WQ0034468_Residual Annual Report 2014_20150218

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2014 ANNUAL REPORT
LAND APPLICATION PROGRAM
COUNTY OF BRUNSWICK PUBLIC UTILITIES
PERMIT #WQ0034468
Compiled By:
Bio-Green Services, Inc.
383 Potts Road
Advance, NC 27006
January 2015
RECIFIVED
FEB 18 '2015
DVVR Z)&TION
INFORMATION PROCESSING UNIT

January 1, 2015
NCDENR-DWR
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attention: Information Processing Unit
Reference: 2014 LAND APPLICATION ANNUAL REPORT
County of Brunswick Public Utilities
Permit No. WQ0034468
Non -Discharge Compliance Unit:
Bio-Green Services, Inc. (Bio-Green) is submitting all monitoring and reporting requirements as
specified in the above referenced permit. Bio-Green compiled this report using data gathered
during the.compliance year by Bio-Green and the County of Brunswick Public Utilities. This
data includes:
1) Certification Form required by permit
2) Residuals Analysis and PathogenNector Data
3) Application Summary
If there is any further information required or questions regarding this annual report please do
not hesitate to contact Bio-Green for further assistance.
Sincerely,
Ray Gambill
NC Land Application/Residuals Operator

January 1, 2015
EPA Region 7
ATTN: BIOSOLIDS CENTER
WWPD /WENF
11201 Renner Boulevard
Lenexa, Kansas 66219
Reference: 2014 LAND APPLICATION ANNUAL REPORT
County of Brunswick Public Utilities, North Carolina
Permit No. WQ0034468
Bio-Green Services, Inc. (Bio-Green) is submitting all monitoring and reporting requirements as
specif ed in the above referenced permit. Bio-Green compiled this report using data gathered
during the compliance year by Bio-Green and the County of Brunswick Public Utilities. This
data includes: 1) certification form required by permit, 2) residuals analysis and pathogen/vector
data, and 3) application summary.
The County of Brunswick Public Utilities conducted application events in Brunswick County
within the year of 2014. During 2014, A total of 444.03 Dry Metric Tons of residuals, solids were � V -
land applied (Northeast Brunswick Regional WWTP land applied 145.71 Dry Metric Tons and
West. Brunswick Regional WWTP land applied 298.32 Dry Metric Tons).
If there is any further information required or questions regarding this annual report please do
not hesitate to contact Bio-Green for further assistance.
Sine ly,
Ray G ill
NC Land Application/Residuals Operator

County of Brunswick Public Utilities
PO Box 249
Bolivia, North Carolina 28422
910-253-2659
NORTHEAST BRUNSWICK REGIONAL WWTP
NPDES # NC0086819
WEST BRUNSWICK REGIONAL WWTP
NPDES # WQ0023693
NC PERMIT # WQ0034468
Mr. Donald Dixon
Water Reclamation System Superintendent
PO BOX 249
Bolivia, NC 28422.
910-253-2485
LAND APPLIERS.
Bio-Green Services, Inc.
383 Potts Road
Advance, North Carolina 27006,
2014'Northeast Brunswick Regional WWTP Dry Tons 160.655
2014 West Brunswick Regional WWTP Dry Tons 328.91
Total Dry Tons 489.565
2014 Northeast Brunswick Regional WWTP Dry Metric Tons 145.71
2014 West Brunswick Regional WWTP Dry Metric Tons 298.32
Total Metric tons 444.03

A X-]K"JJiJ Vt' � viI a—q a"
SECTION NO.
I
II
III
TITLE
Certification Form
Residuals Analysis & Pathogen / Vector
Attraction Data
2014 Application Summary

WEST BRUNSWICK WWTP

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0034468 FACILITY NAME: West Brunswick
PHONE: [phone] COUNTY: Brunswick OPERATOR: Ron Worthington
FACILITY TYPE (please check one): CJ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
Distribution and Marketing (complete Parts A,.B, and C)
Was the facility in operation during the past calendar year? Yes No ❑ --► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Reci lent information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
West Brunswick WQ0023693
6.35
6.35
J Tennant
6.35
Fertilizer
March
West Brunswick WQ0023693
6.35.
6.35
J Tennant
6.35
Fertilizer
April
West Brunswick WQ0023693
14.37
14.37
J Tennant
14.37
Fertilizer
May
West Brunswick WQ0023693
3.31
3.31
C Galloway
3.31
Fertilizer
June
West Brunswick WQ0023693
19.9
19.9
H Bell
19.9
Fertilizer
July
West Brunswick WQ0023693
-10.57
10.57
M McKeithen
10.57
Fertilizer
August
West Brunswick WQ0023693
19.38
19.38
H Bell
19.38
Fertilizer
September
West Brunswick WQ0023693
.3.52
3.52
C Galloway
3.52
Fertilizer
October
West Brunswick WQ0023693
14.48
14.48
P Vereen
14.48
Fertilizer
November
West Brunswick WQ0023693
19.91
19.91
P Vereen
19.91
Fertilizer
December
West Brunswick WQ0023693
Total from FORM DMSDF (sup)
0
210.77
210.77
210.77
Totals:
Annual (dry tons):,
0
328.91
328.91
328.91
Amendments used: 1 Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No ► if No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penal ' r submitting false information, including the possibility of fines and imprisonment for knowing violations."
i/1/2015
Signa!ZRo FenWidj Date Signature ofPreparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING[ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0034468 FACILITY NAME: West Brunswick
PHONE: [phone] COUNTY: Brunswick OPERATOR: Ron Worthington
FACILITY TYPE (please check one): ® Surface Disposal (complete Part A -"Month", "Source(s)" and "Residual In" columns only)
C7 Distribution and Marketing (complete Parts A. and B)
Part A*:
Part B*.
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume
tons)
Intended use(s)
March
West Brunswick WQ0023693
5.56
5.56
J Tennant
5.56
Fertilizer
March
West Brunswick WQ0023693
9.53
9.53
J Brown
0.53
Fertilizer
March
West Brunswick WQ0023693
2.38
2.38
P Vereen
2.38
Fertilizer
March
West Brunswick WQ0023693
14.29
14.29
H Bell
14.29
Fertilizer _
April
West Brunswick WQ0023693
16.59
16.59
W Roach
16.59
Fertilizer
April
West Brunswick WQ0023693
18.8
18.8
W Roach
18.8
Fertilizer -
April
West Brunswick WQ0023693
16.58
16.58
C Galloway
16.58
Fertilizer
June
West Brunswick WQ0023693
•11.05
11.05
M McKeithen
11.05
Fertilizer
June
West Brunswick WQ0023693
4.42
4.42
H Bell
4.42
Fertilizer
June
West Brunswick WQ0023693
12.16
12.16
H Bell
12.16
Fertilizer
June
West Brunswick WQ0023693
33.17
33.17
A Vereen
33.17
Fertilizer .
July
West Brunswick WQ0023693
10.57
10.57
A Vereen
10.57
Fertilizer
August
West Brunswick WQ0023693
28.18
28.18
H Bell
28.18
Fertilizer
September
West Brunswick WQ0023693
11.45
11.45
C Galloway
11.45
Fertilizer
September
West Brunswick WQ0023693
8.8
8.8
P Vereen
8.8
Fertilizer
November
West Brunswick WQ0023693
7.24
7.24
A Hughes
7.24
Fertilizer
Totals:
Annual (dry tons):
0
210.77
210.77 210.77
Amendment(s) used: 1
* If more space is required, attach additional information sheets (FORM DMSDF
Bulkin Agent(s) used:
(supp)): Total Number of Form DMSDF (Supp)i 1
DENR FORM DMSDF (Supp) (12/2006)

NORTHEAST BRUNSWICK WWTP

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
VQ PERMIT #: WQ0034468 FACILITY NAME: North East Brunswick
PHONE: [phone] COUNTY: Brinswick OPERATOR: Ron Worthington
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A; B, and C)
Vas the facility in operation during the past calendar vear?- Yes ® No ❑ —► If No skip parts A. B, C and certify form below
Part A*:
Part B*:
Month
Sources() ( s include NPDES # if
applicable)
Volume (d tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
anuary
'ebruary
larch
NE Brunswick NCO08619
24.369
24.369
H Bell
24.369
Fertilizer
,pril
NE Brunswick NCO08619
14.441
14.441
C Galloway
14.441
Fertilizer
lay
NE Brunswick NCO08619
3.61
3.61
L Roach
3.61
Fertilizer
une
NE Brunswick NCO08619
27.98
27.98
A Vereen
27.98
Fertilizer
my
mgust
NE Brunswick NCO08619
9.025
9.025
C Galloway
9.025
Fertilizer
eptember
NE Brunswick NCO08619
27.98
27.98
C Galloway
27.98
Fertilizer
October
lovember
tecember
NE Brunswick NCO08619
2.707
2.707
P Vereen
2.707
Fertilizer
Total from FORM DMSDF (sup)
. 0
50.543
50.543
50.543
otals:
Annual (dry tons):
0
160.655
160.655
160.655
Amendment(s) used:1 I Bulking A ent(s) used:
If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)r
'art C:
'acility was compliant during the past calendar year with all conditions of the land application .permit ❑ Yes
including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No —► if No, Explain in Narritive
All monitoring was done in accordance with the permit and reported for the year as required and three (3)'copies of certified laboratory results are attached.
All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
ienaltiessfforsubmitting false information, including the possibility of fines and imprisonment for knowing violations."
signature of
I'l5�
Date -
(if different tom Permittee)
"*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
1/1/2015
Date

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0034468 FACILITY NAME: North East Brunswick .
PHONE: [phone] COUNTY: Brunswick OPERATOR: Ron Worthington
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A "Mouth", "Source(s)" and "Residual In" columns only)
r1 Distribution and Marketing (complete Parts A. and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
.
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
kpril
NE Brunswick NCO086819
18.051
18.051
L Roach
18.051
Fertilizer
Fune
NE Brunswick NCO086819
10.831
10.831
H Bell
10.831
Fertilizer
)ecember
NE Brunswick-NCO086819
9.025
9.025
C Galloway
9.025
Fertilizer
)ecember
NE Brunswick NC0086819
12.636
12.636
C Galloway
12.636
Fertilizer
[ otals:
Annual (dry tons):
0
50.543
50.543 50.543
Amendments used:1
If more space is required, attach additional information sheets (FORM DMSDF
I Bulking-Agent(s) used:
(supp)): Total Number of Form DMSDF (Supp) 1

WEST PRUNSWICK WWTP

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF -.B
WQ Permit Number: WQ0023693
Facility Name: County Of Brunswick Utilities
Residual Source WQ # or NCO086819
NPDES #:
WWTP Name: West Brunswick
i2aeia»gl Analveie "ata
Laboratory: - 1) Environmental Chemists Inc.
2)
3)
4)
5)
Parameter
-(mg&g)
Conc.
Limit
m k a
Sam le or -Composite Date
1/8/14
4/28/14
7/30/14
11/12/14
Percent Solids (%)
NA
2.93
4.08
3.25
3.34
Arsenic
75
33.4
10.4
2.55
2.99
Cadmium
85
33.4
2.43 .
2.55
' 2.99
Copper
4,300
567
431
437
518
Chromium
NA
39.6
18.1
22.9
24.1
Lead
840
33.4
11.6
9.57
8.74
Mercury
57
0.717
0.574
0.769
0.449
Molybdenum
75
33.4
.2.43
8.68
8.02
Nickel
420
33.4
17.4
20
19.2
Selenium
100
33.4
6.89
6.8
8.32
Zinc
7,500
1630
1290
1540
1820
Total Phosphorus
NA
52300
40300
57200
59300
TKN
NA
69300
69300-
68900
81600
Ammonia -Nitrogen
NA
45700
38800
60900
50300
Nitrate and Nitrite
NA
75.5
3.68
21.6
0.6
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in- accordance with a system designed
to as, a that qualified personnel properly gathered and evaluated the information- submitted. I am aware that there are significant
p alties or sub g false information, including the possibility of ,fines and imprisonment for knowing violations."
-14
Signature of r parer * Date
*Preparer is fined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006)

;' COUNTY OF BRUNSWICK PUBLIC .UTILITIES LAND APP- L
` RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 8, 2014 1st quarter
�- .West WWTP Permit No.
Mineralization rate 0.30 2.93% Solids
7.52 nH
)N PROGRAM
NCO044873
ier .':
°!o ,
PPM I�*10.0001
LbslDrvTon 7MglKa' b.0021 :
PAN Surface _
30005.5
60.011
PAN Injection
68865 . '
137.73
TKN.
69300
138.E
Ammonia Nitrogen (Am)
45700
91.4
NitrateN(trogen (Nin)
75.5
0,151
Organic Nitrogen (Orn)
0
0
Total Phosphorus(P)
52300
104.6
Total Phosphate(P205)
0
0
Estimated Avail. P205
0
0
Total Potassium (K)
5120
10.24
Total Potash (K20) ,
0
0
Arsenic (As)
33.4
0.'0668
Cadmium (Cd)
. 33.4
0.0668
Chromium (Cr)
39.6
0.0792
Copper (Cu)
567
1.134
Lead (Pb)
33.4
0.0668
Mercury (Hg)
0,717
0.001434
Molybdenum (Ma)
93.4
0.0668
Nickel (NI)'
.33.4
0.0668
Selenium (Se)
33.4
0.0668
Zinc (Zn)
1630
. 3.26
Aluminum (AI)
78300
156.6
Calcium (Ca)
26500
53
Iron (Fe)
0
0
Sodium (Na)
3080
6.16
Sulfur (5)
0
0
Magnesium (Mg)
8190
16.38
Manganese (Mn)
01
0
'Environmental Chemists, Inc. 2014-00289
*Determination of Plant Available Nitrogen (PAN):
( Injected Application:
`Rate TKN-Ammonia N + + +
(Mineralization
( )( i ) Ammonia N Nitrate N Nitrate N - %PAN
Surface Application
I_F (Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N)•+ Nitrate N +Nitrate N - % PAN
Note; Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes.
6500 load .794 lb per load = 47.659 lb PAN per load Surface / 124.301
4500 load .549 lb per load = 32.994lb PAN per load Surface / 85.943
I�I t

COUNTY OF BRUNSWICK ++ West Brunswick-Regional.Laboratory
Public Utilities Department 235 Grey Water Road
Wastewater Treatment Division Supply, NC 28482 .
�9AI CA Phone: [phone]' Fax: [phone] ,
Sample 'Collection and Chain of Custody CS
CollectedBy: G • 4a G . Report No.: 9 .
Sample Tvoe: I = Influent. E = Effluent, W = Wen, ST = Stream, SO '= Soil, SL = Sludge Other.
aim
Nam
MEN
MEMO
,.�►��■■ems
MEEM
I
MOORE
R
r ma
09
0
M
0
M
M
000A
MEAN!
OEM
ATTENTION: Samples submitted for analysis for Ammonia, TKN, Cyanide, Phenol and all Baclesiologicais must be dechiorinated to:S 0.2 ppm at time of collection.
Transfer
Relinquished By:
Date/Time
Received By:
I Dateffime
.2
Temperature when Rece • Accepted: - V���)))) Rejected- Resample Required: t
Delivered B . � ,� e
Comments: (ji/ Y

-
Environmental Chemists, Inc.
indm!23Way(LaW(9fli0 gton, NC 28405
-renvirochem6602
2h (Fax)
710.Boivsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL $ CONSULTING
CHEMISTS
NCDENR; DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Brunswick County Public Utilities
Date of Report: Jan 16, 2014
—' Post Office Box 249
Customer PO #:
Bolivia NC 28422,
Report #: 2014-00265
Attention: Donald Dixon
Report to: Donald Dixon
Project ID: West Brunswick Regional WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
- 14-00599 Site: # 1
1/8/2014 10:06 AM Solid/Sludge Gordon Call
i Test
Method Results Data Analyzed
J Total Solids, (°lo)
SM 2540 ra 3.13 % 01/10/2014
Fecal Density
SM92210EMPN 24hr503 <7 MPN/9 01/09/2014
-f Lab ID Sample ID:
Collect Dateltime Matrix Sampled by
14-00600 Site: # 2
1/8/2014 10:07 AM Solid/Sludge Gordon Call
Test
Method Results Date Analyzed
Total Solids (o/o)
SM 2s4o a
3.06 % 01110/2014
Fecal Density
SM 9221C E MPN 24 hr 503
<7 MPN/g 01/09/2014
Lab ID Sample ID:
Collect Date/Time
Matrix . Sampled by
L 14-00601 Site: # 3
1/8/2014 10.08 AM
Solid/Sludge Gordon Coil
}
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2640 B
3.17 % 01/10/2014
Fecal Density
SM 92210 E MPN 24 hr 503
<7 MPN/g 01/09/2014
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
14-00602 Site: # 4
1/8/2014 10:09 AM
Solid/Sludge Gordon Call
Test
Method
Results Date analyzed
Total Solids (%)
SM 2540 B
2.99 % 01/10/2014
Fecal Density
SM 9221C E MPN 24 hr 603
<7 MPN/g 01/09/2014
Lab ID _ Sample ID:
14-00803 Site: # 5
Collect DateMme Matrix Sampled by
1/8/2014 10:10 AM Solid/Sludge Gordon Call
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 a
2.96 %
01/10/2014
Fecal Density
SM 9221C E MPN 24 hr503
<7 MPN/g
01109/201.4
Report#:: 2014-00265 Page 1 of 2

- Environmental Chemists, Inc.
-' 6602 Windmill Way - Wilmington, NC 28405
r 0 [phone] (Lab) - [phone] (Fax)
— sr+ 710 Bowsertown Road a Manteo, NC 27954
--- [phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
f Brunswick County Public Utilities Date of Report: Jan 16, 2014
Post Office Box 249 Customer PO #:
Bolivia NC 28422 Report M 2014-00265
Attention:. Donald Dixon Report to: Donald Dixon
- Project ID: West Brunswick Regional WWTP
Lab ID D: Sample Collect Date/Time Matrix Sampled b
p p P y
14-00604 Site: # 6 1/8/2014 10:11 AAA Solid/Sludge Gordon Call
rf
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 3.01 % 01/10/2014
Fecal Density SM 92M E MPN 24 hr 603 <7 MPN/9 01/09/2014
Lab 913 Sample ID: Collect DatelTime Matrix Sampled by
14-00605 Site: # 7 1/8/2014 10:12 AM Solid/Sludge Gordon Call
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.97 % 01/10/2014
Fecal Density SM 9221 C E MPN 24 hr 503 <7 MPN/g 01 /09/2014
Comment: Reported on a dry weight basis.
Reviewed by:
Report*.: 20%00295 Page 2 of 2

F
Partial Report
AWAAXTKAL,
5500BLrsinusgDr. US-28405-Wiln*qton.NC t+19103501903 f+19103501657 www.egs.cDjn
Mi:mbrsfd the SGS atop (M SW
Page 10 of 23

An11UAU rAijavtx `n Anju VU'%-itvim Al LLIA%.lLVl\ mnjuUl.11Vl\ r%jn1VL koui nuics)
Facility Name: County of Brunswick Utilities WQ Permit Number: WQ0034468
WWTP Name:. West Brunswick Regional WWTP NPDES Number: WQ0023693
Monitoring Period: From 1/1/2014 To 3/31/20.14
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative nerformed:
Class A:
Alternative 1 ❑
Alternative 2 ❑..
Alternative 3 ❑
Alternative.4 ❑
Alternative 5
Alternative 6 ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost ❑
Heat Drying ❑ Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ra Pasteurization ❑ ❑
Class B:
Alternative 1 ❑ Alternative 2: 0
;>;>;::::::.:::<<:
If applicable to alternative
performed (Class B only) Indicate"Process to Significantly
Reduce Pathogens":
Lime Stabilization, ❑
Air Drying❑ .
Composting ` ❑
jAerobic Digestion El
Anaerobic
c Digestion g
e ton
If applicable to alternative perfbrmed Class A. or Class 13complete the following
monitoring data:
Parameter
Allowalile.Level
in Sludge
in
Pathogen Density
Number o
Excee-
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
nioue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per bf
totals lids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3. MPN per 4 grams
total`solid (dry
weight)
vector Attraction Reduction (40 Cr'K 503.33) - Please indicate option performed:
Alt.l .(VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (M-day bench) EAJAft
4 (Spec. O, uptake)
❑
Alt. 5 (14-D4y Aerobic)
❑
Alt. 6 (Alk Stabilization
❑
Alt 7 (Drying - Stable) ❑
JAR. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met ".
® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer Name and Title (type or print)
'
j Signature & Preparer*' Date
__R a;�� (r_5��M 6"A V_L
Land 'Applier a and-itle-(if applicable)(type or print)
Signature of Land Applier (if applicable) Date
- *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

CountY ol'Brim.swick Pt ' iblic Utilities
Wes; BrUtowick Reoinnal Facility La lvaratory
"Fillijy Day li-orich i `WZQ I d Pei.) Alfia-uov is K Lot ^O*IXFAI
biqe5lor lzira�p Tiff-s!
as Owl ptoi-1 r, hlf.,rw OrOlon
WWTP -,-3
MIMI
14 ft

Legend
Name
WBWW11 Atad Tank No.3
Temperature
Start End Duration Scale Units Min Max Avg
1/21/2014 9:44:22 AM" V24/2014 9:44:22 AIVI, ,„3d,00:00:00;_ 120,-150t3eg F 132.430116 ,138.507 64;, 134.056502
�•�O ���,5 � lQss�
i�4ts
1
AM
Page j
�C-

I
1
2/3/2014 7 00.00 PM 2/412014 3.00.00 AM
2/4/2014 11.00 00 AM
2/412014 7:00 00 PM 2/5/2014 3 OD-00 AM
Legend
Name Start End Duration Scale Units Min Max Avg
WBUU1N11 Atad Tank NO-3 2/3120� 12:55:Q0 PM 6:59:23A Md1;0:23- 2„.8Q125i32498t3t 4
Temperature
.t
` All � C� 1. � -��; ..�.) �.-�`,i�Lf/'� -�- ^ • r
Page 1
c._.. r

Legend Name Start End Duration Scale Units Min Max Avg Std Deviation
WBWW11 Atad Tank NOA W712014 12:51:22 AM 302014 12:51:22 AM 1d00:00:00 32-212 Deg 134.74398 136.8112`17 135.860525 0,597332
UM
Temperature
Page I

COUNTY OF BRUNSWICK West Brunswick Regional Laboratory
Public Utilities Department 235 Grey Water Road
Wastewater Treatment Division Supply. INC 28462
Phone: [phone] Fax: [phone] //�� Sample Collection and Chain of Custody i �r]
Collected By: lS .. Report No.: 1 1
Sample Type: 1= Influent, E = Effluent, W = Well. ST = Stream. SO = Sall, St. = Sludge Other.
ATTENTION; Samples suhrdtted foram1pis forAmmork, Tl%Cyanide, Phenol"all BaUeri lcels must be deohtwfnated toe 02 ppm et lime ofcoeeclion.
Temperature when Rac G 4�V�A&Aepted:�Reswnpta Re*red
Delve
Co ts: Ph was

D
L
F�
Environmental Chemists, Inc.
envir 6602 Windmill Way • Wilmington, NC 28405
ochem [phone] (Lab) -. (910) 3924424 (Fax)
710 Bowsertown Road * Mante6, NC 27954
.[phone]
ANALYTICAL &66NsULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. US CERTIFICATE #37729
Brunswick County Public Utilities
Date of Report- Feb 19, 2014
Post Office Box 249
Customer PO #.
Bolivia NC 28422
Report 2014-00289
Attention: Donald Dixon
-
Report to: Donald Dixon
TC L10
Project ID: West Brunswick Regional WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14,00656 Site: Sludge
118/2014
10:16 AM Solid/Sludge Gordon Call
Test
Method
Results Date Analyzed
ChlordaneI
SW846*1 Method 8081813510
.<0.005 mg/L
01/23/2014
Endrin
$Wfk6 Method 8081W610
<0.00006 mg/L
01/23/2014
Heptachlor
SW046 Method 8081BMIO
<0.00005 mg/L
01123/2014
Heptachlor epoxide
SW Method 80811313610
<0.00005 rng&
01123/2014
Lindane
SW 846 Method 8081913510
<0.00006 mg/L
0112312014
Meth6xychlor
SW 840 Method 0081 B/351 0
<0.00005 mg/L
01/23/2014
Toxaphene
SW 846 Method 8081 81351 0
o4006 mg/L
01/23/2014
1,4-Dichlorobenzene (TCLP)
3W846method 8270W10
<0.050 mg/L
01/23/2014
2,4,5-Trichlorophenal (TCLP)
SW 846 method 82i0J351 0
<0.050 mg/L
01123/2014
2,4,6-Tnchlorophenol (TCLP)
SWW method 8270/3610
<0.050 mg/L
01/2312014
2,4-Dinitrotoluene (TCLP)
SW 846 method 827013510
<0.050 mg/L
01123/2014
Cresol (TCLP)
SW 846 method OV013610
<0.060 mg/L
01/23/2014
Hexachloro-1,3-butadiene (TCLP)
6W.846 method 8270=10
<0.050mg/L
01/23/2014
Hexachlorobenzene (TCLP)
SW 846 method 027OM51 D
-<0.050 mg/L
01123/2014
Hexachloroethane (TCLP)
SW 84e method 0270/3510
<0.050 mg/L
01/23/2014
rn + p-Cresol (TCLP)
SW 846 method 827013610
<0.050 mg/L
01/23/2014
Nitrobenzene (TCLP)
SW846 method $27013510
<0.050 mg/L
01123/2014
o-Cresol (TCLP)
SW 040 method 827o/3510
<0.050 mg/L
0112312014
Pahtachlorophenol (TCLP)
SWO40method 827013510
<0.250 mg/L
0112312014
Pyridine (TCLP)
SW846method S27013510
<0.050 mg/L
01/23/26114
2,4,5-TP
SWW Method 8151A
<0.0003 mg/L
01/28/20-14
2,4-D
SW848 Method 8161A
<0.0003 mg/L
0111284014
1,1-DIGhloroethylene
SW846 Method 826016D30
< 0.01 mg/L
1/29/2014
1,2-Dichloroethane
SWOO Method 11280/560
< 0.01 mg/L
1129/2014
Benzene
SWU8 Method 8280/=0
< 0.01 mg/L
1/29/2014
Carbon Tetrachloride
SW846 Method 8260/5030
< 0.01 mg/L
1129/2014
Report #.: 2014-00289
Page 1 of 3

Environmental. Chemists, Inc.
envirochem
6602 Windmill Way. • Wilmington, NC 28405
L
[phone] (Tab) ,• (910) 392-M24 (Fax)
sM
710 Bowsertown Road • Manteo, NC 27954
-- ,
[phone]
ANALYTICAL & CONSULTING
CHEMIS S
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE ##37729
Brunswick County Public Utilities
Date of Report:. Feb 19, 2014
_- Post Office Box 249
Customer PI, #:
Bolivia NC 28422
Report #: 2014-00289
Attention: Donald Dixon
Report to: Donald Dixon
Project ID,, West Brunswick Regional WWTP
Chiorobenzene
SWe48 Method 82,6015030
<. 0.01 mg/L
1/29/2014
-' Chloroform
SW84a Method 32e0reo3o
< 0.01.mglL
1./291201.4
Methyl ethyl ketone
Sw54e Method 8=16030
< 0.05 mg/L
1/29/2014
ITetrachloroethylene
SWW Method 8280a030
< 0.01 mg/L
1129/2014
Trichloroethylene
SW846 Method e2MIao3o
0.01 mg/L
1/29/2014
Vinyl Chloride .
OWM Method 8260/5030
< 0.01 mg/L
1/29/2014
RCI
Cyanide
EPA335.4
<0.135 mg/kg
01/31/2014
pM
SM4500. H 8
7.52 Units
01/10/2014
Sulfide
SM4500 S o
13.8 mg/kg
02/03/2014
Ignitability
Sw a4e method 1010
>212 OF
01/14/2014
Sludge Residuals
Aiumi'nurn
EPA200.7
78300 mg/kg
02/03/2014
Arsenic
EPA Za0.7
<33.4 mg/kg
01/22/2014
Cadmium
EPA200.7
<33.4mg/kg
01/22/2014
Calcium
EPA2063
26500mg/kg
01/20/2014
_ Chromium
EPA 2003
39.6 mg/kg
01/22/2014
Copper
VA20.7
567 mg/kg
01l22/2014
-- Lead
EPA200.7
" <33.4mg/kg
01/22/2014
Magnesium
EPA2000.7
8190mglkg
01/20/2014
Molybdenum
EPA 200.7
<33.4 mg/kg
01/22/2014
Nickel
EPA200.7
<33.4mg/kg
01/22/2014
f, Potassium
EPA200.7
5120mg/kg
01/20/2014
Selenium
EPA200.7
<33Amg/kg
01/2412014
Sodium
EPA200.7
3080 mg/kg
01/20/2014
-h Zinc
EPA200.7
1630 mg/kg
01/24/2014
- Ammonia Nitrogen
EPA350.1
45700mg1kg
01/15/2014
` Total Kjeldahl Nitrogen (TKN)
EPA 3512
69300mg/kg
01/20/2014
Nitrate+Nitrite-Nitrogen
EPA 353.2
75.5 mg/kg
02/03/2014
ReportA: 2014.00289 Page 2 of 3

Environmental. Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Brunswick County Public Utilities
Date of Report:, Feb 19, 2014
Post Office Box 249
Customer PO #:
Bolivia NC 28422
Report #: 2014-00289
Attention: Donald Dixon
Report to: Donald Dixon
--'
Project ID: Vilest Brunswick Regional WWTP
Total Solids (%)
SM 2540 B
2.93 %
01110/2014
Total Phosphorus
sM 4500 P F
52300 mg/kg
01/21/2014
Mercury
sw8487471.B
0.7170mglkg
01/17/2014
TCLP Metals
Arsenic
EPA 200.7
<0.100 mg/L
02/03/2014
Barium
EPA 200.7
<0.100 mg/L
02/01 /2014
Cadmium
EPA 200.7
<0.100 mg/L
02/03/2014
Chromium
EPA 200.7
<0.100 mg/L
02/03/2014
Lead
EPA 2001
<0.100 mg/L
02/03/2014
Selenium
EPA 200.7
<0.100 mg/L
02/03/2014
Silver
EPA 200.7
<0.100 mg1L
02/01/2014
Mercury
sws46 7470A
<0.002 mg/L
02/14/2014
Comment: Sludge residuals reported on a dry weight
basis. RCI reported on anpass received basis.
Reviewed by: Ze2L 4
41t� U044
'
Report #: 2014-00289 Page 3 of 3

Partial Report
Mau AMA=iau poi¢w�unvse
Print Date: 0211912014 N.C. CerMcatlon # 481
S &AralyYralPe�3lw.ttve5 (55009usims0r. US•22405•WllmingtonX t+18103501003 f+19103501557 www.sgu m
Memberol"Susawwr[SO =
Page 15 of 23

COON'TY:OF 6RUNSWICK� P(JBLIC.UTILITIES°: ' ND - APPLICATION- PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled:.28 April, 2014 2nd Quarter
West WWTP Permit No. NCO044873
Mineralization rate 0.30 4.08% Solids
8.92 nH
P . M` m Ik "/0 *10000 `,`_ 7=` :; ;; ' `; .:..; :.;,
PAN Surfacee
30005.5
60.011
PAN Injection
38812.83
' 77.62566
TKN
69300
138.6
Ammonia Nitrogen (Am)
38800
-77.6
Nitrate Nitrogen (Nin)
3;68
0.00736
Organic Nitrogen (Orn)
0
0
Total Phosphorus (P)
40300
'80.6
Total Phosphate (P205)
0
0
Estimated Avail. P205
0
0
Total Potassium.(K)
6100
12.2
Total Potash (K20)
0
'0
Arsenic (As)
10.4
0.0208
Cadmium (Cd)
2.43
0.00486
Chromium (Cr) -
18.1
0.0362
Copper (Cu)
431
0.862
Lead.(Pb)
11,6
_ 0.0232
Mercury (Hg)
0.574
0.001148
Molybdenum (Mo)
2.43
0.00486
Nickel (NI) i
17.4
. 0.0348
Selenium (Se) ,•
6.89
'0.01378
Zinc (Zn)
1290
2.58
Aluminum (AI)
46600
93.2
Calcium (Ca)
18600
37.2
iron (Fe)
0
-0
Sodium (Na)
1870
3.74
Sulfur (S)
0
0
Magnesium (Mg)
4830
9.66
Manganese (Mn)
01
0
Environmental Chemists, Inc. 2014-04874
'Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+ Ammonia N + Nitrate N +Nitrate N - % PAN
�i Surface Application
- -i (Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N) + Nitrate N +Nitrate N - % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes.
65001oad .794 lb per load = 47.659 lb PAN Per load Surface / 61634Iniected
4500 load .549 lb per load = 32.994 lb PAN ner load Surface 142.616

COUNTY OF BRUNSWICK West Brunswick Regional Laboratory
Public Utilities Department 236 Grey Water Road
WastowraterTreatment Division Supply, NC 28462.
as Phone: [phone] - Fax: 910 75&7927
Sample Collection and Chain of Custody ` [,.C,-o
Collected By:� l X Oa��� [ l � Report No.: 1 6 7 vt
Sample Tvoe: I = Influent, it = Effluent W = Well; ST = Stream, SO = Soil, SL = Sludge Other:
Sample
Identification
Collection
Sample
Type
Composite
or Grab
Container
(Plastic or Glass)
Chlorine
mgfL
LAB ID
NUMBER
PRESERVATION
ANALYSIS
REQUESTED
DATE
TINE
T M
NONE
HCl
HAO,.
HNO3
THIO
OTHER
SDNR Tank
WBR
//
!(�{Ci
SL
C
0
`]
r
X
Fecal Density
4128/2014
:CO
SDNR Tank
WBR
SL
C
0
I7
X '11'em
Density
4/28/2014
SDNR Tank
WBR
SL
C
0
I
X
Fecal Density
412812014 {
40
SDNR Tank
WBR
SL
0
2
�� J
X
Fecal Denslt
4/28/2014
G
G
SDNR Tank
WBR
SL
CL,
rp)
0
yLt
�I 1 l
X
Fecal Density
412812014
SDNR Tank
WBR
SL
P
0
1'I`��!
X
Fecal Density,
4/28/2014
G
SDNR Tank
WBR
SL
0
f�
1 d� 4
X
Fecal Density
4/2012014
CIL
SDNRTAnk
WBR
SL
P
0
I
Residuals
41«2812014
G
P .
G
G
C
P
G
C
.d
C
P
G
G
ATTENTION: Samples submitted for analysis for Ammonia, TKN, Cyanide, Phenol and all Bactedologicals must be dechlorinated to c 0.2 ppm at time of collection,
Transfer
Rellnq earl By:
Date/Time
Received By: L _
Date/Time
1
1
2 -
tk
Zed �a
Temperature when Received:
' L�9!cj rep e[�d: Rejeced;::,_I Resacmp.l�e� Ret�iuired:
Delered
Comments,
(" o®
"r'"

- Environmental Chemists, Inc@
e a 6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) � (910) 392-UM (Fax)
aPA 710 Bowsertown Road • Manteo, NC 27954 . %Jf- Z-*
[phone] .
ANALYTICAL & CONSULTING
CHEMISTS NCDLINR: DWQ CERTOCATE #94. DiS CERTHICATE #37729
I!
Brunswick County Public. Utilities Date of Report: May 27, 2014
LJ Post Office Sax 249 Customer PC
Bolivia NC 28422 report #: 2014-04874
Attention: Donald Dixon Report to: Donald Dixon
Project ID: SDNR Tank
f i Lab -ID Sample ID: SOLAR Collect Date/Tlrne Matrix Sampled by
14-11735 Site: 1 4/28/2014 11:00 AM Solid/Sludge Dixon Medlin
Test Method Results Date Analyzed
Total Solids (°10) SM 2M a 3.90 % 04/2912O14
Fecal Density SM =16E MPN 24 hr 603 46 MPN/9 04/2912014
Lab ID Sample ID: SDNR Collect Date/Time Matrix sampled by
14-11737 Site: # 2 4/28/2014 " 11:00 AM Solld/Siudge Dixon Medlin
Test Method Results Date Analyzed
Total Solids (°f°}
sht 2540 s
3.66 % 04/2912014
r Density
Fecal y
SM 9221C E MPN 24 hr 603
<6 MPN/g 04/29/2014
Lab ID Sample ID: SDNR
Collect Datei ime
Matrix Sampled by
14-11738 Site;# 3
412812014 11:00 AM
Solid/Sludge Dixon Medlin,:
Test
Method
Results Date Analyzed
Total Solids (0l0)
SM 2640 B
3.46 % 04/2912014
PeCEI DensitySM
9221C E MPH 24 hr 603
<6 MPN/g 04129/2014
Lab i® Sample ID: SDNR
Collect DatelTlrne
Matrix Sampled by
14-11739 Site: # 4
4/28/2014 11:00 AM
Solid/Sludge Dixon Medlin
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2UO s
3.94 % 04/2912014
1-1 Fecal Density
SM92210EMPN 24hr6W
<6MPN/g 04129/2014
Lab ID Sample ID: SDNR
Collect Dateirme
Matrix Sampled by
t14-11740 Site: # 5
4/28/2014 11:00 AM
Solid/Sludge Dixon Medlin
Test
Method
results Date Analyzed
Total Solids
SM 2540 a
3.85 % 04/2912014
Fecal Density
SM 9221C f: MPN 24 hr 503
<6 MPN/g 04129/20 l4
Report it.: 2014-US74
i
Page 1 of 3

n V .a.ronwUntal hermits, Inc.
. '
®rs
6602 Windmill Way • W��lv4ngton, NC 28405
[phone] (Lab) • [phone] (Fax)
71G Sowsertown Road • Manteo, NC 27954
_
.[phone]
ANALYTICAL &.CONSULTING
CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE OM9
Brunswick County Public Utilities Date of Report: May 27, 2014
P st Vice Sox 249
:Customer PO #:
Bolivia NC ` 28422
Report #: 2014-04874 ,
Attention: Donald Dixon
Report to: Donald. Dixon
-''
Project [D: SDNR Tank
Lacs ID Sample ID: SDNR,
Collect Date/Time Matrix . Sampled by
- 4-1 i741 Site: # 6
4/28/2014 11:00 AM Solid/Sludge Dixon Medlin
a est
Method Results Date Analyzed
Total Solids (TO) '
sM'2s40 s 3.80 % 04/2912014
Fecal- Density "
SM MIC E MPN 24 hr SD3 <6 MPN/g 04/29/2014
Lab lD Sample ID: SDNR
Collect Date/Time . Matrix Sampled by
14-11742 Site: # 7
4/28/2014 11:00 AM Solid/Sludge Dixon Medlin
Test
Method
Results
Date Analyzed
Total Solids (moo)
SM 2540B
4.05 %
04/29/2014
Fecai Density
SM 92210 E MPN 24 fir 503
<6 MPNIg
04/2912014
Repor@ ai.: 2014.04S74 Page 2 of 3

- Environmental Chemists, Inc.
6602 Windmiii Way . Wiln u gton, NC 28403
(910) 39270223 (La)a) • [phone] (Fax)
C 710 Bowsertown Road • Manteo, NC 27954
[phone]..
ANALYTICAL & C®NSULnNG
CHEMISTS NCD]ENR: DWQ CERTIFICATE #94. DLS CERTIFICATE 437729
Brunswick County Public Utilities Bate of Report: May 27, 2014
Post Office Box 249 ' Customer P® #:
Bolivia NC 28422 Report #: 2014-04874 q`
Attention: Donald Dixon Report to: Donald Dixon �•J 214
'.-- Project ID: SDNR Tank
Lab Ili Sample ID:, SEW Collect Date►Time Matrix Sampled by
14-11744 Site, Sludge 4/28/2014 11:00 AM Solid/Sludge Dixon Medlin
Test
Method
Results
Date Analyzed
I Sludge Residuals
AiLIminum
£PA2Q0.7
466OOm9/k9
04/30/2014
Arsenic
EPA 200.7
10.4 mg/kg
04/29/2014
Cadmium
EPA200.7
<2,43 mg/kg
04/29/2014
Calcium
EPA 200.7
18600 mg/kg
04/2912014
_ Chromium
EPA200.7
18.1 mg/kg
04/2912014
Copper
EPA200.7
431 mg/kg
04/24/2014
Lead
EPA 200.7
11.6 mg/kg
04129/2014
Magnesium
EPA200.7
4830 mg/kg
'04/29/2014
Molybdenum
EPA200.7
<2.43mgikg
04/29/2014
Nickel
EPA200.7
17.4mglkg
04/29/2014
Potassium
EPA 2017
6100 mg/kg
0412W2014
Selenium.
EPA200.7
6.89 mg/kg
0412912014
Sodium
EPA 2co.7
1870 mg/kg
04/2912014
J . Zinc
EPA 2ooa
1290 mg/kg
04/29/2014
Ammonia Nitrogen
EPA 360.1
38800 mg/kg
05/08/2014
Total Kjeldahl Nitropq (TKN)
EPA 351.2
51700 mg/kg
05/07/2014
Nitrate+Nitrite-Nitrogen
EPA353.2
3.68mg/kg
05122/2014
Total Solids (%)
sM 2540 a
4.08 %
04/29/2014
pH
spa 4500 H a
8.92 units
05/0112014
Total Phosphorus
sM 4500 P F
40300 mg/kg
-
05108/2014
Mercury
svasas7a7�s'
0.5740mgikg
05/0712014
Comment: results, except pH, reported oon� a dry weight basis. pH reported on an as received basis.
Reviewed by:
QA
Reportt: 2014-04874 Page 3 of 3

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: County of Brunswick Utilities WQ Permit Number: WQ0034468
WWTP Name: West Brunswick Regional WWTP NPDES Number: WQ0023693.
Monitoring Period:, From 4/.1/2014 To 6/30/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑'
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5
Alternative 6 ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost' ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 [IT
Alternative 2 ❑
If applicable to alternative
performed,(Class B only) indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization ' ❑
Air Drying[]
Composting ❑
Aerobic Digestion ❑
Anaerobic C Digestion 5t10 to n
g
If applicable to, alternative perfermed
Class A or Class B) complete the following
monitoring data:'
Parameter
Allowable Level
in Sludge
Pathogen Density
um er o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nique
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
IvIPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform.)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alta (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) E
Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk Stabilization
[ 3
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector,
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation .why you have not met one or both of the requirements.)
"This determination has ,been made under my direction and supervision in accordance, with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
' Prepa)�r Name and Title (type or print)
.9
SignaturUf Preparer*
Land Appli Nadie a I itle (if applicable)(type or print)
/7
Date Signature o d Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (1212006)

County of Brunswick Public Ut hies
Wiest Brunswick Regional Faces Laboratory
North Caralvra Laboratory Certification Alrnrber. NC00903
Anna laRoux, Lab Supervisar PO Boa 249 235 Grey Water Road Telephone: [phone]
alS�-euxOq)l nM),net Bolivia, NC 29422 Supply, NC 28462 Fax; 910-755-7927
Report Date: 29-N.ay-2014
v3 .. �,a�s�le'€'�t=se asaaa#e FDxte 9C�$_a� �e�had g
West
Brunauficic Thirty Day Bench 4/28/2014 Reduction of Valor Attraction (<I S% is considered passing)
Regional rligestor Scale "rest 5128/2014 as Required to Meet Option 3 2.91 %
WuFt P EPA. [503:33(b)(3)] PASS
5�?GdR
(End of Report)
Certifled by-.
Anna ieRoux, Laboratory Supervisor
F

.., .rc.i.. m,x.x tiv ru<rmruw n. aev.rmmry manr mo,H. n�,�u.+mnc ne na•mi.rmaw
Legend
Name Start End Duration Scale Units Min Max Avg td Deviation
WBVYVJ4 Atad Tank No.1 Temperature 6/112014 2:05.30 PM 6/4/2014 2:05= PM 3q pp;Ap;pp., ' 2 ; p12' peg F, ;128.5Z9624 129.636686.:129.100595 ° ;10.316548

1
Legend
Name Start End Duration Scale Units Min Max Avg S Deviation
WBWW4 Atad Tank No 2 5/1112014 10:42.30 AM 5/12/2014 10.42.30 AM 1d 00 00:00 32 - 212 Deg F 138.163535 140.201 27 139.090515 .629358
Temperature
(d C Iris /y
5 .
s
69,nj
Page S

Legend
Name
�nq
Start End Duration Scale Units Min Max Avg Std Deviation
4130/2014 8 49.18 AM 5/2/2014 B-49-18 AM 2d 00 00 OD 32. 180 Deg F 149 274598 152.38688 150.520787 0937558
0,03 I it s -ro C1gss
44/ W;Lts
Page 1 M Q !
(.J l '

COUNTY OF-$RUNSWICK PUBLIC_UT:IUTIES'IANQ APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: 7/30/14 3rd Quarter
West WWTP Permit No. NCO044873
Mineralization rate 0.30 3.25% Solids
araroe
M,.
P . m "/0 "10 000 ::"
...,,� ... n' M K ,' D.OD
PAN Surface
32871.6
65.7432
PAN ,l njetion
63321.E
126.643
TKN
68900
137.8
Ammonia Nitrogen (Am)
60900
: 12i.8
Nitrate Nitrogen (Nin)
21.6
0.0432
Organic Nitrogen (Orn)
0
0
Total Phosphorus (P)
57200
114.4
Total Phosphate (P205)
0
0
Estimated Avail. 0205 .
0
0
Total Potassium (K)
5480
10.9E
Total Potash (K20) .
- 0
0
Arsenic (As). _ :
2.55
0.0051
Cadmium (Cd)
2.55
0.0051
Chromium (Cr)
22.9
" 0,0458
Copper (Cu)
437
0.874
Lead (Pb)
9.57
0.01914
Mercury (Hg)
0.769
' 0.001538
Molybdenum (Mo)
8.68
0.0173E
Nickel (NQ
20
0.04
Selenium (Se)
6.8
0.0i36
Zinc (Zn)
1540
3.08
Aluminum (AI)
44300
88.6
Calcium (Ca)
26000
52
Iron (Fe)
0
0
Sodium'(Na)
2610
5.22
Sulfur (S)
0
0
Magnesium (Mg)
6680
13.3E
Manganese (Mn)
010
0
Environmental Chemists, Inc. 2014-09109
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+ Ammonia N + Nitrate N +Nitrate N - % PAN
Surface Application -
(Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N) + Nitrate N +Nitrate N - % PAN
- Note: Constituents N.D. (Not Detected) or < detetion limits are listed as detection limits for calculation purposes.
6500load .880 lb per load = S7.913 lb PAN per load Surface 1111.445 Injected
45001oad .609 1b per load = 40.094 lb PAN per load surface /7712S Injected

COUNTY OF BRUNSWICK West Brunswick'Regional Laboratory -�'r
Public Utilities Department .235 Grey Water Road f ` -1-�
Wastewater Treatment Division -Supply, NC 28462
CA Phone: [phone] Fax: [phone]
Sample Collection and Chain of Custody
Collected By: 4'�7��G�' Report No.: 1
Sample Type: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge Other.
Sample
Identification
Collection
Sample
Type
Composite
or Grab
Container
(PlasticorGlass)
Chlorine
mg1L
LAB ID
NUMBER
PRESERVATION
ANALYSIS
REQUESTED
DATE
TIME
NONE
-HCI
HzSO4
HNOa
TRIO
OTHER
SDNR Tank
WBR
(� e�
r
SL_
C
0
+
X
Fecal Density
7/16/2014
/0,30
Q
G
SDNR Tank
WBR
4�
SL
C
0
WC
X-
lFecal Density
7/1612014
/0 �D
G
SDNR Tank
WBR
<
!V
SL
C
0
2to
X
Fecal Density
71IM014
50
G
SDNR Tank
WBR
YO OC
(
SL
0
Q
X
Fecal Density
71IW2014
to 9&7
G.
SDNR Tank
WBR
o C
1�
SL
C
0
Gt(%
X
lFecal Dens'
711612014
la36
SDNRTank
WBR
tL
l Q
St.
C
0
24,0
X-
Fecal Density
7/16/2014
)010
a
G
SDNR Tank
WBR
nn e�
V
SL
C .
0
1.
X
Fecal Density
7/16/2014
1010
G
SDNR Tank
WBR
u OC
0
SL
Id
n
0
X
Residuals
7/16/2014
10 c
G
C
P
G-
G
C
P.
G
G
C
P
G
G
ATTENTION: Samples submitted for analysis ror Ammonia, TKN, Cyanide, Phenol and all Baetedotogioals must be dechkulnated to <0.2 ppm at time or collection.
Transfer
R linquished Sy:
Date/Time
Relaeliveo By:
D te/Time
2
Temperature when Received Accepted: vim.
Delivered By. (T
Rejected: Resample Required:

Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
sM 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #194. DLS CERTIFICATE 437729
Brunswick County Public Utilities
Date of Report: Jul 23, 2014
- Post Office Box 249
Customer PO #:
Bolivia NC 28422
Customer ID: 08100011
Attention: Donald Dixon
Report #: 2014-08528
Project ID: SDNR Tank
Lab ID Sample ID:.
'I
Collect Date/Tirne. Matrix Sampled by
14-21084 Site:
7/16/2014 10:30 AM Solid/Sludge Matt Henry
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2640 a
3.07 % 07/17/2014
Fecal Density
SM 92210 E MPN 24 hr5o3 <7,MPN/g 07/17/2014
Lab 1D Sample ID:
Collect Date/Time Matrix Sampled by
i 14-21085 Site: 2
7/16/2014 10:30 AM Solid/Sludge Matt Henry
Test
Method
Results Date Analyzed
j Total Solids (%)
SM 254o s
3.20 % 07/1712014
Fecal Density
SM 9221C E MPN 24 hr603 <7 MPN/g 07/17/2014
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-21086 Site: 3
7/16/2014 10:30 AM Solid/Sludge Matt Henry
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 s
3.22 % 07/17/2014
Fecal Density
SM 9221C E MPN 24 hr503 <7 MPN/g 07117/2014
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-21087 Site: 4
7/16/2014 10:30 AM Solid/Sludge Matt Henry
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 a
3.14 %
07/17/2014
Fecal Density
SM 9221C E MPN 24 hr 603
<7 MPN/g
07/17/2014
Lab ID Sample 1D:
Collect Dateffime
Matrix Sampled by
F14-21088 Site: 5
7/16/2014 10:30 AM
Solid/Sludge Matt Henry
�J Test
Method
Results Date Analyzed
1 Total Solids (%)
sM 254o B
3.11 %
07/17/2014
1 Fecal Density
SM82210EMPN 24hr503
<7MPN1g
07/17/2014
I'
Report*: 2014-08528 Page 1 of

Environmental Chemists, Inc.
envirochem'(910)
6602 Windmill Way - Wilmington, NC 28405
$92-0223 (Lab) - (910) 3924424 (Fax)
710 Bowsertown Road - Manteo, NC 27954
[phone]
ANALYTICAL S CONSULTING
_ CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE 037429
Brunswick County Public Utilities Date of Report: Jul 23, 2014
Post Office Box 249
Customer PO #:
Bolivia NC. 28422
Customer 10: 08100011
Attention: Donald Dixon
Report #: 2014-08528
-
Project 1b: SDNR Tank
l Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
'- 14-21089 ' Site: 6
7/16R014 10:30 AM Solid/Sludge Matt Henry.
Test
Method Results' Date Analyzed
Total Solids {%)
SM 2540 B 3.22 % 07/11/2014
Fecal,Density
SM 92210 E MPN 24 hr503 <7 MPN/g, 07/17/2014
Lab ID .. _ '' Sample ID:
Collect Date/Time Matrix. Sampled by
14 21090 Site: 7
7/16/2014 10:30 AM Solid/Sludge Matt Henry
Test
Method Results Date Analyzed
Total Solids (%)
SM25ao'a 3.11 °!0 07/17/2014
Fecal Density SM 9221C E MPN 24 hr 50 <7 MPN/g 07/17/2014
Comment Results reported on a dry weight basis.
4_ Reviewed by:
It -, 7 ;
Report#:: 2014.08528 Page 2 °f 2

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: County of Brunswick Utilities WQ Permit Number: WQ0034468
' WWTP Name: West Brunswick Regional WWTP . NPDES Number: WQ0023693
Monitoring Period: From` 7/1/2014 To 9/30/2014
Pathogen Reduction (40 CFR 503,32) - Please "indicate level achieved and alternative performed:
Class A:
Alternative i ' ❑
Altemative 2 ❑.
Alternative 3 ❑
Alternative 4 ❑ ..
Alternative 5
Alternative 6 ❑
If applicable to alternative
performed (Class A oily) indicate "Process to Further
Reduce Pathogens":
Compost ' :. ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic . ❑
Beta Ea ❑
Gamma Ray ❑
Pasteurization. ❑
Class B:
'Alternative l .. ❑
Alternative 2 ❑
If applicable to alternative
erformed (Class
B only) indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization ❑
Air Drying❑
Composting ❑
JAerobic Digestion ❑
Anero a b i c Digestion
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
g.
Pathogen Density '
Number o
Excee-
Frequency
of Analysis
Y
Sample
Type
a Yt:ca
Tech-
aigue
inimu
Geo. Mean
ax'imu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid.,, " (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
vector Attraction Keduetion (4U U14K SUS.Sil - Please indicate antion nprtnrmp t
Alt-1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt, 3 (30-day bench)
Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ '
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable). ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 563.33 have been met."'
® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been meta I am aware that there are
significant penalties for false certification including fine and imprisonment."
e
6amk 1
+ Prepare Name and Title (type or print) Land Ap ' r Name d Title (if applicable)(type' or print)
�-- -
i
Signature(gf Preparer* Date Signature and Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

County of Brunswick Public Utilities
West Brunsivick Regional Facility Laboratory
NOXYM
Anna 10,HouN, 49 -3- Giv, wate., Road Tvlepbc— 9104.15.1921
Roftvm, NC ,W-,
hox
Reimrt Nte, ^T-Am-20R-'---
West
Brunswick Thirty Day Bench Beginning. 07128/17 Reduction of Vector Attraction 15% is considered passing)
Regional Digestor Scale Test Endings 08/27/14 as Required to Meet Option 3 0.00%
VvWTF, EPA [503.33(b)(3)] PASS
SDNR
(End of Report)
Certified by: rs
Anne IeRoux, Laboratory SuPervisor

ur .. ,.�e.u.en nv..,,� raunM ��rr.n., i�wnm.w� m�znaiw,xi sm � �na_uiu,ao.�aa a.+,u,ra
�, «.., y.-+ t-..,�..,,--..r ,e'�...✓' �,r*.e."r':.r^-.� y "4' �-v-....^^j'„°».,�,,sw�"��'"n,,,,r`',.%'" b°b-�""i-.,^t..-^.r°.F.v-•e..-..pe�,.r'iv--5,� �J...a.,..r.�•`+•v,r,,�-�s+..j�'_.��y,J�i...•....,�,°h"-'L+r...t "+J1.n� d
Legend
Name Start End Duration Scale Units Min Max Avg Std Deviation
W$UWV11 Atad Tank No.4 1012/2014 3:12:11 PM 101312014 7:18`28AM 16:06:77 135.'- 145; Deg F' 136,31579, 137.052632 1367629D9 _ 0.151046
Temperature'
Pane 7

Legend
Name Start End Duration Scale Units Min Max Avg Sid Deviation
AAA, 129-12911 128.563332 0.426537
Jos �9 1, ss a ,s g S-6
lY'a�S o. 8 -P�-
Page 7

Legend
Name Start End Duration Scale Units Min Max Avg Std Deviation
WBWW4 Atad Tank No 1 8/1/2014 4:13:19 PM 8/512014 5:37:27 PM dd 01:24:08 ' 125 -135 Deg F129,240099 130.730265 129:946931 0.376251
Temperature .
9 , � 4 , F
1o2I Cl�sS
(93212 to" YO-ro)
Page 1

COUNTY OF BRUNSWICK West Brunswick Regional Laboratory .
Public Utilities'Department 235 Grey Water Road
WastewaterTreatment Division 14 Supply, NC 28462
4C. Phone: [phone] Fax: [phone]
ample Collection and Chain of Custody
Collected Bir Report No.: 1
Sample Type: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soll, SL = Sludge Olher.
�fiilTi���
■�==ego©■■�■■■■■■■■■
ATTENMM Samples submi¢ed for analysis forAmmonla,'fAN, Cyanide, Phenol and all 8aaedobgICals must be detldorinated to :S 02 ppm alone MwlleWon,
Transfer - Relinquished
DateTme
ReceivecLBY.
ateftune
1
9 �i ly
2
TenWralufov&MReceived:'t+-; Accepted Rejected ResampleRe*imd
D
M

i
Enviromamental Chemists,
Inc.
6602 Windmill Way - Wilmington; NC 28405
envirochem
[phone] (Lab) , - (910).392-4424 (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR. DWQ CERTIFICATE #94. DLS CEIZTIFICATB #37729
Brunswick County Public Utilities
Date of Report: Aug 29, 2014
Post Office Box 249
Customer PO #:
Bolivia NC 28422
Customer iD: 08100.01.1
Attention: Donald Dixon
'Report #: 2014-09109
"C �f}
Project ID: Vilest Brunswick Regional 1NWTP
Lab, ID Sample ID:
Collect Date/Time. Matrix Sampled by
14-22499 Site: West Brunswick Reglonal '7130/2014
11:30 AM Solid/Sludge Dixon $ Clint
W WTP
Test:
Method '
Results Date Analyzed
Chlordane
sw 846 Method 8081BI3610
<0.005 mg/L
.08/0612014
Endrin
SW848 Method 8081813510
<0.00005 mg/L •
08/06I2014
Heptachlor
SW 848 Method 60819l3510
<0.00005 mg/L ..
08/06/2014
Heptachlor epoxide.,
SW 846 Method 8081813610
<0.00005 mg/L
08/06/2014
Lindane
SW 846 Method 8081813510
<0.00005 mg/L
08/06/2014
Methoxychlor
SW 846 Method 80818/W10
<0.00005 mg/L
08/06/2014
Toxaphene
SW 846 Method 80818/3510
<0.005 mg/L
08/06/2014
1,4-Dichlorobenzene (TCLP)
SW 846 method 827013510
<omo mg/L
08/11/2014
2,4,5 Tdchlorophenol (TCLP)
SW 60 method $270/3510
<0.050 mg/L
08/11/2014
2,4,6-T6chlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
08/11/2014
-� 2,4-Dinitrotoluene (TCLP)
SW 846 method 827013610
<0.050 mg/L
08/11/2014
Cresol (TCLP)
Sw846methode27013510
<0.050mg/L
08/11/2014
Hexachloro-1,3-butadiene (TCLP)
Sw846 method s27013510
<0.050 mg/L
08/11/2014
Hexachlorobenzene (TCLP) .
SW 846 method 827=61 0
<0.050 ing/L
08/11/2014
Hexachloroethane (TCLP)
SW 846 method 0270/3610
<0.050 mg/L
08/11/2014
m + p-Cresol (TCLP)
SW 846 method 8270MID
<0.050 mg/L
08/11/2014
Nitrobenzene (TCLP)
SW 846 method0270/3510
<0.050 mg/L
08/11/2014
_ o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
08/11/2014
Pentachlorophenol (TCLP)
SW 846 method827013510
<0.250 mg/L
08/11/2014
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
08/11/2014
2,4,5 TP
SW646 Method,8161A
<0.003 mg/L
08/15/8201
2,4-D
SW846 Method 8151A
<0.003 mg/L
08/15/82.01
-- 1,1-Dichloroethylene
sw846 Method826o15030
<0.01 mg/L
8/12/2014
1,2-Dichlorcethans
sw846 Method 8280/5030
< 0.01 mg/L
8/12/2014
Benzene
SW846 Method 8280/5030
< 0.01 mg/L
8/1212014
Report#:: 2014.09100 Page 1 of 3

Environmental Chemists,
Inc.
chem
enviro(910)
6602 Windmill Way • Wilnungton, NC 28405
392-0223 (Lab) • [phone] (Pax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS
NCDENM DWQ CERTIFICATE DLS CERTIFICATE #37729
Brunswick County Public Utilities
Date of Report: Aug 29, 2014
Post Office Box 249
Customer PO #:
Bolivia NO ' 28422
Customer ID: 08100011
Attention: Donald Dixon
Report#: 2614-09109
Project ID: West Brunswick Regional WWTP
Carbon Tetrachloride
sw046 Method 8260/6030
< 0.01 mg/L
8/12/2014
Chlorobenzene
Swe4s Method 826015030
< 0.01 mg/L
8/1212014
Chloroform
SWe48 Method 8260/5030
< 0.01 mg/L
8/12/2014
Methyl ethyl ketone
8VA4e Method e260f5030
< 0.05 mg/L
8112/2614
Tetrachl6eoethylene
Sw8Q Method 8260/5030
< 0.01 mg/L
8/12/2014
Trichloroethyiene
swe46 Method 826015030
< 0.01 mg/L
8112/2014
Vinyl Chloride
swue Method e2so/5030
< 0.01 mg/L
8/12/2014
RCI
Cyanide
EPA 336A
<0.123 mg/kg
08/04/2014
Sulfide
SM4500 s a
9.38 mg/kg
08/04/2014
Ignitability
SW 84e method 1010
>212 OF
08/12/2014
Sludge Residuals
Aluminum
EPA200.7
44300mg/kg
08/12/2014
Arsenic
EPA 200.7
<2.55 mg/kg
08118/2014 .
Cadmium
EPA 200.7
<2.55 mg/kg
08/05/2014
Calcium
EPA 200.7
26000 mg/kg
07/31/2014
Chromium
EPA200.7
22.9 mg/kg
08/05/2D14
Copper
EPA200.7
437 mg/kg
08/04/2014
Lead
EPA 200.7
9.57 mg/kg
08/18/2014
Magnesium
EPA200.7
6680.mg/kg
07/31/2014
Molybdenum
EPA200.7
8.68 mg/kg
08/05/2014
Nickel
EPA200.7
20.0 mglkg
08/05/2014
Potassium
EPA200.7
5480mg/kg
07/31/2014
Selenium
EPA20o.7
6.80mglkg
08/12/2014
�i Sodium
EPA2o°.7
2610 mg/kg
07/31/2014
Zinc
EPA200.7
1540mg/kg
08/04/2014
Ammonia Nitrogen
EPA350.1
60900mg/kg
08/11/2014
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
68900 mg/kg
08/12/2014
Nitrate+Nitrite-Nitrogen
EPA3ft.2
21.6mg/kg
08/27/2014
Report*: 2014-09100 Page 2 of 3

i F
Environmental Chemists, Inc.
•
w'
6602 Windmill Way • Wilntnlgton, NC 28405
[phone],(Lab) • [phone] (Fax)
710 Bowsertown Road Manteo, NC 27954
(252) 473- 702
ANALYTICAL-& CONSULTING
' CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DLS CEIZrMCATE #37729
Brunswick County Public Utilities
Date of Report: Aug.29, 2014
Post Office Box 249
Customer PO #: '
Bolivia NC 28422
Customer ID: 081,00011
Attention: Donald Dixon
Report #: 2014-09109 .
Project ID: West Brunswick Regional WWTP
Total Solids (%) SM 2540 s
3.25 %
08/01/2014
pH SM 4500 H s
8.20 units
08/01/2014
Total Phosphorus sM45oo P F
572{)0 mg/kg
08/12/2014
Mercury , SWIM 7471e
0.7690 mg/kg
08/14/2014
TCLP Metals
Arsenic EPA 200.7
<0,1,00mg/L
08/06/2014
Barium EPA200.7
0.150 mg/L
08/06/2014
Cadmium EPA 200.7
<0.100 rhg/L
08/06/2014
Chromium EPA 200.7
<0.100 mg/L
08/06/2014
Lead EPA 200.7
<0.100 mg/L
08/06/2014
Selenium EPA 200.7
0.124mg/L
08/06/2014
Silver SPA 200.7
<0,100mg/L
08/08/2014
Mercury EPA 245.1
<0.002 mg/L
08/12/2014
Comment: Sludge residual results, except pH, reported on a dry weight basis.
Reviewed by:
Report#:: 2014.09109 Page 3 of 3

COUNTY :4F._ BRUNS.WK PUBLIC UTILITIES LAND: APPLICATION.PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled:11/12/2014
West WWTP Permit No. NCO044873
Mineralization rate 0.30 % Solids 3.34
nH 7.96
Lbe/DrvTon;
PAN Injected
59690.6
119.3812
PAN Surface
34540.6
69.081
TO
81600
163.2
Ammonia Nitrogen (Am)
50300
106.6
Nitrate Nitrogen (Nin)
01,6
0.0012
Organic Nitrogen (Orn)
0
0
Total Phosphorus (P)
59300
118.6
Total Phosphate(P205)',
0
0
Estimated Avail. P205
0
20
Total Potassium (K)
4940
9.88
Total Potash (K20)
0
0
Arsenic (As)
2.99
0.00598
Cadmium (Cd)
2.99
0.00598
Chromium (Cr)
24.1
0.0482
Copper (Cu)
518
.1.036
Lead (Pb)
8.74
0.01748
Mercury (Hg) .
0.449
:0.000898
Molybdenum (Mo)
8.02
0.01604
Nickel (Ni)
19.2
0.0384
Selenium (Se)
8.32
0.01664
Zinc (Zn)
1820
3.64
Aluminum (All'
5.72
. 0,01144
Calcium (Ca)
27800
55.6
Iron (Fe)
0
0
Sodium (Na)
2810
5.62
Sulfur (S)
0
0
Magnesium (Mg)
6770
13.54
Manganese (Mn)
0
0
tnvironmental Lnemists, Inc. ZD14-13993
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+ Ammonia N + Nitrate N +Nitrate N - % PAN
' Surface Application
(Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N) + Nitrate N +Nitrate N - % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes:
6500 load .90S lb per load. 147.696 lb PAN per load lnlected / 62.518 Surface
4500 load .626 !b per load 162.286lb PAN per load injected / 74.732 Surface

1
COUNTY OF BRUNSWICK UK�West Brunswick Regional Laboratory_,_.. ! � r 139R3
Public Utilities Department 236 Grey Water Road
Wastewater Treatment Division p� Supply, NC 28462-
"°►nrKKRoPhone: 910455-7921 ' Fax: [phone]
Sample Collection and Chain of Custody
Collected By: � (�(Q,J ,Report No:: 1
Sample Type: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge Other.
Sample
Identification
Collection
Sample
Type
Composite
or Grab
Container
(PlasiicorGlass)
Chlorine
m91L .
LAB ID
NUMBER
PRESERVATION -
ANALYSIS
REQUESTED
DATE
TIME
TEMP
NONE
HCI
H25o,
HNO3
TRIO
OTHER
SDNRTank
WBR
3 Z°
SL
C
P
0
4agg
X
Fecal Density
11/1212014
lo: 40
G
G
SDNR Tank
WBR
SL
C
P
0
M19
X
Ifecal Den"
11/1212014
0- 4.1
G
G
SDNRTank
WBR
SL
C
P3®a1.
0
X
Fecal Density
11112/2014
Q
G
G
SDNRTank
WBR
SL
C
P
0
30t
X
Fecal Density
11/1212014
p; +3
G
G
SDNRTank
WBR
SL
C
P
0
1004
X
Fecal Density
11/12/2014
10044
G
G
SDNRTank
WBR
SL
C
P
0
34303
X
Fecal Density
11112(20%0'#+S
G
G
SDNRTank
WBR
SL
.0
P
0
3Y3D4
X
Fecal Density
11/1212014
)0,4U
G
G
SDNRTank
WBR
SL
C
P
0
34 305
X
Residuals
11/12/2014
(};
G
G
4
C
P
G
G
C
P
G
G
C
P
G
G
ATTENTION: Samples submitted for analysis for Ammonia, TKN, Cyanide, Phenol and all Bacteriologicals must be dechlorinated to:S 02 ppm at time of collection.
Transfer
Relinquished By:
Date/Time
Received By:
DateITime
2'
Temperature when Received: a( •� Accepted: Rejected' Resample Required:
Delivered By: 1 t
Comments:—
n

Environmental Chemists, Inc.
• ex6602 Windmill Way • Wilmington, NC 28405
® �7
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL &CONSULTINQ [phone]
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE 4377291
• Brunswick. County Public Utilities
Date of Report: Deb 04, 2014
Post Office Box.249
Customer PO #:
Bolivia NC 28422
Customer ID: 08100011
Attention: Donald Dixon
Report #: 2014-13993
Project ID: SDNR Tank
Lab ID Sample ID: SDNR Tank WBR
Collect Date/Time Matrix Sampled by
14-34298 Site: 1
11 /12/2014 ' 10:40 AM Solid/Sludge Dixon Medlin
Test Method
Results Date Analyzed
_ Total Solids (%) SM 2sa0 B
3.22 % 11/13/2014
Fecal Density SM 922ICE MPN 24 hr 503 <7 MPN/g 11/13/2014
Lab ID:. Sample ID: SDNR Tank WBR
Collect Date/Time Matrix Sampled by
14-34299 . Site: 2
11/12/2014 10:41 AM Solid/Sludge . Dixon Medlin
Test Method
i
Results Date Analyzed
Total Solids (%) SM 2640 B
3.18 % 11/13/2014
Fecal Density SM 9221C E MPN 24 hr 603 <7 MPN/g 11/13/2014
Lab ID Sample ID: SDNR Tank WBR
Collect Date/Time 'Matrix Sampled by
14-34300 Site: 3
11/12/2014 10:42 AM Solid/Sludge Dixon Medlin
Test Method
Results Date Analyzed
Total Solids (%) SM 2540 B 3.18 % T 11/13/2014
Fecal Density SM 9221C E MPN 24 hr 503 <7 MPN/g 11/13/2014
Lab ID Sample ID: SDNR Tank WBR Collect Date/Time Matrix Sampled by
14-34301 Site: 4 11/12/2014 10.43 AM . Solid/Sludge Dixon Medlin
Test Method Results Date Analyzed
Total Solids (%) SM 2640 a 3.44 % 11/13/2014
- Fecal Density. SM 9221C E MPN 24 hr 603 <6 MPN/g 11113/2014
Lab ID Sample ID: SDNR Tank WBR Collect Date/Time Matrix Sampled by
14-34302 Site: 5 11/12/2014 10:44 AM Solid/Sludge Dixon Medlin
Test Method Results Date Analyzed
I
Total Solids (%) SM MAO a 2.84 % 11/13/2014
Fecal Density SM92210EMPN 24hr603 <8MPN/g 11113/2014
Report #:: 2414-13993 Page 1 of 3

Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Pax)
sen 710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL & CONSULTING [phone] -.
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Brunswick County Public Utilities Date of Report: Dec 04, 20.14
Post Office Box 249 Customer PO #:
Bolivia NC 28422 Customer ID: 08100011
Attention: Donald Dixon Report #: 2014-13993
Project ID: SDNR Tank
Lab 1D - Sample 1D: SDNR Tank WBR Collect Date/Time Matrix Sampled by
14-34303 Site: 8 11/12/2014 10:45 AM Solid/Sludge Dixon Medlin
Test Method Results Date Analyzed
Total Solids (°!°) SM 2sb0 s 3.36 % 11/13/2014
Fecal Density.::.'., SM92210EMPN 24hr503 <6MPN/g 11/13/2014
Lab ID Sample 1D: SDNR Tank WBR Collect DatelTimo Matrix Sampled -by
14-34304 Site: 7 11/12/2014 10:46 AM Solid/Sludge Dixon Medlin
Test Method Results _ Date Analyzed
Total Solids (%)
SM 2640 a
3.25 %
11/13/2014
Fecal Density
SM 9221C E MPN 24 hr603
<7 MPN/g
11/13/2014
Report #..: 2014-13993 Page 2 of 3

Envir®ninental Chemists, Inc.
` • 6602 Windmill Way • Wilmington, NC 28405
® [phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFKATE#94. DLS CERTIFICATE #37729
Brunswick County Public Utilities
Date of Report: Dec 06, 2014
Post Office Box 249
Customer PO #.
Bolivia NC 28422
Customer ID: 08100011
Attention: `Donald Dixon
Report#: 2014-13993
Project ID: SDNR Tank
Lab ID Sample ID: SDNR Tank WBR
Collect DatelTime Matrix Sampled by
14-34305 Site: Residuals
11/12/2014 10:37 AM Solid/Sludge, Dixon Medlin
Test
Method
Results Date Analyzed
Total Solids (%a)
Sluff 2540 a
3.34 %
11/13/2014
Sludge Residuals
Aluminum
EPA 200.7
5.72 mg/kg
11/18/2014
Arsenic
EPA200.7
<2.99 mglkg
11/18/2014
Cadmium
EPA200.7
<2.99 mg/kg"
11/18/2014
Calcium
EPA200.7
27800mglkg
11/19/2014
Chromium
EPA200.7
24.1 mg/kg
11/18/2014
Copper
EPA20o.7
.518 mg/kg
11/24/2014
Lead
I-PA200.7
8.74 mg/kg
11/18/2014
Magnesium
EPA200.7
6770mg/kg
11/19/2014
Molybdenum
EPA200.7
8.02mg/kg
11/18/2014
Nickel
SPA200.7
19.2 mglkg
11/18/2014
Potassium
EPA20Q•7
4940 mg/kg
11/19/2014
Selenium
EPA200.7
8.32 mg/kg
11/18/2014
Sodium
EPA200.7
2810 mg/kg
11/19/2014
Zinc
EPA200.7
1820mglkg
11/26/2014
Ammonia Nitrogen
EFA 350.1
50300 mg/kg
11/14/2014
Total Kjeldahl Nitrogen (TKN)
EPA351.2
81600 mglkg
11/17/2014
Nitrate+Nitrite-Nitrogen
EPA353.2
<0.60 mglkg
11/26/2014
pH
SM4500 H 9
7.96 units
11/20/2014 ,
Total Phosphorus
SM 4500 P F
59300 mg/kg
11/18/2014
Mercury
sw846 74718
0.4490 mg/kg
11 /25/2014
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report #:: 2014.13093 Page 3 of 3

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: County of Brunswick Utilities WQ Permit Number: WQ0034468
WWTP Name: West Brunswick Regional WWTP NPDES Number: WQ0023693
Monitoring Period: From 10/1/2014 To 12/31/2014 .
Pathogen Reduction (40 CFR 503:32) - Please indicate level achieved and alternative nerformed!
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑ :
Alternative 5
Alternative 6 ❑
If applicable to alternative
performed (Class 'only) indicate "Process to Further
Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thetmophilic ❑
1.
Beta Ray ❑
Gamma R2X ❑
Pasteurization ' ❑
Class B:
Alternative 1 ❑
Alternative 2 ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization. ❑
Air Drying❑
Composting .❑
Aerobk'Digestion ❑
Anaerobic Dig s " ri e on
If applicable to alternative performed Class A or Class B complete the following
monitoring data:
Parameter
Allowable Level
in Sludge'.
Pathogen Density
Number ot
Excee-
d,
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nioue
MinimuniGeo.
Mean
Maximum
Units
Fecal Colifotm
2 x 10 to the
6th power
per gram of
total solids
IVIPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 NTN per 4 grams
total solid (dry
weight)
v ecror artTacuon Keaucnon (4u l J'K 5U3.33) - Please indicate option performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench)
Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day, Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt.7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable) ❑
Alt 9 (Injection) ❑
Alt. 10 (Incorporation) L3
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to. determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
60UM61'1 l IV-10
Preparer Name and ATitle (type or print) Land ier Name and Title (if applicable)(type or print)
f
Signature (&reparer* Date Signa a of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

County of Brunswick Public Utilities
West Brunswick Regional Facility Laboratory
Cen�fi—oon Nuitbor NC00903
Anna Lab PO BoN 249 .1
-33 OCY Water Road TL!ephone: 01
1301ma,NC 28422
Supply. NC 2946Z
I?eportD,,1tr75-M.-2Ij I •
�I
Eadfltx
iskimphiLVIN
$4HIPIC-0-Als
TSn&mkLhW
liimal
West
Brunswick
Thirty Day Bench
Beginning: 11/12/14
Reduction of Vector Affraction
(<15% is considered passing)
Regional
Digestor Scale Test
Ending, 12/15114
as Required to Meet Option 3
11.20%
WWTP
EPA [503.33(b)(3))
PASS
{End of RPporty
in
Certified by. Y.
Anna IeRoux, Laboratory Supervisor

0
11
Legend
Name Start End Duration Scale Units Min Max Avg Sid Deviation
WBWW71 Ated Tank N0.3 12/1912014 4*40:49 PM 12J2012014 4:40:49 PM 1d 00:00.00 120 - 140 Deg F 131.948276 134,035068 133.021435 0.540901
Temperature
7 Cla - 5, 5 A71-�D e,3
r
y365 j C, 11OA-5 ,
Page 1

Legend
Name Start End Duration Scale Units Min Max Avg Sid Deviation
r t' Ng3IAI V 11 Atad Tank No 3 Temperalure 11/2212014 3:10 OD PM 11/25/2014 6'57.20 AM 2d 15 47:20 507 110 - 130 Deg F 123 915033 127 996942 125 915083 1.068512
c�: Vc7
i 10 -
Page 1

Total Solids
Day 1 SOP 35 (SM 2540B)
Analyst A. IeRoux
Date start 01/09/14 Date End 01/13/14
Time 1000 Time 800
Analyst Initials: Reviewed by Initials:
of v
Dup
TruekSample
Tare
Final
Dilution
Required
or
Valueize
Weight
Weight
Sample ID
OC
(ppm)
or g)
(g)
(g)
0.33%
Blank
WBR SDNR 01/08/14
.0000
24.5191
24,5193
0.33%
WBR SDNR 01/08/14
DUP
.6868
9.6578
24.4571
18.3644
24.5518
18.4572
0.33%
WBR SDNR 09/08/14
DUP
9.5433
20.85791
20.9490
Total Volatile Solids
Day 1 SOP 35 (SM 2540E)
.
Analyst A. IeRoux
Date start 01/13/14 Date End 01/13/14
Time 830 Time 1400
Analyst Initials: Reviewed by initials:
0.0000 Blank (g)
TS Doing T.S.S
1 Gravimetric Factor
0.0025 Mininum Wt Gain (g)
Weight
Gain
(9)
TS (ppm),
%
Solids
F
0.0002
20.0
0.0
0.0947
9776.2
1.0
0.0928
9608.8
1.0
1.73°%
0,0911
0.0000
9546.0
#DIV/01
1,0
#6IV/01
0.66%
0.0000
. #DIV O! 1
#DIV101
0.0000 Blank (g)
T5 Doing T.S.S
9 Gravimetric Factor
0.0025 Mininum M Gain ini
Dilution
Required
0.33%
0.33%
0.33%
Sampie'ID
Blank
WBR SDNR 01108114
WBR SDNR 01/08/14
WBR SDNR 01/08114
Dup
or
QC
DUP
DUP
True
Value
(ppm)
Sample
Size
(mL or g)
10.0000
9.6868
9.6578
9.5433
Tare
Weight
(9)
24.5 991
24.4671
18.3644
20.8579
Final
Weight
(9)
24.5189
24,5038
18-4084
, 20.9024
Weight
Gain
(g)
-0.0002
0.0467
0.0440
0.0445
TVS
(PPm).
%
Solids
RPD
-20.0
4821.0
0.0
0.5
4555.9
0.5
5.65%
4663.0
#DIV/01
#DIV/01
0.51
#DIV/0i
#DIV101
2.32%
0.0000
0.0000
0.0000
0.0000
0.0000
0,0000

Total Solids
SOP 35 (SM 25406)
Day 30
Analyst A. IeRoux 0.0000 Blank (g)
Date start 02/07/14 Date End 02/10/14 TS Doing T.S.S
Time 730 Time 900 1 Gravimetric Factor
Analyst Initials: Reviewed by Initials: 0.0025 Mininum Wt Gain (g)
Ddubon
Required
Sample ID
Dup
or,
QC
UG
True
Value
(ppm)
Sample
Size
(mL or g)
Tare
Weight
(g)
Final
Weight
(g)
Weight
Gain
(g)
ITS (ppm).
%
Solids
RPD
N
Blank
10.0005
18.3626
18,3628
0.0002
20.0
0.0
0.33%
WBR SDNR 01/08/14
9.8262
20.8574
20.9509
0,0935
9515.4
1.0
0.33%
WBR SDNR 01/08/14
DUP
9.8416
' 24.5189
24.6124
0.0935
9500>5
1.0
0.16%
0.33%
WBR SDNR 01108/14
DUP
11.2832
21.2829
21.3920
0.1091
9669.2
1.0
1.76%
_
0.0000
#DIV10!
#DN/0I
0.0000
#DIVro!
#DIVl01
Total Volatile Solids
SOP 35 (SM 2540E)
Day 30
Analyst A: IeRoux
0.0000
Blank (g)
Date start 02/10/14
'Date End 02110114
TS
Doing T.S.S
Time 900
Time 1200
1
Gravimetric Factor
Analyst Initials:
Reviewed by Initials:
0.0025 .
Mininum Wt Gain (g) "
Dup
UU
True
Sample
Tare
Final
Weight
Dilution
or
Value
Size
Weight
Weight
Gain
TVs
0
RPD
Required
. Sample ID
QC
(ppm)
(mL or g)
(g)
(9)
(9)
(ppm).
Solids
M
Blank
10.0000
18.3626
18.3625
-0.0001
-10.0
0.0
0.33%
WBR SDNR 01108/14
9,8262
20.8574
20.9032
0.0458
4661.0
0.5
0.33%
WBR SDNR 01/08/14
DUP
9.8416
24.5189
24.5648
0.0459
4663.9
0.5
0.06%
0.33%
W BR SDNR 01/00/14
DUP
11.2832
21.2829
21.3354
0.0525
4652.9
0.5
0.23%
0.0000
0.W00
0.0000
#DN/0!
#DN101
0.0000
#REF!
#REF!
#REF!
Vector Attraction Reduction [EPA 503.33(b)(3)] <15% is considered Passing
amp a10
Volatiles Day I
Volatiles Oay 307
Reduction-
WBR SDNR 01/08/14
-
4821.0
� 4661.0
3.43206-931
WBR SDNR 01/08/14
4555.9
4663.9
-2.315087208
WBR SDNR 01/08/14
4663.0
4652.9
0.215389206
#DN/01
#DN/0l
#DN/01
AVERAGES
4680.0
4659.3
0.443805424
Outliers
If using• the hinhBAt rrnm rig. i nmi
4821.0
L7 .-
4652.9
3.612800619
lowest from day-30, the percentage v
is <15, the test is considered passing. Final Percent Reduction: 3.6128110619
Final Result PASS

Total solids
SOP 35 (SM 26408)
Day !
Analyst A. IeRoux
0.0000
Blank (g)
Date start 04/28/14
Date End 04129114
TS
Doing T.S.S
Time 113310�
Time 840
1
Gravimetric Factor
Analyst Initials: E}
Reviewed by Initials:
0.0026
Mininum Wt Gain (9)
Dilution
Required
Sample ID
Dup
or
QC
True
. Value
(ppm)
Sample
Size
. (ml- or g)
Tare
Weight
(9)
Final
Weight
(9)
Weight
Gain
(g)
TS (ppm).
%
Solids.
RPD
(°1°)
Blank
10:0000
23.6353
23.6354
0,0001
10.0
0.0
0.33`Y°
WBR SDNR 04/28114
10.0650
20.8592
20.9971
0,1379.
13700.9
1.4
0.33%
WBR SDNR 04/28114
DUP
10.6208
18.3630
18.5086
0.1456
13708.9
1.4
0,06%
0,33%
WBR SDNR 04/28/14
DUP
11.0768
24.5198
24.6717
0.1519
13713.3
1.4
0.03%
0.0000
. #DIV/o!
MV101
0.0000
#D{vro!
#DIVIDI
Total Volatile Solids
SOP 35 (SM 2540E)
Day I
Analyst A. IeRoux
0,0000
Blank (g)
Date start 04/29/14
Date End 04/29/14
- TS
Doing T.S.S
Time 1309,
`A",,-
Time 1445
1
Gravimetric Factor
Analyst Initials:
Reviewed by Initials:
0.0025
Mininum Wt Gain (g)
Dilution
Required
Sample ID
Dup
or
QC
True
Value
(ppm)
Sample
Size
(mL or g)
Tare
Weight
(9)
Final
Weight
(9)
Weight
Gain
(9)
TVs
(ppm).
%
Solids
RPD
(%)
Blank
10.0000
23.6353
23.9353
0.0000
0.0
0.0
WBR SDNR 04/28114
10.0650
.20:8592
20,9113
0-0521
5176.4
0.5
D,33°h
WBR SDNR 04/28114
DUP
18.3630
18.4181
0.0551
5187.9
0.5
0.22%
[0,33%
0,33 i
WBR SDNR 04/28114
DUP
24.5198
24.5773
0.0575
519.1.0
��t*0.6208
0.0000
0.0000
#D!V/0!
#DI,
0.0000
0.0000
#D{V/0!
#DIVIO!

Total Solids
SOP 35 (SM 2540B)
Day 36
Analyst A, IeRoux 0.0000 Blank (g)
Date start 05/27/14 Date End 05/28/14 TS Doing T.S.S
Time 1310 . Time 700 1 Gravimetric Factor
Analyst Initials: 777, Reviewed by Initials 0.0026 Mininum Wt Gain (g)
Dilution
Required
Sample ID
Dup
or
QC
QC
True
Value
(ppm),
Sample
Size
(mL or g)
Tare
Weight
(g)
Final
Weight
(g)
Weight
Gain
(g)
TS (ppm)•
%
Solids.
RPD
(%)
Blank -
10.0000
19.9050
19.9051
0.0001
.10.0
0.0
0.33%
WBR SDNR 04128/14
9.4794
23.5477
23,6755
0.127a
13481.9
1.3
0.33%
WBR SDNR 04/28M4
DUP
1
1 9.7537
21.2849
21.4162
0.1313
13461.6
1.3
0.15%
0.33%
WBR SDNR 04128/14
DUP
9.8752
23.6350
23,7740
0,1390
14075.7
1.4
4,46%
0.0000
#DIV/0!
#DIV/OI
0.0000
#DIV/O!
#DIV/0!
Total Volatile Solids
SOP 35 (SM 2540E)
Day 30
Analyst A. IeRoux
Date,start 05/28/14 Date End 05/28/14
Time 700 Time 840
Analyst Initials: Al Reviewed by Initials:
0.0000 Blank (g)
TS Doing T.S.S
1 Gravimetric Factor
0.0025 Mininum Wt Gain (g)
Dilution
Required
Sample ID
Dup
or
QC
True
Value
(ppm)
Sample
Size
(mL or g)
Tare
Weight
(g)
Final
Weight
(g)
Weight
Gain
(g)
TVs
(ppm).
% ,
Solids
RPD
N
Blank
10.0000
19.9050
19.9051
0,0001
10.0
0.0
0.33%
WBR SDNR 04/28/14
9.4794
- 23.5477
23.5962
0. 4485
5116.4
0.5
0.33%
0 33%
WBR SDNR 04/28/14
WBR SDNR 04128114
DUP
. DUP
9.75371
9.87521
21.2849
23.6350
21.33411
23.6876
0,0492
0.0526
5044.2
5326.5
0.5
0.5
1,42%
0.0000
0.0000
0.0000
#DIV/0!
#DIV101
0.0000
0.0000
0.0000
#DIV/01
#DN101
Vector Attraction Reduction [EPA 503.33(b)(3)]
<15% Is considered Passing
Sample
o ati es Day 1
Votatilles ay
o uc on
WBR SDNR 04/28/14
5176.4
6116A
1.172633562
WBR SDNR O4128M4
5187,9
5044.2
2.848665037
WBR SDNR 04/28/14
5191.0
5326.5
-2.542854616
#DN/01
=Vlof
#DIV/Ot
AVERAGES
$185.1
9Outliers
If usinn tha hinhaeF Fmm .4,,,
5185.0
LA:_�__. -
�1111**'*����
5
lowest from day'30, the percentage
!s <15, the test is considered passing
Final Percent Reduction -I 2.910273185
Final Result PASS

f ,
i Total Solids
SOP 35 ISM 2540B)
Day i
Analyst A. IeRoux 0.0000 Blank (g)
Date start 07/28/14 Date End 07/29/14 00 Doing g)
Time 1.40D Time 1200 1 Gravimetric Factor
Analyst Initials: k -- Reviewed by Initials: 0.0025 Mininum Wt rain rm
e utire
Required
0.33
0.33%WHR
0.33%
7331Y.
Sample ID
Blank
SDNR 07128114
WBR SDNR 07128/14
WSR SDNR 0712&14
Dup
or
QC
'DUP
UUP
True
Value
(ppm)
Sample
Size
(mL or g)
10.0006
10.3815
9.6479
9.1468
Tare
Weight
(g)
23.5435
21,2840
23.6334
24.45$1
Final
Weight
(9)
23.5437
21,3979
23.7381
24.5587
Weight
Gain
(g)
0.0002
TS (ppm).
20.0
%
Solids
RPD
(%)
0.0
0.1139
10971.4
1.1
0.1047
1 8852.1
1.1
1.09%
0.1008
10998.4
1.1
1.34%
0.0000
#DIV/0!
#DIV101
0.0000
#DIV/0!
#DMol
Total Volatile Solids
SOP 35 (5M 2540E)
Day 1
Analyst A. IeRoux
Date start 07/29/14
Date End 07l29/14
0.0000
00
Blank (g)
Doing (g)
Time 1200
Analyst Initials: "---
Time 1500
Reviewed by Initials:
1
Gravimetric Factor
0.0025 .
Mininum Wt Gain (g)
Dilution
Required
0.33%
0,33%
0 33°6
Sampie ID
Blank
WBR SDNR 07128114
WBR. SDNR 07/28/14
WBR SDNR 07/28/14
Dup
or
QC
DUP
DUP
True
Value
(ppm)
Sample .
Size
(mL or 9)
10.00DO
10.3815
9.6479
9.1468
Tare
Weight
(9)
23,5435
21.2840
23.6334
24.4581
Final
Weight
(9)
23.5433
21.3353
23.6806
24.5030
Weight
Gain
(9)
-0.0002
TVs
(PPrn).
-20.0
0.0513
4941.5
0.0472
0.0449
4892.3
4908.8
0.0000
O.000D
0.0000
0.D000
0. 0000
#DIV/0!
0.0000
#{71V/Ot
%
Solids
RPD
(%)
0.0
.
0.5
0.5
0.5
1.00%
0.34%'
#DIV/01'
#Dlvrol

Total Solids
SOP 35 (SM 25408)
Day 30
Analyst A. IeRoux
0.0000
Blank (g)
Date start 08/26/14
Date End 08/26/14
TS
Doing T.S.S
Time 730,
Analyst Initials: t,'
Time 1300
Reviewed by Initials:
1
Gravimetric Factor
0.0025
Mininum Wt Gain fa►
Dilution
Required
0.33%
0M%
0.33%
Sample ID
Blank
WBR SDNR 07/28/14
WBR SDNR 07128114
WBR SDNR 07/28/14
Dup
or
QC
DUP
DUP
True
Value
(ppm)
Sample
Size
• (mL or g)
10.0000
10.1446
10A755
9.9544
Tare
Weight .
(g)
19.9036
24.5210
23.6339
23.54451
Final
Weight
(g)
19.9038
24.6335
23.7468
23.6536
Weight
Gain
(9)
0.0002
0.1125
0.1129
0.1091
TS (ppm).
20.0
11089.6
11095.3
10960.0
°%
Solids
0.0
RPD
M)
1.1
1.1
1,.1
0.05%
1.23%
0.0000
#DIV/0!
#DIVroI
o.00�
#Dlv�o!
#Dlvrol
Total Volatile Solids
SOP 35 (SM 2540E)
Day 30
Analyst A. IeRoux
Date start 08/27/14 Date End 08/27/14
Time 900 Time 1200
Analyst initials: Reviewed by Initials:
0.0000 Blank (g)
TS Doing T.S.S
1 Gravimetric Factor
0.0025_ Mininum Wt Gain tal
Dilution
Required
0.33%
0.33%
0.33°fe
Sample 1D
Blank
VIfSR SDNR 07128114
WEIR SDNR 07/28/14
tIVBR SDNR 07l28/14
Dup
or
QC
DUP
DUP
True
Value
(ppm)
Sample
Size
(mL or g)
10.0000
10.1446
10.1755
Tare
Weight
(g)
19.9036
24.5210
23-63391
Final
Weight
(g)
19.9034
24.5721
23.6848
Weight
Gain
(g)
-0.0002
0.0511
0.0509
TVs
(ppm).
-20.0
5037.2
5002.2
4962.E
%
Solids
0.0
0.5
RPD
0.5
0.70%
04
0.79%
Ets2m��
#DNro!
#DIV10!
#REF!
#KEPI
Vector Attraction Reduction [EPA 503.33(b)(3)) <15% is considered Passim
amp
WBR SDNR 07128114"
WBR SDNR07/28/14
WBR SDNR 07/28114
o ea ay
4941.6
4892.3
4908.8
o a ay
5037,2
5002.2
4862.6
u on
71.89MS697
-2.19812485E
-1.084284427
AVERAGES
Outliers
if using the highest from day 1 and
#DIV101
4914.2
4941.6
I i ties.
#DIV/0!
5000.7
4962.6
#DIV/01
-i.72939602$
-0.425180349
lowest from day 30, the percentage '.A OL
is, a15• the test is considered passing Final Percent Reduction. -I -0.4251803 9-
Final Result PASS

Total Solids
SOP 35 (SM 2540B)
Day 1
Analyst A. IeRoux 0.0000 Blank (g)
Date start 11/13/14 Date End 11/14/14 TS Doing T.S.S
Time 130/'1 Time 800 1 Gravimetric Factor
Analyst Initials:] Reviewed by Initials: 0.0025 Mininum Wt Gain (g)
Dilution
Required
Sample ID
Dup
or
QC
True
Value
(ppm)
Sample
Size.,
(mL or g)
Tare
Weight
(g)
Final
Weight
(g)
Weight
Gain
(g)
ITS (ppm).
%
Solids
RPD
(%).
Blank
10.OWO
19.9039
19.9038
0.0002
20.0
0.0
0.33%
WBR SDNR 11/13114
9M95
24.4688
24.5587
.0.0999
10299.5
1.0
0.33%
0.33%
, WBR SDNR 11/13/14
WBR SDNR 11/13/14
DUP
DUP
9.3654
9.6381
20.8165
24.5198
20.9129
24.6188
0.0964
0.0990
10293.2
10271.7
1.0
' 1.0
0.06%
0.21%
0.0000
#DIV/01
#DIV101
o.0000
#Dlvro!
#Dnnot
Total Volatile Solids
Day 1 SOP 35 (SM 2540E)
Analyst A. IeRoux
Date start 11/14/14 Date End 11/14/14
Time 1000 ' Time 1400
Analyst Initials: - Reviewed by Initials:
0.0000 Blank (g)
TS Doing T.S.S
1 Gravimetric Factor
0.0025 Mininum Wt Gain (g)
Dup
True
Sample
Tare
Final
Weight
Dilution
or
Value
Size
Weight
Weight
Gain
TVs
%
RPD
Required
Sample ID
QC
(ppm)
(mL or g)
(g}
(g)
(g)"
(PPm).
Solids
M),
Blank
10.0000
19-WW119-9034
-0.0002
20.0
0.0
0.33%
WBR SDNR 11/13/14
9.6995
24-45881
24.6052
0.0464
4783.8
0.5
0"33°%
WBR SDNR 11/13/14
DUP
9.3654
20.81651
20.8650
0.0485
5178_6
0.5
7.93%
0.33% 1
WBR SDNR 11/13114
DUP
9.6381
24.5198
24.5659
0.0461
4783.1
0.5
7.94°/a
0.0000
0.0000
0.0000
#DiV/0!
j#DIV10I
#DIVroI
0,0000
0.0000
0.0000
#DIV/0!

Total Solids
SOP 35 (SM 2540B)
Day 30
Analyst A. IeRoux 0:0000 Blank (g)
Date start 12/12/14 Date End 12/15/14 TS Doing T.S.S
Time 1310 � Time 1030 1 Gravimetric Factor
Analyst Initials: ,� Reviewed by Initials: 0.0025 Mininum Wt Gain (g)
Dilution
Required
Sample ID
Dup
or
QC
True
Value
(ppm)
Sample
Size
(mL or g)
Tare
Weight
(gj
Final
Weight
(9)
Weight
Gain
(9)
TS (ppm).
%
Solids
RPD
(°�)
Blank
10.0000
24A589
24.4591
0.0002
20,0
0.0
0.33%
WBR SDNR 11113114
11.4337
23.63351
23.7473
0.1138
9953.01
1.0
WBR SDNR 11/13/14
DUP
9.5957
20.8158
20,9100
0.0942
9816.9
1-0
1.38%0.33J
WBR SDNR 1111 4
9,3293
19,9036
19.9956
0.0920�#DIVIO!
9861.4
10
50,33%
0.4
0.0000
#DIV/01
0.0000IV/0!
#DIVroI
Total. Volatile Solids
SOP 35 (SM 2540E)
Day 30
Analyst A. IeRoux 0.0000 Blank (g)
Date start 12/15/14 Date End 12/14/14 TS Doing T.S.S
Time 1030 Time _1430 1 Gravimetric Factor
Analyst Initials: _ Reviewed by Initials: 0.0025 Mininum Wt Gain (g)
Dilution
Required
Sample ID
Dup
or
QC
True
Value
(ppm)
Sample
Size
(mL or g)
Tare
Weight
(9)
Final
Weight
1 (9)
Weight
Gain
(9)
TVs
(ppm).
%
Solids
RPD
(%)
Blank
10-0000
24.4589
24.4587
-0.0002
-20.0
0.0
0.33%
WBR SDNR 11/13/14
11.4337
23.6335
23,6880
0.0545
4766.E
0.5
0.33%,
0.33%
WBR SDNR 11/13114
WBR SDNR 11/13/14
DUP
DUP
9,5957
9.3293
M8158
19.9036
20.8605
19.9476
0.0447
0.0440
4658.3
4716.3
0.5
0.5
2.30%
1.24%
-
0.0000
0.0000
0.0000
#DIV/01
#DN/01
0.0000
#REFI
#REF!
#REFI
Vector Attraction Reduction [EPA 503.33(b)(3)] <15% is considered Passing
Sample 113
vola-Hre-8 May 1
volafiles ayReduction
WBR SDNR 11/13114
4783.8
4766.6
0.35960049
WBR SDNR 11/13/14
5178.6
4658.3
11.16921685
WBR SDNR 11/13114
4753.1
4716.3
1.415860444
#11XN/01
#DN/01
MV101
AVERAGES
4916.2
4713.8
4.272720709
Outliers
5178.6
4658.3
11.16931069
lowest from day 30, the percentage
is <15. the test is considered passing,
Final Percent Reduction: 11.16931069,
Final Result PASS

E
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF = B
WQ Permit Number: W00023693 Laboratory: 1) Environmental Chemists Inc.
Facility Name: County Of Brunswick Utilities 2)
Residual Source WQ # or NCO086819 3)
NPDES #: 4)
WWTP Name: North East WWTP 5)
RPcirinal Analveie Ilata
Parameter
(mg/kg)
Cone.
Limit
m a
Sample or Com osite
Date
11101211
4
Percent Solids (%)
NA
3.33
Arsenic
75
21.4
Cadmium
85
21.4
Copper
4,360
235
Chromium
NA
25.6
Lead
840
'21.4
Mercury
57
1.26
Molybdenum
75
21.4
Nickel
420
26.8
Selenium
100
21.4
Zinc
7,500
1460
Total Phosphorus
NA
866
TKN
NA
109000
Ammonia -Nitrogen
NA
51500
Nitrate and Nitrite
NA
115
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of 1 , th t this docu was prepared under my direction or supervision in accordance with a system designed
Z -(Z-��
Signatur of reparer * Daie
*Preparer is defined in 40 CFR Part 503.9(r) nd 15A NCAC 2T .110
l 102 (26)

... 000NTY OF BRUNSWICK,PUBLIC UTILITIESLAND.APPLICATION PROGRAM
-RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 10, 2014
North East WWTP Permit No. NCO044873
Mineralization rate 0.30 Solids 3.33
6.R4 nH
(rtlkQl'(%*10:0Q01.::; : - : _ ' ::' ".: •.; ,
Lis/DryTon
PAN Surface
43115
86.23
PAN Injected
68865
-137.73
TKN
! 109000
218
Ammonia Nitrogen (Am)
51500
103
Nitrate Nitrogen (Nin)
115
0.23
Organic Nitrogen (Orn)
" 0.002
Total Phosphorus (P)
866
1.732
Total Phosphate (P205)
0.002
Estimated Avail. P205
0,002
Total Potassium (K)
13900
27.8
Total Potash (K20)
0.002
Arsenic (As)
21.4
0.0428
Cadmium (Cd)
21.4
0.0428
Chromium (Cr)
25.6
0,0512
Copper (Cu)
235
0.47
Lead (Pb)
21.4
0.0428
Mercury (Hg)
0.002
0.000004
Molybdenum (Mo)
21.4
0.0428
Nickel (Ni)
26.8
0.0536
Selenium (Se)
21.4
0.0428
Zinc (Zn)
1460
2.92
Aluminum (AI)
7480
14.96
Calcium (Ca)
23600
47.2
Iron (Fe)
0.002
Sodium (Na)
2510
5.02
Sulfur (S)
0.002
Magnesium (Mg)
5170
10.34
Manganese (Mn)
0.002
nnvironmentai Lnemiscs, mc. Lu14-UU3/9
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+ Ammonia N + Nitrate N +Nitrate N - % PAN
' Surface Application (Mineralization Rate)(TKN-Ammonia N)+ (0.5) (Ammonia N) + Nitrate N +Nitrate N -
% PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes.
6500 load .9025 lb per load = 77.830 lb PAN per Load / Injection 124,301
4500 load .624 lb per load = 53.882 lb PAN per/ Injetion 85.943
I

c` ► - �a
. ENVIRONMENTAL CHEMISTS, INC OFFICE: 910392-0223 FAX [phone]
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info®environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
CLIENT: ,Jv-Sw.�C � V19, ��-•
PROJECT NAME: KAIP�Q-
tIEPORTNO: l
'�
ADDRESS: t G k
CONTACT NAME: Y4- -e-r
PO NO:
tn�t Erg S ►�- �� - N C-
REPORT TO: s ��- i O n
PHONE/FAX:
COPY TO: -e —
email:
QamnloA Rv- 1 '09LZL-i SAMPLE TYPE- 1= Influent. E = Effluent. W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
�... __ -Jr.
Sample Identification
Collection
w �
y.
� `o �
c `o
Vo
.2 �
a
Qa'
PRESER1iATION
- -
ANALYSIS REQUESTED
Date
Time
Temp
a
�
�
o
0
0
0
�
o
io"'"
fit-
c-I(i-t
o�45
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G.
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Datelrme
Received By:
Date/Time
2.
Temperature whe eceived: Accepted: je ted: Resamp
Delivered By: `"�/f% � Received By: �� `i A t 7 Date
Comments:

Environmental Chemists, Inc*
6602 Windmill Way • Wilmington, NC 28405
j ! 'L [phone]"(Lab) ! [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
i
Brunswick County Public Utilities
Date.of Report: Mar 11, 2014
Post Office Box 249
Customer PO #:
Bolivia NC 28422
Report #: 2014-00379
Attention: Donald Dixon
Report to: Donald Dixon
-
Project ID: NFEBR
Lab ID Sample ID:
Colledt Date/Time Matrix Sampled by
—
14-00926 Site. NER WWTP
1/10/2014
8:45 AM Solid/Sludge (3. Worley
Test
Method
Results Date Analyzed
Chlordane
SW 846 Method 8081 613510
<0.005 mg/L
01/23/2014
Endrin
sw i)46 Method aoa1ar3510
<0.00005 mg/L
01/23/2014
Heptachlor
Sw846Method 8081613510
<0.00005 mg/L
01/23/201.4
Heptachlor epoxide
SW 848Method 80811313510
<0.00005 mg/L
01/2312014
Lindane
SW 846 Method8001813510
<0.00005 mg/L
01/23/2014
Methoxychlor
SW 846 Method e0s11ir3510,
<0.00005 mg/L
01/23/2014
Toxaphehe
SW 848 Method 808110516
<0.005 mg/L
01/23/2014
1,4-Dichlorobenzene (TOLP)
SW 846 method 827013510
<0.050 mg/L
01/23/2014
2,4,5-Trichlorophenol (TCLP)
SW 846 method 827013510
<0.050 mg/L
01/23/2014
2,4,6-Trichlorophenol (TCLP)
SW846 method 32T013510
<0.050 mg/L
01123/2014
2,4-Dinitrotoluene (TCLP)
I SW846 method 8270/3510
<0.050 mg/L
01/2312014
Cresol (TCLP)
SW 048 method 827013510
<0.050 mg/L
01/23/2014
r
Hexachloro-1 ,3-butadiene (TCLP)
SW 846 method 8270*510
<0.050 mg/L
01/23/2014
Hexachlorobenzene (TCLP)
SW 848 method 627013610
<0.050 mg/L
01/23/2014
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mglL
01123/2014
m + p-Cresol (TCLP)
SW $46 method 8270/351D
<0.050 mg/L
01 /2312014
Nitrobenzene (TCLP)
SW 846 method 8270r3510
<0.050 mg/L
01/23/2014
o-Cresol (TCLP,)
SW 846 method 827013510
<0.050 mg/L
01/23/2014
Pentachlorophenol (TCLP)
SW 846 method $27013510
<0.250 mg/L
01/23/2014
Pyridine (TCLP)
SW 846 method 62701$510
<0.050 mg/L
01/23/2014
'
2,4,5-TP
SWU8 Method 8151A
<0.0003 mg/L
01/28/2014
2,4-D
SWa48 Method 8151A
<0.0003 mg/L
01/28/2014
1,1-Dichloroethylene
SW848Method 826015030
<0.01 mg/L
1/29, 014
1,2-Dichloroethane
SW846Method 826015030
< 0.01 mg/L
1/29/2014
—
Benzene
SW846 Method 82601503D
< 0.01 mg/L
1/29/2014
Carbon Tetrachloride
SW846 Method 826015030
< 0.01 mg/L
1 /29/2014
Report*.: 2014.00370
Page 1 of 3

-
Environmental Chemists,
Inc.
7enviroc
6602 Windmill Way • Wilmington, NC 28405
-
[phone] (Lab) • [phone] (Fax)
L
®
710 Dowsertown Road • Manteo, NC 27954 '
[phone] .
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DL5 CEMRCATE#37729
Brunswick County Public Utilities
Date of Report: Mar 12, 2014
Post Office Box 249
Customer PO #:
Bolivia NC 28422
'Report #: 2014-00379 .
Attention: Donald Dixon
Report to: Donald Dixon
Project ID: NEBR
Chlorobenzene
SW846 Method B26015030
< 0.01 mg/L
1 /29/2014
Chloroform
$W846 Method 826015030
< 0.01 mg/L
1129/2014
Methyl ethyl ketone
SINUS Method826018030
<0.05mg/L
1/29/2014
Tetrachloroethylene
SWOO Method 82601SWO
< 0.01 mglL
1 /29/2014
Tricilloroethylene
SW846 Method 8260/5030
< 0.01 mg/L
1/,29/2014
Vinyl Chloride
SWO46 Method 828015030
< 0.01 mglL
' 1/29/2014
RCI
Cyanide
EPA335A
<0.112mg/kg
02/07/2014
Sulfide
sM 4500 S 0
<0.22 mg/kg
02/14/2014
Ignitability
SW 846 method 1010
>212 °F
01/22/2014
Sludge Residuals
Aluminum
EPA200.7
7480 mglkg
02/03/2014
Arsenic
EPA 200.7
<21.4 mglkg
01122/2014
Cadmium
EPA200.7
<21.4mg/kg
01/22/2014
Calcium
EPA 200.7
23600'mglkg
01/20/2014
Chromium
EPA 200.7
25.6 mg/kg
01/22/2014
--
Copper
EPA200.7
235mg/kg
01122/2014
Lead
EPA 200.7
<21.4mgikg
01/22/2014
Magnesium
EPA 200.7
5170mglkg
01/20/2014
Molybdenum
EPA 200.7
<21.4mg1kg
01/22/2014
Nickel
EPA 200.7
26.8 mg/kg
01/22/2014
Potassium
EPA 200.7
13900 mg/kg
01/20/2014
Selenium
SPA 200.7
<21.4mg/kg
01/22/2014
Sodium
EPA 200.7
2510 mg/kg
01/20/2014
'
Zinc
EPA 200.7
1460 mg/kg
02/11/2014
Ammonia Nitrogen
SPA380.1
51500mg/kg
01/17/2014
Total Kjeldahl Nitrogen (TKN)
EPA 351:2
109000 mg/kg
03/01/2014
Nitrate+Nitrite-Nitrogen
EPA 3W.2
115 mg/kg
02/10/2014
Total Solids (%)
sM 2640 6
3.33 %
01/16/2014
Report #:: 2014-OD379 Page 2 of 3.

Environmental Chemists, Inc.
envitrochem 6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Pax)
4 710 Bowsertown Road • Manteo; NC 27954
ANALYTICAL & CONSULTING [phone]
CHEMISTS NCDENR-. DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Brunswick County Public Utilities
Date of Report: Mar 11, 2014
Post Office Box 249
Customer PO M.
Bolivia NC 28422
Report #; 2014-00378
Attention: Donald Dixon
Report to: Donald Dixon
Project ID: NEBR
( pH
SM 4600 H B
7.42 units
01123/2014
Total Phosphorus
SM 4500 P F
866 mg/kg
03/04/2014
Mercury
SW6467471a
1.26 mg/kg
01/17/2014
TCLP Metals
Arsenic
EPA200.7
<0.100mg/L
02/03/2014
Barium
EPA 200.7
<0.100 mg/L
02101 /2014
Cadmium
EPA200.7
<0.100mg/L
02/03/2014
Chromium
EPA 200.7
<0.1,00 mg/L
02/03/2014
t Lead
EPA200.7
<0.100mg/L
02/03/2014
" Selenium
EPA200.7
<0.100mg/L
02/03/2014
Silver
EPA200.7
<0.100mg/L
02/01/2014
Mercury
Sw846 7470A
<0.002 mg/L
02/1412014
Comment: Sludge residuals reported on a dryweight basis. RCI and pH reported on an as received basis.
Reviewed by; &
o
`L
Repad #:: 2014-00379 Page 3 of 3

AIVIV UAL rAl liVhh N AIND V hU 1 VK A 1 1 KAl: l'1gJA KLIPM 11VP1 UMV1 tM3 Kllres)
Facility Name: County of Brunswick Utilities WQ Permit Number: WQ0034468
WWTP Name: Northeast Brunswick Regional WWTP NPDES Number: W00086819
Monitoring Period: From I/l/20Y4 To 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Class A773
Alternative 1 El
Alternative
Alternative 2
Alternative
........................
Alternative 4 ❑
Alternative 5 C.
Alternative 6 ❑
If applicable to alternative
performed (Class A
only) indicate "Process to Further
Reduce Pathogens":
Compost. ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ra ' ❑
Pasteurization ❑
Class B:
Alternative I El❑
1 rn ive2"
A to at
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying❑
Com ostin ❑
Aerobic Digestion ❑
Anaerobic Digestion
If applicable to alternative porformed Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number,o
Excee-
Frequency
of Analysis
Y
Sample
Type
a ica
Tech-
'nimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
wei ht
Vector Attraction Reduction (40 CER 50.33) - Flease indicate option performed:
Alt.1 (VS reduction) Q
Alta 2 (40-day bench) ❑
Alt..3 (30=day bench)
Alt. 4 (Spec. O: uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑Alt.
S (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
k attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Prepare
,;Name and Title (type or print)
A
Signature f�rP eparer , Date Signature og
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
)(type or print)
ILI/�
Date
DENR FORM PVRF 503 (12/2006)

County of Brunswick Public Utilities
West Brunswick Regional Facility Laboratory
(XD North, Carolina Laboratory Certification Number. NC00903
Anna leRoux, Lab Supervisor PO Box249 235 Grey Water Road Telephone: [phone]
alerouxnbmnsco net $olivia NC 28422 Supply, NC 29462 Fax: [phone]
Report Date: 2-May-2014
- , Eadi ty Sample Tyne Sample Date Resullfi
North
East Thirty Day Bench Beginning: 4/2/2014 Reduction of Vector Attraction (<15% is considered passing)
Regional Digestqr Scale Test Ending: 05/2/14 as Required to Meet Option 3 0.000/9
WWTP EPA [503.33(b)(3)] PASS .
SDNR
(End of Report)
Certified by:
Anna IeRoux, Laboratory Supervisor
0

Total Solids
SOP 35 (SM 2540B)
Day3o
Analyst A. IeRux
Date start 06/01/14 Date End 06/02/14
Time 1424 Time 730
Analyst Initials: 0,1 Reviewed by initials:
0.0000 Blank (g)
TS Doing T.S.S
1 Gravimetric Factor
0'.0025 Minlnum Wt Gain (g)
Dilution
Required
Sample ID
Dup
or
QC,
QC
True
Value
(ppm)
Sample
Size
(mL or 9)
Tare
Weight
(9)
Final
Weight
(9)
Weight
Gain
(9)
TS (ppm).
°%
Solids
RPD
(%)
Blank
10.0000
23.6351
28.6353
0.0002
20.0
0.0
0.33°%
NER 30 Day Bench Test 04/02114
9.5599
21.2832
21.3889
0.1057
11056.6
1.1
0.331/6
NER 30 Day Bench Test 04/02/14
DUP
9.7490
19.9027
- 20.0094
0.1067
10944.7
1.1
1.02%
0.33%
NEW 30Bench Test 04102114
DUP
9.4790
23.5439
23.6478
0.10391
10961.1
1.1
0.15%
0.0000
#DIV/01
#DIVIOi
0=01
#DIV/01
#DIV/0l
Total Volatile Solids_
SOP 35 (SM 2540E)
Day 3D
Analyst A IeRoux
0.0000
Blank (g)
Date start 05/02/14
Date End 05/02/14
TS
Doing T.S.S
Time 730 1
Time 1330
1.
Gravimetric Factor
Analyst Initials:T!
1
Reviewed by Initials:
0.0025
Mininum Wit Gain (g)
Dilution
Required
Sample10
Dup
or
QC
True
Value
(ppm)
Sample
Size
(ml-or9)
Tare
Weight
1 (9)
Final
Weight
(9)
Weight
Gain
(9)
TVs
(ppm).
%
Solids
RPD
(%)
Blank
10.00001
23.6$51
23.6350
-0.0001
-10.0
0.0
0.330%
NER 30 Day Bench Test 04/02114
9.55991
21,2832
21.3180
0.0348
3640.2
OA-
0.33%
NER 30 Day Bench Test 04/02/14
DUP
9.7490
19.9027
19.9375
O.OMI
3569.6
CIA
1.96%
0.33%
NER 30 Day Bench Test 04/02114
DUP
9.4790
23.5439
23.5784
0.0345
3639.6
CIA
1.94%
0.0000
0.0000
0.0000
#DIV/01
MY101
0.0000
0.0000
0.0000
#DIV/OI
#DIV/OI
Vector Attraction Reduction [EPA 503.33(b)(3)] <15% is considered Passing
amp
o a es ay
o tt y
e u on
NER 30 Day Bench Test 04/02M4
3481A
3640.2
-4.361651651
NER 30 Day Bench Test 04/02114
3449.1
3569.6
-3.375579656
NER 30 Day Bench Test 04/02/14
3608.1
3639.6
-3.614666381
#DN/01
#DIV/01
#DN/01
AVERAGES
3479.5
3616.5
-3.780629404
Outliers
3508.1
3569.6
-1.722882116
If using the highest from day 1 and Highest Lowest
lowest from day 30, the percentage
is <16, the test is considered passing. Final Percent Reductlon:j 4.722882116
Final Result PASS

Legend
I
Name Start End Duration Scale Units ffin max Avg Std DevLatton
NEWW2 Mad Tank No.2 Tamp Sensor 1 1/14/2014 10:03:13 AM 1/17/2014 la:03:13 3d 00:00:00 0-100 Deg C 62.319901 68.40049 65,621066 1.540421
GlOODeg C AM
NEWW2 Atad Tank No.2Temp Sensor 2 11141201410:03:13 AM 1117/201410:03:13 Sd 01100:00 0-100 Deg C 62,539684 68.62027 65.828870 1.536411
AM
Page 1

11
-
A,•rwm
4
l
F
I .
Legend -
Namo start End Duration Scale Unite Mn Max Avg Std Deviation
NEW W2 Atad Tank No.2 Temp Sensor 1 211412014 10:03; 13 AM 2/17/201410:03:13 3d 00:00:00 0.100 Deg C 60.537239 67,498946 65.464794 1.951109 "
0-100 Deg C AM
NEW W2 Atad Tank N0.2 Temp Sensor 2 21141201410:03:13 AM 2117/201410:03:13 3d 00:00:00 0.100 Deg C 60.739601 67.692307 65.664" 1.951629
0.100 Deg C AM -
!.n�„ v;,., v--., .!".v.�., ...,➢...,,.,.an:,,!S:tie�Fr,f..r,:".a'n.:..:.,.�: .,;;�x - etr.. - - '
- i% p. ., ' 0,i,{; .,�' � ,:,➢,1-tti�V;�,iti.. „e„vr .,, `�pty" "err:'.-
I � � ..T?►do2 .iD�Y._,. . „',.11/i _ x!ir1 3 .72M .1 :, ' � ,'`d�t 1.:,;�ikT[.,:�8_ ,�ii+'�"` _
P'4. J1Mati..
Ups'+. .i. �W'a;l� r.•,.Ar:,.aad:?.-.ai..�., ..mc, ti'n;Y`^W�;�. :,.::�..,.� �.,.�^ - . �::�:.,,s.,.-:.:'.;,z Wit,
i
Page 1

I
Legend
Name start End Duratlon Scale Units MA Max Avg Std Deviation
NEWW2 Atad Tank No.2 Temp Sensor 1 3/1412014 10:03:13 AM 3117/2014 10;03:13 3d 00:00:00 0-100 Deg C 60AI5142 69.865692 emsim 2.798M
0-100 Deg C AM
NEWW2 Atad Tank No.2 Temp Sensor 2 311412014 10:03:13 AM 3/17/2014 M0313 3d 00:00:00 0-100 Deg C 60.6105 70.085472 65.782714 2.803852
0-iD0DegO AM
Jim ;1�, El RAMMIUM'M
Page 1

i
i
i
Legend
Noma Star[ End Doratlon Seale Units Min Max Avg Sid Deviation
NEW W2 Atad Tank N8.2 Temp Sensor 1 4114/201410:03:13 AM 4/17/201410:03:13 3d 00:00:00 0-100 Deg C 57.045177 69.133097 63.789 3.670726
0-100 DegC AM
® NEWW2 Atad Tank N0.2 Temp Sensor 2 41141201410,03:13 AM 4117/201410:03:13 3d 00:00:00 0.100 peg 67.240536 69.352867 63.994251 3.669192
0.100 DegC AM
kuva>arii1°24e6e�6t0eac att4amglbo3larWrN�reak4�afl313 �dobo� Qrj2 r7 s6 1Do37st� 7is1 ay36s
5 1
�Aggo
"ir,t�+
Page 1

Legend
Name Start End Duration Seale Units Min Mu Avg Std Deviation
NEW W2 Atad Tank No.2 Temp Sensor 1 5/141201410:03:13 AM 5/17/201410:03:13 3d 00:00:00 0.100 Deg 0 60.561661 69.62149 65.191227 2.22448
0.100 Deg C AM
® NEW W2 Atad Tank No.2 Temp Sensor 2 61141201410:03:13 AM 5117/201410:03:13 3d 00:00:00 0 -100 Deg 0 60.757019 69.816849 65.401622 2.22374
0.100 Deg C AM
;-
I
�' utieiIO
a¢r,d `,1��.., o,s, ,.a�. 4-,� �' ,..�.�.,� fit., �.7,. a:..F ..« _I a� Wit, ..ay. tc 5: t .3,` ,hr .r...'. a- .K, �s.. ry�tii. .au'?_",'� ,.�,a�•.
Page 1

__ m, S°° , - - •rmPo`-- "ram
I
Legend
Name Start End Ourgtlon Scale Units Mn Man Avg Std Deviation
NEW W2 Atad Tank Not Temp Sensor t 61141201410:03:13 AM 6117/2014 10:03:13 3d 00:00:00 0 -100 Deg C 59.3895 68.769362 65.064546 2.23929
0.100 Deg c AM
® NEW W2 Mad Tank No.2 Temp Sensor 2 61141201410:03:13 AM 6r17/201410:03:13 3d 00:00:00 0. 100 Deg C 59.60928 69.102896 65.274357 2.234083
0.100 Deg c AM
ra N_N)LW2AInIf14o.2tevq�0.10Y-ee 8(74l`1D1�'I(]d�,'f+4R(Wr6�17I?A14QD73i „ y3�Op,00' iD -12. s iJ661{ 110 �.^�641 8959D951 DO.08729, ,
.
Page 1

Legend
Name Start end Duration Scale Units Mn Max Avg Std Deviation
NEWW2 Atad Tank NO.2 Temp Sensor 1 7/1412014 10:03:13 AM 7117/2014 10:03:13 3d 00:00:00 0-100 Deg C 59.975578 66.435552 64-287178 1.565609
0-100 Deg C AM
NEWW2 Atad Tank No.2 Temp Sensor 2 711412014 1043:13 AM 7117/201410:03:13 3d00:00;00 0-100 D09 C 60.612821 66.655332 64.498598 1.650325
0-100Dag o AM
74-I"79W I
4. A .091 1 Sit
'M Vf" MIPM 41
Page 1

I
Legend
Nome Start End Duration Scala Units L'Un Max Avg Stdl Deviation
NEWW2 Atad Tank Not Temp Sensor 1 8114/2014 10:0313 AM 0/171201410:03:13 3d 00:00:00 0- IOD Deg C 69295483 68.647012 65.599863 1.98816
0-100Deg o AM
NEWWP Atad Tank No.2 Temp Sensor 2 SM41201410:03:13 AM 81171201410:03:13 3d 00:00:00 0-100 Deg C 62AD0841 68.766792 65.80896 1.989387
&iOODeg C AM
Page 1

I
Legend
Nan" Start End Duration Scale Units Mtn Malt Avg
Std Deviation
NEWW2 Atad Tank No.2 Temp Sensor 1 9114/2014 10:03:13 AM 9117/201410;03:13 3d 00:00:00 0-100 Deg C 62.124542 67-52137 66.181195
1.264998
0-100Deg c AM
NEWW2 Atad -rank Not Temp Sensor 2 9/1412014 10:03:13 AM 9117/201410:03:13 3d 00:00:00 0-100 Deg C 62.319901 67.74115 68.393812
1.256801
0-100 Deg C AM
Page 1

Legend
Nam start End Duration SwIO Units Wit Max Avg Sid DGVMon
NEWW2 Ataci -rank Not Temp Sensor 1 10114/201410.03:13 10/17/2014 10:03:13 3d 00:00:00 0.100 Deg C 60.21978 65.445663 63.657009 0.962083
0-100 Deg C AM AM
NEWW2 Atad Tank No.2 Temp Sensor 2 10/141201410:03:13 10MM014 10:03:13 3d D0:00:00 0-100 Deg C 60-561661 65.641029 63.871517 0.955234
0-10ODeg c AM AM
Page 1

Legend
Name Start End Duration Scale Units Min Max Avg End Deviation
NEWW2 Atad Tank No.2 Temp Sensor 1 11114/20141(l.03:13 11117/2014 19.03:13 3d00:00:00 0-100 Deg C 60.781441 67.228325 65.540084 1.612588
0-100 Deg C AM AM
NEWW2 Atad Tank NO.2 Temp Sensor 2 1111412014 10:03:13 11/17/2014 10:03:13 3d 00:00:00 0-100 Deg C 60.976803 67.448105 65.748935 1.614213
0-100pegc AM AM
Page 1

I
Legend
Marna start End Duration Scale Unite Win Max Avg Std Deviation
NEWW2 Atad Tank NO.2 Temp Sensor 1 12/141201410:03.,13 12/17/2014 10:03:13 3d 00:00:00 0-100 Deg 0 59.316238 68-571426 65.840417 2.377615
0-100Deg c AM AM
NEWW2 Atad Tank N0.2 Temp Sensor 2 12/141201410:03:13 12/17/201410:03:13 Sal 00:00:00 0-100 Deg C 59.5116 68.766792 66.054198 2.3788
0-100 Deg C AM AM
Azfj 4 O—Owl �N 0.11 We-,
wf" v
..........
Page 1

COUNTY OF BRUNSWICK PUBLIC UTILITIES
LAND APLICATION PROGRAM
PERMIT W06034468
2014 APPLICATIONS
APPLICATION SUMMARY
Metric Tons 11 444.03 0.907