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HomeMy WebLinkAboutWQ0031725_Residual Annual Report 2014_20150223a, RECEIVED FEB 2' 3 '2015 DWR SECTION INFORMATION PROCESSING UNIT Baxter Health-care20 Baxter Healthcare Corporation 2014 Annual Report Land Application Program NC Permit No. WQ0031725 Medical Products na"er February 17, 2015 NCDENR DWQ Information Processing Unit 1617 Mail Processing Unit Raleigh, NC27699-1617 RE: 2014 Annual Land Application Report Permit No. WQ0031725 Baxter Healthcare Corporation McDowell County FEt3 2`3 2015 VRIF®RMASECTION T"NPROC SSING UNIT Please find the enclosed annual land application report for calendar year 2014. If you have any questions or require additional information, please contact me at 828-756-6017 or michael pisarikAbaxter.com. Sincerely, Michael J. Pisarik Sr. Environmental Engineer Cc: NC Division of Water Quality (3 copies with enclosures) WWTP File Copy EHS File Copy Baxter Healthcare Corporation 61 Pitts Station Road / PO Box 1390 / Marion, North Carolina 28752 T 828.756.4151 r3: ) � a k" ANN UAL PATHUGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Baxter Healthcare WWTP Name: Baxter Healthcare Monitoring Period: From WQ Permit Number: WQ0031725 NPDES Number: NC0006564 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ® Alt B (Alk Treatment) ® Alt. C (Prior Testing) Ah.D (No Prior Test) D Process to Further Reduce Pathogengs D If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost D Heat Drying D Heat Treatment D Theimophilic D Beta Ray D Gamma Ray D Pasteurization D Class B. JAII. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens D If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization D Air Drying D Com ostin D Ae_ robic Digestion D Anaerobi c Di i g est on If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- n s Frequency of Analysis Sample Type Analytical Tech - nicue Minim Geo. Mean axim Units Fecal Coliform 2 x 10, to the 6th power per gram of total solids MPN 8397 225,349 1280000 MPN/g 0 ��� b sm9221 c CFU REB 2 Z 2015 1000 mpn per gram of total solid (dry weight) INFORMA DWR SECTIOI ON PROCESSING UNIT Salmonella bacteria (in lieu of fecal coliform 3 WN per 4 grams total solid (dry weight) vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) Ed Alt. 2 (40-day bench) D Alt. 3 (30-day bench) ®Alt. 4 (Spec. OZ uptake) (� Alt. 5 (14-Day Aerobic) D Alt. 6 (Alk. Stabilization D Alt 7 (Drying - Stable) D 1 Alt. 8 (Drying - Unstable) Alt. 9 (Injection) D Alt. 10 (Incorporation) D No vector attraction reduction alternatives were performed D CERTIFI ATION STATEMENT (please check the appropriate statement) 53' "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." D "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination -has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." o.� Q c% �2 Dennis Key Southern Soil Builders, Inc. Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signa of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Medical Products February 23, 2015 NCDENR DWQ Information Processing Unit 1617 Mail Processing Unit Raleigh, NC27699-1617 RE: 2014 Annual Land Application Report Permit No. WQ0031725 Baxter Healthcare Corporation McDowell County FEB 2 7 2015 INFpRAM D �PSECTION NGUNIT Affe"er Please find enclosed the signed Annual Pathogen and Vector Attraction Reduction Form. This form was mistakenly sent unsigned as part of the annual land application report for calendar year 2014. If you have any questions or require additional information, please contact me at 828-756-6017 or michael-pisarik@,baxter.com. Sincerely, Michael J. Pisarik Sr. Environmental Engineer Cc: NC Division of Water Quality (3 copies) WWTP File Copy EHS File Copy Baxter Healthcare Corporation 61 Pitts Station Road / PO Box 1390 / Marion, North Carolina 28752 T 828.766.4151 a ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0031725 County: McDowell Year: 2014 Facility Name (as shown on permit): Baxter Healthcare Land Application Operator: Southern Soil Builders, Inc. Phone: 336-957-8909 Land application of residuals as allowed by the permit occurred during the past calendar year? 13 Yes . ® No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the ermit: 14 Total number of fields utilized for land application during the year: 7 Total amount of dry tons applied during the year for all application sites: 108.5 Total number of acres utilizes for land application during the year: 1 43.81 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. NYes El No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b),(applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permittee Name and Title (type or print) ~ 2 A 7 /1: ature of Permittee Date a-.7- IT Signature of Preparer* (if different from Permittee) * Preparer is defined in 40 CFR Part 503.9 (r) and Date of laAd Applier Date (if different from Permittee and Preparer) 15A NCAC 02T .l 102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0031725 Facility Name: Residual Source WQ # or NPDES #: WWTP Name: Residual Analvcic data Baxter Healthcare WQ0031725 Baxter Healthcare Laboratory: 1) 2) 3) 4) 5) A&L Eastern Labs. Parameter \mlgl Conc. Limit m x a Sample or Composite Date 1-22-14 Percent Solids (%) NA 9.75 Arsenic 75 8 Cadmium 85 2 Copper 4,300 118 Chromium NA 74 Lead 840 12 Mercury 57 0.6 Molybdenum 75 5 Nickel 420 25 Selenium 100 5 Zinc 7,500 305 Total Phosphorus NA 14800 TKN NA 111000 Ammonia -Nitrogen NA 7900 Nitrate and Nitrite a 17nr mid no 4; .,1 F ..; NA 1;f:,-.. az - 18.5 - - ---r _--- --- -- --� �--� ��•=ems --AU ULIVII 1u111LJ 11 LVLI ul unS 101 W are nor appacame. Keterence the mdividual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for su witting false information, including the possibility, of fines and imprisonment for knowing violations." Sign e of Preparer * Date 01 *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 9.93 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 Acres Used: 5.02 Acres Permitted: 5:02 Site #: DP2 Field #: DP2 Residual Analvsis Data (Heavy Metals and Tntal Phnenharnc r tea v"tr&- of c„14a. . ;� - '� . ; mCom- N E D. Total .:,, . .1.1-11.15 Total L2j 3 4 5 6 7 8 9 10 11 12 DT/Aa/ � App. i Event 1.98 14 Arsenic 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000.1 0.000 0.000 1 0.032 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.008 Copper 0.467 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.467 Chromium 0.293 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.293 Lead 0.047 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.047 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0..002 Molyb- denum 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Nickel 0.099 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.099 Selenium 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.020 Zinc , 1.207 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.207 Total Phos- 58.578 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 58.578 horus 11T nnri'iii ■nr�nr r, ., 11-„ ..F 7..�. i.L ��. �.L__ J_ _- - _ - r -- --✓ - •»••--».....� .,....,■,ateu� nao yicNaa- unuu, u.y u,.-ecuvn or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". SigKture of La Applier -. Date r)l=t%10 CnDhA nncl ec /41)11)nncN + ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare Total :Dry Tons Applied (Annual): WQ0031725 Cation Exchange Capacity (non 503 only): Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: 5.877 Acres Permitted: 5.877 Site #: DP3-Corn Field #: 16.05 FcB2 DP3-Corn Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . . com- posite SEEM d M m Total •M .. Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 J 12 DT/Ac./ o App. ►'. Event 2.73 Arsenic 0.044 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0:000 0.000 1 0.044 Cadmium 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.645 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.645 Chromium 0.404 0.000 0.000 0.000 0.000 0.000- 0.000 0.000 0.000 0.000 0.000 0.000 0.404 Lead 0.066 1 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0.066 Mercury' 0.003 0.000 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 denum Nickel 0.137 0.000 0.000 0.000 0.000 0.000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.137 Selenium 0.027 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.027 Zinc 1.666 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.666 Total Phos- 80.838 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 80.838 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Si ature of Lan pplier, a- 3- ► .5- Date DENR FORM MFLSF (12/2006) ANNUAL METALS HELD LUAll1N(7 SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare Total Dry Tons Applied (Annual): WQ0031725 Cation Exchange Capacity (non 503 only): Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: 19.25 FcB2 6.983 Acres Permitted: 6.983 Site #: DP3-Grass Field #: DP3-Grass Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ... com- posite Date 1 a n 11'I'MU2 lio 0 M. RIM Total Phos- ..• �;�� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 1 21 L 3 4 5 6 7 8 9 10 11 12 H DT/Ac./ C App. E4 Event 2.76 Arsenic 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.044 Cadmium 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.651 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.651 Chromium 0.408.1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.408 Lead 0.066 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.066 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 denum Nickel 1 0.138 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.138 Selenium 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Zinc 1.682 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.682 Total Phos- 81.607 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 81.607 horns "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly, gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Sigpdture of Land Applier Date DENR FORM MFLSF (12/2006) 'Wll A1V 1r U AL 1VIL 1'ALN l+ILLI) LUA EN li N U IVIN AK Y FURM' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare Total Dry Tons Applied (Annual): 15.65 WQ0031725 Cation Exchange Capacity (non 503 only): Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 6.8 Acres Permitted: 6.8 Site #: DP4 Field #: DP4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . , . Corn- posite Date, in M- Total Ph.;�� �� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 131 41 5 1718 9 10 ill 12 DT/Ac./ _qj c App. Event 2.30 Arsenic 0.037 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Cadmium 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 0.543 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.543 0.341 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.341 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.055 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 l 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 0.115 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.115 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 1.404 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.404 Phos- 68.110 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 68.110 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of LaridApplier {0- P s Date DENR FORM MFLSF (12/2006) L' A,kANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Baxter Healthcare WQ0031725 Total Dry Tons Applied (Annual): 30.31 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 Acres Used: 11.82 Acres Permitted: 11.82 Site #: DP5 Field #: DP5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): 10,lpm Com- posite Date Total Phos- .. -:�� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 1 21 3 4 5 6 7 8 9 10 11 12 DT/Ac./ 0 App. Event 2.56 " Arsenic 0.041 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.041 Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 0.605 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.605 Chromium 0.379 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.379 Lead 0.062 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.062 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 denum Nickel 0.128 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.128 Selenium 0.026 0.000 0.000 0.000 0.000 0.000 1 0:000 0.000 1 0.000 0.000 0.000 0.000 0.026 Zinc 1.564 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1.564 Total Phos- 75.894 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 75.894 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". r�- _-Kn- Si ature of La Applier Date I)FNR FnRM MFI SF (1?/?006) IL• � ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare Total Dry Tons Applied (Annual): 9.80 WQ0031725 Cation Exchange Capacity (non 503 only): Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 3.97 Acres Permitted: 3.97 Site #: DP6 Field #: DP6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- -in posite Monsoon' a a non NONE TotalDate • Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 111 2j 31 4 j5j 61 71 L8J9 10 Ij 12 DT/Ac./ o App. Event 2.47 Arsenic 0.040 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000,1 0.000 0.000 0.000 0.040 Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.010 Copper 0.583 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.583 Chromium 0.365 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000' 0.000 0.000 0.000 0.365 Lead 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.059 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 denum Nickel 0.123 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.123 Selenium 0.025 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 1 0.025 Zinc 1.506 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 1.506 Total Phos- 73.082 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 73.082 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". /�/�`". Z:� - - S' ature of Lan Applier Date DENR FORM MFLSF (12/2006) + ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 7.67 Permit #: WQ0031725 Cation, Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 Acres Used: 3.34 Acres Permitted: 3.34 Site #: DP7 Field #: DP7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date, Total Phos- ... �:�� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 11 1 21 1 3 1 5 6 __7j 1 9 10 1Ij 12 DT/Ac./ c App. Event 2.30 Arsenic 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Cadmium 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Copper 0.542 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.542 Chromium 0.340 0.000 0.000 0.000' 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.340 Lead 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.055 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- denum 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Nickel 0.115 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.115 Selenium 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.023 Zinc 1.400 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 1.400 Total Phos- 67.932 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 67.932 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land pplier 9-3-1S Date DENR FORM MFLSF (12/2006) r- ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON �- PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: DP2 Acres Utilized: 5.02 Land Owner: Douglas Poplin Annual Dry Tons Applied: 9.9364 Site #: DP2 Acres Permitted: 5.02 Operator: Douglas Poplin Predominant Soil Series: FcB2 Cation Exchange Capacity (non 503): Crop 1 Name: Corn Crop 1 Max. PAN: 214 Crop 2 Name: Crop 2 Max. PAN: ° ° QLiquid Volume applied enter one Solids/ ( ) Cu. Yds Gallons o /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Soil Cond. Wey' Moist) Precip. Past 24 Hrs. inches Y a oa w o �; ?', G D i .- 0 7y w. w CD �' a TKN mg/kg Z i; o°a o w mglkg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10-2014 121.01 9.75 1.979 WQ0031725 dry 0 Inc 1 0.3 111000 7900 18.5 153.790 NA Corn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 121.011 o As Cd Cu Cr Pb Hg Mo Ni Se Zn P 153.7901 0.000 Lime Applied Annual lbs/acre 0.032 0.07 0.102 36 0.008 0.032 0.040 34 0.467 1.626 2.093 1338 0.293 0.892 1.185 NA 0.047 0.136 0.183 267 0.002 0.003 0.005 15 0.020 0.056 0.076 NA 0.099 0.323 0.422 374 0.020 0.029 0.049 89 1.207 3.484 4.691 2498 58.578 ~ " Date lbs/ac Prior Years Cumulative lbs/ac 10-2014 2500 Current Cumulative lbs/ae Permitted C. P. L. R.**** Permit PAN Limit 1st/2nd Crop 214 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." / *Application Method: S - Surface, IN-- Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 **x Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signa re of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Cron 1 Name: Corn WQ Permit #: WQ0031725 Field #: DP3-Corn Annual Dry Tons Applied: 16.0504 Site #: DP3-Corn Predominant Soil Series: FcB2 Crop 1 Max. PAN: 214 Crop 2 Name: Acres Utilized: 5.877 Acres Permitted: 5.877 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: y Volume applied Volume Residual Sources Soil Precip. ,> C o o Z Nitrate PAN Applied Name of Crop Type ° Y (enter one) Solids/ % Applied per (NpDES #, WQ# Cond. Past 24 �. ;e w =° w TKN o 0 and . ( lbs/acre) Receiving Residual ° ° Liquid Solids Acre Fert., Animal W ems• Q �; * w. �' R. Nitrite lic Application Q Cu. Yds Gallons (Dry TonslAc) Waste, etc) Moist) inches mg/kg mglkg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 1-2014 57.67 9.75 0.806 W00031725 dry 0 INC 1 0.3 111000 7900 18.5 62.604 NA Corn 2-2014 87.13 9.75 1.217 WQ0031725 dry 0 INC 1 0.3 111000 7900 18.5 94.585 NA Corn 3-2014 50.67 9.75 0.708 WQ0031725 dry 0 INC 1 0.3 111000 7900 18.5 55.005 NA Corn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 "0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): TOTAL&I 195.47 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 212.1951 0.000 Lime Applied Annuallbs/acre 0.044 0.011 0.645 0.404 0.066 0.003 0.027 0.137 0.027 1.666 80.838 Date lbs/ac Prior Years Cumulative lbs/ac 0.187 0.071 3.673 2.443 0.305 0.007 0.124 0.692 0.43 8.186 10-2014 1000 Current Cumulative lbs/ac 0.231 0.082 4.318 2.847 0.371 0.010 0.151 0.829 0.457 9.852 Permitted C. P. L. R.**** 36 34 1 1338 1 NA 267 15 NA 374 89 2498 Permit PAN Limit lst/2nd Crop 214 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed iu assure LuaL qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 9-P-I Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin WQ Permit #: WQ0031725 Field #: DP3-Grass Annual Dry Tons Applied: 19.2437 Site #: DP3-Grass Predominant Soil Series: FcB2 Crop 1 Name: Fescue Crop 1 Max. PAN: 194 Crop 2 Name: Acres Utilized: 6.983 Acres Permitted: 6.983 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: o Y +� o (� Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonstAC) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Soil Cond. wry' Wet,a Moist) Precip. Past 24 Hrs. inches > 410 5 �, ^o o ❑. * o o w c �- C' Z 7y P o TKN mglkg Z Y 3 o R o o ? o mg/kg Nitrate and Nitrite mg/kg PAN Applied lbs/acre Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 3-2014 113.84 9.75 1.339 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 93.432 NA Fescue 4-2014 60.52 9.75 0.712 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 49.671 NA Fescue 11-2014 60 9.75 0.706 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 49.244 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS:J 234.36 01 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 192.3461 0.000 Lime Applied Annuallbs/acre 0.044 0.011 0.651 0.408 0.066 0.003 0.028 0.138 0.028 1.684 81.696 Date lbs/ac Prior Years Cumulative lbs/ac 0.187 0.231 36 0.071 0.082 34 3.673 4.324 1338 2.443 2.851 NA 0.305 0.371 267 0.007 0.010 15 0.124 0.152 NA 0.692 0.830 374 0.43 0.458 89 8.186 9.870 2498 10-2014 2500 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop F 194 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC.- Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin WQ Permit #: WQ0031725 Field #: DP4 Annual Dry Tons Applied: 15.6563 Site #: DP4 Acres Permitted: 6.8 Predominant Soil Series: FcB2 Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 194 Crop 2 Name: Acres Utilized: 6.8 Crop 2 Max. PAN: ° Y y ° A Volume applied pp (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert. Animal Waste, etc) Soil Cond. ��' Wet Moist) Precip. Past 24 1Irs. inches a c� o w * 0 o qy �; �, * �' * o a w' `� �' TKN mg/kg Z 9 1 o °o o w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4-2014 25.93 9.75 0.313 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 21.854 NA Fescue 5-2014 53.04 9.75 0.640 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 44.703 NA Fescue 6-2014 29.68 9.75 0.358 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 25.015 NA Fescue 7-2014 82.02 9.75 0.990 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 69.128 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 190.67 o As Cd Cu Cr Pb Hg MoF37489 Zn P 160.700 0.000 Lime A lied Annuallbs/acre 0.037 0.131 0.168 36 0.009 0.046 0.055 34 0.543 2.392 2.935 1338 0.341 1.685 2.026 NA 0.055 0.186 0.241 267 0.003 0.005 0.008 15 0.023 0.081 0.104 NA2498 1.404 5.467 6.871 68.110 Date lbs/ac Prior Years Cumulative lbs/ac 10-2014 1000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop 194 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 9-a-)f Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED_ ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ0031725 Field #: DP5 Annual Dry Tons Applied: 30.3190 Site #: DP5 Predominant Soil Series: FcB2 Crop 1 Max. PAN: 194 Crop 2 Name: Acres Utilized: 11.82 Acres Permitted: 11.82 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° c� o Q Volume applied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons u /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Drys Wet, Moist) Precip. Past 24 Hrs. inches y � 10 co �' o w �o_ o `P'. CD `y �' x� 7d g w , `- TKN mg/kg Z a � o p w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type p yp Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5-2014 59.49 9.75 0.413 WQ0031725 dry 0 s 0.5 0.3 111000 7900 1 18.5 28.845 NA Fescue 6-2014 53.33 9.75 0.370 W00031725 dry 0 s 0.5 0.3 111000 7900 18.5 25.858 NA Fescue 8-2014 140.8 9.75 0.978 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 68.270 NA Fescue 9-2014 115.62 9.75 0.803 W00031725 dry 0 s 0.5 0.3 111000 7900 18.5 56.061 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 b.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 369.241 0 As Cd Cu Cr Pb H.F4 Mo Ni Se Zri I P 179.0331 0.00o Lime Applied Annuallbs/acre 0.041 0.108 1 0.149 36 0.010 0.038 0.048 34 0.605 1.93 2.535 1338 0.379 1.26 1.639 NA' 0.062 0.162 0.224 267 0.003 0.004 0.007 15 0.026 0.065 0.091 NA 0.128 0.461 0.589 374 0.026 0.014 0.040 89 1.564 4.395 5.959 2498 75.894 - Date ibs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop ... .__. -_,_, . . . 194 "I certify, under penalty of law; that this document was prepared under my direction or supervision in accordance with a -system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." l/ Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loadinp_ Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ0031725 Field #: DP6 Annual Dry Tons Applied: 9.8025 Site #: DP6 Predominant Soil Series: FcB2 Crop 1 Max. PAN: . 194 Crop 2 Name: Acres Utilized: 3.97 Acres Permitted: 3.97 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: :e o A Volume applied pP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches y R b a o o �. �, * w w TKN mg/kg Z o mg/kg Nitrate and Nitrite mg/kg PAN Applied lbs/acre ( ) Name of CropType Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 11-2014 62.16 9.75 1.286 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 89.735 NA Fescue 12-2014 57.22 9.75 1.183 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 82.604 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 119.381 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 172.339 0.000 Lime A lied Annuallbs/acre 0.040 0.161 0.201 36 0.010 0.059 0.069 34 0.583 3.045 3.628 1338 0.365 2.142 2.507 NA �0.059 0.273 0.3312 267 0.003 0.005 0.008 15 0.025 0.103 0.128 NA. 0.123 0.491 0.614 374 0.025 0.015 0.040 89 1.506 6.766 8.272 2498 73.082 Date lbs/ac Prior Years Cumulative lbs/ac 10-2014 1000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop - - ,.... -. _ 194 1 certhy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loadinll Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ0031725 Field #: DP7 Annual Dry Tons Applied: 7.6651 Site #: DP7 Predominant Soil Series: FcB2 Crop 1 Max. PAN: 194 Crop 2 Name: Acres Utilized: 3.34 Acres Permitted: 3.34 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° y o Q 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources DES # W # 0 ' Fert., Animal Waste, etc) Soil Cond. D (ry, Wet, Moist) Precip. Past 24 Hrs. inches Y cc o' � a; '� 0 c �y P - � �' o' w � � �• 0 TKNo mg/kg Z ° mg/kg Nitrate and Nitrite mg/kg PAN Applied pp (Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5-2014 32.85 9.75 0.808 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 56.368 NA Fescue 10-2014 60.5 9.75 1.487 W00031725 dry 0 s 0.5 0.3 111000 7900 18.5 103.813 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 93.35 0 ' As Cd Cu Cr Pb Hg Mo Ni Se Zn P 1 0.1811 0.000 Lime Applied Annuallbs/acre 0.037 0.108 0.145 36 0.009 0.038 0.047 34 0.542 1.93 2.472 1338 0.340 1.26 1.600 NA 0.055 0.162 0.217 267 0.003 0.004 0.007 15 0.023 0.065 0.088 NA 0.115 0.461 0.576 374 0.023 0.014 0.037 89 1.400 4.395 5.795 2498 67.932 Date lbs/ac Prior Years Cumulative Ibs/ac 10-2014 2506 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1st/2nd Crop 194 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." � J *Application Method: S - Surface, IN - Injection, INC - Incorporation // F t-- �� " a-t Y **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3,. raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ..�,�,.i�..,ubv...vii�,,,..v.�,i �.cuviwu u►►N.iiuuuicu►aavii.uwu.cuwyiciu��uiucx.jruj�rrwuiir `• 1 `► Realistic field Expectations for North Carolina Soils The North Carolina Realistic Yield Database is the product of an extensive data gathering and review process conducted by NC State University, the Natural Resource Conservation Service, the North Carolina Department of Agriculture and ConsurmerServices, and the North Carolina Division of Soil and Water Conservation. In 1999, county -based representatives of each of the above -named organizations were asked to collect yield data and make a reasoned judgement of the yields for various crops on each of the soils occurring in their county. These data were collected from 87 responses, representing 93 counties. The data were then compared with available research data and intensively reviewed by a panel of field agronomists, soil scientists and researchers familiar with the soils, crops and climatic conditions in each region. In reviewing the data, the following assumptions were made: 1. Realistic Yield Expectations should be based on the average of the best 3 years in a 5 year period which could be achieved with a high level of management (top 20% of growers) 2. For soils that may be mapped in multiple regions or in slightly different landscapes (for example, flood plains or stream terraces), the Realistic Yields are based on the most common prevailing conditions for that soil rather than the most ideal site for agricultural production. 3. For soils that are Somewhat Poorly, Poorly, or Very Poorly Drained, effective artificial drainage MUST be in place to achieve the yields shown in the RYE tables. 4. For tobacco production in the Piedmont physiographic, irrigation was assumed to be available, whereas no irrigation was assumed in the Coastal Plain physiographic region. This is in accordance with numerous surveys which show less than 15%-20% of tobacco in the Coastal Plain is irrigated, while 70 to 80% of tobacco in the Piedmont receives some irrigation Citation: North Carolina Nutrient Management Workgroup. 2003. Realistic yields and nitrogen application factors for North Carolina crops. http://nutrients,soll,ncsu.edu/yields/ North Carolina State University, North Carolina Department of Agriculture and Consumer Services, North Carolina Department of Environment and Natural Resources, Natural Resources Conservation Service. Raleigh NC. To access the database, select a county and at least one crop. Multiple crops may be selected by holding the Ctrl key when selecting crops. A report will be generated showing a summary of currently available data for the county you selected. Select Your County Wilkes EsD: Evard-Cowee complex, 8 to 25 percent slopes, stony Select Your Soil EsE: Evard-Cowee complex, 25 to 60 percent slopes, stony FaD: Fairview sandy loam, 15 to 25 percent slopes FcB2: Fairview sandy clay loam, 2 to 8 percent slopes, moderately eroded Use Representative Slope Typical of the Soil Mapunit Correct for Slope Use my slope 0 Submit Reset 1 of 2 1/20/2014 1:56 PTV .... uiiubvuivu� ui l�viw �.ui viuiu uLLli.iiuuuiciILaavu.uUau.cuuiyicivai UIUOX.iuPttwuuLy Realistic Yields for FcB2: Fairview sandy clay loam, 2 to 8 percent slopes, moderately eroded in Wilkes County Crop Yield Nitrogen Factor Realiistic Nitrogen. Rate (lbs/acre) Estimated Phosphorus Removal (lbs P20s/acre) Barley (Grain) 67 Bushels 1.49 99 25 Corn (Grain) _ 108 Bushels _ 1.11 120 47 Corn (Silage) 19.6 Tons 10.9 214 67 Cotton _ 637_Pounds 0.081 52 18 Sorghum (Silage) 16.7 Tons 7.6 127 50 Oats (Grain) _ _ 83 Bushels__ 1.13___ 94 _ 21 Peanuts _ _ 0 Pounds 0 0 0 Rye (Grain) 49 Bushels _ 2.01 913 16 Small Grain (Silage) 8.8 Tons 11.1 98 48 Sorghum (Grain) _ 49 CWT 1.72 84 37 Soybeans (Double Cropped) 33 Bushels 0 0 _ 27 Soybeans (Full Season) 39 Bushels 0 0 31 Soybeans (Double Cropped - Manured) 33 Bushels 3.89 130 _ 27 Soybeans (Full Season - Manured) _ 39 Bushels 3.89 152 31 Tobacco (Burley) 0 Pounds 0.074 0 0 Tobacco (Flue Cured) 2548 Pounds 0.029 74 13 Triticale (Grain) 69 Bushels 1.52 104 _ 23 Tropical Corn (Silage) 19.6 Tons — 6.5 127 _ 67 Wheat (Grain) _ _ 49 Bushels 2.01 98 25 Bahiagrass (Hay) 3.4 Tons 44 151 39 Caucasion/Old World Bluestem (Hay) 3.4 Tons 44 151 41 Common Bermudagrass (Hay) 3.4 Tons _ 44 151 42 Dallisgrass (Hay) _ _ 3.4 Tons 44 151 45 Fescue (Hay) _ 4.4 Tons 194_ 69 Hybrid Bermudagrass (Hay) 4.4 Tons _44 44 _^ 194 54 Hybrid Bermudagrass overseeded with Rescuegrass (Hay) 0 Tons 44 0 0 Mixed Cool Season Grass (Hay) 3.2_Tons 44 140 45 Orchardgrass (Hay) 3.4 Tons 44 151 50 Pearl Millet (Hay) 3.7 Tons 49 _ 180_ 49 Rescuegrass(Hay) _ 0 Tons 44 _ 0 0 Sorghum Sudan (Hay) 4.2 Tons 49 204 58 Timothy Grass (Hay) 0 Tons 44 0 0 Additional Guidance for speciality crops can be found at: http://nutrients.soil ncsu.edu/guidance/ 2 of 2 1 /20/2014 1:.56 PM Location of Samples The Plant process diagram on the flowing page shows the location of where the following samples were taken. The Analysis from A&L Eastern Laboratories, Inc., report number 14-028-0210 was taken from the Belt Filter Press, and is labeled with a red X (it on the diagram. The Fecal Coliform Samples from Statesville Analytical Sample IDs 14019-20.1, 14019-20.2, 14019-20.3, 140122-27.1, 140122-27.2, 140122-27.3, 140122-27.4 were taken from Aerobic Digester No. 1 and is labeled with a blue X (V on the diagram. The Volatile Solids In, Sample ID 140122-25.1 was taken from where the solids from the clarifier are pumped to the aerobic digesters and is labeled with a green X (K) on the diagram. The Volatile Solids Out, Sample ID 140122-25.2 was taken from Aerobic Digester No. 1 and is labeled with a blue X I on the diagram. The TCLP test Sample ID 14019-18was taken from Aerobic Digester No.I and is labeled with a blue X I on the diagram. PLAN SCALE. 1 40' WASTEWATER TREATMENT PLANT EVALUATION BARTER HEALTHCARE CORPORATION McDOWEII CpUNJY, NORTH CAROLMA — T T -6"PVC----------- I l I �yk\ I CLARIFIER CLARIFIER N 150,000 GALLON FILTER SLUDGE BASIN I I I No.3 No.4 � I I J t0 o AERATION BASIN l ° f No.2 )N D --xL— I n —6"cIP—JI I CHLORINE I a I AEROBIC I I I I v I j�i�i � i CONTACT I DIGESTER c /o � oO° I I I I CHAMBERS No.2 a"cIP'g CLARIFIER " ---°C--- --II �'(I Z -----N-o .III�IIo .2 {IIII1 _ —— ---12"CIP- IjI --U—V —Fl—LT—E—R ---12"CIP---- 4"CIP- PUMP t U AEROBIC I �I� IIIII I I CLARIFIER DIGESTER No.1 AERATION BASIN J Ijl SLUDGE �\ No.1 No.1 III DRYING BEDS i I .00 9c�� I // z I 9syl� i 41PvC N ��� oil �� 'po - I 'BPS\ LAB & BELT OI FILTER PRESS I BUILDING I A I z \- - - - - - - - - - - - - -__-----.--------- Ijl z .O IIIm III III �L12 UNFILTERED k BACKWASH LINE WATER FILTER WASHWATER r I I 1 I I I I - — -t JB 12"CIP TO� HOLDING BASIN Page: 1 of 2 Report Number: 14-028-0210 YY AFL Eastern Laboratories, Inc Account Number: 46381 ^� 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (904)271-6446 Submitted By: ZACH KEY J. www.aleastern.com Send To: SOUTHERN SOIL BUILDERS Project: BAXTER DENNIS KEY NC CERT#257 958 HOOTS ROAD ROARING RIVER, NC 28669 REPORT OF ANALYSIS Date Sampled: 1/22/2014 12:55:00 Lab Number: 97673 Date Received: 01/28/2014 00:00 Sample id,: BAXTER Date Reported: 02/03/2014 ' utaj �Ullull a•i5 Ufbuu 100.0 JM 01/28/2014 15:00 SM-2540G Moisture " 90.25 100.0 JM 01/28/2014 15:00 SM-2640G Total Kjeldahl Nitrogen 11.10 111000 10.0 JM 01/29/2014 09:29 SM-4500-NH3C-TKN Total Phosphorus 1.48 14800 100 KM 01/29/2014 13:31 SW 6010C Total Potassium 0.42, 4160 100 KM 01/29/2014 13:31 SW 6010C Total Sulfur 1.14 11400 100 KM 01/29/2014 13:31' SW 6010C Total Calcium 0.93 9280 100 KM 01/29/2014 13:31 SW 6010C Total Magnesium 0.40 4010 100 KM 01/29/2014 13:31 SW 6010C Total Sodium 0.48 4780 100 KM 01/29/2014 13:31 SW 6010C Total Iron 9150 100 KM 01/29/2014 13:31 SW 6010C Total Aluminum 1300 100, KM 01/29/2014 13:31 SW 6010C Total Manganese 119 5 KM 01/29/2014 13:31 SW 6010C Total Copper 118 5 KM 01/29/2014 13:31 SW 6010C Total Zinc 305 5 KM 01/29/2014 13:31 SW 6010C Ammonia Nitrogen 0.79 7900 10.0 JM 01/29/2024 00:00 SM-4500-NI3C Organic N 10.31 103100 10.0 01/29/2014 09:29 CALCULATION Nitrate+Nitrite-N 18.5 2.00 JM 01/29/2014 09:30 SM-450ONO3F Total Cadmium 2.0 2.0 KM 01/29/2014 13:31 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Drr repo is and letters are inr the exclusive ar rd coofidera!iat !,use of our cfierts, ancr may not be reproduced in v hofe or pat-. nor may atry reference be .made �� to the work, the results, or the company in any adverrising, news release, or other pubLc announcements wirhou: obtaininc our p, ier written a;lthor.'zatior.. Debbie Holt Page: 2 of 2 Report Number: 14-028-0210 DOD A&L EasternLaboratories, Inc. r7Account Number: 46381 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Submitted By: ZACH KEY www.aleastern.com Send To: SOUTHERN SOIL BUILDERS Project: BAXTER DENNIS KEY NC CERT#257 958 HOOTS ROAD ROARING RIVER, NC 28669 REPORT OF ANALYSIS Date Sampled: 1/22/2014 12:55:00 Lab Number: 97673 Date Received: 01/28/2014 00:00 Sample Id: BAXTER Date Reported: 02/03/2014 5 KM 01/29/2014 13:31 SW 6010C Total Nickel 25 5 KM 01/29/2014 13:31 SW 6010C Total Lead 12 5 KM 01/29/2014 13:31 SW 6010C Total Arsenic 8.0 3.0 KM 01/29/2014 13:31 SW 6010C Total Mercury 0.6 0.4 KM 01/29/2014 09:00 SW-7471B Total Selenium <5.0 5.0 KM 01/29/2014 13:31 SW 6010C pH (Standard Units) * 7.93 2.00 JM 01/29/2014 09:29 SW-9045D Total Molybdenum 5 5 KM 01/29/2014 13:31 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: IFIER: THE LRB WAS OU T OF LIMITS FOR "Mn". THE MAT RIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced ir, whole or part, nor -ray any r ereronce be rnade to the ,xrk. the results• or the company in any advertising, news release, or otherpublrc announcements without obtaining our prior written authorizatio,:. . Debbie Holt SAR Sodium Absorption Ratio Na: Sodium (Mg/L) Equivalent weight: 23 Ca: Calcium (Mg/L) Equivalent weight: 20 Mg : Magnesium (Mg/L) Equivalent weight: 12 Milli Equivalent = Mg/L / Equivalent weight Na(Mg/L� Ca M�j //LL M M /L 466.05 T 9-04.8 1 390.975 N_ a (ME) Ca (IVII� 1 45.2.4 �Ic� IV( 1F) 32,58125 20.26304 SAR= Na Milli Equivalent/[0.5 X (("a Milli Equivalent + Mg Milli equivalent)]0.5 power SAR = 3.248408 (Frorn Mg/L entered above) SAR= 3.247946 (From ME entered below) Na ME Ca ME Mc -(ME) 20.26 1 45.24 32.58 The amour amount of E Permitting I PAN Mineralization Rate TK�N:�NH�3�NO3 0.3 111000 7900 18.51;� PAN Surface Ikg 69.797 JbsIdry ton 1261; 0.22 Ibs total pLill 287.8389libs PAN/acre I PAN Injection 2 7.697 lbs! ry Lei. 14037.521!bs totalfA—Lll -320.4131FIbs —PAN/acre Dry Tons/1000 gal. 0.406575 1st year PAN lbs./acre Surface Ibs. Surface 12610.22399 287.8389407 I st year PAN Ibs./acre �njected Ibs. Injected 14037.51699I 32 0.418105-0-71 NO2 % Solids tons/year I ARplied on 0 0.0975 180.67 43.81 MR(TKN-NH3)+ +.5(NH3)+NO3+NO2 =mg/kg mg/kg x.002 =Ibs/dry ton MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg mg/kg x.002 =Ibs/dry ton 1000 X 8.34 X %solids X sp. gravity "=dry tons/1 000gal. 2000 1 4 Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 1/9/2014 Reported: 1/16/2014 For: Baxter Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst 14019-20.1 % Solids 1 1.31 % SM2540B-1997 1/10/14 CL 14019-20.1 Fecal Coliform MTF 1 8397 MPN/g SM92210E-2006 1/10/14 CL 14019-20.2 % Solids 2 1.31 % SM2540B-1997 1110114 CL 14019-20.2 Fecal Coliform MTF 2 129,771 MPN/g SM92210E-2006 1/10/14 CL 14019-20.3 % Solids 3 1.34 % SM254OB-1997 1/10/14 CL 14019-20.3 Fecal Coliform MTF 3 82,090 MPN/g SM92210E-2006 1/10/14 CL Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 P.O. Box 228 • Statesville, North Carolina 28687. 704/872/4697 Client: f .joJiVIP.`r.. 1J(``3e Address: �& STATESVELLE ANALYTICAL 122 CourtStreet - P.O. Box 228 Statesville, NC `8687 (704) 872-469:7 ' Contact Person`.` — Z e.t ! t Phone # 2 _ `i - FAX# a C$ ' Chain of" PO # Requisitioned by: (Time Date) Custody Record Customer Time Sampled Lab-ID #ly) Sample ID# (Grab On Date Sampled (Grab Only) n a 0 Matrix Sludge w Parameters requested for analysis ww Fec- jj 3t / g Relinquished by: � r,✓ ' / t Time •t �$ amjprn Date / / `� Sampled by:- znl / Received by: ibf <✓ �i , �, ' _�• Time , _ <; t,.° � am, 52 Date /� /� Transported by: Relinquished by: Time am, pm Date' / Holding times met: Received by: Time am, pm Date v Composite Sampling #1: Compliance work: Time begin am, pm Date / / Non-compliance work: Time end am, pm Date Composite Sampling #2• rLabComments: S,c", e 1' J3' , . ;� ,e,l e Time begin am, pm Date Time end am, pm Date / / Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 1/22/2014 Reported: 1/29/2014 For: Baxter Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst 140122-27.1 % Solids 1 1.26 % SM2540B-1997 1/22/14 CL 140122-27.1 Fecal Coliform MTF 1 174,603 MPN/g SM92210E-2006 1/22/14 CL 140122-27.2 % Solids 2 1.28 % SM2540B-1997 1/22/14 CL 140122-27.2 Fecal Coliform MTF 2 1,250,000 MPN/g SM92210E-2006 1/22/1.4 CL 140122-27.3 % Solids 3 1.25 % SM2540B-1997 1/22/14 CL 140122-27.3 Fecal Coliform MTF 3 1,280,000 MPN/g SM92210E-2006 1/22/14 CL 140122-27.4 % Solids 4 1.25 % SM2540B-1997 1/22/14 CL 140122-27.4 Fecal Coliform MTF 4 1,280,000 MPN/g SM92210E-2006 1/22/14 CL Respectfully submitted, Dena Myers NC Cert #440,W NCDCert #37755, EPA NCO0909 P.O. Box 228 • Statesville, North Carolina 28687 0 704/872/4697 Client: r a. a_) _. I A " (, , I- ` ( ., No log - STATESVILLE ANALYTICAL 122 Court Street - P.O.Box 228 Address: Statesville, NC 28687. (704) 872-4697 Contact Person: Phone # FAX# -3 �c, Chain of Custody Record PO# Requisitioned by: (Time Date) Customer Sample 1D# Lab -ID # Time Sampled (Grab Only) Date Sampled Only) o CL E a Matrix Parameters requested for analysis VM (Grab 0 0 O> C Relinquished Relinquished by: /7 A - Time 1�) am,rrl Date 1 Sampled by: Received by: Time —2) am,/pm Date 72ZI f Transported by: Relinquished by: Time am, pm Date Holding times met: Received by: Time am, pm Date Compliance work: Composite Sampling #11: Time begin— am, pm Date Non-compliance work: Time end am, pm Date Lab Comments: Composite Sampling #2: bc 01 Time begin— am, pm Date Time end am, pm Date a � , Condition of Receipt Sample ID 140122-27.1-27.4 Client Southern Soil Builders Temp on Arrival 1 pH upon Arrival Parameter Schedule Fecal Coliform WW ❑ HNO3 ❑ HCl ❑ NaOH ❑ H2SO 0 Na2S2O ❑ Dechlorinated ❑ Chemicals in containers, client ❑ Chemicals upon receipt ❑�/ Received on Ice ❑ Samples chilled upon receipt �/❑ Chemicals in containers, lab Page 1 of 1 y Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 1/22/2014 Reported: 1/31/2014 For: Baxter Sample ID Parameter' Cust ID Result Units Method Date Analyzed Analyst 140122-25.1 140122-25.1 140122-25.2 140122-25.2 % Total Solids % Volatile Solids % Total Solids % Volatile Solids in In Out Out 1.23 1.04 0.57 0.38 % % % % SM2540B-1997 SM2540G SM2540B-1997 SM2540G 1/22/14 CL 1/23/14 CL 1/22/14 CL 1/23/14 CL Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 P.O. Box 228 • Statesville, North Carolina 28687 e 704/872/4697 Client: rr t • q }n Address: f STATESVILLE ANALYTICAL I ! 5 fu 4 `� 5 d` r 122 Court Street • P.O- Box 228 Q Statesville, NC 28687 (704) 8724697 Contact Person:` ` Phone # FAX# 33- �. � 1) y Ct Chain of PO # C/ Requisitioned by: (Time Date) Custody Record Customer Lab -ID # Time Sampled Date Sampled a Matrix Sample ID# (Grab Only) (Grab Only) sioaye w vnv Parameters requested for analysis � .�a Y"1 �- (� J lc t i � � , i i . ' ;?`� d� 1 " fi �'• i `4 J�! L fi Relinquished by: '�•� 'f Time �( am 1 / �!/%`, � ' t� � Date p� � Sampled by: �r, �a..t/ Received by: p ' 1 t Time l ] a pm ,, Date /= Transported by: .- Relinquished by: Time am, pm Date / / /f i�Holding times met: Received by: Time am, pm Date / / Compliance work: Composite Sampling #1: Time begin am, pm Date / / Non-compliance work: Time end am, pm Date / / Lab Comments: Composite Sampling#2•i�•� P),,,y' rLied jc` Time begin am, pm Date __L F P Time end am, pm Date / / Condition of Receipt Sample ID 140122-25.1-25.2 Client Southern Soil Builders Temp on Arrival pH upon Arrival Parameter Schedule % Volatile Solids HNO3 ❑ Chemicals in containers, client HCI ❑ Chemicals upon receipt NaOH ❑Q Received on Ice H2SO ❑ Samples chilled upon receipt Na2S2O ❑ Chemicals in containers, lab Dechlorinated Page 1 of 1 VS in 0.0104 VS out 0.0038 VSFR= 0.637036 VSFR=(IN-OUT)/(IN-(IN'OUT)) i k t, Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 1/9/2014 Reported: 1 /28/2014 For: Baxter TCLP Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst 14019-18 14019-18 14019-18 14019-18 Corrosivity Ignitability Reactivity TCLP Baxter Baxter Baxter Baxter See Attached See Attached See Attached See Attached SW-846 1010M SW-846 1311 1/2.3/14 PACE 1/23/14 PACE 1/2.3/14 PACE 1/23/14 PACE Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 P.O. Box 228 0 Statesville, North Carolina 28687 9 7091872/4697 j� ;1 -, 0 aceAnalytical www.pacelabs.com Project: 14019-18 Pace Project No.: 92186027 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc, 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 00111plu; "14ulu-7tf Lab ID: 92186027001 Collected: 01/09/14 13:30 Received: 01/10/14 14:55 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Re ort Limit DF P 8081 GCS Pesticides, TCLP gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) p repared Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 Analyzed CAS No. Qual ND tag/L 0.50 1 01/21/14 10:40 01/23/14 14:55 58-89-9 ND ug/L 3.0 1 01/21/14 10:40 01/23/14 14:55 57-74-9 ND ug/L 0.50 1 01/21/14 10:40 01/23/14 14:55 72-20-8 ND ug/L 0.50 1 01/21/14 10:40 01/23/14 14:55 1024.57-3 ND ug/L 1000 1 01121/1410:40 01/23/14 14:55 72-43-5 ND ug/L 3.0 1 01/21/14 10:40 01/23/14 14:55 8001-35-2 68 % 10-138 1 01/21/14 10:40 01/23/14 14:55 2051-24-3 59 % 10-110 1 01/21/14 10:40 01/23/14 14:55 877-09-8 8151 Chlorinate Herbicide TCLP Analytical Method: EPA 8151 Preparation Method: EPA 3510 2,4-D 2,4,5-TP (Silvex) ND mg/L 0.010 1 01/16/14 08:00 01/18/14 21:00 94-75-7 Surrogates ND rng/L 0.010 1 01/16/14 08:00 01/18/14 21:00 93-72-1 2,4-DCAA (S) 94 % 70-130 1 01/16/14 08:00 01/18/14 21:00 19719-28-9 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Method/Date: EPA 1311; 01/13/14 10:49 Arsenic Barium ND mg/L 0.050 1 01/14/14 11:10 01/14/14 23:13 7440-38-2 Cadmium 0.74 mg/L 0.25 1 01/14/14 11:10 01/14/14 23:13 7440-39-3 Chromium ND mg/L 0.0050 1 01/14/14 11:10 01/14/14 23:13 7440-43-9 Lead ND mg/L 0.025 1 01/14/14 11:10 01/14/14 23:13 7440-47-3 Selenium ND mg/L 0.025 1 01/14/14 11:10 01/14/14 23:13 7439-92-1 Silver ND mg/L 0.10 1 01/14/14 11:10 01/14/14 23:13 7782-49-2 ND mg/L 0.025 1 01/14/14 11:10 01/14/14 23:13 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 01/13/14 10:49 Mercury ND ug/L 0.20 1 01/14/14 11:45 01/15/14 16:02 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 1,4-Dichlorobenzene 2,4-Dinitrotoluene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 106-46-7 Hexachloro-1,3-butadiene ND ug/L 50.0 1 ND ug/L 01/21/14 09:40 01/22/14 16:04 121-14-2 Hexachlorobenzene 50.0 1 ND ug/L 01/21/14 09:40 01/22/14 16:04 87-68-3 Hexachloroethane 50.0 1 ND ug/L 01/21/14 09:40 01/22/14 16:04 118-74-1 2-Methylphenol(o-Cresol) 50.0 1 ND ug/L 01/21/14 09:40 01/22/14 16:04 67-72-1 3&4-Methylphenol(m&p Cresol) 50.0 1 313 ug/L 01/21/14 09:40 01/22/14 16:04 95-48-7 Nitrobenzene 50.0 1 ND ug/L 01/21/14 09:40 01/22/14 16:04 Pentachlorophenol 50.0 1 ND ug/L 01/21/14 09:40 01/22/14 16:04 98-95-3 Pyridine 100 1 01/21/14 09:40 01/22/14 16:04 87-86-5 2,4,5-Trichlorophenol ND ug/L 50.0 1 ND ug/L 01/21/14 09:40 01/22/14 16:04 110-86-1 50.0 1 01/21/14 09:40 01/22/14 16:04 95-95-4 REPORT OF LABORATORY ANALYSIS 'This report shall not be reproduced, except in full, Date: 01/28/2014 11:40 AM without the written consent of Pace Analytical Services, Inc,. Page 4 of 21 acmnalytical www.pacelabs.com Project: 14019-18 Pace Project No.: 92186027 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 sample: 14019-18 Lab ID: 92186027001 Collected: 01/09/14 13:30 Received: 01/10/14 14:55 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Pre ared 8270 MSSV TCLP Sep Funnel 2,4,6-Trichlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) 1010 Flash point, Closed Cup Flashpoint 734S Reactive Sulfide Sulfide, Reactive 9046 pH Soil pH at 25 Degrees C 733C Reactive Cyanide Cyanide, Reactive Date: 01/28/2014 11:40 AM _ p Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 Analyzed CAS No. Qual ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 88-06-2 56 % 12-102 1 01/21/14 09:40 01/22/14 16:04 4165-60-0 56 % 13-107 1 01/21/14 09:40 01/22/14 16:04 321-60-8 69 % 21-132 1 01/21/14 09:40 01/22/14 16:04 1718-51-0 35 % 10-110 1 01/21/14 09:40 01/22/14 16:04 13127-88-3 41 %u 10-110 1 01/21/14 09:40 01/22/14 16:04 367-12-4 77 % 27-108 1 01/21/14 09:40 01/22/14 16:04 118-79-6 Analytical Method: EPA 8260 ND ug/L 5.0 1 01/15/14 13:08 71-43-2 52.6 ug/L 10.0 1 01/15/14 13:08 78-93-3 ND ug/L 5.0 1 01/15/14 13:08 56-23-5 ND ug/L 5.0 1 01/15/14 13:08 108-90-7 ND ug/L 5.0 1 01/15/14 13:08 67-66-3 ND ug/L 5.0 1 01/1511413:08 106-46-7 ND u9/L 5.0 1 01/15/14 13:08 107-06-2 ND ug/L 5.0 1 01/15/14 13:08 75-35-4 ND ug/L 5.0 1 01/15/14 13:08 127-18-4 ND ug/L 5.0 1 01/15/14 13:08 79-01-6 ND ug/L 5.0 1 01/15/14 13:08 75-01-4 109 % 70-130 1 01/15/14 13:08 17060-07-0 98 % 67-135 1 01/15/14 13:08 2037-26-5 98 % 70-130 1 01/15/14 13:08 460-00-4 Analytical Method: EPA 1010 >200 deg F 70.0 1 01/13/14 00:00 Analytical Method: SW-846 7.3.4.2 Modified ND mg/L 10.0 1 01115/1414:00 Analytical Method: EPA 9045 6.9 Std, Units 0.10 1 01/21/14 15:45 Analytical Method: SW-846 7.3.3.2 Modified ND mg/L 0.0050 1 01/15/1412:45 REPORT OF LABORATORY ANALYSIS 'This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 21 Client: z t Address: y 959 Contact Person. p t Phone # PO # Requisitioned by: Customer Sam a ID# Lab -ID # Time Sampled Date Sampled p (Grab Only) (Grab Only) M STATESVILLE ANALYTICAL w 122 Court Street • P.O. Box 228 Q Statesville, NC 28687 (704) 8724697 FAX#�) �� `� Chain of (Time Date) Custody Record Matrix Parameters requested for analysis udge W WW CL C e . .4 �.. Relinquished by: 1, -� Time �•l - � am, 6��iD ate Received by: Time am, pate L /_// Relinquished by: Time am, pm Date Received by: Composite Sampling #1 Time begin am, pm Date Time end am, pm Date _Composite Sampling #2- Time begin am, pm Date Time end am, pm Date Time am, pm Date Sampled by: Transported by: 7 r �r Holding times met: Compliance work: Non-compliance work: Lab Comments:. i �. :_ A C." P I C s I r-t ci �j .` i, C x . ANN UAL FATIIMJL N AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Baxter Healthcare WQ Permit Number: WQ0031725 WWTP Name: Baxter Healthcare NPOES Number: NQ0006564 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ® I Alt B (Alk Treatment) ® Alt. C (Prior Testing) El A1t.D (No Prior Test) ® I Process to Further Reduce Pathogengs D If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ® Heat Drying ® Heat Treatment ® Thermophilic Beta Ray ® Gal Ray ® Pasteurization Class B: JAIt. (1) Fecal Density 5d Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying ® Composting ® Aerobic Digestion E3 naer i A ob c Digestion ElIf applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number ot Excee- e Frequency of Analysis Y Sample Type Analytical Tech - ue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 8397 225,349 1280000 MPN/g 0 7 grab sm9221c CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) 52r Alt. 2 (40-day bench) ® Alt. 3 (30-day bench) ® Alt. 4 (Spec. Oz uptake) Alt. 5 (14-Day Aerobic) ® Alt. 6 (Alk. Stabilization ® Alt 7 (Drying - Stable) ® I Alt. 8 (Drying - Unstable) [� Alt. 9 (Injection) ® Alt. 10 (Incorporation) ® No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT (please check the appropriate statement) E' "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Dennis Key Southern Soil Builders, Inc. P Er Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) OSignature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.neagr.gov/agronomi/ r Predictive Soil Report Mehlich-3 Extraction Client: Southern Soil Builders, Inc. 958 Hoots Rd Roaring River, NC 28669 Sampled County: Wilkes Sampled: Received: 09/30/2014 Completed: 10/08/2014 Farm: Sample ID: DP1A Recommendations: Lime Crop (tons/acre) N P2O5 K2O Lime History: 1 - Fescue/OGrass/Tim, 1 0.0 120-200 0 0 2- Test Results [units - WN in g/cnr3• CEC and Na in me /100 crrr3 NO N ' lrr3 Advisor: Links to Helpful Information Nutrients (lb/acre) More Mg S Mn Zn 77 7CUB Information 0 0 0 0 0 0 Note: 12 q s- in mg/d ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I 0.41 0.93 12.9 Sample ID: DP113 86 1.8 6.1 231 185 Recommendations: 55 24 36 ill 82 435 435 932 Lime Nutrients (lb/acre) Lime History: Crop (tons/acre) 1- Fescue/OGrass/Tim, 1 0.0 N P2O5 120-200 K2O Mg S Mn Zn Cu 2- 0 10 0 0 0 0 0 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/drr?]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn All Mn-AI2 Zn-I Zn-AI Cu-1 0.46 0.86 12.2 Sample ID. DP1C 88 1.4 6.1 150 72 Recommendations: 62 23 43 65 54 539 539 659 Lime Nutrients (lb/acre) Lime History: Crop (tons/acre) 1- Fescue/OGrass/Tim, 1 0.5 N P2O5 K2O Mg S Mn Zn Cu 120-200 0 10 0 0 0 0 0 2- Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cn73; NO3-N in mg/dnr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 0.51 0.92 11.7 83 2.0 5.8 202 75 60 20 45 131 96 am an7 4 nn� Na ESP SS i NOs-„I 0.1 1 More B Information 0 Note: 12 Na ESP SS-1 NO3-N 0.1 1 More B Information 0 Note: 12 Na ESP SS-1 NO3-N .North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Steve Troxler, Commissioner of Agriculture NuuA&GS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL007224 } Page 2 of 4 e Sample ID: DP1D Recommendations: Lime Crop (tons/acre) N P20s Nutrients (lb/acre) More K20 M S Lime History: 1 -Fescue/OGrass/Tim, I 0.9 120-200 0 0 g Mn Zn Cu B Information 2- 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cm3; CEC and Na in meq/100 CO; NO3-N in mg/drrP]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na 90 11.4 81 2.2 5.6 208 116 56 20 49 0.60 07Results 95 ESP SS-1 NO3-N SampleDP2 Recommendations: Lime 74 697 697 785 0.1 1 Crop (tons/acre) N P205 Nutrients (lb/acre) More K20 M S 1 -Corn, silage 9 1.3 180-220 0 80 g Mn Zn Cu B Information 2- 0 0 0 0 0 0 Note:3 [units - WN in g/cm3; CEC and Na in meg1100 cm3; NO3_N i.^..^ry/d.^]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP 0.36 0.96 8.8 72 2.5 5.3 190 59 48 20 60 67 57 SS-1 NO3-N Sample ID: DP3C Recommendations: Lime 666 666 745 0.1 1 Crop (tons/acre) N P205 Nutrients (lb/acre) More K20 M S Lime History: 1 -Corn, sila e 9 0.8 180-220 0 100 g Mn Zn Cu B Information _ 2- 0 0 0 0 0 0 Note:3 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drrP]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na 0.13 0.87 9.3 79 1.9 5.6 91 50 46 31 142 61 ESP SS-1 NO3-N Sample ID: DP3G Recommendations: Lime 54 419 419 378 0.1 1 Crop (tons/acre) N P205 Nutrients (lb/acre) e K20 Mg S Lime History: 1-Fescue/OGrass/Tim, 1 1.4 120-200 0 10 Mn Zn 2- 0 00 02 =BInformation Test Results [units - WN in 9/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na 0.32 0.85 9.2 73 2.4 5.1 95 70 45 24 87 79 ESP SS-1 NO3-N 64 510 510 351 0.1 1 Nt;UA&L;S Agronomic Division Phone: (919' epsite: www.ncagr.gov/agrpnomi/ Report No. FY15-SL007224 Page 3 of 4 + Sample ID: DP4 Recommendations: Lime Crop (tons/acre) Nutrients (lb/acre) More N P2O5 K2O Mg S Mn Zn Lime History: 1- Fescue/OGrass/Tim, 1 0.6 120-200 0 50 0 Cu B Information 2- 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dnr ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 0.91 11.6 81 2.2 5.8 93 44 DP5 Recommendations: Lime 53 26 45 87 69 686 686 637 0.1 1 FSaleD: Crop (tons/acre) Nutrients (Ib/acre) More N P2O6 K2O Mg S Mn tory: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 0 Zn 0 Cu B Information 2- 0 0 0 0 0 Note: 12 Test Results [units - W/V in glca; CEC and Na in mea/100 cm3; NO3-N in mg!rin. '- Soil Class iviineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 0.86 11.8 88 1.4 6.2 95 113 Sample ID: DP6 55 28 49 83 65 805 805 532 0.1 1 Recommendations: Lime Nutrients (lb/acre) Lime History: Crop (tons/acre) 1 - Fescue/OGrass/Tim, 1 0.6 N P2O5 120-200 40 K2O Mg S Mn Zn Cu B More Information 2- 50 0 0 0 0 0 0 Note: 12 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 0.95 7.5 77 1.7 5.7 41 47 Sample ID: DP7 54 20 32 75 62 188 188 94 0.1 1 Recommendations: Lime Nutrients (Ib/acre) Lime History: Crop (tons/acre) 1-Fescue/OGrass/Tim, 1 1.4 N P2O5 120-200 K2O Mg S Mn Zn Cu B More Information 2- 0 10 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 -Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 0.94 7.4 68 2.4 5.1 99 77 - 47 16 39 77 63 305 305 573 0.1 1 NL;uA&GS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ 4 Report No. FY15-SL007224 t the Soil Report: explanation of measurements, abbreviations and units Page 4 of 4 IF,Understanding Recommendations Report Abbreviations Lime If testingfinds that soil H is too low for the crop(s) s indicated, a lime recommendation will be given in units p P() g gc exchangeable acidity of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For BS% boron % CEC no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% occupied by basic cations /a CEC one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is occupied by calcium cation nge capacity needed, use dolomitric lime. Cu-I copper Fertilizer ESP exchangeable sodium percent Recommendations for field crops or other large areas are listed separately for each nutrient to be added in units of ( KM% percent h matter lb/acre unless otherwise specified). Recommendations for ni'14 +:.,. es for , ^_ based potassium index index for the cropon g ro beine p g grown not on soil test results. K-1 and P-1 values are basedoniest're results and should bet>50. Iftheyg% follow y M Potash /o CEC occupied by magnesium are not, the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb acre alone in MIN mineral soil class per or a fertilizer blend will usually satisfy crop needs, SS -I levels appear only on reports for greenhouse soil or problem samples. Mn Mn-All manganese Mn-availability index for crop 1 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-AI2 Mn-I Mn-availability index for crop 2 manganese index notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not need to be concerned about micronutrients. Various M-0 N mineral -organic soil class crop notes also address lime fertilizer needs; visit nitrogen ncagr.gov/agronomi/pubs.htm. Na sodium NO3-N nitrate nitrogen Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot 0H G organic soil class find the exact fertilizer grade recommended on the report, visit P P current soil pH wFvw.ncaQr.aov/aaronomi/oboart4 htm s to find information that may help you choose a comparable alternate. For more information, readA Homeowner's P-1 P205 phosphorus index o Guide to Ferti/iz r phosphate Test Results S-1 sulfur index SS -I soluble salt index The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pHj describe the soil and its degree of acidity. The WN Zn AI weight per volume zinc availability index remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels Zn-I zinc index of plant nutrients or other fertility measurement. Visit :Nvnrv.ncaar gov/agronomi/uyrst htm for more information.