WQ0030998_Residual Annual Report 2014_20150219

v86
RANCH RESIDUALS
&SoiLs, LLC' 46 W. Market St., —,Suite 111 • Greensboro, NC 27409
PHONE [phone], • Fax [phone]
February 1,4, 2015
North Carolina Department of Environment and Natural Resources .
Aquifer Protection Section
1617 Mail Service Center
Raleigh,: North Carolina 276994617,
Reference: 2014 LAND. APPLICATION ANNUAL REPORT
Triple S Farms & Cleaning, Inc.
'Permit No.' WQ0030998
Branch Residuals, & Soils' Proj ect No. 2007-7.0
Information Processing Unit: .
Branch Residuals' &. Soils is submitting all monitoring, and reporting information as required in the referenced,
permit on behalf of the Triple S Farms & Cleaning, Inc. This data includes: ' 1) Certification -Forms and Facility
Information; 2) Annual Residual Sampling Summary.Forms, 3).'Annual Meials..Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis. Lab Sheets, 6).TCLP Lab Sheets, 7) :.
Pathogen &: Vector Attraction Forms, 8) -Pathogen: and Vector Attraction Reduction Documentation; 9). $oils
Lab Data .10) 2014 Application.SummaryTable, and 1,1).2014 Application Condition.Summaries.
r A total of'2,373.,000:gallons (230.5 dry'tons) of Class B lime-stabilizedbiosolids or class B fecal, and injected
biosolids were land applied to 73.27;acres.in 2014. This material was:divided as follows:
• 159,000 gallons (4,71 dry tons). from Beulaville WWTP,
132000
g (
• allons 9.58 dry tons) .from Kenansville WWTP,
•. . 126;000 .gallons-(8.3 ,dry tons) from Rose Hill WWTP ,
• 267,000 gallons (15.7 dry tons) from Warsaw WWTP,
�.. 15,000 gallons ( 1,01 dry:4ons) from Southwest'Plantation WWTP, and'.
1.674,000 gallons (191.21 dry tons): from Wallace WWTP. .
If any further. information is required regarding this land application program, please 'do not Hesitate to contact
me at.(3M) 510-0340.
''Sincerely,
Robert :T.'Branch; L.S:S.
_Land, Application/Residuals Operator "
#15676
RTB
Enclosures
cc: Town of Beulaville
Town of Kenansville
Town of Rose' Hill
Town of Warsaw
Southwest Plantation
Town of Wallace

TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Forms and Facility Information
II Annual Residual Sampling Summary Forms
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Forms
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Reports
X 2014 Application Summary Table
XI 2014 Application Condition Summaries

CERTIFICATION FORMS AND FACILITY INFORMATION

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0030998 County: Duplin Year: 2014
Facility Name (as shown on permit): Triple S Farms & Cleaning
Land Application Operator: Triple S Farms & Cleaning Phone: [phone]
_ Land application of residuals as allowed by the permit occurred during the past calendar year?
B Yes [] No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Annlication Summa :
Total number of application fields in thepermit:
7
Total number of fields utilized for land application during the year:
5
Total amount of dry tons applied during the year for all application sites:
230.5
Total number of acres utilizes for land application during the year:,F
73.27
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. a Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
i
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Mr. Eric R. Smith, Owner
Permittee Name and Title (type or print) Signature of P ttee Date
` See Attached
Signature of Preparer* Date Slinature of'Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF EEULAVILLE
Part B - Annual Conmiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes E] No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for- knowing violations."
Signature of Prer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

_a
ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF KENANSVILLE
Part B - Annual Comuiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. EJ Yes D No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the pen -nit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and 'imprisonment for knowing violations."
Signature Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

f 4
ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF ROSE RILL
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. E] Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
i1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the pemut and reported during the year as required and three
(3) copies of certified laboratory results are attached.
y 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of nay knowledge and belief, true, accurate,
R and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imlgisonment for knowing violations."
(�A -15
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND FORM
SOUTHWEST PLANTAT [ON
Facility was; cootpRiaof du ri rtg pidendar your 2014 with till couditinnN of Me fund mplilkatiori poro0l
(birluding !)M nut limite-J. tij Items 1-13 bAetv) INSUC4 by tht Divitiou of wiltov Quality. 13 No
INIG Okwv, oravittu a wViOvyl On frielfity wag not etntmplhittt, ibt- dal m. mod. explidep eortwtive�
u,041� (RIC011.
1) Qnly ivnidual--up ,urpv(,-d far this pemift., wem �ppl iod tre dim jvr,-njgc4 �--w6.
2) Soil p1l km adjusted as; q=ifti:4 in c�xpzarftsnd 14a;A4- n&-de�, to w;biCM-,Fa --oil pH of al least G-OCT
p
3? Annual soil& M-naYsis"Were PCIfoh1wd Ott gnh during the pest catordInT year and three (j) ck-, c�
nflHboiwoty tv�­.dft w-e atta0h.ed.
4) AMM11111VILP qAMAIYtf% (Ifroqvlmi) vva-� PCm-fortimt flail throe (1) u� pi(;N okenflIkA WRIff'-wtv I-C,51I1 N lwl 1111110%.d,
55) A11 t0or nion kodRp, -%,v.Hx pkirllbl vlej ill, IM-Alvwux� with they per "(4, -wid riqwlud (ttv4;tA Eh4e yctr tip roqu MI and, daec�
(N) copios otuevifwd lohov#14vy roquift MM a0mchad.
(P) 'rhe ffieflity euti PuA c_xMkX'I Aby 6flIC P0Il(19dDt.Ckhn1AmtIzkacn LL-Afts in. J..5A XCAC 02T , I I 05(a) or (it* Palbanit
Uodii-,g Ratus in I 5�-Ik ik.A(0*2T J IWLb) (,V 'llop le tit rsrt 503 tijitla, -d facifitim)-
7) AD Vefie-,Ui Ttq6TCZERMts I'll 0,,vsp=ifiod, in tho wcee confglitxf kv.-fh(appticablo tc; ML (Fl� k
5 3 r;.qUliRECd r-26'46CO;
. 1
8) All muititafSnR ani rc,,vrl htg vcqp i reaicnis iti I 5A N CAC 02,C I I I I wm° winplica %ith, (;&ppjjC.jhl C ter 440 CUR TI,-0
50.1 ruplatod kcififits).
All rmdolcntaloc roclWec", 41s 00bopprillit wittior, in thecaworu 4401111D.I. Ono.
10.) No coMnivc-rition of ieound Witter Qwqlfty I,'vtAjidae(k ndctjrtvd at 4, nknToting wult or -t:xpl=tlow% of viclatiorts arc
tiffitchW in include =d -tartudiadlons.
I I )NIcpailivc ccwax wag maimsined an.d pn3parxwp inxanngr=%. wn PC:; for ocd on: C04-Oh �Ac =.ting.r*Ad.U:315JL as,
sp'buified in tlaz pmill,
12) No tuixiff of rcr&ivafiq fmm- tile Applica6an 1iC6 ftnl:6 Adja=iit pn4p=ty or r.nifts'LiTface. watcn:q NO-o"irmit,
III) All 1y6ffe tcq-uj.rcMcat4 as 6pWMtod, are tho perinit worts rtu:)iqlainod durinf+ cuoll milplizatton of rofildulil.
".11 uvrtifyo uo.drr penalty -A of htw0161: (W aboVo IK, to the hn't of Imy knowleftc and Itellef, trOvi uevarxae.
and e=P104w rsttl swarif (half therid Egre YWItIcxAtpCnkIE0r% fdr*uhtifl(IN&# fidge InforcruMonjactudIng the
pofiSibillty of fines and in' pwimn n nient f , (hr L-1kowing vlvhifir�a&`
.7
Promycr is t1r.rMLd i'll Aro C'Vit ['all 541,M) (i) tood 15A NICAC 011 (26)
I

ANNUAL LAND APPLICATION CERTIFICATION FORM
- TOWN OF WALLACE
Part B - Annual Compiance Statement:-
`_1 Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
L action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on -the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and 'imprisonment for knowing violations."
<-T \
of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WARSAW
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. EJ Yes [] No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, trine, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORMS

i
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or
NC0026018
NPDES #:
WNVTP Name: Town of Beulaville WWTP
Residual Analvsis Data
Laboratory:
1)
2)
3)
4)
5)
Environmental Chemists
Parameter
(mg/kg)
Ceiling
Cone.
Limit
Sample or Composite Date
6/16/2014
Percent Solids (%)
NA
0.71
Arsenic
75
<13.90
Cadmium
85
<13.90
Copper
4,300
1050.00
Chromium
NA
40.70
Lead
840
63.20
Mercury
57
3.80
Molybdenum
75
14.80
Nickel
420
37.00
Selenium
100
<13.90
Zinc
7,500
1620.00
Total Phosphorus
NA
38,100
TKN
NA
75,200
Ammonia -Nitrogen
NA
493
Nitrate and Nitrite
NA
12,100
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, includineAhe possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL. RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or NCO036668
NPDES #:
WWTP Name: Town of Kenansville WWTP
Raeirhial Analveic data
Laboratory:
1)
2)
3)
4)
5)
Environmental Chemists
Parameter '
(mg&g)
Ceiling
Cone.
Limit
Sample or Composite Date
3/5/2014
Percent Solids (%)
NA
1.74
Arsenic
75
<5.46
Cadmium
85
<5.46
Copper
4,300
273.00
Chromium
NA
12.20
Lead
840
16.60
Mercury
57
0.63
Molybdenum
75
13.00
Nickel
420
11.10
Selenium
100
<5.46
Zinc
7,500
561.00
Total Phosphorus
NA
1,140
TKN
NA
17,900
Ammonia -Nitrogen
NA
169
Nitrate and Nitrite
NA
J 2,480
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
� , Lj: r� 1-911-15
Signature ' f Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or NCO056863
NPDES #:
WWTP Name: Town of Rose Hill WWTP
Residual Analvsis Data
Laboratory: 1) Environmental Chemists
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite
Date
12/3/2014
Percent Solids (%)
NA
1.58
Arsenic
75
<6.33
Cadmium
85
<6.33
Copper
4,300
627.00
Chromium
NA
33.10
Lead
840
24.90
Mercury
57
6.96
Molybdenum
75
<6.33
Nickel
420
18.10
Selenium
100
11.00
Zinc
7,500
1040.00
Total Phosphorus
NA
23,500
TKN
NA
61,700
Ammonia -Nitrogen
NA
1,040
Nitrate and Nitrite
NA
180
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualifi d perso el properly gathered and evaluated the information submitted. I am aware that there are significant
penalties submi mg false ! formation, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

AININ UIALL RFSU)UA.L SAINIFLINGSU MAAARY FOUI
Flo natc.thai'mar permik mmy conwim addiliooal p4Lr=cfc-k-s Zo beandymzdL Tbe bra ctm cr&n bc ruportcd, in FUMNI RSSF - R
WIQ Laboralaryi T;,�Ivimnmcaw Chemists
F:acft.y Nzm; Trip-'c S Fps
Sq"m wq 41 or
XFOES 4..
Vr'%VT.F,N-amc.1—
Rmirrlu al i"alv�is D, alm
Pmr4nencr
DrIC
pIcr4cnt SIDI
NA
Anctdc
SS
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D5NH M RASP (i 2JZC06)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998 Laboratory: 1) Environmental Chemists, Inc.
Facility Name: Triple S Farms & Cleaning 2)
Residual Source WQ # or 3)
NPDES #: NC0020702 4
WWTP Name: Town of Wallace WWTP 5)
Residual Analvsis Data
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite
Date
1/20/2014
5/9/2014
7/21/2014
10/23/2014
Percent Solids (%)
NA
2.60
2.56
2.80
2.87
Arsenic
75
<3.73
<3.20
<3.50
<3.14
Cadmium
85
<3.73
<3.20
<3.50
<3.14
Copper
4,300
662.00
691.00
804.00
749.00
Chromium
NA
19.20
18.40
18.20
21.30
Lead
840
57.70
48.40
52.10
62.00
Mercury
57
1.17
0.79
0.72
0.95
Molybdenum
75
<3.73
<3.20
5.32
5.75
Nickel
420
14.70
14.30
15.60
17.50
Selenium
100
<3.73
4.38
6.18
9.76
Zinc
7,500
1250.00
1640.00
1710.00
1540.00
Total Phosphorus
NA
4,150
19,600
4,190
19,900
TKN
NA
51,300
39,600
39,900
40,600
Ammonia -Nitrogen
. NA
52
3,920
1,710
617
Nitrate and Nitrite
NA
79
209
104
24
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
pe lties for sub false information, including the possibility of fines and imprisonment for knowing violations."
2 -Z-15
Signature of Preparer *
*Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998 Laboratory: 1) Environmental Chemists
Facility Name: Triple S Farms & Cleaning 2)
Residual Source WQ # or NC0021903 3)
NPDES #: 4)
WWTP Name: Town of Warsaw WWTP 5)
Residual Analvsis Data
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
6/16/2014
Percent Solids (%)
NA
1.41
Arsenic
75
<6.17
Cadmium
85
<6.17
Copper
4,300
636.00
Chromium
NA
34.00
Lead
840
54.10
Mercury
57
1.49
Molybdenum
75
<6.17
Nickel
420
26.50
Selenium
100
<6.17
zinc
7,500
1380.00
Total Phosphorus
NA
55,300
TKN
NA
72,400
Ammonia -Nitrogen
NA
987
Nitrate and Nitrite
NA
36
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
pen lties for ,,sujAmitting false information, including the possibility of fines and imprisonment for knowing violations."
3ignat-6re of Pieparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORMS

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 123.07
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series NoA
Acres Used: 29.5 Acres Permitted: 29.5 Site #: 1 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
I I1 11 IA I I III AnniA 1 117D nAlA
Sample
or Com-
posite
Date
1/20/14
5/9/14
7/21/14
7/21/14
6/16/14
% Solids
1 2.60
2.56
2.80
1 2.80
1.41
Arsenic
3.73
3.20
3.50
3.50
6.17
Cadmium
3.73
3.20
3.50
3.50
6.17
Chromium
19.20
18.40
18.20
18.20
34.00
Copper
662.00
691.00
804.00
804.001
636.00
Lead
57.70
48.40
52.10
52.10
54.10
Mercury
1.17
0.79
0.72
0.72
1.49
Molyb-
denum
3.73
3.20
5.32
5.32
6.17
Nickel
14.70
14.30
15.60
15.60
26.50
Selenium
3.73
4.38
6.18
6.18
6.17
Zinc
1250.001
1640.00
1710.00
1710.001380.00
Total
Phos-
horus
4,150
19,600
4,190
4,190
55,300
Anneal TAeaw Metal Field T.nadinus iCArnlated in lhs/acrel:
0
` b d
1.01
0.35
1.31
1.23
0.27
o'
a
Arsenic
0.01
0.00
0.01
0.01
0.00
0.03
Cadmium
0.01
0.00
0.01
0.01
0.00
0.03
Chromiury
0.04
0.01
0.05
0.04
0.02
0.16
Copper
1.34
0.48
2.10
1.99
0.34
6.25
Lead
0.12
0.03
0.14
0.13
0.03
0.44
Mercury
0.00
0.00
0.00
0.00
0.00
0.01
Molyb-
0.01
0.00
0.01
0.01
0.00
0.04
denum
Nickel
0.03
0.01
0.04
0.04
0.01
0.13
Selenium
0.01
0.00
0.02
0.02
0.00
0.05
Zinc
2.54
1.14
4.47
4.22
0.74
13.11
Total
Phos-
8.42
13.62
10.95
10.35
29.76
73.09
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the ossibili f fines and imprisonment for knowing violations"
- - its-
Signature of Land Applier Date
8iifhnr nnr17i n Marriff nFNR FORM MFI RF (7/gnoq)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 23.53
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 8.48 Acres Permitted: 8.48 Site #: 1 Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
n OMd V 9lNd 119MA WR 9Md PM JR1d WA901dd-
Samp e
or Com-
posite
Date
6/16/14
3/5/14
6/16/14
6/16/14
12/3/14
10/23/14
% Solids
0.71
1.74
0.71
1.41
1.58
2.87
Arsenic
13.90
5.46
13.90
6.17
6.33
3.14
Cadmium
13.90
5.46
13.90
6.17
6.33
3.14
'Chromium
40.70
12.20
40.70
34.00
33.10
21.30
Copper
1050.00
273.00
1050.00
636.00
627.00
749.00
Lead
63.20
16.60
63.20
54.10
24.90
62.00
Mercury
3.80
0.63
3.80
1.49
6.96
0.95
Molyb-
denum
14.80
13.00
14.80
6.17
6.33
5.75
Nickel
37.00
11.10
37.00
26.50
18.10
17.50
Selenium
13.90
5.46
13.90
6.17
11.00
9.76
Zinc
1620.00
561.00
1620.00
1380.00
1040.00
1540.00
Total
Phos-
horus
38-100
1,140
38,100
55,300
23,500
19,900
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
<b d
0.13
0.56
0.07
0.50
0.33
1.19
a
a
�.
�-
o' "
a
Arsenic
0.00
0.01
0.00
0.01
0.00
0.01
0.03
Cadmium
0.00
0.01
0.00
0.01
0.00
0.01
0.03
Chromiurr
0.01
0.01
0.01
0.03
0.02
0.05
0.14
Copper
0.26
0.31
0.15
0.64
0.41
1.78
3.55
Lead
0.02
0.02
0.01
0.05
0.02
0.15
0.26
Mercury
0.00
0.00
0.00
0.00
0.00
0.00
0.01
Molyb-
0.00
0.01
0.00-
0.01
0.00
0.01
0.04
denum
enum
Nickel
0.01
0.01
0.01
0.03
0.01
0.04
0.11
Selenium
0.00
0.01
0.00
0.01
0.01
0.02
0.05
Zinc
0.41
1 0.63
0.24
1.38
0.68
3.65
6.99
Total
Phos-
9.58
1.29
5.59
55.21
15.34
47.18
134.19
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the(rpossibilitf of fines and imprisonment for knowing violations"�L� n
0Z rcx [ 5
Signature of Land Applier Date
Ai ifti„r nmr„ i n Mcrriff nFNR FORM MFI RF (7/gMg)

ANNUAL. METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 35.16
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 19.95 Acres Permitted: 19.95 Site #: 1 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
n giro AeMA i 1A Q1171Me is 9n1d u,)Ma WR 9M4 RH 7014 WA20144-
Sample
or Com-
posite
Date
6/16/14
1/20/14
12/1/14
3/5/14
6/16/14
6/16/14
12/3/14
10/23/14
% Solids
0.71
2.60
1.61
1.74
0.71
1.41 1
1.58
2.87
Arsenic
13.90
3.73
6.21
5.46
13.90
6.17
6.33
3.14
Cadmium
13.90
3.73
6.21
5.46
13.90
6.17
6.33
3.14
Chromium
40.70
19.20
19.40
12.20
40.70
34.00
33.10
21.30
Copper
1050.00
662.00
255.00
273.00
1050.00
636.00
627.00
749.00
Lead
63.20
57.70
14.30
16.60
63.20
54.10
24.90
62.00
Mercury
3.80
1.17
1.24
0.63
3.80
1.49
6.96
0.95
Molyb-
denum
14.80
3.73
5.34
13.00
14.80
6.17
6.33
5.75
Nickel
37.00
14.70
15.00
11.10
37.00
26.50
18.10
17.50
Selenium
13.90
3.73
13.40
5.46
13.90
6.17
11.00
9.76
Zinc
1620.00
1250.00
4740.00
561.00
1620.00
1380.00
1040.00
1540.00
Total
Phos-
horus
38,100
4,150
16,600
1,140
38,100
55,300
23,500
19,900
Anneal Aeavv Metal Field Loadings (Calculated in lbs/acre):
� o
a
y
t7
0.09
0.65
0.05
0.24
0.06
0.18
0.06
0.43
9
o
Arsenic
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.02
Cadmium
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.02 ,
Chromiurr
0.01
0.03
0.00
0.01
0.01
0.01
0.00
0.02
0.08
Copper
0.19
0.86
0.03
0.13
0.13
0.22
0.07
0.65
2.28
Lead
0.01
0.08
0.00
0.01
0.01
0.02
0.00
0.05
0.18
Mercury
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.01
Molyb-
0.00
0.00
0.00
0.01
0.00
0.00
0.00
0.00
0.02
denum
Nickel
0.01
0.02
0.00
0.01
0.00
0.01
0.00
0.02
0.06
Selenium
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.01
0.02
Zinc
0.29
1.63
0.48
0.27
0.20
0.49
0.12
1.33
4.81
Total
Phos-
6.79
5.41
1.68
0.55
4.75
19.56
2.79
17.19
58.71
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility f nes and imprisonment for knowing violations" y
cz rc�r J
Signature of Land Applier Date
Ai0hrir nnrvi n Marritt nFNR FnRM MRSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 8.95
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA r,
Acres Used: 4.14 Acres Permitted: 4.14 Site #: 1 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
1 A A 1 A
Sample
or Com-
posite
Date
5/9/14
10/23/14
% Solids
2.56
2.87
Arsenic
3.20
3.14
Cadmium
3.20
3.14
Chromium
18.40
21.30
Copper
691.00
749.00
Lead
48.40
62.00
Mercury
0.79
0.95
Molyb-
denum
3.20
5.75
Nickel
14.30
17.50
Selenium
4.38
9.76
Zinc
1640.00
1540.00
Total
Phos-
horus
19,600
19,900
Anneal Apaw Mptal Field LandinQc Wnlrminted in lhs/acre):
Total
Phos-
. • rusmMENEENEENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the po ibility ofines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Darvl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
1
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Triple S Farms Total Dry Tons Applied (Annual):
WQ0030998 Cation Exchange Capacity (non 503 only):
Eric Smith Owner: Eric Smith Predominant Soil Series
40.24
n/a
FoA
11.2 Acres Permitted: 11.2 Site #: 1 Field #: 5
Residual Analysis Data (Leavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
RH 2O14 A2014 2-14 WA2014 3-1 Wz 2014 WA2014 4-
Sample
or Com-
posite
Date
12/3/14
5/9/14
7/21/14
10/19/14
10/23/14
% Solids
1.58
2.56
2.80
1.00
2.87
Arsenic
6.33
3.20
3.50
0.00
3.14
Cadmium
6.33
3.20
3.50
0.01
3.14
Chromium
33.10
18.40
18.20
0.00
21.30
Copper
627.00
691.00
804.00
0.72
749.00
Lead
24.90
48.40
52.10
0.12
62.00
Mercury
6.96
0.79
0.72
0.00
0.95
Molyb-
denum
6.33
3.20
5.32
0.00
5.75
Nickel
18.10
14.30
15.60
0.00
17.50
Selenium
11.00
4.38
6.18
0.00
9.76
Zinc
1040.00
1640.00
1710.00
1.40
1540.00
Total
Phos-
horus
23,500
19,600
4,190
12
19,900
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
�o
to b A=
o
` b d
0.39
0.51
1.69
0.04
0.96
�. n
O �
p
Arsenic
0.00
0.00
0.01
0.00
0.01
0.03
Cadmium
0.00
0.00
0.01
0.00
0.01
0.03
Chrorniun
0.03
0.02
0.06
0.00
0.04
0.15
Copper
0.49
0.71
2.72
0.00
1.44
1
5.35
Lead
0.02
0.05
0.18
0.00
0.12
0.36
Mercury
0.01
0.00
0.00
0.00
0.00
0.01
Molyb-
0.00
0.00
0.02
0.00
0.01
0.04
denum
Nickel
0.01
0.01
0.05
0.00
0.03
1
0.12
Selenium
0.01 1
0.00
0.02
0.00
0.02
0.05
Zinc
0.81 1
1.69
5.78
0.00
2.96
1 11.23
Total
Phos-
18.25
20.18
14.15
0.00
38.28
90.85
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the poss' ility of i s and imprisonment for knowing violations"
Signature of Land Applier Date
Author Darvl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS

G
ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
- - %TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
_ Metals (lbs/ac)
Nutrients (lbs/ac)
As — Arsenic
PAN — Plant Available Nitrogen
Cd — Cadmium
P — Phosphorus
Cr — Chromium
K — Potassium
Cu — Copper
_ Pb — Lead
Hg — Mercury
Mo — Molybdenum
Ni — Nickel
Se — Selenium
Zn — Zinc
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: WQ0030998 Field #: 1 Acres Utilized: 29.50
Owner: Eric Smith .nnual Dry Tons Applied: 123.07 Site #: 1 Acres Permitted: 29:50
Operator: Eric Smith Predominat Soil Series NoA Cation Exchange Capacity (non 503): NA
Cran 1 Name: Bermudaerass Crop 1 Max PAN: 299.00 Crop 2 Name: Oats (Grain) Crop 2 Max. PAN 50.00
S eci Volume Residual Sources Site Precip b o z Nitrate PAN Applied Must Select
oC7 Gal. % Solids Cond. 4 b po EF
$a Cu.Yd. Totals Applied per (NPDES #, WQ#, D Past 24 M w w 1 w TKN aq o and (lbs/acre) Crop 1 or Crop 2
CD i Report Per Acre As Acre Fert., Animal Waste, (Dry, Hrs. o w N * E. Nitrite
Totals Decimal etc) Wet, 0' * o * o w Crop 1 Crop 2 Crop -1 Crop 2
in Gal. DT/Ac Moist) Inches o m m m
Mar-14 276,000 9,356 2.60 1.01 Wallace WWTP IN 1.00 0.30 51,300 52 79 31.46 X
Apr-141 96,000 3,254 2.56 0.35 Wallace WWTP IN 1.00 0.30 39,600 3,920 209 10.31 X
Jul-14 330,000 11,186 2.80 1.31 Wallace WWTP_ IN 1.00 0.30 39,900 1,710 104 _ 34.67 X
Aug-14 312,000 10,576 2.80 1.23 Wallace WWTP IN 1.00 0.30 39,900 1,710 104 32.78 X
Oct-14 135,000 4,576 1.41 0.27 Warsaw WWTP S 0.50 0.30 72,400 987 36 11.81 X
TOTALS: 38,949 <<: As Cd Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied
Annuallbs/acre 0.03 0.03 0.16 6.25 0.44 0.01 0.04 0.13 0.05 13.11 73.09 109.21 11.81 Date lbs/ac
Current
e
0.17 0.15 NA 20.01 2.30 0.03 NA 0.51 0.28 30.96
1 Cumu
lative lbs/acr
Cumua A
0.38
0.2
4
4 17.
86
e
0. 14
0.1
2 NA 13.76
1.86 0.02 N
'
Pr
ior Years Cumulative lbs/acr
48
2 7 15 NA 3 7 4 89
50.00
2 9
1 338 6
C. P. L. R.
36 34 NA ,
Permitted
s 2nd
Crop
,Permi
t
Limi
t 1 t/
"I certify, under penalty of law, that this document was prepared under my turecuvu or -----
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Signature of Land Applier Date Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: W00030998 Field #: 1 Acres Utilized: 8.48
Owner: Eric Smith .nnual Dry Tons Applied: 23.53 Site #: 2 Acres Permitted: 8.48
Operator: Eric Smith Predominat Soil Series FoA - Cation Exchange Capacity (non 503): NA
Crop 1 Name: Millett Crop 1 Max PAN: 100.00 Crop 2 Name: Oats (Grain) Crop 2 Max. PAN 50.00
>>
�
�G
CD
�
Specify
Totals
Per Acre
u
/o Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(Dry'
Wet,
Moist)
Precip.
Past 24
Hrs.
Inches
y
b
4 b
a*
o
w
N
* o
�
5El
w
*
a;
TKN
m
z Y
o f
OQ El
m
Nitrate
and
Nitrite
m
PAN Applied
pp
(lbs/acre)
Must Select
Crop 1 or Crop 2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Feb-14
36,000
4,245
0.71
0.13
Beulaville WWTP
S
0.50
0.30
75,200
493
122100
8.74
X
May-14
66,000
7,783
1.74
0.56
Kenansville WWTP
S
0.50
0.30
17,900
169
2,480
8.90
X
Jun-14
21,000
2,476
0.71
0.07
Beulaville WWTP
S
0.50
0.30
75,200
493
122100
5.10
X
Jul-14
72,000
8,491
1.41
0.50
Warsaw wwTP
S
0.50
0.30
72,400
987
36
21.92
X
Jul-14
42,000
4,953
1.58
0.33
Rose Hill WWTP
S
1 0.50
0.30
61,700
1,040
180
12.33
X
Dec-14
84,000
9,906
2.87
1.19
Wallace WWTP
IN
1.00
0.30
40,600
617
24
29.96
X
TOTALS:
37,854
:i?:,'::':> ::>:'
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.03
0.03
0.14
3.55
0.26
0.01
0.04
0.11
0.05
6.99
134.19
48.25
38.70
Date
lbs/ac
Current Cumulative lbs/acre
0.0 8
0. 7
0
N A
9.84
1.18
0.03
NA
0.23
0.13
16.15
'
Prior Years Cumulative lbs/acre
0 OS
0 04
N A
6.30
0.92
0.01
NA
0.12
0.08
9.17
Permitted C. P. L. R. ****
36
34
NA
1338
267
15
NA
37 4
8 9
4
2 98
,
2 Cro
t PAN Limit 1st/ nd Perms
,.......:...::::.:...:.::.:.....:...:..,...:...:.:.::.::.:::...:...:.:..:..:..:.:.
.. .. '
100
50. 0
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance witn a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting f se information, including the possibility of fines and imprisonment for knowing violations."
- *Application Method: S - Surface, IN - Injection, INC - Incorporation
-�?- **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: W00030998 Field #: 1 Acres Utilized: 19.95
Owner: Eric Smith Lnnual Dry Tons Applied: 35.16 Site #: 3 Acres Permitted: 19.95
Operator: Eric Smith Predominat Soil Series FoA Cation Exchange Capacity (non 503): NA
Crop 1 Name: Bermudagrass Crop 1 Max PAN: 276.00 Crop 2 Name: Oats (Grain) Crop 2 Max. PAN 50.00
C�
o p;
<>
Specify
Totals
Per Acre
a
/o Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)Wet,
Site
Cond.
(Dry,
Moist)
Precip
Past 24
Hrs.
Inches
>
4 b
a w
c
o
P
w w
N
* w
�,
�
:;
*
p
TKN
z a
0 �
CIQ c
� -�
w•
m
Nitrate
and
Nitrite
m
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
GaI.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Feb-14
60,000
3,008
0.71
0.09
Beulaville WWTP
S
0.50
6.30
75,200
493
12,100
6.19
X
Mar-14
120,000
6,015
2.60
0.65
Wallace WWTP
IN
1.00
0.30
51,300
52
79
20.22
X
Apr-14
15,000
752
1.61
0.05
ithwest Plantation WA
S
0.50
0.30
63,900
6
560
1.99
X
May-14
66,000
3,308
1.74
0.24
Kenansville WWTP
S
0.50
0.30
17,900
169 1
2,480
3.78
X
Jun-14
42,000
2,105
0.71
0.06
Beulaville WWTP
S_
0.50
0.30
75,200
493
12,100
4.33
X
Jul-14
60,000
3,008
1.41
0.18
Warsaw WWTP
S
0.50
0.30
72,400
987
36
7.76
X
Jul-14
18,000
902
1.58
0.06
Rose Hill WWTP
S
0.50
0.30
61,700
1,040
180
2.25
X
Dec-14
72,000
3,609
2.87
0.43
Wallace WWTP
IN
1.00
0.30
40,600
617
24
10.92
X
TOTALS:
122,707
<:'':':; `> >:>'::
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.02
0.02
0.08
2.28
0.18
0.01
0.02
0.06
0.02
4.81
58.71
40.34
17.11
Date
lbs/ac
a/ lbs
CurrentCumulative cre
0.10
0.08
NA
7.94
0.85
0.02
NA
0.20
0.14 12.65
0.12 7.84 4
4 2 8
89 9
Years Cu ive lbs acr e
Cumulative / Prior
0 08
0 06
N A
5.65
0.67
0.01
NA
0.14
Permitted C. P. L. R. ** *
36
34
N A
13 38
2 7
6
15
NA
37 4
d ro
L m1t 1 st/2n C
P ermlt PAN 1 p
::.:.:.:. ,.:...:..:.:.,.:.:.:...:..,...:...:.....:.:::.:.:...:.:..:: :..: .
276
50.00
"I certify, under penalty of law, that this document was prepared under my airecnon or supervision m accoruancc wiLu a ay3LUM
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: W00030998 Field #: 1 Acres Utilized:
Owner: Eric Smith ,nnual Dry Tons Applied: 8.95 Site #: 4 Acres Permitted:
Operator: Eric Smith Predominat Soil Series FoA Cation Exchange Capacity (non 503):
Crop 1 Name: -ans (Double Cropped -Man Crop 1 Max PAN: 133.00 Crop 2 Name: Oats (Grain) Crop 2 Max. PAN
4.14
4.14
NA
50.00
G
o rt
CD
Sp ecify
Totals
Per Acre
u
/o Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
eta )
Site
Cond.
wry'
Wet,
Moist)
Precip
Past 24
Hrs.
Inches
�s
m
n# o•
0
w �,
* N
5'
w w
_
*
TKN
m
z
o 5
o
R �
m
Nitrate
and
Nitrite
m
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Apr-14
30,000
7,246
2.56
0.77
Wallace WWTP
IN
1.00
0.30
39,600
3,920
209
22.95
X
Oct-14
48,000
11,594
2.87
1.39
Wallace WWTP
IN
1.00
0.30
40,600
617
24
35.07
X
TOTALS:
18,841
.- :
As
Cd
Cr
Cu
Pb
H2
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Ap plied
Annuallbs/acre
0.01
0.01
0.09
3.15
1 0.25
0.00
0.02
0.07
0.03
6.81
85.55
22.95
35.07
Date
lbs/ac
�ve cre
Current Cumulative lbs/a
0 0
.3
0.02
NA
4 .73
0.3 9
0.01
0.0 0.0 4 7.11
NA 9
NA 0.020.010.30
4
3 4 89 2 98
NA 7
:.... 3 50.00
13
'
Prior Years Cumulative lbs/acr e
0.01
0.00
NA
1.58
0.15
0.00
Permitted C. P. L. R. **
Perms
36
3 4
NA
1338
26 7
15
Permit PAN Limit 1 st/2nd Crop
.... .:.........,...................:
..:....................:..:.<:..:.:::..:::.:::....:::::...:.:;:::..
:
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance witt< a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
K_*Application Method: S - Surface, IN - Injection, INC - Incorporation
Wo� -, �� **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLAND FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: W00030998 Field #: 1 Acres Utilized:
Owner: Eric Smith mnual Dry Tons Applied: 40.24 Site #: 5 Acres Permitted:
Operator: Eric Smith Predominat Soil Series FoA Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max PAN: 207.00 Crop 2 Name: ins (Double Cropped - Ma Crop 2 Max. PAN
11.20
11.20
NA
50.00
C�
o p;
CD `.
o
Specify
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT/AC
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(Dry'
Wet,
Moist)
Precip.
Past 24
Hrs.
Inches
y
�
°
0
o
7�:
w w
* w
o
5
w
*
0
tj
TKN
m
z a
0 o
w
m
Nitrate
and
Nitrite
mg/kg
PAN Applied
pp
(lbs/acre)
Must Select
Crop 1 or Crop 2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Apr-14
66,000
5,893
1.58
0.39
Rose Hill WWTP
S
0.50
0.30
61,700
1,040
180
14.67
X
Apr-14
54,000
4,821
2.56
0.51
Wallace WWTP
IN
1.00
0.30
39,600
3,920
209
15.27
X
Sep-14
162,000
14,464
2.80
1.69
Wallace WWTP
IN
1.00
0.30
39,900
1,710
104
44.83.
X
Sep-14
10,600
946
1.00
0.04
irphy Brown Soybean,
IN
1.00
0.40
1,000
0
0
0.03
X
Oct-14
90,000
8,036
2.87
0.96
Wallace WWTP
IN
1.00
0.30
40,600
617
24
24.30
X
TOTALS:
34,161
":
As
Cd
Cr
Cu
Pb
HR
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.03
0.03
0.15
5.35
0.36
0.01
0.04
0.12
0.05
11.23
90.85
69.16
29.94
Date
lbs/ac
bs acre
1 / C Current Cumulative
0.06
0.05
NA
4
10. 6
1.01
0.02
NA
0.21
0.09
16.21
lbs/ Prior Years Cumulative acre
0.04
0 03
NA
5.11
0 .65
0.01
NA
0.09
0.04
4. 8
9
Permitted C. P. L . R. **
36
34
NA
1,338
267
15
NA
374
89
4
2,498
El
Permit PAN Limit 1st/2nd Crop
..:...:.;:::.:::.:...:..:.. ......
...........207
50.00
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance witn a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
C *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, InjectiomIncorporation - 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

RESIDUAL ANALYSIS LAB SHEETS
I

I
_
Envirom- nental Chemists,
Inc.
-- ichem
envir
6602 Windmill Way - WAxtington, NC 25405
[phone] (Lab) - [phone] (Fax)
_!
710 Bowserta'wn Road • Manfieo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS
NCDE 4&- DWQ CT- RMCATE #94. DLS CERTIFICATE 437729
Town of Beulaville
Date of Report: Jul 09, 2014
- - Post Office Sox 130
Customer PO #:
Seulaville NC 28518
Customer ID: 08100015
Attention: Angie Miller
Report #: 2014-07044
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-17327 Site: Sludge
5/16/2014 9:35 AM Solid/Sludge Angie Miller
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
14000mg/kg
07/02/2014
Arsenic
EPA 200.7
<13.9 mg/kg
07/01l2014
Cadmium
EPA 200.7
<13.9 mglkg
07/01/2014
Calcium
EPA 200.7
35900 mg/kg
07/02/2014
Chromium
EPA 200.7
40.7mg/kg
07/01/2014
Copper
EPA 200.7
1050 mg/kg
07/01/2014
Lead
EPA 200.7
63.2 mg/kg
07/01/2014
Magnesium
EPA 200.7
4070 mglkg
07/02/2014
Molybdenum
EPA 200.7
14.8 mg/kg
07/07/2014
Nickel
EPA206.7
37.0 mglkg
07/0112014
Potassium
EPA 200.7
7240mg/kg
07/02/2014
Selenium
EPA 200.7
<13.9 mglkg
07/01/2014
Sodium
EPA200.7
11300 mglkg
07/02/2014
Zinc
EPA 200.7
1620 mg/kg
07/01/2014
Ammonia Nitrogen
EPA 350.1
493 mglkg
06/20/2014
Total Kjeldahl Nitrogen (TKN)
EPA 3512
75200 mg/kg
06/23/2014
Nitrate+Nitrite-Nitrogen
EPA 353.2
12100 mglkg
06/24/2014
Total Solids (°l°}
sM2540B
0.71 %
06/17/2010
pH
SM4600 H B
5.75 units
06/1812014
Total Phosphorus
SM4500 P F
38100 mg/kg
06/23/2014
Mercury
swe46 7471 B
3.80 mglkg
07/02/2014
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
c
Reviewed by:
/
Report #:: 2014-07044 Pagel of 1

f
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC OFFICE910-9z02 3PAX910.3 228405
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
C'M 1 Rr-TInN ANrf r`I-iAIN AF r:11STnnV
CLIENT:
PROJECT NAME:
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO:
email:
-RaminiPe1 Bv- ,%.. Z fit. RZ;: SAMPLE TYPE: I = Influent. E = Effluent. W a Well. ST = Stream. SO = Sail. SL = Sludge, Other:
Sample Identification
Collection
m
ti
C
w
E `o
�O
`o
va
C
a `�
V E
a W
z
PRESERVATION
ANALYSIS REQUESTED
D to
Time
Temp
z
A
x
a
=
"'
o
_a
o
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
DatelTlme
Received By:
Datei ime
1.
2.
Temperature when
Delivered By: �.
Comments:
I

May 301410;16a Environmental Chemists
9103924424
p.1
Environmental Chemists, Inc.
enviroc�em6602
Windmill Way Wilminb on, VC 28405
'-'111h,(910)
392-0223 (Lab) - [phone] (Fax)
710 Bowsertown Road - Manteo, NC 27954
ANALYTICAL & CONSULTING
[phone]
CHEMISTS
NCDENR: DWQ CERTIRCATE #94. DLS CMUICATE #37739
Town of Kenansville
Date of Report: Apr 07, 2014
PO Box 370
Customer PO #:
Kenansville NC 28349
Report #: 2014-02550
Attention: Gary Benson
report to: Garry Benson
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-06181 Site: sludge
3/5/2014
10:00 AM Solid/Sludge Client
_ Test
Method
Results
Date Analyzed
.Chlordane
SW 846 Method 80818/3510
<0.005 mg/L
0311712014
! Endri n
SW 846 Method 8081 BJ3510
<0.00005 mg/L
03/17/2014
Heptachlor
SW846Meftd6081BJ3510
<0.00005mg/L
0311712014
Heptachlor epoxide
SW 846 Method 6081B/3510
<0.00005 mg/L
0311712014
Lindane
SW 846 Method eBBI8n510
<0.00005 mg/L
03117/2014
Methoxychlor
SNV 846 Method Bo81 ea510
<0.00005 mg/L
03/1 W2014
Toxaphene
SW 846 Method 8081 BJ3510
<0.005 mg/L
03/17/2014
1,4-Dichlorobenzene (TCLP)
SW 846 method B27013510
<0.050 mg/L
03/1412014
2,4,5-Trichlorophenol (TCLP)
SW 846 method8270MIO
<0.050 mg/L
03/1412014
2,4,6-T'richlorophenol(TCLP)
SW 846 method B270/351 0
<0.050mg/L
03/14/2014
2,4-Dinitrotoluene (TCLP)
SW 846 method 827013510
<0.050 mg/L
03/1412014
Cresol (TCLP)
5W 846 method 8270/3510
<0,050 mg/L
03/14/2014
Hexachlorc-1,3-butadiene(TCLP)
5W846method827oJ351a
<0.050 mg/L
03/14/2014
Hexachlorobenzene (TCLP)
SW 846 method 8270/351a
<0.050 mg/L
03/1412014
Hexachlorcethane (TCLP)
SW 845 method 827013 51 0
<0.050 mg/L
03/14/2014
m + p-Cresol (TCLP)
SW 645 method 8270/3510
<0.050 mg/L
03/14/2014
Nitrobenzene (TCLP)
SW W method 827=51 0
<0.050 mg/L
03/1412014
o-Cresol (TCLP)
SW 846 Method 827013510
<0.050 mg/L
03J14/2014
Pentachlorophenol (TCLP)
SW 846 method 8=13510
<0.250 mg/L
03/14/2014
Pyridine (TCLP)
SW 846 method 827013510
<0.050 mg%L
03114J2014
2,4,5-TP
SW846 Method 8151A
<0.0003 mg/L
03/17l2014
2,4-0
SW846 Method 8151A
<0.0003 mg/L
03/1712014
1,1-Dichloroethylene
Sw646Method 8260/5o3o
<0.01 mg/L
03/2812014
1,2-Dichloroethane
SW846 Method 8260/5030
<0.01 mg/L
03/28/2014
Benzene
SW846 Method 8260/5030
<0.01 mg/L
03/28/2014
Carbon Tetrachloride
SWe46 Method 82ea5030
<0.01 mg/L
03/28/2014
Report #:: 2014-02550
Page 1 of 3

May 301410;16a Environmental Chemists
9103924424 p.2
Environmental Chemists, Inc.
envirochem 6602 Wutdmtll Way @ Wibmington, NC 26405
[phone] (lab) • -[phone] (Fax)
sr,
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL &CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE DLS CERTIFICATE #37729
Town of Kenansville
Date of Report: Apr 07, 2014
PO Box 370
Customer PO #:
Kenansville NC
28349
Report #: 2014-02550
Attention: Garry Benson
Report to: Garry Benson
Project 1D: Sludge
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
03128/2014
Chloroform
SW646 Method 826060a0
<0.01 mg/L
03128/2014
Methyl ethyl ketone
SW846 Method 826OP5030
<0.05 mg/L
03/2812014
Tetrdchloroethylene
SWa46 Method 826015030
<0.01 mg/L
03128/2014
Trichloroethylene
SW846 Meftd 826015030
<0.01 mg/L
03128/2014
Vinyl Chloride
SW846 Method 8260l5030
<0.01 mg/L
0312812014
RCI
Cyanide
EPA 336.4
<0.120 mglkg
04102/2014
Sulfide
SM 4500 s o
<Q.240 mglkg
04/01/2014
Ignitability
SW S46 method 1010
>212 OF
03/1412014
Sludge Residuals
Aluminum
EPA 200.7
4170 mglkg
03/13/2014
Cadmium
EPA 200.7
<5-46 mglkg
03/10/2014
Calcium
EPA 2003
25700 mglkg
03/12/2014
Chromium
EPA 200.7
12.2 mglkg
03110/2014
Copper
EPA 200.7
273 mglkg
03/12/2014
Lead
EPA 200.7
16.6 mglkg
03114/2014
Magnesium
EPA2oo.7
1620 mg/kg
0311212014
Potassium
EPA 200.7
2520 mg/kg
03/12/2014
Selenium
EPA 200.7
<5.46mg/kg
03/14/2014
Sodium
EPA200.7
3660 mglkg
03/1212014
Zinc
EPA200.7
561 mglkg
03/10/2014
Arsenic
EPA200.8
<5.46mg/kg
3117/2014
Molybdenum
EPA 200.8
13.0 mg/kg
3/17/2014
Nickel
EPA200-8
11.1 mglkg
3/17/2014
Ammonia Nitrogen
EPA350.1
169 mg/kg
03/1412014
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
17900 mglkg
03/2612014
Nitrate+NMte-Nitrogen
EPA=2
2480mg/kg
03/21/2014
Total Solids (%)
SM 2640 B
1.74 %
03/1012014
Report A: 2014-02550
Page 2 or3

May 301410:17a Environmental Chemists
9103924424
p.3
Environmental Chemists,
Inc,
envirochem6602
Windmill Way • Wilmington, ATC 28405
—' 6
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • lvlanteo, NC 27954
ANALYTICAL & CONSULTING
(252) ` 73-5702
- CHEMISTS
NCDENR DWQ CERTIFICATE *94. DLS CERTIFICATE #37729
Town of Kenansvilie
Date of Report: Apr 07, 2014
PO Box 370
Customer PO #:
Kenansville NC 28349
Report #: 2014-02550
Attention: Garry Benson
Report to: Garry Benson
Project ID: Sludge
pH SM 4500"B
7.04 units
03M 112014
Total Phosphorus SPA 4500 P F
1140 mglkg
04/0312014
Mercury SW84S 74718
0.6320 mg/kg
03/1912014
TCLP Metals
Arsenic EPA200.8
<0.010 mg/L
03/1212014
Barium 8PA200.8
0.070 mg/L
03/12/2014
Cadmium EPA 200.8
<0.010 mg1L
03/12/2014
Chromium EPA200.8
0.028 mg/L
03/1212014
Lead EPA200.8
<0.010mg/L
03/12/2014
Selenium EPA200.8
<0.010 mg/L
03/1212014
Silver EPA200.8
<0.010.mg/L
03/12/2014
Mercury EPA 245.1
<0.002 mg/L
03/24/2014
Comment: Sludge residuals results, except pH,
reported on a dry weight basis. pH and RCI reported on an as
received basis.
Reviewed by:
Report *:: 2014-02550
Page 3of3

a
a-
V
ct
N
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• a ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
P�11 1 1=r"r1MK1 AK1r% nLJAIAI /1c 9-1 Ic.r�rw
0002 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
CLIENT: Town of Kenansville
PROJECT NAME: Annual Sludge
REPORT NO:
ADDRESS:
CONTACT NAME: Garry Benson
PO NO:
REPORT TO:
PHONEIFAX:
COPY TO:
email:
V—I"OV.
-
Sample Identification
e
Collection
W
f
- ••...
o a
a o
E
�i�
a
c a
.. - ..w.awup
C�
; I"w
P E
,..
Hw
m
S z
- a-l—wo1L,
PRESERVATION
vv
- vvunj a 1 = ajream,
sU t: son, sL. = Sludge, Other:
ANALYSIS REQUESTED
Date
Time
Temp
W
a
o
o
a
u�l
Sludge
SI
C
LQ
�,�
Full TCLP/RCl/Nutrients/Meiais
G
C
P
G-1
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
C
G
P
G
G
C P
G G
C P
G G
C P
G G
Transfer
�.a
2.
Temperature when R
Relinquished By:
AA
d
Date/Time
.3-�• ; . m
~�
Received By:
Date/Time
3 cis ��
e Ive Accepted: r Re ctedd: Resample Requested:
co Delivered By: .G 6
,�!' _ Received By: ' t7 f LC. �s� Date: Time: _j dC.�
Comments: ITURNAROUND:

POO"".
Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 2&05
-�L [phone] (Lab) . [phone] (Pax)
® 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL $ CONSULTING
CHEMISTS NCDENIL- DWQ CERTIFICATE 0& DIS CERIMCATE #37729
Town of Rose Hill
Date of Report: Jan 07, 2015
P. 0, Box 8
Customer PO #:
- Rose Hill NC 28458
Customer ID: 09020035
Attention: Ben Hilliard
Report #: 2014-14986
Project ID: Sludge
Lab ID Sample ID:
Collect Daterfime Matrix Sampled by
" 14-36714 Site: Sludge
12/3/2014
10:15 AM Solid/Sludge Ben Hilliard
Test
Method
Results Date Analyzed
f
Chlordane
SW 846 Method 8081BI3510
<0.05 mg/L
12/10/2014
Endrin
SW 846Method 8081B/3510
<0.0005 mg/L
12/10/2014
Heptachlor
SW 846 Memm eoe18 wo
<0.0005 mg/L
12/10/2014
Heptachlor epoxide
SW 846 Method s0B18/3510
<0.0005 mg/L
12/10/2014
Lindane
SW 846 Method 8081B/3510
<0.0005 mg/L
12/10/2014
Methoxychlor
SW 846 Method 808113/3510
<0.0005 mg/L
12/10/2014
Toxaphene
SW 846 Methods0818/3510
<0.05 mg/L
12/10/2014
1,4-Dichlorobenzene (TCLP)
sW e46 method e278/3510
<0.050 mg/L
12/11/2014
2,4,5-Trichlorophenol (TCLP)
<0.050 mg/L
12/11/2014
2,4,6-Trichlorophenol (TCLP)
SW 846 method 6270/3510
<0.050 mg/L
12/11/2014
2,4-Dinitrotoluene (TCLP)
SW 846 method 6270/3510
<0.050 mg/L
12/11/2014
r
Cresol (TCLP)
SW 840 method 0270/3510
<0.050 mg/L
12/11/2014
Hexachloro-1,3-butadiene (TCLP)
SW 646 method 8270/3510
<0.050 mg/L
12/11/2014
Hexachlorobenzene (TCLP)
SW e46 method 827OM510
<0.050 mg/L
12/11/2014
Hexachloroethane (TCLP)
SW 846 method 827OM510
<0.050 mg/L
12/11/2014
m + p-Cresol (TCLP)
SW 846 method 8270► I0
<0.050 mg/L
12/11/2014
Nitrobenzene (TCLP)
SW 848 method 827W51.0
<0.050 mg/L
12/11/2014
o-Cresol (TCLP)
SW 846 method e270M510
<0.050 mg/L
12/11/2014
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
12/11/2014
' Pyridine (TCLP)
SW e46 method W70/3510
<0.050 mg/L
12/11/2014
2,4,5 TP
SW646 Method 8161A
<0.003 mg/L
12/12/2014
2 4-D
SWe46 Method 8151A
<0.003 mg/L
12/12/2014
1,1-Dichloroethylene
SW848Method 828015030
<0.01 mg/L
01/01/2015
1,2-Dichloroethane
SW846Method =0/5030
<0.01 mg/L
01/01/2015
Benzene
SW846 Method 8260/5030
<0.01 mg/L
01/01/2015
Carbon Tetrachloride
SWO46 Method 8260/5030
<0.01 mg/L
011 112015
Report #:: 2014-14986
Page 1 of 3

Environmental Chemists,
Inc,,
• •
6602 Windmill Way . Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
®
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERTIECATE #94. DLS CERTIFICATE #37729
Town of Rose Hilt
Date of Report: Jan 07, 2015
P. O. Box 8
Customer PO #:
Rose Hill NC 28458
Customer ID: 09020035
Attention: Ben Hilliard
Report #: 2014-14986
Project ID: Sludge
`
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
01/01/2015
Chloroform
SWO46 Method 8M.15030
<0.01 mg/L
01/01/2015
Methyl ethyl ketone
SVM6 Method 8260/5030
<0.05 mg/L
01/01/2015
Tetrachloroethylene
SvM8 Method 8NO15030
<0.01 mg/L
01/01/2015 -
Trichlo roeth Iene
SW846 Method 8260/5030
<0.01 m /L
01/01/2015
Vinyl Chloride
SWM6 Method 8260/5030
<0.01 mg/L
01/01/2016
RCI
Cyanide
EPA 335.4
0.1.37 mg/kg
12/19/2014
SuiSde
SM 4500 S D
2.68 mg/kg
12/17/2014
Ignitability
SW 846 method 1010
>212 OF
12/17/2014
Sludge Residuals
Aluminum
EPA200.7
4900 mg/kg
12/09/2014
Arsenic
EPA 200.7
<6.33 mg/kg
12/05/2014 ,
Cadmium
EPA 200.7
<6.33 mg/kg
12/06/2014
Calcium
EPA200.7
40600mg/kg
12/11/2014
Chromium
EPA 200.7
33.1 mg/kg
12/05/2014
Copper
EPA200.7
627 mg/kg
12/16/2014
Lead
EPA200.7
24.9 mg/kg
12/05/2014
Magnesium
EPA20D.7
1660 mg/kg
12/11/2014
Molybdenum
EPA 200.7
<6.33 mg/kg
12/05/2014
Nickel
EPA 200.7
18.1 mg/kg
12/05/2014
Potassium
EPA200.7
3230 mg/kg
12/11/2014
Selenium
EPA200.7
11.0 mg/kg
12/05/2014
Sodium
EPA200.7
2710 mg/kg
12/11/2014
zinc
EPA 200.7
1040 mg/kg
12/05/2014
Ammonia Nitrogen
EPA 350.1
1040 mg/kg
12/10/2014
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
61700 mg/kg
12/12/2014
Nitrate+Nitrite-Nitrogen
EPA 3532
180 mg/kg
12/15/2014
Total Solids (%)
SM 2540 a
1.58 %
12/08/2014
pH
SM 4500 H e
7.23 units
12/05/2014
Report#:: 2014-14980
Page 2 of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Pax)
® 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE *39929
Town of Rose Hill Date of Report: Jan 07, 2015
-' P. O. Box 8 Customer PO #:
Rose Hill NC 28458 Customer ID: 09020035
Attention: Ben Hilliard Report #: 2014-14986
Project ID: Sludge
Total Phosphorus SM 4500 P F 23500 mg/kg 12/12/2014
Mercury Swa46 74718 6.96 mg/kg 12/06/2014
TCL.P Metals
Arsenic
EPA200.8
<0.100 mg/L
12/15/2014
Barium
EPA200.8
<0.100mg/L
12/15/2014.
Cadmium
EPA200.8
<0.100 mg/L
12/15/2014
Chromium
EPA200.8
<0.100 mg/L
12/16/2014
Lead
EPA 200.8
<0.100 mg/L
12/15/2014
Selenium
EPA200.8
<0.100mg/L
12/15/2014
Silver
EPA 200.8
<0.100 mg/L
12/15/2014
Mercury
EPA 245.1
<0.002 mg/L
12/17/2014
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
S
Report*: 201444889 Page 3 of 3

6602
dm
l Way
mington
ENVIRONMENTAL CHEMISTS, INC OFFIC In 10f392- 9 3iiFAX91D-392.4424
Analytical &Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Town of Rose Hill
PROJECT NAME: Sludge
REPORT NO: `f - l ��
ADDRESS:
CONTACT NAME: Ben Hilliard, ORC
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO:
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream. SO = Soil. SL = Sludge. Other.
Sample Identification
Collection
=
av
E
.2 a
o o
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c�
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c
sJ
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c
a
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m'
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PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
c
Z=
u
o
"'
c
o
w
o
Sludge
C
P
� � �
X
Full TCLP, Nutrientstmetals, RCI
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relin shed By:
—,PajeMme
Receiv d By:
D e/Time
1.aAf
2.
I emperature when Received: 'f �— Accepted: k Relect d• Resample Re ed:
Delivered By: Received By: Date: / t Time:�-
Comments: casoll VOISAW TURN OUND:

1 V, 0 OP t [IV k;--
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soot west PlantalJon - Bear Trail GO
Dat& of Report. Occ 25 2014
- ckstin Store Road,
custo"my PO M
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Collect Da1*'Mw72"""`
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Results
Date A nulyzed
12, 1 C120 Ja
-.0 Or.05 M.zl
1 2! 1 W? 0 1
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12' "1 CIL 1
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0681ad-0.
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Date of Ropom Dec 25 20-,4
163 .-,aaksor Slo,uRoad
C;jstumcr PO 4.-
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Report R: 2Z14-14W
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Inc.
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SOUL hwest Plantation Bear Trail Golf
Caw of Report: ""O'c u 2G. 2W, 4
IG3.:s2R$*- 'Stwe -R�Od
Customer PO
Bewavifle INC.
custorner J0,
A:1c-M*n Slv*w M-'iv
Roport V:
Project. ID., $1,Age
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CtIENIISTS. INC
wilminap'".,NC 28405
SAMIlle Collection and Chain pf Custpdy [phone]
2
F2.1 (910) 392.44
�6
V111C
tfie-01'. S01101wel !:!�� ReZort-Nw-4
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Temperature wheii Received.__ AcceptjDow.
Deliverf.-d

I
-1unvironmental Chemists, Inc.
M02 Windmill Way • Wilmington, NC 28405
enviroche M.[phone] (Lab) v (910) 392-W4 (Fax)
® 710 Bowsertown Road • Manteo, NC 27954
(252) 47"702
ANALYTICAL R CONSULTING
CHEMISTS NCDHNB: DWQ CERTIFICATE #94. DLS CERTMCATE #3M9
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (VV TP)
Date of Report: Feb 19, 2014
Customer Po #:
Report #: 2014-00762
Report to: Brent Dean, ORC (WWTP)
Project ID: WVVTP Sludge
Lab 10 Sample ID: Collect Date/Tlme Matrix Sampled by
14-01878 Site: Sludge 1/20/2014 9:00 AM Solid/Sludge Derek Reed
Test
MethodResults
Date.Analyxed
Sludge Residuals
Aluminum
EPA 200.7
9310 mg/kg
02/04/2014
Arsenic
EPA2001
<3.73 mg/kg
01/22/2014
f Cadmium
EPA200.7
<3.73 mg/kg
01)22/2014
Calcium
EPA 200.7
22800 mg/kg
02/05/2014
Chromium
EPA 200.7
19.2 mg/kg
01/22/2014
Copper
EPA 200.7
662 mg/kg
02/11/2014
Lead
EPA 200.7
57.7mg/kg
01/2212014
Magnesium
EPA200.7
2300mg/kg
02/05/2014
Molybdenum
EPA 2007
<3.73 mg/kg
01/22/2014
Nickel
EPA 200.7
14.7 mg/kg
01/22/2014
Potassium
EPA 2W7
2770 mg/kg
02/05/2014
Selenium
EPA2001 .
<3.73 mg/kg
01/22/2014
Sodium
EPA 200.7
4190mg/kg
02/05/2014
Zinc
EPA 200.7
1260 mg/kg
02/04/2014
Ammonia Nitrogen
EPA350.1
51.9mg/kg
01/31/2014
Total ICeldahl Nitrogen (TKN)
EPA351.2
51300 mg/kg
02/05/2014
Nitrate}Nitrite-Nitrogen
EPA353.2
78.8mg/kg
02/14/2014
Total Solids N
SM 2540 a
2.60 %
01/22/2014
pH
SM 4500 H s
6.86 units
01 /23/2014
Total Phosphorus
SM 450o P F
4150 mg/kg
02/05/2014
Mercury
Swe4s 7470A
1.17 mg/kg
02/14/2014

---- G 1 I ISO N M E N TA C H E M' STS N C ---' OFFICE: 910-392.02231FAX [phone]�
Analytical l;< Consulting Chemists
NCDENR: DWQ CERTIFICATION 9 94 NCDHHS: DLS CERTIFICATION S 37no [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Town of Wallace WWTP
PROJECT NAME: Sludge
REPORT NO: L
ADDRESS:
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONEIFAX: 284.7969 284.5073
OPY TO: Jerry James, Public Works
email: bdean@!ownofwallace.com
Sampled By:
SAMPLE
TYPE: I = Influent,
E Effluent,
W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
E
E 0
00
d
`o
"_
E
V
flw
m
z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
x
i
s_
c
c
o
w
Sludge
!g
X
nutrients/metals
G
1
X
fecal density/ %TS
r-
G
2
9'-1
C
IOU)X
_
fecal densi / %TS
I
G
3
C
�b�i
X
fecal densi / %TS
i�
G
4
4 a
C
�
X
fecal density/'/6TS . .
) -
G
5
4,+
X
fecal dens / %TS
G
G
6
4 -
C
I i
X
fecal density/ %TS
---4
G
7
X
fecal density/ %TS
i- -
G
C
P
G
G
Transfer
R qui ed By:
DateRime
Rece ved By_
Date/Time
2.
Temperature when Received: J `' Accepted: r jected: Resample R q sted:
Delivered By: • 2211 Received By: � .P�� Date: H Time: Oil
Comments: TURNAROUND:
1

Environmental Chemists, Inc.
7
' 6m2 Windmill Way o Wilmington, NC 28405
(910) 392-OM (Lab) a [phone] (Fax)
® 710 Bowsertown Road ® Manteo, NC 27954
f [phone]
1 /WN.YrIC/4L&CONSULnNG
CHEMISTS NCDDML- DWQ CERTIRICATE #94. DIS CERT114CATE #37729 -
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Lab ID
,14-13113
1
Test Method Results Date Analyzed
Date of Report: Jun 19, 2014
Customer PO M
Customer ID: 09010063
Report #: 2014-05424
Project ID: WWTP Sludge
Sample ID:
Site: Sludge-TCLP
Collect Date/Time Matrix Sampled by
5/9/2014 9:43 AM Solid/Sludge Client
Total Solids N
SM 2.540 a
2.66 %
05/1Z2014
Chlordane
SW 046 MethOd 6081813510
<0.005 mg/L
05/16/2014
Endrin
SW8461 iethod 6081613510
<0.00005 mg/L
05/16/2014
Heptachlor
Sw e46 Method 80616/3510
<0.00005 mg/L
05/16/2014
Heptachlor epoxide
swe4s Nlelhad eoele►3510
<0.00005 mg/L
05/16/2014
I_indane
SW 84s Method 8081Ni3510
<0.00005 mg/L
05/16/2014
Methoxychlor
sw 646 Method eo618/3510
<0.00005 mg/L
05/16/2014
Toxaphene
SW "0 Method e061613510
<0.005 mg/L
05/16/2014
1,4-Dichlorobenzene (TCLP)
SW s46 method 627013510
<0.050 mg/L
06/15/2014 .
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270010
<0.050 mg/L
05/15/2014
2,4,6 Trichlorophenol (TCLP)
SW "S method 827QG510
<0.050 mg/L
05/15/2014
2,4-Dinitrotoluene (TCLP)
SW 646 method e27018510
<0.050 mg/L
05/15/2014
Cresol (TCLP)
sw 646 method s2mwi0
<0.050 mg/L
05/15/2014
Hexachloro-1,3-butadiene (TCLP)
SW e46 method 82700510
<0.050 mg/L
05/15/2014
Hexachlorobenzene (TCLP)
SW 646 method 027(0510
<0.050 mg/L
05/16/2014
Hexachioroethane (TCLP)
SW ea method W013510
<0.050 mg/L
05/15/2014
m + p-Cresol (TCLP)
SW 60 method e2700510
<0.050 mg/L
05/16/2014
Nitrobenzene (TCLP)
SW 846 method b27ord510
<0.050 mglL
06/15/2014
o-Cresol (TCLP)
SW 846 method 627=510
<0.050 mg/L
05/15/2014
Pentachlorophenol (TCLP)
Sw 646 method 6278/3510
<0.050 mg/L
05/15/2014
Pyridine (TCLP)
sw e46 method 827a13510
<0.050 mg/L
05/15/2014
2,4,5-TP
SW846 Method 8151A
<0.0003 mg/L
05/19/2014
2,4-D
SW846 Method 8151A
<0.0003 mg/L
05/19/2014
1,1-Dichloroethylene
SW846meow SX015030
<0.01 mg/L
05/18/2014
1,2-Dichloroethane
SW846 Method e2 OW30
<0.01 mg/L
05/18/2014
Benzene
SW846 Method 826015030
<0.01 mg/L
05/18/2014

EnvironmentalEnvironmeAontal Chemists,
lace
6602 Wmdm'U Way - WAmm9t0n, NC 28405
envirochem,(910)
392-M (Lab) ® [phone] (Fax)
®
710 Bowsertown Road e Mantm NC 27954
[phone]
ANAL.rnCAL s CONSULTING
CHEMISTS
NCDENR: DWQ CBMECATE 494. DLS CERTIRCATE Q7729
Town of Wallace
Date of Report: Jun 19, 2014
316 E. Murray Street
Customer P® 6:
Wallace NC 28466
Customer ID: 09010063
Attention: Brent Dean, ®RC (WWTP)
Report #: 2014-05424
Project ID: WWTP Sludge
Carbon Tetrachloride
SW846 Method 8260/5030
<0.01 mg/L
05/18/2014
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg1L
05/16/2014
Chloroform
SVM6 Method SM015030
<0.01 mg/L
05/18/2014
Methyl ethyl ketone
Swre46 VAMW tt28015030
<0.05 mg/L
66118/2014
Tetrachloroethylene
Sw846 Method 626K030
<0.01 mglL
05/18/2014
Trichloroethylene
swea Method 826015030
<0.01 mg/L
05/18/2014
Vinyl Chloride
SW846 Method 8260/5030
<0.01 mg/L
05/18/2014
RCI
Cyanide
EPA 335A
<0.116 mg/kg
06/02/2014
pH
SM 4500 H s
7.50 units
05/15/2014
Sulfide
SM 40o s D
0.59 mg/kg
06/04/2014
Ignitabili
sl`%e sample bubbled out of app. Cup
sW 84s method 1010 >207 °F 05/21/2014
putting flame out and creating huge mess. Sample was repeated on 05-22 2014 and the some
thing happened @ 208dog.0
Sludge Residuals
Aluminum
EPA 200.7
9450 mg/kg
05/15/2014
Arsenic
EPA2W.7
<3.20 mg/kg
05/13/2014
Cadmium
EPA200.7
<320 mg/kg
05/13/2014
Calcium
CPA 200.7
26800 mg/kg
05/14/2014
Chromium
EPA 200.7
18.4mg/kg
05/13/2014
Copper
EPA 200.7
691 mg/kg
05/13/2014
Lead -
EPA 200.7
48.4 mg/kg
05/13/2014
Magnesium
EPA 200.7
2570 mg/kg
05/19/2014
Molybdenum
EPA 200.7
<3.20 mg/kg
05/13/2014
Nickel
EPA200.7
14.3 mg/kg
05/13/2014
Potassium
EPA 200.7
3360 mg/kg
05/19/2014
Selenium
EPA 200.7
4.38 mg/kg
05/13/2014
Sodium
EPA 200.7
4530mg/kg
05/14/2014
Zinc
EPA2W.7
1640 mg/kg
05/13/2014
Ammonia Nitrogen
EPA 35o.1
3920 mg/kg
05/12/2014

Environmental Chemists, Inc.
6602 Windmill Way ® Mninngton, NC 28405
[phone] (Lab) C [phone] (Fax)
® 710 Bowsertown Road • Manteo, NC 27954
(252) 473-57M
ANALYTICAL. & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CBRTIRCATE #37729
Town of Wallace
J
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Jun 19, 2014
Customer PO #:
Customer ID: 09010063
Report #: 2014-05424
Project ID: WWTP Sludge
Total Kjeldahi Nitrogen (TKN) EPA 351.2 39600 mg/kg 05/22/2014
Nitrate+Nitrite-Nitrogen EPA353.2 209mg/kg 05/30/2014 .
"Total Phosphorus sM 400 P F 19600 mg/kg 05/27/2014
Mercury SW8407471B 0.7930 mg/kg 05/28/2014
TCLP Metals
Arsenic
EPA 200.7
40.100 mg/L
05/15/2014
Barium
EPA 200.7
<0.100 mg/L
05/15/2014
Cadmium
EPA 200.7
<0.100mg/L
05/15/2014
Chromium
<=PA 200.7
<0.100 mg/L
05/15/2014
Lead
EPA 200.7
<0.100 mg/L
05/15/2014
Selenium
EPA 200.7
<0.100 mg/L
05/18/2014
Silver
EPA 200.7
<0.100 mg/L
05/16/2014
Mercury
EPA 245.1
<0.0020 mg/L
05/14/2014
Comment: Results reported on a try weight basis.
Reviewed by: /

Analytical & Consulting Chemists
ENVIRONMENTAL CI-ItIN-C _ OF 1 E,910'392.0223FAX91
-- - Wilmington, Ni. A wi5
0.392.4424
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
f%n1 1 CTlnnl AAlr% r`I.IAIAI nF M ICTC%nV.
Client: Town of Wallace WVVTP
PROJECT NAME: Sludge
REPORT NO:
ADDRESS:
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Jerry James, Public Works
email: bdean townofwallace.com
e.,.....1...1 Q... RAMPI F TVPE! I o Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludge. Other:
Sample identification -
Collection
e
m
°c
Eo o c7
u
_
o
o `oi
y E
m m
g z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Tam
w
z
v
x
+
N
s
so
z
ac
o
Sludge
C
P
X
I
Ifull
U, rci
O a
G
G
C
P
G
G
C
P—
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received`
Date/Time
Mlw
z.
Temperature hen Race v d: v`° W Accepted: V tKojectea: Kesampie eq eszea:
Delivered By. i Received By' Date: Time: 0
Comments: TU NAROUND:

-`Environmental
Chemists, Ineo
6602 Windmill MY c Wilmington, NC 2WS
'
L lip,
[phone] (Lab) - [phone] (Pax)
®
710 Bow►sertown Road . Manteo, NC 27954
[phone]
ANALYnCAL & CONSULTING
-- ' CHEMISTS
NCDBNR: DWQ CERTMCATE *K DIS CRRTIFICA'TE ii37729
Town of WallaceDate
of Deport: Aug 11, 2014
316 E. Murray Street
Customer PO #:
Wallace NC 28466
Customer ID: 09010063
I Attention: Brent Dean, ORC (WWTP)
Report: 2014-08658
Project ID: WWTP Sludge
- Lab ID Sample 10,
Collect Date/Time Matrix Sampled by
14-21400 Site: Sludge
7/21/2014 10:20 AM Solid/Sludge Derek Reed
Test
MethodResults
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
9460 mg/kg
07/28/2014
Arsenic
EPA200.7
<3.50 mg/kg
07/25/2014.
Cadmium
EPA 200.7
<3.50 mg/kg
07/25/2014
Calcium
EPA 200.7
24700mg/kg
07/31/2014
Chromium
EPA20D3
18.2 mg/kg
07/25/2014
Copper
EPA 200.7
804 mglkg
07/25/2014
Lead
EPA 200.7
62.1 mg/kg
07/25/2014
Magnesium
EPA2W.7
2470 mg/kg
07/31/2014
Molybdenum
EPA 200.7
5.32mg/kg
07/25/2014
Nickel
EPA 200.7
15.6 mg/kg
07/25/2014
Potassium
EPA2007
3040 mg/kg
07/31/2014
Selenium
EPA 200.7
6.18 mg/kg
07/25/2014
Sodium
EPA 200.7
6820 mg/kg
07/31/2014
' Zinc
EPA 200.7
1600 mg/kg
07/25/2014
Ammonia Nitrogen
EPASNA
1710 mg/kg
07/30/2014
Total Kjeldahl Nitrogen (TKN)
EPA351.2
39900mg/kg
08/01/2014
Nitrate+Nitrite-Nitrogen
EPA353.2
104 mg/kg
08/08/2014
Total Solids (%)
814 2MO a
2.80 %
07/23/2014
pH
su 400 It s
7.06 units
08/01/2014
Total Phosphorus
SM4WD P P
4190 mg/kg
08/01/2014
Mercury
$W"6 7471 a
0.7180 mg/kg
07/28/2014
Pmfto 4 of A

Analytical & Consulting Chemists
i M T
IENVIRuNM'EN-YAL L;HEWS B S■ NC
NCDENR: DWQ CERTIFICATION 4 94 NCDHHS: DLS CERTIFICATION * 37729
COLLECTION AND CHAIN OF CUSTODY
660_ .....mill .._, Nllm------- J. NC - ---_
OFFICE: 910.392.0223 FAX [phone]
[e-mail]
client: Town of Wallace WWTP
PROJECT NAME: Sludge
REPORT NO:
ADDRESS:
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Jerry James, Public Works
email: [e-mail]
Sampled by: I Ci SAMPLE
TYPE:1= Influent,
E = Effluent, W = Well, ST = Stream, SO = Sol], SL = Sludge, Other:
Sample Identification
Collection
E�A
v)
M
`o
o
U. ^,
C
`o
V
=
V
a
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Tam
_
z
x
"
g
a
o
o
p
Sludge
C
P
far
X
nutrients/metals
1- _/��
��
G
G
9
C
P
V401
X
fecal densi l %TS
G
G
2
C
P
LA
X
fecal density/ %TS
-7-Q / /L
I CID
G
G
3
C
P
its
X
I
Ifecal density/ %TS
7$1
®
G
G
4
C
P
vol
X
fecal densit / %TS
7 a )4q
I
G
G
5
C
P01
bt
X
fecal density/ %TS
7- J-1
a U
G
G
6
C
P
V�
X
fecal densi l %TS
-
1
G
G
7)
C
P
X
fecal density/ %TS
G
G�
C
P
G
G
Transfer
Relf ulshe By:
DateMme
Received By:
Datefrime
2.
Temperature when Received: 2- Accepted: a jected: Resample Req s d:
Delivered By. Received Bb; Date: 49 9'4 Time:
Comments: TURNAROUND:

n.virc ent Chem"sts, Inc®
( i 6W2 Windmill Way a Wilmington, NC 2&05
envirochem(910) 392-0223 (Lab) ® [phone] {Fax)
710 Bowsertown Road a Manteo, ITC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CE fIFICATE #9C DLS CERTIFICATE #37729
Town of Wallace Date of Report: Nov 14, 2014
316 E. Murray Street Customer PO #:
Wallace NC 28466 Customer ID: 09010063
Attention: Brent Dean, ORC (WWTP) Report #: 2014-13124
Project ID: WWTP Sludge
Laub ID
14-32262
Sample ID: Collect Date/Time Matrix Sampled by
Site: Sludge 10/23/2014 10:05 AM Solid/Sludge Derek Reed
Teat
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA200.7
15400mg/kg
11/05/2014
Arsenic
EPA200.7
<3.14mg/kg
11/03/2014
Cadmium
EPA200.7
<3.14 mg/kg
11/03/2014
Calcium
EPA20o7
31100 mglkg
10/30/2014
} Chromium
EPA700.7
21.3 mg/kg
11/03/2014
Copper
EPA200.7
749mg/kg
11/03/2014
Lead
EPA200.7
62.0mg/kg
11/05/2014
Magnesium
EPA 200.7
3060 mg/kg.
10/30/2014
Molybdenum
EPA200.7
5.75 mg/kg
11/03/2014
Nickel
EPA2007
17.5 mglkg
11/03/2014
Potassium
EPA200.7
3430 mg/kg
10/30/2014
Selenium
EPA200.7
9.76 mg/kg
11/05/2014
Sodium
EPA200.7
5230 mg/kg
10/30/2014
Zinc
EPA 200.7
1540 mg/kg'
11 /05/2014
Ammonia Nitrogen
EPA SMA
617 mg/kg
10/27/2014
Total ICjeldahl Nitrogen (TKN)
EPA351.2
40600mg/kg
10/28/2014
Nitrate+Nitrite-Nitrogen
EPA353.2
24.1 mg/kg
11/10/2014
ri Total Solids (%)
SM 2540 a
2.87 %
10/24/2014
pH
sm 45M H e
6.96 units
10/30/2014
Total Phosphorus
SM4500 P F
19900 mg/kg
10/28/2014
Mercury
SWU67471B
0.9480 mg/kg
11/11/2014
Pane 7 of 3

NC
ENVIRONMENTAL CHEMIST 59 INC OFFICE: ,910I392-02231FAX [phone]
NCDENR: DW® CERTIFICATION 0 94 NCDHHS: OLS CERTIFICATION 0 37729 [e-mail]
Analytical & Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
:lient: Town of Wallace WWWTP
PROJECT NAME: Sludge
REPORT NO: U41'
kODRESS-
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Jerry James, Public Works
email: bdean ownofwallace.com'-,
uvnr. =8A.....d w - w-ll air- C4va�m Cn = Snit d Al � Slune- nthar-
sarnpieci t5y:
7 r••' ' `c
.SAMPLE
c o
1 ErC:
_.
�`o
1 m Oulucell/
6 1.
L _
lu
z
"ulucny •• - ••vn,
PRESERVATION
v.
.y .. _..__ -tea-• -- ----
ANALYSIS REQUESTED
Sample Identification
Collection
Date
Time
Temp13
s
g
0
O
Sludge
X
nutrients/metals
/U-�3
lczS�
G'
G
C
P
?.1-4Z
X
fecal density/ %TS
G
G I
2
C
P
'7
X
fecal densi l %TS
/Cy0-{ Lf
lz;oc—
G
G
3
C
P
X
fecal densi / %TS
V�
G
G
4
C
P
X
fecal densi / %TS
G
G
C
P
X
fecal density/ °/6TS
G
G
6
C
P
X
fecal densi / %TS
/06;;)
� ��
G
G
7
C
P
�9
X
fecal density/ %TS
/O I
I�G r
G
G
C
P
G
G
Transfer
Reli cashed y:
Date/Time
Received By:
Date/Time
2.
_..
Temperature when Received: oS 1 Accepted: V
Delivered By: Received
%ewilmline r
Comments: r TU
D:

Environmental Chemists,
Inc.
7envirochern
6602 Windmill Way - Wiin dngton, NC 28405
[phone] (Lab) - [phone] (Fax)
710 Bowsertown Road - Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR DWQ CERTOCATE #94. DLS CERnFlCATE #37729
Town of Warsaw
Date of Report: Jul 09, 2014
P.O. Box 464
Customer PO #:
Warsaw NC 28398
Customer ID: 09070029
Attention: Greg Hughes
Report #: 2014-07045
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-17328 Site: Sludge
6/1612014 12:15 PM Solid/Sludge Client
Vest
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
18600 mg/kg
07/02/2014
Arsenic
EPA 200.7
<6.17 mg/kg
06/26/2014
Cadmium
EPA 20oa
<6.17 mglkg
0612612014
Calcium
ePA200.7
43900mg/kg
07/0212014
Chromium
EPA 200.7
34.0mg/kg
06/26/2014
Copper
EPA 200.7
636mglkg
07/01/2014
Lead
EPA260.7
54.1 mglkg
06/26/2014
Magnesium
EPA 200.7
2960mglkg
07/02/2014
Molybdenum
EPA 200-7
<6.17 mg/kg
07/07/2014
Nickel
EPA20o,7
26.5 mglkg
06/26/2014
Potassium
PPA 200-7
4970 mg/kg
07/02/2014
- Selenium
EPA 200.7
<6.17 mg/kg
07/01/2014
Sodium
EPA 200.7
5730 mg/kg
07/02/2014
Zinc
EPA20o.7
1380 mg/kg
07/01/2614
4 Ammonia Nitrogen
EPA 350.1
987 mg/kg
06/18/2014
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
72400 mg/kg
06/23/2014
Nitrate+Nitrite-Nitrogen
EPA 353.2
35.7 mg/kg
0710712014
Total Solids (%)
sM 2540 B
1.41 %
06/1712010
pH
$M4500 H B
6.64 units
06/18/2014
Total Phosphorus
sM 4600 P F
55300 mg/kg
06/2312014
Mercury
SW840 7471 B
1.49 mglkg
07/02/2014
Comment: Results, except pH, reported on a dry weight basis. pH on an as received basis.
Reviewed by:
reported
l&X-n A A
r
LJ Report #__ 201"7045
Page 1 of 1

Windmili Way
05
502
ENVIRONMENTAL CHEMISTS, [ N �i — I~: �OFFIC910.3924223 FiAX 910.302 "24
Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION #94 NCDHHS: DLS CERTIFICATION# 37129 [e-mail]
COLLECTION AN❑ CHAIN OF CUSTODY
CLIENT: 4er 'j
PROJECT NAME: - - - -
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONEIFAX:
COPY TO:
email:
Samrtlad RV! SAMPLE TYPE: I = Influent. E = Effluent. W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
F�
E°
o
V�
m
PRESERVATION
ANALYSIS REQUESTED
D e
Time
Temp
Z
a
o
0
0
o
w
S�
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
-d
I
G
G
C
P
G
0-
Transfer
Relinquished By:
Date/Time
Received By.
Date/Time
1.
2.
Temperature whea�g
: Z.D-C iAccepted: ✓
Delivered By: Receive
Ile Repluested:
lr �L c Time:
TURN ROUND:

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORTS

May 301410:16a Environmental Chemists
9103924424
P.1
Environmental Chehilsts,
Inc.
j•
6602 Windmill Way • Wilmington, NlC 28405
[phone] (Lab) s [phone] (Fax)
710 Bow5ertown Road • Manteo, NC 27954
ANALYTICAL & CON5UL71NG
[phone]
CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DES CEMTFICATE #37729
Town of Kenansville
Date of Report: Apr 07, 2014
PC Box 370
Customer PO 0:
Kenansville NC 28349
Report #: 2014-02550
Attention: Cary Benson
Report to: Carry Benson
Project ID: Sludge
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
14-06181 Site: sludge
3/5/2014
10:00 AM Solid/Sludge Client
Test
Method
Results Date Analyzed
Chlordane
SW046Meted 8081BI3610
<0.005mg/L
0311712014
Endrin
SW 846 Method 80811313510
<0.00005 mg/L
03/17/2014
_
l
Heptachlor
%V 846 Method 8081 B13510
<0.00005 mg/L
03117/2014
Heptachlor epoxide
SW 8461Jtethod 8081 B1351 0
<0.00005 mg/L
03/1712014
Lindane
SW 846 Method BOB1 B13510
<0.00005 mg/L
03/1712014
Methoxychlor
SW 846 Method 80818/3510
<0,00005 mg/L
0311712014
Toxaphene
SW 846 Method 5081813510
<0.005 mg/L
03117/2014
1,4-Dichlorobenzene (TCLP)
SW 846 method U70MIO
<0.050 mg/L
0311412014
2,4,5-Tdchlorophenol (TCLP)
SW 846 method 827013510
<0-050 mg/L
03/1412014
2,4,6-Trichlorophenol (TCLP)
SW 846 method B270/3510
<0.050 mg/L
03I1412014
2,4-Dinitrotoluene (TCLP)
SW 846 method 5270/3510
<0.050 mg/L
03JI412014
Cresol (TCLP)
SW 846 method827013510
<D.050 mg/L
03/1412614
Hexachlorc-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0,050 mg/L
03/1412014
Hexachlorobenzene (TCLP)
SW B46 method 8270/351 a
<0.050 mg/L
03/14/2014
Hexachloroethane(TCLP)
SW 846 method 8270/351 a
<0.050 mg/L
03114I2014
ID
m + p-Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
03/1412014
Nitrobenzene (TCLP)
SW 846 method wa13510
<0.050 mg/L
03/1412014
i
o-Cresol (TCLP)
SW 846 method 827ora510
<0.050 mg1L
03/14/2014
Pentachlorophenol (TCLP)
Sw 846 method 62 OMI0
<0.250 mg/L
03/1412014
Pyridine (TCLP)
SW 846 method 827a13510
<0-050 mg/L
03/14/2014
2,4,5_Tp
swath Method 8151A
<0,0003 mg/L
0311712014
2,4-01
SW846 Method 8151A
<0.0003 mg1L
03117/2014
I,1-Dichloroethylene
SW648Method 8260/5030
<0.01 mg/L
OW812014
1,2-Dichloroethane
SW846 Method 826015030
<0.01 mg/L
03/2812014
Benzene
SW848 method 8260/5030
<0.01 mg/L
03/2812014
Carbon Tetrachloride
SW846 Method 826015030
<0.01 mg/L
03/2812014
j
Repoa #:: 2014-02550
Page 1 of 3

May 30 1410:16a Environmental Chemists
9103924424 p.2
envirochem
kL
WA
.ANALYTICAL & CONSUL71NG
. CHEM[STS
Town of Kenansville
PO Box 370
Kenansville NC
Attention: Garry Benson
Chlorobenzene
Chloroform
Methyl ethyl ketone
Tetrachloroethylene
Trichloroethylene
Vinyl Chloride
RCI
Cyanide
Sulfide
Ignitability
Sludge Residuals
Aluminum
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Potassium
Selenium
Sodium
Zinc
Arsenic
Molybdenum
Nickel
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
N itrate+N itrite-Nitrogen
Total Solids (%)
Environmental Chemists, Inc.
6602 Windmill. Way - Wilmington, NC 28405
[phone] (Lab) - (910) 392-424 (Fax)
710 Bowsertown Road - Manteo, NC 27954
[phone]
NCDENR: DWQ CERTIFICATE 094. DLS CERTIFICATE #37729
Date of Report: Apr D7, 2014
Customer PO #:
28349 Report #: 2014-02550
Report to: Garry Benson
Project ID: Sludge
SW846 Method 8260/5030
SW846 Method 826mwo
SVV546 Method 8260/5030
SW846 Method 8260/5030
S%V8K6 Method 8260/503o
SW846 Method 8260/5030
EPA 335.4
SM 4500 S D
SW 846 method 1010
EPA 200.7
EPA 200.7
EPA 260.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 2o0.7
EPA 200.7
EPA 200.7
EPA 2D0.7
EPA 200.8
EPA 200.8
EPA 200.8
EPA 350.1
EPA 351.2
EPA 3532
SM 2540 8
<0.01 mg/L
<0.01 mg/L
<0.05 mg/L
<0.01 mg/L
<0.01 mg/L
<0.01 mg/L
<0.120 mglkg
<0.240 m g/kg
>212 °F
4170 mglkg
<5.46 mglkg
25700 mg/kg
12.2 mg/kg
273 mg/kg
16.6 mg/kg
1620 mg/kg
2520 mg/kg
<5.46 mg/kg
3660 mg/kg
561 mg/kg
<5.46 mg/kg
13.0 mg/kg
11.1 mg/kg
169 mg/kg
179DO mg/kg
2480 mg/kg
1.74 %
0312812014
03128/2014
0312812014
0312812014
03128/2014
0312812014
0410212014
04/0112014
03/1412014` _
03/1312014
03/10/2014
03/12/2014
03/10/2014
03112/2014
03114/2014
0311212014
0311212014
03/14/2014
03/1212014
03/10)2014
3/17/2014
311712014
3/17/2014
03/1412014
03/2612014
03/21/2014
03/10/2014
Repot #:: 2014-02550
Page 2 of 3

May 301410:17a Environmental Chemists 9103924424 p.3
Environmental Chemists, Inc.
1iL. envirochem6602 Windmill Way + Wilmington, NC 28405
[phone] (Lab) - [phone] (Fax)
710 Bowsertown Road • Nfanteo, NC 27954
ANALYTICAL & CONSULTING (2) 473 5702
CHEMISTS NCDENR DWQ,CERTIFIC.4TE *94. DLS CERTIFICATE #37729
Town of Kenansville
PO Box 370
Kenansville NC
Attention_ Garry Benson
28349
Date of Report: Apr 07, 2014
Customer PO #:
Report #: 2014-02550
Report to: Garry Benson
Project ID: Sludge
pH
sM 4500 H B
7.04 units
0311112014
Total Phosphorus
sM 4500 ;1 is
1140 mg/kg
04/03/2014
Mercury
Swage 74719
0.6320 mg/kg
03/19/2014
TCLP Metals
Arsenic
EPA200.8
<0.010mg1L
03/12/2014
- Barium
EPA200.8
0.070 mg/L
03/12/2014
Cadmium
EPA200.5
<0.010mg/L
03/12/2014
Chromium
EPA200.8
0.028 mg/L
03/1212014
Lead
EPA200.e
<0.010mg/L
03/12/2014
Selenium
EPA200.9
<0.010mg/L
03/1212014
Silver
EPA200.8
<0.010-mg/L
03/12/2014
Mercury
EPA245.1
<0.002mg/L
03/24/2014
Comment: Sludge residuals
results, except pH,
reported on a dry weight basis. pH and RCI reported on an as
received basis.
Reviewed
I
Report*: 2014-02550
Page 3ofa

• 6
Analytical & Consulting Chemists
I 1
.ENVIRONMENTAL CHEMISTS, I N C 0602 Windmill Way Wilmington, NC 28405
NCDENR: DWQ CERTIFICATION # 94 NCDHH9: DL5 CERTIFICATION # 3T729 OFFICE: 910.392-0223 FAX [phone]
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Town of Kenansville
PROJECT NAME: Annual Sludge REPORT NO:CL
ADDRESS:
CONTACT NAME: Garry Benson Po No:
REPORT TO; PHONE/FAX:
COPY TO: email:
9Date
Sampled By:
Sample identification
SAMPLE TYPE: I = Influent, E = Effluent; W = Well, ST = Stream, SO a Soil, SL = Sludge, Other:
Collection .. d x PRESERVATION
,p3° o= M m LUo o ANALYSIS REQUESTED
Time Tem C� u «1 z z z x y o
n
Sludge
SI
C
p
//
IQ i�
Full TCLP/RCl/Nutrients/Metals
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
c
aEi
j
G
G
C
P
G
G
o
L
C
P
G
C
G
P
G
G
Transfer
Relinquished By: Date/Time Received B p
co Y awlTime
` 1• � c• 3
2•
Temperature when Re eived:
Accepted: r Re' cte
Delivered By: '&.G �.�c« Resample Requested:
_ Received By: c r7 f LC'. �'•� Date: '3-�s 'i'j Time: 36C�
m Comments: TURNAROUND`

Environmental Chemists,
Inc.
_
envirochem
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) v [phone] (Fax)
®
710 Bowsertown Road • Manteo, NC 27954
[phone]
"
ANALYTICAL & CONSULTING
CHEMISTS
NCDENR: DWQ CERTIFICATE #94. DIS CERTIFICATE #37929
Town of Rose Hill
Date of Report: Jan 07, 2015
— J
P. O. Box 8
Customer PO #:
-
Rose Hill NC 28458
Customer ID: 09020035
Attention: Ben Hilliard
Report #: 2014-14986
Project ID:- Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-36714 Site: Sludge
12/3/2014 10:15 AM Solid/Sludge Ben Hilliard
Test
Method
Results Date Analyzed
Chlordane
Sw 646 Method e081ar3510
<0.05 mg/L
12/10/2014
Endrin
SW 846 Method 80818/3510
<0.0005 mg/L
12/10/2014
Heptachlor
SW846 Method 8081W510
<0.0005 mg/L
12/10/2014
Heptachlor epoxide
SW 846 Method 6081BM10
<0.0005 mg/L
12/10/2014
Lindane
SW 846 Method 8081M510"
<0.0005 mg/L
12/10/2014
Methoxychlor
SW 846 Method 6081e/3510
<0.0005 mg/L
12/10/2014
Toxaphene
SW 846 Method eo81813510
<0.05 mg/L
12/10/2014
1,4-Dichlorobenzene (TCLP)
6W64s me#W WW3510
<0.050 mg/L
12/11/2014
2,4,5 Trichlorophenol (TCLP)
SW 646 method 8270r3510
<0:050 mg/L
12/11/2014
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3610
<0.050 mg/L
12111 /2014
2,4-Dinitrotoluene (TCLP)
sW 64s method e2700510
<0.050 mg/L
12/11 /2014
Cresol (TCLP)
SW 646 method 827013510
<0.050 mg/L
12111 /2014
Hexachloro-1,3-butadiene(TCLP).
SW N6 Method 82TOM510
<0.050 mg/L
12/11/2014
Hexachlorobenzene (TCLP)
Swso method 827013510
<0.050 mg/L
12/11/2014
Hexachloroethane (TCLP)
SW 846 method 627013510
<0.050 mg/L
12/11/2014
m + p-Cresol (TCLP)
SW 646 method 8270r3510
<0.050 mg/L
12/11/2014
- ,
Nitrobenzene (TCLP)
sw646 method 6270r3510
<0.050 mg/L
12/11/2014
o-Cresol (TCLP)
sW Safi method 6270MIO
<0.050 mg/L
12/11/2014
Pentachlorophenol (TCLP)
SW 646 method 6270r3510
<0.250 mg/L
12/11/2014
1
Pyridine (TCLP)
SW846 method W70W10
<0.050 mg/L
12/11/2014
2,4,5-TP
SW846 Method 8151A
<0.003 mg/L
12/12/2014
2,4-D
SWM6 Method 8161A
<0.003 mg/L
12/12/2014
1,1-Dichloroethylene
SW846 Method 626015030
<0.01 mg/L
01/01/2015
1,2-Dichloroethane
SW846 Method 8MWO30
<0.01 mg/L
01/01/2015
Benzene
SW846 Method 826015030
<0.01 mg/L
01/01/2015
Carbon Tetrachloride
SWM6Method 826015030
<0.01 mg/L
01/01/2015
Report #:: =4-14086
Page 1 of 3

Environmental Chemists, Inc©
• • 6602 Windmill Way a Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 j
Town of Rose Hill
Date of Report: Jan 07, 2015
,
P. O. Box 8
Customer PO #:
' -
Rose Hill NC
28458
Customer ID: 09020035
Attention: Ben Hilliard
Report #: 2014-14986
{
Project ID: Sludge
Chlorobenzene
SW846 Method 826015030
<0.01 mg/L
01/01/2015
Chloroform
SW846 Method 828015030
<0.01 mg/L
01/01/2015
Methyl ethyl ketone
swa4s Method =015030
<0.05 mg/L
01/01/2015
Tetrachloroethylene
swe48 Method 828015030
<0,01 mg/L
01 /01/2015 -
Trichloroethylene
SW848 Method 8260/5030
<0.01 mg1L
01/01/2015
Vinyl Chloride
SW848 Method 8260/6030
<0.01 mg/L
01/01/2016
RCI
Cyanide
-EPA335A
0.137mg/kg
12/19/2014
Suffide
SM 4500 S o
2.68 mg/kg
12/17/2014
Ignitability
SW 848 method 1010
>212 OF
12/17/2014
Sludge Residuals
Aluminum
EPA200.7
4900 mg/kg
12/09/2014
i
Arsenic
EPA200.7
<6.33 mg/kg
12/05/2014
Cadmium
EPA200.7
<6.33 mg/kg
12/05/2014
Calcium
EPA2W.7
40600mg/kg
12/11/2014 1
Chromium
EPA 200.7
33.1 mg/kg
12/05/2014
Copper
EPA200.7
627 mg/kg
12/16/2014
Lead
EPA200.7
24.9 mg/kg
12/05/2014
Magnesium
EPA200.7
1660 mg/kg
12/11/2014
Molybdenum
EPA 200.7
<6.33 mg/kg
12/05/2014
Nickel
EPA200.7
18.1 mg/kg
12/05/2014
Potassium
EPA200.7
3230 mg/kg
12/11/2014
Selenium
EPA 200.7
11.0 mg/kg
12/05/2014 ; -.
Sodium
EPA200.7
2710 mg/kg
12/11/2014
Zinc
EPA 200.7
1040 mg/kg
12/05/2014
Ammonia Nitrogen
EPA 350.1
1040 mg/kg
12/10/2014
Total lgeldahl Nitrogen (TKN)
EPA 351.2
61700 mg/kg
12/12/2014
Nitrate+Nitrite-Nitrogen
EPA 3532
180 mg/kg
12/15/2014
Total Solids (%)
SM 2540 B
1.58 %
12/08/2014
pH
SM 4500 H S
7.23 units
12/05/2014
Report #:: 2014.14985
Page 2 of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
-bibs.,® 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTTRCATE #37729
Town of Rose Hill Date of Report: Jan 07, 2015
P. O. Box 8 Customer PO #:
Rose Hill NC 28458 Customer 1D: 09020036
Attention: Ben Hilliard Report #: 2014-14986
Project ID: Sludge
Total Phosphorus SM 4500 P F
Mercury SW846 7471e
TCLP Metals
23500 mg/kg 12/12/2014
6.96 mg/kg 12/05/2014
Arsenic
EPA200.8
<0.100mg/L
12/15/2014
Barium
EPA200.8
<0.100mg/L
12/16/2014
Cadmium
EPA200.8
<0.100mg/L
12/15/2014
Chromium
EPA200.8
<0.100 mg/L
12/16/2014
Lead
EPA 200.8 •
<0.100 mg/L
12/16/2014
Selenium
EPA200.8
<0.100mg/L
12/15/2014
Silver
EPA 2W.8
<0.100 mg/L
12/15/2014
Mercury
EPA 245.1
<0.002 mg/L
12/17/2014
I
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: --ye- 2AL
Report#_: 2OW14986 Page 3 01.3

Analytical l£ Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC OFIC :910-3s 223FAX970. 92"2lmington, NC 4
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Town of Rose Hill
PROJECT NAME: Sludge
REPORT NO:
ADDRESS:
CONTACT NAME: Ben Hilliard, ORC
PO NO:
REPORT TO:
PHONEIFAX:
COPY TO:
email -
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
a `a
0
6
$ a
J
o f
"
m
g Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
i
=
ro
�+
c
ic
°
Sludge
C
P
ow
X
Full TCLP, Nutrientstmetals, RCI
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relln shed BY:
Dajefflme
Recely d By,
D e/Time
1.
A
2.
Temperature when Received: ' o Accepted: ale t d• Resample Re ed:
Delivered By: Q/3 Received By: Date: f Tirne:
Comments: TURN OUND:

-'0 "Y i C "I'D r- 11V Mlpflof
;I; U *I I VIC,
91103024424 j'..' A
Environal Chemists, Inc.
me Mal
WAY N:1C 26,'05
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AhAtYl'.,CAL 9 C.0145t)j,rjt.G
4,-.3-57W
cli E4't S I s'
Southwest Plantation - Bear Trail Golf
Date of Report. Occ 25 2014
1 n 63 -acks.o StCFE- Road
C Ustomer PO IN:
NC 7 1.4
Customer In: 1 b0400055
kcpor% 2014-1001t1
Project 10:
Lab 10 sample 10:
Collect 0210i7ime Matrix Sampled by
4 -' .30078 Site: S'ajd-no
d?S.udp rt Sla-OeV Mellor
Test
Wthod
Date Analyzed
v
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runvironmental Chemists., Inc.
vm-- 4, •INC- U-wts
PVVQIc: Y : IF![
S011thwe-st Plantation - Bear
Ttail Golf
Date of Report-. Dec 25 2014
163 .-�BNSor 'S'to,v Road
c-'istuaw PO 4..
Sculavi'le .44 C'
o- M" I E
Cu Storner )0: 1004DOC-�
Report 0: 2:14-141.471
Project ID, Slidge
..hicynbanzene
1 2 Y20 14
­10 01 Mck"I
12. '1."'
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ine,
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CMAUSTS
"0'
".0uthwelt Plantation Sear Trail Golf
Date of Report: eY 28, 2o' 14
163 .-3-`kkCn Stwe RN�>ad
Custanwr POM
zi
28-
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customer)D: 1040'
AIAllion SIvIe. U., eT
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t-
ENVIRONTIMENTAL CHEN ISTS. INC
Sam le Coltecteon :�n._d in of Cic�ttidv
6f;gz ti`intimiii NN'A►'
Plana: (9191392-0123
Fax (910) -392.4421
Creek ltc�a .laekaanvll#c C 28540 9 Ma2d (1�
Rrnartv___ 7 i-ft
c.0iterten 11t ;;
t� -Weil si = t'rcam so -; nil.. _ n e-
�3m is T ' e: # - #nil . nt L f'Ructct ! PR1Y„SERVATION
G1 Collection = j g rl C: 5 „i 1 i G q!di.l'5I5itt96
l6�f.ST'F�
Lion! ' " F-
ample 6drnti�ica —r — ..,— '
DATE : TE: tP
TS
Near Trait Calf -��
x IN
L iff Pll:.
Fecal rulitarm
I/Month sampling
4L:
-- — — _ _ • _— i Ix
Chloride
�.ti troaccnurele (durMarch, J.*. November)
-
-
Ir
f �
S(}I) lianit is 10 (tcrnathh°t. L + (dilly): Fetal timi! ie 14 (an0atht!r), y4 (dicit�}; K tantisly), 6 (daily)-.'P.. — —
... v d BDerl'ime
—� li}.; �U:itrll'iroc ` tteeci v: e � _..�� _ �-.�,.---- --
Trari�fer I lte#in uislscd q
Temp erattsre when Rete 'ed: �� Accej�ted:�o.- . R'�je - L _Circe•
Delivered B. _ — RCCet & ,

iv,nvironnmental Chemists, Inc.
"02 Windmill Way o Wilmington, NC 28405
[phone] (lAb) c (910) 3924424 (Fax)
® 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS WIDEN& DWQ CER'T'IRCATE Ot DTS CERTIRCATE#37729
Town of Wallace Date of Report: Jun 19, 2014
316 E. Murray Street Customer PO M.
Wallace NC 28466 Customer ID: 09010063
Attention: Brent Dean, ORC (WWTP) Report#: 2014-05424
Project ID: WWTP Sludge
Lab ID Sample ID:
14-13113 Site: Sludge-TCLP
Test
Collect Date/Time
5/9/2014 9:43 AM
Method
Matrix Sampled by
Solid/Sludge Client
Results Date Analyzed
Total Solids (%)
SM 2540 a
2.56 %
05/12/2014
Chlordane
SW e46 Method W818i3510
<0.005 mg/L
05/16/2014
Endrin
SW 846 Method $081813510
<0.00005 mg/L
05/16/2014
Heptachlor
SW w Method 80818l3610
<0.00005 mg/L
05/16/2014
Heptachlor epoxide
SW 8" meow 80811IM10
<0.00005 mg/L
05/16/2014
Ldndane
SW U6 Method e0a18/3510
<0.00005 mg/L
05/16/2014
Methoxychlor
sw e46 Method OOBI P3510
<0.00005 mg1L
05/16/2014
Toxaphene
Swso Method W8181351a
<0.005 mg/L
05/16/2014
1,4-Dichlorobenzene (TCLP)
Swea meamd s270r3510
<0.050 mg/L
05/15/2014
2,4,5 Trichlorophenol (TCLP)
SW 84s meovod 827=10
<0.050 mg/L
05/15/2014
2,4,6 Trichlorophenol (TCLP)
SW W6 method 6270t$510
<0.050 mg/L
05/15/2014
2,4-Dinitrotoluene (TCLP)
Sw846 method 927CM10
<0.050 mg/L
05/1512014
Cresol (TCLP)
SW 646 method 6270r3510
<0.050 mg/L
05/15/2014
Hexachloro-1,3-butadiene (TCLP)
SW W method eVOI3510
<0.050 mg/L
05/15/2014
Hexachlorobenzene (TCLP)
Sw 848 method WOM510
<0.050 mg/L
05116/2014
Hexachloraethane (TCLP)
SW 846 method OV013510
<0.050 mg/L
05/15/2014
} m + p-Cresol (TCLP)
SW 848 method 827013510
<0.050 mg/L
05/15/2014
Nitrobenzene (TCLP)
SW 846 method 627MI0
<0.050 mg/L
05/15/2014
o-Cresol (TCLP)
SW e46 method 8271113510
<0.050 mg/L
05/15/2014
Pentachlorophenol (TCLP)
SW 84s method s27aM10
<0.050 mg/L
05/15/2014
Pyridine (TCLP)
SW US method 827035W
<0.050 mg/L
05/15/2014
2,4,5-TP
SW848 Method 8151A
<0.0003 mg/L
05/19/2014
2,4-D
SW846 Method 8151A
<0.0003 mg/L
05/19/2014
1,1-Dichloroethylene
Sw846Method OM15030
<0.01 mg/L
05/18/2014
1,2-Dichloroethane
St AKG Method U6015030
<0.01 mg/L
05/1812014
Benzene
SWe46 Method 826015030
<0.01 mg/L
05/18/2014
_ ... ..__
a....e..Fa

[enviroche7m]:
ANALYTICAL & CONSULTING
CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way o Wilmington, NC 28405 r
(910) 392-= (Iab) • [phone] (Pax) ;
710 Bowsertown Road • Manteo, NC 27954
[phone]
NCDENR-. DWQ CERTFICATE 094. DLS CER7MCATE *37729
Town of Wallace
Date of Report: Jun 19, 2014
316 E. Murray Street
Customer PO #:
Wallace NC 28466
Customer ID: 09010063
Attention: Brent Dean, ORC (WWTP)
Report#: 2014-05424
Project ID: WWTP Sludge
Carbon Tetrachloride
SWM Method 8260/5030
<0.01 mg/L
05/18/2014
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
05/18/2014
Chloroform
SWe46 Memos 826015030
<0.01 mg/L
05/18/2014
Methyl ethyl ketone
sw646 AWUM 8MU030
<0.05 mg/L
05/1812014
Tetrachloroethylene
swan Memos 82MO30
<0.01 mg/L
05/18/2014
Tdchloroethylene
sYM6 Method 82W/5030
<0.01 mg/L
05/18/2014
Vinyl Chloride
SW846 Method 626OW30
<0.01 mg/L
05/18/2014
iRCI
Cyanide
EPA 335.4
<0.116 mg/kg
08/02/2014
pH
SM 4500 H B
7.50 units
05/15/2014
Sulfide
SM 4500 S o
0.59 mg/kg
08/04/2014
lgnitability
sw ers methoa io�o
�207 °F
05/21/2014
slu a sample bubbled out of app. Cup putting flame out and creating huge mess. Sample was repeated on Orr22 20i4 and the same
thing happened @ 208deg.0
Sludge Residuals
Aluminum
EPA2W•7
9450mg/kg
05/15/2014
Arsenic
EPA200.7
<3.20 mg/kg
05/13/2014
Cadmium
EPA 200.7
<3.20 mg/kg
05113/2014
Calcium
EPA 200.7
26800 mg/kg
05/14/2014
Chromium
EPA 200.7
18.4mg/kg
05/13/2014
Copper
EPA 200.7
691 mg/kg
05/13/2014
Lead
EPA 200.7
48.4 mg/kg
05/13/2014
Magnesium
EPA2001
2570 mg/kg
05/19/2014
Molybdenum
EPA 200.7
<3.20 mg/kg
05/13/2014
Nickel
EPA200.7
14.3mglkg
05/13/2014
Potassium
EPA 200.7
3360 mg/kg
05/19/2014
Selenium
EPA 200.7
4.38 mg/kg
05/13/2014
Sodium
EPA 200.7
4530mg/kg
05/14/2014
Zinc
EPA 200.7
1640mg/kg
05/13/2014
Ammonia Nitrogen
EPA 350.1
3920 mg/kg
05/12/2014

I
-�Envwonmental Chemists, Inc.
6602 WmdmW Way • Wilmington, NC 28405
[phone] (Lab) s [phone] (Fax)
® 710 Bowsertown Road • Manteo, NC 27954
[phone]
j ANALYTICAL & CONSULTING
! CHEMISTS NCDENP. DWQ CBRTISCATE 494. DIS CBRTfflCATE #i37729
Town of Wallace Dane of Report: Jun 19, 2014
316 E. Murray Street Customer PO #:
Wallace NC 28466 Customer ID: 09010063
Attention: Brent Dean, ORC (WWTP) Report #: 2014-05424
Project ID: WWTP Sludge
Total lyeidahl Nitrogen (TKN) EPA 351.2 39600 mg/kg 05/22/2014
Nitrate+Nitrite-Nitrogen EPA 353.2 209 mg/kg 05/30/2014
Total Phosphorus SM 4500 P P 19600 mg/kg 05/27/2014
Mercury Sw8467471B 0.7930 mg/kq 05/28/2014
TCLP Motels
Arsenic
EPA 200.7
<0.100 mg/L
05/15/2014
Barium
EPA 200.7
<0.100 mg/L
05/15/2014
Cadmium
EPA 200.7
<0.100mg/L
05/15/2014
Chromium
EPA 200.7
<0.100 mg/L
05/15/2014
Lead
EPA 200.7
<0.100 mg/L
05/15/2014
Selenium
EPA200.7
<0.100mg/L
05/15/2014
Silver
EPA 200.7
<0.100 mg/L
05/15/2014
Mercury
EPA 245.1
<0.0020 mg/L
05/14/2014
Comment Results reported on a qry weight basis.
Reviewed by:
aannd g-1 2MA.nae9e Pace 3 of 3

'' 660z windmill roay Wilmmgzon, NC AGRUO
ENVIRONMENTAL CHEMISTS, INC OFFICE, 910-392-0223FAX[phone]
Analytical & Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Town of Wallace WWTP
PROJECT NAME: Sludge
REPORT NO:
ADDRESS:
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PRONE/FAX: [phone]
COPY TO: Jerry James, Public Works
email: [e-mail]
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
v
x
E `o
d ,.,
`o
o f
00
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
o
c
o
W
Sludge
C
P
��J
X
full U, rci
S-i�
0 3
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C-
P
I
G
d.
G
Transfer
Relinquished By:
DatelTime
Receiv&
DatelFlme
2.
Ap
Temperature Khen Rece v d: o'C0 tp Accepted: ejected: Resample eq ested:
Delivered By. Receivei Date: 51011 A Time: 0
Comments: ITURNAROUND;

PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORMS
I

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The Town of Rose Hill, Town of Kenansville, Town of Beulaville, Town of Warsaw, and
Southwest Plantation meet pathogen reduction and vector attraction reduction requirements through
lime stabilization. The Town of Wallace met pathogen reduction through fecal density and vector
attraction reduction through injection.

ANNUAL. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Beulaville WWTP
Monitoring Period: From 1/1/2014 To
WQ Permit Number: WQ0030998
NPDES Number: NCO026018
12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative pertormi
Class A: LAlt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑
Alt.D (N Test o Prior ® Process to Further Reduce Pathogengs ❑
)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray L] Pasteurization
Class B: Alt. (1) Fecal Density ® r Alt. (2) Process to Significantly Reduce Pathogens p
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying ❑ Com osting ❑ Aerobic Digestion
Aner Digestion
a obic i es ion If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen Density umer oFrequency Sample
Parameter in Sludge Excee- of Analysis Type
g im Geo. Mean aximu Units r�anrPe
2 x 10 to the MPN
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
Jrnonella bactena 3 AWN per 4 grams
(in lieu of fecal I total solid (dry
Vaetnr Altraetinn RPrinefinn 11SA N(`Ar W..T _11071 - Pleace. indicate alternative nerfarmed:
Tech-
Alt.1 (VS reduction) ®
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) ❑
1
Alt. 4 (Spec. 02,uptake) ❑
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CEKFIF1CATlON STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector, attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am awar that there are
significant penalties for false certification including fine and imprisonment."
J Mr. Stanley Miller, WWTP ORC -
Preparer ame and Title (type or print) Land Applier N m and Title i applicable)(type or print)
Signature of repa r* Date Signa re of Land Applier (if ap licable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
nr=mP FC1R1%A P\/P1= ()9T /19/9(111R1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
T Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Kenansville WWTP NPDES Number: NCO036668
Monitoring Period: From 1/1/2014 , To 12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)
A e n
gs r Reduce Pathog
It D o Prior Tes
t) Process
to Further
........................:::..::::.:...
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
................. .
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta RayGamma Raysteu Parization
Class B: Alt. (1) Fecal Density ® Alt. (2) Process to Sigqficantly Reduce Patho ens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El Air Drying ❑ composting ❑ Aerobic Digestion
ae bi stion An ro c Di e El .....:.....:. „ .,............. .
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen Density Number o Frequency Sample Analytical
Parameter Excee-
in Sludge MinimumGeo. Mean MaximumUnits of Analysis Type Tech-
ninne
2 x 10 to the MPN
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
Salmonella bacterial 3 MPN per 4 grams
(in lieu of fecal total solid (dry
coliform weight)
Vertnr Aurae- inn Reductinn WrNA NCAC 02T _1107) - Please indicate alternative nerformed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization B
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
y vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
IMr. Garry Benson, WWTP ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
SignaturPof Prepare? Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
r1FNR Pr)PKA P\/RF n9T ti 9/9nns1

ANNUAL. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Rose Hill WWTP NPDES Number: NCO056863
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (15A NCAC 02T .110
Class A: Alt. A (time/temp)
.................................... .
A1t.D (No Prior Test)
If applicable to alternative performed (Class A
Compost ® Heat Drying
Beta RayGamma Ray
Class B: Alt. (1) Fecal Density
If applicable to alternative performed (Class B
Lime Stabilization El Air D
Anaerobic Dry
aerobc i estion
If applicable to alternative performed (Cla
Parameter Allowable Level
in Sludge Minimum
2 x 10 to the MPN
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
off total solid (dry
dnionella bacteria 13 MPN per 4 grams
(in lieu of fecal total solid (dry
6) - Please indicate level achieved and alternative pertormi
Alt B (Alk Treatment) El I Alt. C (Prior Testing) 13
Process to Further Reduce Pathogengs El
only) indicate "Process to Further Reduce Pathogens":
Heat Treatment ® Thermophilic
Pasteurization
Alt. (2) Process to Significantly Reduce Patho ens El
only) indicate "Process to Significantly Reduce Pathogens":
ing 11 Composting ® J Aerobic Digestion
ss A or Class B) complete the following monitoring data:
Pathogen Density NumnerotiFrequency Sample
Excee- of Analysis T e
Geo. Meanaximu Units drnrPc yP
Vnn+nr Af+rarlinn Rarinrtinn 11SA N!`AC' 0?.T _11(171 _ Please indicate alternative performed:
Tech-
Alt.1 (VS reduction) ®
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) ®
Alt. 4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) D
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) ®
Alt. 8 (Drying - Unstable) Q
Alt. 9 (Injection) 11
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed El
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
Ll vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Ben Hilliard, WWTP ORC
Prepare r Name d Title ( e or print) Land Applier Name and Title (if applicable)(type or print)
,Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Southwest Plantation WWTP
Monitoring Period: From 1/1/2014 To
WQ Permit Number: WQ0030998
NPDES Number: WQ0029601
12/31/2014
liogen Recluction (15A .NUAU U21' .11U6) - Ylease maicate ievei acnievea ana anernanve performeu:
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑
ce
Process
to Further Redu Pathogen lt. o Prior Test
®
A D
g gs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ElHeat Drying ElHeat Treatment ❑ Thermophilic ❑
Pasteuriz
ation Pas
Beta Ray Gamma Ray ❑
y
Class B: Alt. (1) Fecal Density ® Alt. (2) Process to Significantly Reduce Pathogens R1
If applicable to alternative performed (Class B only) indicate `Process to Significantly Reduce Pathogens":
Lime Stabilization Air D in ❑ Composting ® Aerobic Digestion ❑
Anaerobic ti ae obic Di es 'on
..:..............................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter Allowable Level Pathogen Density uni eeExc° Frequency Sample AnaiytiTech-
in Sludge 'nimu Geo. Mean aximu Areneee Units of Analysis Type
ni
Fecal Coliform
(in lieu of fecal
2 x 10 to the MPN
6th power
per gram of total solids CFU
1000 mpn per gram
of total solid (dry
.WIN per 4 grams
total solid (dry
Veetnr Attractinn Reduction (15A NCAC 02T .11071- Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) ®
Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMEMU (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Stanley Miller, WWTP ORC ez ac_
Preparer Name and Title (type or print) Land Applier me and tle (if applicable)(type or print)
--' r
Signature qTWeparer* Date , Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
nF=1%1P Pr)PRA P\/RF n9T (17/9nnA1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NCO020702
Monitoring Period: From 1/1/2014 To 3/31/2014
athogen Reduction (15A NCAC 02T .110f
Class A: Alt. A (timehemp) ❑
................................
Alt.D No Prior Test) ❑
applicable to alternative performed (Class A
ompost ❑ Heat Drying ❑
eta Ray ® I Gamma Ray ❑ 4
Please indicate level achieved and alternative perforn
Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑
Process to Further Reduce Pathogengs ❑
n1y) indicate "Process to Farther Reduce Pathogens":
Heat Treatment ❑ Thermophilic ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density El
F Alt. (2) Process to Significantly Reduce Patho ens ❑
If applicable to alternative performed (Class B only) indicate "Process.to Significantly Reduce Pathogens":
Lime Stabilization ®
Air Drying ❑ I
Composting ❑'
Aerobic Digestion
b' i estion
Anaerobic is D
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Towable Level
in Sludge
Pathogen Density
Number o
Excee-
encesType
Frequency'
of Analysis
Y
Sample
T emoue
Analytical
Minimu
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
66,930
'
119,410
'
196,079
'
MPN/
Gram
0
Quarterly
Grab
SM 9221
C,E
CFU
1000 mpn per gram
of total solid (dry
ISalmonella bactej
(in lieu of fecal
VIM per 4 grams
total solid (dry
vantnr Affrartinn RPrinrtinn 115A NrAC 07T _1107)- Please indicate alternative nerformed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ®
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ®
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMEN'I' (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Brent M. Dean, WWTP ORC
Preparer Name aitijitle (type or print) Land Applier Nad Titl applicable)(type or print)
2' � � me
Signature of Preparer* Date Signature of Land Applie'r (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NCO020702
Monitoring Period: From 4/1/2014 To 6/30/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ®
Alt. C (Prior Testing)
Alt .D o Prior Test) ®
Pr a o e s ocess to Further Reduce P th n
g g
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ®
Heat Treatment ®
Thermophilic ®:
Beta Ray
Gamma RayPa
zation
steurization
Class B:
Alt. (1) Fecal Density El
Alt. (2) Process to Significantly Reduce Pathogens ❑
.................. .
If applicable to alternative performed_ (Class B only) indicate `Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
1 Aerobic Digestion
e obic Digestion Anaerobic
............................................... .
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
um er o
Excee-
Frequency
of Analysis
Y
Sample
Type
a ica
Tech -
niaue
Minim
Geo. Mean
axim
UnitsenceR
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
105,264
190,158
319 149
MPN/
Gram
0
Quarterly
Grab
SM.9221 C
E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC
02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2. (40-day bench) ®
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying.- Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty 'of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
y vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to .determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment." ,
Mr. Brent M. Dean, WWTP ORC
Pre arer Name and Title (type or print)
2—z• e5
Signature of Preparer* Date
Land Applier Na e and T' (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40, CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DFNR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NCO020702
Monitoring Period: From 7/1/2014 To 9/30/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Class A=
Alt. A (timehemp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
>'
AltEl
'oTest) ®
J) o Prr r
er en t FurthReduce Patho
Process o F
r g gs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost DI
Heat Drying ❑
Heat Treatment ❑
Thermophilic
Beta Ray El
Gamma Ray❑
z
Pasteurization
Class B:
JAlt. (1) Fecal Density El
Alt. (2) Process to Significantly Reduce Pathogen
............
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion
b'rc Dr e r
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um er ot
Excee-
Frequency
of Analysis
Sample
Type
An a ica
Tech -
ninue
Minimum
Mean
Maximum
Unitsenc
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
9,267
15,225
31,035
MPN/
Gram
0
Quarterly
Grab
SM 9221
C E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Verf-nr Attrnetinn Redurtinn (15A NCAC
02T .11071- Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAlt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ®
1 Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ll
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Brent M. Dean, WWTP ORC
Preparer N e and Title (type or print)
2- I
Signature h Preparer* Date
Land Applier Name and Titl f applicable)(type or print)
J
Signature of Land Applier (k applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF-02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NCO020702
Monitoring Period: From 10/1/2014 To 12/31/2014
hogen Reduction (15A NCAC 02T .11
Class A: Alt. A (tune/temp)
............................
A1t.D (No Prior Test)
aplicable to alternative performed (Class
apost ® Heat Drying
i Rav ® Gamma Rav
Class B: I Alt. (1) Fecal Di
pplicable to alternative perforn
le Stabilization
i aerobic Digestion
applicable to alternative perf
Parameter Allowable Level
in Sludge
Fecal Coliform
2 x 10 to the MpN
6th power
per gram of CFU
total solids
1000 mpn per gram
of total solid (dry
.lmonella bacterial 3 WN per 4 grams
(in lieu of fecal total solid (dry
06) - Please indicate level achieved and alternative F
Alt B (Alk Treatment) ® I Alt. C (Prior Testis
® I Process to Further Reduce Pathogei
A only) indicate "Process to Further Reduce Pathogens"
Heat Treatment ® I Thermophili
Pasteurization
sity [] I Alt. (2) Process to Significant.
d (Class B only) indicate "Process to Signil
Air Drying ® Compostir
med Class A or Class B complete the
Pathogen Density
4inimurn Geo. Meanj Maximum Units
169,492 437,107 1,347,369 WNN/ GraI
Reduce Pathogen
antly Reduce Patl
® lAerobic
•formed:
lowingmonitorin data:
umuer or Frequency Sample a �c Ex
Excee- of Analysis Type Tech-
APnePs Yp nimie
0 I Quarterly I Grab I SM 9221
CE
Veetnr Attraction Rednetian 115A NCAC 02T .11071 - Please indicate alternative nerformed:
Alt.1 (VS reduction) ®
Alt. 2 (40-day bench) El
Alt. 3 (30-day bench) ®
jAlt. 4 (Spec. 02 uptake)
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization®
Alt 7 (Drying - Stable) 13
1 Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) El
Alt. 10 (Incorporation) ®
No vector attraction reduction alternatives were performed El
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Brent M. Dean, WWTP ORC Mr. Eric R. Smith, Land Applier
Pre arer Name 4MTitle (type or print) Land Applier Name nd Title i pplicable)(type or print)
2-2-I5, /5
Signature of Preparer* Date Signature of Land Applier rif applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
L
nFNR FnRM P\/RF n9T /17/gnns)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
�a Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
- WWTP Name: Town of Warsaw WWTP NPDES Number: WQ0021903
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative pertormea:
Class A:, Alt. A (time/temp) D Alt B (Alk Treatment) D Alt. C (Prior Testing) D
0 en s
Reduce ath Process t o Further Red P
t Pr
'o es oPn Prior g A1t.D ® g El
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost D Heat Drying D Heat Treatment D Thermophilic ®
a Ray
Pasteurization
Beta Ra ® Gamm
Class B: lAlt. (1) Fecal Density D Alt. (2) Process to Sipificantly Reduce Patho ens El
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Ia Air Drying D T Composting D Aerobic Digestion D
Anaerobic Digestion
n If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen Density um er ot Frequency Sample Analytical
Parameter in Sludge Excee- of Analysis encesType Tech-
g inimu Geo. Mean aximu Units Y T enioue
2 x 10 to the MPN
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
Imonella bacteria 13 MPN per 4 grams
(in lieu of fecal total solid (dry
vo..+nr Aff-vad•4inn U.-thietinn 11SA iVrAr 02T _11f171- Please indicate alternative performed:
Alt.1 (VS reduction) D
Alt. 2 (40-day bench) D
Alt. 3 (30-day bench) D
Alt. 4 (Spec. Oz uptake) D
Alt. 5 (14-Day Aerobic) D
Alt. 6 (Alk. StabilizationB
Alt 7 (Drying - Stable) D
Alt. 8 (Drying - Unstable) D
Alt. 9 (Injection) D
Alt. 10 (Incorporation) D
No vector attraction reduction alternatives were performed D
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
D "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Greg Hughes, WWTP ORC
Pre arer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
JA
Signature o Prepares* Date . Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
nr-mp t:nPRA P\/RF n7T /17/9nnA)

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
Ci

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
` The Town of Rose Hill, Town of Kenansville, Town of Beulaville, Town of Warsaw, and
Southwest Plantation meet pathogen reduction and vector attraction reduction requirements through
lime stabilization. The. Town of Wallace met pathogen reduction through fecal density and vector
attraction reduction through injection. Documentation of these activities are found in the following
section.
1

—rb f.Pit6S FARMS Off" B UL �q U 4- L
WQQ000455 ALKALM STABILIZATION OF WASWWATM BIOSOUMS
Batch Size (gallons) Lbs. of Lim® d (�
'mono
a
man
OEM
mmmm,
mm�
mmmm
Comments: _ DAM, �,�. i `� SOURCE
e0
O
3cnm,
O
e1; _
O
ry
0
Q
^
O
w
OQ
NO
OO
O,
p
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®
O
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C
O
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U
0
-
Q. o a ao
u�f N1 9n N1 M M M M
f"�

f
TQf.P FARMS i9F B6 UL�qU: t�1-r
WQ000045S ALK&LM ST"HnAUON OF WASTEWATER BiOSOLMS
Batch Size (gallons) 0 o Lbs. of Lime ,
comments: - DATE l - / �1 �{ SOURCE .
O O CS O
OM,
O
H
O
N
IN,
Q
O
OO
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lY
N
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h
N
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..�i
.�i
O

Temp °C
Correction
0
Factor
co
i
Plus 0.45
Plus 0.42 i
Plus 0.39
t
Plus 0.36
Plus 0.33
i
i
Plus 0.30 i
i
Plus 0.27
t
Plus 0.24
Plus 0.21
Plus 0.18 i
Plus 0.15
Plus 0.12 j
'
40
39
38
37
36
35
34
33
32
31
30
29
d
28
Plus 0.09
Plus 0.06
CO
UN
27
i
26
Plus 0.03 i
1
25
0.00 i
Minus 0.03 i
24
t
i
Minus 0.06
s
Minus 0.09
23
22
Minus 0.12
21
's
H
20
Minus 0.15
�
0
19
Minus 0.18
1
'C
18
Minus 0.21
Minus 0.24
17
Minus 0.27
--------------
16
Minus 0.30
Minus 0.33 {
i
Minus 0.36
Minus 0.39 i
Minus 0.42
Minus 0.45
15
14
13
12
11
10
e
d
®a
.s
x
b
Y
H ti
+
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x
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9
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rC.
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FA
fAX I eA 1
Q®OO 55 A LKy.ALM STABILIZATION OF WASTMATJER BIOSOLIIDS
Batch Size (gallons) j 5"v 6) 0 Lbso of Lima .266
�!►�f!l��111
Comments:
DATE -a SOURCE -
O
Oyy
Oqy
pyy
Oyq
O
C
O
O
®
C
Oqq
Cy5
a
yO�
H
M
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N
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Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Feb-14
Fn�rirnnmPntal ('lkPmictr Tnr
Falb #
VatA-Iml zed>
C` ild, i 41ro"g Dolt
,og
1
1/22/14
119,048
5.076
2
1/22/14
66,930
4.826
3
1/22/14
90,910
4.959
4
1/22/14
196,079
5.292
5
1/22/14
112,360
5.051
6
1/22/14
112,360
5.051
7
1/22/14
193,051
5.286
Total
Average
Most Probable Number / Gram 1:1'.1ap . `' Fecal Cofliform/gram
Fecal Coliform values are less than 2,000,000 and meets 'the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

viron ental C h.emlists9 Inc.
6602 Wlndmf ll way . Wilmington, NC 28405
[phone] (Lab) a [phone] (Fax)
® 710 Bowsertown Road - Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DI.S CERTIFICATE #37729
Town of Wallace
Dateof Report: Feb 19, 2014
316 E. Murray Street
Customer PO #:
Wallace NC
28466 Deport #: 2014-W762
Attention: Brent Dean, ORC (WWTP) Report to: Brent Dean, ORC (WWTP)
Project 113: WWTP Sludge
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
14-01879 Sits: #1
1/20/2014 9:01 AM Solid/Sludge Derek Reed
Teat
Method Results - Dante Analyzed
Total Solids (o/®)
SM 2540 a 2.52 % 01 /22/2014
Fecal Density
SM 9221C E MPN 24 hr 508 119048 MPN/g 01 /21/2014
Lab ID Sample ID;
Collect Date/Time Matrix Sampled by
14-01880 Site: #2
1/20/2014 9:02 AM Solid/Sludge Derek Reed
'Pest
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 2.54 % 01/22/2014
Fecal Density
SM 0221C E MPN 24 hr 503 66930 MPN/g 01/21/2014
Lab 10 Sample 10:
14-01881 Site: #3
Collect Date/Time matrix Sampled by
1/20/2014 9.03 AM Solid/Sludge Derek Reed
Test Method Results Date Analyzed
Total Solids N
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.64 % 01/22/2014
90910 MPN/9 01/21/2014
Lab ID Sample ID: Collect Datefilme Matrix Sampled by
14-01882 Site: # 1/20/2014 9:04 AM Solid/Sludge Derek Reed
Test Method Results Date Analyzed
Total Solids (®/o) sty 2W B 2.66 % 01122/2014
Fecal Density
SM 9221C E MPN 24 hr 503 196079 MPN/g 01121 /2014
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-01883 Site: #5 1/20/2014 9:05 AM SolidlSludge Derek Reed
Beet Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.67 % 01/22/2014
Fecal Density SM 9221C E MPN 24 hr$03 112360 MPN/g 01/2112014

-
Environmental Chemists, Inc*
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) c [phone] (Fax)
®
710 Bowsertown Road o Manteo, NC 27954
`
[phone]
ANALYTICAL a CONSULTING
CHEMISTS
NCDENR DWQ CEMMCAT E #94. DL9 CERTIFICATE #37729
Town of Wallace
Date of Report: Feb 19, 2014
_
316 E. Murray Street
Customer PO #:
i Wallace NC 28466
Report #: 2014-00762
- Attention: Brent Dean, ORC (WWTP) Report to: Brent Dean, ORC (WIA/TP)
Project ID: WWTP Sludge
Lab ID Sample I®:
Collect Date/Time Matrix Sampled by
14-01884 Site: #6
1/20/2014 9:06 AM Solid/Sludge Derek Reed
- . Test
Method Results Date Analyzed
Total Solids (®/o)
Sin 2540 a 2.67 % O1/22/2014
Fecal Density
SM92210EMPN 24hr603 112360MPN/g 01/21/2014
(Laub ID Sample ID:
Collect Daterrime Matrix Sampled by
14-01885 Site: #7
1/20/2014 9:07 AID Solid/Sludge Derek Reed
. Test
Method Results Date Analyzed
Total Solids (%)
SM2540B 2.59% 01/22/2014'
Fecal Density
SM 9221C E MPN 24 hr 503 193051 MPN/g 01 /21/2014
Comment: Results, except pH reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:

- CCww''`' b ppAACC r j� pA f�
GAS IRON E N TA L C 1 E 1� I S T S 9 I N C J OFFICE-. 910 392.02 31f FAX [phone] -- -
Analytical il< Consulting Chemists
NCDENR: DWq CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Town of Wallace VVVVTP
PROJECT NAME: Sludge
REPORT NO: L
ADDRESS:
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONEIFAX: 284.7969 284.5073
OPY TO: Jerry James, Public Works
email: [e-mail]
Sampled By: l
SAMPLE
TYPE: 1= Influent,
E = Effluent, W = Well, ST = stream, 50 = sou, 5L = swage, utner:
Sample Identification
Collection i
v
ILo
A!
a a
o
,.,
et7
`o
v�
o
o
°c
ow
m 2
Sz
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Tem
=
°a
x
o
=
112.11
Sludge
11}
X
nutrients/metals
G
1
et i
X
fecal density/ %TS
1_ �
G
2
9
C
�Q`�
X
.
fecal density/ %TS
i - �}
G
3
�b
X
Ifecal density/ %TS
j
G
4
4
C
i
X
fecal density/ %TS • .
) -
G
5
4�
X1
fecal density/ %TS
G
G
g
a ✓
C
X
Ifecal density/ %TS
,.j0
G
7)
C
01.
l
X
fecal density/ %TS
G
C
P
G
G
Transfer
R qw ed By:
DateMme
Rece ved By.
DateMme
2.
Temperature when Received: d Accepted: jected: Resample R q sted: A_
Delivered By:. � Received By: • Z/0 Date:
K Time: Wd fr
Comments- TURNAROUND:

r
t
Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
May-14
O'kPm4e4e Tnr
>
D t+e y 6d
+Cold ay'F" ro g` a i .:.
09
...... . .......... .
1
5/20/14
197,629
5.296
2
5/20/14
121,458
5.084
3
5/20/14
204,082
5.310
4
5/20/14
227,273
5.357
5
5/20/14
240,385
5.381
6
5/20/14
105,264
5.022
7
5/20/14
319,149
5.504
Total
Average5.,2'.:..: 1
Coliform/
Fecal ram
Most Probable Number / Gram '" 01 g
Fecal Coliform values are less than 2,000,000 and meets the Class E pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
1` application event.
a

vo ental Chemists, Inc®
6602 Windmill Way ® Wilmington, NC 2W5
IL envirochem(910) 392-0223 (Lab) ® (910) 3924424 (Fax)
® 710 Bowsertown Road . Manteo, NC 27954
[phone] -
ANALYnCAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIECATE #944. DLS CERTIFICATE #37729 —
Town of Wallace Date of Report: May 27, 2014 j
316 E. Murray Street Customer PO #:
Wallace NC 28466 Report #: 2014-05769 a
Attention: Brent Dean, ORC (WWTP) Report to: Brent Dean, ORC (yVll1/TP)
Project ID: V1li111TP Sludge
Lab ID Sample ID. Collect .Date/Tirne Matrix Sampled by
14-13962 Site: #1 5/19/2014 9:40 AM Solid/Sludge - Bradley Vann
i
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 2.53 % 05/20/2014
Fecal Density SM 9221C E MPW 24 hr503 197629 MPN/g 05/20/2014
Lab 1D Sample 10, Collect Date/Time Matrix Sampled by
14-13964 Site: #2 5/19/2014 9:40 AM Solid/Sludge Bradley Vann
Test Method Results Date Analyzed
1
Total Solids (%)
SM 254o B
2.47 %
05/20/2014
Fecal Density
SM 9221C E MPN 24 hr $03
121458 MIEN/g
05/20/2014 r
Lab 10 Sample ID:
Collect Dateffirne
Matrix Sampled by
14-13965 Site: #3
5/19/2014 9:40 AM
Solid/Sludge Bradley Vann
Test
Method
Results Date Analyzed
Total Solids N
SM 254o B
2.45 %
05/20/2014
Fecal Density
SM 9221 C E MPN 24 hr 503
204082MPN/g
05/20/2014 �-
Lab ID Sample ID:
Collect DatelT me
Matrix Sampled by
14-13966 Site: #4
6/19/2014 9:40 AM
Solid/Sludge Bradley Vann
Test
Method
Results Date Analyzed
Total Solids (%)
SM 254o B
2.20 %
05/20/2014
Fecal Density
SM 9221C E MPN 24 hr 5W
227273 MPN/g
05/20/2014
4 '
Lab 10 Sample ID:
Collect Date/Time
Matrix Sampled by
14-13967 Site: #5
5/19/2014 9:40 All
Solid/Sludge Bradley Vann
Test
Method
Rezule Date Analyzed
Total Solids (%)
SM 264013
2.08 %
05/20/2014
Feral Density
SM 9221C E MPN 24 hr 03
240386 MPN/g
05/20/2014

Environmental Chemists, Inc®
6602 Windmill Way 0 Wilmington, NC 28405
[phone] (Lab) ® [phone] (Pax)
® 710 Bowsertown Road c Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTJNG
CHEMISTS NCDENR. DWQ CERTIFICATE #94. DIS CERTIFICATE #37729
Town of Wallace Dat® of Report: May 27, 2014
316 E. Murray Street Customer PO #:
Wallace NC 28466 Report #: 2014-05769
_! Attention: Brent Dean, ORC (WWTP) Report to: Brent Dean, ORC (WWTP)
project ID: WffrP Sludge
Gala ID Sample ID: Collect Date/Time Matrix Sampled by
14-13968 Site: #6 5/19/2014 9,40 AM! Solid/Sludge Bradley Vann
Vest Method Resu is Date Analyzed
Total Solids M SM 2540 9 2.28 % 05/20/2014
Fecal Density SM 9221C E MPN 24 hr 503 105264 MPN/g 05/20/2014
Lab ID Sample ID:
`14-13969 Site: e7
Collect Date/Time matrix Sampled by
5/19/2014 9:40 AM Solid/Sludge Bradley Vann
Vest" Method. Results Date Analyzed
Total Solids (%)
Fecal Density
Comment:
Reviewed by:
SM 2540 B
SM 9221C.E MPN 24 hr 503
Results reported on a dry weight basis.
2.82 % 05/20/2014
319149 MPN19 05/20/2014

Analytical & Consulting Chemists
6 _
ENVIRONMENTALCHEMISTS,` INC - - OFFICE: 910392- 2231FAX[phone] -
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Town of Wallace WWTP
PROJECT NAME: Sludge
REPORT NO: 7(0
ADDRESS:
CONTACT NAME: Brent Dean, ORC
PO NO: _
REPORT TO:
PHONEIFAX: 284.7969 284.6073
COPY TO: Jerry James;;Public Works
email: bdean ownofwallace.com
95% - - — AAMPI E TYPE• I = Influent. E = Effluent. W = Well. ST = Stream, SO = Soil, SL = Sludge, Other:
-2011111rov oy.-
Collection
=
E
vi
a
a `o
o
cp6 '
�;
S o' w
�
c
m
Sz
PRESERVATION
ANALYSIS REQUESTED
Sample Identification
P
Date
Time
Temp
z°
x
g
s
c
o
W
o
Sludge
C
P
X
nutrients/metals
EE
d1
��`t 2
X
fecal densi l %TS
,,J
G
2
C
P
X
fecal density/ %TS
S I _f
e9Ko
G
G
3) .
4
C
P
pow
X
X
fecal density/ %TS
fecal density/ %TS
T-19-1
01910
G
C
G
P
S Q_JY
QYo
G
G
5155-0-H
C
P
IMP7
X
fecal density/ %TS
IR&
G
G
6
X
fecal density/ %TS
S�I`1-ly
m9Ke
G
G
7-
C
P
X
fecal density/ %TS
I
o9+�p
G
G
C
P
J,
G
G
Transfer.
s.4
Relinquished By:
Date/Time
19-ter o9 S
Received By:
Date/Time
A N14 l 0 -, 20
Temperature when Received: Accepted:,
%example
Delivered By: Received•By: O v pate:_
Comments: .T
Time. 165-+

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit'# NCO020702
Jul-14
U -+.l T"n
- - - - -
- - - - - - ---
p�r.gra�
A.
1
7/23/14
11,195
4.049
2
7/23/14
18,116
4.258
3
7/23/14
18,519
4.268
4
7/23/14
9,303
3.969
5
7/23/14
18,868
4.276
6
7/23/14
9,267
3.967
7
7/23/14
31,035
4.492
Fecal 'Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector attraction Reduction Form for this land
application event.

• ,en�71 6602 WindnO Way ® WdEdngton, NC 28405
[phone] (Lab) - (910) 392-44424 (Fax)
® 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYnCAL & CONSULTING
CHEMISTS NCDEW. DWQ CEEtTmCATE #94. DLS CEIT MCAT E #l37729
Town of Wallace
Date of Report: Aug 11, 2014
316 E. Murray Street
Customer P® #:
Wallace NC
28466
Customer ID: 09010063
Attention: Brent Dean, ®RC (WWTP)
Report #: 2014-08658
Project 10: WWTP Sludge
Lab ID Sample ID:
Collect datefT-1me Matrix Sampled by
14-21401 Site:1)
7/21/2014 10:20 AM Solid/Sludge Derek Reed
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.68 % 07/23/2014
Fecal Density
SM 9221C E MPN 24 hr 603 11195 MPN/g 07/22/2014
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-21402 Site: 2)
7/21/2014 10:20 AM Solid/Sludge Derek Reed
Vest
Method
Resuke Date Analyzed.
Total Solids (%)
SM 2540 B
2.76 % 07/23/2014
Fecal Density
SM 9221C E MPN 24 hr 503 18116 MPN/g 07/22/2014
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
14-21403 Site: 3)
7121/2014 10:20 AM Solid/Sludge Derek Reed
Test
Method
Results - Date Analyzed
Total Solids (%)
SM 2640 B
2.70 % 07/23/2014
Fecal Density
SM 9ZHC E MPN 24 hr 503 18619 MPN/g 07/22/2014
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-21404 Site: 4)
7/21/2014 10:20 AM Solid/Sludge Derek Reed
Test
Method
Results Date Analyzed
Total Solids N
SM 2540 B
2.58 % 07/23/2014
Fecal Density
SM MIC E MPN 24 hr 503 9303 MPN/g 07/22/2014
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-21405 Site: 5)
7/21/2014 10:20 AM Solid/Sludge Derek Reed
Test Method! Results Date Analyzed
Total Solids (%) SM 2540 B 2.65 % 07/23/2014
Fecal Density SM WIC E MPN 24 hr 503 18868 MPN/9 07/22/2014
r-
L

i
-Env=onmental Chemists, Inc°
6602 Windmill way ® Wilmington, NC 28405
[phone] (Lab) ® [phone] (Fax)
® 710 Bowsertown Road . Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS WDEM: DWQ CER7IMCATE #94. DLS aR MCATE #37729
Town of Wallace Date of Report: Aug 11, 2014
316 E. Murray Street Customer PO #:
Wallace NC 28466 Customer ID: 09010063
Attention: Brent Dean, ORC (WWTP) Report #: 2014-08658
Project ID: WWTP Sludge
Lab I® Sample I®: Collect Date/Time Matrix Sampled by
_ 14-21406 Site:6) 7/21/2014 10:20 AM Solid/Sludge Derek Reed
Test MethodResults Date Analyzed
Total Solids (%) Su 2540 B 2.69 % 07/23/2014
Fecal Density SM 9221C E MPN 24 hr 603 9267 MPN/9 07/22/2014
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14 21407 Site., 7) 7/21/2014 10:20 AM Solid/Sludge Derek Reed
Feat Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.90 %
31035 MPN/g
Comment Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
r 1
Reviewed by: r 1 l
07/23/2014
07/22/2014

'— '~ E N N' R V N hn N I A v l E m l V 114dd ---OFFICE: 9 0i1392-0223FAX SI C-392.4424
Analytical & Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
client: Town of Wallace WWTP
PROJECT NAME: Sludge
REPORT NO:
ADDRESS:
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONEIFAX: 284.7969 284.5073
COPY TO: Jerry James, Public Works
email: [e-mail]
Sampled By: l C1 SAMPLE
TYPE: I = Influent,
E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other,:
Sample Identification
Collection
p F
N
£ o e
`o
v
c E
"
x
m
g Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp"
Z
z=
Q
z
o
s
so
o
3lud a
C
P
X
nutrients/metals
7- -Ic-t
G
G
I
C
P
u.>Eol
X
fecal density/ %TS
7 _lam
/CAO
G
G
Z
C
P
X
fecal densi ! %TS
-7-a /-IL
i QZ CD
G
G
3
C
P
42S
I
I
X1
fecal density/ %TS
7
0
G
G
4
C
P
L;4vi
I
X
fecal density/ %TS
7-,.))-(Ll
inzQ,
G
G
5
C
P
r
bt
X
I
fecal density/ %TS
-2-2)LM
tozjo
G
G
5
C
P
IX
fecal density/ %TS
1
G
G�a�
7)
C
P
X
fecal density/ %TS
G
C
P
G
G
Transfer
Reli ulshe By:
Datemme
Received By:
Datemme
Temperature when Received: 2- Accepted: jected: Resam;
Delivered By: Received Bv: Date
Comments:

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Oct-14
ate An rz (
+ ►L .0
�t°gra�
1
10/24/14
1,347,369
6.129
2
10/24/14
730,898
5.864
3
10/24/14
376,713
5.576
4
10/24/14
384,616
5.585
5
10/24/14
242,425
5.385
6
10/24/14
520,000
5.716
7
10/24/14
169,492
5.229
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

viroenta1 Chemists, Inc.
6602 Windmill way • Wilmington, NC 28405
[phone] (Lab) . (910) 3924424 (Fax)
® 710 Bowsertown Road a Manteo, NC 27954
[phone]
ANALYTICAL S CONSULTING
CHEMISTS NCDHNM DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Town of Wallace.
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WVyTP)
Date of Report: Nov 14, 2014
Customer P® M -
Customer ID: 09010063
Report #: 2014-13124
Project ID: W TP Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-32263 Site: *1 10/23/2014 10:05 AM Solid/Sludge Derek Reed
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 2.85 % 10/24/2014
Fecal Density SM 9221C E MPN 24 hr 503 1347369 MP N/g 10/24/2014
Lab ID Sample ➢D: Collect DatefTime Matrix Sampled by
14-32264 Site: 92 10/23/2014 10:06 AM Solid/Sludge Derek Reed
Test Method Results Date Analyzed
Total Solids (%) SM 2640 B 3.01 % 10/24/2014
Fecal Density SM 9221C E MPN 24 hr 603 730898 MPN/g 10/24/2014
Lab ID Sample ID:
14-32265 Site: #3
Collect DsteMme matrix Sampled by
10/23/2014 10:05 AM Solid/Sludge Derek Reed
Test
Method
Results Date Analyzed
Total Solids (%)
SM 25N B
2.92 % 10/24/2014
Fecal Density
SM MIC E MPN 24 hr 503
376713 MPN/g 10/24/2014 t
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
14-32266 Site: #4
10/23/2014 10:05 AM
Solid/Sludge Derek Reed J
Test
Method
Results Date Analyzed
Total Solids (°i6)
SM 2w0 a
. 2.86 % 10/24/2014
Fecal Density
SM =1 C E MPN 24 hr 603
384616 MPN/g 10/24/2014
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
14-32267 Site: #5
10/23/2014 10:05 AM
Solid/Sludge Derek Reed
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.30 % 10/24/2014
Fecal Density
sM9221c EMPH 24 hrs03
242425 MPN/g 10/24/2014

.r,nvironmental Chemists, Inc.
6602 Windmill Way ® Wilmington, NC 28405
[phone] (Lab) o [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
_ CHEMISTS NCDENIL DWQ CERTIFICATE #94. DIS CERTIFICATE #37729
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWI'P)
Date of Report: Nov 14, 2014
Customer PO 0:
Customer 10: 09010063
Report M 2014-13124
Project ID: WNVTP Sludge
Lab ID
Sample ID:
Collect Date/Time
Matrix
Sampled by
14-32266
Site: #6
10/23/2014. 10:05 AM
Solid/Sludge
Derek Reed
i 'Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
14-32269 Site: e7
Teat
Total Solids (%j
Fecal Density
Comment
- Reviewed by:
Say 254o e
SM 9221C E MPN 24 hr 503
2.50 % 10/24/2014
520000 MPNlg 10/24/2014
Collect Date/Time Matrix
10/23/2014 10:06 AM Solid/Sludge
Method Results
sM 254o s
SM 9221C E MPJM 24 hr 503
Sampled by
Derek Reed
Date Analyzed
2.95 % 10/24/2014
169492 MPN/9 10/24/2014
cb- % z

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, I N C QFPICEn9101392-022311FAX [phone]
NCDENR: DWQ CERTIFICATION 9 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
client: Town of Wallace WWTP
PROJECT NAME: Sludge
REPORT NO: `
WDRESS:
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONEIFAX: 284.7969 284.6073
COPY TO: Jerry James, Public Works
email: bdean ownofwallace.com ,
3arnpled By: 4.2E� - SAMPLE
TYPE:
I = Influent,
E Effluent, W = Well, ST = Stream, 50 5011, 51. = 5luage, Omer:
Sample Identification
Collection
CL e
r
o
;,
ze
o
(D V
c
°LU
g
Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time _
Tom
a
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o
SQ
e
w
3lud a
C
P
3
X
nutrients/metals
fa-s—
G
G
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X
fecal density/ %TS
ilaU3./
(xS-
G
G
C
P
X
fecal density/ %TS
G
G
3)
C
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I X
fecal density/ %TS
5-
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4)
C
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X
ifecal density/ %TS
)n-:Z?4q
G I
G
5
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fecal density/ %TS
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6
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fecal density/ %TS
/�j��j
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G
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7
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fecal density/ %TS
/ozw-
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Transfer
Reli ulshed y:
Datefl'ime
Received By.
DateMme
1.0 : l
2
Temperature when Received:. 41 "1 Accepted: ✓ 4 R ject d: Resample
Delivered By: Received B •6 Date:_
Comments: TI
11
ND:

Temp °C
Correction
Factor
40
Plus 0.45
39
Plus 0.42
38
Plus 0.39
37
Plus 0.36
36
Plus 0.33
35
Plus 0.30
34
Plus 0.27
33
Plus 0.24
32
Plus 0.21
31
Plus 0.18
30
.Plus 0.15
29
Plus 0.12
28
Plus 0.09
�27
Plus 0.06
26
Plus 0.03
25
0.00
24
Minus 0.03
23
Minus 0.06
22
Minus 0.09
21
Minus-0.12
20
Minus 0.15
19
Minus 0.18
18
Minus 0.21
17
Mums 0.24
16
Minus 0.27
15
Minus 0.30
14
M_inns 0.33
13
Minus 0.36
12
Minus 0.3.9
11
Minus 0.42
10
Minus 0.43
W
Me
logoA1�oi
o
IM
oil'
iiii�
u�

Temp,C
Correction
Factor
40
Plus 0.45
39
Plus 0.42
38
Plus 0.39
37
Plus 0.36
36
Plus 0.33
35
Plus 0.30
34
Plus 0.27
33
Plus 0.24
32
Plus 0.21
31
Plus 0.18
30
.Plus 0.15
29
Plus 0.12
28
Plus 0.09
127
Plus 0.06
26
Plus 0.03
25
0.00
24
Minus 0.03
23
Minus 0.06
22
Minus 0.09
21
Minus •0.12
20
Minus 0.15
19
Minus 0.18
18
Minus 0.21
17
Minus 0.24
16
Minus 0.27
15
Minus 0.30
14
Minus 0.33
13
Minus 0.36
12
Minus 0.3.9
1 I
Minus 0.42
10
Minus 0.45
Gm
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I
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SOIL ANALYSIS REPORTS

SOIL SAMPLE ANALYSES
The Town of Rose Hill, the Town of Kenansville, the Town of Beulaville, the Town of Warsaw and
Southwest Plantation met pathogen reduction and vector attraction reduction requirements through
lime stabilization. The soil pH will continue to be raised through the continued application of lime
stabilized biosolids to these application fields.

Waters Agricultural Laboratories, Inc.
WATERS�Y4ry4ciclRAL WA� RS`4 lCU��URAL
LA6.OR .012 �V' -;. 364 West Park Drive Warsaw, NC 28398 257 Newton Hwy - P.O. Box 382 LAtloRr TIESc.
;, •,,k ., t t_ -T [phone] FAX [phone] Camilla, Georgia 31730 lr:
[phone] FAX [phone] b '"'
HARVEY FERTILIZER & GAS
QII Analysis ReportGrower:
TRIPLE S FARMS
Account#:
60126
1060 S NC 41 & 111
NCDA
Index
Field ID.
Received:
01/20/2015
BEULAVILLE, NC 28518
Processed:
01/22/2015
........................................ _. -._ ..-..................................................
......................._.._.....................................__.._.._......-..-..........
. _.._...
_ .....
Wate ......::::....._..._...._.__...__._.
--...-.-.._.-.._...-..._..._._.............-................._..........__........
......_..
-
.... -
-
Lab Number Sample ID
P-l:
K-I
Mg%;
Ca%
.
pH ; ' Ac;
S-I I
jZn-I'
Zn-AL
iMn-I :
iMn-AI!
!Cu-I
CEC
BS% HM% Soil Ctass;
894650ZW 1
79
24
8.7 .
66.7 5.8 1.2
38
203
203'
31
28
150
5.4
77,7
1.31 Min
Recommendations - Ibs./A
Lime-Tons/A
®
P205
K20
Mg
S '
Cu
Zn
©
Mn
See Note
Crop BERMUDA Pasture M
0.3
220
0
180
0
0
0
0
12
894651ZW ,2
39
14
7.8
59.1 5.5 2.2
39
111
111
21
22
92
6.9
68.0
1.39 Min
Recommendations - Ibs./A
FP2051
K20
Mg
S
Cu
Zn
©
Mn
See Note
Crop BERMUDA Pasture M
1.0
220
40
200
0
0
0
0
12
894652ZW 3
44.
21
11.01
70.8 6.2 0.7
35
151
.151
34
35
102
5.0
84.0
.1.50 Min
Recommendations - Ibs./A
Lime-Tons/A
®
P205
K20
Mg
Cu
Zn
©
Mn
See Note
Crop BERMUDA Pasture M
0.0
220
30
190
0
0
0
0
12
694653ZW .3A
29
28
11.1
50.5
5.6 2.0
53
82
82
12
24
59
5.6
64.2
1.78 Min
Recommendations - Ibs./A
Lime-Tons/A
®
P205
K20
Mg
n_
Cu .
Zn
©
Mn
See Note
Crop FESCUE M
0.8
200
70 _
80
0
0
0
0
12
894654ZW 4
27
12
6:6 =
34.2
4.8 2.2
31
85
85
9
15
49
3.8
42.5 ,
0.92 ,Min
Recommendations -Ibs./A
Lime-Tons/A
®
P205
K20
Mg
S
Cu .
Zn
©
Mn
See Note
Crop BERMUDA Pasture M
1.5
220
80
220
0
0
0
01
12
894655ZW 5
84
20
6.2
501 :.5.4
2.2
38
236
236
28
34
136
5.3
58.2
0.89 Min
Recommendations - Ibs./A
Lime-Tons/A
®
P205
K20
Mg
S
Cu
Zn
©
Mn
See Note
Crop FESCUE M
1.1
200
0
100
0
0
0
0
12
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Plumber 635

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TRIPLE S FARMS
LAND APPLICATION PROGRAM
PERMIT NO. WQ0030998
2014 APPLICATION SUMMARY
Farmer
Tract
/Site
Field
Acres
Date
Spread
Gallo..ns
Dry`Tons L
Acre
Dry Tons
Crop
Source
PAN
Ob.s/ac)
Eric Smith
1
1
29.5
Mar-14
276,000
1.01
29.92
Bermudagrass
Wallace WWTP
121.02
Apr-14
96,000
0.35
10.25
Bermudagrass
Wallace WWTP
Jul-14
330,000
1.31
38.53
Bermudagrass
Wallace WWTP
Aug-14
312,000
1.23
36.43
Bermudagrass
Wallace WWTP
Oct-14
135,000
0.27
7.94
Oats (Grain)
Warsaw WWTP
2
8.48
Feb-14
36,000
0.13
1.07
Oats (Grain)
Beulaville WWTP
86.95
May-14
66,000
0.56
4.79
Millett
Kenansville WWTP
Jun-14
21,000
0.07
0.62
Millett
Beulaville WWTP
Jul-14
72,000
0.50
4.23
Millett
Warsaw WWTP
Jul-14
42,000
0.33
2.77
Millett
Rose Hill WWTP
Dec-14
84,000
1.19
10.05
Oats (Grain)
Wallace WWTP
3
19.95
Feb-14
60,000
0.09
1.78
Oats (Grain)
Beulaville WWTP
57.45
Mar-14
120,000
0.65
13.01
Bermudagrass
Wallace WWTP
Apr-14
15,000
0.05
1.01
Bermudagrass
Southwest Plantation WWTP
May-14
66,000
0.24
4.79
Bermudagrass
Kenansville WWTP
Jun-14
42,000
0.06
1.24
Bermudagrass
Beulaville WWTP
Jul-14
60,000
0.18
3.53
Bermudagrass
Warsaw WWTP
Jul-14
18,000
0.06
1.19
Bermudagrass
Rose Hill WWTP
Dec-14
72,000
0.43
8.62
Oats (Grain)
Wallace WWTP
4
4.14
Apr-14
30,000
0.77
3.20
Soybeans (Double Cropped - Manured)
Wallace WWTP
58.02
Oct-14
48,000
1.39
5.74
Oats (Grain)
Wallace WWTP
5
11.2
Apr-14
66,000
0.39
4.35
Soybeans (Double Cropped - Manured)
Rose Hill WWTP
99.10
Apr-14
54,000
0.51
5.76
Soybeans (Double Cropped - Manured)
Wallace WWTP
Sep-14
162,000
1.69
18.92
Fescue
Wallace WWTP
Sep-14
10,600
0.04
0.44
Fescue
Murphy Brown Soybean Oil
Oct-14
90,000
0.96
10.77
Fescue
Wallace WWTP
Wields Applied to: 5 73.27
Tota:
Town of Beulavill(
Town of Kenansvillc
Town of Rose Hill
Sothwest Plantatior,
Town of Wallac(
Town of Warsam
Gallons
Dry Tons
Metric
Tons
Permit Limit.Dry Tons
2,383,600
230.50
209.55
NA
159,000
4.71
4.28
50
132,000
9.58
8.71
60
126,000
8.30
7.55
51.51
15,000
1.01
0.92
15
1,674,000
191.21
173.83
380
267,000
15.70
14.27
90
Branch Residuals Soils, LLC Confidential 1/24/2015 Page 1

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Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Beulaville WWTP
Farmer: Eric Smith
Acres: 19.95
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 0.71
Residual Report No.: B 2014
Crop: Oats (Grain)
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/24/14
3
60,000.0
Moist
Wann, Partly Cloud
0.00

Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Beulaville WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 0.71
Residual Report No.: B 2014
Crop: Oats (Grain)
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Dour
Rainfall
2/25/14
2
36,000.0
Moist
Cool, Partly Cloudy
Trace

Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Beulaville WWTP
Farmer: Eric Smith
Acres: 19.95
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 0.71
Residual Report No.: B 2014
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/19/14
3
42,000.0
Dry
Wann, Partly Cloud
0.10
of :::.:«:
T... L.Gallo
2'OOi)0

Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Beulaville WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 0.71
Residual Report No.: B 2014
Crop: Mittett
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/20/14
2
21,000.0
Dry
Hot, overcast
0.00
0 :.::.::.:

Triple S Farms
Kenansville, North Carolina
Triple S Farms
WQ0023178
Annual 2014
iKenansville WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 1.74
Residual Report No.: K 2014
Crop: Millett
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/22/14
2
66,000.0
Moist
sunny
0.08

Triple S Farms
Kenansville, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Kenansville WWTP
Farmer: Eric Smith
Acres: 19.95
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 1.74
Residual Report No.: K 2014
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/23/14
3
54,000.0
Moist
cloudy, Hot
0.40
5/27/14
3
12,000.0
Dry
Warm, Clear
0.00
ota. Gad.::ons:,:
..6�::::.::.::

Triple S Farms
Rose Hill, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Rose Hill WWTP
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Surface
Field: 5
Percent Solids: 1.58
Residual Report No.: RH 2014
Crop: Soybeans (Double Cropped - Manured)
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/2/14
5
48,000.0
Moist
sunny
0.00
4/3/14
5
18,000.0
Moist
Cool
0.00

Triple S Farms
Rose Hill, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Rose Hill WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 1.58
Residual Report No.: RH 2O14
Crop: Millett
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/30/14
2
42,000.0
Dry
sunny
0.00
> ::
0. A. .

Triple S Farms
Rose Hill, forth Carolina
Triple S Farms
WQ0023178
Annual 2014
Rose Hill WWTP
Farmer: Eric Smith
Acres: 19.95
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 1.58
Residual Report No.: RH 2O14
Crop: Bermudagrass
Date
Field No.
Sulbfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/30/14
3
18,000.0
Dry
overcast
Trace
» :Total:;Gallons:,..:...... ..::.::..:::«.;;::<.;;;:::::.;:::::18,
.:000,..;

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Southwest Plantation WWTP
Farmer: Eric Smith
Acres: 19.95
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 1.61
Residual Report No.: SW 2014
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/23/14
3
15,000.0
Moist
Sunny
0.00
..Gallons;
:....:.:;:.::...:;
>>:>>
....:.:::....:::::.....
'...0 .
5,00 . ,0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
1st Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 29.5
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 2.60
Residual Report No.: WA2014 1-14
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/14/14
1
72,000.0
Dry
Cool, Sunny
0.00
3/22/14
1
60,000.0
Dry
Cool, Sunny
0.00
3/24/14
1
66,000.0
Moist
Cool, Sunny
0.00
3/26/14
1
78,000.0
Moist
Cool, Cloudy
Trace
<0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
1st Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 19.95
Site/Tract: 1
Application Method: Injected
Field: 3
Percent Solids: 2.60
Residual Report No.: WA2014 1-14
Crop: Bermudagrass
Date
Field No.
' Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/27/14
3
54,000.0
Moist
Cool, Sunny
0.00
3/28/14
3
66,000.0
Dry
Cool, Sunny
0.00
>000,0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
2nd Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 4.14
Site/Tract: 1
Application Method: Injected
Field: 4
Percent Solids: 2.56
Residual Report No.: WA2014 2-14
Crop: Soybeans (Double Cropped - Manured)
Date
Field No.
Subffield
Gallons
Soil
Conditions
Weather
Conditions
Frev. 24 dour
Rainfall
4/3/14
4
30,000.0
Dry
VVann, Cloud
0.00
0 '0.O
. .

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
2nd Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Injected
Field: 5
Percent Solids: 2.56
Residual Report No.: WA2014 2-14
Crop: Soybeans (Double Cropped - Manured)
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/4/14
5
54,000.0
Moist
Cool, Cloudy
0.00
wx-
77
0. 004. .

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
2nd Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 29.5
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 2.56
Residual Report No.: WA2014 2-14
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/9/14
1
66,000.0
Dry
Warm, Sunn
0.00
4/10/14
1
30,000.0
Dry
Warm, Sunn
0.00
�U

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
3rd Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 29.5
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 2.80
Residual Report No.: WA2014 3-14
Crop: Bermudagrass
Date
Field No.
Subrield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/5/14
1
72,000.0
Dry
Hot, Clear
0.00
7/6/14
1
60,000.0
Dry
Hot, Clear
0.00
7/9/14
1
72,000.0
Moist
Hot, Clear
0.30
7/10/14
1
66,000.0
Moist
Hot, Cloudy
Trace
7/11/14
1
60,000.0
Moist
Hot, Cloudy
0.20
`0 p00..

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
3rd Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 29.5
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 2.80
Residual Report No.: WA2014 3-14
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/18/14
1
30,000.0
Moist
t, Partly Clot
0.30
8/19/14
1
24,000.0
Moist
t, Partly CloL
Trace
8/20/14
1
30,000.0
Moist
t, Partly Clo
0.00
8/26/14
1
66,000.0
Dry
Hot, Clear
0.00
8/27/14
1
78,000.0
Dry
Hot, Clear
0.00
8/28/14
1
72,000.0
Dry
Hot, Clear
0.00
8/29/14
1
12,000.0
Dry
Hot, Clear
0.00
>:

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
3rd Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Injected
Field: 5
Percent Solids: 2.80
Residual Report No.: WA2014 3-14
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/11/14
5
30,000.0.
Dry
Hot, Clear
0.00
9/12/14
5
36,000.0
Moist
t, Partly Clot
0.00
9/22/14
5
72,000.0
Dry
Warm, Sunn3
Trace
9/23/14
5
24,000.0
Moist
Warm, Cloud
Trace
1d < OQ0.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
4th Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Injected
Field: 5
Percent Solids: 2.87
Residual Report No.: WA2014 4-14
Crop: Fescue
Date
Field No.
Subfneld
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/2/14
5
60,000.0
Dry
Warm, Clear
0.00
10/3/14
5
30,000.0
Dry
Wann, Cloud
Trace
:
iDo::;::s
00..0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
4th Quarter 2014
Wallace WWTP .
Farmer: Eric Smith
Acres: 4.14
Site/Tract: 1
Application Method: Injected
Field: 4
Percent Solids: 2.87
Residual Report No.: WA2014 4-14
Crop: Oats (Grain)
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/6/14
4
48,000.0
Dry
Warm, Cloud
0.00

fl
Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
4th Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Injected .
Field: 2
Percent Solids: 2.87
Residual Report No.: WA2014 4-14
Crop: Oats (Grain)
:
Date
Field No.
Sub£eld
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/15/14
2
24,000.0
Dry
Warm, Clear
0.00
12/16/14
2
60,000.0
Moist
Warm, Cloud
0.15

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0023178
4th Quarter 2014
Wallace WWTP
Farmer: Eric Smith
Acres: 19.95
Site/Tract:' 1
Application Method: Injected
Field: 3
Percent Solids: 2.87
Residual Report No.: WA2014 4-14
Crop: Oats (Grain)
Date
Field No.
Subfield
Gallons
Sod
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/17/14
3
72,000.0
Moist
Warm, Cloud
0.00
00` '0
::..::.�:::.:::::.::::

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Warsaw WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 1.41
Residual Report No.: WR 2014
Crop: Millett
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/14/14
2
60,000.0
Moist
Hot Partly Cloudy
0.00
7/15/14
2
12,000.0
Moist
Hot Partly Cloudy
0.00

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Warsaw WWTP
Farmer: Eric Smith
Acres: 19.95
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 1.41
Residual Report No.: WR 2014
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 hour
Rainfall
7/14/14
3
18,000.0
Moist
Hot Partly Cloudy
0.00
7/15/14
3
12,000.0
Moist
Hot Partly Cloudy
0.00
7/16/14
3
6,000.0
Dry
Hot, Clear
0.00
7/18/14
3
24,000.0
Dry
Hot, Clear
0.00

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0023178
Annual 2014
Warsaw WWTP
Farmer: Eric Smith
Acres: 29.5
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.41
Residual Report No.: WR 2014
Crop: Oats (Grain)
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/13/14
1
96,000.0
Dry
Hot, clear
0.00
10/14/14
1
39,000.0
Moist
Hot Partly Cloudy
Trace
otal:G:* 1l:::ns
.�35:000 0