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HomeMy WebLinkAboutWQ0034513_Residual Annual Report 2014_20150218WP � 3 C5 014 ANNUAL REPORT LAND APPLICATION PROGRAM COUNTY OF BRUNSWICK PUBLIC UTILITIES PERMIT #WQ0034513 Compiled By: Bio-Green Services, Inc. 383 Potts Road Advance, NC 27006 January 2015 FFR 18 /015 January 1, 2015 NCDENR-DWR 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Information Processing Unit Reference: 2014 LAND APPLICATION ANNUAL REPORT County of Brunswick Public Utilities Permit No. WQ0034513 Non -Discharge Compliance Unit: Bio-Green Services, Inc. (Bio-Green) is submitting all monitoring and reporting-:equirements as specified in the above referenced permit. Bio-Green compiled this report using data gathered during the compliance year by Bio-Green and the County of Brunswick Public Utilities. This data includes: 1) Certification Form required by permit 2) Residuals Analysis and Pathogen/Wctor data 3) Application Summary 4) Soil Analysis If there is any further information required or questions regarding this annual report please do not hesitate, to contact Bio-Green for further assistance. Sincerely, Ray Gambill NC Land Application/Residuals Operator c� January 1, 2015 EPA Region 7 ATTN: BIOSOLIDS CENTER WWPD /WENF 11201 Renner Boulevard Lenexa, Kansas 66219 Reference: 2014 LAND APPLICATION ANNUAL REPORT County of Brunswick Public Utilities, North Carolina Permit No. WQ0034513 Bio-Green Services, Inc. (Bio-Green) is submitting all monitoring and reporting requirements as specified in the above referenced permit. Bio-Green compiled this report using data gathered during the compliance year by Bio-Green and the County of Brunswick Public Utilities. This data includes: 1) Certification Form required by permit 2) Residuals Analysis and Pathogen/Vector Data 3) Application Summary 4) Soil Analysis The County of Brunswick Public Utilities conducted application events in Brunswick County within the year of 2014. During 2014, A total of 134.77 Dry Metric Tons of residuals solids were land applied. (Carolina Shores WWTP land applied 18.85 Dry Metric Tons, Sea Trail WWTP land applied 7.93 Dry Metric Tons, Ocean Ridge Plantation WWTP land applied 4.73 Dry Metric Tons. West Brunswick WWTP applied 103.26). If there is any further information required or questions regarding this annual report please do not hesitate to contact Bio-Green for further assistance. Sincerely, %lam ,ram-w�i Ray Gambill NC Land Application/Residuals Operator County of Brunswick Public Utilities PO Box 249 Bolivia, North Carolina 28422 910-253-2659 r- CAROLINA SHORES WWTP NPDES# NCO044873 ? SEA TRAIL WWTP NPDES# WQ0012748 f OCEAN RIDGE PLANTATION WWTP NPDES# WQ0011614 WEST BRUNSWICK REGIONAL WWTP NPDES WQ0023693 NC PERMIT # WQ0034513 Mr. Donald Dixon Water Reclamation System Superintendent PO BOX 249 Bolivia, NC 28422 910 253-2485 I "' LAND APPLIERS: Bio-Green Services, Inc. 383 Potts Road ( Advance, North Carolina 27006 2014 Carolina Shores WWTP Dry Tons 20.78 2014 Sea 'Nail WWTP Dry Tons 8.74 2014 Ocean Ridge Plantation WWTP Dry Tons 5.21 2014 West Brunswick Regional WWTP Dry Tons 113.85 Total Dry Tons 148.58 2014 Carolina Shores WWTP Dry Metric Tons 18.85 2014 Sea Trail WWTP Dry Metric Tons 7.93 2014 Ocean Ridge Plantation WWTP Dry Metric Tons 4.73 2014 West Brunswick Regional WWTP Dry Metric Tons 103.26 Total Metric Tons 134.77 TABLE OF CONTENTS SECTION NO. I II III IV TITLE Certification Form Residuals Analysis & Pathogen / Vector Attraction Data Application Summary and Field Loading Rate Report Soil Analysis 0 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) n ,Facility Name: County of Brunswick Utilities WQ•Permit Number: WQ0034513 WWTP Name: Carolina Shores WWTP NPDES Number: NC0044873 Monitoring- Period: - . From 1/1/2014 To 12/31/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative nerfnrmed: Class A: Alternative.1 ❑ Alternative 2 ❑ - Alternative 3 ❑ Alternative 4 ❑ Alternative 5 Alternative 6 El T7 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens"; Compost `. ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Rd ❑ Gamma Ray ❑ Pasteurization Class B: : 'Alternative 1 ❑ Alternative 2 If applicable to alternative performed Class B onl ) indicate."Process to Significantly Reduce Pathogens": Lime Stabilization ❑. Air Drying[] Com ostin I Aerobic. Digestion ❑ Anaero rc Digestion es ron = If'applicable to ''alternative performed Class A or Class B complete the following monitoring data: Parameter. Allowable Level, in SW,d a Pathogen Density Number o Excee- ences. Frequency of Analysis Y ' Sample T e Y� a,ytica Tech - Mini Geo. Mean aximu Units Units Fecal Colifofm 2 x 10 to the.MPN 6th power, per gram of total solids CFU 100.0 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) tT_ 3 MPN per'4 grams totai solid (dry weight) vector ,muracnon Keauctron (4U U K 5U3.33) - Please indicate o tion erformed: Alt.1 (VS reduction) ❑" Alt. 2 (40-day bench) . ❑ JAI. 3 (30-day bench) JAlt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ® Alt. 6 (Alk Stabilization ❑ JAlt.7. (Drying - Stable) ❑ JAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were perfortned ❑ CERTIFICATION STATEMENT (please check the appropriate statement) P "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Prepaper Name and Title (type or print) Signaturejqt Preparer* lac I JJ__v Q Land Appher Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) S Brunswwck County Lime Stabilization Ph Test Results Hauler: B104REEN Services, Inc. Sludge Source: ' ^ !-�=� ___ WWTP Permit #:ie4 `2Approximate Gallons: O , Initial Ph Test Date_ f1 Time 1-4- i a_ ia#�t Ph 1.3 Temp Temperature Corrected Ph - -- - Z Hoar Pit Test )ate A/dl)[A Time �� Operator Temp Temp Corrected Ph l Z • 86 ._----------_. 24 Dour Ph Test---�------_.� Time _12 Operator Ph.. _�'Z - TexnP Temp Corrected Ph 2 ' SEEDS, FEEDS, HARDWARE I` FERTILIZERS, CHEMICALS BRUNSWICK FARM SUPPLY 3546 WHITEVILLE RD. N.W. ASH, N.C. 28420 PHONE (910) 287-6343 OR 6329 DATE 2!)-Lg-- CUSTOMER NUMBER SOLD TO �,{� A) CASH CHARGE ON ACCOUNT I MDSE.RETD. I MEMO I DELIVERED I SOLD BY v 9 REGISTER VALIDATION QUANTITY 'DESCRIPTION PRICE AMOUNT Grd / lJ h,4 � OYA� TOTAL PI EASE KFFP THI.4 INVnle rTe')0 (-Wl:e kgfde CTATCAACNT ACCOUNTS 30 DAYS PAST DUE SUBJECT TO 1112 % PER MONTH INTEREST �W602 df. 11 D C 1BrU' sw1idk Cou hty Lime Stabilintioni Ph Feet Reeu Ns "auler: 810-GREEN Seirvkas, Inc. Sludge Source: C Perinit #: C 44d-A�'13 _ ; . APpZmdrzu►ate Cidlons: Q , Initial Ph Test Date ry� _"Z �A1. T60 t3perator _ - -..L__.- , . ,.. Ph Tel"p, Temperature C'osrected Ph 12. 13 2 Hour Ph Test Date Temp Corrected P 24 Maur Ph Test.....-------------.- ; Time opemor Temp Corrected Ph �i L ru-n9wick county n ph Test ROSUMB U Mg StabilizatIO ' Hauler: IBI04REEN Services, Inc W. SjUdge Source: App.r�mate (AlOW. Permit 0: Inifig, Pb Test OpeMtDf Date Time Ternp,-7A: TemparatuM Colrected Ph tz 2 lJour Ph Test. Date Time 1-21.97 'Ope rator Ph Iremp --A -+F:- ,r . 1 .. emp Corrected Ph our Pb Test F! Time operator Date Temp Corrected ® SEEDS, FEEDS, HARDWARE ® ® FERTILIZERS, CHEMICALS ® o r BRUNSWICK FARM SUPPLY 3546 WHITEVILLE RD. N.W. ASH, N.C. 28420 PHONE (910) 287-6343 OR 6329 �j DATE / 20 CUSTOMER NUMBER SOLD TO 'K' 0 CASH CHARGE ON ACCOUNT I MDSE. RET'D. I MEMO I DELIVERED SOLD BY REGISTER VALIDATION C� d- QUANTITY DESCRIPTION PRICE . AMOUNT /a s TOTAL I'LtAJt Kttl' IHIS IIVVUII.t I-Uk I.HtUK]Nkh JV-11tIVItIVI ACCOUNTS 30 DAYS PAST DUE SUBJECT TO 1 1 /2 % PER MONTH INTEREST RECEIVED �y BY G REG iRA0Et.41RNR !NA CD ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0034513 County: -Brunswick Year: 2014 Facility Name (as shown on permit): County of Brunswick Utilities Land Application Operator: Bio-Green Services, Inc. Phone: 336-813-8063 Land application of residuals as allowed by the permit occurred during the past calendar year? ❑ Yes _ ❑ No - If No, skip Part A, and Part B and proceed to Part.C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of a lication fields in the ermit: :18 Total number of fields utilized for land application during the year: 9 Total amount of dry tons applied during the year for all application sites: 13.561 Total number of acres utilizes for land application during the year: 102.1 L ? Part'B Annual Comuiance Statement: Facility was,compliant during calendar year 2014. with all conditions of the land application permit (including but not limited to items 1-13 below) issued, by the Division of Water Resources. r5l Yes ❑ No If no please, provide a written description why the facility was, not compliant, the dates, and explain corrective action taken: 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified_ in the permit and lime was, applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the.permit.. . 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant " - Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All, general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T . I I I 1 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. '—� Part C - Certification: "I certify, under penalty of law, that the above information is, to the of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for sul5mittin't false information, including the -' possibility of fines and imprisonment for knowing violations." ` j Zr'Tt'i'ry P, / �7 /PrCP X/'eCIOr 0� L Permi ee-Name qncf Title (type or print) Signatue f i ee Date 1/1/2015 Signature of P eparer* Date Siinatt&& Land Ape plier — Date (if different from Permittee) (if different from Permittee and Preparer) * Prenarer is defined in 40 C°FR Part50I.9-(r)and 1.5A NCAC; 02T .1102 (26) DENR FORM ACF (12/2006) CAROLINA SHORES WWTP ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed:. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0034513 Laboratory:_, - 1) .Environmental Chemists - Facility Name: County of Brunswik Utilities 2) Residual Source WQ # or NC0044873 3) NPDES #: 4) WWTP Name: Carolina Shores 5) Residual Analvsis Data Parameter (mg/kg)(mg/kg Conc. Limit a Sample or: Composite Date 1 /8/2014 Percent Solids (%) NA 1.47 Arsenic 75 6.74 Cadmium 85 6.74 Copper 4,300 149 Chromium NA 10.1 Lead 840 11 Mercury 57 0.68 Molybdenum 75 6.74 Nickel 420 8.1 Selenium 100 6.74 Zinc 7,500 353 Total Phosphorus NA 12300 TKN NA 76300 Ammonia -Nitrogen NA 1080 Nitrate and Nitrite NA 5 33 " For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. - "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assur ualified personnel properly gathered and evaluated the information -submitted.' I am aware that there are significant penal es for bmitti f formation; including the possibility of fines and imprisonment for knowing violations." 1/l/2015 Sign at f P p r Date *Preoarer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) COUNTY. OF:BRUNSWICK PUBLIC UTILITIES.LAND APPLICATION PROGRAM - RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 8, 2014 Carolina Shores WWTP Mineralization rate 0.30 1.47 % Solids u 7.24 pH Permit No. NCO044873 PPM k °% *1 000 ...::. _. .. LW _.. Tori-_ M' .. `""0: 02 PAN 23699 47.398 TKN. 76300 152.6 Ammonia Nitrogen'(Am) 1080 2.16 Nitrate Nitrogen (Nin) 593 1.186 Organic Nitrogen (Orn) 0.002 Total Phosphorus (P) 12300 24.6 Total Phosphate (P205) " 0.002 Estimated, Avail. P205 `. 0.002 Total Potassium(K) 3360 . - 6.72 Total Potash (K20) 0.002 Arsenic (As) 6.74 0.01348 Cadmium (Cd) 6.74 0.01348 Chromium (Cr) 10.1 0.0202 Copper(Cu) 149 0.298 Lead (Pb) 11 0.022 Mercury (Hg) 0.68 0.00136 Molybdenum (Mo) 6.74 0.01348 Nickel (Ni) 8.1 0.0162 Selenium'(Se) 6.74 0.01348 Zinc (Zn) 353 0.706 Aluminum (AI) 1920 '3.84 Calcium (Ca) 22200 44.4 Iron (Fe), 0.002 Sodium (Na) 3560 7.12 Sulfur (S) 0.002 Magnesium (Mg) 1480 2.96 Manganese (Mn) 0.002 Environmental Chemists, Inc. 2014-00290 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N)+ Ammonia N + Nitrate N +Nitrate N - % PAN Surface Application, (Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N) + Nitrate N +Nitrate N - % PAN Note: Constituents N.D. (Not Detected) or < Detection limits are listed as detection limits for calculation purposes.. 6500 load .398 lb per load=11.310 Ib PAN per load 4500 load .275 lb per load=13.074 lb PAN per load i QffICIot 00410-M3 FA7[81 M HCC6NR: DWC CGXAI2C1►IWN #9# NCiJHHB: USC IGAlnOU#3fJP,'{# ii j Enio®��Ylto��nmlalcfiatnt �ocn Comments.. !-B&*f —s;Ly c !7r a I 'u44 ; - ; - -T 1 OUP[®: _—.. . b1/ 1 //'Lb14 by: b / `jlt75 /`1'J 3'L UHKULINM anURea rHvr ULI 1L Envko'nmental Chemists, Inc 6602 windmill 'Way • Wtlwtngtm SIC 28405 • (910) 392.J= (Lab) 1* (910) M 4424 (Pax) - ® 710 ftwsertowa Road • Manteo, NC 27954 (752) 4iW702 ANALYTICAL A CONSULTING NCow m. DWQ CERTIFICATE 694 ULS CB=KCATS 46"D WWI= Brunswick County Public Utilities Data of Repot: Feb 13, Z014 — Post Office Box ?.49 Customer PO t#: Bolivia NC 28422 Report* 2014-00290 Attention: Donald Dixon Reportto: Donald Dixon Projeat ID: Carolina Shores Chlorobenzene Sw840MOM OzeO=" < 0.01 mg/L 1129/2 4 Chloroform sWegBMeueoae2aorsoso < 0.01 mg/L 11295 14 Methyl ethyl ketone swe4aMelhodersOrsoao < 0.05mgIL 1/29/; 114 Tehachloroethyllene s"naKeM°u`°"s�°�sosn < 0.01 mgIL 11291% 114 Trichloroemylene 3w84eeWeuwd$2sas0ao < 0.01 mg1L 1/294o 114 -1 Vinyl Chloride swe4eMau�easxe0isoso < 0.01 mgm 1129C i 14 ' RCI Cyanide M=4 <0,118 mglkg 01/31 !)14 pH rM 4500 H 0 7.24 units 01110 ! 314 Sulfide SM 45W S D .0.239 mglkg 02103 ! 314 ignilabilityr SWO40 resthW 1010 :�212 °F 01114 : D14 Sludge Residuals Aluminum EPAM.7 1920 mg/kg 01/24 ; 014 Arsenic EPA 200.7 <6.74 mglkg 01/2e 014 Cadmium EPA200.7 46.74 mgft 010 ;014 Calcium EPA 200.7 =00 mg" 01 /2( ; 014 Chromium EPA 200.7 10.1 mg/kg 01125 ;014 Copper EPA200.7 149 mg/kg 01/2: ; 014 Lead EPA 200.7 11,0 mglkg 01125 ;014 _ Magnesium EPA2W.7 1480 mg/kg 01)2l :014 Molybdenum CPA 200.7 <6.74 mglkg 011Z; ;.014 Nickel VA 200.7 8.10 mgikg 01 J2; :.014 Potassium EPA200a 3380 mglkg 01121 ::014 —j Selenium EPAW.7 .46.74mg/kg 01/Z ::014 _ Sodfum EPA2W.7 3580 mglkg 01/21 '!014 Zinc EPA2W.7 353 mg/kg 0210 :!014 Ammonia Nitrogen EPA 350.1 1080 mg/kg 01/11 :'014 Total Kjeldahl Nitrogen (TKN) EPA ast.a 76300 mg/kg 01121 ".!014 - J Nftrate+Nftrite-Nitrogen EPA 9ss.2 693 mg/kg 02M, '!014 wwm� RaPW*, 20144DOM Pape3d 02/1I/2014 09:07 910579532J UAKULINA SHUKLb Environmental Chemists, Inn , 66o2 Windmill Way • WilminSton, NC 28405 i (910) 392,= (Lob) • (910) 392 4424 (Fax) -- 710 Bowsertown Road • Macteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDLt - DWQ CtE1.i RCATS #94, VW(TIUMCATE 413M Brunswick County Public Utilltles ®ate of Report: Feb 13, 2014 Post Office Sox 249 customer PO #: -- Bolivia NO 28422, Report #: 201400290 Attention: Donald Dixon Report to: Donald Dixon - Project ID:. Carolina Shores Total Solids (%) SM Zs�o 8 1.47 % 01 /10 ! )14 - " Total Phosphorus sew far) P P 12300 rrtglkg 01121 ! )14 mercury SWN6747% 0.6600 mglkg 01/17 014 TCL.P Metals Arsenic EPA 2O .7 <0.100 mg1L 02103 ! 314 Barium EPA 200.7 <0.100 mg1L 02101 ? 314 Cadmium EPA 200.7 <0.100 rng1L 02/0:: 014 Chromium EPA 200.7 <0.100 mg/L , 02/02 : D14 Lead EPA 200.7 <0.100 mg1L 02/0: : 014 Selenium EPA200.7 <0.100 mg/L 020% 1014 i Silver EPA200.7 <0.100 mg/L 02/0' 1014 -- Mercury EPA2as•t <0.002 rng1l- 01/21' 014 Comment Sludge res+divals reported on a,dry weight basis. RCI repotted on an as received basis. L Reviewed by: M�1� (i & 06 1 _ i L RepM *-' 2014-0290 �a0e e p ••••�•' 02/17/2014 0y:0/ '�105tyJbJZJ UAKULINA bHUNtb. rain Uii14 Environmental Chemists.) In(, 6602 Windmill way • Wilmlflgton, NC 28405 s (910) 392.0223,(T-ab) " (910) 392-447A (.Fax) 710 BowM rbown Road - Mantm, NC 27954 (2%) 473.5702 ANALYTICAL 8 CDNSUt.71NG NCDBM. DWQ CEIi!INCATE 094. DLS CMFICATO rFVM C14EMIWM Brunswick County Public UtHltIGS Date of Report: Feb 13, 2014. Post Office Box 249 Customer PO M Bolivia NC 2a422 Report #: 2014-6.0290 Attention: Donald Dixon Report to: Donald Dixon Project ID: Carolina Shores Lab ID Sample ID: Collect patefrime Illlatrlx . Sampled by 14-00659 Site: Sludge TCLP 1/8/2014 9:62 AM Solid/Sludge S. Leonard & I Cool ; in Test Method Results Date Ant I zed Chlordane SW eq6 Nathan e081819510 <0.005 mq/L 0123 914 Endrin swa40M~1199180510 <0.00005 mg/L 01/23 ! 314 Heptachlor swe�sr noeeot er3s�o . <0.00006Mg/L' 01/23 ,!014 Heptachlor epoxide 5091 10 -400005 mg/L 0112: ; D14 Undane yweleMaihod>laeleraslo <0.00005rng/L 0112.:D14 Methoxychlor sw ens method eoelewo <0.00005 mg/L 0112%1 D14 Toxaphene swe48nMMdOW'1813510 <0.005 mg/L 01/2; :014 1,4431chlorobenzene (TCLP) 'r'oo1°d 70e510 .40.050 mg/L 0112. ; 014 2,4,5-Trichiomphenol (OLP) ews"M"GWo4610 40.050 mg/L 01/2 ; 014 2,4,6-Trichlorophenol (TCLP) o <0.050 mg/L 01/21 :014 2A-Dinitnotoluene (TCLP) ^ems arasao <0.050 mg/L Ojai ;,.014 Cresol (TCLP) swetsmemloee�r0rasle ; <0.050 mg/L D112 :!014 Hexachloro-1,3-butadlene (TCLP) swaeem�nodez�oraslo cD.050mg/L 01/2: ; :014 Hexachlorlobenzene (TCLP) <0.050 mg/L 0112:: 1.014 Mexachlomethane (TCLP) sw e4s melnad szraraslo <0.050 mg/L 0112: :,014 m f p-Cresol (TCLP) SWIMI "EMO10 c(t.050 mgll 0112 ; ;014 N twbenxene (TCLP) SIN ets nleslad OrM01110 <0.050 mg/L 01/2 ' !014 o-Cresol(TCLP) sw946Method a2'iws3lo <0.050mg/l. 01/2 1!014. Pentachlorophenol (TCLP) SW 840 0MftW 8770M10 <0.250 mg/L 0112 " !014 Pyridine (TCLP) SW M.. ei . 02701WIC <0.050 mg/L 01 /2 ' !014 2,4,5-TP SVIMe"B161A <0.0003m9lL 0112 11014 2,4-Q SMOMewrod®1s1A <0.6003 mg/l. 0112 11014 - 1,1-Dlchloroethylene Mon Me" 8260r5030 < 0.01 mg/L 1/29 ! )14 1,2-Dlchlomethane SWV45 Mv° 82=5WO < 0.01 mg1L 1129 ! 314 Benzene ' SW846 Method SMUSM 4 0.01 mg/L 1/29 ! 714 Carbon Tetrachloride' swe46 MOM 82OM30 t 0.01 MA 1/29 : 314 Repoli ft 2014.00M) Poo 2 0 I i SEEDS, FEEDS, HARDWARE FERTILIZERS, .CHEMICALS i BRUNSWICK FARM SUPPLY J '3846 WHITEVILLE RD. N.W. ASH, N,C. 28420 -I PHONE (910) 287-6343 OR,6329 DATE -I& 2-7 20-J - ! CUSTOMER NUMBER SOLD TO 1910 �.� ADDRESS CASH CHARGE ON ACCOUNT MDSE. RET'D. MEMO DELIVERED SOLD BY REGISTER VALIDATION „rTT QUANTITY DESCRIPTION PRICE AMOUNT kG `tci�-e TOTAL PLEASE KEEP THIS INVOICE FOR CHECKING STATEMENT ACCOUNTS 30 DAYS PAST DUE SUBJECT TO 1 1/2 % PER MONTH INTEREST RECEIV BY t� ° REG TRADEMARK RALSTON PURWAGO. t I l I i ® SEEDS, FEEDS, HARDWARE FERTILIZERS, CHEMICALS BRUNSWICK FARM SUPPLY i 1 3546 WHITEVILLE RD. N.W. ASH, N.C. 28420 PHONE (910) 287-6343 OR 6329 DATE_ 20 CUSTOMER NUMBER SOLD TO ! D ADDRESS CASH CHARGE ON ACCOUNT NIDSE. RETD. MEK40 D5LIVERED SOLD BY. REGISTER VALIDATION QUANTITY DESCRIPTION PRICE., AMOUNT., 37 8eal- ``ol TOTAL r �cna❑ n¢r i - - ACCOUNTS 30 DAYS PAST DUE SUBJECT TO 1 1 J2 % PER MONTH INTEREST RYCEIVED`/� ,�7���� f // 'REGTRADEWURALSTONPURWACO. -, Brunswick County Lime Stabilization Ph `hest Results _ Hauler: 0104REEN Services., Inc. Sagdge Source: ( A A Q ` �i P ,Permit #: w t1C� _ Approidmaite Gallons:. c3Q0 _- _ Iaiti 'Pest Date Time operator _ Ph 1�-• 1� Temp Temperature Corrected Ph 1"�-•?Z 2 Haug Ph. Test Date I ottl 'rime _e LI S __ Q1PMktor _C _ F romp Ph Temp Corrected Ph . 24 Maur Ph Test----------�-��---- ()ate �'ixne operator T OMP Temp Corrected Ph _ { j Brunswick County Lire Stabilization Ph Test Ult� Hauler. w4REEN Services, Inc. Sledge Source: :Permit #: 1�L _ ,A.pprbodmate Odlow._ v � .initial Ph Tes Date �t -2p,4 Time _9 O rotor .C. w' _r - Ph • 1-Al Temp 2�� v Temperature Corrected Ph i� •2( ___,_ 2 Hour Ph Ted - -- Date (p ! Time a — -.��_� .�.�1 ��.__ Operator „uc�.._.._ Pla Temp 'c Temp Corrected Ph 24 Hour Ph Test Date Time _ Operator I'll I __ 'F emp Corrected Ph Brunswick COUntY bili=00n Ph TOSt Ftesuits r LIMG StN 13,04REEN Sam, Inc. aular WWTP S He lad Soure, Al)proldmat, .Permit L I n itiai Ph Tes Time C"ralo, Dfitel� Temp emp Corrected Ph T 2 flour Ph Test 'Date A42f2b* 'rime Opaawr ph z.2 TeMP .Comp Corrected Ph a. Test Time operatorc—AA I-emp C ,Orreded Ph smnswick Count.Y . UMO Stabili2glon Ph Test RQs #5 Haunter: BIO-GIkEEN sOrvices,1 , WWTP Sludgy ounce: c :Permit:AC-OQ �' _PPnr�axe �niti Test: Timb J4.&!A Opumar - - Date . v �.... n� 1 � • v Tsuap , 2. - Temperature CoUected - — -- Ho or Ph 'hest . `Time 12 r%ow-%_ Opelrator C - Ph r ,Mp Corrected 24 Hour Ph Test - -- -- - � - --- ---- bate .�9} Thile Operator •P,Mp Corrected -Ph 1 Brunswick County, Lime Stabilization Ph- Test Results Hauler 1310-GREEN Services, Ino. Sludge Source. Permit#: Appro4mate Wons, initial Oji—Test Date Operator Ph- 17-.65 Temp Tempemure Covected Ph 2 Hour Ph Test 'Date3h420-4 Time or r. ...... Operat TMp Corrected Ph &,Z - - -------- Time Opamtor I'MPCOrrested ph____ Brunswick County UMO Stabilization Ph Test Resin Hauler 3104REEN . Imo. Permit #: �1 �.Q — �"-� � -- .. �PprMnr��� Initial.Ph Test Time Tempertom ConeeNd.- 2 Hour Ph Test 1311 Temp, a. 2- '1'emp Correded Oat $ -' �? The _f _.opera r - - _- em �- Br ihawick County Lime Stabilization'Ph `Feat Rnu fts Neuter. 310413REEN ftrw1cm, Inc. �- Sludge Source: WWT LOermit A roximae C oms.• , - Znifial Ph Test • - ; :Usk Time T . ___- 7T Temp ._1a-�.__ _ Temperature CDff ctedPh-------12'444__--..-___�_.._. 2 flour ph'I'leo �at+s 1�--14_Z�Zt 'rime +pcff_ Pig ..__. k -- __. `camp Tomp Corrmted Ph r 24 Hour Ph "rest __...__�... _. Time Temp Cn+�re Y ..-------�Z-S5- —... -• ® SEEDS, FEEDS, HARDWARE FERTILIZERS, CHEMICALS 0 0 ' BRUNSWICK FARM SUPPLY 3546 WHITEVILLE RD. N.W. ASH, N.C. 28420 PHONE (910) 287-6343'OR 6329 DAT �`] 20- CUSTOMER NUMBER ADDRESS I CASH CHARGE ON ACCOUNT MDSE. RET'D. MEMO DELIVERED SOLD BY REGISTER VALIDATION QUANTITY DESCRIPTION PRICE AMOUNT �• v 10 TOTAL rLrMOt Kttr InIJ 11VVCA4t VUH L HtGKING SIAItMLNI ACCOUNTS 30 DAYS PAST DUE SUBJECT TO 1 1 /2 % PER MONTH INTEREST RECEIVED BY .R-1WEMARK RALSTON PIIRINACO, 25393 L P L F-' [-I A. Brunswick County Urne Stabilintion Ph Test Rejulft Hifuler: 01"REEN Servicals, Inc. Sludge Source:, ww'rp Permit Approximate Gallons: Initial -Ph Vest Date 0.p Time =wr Tbmpemur6 Corrected Ph 7 2 :our Ph Test 'I)ate AZ--t 4=t.4 "rime 1 220 Operator p" TeMp Corrected Ph -I 24 Hour Ph Test Ante 12- L-LA Time r i Operator rr,,P-- erne C-bfrectedPh____ -;A JAA--131 r, Brunswick County Lime Stabilization Ph Test Results Hauler: 81043REEN Services, Inc. Sludge Source 'Perink 4ppro eA Inifiw A Date te Time Operator,. Ph Temp 1Z Temperature Corrected Ph 17, 4---s 2 :our Ph Test Date 1'2- 1 Le rime 1Z_4.75 Operator Ph Temp Corrected Ph­ 24 Hour Ph Test Date- =-14 Time Operator -C rr,,p Vemp Corrected Ph .6. SEA TRAIL WWTP l ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: W00034513 Laboratory: 1) Facility Name: County of Brunswik Utilities - 2) Residual Source WQ # or NCO012748 3) NPDES #: 4) WWTP Name: Sea Trail S7 -Environmental Chemists Parameter (mg/kg) Cone. Limit m /k a Sample or Composite Date 1/8/2014 Percent Solids (%) NA 1.07 Arsenic 75 8.6 Cadmium 85 8.6 Copper 4,300 106 Chromium NA 12.1 Lead 840 10 Mercury 57 0.654 Molybdenum 75 8.6 _ Nickel 420 8.6 Selenium 100 8.6 Zinc 7,500 236 Total Phosphorus NA 3170 TKN NA 37300 Ammonia -Nitrogen NA 1420 Nitrate and Nitrite _ NA 25 For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. 66I certify, un r penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed, to as a that q alified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pe alties fors m' t' I information, including the possibility of fines and imprisonment for knowing violations." 1/1/2015 Signat e o P eparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .1.102 (26) COUNTY 05 BRUNSWICK..PUBLIC .UTILITIES: LAND'APPLI RESIDUALS ANALYSIS i Residual Type: Wastewater Treatment Plant 1_J Date Sampled: January 8, 2014 Sea Trail WWTP Mineralization rate 0.30 1.07% Solids 7.25 pH I i L� )N.PROGRAM... -..: Permit No. NCO044873 P m Ik °e." 10 00 ='::.. LbsiDrvTon` muika-." 0.0021'` PAN, 11499 22.99$ TKN 37300 74.6 Ammonia Nitrogen (Am) 1420 2.84 Nitrate Nitrogen (Nin) 25 .. 0.05 Organic Nitrogen (Orn) 0 0 Total Phosphorus (P) 3170 6.34 Total Phosphate (P205) 0 0 Estimated Avail. 0205 0.002 Total Potassium (K) 3070 6.14 Total Potash (K20) 0 0 Arsenic (As) 8.6 0.0172 Cadmium (Cd) 8.6 0.0172 Chromium (Cr) 12.1 0.0242 Copper (Cu) 106 0.212 Lead (Pb) 10 0.02 Mercury (Hg) 0.654 - 0.001308 Molybdenum (Mo) 8.6 0.0172 Nickel (Ni) 8.6 0.0172 Selenium (Se) 8.6 0.0172 Zinc (Zn) 236 0.472 Aluminum (Al) 2040 4.08 Calcium (Ca) 17900 35.8 Iron (Fe) 0 0 Sodium (Na) 5040 10.08 Sulfur (S) 0 0 Magnesium (Mg) 2580i 5.16 Manganese (Mn) 0 0 t:wronmentai Cnemists, Inc. 1U14-UUZ9U *Determination of Plant,Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N)+ Ammonia N + Nitrate N +Nitrate N - % PAN Surface Application (Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N) + Nitrate N +Nitrate N - % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. 6500 load .290 lb per load = 6.669 lb PAN per load 4500 load .200 lb per load = 4.617 ib PAN per load " 31 rangy Sw RAR O.,� _ ` Wilmington, NC A, Sample Collet#ion and Chain of Custody Phone: (9�oi 342-aZ�3 � Fax (910).3914424 Sawgiee: = e t E = fl1u L W — ellS =Cream NU M-3 a PRESERVATION sampleIdeatifscation Collection -11 a . ANtsMIS IMQIMTED DATE THE TEMl2' SIL c G y i C F -- G G -/-' c �.�G..Ttt�rfl,C.2 G C G St-- G ` C Y G G C P G G C I P -G I G G G c. P G G C P iY(}T1CL — DECf3iORiNA1'fO�T : Samples far Ammonia,:T`KN,' C` antde, Phenok and Bacteria must be dedgerinated a2 m or iess in the field at the time of colleetion. See reverse side for instructions. Transfer Reiingntshed BY: Date/Time Received : DateMme - - s 1. -e-x0+ -� Temperature eceived: v e ecs c��.., ,y .�`.t" ccep : �3 V i �� . - Comments: ;Ei a D 02/17/2014 09: 07 9105795323 CAROLINA SHORES PAGE 10/12 Environmental.Chemists, Inf 6602 Windmill way - Wnmingtm NC 26405 (910) 392-OW (Lob) o (910) 3924424 (Pax) 710 Bowm town Road 9 Mmteo, NC 27954 (252) 473-5702 ANALYTICAL & OONSULTING CHEW= WcDEM. 0WQ CEMFICATF, "0, J)LS C I nWICATE #37729 Brunswick County Public Utilities Date of Report: Feb 10, 2014 Post office Box 249 Customer PO Bolivia NC 28422 Report ft 2014-=91 Attention:. Donald Dixon Report to, 'aid Dixon it). sea Tray ocean Ridge Project Chlorobenzene Ww"s Mel* 62001mm is 0.01 mg/L 1/29f. :14 Chloroformsuve�sMeviode2eosoao-c 0.01 mgfL 11291., :14 Methyl ethyl ketonesnreas roes < 0-06 mg/L 1/291, Tetrac hioroethylene swa4azardhoas2soesoao< 0.01 mg/L 1)29/ :14 Trichloro . Lethylene SWO48 Whad 8200030 --c 0.01. mg/L 1291 :14 Vinyl Chloride swiss meow qewsma < 0.01 mg/L .11291 14 Cyanide EPA335A <0.1 18 Mg/kg .0113' :014 Sulfide im -45W S 1) 0.55 mglkg 0210.' ;.014 Ignitability SW 046 fnethCd 1010 >212 OF 0.1114'::014 Sludge Residuals Aluminum EPA2W.7 2040 mglkg 01/2, :,.014 Arsenic EPA200.7 <8.60Mg*g 01a ; 1,0 14 Cadmium EPA 200.7 <8.60 mg/kg 01r2: '!014 Callum EPA2M.7 17900 rngft 01/2 :!014 Chromium EPA200.7 12.1 mg/kg 0112. :!014 Copper EPA M.7 106 mg/kg 01/2: '!014 Lead EPA*.7 10.0 mg/kg 01/2; 1014 Magnesium EPA2007 2580 nV/kq_ 01/2 '!014 Molybdenum EPA200.7 <8.60 mgft 0112 11014 Nickel EPA200.7 <8.60 mg/kg 0112 1,1014 Potassium EPA200'7 3070 mglkg 01/2 '!014 Selenium EPA 200.7 <8.60 mglkg 012 1!014 Sodium WAM7 5040 mg/kg 0112 0014 Zino EPA= 235mg/kg 0210 11014 Ammonia Nitrogen EPA 350.1 1420 mpg 01/1 Q014 Total Kjoldahl Nitrogen (TKN) EPA351.2 37300 mg/kg 01/2. 1!014 Nitrate+N[trite-Nitrogen EPA3932 25.0 mglkg 02/0 1 W14 Total solids (%) SM2W0B 1.07% 0111 1 !014 Rep""": 2014-OMI Panels I 02/17/2014 09:07 9105795323 CAROLINA SHORES HAVE 11/11 Envi rm enter. Chem. ists, In1 6M Wincircmill way + Wilmington, NC 28405 (9'tQ) 392-OW (Lab) ® (910) 3922-"24 (FaX) 710 Dow3 rtown Road • Manteo, NC 27954 (252) 473 570Z ANALYTICAL A CONSUMNG NICDEMI nWQ C13RTI - CATE 094. M C81,i17FICATG #37729 CMEMiSTS Srunmwick County Public Utilities Date of Report Feb 10, 20.14 Post Office Box 249 .. Customer PO 0: Milvia NC 28422 Report#: 2014-00291 Attention; Donald Dixon Report to: Donpld Dixon Project IDSea : Trail /Ocean Ridge 01i10 ! D14 PH SM 460 H9 7.25 units Total Phosphorus SM4600PF 3170 mgikg 01121 D14 mercury su 4®�47,s 0.6540mg1kg 01/11 :D14 TCLP.Metals Arsenic EPA 200a <0.100 mg/L 02/0:: 014 Barium EPA VO.7 <0.100 mg/L 02/01 ; 01,4 Cadmium SPA20.7 <0.100 mg/L 02/0: ; 014 Chromium EPA 20 .7 40.100 mg/L 02/0; ; 014 Lead ePa zoo.7 <0.100 mg/L 02/0; 414 Selenium EPA200.7 <0.100 mg/L 0210. ; ;014 Silver EPA200.7 <0.106 mg/l. 02/0, ;1.014 Mercury HPAWA 0.00SO mg/L 01/2: ; ;014 Report S.': 201400201 Page 3 9 1 02/17/2014 09: 07 91bb l9bJ2J UANUL1NA bMUKtb rfAuc CJ 71 1L i Environmental Chemists, Ino .. ( 6602 Windmill Way - Wibhnvlgton, NC 28405 T I(j (910) 392- rm (Lab) - (910) 392-"24 (Pax) I_ ® 710 Bovi M town Road - Ma nteo. NC 27954 (252) 473.5702 ANALYTICAL & CONSUL7INQ NCDENR1 nWQ CERTIFICATEM94. DL9 CgFi77FIG12b dr377Z9 CHE1Nt97S Brunswick County Public U6110ee Date Of Report Feb 10, 2014 Past Office Box 249 Customer PO #: Bolivia NC 28422 Report d: 2014-00291 Attention: Donald Dixon Report to: --'DQnald Dixon - Project iD: f / ocean Ridge Irab IQ Sample 1 . Son Trail collect DateMme Matrix Sampled by `- 14600660 Site: SiudN 1/8/2014 9:32 AM Solid/Sludge Aaron Hewett Test Mettiood Results Date Am -heed i.� Chlordane SWh3t8Mettiode081®►0s10 r0.005mgIL 01/22 :314 Endrin sw ea®eanrnod s0e1er3510 . <0.00005 mglL 01122 !014 Heptachlor SW 046 Method 8061SM10 <0.00005 mg/L 01 /2s ; 014 Heptachlor epoxide sW848method 806181d510 <0.00005 mglL 0112.: 014 Ondane sw e4e nhl�mar oval slo <0,00005 mg/L 0112; ;014 Methoxychlor S1N e48 MBU O M OM510 <0.00005 mg/L 0100 ; 014 Toxaphene SW OM Mettmd s08187 M <0.005 mg/L 01 /24 ; 014 I.4-Dichlombenzene (TCLP) sw e" meOW eMM510 <0.050 mg1L 01121 ;.014 2,4,5-Trlchlorophenol (TCLP) SW 940 msaad0270/3519 <0.050 mg/L 01M. ;.014 2,4,6-Trichfomphenol (TCLP) SW 846 method 82TW510 <0.050 mg/L 0112'. ::014 2,4.UMMi tpluene (TCLP) SW MG moth°° 8=13510 <0.050 mg/L 0112. A14 Cresol (TCLP)SW eea ffmU d 02MW10 <0.050 mg/L 0112:: ;014 Hexachl=4,3-buladiene (TCLP) sw 040 h1h°nhod 82r wiO <0.050 mg/L 0112: ::014 Hexachlarobenzene (TCLP) sw $40 merh°d 82 M610 <0.050 mg/L 01 /2:::014 I` Hexachlomethane (TCLP) SW we "1 mw Ovori610 <0A50 mg/L OW ".!014 In + p-Cresol (TCLP) SW OO MW0 827=10 <0.050 "IL 01 /2,' :1014 ( N11mbenzene (TCLP) sw a" ntedied 827013510 <0.050 mg/L 01122 '!014 aCresol (TCLP) swvsmemod8270f3510 <0.050 mg/L 01/2 1!014 Pentachloraphenol (TCLP) sw040 meumd UvW610 <0.250 mg/L 0112 '!014 Pyridine (TCLP) SW 848 meMod 87=510 <0.050 mg/L 01 /2 1'.014 2,4,5 TP SW84®a+aplodelslA <0.0003Mg& 0112 ' a014 2.4-D SyV°4eMewhod 8151A 40.0003 mg/L 01/2 ' t014 1,1-Dichlomethylene SWO40 Mevpd SWUM -c 0.01 mglL 1129 ! )14 1,2-Dichiamethane �- 0.01 mg/L 1129 ! )14 v Benzene SWUS Mehod em < 0.01 mglL 1129 114 Carbon Tetrachloride swe4$ M AUd 6280rsm < 0.01 m9/1. 1/29 1)14 Repoli ft 2014-MO1 Pope 1 0 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name:. County of Brunswick Utilities WQ Permit Number: WQ0034513 WWTP Name: Sea Trail WWTP NPDES Number: WQ0012748 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved'and alternative. performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 L'� Alternative 6 If applicable to alternative performed (Class A only) indicate `Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alterhative.l ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization, ❑ Air Drying❑ Composting ❑ Aerobic Digestion ❑ Ana erobi c Di t' es ion g - If a licable to alternative perfo,rwed Class A or Class B complete the followin monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number oil Excee- encesy Frequency of Analysis Sample Type Analytical Tech - nioue inimu Geo-Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids WN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt I (VS reduction) ❑ Alt. 2 (40-day bench) 'I ❑ Alt. 3 (30-day bench) JAlt. 4 (Spec. (:; uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑' Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) 1 "This determination has been made under my direction and supervision in accordance with the system J designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are isignificant penalties for false certification including fine and imprisonment." J Preparer Name and Title (type or print) Land A fiWr Name and Title (if applicable)(type or print) CSignature Preparer* Date Signature Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) J DENR FORM PVRF 503 (12/2006) ('yj 13m nswick County Urne Stebuintion Ph Ted Resin Haular: W"REEN SOMIC"s loc. sjase fie: Sep T L P-' WWTIP Permit 0: ApmximM WOW- 5�-- imittial Ph Test Date3 -f j Teams .11 }mad _ OPW&w * 19 Ph .13 . (, S TOV 13 Temperer Corrected Ph _ 13 . Lf I 2 Sour Ph Test Daft TM'-- Operalor Tom—. Temp Corrected Ph 1'3.. $ 9 ----.�-- 24 Sour Ph Test --.-.- i Time Operator Temp Corrected Ph r r% I Brunswick County LiMG Stabill tion Ph 'Test Resulm Hsulur: INO.[3REEN Smhms,10C. ,Sludge : Sep Ana ; .L. Z �-��"� viwm ,Appmximm won$: Initial Ph Ted Dare 1'f _� Thu _ � Q " 2 Hour Phi Teo Date 3 ^ q—)-Lj Tim O Opwatm Pu ��x .5 73 .__, `rem I 1 Tamp Conwm Ph 7.. `'-- - U Hour Ph Test._— - JDste der- )� rime air TeMp Co rJrecW Ph �1 -� Eve SEEDS, FEEDS, HARDWARE FERTILIZERS, CHEMICALS CBRUNSWICK FARM SUPPLY.. . 350 WHITEVILLE RD. NA' ASH, N.C. 28420 . PHONE (910) 28748343 OR 6M DATE3-t r 20jT CUSTOMER NUMBER i SOLDTO A�8 { ADDRESS L' CASH CHARGE DNACMW MDSE REPO. MEMO DELIVERED SM BY REGISTER VALIDATION QUANTITY DESCRIPTION PRICE AMOUNT OL TOTAL PLEASE KEEP THIS INVOICE FOR aiL Qt MAT MW0 ACCOUNTS 30 DAYS PAST DUE SUEUE-M70 1 I /2 % PM-MON M INTEREST RECE VED BY - •xEawusroxe�ca 223, griaeswkk County Limp iljWWon Ph Tnt Rift Ir: sv, W.• WWTp AVMWuvde GAW. 3 0 Initial Ph Test l tom— �', 2 Houl s Ph Tat Ph ) -4,TOMP S. Temp CmTeded Ph I -, . 3 CC) U Hour Ph 'hest - I l4°-7,a�5`Time O �?t o Cp rc lPh. � 1 1 �Q � Two S - TMV Cad Ph Brunswick County Urnn Sib,1l1xatIo. n Pb- T4wt W%+W*ults Neuler; 81Q�3R�EM Sorvlcas, �. Sludge Soum: �� �. =r� : _ L P�,o4,.rt� _ 2WWTp Permit #: ,A,ppraWMM GOODS. ial A Test Date S - 133 Time I `i� OpeflitW . Ct �- 'Pit ,IF),.,G -0--- Temp Terre CosrecW lit i 2 Hour Ph Test Date _ Y-13-1ply rim OPMUM Ph 'Z, Temp _i Temp Corrected ]Ph i 1 '�, 5 Co _ � ----- 24 hoar Ph Test------.- Dee s.� ) y Mime ILIQQ Opavw a . - - ph 9 '1, , p TMp S -7 - Ternp co, t Pb 1 % " 0 �' Brunswick County Lime Stabilization Ph Test Results Hauler 010-GREEN Services, IM Sludge Source: 2S e ol�, -r n-*.: f- WWTP 4 r Perrrnit #: 5- 4 00 d C? C2-1 '' Approximate Wow Initial Ph rest .Date _6 -17 -lo t -�E Time a. p o o Operator %4 H two Temp '1.b ► -3 Temperature Corrected Ph I '), 2 Hour Ph Test Date G v3,-7 Time Temp let., 3 Temp Correeted Ph 24 Hour Ph Test - - Date g-7,� l� Time o Y -Od operator f'emp Corrected Ph _ll177 :7 I. L_` BrubsWlck County Line Stabilization Phi Test results Hauler. 810-3REEN ,ServIces,1nc. Sludge source: SC ci. '7�i�a : L L �_ -� _ - WWTP Perraait #: 0 Approximate melons:.- I 7� D 2) 0 ^. Initial Ph 'hest Date _(Q )! 7-lo I y Time � _ Operator pjjp -g-_ Ph _ j 'l- .1.'i Temp ')$ , 3 Temperature Corrected Ph 1 117 2 .Tour Ph Zest Date (a__'1.7 -3.ui�t Ph _i�,��-------- 'Temp Temp Corrected Ph __ 1� g L 24 Maur Ph Test------_—___-- - -- Tate A`_1L-x-O-w Time p 1 3 p Operator - - Ph. I_I -)--1 temp Corrected Ph _ 1. , 3 p Brunswick County LIM9 ftbllfttlon Ph TeM Resufts WO -GREEN sorvic"o Inc., Sludge Soww. Seaw L L -ftnk VVI M Permit _oQ 117H S AppWmale Od.low. Ov C-) Inifild: It Teo. Date- Time O"Iftf A 0 'Pit, 11. Temp 19 Tempmam ConWf4 It. .-J I HOTAN. IFIk T"t Daft _1!:_XQ -Itq ly no* 1 OpM%W A ff pit TMp Temp Corvaded Ph Li ---O� 24 Hour Ph Opmtor tWIT IrMp Temp comxftdPh-AI I-u---, qa PWMIIKYadLU., �0 `t I qa POPWOO duwl ~---� _=%ado ca LL qa"Oft r Of OIL- t alloa =L `fit-T� a5 "*Ur 688rnu" Nuav I11'n"N WJL yid uopezltllqmS owi'7 XiunaJ j1*IN►sunjg 1 SEEDS, FEEDS, HARDWARE FERTILIZERS, CHEMICALS 0 0 ,BRUNSWICK FARM SUPPLY 3546 WHITEVILLE RD. N.W. ASH, N.C..28420 PHONE (910) 287-6343 OR 6329 4- DATE s r (O 20 j CUSTOMER NUMBER ,_aOLD TO% CASH CHARGE DNACCOUNT MDSE. RET'D. MEMO I DELIVERED jSOLD BY f REGISTER VALIDATION QUANTITY DESCRIPTION PRICE AMOUNT 3 TOTAL ­aC n¢r irna irvvviL r rIJK l NtA.KINC�J I A ItMtlVl ACCOUNTS 30 DAYS PAST DUE SUBJECT TO 1 1 /2 % PER MONTH INTEREST RECEIVED BY -REG TRADEMARK RALSMN PURINACO. 25397 539 7 �aP F Brunswo It bounty Lime Stabilization P.h Vest Results Hauler. B10-GRE. EN Services., Inc. Sludge Soutdc . S C n L P A - vt_"�� _ _=- WWTP Permit #: �► _ Approximate Gallons: Initial Ph Vest Date _l, 7 : �1� Time CCU Nam_ Operator _ - Ph Temp 3 .L{ C Temperature Corrected Ph' 2 J 2 Hour Ph Feat 'Tate 7 -)-0 r y Time f (� �. S� _ Operator � I� P11- Temp, Temp Corrected Ph ._-�—V .------_-------- 24 dour Ph Test---�----- ---- lasts )�--I �-Zot Time ©m'sJ operator r • v Z ��. _ . `remp ) 3 • s-- 1'emp Corrected Ph /,2.o� F� �'4 Lee,✓ O�,ve0L c��� Brunswick County Lime Stabilization Phi Vest Results Hauler: 810-GREEN Services, Inc. Slndge Source: "'t A-_ ' L_-L _ - .:._. WWTP Permit #: ln% CEO I 1 -7 Approximate Gallons: �__---- Initial Ph 'hest .Tate _� a��� � Time C)� Operator.__A Ph-) 7 'L Temp Temperature Corrected Ph 2 Hour Ph Test Date j _), -) 7 -)_o j LA Time _ Operator __ jj 6 Ph _l� ' & ) - Temp Temp Corrected Ph. --------- 24 dour Ph Test---------Y--- l �'-'�� 0 S30S' - Operator _L late 1��. Tinne Vemp Corrected. Ph ri OCEAN RIDGE PLANTATION WWTP - -- -- --' j ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: W00034513 Laboratory: 1) Environmental Chemists Facility Name: County of Brunswik Utilities 2) Residual Source WQ # or WQ0011614 3) NPDES #: 4) WWTP Name: Ocean Ridge 5) 7?noifl ■.ol A nnwcie r►n*n - Parameter (mg/kg)(Mg/kga Cone. Limit Sample or Composite Date 1/8/2014 Percent Solids_ (%) NA 0.95 Arsenic 75 8.84 Cadmium 85 8.84 Copper 4,300 82.7 Chromium NA 8.84 Lead 840 14.6 Mercury 57 0.421 Molybdenum 75 8.84 Nickel 420 8.84 Selenium. 100 8.84 Zinc 7,500 207 Total Phosphorus NA 12200 TKN NA 49800 Ammonia -Nitrogen NA 2440 Nitrate and Nitrite NA 509 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or:supervision in accordance with a system designed to assure that allied perso el properly gathered and evaluated the information submitted. I am aware that there are significant penalties r subm' tin i fgrmation, including the possibility of fines and imprisonment'for knowing violations:" 1/1/2015 Signature of r e * Date *Preparer is defined. 40 CFR Part 503.9(r) and I5A NCAC 2T .1102 (26) COUNTY OF BRUNSWICK PUBLIC UTILITIES LAND APPLICA - RESIDUALS ANALYSIS -- Residual Type: wastewater Treatment. Plant Date Sampled: January 8, 2014 Ocean Ridge WWTP Permit No. NCO044873 Mineralization rate 0.30 0.95 % Solids - 7.52 off Par, meter•. % PPM m /k % M0 0 0 . LbslDrvTon ' MKst * 0002) PAN 15937 31.874 TKN 49800 99.6 Ammonia Nitrogen (Am) 2440 4.88 Nitrate Nitrogen (Nin) 509 1.018 Organic Nitrogen (Orn) 0 0 Total Phosphorus (P) 12200 24.4 Total Phosphate (P205) 0 0 Estimated Avail. P205 0 0 Total Potassium (K) 3660 7.32 Total Potash (K20) 0 0 Arsenic (As) 8.84 0.01768 Cadmium (Cd) 8.84 0.01768 Chromium (Cr) 8.84 0.01768 Copper (Cu) 82.7 0.1654 Lead (Pb) 14.6 0.0292 Mercury (Hg) 0.421 0.000842 Molybdenum (Mo) 8.84 0.01768 Nickel (Ni) 8.84 0.01768 Selenium (Se) 8.84 0.01768 Zinc (Zn) 207 0.414 Aluminum (AI) 914 1.828 Calcium (Ca) 9470 18.94 Iron (Fe) 0 0 Sodium (Na) 5610 11.22 Sulfur (S) 0 0 Magnesium (Mg) 3400 6.8 Manganese NO 0 0 environmental Chemists, Inc. 2014-00290 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N)+ Ammonia N + Nitrate N +Nitrate N - % PAN Surface Application (Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N) + Nitrate N +Nitrate N - % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. 6500 load .794 lb per load = 25.313 Ib PAN per load 4500 toad .549 lb per load=17.524 Ib PAN per load 1 �r Wi1®ingtsn, N� 28405 Sample Coflf&don an___d C_-h_lin of LAtadv - Phaw. (9LQJ.392-U3)3 Tier 10181 347_dd2d ,J .a ►i11't!Q _ `L��.1'�.'7+�f_���Ll+1S�Ta - Mir "of, f one MEMO 111"010FAN MEN IN 718"m 4 KCA" ME ONE Ii ONE a,csaucapspic iv>t� '�A:Tiil4lii i9ti:�•*+'f+w1a. •' - - i�cL� i--'G�wmYac gy{;sa. :cat �Jt!!t>rti� �a irk �_' �.�..�..........J . «� _,,,�� � - ��� .• Comments: S°L Yi►rLi L • — `7� �. as 02/17/2014 09:07 9105795323 CAROLINA SHORES PAGE 06/12 Environmental Chemists, ln( 6602 WiindmM Way - WihnbWon, NC 28405 (910) 392.0223 (tab) - (911D) 3924424 (Fax) 710 Howmtown Road • Manteo, NC 27954 (232) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIPICAM 04. DU CERTII-ICATE N37729 Brunswick County Public Utilities Datwof Report; Feb 10, 2014 Post Office Box 249 Customer PO: Boilvie , NC 28422 Report * 2014-00291 Attention: Donald Dixon Report to: 0onai Dixon_ Project ID; Sea Trailrgcean Ridge Chlorobenxene SWWMalMd92=503.0 < 0.01 mq/L 1/29/: 114 Chloroform SW046 WhOd 826015030 < 0.01 mg/L 1/2915 114 Methyl Ethyl ketone swims 14erhpd820015080 < 0.05 mg/L IJ29/: 114 Tetrachloroethylene swage Net wd 82ea403o < 0,01 mg/L 1/294 114 Trichlomethylene SWO40 MdW 9260 030 < 0.01. mglL 11294 114 Vinyl Chloride SWO46 NCtW 82901503D < 0.01 mg/L 1129A 114 RCI Cyanide EPA3354 <6.131 mgJkg 01/31.: 114 Sulfide SM 4500 S ° 1.25 mg/kq 02103, .114 Ignitability sw 040 meM1010 >212 OF 01/14' . )14 Sludge Residuals Aluminum EPA200.7 914 mglkg 01/24 :114 Arsenic EPA200.7 <8.84mg/kq 01/22 .114 Cadmium EPA zoos <8.84 mg/kq, 01122 .114 Calcium EPA200.7 9470 mg/kq 01/20, 114 Chromium EPA 200.7 <8.84 mglkg 01122 114 Copper EPA 200.7 82.7 mglkg 01J22 -1114 Lead EPA200.7 14.6 mglkg 01/22 -114 Magnesium EPA 200.7 3400mglkg 0112Q 1114 Molybdenum EPA NO.? `8.84 mglkg 01/22, 1114 Nickel EPA 200.7 <8.84 mglkg 011221 1114 Potassium EPA200.7 3550 mglkg . 01/20 1114 Selenium EPA 2001 <8.84 mg/kq 011241 1114 Sodium EPA 200.7 5610 mglkg 01 /20) 1114 Zinc EPA 200.7 207 mglkg 021041 1114 Ammonia Nitrogen EPA=.1 2440mglkg 011151 114 Total Kieldahl Nitrogen (TKN) EPA061.2 49800 mg/kg 011201 1,14 Nitrate+Nitrite-Nitrogen EPA 953.2 609 mglkq 02/031 1,14 Total Solids SM25409 0.95% 01/101 114 Report *;: 201+00291 Parma 6 "Is 02/17/2014 09:07 9105795323 CAROLINA SHORES PAGE 07/12 Environmental Chemists, Inc em windmill Way • V1fi MWgWn, NC 28405 • (93.0) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Howsertown Road • Mameo, NC 27954 • (292) 473-5702 ANALYTICAL & CONSULTING NCDEM DWQ CEKnRCATE 094• DL9 CERTIFlCA'TE u37929 CHEMISTS Brunswick County Public Utilities Date of Report Feb 10, 2014 Post Once Box 248 Customer PO #: Bolivia NC 28422 Report M 2014-00291 Attention: Donald Dixon Report to: Donald -Dixon -- Project m_ ID: Sea Trail (0ean Ridge pH SM.4500 H a 6.94 units 01 /10l i 114 Total Phosphorus 4500P F 12200 mglkg 01121i 1114 Mercury SWO"1471B <0.421 mglkq 01/171 ., 114 TCLP McMis A rsenic rsen'I EPA20oa <0,100 mglL 02/0a ,114 Barium 5PA200.7 .0.100mg1L 02101, .114 Cadmium SPA200.7 40.100 mg/I.. 02/03 A14 Chromium SPA200.7 <0.100 rrlg/L )14 02103.114 Lead EPAzoO.? . <0.100 mg/L 02103 .)14 Selenium EPA202.7 <0.100 mg/L 02103 ! )14 Silver EPA200.7 0,0.100 mg/L 02101 114 Mercury EPA245.1 <0.002 mg/L 01/23 014 Comment: Sludge Residuals reported on a dry weight basis. pH and RCI reported on an as received basis. • - �n-' - ►- � - .c Reviewed by: L� Repart�k: 20t400291 Pope$ of I' 02/ 17/ 2014 09: 07 910b /Jb323 kANULINA bMU►tt5 resat rJoi 1 Environ exatal Chemists, Inc 6= Windmill Way Wilmington, NC 28405 1 (910) 392-0123 (l.ab) + (910) 3924424 (FOX) 710 Bowsextown Road - Manteo, NC 27954 (252) 473.5702 ANALYITCAL & CON$11LTiN43 NCDE NR: DWQ C6tiT1FiCATB �1n DLS Ct3ti'McA?8 �FVM CHEMISTS _ BrunwWok County Public Utilltles Post Office Box 249 Bolivia NC 284222 Attention: Donald Dixon Lab ID Sample lk- 1400661 Site: Sludge Date of Report: Feb 10, 2014 Customer PC #: Report#: 2014430291 Report to: Donald Dixpri Project ID: Sea Tray`% Ooean Ridge Collect DateITime Matrix Sampled by 1/8/2014 9:12 AM SolidlSiudge Aaron Hewett Test Method Results Date Ana iced Chlordane SIN640 MOW eoaI W510 <0.005 mgfL 011231 1114 Endrin swea8n odeosltvaslo {0.00005 mg/1. 011231 114 Heptachlor sw"aMead atltllt 6510 <0.00005 mgfL 01/231 114 Heptachlor epoxide Sw+das ^'+eho° eaetelssl° <0.00005 mglL 0112S .114 Undane �"' a t d 7e 'o 40.00005 mg/L 01123 114 Methoxychlor 0 4.00005mg/L 01123 .)14 7oxaphene sw e4s Meo+od e0®1ttl8510 <0.005 mg/L - 01123, : )14 1,4-Dichicrobenxene (TCLP) SW 840 MOVIodl exrWW10 <0,050 mglL 01 /23 !)14 2,4,5 Trichlorophenol (TCLP) swims mofhod 02MOSI° 41.050 mg/L 01123 !)14 2,4,6-Trichlorophenol (TCLP) sw eea mv�nod ezroras+° <O.650 mg/L 01123 114 2,4-Dinftrotoluene (TCLP) <0.050 mg/L 01/23 !)14 Cresol (TCLP) sw B48 °1O0d 8UM10 <0.050 mg/L 01123 :114 Hexachloro-1,3-butadiene (TCLP) ' sw w ffwv o B2"mslo - 0.060 mgIL 01122 ! 314 Hexachicrobenzene (TCLP) swmemenmdezmasi0 <0.050 mgiL 01123 !)14 Hexechloraethane (TCLP) We" Method ®x7M510 <0,050 mg/L 01123 114 m + p-Creel (TCLP) sw e46 mead 827 S40 <0.050 mg/L 01123 ! 314 Nitrobenzene (TCLP) SW6411 MW10d e$7M3s10 <0.060 mg/L 01129 ' Y14 o-Cresol (TCLP) SW 845 metnad ez70=10 <0.050 mg/L 01123 ! D14 Pentachlomphenol (TCLP) sw a40 method ezr°r4510 N.250 mg/L 01123 :D14 Pyridine (TCLP) SW 84e MOO Od W01351° <0.050 mg/L 01122 ! D14 2,4,5-TP SMO Method B751A =0.0003 mg/L 01129 : 014 2,4-0 SVN646 Method 2151A -0.0003 mg/L 01121 ; D14 1,1-Dichlvroethylene Swe4e MOUNd =01613" < 0.01 ntg1L 1/29C :14 1,2-Dichloroethene swe4e M" Gomm < 0.01 mgfL 11291'. :14 Benzene SW846 MOMM * < 0.01 mg/L 11291, ;14 Carbon Tetrachloride sweaetod ezeau5oa0 < 0.01 mg/L 1/291.:14 M. Reportr► , 2014-002911 Page 4 d ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) i Facility Name: County of Brunswick Utilities WQ Permit Number:. WQ0034513 WWTP Name: Ocean Ridge WWTP NPDES Number: WQ0011614 Monitoring Period:.. From 1/1/2014 To '12/31/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 E3, Alternative 5, ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Rayas ❑ Pasteurization ' rtzation ❑ , Class B: Alternative 1 ❑ Alternative 2 ❑ :...:....:.::..:.,-:::............:..:...:....:......... . . If applicable to alternative performed (Class B only) tndicate "Process to Significantly Reduce Pathogens": Lirne.Stabilization [3 Air Air Drying C6m osting . ❑ . JAerobic Digestion ❑ Ana erob' rc Drg s ' e tron If a licable to alternative peiformed Class A or Class B) complete the following monitod g data: . Parameter Allowable Level in in Sludge Pathogen Density Number o Excee- � Frequency of Analysis y Sample Type $ ytica Tech - nimu Geo. Mean aximu Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliforni) 3 MPNper 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ® Alt. 2 (40-day bench) ❑ Alt.- 3 (30-day bench) ❑ Alt. 4 (Spec: O, uptake) Alt. S (14-Day Aerobic) ® Alta 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) 0 JAIt. S (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met " (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment. Preparer Name and Title (type or print) Land App'er Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) I. l �T' Applier (if applicable) Date DENR FORM PVRF 503 (12/2006) Bru,nsw1ck County_ Le Sts►bjjjti►on Ph Tost ROSU is Hauleir. B"REEN Sorvicea, Inc. - Sedge SOUM: A,ppxo4MM Giftfka: Initial Ph Test 3-1 Time �. Ph t Tempure Corrected Ph 13 -3 4 2 Hong Ph Ted u Ph r-7------ `ram _ i`f •. �- . Temp Corrected Ph 7 L. 24 Hour Phi 'hest ])ate - 5- Time 0 190 o .� pemor _ Ph `renlp Temp Corrected Ph Of CO Bm niswick County Lime Stabilization Phi Test Resuft Hauler: 3104REEN Bervims,1nc. fihWge Source: ® C a: o f WVM i of � I I G IT- Approsimu Wons: �9oe�6 InAfid 1% Test Fete7,1-7.o r y Time Cz.p.S�Owator 0 Ph _11,11-Is Temp (., $ Tempemwe COMW Ph 11, 13 (2 2 Hour Ph Test - Date TimmyOpauor - Ph _ ) X., 0 1 ----- Taw .47, o -- Temp Conwed Ph 1 0 7 24 Hour Ph TWt Date 9 2's -)-o, y Time 0 f s o r'ernp �f temp corn ed Pin 1117 6 SEEDS, FEEDS, HARDWARE FERTILIZERS, CHEMICALS BRUNSWICK FARM SUPPLY 3546 WHITEVILLE RD. N.W. ASH, N.C. 28420 PHONE (910) 287-6343 OR 6329 DATE 20 CUSTOMER NUMBER SOLDTO ADDRESS CASH CHARGE ON ACCOUNT MDSE. RErm MEMO REGISTER VALIDATION SOLD By ACCOUNTS 30 DAYS PAST DUE SUBJECT TO 11/2 % PER MONTH INTEREST RECEIVED BY -REGYRADEUARK RAI STON ROAM 2 2 3 "17 L.� ,.r-; a SEEDS, FEEDS, HARDWARE vimFERTILIZERS, CHEMICALS BRUNSWICK FARM SUPPLY _ 3546 WHITEVILLE RD. N.W. ASH, N.C. 28420 - PHONE (910) 287-6343 OR 6329 DATE 20� CUSTOMER NUMBER SOLDTO CASH CHARGE I ON ACCOUNT I MDSE. RET'D. I MEMO DELIVERED I SOLD BY REGISTER VALIDATION QUANTITY DESCRIPTION PRICE" AMOUNT Ali TOTAL YLtAJt KttY INIZ, IIVVUK.t t-UH UltUKI111l� JIAItIVItIVI ACCOUNTS 30 DAYS PAST DUE SUBJECT TO 1 1 /2 % PER MONTH INTEREST RECEIVE�� BY -REG TRADEMARK RALSTON FURINACO. ® ® SEEDS, FEEDS, HARDWARE FERTILIZERS, CHEMICALS ® o BRUNSWICK FARM SUPPLY 3546 WHITEVILLE RD. N.W. ASH, N.C. 28420 PHONE-(910) 287-6343 OR 6329 DATE L�1 G 20-1-�— CUSTOMER NUMBER SOLD TO��d AllUKtSJ CASH CHARGIE ONACCOUNT MDSE.RETD_ MEMO DELIVERED SOLD BY REGISTER VALIDATION ACCOUNTS 30 DAYS PAST DUE SUBJECT TO 1 112 % PER MONTH INTERL5I RECEIVED BY ° REGTRADEMARK RALSTON PURINA CO. WEST BRUNSWICK WWTP 1, 1 ANNUAL RESIDUAL. SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed.. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0023693 . Facility Name: County Of Brunswick Utilities Residual.Source WQ # or NC0086819 NPDES #: WWTP Name: West Brunswick Laboratory: 1) Environmental Chemists Inc. 2) 3) 4) 5) 1<VuaY 4Nl L-YfMa Parameter (mg/kg) Cone. Limit m a Sample or Composite -Date 4128/14 I1l12/14 - Percent Solids (%) NA 4.08 3.34 Arsenic 75 10.4 2.99 Cadmium 85 2.43 2.99 Copper 4,300 431 518 Chromium NA 18.1 24.1 Lead 840 11.6. 8.74 Mercury 57 0.574 0.449 Molybdenum 75 2.43 8.02 - Nickel 420 17.4 19.2 Selenium 100 6.89 8.32 Zinc 7,500 1290 1820 - Total Phosphorus NA 40300 59300 TKN NA 51700 81600 Ammonia -Nitrogen NA 38800 50300 Nitrate and Nitrite NA 3.68 0.6 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the -individual permit.tor metals iumts. "I certify; under penalty of law, that this document was prepared under my direction or supervision in accordance -with a system designed to assure that qu personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties fors mitti falsq(ation, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer fin__._____ :_ �_r_� :__ •n /1TT T__.a rnn —A __ A . c Date . ... COUNW:OF BRUNSWICK PUBLIC UTIL11 RESIDUALS ANALYSIS - Residual Type: Wastewater Treatment Plant Date Sampled: 28 April, 2014 West WWTP Mineralization rate 0.30 4.08% Solids 8.92 DH 2nd Quarter Permit No. NCO044873 Parameter °k- .: PPM m 1k % *70 000 :,-, :. L Ton M * 0 2 PAN $urfacee 23273 46.546 PAN Injection 42673.68 85.34736 TKN• 51700 103.4 Ammonia Nitrogen (Am) 38800 77,6 Nitrate Nitrogen (Nin) 3.68 0.00736 Organic Nitrogen (Orn) 0 0 Total Phosphorus (P) ' 40300 80.6 Total Phosphate (P205) 0 0 Estimated Avail. P205 0 0 Total Potassium (K) 6100 12.2 Total Potash (K20) 0 0 Arsenic (As) 10.4 0.0208 Cadmium (Cd) 2.43 0.00486 Chromium (Cr) 18.1 0.0362 Copper (Cu) 431 ' 0.862 Lead (Pb) 11.6 0.0232 Mercury (Hg) 0,574 0.001148 Molybdenum (MO) 2.43 0.00486 Nickel (Ni) 17.4 0.0348 Selenium (Se) 6.89 0.01378 Zinc (Zn) 1290 2.58 Aluminum (Al) 46600 93.2 Calcium (Ca) 18600 37.2 Iron (Fe) 0 0 Sodium (Na) 1870 3.74 Sulfur (S) 0 0 Magnesium (Mg) 1 4830 9.66 Manganese (Mn) 1 01 0 Environmental Chemists, Inc. 2014-04874 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N)+ Ammonia N + Nitrate N +Nitrate N - % PAN Surface Application (Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N) + Nitrate N +Nitrate N - % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. 6500 load .794 lb per load = 36.9581b PAN per load Surface / 67.7651nlected - 4500 /oad .549 lb per load = 25.5541b PAN per load $urface 146.8551nJeded Environmental Chemists, l.e® 4 m®r., 6602 Windna+-11 Way - sfiihmng"ron, NC 28403 (910) 342-0223 (Lab) s (910) 392.4424 (Pax) 710 Bois: sertown Road. o %Vlanteo, NC 27954 (252) 4.73 5702 NALNMOAL & CONSULT NG CHEMISTS AiCJENIL BWQ C RUPICA E #94. BLS CERTIFICATE 437729 BrUnstwick Counts nubile U6i;!?€es bats of Report: May 27, 2014 Pcst Office eox 249 'Customer PO #: �c'si t+ia NC28422 Report # : 201-4 "4874 AUents©n: 'Donald Dixon: Report to: Donald Dixon Project ID: Sl NIR Tank Lab is: Sam. pie lD: STAIR Collect Date!Time fiftatix sampled by 14-117 3iudge 4128120 14 11:00 tVA1 Solid/Sludge D€xon ;qAedfin est Method Rlesults Date Analyzed Siud- aRtaA.sldtiiahs ' w inum EPA20C.? 46600 mgikg 0413G+120i/? :senic soy 2c0.? 10. mg/kg 04/29,:2J1�1 6, niurI E?P.2oC.? mg/kg 041�2+9i�2G14 '^v�cS41=.::' i? r�FY 2Qu.Z p3 q<{2�+.4 i VVQLC Tn /:Sg OQ29120 i4 _. `'-c�r.:=I'9: =F '0'z 18. c mgi?cg 04P-912014 Copse, �PA2C4.7 43n irg/kg 04/29/2014 -ad EPA 203.7 11.6 mg/kg ©442912014 Magenesiurn SPA. 203.7 4830 nig/kg 04129/2a'i4 'Rcivbddenum c?�2ea.z <2.43mg/kg 04/2912014 l-c- l ep,20n.z 17.A mg/kg i'V u�ltl:,r6t E:�n .Z'U3.'I 6100 mglkg r0�4�fv2SP9•�j(2]fa�14 04129120 !4 Selenium 203.7 6.89rnglkg 04/2912014 Scd Urn ERA 200.7 ? S,7fl g1'�Cg 0412912014 ?l^c aRk200.749v mgft 04/2912014 A- m-mania Ni4 rge=: ERA 350.1 38800 mgtkg 05108i2J14 ctai 1t1ah-J2t7i N tr gen (s ' ') EPA351.2 51700mg/kg 0$1OW20i4 .. «' :a..`•:V sitar:tl1traga': LPA.353.2 3.58mg/lCg 15/22i2C 4 Solids ;eio: SIM2540 s n.G8'!c 04129120 i4 PH SM 4500 H e 8.92 units 0513h12014 -yi-GiPhosI'horus SW4500PF 403007iigiiCg 05/0$/2014 ;Vse6CE:s''y` SW$4674?iB 0.5740 rng1k 05/107120 1'} Comment: Res:ft% exce.0t PH. rayoi-ted on a dry weight basis. p: ; reported on an as received basis. 01 o , i ,iVPVI? '.: 2O N-C4S74 Page 3 of 3 l COUNTY 01 BRUNSWICK West Brunswick Regional Laboratory Public Utilities Department 235 Grey Water Road Wastowater Treatment Division Supply, NC 28462 ' � r • � `-�� Phone: 910765 7921 pax: 910-756-7927. -.jC•" '' Sample Collection and Chain of Custody ``>;: �! � Collected 13y: a[_(iA) .��.� �--"--__ — _ _ __ Report No. Sample't'ype: l = Influent, E z Effluent, W = Well, ST = Stream, So = Soil, St. = Sludge Other. ANALYSIS Sail►pto Identification Collection sample •type St. Composite or Oral) Container 9 (Plastic or Gass) _ 09orine mg/L 0 LAB ID NUMBER 1 ✓ PRESERVATION REQUESTED DAl E 412812014_ Tt _ :(](� _ l ENiF�' tGK%. �( NONE � HAI ti25t�., flNO3 'ftiiO X Fecal Densl _WBR SDNR Tank Willi _ _ 4Pd012..019 SL C �' fa' o 17 X Fecal Density SCW__ R WBR 412o/?_u14 _ SL LA o t i • V� _ y —_ __„ _ X Fecal Dandy WOR SL 1) �� X Fecal Deit ,r en 4/20/2014 G G MSDNR Tank � � SL Q, a ��6 V X _ Fecal Density 412012014 G _WSR SDHRTank WBR _ SL F _ U d — X _ Fecal Densityw— 412812014 G _ Y SDNR Tankw WBR 5L G a � N 0 1 `7 X Fcmd DenyAy 4120/2014 SDNRTankAt WBR —412812014 St. C9 G 0 � t _ _ _ Residuals .. P _ C_ P _ _ C, P A I TEiN IiON: for AsAf r:unio, TKN, Cyanide, Phenol &md as Bactertolcglcnla must lie dechlolinated to :s 0.2ppn at f6ne ofec:itection. 4 u Ten,per:turro where Rocalmd:�; �� _ a ` 003li�u Rejecfed: Resample Roqu'teci: ............. DeAveraclF3y:�l�.�� t�./::` ✓ L� ? j [�C .... .../ j " (vC_)..._.,....... nvironment + ! 6602 JtmdnO inlay • Wil= ngion, NC 284ra y" a ya (910) 392-0223 (Lab) _ (910) 392-4424 (Pax) 71_0 Bowser town Load a Mant:eo, NC 27954 J , • ;?.i c (42) 473-5702 , AN.4 YTICPL & CONSULTING . CHEMISTS ATCpETR: DbvQ CsE iiFICNI11994. DLS CERTIFICATE 07729 isrunsvvlok County -Public Utilities Post OfficeBox 249 Bolivia NC 28422 Atnton: Donald Dixon Date of Report- May 27, 2014 Customer PC 0: Reporl; #: 2014-04874 Report to: Donald Dixon Project ID: SDNR Tani: ' . Lab 0 Sample 1D: WNR Co'Hcot Date/Time Matrix Saw -pled -by 14-:f3 1lc 'pl Site." 1 428/2014 11:00Air; Solid/Sludge ' Dixon Medlin Test Method Results Date Analyzed T ezi Solids to° sr,� � e s 04/29/2014. =eca1 Density Sal S221c a MPN 24 hr SW <6 MPN/Q 0412914'2014 :.ab i0 Sample ID: 3DNR Collect Datel Time Matrix Sampled by 144 1, 73alLo. 4 2 4128/2014 11:00 AM Solid/Sludge Dixon Medlin Test Method Results Date.Analyzed -�JEc �©iics (elo; sra 2640 a 3.66 % 04/29/2014 -ems! `ei ,sET; - =10 E �3.- M 24 hr SM <6 riffP! ft 04129:2014 =Cis iD Sample 1D: SDNR Collect Date-, I ime Matrix Sampled by E4_J 1738 Site: 43 412812014 1 F:00 AM Solid/Sludge Dixon Medlin. Tact method Results Date Analyzed tal Solids F°f ; Fecal Densiiby Sr,125Qa s $Si sm 1¢ a MtN 24 hr ew 3.46 % <6 MPNfg 04/29.2014 04129=14 Lab io Sample JD: SDNR Collect DatefTime Matrix Sampled by 14 i ? 739 Site: ;= 4 4128=14 1 1:00 . ;M Solld/Sludge Dixon Medlin Tee. Method Results Date Analyzed ctai S©lids took SM 2W S 3.94 % 04/2912014 yacal hers`;; SM, =4EMPN 24hr5M <6IMP iil/CS OQW2014 Lab ID Sa%-npee iD: SDNR eoffect Date/TIm's Matrix Sampled by - 14-1 1 140 Site: 4 e 412$i2014 11:00 AIM Solid/Sludge Dixon Medlin Test Method Results Date Analyzed i owl Solids ;c�°) sr�, 2540 s 3.85 % 04129/2014 - F Gal Density ShA 5221C. E ih?N 24 hr 603 46 WIPl�l/C 04/29/2014 Repay k : VH4 ,4"4 - Page 1 of a Enwrowne .6502 °ylrin&jnj;A'ay • WainingEon, NC 28405 9 1 g i (910) 392-G23 (Lab) + 1911, 0) 392-"24 (rax) 710'Bowsertown Road o Manteo, IC 27954 (252) 473-5702 j -_' ANALYTICAL & CONSULTING CHEMIS S NcDr.-Na. DiSCEI�iIftChTS#?3T789 Sm.tvwick County Publilc Urilitles Date of Report: May 2�, 2014 Past Ot ice Box 249 .re$Stoli9eE' PO #. , r so'.1vie NC 28422 report #: 2014404574 Attention: Donald Dixon Reportto: Donald Dixon Project 1D: SDNR Tank Lai °sD sample iD: SDNR Collect Datefrume Matrix Sampled by 4= i s 4'i Site, 8 40?B/2O14 11:00 r` NA Solid/Sludge Dixon Medlin --i Rest M2tnad Results Date Analyzed i obi Seiids �r`�3 sty 2;�a a 3.80 % 04/2Qi2014 �..,...9 ODDens.. say+ ew it M h u sa; <611� PN/g 041e9120 ; 4 LJ Baia C. Sample jo. Gi3 R Collect Datell'ime 1'cr?atrix Sampled by 4a 11742 S;tao � : 4028:2014 11:00.AM Solid/Sludge Dixon Medlin i ev Method Results Date Ana"d `1fi6E So,ids �� � S 23ats 5 4.05 °lo OA128/2�J14 i=eG2B `enS:L,E St_7 --,21^v E'rv1PN 24 hr 603 <5 V, ,PN/g 04/2S/20?4 RAwr,, n 2354-t48"14 Page 2 of 3 d-.'.s i'iii�..? 'N.'L� Cr �I•�fri Y�e17�.��,t,^• v : •^y�.r':T�Y `y LL�� 14 R J63�: h7 S'r'v V i31r.: �:", ��`Q. "JC' env �7� s'Y!� :����dJ`._Ir.•vJ.`�:�eY i^'IG. •�w�b�w L� o ��� %r° 3�oCe PI'c`19e}SLG^ cc C�Cd%>: ^G324?`i- 1Gt^� e.0 3Ct-,on*- !4 ?^ " c• LZ6/ SS! QiE "" Z9rnz o.m. Atc:,::Is 3\ iZ6L•SSL'Otg:azy�aa� =,F-_..A-D5£Z 6 c,=zCe si; 5C-`--tc-�o mitt f�llssi?!• No ` iLi,+a.e .•'w 1`'Yl �t/� � Ia. 1�3� Y YA�r 'aw��y 'g ,}'y, It P�y� y{ 'V t✓' r•�H�� GI'.-.v�ry'4u 19EJ s L'_YY SiC'� a eSa'a�i!^ iuffirZ .�.33'.+.� , �+ r,�c<1xtr�"�`r ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name:. County of Brunswick Utilities WQ,Permit Number: , WQQ034513 WWTP Name: , West Brunswick WWTF NPDES Number:, WQ0023693 Monitoring Period: From 4/l/2014 To. 6/30/2014, ` Pathogen Reduction (40 CFR 503.32) -. Please indicate level -achieved and alternative performed: Class A: Alternative 1 ❑ Alternative2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 Alternative 6 ❑ If applicable, to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens"; Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Ra ❑ Pasteurization ❑ y -.................................. Class B: Alternative 1 ❑ Alternative 2 C7 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":. Lime Stabilization , ❑ Air Drying❑ Composting ❑' JAerobic Digestion '❑ Anaerob ic i c Digestion ❑ If applicable to alternative erformed Class A or Class B coml2lete the,following monitorin data: Allowable Level Pathogen Density um 01 Frequency. Sample a cal Parameter Excee- Tech - in, Sludge MinimumGeo. Mean MaximumUnits of Analencesysis Type nigue 2 x 10 to the 6th power Pei grain of CFU Fecal Coliforni total solids 1000 mpn per gram of total solid (dry amonella bacteria 3 MPN per grams (in lieu of fecal total solid (dy ector Attraction Reduction - Please indicate antinn nerfnrmpd- Alt.1 (VS'reduction) ❑ Alt.1 (40-day bench) ❑ Alt. 3 (30=day bench) Alt. 4 (Spec. OZ uptake) El Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Allc Stabilization Ll Alt 7.(Drying - Stable) ❑ Alt. 8 (Drying - tJnstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑, No vector attraction reduction alternatives were.performed ❑ CIEKY ICATION STATEMENT (please check the appropriate statement) U "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met" ® "I certify, under penalty of law, that the pathogen requirements in 40 CFit 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." �C Prepawr Name and Xitle (type or print) Land Ap lieAame and Title (if applicable)(type or print) Signaturof Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) COUNTY OF BRUNSWICK PUBLIC. UTILITIES LAND APPLICATION_ PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled:11/12/2014 West WWTP Permit No. NCO044873 Mineralization rate 0.30 % Solids 3.34 aH 7.96 Parameter % PPM m Ik % *10 000 Lbs/D Ton (Mg1Kn 0.0021 PAN Injected 59690.6 119.3812 PAN Surface 34540.6 69.081 TKN 81600 163.2 Ammonia Nitrogen (Am) 50300 100.6 Nitrate Nitrogen (Nin) 0.6 0.0012 Organic Nitrogen (Orn) 0 0 Total Phosphorus (P) 59300 118.6 Total,Phosphate (P205) 0 0 Estimated Avail. P205 0 0 Total Potassium. (K) 4940 9-88 Total Potash (K20) 0 0 Arsenic,(As) 2.99 0.00598 Cadmium (Cd) 2.99 0.00598 Chromium (Cr) 24.1 0.0482 Copper (Cu) 518 1.036 Lead (Pb) 8.74 0.01748 Mercury (Hg) 0.449 0.000898 Molybdenum (Mo) 8,02 0.01604 Nickel (Ni) 19.2 0.0384 Selenium (Se) 8.32 0.01664 Zinc (Zn) 1820 3.64 Aluminum (AI) 5.72 0.01144 Calcium (Ca) 27800 55.6 Iron (Fe) 0 0 Sodium (Na) 2810 5.62 Sulfur (S) 0 0 Magnesium (Mg) 6770 13.54 Manganese (Mn) J 0 0 Environmental Chemists, Inc. 2014-13993 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N)+ Ammonia N + Nitrate N +Nitrate N - % PAN Surface Application (Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N) + Nitrate N +Nitrate N - % PAN Note: Constituents N.D. (Not Detected) or < direction limits are listed as detection limits for calculation purposes. 65001oad .905 1b per load. 147.696 lb PAN per load injected / 62.518 Surface 45001oad .626 1b per load 162.2861b PAN per load infected /74.732 Surface COUNTY OF BRUNSWICK �gw�°�f West Brunswick Regional Laboratory Public Utilities Department .235 Grey Water Road Wastewater. Treatment Division Supply, NC 28462 CA��Phone: 910-755-7921 Fax: 910-766-7927 Sample Collection and Chain of Custody Collected By: r i(n,8j Report No.: 1 Sample Tvoe: I = Influent. E = Effluent. W = Well: ST = Stream, SO = Soil, SL = Sludge Other. r-� �f q 13CR3 Container (Plastic or Glass), Chlorine mglL LAB ID NUMBER PRESERVATION ANALYSIS REQUESTED Sample Identification Collection Sample Type Composite or Grab DATE TIME NONE HCI . H2SO4 HNO, THIO OTHER SDNR Tank WBR � �a SL C P 0 ya9g X Fecal Density 11112/2014 10: 40 G G SDNR Tank WBR SL C P 0 X Fecal 1111=014 0•y.l G G SDNRTank WBR SL C .. P 0 r{30b X Fecal Density 11112P2014 0 G G SDNR Tank WBR SL C P 0 301 X Fecal Density 11.11212014 p: $ G G SDNRTank WBR SL C P 0 4304 X Fecal Dens ty 11/12/2014 Oc 4 Lf G G SDNRTank WBR SL C P 0 3k3©3t 7 X IFecal Density 1111212014 : CF G G SDNRTank WBR SL C P 0 3y3D4 X Fecal Density 11/1212014 Q• G G SDNRTank WBR SL C P� 03D4 X Residuals 11/1212014 p; G G C P G G C P G G C P G G ATTENTION: Samples submitted for analysis for Ammonia, TKN, Cyanide, Phenol and all Bactedoiogicals must be dechlorinated td <_ 02 ppm at time of collection. Transfer Relinquished By: Date/Time Received By: DateITime 1 t/ IG 2 Temperature when Received: •� Accepted: Rejected: Resample Required: Delivered By. Comments•, -� �]• i { Environi.Vnenta. Chemists, Inc. envirochei!(910) 6602 VAndmfIi Way • Wilmington, NC 28405 $?2-0223 (Lab)' • (910) 392-4424 (Fax) ® - - , 710 Bo,Nsertown Road •. Mantec, NC 27954 `, ( 2) 473-5702 ANALYTICAL & CONSULTING } CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Brunswick County Public Utilities Date of Report: Dec 04, 2014 - Post Office Box 249 '.Customer PO #: _ Bolivia NC 28422 Customer iD: 08100011 Attention: Donald Dixon j Re'port#: �. 2014-13993 Project ID: SDNR Tank, Lab ID, "Sample ID: SDNR Tank WBR Collect Date/Time Matrix Sampled by 14-34298 Site:1 11/12/2014 10:40 AM, Solid/Sludge Dixon Medlin Test Method Results Date Analyzed - Total Solids (%) ; SM 2540 s 3.22 % 11/13/2014 Fecal Density 'SM 9221c E MPN 24 hr 503 <7 MPN/g . 11/13/2014 Lab ID'Sample ID: SDNR Tank WBR' Collect DateITime Matrix Sampled by 14-34299 Site: 2 11/12/2014 10:41 AM . Solid/Sludge Dixon Medlin Test Method Results Date Analyzed Total Solids (%). SM 2540 g . 3.18 % 11/13/2014 Fecal Density SM 92216 E MPN 24 hr503 <7 MPNIg 11l13/2014 Lab ID Sample ID: SDNR Tank WBR Collect DateITime Matrix Sampled by 14-34300 Site: 3 11/12/2014..10:42 AM Solid/Sludge Dixon Medlin Test Method Results Date Analyzed Total Solids (%) SM2540 s 3.18 % 11/13/2014 Fecal Density SM9221CSMPN 24hr603 <7MPN/g 11/13/2014 Lab ID Sample ID: SDNR Tank WBR Collect DateITime Matrix Sampled by 14-34301 Site: 4 11/12/2014 10:43 AM Solid/Sludge Dixon Medlin Test Method Results Date Analyzed Total Solids (%) SM 2540 s 3.44 % 11/13/2014 Fecal Density SM92216EMPN 24hr503 <6MPN/g 11/13/2014 Lab 10 Sample ID: SDNR Tank WBR Collect Date/Time Matrix Sampled by 14-34302 Site: 5 11/12/2014 10:44 AM Solid/Sludge Dixon Medlin Test Method Results Date Analyzed Total Solids (%) SM 2540 8 2.84 % 11/1312014 Fecal Density SM 92210 E MPN 24 hr503 <8 MPN/g 11/13/2014 Report f : 2014-13903 Page t of 3 7 J Environmental' Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 envirochem (910)392-0223(Lab) • (910)392-4424(Paz) sM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Brunswick County Public Utilities Date of Report: Dec 04, 2014 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Aitentlon: Donald Dixon Report #: 2014-13993 'L Project ID: SDNR Tank Lab ID Sample ID: SDNR Tank WBR Collect Date/Time Matrix Sampled by L 14-34303 Site: a 11/12/2014 10:46 AM Solid/Sludge Dixon Medlin Test Method. Results' Date Analyzed Total Solids (°/a) SM2540 1 3.36% 11/13/2014 Fecal Density SM 02216 E MPN N hr5o3 <6 MPN/g 11/13/2014 Lab ID Sample ID: SDNR Tank WBR Collect Date/Time Matrix Sampled by 14-34304 Site: 7 11/12/2014 10:46 AM Solid/Sludge Dixon Medlin Test Method, Results Date Analyzed Total Solids (%) SM 2540 a . 3.25 % 11/13/2014 Fecal Density SM 92216 E MPN 24 hr503 <7 MPN/g 11/13/2014 Report#:: 2014-13003 Page 2 of 3 F' -- Environmental Chemists_ , Inc. L env irochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Pax) ® 710 Bowsertown Road • Manteo, NC 27954 ' (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR. DWQ CERTIFICATE #94. DiS CERTIFICATE #f3T12� Brunswick.County Public Utilities Date of Report: Dec: 05, 2014 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #:. 2014-13993 '- Project ID: SDNR Tank Lab ID Sample ID: SDNR Tank WBR Collect DateITime 'Matrix Sampled by 14-34305 Site: Residuals 11/12/2014 10:37 AM Solid/Sludge Dixon Medlin Test Method Results Date Analyzed Total Solids (%) son 25ao a 3.34 % 11113/2014 Sludge Residuals Aluminum EPA200.7 .5.72mg/kg 11/18/2014 Arsenic EPA20a.7 <2.99mg/kg 11/18/2014 Cadmium EPA200.7 <2.99 mglkg 11/18/2014 - Calcium VA2001 27800 mg/kg 11/19/2014 Chromium EPA206. 24.1 mg/kg 11/18/2014 Copper EPA 200. 518 mg/kg 11/2412014 Lead EPA 200. 8.74 mg/kg 11118/201.4 Magnesium EPA200.7 6770mg/kg 11/19/2014 Molybdenum EPA 200.7 8.02 mg/kg 11/18/2014 Nickel EPA200.7 19.2 mg/kg 11/18/2014 Potassium EPA200.7 4940 mg/kg 11/19/2014 Selenium EPA200.7 8.32mg/kg 11/18/2014 Sodium EPA200.7 2810 mg/kg 11/19/2014 Zinc EPA2004 1820mglkg 11126/2014 Ammonia Nitrogen EPA 450.1 50300 mg/kg 11/14/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 81600 mg/kg 11/17/2014 Nitrate+Nitrite-Nitrogen EPA353.2 <0.60 mg/kg 11/26/2014 pH SM 4500 H B 7.96 units 11/20/2014 Total Phosphorus SM 4500 P F 59300 mg/kg 11/18/2014 r Mercury SW8487471B 0.4490mg/kg 11/26/2014. Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: ll i � Report #.: 2014A3893 'f Page 3 o3 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: County of Brunswick Utilities WQ Permit Number: WQ0034513 WWTP Name: West Brunswick WWTP NPDES Number: WQ0023693 Monitoring Period: From 10/l/2014 To 12/31/2014 . Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 : ® Alternative 3 ❑ . .......... Alterative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ . Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma'Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑. Composting ❑ jAerobic Digestion ❑ aero i Digestion An b c Di a tion g If !Rplicable to alternative performed Class A or Class B complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- Frequency of of Analysis Y Sample Type Analytical Tech - imu Geo. Mean . aximu Units Fecal Coliform 2 x 10 to the 6th power Per gram of - total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria On lieu of fecal coliform)' 3 NTN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) -Please indicate option performed: Alt 1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAR. 4 (Spec. 42 uptake) ❑ Alt. 5 (14-Day_Aerobic) ❑ Alt. 6 (Alic Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable). ❑ Alt. 9 (Injection) 0 Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements, in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel property gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Preparer Name and Title (type or print) Signature of Preparer* Land Appiei Name and Title (if applicable)(type or print) Date S `--- *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Applier (if -4 Date DENR FORM PVRF 503 (12/2006) County of Brunswick Public 6tilities West Brunswick Regional Facility Laboratory V,,rlh f ( Nuridwr . Aims 110 BoN 249 -IJJ Grey' W,11C. RAM SmVph% N( 75",-'7W'7 Date '15-iXIC201 I West Brunswick Thirty Day Bench Beginning: 11112114 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 12115/14 as Required to Meet Option 3 11.20% WWTP EPA [503.3 . 3(b)(3)] PASS Lam {End or RtSporti —. Certified by: Anna teRoux, Laboratory Supervisor E 0 41 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: County of Brunswick WQ Permit #: WQ0023693 Field#: 2 Acres Utilized: 19.2 Land Owner: A Hughes Annual Dry Tons Applied; 48.8428 'Site #: AH Acres Permitted: 19.2 Operator:. Same Predominant Soil Series: Lynchburg Cation Exchange Capacity (non 503): Crop 1 Name: Soy, Beans Crop 1 Max. PAN: 178 :Crop 2-Name: ; Rye Crop 2 Max. PAN: 50 .� 04 o A 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/AC) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches A 'd a o a� c - < o �; i9 # -� * TKN mg/kg Z Y o o r, mg/kg . Nitrate and Nitrite. mg/kg "PAN Applied ( Ibs/acre) Name of Crop P Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 April 227500 4.08 2.016 2 West Moist 0 S 0.5 1 0.3 69300 - 38800 3.68 115.125 NA SB March 16500 0.95 0.034 OR Moist 0 S 0.5 0.3 49800 2440 509 1.085 NA SB March 45500 1.07 0.106 ST Moist 0 S 0.5 0.3 37100 1420 25 2.432 NA. SB november 71500 1.47 0.228 CS Moist 0 S 0.5 0.3 76300 1080 593 Na 10.820 Rye vovem 26000 0.95 0.054 OR Moist 0 S 0.5 0.3' 40800 2440. 509 Na 1.710. Rye lovember 51500 0.95 0.106 OR Moist 0 1 S 0.5 0.3 49800 .2440 5090 Na: 4.360 Rye 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 D.000. .0.000 0.000 0.000: : 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF"supp to this form): TOTALS: 01 438500 - As Cd Cu Cr Pb Hg Mo Ni Se Zn P. 118.642 . 16190 Lime Applied Annual lbs/acre 0.051 0.149 0.200 36 0.018 0.148 0.166 34 1 L866 5.83 7.696. 1338 1 0.094 0.141 0.225- :- 0.060` 0.317 . 0.377 267 0.003 0.015 _ 0.018. 15 0.018, - 0.219 ' 0.237 0:079' 0.342 0.42'1 374 0.036 0.235 0.271 89 5.509: 14.689 20.198 2498 174.047 '. Date ' lbs/ac Prior Years Cumulative lbs/ac Current Cumulative Ibs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop - 178 50 "I certify, under .penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly, gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, ' Inding the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC, - Incorporation i **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Si ture of Land AppIier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested.-0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 49.15 Permit #: WQ0034513 Cation Exchange Capacity (non 503 only): _ 7 -erator: A Hughes Owner: Same Predominant Soil Series: Lynchburg , . . ces.Used: 19.2 Acres Permitted: 19.2 Site #: AH Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mglkg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 West _2j 4West 3 CS _4j OR 51 ST CS 7 CS. 81 ;OR 9 ST io-I CS 11 OR 12 % Solids 4.08 3.34 1.47 1 0.95 1.07 1.47 1 1.47 0.95 1 1.07 1.47 0.95 Arsenic `10.4 2.99 '6.74 8.84. 8.6 6.74 6.74 8.84 8.6 6.74 8.84 Cadmium 2.431 2.99 6.74 8.84 8..6 6.74 6.74 8.84 8.6 6.74 8.84 Copper 431 518 149. 82.7 . 106 149 149 82.7 106 149 82.7 Chromium 18.1 24.1 10.1 8.84 ' 12.1 10.1 10.1 8.84 12.1 10.1 8.84 Lead 11..6 8.74 11 14.6 10 11 11 14.6 10- 11 14.6 Mercury 0.574 0.449 0.68 0.421 0.654 0.68 0.68 0.421 0,654 0-.68 0.421 Molyb- denum 2.43 8,02 6.74 8.4 , 8.6 6.74 6.74 8.84 8.6 6..74 8.84. Nickel 17.4 19.2-;'8.1 8.84 8:6 8:1 8.1 - 8:84 8.6,_, : 8.I `8.84, Selenium 6.89 8.32 6.74.: 8.84 1 8.6 6.74 6.74. 8.84 8.6 j 6.74 8.84 Zinc 1290 .1820 353 207 236 353 353. 207 236 353 207 Total Phos- n_horus 40300 59306 12300 12200 3170 12300 12300 12200 3170 12300 12200 anal Heavy Metal. Field' Loadings (Calculated in Ibs/acre): Total 717. 2 1 31 141_5j 6 7 8 9 1, 0 11 12 DT/Ac./ App. Event 2.02 0.23 0.04 0.11 0.05 0.11 Arsenic 0.042 ' 0.000 :. 0.003 0.001 0.002 0.000 0.000 - 0.001 0.000 0.000 1 0.002 0.000 0.051 Cadmium 0.010 0.000 0.003- 0.001_ 0.002 0.000 0.000 0.001` ..0.000 0.000 0.002 0.000 0.018 Copper 1.741 0.000 -, 0.069, 0.007 .0.023 0.000 0.000, 0.008... 0.000 . 0.000 0,018 . 0.000 1.866 Chromium 0.073 0.000, 0.005 0.001 0.003 0.000 .0.000: 0:001. 0.000. 0.000 0.002 0.000 0.084 Lead - 0.047 0.000 0.005 0.001, 0.002 0.000 0.000 0.001;' . 0.000 0.000- 0.003 0.000 0A60 Mercury 0.002- 0.000 0.000 .0'.000 0.000.. 0.000 0.000 0.000 0.000..0.060 0.000 0.000 0.003 Molyb- 0.0.10 0.000 0.003 0.001 0.002' 0.000 OA06 0.001 0:000 0.000 0.002 0.000 0.018 denurn Nickel 0.070 0.000 0.004 0.001 0.002 0.000 _ 0.000 0.001 0.000 0.000 0.002 0.000 0.079 Selenium 0.028 0.000 0.003 0.001 0.002 0.'000 0.000 0.001 0.000 0.000 0.002. 0.000 0.036 Zinc 5.212 0.000 0.162, 0.017 0.-052 0.000, 0.000-1 0.021 0.000 0.000 0.046 0.000 5.509 Total Phos- 162.812 0.000 5.658 0.976 0.697 0.000 0.000 1.220 0.000 0.000 2.684 0.000 174.047 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance - with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signifcaut penalties for submitting false information, including the possibility of fines and ;---,qrisonment for knowing violations". &= 6,��c - I /I Signature of L6d Applier Date DENR FORM MFLSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY. FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: County of Brunswick WQ Permit #: WQ0023693 Field #: 1 Acres Utilized: 10.3 Land Owner: A Hughes Annual Dry Tons Applied: 13.5796 Site #: CG Acres Permitted: 10.3 Operator: Same Predominant Soil Series: Onslow Cation Exchange Capacity (non 503): Crop 1 Name: Rye Crop 1 Max. PAN: 136 Crop 2 Name: = Bermuda Crop 2 Max. PAN: 50 o a Volume applied pp (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonslAc) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Moist) Preci . p Past 24 Its.w' inches Y b * o �; .-• 0 . m .» '✓ 0 TKN mg/kg. Z c o E. mglkg Nitrate and Nitrite mglkg PAN Applied .., (lbs/acre) Name of Crop Type Receiving Residual Application . Crop 1 Crop 2 Crop 1 Crop 2 Swc 97500 3.34 1.318 4 West Moist 0 S 0.5 0.3 81600 50300 0.6 91.077 NA Rye 0.000 0.000 oxob 0:000 0.000 0.000 0.000 0.000 0.000 0.000 01.00.0 0.000 0.000. 0.000 0.000 0.000 0.0001 0.000 0.000 6.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 4 000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp-(-attach FORM FSF supp to this form): ai7j S: 0 97500 : As Cd Cu Cr Pb H Mo Ni Se Zn P 91.077 '. 0.000 Lime A lied knnual lbs/acre 0.008 0.317 0.325 36 0.008 0.317 0.325 34 1368 _ 4.205 5,573 1 1338 0.064 0.298 0.362 ' 0.023 _ 0.441 0:464 267 .. 0.001 0.007 0.008 15 0.021 0.367 0.388 0.451 0.438 0.489 374 0:022 • 0.632. 0.654 89 4.805' 11.61 16.415 2498 156.552 '.:' : = :' _ ; '. ``'' ;` ' ; Date lbs/ac 'rior Years Cumulative lbs/ac .urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** ermit PAN Limit 1 st/2nd Crop 1- ' ` 136 M I certify, under penalty of law, that this document was prepared under my direction or supervision, in accordance with a system designed to assure that jualified personnel properly gathered and evaluated the information, submitted. I am aware that there are significant penalties for submitting false aformation, inc ing the possibility of fines and imprisonment for knowing violations." .*Application Method: S - Surface, IN - Injection, INC - Incorporation ­-*-wolatilization Rate: Surface - 0.5, Injecdon/Incorporation --1.0 Si re of Land Applier Date *** Mineralization Rates; Compost -0.1, anaerobially digested =0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loadina Rate ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report T Facility Name: Brunswick County Total Dry Tons Applied (Annual): 13.33 Permit #: WQ0034513 Cation Exchange Capacity (non 503 only): '- aerator: C. Galloway Owner: Same Predominant Soil Series: Onslow res Used: 10.1 Acres Permitted: 10.1 . .. Site #: CG Field M 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ' Sample or Com- posite Date 1 2 West 2 West _3j CS 4j OR 5 ST 6 CS _yj CS 8 OR _9_j ST 10 CS 11 '. OR 12 % Solids 1 4.08 3.34 1.47 1 0.95 1.07 1 1.47 1.47 1 0.95 1.07 1.47 1 0.95 Arsenic 10.4 2.99 6.74., 8.84 8.6 6.74 6.74 8.84 8.6 6.74 8.84 Cadmium 2.43 2.99 6.74 8.84 8.6 6:74 6.14 8:84 8.6 6.74 8.84 Copper 431 518 149 82.7 . 106 149 149 823 106 149, 82.7 Chromiur4 18.1 24.1 10.1 8.84 12,1 10.1' 10.1 8.84 12.1 1 10.1 8.84 Lead, 11.6 8.74 11 14.6 10 . 11 11 14.6 10 11 14.6 -Mercury 0.574 0.449 0.68 0.421 0.654 0.68 0.68 0.421. 0.654 0.68 0.421 Molyb- d num 2.43 8.02 6.74. 8.4 8.6 634 6.74 8.84 8.6 6.74 8.84 Nickel 17.4 19.2 . ' 8.1' 8.84 8.6 8.1 8.1 8.84 8.6 8.1 8:84 Selenium 6.89' 832 ' 6:74 8.84 8.6 6.74 6.74 8.84 8.6 6.74 8.84 Zinc 1290 1820 '353 207 236 353 353 207 236 353- 207 Total Phos- chorus 40300 59300 12300 .12200 3170 12300 12300. 12200 3170 12300 12200 nual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 71 2 1 3 1 4 5 6 7 8 9 10 11 12 DT/Ac./ App. y Event 1.32 " Arsenic 0.000. 0.008 0.000 0.000.-1 0.000 0.000.. 0.000.,0.000 J.000 0.000. 0.000 0.000 0.008 Cadmium . 0.000 0.008-, _ 0.000 0.000 , ; 0:000 0:000 0.000 . . 0.000 0.000 _ :"0.000. 0.000 0.000 . 0.008 Copper 0.006 1.3W ..0.000, :0.000 ,0.000 A.000 0.000:. 0.000 0.000 0.000 0.000 0.600, 1.368 Chromium 0.000 0.064 0.000 0.000 0.000'- 0.000 ..0.000. • -0.000 0.000 0.000 . 0.000 0.000 0.064 Lead 0,000 0.023:: . 0.000..: 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Mercury 0.000. 0.001 0.000 0.000 0.000 : :0.000 . - 0.000 '. 0:000 . '0.000.-, 6.000 0.000 0.000 0.001 Molyb- 0.000 0.021 0.000 0.000. 0.000 0.000 0.000 0.000.. 0.000 0.000 0.000 0.000 .0.021 num Nickel 0.000 0.051. 0.000 0.000 0.000 0.000 , 0.000 0,000 0.000 0.000.1 0.000 0.000 0.051 Selenium 0.000 0.022 0.000 0.000 0:000 0.000, -0.000 0.000 0.000 0.000 0.000 0.000 _ 0.022 Zinc 0.000 4.805 0.000 0.000 0.000 6.000 -,0.000 0.000 0.000 0.000 0.000' • 0.000 4.805 Total - Phos- 0.000 156.552 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 156.552 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that.qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and �--orisonment for knowing violations". v6qn1_1_/W ,! Signature of n Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLAND FORM -TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: County of Brunswick WQ Permit #: WQ6023693 Field #: 2 Acres Utilized: 6.4 Land Owner: C Galloway Annual Dry Tons Applied: 11.7690 . Site #: CG Acres Permitted: 6.4 Operator: Same Predominant Soil Series: Onslow Cation Exchange Capacity (non 503): Cran 9 Name: Rve Croa 1 Max. PAN: 136 Crop 2 Name: - Bermuda Crop 2 Max. PAN: 50 +� °3 o A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume p per Applied r Acre (Dry TonslAC) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may, Wet, Moist) Precip. Past 24 Hrs. inches n co ter* .- Q a * � C o '"� » CD = �+ * o TKN mg/kg z Y o coo ? w' mglkg Nitrate and Nitrite mg/kg PAN Applied pp (lb� ) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 Dec 84500 3.34 1 1.839 4 West Moist 0 S 0.5 0.3 81600 56300 0.6 127.034 ' NA Rye 0.000 0.000 0.000 0.000 0.000 0.000 0.000" 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000- 0.000 0.060 6.000 0.000 0.000 0.000: 0.000 0.000 _ 0.000 - 0.000 0.000-, 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF. supp (a ch FORM FSF supp to this form): 'OTALS: 0 84500 As Cd Cu Cr Pb H Mo Ni Se Zn P 127,034 .' 0.000 Lime A lied knnual lbs/acre 0.011 0,011 1.906 0.089 0.032 0.002 0,030 0.071 0.031 6.698 218:224 ' . ;. _: ;, ;' `; ;`<-`;.:: Date 'lbs/ac 'rior Years Cumulative lbs/ac 0.025 0.025 2.851 0.015 0.145 0.007 0.075 - 0.165 0.06 8.25 Cumulative lbs/ac 0.036 0.036 4.757 0.104 0.177 0.009 0.105 0.236- 0,001 14.948 -urrent 'ermitted C: P. L. R,**** 36 1 34 1 1338 1 267 15 374 89 2498 'ermit PAN Limit Istl2nd Crop 136 50 `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system uestgnea to -assure tnat lualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false' reformation, incl ing the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1 /S�Volatilization Rate: Surface - 0.5, Injection/Incorporation,- 1.0 Si re of Land Applier Date *** Mineralization, Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0:3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 11.78 Permit #: 'WQ0034513 Cation Exchange Capacity (non 503 only): r'-erator: C Galloway Owner: Same Predominant Soil Series: Onslow Wires Used: 6.4 Acres Permitted: 6.4 Site #: CG Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 West _2j 4West 31 CS 4j OR 61 ST 6 CS _7j CS Sj OR 91 ST i2i CS iij OR 12 Solids 1 4.08. 3.34 1.47 1 0.95 1.07 1 1.47 1.47 0.95 1 1.07 1.47 0.95 Arsenic 10.4 2.99 6.74 8.84 8.6 6.74 6.74 8.84 8.6 6.74 8.84 Cadmium 2.43 2.99 6.74 , 8.84 8.6 , 6.74 6.74 8.84 8.6 6.74 8.84 , Copper 431. 518 149 82.7 106 149 149 82.7 106 149 82.7 Chromi 18.1 24.1 10.1 8.84 1 12.1 10.1 10.1 8.84 12.1 10.1 8.84, Lead 11.6 8.74 11 14.6 10 11' 11 14.6 10 11 14.6 Mercury 0.574 0.449 0.68 0.421 0.654 0.68 0.68 ' 0.421 0.654 0.68 0.421 Molyb- de um 2.43 8.02 6.74 8.4 8.6 6.74 6.74 884 8.6 6.74 8.84 Nickel 17.4 19.2 8.1 8.84 8.6 8.1 8.1 8.84 8.6 8.1 8.84. Selenium 6.89 8.32 6.74 8.84 8.6 6.74 6.74 8.84_ 8.6 6.74 8.84 Zinc 1290 1820 353 207 236 353 353 207 236 353 207 Total Phos- phorus 40300 59300 12300 12200 3.170 12300 12300 12200 3170 12300 12200 ival Heavy Metal Field Loadings (Calculated in lbs/acre): otai 1 2 31 4 LS 6 7 8 9 10 11 12 DT/Ac./ - o App. Event 1.84 Arsenic 0.000 0'.01-1: 0.000 0.000 0.000 .0.000-, 0.000 1 0.000 0.000 Z 0.000 1 0.000 0.000 0.011 Cadmium 0.000 .0.011 0.000 .. 0'.000' 0.000 0.000 0.000 0.000, 0.000- , 0.000 0.000 0.000 0.011 Copper 0.000 (1.906 0.600 0.000 0.000 0.000 0.000 0:000 .0.000 . 0.000 0.000 . 0.000 1.906 Chromium 0.000 0.089 0.000, 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.089 Lead 0.000- 0.032 0.000 0.000'. `0;000 0.000 -0.000- 0.000 0.000 0.000 0.000 0.000 0.032 Mercury 0.000 - 0.002 - 0.000 0.000 0.000. 0.000, . 0.0001 .0.000. _ 0.000 0.000 , 0.000 0.000 0.002 Molyb- denum 0.000 0.030 0.000 0.000 0.000 ` 0.000 1 0.000 0.006 0.000 . 0.000 0.000 0.000 0.030 Nickel 0.000 0.071 0.000 0.060. 0.000" 0.000 0.000 -0.000. 0.000 0.000 0.000 0.000 0.071 Selenium 0.000 0.031 0.000 0.006 . 0.000 0.000 0.000 0:000 -.0.000 0.000 0.000 - 0.000 0.031 Zinc 0.000 6.698 0.000 0.000 0.000 0.000- 0.000 .0.000- 0.000- 0.000 0.000 0.000 6.698 Total Phos- 0.000 218.224 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000, 0.000 0.000 218.224 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and i-nrisonment for knowing violations". b 1- Signature of Land plier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: County of Brunswick WQ Permit #: WQ0023693 Field #: 3 Acres Utilized: 5.9 Land Owner: C Galloway Annual Dry Tons Applied: 9.9584 Site #: CG Acres Permitted: 5.9 Operator: Same Predominant Soil Series: Onslow Cation Exchange'Capacity (non 503): Crop 1 Name: Rye Crop 1 Max. PAN: 136 Crop 2 Name: Bermuda Crop 2 Max. PAN: 50 A Volume applied (enter one) Solids/ Liquid 9 Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES # WQ# Fert., Animal Waste, etc)- Solt Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches � o . 'd � F51 A o �' '" * :O co .4 D �' 8 TKN - mgtkg _ Z ; o a a n mglkg Nitrate and Nitrite mgtkg PAN Applied PP ( lbs/acre) Name of Crop p Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Dec 71500 3.34 1.688 4 West Moist 0 S -0.5 0.3 -81600 50300 0.6 116.599 :. NA Rye 0.000 0.000 0:000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000- 0.000 0.000 0.000;. 0.000 0.000. 0.060 O.00D 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000, , _ . 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF. supp-( attach FORM FSF supp to this form).- r0TALS:1 01 7I506 As Cd Cu Cr Pb H g Ma ) Ni Se I Zn P 116.599 0.000: Lim&Applieedd Annual Ibs/acre 0.011 0.296 0.307 36 0.011 .0.296 0.307 34 1.906 2.589 4.495 1338 0.089 0.276 0.365 0.032 0.386 0.418 267 0.002 - 0.007 0.009 IS 0.030 - 0.306 0.336 0.07I: 0.346.. 0.417 374 0.031 0.583 ' 0.614 89 6.698 6.544 13.242 2498 218.224 ; ': .:: ; • ` :: `.. ;' :` < ;.. Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative Ibs/ac Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop 136 50 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure.that qualified personnel properly gathered and evaluated the information submitted. I am aware that.there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." jj' *Application Method: S - Surface, IN - Injection, INC - Incorporation /�J'____**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 S ature of Land Applier Date's Mineralization Rates: -Compost -0.1, anaerobially digested-0.2, aerobically digested 7 .0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report i- eility Name: Brunswick County Total Dry Tons Applied (Annual): 9.96 Permit #: WQ0034513 Cation Exchange Capacity (non 503 only): . ___r Operator: C Galloway Owner: Same Predominant Soil Series: Goldsboro Acres Used: 5.9 Acres Permitted: 5.9 Site #: CG Field #: 3. Residual Analysis Data (Heald Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 2 West 4 West __3' CS 4..' OR S._ ST 6_.! CS", 7 i CS 8, OR 91 ST 10 CS 11 f OR 12 Solids 4.08- 3.34 1.47 ` 0.95 1.07 1.47 1.47 0:95 1.07 1.47 0.95 Arsenic 10.4 2.99 6.14 8.84 8.6 6.74 6.74 8.84 8.6 6.74 8.84 Cadmium 2.43 ' 2.99 6.74 8.84 8.6 6.74 6.74 8.84 8:6 6.74 8.84 Copper 431 518 ; 149 82.7 106 149 149 82.7 106 149 82.7 Chromium 18.1 24.1 10.1 8.84 1 12.1 10A 10.1 _ 8.84 12.1 10.1 8.84 Lead : 11.6 8.74Al 14.6 10 11 11 14.6 10 11 14.6 Mercury 0.574 1 '0.449 0.68 0.421 0.654 0.68-, 0,68 0.421 0.654 0.68 1 0.421 Molyb-: denum 2.43 8.02 6.74 8.84 '8.6 6.74 6.74 8.84 8.6 6.74 '. 8.84 Nickel. 17.4 19.2 8.1 8.84',. 8.6 8.1 8.1 &84 8.6 8.1 8.84 Selenium 6.89 8.32 6.74 8.84 8.6 6.74 6.74 8.84 8.6 ' 6.74 8.84 Zinc • 1290 1820 353 207 236 353 353 207 236 353 207 Total Dhos- orus 40300 59300 12300 12200 3170 12300 12300 12200 3170 12300 1220.0 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1! 2� 3 4= 5� 6 7j 8! 9j 10f 11 1 2' DT/Ac.! App. y Event 1.69 _ Arsenic 0.000 0.010 0.000 0.000 0.000 0.000 0.000 0.000 '0.000 0.000 0.000 0.000 0.010 Cadmium 0.000 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 0.000 1.749 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.749 Chromium 0.000 0.081 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081 Lead 0,000 0.030 0.000 0.000 0.000 0.000 0.000 0.000 0.000 . 0.000 0.000 0.000 0.030 Mercury' 0.000 0.002 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molt' - 0.000 0.027 0.000 0.000 0.000 0.000 0.000 '0.000 0.000 0.000 0.000 0.000 0.027 denum Nickel 0.000 0.065 . 0.060 0.000 0.000 0.000 0.000 0.000 0.000, 0.000 0.000 06000 0.065 'Selenium 0.000 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Zinc 0.000 6.144 0.000 0.000 0.000 0.600 0.000 0.006 0.000 0.000 0.000' 0.000 6.144 Total Phos- 0.000 200A97 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 200.197 horus "I certify,, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel' properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". - �l% Signature of Land 6hier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: County of Brunswick WQ Permit #: WQ0023693 Field #: 4 Acres Utilized:. 11.5 Land Owner: C Galloway Annual Dry Tons Applied: 9.0531 Site M. CG Acres Permitted: 11.5 Operator: Same Predominant Soil Series: Onslow Cation- Exchange Capacity (non 503): Crnn 1 Name: Rve Cron 1 Max. PAN: 136 Crop 2 Name: Bermuda . . Crop 2 Max. PAN:. 50 ALiquid Volume applied - (enter one) Solids/ Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. Wei Moist) Precip. Past 24 Ws. inches Y " 'O w _ 8 o m �'. . _ * 5 r.Z ,. w * o o TKN mg/kq " o c w• mg/kg Nitrate and Nitrite mg/kg . PAN Applied lbs/acre ( ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Dec 65000 3.34 0.787 4 West Moist 0 S 0.5 0.3 81600. -50300 1 0.6 54.382. NA Rye 0.000 0.000 0.000 0.000- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0w . Residuals Applications totals on FORM FSF supp- ( attach FORM FSF supp to this form): `. . 'OTALS:l 01, 650001 As Cd Cu Cr Pb HP, Mo Ni Se Zn P 54.382 1. -0.000 Lime Applied Annual lbs/acre 0.005 0.226 0.231 36 0.605, 0.262 0.267 34 0.818 - 1.485 2.303 .1338 0.038 0.293 0.331 0.014. 0.27 0.284 1 267 0.001 0.011 .. 0.012 1 I5 0.013, 0.265 0 278 1 0.030 1 0.271 0.301 1 374 0.013, 0.527 0.540 89 2.876 3.958 6.834 - 2498 . 93.694 "; ' ;;:,' : - °.' ' . Date lbs/ac ?rior Years Cumulative lbs/ac _urrent Cumulative Ibs/ac ?ermitted C. P. L. R.**** "ermit PAN Limit Ist/2nd Crop : = ": ;:'. 136 50 `I certify, under penalty of law, .that this document was prepared under my direction or supervision in accordance with a• system designed to assure that Iualified personnel properly gathered and evaluated the information submitted. I ant aware that there are significant penalties for submitting false - !nformatio including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN -Injection, INC - Incorporation 6 / -�**Volatilization Rate: Surface - 0.3, Injection/Incorporation -1.0 nature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0:4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form .to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 9.09 'Permit #: WQ0034513 Cation Exchange Capacity (non 503 only): r' -erator: C Galloway Owner:. Same Predominant Soil Series: Onslow i--;,ees Used: 11.5 Acres Permitted: 11.5 Site*: CG. Field #: 4 Residual Analvsis Data (Heave Metals and Total Phosahorus use ma/kLr. % Solids use Raw Percent #1: Sample or Com- posite Date 1 2 West 21. 4West 3 'CS 4 OR 5 ST 6 CS 7 CS 8 OR 9 ST 10 CS 11 OR 12 Solids 4.08 3.34 1.47 0.95 1 1.07 1.47 1,.47 095 1.07 1.47 0.95 'Arsenic 10.4 2.99 6.74 8.84 8.6- 6.74 6.74' 8.84 8.6 6.74 8.84 Cadmium 2.43 2.99 6.74 8.84 8.6 6.74 6.74' 8.84 8.6 6.74. 8.84 Copper 431 518 149 82.7 166 140 .149 82.1 106 149 tj'- Chromium 18.1 24.1.: 10.1 8.84 12.1 1 10.1 10.1 8.84 12.1 T0.1. 8,84 Lead 11.6 8.74 11 14.6 . 10 41, 11 . 14.6 10 '11 14.6 Mercury 0.574 0.449 0.68 0.421 0.654 0.68 0:68 0.421 0.654 0.68 0.421 Molyb= enum 2.43 8.02 6.74 8.4 8.6 6.74 "6:74 8.84 8.6 6.74 8.84.. Nickel, ; _ 17A 19.2 .8.1 8.84 8.6 8.1 ' . - 8.1 8.84 8.6 8.1 .9.84, Selenium 6.89 - -8.32, 6.74 8.84 -8.6- . 6.74. 6.74 .8.84 8.6 6.74 8.84 Zinc 1290 1820' 353 207 236 353 353 '207 .236 . 353 207 Total Phos- phorus 40300 59300 .12300 12200 3170 12300 12300 12200 3170 12300 12200 auat neavv ivietai rieia.Loaum2s it:aicuiatea in msiacren otal 1 2 31 L4]_5j 1617 81 91 110111 12 DT/Ac./ o App. Event 0.79 y Arsenic 1 0.000 0.005 0.000. 0.000- _ . 0.000„ ..0.000 0.000 : 0;000 0.000 - O000 1 0.000 0.000 0.005 Cadmium 0.000 . 0.005 0.000 . 0:000 0.000 0.000' : 0:000. 0.000:, . '0.000. .0.000 0.000, 0.000 0.005 Copper 0.000 . 0.818. 0.000 0A00 - 0.000 0.000- . 0.000 .. 0.000 0.000 0.000 0.000 0.000 0.818 Chromium 0:000 0.038 0.000 ; 0.000, 0.000 : 0.000 0:000 0;000' -0:000 _; . 0,000 0.000 0.000 0.638 - Lead . 0.000 1, 0.014- 0.000 0.000 0.000. : 0.000 0.000 0:000. 0:000 0.000 . 0.000 0.000 0.014 Mercury 0.000 0.001 , 0.000 0.000 0:000.:.0.000 0.000 0.000, .'0.000. ,0:000::.0.000 0.000 0.001 Molyb- denum 0.000 0.013 0.000 . 0.000 0.000 0.000 0.000 0.000 - 0.000 0.000. 0:000 0.000 0.013 Nickel 0.000 0.030 . 0.000 0.000- 0.000 _ 0.000' 01000 0.000 0.000 0.000._ 0.000 0.000, 0.030 Selenium 0.000 0.013 0.000 0.000 0.000 0.000 0.000' 0.000' 0.000 0.000 0:000 0.000 0.013 Zinc 0.000 2:876 0.000 0.000 0:000:.-0.000 0.000- 0.000 0.000 .0.000 0.000.1 0.000 .2.876 Total Phos- 0.000 93.694 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 93.694 horus -i cerwy, under penany of iaw, inaz tms aocument was preparea under my airection or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and D---orisonment for knowing violations". - )Z,- 6z__� - 1 Signature of L d plier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: County of Brunswick WQ Permit #: WQ0023693 Field #: 5 Acres Utilized: 6.1 Land Owner: C Galloway Annual Dry Tons Applied: 8.1478 Site #: CG Acres Permitted: 6.1 Operator: Same Predominant Soil Series: Onslow Cation Exchange Capacity (non 503): CroD 1 Name: Rye Crop 1 Max. PAN: 136 Crop 2 Name: . Bermuda Crop Z_Max. PAN: 50 = ° 1 y ° ° A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonslAC) Residual Sources � PDES #, W Fert., Animal Waste, etc) Soil Cond. (Dry' Mist) Precip. Past 24. Hrs. inches Y 410 I �..- # o .- R a * 9 M ? w , �, �, + N' TKN mg/kg . Z o av o p mg/kg- Nitrate and Nitrite mg/kg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop I Crop 2 Dec 58500 3.34 1.336 4 West Moist 0 S 0.5 0.3 81600 50300 0.6 . -92.272 NA Rye 0.000 0.000 0.000 0.000 0.000, 0.000 0.000 -0.000 O.Ooo 0.000 f 0.000 0.00o 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000: 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 - Residuals Applications totals on FORM FSF supp (attach FORM FSF`supp to this form): ` . 'oTALS: 0 5850o As Cd Cu Cr Pb H Mo Ni Se': -" Zn P . -92.272 0.000 Lime A lied knnual lbs/acre 0.008 0.033 0.041 36 1 0.008 0.033 0.041 34 1.388 0.697 2.085 1338 0.065 0.046 0.111 0.023 0.035 0.058 267 . 0.001 0.001 0.002 - 15 0.021 '0.033 0.054 0,051 0.043 .0.094 1 374 .0.022„ 0.034 0.056 89 4.878 1.667 6.545 2498 158.924 .' : ::., "'.:< ` ' :` `` Date Ibs/ac. ?rior Years Cumulative lbs/ac -urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** 'ermit PAN Limit Ist/2nd Crop 136 50. `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure:that lualified personnel properly gathered and ,evaluated the information submitted. I am aware that there -are significant penalties for submitting false ,nformati including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation /ZZ-=**Volatilization Rate: Surface - 0.5, InjectionAncorporation -1.0 igtlature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant' Loading Rate i ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 8.17 Permit #: WQ0034513 Cation Exchange Capacity_ (non 503 only): v- r'-erator:. C Galloway Owner: Same Predominant Soil Series: Onslow .•es ,Used; 6.1 Acres Permitted: 6.1 Site #: CG Field #: 5 Residual Analysis'Data (Heavy Metals and Total Phosphorus use mg/kg, % SoIids use Raw Percent #): Sample or Com- posite Date 11, 2 West 2 4West __3j CS 4 OR _5j ST 6 1 CS 7 CS 8 OR _9j ST 101 CS 11 j OR 12 % Solids 1 4.08 3.34 1.47 0.95 1 1.07 1.47 1.47 1 0.95 1.07 1.47 1 0.95 Arsenic 10.4 2.09 6.74 8.84 8.6 6.74 6.74 8.84 8.6 6.74 8.84 Cadmium 2.43 2.99 6.74 8.84 8.6 6.74 6.74 8.84 8.6 6.74 8.84 Copper 431 518 149 82.7 106 149 149 82.7 106 149 82.7 Chromium 18.1: 24.1 10.1 8.84 12.1 10.1 10.1 8.84 12.1 10.1 8.84 Lead 11.6 8.74 11 14.6 10 11 11 14.6 10 11 14.6 Mercury 0.574 0.449 0.68 0.421 0.654 -0.68 0.68 0.421 0.654 0.68 0.421 Molyb- denum 2.43 8.02 6.74 8.4 8.6 6.74 6.74 8.84. 8.6 6.74 8.84 Nickel 17.4 19.2 8.1 8.84 8.6 8.1 8.1 8.84 8.6 8.1 8.84 Selenium 6.89 '. 8.32 6.74 8.84 8.6 6.74 6.74 8.84 _ 8.6 6.74 8.84 Zinc 1290 1820 353 207 236 353. 353 207 236 353 207 Total Phos- horus 40300 -59300 12300 12200 3110 12300 12300 12200 3170 12300 12200 Waal Heavy Metal Field Loadings (Calculated in lbs/acre): `Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ App. „oyr Event 1.34 Arsenic 0.000 . 0.008- 0.000 0.000 : 0.000 - 0.000._ 1 0.0.00. . 0:000 0.000 0:000 1 0.000 0.000 0.008 Cadmium 0.000 0.008 0.000 0-.000 0.000 0.000,- :.0.000 0.000.. - 0-.000 0,000 . 0.000 0.000 0.008 Copper 0.000 1.388 0.000 0-.000 0.000 0:000 0.000- 0.000 0.000 -0.000 0.000 0.000 . 1.388 Chromium 0.000 0.065 0.000; 0.600 0.000... 0-.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.065 Lead '0.000 0.023.. -0.000- 0.000 0:000 0.00Q '0.000` 0.000 0.000 0.000-, .01000 0.000, 0,023 Mercury 0.000 0.001 0.000. 0.000 0.000 0.000'- 0.000. ' . 0.000 0.000 0.000 0.000 0.000 0.001, Molyb- 0.000 0.021 " 0.600 - 0.000 0.000 0.000" -0.000 0.600 0.000 0.000 0.000 0.000 0.021 denum Nickel 0.000 0.051 .0.000 0.000 0.000, 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Selenium 0,000 , 0.022 6.000 0.000 -0.000- 0.000 0.000 , 0.000-. . 0.000 0.000 0.000 0.000 0.022 Zinc 0.000 4.878 0.000 0.000 1 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 4.878 Total Phos- 0.000 158.924 0.000 0.000 0.000 0.000 0.000 0.000' 0.000 0.000 0.000 0.000 158.924 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and i-orisonment for knowing violations". Signature o LCn Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: County of Brunswick WQ Permit #: WQ0023693 Field #: 6 ., Acres Utilized: 11.5 Land Owner: C Galloway Annual Dry Tons Applied: 21.6327 Site #: CG Acres Permitted:.11.5 Operator: Same Predominant Soil Series: Onslow Cation Exchange Capacity (non 503): - Crop 1 Name: Rye Crop 1 Max. PAN: 136 Crop 2 Name: , .Bermuda Crop 2 Max. PAN:: 50 w N G A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonslAc) Residual Sources (NPDES #, W #, Q Fert., Animal Waste, etc) Soil Cond. D-_ Wei Moist) Precip. Past 24 IIrs. inches Y d e; 'd c w o "* p 5 g �, o: * P: w TKN mglkg Z � o 3 as c mg/kg . Nitrate and Nitrite mg/kg PAN Applied lbs/acre ( ) Name of Crop Type Receiving Residual, Application Crop 1, Crop'2 Crop 1 Crop 2 Dec 162500 3.34 1.968 4 West Moist 0 S 0.5 A3 81606 50300 - 0.6 135.956 NA Rye 0.000 0.000 0.000 0.000 - 0.000 aOOo 0.000 0.000. 0.000 0.000 0.000- 0.000 0.000 0.000 0.000 0.000' 0.000� 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000: 0.000 0.000 0.000 0.000 0.000 0.000 . 0.000 Residuals Applications totals on FORM FSF supp'(attach FORM FSF supp to this form): ornLs: 162500 As Cd Cu Cr Pb N Mo Ni.. Se _ . Zn P - 135.956 � 0:000 Lime Applied knnual lbs/acre 0.012 0.149 0.161 36 0.012 0.148 0.160 34 2.641 5.083 7.124 1338 0.095: 0.141 0.236 . 0.034 0.317 0.351, 267 0.002' 0.015 0.017 15 0.032 - 0.219 0.251 0.076 0.342 -. OA18 374 . . 0.033 0.235. .0.268 89 7.171 14.689 21.860 2498 233.642 ; ;,=` .`=:` ` .=; Date lbs/ac 'rior Years Cumulative Ibs/ac �urrent Cumulative lbs/ac ?ermitted C. P. L. R.**** ?ermit PAN Limit lst/2nd Crop '136 50 `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that Iualified personnel properly gathered and evaluated the information submitted. I am. aware that there are signifcant penalties for submitting false nformation ' eluding the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection,.INC -Incorporation **Volatilization Rate: Surface.- 0.5, InjectioWIncorporation -1:0 *** Mineralization' Rates: Compost -0.1, anaerobially digested -0.2, Saature of Land Applier Date aerobically digested -0.3, raw sludge,4A ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 22.66 Permit #: WQ0034513 Cation Exchange Capacity. (non 503 only): 0- erator: C Galloway Owner: Same Predominant Soil Series: Onslow i-res Used: 11.5 Acres Permitted: 11.5 , Site #: CG Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg,- % Solids use Raw Percent #): Sample or Com- posite Date 1 . 2 West 2 4West 3 CS _4j OR L5 J SIT 6. CS 7 CS 8 OR 9 ST 10 CS 11 OR 12 % Solids 4.08 1 3.34 1.47 0.95 1.07 1.47 1.47 1 0.95 1.07 1.47 1 0.95 Arsenic 10.4 2.99 6.74 8.84 8.6 6.74 6.74 8.84 8.6 6.74 8.84 Cadmium 2.43 2.99 6.74 8.84 8.6 6.74 6.74 8.844 8.6 6.74. 8.84' Copper 431 51'8 149 82.7 106 149 149 82.7 106 149 82.7 Chromium 18.1 24.1 . 10.1 8.84 12.1 10.1 10.1 8.84 12.1 10.1' 8.84 Lead 11.6 8.74 11 14.6 10 11 11 14.6 10 11 14.6 Mercury 0.574 0.449 0.68- 0.421 0.654 0:68 0.68 0.421 0.654 0.68 0.421 Molyb denum 2.43 .8.02. 6.74 8A 8.6 6.74 6.74 8.84 8.6 6.74 8.84 Nickel 1744, 19.2 8.1 8.84 8.6 8.1 8.1 8.84 8.6 8.1 8.84 Selenium 6.89 832 6.74 8.84 8.6 6.74 6.74 1 8.84 8.6 6.74 8.84 Zinc 1290 1820 353 207 236 353 353 207 236 353 207 Total Phos- phorus 40300 59300 12300- 12200 3170 12300 12300 12200 3170 12300 12200 ival Heavy Metal Field Loadings (Calculated in lbs/acre): otal IJ L2J 3 L4J 6 L7J 8j 8 10 III-12 DT/Ac./ 0 App. Event 1.97 y Arsenic 0.000 0.012 - 0.000., 0.000 ' 0.000 0.000 0.000 0.000. 0.000. 0.000 0.000 0.000 0.012 Cadmium 0.000 0.012. 0.000.- -0.000 0.000 0.000 . 0.000 0.000 10.000 '0.000 0.000 0.000 0.012 Copper 0.000 -2.041 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 .0.000 0.000 0.000 2.041 Chromium 0.000 0.095 0.000 0.000 0.000, 0.000 0.000 0.000, 0.000 0.000 0.000 0:000 0.095 Lead 0.000 0.034 0.000 _ 0.000 0.000. 0.000 -0.000 0.000 0.000 .0.000 0.000 0.000 0.034 Mercury 0.000 0.002 0.000 0.000 -0.000 0.000. 0.000 0:000 0.000 0.000 0.000 0:000 0.002 Molyb- denum. 0.000 0.032 0.000 0.000 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Nickel 0.000 0.076 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.076 Selenium 0.000 0.033 0.000 0.000. 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.033 Zinc 0.000- 7.171 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 7.171 Total Phos- 0.000 233.642 0.000 0.000- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 233.642 horus I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and 1-nrisonme7r knowing violations". A-. Signature of Land plier Date DENR FORM MFLSF (12/2006) l ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: County of Brunswick Utilities WQ Permit #: WQ0023693 Field #: 1 Acres Utilized: 10.2 Land Owner: H Bell Annual Dry Tons Applied: 17,8951 Site #: HB Acres Permitted: 10.2 Operator: Same Predominant Soil Series: Goldsboro Cation Exchange Capacity (non 503): , ILT- . f, 1 no...,, A. Vrnn 1 Mar- PAN! 230 Crop 2 Name: Rye. Crop 2 Max. PAN: 50 Soil C Z Nitrate Name of Crop Type Volume applied Volume Residual Sources Cond: Preclp. d ;d TKN o and PAN Applied . ReceivingResidual +� (enter one) Solids/ % Applied per (NPDES #, WQ#, (D�' Past 24 o " ,� -* , ; F; ua o Nitrite lbs/acre ( ) Application c� o Liquid Solids Acre Fert., Animal Wet' Hrs. �, K * K' m * �' * e p A Cu. Yds Gallons (Dry Tons/Ac) Waste etc) Moist) inches * °n o o mg/kg- , mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 March 39000 1.47 CS Moist 0 S 0.5 0.3 76300 1080. 593 11.109 NA.' BG June 18500 0.95 .0.234 0.072. OR Moist 0 S 0.5` 0.3 49800 2440 509 2.290.. NA' BG 53000 1.07 0.232.'': ST Moist 0 S 0.5 0.3 37300 1420 25 , 5.332 - -, NA BG June 1.47 0.391, CS Moist 0 S 0.5 0.3 76300 1080 593 18,.800 'NA, BG June 66000 August 65000 1.47 0.30t CS Moist 0 S 0.5 0.3 76300 1080 -593 . ='48.515`. NA .. BG August 19000 0.95 0.074 OR Moist 0 S 0.5 0.3 49800 2440 509 . ;-2:352 :: NA : BG August 45500 1.07 0.199".. ST Moist 0 S 0.5 0.3 37300 1420 25 4:SZ7. NA :` BG March 26000 1.47 0.156: _ CS Moist 0 S 0.5 0.3 - 16300 1080 593 .. 7 406, ' `: NA BG 0.000 O':060` 0.000'. 0.600,. 0.000 0:000..0.000-:- `0:000 0.000 ' -`0.000 , 0.000 Residuals Applications totals on FORM FSF supp,( attach FORM FSF supp to this form): rOTALS• 0 3320010 As Cd Cu Cr Pb H Mo Ni Se Zn P 70.382 0:000 Lime A lied Annual lbs/acre 0.264 0.264 4.760 0376 0:396 , 0:023 : 0:264 ';,0297 , , 0.264: ' 11;177 359.888 Date lbs/ac Prior Years Cumulative lbs/ac 0.01 0.01 0.23 0.014 0.017 0 0.01 0.013 0.01 :. 0.274.: 89 0.505 11;.6$2 2498 Current Cumulative lbs/ac 0.274-. 0.274: ,.'.4.990 :..0.390 0.413 . 0:023 ,. 0.274 .... 0.310: Permitted C. P. L. R.**** 36 34 1338 267 15 374 Permit PAN Limit lst/2nd Crop 230 W. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accuruaucc w,tu a 1LA-Ar qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submittingfalse infortnati , including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation . / Volatilization Rates Surface - 0.5, Injectiontincorporation -1.0 ** Mineralization Rates: Compost 70.1, anaerobially digested -0.2, ignature of Land Applier Date aerobically digested -0.3; raw sludge -0.4. ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form -to be submitted in Annual Report Name: Brunswick County Total Dry Tans Applied (Annual): 182.63 Permit #: WQ0034513 Cation Exchange Capacity (non 503 only):,.. Operator: H Bell Owner: Same Predominant Soil Series: Goldsboro Acres Used: 10.2 Acres Permitted: 10.2 Site #: HB. Field #: 1 Residual Analysis Data.(Heavy Metals and Total -Phosphorus use mg/kg, % Solids 'use Raw Percent #): Sample or Com- posite Date 2 West 2 4 West 3 CS 4 OR 5 ST 8 CS 7 CS 8 OR " 9 ST 10 CS 11 12 - % Solids 4.08 3.34. 1.47 0.95 LOT 1.47 1.47 . 0.95 - 1.07. 1.47 Arsenic 10.4 2.99 6.74 8.84 8.6 6.74 6.74 8.84 8fi 6:74 Cadmium 2.43 2.99 6.74 8.84 8.6 6.74 6.74 8.84 -8.6 6.74 Copper 431 518 149 82.7 106, 149 149.- 82.7 106 149 Chromium 18.1 24.1 10.1 8.84 12.1 10.1 10.1 8.84 12.1 10.1 Lead 11.6 . 8.74 11 14.6 10 11 .' 11 14.6 10 . • 11 Mercury 0.574 : 0.449 0.68 0.421 0.654. 0:68 .0.68 0.421 OAM _ 0.68 Mol'yb- denum 2.43 " 8.02 6.74 8.84 8.6 6.74 6.74 8:84 . 8.6 6.74 Nickel 17.4 19.2, 8.1 8.84 8.6 8.1 8.1 8.84 8.6 8.1 . Selenium 6.89 8.32 6.74 8.84 8.6 6.74 6.74 8.84 8.6 6.74 Zinc 1290 1820 353 207 236 353 353 207 236 353 Total Phos- torus 40300 59300 12300 12200 3170. 12300 12300 12200 3170 12300 `Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total 1 2 _3j 4 5j 6j, 71 8j 10 j III 12 y DT/Ac./ App. it Event 2.39 0.73 2.37 - 4.05_. 3.99 - 0.75 2.03 1.59 Arsenic 0.000 .: 0:000:' : '0.031 .0.013 0 - 1, ..:A.055.-.: _0.054 -. .0.013. ' 0.035 ; 0.021" 0.000 : .` 0.000. ..0.264. Cadmium 0.000 0.000 . ; :0.032 ` 0:013, -, , 0 041. _ 0:0551. 'A:054:: ; .0.013. 0.035 .: 0:021:._ " 0:000':.:0.000 0.264- Copper _ 0:000: .,0.000:: 0312 ,-04121-,: -.OS02-" . 1.20T :if. 189 0.125- ;.0:430 : =0:474, .; 0.000: _.0:000.:.4360. hromiu 0:000 :.'.0.000' : 0.048:.: 0.013 _" .0:05T. ,0.082 : -.0:081: 0.013 0.040.. 0.032.--- 0.000-. 1_ 0.000`:. -, 0.376 Lead 0:000;. .,:0.000: OA53 . 0:021; :: :0:04T .:0:089:: 0,000' 0.396 Mercury 0.000 0.000.: 0.003 0.001 _ 0:003 : 0.606:.: 0.005, ...0.001= . 0.0031. .0.002 _ : 0.006 . O.00,Q " 0:023- Molyb- 0.000 "0.032 0:01`3 0.041 0.055 0.054 . 0.013: 0.035 0'.021 6 000" 0:000 . •0:264 denum .0.000 Nickel 0:000 : ' 0.000, 0.030 0.013. 0.041 . 0.066: , .0.065 ` 0.013 .., 0.035 • 0.026 '. '0.000 . 0.000< •; 0.297 Selenium 0.000. '0.000. 0.032 l 0.01-3 . 0:041. 0.055" 0.054 :_ 0:013 0.035.: 0.021. 0.000 0.000. 0:264. Zinc 0.000, 0.000 - 1.688 , 0.304 1.117 - 2.859 2:816 0.312 ' -0.958 1123 0:000'. 0.000 11,177 Total Phos- 0.000 0.000 58.811 17.919 15.003 99.615 98.11A 18.417 • 12.860 39.144 .0.000. 0:000' 359.888 horus , "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment felr knowing violations". Signature of Lan plier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: County of nswick>3t'lities WQ Permit #: WQ0023693 Field #: 1 Acres Utilized: 21 Land Owner: rdee ) Annual Dry Tons Applied: 6.7031. Site #: RH Acres Permitted: 21 Operator: Same Predominant Soil Series: Goldsboro Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda Grass Crop 1 Max. PAN: 230 Crop 2 Name: Wheat Crop.2 Max: PAN: 106 Volume applied Volume Residual Sources Soil Cond. Precip. ,oY C �_ Z Nitrate PAN Applied Name of Crop Type ReceivingResidual o o (enter one) Solids/ o /a pp per Applied r (N PDES #, WQ#, (y� Past 24 ° '° 1 ss TKN ° o and Nitrite lbs/acre ( ) Application �' o A Li uid Solids Acre Fert., Animal C , I. # °a * I Crop 2 Crop 1 Crop 2 Cu. YdsS Gallons (DryTons/Ac) Waste, etc) Moist) inches ti 0 mgikg mglkg mg/kg -Crop A.892 NA-;;. BG May 71500 1.47 0.209 - CS Moist 0 S 0.5 0.3 76300 1080 593 0.3 37300 1420 25 2:541' .:':. NA= BG May 52000 1.07 0.I10 . ST Moist 0 S 0.5 - 0:000 ` 0.000 0.000 ' 0.000 '. 0.000" • n nnn .. 0:000. 0.006 0.000,.. Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): rOTALs: o 1235001 As Cd Cu Cr Pb Hg Mo Ni . Se .: Zn P 12:433 ": ,:0.000 Lime APP lied lbs/ac Annua 1 lbs/acre 0.005 . 0.005 . .086 . 0.007 . 0:007 - : 0.000 ";` ;:: 0:005 , :.0 005' •: : 0.005:;` :: 019 _ :. ,: 5.831: ". ;:'.;. ''' .:'' - ':' :'., ; Date Prior Years Cumulative lbs/ac 0.013 0.031 0.316 0.019 0.021 0.001 0.013 . 0.018 0.014. 0.695 -urrent Cumulative lbs/ac 0.018 0.036 0.402, 0.026 ": 0.028 0.00t 0.018: ` .OA23 , 0.019, 0.894 Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2499 Permit PAN Limit lst/2nd Crop 230 106. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system. designed -to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, incl ing the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation J/ �4**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobiaily digested =0.2, Signat of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report _.:ility Name: Brunswick County Total Dry Tons Applied (Annual): 6.70 Permit #: WQ0034513 Cation Exchange Capacity (non 503 only): Operator: R Hardy Owner: Same Predominant Soil Series: Goldsboro Acres Used: 21 Acres Permitted: 21 Site #: RH . Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent: Sample or Com- posite Date 1 2 West 2 4 West rCS 4 OR 5 ST 6 CS 7 CS 8 OR 9 ST ' 10 CS 11 12 % Solids 4.08 3.34.47 0.95 1.07 1.47 1.47 0.95 1.07 1.47 Arsenic 10.4 2.99 6.74 8.84 8.6 6.74 6.74 8.84 8.6 6.74 Cadmium 2A3 2.99 6.74 8.84 8.6 6.74 6.74 8.84 8.6 6.74 Copper 431 518 149 82.7 106 149 149 82.7 106 149 Chromium 18.1 24.1 10.1 8.84 12.1 10.1 10.1 8.84 12.1 10.1 Lead 11.6 8.74 11. 14.6 10 11 11 14.6 10 11 Mercury 0.574 0.449 0.68 0.421 0.654 0.68 0.68 0.421 0.654 0.68 Molyb- denum 2 43 8.62 6.74 8.84 8.6 6.74 6.74 8.84 8.6 6.74 Nickel 17.4 19.2 8.1 8.84 8.6 8.1 8.1 8.84 8.6 8.1 Selenium 6.89 8.32 6.74 8.84' 8.6 6.74 6.74 8.84 8.6 6.74 Zinc 1290 1820 353 207 236 353 353 207 236 353 Total Phos- orus 40300 59300 12300 12200 3170 12300 12300 12200 3170 12300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 1 2j 3 41 51 6. 71 8 9 101 11 12 DT/Ac./ App. m Event 0.21 0.11 Arsenic 0.000.-'' 0.000 :. 0.003 0.0010'. 0.002- :-.0.000 0.000 -0.000 ' 0.000;- 0.000 0.000 0:000 0.005 Cadmium 0.000 0.000 0.003 0.000 0.002- 0.000. 0:000 _ ': 0.000 0 006 01,000 •0.000 0:0M 0.005 Copper 0.000 0.000- 0:062 . 0.000 0.023: ` 0.000 0.000 0.000 . 0:000 . 0.000 0.000 0.000 0:086 Chromium, 0.000, 0.000'- . 0:004 0.000.: 0'003-_ ; .:0.000' 0.000 0.000 0.000 0 000 0.000: : 0.000. _ 0.007 Lead 0.000' 0.000. - 0.005 0.000 0.002. -`0.000 - 0.000, 0.000 .0.000, ' 0A00 0:000 0.000 0.007, Mercury 1 0.000 0.000 1 0.000 0.000- 0.000. :'0.000 0.000 ' 0:000.. . 0.000-: = 0.000. 1 0.000• 0.000 0:000 - Molyb- 0.000. - 0.000 0.003. 0.000- 0.002 - .000. _-0.000' 0.000 0.000. 0.000. 0.000- 0.000- 0.005_ denum - . . Nickel 0.000 0.000'. 0.003 0.000.. 0.002 0.000' 0.000. .0.000., 0.000 0.000 - 0.000. - 0.000 0.005 Selenium .0-.000", '0.000 0.003 0.000_ .0.002. "0.000 .. 0.000 ..0.000 . _ 0.000 0.000 0.000, 0.000 .0.005 Zinc 0.000 0.000- . 0.148 0:000 0.052 0.000 0.000 0:000 0.000 ' 0.000 0.000 0.000 M99 Total Phos- -0.000 0.060 5.141 0.000 0.697 0.000 0.000 0.000- 0.000 0.000 0.000. 0.000 5.839 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Lanedplier Date DENR FORM MFLSF (1212006) M NCDASCS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomi/ Report No. FY15-SL023969 %. ,,.. Predictive Client: Denise Harrison Bio-Green Services Inc. Advisor. r _ ,�-�, •• ..' y 383 Potts Rd NC 27006 iw ehlich-3 Soil Report Extraction Advance, Sampled County: Brunswick. Sampled: 12/01/2014 Received: 12/22/2014 Completed: 02/09/2015 Farm: Brunswick Links to Helpful Information - Sample ID: BRHB1 Recommendations: Lime Nutrients (lb/acre) More crop (tonslacre) N P20s K20 Mg S Ma Zn Cu B Information ` Lime History: 1 -Bermuda hay/past., M 0.0 180-220' 0 130 - 0 0 0 0 0 0 Note: 12 2 -Small Grain (SG) 0.0 80-100 0 50 0 0 0 0 0 -0 Note: 3 Test Results [units - WN in g/cni; CEC and Na in meq/100 cd; NO3-N in mg/dOl: Soil Class: Mineral HM% WN CEC BS% Ac , pH P4 K-1 Ca% Mg% S4 Mn4 Mn-All Mn AI2 Zn-1- - Zn-AI Cu4 Na ESP SS4 - NO3-N 0.46 0.99 16.4 92 1.4 6.3 935 44 82 8 59, 59 47 40 1371 1371 364 0.2 1 Sample ID: BRCG1 Recommendations: Lime Nutrients (Iblacre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: CCU l 1 -Corn, grain 0.0 120 -160 0 0 0 0 pH$ 0 0 0 Note: 3 Note: 2 -Small Grain (SG) 0.0 80-100 0 0 0 0 pH$ 0 0 0 Note: 3 Note: Test Results [units - WN in g/cn?; CEC and Na in meq/100 cd; NO3-N in mg/dmP]: =.Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S4 Mn4 Mn4U1 Mn AI2 Zn-I Zn AI Cu4Na ESP SS4 NO3-N 0.60 1.08 19.4 96 0.8 6.7 1093 87 74 19 61 59 43 36 1278 1278 310 0.2 1 Sample ID: BRCG2 Recommendations: Lime Nutrients (Iblacre) More Crop (tonslacre) N P20s K20 Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.0 120 =160 0 20 0 0 pH$ 0 0 0 Note: 3 Note: 2 -Small Grain (SG) 0.0 80-100 0 20 0 0 pH$ 0 0 0 Note: 3 Note: Test Results [units - WN in glcrd; CEC and Na in meq/100 cd; NO3-N in mg/drO]: _ Soil Class: Mineral HM% WN CEC BS% Ac pH P4 K-1 Ca% Mg% S-1 Mn4 Mn-All . Mn Al2 Zn4 Zn-Al Cu4 Na ESP SS4 M03-N 0.92 1.14 13.3 93 1.0 6.5 714 69 76 14 54 68 50 43 767 767 205 0.2 2 Norlh Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Steve Troxler, Commissioner ofAgriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: ww.ncagr.govlagronomi/ w Report.No.. FY15-SL023969 Denise Harrison Page 2 of 5 Sample ID: BRCG3 �j Lime History: C� Recommendations: Lime Crop (tonslacre) 1 -Corn, grain 0.0 2 -Small Grain (SG) 0.0 N P205 120 -160 0 60-100 0 K20 40 40 Nutrients (lblacre) Mg S Mn 0 0 0' 0 0 0 Zn 0 0 Cu 0 0 B 0 0 More -Information Note: 3 Note: 3 Test Results [units - W1V in glcrr>3; CEC and Na in meg1100 curl; NO3-N in mgldn>1]: Soil Class: Mineral HM% WN CEC BS% Ac pH P4 K4 Ca% Mg% S4 Mn4. Mn-All Mn Al2 Zn4 Zn-Al Cu4 Na ESP SS4 NO3-N 1.25 1.15 7.9 Sample ID: . BRCH4 C�� Lime History: 84 1.3 6.0 277 48 Recommendations: Lime Crop (tonslacre) 1 -Corn, grain 0.0 2 -Small Grain (SG) 0.0 73 8 N P205 120- 160 0 80-100 0 39 73 K20 20 20 61 54 304 Nutrients (Ib/acre) Mg 5 Mn 0 0 Or 0 0 0 304 Zn 0 0 97 Cu U 0 0.1 .1 B 0 0 More Information Note: 3 Note: 3 Test Results [units - WN in gicrr?; CEC and Na in meg1100 cd; NO3-N in mg/daft Soil Class: Mineral HM% WN CEC BS% Ac pH P4 K-I Ca% Mg% S4 Mn-1 Mn-Ail Mn AI2 Zn4 Zn-AI Cu-I Na ESP SS4 NO3-N 0.86 1.18 15.0 Sample ID: BRCH6 Lime History: 94 1.0 6.6 833 69 Recommendations: Lime Crop (tonslacre) 1 -Corn, grain 0.0 2 -Small Grain (SG) 0.0 74 17 N P205 120 -160 0 80.400 0 - 53 67 K20 10 10 50 43 947. Nutrients (lb/acre) Mg S Mn 0 0 PH$ 0 0 PH$ 947 Zn 0 0 219 � Cu 0 0 ..0.2 B 0 0 1 More. Information Note: 3 Note: Note: 3 -Note: Test Results [units - WN in gicnr1; GEC and Na in meg1100 crirl; NO3-N in mgfdm&]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K4 Ca% Mg% S4 Mn4 Mn All MnAl2._ . Zn4 Zn-AI Cu4 Na ESP SS4, NO3-N 0.66 1.15 17.3 94 1.0 6.5 992 75 74 18 52 -- 56 43. 36 1114 1114 276 0.1 1 Sample ID: BRRH7 !1 Lime History: n Recommendations: Lime Crop (tonslacre) 1 -Corn, grain 0.0 2 - Small Grain (SG) 0.0 N P205 120 -160 0 80-100 0 K20 40 40 Nutrients (lb/acre) Mg S Mn 0 0 0 0 0 0 Zn 0 0 Cu 0 .0 B . 0 0. More Information Note: 3 'Note: 3 Test Results [units - WN in gfcn?; CEC and Na in meg1100 crrrl; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P4 K4 Ca% Mg%o S-1 Mn4 Mn-All Mn-AI2 Zn4 Zn-AI Cud Na ESP SS4 NO3-N 0.92 1.17 5.7 76 1.4 5.9 � 173 50 63 9 38 26, 33 ., 26 118 118 77 0.2 4 NCDABCs Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL023969 Denise Harrison Page 3 of 5 Sample ID: BRPV1 Recommendations: Lime Nutrients (Ib/acre) More ji Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: I 1 -Corn, grain 03 120-160 0 0 0 0 0 0 0 0 Note: 3 2 -Small Grain (SG) 0.0 80-100 0 0 0 0 0 0 0 0 Note: 3 Test Results [units - WN in g/crrrl; CEC and Na in meq/100 cd; NO3-N in mg/drrf]: Soil Class: Mineral HM% WN CEC BS% Ac pH P4 K-1 Ca% Mg% S-1 Mn4 Mn-All Mn-AI2 Zn4 Zn-AI Cu-I Na ESP SS4 NO3-N 1.87 1.02 7.6 71 2.2 5.7 339 118 57 6 47 41 42 35 453 .. 453' 145 0.2 3 Sample ID: BRPV2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: V 1 -Corn, grain 0.0 120 - 160 0 10 0 0 0 0 0 0 Note: 3 2- Small Grain (SG) 0.0 80-100 0 10 0. 0 0 0 0 0 Note: 3 Test Results [units - WN in g/crri3; CEC and Na in meq/100 cn7l; NO3-N in mg/do]: Soil Class: Mineral HM% WN CEC BS% Ac pH P4 K4 Ca% Mg% S4 Mn4 Mn-All . MnAl2 Zn-1 Zn-AI Cu4 'Na ESP SS4 NO3-N 1.61 0.93 9.2 87 1.2 6.2 162 73 74 9 54 _ 32 33 _ 26 215 215 " 77 0.2 _ 2 Sample RD: BRAH1 Recommendations: Lime Nutrients (Ib/acre) More 1' ( Crop (tons/acre) N P205 K2O . Mg S Mn Zn Cu B Information Lime History: (7 1 -Corn, grain 0.5 120 -160 0 10 0 0 0 0 2 0 Note: 3 2 -Small Grain (SG) 0.0 80-100 0 10 0 0 $pH 0 $ 0 Note: 3 Note: Test Results [units - WN in g/cnf ; CEC and Na in meq/100 crrrl; NO3-N in mg/d"PI: Soil Class: Mineral - HM% WN CEC BS% Ac pH P4 K-1 Ca% Mg% S4- Mn4 Mn-AI1 MnAI2 Zn4 Zn-AI Cu4 Na ESP SS4 NO3-N 1.25 1.10 6.6 78 1.4 5.7 68 78 65 8 58 25 32 .25 90 90 16 0.1 2 Sample ID: BRAH2 Recommendations: Lime Nutrients (lb/acre) More /�t� Crop (ton-slacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: Pro 1-Corn, grain 0.0 120 -160 0 10 0 0 0 0 0 0 Note: 3 2 -Small Grain (SG) 0.0 80-100 0 10 0 0 0 0 0 0 Note: 3 Test Results [units - WN in glcrrrl; CEC and Na in meq/100 crrrl; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S4 Mn4 Mn-All MnAl2• Zn-l- Zn-AI Cu-1 Na ESP SS4 NO3-N 1.02 1.13 6.9 82 1.2 6.0 140 74 61 16 45 34 37 30 162 . 162 85 0.1 1 NCDASCS Agronomic Division Phone: (919) 733-2655 Wehsite: -www.ncagr.goviagronomcl Report No. FY15-SL023969 Denise Harrison Page 4 of 5 Sample ID: BRAH3 Recommendations: Lime Nutrients (Ib/acre) Mom ?� Crop (tonsfacre) N P20s K20 Mg S Mn Zn Cu B Information Lime History: P 14" / 1 -Com, grain 0.0 120 -160 0 30 0 0 0 0 0 0 Note: 3 2 -Small Grain (SG) 0.0 80-100 0 30 0 0 0 0 0 0 Note: 3. Test Results [units - WN in glcn?; CEC and Na in meq/100 crr?; NO3-N in mgldn?]: Soil Class: Mineral HM°% WN CEC BS°% Ac pH P4 Kd Ca°% Mg°% S4 Mn-1 " Mn=All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS4 NO3-N 1.43 1.05 7.9 88 0.9 6.0 90 61 71 14 41 35 38 31 121 121 52 0.1 1 _._ NCDA&CS Agronomic Division Phone: (919) 733.2655 Website: www.ncagr.gov/agronomcl Report No. FY14-SLO12174 Page 2 of-3 Sample ID: brcg5 Recommendations: Lime Nutrients (lblacre) More "Information Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Lime History: , 1 - Bermuda haylpast., M 0.0 180-220 0 60 0 0 pH$ 0 0 0 Note: 12 Note: 2 - Bermuda hay/past., h 0.0 180-220 0 60 0 0 pH$ 0 0 0 Note: 12 Note: Test Results [units - WN in glcd; CEC and Na in meq/100 cd; NO3-N in mg/dirt?]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K4 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-1 Zn AI Cu4 Na ESP SS-1 NO3-N 0.36 1.17 11.6 . 96 0.4 6.9 628 77 83 10 44 42 29 29 684 684 236 0.2 2 Sample ID: brrhl Recommendations: Lime Nutrients (lblacre) More RA t Crop (tons/acre) N P20s " K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 0.5 180-220 0 130 0 0 0 0 0 0 Note: 12 2- Bermuda hay/past., A 0.0 180-220 0 130 0 0 0 0 0 0 Note: 12 Test Results [units -WIV in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/ddl: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S4 Mn-I Mn-AI4 Mn-AI2 Zn4 Zn-AI Cu-I Na ESP SS-1 NO3-N 1.67 1._12 8.0 82 - 1.4 5.7 80 43 73 7 42 25 32 32 104 104 86 0.1 1 Sample ID: brah3 Recommendations: Lime Nutrients (lb/acre) More Crop - (tons/acre) N P205 K20 Mg. S Mn Zn Cu B Information Lime History: 1 -SG/Soybean (DC) 1.0 80-100 110 70 0 0 10 6 2 0 Note: 3 2 -Small Grain (SG) 0.0 80-100 80 50 0 0 $ $ $ 0 Note: 3 Note: Test Results [units - WN in"g/cnf; CEC and Na in meg1100 crrr?; NO3-N in mg/dnf]: Soil Class: Mineral HM% WN CEC BS% Ac pH - P-1 K4 Ca% Mg% S4 Mn4 Mn-All Mn-Al2 Zn4 Zn-AI Cu4 Na ESPSS4 NO3-N 1.55 1.22 7.3 76 1.8 5.3 23 47 58 15 42 20 22 22 20 20 14 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733-2656 Website: www.ncagr.goviagronomit Kepout FW! r-1 Client: Bio-Green Services Inc. Advisor: 'In A Predictive 383 Potts- Rd Advance, NC-27006 Mehlich-3 Soil Report Extraction Sampled County: Brunswick Links to Helpful Information Sampled: 10/01/2013 Received: 10/22/2013 Completed: 11/04/2013 Farm: Brunswick, Sample ID: brcg . 1 Recommendations: Lime Nutrients (Iblacre) More C67i Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 - Bermuda hay/past., M 1.3 180-220 0 170 25 0 0 0 0 0 Note: 12 2-Bermuda hay/past., h 0.0 180-220 0 170 $ 0 0 0 0 0 hLo�tl 2 Hot@..j_a Test Results (units - WN in gicnf ; CEC and Na in meq/100 cnf; NO3-N in mg1dnfj: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn4 Mn-Ali Mn-Al2 Zn-I Zn-Al Cu-1 Na ESP SS4 > NO3-N 0.97 1.13 6.3 64 2.2 5.1 279 26 57 6 42 71 60 . 60 ' - 299 299 144 0.1 2 Sample ID: brcg6 Recommendations: Lime Nutrients (lb/acre) More tC-i (p crop (tans/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past, M 0.3 180-220 0 110 0 0 0 0 0 0 Note: 12 2-Bermuda hay/past., K 0.0 180-220 0 110 0 0 0 0 0 .0 - Note: 12 Test Results [units - W/V in g/cfO; CEC and',Na in meq/100 cn13; NO3-N in mgldnf]: S oil Class:- Mineral HM% WIV CEC BS% Ac pH P4 K4 Ca% Mg% . S4. Mn'-I Mn-All Mn-Al2 - Zn4, Zn-Al Cu4. - Na ' ESP. SS4 NO3-N 0.86 1.26 8.4 78 1.8 5.9 587 53 48 27 59.. 20 29 29 225 225 78 0.1 Sample ID: brhbl Recommendations: Lime Nutrients (lb/acre) More . Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu S. Information Lime History: 1-Bermuda hay/past., AA 0.0 180-220 0 160 0 0 pH$ 0 0 0 Note: 12 Note: 2-Bermuda hay/past., h 0.0 180-220 0 160 0 0 PH$ 0 0 0 Note: 12 Not I pL Test Results [units - W/V in g1cnf; CEC and Na in meq/100 cnf NO3-N in mg/drift Soil Class: Vineral. HM% WIV CEC BS% Ac pH P4 K4 Ca% Mg% S-I Mn4 Mn-All Mn-Al2 Zn-I Zn-Al Cu4 Na ESP SS4 'NO3-N 0.36 1.15 24.3 97 0.6 6.7 1288 30 90 7 1 74 75 51 51 1351 1351 232 - '0.2 North Carolina A. Reprogramming of the laborat6ry-information-management system that makes this report possible is being funded, through a grant from. the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. St6ve.Troxler, Commissioner of Agriculture * NOTE — Lime stabilized biosolids are being added to the soil to raise pH.