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HomeMy WebLinkAboutWQ0006816_Residual Annual Report 2016_20170223McGill Environmental Systems Delway Compost Facility Permit # WQ0006816 2016 Annual Report Submitted by: McGill Environmental Systems 1100 Herring Road Rose Hill, North Carolina 28458 RECEIVEDINCDE�DWR FEB 2 3 2017 FEB 2 4 2017 Non-Discharge permitting Table of Contents 2016 Delway Facility Highlights Section 1 Compost Feedstock Sources Section 2 Annual Distribution Summary Form Residuals Summary Amendments Summary Quality Assurance and Monitoring Section 3 Process Description Temperature Reports Temperature Snapshots Analysis of Finished Compost Section 4 Pathogen Certifications Seal of Testing Assurance TCLP Analysis Compost Distribution and Marketing Section 5 Overview Compost Distribution Summary 2016 Delway Facility Highlights 1. Volumes processed at the Delway facility in 2016 were on par with 2015 totals. 2. Compost sales continue to grow as our sales staff continues to create awareness of compost product uses. 3. McGill continues to participate in the U. S. Composting Council's Seal of Testing Assurance Program. 4. Throughout 2016, product formulation was adjusted to reflect an overall strategy to improve efficiency and product quality. CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0006816 FACILITY NAME: McGill Environmental Systems of NC Inc. PHONE: 919-532-2539 COUNTY: Sampson OPERATOR: Steve Cockman FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) El Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes 0 No ❑ -► If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources s ( include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January 736.47 873.08 441.45 441.45 February 700.73 843.14 763.17 763.17 March 751.54 962.26 891.38 SEE ATTACHED 891.38 April 557.87 838.53 1991.17 1991.17 May 368.55 819.24 1753.56 1753.56 June 381.11 767.51 1554.99 1554.99 July 397.79 773.39 1306.79 1306.79 August 431.03 1059.63 1644.16 1644.16 September 570.01 1069.08 1226.35 1226.35 October 623.62 1052.45 617.79 617.79 November 562.27 953.1 1277.46 1277.46 December 812.51 1035.4 551.75 551.75 Total from FORM DMSDF (sup) Totals: Annual (dry tons): 6893.5 11046.81 14020.02 14020.02 Amendment(s) used: I I Bulking, Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) Part C: Facility was compliant during the past calendar year with all conditions of the land application permit p Yes (including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No 0, If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Date **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Signature of Preparer** (if different from Permittee) Date r-N`--7c -m `4F-•c P -1,57-18 - S3:)ijnos >i:)oisa333 ISOdVYO:) 2016 Residuals Summary CUSTOMER County Permit Month Dry Tons AVINTIWPGI Johnston I00001 Jan 152.68 Feb 140.17 Mar 145.82 Apr 119.66 May 108.44 Jun 103.62 Jul 108.62 Aug 106.16 Sep 125.22 Oct 110.90 Nov 117.38 Dec 128.09 AVINTIWPGI Total - - ^� - - - 1,466.77 Brian's Waste -Rock Rocco Brian's Waste -Rock Rocco Total_ Brunswick Regional W&S H2GO Brunswick Regional W&S H2GO Total Brunswick, SE (Southport) Brunswick, SE (Southport) Total Bunn,Town of (Dewatering) _ Bunn,Town of (Dewatering) Total Cottonwood Cottonwood Total DAK Americas (Dewatering) Brunswick Brunswick Franklin Wake Cumberland WQ0000469 Jan 5.17 5.17 NCO075540 Jan 1.07 Feb 1.04 Mar 0.84 May 0.97 Jul 0.83 Aug 0.69 Oct 0.91 Dec _1.04 7.40 WQ0013200 Apr 2.82 May 2.99 Aug 8.02 13.83 NCO042269 Jan 1.15 Feb 1.18 Apr 1.24 Jul 1.54 5.11 NCO065706 Feb _ 1.64 Jun 0.69 Aug -0.34 Dec 0.42 �. 2.41 �~NC0003719 Jan A 11.13 Feb 12.25 Mar 23.78 Apr 30.23 May 31.22 Jun 46.09 Jul 32.72 Aug 45.01 Sep 34.31 Oct 20.72 Page 10f 5 2016 Residuals Summary CUSTOMER County Permit Month Dry Tons DAK Americas (Dewatering) Cumberland NC0003719 Nov 26.89 Dec 21.33 DAK Americas (Dewatering) Total _ 3.35.68 DAK Americas, LLC (Columbia) Calhoun,SC SC0001333 Jun 25.82 DAK Americas, LLC (Columbia) Total 25.82 Fuquay-Varina, Town (Terrible) Johnston NCO066516 Jan 11.96 Feb 8.87 Mar 17.24 Apr 14.02 May 18.07 Jun 12.81 Jul 10.63 Aug 7.85 Sep 16.40 Oct 9.64 Nov 10.42 Dec 7.11 Fuquay-Varina, Town (Terrible) Total 145.02 _ Greenville Utits. Commission Pitt NCO023931 Jan 176.31 Feb 177.09 Mar 200.74 Apr 156.58 May 141.61 Jun 140.42 J u I 124.60 Aug 168.68 Sep 180.86 Oct 205.48 Nov 194.62 Dec 177.10 Greenville Utlts. Commission Total _ _ _ _ V 2,044.09 Grifols Therapeutics, Inc. Johnston I00001-97 May 0.35 Jun 0.11 Oct 3.68 Nov 11.51 Dec 3.58 Grifols Therapeutics, Inc. Total ^_T 19.23 Hoke County WWTP Hoke _ NCO089176 Sep 20.34 Oct 4.39 Hoke County WWTP Total _ _ 24.73 INVISTA - DMT New Hanover NC0001112 Aug 17.22 Dec 38.47 INVISTA - DMT Total 55.68 Kure Beach, Town of WWTP New Hanover NCO025763 Oct 3.99 Nov 33.80 Dec 21.60 Kure Beach, Town of WWTP Total 59.39 Lake Waccamaw Columbus _ NCO021881 Feb 1.10 Mar 2.74 Aug 2.16 Sep 13.48 _- -- -- Oct 5.44 Page 2 of 5 2016 Residuals Summary CUSTOMER County Permit Month Dry Tons Lake Waccamaw Total 24.92 Lear Corporation/Guilford East-Kenansville _ Duplin NC0002305 Jan 4.56 Jul 4.69 Sep 11.89 Lear Corporation/Guilford East-Kenansville Total 21.14 Maxton-LaurinburgAP Scotland NCO044725 _ Mar 14.44 Apr 17.45 Maxton-LaurinburgAP Total _ 31.88 Mount Olive, Town of Wayne NCO020575 Apr 8.28 May 7.14 Jun 4.29 Jul 2.31 Aug 4.39 Sep 2.66 Dec 10.90 Mount Olive, Town of Total _ 39.97 Pembroke, Town of Pembroke, Town of Total Princeton_,_ Town of _ Princeton, Town of Total Raeford, City of WWTP Robeson Johnston Hoke Raeford, City of WWTP Total _ Raleigh, City of Public Utilit _ Wake NCO027103 Jan Feb Mar Apr May Jun Jul Aug Sep Oct Nov Dec NCO026662� Oct NCO026514 Jan Feb Mar Apr May Jun Jul Aug Sep Oct Nov Dec NCO029033 Jan Feb 5.74 13.37 14.33 4.35 11.32 13.41 9.17 5.82 19.00 11.75 9.46 20.01 137.73 6.19 _ 6.19 44.63 85.97 61.24 75.11 66.51 77.55 62.54 32.33 33.54 46.70 48.80 295.39 286.71 Page 3 of 5 2016 Residuals Summary CUSTOMER County Permit Month Dry Tons Raleigh, City of Public Utilit Wake NC0029033 Mar 287.32 Apr 232.91 May 233.94 Jun 152.02 Jul 188.20 Aug 319.13 Sep 241.96 Oct 254.36 Nov 287.14 Dec 399.69 Raleigh, City of Public Utilit Total 3,178.78 Saint Pauls,Town of Robeson NCO020095 Jan 3.28 Apr 4.20 May 3.19 Jun 4.81 Aug 3.01 Sep 3.63 Oct 1.37 _ Dec 4.80 Saint Pauls,To_wn of Total tl_ _ Smithfield Farmland -Kinston _ _ Lenoir WRO07 ^ Jan _28.29 50.00 Feb 54.53 Mar 59.70 Apr 55.60 May 66.19 Jun 62.71 Jul 71.73 Aug 80.67 Sep 81.28 Oct 65.22 Nov 75.11 77.29 Smithfield Farmland -Kinston Total _.Dec _ 800.03 Smithfield Farmland-Tarheei Bladen _ NCO078344 Feb 2.21 Mar 6.75 Aug 9.51 Sep 19.44 Oct 7.34 Nov 7.66 Dec 3.74 Smithfield Farmland-Tarheel Total Smithfield Farmland -Wilson Wilson NC9525 Jan Feb Mar Apr May Jun Jul Aug 56.65 6.66 3.97 7.72 6.74 5.87 4.30 7.44 8.34 Page 4 of 5 2016 Residuals Summary CUSTOMER County Permit Month Dry Tons Smithfield Farmland -Wilson Wilson NC9525 Sep 7.13 Smithfield Farmland -Wilson Total Sun River Service Corp. Nash _ Sun River Service Corp. Total +^Synagro-Brunswick County NW _ - Brunswick Synagro-Brunswick County NW Total Tabor City WWTP Columbus Tabor City WWTP Total Valley Proteins (Rose Hill) Duplin Valley Proteins (Rose Hill) Total Grand Total i Oct 5.54 Nov 10.17 Dec -- 4.06 7.7.93 2009-020 May 1.06 Sep — - - 1.19 - 2.25 NCO057533 Feb - - 18.37 18.37 NCO02600 Jun 14.11 14.11 WQ000485 Jan 103.35 Feb 34.67 Mar 119.60 Apr 109.34 May 120.37 Jun 104.75 Jul 148.37 Aug 240.64 Sep 256.75 Oct 288.83 Nov 120.14 Dec 70.79 1,717.59 11,046 Page 5 of 5 2016 Amendment Summary Month Jan Jan Total Feb Feb Total Mar Mar Total Apr Apr Total Material Feed Mill Waste Food Waste & Peelings Livestock Waste Poultry Litter Sheetrock Silica Wood Waste Feed Mill Waste Food Waste & Peelings Livestock Waste Poultry Litter Sheetrock Silica Wood Waste Feed Mill Waste Food Waste & Peelings Livestock Waste Poultry Litter Sheetrock Wood Waste Yard Waste Feed Mill Waste Food Waste & Peelings Livestock Waste Poultry Litter Sheetrock Silica Wood Waste May Feed Mill Waste Food Waste & Peelings Livestock Waste Sheetrock Silica Wood Waste May Total Jun Feed Mill Waste Dry Tons 50.95 81.48 19.36 46.85 39.12 7.87 490.83 ..736.47 54.35 74.30 19.70 135.85 25.10 7.43 384.00 700.73 58.71 51.72 21.51 266.04 36.33 317.23 (0.00) 751.54 51.22 81.20 19.73 30.00 87.34 9.09 279.29 557.87 55.90 64.81 19.87 115.96 7.87 104.15 368.55 84.76 2016 Amendment Summary Month Material Dry Tons Jun Food Waste & Peelings 67.07 Livestock Waste 21.67 Poultry Litter 16.97 Sheetrock 29.20 Silica 7.22 Wood Waste 154.22 Jun Total ����381.11 Jul Feed Mill Waste 59.29 Food Waste & Peelings 99.37 Livestock Waste 23.27 Poultry Litter 5.47 Sheetrock 16.39 Wood Waste 194.01 Jul Total 397.79 Aug Feed Mill Waste 51.35 Food Waste & Peelings 144.65 Livestock Waste 26.36 Poultry Litter 11.15 Sheetrock 12.38 Silica 8.39 Wood Waste 176.75 Aug Total 431.03 Sep Feed Mill Waste 74.42 Food Waste & Peelings 183.62 Livestock Waste 17.73 Poultry Litter 10.97 Sheetrock 32.61 Silica 10.39 Wood Waste 240.28 Sep Total 570.01 Oct Feed Mill Waste 48.51 Food Waste & Peelings 120.12 Livestock Waste 22.31 Poultry Litter 4.64 Sheetrock 71.89 Silica 37.86 Wood Waste 318.30 Oct Total 623.62 Nov Feed Mill Waste 39.75 Food Waste & Peelings 133.94 2016 Amendment Summary Month Material Dry Tons Nov Livestock Waste 20.61 Poultry Litter 16.75 Sheetrock 118.66 Silica 10.12 Wood Waste 222.45 Nov Total 562.27 Dec Feed Mill Waste 53.74 Food Waste & Peelings 86.05 Livestock Waste 18.56 Poultry Litter 16.77 Sheetrock 58.44 Silica 8.47 Wood Waste _ _ _ 570.48 Dec Total 812.51 Grand Total 6,893.49 COMPOST QUALITY ASSURANCE ILI I ii 111 MONITORING DATA MCGILL COMPOSTING PROCESS DESCRIPTION Incoming sludge is evaluated with respect to all of those parameters that are known to influence the kinetics of the process. Volatile solids, moisture content, void space and compaction tests are routinely performed. Volatile solids are of particular significance in that they give an indication of the inherent energy associated with a particular sludge. When necessary, volatile solids in the form of putrescible fresh poultry waste are added to ensure protracted elevated temperatures. This accomplishes two process goals: pathogen destruction and water removal. The latter is accomplished through the use of forced ventilation. MES has established, through experience, that the volatile solids test has to be interpreted in a manner which takes into consideration that the tests lack both specificity and sensitivity. The ignition of dry solids at 550F may be used as a rough measure of organic matters, but does not differentiate between ready metabolized material and organic matter that has not decomposed within the duration of the composting period. To overcome this shortcoming inherent in the volatile solids test, MES performs bench scaJ-E treatability test on all sludge it processes. Microbial decomposition of organic matter in a specially designed vessel allows for a direct bench scale measurement of stabilization. Since microbial decomposition of sludge generates metabolically derived heat at the expense of substrate, it is possible to establish optimum degradation rates through enthalpy comparison tests. Adjustments of physio/chemical parameters that are known to influence degradation rates are also established during bench scale treatability tests. The total mixture is placed on aerated floors, under roof. MES installed a new custom application computer monitoring and control system to automatically monitor composting process temperatui and control the blower system, assuring that the temperatures of the composting residuals meets levels required for PFRP and Vector Attraction Reduction. Temperature data is collected daily Examples of the data are on the following pages. Delwav Processine Ba Temperature log for Pathaeen Reduction (PFRP)i McGill Environmental Temperature Report Batch Bay Initials Amendments: compost woodwaste e06120716 BayE06 Residuals: biosolids Start Date/Time: Comment 12/8/2016 7:44:47 AM •Stop Date/Time: Comment 12/16/2016 8:08:03 AM ,Blower: 0 Date/Time Temperature Date/Time Name Comment 12/8/2016 5:00:00 PM 155.9483 12/8/2016 7:45:03 AM adt blended by oscar filled by roman 12/9/2016 5:00:00 PM 166.0462 12/10/2016 5:00:00 PM 165.0698 n 12/11/2016 5:00:00 PM 158.8899 1 / 12/12/2016 5:00:00 PM 155.0955 12l13/2016 5:00:00 PM 153.3404 p 12/14/2016 5:00:00 PM 150.6088 12/15/2016 5:00:00 PM 119.4745 47riday, December 16, 2016 Page 1 of I McGill Environmental Temperature Report Batch Bay Initials Amendments: e05110216 BayE05 Residuals: biosolids Start Date/Time: Comment 11/2/2016 5:41:27 PM ,Stop Date/Time: Com►nent 11/10/2016 2:42:39 PM Blower: 0 Date/Time Temperature Date/Time 11/3/2016 5:00:00 PM 160.7315 11/4/2016 5:00:00 PM 163.9327 11/5/2016 5:00:00 PM 160.8057 !� 11/6/2016 5:00:00 PM 150.547 11/7/2016 5:00:00 PM 136.7411 11/8/2016 5:00:00 PM 121.4397 11/9/2016 5:00:00 PM 97.86954 Name Comment %rhursday, November 10, 2016 Page I of 1 McGill Environmental Temperature Report Batch Bay Initials Amendments: compost woodwaste b06101716 Bay1306 Residuals: biosolids ,Start Date/Time: Comment 10/17/2016 2:15:23 PM .Stop Date/Time: Comment 10/24/2016 3:47:14 PM Blower: 0 Date/Tinte Teninerature Date/Tinte Nante 10/17/2016 5:00:00 PM 139.5839 10/17/2016 2:15:38 PM adt 10/18/2016 5:00:00 PM 152.228 10/19/2016 5:00:00 PM 162.5608 10/20/2016 5:00:00 PM 10/21/2016 5:00:00 PM 162.5484 154.2673 l 10/22/2016 5:00:00 PM 140.8446 10/23/2016 5:00:01 PM 115.7542 Contntent blended by luther filled by oscar )Monday, October 24, 2016 Page 1 of 1 McGill Environmental Temperature Report Batch Bay Initials Amendments: compost woodwaste e03 092016 BayE03 Residuals: biosolids Start Date/Time: Comment 9/21 /2016 8:19:10 AM Stop Date/Time: Commernt 9/29/2016 4:12:45 PM Blower: 0 Date/Tinte Tentnerature Date/Tinge Natne 9/21 /2016 5:00:00 PM 168.5305 9/21 /2016 8:19:28 AM adt 9/22/2016 5:00:00 PM 173.3509 9/24/2016 5:00:00 PM 167.653 9/25/2016 5:00:01 PM 163.6361)n � I 9/26/2016 5:00:00 PM 157.0854 9/27/2016 5:00:00 PM 152.71 9/28/2016 5:00:00 PM 124.2454 Continent blended by luther filled by roman 'Thursday, September 29, 2016 Page I of I McGill Environmental Temperature Report Batch Bay b01 081616 BayB01 Start Date/Time: 8/18/2016 8:33:01 AM Stop Date/Time: 8/24/2016 8:07:02 AM Slower: 0 Date/Time 8/18/2016 5:00:04 PM 8/19/2016 5:00:00 PM 8/20/2016 5:00:03 PM 8/21/2016 5:00:01 PM 8122/2016 5:00:00 PM 8/23/2016 5:00:03 PM Initials Amendments: compost woodwaste Residuals: biosolids Comment Comment Temnerature Date/Time Name 158.9393 8/18/2016 8:33:14 AM adt 152.4752 154.1314 141.7963 123.6397 1 1 97.86954 Comment filled by earl Wednesday, August 24, 2016 Page I of I McGill Environmental Temperature Report Batch Bay Initials Amendments: compost woodwaste e05070716 BayE05 Residuals: biosolids Start Date/Time: Comment 7/7/2016 11:11:10 AM Stop DatelTime: Comment 7/14/2016 7:39:44 AM Blower: 0 Date/Time Temperature Date/Time Name 7/7/2016 5:00:00 PM 156.0842 7/7/2016 11:15:27 AM f.b.t. 7/8/2016 5:00:00 PM 155.5775 7/9/2016 5:00:00 PM 146.5548 7/10/2016 5:00:00 PM 7/11/2016 5:00:00 PM 146.5548 127.2735 5' �V ' 7/12/2016 5:00:00 PM 127.2859 7/13/2016 5:00:00 PM 95.01443 Comment blended by luther and filled by oscar 'Thursday, July 14, 2016 Page I of 1 4 McGill Environmental Temperature Deport Batch Bay Initials Amendments: compost woodwaste e04 060716 BayE04 Residuals: biosolids Start Date/Time: Comment 6/7/2016 10:18:58 AM ,Stop DatelTime: Comment 6/15/2016 8:15:56 AM dower: 0 Date/Time Temperature Date/Time Name Comment 6/7/2016 5:00:01 PM 142.921 6/7/2016 10:19:18 AM adt blended by otis filled by oscar 6/8/2016 5:00:00 PM 142.8716 6/9/2016 5:00:00 PM 138.4221 6/10/2016 5:00:00 PM 148.4829 6/11/2016 5:00:00 PM 146.8144 d_ 6/12/2016 5:00:00 PM 146.6166 6/13/2016 5:00:00 PM 139.9052 ll 6/14/2016 5:00:00 PM 122.997 Wednesday, June 15, 2016 Page I of I McGill Environmental Temperature Report Batch Bay Initials Amendments: compost woodwaste b03 050916 BayB03 Residuals: biosolids ,Start Date/Time: Comment 5/9/2016 10:26:34 AM Stop Date/Time: Comment /5/17/2016 11:37:32 AM ,Blower: 0 Date/Time Temperature Date/Time Name Comment 5/9/2016 5:00:00 PM 142.7851 5/9/2016 10:26:48 AM adt blended and filled by luther 5/10/2016 5:00:00 PM 141.9075 5/11/2016 5:00:00 PM 160.7439 5/12/2016 5:00:00 PM 171.5711 5/13/2016 5:00:00 PM 166.3552 5/14/2016 5:00:00 PM 145.5166 5/15/2016 5:00:00 PM 125.3454 VV 5/16/2016 5:00:00 PM 105.6562 Tuesday, May 17, 2016 Page I of 1 McGill Environmental Temperature Report Batch Bay Lutials Amendments: compost woodwaste e09 041916 BayE09 Residuals: biosolids Start Date/Time: Comment 4/20/2016 9:05:09 AM Stop Date/Time: Comment 4/28/2016 3:00:08 PM glower: 0 Date/Time Temnerature Date/Time Name Comment 4/20/2016 5:00:00 PM 158.7169 4/20/2016 9:05:25 AM adt blended by luther filled by roman 4/21/2016 5:00:00 PM 160.4843 4/22/2016 5:00:00 PM 147.5189 4/23/2016 5:00:00 PM 131.2781 4/24/2016 5:00:00 PM 127.5454 j 4/25/2016 5:00:00 PM 114.6047 4/26/2016 5:00:00 PM 121.4273 4/27/2016 5:00:00 PM 121.2296 Thursday, April 28, 2016 Page 1 of I McGill Environmental Temperature Report Batch Bay Initials Amendments: compost woodwaste e02 031016 BayE02 Residuals: biosolids Start Date/Time: Comment 3/10/2016 4:42:00 PM ,Stop Date/Time: Comment 3/18/2016 8:16:44 AM ,Blower: 0 Date/Time Temperature Date/Time Name Comment 3/10/2016 5:00:00 PM 81.22089 3/10/2016 4:42:16 PM adt blended by earl filled by pernell 3/11/2016 5:00:00 PM 182.6702 3/12/2016 5:00:00 PM 160.6079 3/11/2016 7:40:42 AM adt filled by pernell 3/13/2016 5:00:00 PM 165.3912 3/15/2016 5:00:00 PM 158.6056 3/16/2016 5:00:00 PM 150.1639 3/17/2016 5:00:00 PM 131.4264 Friday, March 18, 2016 Page 1 of 1 McGill Environmental Temperature deport Batch Bay Initials An:endnients: compost woodwaste a03 021016 BayA03 Residuals: biosolids �4tart Date/Time Comment 2/11 /2016 8:03:13 AM Stop Date/Time: Comment 2/19/2016 8:01:54 AM Blower: 0 Date/Time Temperature Date/Time 2/11/2016 5:00:00 PM 166.8372 2/12/2016 5:00:00 PM 172.2385 2/13/2016 5:00:00 PM 164.39 2/14/2016 5:00:00 PM 160.4102 ' 2/15/2016 5:00:00 PM 136.7906 0 2/16/2016 5:00:00 PM 107.881 2/17/2016 5:00:00 PM 94.07507 2/18/2016 5:00:00 PM 89.06937 Name Comment ,i riday, February 19, 2016 Page 1 of I McGill Environmental Temperature Report Batch Bay e03 012516 BayE03 Start Date/Time: 1/26/2016 8:47:28 AM .Stop Date/Time: 2/1/2016 4:28:09 PM Blower: 0 Date/Time 1/26/2016 5:00:00 PM 1/27/2016 5:00:00 PM 1/28/2016 5:00:00 PM 1/29/2016 5:00:00 PM 1/30/2016 5:00:00 PM 1/31/2016 5:00:00 PM Initials Amendments: Residuals: Comment Comment Temperature 138 152.1044 151.2763 145.257 154.6258 132.6253 biosolids Date/Time Name Comment 'Jonday, February 01, 2016 Page 1 of 1 Delwav Curing. Te t)erature Lo for Vector Reduction (VAR Legend : Yellow Block Indicates Start of Bay "R" Indicates Removal of Bay Monday 12/21/2015 AT 150.0 140.0 130.0 140.0 Tuesday 12/22/2015 AT 150.0 140.0 130.0 140.0 Wednesday 12/23/2015 AT 150.0 140.0 130.0 150.0 140 Thursday 12/24/2015 AT 150.0 140.0 130.0 150.0 140 Friday 12/25/2015 AT 150.0 140.0 130.0 150.0 140 Saturday 12/26/2015 Sunday 12/27/2015 Monday 12/28/2015 AT 150.0 140.0 130.0 150.0 130 Tuesday 12/29/2015 AT 1 150.0 140.0 130.01 150.0 130 Wednesday 12/30/2015 AT 150.0 140.0 130.0 140.0 130 Thursday 12/31/2015 AT 130.0 124.0 110.0 120.0 130 Friday 1/1/2016 AT 130.0 124.0 110.0 120.0 130 Saturday 1/2/2016 Sunday 1/3/2016 Monday 1/4/2016 AT 90.0 110.0 100.0 100.0 140 Tuesday 1/5/2016 AT 90.0 110.0 100.0 100.0 140 Wednesday 1/6/2016 AT 90.0 110.01 100.0 100.0 140 Thursday 1/7/2016 AT 90.0 110.0 100.0 100.0 140 Friday 1/8/2016 AT 90.0 R 100.0 100.0 140 Saturday 1/9/2016 Sunday 1/10/2016 Monday 1/11/2016 AT 90.0 138.0 100.0 100.0 140 Tuesday 1/12/2016 AT 90.0 148.0 100.0 R 160 Wednesday 1/13/2016 AT 90.0 150.0 R 146.0 160 Thursday 1/14/2016 AT 90.0 160.0 160.0 154 Friday 1/15/2016 AT 90.0 154.0 154.0 160.0 154 Saturday 1/16/2016 90.0 140.0 154.0 160.0 154 Sunday 1/17/2016 Monday 1/18/2016 AT 90.0 140.0 140.0 140.0 140 Tuesday 1/19/2016 AT 1 90.0 140.01 140.0 140.0 140 Wednesday 1/20/2016 AT R 140.0 140.0 140.0 140 Thursday 1/21/2016 AT 140.0 140.0 130.0 140 Friday 1/22/2016 AT 130.0 140.0 140.0 130.0 140 Saturday 1/23/2016 Sunday 1/24/2016 Monday 1/25/2016 AT 140.0 130.0 140.0 130.01 1 140 Stock pile beside E building 140.0 Tuesday 1/26/2016 AT 140.0 130.0 140.0 130.0 140 Wednesday 1/27/2016 AT 140.0 130.0 140.0 130.0 140 Thursday 1/28/2016 AT 140.0 130.0 140.0 R 140 Friday 1/29/2016 AT 140.0 130.0 140.0 Blend R Saturday 1/30/2016 Sunday 1/31/2016 Monday 2/1/2016 AT 110.0 100.0 120.0 160.0 160 Tuesday 2/2/2016 AT 110.0 100.0 120.0 160.0 160 Wednesday 2/3/2016 AT 110.01 100.0 120.0 160.0 150 Thursday 2/4/2016 AT 100.0 110.0 110.0 150.0 150.0 Friday 2/5/2016 AT 100.0 R 110.0 150.0 150.0 Saturday 2/6/2016 Blend Sunday 2/7/2016 Monday 2/8/2016 AT 90.0 140.01 100.0 140.0 140 Tuesday 2/9/2016 AT 90.0 140.0 100.0 140.0 140 Wednesday 2/10/2016 AT 90.0 140.0 100.0 140.0 140 Thursday 2/11/2016 AT 90.0 140.0 100.01 120.0 1 140 Friday 2/12/2016 AT 90.0 140.0 100.0 R 140 Saturday 2/13/2016 R Blend Sunday 2/14/2016 Monday 2/15/2016 AT 90.0 150.0 R 152.0 140 Tuesday 2/16/2016 AT 90.0 150.0 152.0 140 Wednesday 2/17/2016 AT 90.0 150.0 148.0 152.0 140 Thursday 2/18/2016 AT 90.0 150.0 148.0 152.0 140 Friday 2/19/2016 AT R 144.0 148.0 152.0 140 Saturday 2/20/2016 Sunday 2/21/2016 Monday 2/22/2016 AT 150.0 100.0 136.0 148.0 120 Tuesday 2/23/2016 AT 150.0 100.0 136.0 148.0 120 Wednesday 2/24/2016 AT 150.0 100.0 136.0 148.0 120 Thursday 2/25/2016 AT 150.0 100.0 136.0 148.0 120 Friday 2/26/2016 AT 150.0 100.0 136.0 148.0 120 Saturday 2/27/2016 Sunday 2/28/2016 Monday 2/29/2016 AT 100.0 110.0 130.0 140.0 120 Tuesday 3/1/2016 d77AT 100.0 110.01 130.01 140.01 1 120 140.0 140.0 140.0 140.0 140.0 140.0 140.0 140.0 140.0 140.0 136.0 136.0 136.0 136.0 136.0 136.0 136.0 136.0 136.0 Stock pile beside E building 150.0 150.0 150.0 150.0 150.0 150.0 150.0 Wednesday 3/2/2016 AT 100.0 110.0 130.0 110.0 120 Thursday 3/3/2016 AT 100.0 110.0 130.0 110.0 120 Friday ' 3/4/2016 AT 100.0 110.0 130.0 110.0 120 Saturday 3/5/2016 R Sunday 3/6/2016 R Monday 3/7/2016 AT 100.0 130.0 140.0 R Tuesday 3/8/2016 AT 100.0 160.0 130.0 140.0 R Wednesday 3/9/2016 AT R 160.0 130.0 140.0 R Thursday 3/10/2016 AT R 160.0 130.01 140.0 R Friday 3/11/2016 AT R 148.0 130.0 140.0 SB Saturday 3/12/2016 Sunday 3/13/2016 Monday 3/14/2016 AT 150.0 130.0 140.0 150 Tuesday 3/15/2016 AT 154.0 150.0 130.0 140.0 150 Wednesday 3/16/2016 AT 154.0 150.0 130.0 Blend 150 Thursday 3/17/2016 AT 154.0 150.0 130.0 150.0 150 Friday 3/18/2016 AT 154.0 150.0 R 150.0 150 Saturday 3/19/2016 SB Sunday 3/20/2016 Monday 3/21/2016 AT 160.0 150.0 156.0 160.0 150 Tuesday 3/22/2016 AT 160.0 150.0 156.0 160.0 150 Wednesday 3/23/2016 AT 160.0 R 150.0 160.0 150 Thursday 3/24/2016 AT 150.0 R 150.0 156.0 110 Friday 3/25/2016 AT 150.0 150.0 156.0 110 Saturday 3/26/2016 Sunday 3/27/2016 Monday 3/28/2016 AT 110.0 150.0 100.0 120.0 R Tuesday 3/29/2016 AT 110.0 150.0 100.0 120.0 R Wednesday 3/30/2016 AT 110.0 150.0 100.0 R Thursday 3/31/2016 AT 110.0 150.0 100.0 Blend 148 Friday 4/1/2016 AT 110.0 150.0 100.0 150.0 148 Saturday 4/2/2016 Sunday 4/3/2016 Monday 4/4/2016 AT 110.0 126.0 R 150.0 156 Tuesday 4/5/2016 AT 110.0 126.0 R 150.0 156 Wednesday 4/6/2016 1 AT 1 110.01 126.0 R 150.0 156 150.0 150.0 150.0 150.0 150.0 150.0 150.0 150.0 Stock pile behind screen 150.0 138.0 140.0 138.0 140.0 138.0 140.0 138.0 140.0 138.0 140.0 138.0 140.0 138.0 140.0 138.0 140.0 138.0 140.0 138.0 138.0 138.0 138.0 138.0 138.0 138.0 138.0 Thursday 4/7/2016 AT 110.0 126.0 150.0 156 Friday 4/8/2016 AT R 126.0 138.0 150.0 156 Saturday 4/9/2016 Sunday 4/10/2016 Monday 4/11/2016 AT 120.0 148.0 150.0 148 Tuesday 4/12/2016 AT 162.0 120.0 148.0 144.0 148 Wednesday 4/13/2016 AT 162.0 120.0 148.0 144.0 148 Thursday 4/14/2016 AT 162.0 120.0 148.0 144.0 148 Friday 4/15/2016 AT 162.0 120.0 148.0 144.0 148 Saturday 4/16/2016 Sunday 4/17/2016 Monday 4/18/2016 AT 150.0 110.0 120.0 R 120 Tuesday 4/19/2016 AT 150.0 110.0 120.0 Blend 120 Wednesday 4/20/2016 AT 150.0 110.0 120.0 160.0 120 Thursday 4/21/2016 AT 150.0 110.0 120.0 160.0 120 Friday 4/22/2016 AT 150.0 110.0 120.0 160.0 120 Saturday 4/23/2016 Sunday 4/24/2016 Monday 4/25/2016 AT 146.0 100.0 120.0 154.0 100 Tuesday 4/26/2016 AT 146.0 100.0 120.0 154.0 100 Wednesday 4/27/2016 AT 146.0 100.0 R 154.0 100 Thursday 4/28/2016 AT 146.0 R 150.0 100 Friday 4/29/2016 AT 146.0 152.0 150.0 100 Saturday 4/30/2016 Sunday 5/1/2016 Monday 5/2/2016 AT 146.0 154.0 152.0 156.0 140 Tuesday 5/3/2016 AT 146.0 154.0 152.0 156.0 140 Wednesday 5/4/2016 AT 146.0 154.0 152.0 156.0 140 Thursday 5/5/2016 AT 146.0 154.0 152.0 156.0 140 Friday 5/6/2016 AT 146.0 154.0 152.0 156.0 R Saturday 5/7/2016 Sunday 5/8/2016 Monday 5/9/2016 AT 120.0 140.0 120.0 R 120 Tuesday 5/10/2016 AT 120.0 140.0 120.0 Blend 120 Wednesday 5/11/2016 AT 120.0 140.0 120.0 160.0 120 Thursday 5/12/2016 AT R 140.0 120.0 160.0 120 138.0 138.0 Friday 5/13/2016 AT 140.0 120.0 160.0 120 Saturday 5/14/2016 Sunday 5/15/2016 Monday 5/16/2016 AT 140.01 130.0 120.0 160.0 160 Tuesday 5/17/2016 AT 140.0 130.0 120.0 160.0 160 Wednesday 5/18/2016 AT 140.0 130.0 120.0 160.0 160 Thursday 5/19/2016 AT 140.0 130.0 120.0 160.0 160 Friday 5/20/2016 AT 140.0 130.0 120.0 160.0 160 Saturday 5/21/2016 Sunday 5/22/2016 Monday 5/23/2016 AT 140.0 120.0 140 Tuesday 5/24/2016 AT 140.0 120.0 R 140 Wednesday 5/25/2016 AT 140.0 R 120.0 Blend 140 Thursday 5/26/2016 AT 140.0 120.0 150.0 140 Friday 5/27/2016 AT 140.0 140.0 120.0 150.0 140 Saturday 5/28/2016 Sunday 5/29/2016 Monday 5/30/2016 AT Tuesday 5/31/2016 AT 130.0 140.0 120.0 150.0 140 Wednesday 6/1/2016 AT 130.0 140.0 120.0 150.0 140 Thursday 6/2/2016 AT 130.0 140.0 R 150.0 140 Friday 6/3/2016 AT 130.0 140.0 150.0 140 Saturday 6/4/2016 Sunday 6/5/2016 Monday 6/6/2016 AT 120.0 122.0 160.0 140.0 140 Tuesday 6/7/2016 AT 120.0 122.0 160.0 140.0 140 Wednesday 6/8/2016 AT 120.0 122.0 160.0 140.0 140 Thursday 6/9/2016 AT 100.0 120.0 150.0 R R Friday 6/10/2016 AT 100.0 120.0 150.0 Blend Saturday 6/11/2016 Sunday 6/12/2016 Monday 6/13/2016 AT 100.0 110.0 120.0 160.0 160 Tuesday 6/14/2016 AT 100.0 110.0 120.0 160.0 160 Wednesday 6/15/2016 AT R 110.0 120.01 160.0 160 Thursday 6/16/2016 AT 110.0 120.0 1 0.01 1 160 Friday 6/17/2016 AT 156.0 110.0 120.0 158.0 158 Saturday 6/18/2016 Sunday 6/19/2016 Monday 6/20/2016 AT 156.0 R 120.0 130.0 158 Tuesday 6/21/2016 AT 150.0 124.0 130.0 158 Wednesday 6/22/2016 AT 150.0 160.01 124.0 130.01 120 Thursday 6/23/2016 AT 150.0 160.0 124.0 130.0 120 Friday 6/24/2016 AT 150.0 160.0 R 130.0 120 Saturday 6/25/2016 Sunday 6/26/2016 Monday 6/27/2016 AT 150.0 160.0 154 R 120 Tuesday 6/28/2016 AT 150.0 160.0 154 120 Wednesday 6/29/2016 AT 150.0 160.0 154.0 154.0 120 Thursday 6/30/2016 AT 150.0 160.0 154.0 154.0 120 Friday 7/1/2016 AT 150.0 160.0 154.0 154.0 120 Saturday 7/2/2016 Sunday 7/3/2016 Monday 7/4/2016 AT Tuesday 7/5/2016 AT 120.0 124.0 140.0 154.0 R Wednesday 7/6/2016 AT 120.0 124.0 140.0 154.0 160 Thursday 7/7/2016 AT 120.0 124.0 140.0 154.0 160 Friday 7/8/2016 AT R 124.0 140.0 154.0 160 Saturday 7/9/2016 Sunday 7/10/2016 Monday 7/11/2016 AT 132.0 124.0 126.0 138.0 156 Tuesday 7/12/2016 AT 132.0 124.0 126.0 R 156 Wednesday 7/13/2016 AT 132.01 124.0 126.0 160 156 Thursday 7/14/2016 AT 132.0 R 126.0 160.0 156 Friday 7/15/2016 AT Saturday 7/16/2016 Sunday 7/17/2016 Monday 7/18/2016 AT 132.0 150.0 126.0 160.0 146 Tuesday 7/19/2016 AT 132.0 150.0 126.0 160.0 146 Wednesday 7/20/2016 AT 132.0 150.0 R 160.0 146 Thursday 7/21/2016 1 AT 1 132.01 150.01 1 160.01 1 146 Friday 7/22/2016 1 AT 1 132.01 150.01 156.01 160.01 1 146 Saturday 7/23/2016 Sunday 7/24/2016 Monday 7/25/2016 AT 104.0 146.0 140.0 156.0 100 Tuesday 7/26/2016 AT 100.0 104.0 140.0 156.0 100 Wednesday 7/27/2016 AT 100.0 104.0 140.0 140.0 R Thursday 7/28/2016 AT 100.0 104.01 140.0 140.0 140 Friday 7/29/2016 AT 100.0 104.0 140.0 140.0 180 Saturday 7/30/2016 R Sunday 7/31/2016 Monday 8/1/2016 AT R 138.0 120.0 160.0 146 Tuesday 8/2/2016 AT 138.01 120.0 160.0 146 Wednesday 8/3/2016 AT 160.0 138.0 110.0 160.0 134 Thursday 8/4/2016 AT 160.0 R 110.0 156.0 134 Friday 8/5/2016 AT 160.0 110.0 156.0 134 Saturday 8/6/2016 Sunday 8/7/2016 Monday 8/8/2016 AT 124.0 130.0 110.0 124.0 110 Tuesday 8/9/2016 AT 120.0 140.01 160.0 124.0 110 Wednesday 8/10/2016 AT 120.0 140.0 160.0 124.0 110 Thursday 8/11/2016 AT 120.0 140.0 R 124.0 110 Friday 8/12/2016 AT 120.0 140.0 R 110 Saturday 8/13/2016 Sunday 8/14/2016 Monday 8/15/2016 AT 120.0 140.0 160.0 154.0 130 Tuesday 8/16/2016 AT 120.0 140.0 160.0 154.0 130 Wednesday 8/17/2016 AT 120.0 140.0 160.01 154.0 130 Thursday 8/18/2016 AT 120.0 120.0 140.0 146.0 130 Friday 8/19/2016 AT 120.0 120.0 140.0 146.0 R Saturday 8/20/2016 Sunday 8/21/2016 Monday 8/22/2016 AT 118.0 100.0 106.0 120.0 178 Tuesday 8/23/2016 AT 118.0 100.0 106.0 120.0 178 Wednesday 8/24/2016 AT 118.0 96.0 104.0 130.0 158 Thursday 8/25/2016 AT 118.0 96.01 104.0 130.0 158 Friday 8/26/2016 AT Saturday 8/27/2016 Sunday 8/28/2016 CB4 filled from old pile Monday 8/29/2016 AT R 96.0 104.0 130.0 120 Tuesday 8/30/2016 AT 96.0 104.0 130.0 120 Wednesday 8/31/2016 AT 148.0 96.0 104.0 R 120 Thursday 9/1/2016 AT 148.0 96.0 104.0 120 Friday 9/2/2016 AT 1 148.0 96.0 104.0 154.0 120 Saturday 9/3/2016 Sunday 9/4/2016 Monday 9/5/2016 AT Tuesday 9/6/2016 AT 148.0 96.0 104.0 154.0 120 Wednesday 9/7/2016 AT 148.01 96.0 104.0 154.0 120 Thursday 9/8/2016 AT 148.0 96.0 104.0 154.0 120 Friday 9/9/2016 AT 148.0 R 104.0 154.0 120 Saturday 9/10/2016 Sunday 9/11/2016 Monday 9/12/2016 AT 146.0 1S0.0 104.0 160.0 110 Tuesday 9/13/2016 AT 146.0 150.0 104.0 160.0 110 Wednesday 9/14/2016 AT 146.0 150.0 R 160.0 110 Thursday 9/15/2016 AT 146.0 150.0 160.0 110 Friday 9/16/2016 AT 146.0 150.0 170.0 160.0 110 Saturday 9/17/2016 Sunday 9/18/2016 Monday 9/19/2016 AT 146.0 140.0 170.0 160.0 110 Tuesday 9/20/2016 AT 146.0 140.0 170.0 160.0 110 Wednesday 9/21/2016 AT 146.01 140.0 170.0 160.0 110 Thursday 9/22/2016 AT 146.0 140.0 170.0 160.0 110 Friday 9/23/2016 AT 146.0 140.0 170.01 160.0 110 Saturday 9/24/2016 Sunday 9/25/2016 Monday 9/26/2016 AT 144.0 130.0 152.0 120.0 110 Tuesday 9/27/2016 AT 144.0 130.0 152.0 120.0 R Wednesday 9/28/2016 AT 144.0 130.0 152.0 120.0 160 Thursday 9/29/2016 AT 144.0 130.0 152.0 120.0 160 Friday 9/30/2016 AT 144.0 130.0 152.0 120.0 160 Saturday 10/1/2016 Sunday 10/2/2016 Monday 10/3/2016 AT 144.0 120.01 138.01 R 152 Tuesday 10/4/2016 AT 144.0 120.0 138.0 140.0 152 Wednesday 10/5/2016 AT 144.0 120.0 138.0 140.0 152 Thursday 10/6/2016 AT 144.0 R 138.0 140.0 152 Friday 10/7/2016 AT 144.0 138.0 140.0 152 Saturday 10/8/2016 Sunday 10/9/2016 Monday 10/10/2016 AT 150.0 160.0 160.0 160.0 144 Tuesday 10/11/2016 AT 150.0 160.0 160.0 160.0 144 Wednesday 10/12/2016 AT 150.0 160.0 160.01 160.0 144 Thursday 10/13/2016 AT 150.0 160.0 160.0 160.0 144 Friday 10/14/2016 AT 150.0 160.0 160.0 160.0 144 Saturday 10/15/2016 Sunday 10/16/2016 Monday 10/17/2016 AT R 150.0 130.0 160.0 130 Tuesday 10/18/2016 AT 150.0 130.0 160.0 130 Wednesday 10/19/2016 AT 170.0 150.0 130.0 160.0 130 Thursday 10/20/2016 AT 160.0 150.0 R 160.0 130 Friday 10/21/2016 AT 160.0 150.0 160.0 130 Saturday 10/22/2016 Sunday 10/23/2016 Monday 10/24/2016 AT 170.0 160.0 162.0 158.0 130 Tuesday 10/25/2016 AT 170.0 160.0 162.01 158.0 130 Wednesday 10/26/2016 AT Thursday 10/27/2016 AT Friday 10/28/2016 AT Saturday 10/29/2016 Sunday 10/30/2016 Monday 10/31/2016 AT Tuesday 11/1/2016 AT Wednesday 11/2/2016 AT Thursday 11/3/2016 AT Friday 11/4/2016 AT Saturday 11/5/2016 Sunday 11/6/2016 Monday 11/7/2016 AT Tuesday 1 11/8/2016 1 AT Wednesday 11/9/2016 AT 120.0 152.0 130.0 152.0 130 Thursday 11/10/2016 AT 120.0 152.0 130.0 152.0 130 Friday 11/11/2016 AT 120.0 152.0 130.0 152..0 R Saturday 11/12/2016 Sunday 11/13/2016 Monday 11/14/2016 AT 120.0 152.0 130.0 152.0 154 Tuesday 11/15/2016 AT 120.0 152.0 130.0 152.0 156 Wednesday 11/16/2016 AT 120.0 152.0 130.0 152.0 156 Thursday 11/17/2016 AT 120.0 152.0 130.0 152.0 156 Friday 11/18/2016 AT 120.0 152.0 130.0 152.0 156 Saturday 11/19/2016 Sunday 11/20/2016 Monday 11/21/2016 AT R 140.0 130.0 144.0 148 Tuesday 11/22/2016 AT 140.0 130.01 144.0 148 Wednesday 11/23/2016 AT 150.0 140.0 R 144.0 148 Thursday 11/24/2016 AT Friday 1 11/25/2016 AT 150.0 140.0 144.0 148 Saturday 11/26/2016 Sunday 11/27/2016 Monday 11/28/2016 AT 160.0 R 164.0 120.0 110 Tuesday 11/29/2016 AT 160.0 164.0 120.0 110 Wednesday 11/30/2016 AT 160.0 158.0 160.0 100.0 110 Thursday 12/1/2016 AT 160.0 158.0 158.0 100.0 R Friday 12/2/2016 AT 160.0 158.0 158.0 R 90 Saturday 12/3/2016 Sunday 12/4/2016 Monday 12/5/2016 AT 144.0 150.0 158.0 148.0 140 Tuesday 12/6/2016 AT 144.0 150.0 158.0 148.0 140 Wednesday 12/7/2016 AT 144.0 150.0 140.0 148.0 140 Thursday 12/8/2016 AT R 110.0 140.0 158.0 140 Friday 12/9/2016 AT 110.01 140 158.0 140 Saturday 12/10/2016 Sunday 12/11/2016 Monday 12/12/2016 AT 160.0 110 140.0 158.0 128 Tuesday 12/13/2016 AT 160.0 110.0 140.0 158.0 128 Wednesday 12/14/2016 AT 160.0 110.0 140.0 158.0 128 12/14/2016 AT 160.0 110.0 140.0 158.0 128 12/15/2016 AT 160.0 110.0 R 154.0 128 12/16/2016 AT 160.0 110.0 154.0 128 12/17/2016 12/18/2016 12/19/2016 AT 140.0 100.0 154.0 136.0 128 12/20/2016 AT 140.0 100.0 154.0 136.0 128 12/21/2016 AT 140.0 100.0 154.0 R 128 12/22/2016 AT 140.0 100.0 154.0 128 12/23/2016 AT 140.0 100.0 154.0 138.0 128 12/24/2016 12/25/2016 12/26/2016 AT 12/27/2016 AT 140.0 100.0 154.0 140.0 128 12/28/2016 AT 140.0 R 154.0 164.0 128 12/29/2016 AT 110.0 164.0 120.0 164.0 80 12/30/2016 T AT 110.01 164.01 120.0 164.0 80 ANALYSIS OF FINISHED COMPOST ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: WQ0006816 WWTP Name: NPDES Number: Monitoring Period: From 1/1/2016 To 1/31/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative I El Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alterative 5 0 Alterative 6 ❑ If applicable to alternative performed (Class A only indicate "Process to Further Reduce Pathogens": Compost Heat Drying ❑ Heat Treatment ❑ Thermophilic Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ .. Class B: Alternative 1 ❑ Alterative 2 ❑ _.... . _............................ . ............. . If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying[] I Composting ❑ jAcrobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number ol Excee- Frequency of Analysis y Sample Type Analytical Tech - nl ue Minimun Geo. Mean Maximus Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry Wei.-ht) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei.ht) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. Oz uptake) D Alt. 5 (14-Day Aerobic) 0 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Z G 17 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) i a.r,uur!lcn.r 15rYrlrtrrr.r ,rr.ti/J %rr 5p:r,rrr ,rqr ,r,t.r,r5 t,�11.>y r,J 5rrn.,trr rr ,r� ,u,rr}.�+r.rl5rr/ .r5•rt prr., JSr,Jrrrr,.r r/l�.5r �'rrryn •nlnp 5njl d/rttrr.rJ /uur 5nny p,tyt.r.rt.vt! r1 un 51•rnpuarllsnrlurn , .rr.ufl l5.r1 -rJ lu,rrulrrrrup,,t .uj1 u.aug5 ,r.rnrj urn.rhu�rj .r.�rur�rrsc{ ,Yuus✓1 !n pa,y 5,11-rrrrm 1 ; rtjl5ttr/tuu_! `' f arjJ uj 5nuultrurn,l I Id �• � • '— _— I. 111. •1I.�1 t• , I I11.�11111 I,� .I arlu.5.r11 Isrr1 c11n5.t1f M111. r.urrvr.rro (r, winy) cn palfmbg ( 5.r.rl.truumr1 Lurt/uru 1 64'R lit , bZ1'!£8 7131 ;, I joiltiol po$-anoinclon L.l J 1-i S V IV (1 -1 V-.) ] ko-1.x1 jL J,S Od tAj OD �� sr »Ia�� .r,f,Ilnil II"ti � , _� I,;Ir , ..;.•,::1 ts�alull+.i ungn.r{(/Jua/,f I,,rtprrJr! tybb8Z ON I r IIONf103�a 9NIISOdW09 ai� ,uta}5�� {r)u�niun.ii5ua III'1-51! i 1 •tia.>trrrrl�u.o fort/urrt.r liar/f !�t �p.�.ou .+r/f dNIt Withuu.o r/y.0 Purr/n v)Pp %pp ,l/lpf t/ pun inn,/ pvgt.f.+c.+.rd ra tit) tif.tnprtjd t+ttdurrr,+.rrar/l f�.ot .rill tr•luttp .+[nil rrrn.r.Ytrrcj .o•orrnincil !t) /1a5• SX.,urrt+ � Trr�fcralrurr� 5 ! .rrl1 nr dune//.rrfrntl t i I l t''O , � `tu��Jttl� un'Itl r✓frr+n.nrr Ito .nurn ti'n p.q-ttn/.a11 »d/.+tutr�nd /urcfaun . . +tl J l 7i1011Y ji-- Imidtrr 1 uu/ffr.ar��frr.'pf f.rnpul,! 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It?L7U(�il �t" IUf}l1CO II(7S :Atl011M09V1 .1,00 VNl'I MV3 111MA j(9 J.".1Ml4 wJ.lNU --—,.._�..,......_.._. �t1iil��I.lalljinfl►iu` '111 �, 17Vt?9Z ON '{ 113Nn0ul S+ t SNIISOdWOO S .u1�lti�� ite)uatuuu.1i111'1 II!')•�l1 SOIL CONTROL LAB Attn Ruth Kinq Snmnle Identification , Nutrients Nitrate kNO,-N) N Ph0RtYiY,f 35 P U Pmosphorus il"i Pn?as,;iw­ ias K 0, Potassium iK, Calf-'amy Ca, Ma Moisture. pH Value Date 24 J/L, Try wt Ru-'(1i r it Stability Indicator- 1 4 11/1) CO2 Evolution ]VIC1,KU mg 0 2 very .stable: 13000 401`1 0 4 f Maturity Indicator: CUCUmber Bioassay v f T I J Phirlts 0 Pathogens Fecal Goliform 520 NA 86 NA In erts 9_7 < Metal Aqlndex 10 ratio]—' Metals Size Distribution . I iAl - nig/k g MM 16 to 25 mg/kg 1, mg/kg 4 1. eac Pt rog/kg 2 k4xqan�, . , ; 2 (0- 17 , 0.5 .5 mg/kg 13 mg/kg mg/kg ZIF)c �: Zn 1 410 N. e ..,3, j lee) In Ir, 0 0 Analyst ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: W00006816 WWTP Name: NPDES Number: Monitoring Period: From 2/1/2016 To 2/28/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 0 Alternative 6 El If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 21 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray Li Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting, ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- s Frequency of Analysis. Sample Type Analytical Tech - nioue Minimu Geo. Mean%laximun Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei-htr Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) 0 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ® Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (type or print) Z -� r7 Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) r COMPOSTING US COUNCIL Seal of Testing Assurance Date Sampled/Received: 03 Feb. 16 / 05 Feb. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET u►soRAToar: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel: 831.724.5422 fax., 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis Not reported Not reported Moisture Content %, wet weight basis 42.7 I Organic Matter Content %, dry weight basis 45.2 pH units 7.06 Soluble Salts dS/m (mmhos/cm) 10 (electrical conductivity EC5) is Particle Size or Sieve Size maxium aggregate size, inches 0.25 1 Stability Indicator (respirometry) Stability Rating: COz Evolution mg COZ C/g OM/day 2.7 a+ Stable Mg COz-C/g TS/day 1.2 Maturity Indicator (bioassay) Percent Emergence average % of control 100.0 Relative Seedling Vigor average %of control 87.6 1 Select Pathogens PASS/FAIL: per US EPA Class A standard, 40 CFR § 50332(a) Pass Fecal coliform Pass Salmonella �I Trace Metals PASS/FAIL: per us EPA Class A As,Cd,Cr,Cu,Pb,Hg standard, 40 CFR § 503.13, Pass Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compostproducts on a prescribed basis andprovide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laborator) Group: Feb. 16 A Laboratory Number: 6020211-1/1 Assaf Sadeh �i 4�t �.. � www.compostlab.com r F, COMPOSTING US COUNCIL Seal of Testing LAssurance Date Sampled/Received: 03 Feb. 16105 Feb. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET LABORATORY: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 te% 831.724.5422 fax.- 831.724.3188 Compost Parameters _ Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis %, wet weight basis %, dry weight basis Nitrogen Total N 1.3 a 2.3 Phosphorus P205 1.7 3.0 Potassium K20 0.46 0.79 Calcium Ca 3.8 6.6 Magnesium Mg 0.20 0.35 Moisture Content %, wet weight basis 42.7 Organic Matter Content %, dry weight basis 45.2 pH units 7.06 Soluble Salts dS/m (mmhos/cm) 10 (electrical conductivity EC5) Particle Size or Sieve Size % under 9.5 ram, dw basis 100.0 3 Stability Indicator (respirometry) Stability Rating: CO2 Evolution mg CO2-C/g OM/day 2.7 Stable mg CO2-C/g TS/day 1.2 Maturity Indicator (bioassay) Percent Emergence average % of control 100.0 Relative Seedling Vigor average %of control 87.6 Select Pathogens PASS/FAIL.: per US EPA Class A standard, 40 CFR § 503.32(a) Pass Fecal coliform Pass Salmonella i Trace Metals PASS/FAIL: per US EPA Class A As,Cd,Cr,Cu,Pb,Hg fI standard, 40 CFR § 503.13, Pass Tables I and 3. Mo,Ni,Se,Zn i Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on aprescribed basis andprovide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laboratory Group: Feb.16 A Laboratory Number: 6020211-1/1 Analyst: Assaf Sadeh s < �� �t-=�+' • '" www.compostlab.com USCOMPOSTING :P COUNCIL —, Seal of Testing Assurance OF Date Sampled/Received: 03 Feb. 16 / 05 Feb. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification: Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET for NORTH CAROLINA DOT LABORATORY: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel.- 831.724.5422 fax: 831.724.3188 Compost Parameters Test Results Reported as (units of measure) Project Specification i (Allowable Limit) !Organic Matter Content 45.2 %, dry weight basis 25 - 65 H 7.06 Unitless 5.0 - 8.5 i Moisture Content 42.7 %, wet weight basis 30 - 60 Soluble Salts 10 dS/m (mmhos/cm) 5.0 dS/m, maximum (electrical conductiviv,) � %, dry weight passing through € 100.0 3 inch screen and 100% j Particle Size 100.0 1 inch screen and 90% minimum 100.0 3/4 inch screen and 65%minimum 100.0 1/4 inch screen 50% maximum t3 i Stability Indicator (respirometry) 2.7 mg CO2-C/g CINUday 5 8 CO2 Evolution ! Maturity Indicator (bioassay) 100.0 average % of control 80%, minimum Percent Emersrence I Relative Seedling Vigor 87.6 average % of control 80%, minimum l f Select Pathogens PASS/FAIL: Per US EPA Class A Pass Pass (Fecal Coliform) standard, 40 CFR 50332(a) s Metals Pass PASS/FAIL: Per US EPA Class A Pass jTrace 40 CFR 503.13, tables 1 and 3. I Inert Contamination (man-made) None Detected %, dry weight <1.0 % Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of -their compost customers. For additional information pertaining to compost use, the specific compost parameters tested for within the Seal of Testing assurance Program, or the program in general, log on to the US Composting Council's TMECC web -site at h tip.11www. tm ecc. o r, . This compost product has been sampled and tested as required by the Seal of Testing assurance Program on the United States Composting Council (USCG), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by contacting the compost producer (address at top of page). The USCC makes no warranties regarding this product or its content, quality. or suitability for any particular use. Laboratory Group: Feb. 16 A Laboratory Number: 6020211-1/1 Analyst: Assaf Sadeh www.compostlab.com ANALYTICAL CHEMISTS and BACTERIOLOGISTS Approved by State of Caldorrim SOIL CONTROL LAB 4 HANGAR WAY. wATSOW110 CALIFORMA ' o507d VSA McGill Environmental Systems P.O. Box 61 Harrelis, NC 28444 Attn: Ruth King Date Received: 05 Feb. 16 Sample Identification: Soil Builder Delway Sample ID #: 6020211 - 1/1 TEL: 831-724-5422 FAX: 831-724-3188 www.com,-ostlab.com Account #: 6020211-1 /1-2215 Group: Feb.16 A #25 Reporting Date: February 18, 2016 Nutrients Dry wt. As Rcvd. units Stability Indicator: Biologically Total Nitrogen: 2.3 1.3 % CO2 Evolution Respirometery Available C Ammonia (NH4-N): 1300 770 mg/kg mg CO2-C/9 OM/day 2.7 2.8 Nitrate (NO3-N): 510 290 mg/kg mg CO2-C/g TS/day 1.2 1.3 Org. Nitrogen (Org.-N): 2.1 1.2 % Stability Rating stable stable Phosphorus (as P205): 3.0 1.7 % Phosphorus (P): 13000 7600 mg/kg Potassium (as K20): 0.79 0.46 % Maturity Indicator: Cucumber Bioassay Potassium (K): 6600 3800 mg/kg Compost:Vermiculite(v:v) 1:2 Calcium (Ca): 6.6 3.8 % Emergence (%) 100 Magnesium (Mg): 0.35 0.20 % Seedling Vigor (%) 88 Sulfate (SO4-S): 4300 2500 mg/kg Description of Plants healthy Boron (Total B): 35 20 mg/kg Moisture: 0 42.7 % Sodium (Na): 0.27 0.15 % Pathogens Results Units Rating Chloride (Cl): 0.21 0.12 % Fecal Coliform 80 MPN/g pass pH Value: NA 7.06 unit Salmonella < 3 MPN/4g pass Bulk Density : 22 39 Ib/cu ft Date Tested: 05 Feb. 16 Carbonates (CaCO3): 44 25 lb/ton Conductivity (EC5): 10 NA mmhos/cm Organic Matter: 45.2 25.9 % Inerts % by weight Organic Carbon: 25.0 14.0 % Plastic < 0.5 Ash: 54.9 31.4 % Glass < 0.5 C/N Ratio 11 11 ratio Metal < 0.5 Aglndex > 10 > 10 ratio Sharps ND Metals Aluminum (AI) Arsenic (As): Cadmium (Cd): Chromium (Cr): Cobalt (Co) Copper (Cu): Iron (Fe): Lead (Pb): Manganese (Mn): Mercury (Hg): Molybdenum (Mo): Nickel (Ni): Selenium (Se): Zinc (Zn): 8800 16 < 1.0 26 8.4 160 11000 16 360 < 1.0 4.0 12 2.9 420 'A Limit 41 39 1200 1500 300 17 75 420 36 2800 units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mq/kq Size Distribution VIM % by weight > 50 0.0 25 to 50 0.0 16 to 25 0.0 3.5 to 16 0.0 3.3 to 9.5 0.0 4.0 to 6.3 1.3 2.0 to 4.0 2.9 c 2.0 95.8 was received and handled in accordance with TMECC procedures. Analyst: Assaf Sadeh ,- s ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WWTP Name: WQ Permit Number: NPDES Number: WQ0006816 Monitoring Period: From 3/1/2016 To 3/31/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alterative 2 ❑ Alternative 3 ❑ Alterative 4 ❑ Alternative 5 0 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 0 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ .: Class B: Alternative 1 ❑ Alternative 2 ❑ _.. _ __...._.._ _... _....._ .................. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑. Aerobic Digestion El_... Anaerobic Digestion ❑ _ .. .. . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- Frequency of Analysis Sample Type Analytical Tech - MUM ''9inimtin Geo. MeanNlaximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform 1 3 WN per 4 grams total solid (dry weir=ht) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑. Alt. 5 (14-Day Aerobic) 0 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (types or print) Land Applier Name and Title (if applicable)(type or print) Cam-' - Z. -477 - Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) UCOMPOSTING COUNCIL Seal of Testing Assurance Date Sampled/Received: 01 Mar. 16 / 02 Mar. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder- Delway COMPOST TEmNicAL DATA SHEET u►soRAToey: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel. • 831.724.5422 fax.- 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results s Plant Nutrients: % weight basis Not reported Not reported Moisture Content %, wet weight basis 53.3 Organic Matter Content %, dry weight basis 41.2 j pH units 6.76 Soluble Salts f dS/m (mmhos/ctn) 10 (electrical conductivity EC 5) e Particle Size or Sieve Size maxium aggregate size, inches _ 0.38 Stability Indicator (respirometry) Stability Rating: CO2 Evolution mg COz-C/g OWday 0.4 Very Stable mg COz-C/g TS/day 0.16 Maturity Indicator (bioassay) i s Percent Emergence average % of control 100.0 Relative Seedling Vigor average % of control 77.1 Select Pathogens PASS/FAIL: per US EPA Class A standard, 40 CFR § 50332(a) Pass Fecal coliform 1 i Pass Salmonella Trace Metals PASS/FAIL: per US EPA Class A As, Cd, Cr, Cu,Pb, Hg i standard, 40 CFR § 503-13, Pass Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laborator-% Group: Mar. 16 A Laboratory Number: 6030074-1/1 Analyst: Assaf Sadeh . �' www.compostlab.com UQ COMPOSTING VVV COUNCIL .090 Seal of Testing 6T"*) Assurance Date Sampled/Received: 01 Mar. 16 / 02 Mar. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder- Delway COMPOST TECHNICAL DATA SHEET . n.�...�w..... c-a ,k- A'1 L2•.nn-.. U/•.!'A nCn7C F 1• 471 '77A CA)) F-v 4'21 77A '2100 Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis %, wet weight basis %, dry weight basis Nitrogen Total N 0.96 2.1 I 6 Phosphorus P201 1.4 3.0 Potassium KO 0.35 0.75 Calcium Ca 2.9 6.3 Magnesium Mg 0.16 0.35 Moisture Content % wet weight basis 53.3 Organic Matter Content %, dry weight basis 41.2 pH units 6.76 Soluble Salts (electrical conductivity EC 5) dS/m (mmhos/cm) 10 Particle Size or Sieve Size % under 9.5 mm, dw basis 100.0 Stability Indicator (respirometry) Stability Rating: CO2 Evolution mg CO2-C/g OM/day 0.4 Very Stable mg CO,-C/g TS/day 0.16 Maturity Indicator (bioassay) - Percent Emergence average % of control 100.0 Relative Seedling Vigor average % of control 77.1 Select Pathogens PASS/FAIL: per US EPA Class A standard, 40 CFR § 503.32(a) Pass Fecal coliform Pass Salmonella Trace Metals PASS/FAIL: per US EPA Class A As,Cd,Cr,Cu,Pb,Hg standard, 40 CFR § 503.13, Pass Tables I and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laborator, Group: Mar.16 A Laborator+ Number: 6030074-1/1 Analyst: Assaf Sadeh G<�.1• www.compostlab.com USCOMPOSTING COUNCIL**, Seal of Testing J-PS �+ Assurance �-oF _, ' Date Sampled/Received: 01 Mar. 16 / 02 Mar. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification: Compost Soil Builder- Delway COMPOST TECHNICAL DATA SHEET for NORTH CAROLINA DOT I LABORATORY: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel. • 831.724.5422 fax: 831.724.3188 € Compost Parameters Test Results Reported as (units of measure) I Project Specification Organic Matter Content 41.2 %, dry weight basis 25 - 65 1 H 6.76 Unitless 5.0 - 8.5 Moisture Content 53.3 %, wet weight basis 30 - 60 Soluble Salts 10 dS/m (mmhos/cm) 5.0 dS/m, maximum (electrical conductivii � ) dry weight passing through 100.0 3 inch screen and 100% 100.0 1 inch screen and 90% minimum Particle Size I l 100.0 3/4 inch screen and 65%minimum ! f 94.6 1/4 inch screen 50% maximum 4j Stability Indicator (respirometry) i 0.4 mg CO2-C/g OM/day <_ 8 CO2 Evolution Maturity Indicator (bioassay) i 100.0 average % of control 80%,minimum Percent Emengence Relative Seedling Vigor 77.1 average % of control 80%, minimum i Select Pathogens PASSNAIL: Per US EPA Class A Pass Pass (Fecal Coliform) standard, 40 CFR 503.32(a) Trace Metals Pass PASS/FAIL: Per US EPA Class A Pass 40 CFR 503.13_ tables 1 and 3. Inert Contamination (man made)T None Detected %, dry weight <1.0 Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of -their compost customers. For additional information pertaining to compost use, the specific compost parameters tested for within the Seal of Testing assurance Program, or the program in general, log on to the US Composting Council's TMECC web -site at htt .IAwww.tmecc.org, This compost product has been sampled and tested as required by the Seal of Testing assurance Program on the United States Composting Council (USCG), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by contacting the compost producer (address at top of page). The USCC makes no warranties regarding this product or its content, quality. or suitability for any particular use. Laboratory Group: Mar.16 A Laboratory Number: 6030074-1/1 Analyst: Assaf Sadeh www.compostiab.com ANALYTICAL CHEMISTS and BACTERIOLOGISTS Approved by Stole of California SOIL CONTROL LAB 42HAMGARWAY WATSONVILLF tCAUFORNIA 9SO76 JSA McGill Environmental Systems P.O. Box 61 Harrells, NC 28444 Attn: Ruth King Date Received: 02 Mar. 16 Sample Identification: Soil Builder- Delway Sample ID #: 6030074 - 1/1 TEL: 831-724-5422 FAX: 831-724-3188 www.com. ostlab.corn Account* 6030074-1 /1-2215 Group: Mar. 16 A #9 Reporting Date: March 17, 2016 Nutrients Dry wt. As Rcvd. units Stability Indicator: Biologically Total Nitrogen: 2.1 0.96 % CO2 Evolution Respirometery Available C Ammonia (NH4-N): 1600 730 mg/kg mg CO2-C/9 OM/day 0.4 0.9 Nitrate (NO3-N): 1200 540 mg/kg mg CO2-C/g TS/day 0.16 0.37 Org. Nitrogen (Org.-N): 1.8 0.84 % Stability Rating very stable very stable Phosphorus (as P205): 3.0 1.4 % Phosphorus (P): 13000 6200 mg/kg Potassium (as K20): 0.75 0.35 % Maturity Indicator: Cucumber Bioassay Potassium (K): 6200 2900 mg/kg Compost:Vermiculite(v:v) 1:2 Calcium (Ca): 6.3 2.9 % Emergence (%) 100 Magnesium (Mg): 0.35 0.16 % Seedling Vigor (%) 77 Sulfate (SO4-S): 4600 2100 mg/kg Description of Plants stunted Boron (Total B): 40 19 mg/kg Moisture: 0 53.3 % Sodium (Na): 0.25 0.12 % Pathogens Results Units Rating Chloride (Cl): 0.2 0.096 % Fecal Coliform 40 MPN/g pass pH Value: NA 6.76 unit Salmonella < 3 MPN/4g pass Bulk Density : 23 49 Ib/cu ft Date Tested: 02 Mar. 16 Carbonates (CaCO3): 61 28 lb/ton Conductivity (EC5): 10 NA mmhos/cm Organic Matter: 41.2 19.2 % Inerts % by weight Organic Carbon: 21.0 9.8 % Plastic < 0.5 Ash: 58.8 27.5 % Glass < 0.5 C/N Ratio 10 10 ratio Metal < 0.5 Ag Index > 10 > 10 ratio JISharps ND Metals Dry wt. EPA Limit units Aluminum (AI) 9300 - mg/kg Arsenic (As): 14 41 mg/kg Cadmium (Cd): < 1.0 39 mg/kg Chromium (Cr): 29 1200 mg/kg Cobalt (Co) 13 - mg/kg Copper (Cu): 180 1500 mg/kg Iron (Fe): 12000 - mg/kg Lead (Pb): 13 300 mg/kg Manganese (Mn): 360 - mg/kg Mercury (Hg): < 1.0 17 mg/kg Molybdenum (Mo): 3.6 75 mg/kg Nickel (Ni): 13 420 mg/kg Selenium (Se): 2.5 36 mg/kg Zinc (Zn): 420 2800 mg/kg *Sample was received and handled in accordance with l Size Distribution MM % by weight > 50 0.0 25 to 50 0.0 16 to 25 0.0 9.5 to 16 0.0 6.3 to 9.5 5.4 4.0 to 6.3 15.5 2.0 to 4.0 28.3 < 2.0 50.9 procedures. Analyst: Assaf Sadeh ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WWTP Name: WQ Permit Number: NPDES Number: WQ0006816 Monitoring Period: From 4/1/2016 To 4/30/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alterative i ❑ Alternative 2 ❑ Alternative 3 ❑ .... Alternative 4 ❑ Alternative 5 R1 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 0 Heat Drying El Heat Treatment ElThelmophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ :... .... .. ... Class B: Alterative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Num er o Excee- Frequency of Analysis Ys Sample Type Ana"cal Tech - maue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids WN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) 0 Alt. 6 (Alk. Stabilization Cj Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) El Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) bd "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cocicman/Compliance Manager Preparer Name and Title (type or print) ,�, &� --I - -- Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) 2 •6-/7 Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) r 1 A UCOMPOSTING COUNCIL .Setif of Testing Assurance Date Sampled/Received: 04 Apr. 16 / 05 Apr. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET LABORATORY: Soil Control lab; 42 Hangar Way; Watsonville, CA' 95076 tek 831.724.5422 fax.• 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: % weight basis Not reported Not reported Moisture Content %, wet weight basis 44.7 Organic Matter Content %, dry weight basis 48.5 pH units 7.52 Soluble Salts dS/m (mmhos/cm) 14 (electrical conductivity ECs) Particle Size or Sieve Size maxium aggregate size, inches 0.64 Stability Indicator (respirometry) Stability Rating: CO2 Evolution mg COZ-C/g OM/day 4.0 Moderately Un-Stable mg CO2-C/g TS/day 1.8 I Maturity Indicator (bioassay) - Percent Emergence average % of control 100.0� Relative Seedling Vigor average %of control 64.7 Select Pathogens PASSNAIL: per US EPA Class A standard, 40 CFR § 503.32(a) Pass Fecal coliform !!i 41 Pass Salmonella j Trace Metals PASSNAIL: per US EPA Class A As, Cd, Cr, Cu,Pb, Hg standard, 40 CFR § 503,13, Pass II Tables I and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compostproducts on a prescribed basis andprovide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laborato ,. Group: AI .16 B Laboraton_ Number: 6040104-1/1 Analyst: Assaf Sadeh <,�r www.compostlab.com McGill Environmental Systems COMPOSTING Ruth King COUNCIL P.O. Box 61 Seal of Testing Harrells Assurance NC 28444 Product Identification Compost Date Sampled/Received: 04 Apr. 16 105 Apr. 16 Soil Builder Delway COMPOST TECHNICAL DATA SHEET LABORATORY: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tet.• 831.724.5422 fax., 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis %, wet weight basis %, dry weight basis Nitrogen Total N 1.2 2.2 Phosphorus P201 1.6 3.0 Potassium KO 0.43 0.77 Calcium Ca 3.6 6.6 Magnesium Mg 0.18 0.33 Moisture Content %, wet weight basis 44.7 Organic Matter Content %, dry weight basis 48.5 pH units 7.52 Soluble Salts dS/m (mmhos/cm) 14 (electrical conductivity EC5) Particle Size or Sieve Size % under 9.5 nun, dw basis 99.5 { Stability Indicator (respirometry) Stability Rating: COZ Evolution mg COZ-C/g OM/day 4.0 Moderately Un-Stable Mg COZ-C/g TS/day 1.8 Maturity Indicator (bioassay) Percent Emergence average % of control 100.0 Relative Seedling Vigor average %of control 64.7 Select Pathogens PASS/FAIL: per US EPA Class A standard, 40 CFR § 503.32(a) Pass Fecal coliform I!{ ii Pass Salmonella Trace Metals PASS/FAIL: per us EPA Class A As, Cd,Cr,Cu,Pb,Hg standard, 40 CFR § 503.13, Pass ! Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seat of Testing Assurance Program have shown the commitment to test their compost products on aprescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laboratory Group: Apr. 16 B Laboratory Number: 6040104-1/1 Analyst: Assaf Sadeh ��•-by' --•� www.compostlab.com USCOMPOSTINGIr COUNCIL *�. Seal of Testing Assurance ` Date Sampled/Received: 04 Apr. 16 ! 05 Apr. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification: Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET for NORTH CAROLINA DOT t:..o._ _ _ - - I LABORAToRv: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel., 831.724.5422 fax., 831.724.3188 Compost Parameters Test Results Reported as (units of measure) Project Specification (Allowable Limit) i !Organic Matter Content 48.5 %, dry weight basis 25 - 65 ; H 7.52 Unitless 5.0 - 8.5 i Moisture Content 44.7 %, wet weight basis 30 - 60 Soluble Salts 14 dS/m (mmhos/cm) 5"0 dS/m, maximum I electrical conductivity) dry weight passing through 100.0 3 inch screen and 100% Particle Size 100.0 1 inch screen and 90% minimum i 100.0 3/4 inch screen and 65% minimum 1 91.6 1/4 inch screen 50% maximum I I Stability Indicator (respirometry) 4.0 mg CO2-C!g OM/day 58 � CO2 Evolution e Maturity Indicator (bioassay) 100.0 average % of control 80%, minimum i Percent Emergence Relative Seedling Vigor 64.7 average % of control 80%, minimum Select Pathogens PASSNAIL: Per US EPA Class A Pass Pass (Fecal Coliform) standard, 40 CFR 503.32(a) Trace Metals Pass PASSNAIL: Per US EPA Class A Pass 40 CFR 503.13, tables 1 and 3.__T Inert Contamination (man made)T None Detected %, dry weight <1.0 % Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. For additional information pertaining to compost use, the specific compost parameters tested for within the Seal of Testing assurance Program, or the program in general, log on to the US Composting Council's TMECC web -site at http:/fwww. tmecc. o1Wr This compost product has been sampled and tested as required by the Seal of Testing assurance Program on the United States Composting Council (USCC), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by contacting the compost producer (address at top of page). The USCC makes no warranties regarding this product or its content, quality. or suitability for any particular use. Laboratory Group: Apr. 16 B Laboraton Number: 6040104-1/1 Analyst: Assaf Sadeh <,« G� "� www.compostlab.com ANALYTICAL CHEMISTS and BACTERIOLOGISTS Approved by stele of California SOIL CONTROL LAB �2 "- t`4' :t WAY' WATSOWUF CAUFORP" 9SW6 USA McGill Environmental Systems P.O. Box 61 Harrells, NC 28444 Attn: Ruth King Date Received: 05 Apr. 16 Sample Identification: Soil Builder Delway Sample ID #: 6040104 - 1/1 TEL: 831-724-5422 FAX:831-724-3188 www.com_ ostlab.com Account #: 6040104-1/1-2215 Group: Apr. 16 B #4 Reporting Date: April 22, 2016 Nutrients Dry wt. As Rcvd. units Stability Indicator: Biologically Total Nitrogen: 2.2 1.2 % CO2 Evolution Respirometery Available C Ammonia (NH4-N): 3300 1800 mg/kg mg CO2-C/9 OM/day 4.0 4.1 Nitrate (NO3-N): 56 31 mg/kg mg CO2-C/g TS/day 1.8 2.0 Org. Nitrogen (Org.-N): 1.9 1.1 % Stability Rating stable moderately unstable Phosphorus (as P205): 2.8 1.6 % Phosphorus (P): 13000 6900 mg/kg Potassium (as K20): 0.77 0.43 % Maturity Indicator: Cucumber Bioassay Potassium (K): 6400 3600 mg/kg Compost:Vermiculite(v:v) 1:2 Calcium (Ca): 6.6 3.6 % Emergence (%) 100 Magnesium (Mg): 0.33 0.18 % Seedling Vigor (%) 65 Sulfate (SO4-S): 7200 4000 mg/kg Description of Plants stunted Boron (Total B): 32 18 mg/kg Moisture: 0 44.7 % Sodium (Na): 0.30 0.17 % Pathogens Results Units Rating Chloride (Cl): 0.26 0.15 % Fecal Coliform 7.3 MPN/g pass pH Value: NA 7.52 unit Salmonella < 3 MPN/4g pass Bulk Density: 22 39 Ib/cu ft Date Tested: 05 Apr. 16 Carbonates (CaCO3): 66 36 lb/ton Conductivity (EC5): 14 NA mrrhos/cm Organic Matter: 48.5 26.8 % i Inerts % by weight Organic Carbon: 24.0 13.0 % Plastic < 0.5 Ash: 51.5 28.5 % Glass < 0.5 C/N Ratio 11 11 ratio Metal < 0.5 Ac Index > 10 > 10 ratio, Sharps ND Aluminum (AI) Arsenic (As): Cadmium (Cd): Chromium (Cr): Cobalt (Co) Copper (Cu): Iron (Fe): Lead (Pb): Manganese (Mn): Mercury (Hg): Molybdenum (Mo): Nickel (Ni): Selenium (Se): Zinc (Zn): was receivea a 9300 14 < 1.0 27 17 170 10000 11 280 < 1.0 4.5 13 3.5 400 41 39 1200 1500 300 17 75 420 36 2800 units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Size Distribution MM % by weight > 50 0.0 25 to 50 0.0 16 to 25 0.0 9.5 to 16 0.5 6.3 to 9.5 7.9 4.0 to 6.3 19.0 2.0 to 4.0 31.9 < 2.0 40.8 procedures. Analyst: Assaf Sadeh ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: WQ0006816 WWTP Name: NPDES Number: Monitoring Period: From 5/1/2016 To 5/31/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alterative 2 ❑ Alternative 3 El.. . Alternative 4 ❑ Alternative 5 0 Alterative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost El Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 ❑ _ ..._............._............ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ coml-losting jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g ty Number o Xcee- , ,e Frequency of Analysis Sample Type . na ytica Tech - maue Minimum Geo. Mean Maximur Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei,,ht) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) 21 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed i:.l CERTIFICATION STATEMENT (please check the appropriate statement) C�3 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (ty e or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) 2 C7 - --- -- Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) USCOMPOSTING COUNCIL Seal of Testing Assurance Date Sampled/Received: 02 May. 16 / 03 May. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET LA►soRAroRy: -Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel: 831.724.5422 fax: 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis Not reported Not reported Moisture Content %, wet weight basis 45.1 Organic Matter Content %, dry weight basis 42.2 pH units 7.10 l Soluble Salts dS/m (mmhos/cm) 12 (electrical conductivity EC 5) Particle Size or Sieve Size maxium aggregate size, inches 0.25 Stability Indicator (respirometry) Stability Rating: COZ Evolution mg COZ-C/g OM/day 3.4 Stable mg COZ-C/g TS/day 1.3 Maturity Indicator (bioassay) Percent Emergence average % of control 100.0 Relative Seedling Vigor average %of control 72.2 Select Pathogens PASS/FAIL: per US EPA Class A standard, 40 CFR § 503.32(a) i i Pass Salmonella Trace Metals PASS/FAIL: per US EPA Class A As, Cd, Cr, Cu,Pb, Hg ! f standard, 40 CFR § 503.13, Pass Im Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis andprovide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laboratory Group: Ma,16A Laboratory Number: 6050066-1/1 Analyst: Assaf Sadeh ✓ <; ;z' www.compostiab.com UCOMPOSTING COUNCIL Seal of Testing Assurance Date Sampled/Received: 02 May. 16 / 03 May. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST 'TECHNICAL DATA SHEET LABORATORY: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel. 831.724.5422 fax. • 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis %, wet weight basis %, dry weight basis Nitrogen Total N 1.2 2.1 Phosphorus P201 1.6 3.0 Potassium KO 0.36 0.66 Calcium Ca 3.7 6.8 Magnesium Mg 0.18 0.32 Moisture Content %, wet weight basis 45.1 Organic Matter Content %, dry weight basis 42.2 pH units 7.10 Soluble Salts (electrical conductivity EC5) dS/m (mmhos/cm) 12 I Particle Size or Sieve Size % under 9.5 mm, dw basis 100.0 Stability Indicator (respirometry) Stability Rating: COZ Evolution mg CO2-C/9 OM/day 3.4 Stable me CO, -C/a TS/day 1.3 Maturity Indicator (bioassay) i Percent Emergence average % of control 100.0 Relative Seedling Vigor average % of control 72.2 Select Pathogens PASS/FAIL: per US EPA Class A standard, 40 CFR § 503.32(a) I i Pass Salmonella Trace Metals PASS/FAIL: per US EPA Class A As, Cd, Cr, Cu,Pb,Hg standard, 40 CFR § 503.13, Pass Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laboraton, Group: Mav16A Laboratory Number: 6050066-1/1 Analyst: Assaf Sadeh �'�� •- '` www.compostlab.com o><Q4. McGill Environmental Systems US COMPOSTING%Ruth King COUNCIL.. P.O. Box 61 Seal of Testing `� Harrells Assurance NC 28444 _Of TM - Product Identification: Compost Date Sampled/Received: 02 May. 16 / 03 May. 16 Soil Builder Delway COMPOST TECHNICAL DATA SHEET for NORTH CAROLINA DOT j LmomToRy: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tek 831.724.5422 fax: 831.724.3188 Compost Parameters Test Results Reported as (units of measure) Project Specification (Allowable Limit) Organic Matter Content 42.2 %, dry weight basis 25 - 65 H 7.10 Unitless 5.0 - 8.5 Moisture Content 45.1 %, wet weight basis 30 - 60 Soluble Salts 12 dS/m (mmhos/cm) 5.0 dS/m, maximum ( electrical conductivity) dry weight passing through 100.0 3 inch screen and 100% Particle Size 100.0 1 inch screen and 90% minimum 100.0 3/4 inch screen and 65% minimum 100.0 1/4 inch screen 50% maximum Stability Indicator (respirometry) 3.4 mg CO2-C/g OM/day s 8 CO2 Evolution Maturity Indicator (bioassay) 100.0 average % of control 800/a,minimum Percent Emergence Relative Seedlina Visor 72.2 average % of control 80%, minimum Select Pathogens PASSNAIL: Per US EPA Class A Pass Pass (Salmonella) standard, 40 CFR 503.32(a) Trace Metals Pass PASS/FAIL: Per US EPA Class A Pass 40 CFR 503.13_ tables 1 and 3. Inert Contamination (man-made) None Detected %, dry weight _T <I.0 % Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better verve the needs of their compost customers. For additional information pertaining to compost use, the specific compost parameters tested for within the Seal of Testing assurance Program, or the program in general, log on to the US Composting Council's TMECC web -site at http.1Avww.tmecc.org. This compost product has been sampled and tested as required by the Seal of Testing assurance Program on the United States Composting Council (USCC), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by contacting the compost producer (address at top of page). The USCC makes no warranties regarding this product or its content, quality. or suitability for any particular use. I Laboratory Group: Mar 16A Laboratory Number: 6050066-1/1 1 Analyst: Assaf Sadeh www.compostlab.com ANALYTICAL CHEMISTS and BACTERIOLOGISTS Approved by State of Callfomte SOIL CONTROL LAB Q HANGAR WAY. WATSONVILLE ,CALIFORNIA 9W6 USA McGill Environmental Systems P.O. Box 61 Harrells, NC 28444 Attn: Ruth King Date Received: 03 May. 16 Sample Identification: Soil Builder Delway Sample ID #: 6050066 - 1/1 TEL: 831-724-5422 FAX: 831-724-3188 www.compostiab.com Account #: 6050066-1/1-2215 Group: Mayl6A #7 Reporting Date: May 18, 2016 Nutrients Dry wt. As Rcvd. units Stability Indicator: Biologically Total Nitrogen: 2.1 1.2 % CO2 Evolution Respirometery Available C Ammonia (NH4-N): 2400 1300 mg/kg mg CO2-C/9 OM/day 3.4 3.5 Nitrate (NO3-N): 4100 2300 mg/kg mg CO2-C/g TS/day 1.3 1.9 Org. Nitrogen (Org.-N): 1.5 0.82 % Stability Rating stable stable Phosphorus (as P205): 2.9 1.6 % Phosphorus (P): 13000 6900 mg/kg Potassium (as K20): 0.66 0.36 % Maturity Indicator: Cucumber Bioassay Potassium (K): 5500 3000 mg/kg Compost:Vermiculite(v:v) 1:2 Calcium (Ca): 6.8 3.7 % Emergence (%) 100 Magnesium (Mg): 0.32 0.18 % Seedling Vigor (%) 72 Sulfate (SO4-S): 20 11 mg/kg Description of Plants stunted Boron (Total B): 31 17 mg/kg Moisture: 0 45.1 % Sodium (Na): 0.24 0.13 % Pathogens Results Units Rating Chloride (Cl): 0.23 0.13 % Fecal Coliform > 3400 MPN/g fail pH Value: NA 7.10 unit Salmonella < 3 MPN/4g pass Bulk Density : 22 40 Ib/cu ft Date Tested: 03 May. 16 Carbonates (CaCO3): 110 62 lb/ton Conductivity (EC5): 12 NA mmhos/cm Organic Matter: 42.2 23.2 % Inerts % by weight Organic Carbon: 21.0 12.0 % Plastic < 0.5 Ash: 57.8 31.7 % Glass < 0.5 C/N Ratio 10 10 ratio Metal < 0.5 A Index > 10 > 10 ratio I ISharps ND Metals Dry wt. EPA Limit units Aluminum (AI) 10000 - mg/kg Arsenic (As): 15 41 mg/kg Cadmium (Cd): < 1.0 39 mg/kg Chromium (Cr): 28 1200 mg/kg Cobalt (Co) 19 - mg/kg Copper (Cu): 160 1500 mg/kg Iron (Fe): 11000 - mg/kg Lead (Pb): 11 300 mg/kg Manganese (Mn): 270 - mg/kg Mercury (Hg): < 1.0 17 mg/kg Molybdenum (Mo): 3.6 75 mg/kg Nickel (Ni)-. 13 420 mg/kg Selenium (Se): 3.3 36 mg/kg Zinc (Zn): 380 2800 mg/kg *Samnle was received and handled in accordance with TM Size Distribution MM % by weight > 50 0.0 25 to 50 0.0 16 to 25 0.0 9.5 to 16 0.0 6.3 to 9.5 0.0 4.0 to 6.3 5.7 2.0 to 4.0 40.8 < 2.0 53.5 =CC procedures. Analyst: Assaf Sadeh ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: WWTP Name: NPDES Number: WQ0006816 Monitoring Period: From 6/1/2016 To 6/30/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative I ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 0 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost R) Heat Drying ❑ Heat Treatment ❑ Theimophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization C] Class B: Alternative 1 ® Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying[:] Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion El _...... _.........._... _ __ ................. ....__. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- dences Frequency of Analysis Sample Type Analytical Tech - woue Minimum Geo. Mean Maximunj Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 N?N per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) Alt. 5 (14-Day Aerobic) R1 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) I Alt. 8 (Drying - Unstable) El Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Cl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (type or print) Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) USCOMPOSTING COUNCIL Seal of Testing - Assurance Date Sampled/Received: 01 Jun. 16103 Jun. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET LABORATORY: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel. 831.724.5422 fax.- 831.724.3188 F Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis Not reported Not reported Moisture Content %, wet weight basis 39.8 Organic Matter Content %, dry weight basis 57.1 pH units 7.12 Soluble Salts (electrical conductivity EC;) dS/m (mmhos/cm) I 12 Particle Size or Sieve Size mamum aggregate size, inches 0.64 (� Stability Indicator (respirometry) Stability Rating: CO2 Evolution mg COZ-C/g OM/day 1.3 Very Stable mg CO,-C/g TS/day 0.79 Maturity Indicator (bioassay) Percent Emergence average % of control 100.0 Relative Seedling Vigor average % of control 93.8 Select Pathogens PASS/FAIL: per US EPA Class A standard, 40 CFR § 503.32(a) Pass Fecal coliform Pass Salmonella Trace Metals PASS/FAIL: per US EPA Class A As, Cc4 Cr, Cu, Pb,Hg standard, 40 CFR § 503.13, Pass Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. .aboratory Group: Junl6A Laborator Number: 6060129-1/1 knalyst: Assaf Sadeh www.compostiab.com USCOMPOSTING COUNCIL Seal of Testing Assurance Date Sampled/Received: 01 Jun. 16 / 03 Jun. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET LABORAToRy: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel.• 831.724.5422 fax. • 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: °/a, weight basis %, wet weight basis %, dry weight basis Nitrogen Total N 1.2 1.9 Phosphorus PZOS 1.4 2.5 Potassium KO 0.42 0.70 Calcium Ca 2.7 4.4 Magnesium Mg 0.16 0.26 Moisture Content %, wet weight basis 39.8 Organic Matter Content %, dry weight basis 57.1 pH units 7.12 f Soluble Salts dS/m (mmhos/cm) 12 (electrical conductivity EC 5) Particle Size or Sieve Size % under 9.5 nun, dw basis 99.4 !; Stability Indicator (respirometry) Stability Rating: i COZ Evolution mg COz-C/g OM/day 1.3 Very Stable mg COz-C/g TS/day 0.79 E Maturity Indicator (bioassay) Percent Emergence average % of control 100.0 Relative Seedling Vigor average % of control 93.8 Select Pathogens PASS/FAIL: per US EPA Class A I standard, 40 CFR § 503.32(a) Pass Fecal coliform li Pass Salmonella I I Trace Metals PASS/FAIL: per US EPA Class A As,Cd,Cr,Cu,Pb,Hg $ ( standard, 40 CFR § 503.13, Pass ' Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compostproducts on a prescribed basis andprovide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laborator. Group: Jun16A Laboraton Number: 6060129-1/1 Analyst: Assaf Sadeh�- sir'--�?' • � www.compostlab.com i p__cF " McGill Environmental Systems USCOMPOSTING �! Ruth King COUNCIL P.O. Box 61 Seal of Testing J Harrells Asstcrrtnce of NC 28444 Product Identification: Compost Date Sampled/Received: 01 Jun. 16 / 03 Jun. 16 Soil Builder Delway COMPOST TECHNICAL DATA SHEET for NORTH CAROLINA DOT u►eoRAToey: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tek 831.724.5422 fax: 831.724.3188 Compost Parameters I Test Results I Reported as (units of measure) I Project Specification Organic Matter Content 57.1 %, dry weight basis 25 - 65 !pH 7.12 Unitless 5.0 - 8.5 Moisture Content 39.8 %, wet weight basis 30 - 60 Soluble Salts 12 dS/m (mmhos/cm) 5.0 d5/m, maximum (electrical conductivity) dry weight passing through j 100.0 3 inch screen and 100% Particle Size 100.0 1 inch screen and 90% minimum 100.0 3/4 inch screen and 65% minimum I 90.6 1/4 inch screen 50% maximum Stability Indicator (respirometry) 1.3 mg CO2-C/g OM/day s 8 i CO2 Evolution Maturity Indicator (bioassay) 100.0 average % of control 801/o,minimum Percent Emergence L Relative Seedlinu Viaor 93.8 average % of control 80%, minimum Select Pathogens PASS/FAIL: Per US EPA Class A Pass Pass (Fecal Colifonn) standard, 40 CFR 503.32(a) Trace Metals Pass PASSNAIL: Per US EPA Class A Pass 40 CFR 503.13. tables 1 and 3. Inert Contamination (man-made) None Detected %, dry weight <1.0 % Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. For additional information pertaining to compost use, the specific compost parameters tested far within the Seal of Testing assurance Program, or the program in general, log on to the US Composting Council's TMECC web -site at http:/fwww. tmeca org. This compost product has been sampled and tested as required by the Seal of Testing assurance Program on the United States Composting Council (USCC), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by contacting the compost producer (address at top of page). The USCC makes no warranties regarding this product or its content, quality. or suitability for any particular use. Laborato Group: Junl6A Laborator\ Number: 6060129-1/1 Analyst: Assaf Sadeh < _ - f - www.compostlab.com ANALYTICAL CHEMISTS and BACTERIOLOGISTS Approved by State o/ California SOIL CONTROL LAB 42 HANGAR WAY, WATSONVILLE ICAUFORNIA v5G76 USA McGill Environmental Systems P.O. Box 61 Harrells, NC 28444 Attn: Ruth King Date Received: 03 Jun. 16 Sample Identification: Soil Builder Delway Sample ID #: 6060129 -1/1 TEL: 831-724-5422 FAX: 831-724-3188 www.compostlab.com Account #: 6060129-1/1-2215 Group: Jun16A #26 Reporting Date: June 17, 2016 Nutrients Dry wt. As Rcvd. units Stability Indicator: Biologically Total Nitrogen: 1.9 1.2 % CO2 Evolution Respirometery Available C Ammonia (NH4-N): 2600 1600 mg/kg mg CO2-C/g OM/day 1.3 1.5 Nitrate (NO3-N): 210 130 mg/kg mg CO2-C/g TS/day 0.79 1.0 Org. Nitrogen (Org.-N): 1.6 0.96 % Stability Rating very stable very stable Phosphorus (as P205): 2.4 1.4 % Phosphorus (P): 11000 6300 mg/kg Potassium (as K20): 0.69 0.42 % Maturity Indicator: Cucumber Bioassay Potassium (K): 5800 3500 mg/kg Compost:Vermiculite(v:v) 1:2 Calcium (Ca): 4.4 2.7 % Emergence (%) 100 Magnesium (Mg): 0.26 0.16 % Seedling Vigor (%) 94 Sulfate (SO4-S): 4200 2500 mg/kg Description of Plants healthy Boron (Total B): 59 36 mg/kg Moisture: 0 39.8 % Sodium (Na): 0.26 0.15 % Pathogens Results Units Rating Chloride (CI): 0.17 0.1 % Fecal Coliform 42 MPN/g pass pH Value: NA 7.12 unit Salmonella < 3 MPN/4g pass Bulk Density : 20 33 lb/cu ft Date Tested: 03 Jun. 16 Carbonates (CaCO3): 65 39 lb/ton Conductivity (EC5): 12 NA mmhos/cm Organic Matter: 57.1 34.4 % Inerts % by weight Organic Carbon: 28.0 17.0 % Plastic < 0.5 Ash: 42.9 25.8 % Glass < 0.5 C/N Ratio 15 15 ratio Metal < 0.5 AgIndex > 10 > 10 ratio ISharps ND Metals Dry wt. EPA Limit units Aluminum (AI) 5800 - mg/kg Arsenic (As): 11 41 mg/kg Cadmium (Cd): < 1.0 39 mg/kg Chromium (Cr): 23 1200 mg/kg Cobalt (Co) 63 - mg/kg Copper (Cu): 150 1500 mg/kg Iron (Fe): 8600 - mg/kg Lead (Pb): 9.6 300 mg/kg Manganese (Mn): 260 - mg/kg Mercury (Hg): < 1.0 17 mg/kg Molybdenum (Mo): 4.1 75 mg/kg Nickel (Ni): 11 420 mg/kg Selenium (Se): 2.6 36 mg/kg Zinc (Zn): 330 2800 mg/kg *Sample was received and handled in accordance with 1 Size Distribution MM % by weight > 50 0.0 25 to 50 0.0 16 to 25 0.0 9.5 to 16 0.6 6.3 to 9.5 8.8 4.0 to 6.3 17.8 2.0 to 4.0 24.7 < 2.0 48.1 procedures. Analyst: Assaf Sadeh ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: WQ0006816 WWTP Name: NPDES Number: Monitoring Period: From 7/1/2016 To 7/31/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 0 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost R1 Heat Drying ❑ Heat Treatment ') Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization '�j Class B: Alternative 1 ❑ Alternative 2 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying[] Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion If applicable to alternative perfformed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- dences Frequency of Analysis Sample Type Analytical Tech - niaue Nlinimun Geo. Mean Maximurn Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) 21 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) C7 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ►❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) USCOMPOSTING COUNCIL Seal of Testing Assurance. Date Sampled/Received: 11 Jul. 16 / 12 Jul. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET LABORATORY: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 f tel.- 831.724.5422 fax., 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results Y Plant Nutrients: %, weight basis Not reported Not reported Moisture Content °/q wet weight basis 29.5 Organic Matter Content °/% dry weight basis 43.4 pH units 7.40 Soluble Salts j (electrical conductivity EC 5) dS/m (mmhos/cm) 12 Particle Size or Sieve Size mamum aggregate size, inches 0.38 Indicator (res irometr) tY Stabili Rath Stabilit5' P g. CO2 Evolution mg CO2-C/9 OM/day 1.8 Very Stable Mg COZ-C/g TS/day 0.97 Maturity Indicator (bioassay) I Percent Emergence average % of control 93.3 Relative Seedling Vigor average %of control 35.4 Select Pathogens PASS/FAIL: per US EPA Class A standard, 40 CFR § 503.32(a) Pass Fecal coliform Pass Salmonella I Trace Metals PASS/FAIL: per US EPA Class A As, Cd,Cr, Cu,Pb,Hg standard, 40 CFR § 503.13, Pass 1 Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on aprescribed basis andprovide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laborator, Group: Jul. 16 C Laboratory Number: 6070297-1/1 (Analyst: Assaf Sadeh c`l www.compostlab.com USCOMPOSTING COUNCIL Seal of Testing Assurance Date Sampled/Received: 11 Jul. 16 / 12 Jul. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET tABow►roar: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel: 831.724.5422 fax.- 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results I Plant Nutrients: %, weight basis %, wet weight basis %, dry weight basis I Nitrogen Total N 1.4 2.0 Phosphorus PZOS 2.0 2.7 Potassium K20 0.49 0.70 Calcium Ca 4.7 6.6 Magnesium Mg 0.21 0.29 Moisture Content %, wet weight basis 29.5 Organic Matter Content %, dry weight basis 43.4 pH units 7.40 Soluble Salts (electrical conductivity EC s) dS/m (mmhos/cm) 12 a Particle Size or Sieve Size % under 9.5 nun, dw basis 100.0 Stability Indicator (respirometry) Stability Rating. CO2 Evolution mg CO2 C/g OM/day 1.8 mg CO,-C/g TS/day 0.97 —.Y Maturity Indicator (bioassay) Percent Emergence average % of control 93.3 Relative Seedling Vigor average %of control 35.4 Select Pathogens PASSTAIL: per US EPA Class A standard, 40 CFR § 503.32(a) Pass Fecal coliform 1 Pass Salmonella Trace Metals PASSTAIL: per US EPA Class A As, Cd,Cr, Cu,Pb,Hg standard, 40 CFR § 503.13, Pass Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laboratory Group: Jul. 16 C Laborato, .� Number: 6070297-1/1 Analyst: Assaf Sadeh�� www.compostlab.com U5COMPOSTING COUNCIL Seal of Testing Assurance Date Sampled/Received: 11 Jul. 16 / 12 Jul. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 F duct Identification: Compost l Builder Delway COMPOST TECHNICAL DATA SHEET for NORTH CAROLINA DOT LABORATORY. Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tek 831.724.5422 far: 831.724.3188 Compost Parameters Test Results Reported as (units of measure) Project Specification (Allowable Limit) i !Organic Matter Content 43.4 %, dry weight basis 25 - 65 )H 7.40 Unitless 5.0 - 8.5 Moisture Content 29.5 %, wet weight basis 30 - 60 Soluble Salts 12 dS/m (mmhos/cm) 5.0 dS/m, maximum I ( electrical conductivity) i dry weight passing through 100.0 3 inch screen and 100% l I Particle Size 100.0 1 inch screen and 90% minimum I 100.0 3/4 inch screen and 65% minimum 97.1 1/4 inch screen 50% maximum Stability Indicator (respirometry) 1.8 mg CO2-C/g OM/day s 8 CO2 Evolution Maturity Indicator (bioassay) 93.3 average % of control 80%, minimum Percent Emergence Relative Seedling Vigor 35.4 average % of control 80%, minimum Select Pathogens PASS/FAIL: Per US EPA Class A Pass Pass (Fecal Coliform) standard, 40 CFR 503.32(a) Trace Metals Pass PASS/FAIL: Per US EPA Class A Pass 40 CFR 503.13, tables 1 and 3. Inert Contamination (man-made) None Detected %, dry weight <1.0 % Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. For additional information pertaining to compost use, the specific compost parameters tested for within the Seal of Testing assurance Program, or the program in general, log on to the US Composting Council's TMECC web -site at h ttp.1Avww. tmecc. org. This compost product has been sampled and tested as required by the Seal of Testing assurance Program on the United States Composting Council (USCC), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by contacting the compost producer (address at top of page). The USCC makes no warranties regarding this product or its content, quality. or suitability for any particular use. Laboraton Group: Jul. 16 C Laboraton Number: 6070297-1/1 Analyst: Assaf Sadeh�,r w't' www.compostlab.com ANALYTICAL CHEMISTS and BACTERIOLOGISTS Approved by stela of California SOIL CONTROL LAB 4 HANGAR WAY WATSONVR,tE CAUFORNIA 95076 W McGill Environmental Systems P.O. Box 61 Harrells, NC 28444 Attn: Ruth King Date Received: 12 Jul. 16 Sample Identification: Soil Builder Delway Sample ID #: 6070297 -1/1 Nutrients Dry wt. As Rcvd. units Total Nitrogen: 2.0 1.4 % Ammonia (NH4-N): 2700 1900 mg/kg Nitrate (NO3-N): 110 76 mg/kg Org. Nitrogen (Org.-N): 1.7 1.2 % Phosphorus (as P205): 2.8 1.9 % Phosphorus (P): 12000 8600 mg/kg Potassium (as K20): 0.70 0.49 % Potassium (K): 5800 4100 mg/kg Calcium (Ca): 6.6 4.7 % Magnesium (Mg): 0.29 0.21 % Sulfate (SO4-S): 6200 4400 mg/kg Boron (Total B): 43 31 mg/kg Moisture: 0 29.5 % Sodium (Na): 0.28 0.20 % Chloride (Cl): 0.21 0.15 % pH Value: NA 7.40 unit Bulk Density : 30 42 lb/cu ft Carbonates (CaCO3): 71 50 lb/ton Conductivity (EC5): 12 NA mmhos/cm Organic Matter: 43.4 30.6 % Organic Carbon: 21.0 15.0 % Ash: 56.6 39.9 % C/N Ratio 10 10 ratio AgIndex > 10 > 10 ratio Metals Dry wt. EPA Limit units Aluminum (AI) 8600 - mg/kg Arsenic (As): 9.7 41 mg/kg Cadmium (Cd): < 1.0 39 mg/kg Chromium (Cr): 21 1200 mg/kg Cobalt (Co) 87 - mg/kg Copper (Cu): 140 1500 mg/kg Iron (Fe): 11000 - mg/kg Lead (Pb): 9.9 300 mg/kg Manganese (Mn): 330 - mg/kg Mercury (Hg): < 1.0 17 mg/kg Molybdenum (Mo): 4.1 75 mg/kg Nickel (Ni): 11 420 mg/kg Selenium (Se): 3.4 36 mg/kg Zinc (Zn): 360 2800 mg/kg *Sample was received and handled in accordance with l TEL: 831-724-5422 FAX: 831-724-3188 www.com _ostlab.com Account #: 6070297-1 /1-2215 Group: Jul.16 C #6 Reporting Date: July 29, 2016 Stability Indicator: Biologically CO2 Evolution Respirometery Available C Mg CO2-C/9 OM/day 1.8 2.0 Mg CO2-C/g TS/day 0.97 1.0 Stability Rating very stable very stable Maturity Indicator: Cucumber Bioassay Compost:Vermiculite(v:v) 1:2 Emergence (%) 93 Seedling Vigor (%) 35 Description of Plants stunted Pathogens Results Units Rating Fecal Coliform < 7.5 MPN/g pass Salmonella < 3 MPN/4g pass Date Tested: 12 Jul. 16 Inerts % by weight Plastic < 0.5 Glass < 0.5 Metal < 0.5 Sharps ND Size Distribution MM % by weight > 50 0.0 25 to 50 0.0 16 to 25 0.0 9.5 to 16 0.0 6.3 to 9.5 2.9 4.0 to 6.3 7.5 2.0 to 4.0 16.4 < 2.0 73.2 Analyst: Assaf Sadeh G procedures. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: WWTP Name: NPDES Number: WQ0006816 Monitoring Period: From 8/1/2016 To 8/31/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 0 Alternative 6 ❑ If applicable to alternative pet -formed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 ❑77 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ ... ............... .. ....... ..*,.....*..,.,.,.,.":::**.,."",.*.".,..-..-...,- If.- applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of deuces e- Frequency of Analysis Sample Type • na ytica Tech- nioue Minimum Geo. Mean Maximun Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) p Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (type or print) <&-1( 9 � 2--- _6 -/ Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) UCOMPOSTING COUNCIL Seal of Testing Assurance Date Sampled/Received: 01 Aug. 16 / 02 Aug. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 Product Identification Compost Soil Builder Delway COMPOST TECHNICAL DATA SHEET LABORAToRy: Soil Control Lab; 42THangar Way; Watsonville, CA 95076 te% 831.724.5422 fax.- 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis Not reported Not reported Moisture Content %, wet weight basis 30.3 Organic Matter Content %, dry weight basis 51.5 pH units 7.56 Soluble Salts dS/m (mmhos/cm) 15 (electrical conductivity EC y) Particle Size or Sieve Size maxium aggregate size, inches 0.25 i Stability Indicator (respirometry) Stability Rating: CO2 Evolution mg COZ C/g OWday 2.9 Stable mg COZ-C/g TS/day 1.5 Maturity Indicator (bioassay) Percent Emergence average % of control 0.0 g Vidli S ti Relave Seedling or � g average %f control NA 1 _ Select Pathogens PASS/FAIL: per US EPA Class A !I!I standard, 40 CFR § 503.32(a) Pass Fecal coliform� i I C I Pass Salmonella � Trace Metals PASS/FAIL: per US EPA Class A As, Cd, Cr, Cu,Pb, Hg' standard, 40 CFR § 503.13, Pass Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on aprescribed basis andprovide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laboratory Group: Au 16A Laboratory Number: 6080101-1/1 Analyst: Assaf Sadeh www.compostlab.com McGill Environmental Systems UCOMPOSTING Ruth King COUNCIL P.O. Box 61 Seal of Testing Harrells Assurance NC 28444 Product Identification Compost Date Sampled/Received: 01 Aug. 16 / 02 Aug. 16 Soil Builder Delway COMPOST TECHNICAL DATA SHEET u►aoRAToev: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel.- 831.724.5422 fax. 831.724.3188 Compost Parameters Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis %, wet weight basis %, dry weight basis Nitrogen Total N 1.6 2.3 Phosphorus P205 1.9 2.7 Potassium K20 0.46 0.65 Calcium Ca 4.0 5.8 Magnesium I Mg 0.19 0.27 Moisture Content %, wet weight basis 30.3 Organic Matter Content %, dry weight basis 51.5 pH units 7.56 Soluble Salts (electhz'cal conductivity EC 5) dS/m (mmhos/cm) 15 I Particle Size or Sieve Size % under 9.5 mm, dw basis 100.0 Stability Indicator (respirometry) Stability Rating. nn L`.,.1..�:,... n� ni� rig ria ., � n l i, UU2 ZVOWLavai rug t-v2-ws vivyuay 4.7 .Stable ' I1 mg CO2-C/g TS/day 1.5 Maturity Indicator (bioassay) Percent Emergence average % of control 0.0 Relative Seedling Vigor average % of control NA Select Pathogens PASS/FAIL: per US EPA Class A I standard, 40 CFR § 503.32(a) Pass Fecal coliform Pass Salmonella Trace Metals PASSTAIL: per US EPA Class A As, Cd, Cr, Cu,Pb,Hg standard, 40 CFR § 503-13, Pass Tables 1 and 3. Mo,Ni,Se,Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. Laborato . Group: Au_L,,16A Laborator, Number: 6080101-1/1 Analyst: Assaf Sadeh Ci/ -� www.compostlab.com USCOMPOSTING COUNCIL Seal of Testing Assurance Date Sampled/Received: 01 Aug. 16 / 02 Aug. 16 McGill Environmental Systems Ruth King P.O. Box 61 Harrells NC 28444 ro—d"clldendfication: Compost il Builder Delway COMPOST TECHNICAL DATA SHEET for NORTH CAROLINA DOT LABORATORY: Soil Control Lab; 42 Hangar Way; Watsonville, CA 95076 tel. 831.724.5422 fax.- 831.724.3188 Compost Parameters Test Results Reported as (units of measure) Project Specification (Allowable Limit) ,Organic Matter Content 51.5 %, dry weight basis 25 - 65 S H 7.56 Unitless 5.0 - 8.5 R Moisture Content 30.3 %, wet weight basis 30 - 60 Soluble Salts 15 dS/m (mmhos/cm) 5.0 dStm, maximum (electrical conductivitti ) dry weight passing through 100.0 3 inch screen and 100% Particle Size 100.0 1 inch screen and 90% minimum 1 100.0 3/4 inch screen and 65%minimum 100.0 1/4 inch screen 50% maximum Stability Indicator (respirometry) 2.9 mg CO2 C/g OM/day s 8 CO2 Evolution Maturity Indicator (bioassay) 0.0 average % of control 80%, minimum Percent Emergence Relative Seedling Vigor NA average % of control 80%, minimum Select Pathogens Pass PASSNAIL: Per US EPA Class A Pass 1 (Fecal Coliform) standard. 40 CFR 503.32(a) Trace Metals Pass PASS/FAIL: Per US EPA Class A Pass 40 CFR 503.13, tables 1 and 3. Inert Contamination (man-made) None Detected %, dry weight <1.0 % Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. For additional information pertaining to compost use, the specific compost parameters tested far within the Seal of Testing assurance Program, or the program in general, log on to the US Composting Council's TMECC web -site at h11p.1Avww. tmecc. orb This compost product has been sampled and tested as required by the Seal of Testing assurance Program on the United States Composting Council (USCG), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by contacting the compost producer (address at top of page). The USCC makes no warranties regarding this product or its content, quality. or suitability for any particular use. Laboratory Group: Au 16A Laboratory Number: 6080101-1/1 Analyst: Assaf Sadeh r=�+' > www.compostlab.com ANALYTICAL CHEMISTS and BACTERIOLOGISTS Approved by Srota of California SOIL CONTROL LAB 42 HAi4q;4 SNAy WAt50NVILLE CAUFORNM 95076 USA McGill Environmental Systems P.O. Box 61 Harrells, NC 28444 Attn: Ruth King Date Received: 02 Aug. 16 Sample Identification: Soil Builder Delway Sample ID #: 6080101 - 1/1 TEL: 831-724-5422 FAX: 831-724-3188 www.compostlab.com Account #: 6080101-1/1-2215 Group: Aug16A #17 Reporting Date: August 19, 2016 Nutrients Dry wt. As Rcvd. units Stability Indicator: Biologically Total Nitrogen: 2.3 1.6 % CO2 Evolution Respirometery Available C Ammonia (NH4-N): 4200 2900 mg/kg mg CO2-C/9 OM/day 2.9 3.0 Nitrate (NO3-N): 8.5 5.9 mg/kg mg CO2-Clg TS/day 1.5 1.5 Org. Nitrogen (Org.-N): 1.9 1.3 % Stability Rating stable stable Phosphorus (as P205): 2.7 1.9 % Phosphorus (P): 12000 8300 mg/kg Potassium (as K20): 0.65 0.45 % Maturity Indicator: Cucumber Bioassay Potassium (K): 5400 3800 mg/kg Compost:Vermiculite(v:v) 1:2 Calcium (Ca): 5.8 4.0 % Emergence (%) 0 Magnesium (Mg): 0.27 0.19 % Seedling Vigor (%) NA Sulfate (SO4-S): 4700 3300 mg/kg Description of Plants Boron (Total B): 44 31 mg/kg Moisture: 0 30.3 % Sodium (Na): 0.31 0.22 % Pathogens Results Units Rating Chloride (Cl): 0.17 0.12 % Fecal Coliform 68 MPN/g pass pH Value: NA 7.56 unit Salmonella < 3 MPN/4g pass Bulk Density : 26 37 Ib/cu ft Date Tested: 02 Aug. 16 Carbonates (CaCO3): 80 56 lb/ton Conductivity (EC5): 15 NA mmhos/cm Organic Matter: 51.5 35.9 % Inerts % by weight Organic Carbon: 26.0 18.0 % Plastic < 0.5 Ash: 48.5 33.8 % Glass < 0.5 C/N Ratio 11 11 ratio Metal < 0.5 A Index > 10 > 10 ratio Sharps ND Metals Dry wt. EPA Limit units Aluminum (Al) 9300 - mg/kg Arsenic (As): 8.2 41 mg/kg Cadmium (Cd): < 1.0 39 mg/kg Chromium (Cr): 21 1200 mg/kg Cobalt (Co) 70 - mg/kg Copper (Cu): 130 1500 mg/kg Iron (Fe): 10000 - mg/kg Lead (Pb): 9.7 300 mg/kg Manganese (Mn): 290 - mg/kg Mercury (Hg): < 1.0 17 mg/kg Molybdenum (Mo): 4.3 75 mg/kg Nickel (Ni): 11 420 mg/kg Selenium (Se): 2.9 36 mg/kg Zinc (Zn): 440 2800 ma/ka *Sample was received and handled in accordance with l Size Distribution MM % by weight > 50 0.0 25 to 50 0.0 16 to 25 0.0 9.5 to 16 0.0 6.3 to 9.5 0.0 4.0 to 6.3 3.1 2.0 to 4.0 17.9 < 2.0 79.0 Analyst: Assaf Sadeh procedures. ' ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: WQ0006816 WWTP Name: NPDES Number: Monitoring Period: From 9/1/2016 To 913OY2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ rs.s Alternative 4❑ Alterative 5 0 Alternative 6❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Ell Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alterative 2 ❑ _ . _ ....................._ ................ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ I Air Drying[] composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Stud Pathogen Density Num er o Excee- Frequency of Analysis Sample Type na ytica Tech- Minimum Geo. Mean Maximum Units Fecal Coliform 2x10tothe 6th power per gram of total solids WN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei-lrti Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) 0 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) [] No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) 21 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) Z-3-r 7 Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 503 (12/2006) USCOMPOSTING COUNCIL Seal of Te.ting. Assur anee McGill Env. Sys. / Delway Plant Anthony Teachey 1100 Herring Road Rose Hill, NC 28458 910-260-0121 Product Name: Compost .Sample Date: 9/6/16 9:30 AM Receive Date: 917/16 A & L Lab Number: 87749 A & L Report Number: F16251-6014 COMPOST TECHNICAL DATA SHEET A & L Great Lakes Laboratories, Inc. 3505 Conestoga Drive Fort Wayne IN 46808 Compost Parameters _ Method Reported as (units of measure) Test Results Test Results Plant Nutrients: %, weight basis %, wet weight basis %, dry weight basis Nitrogen TMECC 04.02-D Total N 1.55 2.10 Phosphorus TMECC 04.03-A P205 2.42 3.25 Potassium TMECC 04.04-A KO 0.63 0.85 Calcium TMECC 04.05-CA Ca 5.20 7.03 Magnesium TMECC 04.05-MG Mg 0.22 0.30 Moisture Content TMECC 03.09-A %, wet weight basis 25.99 Organic Matter Content TMECC 05.07-A °l°, dry weight basis 36.96 pH TMECC 04.11-A pH units 7.7 Soluble Salts (electrical conductivity EC 5) TMECC 04.10-A dS/m (mmhos/cm) 7.49 Particle Size TMECC 02.02-B % < 9.5 mtn (3/8 in.), dw basis 98.49 Stability Indicator (respirometry) CO2 Evolution TMECC 05.08-B mg COZ-C/g OM/day mg COz-C/g TS/day I I Stability Rating: Very Stable Maturity Indicator (bioassay) Percent Emergence TMECC 05.05-A Relative Seedling Vigor TMECC 05.05-A average % of control average % of control 87 48 Select Pathogens TMECC 07.01-B PASS/FAIL: per US EPAC1ass A standard, 40 CFR § 503.32(a) PASS Fecal Coliform Trace Metals TMECC 04.06 PASS/FAIL: per uS EPA Class A standard, 40 CFR § 503.13, Tables 1 and 3. PASS As, Cd, Ph, Hg, Mo, Ni, Se, Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serge ti:e needs of their compost customers. m,/ USCOMPOSTING COUNCIL Szal 1T 7'esfin; Assuran-re McGill Env. Sys. / Delway Plant Anthony Teachey 1100 Herring Road Rose Hill, NC 28458 910-260-0121 Product Name: Compost Sample Date: 9/6/16 9:30 AM Receive Date: 9/7/16 A & L Lab Number. 87749 A & L Report Number. F16251-6014 COMPOST TECHNICAL DATA SHEET A & L Great Lakes Laboratories, Inc. 3505 Conestoga Drive FortWayne IN 46808 Compost Parameters _ Methodl Reported as (units ofineasure) Test Results !^ Plant Nutrients: %, weight basis Not Reported Moisture Content TMECC 03.09-A %, wet weight basis 2599 Organic Matter Content TMECC 05.07-A %, dry weight basis 36.96 PH TMECC 04.11-A pH units 7.7 Soluble Salts (electrical TMECC 04.10-A dS/m (mmhos/cm) 7.49 conductivity EC y) Particle Size TMECC 02.02-B % < 9.5 mm (3/8 in.), dw basis 98.49 Stability Indicator (respirometry) Stability Rating: CO2 Evolution TMECC 05.08-13 mg COZ-C/g OM/day 1 Very Stable mg CO2-C/g TS/day 1 Maturity Indicator (bioassay) Percent Emergence TMECC 05.05-A average % of control 87 Relative Seedling Vigor TMECC 05.05-A average % of control 48 Select Pathogens TMECC07.01-B PASS/FAIL: per US EPA Class A PASS Fecal Coliform standard, 40 CFR § 503.32(a) Trace Metals TMECC 04.06 PASSNAIL: per US EPA Class A PASS As, Cd, Pb, Hg, standard, 40 CFR § 503.13, Mo, Ni, Se, Zn Participants in the US Composting Councils Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along will) compost end use instructions, as a means to better serve the needs oftheir compost customers. This product meets or exceeds the parameters of the Acceptable Range of compost characteristics contained in the USCC's Consumer Compost Use program. ComPOSt Ingredients: This compost product has been sampled and tested as required by the Seal of Testing Assurance Program of the United States Composting Council (USCG), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by calling McGill Environmental Systems 919-362-1161. The USCC makes no warranties regarding this product or its contents, quality, or suitability for any particular use. For additional information pertaining to compost use, the specific compost parameters tested for within the Seal of Testing Assurance Program, or the program in general, log on to the US Composting Council's TMECC web -site at http:/!ww►v. tmeceorg/stal Report Number F16251-6014 r Account Number a! i rz 58010 To: MCGILL ENV SYS / DELWAY PLANT For: COMPOST copy: AL RATTIE 1100 HERRING RD ROSE HILL, NC 28458 STA Attn: ANTHONY TEACH EY Date Sampled: 9/6/2016 Sample ID: MGSB Date Received: 9/7/2016 Lab Number: 87749 COMPOST ANALYSIS Date Reported: 9/23/2016 Page: 1 of 3 Analysis Unit Analysts Result Dry Basis Result Analysis Method Moisture @ 70 C % 25.99 TMECC 03.09-A Solids % 74.01 TMECC 03.09-A Total Nitrogen (N) % 1.55 2.10 TMECC 04.02-D Phosphorus (P) % 1.05 1.42 TMECC 04.03-A Phosphate (P205) % 2.42 3,25 TMECC 04.03-A Potassium (K) % 0.53 0.71 TMECC 04.04-A Potash (K20) % 0.63 0.85 TMECC 04.04-A Magnesium (Mg) % 0.22 0.30 TMECC 04.05-MG Calcium (Ca) % 5.20 7.03 TMECC 04.05-CA Arsenic mg/kg 7.04 9.51 SW846-6020 04.06-As Cadmium mg/kg <0.358 < 0.484 SW846-6020 04.06-Cd Chromium mg/kg 16.9 22.8 SW846-6020 04.06-Cr Copper mg/kg 104 141 SW846-6020 04.06-Cu Mercury mg/kg <0.423 < 0.572 SW846-6020 04.06-Hg Molybdenum mg/kg 2.47 3.34 SW846-6020 04.06-Mo TMECC - Test Methods for the Examination of Composting and Compost (TMECC), The U.S. Composting Council. Report Approved By: Approval Date: 9/23/2016 Greg Neyman - Vice President / COO Report (Number F16251-6014 Account (Number 58010 To: MCGILL ENV SYS / DELWAY PLANT 1100 HERRING RD ROSE HILL, NC 28458 Attn: ANTHONY TEACHEY sample ID: MGSB Lab Number: 87749 For: COMPOST STA COMPOST ANALYSIS Analysis Unit Nickel mg/kg Lead mg/kg Selenium mg/kg Zinc mg/kg 503 Metals PASS/FAIL pass/fail pH - Soluble Salts dS/m Fecal Coliform/MPN MPN/g dry Pathogen Reduction - PASS/FAIL pass/fail Ash @ 550 C Organic Matter (LOI @ 550 C) Total Organic Carbon (C) Carbon:Nitrogen Ratio (C:N) - Foreign Material Germination - Emergence Analysis Result 9.5 8.0 1.61 742 7.7 7.49 46.66 27.35 13,68 8.8:1 87 copy: AL RATTIE Date Sampled: 9/6/2016 Date Received: 9/7/2016 Date Reported: 9/23/2016 Page: 2 of 3 Dry Basis Result Analysis Method 12.8 SW846-6020 04,06-Ni 10.8 SW846-6020 04,06-Pb 2.18 SW846-6020 04,06-Se 1003 SW846-6020 04.06-Zn PASS EPA 503 Metal Limits TMECC 04.11-A TMECC 04.10-A < 2 SM(20th)-9221E TMECC PASS 40 CFR 503 Class A Compost 63.04 TMECC 03.02-13 36.96 TMECC 05.07-A 18.48 TMECC 04.01-A 8.8:1 TMECC 05.02-A 0.44 TMECC 03.08-A TMECC 05.05-A TMECC - Test Methods for the Examination of Composting and Compost (TMECC), The U.S. Composting Council. Report Number F16251-6014 Account Number 58010 To: MCGILL ENV SYS / DELWAY PLANT 1100 HERRING RD ROSE HILL, NC 28458 Attn: ANTHONYTEACHEY Sample ID: MGSB Lab Number: 87749 For: COMPOST STA COMPOST ANALYSIS copy: AL RATTI E Date Sampled: 9/6/2016 Date Received: 9/7/2016 Date Reported: 9/23/2016 Page: 3 of 3 Analysis Unit Analysis Result Dry Basis Result Analysis Method Germination - Vigor % 48 TMECC 05.05-A Ave Ht of Seedlings in Control centimeters 7.3 TMECC 05.05-A Ave Ht of Seedlings in Compost centimeters 3.5 TMECC 05.05-A Respiration - CO2-C/g TS mg CO2-C / g TS/Day 1 TMECC 05.08-13 Respiration - CO2-C/g OM mg CO2-C / g OM/Day 1 TMECC 05.08-13 Compost Stability Index - Very Stable TMECC 05.08 Retained on U.S. 2-inch Sieve % 0.00 TMECC 02.02-13 Retained on U.S. 1-inch Sieve % 0.00 TMECC 02.02-8 Retained on U.S. 5/8-inch Sieve % 0.00 TMECC 02.02-13 Retained on U.S. 3/8-inch Sieve % 1.51 TMECC 02.02-B Retained on U.S. 1/4-inch Sieve % 8.85 TMECC 02.02-B Retained on U.S. 5/32-inch % 10.59 TMECC 02.02-13 TMECC - Test Methods for the Examination of Composting and Compost (TMECC), The U.S. Composting Council. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: WQ0006816 WWTP Name: NPDES Number: Monitoring Period: From 10/1/2016 To 10/31/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative I ❑ Alterative 2 ❑ Alternative 3 ❑ . Alternative 4 ❑ Alterative 5 C7 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 0 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alterative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying[] Com )ostinE ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative perfarmed (Class A or Class B) com lete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g ty um er o a Excee- de Frequency of Analysis Sample Type Analytical �ica Tech - .i ue Minimuni Geo. Mean Maximuir Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform ) 3 MPN per 4 grams total solid (dry wei.-fit) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) 0 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ lAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed L] CERTIFICATION STATEMENT (please check the appropriate statement) Ltl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) r .f Z G- 7 Signature of Preparer* Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 503 (12/2006) _ I McGill Env. Svs. I Delwav Plant COMPOSTINGCOUNCIL Anlhimy I rtrc•hc� US `i 0 V N C I L I I lit) I I'crrurp; Ruud Jtuu• Bill, NC 28 4SS Sr'l l o f "es, in K 410- wl 01:? 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Sys./ Delway Mani USCOMPOSTING Anthony cachet COUNCIL 1 101) 1lcrring Road Rase IIill, ail' `veil of %e'+t•ur[q ')lU-?tdt-tll�l 1 u ra if r e Produ(t Ntit"tr McGill Suillmilder -- - Sample AM,. 10/31201 G Rec oirc, AM-. 10,14/20116 & 1. t al) Number., 88311 — A & (_ Rrpnrt NtJmbor F1 h278-G(109 COMN)S7' TECHNICYAL, DATA SHETT A & L Great takes Laboratories, Inc. 3.505 Conestoga Drive Fort Wayne IN 468M Comparst Puramc•trr.,, ,Ne°rlrod Ili porwal' as tunics (,( mra,urri Test me.w t, Not Repoilud U'i f),)-A wo welltht halts 14 11 Putt°.('( I1 0-17-A dr,y+teq-jl1 45.70 — �Y M11•(Y"I)•1 11 A l,lllullls I M11FC( 04 10-A ds•[[111111111tus ri,i 111 •11 CA11 ('l .02-11 „ y S nnn (l-K m )• dw I [11i.�ta "ff, �lUh/hr4' li err./h� Illl„ (. •l 1 ( i Ill 11:1\ I ('(a I't11.1'1' 1t �'i'tt� stahlc fill- 1. i 1 (. l -,,iav 1 ('t't,rnt I•tni•I:�rttcr I A11•('(.' 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Ilns pluluil nxcls ,a . �, tti,I> the l,druncttr; it Ihr a A, rtll;,hl[° Ranl;c' fit , 01111)u:.1 a hdrac li•rIs111 s, unL•unril (hr �ti(•t l'unsuulrra'untpu•:11 pn,prant us!=— 't1117ft(1,ti't %ri)tiYt'111r _ _ -_ __ _- 1 ntul IeslrJ as tctluuctl h� Ihr Viral nl`I�•,tutp! 1'rul;ram rt the ltnurtl ('t,ntln,tiUlth. leant tlie" l "I INlediiitk It,r thI•. e xaminatuan of (nm -upusl silt] 0mip„stiril,•' nt.luual le:,l result, are ,.,lhlhlc upon rt'alu st I,y r.111u1>,'�1rtrrll } ntlrnunuutal `i��trntti`1!'I•ln_' 1161 The IN(V 1nakes 111) ,karrlflttrs rcl;: udifil. prudur; 11r 00MVnts. ,lualtlti, of •<ullablill't Ilu :un JIMticular use Por idditio► al infarintition perrtrining to c•ompo.c•t um,, rhr.a/►rri/ic compost pu►ameterr wkwif for ►rithirt th t, Seal elf Tewin•t; 9tisuratict' 1'rorrrum, or the progritm in gernerrul, lo,; on to thr, f `3• ('omposfinlr ('oune•il s T[tiffiC•C t~v,b-s'itt• ut hup. /i as ww.filleci%or4; i.ktaf. .; . - Number Account . Number a&Lgreat4akes L I- i OR I 28458 AM: Sample ID: Lab Number; 88311 COMPOST ANALYSIS Analysis Analysis Unit Result C 34.31 Total Nitrogen (N) 0,54 0,21 Calcium (Ca) 4.11 mg/kg - 7.8 <0.379 COT7,PU5- COPY A,- IE Date Sampled: Date Received: Date Reperted; Page: 1 of 3 Dry Basis Result Analysis Method TMECC TMECC 13 TMECC, 0.68 TMECC 04.04-A TMECC 6.25 04.05-CA < 0.1.06-HR 's ce.", Rvva,' Numt;vr F 1L,278-5009 a&Lq reat�cj ke5---. Accuun, Nufte' G 0 58010 -0 MCUILL rV, sv j `DE, y r dear vICC -L �,r L 110C POSE H!LL %C Attn: Sample ID: MCG ILL Lab Number: 88311 COMPOST ANALYSIS Analysis Analysis Unit Result mg/'kg 7.9 Lead mg/kg 7.5 Selenium mg/kg 2,63 346 503 V. pH 7-0- Soluble Salts 10.41 teCaj '1-oi1jf0rn/r,,' Pathogen Reduction PASS/FAIL k., n COD' 5 -1- _. i- — Organ,- :"e,- (-01 .ED 55.c., T :, a 1 171 1 (. a r on, C) Carbon: Nitrogen,-,-.* copy. Date Sampled: Date Recelvea: DateReperted: 10/21/2016 Page: —?of3 Dry Basis Result Analysis Method SW846-6020 527 SW846-6020 PASS TIVIECC 04.1 !-A TIVI ECC 04. 10-A < 2 SM(20th)-9221E PASS 40 CFR 503 Class A T M E C 04.01-A 0.99 E T IC- Report Nunur? F16278-6009 a&Lgceatl.a kes AccoQnt Numbe, .801 C ••r i' R *o MCGILL EN,. % 7E1.'- "'y PLAINT 1100 RRINC i. ROSE ., rvC : _16 Attn: Samplelo: MCGILL Lab Number: 88311 Analysis Ave Ht of Seedlings in Ave Ht of Seedlings in Respiration - CO2-C/g TS Respiration - CO2-C/g OM Compost Stability Index Salmonella Retained on U.S. 2-inch Sieve Retained on Sieve Retained U.S. Retained Retained i COMPOST ANALYSIS Analysis Result 76 mg CO2-C / g TS/Day mg CO2-C / g MPN/4g dry Unit �h :4hC;t copy: A_ -,",.— Date Sampled: Date Received: 10/4/2016 Date Reported: 10/21/2016 Page: 3 3 Dry Basis �'— Result Analysis Method TIVIECC - 1 05.08-6 1 TM- Very Stable TIVIECC 05.08 SM(29th)-9260D TMECC 02.02-6 0.00 1.74 02 8 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: WWTP Name: NPDES Number: WQ0006816 Monitoring Period: From 11/1/2016 To 11/30/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 0 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost❑ Heat Drying ❑ Heat Treatment ❑ Thermophilie ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ElAlternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air DlyingC7 Composting ❑ jAerobic Digestion El Anaerobic DigestioE ❑ .. .. _ . . - If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- Frequency of Analencesysis Sample Type Analytical Tech - niuLie klinimu Geo. Mean Maximo Units Fecal Coliform 2x10tothe 6th power per gram of total solids WN CFU 1000 mpn per gram of total solid (dry weight) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 WN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) 0 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) C� Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (type or print) �� Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) USCOMPOSTING COUNCIL Sedl of Testing Assurance McGill Env. Sys. I Delway Plant Anthony Teachey 1100 Herring Road Rose Hill, NC 28458 910-260-0121 Product Name: McGill Soilbuilder Sample Date: 11/8/2016 Receive Date: 11/9/2016 A & L Lab Number: 89176 A & L Report Number F16314-6023 COMPOST TECHNICAL DATA SHEET A & L Great Lakes Laboratories, Inc. 3505 Conestoga Drive Fort Wayne IN 46808 �� x Compost Parameters illethod _ e _ Reported as (units ofineasure) Test Results _ Test Results Plant Nutrients: %, weight basis %, wet weight basis %, dry weight basis Nitrogen TMECC 04.02-D Total N 1.41 2.22 Phosphorus TMECC 04.03-A P205 1.96 3.07 Potassium TMECC 04.04-A K20 0.42 0.66 Calcium TMECC 04.05-CA Ca 3.70 5.83 Magnesium TMECC 04.05-MC Mg 0.18 0.28 Moisture Content TMECC 03.09-A %, wet weight basis 36.47 Organic Matter Content TMECC 05.07-A %, dry weight basis 48.60 PH TMECC 04.11-A pH units 7.7 Soluble Salts (electrical conductivity EC;) TMECC 04.10-A dS/m (mmhos/cm) 7.96 Particle Size TMECC 02.02-B % < 9.5 mm (3/8 in.), dw basis 96.52 Stability Indicator (respirometry) CO2 Evolution TMECC 05.08-B mg CO2-CIg OWday mg CO2-C/g TS/day 1 1 Stability Rating: Very Stable Maturity Indicator (bioassay) Percent Emergence TMECC 05.05-A Relative Seedling Vigor TMECC 05.05-A average % of control average % of control 93 60 Select Pathogens TMECC 07.01-B PASS/FAIL: per us EPA Class A standard, 40 CFR § 503.32(a) PASS Fecal Coliform Trace Metals TMECC 04.06 PASS/FAIL..: per US EPA Class A standard, 40 CFR § 503.13, Tables I and 3. PASS As, Cd, Pb, Hg, MO, Ni, Se, Zit Participants in the US Cottrposting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. r map J USCOMPOSTING COUNCIL .Seal of testing Assitrance McGill Env. Sys. / Delway Plant Anthony Teachey 1100 Herring Road Rose Hill, NC 29458 910-260-0121 Product Name: McGill Soilbuilder Sample Date: 11/8/2016 Receive Date: 11/9/2016 A & L Lab Number: 89176 A & L Report Number: F16314-6023 COMPOST TECHNICAL DATA SHEET A & L Great Lakes Laboratories, Inc. 3505 Conestoga Drive Fort Wayne IN 46808 Compost Parameters Method Reported as (units ofineasure) Test Results Plant Nutrients: %, weight basis Not Reported Moisture Content TMECC 03.09-A %, wet weight basis 36.47 Organic Matter Content TMECC 05.07-A %, dry weight basis 48.60 pH TMECC 04.11-A pH units 7.7 Soluble Salts (electrical TMECC 04.10-A dS/m (mmbos/cm) 7.96 conductivityEC5) Particle Size =TMECC 02.02-B % < 9.5 mm (318 in.), dw basis 96.52 Stability Indicator (respirometry) Stability Rating: CO, Evolution TMECC 05.08-B mg-COz-C/g OM/day 1 Very Stable mg CO2-C/g TS/day I Maturity Indicator (bioassay) Percent Emergence TMECC 05.05-A average % of control 93 Relative Seedling Vigor TMECC 05.05-A average % of control 60 Select Pathogens TMECC 07.01-B PASSIFAIL: per US EPA Class A PASS Fecal Coliform standard, 40 CFR § 503.32(a) Trace Metals TMECC 04.06 PASS/FAIL: per Us EPA Gass A PASS As, Cd, Pb, Hg, standard, 40 CFR § 503.13, Mo, Ni, Se, Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs of their compost customers. :r0m4� Milo fImWN :Yip�7/bf* I laYun ce I M M Imm Compost Ingredients: This product meets or exceeds the parameters of the Acceptable Range of compost characteristics contained in the USCC's Consumer Compost Use program. This compost product has been sampled and tested as required by the Seal of Testing Assurance Program of the United States Composting Council (USCC), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by calling McGill Environmental Systems 919-362-1161. The USCC makes no warranties regarding this product or its contents, quality, or suitability for any particular use. For additional infbrmation pertaining to compost use, the specific compost parameters tested for within the Seal of Testing Assurance Program, or the program in general, log on to the US Composting Council °s TMECC web -site at hop✓lwww. tmece. org/stal. Report Number F16314-6023 Account Number 58010 To: MCGILL ENV SYS / DELWAY PLANT 1100 HERRING RD ROSE HILL, NC 28458 Attn: ANTHONY TEACHEY samplelD: MCGILLSOILBUILDER Lab Number: 89176 For: MCGILL SOILBUILDER STA COMPOST ANALYSIS M 0 ;11 copy: AL RATTIE Date sampled: 11/8/2016 Date Received: 11/9/2016 Date Reported: 12/1/2016 Page: 1 of 3 Analysis Unit Analysis Result Dry Basis Result Analysis Method Moisture @ 70 C % 36.47 TMECC 03.09-A Solids % 63.53 TMECC 03.09-A Total Nitrogen (N) % 1.41 2.22 TMECC 04.02-D Phosphorus (P) % 0.85 1.34 TMECC 04.03-A Phosphate (P205) % 1.96 3.07 TMECC 04.03-A Potassium (K) % 0.35 0.55 TMECC 04.04-A Potash (K20) % 0.42 0.66 TMECC 04.04-A Magnesium (Mg) % 0.18 0.28 TMECC 04.05-MG Calcium (Ca) % 3.70 5.83 TMECC 04.05-CA Arsenic mg/kg 5.77 9.08 SW846-6020 04.06-As Cadmium mg/kg <0.316 < 0.498 SW846-6020 04.06-Cd Chromium mg/kg 20.6 32.5 SW846-6020 04.06-Cr Copper mg/kg 116 182 SW846-6020 04.06-Cu Mercury mg/kg <0.367 < 0.578 SW846-6020 04.06-Hg Molybdenum mg/kg 3.51 5.53 SW846-6020 04.06-Mo TMECC - Test Methods for the Examination of Composting and Compost (TMECC), The U.S, Composting Council. Report Approved By: �'Approval Date: 12/01/2016 Greg Neyman - Vice President / COO Report Number F16314-6023 Account Number 58010 To: MCGILL ENV SYS / DELWAY PLANT 1100 HERRING RD ROSE HILL, NC 28458 Attn: ANTHONYTEACHEY SampleID: MCGILL SOILBUILDER Lab Number: 89176 Analysis Nickel Lead Selenium Zinc 503 Metals PASS/FAIL pH Soluble Salts Fecal Coliform/MPN Pathogen Reduction - PASS/FAIL Ash @ 550 C Organic Matter (LOI @ 550 C) Total Organic Carbon (C) Carbon:Nitrogen Ratio (C:N) Foreign Material Germination - Emergence For: MCGILL SOILBUILDER STA COMPOST ANALYSIS ----- --- _ Analysis Unit Result mg/kg 7.4 mg/kg 8.7 mg/kg 1.45 mg/kg 252 pass/fail - 7.7 dS/m 7.96 MPN/g dry pass/fail % 32.65 30.88 % 15.44 10.9:1 o� % 93 copy: AL RATTIE Date Sampled: 11/8/2016 Date Received: 11/9/2016 Date Reported: 12/1/2016 Page: 2 of 3 Dry Basis Result Analysis Method 11.6 SW846-6020 04.06-Ni 13.7 SW846-6020 04.06-Pb 2.29 SW846-6020 04.06-Se 397 SW846-6020 04.06-Zn PASS EPA 503 Metal Limits TMECC 04.11-A TMECC 04.10-A < 2 SM(20th)-9221E TMECC PASS 40 CFR 503 Class A Compost 51.40 TMECC 03.02-13 48.60 TMECC 05.07-A 24.30 TMECC 04.01-A 10.9:1 TMECC 05.02-A 0.00 TMECC 03.08-A TMECC 05.05-A TMECC - Test Methods for the Examination of Composting and Compost (TMECC), The U.S, Composting Council. Report Number F 16314-6023 Account Number 58010 To: MCGILL ENV SYS / DELWAY PLANT 1100 HERRING RD ROSE HILL, NC 28458 Attn: ANTHONY TEACHEY sampleID: MCGILL SOILBUILDER Lab Number: 89176 Analysis Germination - Vigor Ave Ht of Seedlings in Control Ave Ht of Seedlings in Compost Respiration - CO2-C/g TS Respiration - CO2-C/g OM Compost Stability Index Salmonella Retained on U.S. 2-inch Sieve Retained on U.S. 1-inch Sieve Retained on U.S. 5/8-inch Sieve Retained on U.S. 3/8-inch Sieve Retained on U.S. 1/4-inch Sieve Retained on U.S. 5/32-inch For: MCGILL SOILBUILDER STA COMPOST ANALYSIS Analysis Unit Result % 60 centimeters 7.2 centimeters 5.2 mg CO2-C / g TS/Day mg CO2-C / g OM/Day MPN/4g dry % o� TMECC - Test Methods for she Examination of Composting and Compost (TMECC), The U.S. Composting Council. G'] COtttSti.t -kcs:.com copy: AL RATTLE Date sampled: 11/8/2016 Date Received: 11/9/2016 Date Reported: 12/1/2016 page: 3 of 3 Dry Basis Result Analysis Method TMECC 05.05-A TMECC 05.05-A TMECC 05.05-A 1 TMECC 05.08-13 1 TMECC 05.08-8 Very Stable TMECC 05.08 < 3 5M(29th)-9260D 0.00 TMECC 02.02-B 0.00 TMECC 02.02-8 0.00 TMECC 02.02-8 3.48 TM ECC 02.02-8 8.90 TMECC 02.02-B 15.14 TMECC 02.02-8 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: McGill Environmental Systems WQ Permit Number: WQ0006816 WWTP Name: NPDES Number: Monitoring Period: From 12/1/2016 To 12/31/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alterative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alterative 4 ❑ Alternative 5❑ Alterative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Ell Heat Dtyina ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ElV jAerobic Digestion ❑ Anaerobic Di<uestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge en Density Pathogen � : um er o Excee- d nces Frequency of Analysis Sample Type a Tech - � Minimum Geo. Mean MaxiML1111 Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weir=ht) <2mpn/g <2mpn/g <2mpn/g grams 0 monthly comp. 92218 Salmonella bacteria (in lieu of fecal coliform) 3 WN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) Q All. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Cockman/Compliance Manager Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Z -G Y7 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) PVT USCOMPOSTING COUNCIL SedI of Testing Assuva,ni:e McGill Env. Sys. / Delway Plant Anthony Teachey 1100 Herring Road Rose Hill, NC 28458 910-260-0121 Product Name: McGill Soilbuilder Sample Date: 12112/1613:00 Receive Dale: 12/13/2016 A & L Lab Number: 89992 A & L Report Number.' F16348-6011 COMPOST TECHNICAL DATA SHEET A & L Great Lakes Laboratories, Inc. 3505 Conestoga Drive Fort Wavne IN 46808 Compost Parameters _ Method ~ Reported as (anifs of measure) Test Results Test Results y. ' Plant Nutrients: %, weight basis %, wet weight basis %, dry weight basis Nitrogen TMECC 04.02-D Total N 1.51 2.45 Phosphorus TMECC 04.03-A PZOS 2.11 3.41 Potassium TMECC 04.04-A K20 0.49 0.79 Calcium TMECC 04,05-CA Ca 3.27 5.31 Magnesium TMECC 04.05-MG Mg 0.20 0.32 Moisture Content TMECC 03.09-A %, wet weight basis 38.47 Organic Matter Content TMECC 05.07-A %, dry weight basis 48.06 pH TMECC 04.11-A pH units 7.4 Soluble Salts (electrical conductivity EC5) TMECC 04.10-A dS/m (mmhos/em) 8.53 Particle Size TMECC 02.02-B % < 9.5 mm (3/8 in.), dw basis 99.27 Stability Indicator (respitometry) COZ Evolution TMECC 05.08-B mgCOZ-C/g OM/day Mg CO2-C/g TS/day 1 2 Stability Rating: Very Stable Maturity Indicator (bioassay) Percent Emergence TMECC 05.05-A Relative Seedling Vigor TMECC 05.05-A average % of control average % of control 93 80 Select Pathogens TMECC 07.01-13 PASS/FAIL: per US EPA Class A standard, 40 CFR § 503.32(a) PASS Fecal Coliform Trace Metals TMECC 04.06 PASS/FAIL: per US EPA Class A standard, 40 CFR § 503.13, Tables I and 3. PASS As, Cd, Pb, Hg, Mo, Ni, Se, Zn Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, us a means to better serve the needs of their compost customers. USCOMPOSTING COUNCIL Seal of Testine Assurance McGill Env. Sys. / Delway Plant Anthony Teachey 1100 Herring Road Rose Hill, NC 28458 910-260-0121 Product Name: McGill Soilbuilder Sample Date: 12/12/1613:00 Receive Date: 12/13/2016 A & L Lab Number.' 89992 A & L Report Number. F16348-6011 COMPOST TECHNICAL DATA SHEET A & L Great Lakes Laboratories, Inc. 3S05 Conestoga Drive Fort Wayne IN 46808 ^ Compost Parameters - Method Reported as (units of measure) � Test Results Plant Nutrients: %, weight basis Not Reported Moisture Content TMECC 03.09-A %, wet weight basis 38.47 Organic Matter Content TMECC 05.07-A %, dry weight basis 48.06 pH TMECC 04.11-A pH units 7.4 Soluble Salts (electrical TMECC 04.10-A dS/m (mmhos/cm) 8.53 conducitvio, EC5) Particle Size TMECC 02.02-B % < 9.5 mm (3/8 in_), dw basis 99.27 Stability Indicator (respirometay) Stability Rating: CO2 Evolution TMECC 05.08-13 mg CO,-C/g OM/day 1 Very Stable mg CO,-C/g TS/day 2 Maturity Indicator (bioassay) Percent Emergence TMECC 05.05-A average % of control 93 Relative Seedling Vigor TMECC 05.05-A average % of control 80 Select Pathogens TMECC 07.01-B PASSNAIL: per US EPA Class A PASS Fecal Colifonn standard, 40 CFR $ 503.32(a) Trace Metals TMECC 04.06 PASS/FAIL: per EPA Class A PASS As, Cd, Pb, Hg, standard, 40 CFR § 503.13, Mo, Ni, Se, Zrt Participants in the US Composting Council's Seal of Testing Assurance Program have shown the commitment to test their compost products on a prescribed basis and provide this data, along with compost end use instructions, as a means to better serve the needs oftheir compost customers. Oki Y V t us:._..., I us Compost Ingredients Thus product meets or exceeds the parameters of the Acceptable Range of compost characteristics contained in the USCC's Consumer Compost Use program. This compost product has been sampled and tested as required by the Seal of Testing Assurance Program of the United States Composting Council (USCC), using certain methods from the "Test Methods for the Examination of Compost and Composting" manual. Test results are available upon request by calling McGill Environmental Systems 919-362-1161. The USCC makes no warranties regarding this product or its contents, quality, or suitability for any particular use. For additional information pertaining to compost use, the specific compost parameters tested for within the .Seal of Testing Assurance Program, or the program in general, log on to the US Coinposting Coancil:s TMECC web -site at http://►vww. intecc.orglstal Report Number F16348-6011 Account Number 58010 To: MCGILL ENV SYS / DELWAY PLANT 1100 HERRING RD ROSE HILL, NC 28458 Attn: ANTHONY TEACHEY SampleID: MCGILL SOILBUILDER Lab Number: 89992 ]LI U I For: MCGILL SOILBUILDER copy: AL RATTIE STA Date Received: 12/13/2016 COMPOST ANALYSIS Date Reported: 1/16/2017 Page: 1 of 3 K Analysis Unit Analysis Result Dry Basis Result Analysis Method Moisture @ 70 C % 38.47 TMECC 03.09-A Solids % 61.53 TMECC 03.09-A Total Nitrogen (N) % 1.51 2.45 TMECC 04.02-1) Phosphorus (P) % 0.92 1.49 TMECC 04.03-A Phosphate (P205) % 2.11 3.41 TMECC 04.03-A Potassium (K) % 0.41 0.66 TMECC 04.04-A Potash (K20) % 0.49 0.79 TMECC 04.04-A Magnesium (Mg) % 0.20 0.32 TMECC 04.05-MG Calcium (Ca) % 3.27 5.31 TMECC 04.05-CA Arsenic mg/kg 6.7 10.9 SW846-6020 04.06-As Cadmium mg/kg 0.332 0.540 SW846-6020 04.06-Cd Chromium mg/kg 17.5 28.4 SW846-6020 04.06-Cr Copper mg/kg 113 183 SW846-6020 04.06-Cu Mercury mg/kg <0.346 < 0.562 SW846-6020 04.06-Hg Molybdenum mg/kg 3.04 4.94 SW846-6020 04.06-Mo TMECC - Test Methods for the Examination of Composting and Compost (TMECC), The U.S. Composting Council. Report Approved By: �` ,` Approval Date: 1/16/2017 Greg Neyman - Vice President / COO Report Number F16348-6011 Account Number 58010 To: MCGILL ENV SYS / DELWAY PLANT 1100 HERRING RD ROSE HILL, NC 28458 Attn: ANTHONY TEACHEY sampleID: MCGILL SOILBUILDER Lab Number: 89992 Analysis Nickel Lead Selenium Zinc 503 Metals PASS/FAIL pH Soluble Salts Fecal Coliform/MPN Pathogen Reduction - PASS/FAIL Ash @ 550 C Organic Matter (LOI @ 550 C) Total Organic Carbon (C) Carbon:Nitrogen Ratio (C:N) Foreign Material Germination - Emergence For: MCGILL SOILBUILDER STA COMPOST ANALYSIS Analysis Unit Result mg/kg 7.9 mg/kg 7.4 mg/kg 1.91 mg/kg 295 pass/fail - 7.4 dS/m 8.53 MPN/g dry pass/fail % 31.96 % 29.57 % 14.79 9.8:1 93 i t: tl U r .d.. ..c..la copy: AL RATTIE Date Received: 12/13/2016 Date Reported: 1/16/2017 Page: 2 of 3 Dry Basis ------ —-- -- -- Result Analysis Method 12.9 SW846-6020 04.06-Ni 12.1 SW846-6020 04.06-Pb 3.10 SW846-6020 04.06-Se 480 SW846-6020 04.06-Zn PASS EPA 503 Metal Limits TMECC 04.11-A TMECC 04.10-A < 2 SM(20th)-9221E TMECC PASS 40 CFR 503 Class A Compost 51.94 TMECC 03.02-8 48.06 TMECC 05.07-A 24.03 TMECC 04.01-A 9.8:1 TMECC 05.02-A 0.00 TM ECC 03.08-A TMECC 05.05-A TMECC - Test Methods for the Examination of Composting and Compost (TMECC), The U.S. Composting Council. Report Number F16348-6011 Account Number 58010 To: MCGILL ENV SYS / DELWAY PLANT 1100 HERRING RD ROSE HILL, NC 28458 Attn: ANTHONY TEACHEY sample ID: MCGILL SOILBUILDER Lab Plumber: 89992 For: MCGILL SOILBUILDER STA COMPOST ANALYSIS copy: AL RATTIE Date Received: 12/13/2016 Date Reported: 1/16/2017 Page: 3 of 3 El Analysis Unit Analysis Result Dry Basis Result Analysis Method Germination - Vigor % 80 TMECC 05.05-A Ave Ht of Seedlings in Control centimeters 8.9 TMECC 05.05-A Ave Ht of Seedlings in Compost centimeters 6.0 TMECC 05.05-A Respiration - CO2-C/g TS mg CO2-C / g TS/Day 2 TMECC 05.08-13 Respiration - CO2-C/g OM mg CO2-C / g OM/Day 1 TMECC 05.08-13 Compost Stability Index - Very Stable TMECC 05.08 Salmonella MPN/4g dry < 3 SM(29th)-9260D Retained on U.S. 2-inch Sieve % 0.00 TMECC 02.02-13 Retained on U.S. 1-inch Sieve % 0.00 TMECC 02.02-13 Retained on U.S. 5/8-inch Sieve % 0.00 TMECC 02.02-13 Retained on U.S. 3/8-inch Sieve % 0.73 TMECC 02.02-13 Retained on U.S. 1/4-inch Sieve % 7.93 TMECC 02.02-13 Retained on U.S. 5/32-inch % 13.56 TMECC 02.02-13 TMECC - Test Methods for the Examination of Composting and Compost (TMECC), The U.S. Composting Council. /* aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Delway/Merry Oaks Semi Annual Pace Project No.: 92322440 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Delway Soil Builder Lab ID: 92322440002 Collected: 12/07/16 00:00 Received: 12/07/16 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 12/19/16 16:00 ND mg/L 0.00050 1 12/21/16 09:35 12/21/16 13:48 58-89-9 ND mg/L 0.0030 1 12/21/16 09:35 12121/1613:48 57-74-9 ND mg/L 0.00050 1 12/2111609:35 12121/1613:48 72-20-8 ND mg/L 0.00050 1 12/21/16 09:35 12/21/16 13:48 1024-57-3 ND mg/L 1.0 1 12/2111609:35 12/21/16 13:48 72-43-5 ND mg/L 0.0030 1 12/21/16 09:35 12/2111613:48 8001-35-2 40 % 10-138 1 12/21/16 09:35 12/21/16 13:48 2051-24-3 63 % 10-110 1 12/21/16 09:35 12/21/16 13:48 877-09-8 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum 8390 mg/kg 11.4 1 12113/1619:15 12/1411614:46 7429-90-5 Arsenic 5.9 mg/kg 1.1 1 12/13/1619:15 12/1411614:46 7440-38-2 Cadmium ND mg/kg 0.11 1 12/13/1619:15 12114/1614:46 7440-43-9 Calcium 48200 mg/kg 114 10 12113/1619:15 12/15/1611:46 7440-70-2 Chromium 13.2 mg/kg 0.57 1 12113/1619:15 1211411614:46 7440-47-3 Copper 125 mg/kg 0.57 1 12/1311619:15 12/1411614:46 7440-50-8 Lead 7.4 mg/kg 0.57 1 12113/1619:15 12/1411614:46 7439-92-1 Magnesium 1840 mg/kg 11.4 1 12113/1619:15 1211411614:46 7439-95-4 Molybdenum 3.0 mg/kg 0.57 1 12/13/1619:15 12/14/1614:46 7439-98-7 Nickel 7.6 mg/kg 0.57 1 12/13/1619:15 12114/1614:46 7440-02-0 Potassium 3370 mg/kg 570 1 12/13/1619:15 12114/1614:46 7440-09-7 Selenium 2.6 mg/kg 1.1 1 12/13/1619:15 12114/1614:46 7782-49-2 Sodium 2240 mg/kg 570 1 12113/1619:15 12/14/1614:46 7440-23-5 Zinc 249 mg/kg 1.1 1 12/13/1619:15 12/1411614:46 7440-66-6 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311; 12/12/16 17:45 Initial pH: 7.8; Final pH: 5.5 Arsenic ND mg/L 0.050 1 1211311616:29 12/14/1611:55 7440-38-2 Barium 0.36 mg1L 0.25 1 12/13/1616:29 12/14/1611:55 7440-39-3 Cadmium ND mg/L 0.0050 1 12/13/1616:29 12/14/1611:55 7440-43-9 Chromium ND mg/L 0.050 1 12/13/1616:29 12114/1611:55 7440-47-3 Lead 0.027 mg/L 0.025 1 12/13/1616:29 12/14/1611:55 7439-92-1 Selenium ND mg/L 0.10 1 12113/1616:29 12114/1611:55 7782-49-2 Silver ND mg/L 0.025 1 12/1311616:29 12/1411611:55 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 12/12116 17:45 Initial pH: 7.8; Final pH: 5.5 Mercury 0.00084 mg/L 0.00020 1 12/14/16 03:50 12/14/16 15:43 7439-97-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.11 mg/kg 0.0043 1 12/14/16 04:45 12/14/16 23:21 7439-97-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/28/2016 05:49 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 45 / ,, aceAnal ical www.pacelabsxom ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Delway/Merry Oaks Semi Annual Pace Project No.: 92322440 Sample: Delway Soil Builder Lab ID: 92322440002 Collected: 12/07/16 00:00 Received: 12/07/16 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 12/19/16 16:00 1,4-Dichlorobenzene ND mg/L 0.050 1 12120/1615:54 12121/1613:30 106-46-7 2-Methylphenol(o-Cresol) ND mg/L 0.050 1 12/20/1615:54 12/21/1613:30 95-48-7 3&4-Methylphenol(m&p Cresol) ND mg/L 0.050 1 12120/1615:54 12/21/1613:30 Hexachloroethane ND mg/L 0.050 1 12/2011615:54 12/2111613:30 67-72-1 Nitrobenzene ND mg/L 0.050 1 12/20/1615:54 12/21/1613:30 98-95-3 Hexachloro-1,3-butadiene ND mg/L 0.050 1 12120/1615:54 12/21/1613:30 87-68-3 2,4,6-Tdchlorophenol ND mg/L 0.050 1 12/2011615:54 12/21/1613:30 88-06-2 2,4,5-Tdchlorophenol ND mg/L 0.050 1 12/20/1615:54 12/21/1613:30 95-95-4 2,4-Dinitrotoluene ND mg/L 0.050 1 12/20/1615:54 12/2111613:30 121-14-2 Hexachlorobenzene ND mg/L 0.050 1 12/2011615:54 12/21/1613:30 118-74-1 Pentachlorophenol ND mg/L 0.10 1 12120/1615:54 12/21/1613:30 87-86-5 Pyridine ND mg/L 0.050 1 1212011615:54 1212111613:30 110-86-1 Surrogates Nitrobenzene-d5 (S) 42 % 12-102 1 12120/1615:54 12/21/16 13:30 4165-60-0 2-Fluorobiphenyl (S) 42 % 13-107 1 12/20/1615:54 12121/1613:30 321-60-8 Terphenyl-dl4 (S) 55 % 21-132 1 12/20/16 15:54 12/21/1613:30 1718-51-0 Phenol-d6 (S) 19 % 10-110 1 12/20/16 15:54 12/2111613:30 13127-88-3 2-Fluorophenol (S) 28 % 10-110 1 12/20/16 15:54 12/21/16 13:30 367-12-4 2,4,6-Tribromophenol (S) 58 % 27-108 1 12/20/16 15:54 12/21/1613:30 118-79-6 8260 MSV TCLP Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 12/12/16 11:34 Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture ND mg/L 0.19 38.5 12/14/16 22:28 71-43-2 ND mg/L 0.38 38.5 12/14/16 22:28 78-93-3 ND mg/L 0.19 38.5 12/14/16 22:28 56-23-5 ND mg/L 0.19 38.5 12/14/16 22:28 108-90-7 ND mg/L 0.19 38.5 12/14/16 22:28 67-66-3 ND mg/L 0.19 38.6 12/14/16 22:28 106-46-7 ND mg/L 0.19 38.5 12/14/16 22:28 107-06-2 ND mg/L 0.19 38.5 12/14/16 22:28 75-35-4 ND mg/L 0.19 38.5 12/14/16 22:28 127-18-4 ND mg/L 0.19 38.5 12/1411622:28 79-01-6 ND mg/L 0.19 38.5 12/14/16 22:28 75-01-4 97 % 70-130 38.5 104 % 67-135 38.5 99 % 70-130 38.5 Analytical Method: SM 254OG 56.2 % 0.000010 1 Analytical Method: ASTM D2974-87 43.8 % 0.10 1 REPORT OF LABORATORY ANALYSIS 12/14/16 22:28 17060-07-0 1 g 12/14/16 22:28 2037-26-5 12/14/16 22:28 460-00-4 12/0911617:14 12/12/16 07:43 This report shall not be reproduced, except in full, Date: 12/28/2016 05:49 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 45 2aceAnalXical ww.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Delway/Merry Oaks Semi Annual Pace Project No.: 92322440 Sample: Delway Soil Builder Lab ID: 92322440002 Collected: 12/07/16 00:00 Received: 12/07/16 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1010 Flashpoint,Closed Cup Analytical Method: EPA 1010 Flashpoint >200 deg F 70.0 1 12/13/16 09:45 160.4 Total Volatile Solids Analytical Method: EPA 160.4 Total Volatile Solids 462000 mg/kg 10000 1 12/11/16 14:25 9046 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.5 Std. Units 0.10 1 12/14/1610:39 H1 Plant Available Nitrogen Analytical Method: SM 2710B Plant Available Nitrogen 5590 mg/kg 0.12 1 12/28/16 17:48 N2 350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0 Nitrogen, Ammonia 1720 mg/kg 17A 1 12/28/16 12:42 7664.41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 17400 mg/kg 1050 20 12/16/16 02:56 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate 11.1 mg/kg 3.6 1 12/13/16 18:22 Nitrogen, Nitrite 17.5 mg/kg 1.8 1 12/13/16 18:22 Nitrogen, NO2 plus NO3 28.6 mg/kg 3.6 1 12/13/16 18:22 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 9480 mg/kg 214 60 12/17/16 00:20 7723-14-0 733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/kg 1.8 1 12/1311615:18 12/14/16 00:04 734S Reactive Sulfide Analytical Method: SM4500S2F-00 Preparation Method: SW-846 7.3.4.2 Sulfide, Reactive ND mg/kg 17.7 1 12/13/16 15:18 12/13/16 22:14 Total Organic Carbon Analytical Method: EPA 9060 Modified Surrogates RPD% 37.4 % 0.10 1 12/19/1615:07 Total Organic Carbon 247000 mg/kg 30000 1 12/19116 15:07 7440-44-0 Total Organic Carbon 169000 mg/kg 32300 1 12/19/16 15:14 7440-44-0 Mean Total Organic Carbon 208000 mg/kg 31200 1 12/19/1615:07 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/28/2016 05:49 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 45 �,..PalceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: DELWAY/MERRY OAKS SEMI ANNUAL Pace Project No.: 92299337 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DELWAY SOIL BUILDER Lab ID: 92299337002 Collected: 05/27/16 00:00 Received: 05/27/16 11:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilufions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 06/09/16 14:00 ND mg/L 0.00050 1 06111/1611:53 06113/1613:07 58-89-9 ND mg/L 0.0030 1 06/11/1611:53 06/13/1613:07 57-74-9 ND mg/L 0.00050 1 06111/1611:53 06113/1613:07 72-20-8 ND mg/L 0.00050 1 06/11/1611:53 06/1311613:07 1024-57-3 ND mg/L 1.0 1 06/11/1611:63 06/13/1613:07 72-43-5 ND mg/L 0.0030 1 06111/1611:53 06/13/1613:07 8001-35-2 46 % 10-138 1 06111/1611:53 06/13/1613:07 2051-24-3 30 % 10-110 1 06/1111611:53 06/1311613:07 877-09-8 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum 5070 mglkg 9.0 1 06/02/16 20:30 06/04/16 00:21 7429-90-5 Arsenic 6.0 mglkg 0.90 1 06/02/16 20:30 06/04/16 00:21 7440-38-2 Cadmium 0.16 mglkg 0.090 1 06/02/16 20:30 06/04/16 00:21 7440-43-9 Calcium 24700 mglkg 45.2 5 06102/16 20:30 06/04/16 15:57 7440-70-2 Chromium 13.2 mg/kg 0.45 1 06/02/16 20:30 06/04/16 00:21 7440-47-3 Copper 102 mg/kg 0.45 1 06/02/16 20:30 06/04116 00:21 7440-50-8 Lead 7.1 mg/kg 0.45 1 06/02/16 20:30 06/04/16 00:21 7439-92-1 Magnesium 1780 mg/kg 9.0 1 06/02/16 20:30 06/04/16 00:21 7439-95-4 Molybdenum 2.3 mg/kg 0.45 1 06/02/16 20:30 06/04/16 00:21 7439-98-7 Nickel 8.1 mglkg 0.45 1 06/02/16 20:30 06/04/16 00:21 7440-02-0 Potassium 3750 mg/kg 452 1 06/02/16 20:30 06/04/16 00:21 7440-09-7 Selenium 1.7 mg/kg 0.90 1 06/02/16 20:30 06/04116 00:21 7782-49-2 Sodium 1730 mg/kg 452 1 06/02/16 20:30 06/04/16 00:21 7440-23-5 Zinc 2" mg/kg 0.90 1 06/02/16 20:30 06/04/16 00:21 7440-66-6 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311; 06/03/16 12:00 Initial pH: 7.7; Final pH: 5.2 Arsenic 0.059 mg/L 0.050 1 06/06/1611:35 06/0711613:57 7440-38-2 Barium ND mg/L 0.25 1 06/06/1611:35 06/07/1613:57 7440-39-3 Cadmium ND mg/L 0.0050 1 06/06/1611:35 06107/1613:57 7440-43-9 Chromium ND mg/L 0.025 1 06/06/1611:35 06/0711613:57 7440-47-3 Lead ND mg/L 0.025 1 06/06/1611:35 06/07/1613:57 7439-92-1 Selenium ND mg/L 0.10 1 06/06/1611:35 0610711613:57 7782-49-2 Silver ND mg/L 0.025 1 06106/1611:35 06/07/1613:57 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 06/03/16 12:00 Initial pH: 7.7; Final pH: 5.2 Mercury 0.00024 mg/L 0.00020 1 06/06/1614:25 06/07/1614:57 7439-97-6 7471 Mercury Analytical Method: EPA7471 Preparation Method: EPA7471 Mercury 0.077 mg/kg 0.0024 1 06/02/16 09:45 06/02/16 13:41 7439-97-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/14/2016 04:14 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 44 2aceAnalj4ical' wvnvpacelabs.com ANALYTICAL RESULTS Project: DELWAY/MERRY OAKS SEMI ANNUAL Pace Project No.: 92299337 Pace Analytical Services, Inc. 9800 KinoeyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DELWAY SOIL BUILDER Lab ID: 92299337002 Collected: 05/27/16 00:00 Received: 05127/16 11:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8270 MSSV TCLP Sep Funnel 1,4-Dichlorobenzene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Hexachloroethane Nitrobenzene Hexachloro-1,3-butadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4-Dinitrotoluene Hexachlorobenzene Pentachlorophenol Pyridine Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture Date: 06/14/2016 04:14 PM Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 06109/16 14:00 ND mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 106-46-7 ND mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 9548-7 NO mg/L 0,050 1 06/14/16 09:48 06/14/1615:37 NO mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 67-72-1 NO mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 98-95-3 NO mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 87-08-3 ND mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 88-06-2 ND mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 95-95-4 ND mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 121-14-2 ND mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 118-74-1 ND mg/L 0.10 1 06/14/16 09:48 06/14/16 15:37 87-86-5 ND mg/L 0.050 1 06/14/16 09:48 06/14/16 15:37 110-86-1 19 % 12-102 1 06/14/16 09:48 06114/1615:37 4165-60-0 25 % 13-107 1 06/14/16 09:48 06/14/16 15:37 321-60-8 65 % 21-132 1 06/14/16 09:48 06/14/16 15:37 1718-51-0 7 % 10-110 1 06/14/16 09:48 06/14/16 15:37 13127-88-3 SO 13 % 10-110 1 06/14/16 09:48 06/14/16 15:37 367-12-4 49 % 27-108 1 06/14/16 09:48 06/14/16 15:37 118-79-6 Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 06103/16 10:20 ND mg/L 0.19 38.5 06/03/16 22:44 71-43-2 ND mg/L 0.38 38.5 06/03/16 22:44 78-93-3 ND mg/L 0,19 38.5 06/03/16 22:44 56-23-5 ND mg/L 0.19 38.5 06/03/16 22:44 108-90-7 ND mg/L 0.19 38.5 06/03/16 22:44 67-66-3 ND mg/L 0.19 38.5 06/03/16 22:44 106-46-7 NO mg/L 0.19 38.5 06/03/16 22:44 107-06-2 ND mg/L 0.19 38.5 06/03/16 22:44 75-35-4 NO mg/L 0.19 38.5 06/03/16 22:44 127-18-4 NO mg/L 0.19 38.5 06/03/16 22:44 79-01-6 NO mg/L 0.19 38.5 06/03/16 22:44 75-01-4 107 % 70-130 38.5 06/03/16 22:44 17060-07-0 1 g 101 % 67-135 38.5 06/03/16 22:44 2037-26-5 98 % 70-130 38.5 06/03/16 22:44 460-00-4 Analytical Method: SM 254OG 65.0 % 0.000010 1 0610111613:31 Analytical Method: ASTM D2974-87 35.0 % 0.10 1 06/02/1611:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 44 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: DELWAY/MERRY OAKS SEMI ANNUAL Pace Project No.: 92299337 Sample: DELWAY SOIL BUILDER Lab ID: 92299337002 Collected: 05/27/16 00:00 Received: 05/27/16 11:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1010 Flashpoint,Closed Cup Analytical Method: EPA 1010 Flashpoint >200 deg F 70.0 1 06/13/16 10:22 160.4 Total Volatile Solids Analytical Method: EPA 160.4 Total Volatile Solids 616000 mg/kg 10000 1 06/02/16 16:13 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.4 Std. Units 0.10 1 06/07/16 10:00 H6 Plant Available Nitrogen Analytical Method: SM 271013 Plant Available Nitrogen 4750 mg/kg 0.12 1 06/10/16 15:42 N2 350.1 Ammonia Analytical Method: EPA 350.1 Nitrogen, Ammonia 2430 mg/kg 76.9 5 06/08/16 15:33 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 3512 Nitrogen, Kjeldahl, Total 14200 mg/kg 1460 20 06/10/16 03:16 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg 3.1 1 06/08/16 17:38 Nitrogen, Nitrite ND mg/kg 1.5 1 06/08/16 17:38 Nitrogen, NO2 plus NO3 ND mg/kg 3.1 1 06/08/16 17:38 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 6880 mg/kg 154 50 06/0611616:42 7723-14-0 733C S Reactive Cyanide Analytical Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/kg 3.1 1 06/06/16 19:31 735S Reactive Sulfide Analytical Method: SW-846 7.3.4.2 Sulfide, Reactive ND mg/kg 30.6 1 06/06/16 15:10 Total Organic Carbon Analytical Method: EPA 9060 Modified Surrogates RPD% 4.0 % 0.10 1 06/13/16 08:41 Total Organic Carbon 228000 mg/kg 24800 1 06/13/16 08:41 7440-44-0 Total Organic Carbon 237000 mg/kg 22600 1 06/13/16 08:47 7440-44-0 Mean Total Organic Carbon 232000 mg/kg 23700 1 06/13/16 08:41 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/14/2016 04:14 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 44 2016 Compost Distribution Summary Month MATERIAL CUSTOMER Dry Tons Jan MCGILLAG Eco Express Solutions 77.85 Hoke County Sand Co. Inc. 325.65 MCGILLAG Total 403.50 SOILBLD Eco Express Solutions 17.74 Davisson Golf, Inc. (Delway) 10.70 Jacksonville, City Parks & Rec 9.51 SOILBLD Total 37.95 Jan Total 441.45 Feb MCGILLAG Eco Express Solutions 28.12 Kornegay Farms 68.68 Raeford, City of WWTP 15.15 Parker, Kimberly 2.33 Earl Smith, Inc. 19.95 Creekside Farming, LLC 299.78 Cummings Farm 301.63 MCGILLAG Total 735.64 SOILBLD Carolina Seasons Nursery, LLC 9.20 Stone Garden 9.62 Carolina Home & Garden, Inc. 8.70 SOILBLD Total 27.53 Feb Total 763.17 Mar MCGILLAG Nathan Coe Murray 10.40 Allen Weatherly 8.72 Rawls, William G. 9.88 Mark E. Reeves 9.92 Joseph R. Bruce 10.82 Lucas, James Wilson 70.25 Premier Builders & Homes 10.08 Creekside Farming, LLC 131.09 RYS Farms (CFMC, Inc.) 121.78 Cummings Farm 224.33 2016 Compost Distribution Summary Month Mar Total Apr MATERIAL CUSTOMER Dry Tons MCGILLAG Dail Farms 9.20 Vance Edward Pittman 30.00 Maynor Farms, LLC 42.03 CW Graham 8.47 MCGILLAG Total 696.96 SOILBLD BC Mulch & More 10.47 Family Home & Garden 10.38 Norwood Road Garden Center 19.49 The Rock Shop 10.08 Triangle Landscape Supplies 50.75 Jacksonville, City Parks & Rec 10.49 Carolina Seasons Nursery, LLC 10.59 Stone Garden 10.41 Carolina Home & Garden, Inc. 10.17 Bradsher Landscape Supplies 10.07 Mulch Bucket (Oasis Landscape) 10.71 Wendell Landscape Supply 10.10 Ken's Produce & Garden Center 10.51 M W Blake Landscaping, Inc. 10.20 SOILBLD Total 194.43 891.38 MCGILLAG Eco Express Solutions 86.37 Kornegay Farms 268.15 Nathan Coe Murray 67.39 William Terry Ivey 44.98 Joseph R. Bruce 27.77 Earl Smith, Inc. 64.87 Lucas, lames Wilson 455.82 Cummings Farm 161.83 Vance Edward Pittman 8.78 Hydroseeding Technologies, LLC 226.18 Green Chapel Farm, LLC 8.34 MCGILLAG Total 1,420.48 SOILBLD American Soil & Mulch 20.86 BC Mulch & More 18.82 Family Home & Garden 49.22 Garden Supply Company 10.07 2016 Compost Distribution Summary Month MATERIAL CUSTOMER Dry Tons SOILBLD Koster Landscape Mgmnt Inc. 8.69 Sands and Soils 39.06 The Rock Shop 9.71 Triangle Landscape Supplies 94.45 Fulford's Landscape Source 9.14 UNC Wilmington 19.69 Stone Garden 29.44 Carolina Home & Garden, Inc. 8.32 Bradsher Landscape Supplies 30.16 Wendell Landscape Supply 18.79 M W Blake Landscaping, Inc. 10.11 American Property Experts 10.87 Mirimichi Green Express, LLC 173.63 Cleveland Enterprises 9.67 SOILBLD Total 570.69 Apr Total 1,991.17 May MCGILLAG Eco Express Solutions 135.55 Forbis Farms 9.23 Kornegay Farms 538.55 Raeford, City of WWTP 7.21 William Terry Ivey 19.45 Indigo Farms 9.12 Vance Edward Pittman 16.18 Maynor Farms, LLC 8.82 Ken's Produce & Garden Center 40.26 Hydroseeding Technologies, LLC 260.55 Jeffery Stewart Grady 10.01 MCGILLAG Total 1,054.94 SOILBLD American Soil & Mulch 8.16 BC Mulch & More 8.29 Family Home & Garden 36.11 Garden Supply Company 29.27 Norwood Road Garden Center 26.42 Sands and Soils 7.60 Seaside Mulch 19.84 Triangle Landscape Supplies 167.48 Davisson Golf, Inc. (Delway) 45.65 Fulford's Landscape Source 8.67 Atlantic Elite Services, LLC 8.12 2016 Compost Distribution Summary Month Total Jun MATERIAL CUSTOMER Dry Tons SOILBLD Jacksonville, City Parks & Rec 16.55 Little's Nursery of Greenville 10.49 Stone Garden 10.21 All About The Yard, LLC 8.95 Carolina Home & Garden, Inc. 9.36 Bradsher Landscape Supplies 26.15 Murphy Family Ventures (RL) 9.14 Mulch Bucket (Oasis Landscape) 9.01 Wendell Landscape Supply 18.75 Ken's Produce & Garden Center 7.93 M W Blake Landscaping, Inc. 8.37 American Property Experts 9.12 Mirimichi Green Express, LLC 129.88 Stephenson's Nursery, Inc. 8.97 Stager's Fresh Cut Grdn Roses 9.25 Carolina Mushroom Farm, LLC 8.52 Morgan Landscaping Supply 15.00 Barnhill Contracting Company 8.30 Kiefer Landscaping Inc. 9.06 SOILBLD Total 698.63 2,753.56 MCGILLAG Eco Express Solutions 104.39 Hoke County Sand Co. Inc. 149.54 Kornegay Farms 20.27 Vance Edward Pittman 41.51 Mirimichi Green Express, LLC 68.34 JBS Construction 19.40 MCGILLAG Total 403.45 SOILBLD American Soil & Mulch 45.38 BC Mulch & More 9.63 Daniels Supply Co, LLC 78.25 Eco Express Solutions 8.61 Family Home & Garden 27.05 Norwood Road Garden Center 59.86 Sands and Soils 15.49 Seaside Mulch 18.19 The Rock Shop 17.20 Triangle Landscape Supplies 130.72 Davisson Golf, Inc. (Delway) 65.81 2016 Compost Distribution Summary Month Jun Total Jul Jul Total Aug MATERIAL CUSTOMER SOILBLD New River Mulch, LLC Gary Gittere Carolina Seasons Nursery, LLC Stone Garden Carolina Home & Garden, Inc. Bradsher Landscape Supplies Sunshine Garden Market Wendell Landscape Supply Mirimichi Green Express, LLC Morgan Landscaping Supply John L. Atkins Grading Inc. CALIBRE Project No. LT004 Hidden Pond Mulch & Landscapin SOILBLD Total Dry Tons 10.57 3.96 10.25 16.02 8.64 33.85 8.89 8.37 17.58 7.52 542.43 7.29 1,151.54 1,554.99 MCGILLAG Hoke County Sand Co. Inc. 19.45 Lucas, James Wilson 490.14 Vance Edward Pittman 9.81 Weyerhaeuser Nursery (GHW) 81.12 Kilpatrick Farms, Inc. 9.95 MCGILLAG Total 610.48 SOILBLD Eco Express Solutions 126.92 Triangle Landscape Supplies 23.53 Davisson Golf, Inc. (Delway) 16.08 Carolina Home & Garden, Inc. 9.36 CALIBRE Project No. LT004 483.04 Cardinal Landscaping - Fay 9.51 Brian Kelleher 27.87 SOILBLD Total 696.31 MCGILLAG 1,306.79 Carr, Daniel 222.22 Eco Express Solutions 71.91 Hoke County Sand Co. Inc. 679.46 Moores Farms 224.73 Vance Edward Pittman 17.48 2016 Compost Distribution Summary Month MATERIAL CUSTOMER Dry Tons MCGILLAG Weyerhaeuser Nursery (GHW) 21.20 Mirimichi Green Express, LLC 8.85 Hydroseeding Technologies, LLC 99.00 MCGILLAG Total 1,344.84 SOILBLD BC Mulch & More 9.12 Eco Express Solutions 96.97 Family Home & Garden 9.61 Norwood Road Garden Center 9.42 The Rock Shop 9.65 Triangle Landscape Supplies 28.93 Landart Solutions, LLC 8.84 New River Mulch, LLC 10.17 Gary Gittere 19.49 Carolina Home & Garden, Inc. 9.14 Bradsher Landscape Supplies 9.67 Sunshine Garden Market 8.24 Wendell Landscape Supply 9.42 M W Blake Landscaping, Inc. 9.59 Carolina Mushroom Farm, LLC - Barnhill Contracting Company 30.75 City of Clinton, NC 10.10 Cardinal Landscaping - Cary 10.22 SOILBLD Total 299.32 Aug Total 1,644.16 Sep MCGILLAG Carr, Daniel 499.09 Eco Express Solutions 39.25 Hoke County Sand Co. Inc. 507.66 Indigo Farms 9.57 Mirimichi Green Express, LLC 27.94 Kilpatrick Farms, Inc. 9.07 Andrew Spain 9.42 MCGILLAG Total 1,102.00 SOILBLD Eco Express Solutions 58.19 Triangle Landscape Supplies 42.42 Gary Gittere 2.20 Mulch Bucket (Oasis Landscape) 9.20 Brian Kelleher 12.33 2016 Compost Distribution Summary Month MATERIAL CUSTOMER Dry Tons Sep SOILBLD Total 124.35 Sep Total _ v v N 1,226.35 Oct MCGILLAG Carr, Daniel 99.72 Eco Express Solutions 97.74 Hoke County Sand Co. Inc. 51.49 Ronald L. McDonald Sr. 63.69 Earl Smith, Inc. 176.36 Green Chapel Farm, LLC 30.47 MCGILLAG Total 519.48 SOILBLD Triangle Landscape Supplies 9.30 Sunshine Garden Market 10.83 Mirimichi Green Express, LLC 11.69 Power Mulch Inc 7.36 NC DOT Burgaw PO#4300318412 59.14 SOILBLD Total 98.31 Oct Total 617.79 Nov MCGILLAG Carr, Daniel 458.96 Craig Tyson 63.11 Eco Express Solutions 180.23 Ronald L. McDonald Sr. 272.77 Seaside Mulch 8.29 Earl Smith, Inc. 73.49 Cummings Farm 94.18 Mirimichi Green Express, LLC 9.30 Wallace, Thomas Ray 18.31 MCGILLAG Total 1,178.64 SOILBLD Eco Express Solutions 20.62 Triangle Landscape Supplies 9.81 Jacksonville, City Parks & Rec 9.60 New River Mulch, LLC 8.60 Smithfield Farmland-Tarheel 9.12 Carolina Seasons Nursery, LLC 9.76 Stone Garden 9.20 Month Dec Dec Total Grand Total 2016 Compost Distribution Summary MATERIAL CUSTOMER SOILBLD Carolina Home & Garden, Inc. Murphy Family Ventures (RL) Mulch Bucket (Oasis Landscape) SOILBLD Total M CG I LLAG MCGILLAG Total SOILBLD SOILBLD Total Carr, Daniel Earl Smith, Inc. Cummings Farm Vance Edward Pittman Green Chapel Farm, LLC Powers, James M. BC Mulch & More Grady Dobson Triangle Landscape Supplies Smithfield Farmland-Tarheel Brian Kelleher Dry Tons 10.93 1.72 9.45 98.81 1,277.46 61.22 238.06 61.23 7.65 16.43 105.64 490.23 9.99 3.12 21.11 20.53 6.77 61.53 551.75 14,020.02