (12/2006) A, COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: June 2, 2014 Surf City WWTP 1.06 % Solids 7_nn nu Permit No. WQ0000795 Parameter % �Mg/KgDryWeightl % x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 2.630 26,300.000 52.600 Phosphorus 2.610 26,100.000 52.200 Potassium 0.585 5,850.000 11.700 PAN (injected)* 0.816 8,156.200 16.312 PAN surface)* 0.806 8,058.200 16.116 Ammonia Nitrogen 0.020 196.000 0.392 Calcium 5.390 53,900.000 107.800 Calcium Carbonate E . --- --- --- Magnesium --- 4,760.000 9.520 Sodium --- 13,400.000 26.800 Sulfur --- --- --- Nitrate N / Nitrite N --- 129.000 0.258 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 4,010.00 8.020 Arsenic --- 11.90 0.024 Cadmium --- 9.34 0.019 Chromium - 26.800 0.054 Copper --- 736.00 1.472 Lead --- 24.20 0.048 Mercury --- 0.57 0.001 Molybdenum --- 9.34 0.019 Nickel --- 21.50 0.043 Selenium --- 9.34 0.019 Zinc --- 2,110.00 4.220 Environmental Chemists # 2014-06321 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Surf City WWTP D.ca'1'01 a >1'`>< 06/02/14 53,847 4.7312 06/02/14 16,912 4.2282 06/02/14 99,237 4.9967 06/02/14 60,607 4.7825 06/02/14 53,031 4.7245 06/02/14 77,465 4.8891 06/02/14 112,583 5.0515 Total 33.4037 Average 4.7720 Geometric Mean Fecal Coliform NON / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. 1 Environmental Chemists, Inc. __ t 6602 Windmill Way a Wilmington, NC 28405 (910) 392-0223 (Lab) - (910) 392-4424 (Fax) sM 710 Bowsertown Road - Manteo, NC 27954 - (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENF- DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 i' - Town of Surf City Date of Report: Jul 15, 201'4 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Steve Smith Report #: 2014-06321 —� Project ID: Sludge f Lab ID Sample ID: Surf City Collect DatelTime Matrix Sampled by 14-15266 Site: Sludge 6/2/2014 11:30 AM Solid/Sludge Client . ' k Test Method' Results Date Analyzed Chlordane SW 846 Method 8081B/3510 <0.005 mg/L 06/05/2014 Endrin SW 846 Method 8081 B/3510 <0.00005 mg/L 06/05/2014 r Heptachlor SW 846 Method Sol B13510 <0.00005. mg/L 06/05/2014 Heptachlor epoxide SW 846 Method 8081 EM510 <0.00005 mg/L 06/05/2014 Lindane SW 846 Method 8081 B13s10 <0.00005 mg/L 06/05/2014 Methoxychlor SW 846 Method 8081 B13510 <0.00005 mg/L 06/05/2014 Toxaphene SW 846 Method 8081 B/3510 <0.005 mg/L 06/05/2014 1,4-Dichlorobenzene(TCLP) SW848 method 8270/3610 <0.05mg/L 06/04/2014 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 Cresol (TCLP) SW 846 method 8270/3510 <0:05 mg/L 66/04/2014 Hexachloro-1,3-butadiene(TCLP) SW 846 method 8270/3510 <0.05mg/L 06/04/2014 _ Hexachlorobenzene (TCLP) SW 846 method.8270/3610 <0.05 mg1L 06/04/2014 Hexachloroethane (TCLP) SW 846 method 827013510 <0.05 mg1L 06/04/2014 m + p-Cresol (TCLP) SW 846 method B270MIO <0.05 mg/L 05/04/2014 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06104/2014 o-Cresol (TCLP) SW 846 method 827013510 <0.05 mg/L 06/04/2014 - Pentachlorophenol (TCLP) SW 846 method 827013510 <0.25 mg/L 06/04/2014 Pyridine (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 i 2,4,5-TP sw84s Method s151A <0.0003 mg/L 06/09/2014 2,4-D SW846 Method 8151A <0.0003 mg/L 0610912014 1,1-Dichloroethylene SW846 Method 8260/5030 _ < 0.01 mg/L 06/20/2014 1;2-Dichloroethane SW846 Method 826015030 <0.01 mg/L 06/20/2014 Benzene SW846 Method 8260/5030 <0.01 mg/L 06/20/2014 Carbon Tetrachloride SW846 Method 8260/5030 <0.01 mg/L 06/20/2014 Report #.: 2014-06321 Page 1 of 4 -� Environmental Chemists, Inc. �- 6602 Windmill Way c Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road a Manteo, NC 27954 (252) 473-5702 - ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERT1RCATE #94. DLS CERTIFICATE #37729 ti - Town of Surf City Date -of Report: Jul 15, 2014 Post Office Box 2476 Customer PO #. Surf City NC 28445 Customer ID: 08110024 Attention: Steve Smith Report #: 2014-06321 Project ID: Sludge I ~ _ Chlorobenzene SW846 Method 8280/5030 <0.01 mg/L 06/20/2014 e= Chloroform SW846 Method 8260/5030 <0.01 mg/L 06/20/2014 Methyl ethyl ketone SW846 Method 826015030 <0.05 mg/L 06/20/2014 Tetrach loroethylene SW846 Method 8260/6030 <0.01 mg/L 06/20/2014 Trichloroethylene SW846 Method 8260/5030 <0.01 mg/L 06/20/2014 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 06120/2014 RCI Cyanide EPA 335A <0.120 mg/kg 06/04/2014 Sulfide SM 4500 S D <0.239 mg/kg 06/04/2014 r; Ignitability SW 846 method 1010 >212 OF 06/06/2014 Sludge Residuals Aluminum EPA200.7 4010mg/kg 0611612014 - Arsenic EPA200.7 11.9mg/kg 06/12/2014 t Cadmium EPA200.7 <9.34mg/kg 06/12/2014 Calcium EPA200.7 53900mg/kg 06/17/2014 Chromium EPA200.7 26.8mg/kg 06/12/2014 Copper EPA 200.7 736 mg/kg 06/12/2014 Lead EPA200.7 24.2 mg/kg 06112/2014 Magnesium EPA200.7 4760 mg/kg 06/17/2014 Molybdenum EPA 200.7 <9.34 mg/kg 06/12/2014 Nickel EPA200.7 21.5mg/kg 06/12/2014 Potassium EPA200.7 5850 mg/kg 06/17/2014 Selenium EPA200.7 <9.34 mg/kg 06/12/2014 Sodium EPA200.7 13400 mg/kg 06/17/2014 Zinc EPA200.7 2110 mg/kg 06/12/2014 Ammonia Nitrogen EPA350.1 <196mg/kg 06/05/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 26300mg/kg 06/09/2014 Nitrate+Nitrite-Nitrogen EPA353.2 129 mg/kg 06/24/2014 Total Solids (%) sM 2640 B 1.06 % 06/03/2014 i Report #:: 2014-08321 Page 2 of 4 Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town of Surf City Date of Report: Jul 15, 2014 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Steve Smith Report #: 2014-06321 Project ID: Sludge pH SM 4500 H B 7.00 units 06/05/2014 - Total Phosphorus SM 4500 P F 26100 mg/kg 06/09/2014 Mercury SWM7471a 0.5660 mg/kg 06/09/2014 TCLP Metals Arsenic EPA200.7 <0.100mg/L 06/06/2014 Barium EPA200.7 <0.100mg/L 06/06/2014 Cadmium EPA200.7 <0.100 mg/L 06/06/2014 _ Chromium EPA200.7 <0.100mg/L 06/06/2014 Lead EPA200.7 <0.100mg/L d6/06/2014 Selenium EPA200.7 <0.100mg/L 06/06/2014 Silver EPA200.7 <0.100 mg/L 06/06/2014 t Mercury EPA245.1 <0.002mg/L 06/17/2014 Lab ID Sample ID: Surf City Collect DatelTime Matrix Sampled by 14-15267 Site: # 1 6/2/2014 11:30 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 a 1.30 % 06/03/2014 Fecal Density SM 9221 C E MPN 24 hr 503 53847 M PN/g 06/03/2014 Lab ID Sample ID: Surf City Collect DatelTime Matrix Sampled by 14-16268 Site: # 2 6/2/2014 11:30 AM Solid/Sludge Client T- Test Method Results Date Analyzed Total Solids (%) SM 2540 s 1.36 % 06/03/2014 Fecal Density SM 9221C E MPN 24 hr503 16912 MPN/g 06/03/2014 Lab ID Sample ID: Surf City Collect Date/Time Matrix Sampled by 14-15269 Site: # 3 6/2/2014 11:30 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 a 1.31 % 06/03/2014 sFecal Density SM 9221C E MPN 24 hr603 99237 MPN/g 06/03/2014 r Report #:: 2014-06321 Page 3 of 4 11__i 7 Environmental Chemists, Inc. envirochem(910) 6602 WindmillWay • WlnUngton, NC 28405 392-0223 (Lab) • (910) 392-4424 (Fax) sn+ 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE 4194. DLS CERTIFICATE #37729 Town of Surf City Date of Report: Jul 15, 2014 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Steve Smith Report #: 2014-06321 Project ID: Sludge Lab ID Sample ID: Surf City Collect Date/Time Matrix Sampled by 14-15270 Site: # 4 6/2/2014 11:30 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.32 % 06/03/2014 Fecal Density SM 9221C E MPN 24 hr 503 60607 MPN/g 06/03/2014 Lab ID Sample ID: Surf City Collect Date/Time Matrix Sampled by 14-15271 Site: # 5 6/212014 11:30 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.32 % 06/03/2014 Fecal Density SM92210EMPN 24hr503 53031 MPN/g 06/03/2014 Lab ID Sample ID: Surf City Collect Date/Time Matrix Sampled by 14-15272 Site: # 6 6/2/2014 11:30 AM Solid/Sludge Client Test Method Results Date Analyzed .a Total Solids (%) SM 2540 B 1.42 % 06/03/2014 Fecal Density SM 9221C E MPN 24 hr 503 77465 MPN/g 06/03/2014 Lab ID Sample ID: Surf city Collect Date/Time Matrix Sampled by 14-15273 Site: # 7 6/2/2014 11:30 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 a 1.51 % 06/03/2014 Fecal Density SM 9221C E MPN 24 hr 503 112583 MPN/g 06/03/2014 Comment: Sludge residuals, except H, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: / r Report#:: 2014.05321 Page 4 of4 _-ENARONMEN SAL—C.HEM1STSjNC—..- _ 5602-Windmill-Way Wilmington, N'C28405 y NCDENR: DWQ CERTERICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 OFFICE: 910-392-0223 FAX 910-392-4424 Angly0C9i $, Copsuillng Chemists 1PWFNT- Town of 61prf c" yylryTP PROJECT NAME: Influent Sampling REPORT NO: 1 �" (12e3A ANKH, CONTACTNAME: E: PO NO: REPORT TO: PHONEIFAX: COPY TO: E-MAIL: Samoled Bv: SAMPLE TYPE: 1= Influent. E = Effluent. W = Well. ST = Stream_ SO = Seii_ SL = Sludna_ Other: _.._. @mgie cat on _...., ........Collection o E `o fl o` = E " z PRESERVATION ' ANALYSIS REQUESTED Date Date Time Time emis Tem $ is g _ o c C P XSOD, US, NW -ate G G C P I X G G C P G G ' C P G G cep w M4 R,,I,�� G P l5 7xeC wL . eWIAarA, C P p -G C P _ G G G P 4 1p Yo G G C P G G C P G G NOTIM - DECH1.011INATION: SampNs TorAmmonla, TKN. Cyanld% Phenol and Bacteria must be d chlerinated (02 ppm or less) In the field at the time 9f collection. See ravers- for Instructions Thaofer Relinquished By: Datemme AA to 90ce)ved By: Date/Time ■ ■+nP*r7rsar R lIr r ` �AYYO+J&OY._ X _ 1 Bjeuxe K@Sample K@ U@ ted: 9ellvered By, a `y_'�Jfj'� Received By. L-{!' Date: FQllllil@n V TUR AR UN. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W000034806 WBVTP Name: Town of Surf City WWTP NPDES Number: W00000795 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .110Q - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ AIt.D (No Prior Test) Process to Further Reduce Pathogen as ❑ :ff V.. If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ r, Beta Ray ❑ Gamma Ray ❑ Pasteurization - ❑ Class B: Alt- (1) Fecal Density ® Alt. (2)Process to Significantly Reduce Pathogens❑ -- .a'r,� i. If applicable to alternative performed Class B only indicate "Process to Signiflcantly Reduce Pathogens": Lime Stabilization ❑ Air ❑ composting ❑ Aerobic Digestion [3Anaerobic Digestion [3_ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um r ° Excee Frequency of Analysis Sample Typenioue AnalYu Tech - Minimum inimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 16,912 59,150 112,583 MPN/g 0 Annual Grab SM 9221 C Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 co oration) ® No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Smith, ORC Wesley Wooten, Manager Preparer Name and Title (type or print) Land Appl' r e d T' a (if applicable (type or print) /S Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) 2014 APPLICATION SUMMARY COASTAL FARMS AND RESIDUALS, LLC Permit # WQ 0034606 2014 RESIDUALS APPLICATIONS APPLICATION. SUMMARY .......... AN AL W E-T.: T. T*� . . .. N ky ..... ..... ..... ........ . ....... ... FAN...... Wilber Corbett 1 93.40 1,901,234 226.650 28.89 25.12 Totals jig Metric Tons 205.57 FIELD LOADING RATE REPORTS ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Dame: Coastal Farms and Residuals WQ Permit# WQ0034806 Field N WC-1 Acres Utilized: 93.4 Land Owner: Wilber Corbett Annual DT's Applied: 226.65 - Site 4: Corbett Shop Acres Permitted; 93.4 Operator: Allen Predominant Soil Series: Au ille - AuB Cation Exchange Capacity (non 503): 41 Crop 1 Name: Bermuda Crop 1 Max. PAN: 196 Crop 2 Naine: 2yagrass Crop 2 Max. PAN: SO Application Method: S - Surface 'Volatilization Rate: Carolina Beach, MOTSU North Topsail, & Surf cit y (Incorporated -1.0) . KJJA.FV Y 2014 2014 2014 2014 •. %.:"3 1,113,750 9,984 222,000 555,500 .£' 11,925 107 2,377 5,948 . > 3.76 2.39 2.96 1.06 < ^ . 1.87 0.01 0.29 0.26 E; zP. '..' M.. Cato ;M. U Will op �c�'a' . •y�N�.�q� ff O/D 0.008 0.000 0.002 0.006 �t.:... 0.008 3.223 0.000 0.001 0.002 0.141 0.005 0.387 0.105 0.000 0.004 0.013 F! 0.002 0.000 0.000 0.000 •.i-1:2. r..... 20.70 0.59 3.93 26.51 0.02 8.22 13.72 V 1.91 0.00 0.008 0.000 0.002 0.005 0.055 0.000 0.011 0.011 0.018 0.000 0.003 0.005 3.739 0.001 1,759 1.109 24.84 0.05 2.54 1.46 Bamude . Bennuda Bermuda "Br>nfuda R or13-27 Rye gye .. 13. . 0.05 0.07 Total 1,901,234 Annual Ibafacre C'unent Cumulative Ibdacre PrlorYears Cumulative Midas PermittC.P.L10*6 0.016 0.014 3.751 0.123 0.002 0.014 0.078 0.026 6.607 28.89 25.12 1 48.48 Lime AVID. 0.08 0,08 5.46 0.21 0.00 0.08 0.16 0.09 11.06 196 50 Permit PAN Lilt lst/2ad Crot Date Lbs/A c. 0.06 0.06 L71 0.08 0.00 0.06 0.08 1 0.06 4.45 36 34 1,338 267 IS n/a 374 1 89 1 2,498 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalti fo b ' ng false information, Including the possibility of fines and imprisonment for knowing violations., X 2 r?- ^/ - !Application Method: S - Surface. IN - Injection. INC - Incorporation (Signature of Land Applier) Date "Volatilization Rate' Surf 0 5 I Surface . , .Jectaoa/Inwrporation- 1.0 ••'C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes application that was Injected SBME, Inc. DENR FORM FSF(12/2006) Mod. FIELD APPLICATION SUMMARIES Coastal Farms and Residuals, LLC Permit # WQ0034806 2014 Field Application Summary SOURCE: Town of Carolina Beach WWTP FIELD NO. AW-1 AVV-2 AW-3 AW4 JB-1 JB-2 CPC-1 CPC-2 CB-1 CFC-1 CFC-2 AS-1 WC-1 NET ACRES 13.90 21.50 16.90 5.90 28.90 59.30 71.80 55.40 11.80 81.90 72.80 70.20 93.40 SITE, Wooten Wooten Wooten Wooten Rnrnc Rnms ('.nrhett Panlcina' Cnrhett P-1rina Cnrhrtt Rroth— Cnrhett v—;na rnrhett P—ina RA--, W ('. A—ff January ............................... February March April i May June .......... 384,750 t............July �. 222;750 August . ............................... September ............................... October November ............................... 202,500 December 303,750 Total - - - - - - - - - - - 1,113,750 Soybeans Com Wheat Rye Bermuda ------------- SOURCE: MOTSU FIELD NO. AW-i AW-2 AW-3 AW4 NET ACRES 13.90 .21.50 16.90 5.90 SITE Wooten Wooten Wooten Wooten Coastal Farms and Residuals, LLC Permit # WQ0034806 2014 Field Application Summary JB-1 JB-2 CPC-1 CPC-2 CB-1 CFC-1 CFC-2 AS-1 WC-1 28.90 59.30 71.80 55.40 11.80 81.90 72.80 70.20 93.40 Roma Rnmc r —hatt Pa Arina c:,tt...., nr n,._t..... January 1 ............................... o February March ............................ April .............................. May June July August ................................. September ............................... October p ............................... 9,984 November December Total 9,984 Soybeans Corn Wheat Rye Bermuda ------------- SOURCE: North Topsail WWTF FIELD NO. AW-1 AW-2 AW-3 AW4 JB-1 NET ACRES 13.90 21.50 16.90 5.90 28.90 STTR Wooten Wooten Wooten Wooten Bums Coastal Farms and Residuals, LLC Permit # WQ0034806 2014 Field Application Summary JB-2 CPC-1 CPC-2 CB-1 CFC-1 CFC-2 AS-1 WC-1 59.30 71.80 55.40 11.80 81.90 72.80 70.20 93.40 Bums CorbettPacking Corbett Packing CorbettBrothers CnrbettFarming Corbett Farming Sidhury W Corbett January ............................... February 18,000 ........................... March 30,000 April 18,000 ........................... May 36,000 ........... June ........................... July 36,000 .......... 1 August 36,000 ................................ September ............................... October 24,000 November 24,000 ........................... December Total 222,000 Soybeans Corn Wheat Rye Bermuda ------------- ------------- SOURCE: Surf City FIELD NO. AW-1 AW-2 AW-3 AW4 NET ACRES 13.90 21.50 16.90 5.90 SITE Wooten Wooten Wooten Wooten Coastal Farms and Residuals, LLC Permit # WQ0034806 2014 Field Application Summary JB-1 JB-2 CPC-1 CPC-2 CB-1 CFC-1 CFC-2 28.90 59.30 71.80 55.40 11.80 81.90 72.80 Bums Bums Corbett Packing Corbett Packing Corbett Brothers Corbett Farming Corbett Farming AS-1 70.20 Sidbury WC-1 93.40 W. Corbett January 151,000 February March t.........-April . May June - ............................ July.... �...... August September 188,500 ............................... October ............................... November December 216,000 Total - - - - - - - - - - - - 555,500 Soybeans Corn Wheat Rye Bermuda SOIL ANALYSIS REPORTS Page 1 of 1 Report Number: 15-027-0509 Account Number:45819 Send To: S&ME (1588) MARTIN MABE 3718 OLD BATTLEGROUND RD GREENSBORO NC 27410-2314 �L WWW.aleaderd C0111 Date Received: 01/27/2015 Date Of Analysis: 01/28/2015 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Grower: Submitted By: MARTIN MABE COASTAL FARMS Farm ID: JOB#1588-09-054 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 01/28/2015 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number ENR % Rate Mehlich 3 Reserve K Mg Ca Na Soil Buffer H lbs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meq/100g meq/100g AS-1 46 M 110 H 52 M 263 L 16 VL 11664 3.5 M 114 4.7 6.72 2.1 4.2 NC=38 NC=56 WC-1 1 VH 64 L M M L 11665 2.2 L 89 181 1 1 156 1464 122 1 5.9 6.87 0.6 3.7 NC=676 NC=33 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl Al 0/6 % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm AS-1 32 H 2.4 M 2 VL 330 VH 0.9 M 0.7 M 6.7 10.3 31.3 1.7 50.0 NC=67 INC=60.0 NC=13 I I NC=45.0 WC-1 H VH 19 M VH VH L 4.4 12.6 62.7 2.6 17.0 127 123.9 1391 116.2 10.4 NC=56 NC=597.5 1 NC=119 NC=810.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: P` H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Paudc McGroary It should be noted that the majority of residuals land applied under NCDENR Permit No. WQ0034806 achieve pathogen reduction and vector attraction reduction requirements through alkaline stabilization. Therefore, the material being land applied is adding lime through most of the land application events. It should also be noted that the Wilber Corbett — Field 1 has a predominant soil series of Autryville loamy sand that is strongly acid by nature. Achieving a pH of 6.0 on this site by the addition of liming material is nearly impossible due to the predominant soil series and the leaching of the liming material through the loamy sand material throughout the soil profile. The pH of 5.9 on Wilber Corbett's — Field 1 (WC-1) is well suited for the growth of the common bermuda hay crop overseeded with ryegrass. au--2�L 4.4-4 Martin Mabe Agronomist/Project Manager