HomeMy WebLinkAboutWQ0034806_Residual Annual Report 2014_20150204RECRVED
2014 ANNUAL REP6k*u 4 2015
LAND APPLICATION PRQyN
COASTAL FARMS AND ANNOWXINNIT
PERMIT OWQ0034806
Prepared For:
Coastal Farms and Residuals, LLC
8155 Malpass Corner Road
Currie, North Carolina 28435
Compiled By:
S&ME, Inc.
8646 West Market Street, Suite 105
Greensboro, North Carolina 27409
February 2015
February 2, 2015 I
I
NCDENR-DWQ
512 North Salisbury Street
Raleigh, North Carolina 27604
Attention: Information Processing Unit
Reference: 2014 LAND APPLICATION ANNUAL REPORT
Coastal Farms and Residuals, LLC
Permit No. WQ0034806
S&ME, Inc. Project No. 1588-09-034
1 Non -Discharge Compliance Unit:
S&ME, Inc. (S&ME) is submitting all monitoring and reporting requirements as specified in
' the above referenced permit on behalf of Coastal Farms and Residuals, LLC. S&ME
compiled this report using data gathered during the compliance year by Coastal Farms and
r Residuals, LLC. This data includes: 1) certification form, 2) residuals analyses and pathogen /
5 vector data, 3) application summaries and field loading rate reports, 4) soil analyses.
If there is any further information required or questions regarding this annual report please do
not hesitate to contact Coastal Farms and Residuals, LLC or S&ME for further assistance.
Sincerely,
S&ME, Inc.
Martin Mabe �obWillcox, L.S.S.
a NC Land Application/Residuals Operator Natural Resources Services Leader
#22753
Enclosures
T:\Projects\2009\ENV\1588-09-034 Coastal Residuals\2014 Annual Report\2014 ANNUAL REPORT.doc
S&ME, INC. / 8646 W. Market Street, Suite 105 / Greensboro, NC 27409 / p 336.288.7180 f 336.288.8980 / www.smeinc.com
TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Form
H Residuals Analyses & Pathogen / Vector Attraction Data
III 2014 Application Summary and Field Loading Rate Reports
IV Soil Analysis
CERTIFICATION FORM
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0034806 County: Pender Year: 2014
Facility Name (as shown on permit): Coastal Farms and Residuals, LLC
Land Application Operator: Mr. Wesley Wooten Phone: 910-283-5444
Land application of residuals as allowed by the permit occurred during the past calendar year?
! ► Yes No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach.an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
13
Total number of fields utilized for land, application during the year:
1
Total amount of dry tons applied during the year for all application sites:
226.65
Total number of acres utilized' for land application during the year:
93.4
Part B - Annual Comoiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. vi Yes =J No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least
6.0 or the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and,three (3)
copies of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are
5) All other monitoring was performed in accordance with the permit and reported during the year as required and
three (3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T . I I05(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40
CFR Part 503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .11 l 1 were complied with (applicable to 40 CFR
Part 503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations
are attached to include appropriate actions and remediations.
1 I) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified' in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing viola _ons
Mr. Wesley W000ten, President
Permittee Name and Title (type or print) Signature of Permittee Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
RESIDUAL ANALYSES
TCLP ANALYSES IF REQUIRED
AND PATHOGEN AND VECTOR ATTRACTION REDUCTION
Ll
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach ft fwm to tha corteapandirg hrboretmy enalyds.
Pkeae now that your permit may contain additional pammetera to ba snaWed then (ham required to be su nnuffued on this form.
Permit Number Effii;�:
Facility Name siduals Laboratory ironmenta�Inq-
t3
NPDES 9 ,WWTP Name
2014 DATA
Arseft
- 2.05
Cadmium
2.05
Comr
882 00
Lead
Mercury
2820
OAS
Mc um
NidW
2.05
14.80
Selemlum
4.92
23nc
TKN
Ammonla•N an
1 000. 00
30 700.00
3 550.00
Ntb WN
4115.00
Total Phosohorus
7 o9o.o0
x 2 _2 S^
(SIGNATU OF PREPARER) DATE
I certify, and r penally of law, that this document was prepared under my direction or supervision In accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations.
COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: May 6, 2014
Carolina Beach WWTP Permit No. NCO023256
3.76 % Solids
6.8 nH
Parameter
I %
JMg/KgDrXWeighf
x 10,000)
Pounds/Dry Ton
(Mg/Kg (Mg/Kgx 0.002
Nitrogen (TKN)
3.070
30,700.000
61.400
Phosphorus
0.709
7,090.000
14.180
Potassium
0.219
2,190.000
4.380
PAN (injected)*
1.218
12,180.000
24.360
PAN surface)*
1.041
10,405.000
20.810
Ammonia Nitrogen
0.355
3,550.000
7.100
Calcium
3.620
36,200.000
72.400
Calcium Carbonate E .
---
---
---
Magnesium
---
4,630.000
9.260
Sodium
---
4,760.000
9.520
Sulfur
---
---
---
Nitrate N / Nitrite N
---
485.000
0.970
Barium
---
---
---
SAR
1.21
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
/K
Aluminum
---
4,390.00
8.780
Arsenic
---
2.05
0.004
75
Cadmium
---
2.05
0.004
85
Chromium
---
18.800
0.038
---
Copper
---
862.00
1.724
4,300
Lead
---
28.20
0.056
840
Mercury
---
0.48
0.001
57
Molybdenum
---
2.05
0.004
75
Nickel
---
14.80
0.030
420
Selenium
--
4.92
0.010
100
Zinc
---
1,000.00
2.000
7,500
Environmental Chemists # 2014-05216
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
' (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 28405
(910) 392-0223 (Lab) • (910) 392-4424 (Fax)
$M
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL & CONSULTING (252)473-5702
CHEMISTS NCDENR.- DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Town of Carolina Beach Date of Report: Jun 19, 2014
1121 North Lake Park Blvd Customer PO M
Carolina Beach NC 28428 Customer ID: 08100295
Attention: Bill Raymond Report M 2014-05216
Project ID: Wastewater
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-12545 Site: SSB#2 6/6/2014 10:03 AM SolidlSludge Bill Raymond
Test Method Results Date Analyzed
Chlordane
SW846 Method 8081B/3510
<0.005 mg/L
05/16/2014
Endrin
SW 846 Method 8081 B/3510
<0.00005 mg/L
05/16/2014
Heptachlor
SW 846 Method 8081 B1351 0
<0.00005 mg/L
05/16/2014
Heptachlor epoxide
SW 846 Method 8081B/3510
<0.00005 mg/L
05/16/2014
Lindane
SW 846 Method 8081B/3510
<0.00005 mg/L
05/16/2014
Methoxychlor
SW 846 Method 80818/3510
<0.00005 mg/L
05/16/2014
Toxaphene
SW 846 Method 8081 B1351 0
<0.005 mg/L
05/16/2014
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/16/2014
2,4,5-Trichlorophenol(TCLP)
SW 846 method8270MIO
<0.050 mg/L
05/15/2014
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/15/2014
2,4-Dinitrotoluene (TCLP)
SW 846 method 827013510
<0.050 mg/L
05/15/2014
Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
05/15/2014
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270=10
<0.050 mg/L
05/16/2014
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050. mg/L
05/15/2014
Hexachloroethane (TCLP)
SW846 method 827013510
<0.050 mg/L
05115/2014
m + p- Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05115/2014
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/15/2014
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/15/2014
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/15/2014
Pyridine (TCLP)
SW846 method 827013510
<0.050 mg/L
05/15/2014
2,4,5-TP
SW646 Method 8151A
<0.0003 mg/L----
-05/1912014 - -
2,4-D
SW846 Method 8151A
<0.0003 mg/L
05/19/2014
1,1-Dichloroethylene
SW846Method 8260/5030
<0.01 mg/L
05/16/2014
1,2-Dichloroethane
SW846 Method 826015030
<0.01 mg/L
05/16/2014
Benzene
SW846 Method 826015030
<0.01 mg/L
05/16/2014
Carbon Tetrachloride
SW846 Method 8260/6030
<0.01 mg/L
05/16/2014
Report #:: 2014-05216
Page 1 of 3
I
I
Environmental Chemists, Inc.
env
6602 Windmill Way •Wilmington, NC 28405
(910) 392-0223 (Lab) • (910) 392-4424 (Fax)
®
710 Bowsertown Road • Manteo, NC 27954
(252) 473-5702
- ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Town of Carolina Beach
Date of Report: Jun 19, 2014
1121 North Lake Park Blvd
Customer PO #:
Carolina Beach NC 28428
Customer ID: 08100295
Attention: Bill Raymond
Report #: 2014-05216
Project ID: Wastewater
Chlorobenzene
SW846 Method 8260/6030
<0.01 mg/L
06/16/2014
Chloroform
SW846 Method 8260/5030
<0.01 mg/L
06/16/2014
Methyl ethyl ketone
SW846 Method 826015030
<0.05 mg/L
06/16/2014
Tetrachloroethylene
SW846 Method 8260/5030
<0.01 mg/L
05/16/2014
Trichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
05/1612014
Vinyl Chloride
SW846 Method 8260/5030
<0.01 mg/L
05/16/2014
RCI
Cyanide
EPA 335.4
<0.124 mg/kg
05/20/2014
pH
SM 4500 H B
6.80 units
05/15/2014
Sulfide
SM 4500 S o
<0.249 mg/kg
05/20/2014
lgnitability
SW 846 method 1010
>212 °F
05/08/2014
Sludge Residuals
Aluminum
EPA200.7
4390 mg/kg
05/16/2014
Arsenic
EPA200.7
<2.05mg/kg
05113/2014
Cadmium
EPA200.7
<2.05mg/kg
05/13/2014
Calcium
EPA200.7
36200mg/kg
05/14/2014
Chromium
EPA200.7
18.8 mg/kg
06/13/2014
Copper
EPA 200.7
862 mg/kg
05/13/2014
Lead
EPA200.7
28.2 mg/kg
05/13/2014
Magnesium
EPA200.7
4630mg/kg
05/14/2014
Molybdenum
EPA200.7
<2.05mg/kg
05/13/2014
Nickel
EPA200.7
14.8mg/kg
06/13/2014
Potassium
EPA200.7
2190 mg/kg
05/14/2014
Selenium
EPA200.7
4.92mg/kg
05/13/2014
Sodium
EPA200.7
4760mg/kg
05/14/2014
Zinc
EPA200.7
1000mg/kg
05/13/2014
Ammonia Nitrogen
EPA350.1
3550mg/kg
05/12/2014
Total Kjeldahl Nitrogen (TKN)
EPA351.2
30700mg/kg
05/14/2014
Nitrate+Nitrite-Nitrogen
EPA353.2
485mg/kg
05/14/2014
Report#r 2014-05216
Page 2 of 3
Environmental Chemists, Inc.
7envirochem 6602 Windmill Way - Wilmington, NC 28405
(910) 392-0223 (Lab) • (910) 392-4424 (Fax)
SM
710 Bowsertown Road • Manteo, NC 27954
(252) 473-5702
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DI.S CERTIFICATE #37729
Town of Carolina Beach
1121 North Lake Park Blvd
Carolina Beach NC 28428
Attention: Bill Raymond
Date of Report: Jun 19, 2014
Customer PO #:
Customer ID: 08100295
Report #: 2014-05216
Project ID: Wastewater -
Total Solids (%) SM2540 B
3.76 %
05/07/2014
Total Phosphorus SM 4500 P F
7090 mg/kg
05/21 /2014
Mercury SWW7471B
0.4840mg/kg
06/07/2014
TCLP Metals
Arsenic EPA 200.7
<0.100mg/L
05/15/2014
Barium EPA 200.7
<0.100 mg/L
05/15/2014
Cadmium EPA 200.7
<0.100 mg/L
05/15/2014
Chromium EPA 200.7
<0.100mg/L
05/15/2014
Lead EPA 200.7
<0.100 mg/L
05/15/2014
Selenium EPA 200.7
<0.100mg/L
05/15/2014
Silver EPA200.7
<0.100mg/L
05/15/2014
Mercury EPA245.1
<0.0020mg/L
05/14/2014
Comment: Sludge residual results reported on a dry weight basis.
Reviewed by:
Report*: 2014-05216 Page 3 of 3
Anaiytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLI=CTION AND CHAIN OP CUSTODY .
6692 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX 910-392-4424
Info@environmentalchemists.com
CLIENT: (TttT1.1 O
WU j"ZOC
PROJECT NAME: V)OG�t G`!�1 t`•M
t'.11;
REPORT NO:
ADDRESS:
O S •�
CONTACT NAME:
,% C f�nc
PO NO: -7 Z 7
VOLMUM-ReCICL, NC 1. 20
REPORT TO: IiG&CdI.Cr C UVAV�ek.O M
PRONE/PAX: qt0% IJR-1%'7Oi-7000
COPY TO: -
email: b ll Yx µow caolir4y-Of
Ramnlprl Rv- t 112-ri\i AffkA SAMPLE TYPE: I = Influent. E = Effluent, W = Well, ST = Stream. SO = Soil. SL = Sludge. Other:
'Sample Identification
Collection
M.y
5
N
w
w a
E'
G
0
;,
c t9
c
U V
z
e
.5
o LU
a M
-� z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
Z
N
o
o
c
SSl3 2
rrlo-I
1 UO3
1:7
i/ Ia
ll�
a#
)(
1,
cfi0.1 5
G
c
P
sy
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished -By:
Date/Time
Received By:
Dateffime
/aji
1Lisa
GIs-t41 loll
z.
116
l�{l
4 : a o
Temperature when Received: Accepted: ejec e : rcesampie rcequestea. I
Delivered By: Received By. Q� �� Date: 5-CGIV Time: /S o
Comments: TURNAROUND:
LEWIS FARMS
WQ0000455
Carolina Beach WWTP
.
. . ..... ..
............................
...........
. ......... .............. . ......
.................
..... . . .. .....
....
04/15/14
6,389
3.8054
04/15/14
3,602
3.5565
04/23/14
219,513
5.3415
04/23/14
415,585
5.6187
04/23/14
241,936
5.3837
04/23/14
240,642
5.3814
04/23/14
415,585
5.6187
Total 1 34.7058
Average 1 4.9580
Geometric Mean Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction
requirement.
I
Environmental Chemists, Inc.
envirochem
6602 Windmill Way • Wilmington, NC 28405
(910) 392-0223 (Lab),• (910)392-4424(Fax)
710 Bowsertown Road • Manteo, NC 27954
(252) 473-5702
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DI.S CERTIFICATE #37729
Town of Carolina Beach
Date of Report: Apr 21, 2014
1121 North Lake Park Blvd
Customer PO #:
Carolina Beach NC 28428
Report #: 2014-04382
Attention: Bill Raymond
Report to: Bill Raymond
A
Project ID:
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-10545 Site: Basin #1
4/15/2014 10:17 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (°!°)
sM 2540 B 3.60 % 04/16/2014
Fecal Density
SM 9221C E MPN 24 hr503 6389 MPN/g 04116/2014
Lab ID Sample ID:
�i
Collect Date/Titne Matrix Sampled by
14-10546 Site: Basin #2
4/15/2014, 10:17 AM Solid/Sludge Client
Test
Method Results Date Analyzed
I
Total Solids (%) - sM 2540 B 3.61 % - 04/16/2014
Fecal Density SM 9221C E MPN 24 hr.903 3602 MPN/g 04/16/2014
Comment: Results reported on a dry weight basis.
Reviewed by: / N),'0 , NQ'InAt
Report #:: 2014-04382 Page 1 of 1
� .NC
PRIM
ON
07
I'lTo.
Date
Temp.
.5a.1p lit �rl
-c
..-CRI(
Fe-ca
jd
P.
P
I.
G
mm
it
No
eml dQChkM Pm.
A,
V.
r
Environmental Chemists, Inc.
• 'chem 6602 Windmill Way •Wilmington, NC 28405
(910)392-0223(Lab) • (910) 392-4424 (Fax)
sM 710 Bowsertown Road a Manteo, NC 27954
ANALYTICAL & CONSULTING (252) 473-5702
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Town of Carolina Beach, Date of Report: Apr 28, 2014
1121 North Lake Park Blvd Customer PO #:
Carolina Beach NC 28428 Report #: 2014-04734
Attention: Bill Raymond Report to: Bill Raymond
Project ID: Wastewater Treatment- Pollutant
Scan
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-11387 Site: Sludge #1 4/23/2014 11:58 AM Solid/Sludge Bill Raymond
- Test Method Results Date Analyzed
Total Solids (°to)
SM 2540 B
4.10 % 04/24/2014
Fecal Density
SM 9221C E: MPN 24 hr 503
219513 MPN/g 04/24/2014
Lab ID Sample ID:
Collect DateITime
Matrix Sampled by
j 14-11388 Site--- Sludge #2
4/23/2014 11:58 AM
Solid/Sludge Bill Raymond
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.85 % 04/24/2014
Fecal Density
SM 9221 C E MPN 24 hr 503
415585 MPN/g 04/24/2014
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
14-11389 Site: Sludge #3
4/23/2014 11:58 AM
Solid/Sludge Bill Raymond
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.72 % 04/24/2014
Fecal Density
SM 9221C E MPN 24 hr 503
241936 MPN/g 04/2412014
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
14-11,390 Site: Sludge #4
4/23/2014 11:58 AM
Solid/Sludge Bill Raymond,
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2640 B
3.74 % 04/24/2014
Fecal Density
SM 9221C E MPN 24 hr 503
240642 MPN/g '04/24/2014
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
14-11391 Site: Sludge #5
4/23/2014 11:58 AM
-Solid/Sludge Bill Raymond
Test
Method
Results Date Analyzed
j,
Total Solids (%)
SM 2640 B
3.85 % 04/2412014
Fecal Density
SM 9221C E MPN 24 hr 603
415585 MPN/g 04/24/2014 -
Report #:: 2014-04734
Page 1 of 2
envirochem
ANALYTICAL & CONSULTING
CHEMISTS
Town of Carolina Beach
1121 North Lake Park Blvd
Carolina Beach NC 28428
Attention: Bill Raymond
Environmental Chemists, Inc.
6602 Windmill Way o Wilmington, NC 28405
(910) 392-0223 (Lab) • (910) 392-4424 (Fax)
710 Bowsertown Road • Manteo, NC 27954
(252) 473-5702
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Date of Report: Apr 28, 2014
Customer PO #:
Report #: 2014-04734
Report to: Bill Raymond
Project ID: Wastewater Treatment - Pollutant
Scan
Comment: Results reported on a dry weight basis.
Reviewed by:
4
I
I7
Page 2 of 2
Report#:: 201404734
»sw� t.srs'ars a
EN l:; _•t�ilUTLC. 1FM[ST;.IC�►
���': < • •�,'.Chemises 11COENR:•DWWQ`CERTIFICATIdtilr' . OFFICE: T110 392-0223 FAX �10 392�f424
�;g' �.94'NCaliHS: DL•S`G.ERTlFICATgN * 37729
COLLECTION•AND'CHAIN OF CUSTODY
CLIENT: Ct f-0 1'CQC•
PROJECT NAME:' S �,4ift?Q tt�i`} ' REPORT NO• 1 T -%
ADDRESS,y:� s• Oic)00
CONTACT NAME: [: •• PO NO.
K3 `?x�c�,, C E24 ZQ
;.'
REPORTTO:1`i PHONEIFAX: (gt0)4N-Z9Ib Z
.
CQPYT0:.:•;2--1.:Mti
iL
S
SarrpletiBy �
.•:n.
.ILI
.:•�-.;:' C�•p�:q�W
SAiMF l:E TYPE I = IMluent, E:= Ef(IW it, W = Well, ST = Stream, SO = Soi! ;SL = `Sludge, O&r:
Collection:
:: -` PRESERVATION
_
t-
.. Wy
.: .zO ''•'�m yp
Date Timie Tern
J: :t
.
. REQUESTEDO ANAYSISAIl
B (m_ • o xo.
�4,O. _ ; O �4,r• ., V J..�•.', • O i =i. N 2 t '
�:
�. z' _ _' a 4
sluff e
SL
;c
13]
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--' x
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G
G:=:
_
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c 5 L P.
43.1)q l i d.
S�N :� # y13
SL c
G �' i 13RI
C. P'
G G
:.:
G .t P :}
r'
G ::h
`4
C.
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:•'
No o�c +�o+3iaWK
Z1C� ;. G.. -'^^� • M. ryifl{df• P. hMld.ilidBlGi�fli
•..-
..
' 7ranahr'
.t *:� .y 1.
11N� be dlCI7{Ofl{IKb l02 PPm, ).liill.iiwstts:ti�arca�f.cMioe. s•�':.+�es. for issOructioss.
: Reli` uistiei!
B DafialTime' �ad Da,om- e
;—'j
T*aWmaWm when Received: Z3 :l
�P�= jetted
_ Dalivsr�d By: —�i
CGY�r1Ar1�'•
F% elired B s i�I
y Date: .`i'1 t-i�i 14 Tiw.®•
ANNUAL PATHOGEN AND VECTOR ATTRACTION R { DUCTION FORM (02T Bales)
Facility Name: Coastal Farms and Residuals, LLC wQ permit Number- WQ0034806
WI'VTP Name! Town of Carolina Beach WWTP NPIDES Number: NCO023256
------
Monitoring Period: From 1 /1 /2014 TO 12/31 /2014
Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternative pt l'1'avmed'.
C.lass A.: Alt. Ei (Bane/temp) 0 Alt B (All; Treatment) Alt. C (Prior Testing) M
A1t.D (114o Prior Test) Process to Further Reduce Pathogengs 0
rf annlioahlp fn enlf-prn anvil TZ0,1 i'ahrmpil dd'`lne% A nnIVA ieaalietate to-Furalter Reduce Patlaexiens":
Compost
at Drying ®
- beat Treatment 13
Thermophilic El
Beta Ray
Gamma Ray ®
Pasteurization 0
Class 9:
JAlt_ (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applit:blale to alternative peaforined (Class B onl3) indicate `T ocess to Ssgnifica fitly Reduce 1'uthogepp":
Lime Stabilization ® Air Drying ® CoTj)osting CI jAcrobic Digestion 13
nae o c .D' a ti ti r bi i s o A �
If nianlicalele to alternaf i er nerf'ormed (Class A or Class R) cesm nlete the folloWinE mordtorine data:
Parameter
Allowable Level
Sludge
Pathogen Density
NUMber o
Excc-
donee
Frequency
of Analysis
Sample
Type
Ana ytrca
Tech-
ni h-
auc
Minima
Geo. Dean
Vlaximn
Units
2 x 10 to the
2
MPN
6111 power
CFU
Fecal Coliforrit
per gram of
total solids
1000 mpn per grata
of total solid (dry.
3,602
90,777
415,585
id1PN/9
0
Annual
Grab
SM 9221C
weight)
Salmonella bacteria
3 MPN per 4 ,b77ratns
(in lieu of fecal
total solid (dry
coliform)
weight)
ector Attraction Red®rction (1SA NCAC
02T .11I0 71- Pleaseitbdiente aide` not ve ne'rfiDrmeal:
AltJ ( S reduction) "
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) ®
Alt. 4 (Spec. O, uptalcc) (�
Alt., 5 (14-Day Aerobic),
Alt. 6 (Alit. Stabilization ®
Alt 7 (Drying - Stable) 0
JAIL 8 (Drying -Unstable)
Alt. 9 (Injection) [3
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed [�
CERTIFICATION STATEI Il1'l' (pleases checic the appropriate statement)
R1 "I certify, sander penalty of law, that the pathogen requirements in f Si) NCAC 02T .1106 and the
vector attractiatr reduction requirement in 15A, NCAC 02T _1107 have been ineLl'
El "I certify, under penalty of law, that the pathogen requirements in ISA. NCAC 02T .1106 and the
vector attraction reduction requirement in ISA NCAC 027'.1107 have not been met." (Please mote if
you check this statement attach an explanation why you have not abet cite or both of tiler
requirements.)
"This determination has been trade tinder my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I arts aware that there are
significant pettalties f"or false certification including dart' -and imprisonment.',
William J.Raymond, ORC Wesley Wooten, Manager
Preparer Name and Title (type or print) Land Appli - Na ie • ,id T' e (if applicable)(type or print)
i Ol -2 n •Z��.� 02� IS
Signature repay _4 Date Sign4tuK. of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
l
DENR FORM PVRF 02T (1212006)
COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: July 28, 2014
MOTSU - North Wharf Permit No. NCO029122
2.39 % Solids
6.26 nH
Parameter
1. %
lMg/KgDryWeightl
x 10,000)
Pounds/Dry Ton
(Mg/Kg (Mg/Kgx 0.002
Nitrogen (TKN)
0.667
6,670.000
13.34.0
Phosphorus
0.097
967.000
1.934
Potassium
0.099
992.000
1.984
PAN injected)*
0.211
2,114.200
4.228
PAN surface)*
0.205
2,049.200
4.098
Ammonia Nitrogen
0.013
130.000
0.260
Calcium
0.191
1,910.000
3.820
Calcium Carbonate E .
---
---
---
Magnesium
---
849.000
1.698
Sodium
---
242.000
0.484
Sulfur
---
---
Nitrate N / Nitrite N
---
22.200
0.044
Barium
---
---
SAR
Chloride
---
---
0.18
Iron
---
---
---
Ceilin ' Concen.
g
Aluminum
--
13,100.00
26.200
(Mg/Kg)
Arsenic
---
3.77
0.008
75
Cadmium
---
3.77
0.008
85
Chromium
---
20.300
0.041
---
Copper
---
23.90
0.048
4,300
Lead
---
13.20
0.026
840
Mercury
---
0.13
0.000
57
Molybdenum
---
3.77
0.008
75
Nickel
---
11.20
0.022
420
Selenium
---
3.77
0.008
100
Zinc
-
53.60
0.107
7,500
Environmental Chemists # 2014-08955
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
COSTAL FARMS AND RESIDUALS, LLC
WQ003480600.455
MOTSU
. .............
..........
.............
....
... ... ...
.
::e
........ .. l: .. :
...........................
. . . .....................
07/28/14
662,651
5.8213
07/28/14
758,621
5.8800
07/28/14
160,772
5.2062
07/28/14
130,549
5.1158
07/28/14
281,691
5.4498
07/28/14
357,143
5.5528
07/28/14
412,699
5.6156
Total 1 38.6415 —]
Average 1 5.5202
Geometric Mean Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen for Reduction
requirement.
4 '
Environmental Chemists, Inc.
envirochem6602 Windmill Way • Wilmington, NC 28405
-= (910)392-0223(Lab) • (910)392-4424(Fax)
SM
710 Bowsertown Road a Manteo, NC 27954
ANALYTICAL & CONSULTING (252) 473-5702
-' CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Lewis Farms & Liquid Waste, INC. Date of Report: Aug 15, 2014
8155 Malpass Corner Road Customer PO #;
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2014-08955
Project ID: MOTSU-North Wharf Lagoon
Lab ID Sample ID:
14-22162 Site: Sludge
Test
Collect DatelTime
7/28/2014 11:05 AM
Method
Matrix Sampled by
Solid/Sludge Jay Baker
Results Date Analyzed
Sludge Residuals
Aluminum
EPA200.7
131.00 mg/kg
08/04/2014
Arsenic
EPA200.7
<3.77 mglkg
07/31/2014
Cadmium
EPA200.7
<3.77 mg/kg
07/31/2014
Calcium
EPA200.7
1910.mg/kg
07/31/2014
Chromium
EPA200.7
20.3 mg/kg
07/31/2014
Copper
EPA2o0.7
23.9 mg/kg
07/31/2014
Lead
EPA200.7
13.2 mg/kg
07/31/2014
Magnesium
EPA200.7
849 mg/kg
07/31/2014
Molybdenum
EPA 200.7
<3.77 mg/kg
08/05/2014
Nickel
EPA200.7
11.2 mg/kg
07/31/2014
Potassium
EPA200.7
992 mg/kg
07/31/2014
Selenium
EPA200.7
<3.77 mg/kg
07/31/2014
Sodium
EPA200.7
242 mg/kg
07/31/2014
Zinc
EPA200.7
53.6 mg/kg
07/31/2014
Ammonia Nitrogen
�l
EPA350.1
130mg/kg
07/31/2014
Total Kjeldahl Nitrogen (TKN)
EPA351.2
6670 mg/kg
08/07/2014
Nitrate+Nitrite-Nitrogen
EPA353.2
22.2 mg/kg
08/01/2014
Total Solids (%)
SM 2540 B
2.39 %
07/30/2014
pH
SM4500 H 8
6.26 units
08/01/2014
- Total Phosphorus
SM 4500 P F
967 mg/kg
08/07/2014
Mercury
SW8467471B
<0.126mg/kg
08/14/2014
Report #:: 2014-08955 Page 1 of 3
Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
(910) 392-0223 (Lab) • (910) 392-4424 (Fax)
SM
710 Bowsertown Road • Manteo, NC 27954
(252)473-5702
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Lewis Farms & Liquid Waste, INC.
Date of Report: Aug 15, 2014
8155 Malpass Corner Road
Customer PO M
t Currie NC 28435
Customer ID: 14020008
Attention: Wesley Wooten
Report #: 2014-08955
Project ID: MOTSU-North Wharf Lagoon
LabID Sample ID:
Collect Date/Time Matrix Sampled by
14-22163 Site: 1
7/28/2014 11:06 AM Solid/Sludge Jay Baker
Test
Method Results Date Analyzed
Total Solids {%) SM 2540 8 3.32 % 07/30/2014
Fecal Density SM 9221C EMPN 24 hr 503 662651 MPN/g 07/29/2014
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-22164 Site: 2
7/28/2014 11:06 AM Solid/Sludge Jay Baker
Test
Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.45 % . 07/30/2014
Fecal Density SM92210EMPN 24hr503 758621 MPN/g 07/29/2014
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14 22165 Site: 3 7/28/2614 11:07 AM Solid/Sludge Jay Baker
Test Method Results Date Analyzed
Total Solids (%) sM 2540 B 3.11 % 07/30/2014
Fecal Density SM 9221C E MPN 24 hr 503 160772 MPN/g 07/29/2014
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-22166 Site: 4 7/28/2014 11:07 AM Solid/Sludge Jay Baker
t Test Method Results Date Analyzed
Total Solids (%)
SM 2540 B
3.83 %
07/30/2014
Fecal Density
SM 9221C E MPN 24 hr 503
130549 MPN/g
07/2912014
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
14-22167 Site: 5
7/28/2014 11:07 AM
Solid/Sludge Jay Baker
Test
Method
Results
Date Analyzed
r_
1 Total Solids (%)
SM 2540 B
2.84 %
07/30/2014
Fecal Density
SM 9221C E MPN 24 hr 503
281691 MPN/g
07/29/2014
Report #:: 2014-08955
f •
1
Page 2 of 3
_a
F77Environmental Chemists, Inc.
Lienvirochem 6602 WindmillWay • Wilmington, NC 28405
(910)392-0223(Lab) • (910) 392-4424 (Fax)
SM
710 Bbwsertown ].load a Manteo, NC 27954
ANALYTICAL & CONSULTING (252) 473-5702
CHEMISTS NCDENR: DWQ CERTIFICATE 494. DIS CERTIFICATE 437729
Lewis Farms & Liquid Waste, INC. Date of Report: Aug 15, 2014
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2014-08955
Project ID: MOTSU-North Wharf Lagoon
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-22168 Site: 6 7/28/2014 11:08 AM Solid/Sludge Jay Baker
i Test Method Results Date Analyzed
Total Solids (%)
SM 2540 s
1.96 %
07/30/2014
Fecal Density
SM 9221C E MPN 24 hr 503
357143 MPN/g
07/29/2014
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
14-22169 Site: 7
7/28/2014 11:08 AM
Solid/Sludge Jay Baker
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 a
3.15 %
07/30/2014
Fecal Density
SM 9221C E MPN 24 hr 503
412699 MPN/g
07/29/2014
Comment: Results, except pH,
reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report #:: 2014-08955 Page 3 of 3 ..r
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLFCTION AND CHAIN OF rtISTC)DY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX 910-392-4424
info@environmentalchemists.com
CLIENT: f..r; J
PROJECT NAME: 1*0>7-5q- 1JjtC 4jC..•X
REPORT NO: iY- Pqs
ADDRESS:
CONTACT NAME: ++�
PO NO:
REPORT TO: Sl+
PHONEIFAX:
COPY TO: sr : a. /Vf -457/�
email:
Samnled Bv: t/ ZZ SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludae. Other:
Sample Identification
Collection
4 d
S
y
No .c
E `o
c
;,
a (7
�o
va
c
_o` �+
u E
O W
m g
gz
PRESERVATION
ANALYSIS REQUESTED
ate
Time
Temp
i
i
s
o
=
0
=
0
z
o
w
a
ff
f
/a
C
P
• ,� 114UXI
C
P
/ / f
L
K•
C
P
b
G
G
aa�
C
P
G
G
Lug
G
G
tNs}
L�L�
G
G
eJ
Ly�l
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Daterrime
Received By:
Date/Time
1.
2.
e
Temperature when Received:- 3 — Accepted: - Rejected: Resample Re a ed:
Delivered By: r✓! Received By: Date: Time:
Comments: TURNAROUND:
Lb( AQ {
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
l
r,
1
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: MOTSU - ^ NPDES Number: NCO029122
Monitoring Period: From 1/l/2014 To 12/31/2014
Pathoeven Reduction (15A NCAC 02T .1106) - Please indicate level nehieverl and alternative nerfnrmoA-
Class A:
All. A (time/temp) 0
1 Alt B (Alk Treatment) [I
Alt. C (Prior Testing) E3
A1t.D (No Prior Test) ES I
I Process to Further Reduce Pathogengs 014
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 1I
I Heat Drying 0
Heat Treatment ®
Theiinophilic
Beta Ray 01
Gamma Ray 0
Pasteurization
Class B:
I Alt. (1) Fecal Density R1
Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ®
Air Drying 0
Composting
Aerobic Digestion 0
Anaerobic Digestio
n on
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um er oFrequency
Excee-
dences
of Analysis
Sample
Type
Analytical
Tech -
ni ue ,
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
oftotal solid (dry
weight)
130,549
331,299
758,621
MPN/g
0
Annual
Grab
SM 9221
Salmonella'bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Keduction 05A NUAC 02T .1107) - Please indicate alternative performed:,
Alt. ] (VS reduction)
®
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) ® Alt. 4 (Spec. OZ uptake)
El
Alt. 5 (14-Day Aerobic)
[3
Alt. 6 (Alk. Stabilization E3
jAlt 7 (Drying - Stable) ®Alt. 8 (Drying - Unstable)
Alt. 9 (Injection)
®
Alt. 10 (Incorporation) R1
INo vector attraction reduction alternatives were performed
E3
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T..1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my ,direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information, used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Wesley Wooten, Manager
Preparer N e and Ti lei print) o Land Applier Name and Title (if applicable)(type or print)
Signature o reparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21'^".1102 (26)
1
DENR FORM PVRF 02T (12/2006)
COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 27, 2014
North Topsail WWTF Permit No. W00005849
2.86 % Solids
7.03 nH
Parameter
%
Mg/Kg Dry Weight
% x 10,000)
Pounds/Dry Ton
M /K x 0.002
Nitrogen (TKN)
1.790
17,900.000
35.800
Phosphorus
1.450
14,500.000
29.000
Potassium
0.493
4,930.000
9.860
PAN (injected)*
0.552
5,524.260
11.049
PAN surface)*
0.548
5,475.360
10.951
Ammonia Nitrogen
0.010
97.800
0.196
Calcium
2.870
28,700.000
57.400
Calcium Carbonate E .
---
---
---
Magnesium
---
3,060.000
6.120
Sodium
---
5,240.000
10.480
Sulfur
---
___
Nitrate N / Nitrite N
---
85.800
0.172
Barium
---
---
SAR
1.33
Chloride
---
---
Iron
---
---
---
Ceiling Concen. '
(Mg/Kg)
Aluminum
---
45,500.00
91.000
Arsenic
---
3.91
0.008
75
Cadmium
---
3.22
0.006
85
Chromium
---
26.700
---
---
Copper
---
248.00
0.496
4,300
Lead
---
7.41
0.015
840
Mercury
---
0.52
0.001
57
Molybdenum
---
3.22
0.006
75
Nickel
---
20.20
0.040
420
Selenium
--
4.65
0.009
100
Zinc
=--
3,100.00
6.200
7,500
Environment 1 # 2014-02332
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
r
COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
North Topsail WWTF
...........................
..
02/27/14
29,963
4.4766
02/27/14
38,462
4.5850
02/27/14
176,679
5.2472
02/27/14
17,858
4.2518
02/27/14
38,063
4.5805
02/27/14
59,441
4.7741
02/27/14
107,914
5.0331
Total 1 32.9483
Average 4.7069
Geometric Mean € 3p€€'€€ Fecal Coliform MPN /gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.
rop'".
Environmental Chemists,
Inc.
-7-
L —7 envirochem6602
Windmill Way • Wilmington, NC 28405
i
(910)392-0223(Lab) (910)392-4424(Fax)
710 Bowsertown Road • Manteo, NC 27954
(252) 473-5702
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Pluris LLC. (Utility Partners LLC.)
Date of Report: Apr 09, 2014
P. O. Box 856
Customer PO #:
t
Sneads Ferry NC 28460
Report #: 2014-02332
Attention: Randy Hoffer
Report to: Randy Hoffer
Project ID: Sludge
+ i
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-05703 Site: Sludge
2/27/2014 11:40 AM Solid/Sludge Pete Peterson
Test
Method
Results Date Analyzed
Sludge Residuals
'
Aluminum
EPA200.7
45500 Mg/kg
03/13/2014
I
Cadmium
EPA200.7
<3.22 mg/kg
03/1012014
Calcium
EPA200.7
28700 mg/kg
03/12/2014
Chromium
EPA200.7
26.7 mg/kg
03/10/2014
Copper
EPA200.7
248 mg/kg
03/10/2014
i
Magnesium
EPA200.7
3060 mg/kg
03/12/2014
Molybdenum
EPA200.7
<3.22 mg/kg
03/10/2014
Nickel
EPA200.7
20.2 mg/kg
03/10/2014
Potassium
EPA200.7
4930mg/kg
03/12/2014
Selenium
EPA200.7
4.65mg/kg
03/14/2014
Sodium
EPA200.7
5240mg/kg
03/12-/2014
Zinc
EPA 200.7
3100 mg/kg
03/12/2014
}
Arsenic
EPA200.8
3.91 mg/kg
3/17/2014
s1
Ammonia Nitrogen
EPA 350.1
97.8 mg/kg
03/04/2014
Total Kjeldahl Nitrogen (TKN)
EPA $51.2
17900 mg/kg
03/26/2014
I P
i
Nitrate+Nitrite-Nitrogen
EPA 353.2
85.8 mg/kg
03/11/2014
Total Solids (%)
sM 2540 B
2.86 %
02/28/2014
pH
SM4500 H B
7.03 units
03/11/2014
Total Phosphorus
SM450D P F
14500 mg/kg
04/03/2014
Mercury
SWM7471B
0.5240 mg/kg
02/28/2014
5�'
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
14-05703A Site: Sludge
2/27/2014 11:40 AM Solid/Sludge Pete Peterson
Test .
Method
Results Date Analyzed
Lead EPA200.7 7.41 mg/kg 04/08/2014
Report #:: 2014-02332 Page 1 of 3
Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
(910) 392-0223 (Lab) - (910) 392-4424 (Fax)
SM
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL &CONSULTING (252) 473-5702-
CHEMISTS NCDENR- DWQ CERTIFICATE #94. DL5 CERTIFICATE #37729
Pluris LLC. (Utility Partners LLC.) Date of Report: Apr 09, 2014
P. O. Box 856 Customer PO #:
Sneads Ferry NC 28460 Report#: 2014-02332
Attention: Randy Hoffer Report to: Randy Hoffer
Project ID: Sludge
Lab ID Sample ID: 1 Collect Date/Time Matrix Sampled by
14-05710 Site: 2/27/2014 11:40 AM Solid/Sludge Pete Peterson
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 6
2.67 %
02/28/2014
Fecal Density
SM 9221C E MPN 24 hr503
29963 MPN/g
02/2812014
Lab 1D
t
,._r Test
Sample ID: 2 Collect Date/Time Matrix " Sampled by
C*#_. --_. _ 7/77111A4A _.14.An A1111
Method Results Date Analyzed
I Total Solids (%)
SM2540 a
2.86 % 02/2-8/2014
Fecal Density
SMD2210EMPN 24hr503
38462MPN/g 02/28/2014
Lab ID Sample 1D: 3
CollectDatelTime
Matrix Sampled by
14-05712 Site:
2/27/2014 11:40 AM
Solid/Sludge Pete Peterson
Test
Method
Results Date Analyzed
Total Solids {%)
SM 2540 s
2.83 % 02/28/2014
Fecal Density
SM 9221C E MPN 24 hr503
176679 MPN/g 02/28/2014
Lab ID Sample ID: 4
Collect Date/Time
Matrix Sampled by
14-05713 Site:
2/27/2014 11:40 AM
Solid/Sludge Pete Peterson
} I Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.80 % 02/28/2014'
Fecal Density
SM 9221C E MPN 24 hr 503
17858 MPN/g 02/28/2014
Lab ID Sample ID: 5
Collect Date/Time
Matrix Sampled by
14-05714 Site:
2/27/2014 .11:40 AM
Solid/Sludge Pete Peterson
Test
Method
� Results Date Analyzed
S Total Solids %
( )
SM 2540 s
o
2.89 /0 02/28/2014
Fecal Density
SM 9221C E MPN 24 hr 503
38063 MPN/g 02/28/2014
i l
Report #:: 2014-02332
I
� 1
i �
Page 2 of 3
f 1.
T Environmental Chemists, Inc.
envirochem
6602 WindmillWay. • Wilmington, NC 28405
(910) 392-0223 (Lab) • (910) 392-4424 (Fax)
sna
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL & CONSULTING (252) 473-5702
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
i
Pluris LLC. (Utility Partners LLC.) Date of Report: Apr 09, 2014
P. O. Box 856 Customer PO #:
i Sneads Ferry NC 28460 Report #: 2014-02332
Attention: Randy Hoffer Report to: Randy Hoffer
Project ID: Sludge
Lab ID Sample ID: 6- Collect Date/Time Matrix Sampled by
14-05715 Site: 2/27/2014 11:40 AM Solid/Sludge Pete Peterson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 2.86 % 02/28/2014
Fecal Density SM 9221c a MPN 24 hr 503 59441 MPN/g 02/28/2014
Lab ID Sample ID: 7 Collect Date/Time Matrix Sampled by
14�15716 Siite: 21277-2-0a4- 11;40-AM-Solid/Sludge - Pete-Reterson-
�I
Test Method Results Date Analyzed
a j Total Solids (%) SM 2540 s' 2.78 % 02/28/2014
Fecal Density SM 9221C E MPN 24 hr 503 107914 MPN/g 02/28/2014
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
y
Report #:: 2014-02332 Page 3 of 3
a
I ,
Analytical & Consulting Chemists .
ENVIRONMENTAL CHEMISTS, ING
NCDENR: DWQ CERTERICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
6602 Windmill Way Wilmington, NU 204u0
OFFICE: 910-392-0223 FAX 910-392-4424
COLLECTION AND CHAIN OF CUSTODY
CLIENTc_Pluris PROJECT NAME: —Groundwater Lowering REPORT NO:
Ic
ADDRESS: CONTACT NAME: C(� Get _PO NO:
REPORT TO: PHONE/FAX:
71 COPY TO: E-MAIL:
__a ••1 ...-uL.11 e7 - e# Cn = _qr%u 4;1 _ = studae. Other:
Sample Identification
Collection
MM
ANALYSIS REQUESTED
Fwam
bIVA
Snow,
monolog
r
L4
ArrAfAM
0 VAP
IF,
PASS
7AF
O1111101111"T
WAM
W, 'A
�sM
w
gm
"AF
�T��W
WA
4�
W
���
paterrime
Temperat
Delivered
Comment
1
I
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: North Topsail WWTF NPDES Number: WQ0005849
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed:
Class A:
Alt A (time/temp) ❑
Alt B (Alk Treatment) ElAlt.
C (Prior Testing) ❑
AIt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) Indicate "Process to Further Reduce Pathogens-:
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ra ❑
Gamma Pay ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Com ostin g ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
-
If applicable to alternative performed (Class A or Class B) complete the
Ilowing monitoring data:
Parameter
Allowable Level
in Sludge
in
Pathogen Density
Number o
Excee-
deuces
Frequency
of Analysis
y
Sample
Type
a ytica
Tech -
ni ue
Minimu
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
17,858
50,921
176,679
MPN/g
0
Annual
Grab
SM 9221
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative Derformed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench). ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) (]
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
t] "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Randy Hoffer, ORC Wesley Wooten, Manager
Preparer a and Title (type or print) Land Appli N e d T' le (if applicable)(type or print)
1 ao>s of 24 iS
Signatur f Preparer* Date Signatu e o Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
DENR FORM PVRF 02T (12/2006)
A,
COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: June 2, 2014
Surf City WWTP
1.06 % Solids
7_nn nu
Permit No. WQ0000795
Parameter
%
�Mg/KgDryWeightl
% x 10,000)
Pounds/Dry Ton
(Mg/Kg (Mg/Kgx 0.002
Nitrogen (TKN)
2.630
26,300.000
52.600
Phosphorus
2.610
26,100.000
52.200
Potassium
0.585
5,850.000
11.700
PAN (injected)*
0.816
8,156.200
16.312
PAN surface)*
0.806
8,058.200
16.116
Ammonia Nitrogen
0.020
196.000
0.392
Calcium
5.390
53,900.000
107.800
Calcium Carbonate E .
---
---
---
Magnesium
---
4,760.000
9.520
Sodium
---
13,400.000
26.800
Sulfur
---
---
---
Nitrate N / Nitrite N
---
129.000
0.258
Barium
---
---
---
Chloride
---
---
---
Iron
---
---
---
Aluminum
---
4,010.00
8.020
Arsenic
---
11.90
0.024
Cadmium
---
9.34
0.019
Chromium
-
26.800
0.054
Copper
---
736.00
1.472
Lead
---
24.20
0.048
Mercury
---
0.57
0.001
Molybdenum
---
9.34
0.019
Nickel
---
21.50
0.043
Selenium
---
9.34
0.019
Zinc
---
2,110.00
4.220
Environmental Chemists # 2014-06321
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Surf City WWTP
D.ca'1'01
a
>1'`><
06/02/14
53,847
4.7312
06/02/14
16,912
4.2282
06/02/14
99,237
4.9967
06/02/14
60,607
4.7825
06/02/14
53,031
4.7245
06/02/14
77,465
4.8891
06/02/14
112,583
5.0515
Total 33.4037
Average 4.7720
Geometric Mean Fecal Coliform NON / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.
1
Environmental Chemists,
Inc.
__ t
6602 Windmill Way a Wilmington, NC 28405
(910) 392-0223 (Lab) - (910) 392-4424 (Fax)
sM
710 Bowsertown Road - Manteo, NC 27954
-
(252) 473-5702
ANALYTICAL & CONSULTING
CHEMISTS
NCDENF- DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
i'
-
Town of Surf City
Date of Report: Jul 15, 201'4
Post Office Box 2475
Customer PO #:
Surf City NC 28445
Customer ID: 08110024
Attention: Steve Smith
Report #: 2014-06321
—�
Project ID: Sludge
f
Lab ID Sample ID: Surf City
Collect DatelTime Matrix Sampled by
14-15266 Site: Sludge
6/2/2014
11:30 AM Solid/Sludge Client .
' k
Test
Method'
Results Date Analyzed
Chlordane
SW 846 Method 8081B/3510
<0.005 mg/L
06/05/2014
Endrin
SW 846 Method 8081 B/3510
<0.00005 mg/L
06/05/2014
r
Heptachlor
SW 846 Method Sol B13510
<0.00005. mg/L
06/05/2014
Heptachlor epoxide
SW 846 Method 8081 EM510
<0.00005 mg/L
06/05/2014
Lindane
SW 846 Method 8081 B13s10
<0.00005 mg/L
06/05/2014
Methoxychlor
SW 846 Method 8081 B13510
<0.00005 mg/L
06/05/2014
Toxaphene
SW 846 Method 8081 B/3510
<0.005 mg/L
06/05/2014
1,4-Dichlorobenzene(TCLP)
SW848 method 8270/3610
<0.05mg/L
06/04/2014
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.05 mg/L
06/04/2014
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.05 mg/L
06/04/2014
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.05 mg/L
06/04/2014
Cresol (TCLP)
SW 846 method 8270/3510
<0:05 mg/L
66/04/2014
Hexachloro-1,3-butadiene(TCLP)
SW 846 method 8270/3510
<0.05mg/L
06/04/2014
_
Hexachlorobenzene (TCLP)
SW 846 method.8270/3610
<0.05 mg1L
06/04/2014
Hexachloroethane (TCLP)
SW 846 method 827013510
<0.05 mg1L
06/04/2014
m + p-Cresol (TCLP)
SW 846 method B270MIO
<0.05 mg/L
05/04/2014
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.05 mg/L
06104/2014
o-Cresol (TCLP)
SW 846 method 827013510
<0.05 mg/L
06/04/2014
-
Pentachlorophenol (TCLP)
SW 846 method 827013510
<0.25 mg/L
06/04/2014
Pyridine (TCLP)
SW 846 method 8270/3510
<0.05 mg/L
06/04/2014
i
2,4,5-TP
sw84s Method s151A
<0.0003 mg/L
06/09/2014
2,4-D
SW846 Method 8151A
<0.0003 mg/L
0610912014
1,1-Dichloroethylene
SW846 Method 8260/5030 _
< 0.01 mg/L
06/20/2014
1;2-Dichloroethane
SW846 Method 826015030
<0.01 mg/L
06/20/2014
Benzene
SW846 Method 8260/5030
<0.01 mg/L
06/20/2014
Carbon Tetrachloride
SW846 Method 8260/5030
<0.01 mg/L
06/20/2014
Report #.: 2014-06321
Page 1 of 4
-�
Environmental Chemists,
Inc.
�-
6602 Windmill Way c Wilmington, NC 28405
(910) 392-0223 (Lab) • (910) 392-4424 (Fax)
SM
710 Bowsertown Road a Manteo, NC 27954
(252) 473-5702
-
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERT1RCATE #94. DLS CERTIFICATE #37729
ti
-
Town of Surf City
Date -of Report: Jul 15, 2014
Post Office Box 2476
Customer PO #.
Surf City NC 28445
Customer ID: 08110024
Attention: Steve Smith
Report #: 2014-06321
Project ID: Sludge
I
~
_
Chlorobenzene
SW846 Method 8280/5030
<0.01 mg/L
06/20/2014
e=
Chloroform
SW846 Method 8260/5030
<0.01 mg/L
06/20/2014
Methyl ethyl ketone
SW846 Method 826015030
<0.05 mg/L
06/20/2014
Tetrach loroethylene
SW846 Method 8260/6030
<0.01 mg/L
06/20/2014
Trichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
06/20/2014
Vinyl Chloride
SW846 Method 8260/5030
<0.01 mg/L
06120/2014
RCI
Cyanide
EPA 335A
<0.120 mg/kg
06/04/2014
Sulfide
SM 4500 S D
<0.239 mg/kg
06/04/2014
r;
Ignitability
SW 846 method 1010
>212 OF
06/06/2014
Sludge Residuals
Aluminum
EPA200.7
4010mg/kg
0611612014
-
Arsenic
EPA200.7
11.9mg/kg
06/12/2014
t
Cadmium
EPA200.7
<9.34mg/kg
06/12/2014
Calcium
EPA200.7
53900mg/kg
06/17/2014
Chromium
EPA200.7
26.8mg/kg
06/12/2014
Copper
EPA 200.7
736 mg/kg
06/12/2014
Lead
EPA200.7
24.2 mg/kg
06112/2014
Magnesium
EPA200.7
4760 mg/kg
06/17/2014
Molybdenum
EPA 200.7
<9.34 mg/kg
06/12/2014
Nickel
EPA200.7
21.5mg/kg
06/12/2014
Potassium
EPA200.7
5850 mg/kg
06/17/2014
Selenium
EPA200.7
<9.34 mg/kg
06/12/2014
Sodium
EPA200.7
13400 mg/kg
06/17/2014
Zinc
EPA200.7
2110 mg/kg
06/12/2014
Ammonia Nitrogen
EPA350.1
<196mg/kg
06/05/2014
Total Kjeldahl Nitrogen (TKN)
EPA351.2
26300mg/kg
06/09/2014
Nitrate+Nitrite-Nitrogen
EPA353.2
129 mg/kg
06/24/2014
Total Solids (%)
sM 2640 B
1.06 %
06/03/2014
i
Report #:: 2014-08321
Page 2 of 4
Environmental Chemists,
Inc.
6602 Windmill Way • Wilmington, NC 28405
(910) 392-0223 (Lab) • (910) 392-4424 (Fax)
710 Bowsertown Road • Manteo, NC 27954
(252)473-5702
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Town of Surf City
Date of Report: Jul 15, 2014
Post Office Box 2475
Customer PO #:
Surf City NC 28445
Customer ID: 08110024
Attention: Steve Smith
Report #: 2014-06321
Project ID: Sludge
pH
SM 4500 H B
7.00 units
06/05/2014
-
Total Phosphorus
SM 4500 P F
26100 mg/kg
06/09/2014
Mercury
SWM7471a
0.5660 mg/kg
06/09/2014
TCLP Metals
Arsenic
EPA200.7
<0.100mg/L
06/06/2014
Barium
EPA200.7
<0.100mg/L
06/06/2014
Cadmium
EPA200.7
<0.100 mg/L
06/06/2014
_
Chromium
EPA200.7
<0.100mg/L
06/06/2014
Lead
EPA200.7
<0.100mg/L
d6/06/2014
Selenium
EPA200.7
<0.100mg/L
06/06/2014
Silver
EPA200.7
<0.100 mg/L
06/06/2014
t
Mercury
EPA245.1
<0.002mg/L
06/17/2014
Lab ID Sample ID: Surf City
Collect DatelTime Matrix Sampled by
14-15267 Site: # 1
6/2/2014 11:30 AM Solid/Sludge Client
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 a
1.30 %
06/03/2014
Fecal Density
SM 9221 C E MPN 24 hr 503 53847 M PN/g
06/03/2014
Lab ID Sample ID: Surf City
Collect DatelTime Matrix Sampled by
14-16268 Site: # 2
6/2/2014 11:30 AM Solid/Sludge Client
T-
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 s
1.36 %
06/03/2014
Fecal Density
SM 9221C E MPN
24 hr503 16912 MPN/g
06/03/2014
Lab ID Sample ID: Surf City
Collect Date/Time Matrix Sampled by
14-15269 Site: # 3
6/2/2014 11:30 AM Solid/Sludge Client
Test
Method
Results Date Analyzed
Total Solids (%) SM 2540 a 1.31 % 06/03/2014
sFecal Density SM 9221C E MPN 24 hr603 99237 MPN/g 06/03/2014
r Report #:: 2014-06321 Page 3 of 4
11__i
7
Environmental Chemists, Inc.
envirochem(910)
6602 WindmillWay • WlnUngton, NC 28405
392-0223 (Lab) • (910) 392-4424 (Fax)
sn+
710 Bowsertown Road • Manteo, NC 27954
(252) 473-5702
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERTIFICATE 4194. DLS CERTIFICATE #37729
Town of Surf City
Date of Report: Jul 15, 2014
Post Office Box 2475
Customer PO #:
Surf City NC 28445
Customer ID: 08110024
Attention: Steve Smith
Report #: 2014-06321
Project ID: Sludge
Lab ID Sample ID: Surf City
Collect Date/Time Matrix Sampled by
14-15270 Site: # 4
6/2/2014 11:30 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 1.32 % 06/03/2014
Fecal Density
SM 9221C E MPN 24 hr 503 60607 MPN/g 06/03/2014
Lab ID Sample ID: Surf City
Collect Date/Time Matrix Sampled by
14-15271 Site: # 5
6/212014 11:30 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 1.32 % 06/03/2014
Fecal Density
SM92210EMPN 24hr503 53031 MPN/g 06/03/2014
Lab ID Sample ID: Surf City
Collect Date/Time Matrix Sampled by
14-15272 Site: # 6
6/2/2014 11:30 AM Solid/Sludge Client
Test
Method Results Date Analyzed
.a
Total Solids (%)
SM 2540 B 1.42 % 06/03/2014
Fecal Density
SM 9221C E MPN 24 hr 503 77465 MPN/g 06/03/2014
Lab ID Sample ID: Surf city Collect Date/Time Matrix Sampled by
14-15273 Site: # 7 6/2/2014 11:30 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 1.51 % 06/03/2014
Fecal Density SM 9221C E MPN 24 hr 503 112583 MPN/g 06/03/2014
Comment: Sludge residuals, except H, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: /
r
Report#:: 2014.05321 Page 4 of4
_-ENARONMEN SAL—C.HEM1STSjNC—..- _ 5602-Windmill-Way Wilmington, N'C28405
y NCDENR: DWQ CERTERICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 OFFICE: 910-392-0223 FAX 910-392-4424
Angly0C9i $, Copsuillng Chemists
1PWFNT- Town of 61prf c" yylryTP PROJECT NAME: Influent Sampling REPORT NO: 1 �" (12e3A
ANKH, CONTACTNAME: E: PO NO:
REPORT TO: PHONEIFAX:
COPY TO: E-MAIL:
Samoled Bv: SAMPLE TYPE: 1= Influent. E = Effluent. W = Well. ST = Stream_ SO = Seii_ SL = Sludna_ Other:
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PRESERVATION
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ANALYSIS REQUESTED
Date
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NOTIM - DECH1.011INATION: SampNs TorAmmonla, TKN. Cyanld% Phenol and Bacteria must be d chlerinated (02 ppm or less) In the field at the time 9f collection. See ravers- for Instructions
Thaofer
Relinquished By:
Datemme
AA to 90ce)ved By:
Date/Time
■ ■+nP*r7rsar R lIr r ` �AYYO+J&OY._ X _ 1 Bjeuxe K@Sample K@ U@ ted:
9ellvered By, a `y_'�Jfj'� Received By. L-{!' Date:
FQllllil@n V TUR AR UN.
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W000034806
WBVTP Name: Town of Surf City WWTP NPDES Number: W00000795
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (15A NCAC 02T .110Q - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
AIt.D (No Prior Test)
Process to Further Reduce Pathogen as ❑
:ff V..
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
r,
Beta Ray ❑
Gamma Ray ❑
Pasteurization - ❑
Class B:
Alt- (1) Fecal Density ®
Alt. (2)Process to Significantly Reduce Pathogens❑ -- .a'r,� i.
If applicable to alternative performed Class B only indicate "Process to Signiflcantly Reduce Pathogens":
Lime Stabilization ❑
Air ❑
composting ❑
Aerobic Digestion [3Anaerobic
Digestion [3_
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um r °
Excee
Frequency
of Analysis
Sample
Typenioue
AnalYu
Tech -
Minimum inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
16,912
59,150
112,583
MPN/g
0
Annual
Grab
SM 9221 C
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
1 Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 co oration) ®
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Steve Smith, ORC Wesley Wooten, Manager
Preparer Name and Title (type or print) Land Appl' r e d T' a (if applicable (type or print)
/S
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
2014 APPLICATION SUMMARY
COASTAL FARMS AND RESIDUALS, LLC
Permit # WQ 0034606
2014
RESIDUALS APPLICATIONS
APPLICATION. SUMMARY
..........
AN
AL
W E-T.: T.
T*�
. . .. N
ky .....
.....
..... ........
.
....... ... FAN......
Wilber Corbett
1
93.40
1,901,234
226.650
28.89
25.12
Totals
jig
Metric Tons 205.57
FIELD LOADING RATE REPORTS
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Dame: Coastal Farms and Residuals WQ Permit# WQ0034806 Field N WC-1
Acres Utilized: 93.4
Land Owner: Wilber Corbett Annual DT's Applied: 226.65 - Site 4: Corbett Shop Acres Permitted; 93.4
Operator: Allen Predominant Soil Series: Au ille - AuB Cation Exchange Capacity (non 503): 41
Crop 1 Name: Bermuda Crop 1 Max. PAN: 196 Crop 2 Naine: 2yagrass Crop 2 Max. PAN: SO
Application Method: S - Surface 'Volatilization Rate: Carolina Beach, MOTSU North Topsail, & Surf cit
y (Incorporated -1.0)
. KJJA.FV Y
2014
2014
2014
2014
•. %.:"3
1,113,750
9,984
222,000
555,500
.£'
11,925
107
2,377
5,948
. >
3.76
2.39
2.96
1.06
< ^ .
1.87
0.01
0.29
0.26
E; zP. '..' M..
Cato ;M.
U Will
op
�c�'a'
. •y�N�.�q�
ff
O/D
0.008
0.000
0.002
0.006
�t.:...
0.008 3.223
0.000 0.001
0.002 0.141
0.005 0.387
0.105
0.000
0.004
0.013
F!
0.002
0.000
0.000
0.000
•.i-1:2. r.....
20.70
0.59
3.93
26.51
0.02
8.22
13.72
V
1.91
0.00
0.008
0.000
0.002
0.005
0.055
0.000
0.011
0.011
0.018
0.000
0.003
0.005
3.739
0.001
1,759
1.109
24.84
0.05
2.54
1.46
Bamude
. Bennuda
Bermuda
"Br>nfuda
R or13-27
Rye
gye
..
13.
.
0.05
0.07
Total
1,901,234
Annual Ibafacre
C'unent Cumulative Ibdacre
PrlorYears Cumulative Midas
PermittC.P.L10*6
0.016
0.014
3.751
0.123
0.002
0.014
0.078
0.026
6.607
28.89
25.12 1
48.48
Lime AVID.
0.08
0,08
5.46
0.21
0.00
0.08
0.16
0.09
11.06
196
50
Permit PAN Lilt lst/2ad Crot
Date
Lbs/A c.
0.06
0.06
L71
0.08
0.00
0.06
0.08 1
0.06
4.45
36
34
1,338
267
IS
n/a
374 1
89 1
2,498
'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalti fo b ' ng false information, Including the possibility of fines and imprisonment for knowing violations.,
X 2 r?- ^/ -
!Application Method: S - Surface. IN - Injection. INC - Incorporation
(Signature of Land Applier) Date "Volatilization Rate' Surf 0 5 I
Surface
. , .Jectaoa/Inwrporation- 1.0
••'C.P.L.R.: Cumulative Pollutant Loading Rate
Bold denotes application that was Injected
SBME, Inc.
DENR FORM FSF(12/2006) Mod.
FIELD APPLICATION SUMMARIES
Coastal Farms and Residuals, LLC
Permit # WQ0034806
2014 Field Application Summary
SOURCE: Town of Carolina Beach WWTP
FIELD NO. AW-1 AVV-2 AW-3 AW4
JB-1 JB-2 CPC-1 CPC-2
CB-1 CFC-1 CFC-2 AS-1 WC-1
NET ACRES 13.90 21.50 16.90 5.90
28.90 59.30 71.80 55.40
11.80 81.90 72.80 70.20 93.40
SITE, Wooten Wooten Wooten Wooten
Rnrnc Rnms ('.nrhett Panlcina' Cnrhett P-1rina
Cnrhrtt Rroth— Cnrhett v—;na rnrhett P—ina RA--, W ('. A—ff
January
...............................
February
March
April
i
May
June
..........
384,750
t............July
�.
222;750
August
. ...............................
September
...............................
October
November
...............................
202,500
December
303,750
Total
-
-
-
-
-
-
-
-
-
-
-
1,113,750
Soybeans
Com
Wheat
Rye
Bermuda
-------------
SOURCE: MOTSU
FIELD NO. AW-i AW-2 AW-3 AW4
NET ACRES 13.90 .21.50 16.90 5.90
SITE Wooten Wooten Wooten Wooten
Coastal Farms and Residuals, LLC
Permit # WQ0034806
2014 Field Application Summary
JB-1 JB-2 CPC-1 CPC-2 CB-1 CFC-1 CFC-2 AS-1 WC-1
28.90 59.30 71.80 55.40 11.80 81.90 72.80 70.20 93.40
Roma Rnmc r —hatt Pa Arina c:,tt...., nr n,._t.....
January
1 ...............................
o
February
March
............................
April
..............................
May
June
July
August
.................................
September
...............................
October
p ...............................
9,984
November
December
Total
9,984
Soybeans
Corn
Wheat
Rye
Bermuda
-------------
SOURCE: North Topsail WWTF
FIELD NO. AW-1 AW-2 AW-3 AW4 JB-1
NET ACRES 13.90 21.50 16.90 5.90 28.90
STTR Wooten Wooten Wooten Wooten Bums
Coastal Farms and Residuals, LLC
Permit # WQ0034806
2014 Field Application Summary
JB-2 CPC-1 CPC-2 CB-1 CFC-1 CFC-2 AS-1 WC-1
59.30 71.80 55.40 11.80 81.90 72.80 70.20 93.40
Bums CorbettPacking Corbett Packing CorbettBrothers CnrbettFarming Corbett Farming Sidhury W Corbett
January
...............................
February
18,000
...........................
March
30,000
April
18,000
...........................
May
36,000
...........
June
...........................
July
36,000
..........
1 August
36,000
................................
September
...............................
October
24,000
November
24,000
...........................
December
Total
222,000
Soybeans
Corn
Wheat
Rye
Bermuda
-------------
-------------
SOURCE: Surf City
FIELD NO. AW-1 AW-2 AW-3 AW4
NET ACRES 13.90 21.50 16.90 5.90
SITE Wooten Wooten Wooten Wooten
Coastal Farms and Residuals, LLC
Permit # WQ0034806
2014 Field Application Summary
JB-1 JB-2 CPC-1 CPC-2 CB-1 CFC-1 CFC-2
28.90 59.30 71.80 55.40 11.80 81.90 72.80
Bums Bums Corbett Packing Corbett Packing Corbett Brothers Corbett Farming Corbett Farming
AS-1
70.20
Sidbury
WC-1
93.40
W. Corbett
January
151,000
February
March
t.........-April .
May
June
-
............................
July....
�......
August
September
188,500
...............................
October
...............................
November
December
216,000
Total
-
-
-
-
-
-
-
-
-
-
-
-
555,500
Soybeans
Corn
Wheat
Rye
Bermuda
SOIL ANALYSIS REPORTS
Page 1 of 1
Report Number: 15-027-0509
Account Number:45819
Send To: S&ME (1588)
MARTIN MABE
3718 OLD BATTLEGROUND RD
GREENSBORO NC 27410-2314
�L
WWW.aleaderd C0111
Date Received: 01/27/2015 Date Of Analysis: 01/28/2015
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
Grower: Submitted By: MARTIN MABE
COASTAL FARMS Farm ID:
JOB#1588-09-054
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Of Report: 01/28/2015
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
ENR
% Rate
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
lbs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
P H
Index
meq/100g
meq/100g
AS-1
46 M
110 H
52 M
263
L
16 VL
11664
3.5 M 114
4.7
6.72
2.1
4.2
NC=38
NC=56
WC-1
1 VH
64 L
M
M
L
11665
2.2 L 89
181
1
1
156
1464
122
1
5.9
6.87
0.6
3.7
NC=676
NC=33
Percent
Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
Field ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
Cl
Al
0/6
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
AS-1
32 H
2.4 M
2 VL
330
VH
0.9 M
0.7 M
6.7
10.3
31.3
1.7
50.0
NC=67
INC=60.0
NC=13
I
I NC=45.0
WC-1
H
VH
19 M
VH
VH
L
4.4
12.6
62.7
2.6
17.0
127
123.9
1391
116.2
10.4
NC=56
NC=597.5
1 NC=119
NC=810.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: P`
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Paudc McGroary
It should be noted that the majority of residuals land applied under NCDENR Permit No.
WQ0034806 achieve pathogen reduction and vector attraction reduction requirements through
alkaline stabilization. Therefore, the material being land applied is adding lime through most of the
land application events. It should also be noted that the Wilber Corbett — Field 1 has a predominant
soil series of Autryville loamy sand that is strongly acid by nature. Achieving a pH of 6.0 on this site
by the addition of liming material is nearly impossible due to the predominant soil series and the
leaching of the liming material through the loamy sand material throughout the soil profile. The pH of
5.9 on Wilber Corbett's — Field 1 (WC-1) is well suited for the growth of the common bermuda hay
crop overseeded with ryegrass.
au--2�L 4.4-4
Martin Mabe
Agronomist/Project Manager