3412_OldSalisbury_CDLF_November_GWM.pdf

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OLD SALISBURY ROAD LANDFILL
NC DEQ Permit NO. 34-12
ASSESSMENT
MONITORING REPORT
Including the November 2015 Groundwater
Sampling Event
HDR Project No. 00162-218490-018
Forsyth County, North Carolina
January 2016

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Winston-Salem City/County Utilities | Assessment Monitoring Report
TABLE OF CONTENTS
Table of Contents
OLD SALISBURY ROAD LANDFILL NC DEQ Permit NO. 34-12 ..........................................
Table of Contents ......................................................................................................................... i
List of Tables ........................................................................................................................ i
Table of Figures .................................................................................................................... i
Appendices ........................................................................................................................... i
List of Acronyms .................................................................................................................. ii
1.0 INTRODUCTION ............................................................................................................. 1
1.1. Facility Background ...................................................................................................... 1
1.2. Regulatory Authority .................................................................................................... 1
1.3. Geologic Characteristics .............................................................................................. 3
1.3.1. Regional Geologic and Hydrogeologic Setting ...................................................... 3
1.3.2. Site Specific Topography and Drainage ................................................................ 3
1.3.3. Site Specific Hydrogeology ................................................................................... 3
2.0 MONITORING NETWORK .............................................................................................. 4
3.0 DATA COLLECTION ....................................................................................................... 7
4.0 RESULTS ........................................................................................................................ 9
4.1. Detected Groundwater Constituents ............................................................................ 9
4.2. Landfill Gas .................................................................................................................11
5.0 SUMMARY & RECOMMENDATIONS ............................................................................12
List of Tables
Table 1 - Existing Groundwater Monitoring Well Details ............................................................. 5
Table 2 - Sampling Schedule ..................................................................................................... 6
Table 3 - Recent Water Level Readings ..................................................................................... 7
Table 4 - Hydraulic Gradient & Flow Velocity ............................................................................. 8
Table 7 - Methane Gas Readings..............................................................................................11
Table 8 - Recommended Sampling Schedule ...........................................................................12
Table 5 - Event Lab Summary – November 2015 ......................................................................13
Table 6 - Event Field Summary November 2015 .......................................................................14
Table of Figures
Figure 1- Groundwater Contours and Sample Locations – Fall 2015 ......................................... 2
Figure 2 - Historic Groundwater Elevations ................................................................................ 7
Figure 3 - Selected Groundwater Detections in MW-2R ............................................................. 9
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TABLE OF CONTENTS

Appendices
Appendix A – Summary of Groundwater Monitoring Results ................................................... A-1
Appendix B – Laboratory Groundwater Report ........................................................................ B-1
Appendix C – Field Data ......................................................................................................... C-1
Appendix D – Electronic Files ................................................................................................. D-1

List of Acronyms
• 2L 15A NCAC Subchapter 02L - Groundwater Classification and Standards
• µg/L micrograms per liter
• EPA United States Environmental Protection Agency
• MCL Maximum Contaminant Level
• MDL method detction limit
• NC DENR North Carolina Department of Environment and Natural Resources
• NC DEQ North Carolina Department of Environmental Quality1
• ND not detected in sample
• NS not sampled
• NTU Nephelometric turbidity units
• PCB polychlorinated biphenyl
• PCE tetrachloroethene
• PRL practical reporting limit
• PVC polyvinyl chloride
• SWSL solid waste section limits
• SVOC semi-volatile organic compound
• VOC volatile organic compound
• USGS U.S. Geological Survey
1Prior to September 18, 2015, the NC DEQ was referred to as the North Carolina Department of
Environment and Natural Resources (NC DENR). Both naming conventions are used in this report, as
appropriate.

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Winston-Salem City/County Utilities | Assessment Monitoring Report
INTRODUCTION
1.0 INTRODUCTION
HDR Engineering, Inc. of the Carolinas (HDR), on behalf of the Winston-Salem City/County
Utility Commission (the City), is hereby submitting assessment monitoring results for
groundwater at the Old Salisbury Road C&D Landfill (OSR) located in Forsyth County, North
Carolina. The assessment monitoring is being conducted to address the detection of benzene
and tetrachloroethene (PCE) above the groundwater monitoring standards in samples collected
from groundwater monitoring well MW-2R during the May 2011 and June 2011 events.
1.1. Facility Background
The OSR landfill covers approximately 56 acres and is situated within a 140-acre tract north of
Friedberg Church Road and west of Old Salisbury Road in Forsyth County, North Carolina. The
site is accessed via Old Salisbury Road (State Road 3011). The Forsyth/Davidson County line
borders the site to the south. Figure 1 illustrates the location of the OSR landfill. The facility was
issued a permit to operate on July 3, 1996 and opened in August of the same year.
1.2. Regulatory Authority
The site is operated under NC DENR facility permit number 34-12 dated April 6, 2015 (DIN
23258). The groundwater monitoring and reporting requirements are addressed in Items 36 to
45 of the permit. A Groundwater Monitoring Plan was last approved as noted by NC DENR on
March 5, 2015 (DIN 23910). Groundwater and surface water monitoring plans for the site are
addressed by NC Solid Waste Management Rules 15A NCAC 13B .0544(b) and .0544(c)
respectively. The site is currently in assessment monitoring due to detections in MW-2R.
An Assessment Monitoring Plan for MW-2R was submitted in accordance with 15A NCAC 13B
.0545 by HDR on December 9, 2011. The plan was approved with two exceptions on January
17, 2012. The first exception required the location of MW-15 to be in the same flow path as
MW-2R; the second required all wells to be sampled for Appendix II constituents.
In February of 2014 the City requested, and NC DENR approved, the following modifications to
the facility’s assessment monitoring program.
• Groundwater monitoring wells MW-1R, MW-2R, MW-4R and MW-15 will be sampled
semiannually for Appendix I constituents and those additional constituents in Appendix II
that have been detected in the last two years;
• Groundwater monitoring wells MW-1R, MW-2R, MW-4R and MW-15 will be sampled
during every other Fall event for the entire Appendix II constituent list. The next event for
this occurred in the Fall of 2015. Additional Appendix II constituents detected will be
added to the sampling program for subsequent semiannual events; and
• All of the other remaining groundwater monitoring wells and surface water locations will
continue to be sampled semiannually for the full Appendix I constituent list.
In May 2014, the monitoring plan for the facility was updated to incorporate the recent changes
and submitted as part of the renewal package for the facility’s NC DENR Permit to Operate.

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Winston-Salem City/County Utilities | Assessment Monitoring Report
INTRODUCTION
1.3. Geologic Characteristics
This section paraphrases the descriptions in the July 2003 Ground Water Monitoring Plan and
the 2003 Design Hydrogeologic Investigation Report.
1.3.1. Regional Geologic and Hydrogeologic Setting
According to the 1985 Geologic Map of North Carolina, OSR is located in the Charlotte belt of
the Piedmont Physiographic Province. This Province contains metamorphic and igneous
plutonic rocks, which in some areas have been extensively weathered and eroded forming an
undulating and well-dissected topography.
Subsurface conditions generally consist of a veneer of topsoil underlain by residual soils,
saprolite, partially weathered rock, and fractured rock. There is generally a gradual transition
from one material type to the next with varying thickness of each.
The area is underlain by granite rock. The bedrock is typically fractured and is overlain by highly
weathered bedrock called saprolite. The saprolite varies in thickness from a few feet near
bedrock outcrops to over 100 feet. The saprolitic material retains some of the original (relict)
structural features of the parent rock. The nearer surface residual soils are formed by the in-
place physical and chemical weathering of the saprolite and usually do not retain the relict
structural features.
In the Piedmont Physiographic Province, groundwater is present within the openings created by
fractures and joints within the bedrock and within the pore spaces of the overlying-saprolite. The
saprolite/bedrock aquifers are primarily recharged by precipitation in the interstream areas,
which infiltrates through the unsaturated zone to the water table. The depth to groundwater is
generally deeper beneath uplands than beneath valleys. The water table is commonly close to
the top of bedrock and is more often than not, located within the saprolite. Groundwater
generally moves laterally and downward through the saprolite and bedrock toward streams, and
surface water bodies. The water table surface is generally a subdued reflection of the surface
topography.
1.3.2. Site Specific Topography and Drainage
Surface drainage at the subject site is primarily controlled by a north-northwesterly trending
ridge within the property. Surface runoff is directed by a ridge within the site. Construction of the
landfill generally mimics and replaced the natural ridge that existed prior to the landfill. This
ridge directs runoff northeast, west and southwest into tributaries of South Fork Muddy Creek.
The majority of surface runoff within this site is directed to South Fork Muddy Creek on the
north. A small area in the extreme southeasterly section of the site appears to drain south into
Miller Creek. Both the South Fork Muddy Creek and Miller Creek flow to the west where they
converge with Muddy Creek. Muddy Creek flows to the south and converges with the Yadkin
River.
1.3.3. Site Specific Hydrogeology
As documented in the Design Hydrogeological Investigation Report submitted by HDR on
December 2, 2003, the uppermost aquifer underlying the facility is comprised of three
stratigraphic units. The stratigraphic downward progression of the three units is saprolite
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Winston-Salem City/County Utilities | Assessment Monitoring Report
MONITORING NETWORK
transitioning into partially weather bedrock, then competent bedrock. Groundwater flow through
the saprolite and partially weathered bedrock is through the soil matrix, while groundwater flow
through the bedrock is primarily fracture flow.
The average effective porosity of the saprolite stratum is 17 (unitless), while the saprolite
transition zone has an effective porosity of 25. The effective porosity of the bedrock is
significantly less at 2.
The historical hydraulic conductivity (K) calculated for the saprolite is 0.259 feet per day (ft/day)
(9.1 x 10-5 cm/sec). The historical average hydraulic conductivity for the transition zone is 0.466
ft/day (1.65 x 10-4 cm/sec). The historic hydraulic conductivity of the bedrock aquifer was
considerably less than either the saprolite or transition zone units with a K value of 0.043 ft/day
(1.5 x 10-5 cm/sec). Detailed calculations of the hydraulic conductivity, flow rates, and porosity
were provided in the 2003 Design Hydrogeologic Investigation Report.
Based on historical field observations (i.e., soil boring records) and laboratory test results from
the 2003 Design Hydrogeologic Investigation Report, the uppermost aquifer beneath the facility
predominantly exists within the unconsolidated saprolitic soil and transition zone units that have
been classified as micaceous silty sands and sandy silts produced by the in-situ weathering of
the granodiorite parent rock. Groundwater flow within the uppermost aquifer is predominantly
porous flow through the unconsolidated units. There is no evidence of discrete flow patterns
within the saprolite and transition zones of the uppermost aquifer resulting from relict quartz
veins, dikes, healed fractures, or strong preferential alignment of minerals (i.e., foliation). In
general, the flow of groundwater occurs for the facility is from higher elevations onsite to lower
elevations onsite under unconfined (water table) conditions regardless of the stratigraphic unit in
which it resides. As such, the static water table generally mimics the topography.
2.0 MONITORING NETWORK
Sampling occurs semiannually for the site monitoring wells and four surface water monitoring
locations. The groundwater monitoring locations are depicted on the Figure 1. Table 1 provides
location and construction details for the existing monitoring wells.

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MONITORING NETWORK

Table 1 - Existing Groundwater Monitoring Well Details

Groundwater monitoring well MW-1R is located hydraulically upgradient of the landfill and is
considered as the background well for the site. Upstream surface water (SW-1) and
downstream surface water (SW-2) samples are obtained from the adjacent stream to the east.
Surface water samples (SW-3 and SW-4) are obtained from the drainage channel in the vicinity
of MW-2R. SW-3 is located south of the entrance road near MW-2R; SW-4 is located on the
north side of the entrance road, downstream of SW-3.
The sampled locations were evaluated by the methods and for the analytical parameters listed
in Table 2. Samples were collected from each of the landfill groundwater wells using the
dedicated QEDTM MicroPurge ® pumps that were installed in August 2004, except MW-15,
which is sampled with a bailer. Field measurements of pH, conductivity, redox, temperature,
turbidity, dissolved oxygen, and depth to groundwater are collected for each well in addition to
the parameters listed in Table 2.
OSR LF
WELL Installed
NC Sate
Plane
Northing
NC Sate
Plane
Easting
Well
Diameter
(inches)
Well
Depth
(below
ground)
Depth:
Ground to
Top of
Screen
Screened
Interval
(ft)
Screened Interval
Geology
Top Of
Casing
Elevation
(ft MSL)
Ground
Elevation
(ft MSL)
MW-1R 12/27/1995 820,411 1,622,983 2 60.0 45 15 Granitic saprolite 836.42 833.40MW-2R 12/29/1995 820,974 1,622,722 2 23.0 8 15 Granitic saprolite 785.22 781.81
MW-3R 7/7/1999 821,237 1,621,463 2 27.0 12 15 Granitic saprolite 776.60 772.90MW-4R 12/28/1995 820,435 1,621,428 2 20.0 5 15 Granitic saprolite 767.96 765.70MW-5R 12/29/1995 820,137 1,622,130 2 32.0 17 15 Granitic saprolite 784.36 782.30
MW-7 12/28/1995 820,886 1,621,424 2 48.0 33 15 Granitic saprolite 803.66 802.10MW-8 7/7/1999 821,930 1,621,485 2 27.0 12 15 Granitic saprolite 762.50 759.80MW-9 8/11/2004 822,311 1,621,986 2 60.0 45 15 Sand 790.28 788.04
MW-10 8/10/2004 822,626 1,622,699 2 21.0 6 15 Sand 738.21 735.70MW-11 8/10/2004 822,307 1,622,838 2 20.0 5 15 Sand 732.59 730.35MW-12 8/9/2004 821,844 1,622,955 2 16.0 6 10 Silt 739.07 736.41
MW-13 8/9/2004 821,500 1,622,915 2 20.0 5 15 Sand 751.23 749.19MW-14 8/11/2004 822,420 1,622,260 2 60.0 45 15 Sand 783.88 781.44
MW-15 4/6/2012 821,083 1,622,884 2 48.2 33.2 15 Bedrock 802.85 800.58
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MONITORING NETWORK

Table 2 - Sampling Schedule
Method Parameter(s) Frequency Monitoring
Wells
Surface
Water
EPA 300.0 Sulfate 2x/year All All
EPA 6010 Trace Metals 2x/year All All
EPA 7470 Mercury 2x/year All All
EPA 8081
Pesticides Fall of odd years (2015) All None
Pesticides
(Previously detected, see below) 2x/year MW-1R, MW-2R,
MW-4R & MW-15 None
EPA 8082
PCB’s Fall of odd years (2015) All None
PCB’s
(Previously detected, see below) 2x/year MW-1R, MW-2R, MW-4R & MW-15 None
EPA 8151
Herbicides Fall of odd years (2015) All None
Herbicides
(Previously detected, see below) 2x/year MW-1R, MW-2R, MW-4R & MW-15 None
EPA 8260 App I VOCs + Tetrahydrofuran 2x/year All All
Appendix II VOCs Fall of odd years (2015) All None
EPA 8270
SVOCs Fall of odd years (2015) All None
SVOCs
(Previously detected, see below) 2x/year MW-1R, MW-2R, MW-4R & MW-15 None
SM 2320B Alkalinity 2x/year All All
SM 2540C Total Dissolved Solids 2x/year All All
SM 4500 Chloride, Cyanide, Sulfide 2x/year All All
Field Temperature, Specific conductance, Dissolved Oxygen,
Redox, Turbidity, pH
2x/year All All
Field Total well depth and
static water level 2x/year All NA
Previous Detects for:
EPA Method 8081: 4,4'-DDD, 4,4'-DDT, Aldrin, alpha-BHC, delta-BHC, Endosulfan II, Endrin, Endrin aldehyde, Heptachlor, Methoxychlor
EPA Method 8082: None.
EPA Method 8151: 2,4,5-TP (Silvex), 2,4-D
EPA Method 8270: Benzo(a)anthracene, Bis(2-ethylhexyl)phthalate, Chrysene

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Winston-Salem City/County Utilities | Assessment Monitoring Report
DATA COLLECTION
3.0 DATA COLLECTION
As described in Section 2.0, the monitoring program consists of collection and analysis of
groundwater samples from 14 wells. The fall sampling event occurred over four days
(November 16 to 19, 2015). MW-3R was resampled on December 22, 2015 for EPA method
8151 due to sample hold time elapsing before the laboratory was able to perform the analysis.
Pace Analytical Laboratories, Inc. (Pace) of Huntersville, North Carolina (NC Cert. # 5342), on
behalf of HDR, sampled the groundwater monitoring wells for this report. Synoptic groundwater
elevations were also measured at all wells on November 16, 2015.
The depth from the top of the PVC casing to groundwater is measured to the nearest 0.01 foot
prior to purging each well. This depth to water, when subtracted from the reference datum,
provides a groundwater surface elevation. Table 3 provides the recent water level readings.
Figure 2 depicts the relative groundwater elevations in the on-site monitoring wells over time.
During the November 2012 and November 2013 events, the water level in MW-3R was
somewhere in the zone occupied by the pump. The MW-3R elevations illustrated on Figure 2 for
those dates are the point where the water level meter encountered the dedicated pump.
Table 3 - Recent Water Level Readings

Figure 2 - Historic Groundwater Elevations

720
730
740
750
760
770
780
790
800
810
Jan-03 Jan-04 Jan-05 Jan-06 Jan-07 Jan-08 Jan-09 Jan-10 Jan-11 Jan-12 Jan-13 Jan-14 Jan-15 Jan-16 Jan-17
Gr
o
u
n
d
w
a
t
e
r

S
u
r
f
a
c
e

E
l
e
v
a
t
i
o
n

(
f
e
e
t

a
b
o
v
e

m
s
l
)
Sample Date
MW-1R
MW-2R
MW-5R
MW-6R
MW-7
MW-15
MW-4R
MW-3R
MW-8
MW-13
MW-9
MW-12
MW-14
MW-11
MW-10
MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8
11/16/2015 800.32 777.09 754.72 757.85 772.78 765.3 744.1
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15
11/16/2015 736.4 726.11 729 734.33 742.42 731.42 763.41
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Winston-Salem City/County Utilities | Assessment Monitoring Report
DATA COLLECTION
A variable speed micro-purge pump (or bailer in the case of MW-15) was used to purge
groundwater from each well until stabilization of measured field parameters (pH, conductivity,
redox, temperature, turbidity, and dissolved oxygen) occurred. Following completion of purging
activities, the wells were sampled using the same pump and field parameters (pH, specific
conductance, redox, turbidity, dissolved oxygen, and temperature) were recorded on field
sampling logs. Copies of these logs are provided in Appendix B.
Table 3 illustrates the hydraulic gradients calculated between representative well pairs and the
corresponding flow velocities. The flow velocities have been calculated based on the values for
hydraulic conductivity (0.466 ft/day) and effective porosity (25%), as presented in Table 2-9 of
the December 2003 OSR Design Hydrogeologic Investigation Report for the landfill. For your
reference similar numbers presented in previous reports were based on a hydraulic conductivity
(0.259 ft/day) and effective porosity (18.6%), as presented on pages 3 & 5 of the August 2002
version of the OSR Design Hydrogeologic Investigation Report. The current assumptions result
in higher flow rates than those using the values reported in 2002.
The minimum and maximum values are based on the historic data collected from the site
beginning in May 2003. HDR estimates a travel time of about four years between MW-2R and
MW-15, based on the estimated flow rate of 48 ft/yr and a distance of 195 feet.
Table 4 - Hydraulic Gradient & Flow Velocity
Hydraulic
Gradient (ft/ft)
Flow
Velocity (ft/yr)
Based on Historic
Record
Minimum Maximum April 2013 Nov 2013 May 2014 Nov 2014 May 2015 Nov 2015
MW-1R to
MW-4R
0.024
17
0.028
19
0.026
18
0.027
18
0.026
18
0.028
19
0.027
18
0.027
19
MW-1R to
MW-2R
0.032
22
0.040
27
0.036
25
0.038
26
0.037
25
0.040
27
0.038
26
0.037
25
MW-2R to
MW-13
0.060
41
0.064
44
0.062
43
0.063
43
0.064
44
0.062
42
0.062
42
0.062
42
MW-13 to
MW-10
0.013
9
0.014
10
0.014
10
0.014
9
0.013
9
0.014
10
0.014
9
0.014
10
MW-2R to
MW-15
0.068
46
0.071
48
0.071
48
0.070
48
0.071
48
0.068
46
0.069
47
0.070
48

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Winston-Salem City/County Utilities | Assessment Monitoring Report
RESULTS
4.0 RESULTS
4.1. Detected Groundwater Constituents
Detections of benzene and PCE above the groundwater standards triggered assessment
monitoring for well MW-2R. The trends of selected containments detected in MW-2R above the
MCL are shown on Figure 3. During this event every well was sampled for the full Appendix II
list.
Figure 3 - Selected Groundwater Detections in MW-2R

A summary of the constituents detected during this period, along with the NC DEQ solid waste
section limits (SWSL) and applicable North Carolina state maximum concentration levels, are
provided in Table 5. There were thirty-three detections above the 2L standard; these detections
comprised ten parameters in fourteen locations during this event. Methylene chloride was
detected in MW-2R, MW-3R, MW-7, MW-10, MW-12 and the equipment blank between the
SWSL and 2L standards during this event. Seven other constituents were also detected
between the two standards.
Appendix A contains historical summaries of detections by well and by parameter. The complete
laboratory analyses are provided in Appendix B. The field data sheets are provided in Appendix
C. A Microsoft Excel file containing the analysis data in NC DEQ electronic data deliverable
format is include as part of Appendix D.
0.1
1
10
100
1000
10000
100000
1000000
1-Jan-09 1-Jan-10 1-Jan-11 1-Jan-12 1-Jan-13 1-Jan-14 1-Jan-15 1-Jan-16 1-Jan-17
De
t
e
c
t
e
d

C
o
n
c
e
n
t
r
a
t
i
o
n

(
u
g
/
L
)
Date Sample Collected
MW-2R Groundwater Detections
OSR Construction & Demolition Landfill Permit 34-12
Total Dissolved Solids
Manganese
Iron
Barium
Selenium
Lead
Chromium
Methylene Chloride
Benzene
bis(2-Ethylhexyl)phthalate
Tetrachloroethene
Vinyl chloride
4,4'-DDT
Heptachlor
Chloromethane
delta-BHC
alpha-BHC
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Winston-Salem City/County Utilities | Assessment Monitoring Report
RESULTS
Previously the City tested for the fifteen Appendix II constituents selected from the detections
during the 2012 and 2013 sampling events. For this event the entire Appendix II list was run on
all wells. Two herbicides were detected in the May 2015 event. Ten Appendix II constituents
were detected during the November 2015 event. Of the ten detected during this event, only two
heptachlor and dichlordiflouromethane were previously detected. Nine of the constituents that
were sampled for have not been detected in the last two years. Several of the detections are
below the SWSL for the respective constituent. PCBs have never been detected at this facility.
See appendix A for a summary of the Appendix II constituents that have been detected and the
recommendations in section 5.0.
The constituents detected above 2L groundwater standards for this event are as follows.
• Appendix I constituents
o Iron in MW-2R, MW-3R, MW-4R, MW-5, MW-10, MW-11, MW-12, MW-13, MW-
14, MW-15 and all four surface water samples.
o Manganese in MW-2R, MW-3R, MW-4R, MW-5, MW-10, MW-11, MW-13, MW-
14, MW-15 and all four surface water samples.
o Benzene in MW-2R.
o Tetrachloroethene in MW-2R.
o Vinyl Chloride in MW-2R.
o Total dissolved solids in MW-2R.
• Appendix II Pesticide List
o Heptachlor in MW-10
o Heptachlor Epoxide in MW-10
• Appendix II Semi-Volatile Organic Compound List
o Dibenz(a,h)anthracene in MW-3R
o Indo(1,2,3-cd)pyrene in MW-3R
The appendix II constituents detected below the 2L groundwater standard between May 2013
and November 2015 can be summarized as follows.
• Herbicides
o 2,4,5-TP (silvex) was detected in MW-2R during the November 2103 and May
2015 events below the SWSL
o 2,4-D was detected in MW-2R during the November 2103 and May 2015 events
below the SWSL
• Pesticides
o none of the pesticides previously detected above the SWSL (4,4'-DDD, 4,4'-
DDT, Aldrin, alpha-BHC, delta-BHC, Endosulfan II, Endrin, Endrin aldehyde,
Heptachlor, Methoxychlor) have been detected since November 2012, with the
exception of Heptachlor listed above
o Endosulfan I was newly detected in MW-10 during the November 2015 event at
0.17 µg/L which is above the SWSL of 0.1 µg/L.
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Winston-Salem City/County Utilities | Assessment Monitoring Report
RESULTS
• Semi-volatile Organic Compounds
o None of the semi-volatile organic compounds previously on the sampling
schedule (Benzo(a)anthracene, Bis(2-ethylhexyl)phthalate, Chrysene) have
been detected since November 2012.
o 2,4-Dinitrotoluene was detected at 5.9 µg/L in MW-2R below the SWSL of 10
µg/L in November 2015
o 2,6-Dinitrotoluene was detected at 8.1 µg/L in MW-2R below the SWSL of 10
µg/L in November 2015
o 3&4-Methylphenol (m&p cresol) was detected once at 3.6 µg/L in SW-3 below
the SWSL of 10 µg/L in November 2013
o Benzo(g,h,i)perylene was detected at 1 µg/L in MW-3R below the SWSL of 10
µg/L in November 2015
o Di-n-octylphthalate was detected at 5.6 µg/L in MW-8 and MW-12 below the
SWSL of 10 µg/L in November 2015
• Volatile Organic Compounds
o Dichlordiflouromethane was detected at up to 2.1 µg/L in MW-2R, MW-7, MW-
9, MW-12, MW-14 below the SWSL of 5 µg/L in November 2015

4.2. Landfill Gas
Landfill gas is measured at MW-2R and wells in the vicinity of MM-1 during each groundwater
event. These results do not indicate the presence of methane gas in these wells. The results do
indicate the presence of carbon dioxide above ambient levels in MM-1 and recently in MW-13.
The City is responsible for quarterly sampling of all methane monitoring wells and the related
reporting, which is not included in this document.
Table 5 - Methane Gas Readings
Date Time ID # CH4 (%) CO2 (%) O2 (%)
5-May-15 11:11 MM-1 0.0% 3.6% 17.4%
5-May-15 11:26 MW-13 0.0% 0.5% 20.2%
5-May-15 11:19 MW-15 0.0% 0.4% 20.4%
5-May-15 11:05 MW-1R 0.0% 0.1% 20.9%
5-May-15 11:14 MW-2R 0.0% 0.0% 20.7%
16-Nov-15 10:41 ambient 0.0% 0.1% 21.1%
16-Nov-15 13:46 MM-1 0.0% 5.5% 15.5%
16-Nov-15 10:45 MW-13 0.0% 0.7% 20.6%
16-Nov-15 13:30 MW-15 0.0% 0.1% 21.1%
16-Nov-15 13:58 MW-1R 0.0% 0.1% 21.2%
16-Nov-15 13:22 MW-2R 0.0% 0.1% 21.2%
Highlighted cells are outside of normal atmospheric ranges

11
Winston-Salem City/County Utilities | Assessment Monitoring Report
SUMMARY & RECOMMENDATIONS
5.0 SUMMARY & RECOMMENDATIONS
With the exception of the Appendix II constituents, the level of detections from this event is
generally consistent with previous events.
HDR recommends a change to the semi-annual sampling schedule as provided below. The
additional parameters and wells are shown in bold. The items removed are struck through.
• Drop all constituents that have not been detected since November 2012.
• Add all Appendix II constituents that were detected above the SWSL since November
2012.
• Add all Appendix II VOCs that have been detected since November 2013.
Table 6 - Recommended Sampling Schedule
Method Parameter(s) Frequency Monitoring
Wells
Surface
Water
EPA 300.0 Sulfate 2x/year All All
EPA 6010 Trace Metals 2x/year All All
EPA 7470 Mercury 2x/year All All
EPA 8081
Pesticides Fall of odd years (2015) All None
4,4'-DDD, 4,4'-DDT, Aldrin, alpha-BHC, delta-BHC, Endosulfin I,
Endosulfan II, Endrin, Endrin aldehyde, Heptachlor, Heptachlor epoxide & Methoxychlor
(Pesticides recently detected)
2x/year MW-1R, MW-2R, MW-4, MW-7, MW-10 & MW-15 None
EPA 8082 PCB’s Fall of odd years (2015) All None
EPA 8151
Herbicides Fall of odd years (2015) All None
2,4,5-TP (Silvex), 2,4-D
(Herbicides previously detected) 2x/year MW-1R, MW-2R, MW-4R & MW-15 None
EPA 8260
App I VOCs + Tetrahydrofuran 2x/year All All
Appendix II VOCs Fall of odd years (2015) All None
Dichlordiflouromethane
(Appendix II VOC
recently detected)
2x/year All None
EPA 8270
SVOCs Fall of odd years (2015) All None
Benzo(a)anthracene, Bis(2-ethylhexyl)phthalate, Chrysene Dibenz(a,h)anthracene &
Indeno(1,2,3-cd)pyrene
(SVOCs recently detected)
2x/year MW-1R, MW-2R, MW-4R , MW-3R
& MW-15
SW-2
SM 2320B Alkalinity 2x/year All All
SM 2540C Total Dissolved Solids 2x/year All All
SM 4500 Chloride, Cyanide, Sulfide 2x/year All All
Field Temperature, Specific conductance, Dissolved Oxygen, Redox, Turbidity, pH 2x/year All All
Field Total well depth and static water level 2x/year All NA
12
Winston-Salem City/County Utilities | Assessment Monitoring Report
SUMMARY & RECOMMENDATIONS Table 7 - Event Lab Summary – November 2015

• To distinguish non detections (ND) from not sampled (NS), refer to complete laboratory analysis. This table represents both ND and NS as blanks.
SWSL 2L units Row Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Equipment
Blank
µg/L EPA 300.0
250000 250000 µg/L Sulfate 1070 115000 2200 70300 7430 10100 1350 1110 63600 19100 70800 10100 1080 70000 4460 11600 27000 24900 EPA 6010
10 10 µg/L Arsenic 2.6 4.5
100 700 µg/L Barium 207 279 271 184 92.7 140 34.4 186 241 97.2 95.7 71.5 183 74 65 70 152 115
1 4000 µg/L Beryllium 1.9 0.68 0.63
10 10 µg/L Chromium 3.5 5.4
10 1000 µg/L Cobalt 17.4 9.1 28.3 2.5 3.1 2.9
10 1000 µg/L Copper 6.2 6.3 2.8 7.1 3.9
300 300 µg/L Iron 82.8 3080 68200 312 32600 48.6 3690 34600 523 790 466 8180 9830 2070 4160 2240
10 15 µg/L Lead 3.8 8.5 6
50 50 µg/L Manganese 2.8 9010 7100 407 1890 33.6 3.3 4 587 2020 49.6 62.1 69.3 297 688 291 3860 2550
50 100 µg/L Nickel 18 3.7 3.9 3.2 2.8 3.9 2.8
10 20 µg/L Selenium 5.6
NE NE µg/L Sodium 13200 61400 2590 23800 11300 15700 7940 14500 19800 12000 13700 12200 15800 21800 12800 11300 20900 20200
5.5 200 µg/L Thallium 8.8
100 2E+06 µg/L Tin 8.5
25 300 µg/L Vanadium 11.9 9.9 3.7 5.6 3.5 2.6 18.9 4.3 5.6 3.5
10 1000 µg/L Zinc 5.6 5.8 8.7 5.9 7.1 27.2 8.6 6.3 35.4 7.5 EPA 7470
0.2 1 µg/L Mercury 0.12
EPA 8081
0.1 40 µg/L Endosulfan I 0.17
0.05 0.008 µg/L Heptachlor 0.12
0.075 0.004 µg/L Heptachlor epoxide 0.093 EPA 8260
5 6 µg/L 1,1-Dichloroethane 0.91
1 6 µg/L 1,4-Dichlorobenzene 0.38
50 NE µg/L 2-Hexanone 0.69
100 NE µg/L 4-Methyl-2-pentanone (MIBK)2.6
100 6000 µg/L Acetone 11.8
1 1 µg/L Benzene 1.5
5 70 µg/L Chloroform 0.44
1 3 µg/L Chloromethane 0.25
5 70 µg/L cis-1,2-Dichloroethene 0.26 0.8
5 1000 µg/L Dichlorodifluoromethane 0.26 1 0.76 0.23 2.1
1 600 µg/L Ethylbenzene 0.4
5 500 µg/L m&p-Xylene 0.84 0.68
1 5 µg/L Methylene Chloride 1.3 2.3 3.9 1.2 2 1.1
NE NE µg/L o-Xylene 0.27 0.43
1 0.7 µg/L Tetrachloroethene 0.95
NS NS µg/L Tetrahydrofuran 35.8 7 17.7 120 19.8 3.3
1 600 µg/L Toluene 0.27
1 3 µg/L Trichloroethene 0.66
1 2000 µg/L Trichlorofluoromethane 1 1.4 1.1 0.82 0.54 4.8
1 0.03 µg/L Vinyl chloride 0.75
EPA 8270
10 NE µg/L 2,4-Dinitrotoluene 5.9
10 NE µg/L 2,6-Dinitrotoluene 8.1
10 200 µg/L Benzo(g,h,i)perylene 1
10 0.005 µg/L Dibenz(a,h)anthracene 1
Di-n-octylphthalate 5.6 5.6
10 0.05 µg/L Indeno(1,2,3-cd)pyrene 1.1 SM 2320B
NE NE µg/L Alkalinity, Total as CaCO3 48100 440000 102000 144000 32300 67300 23200 23400 48200 127000 41000 37100 51500 103000 35100 43200 210000 187000 SM 4500-Cl-E
NE 250000 µg/L Chloride 8510 48700 2990 16900 16200 6050 2040 4710 47400 14900 9000 3270 3930 113000 21600 12500 16300 19800 SM 4500-CN-E
10 70 µg/L Cyanide 7.5 5.1 4.7 9.8 4.2 5.3 5 5.3 SM 2540C
NE 500000 µg/L Total Dissolved Solids 78000 806000 137000 161000 104000 78000 79000 142000 403000 281000 234000 110000 135000 362000 113000 105000 300000 267000
13
Winston-Salem City/County Utilities | Assessment Monitoring Report
SUMMARY & RECOMMENDATIONS
Table 8 - Event Field Summary November 2015

MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Field
°C
Field Temperature 16 15.9 15.2 15.5 15.9 15.3 15.6 15.9 16.5 15.8 16.2 16.2 16.3 15.6 9.4 11.9 8.2 9
µmhos/cm
Field Specific Conductance 163.2 1044 365.6 395.9 164.5 196.6 58.4 151.5 365.1 400.8 281.5 108.9 152.1 596.2 92.6 88.6 274.8 247.9
mg/L
Oxygen, Dissolved 2.2 2 1 3.3 5.9 0.7 4.4 6.3 0.2 0.1 3.4 1.2 4.8 2.8 5.5 3.5 3.2 7.6
mV
REDOX 34.8 -35.2 -71.6 48.8 52.6 30.9 4 54.3 -77.7 -38.7 -23.3 5.2 49.6 34.8 -78.3 -84.6 -90 -87.1
NTU
Turbidity 1 5.6 7.8 9.6 1 1 1.6 2.6 295 9.3 8.9 51.6 5.9 154.9 48.7 20.5 9.1 3.2
Std. Units
Field pH 5.4 6.1 6.3 5.8 5.8 5.5 5.4 5.3 5.4 5.9 5.8 5.5 5.4 6.2 6.7 6.6 6.4 7
feet
Static Water Level 36.1 8.13 21.88 10.11 11.58 38.41 18.45 53.85 12.1 3.59 4.74 8.81 52.46 39.44
Total Well Depth 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85

14
Winston-Salem City/County Utilities | Assessment Monitoring Report
APPENDIX A – SUMMARY OF GROUNDWATER MONITORING RESULTS
A. a

A
Appendix A –
Summary of
Groundwater
Monitoring Results

A-1 Appendix II Detections (6 pages)
A-2 Detections by Well Location (16 pages)
A-3 Detections by Date (47 pages)

A-1

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6 of 6

This page intentionally left blank.
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels No
v
-
1
5
Ma
y
-
1
5
No
v
-
1
4
Ma
y
-
1
4
No
v
-
1
3
Ma
y
-
1
3
No
v
-
1
2
Ap
r
-
1
2
De
c
-
1
1
No
v
-
1
1
Ju
n
-
1
1
Ma
y
-
1
1
No
v
-
1
0
Ap
r
-
1
0
µg/L
MW-1R
NE NE µg/L Alkalinity, Total as CaCO3 48100 39600 37600 30000 28100 29800 26300 27100 27500
10 10 µg/L Arsenic100 700 µg/L Barium 207 164 142 124 106 109 91.7 93.8 82.6 84.7 85.4
10 0.05 µg/L Benzo(a)anthracene 1.4
15 3 µg/L bis(2-Ethylhexyl)phthalate 2.4
100 700 µg/L Carbon disulfideNE 250000 µg/L Chloride 8510 7640 7090 5600 5880 5910 5320 5350
10 10 µg/L Chromium 1.4 0.96
10 5 µg/L Chrysene 1.5
10 70 µg/L Cyanide 4.4300 300 µg/L Iron 82.8 85.8 52.9
10 15 µg/L Lead
50 50 µg/L Manganese 2.8 2.9
0.2 1 µg/L Mercury1.0 5.0 µg/L Methylene chloride
10 20 µg/L Selenium
10 20 µg/L Silver 0.51
NE NE µg/L Sodium 13200 11600 10600 10800 9940 9080 9180 9440 7670250000 250000 µg/L Sulfate 1070 1700 1720
1 600 µg/L Toluene
NE 500000 µg/L Total Dissolved Solids 78000 133000 120000 91000 103000 84000 95000 93000 95000
10 1000 µg/L Zinc 5.6MW-2R
5 6 µg/L 1,1-Dichloroethane 0.49 1.1 0.83 1.3 1.2 1.2 1.1 1.2 1.1
5 350 µg/L 1,1-Dichloroethene 36.6 38.7
1 6 µg/L 1,4-Dichlorobenzene 0.38 0.4
2 50 µg/L 2,4,5-TP (Silvex) 0.14 0.232 70 µg/L 2,4-D 0.43 1.1
10 NE µg/L 2,4-Dinitrotoluene 5.9
10 NE µg/L 2,6-Dinitrotoluene 8.1
100 4000 µg/L 2-Butanone (MEK)50 NE µg/L 2-Hexanone 0.48
0.1 0.1 µg/L 4,4'-DDT 0.54
100 6000 µg/L Acetone 20.3 3.7
0.05 2 µg/L Aldrin 0.12NE NE µg/L Alkalinity, Total as CaCO3 440000 358000 453000 344000 349000 363000 277000 196000 219000 165000
0.05 0.006 µg/L alpha-BHC 0.12
6 1000 µg/L Antimony 5.4
10 10 µg/L Arsenic100 700 µg/L Barium 279 287 339 324 311 324 335 366 351 273 223
1 1 µg/L Benzene 1.5 1.7 2.5 1.8 1.9 1.4 1.3 1.5 2 1.6 1.3
15 3 µg/L bis(2-Ethylhexyl)phthalate 1.1
1 2 µg/L CadmiumNE 250000 µg/L Chloride 48700 44200 49800 50500 56700 50000 64000 61500 62400 39900
10 3000 µg/L Chloroethane 2.1
5 70 µg/L Chloroform 0.16 0.26 0.36
1 3 µg/L Chloromethane 0.2510 10 µg/L Chromium 3.4 5.4 0.49
5 70 µg/L cis-1,2-Dichloroethene 0.26 0.5 0.38 0.41 0.26 0.25 0.33 0.46 0.26
10 1000 µg/L Cobalt 17.4 20.3 25 22.8 19.2 18.2 15.2 14.8 11.8
10 1000 µg/L Copper 6.3 9.6
10 70 µg/L Cyanide 7.5 4.20.05 0.019 µg/L delta-BHC 0.18
5 1000 µg/L Dichlorodifluoromethane 0.26
0.1 2 µg/L Endrin 0.27
0.1 2 µg/L Endrin aldehyde 0.23 0.280.05 0.008 µg/L Heptachlor 0.48
300 300 µg/L Iron 3080 9560 2580 1650 766 877 1730 3190 2980
10 15 µg/L Lead 3.3
5 500 µg/L m&p-Xylene 0.66 0.7450 50 µg/L Manganese 9010 11900 9880 7950 8710 7880 8400 8280 7920
0.2 1 µg/L Mercury
NS NS µg/L Methane 1280
1 40 µg/L Methoxychlor 0.831 5 µg/L Methylene chloride 1.3 2.3 3.7 3.7 3 4.2 4.5 3.2 3.5 4.1 4.2
10 6 µg/L Naphthalene 0.86 1.3 1.6 1.9
50 100 µg/L Nickel 18 17 25.9 20.6 27.1 20.7 21.8 22.3 20.9
NS NS µg/L Nitrogen, Ammonia 0.12NE NE µg/L o-Xylene 0.33 0.31 0.54 0.54 0.63 1 1.2 0.84
10 20 µg/L Selenium 16.5
10 20 µg/L Silver 5.2 5 2.5 0.85
NE NE µg/L Sodium 61400 51400 58300 59700 46200 45700 43400 38400 31800 27200250000 250000 µg/L Sulfate 115000 98400 117000 136000 128000 115000 79500 95000 96300
1 0.7 µg/L Tetrachloroethene 0.95 1.2 2 1.8 2.2 1.5 1.8 1.7 1.8 1.6 1.4
NS NS µg/L Tetrahydrofuran 35.8 34.6 79.2 72.6 99.6 111 93.2 152 197 274 226
5.5 200 µg/L Thallium 5.1
MCL
c:\pwworking\tpa\d0269489\W-S GW Revised
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Ma
r
-
1
0
Se
p
-
0
9
Ma
r
-
0
9
De
c
-
0
8
Ma
r
-
0
8
No
v
-
0
7
Ap
r
-
0
7
No
v
-
0
6
Ap
r
-
0
6
No
v
-
0
5
Ju
n
-
0
5
No
v
-
0
4
Au
g
-
0
4
Ma
y
-
0
4
No
v
-
0
3
Ma
y
-
0
3
De
c
-
0
2
Ap
r
-
0
2
No
v
-
0
1
Ju
l
-
0
1
De
c
-
0
0
Ju
n
-
0
0
No
v
-
9
9
Ju
n
-
9
9
No
v
-
9
8
Ma
y
-
9
8
Oc
t
-
9
7
Ma
y
-
9
7
Oc
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9
6
Ja
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6
5.885.3 92.8 74.3 85 90.3 105 81 94 82 78 48 95 96.3 460 120 100 130 280 87 150 110 130 150 160 100 290 100 180 224
28 23
1.4 2 0.88 0.64 0.49 2 3.5 4.3 2.3 5 22 6.6 6.6 5.2 7.8 12 49 11 36
22 10 12 6
0.2 1.813
5.5
0.29 0.48 0.62 0.43
21
86
11103 80.7 88.5 98.8 102 107 79 90 52 62 43 52 55 60 56 140 100 160 280 61 180 120 150 1100 190 340 200 160 350
1.9 3
3.4
1.2 1.6 0.5 0.79 2.2 2.1 16 16 3.9 3 14 7.8 210 34 43 4912
7 8.9 6.5 6.9 68 19 31 14 8 26
0.34 0.4
13
0.67 0.68 0.58 1.2 0.93 6
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels No
v
-
1
5
Ma
y
-
1
5
No
v
-
1
4
Ma
y
-
1
4
No
v
-
1
3
Ma
y
-
1
3
No
v
-
1
2
Ap
r
-
1
2
De
c
-
1
1
No
v
-
1
1
Ju
n
-
1
1
Ma
y
-
1
1
No
v
-
1
0
Ap
r
-
1
0
MCL
1 600 µg/L Toluene 0.27
NE 500000 µg/L Total Dissolved Solids 806000 632000 769000 549000 654000 589000 564000 531000 498000
1 3 µg/L Trichloroethene 0.66 0.79 0.85 0.71 0.89 0.68 0.77 0.82 0.88 0.65
1 2000 µg/L Trichlorofluoromethane 1 1.5 2.4 3.7 12 12.1 16.9 20.9 20.1 31.6 36.1 21.925 300 µg/L Vanadium 11.9 11.4 5.5
1 0.03 µg/L Vinyl chloride 0.75 0.7 1.2 0.95
5 500 µg/L Xylenes (Total) 0.98 1.6
10 1000 µg/L Zinc 5.8 8.7 16.8 12.2 21.1 24.5 35.2 33.3MW-3R
NE NE µg/L Alkalinity, Total as CaCO3 102000 107000 177000 155000 155000 175000 142000 150000 155000
10 10 µg/L Arsenic 8.9
100 700 µg/L Barium 271 214 221 205 201 216 173 228 237 301 30210 200 µg/L Benzo(g,h,i)perylene 1
15 3 µg/L bis(2-Ethylhexyl)phthalate 5.5
1 2 µg/L Cadmium
100 700 µg/L Carbon disulfideNE 250000 µg/L Chloride 2990 2990 2940 3260 3620 3860 3920
10 10 µg/L Chromium
10 1000 µg/L Cobalt 9.1 10.1 13.3 53.5 64.1 16.4
10 1000 µg/L Copper 6.210 70 µg/L Cyanide 10.4 7.1 8.1 9.1 6.5
10 0.005 µg/L Dibenz(a,h)anthracene 1
10 0.05 µg/L Indeno(1,2,3-cd)pyrene 1.1
300 300 µg/L Iron 68200 56000 49700 38200 31300 34100 25300 41500 4030010 15 µg/L Lead 3.8 2.7 2.7
50 50 µg/L Manganese 7100 7980 9380 9260 9990 9630 11600 9310 7310
0.2 1 µg/L Mercury
1 5 µg/L Methylene chloride 2.3
10 20 µg/L Selenium10 20 µg/L Silver 0.6
NE NE µg/L Sodium 2590 2770
250000 250000 µg/L Sulfate 2200 3000 3740 4230 3400 5070 5420 6860
100 2E+06 µg/L Tin 5.8NE 500000 µg/L Total Dissolved Solids 137000 182000 191000 187000 193000 175000 172000 168000 180000
25 300 µg/L Vanadium 9.9 8.8 2.8
10 1000 µg/L Zinc 8.7 10.5
MW-4R0.1 0.1 µg/L 4,4'-DDT 0.14
NE NE µg/L Alkalinity, Total as CaCO3 144000 117000 286000 222000 224000 203000 174000 64300 143000
10 10 µg/L Arsenic
100 700 µg/L Barium 184 306 305 264 296 375 400 407 328 126 3351 1 µg/L Benzene 0.42 0.28 0.27
1 2 µg/L Cadmium
NE 250000 µg/L Chloride 16900 22200 50500 29700 36500 33700 34500 33200 29200
1 3 µg/L Chloromethane 0.1510 10 µg/L Chromium 1.3 0.68
10 1000 µg/L Cobalt 28.3 15.2 82 46.6 49.4 35.3 35.5 21.5 15
10 70 µg/L Cyanide 4.3 5.9
0.05 0.019 µg/L delta-BHC 0.0690.1 42 µg/L Endosulfan II 0.12
300 300 µg/L Iron 312 292 126 89.5 158 344 145 368
10 15 µg/L Lead
50 50 µg/L Manganese 407 315 1040 641 688 496 541 370 257
0.2 1 µg/L Mercury1 5 µg/L Methylene chloride
50 100 µg/L Nickel 3.7 2.8 7.2 5.3
10 20 µg/L Selenium 11.5
10 20 µg/L Silver 0.88 1.3NE NE µg/L Sodium 23800 23000 55400 39700 42600 42600 43600 40400 35300
250000 250000 µg/L Sulfate 70300 72700 143000 85200 113000 97600 73600 98700 61800
NS NS µg/L Tetrahydrofuran 7 5.8 15.9 11.8 11.7 8.5 13.5 8.8
NE 500000 µg/L Total Dissolved Solids 161000 304000 692000 445000 496000 413000 435000 374000 34500025 300 µg/L Vanadium 2.7
10 1000 µg/L Zinc 5.9 7.5 7.2 13.6
c:\pwworking\tpa\d0269489\W-S GW Revised
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Ma
r
-
1
0
Se
p
-
0
9
Ma
r
-
0
9
De
c
-
0
8
Ma
r
-
0
8
No
v
-
0
7
Ap
r
-
0
7
No
v
-
0
6
Ap
r
-
0
6
No
v
-
0
5
Ju
n
-
0
5
No
v
-
0
4
Au
g
-
0
4
Ma
y
-
0
4
No
v
-
0
3
Ma
y
-
0
3
De
c
-
0
2
Ap
r
-
0
2
No
v
-
0
1
Ju
l
-
0
1
De
c
-
0
0
Ju
n
-
0
0
No
v
-
9
9
Ju
n
-
9
9
No
v
-
9
8
Ma
y
-
9
8
Oc
t
-
9
7
Ma
y
-
9
7
Oc
t
-
9
6
Ja
n
-
9
6
22.2
4 7.4 8.4 18 31 5.9
314 289 252 231 293 273 310 230 290 300 300 340 270 200 220 13 370 400 950 1500 300 52 1400 860 620 800 790 1230
0.82 2
26.1 3.3
0.63 2.3 3.7 2.3 15 19 50 100 24 77 25 16 28 20 9
14 21 35 53 80 40 39 32 26 27 15 15
0.2 0.7
11.8 4.9 18.1 240.45 1 0.29 1.5 0.87
9.2 12 5.6 7.5
55.9 334 58.3 263 172 287 200 220 220 180 150 140 380 97 94 86 61 900 550 350 570 860 950 2000 850 650 280 720 595
7
1.3 5.4 1.2 0.58 0.4 14 2.6 5.5 5 95 38 28 60 110 300 130 55 47 21
4.8 18 5.3 6 36 14 8.1 9.5 40 50 76 43 29 12 16 17
0.36 0.21 0.3 1.710
2.4 2.6 0.94 6
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels No
v
-
1
5
Ma
y
-
1
5
No
v
-
1
4
Ma
y
-
1
4
No
v
-
1
3
Ma
y
-
1
3
No
v
-
1
2
Ap
r
-
1
2
De
c
-
1
1
No
v
-
1
1
Ju
n
-
1
1
Ma
y
-
1
1
No
v
-
1
0
Ap
r
-
1
0
MCL
MW-5R
100 6000 µg/L Acetone
NE NE µg/L Alkalinity, Total as CaCO3 32300 28600 24000 31900 31700 34800 31200 134000 32800
10 10 µg/L Arsenic100 700 µg/L Barium 92.7 54 58.2 54.4 53.9 57.7 53.4 57.5 85.2 63.7 53
15 3 µg/L bis(2-Ethylhexyl)phthalate 1
1 2 µg/L Cadmium
100 700 µg/L Carbon disulfideNE 250000 µg/L Chloride 16200 15700 15500 13900 15200 16200 16100 16100 16400
1 3 µg/L Chloromethane
10 10 µg/L Chromium 4.8 4.8 5.6 5.2 14.7 7.6 5.8
10 1000 µg/L Cobalt 2.510 70 µg/L Cyanide 5.1
300 300 µg/L Iron 32600 113 221 123 126 102 209 3540
10 15 µg/L Lead
50 50 µg/L Manganese 1890 2.6 6.1 43.50.2 1 µg/L Mercury
1 5 µg/L Methylene chloride
10 20 µg/L Silver 0.57 0.16
NE NE µg/L Sodium 11300 13100 13700 13600 13800 13000 14500 14200 13300250000 250000 µg/L Sulfate 7430 8000 8180 8060 8310 11200 8400 7910 7020
NE 500000 µg/L Total Dissolved Solids 104000 166000 163000 167000 154000 131000 157000 149000 139000
25 300 µg/L Vanadium 3.7 4.3 5.6 13
10 1000 µg/L Zinc 11.4 15.3MW-6R
10 10 µg/L Arsenic
100 700 µg/L Barium
10 10 µg/L Chromium
10 15 µg/L Lead0.2 1 µg/L Mercury
MW-7
1 200 µg/L 1,1,1-Trichloroethane 0.82
5 6 µg/L 1,1-Dichloroethane 0.91 1.1 1.3 0.81 0.9 0.84 1.2 1.2 1.9 3.80.1 0.1 µg/L 4,4'-DDD 0.13
NE NE µg/L Alkalinity, Total as CaCO3 67300 64100 62400 51900 51600 63500 51900 50200 47700
10 10 µg/L Arsenic
100 700 µg/L Barium 140 122 111 90.8 98.8 115 95.1 100 97.1 104 1001 1 µg/L Benzene 0.29
0.05 0.019 µg/L beta-BHC 0.1
100 700 µg/L Carbon disulfide
NE 250000 µg/L Chloride 6050 4340 4300 3600 5160 5340 381010 3000 µg/L Chloroethane 1.3
1 3 µg/L Chloromethane 0.13
10 10 µg/L Chromium 0.55
5 70 µg/L cis-1,2-Dichloroethene 0.8 0.73 0.73 0.37 0.54 0.72 0.62 0.5 0.67 0.7110 70 µg/L Cyanide 5
5 1000 µg/L Dichlorodifluoromethane 1
0.002 0.002 µg/L Dieldrin 0.11 0.081
0.075 0.004 µg/L Heptachlor epoxide 0.12 0.066300 300 µg/L Iron 76.5
10 15 µg/L Lead
5 500 µg/L m&p-Xylene 0.84 1.5 1.1 0.96 1.4
50 50 µg/L Manganese 33.6 27.1 22.9 15.5 19.4 24.9 17.4 10.2 12.7
0.2 1 µg/L Mercury1 5 µg/L Methylene chloride 3.9 2.1 2.9
NE NE µg/L o-Xylene 0.27 0.4 0.36 0.27 0.39
10 20 µg/L Silver 0.84 0.23
NE NE µg/L Sodium 15700 16300 16600 14200 13000 14300 13900 13700 12000250000 250000 µg/L Sulfate 10100 1850 1360 2090
NS NS µg/L Tetrahydrofuran 17.7 14.1 8.8 5.2 13.7 24.2 26 18.9
NE 500000 µg/L Total Dissolved Solids 78000 145000 138000 126000 116000 108000 111000 109000 124000
1 2000 µg/L Trichlorofluoromethane 1.4 0.79 1.2 0.62 0.47 0.25 0.29 0.34 0.485 500 µg/L Xylenes (Total) 1.2 0.79
10 1000 µg/L Zinc 6.8
c:\pwworking\tpa\d0269489\W-S GW Revised
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Ma
r
-
1
0
Se
p
-
0
9
Ma
r
-
0
9
De
c
-
0
8
Ma
r
-
0
8
No
v
-
0
7
Ap
r
-
0
7
No
v
-
0
6
Ap
r
-
0
6
No
v
-
0
5
Ju
n
-
0
5
No
v
-
0
4
Au
g
-
0
4
Ma
y
-
0
4
No
v
-
0
3
Ma
y
-
0
3
De
c
-
0
2
Ap
r
-
0
2
No
v
-
0
1
Ju
l
-
0
1
De
c
-
0
0
Ju
n
-
0
0
No
v
-
9
9
Ju
n
-
9
9
No
v
-
9
8
Ma
y
-
9
8
Oc
t
-
9
7
Ma
y
-
9
7
Oc
t
-
9
6
Ja
n
-
9
6
150
4.2 5.1 5 7 5 554.3 66.8 52.6 56.1 57.5 70.6 58 58 57 54 53 80 76 65 72 65 150 610 270 400 200 200 240 480 820 610 330 620 1000
2.7
25
5.4
5 8.6 5.2 5.3 5.6 8.4 6.4 6.2 6.2 3.5 5.6 14 7.3 8.7 9.5 7.4 23 140 49 82 8.1 29 38 96 170 16 70 43 96
5.1 13 7.6 7.6 8.2 16 29 69 31 14 20 19
0.4 0.8
10
0.46 0.6 0.28 0.78 0.56
16
28 25 24 41 180 530 62 41 82 59 160 360 260 300 590 1400
2.2 2.4 3.2 26 95 4.1 2.6 2.8 12 33 14 21 10 12
7.6 38 5.8 20 14 14 11 181.4
3.4 8.6 17 16 45 9.8
99.3 104 86.9 99 95.7 101 89 76 74 60 53 63 180 820 130 210 84 1300 1300 2600 360 390 960 1300 1200 1800 750 970 1930
12.5 9
0.65 0.91 7.3 4.4 26 150 17 32 6.8 270 210 580 2.5 62 190 350 430 410 180 21 28
24 5.3 6 36 26 65 8.7 12 30 36 38 53 23 6 17
0.24 0.2 0.4 1.410
0.56 0.88 0.42 0.96 0.66 2.6
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels No
v
-
1
5
Ma
y
-
1
5
No
v
-
1
4
Ma
y
-
1
4
No
v
-
1
3
Ma
y
-
1
3
No
v
-
1
2
Ap
r
-
1
2
De
c
-
1
1
No
v
-
1
1
Ju
n
-
1
1
Ma
y
-
1
1
No
v
-
1
0
Ap
r
-
1
0
MCL
MW-8
100 6000 µg/L Acetone 3.8
NE NE µg/L Alkalinity, Total as CaCO3 23200 20000 22800 21300 19700 22800 19500 20100 19600
10 10 µg/L Arsenic 2.6100 700 µg/L Barium 34.4 30 38 30.7 25.4 28.5 26.9 27.5 24.4 27.3 26.8
NE 250000 µg/L Chloride 2040 1960 1350 1800 1510 2070 1860
10 10 µg/L Chromium 0.96 0.62
10 70 µg/L Cyanide 5.110 100 µg/L Di-n-octylphthalate 5.6
300 300 µg/L Iron 48.6 54 529 136 61.5 60.8 57.8 151
10 15 µg/L Lead
50 50 µg/L Manganese 3.3 3.4 19.9 6.8 70.2 1 µg/L Mercury
10 20 µg/L Silver 0.1
NE NE µg/L Sodium 7940 6940 7810 6160 5580 6120 6980 6250 5410
250000 250000 µg/L Sulfate 1350 1860 2100NE 500000 µg/L Total Dissolved Solids 79000 61000 64000 50000 61000 51000 58000 52000 81000
10 1000 µg/L Zinc 7.1 15.2 45.4
MW-9
NE NE µg/L Alkalinity, Total as CaCO3 23400 18900 18300 18300 18400 21700 17200 20100 1740010 10 µg/L Arsenic 3.5
100 700 µg/L Barium 186 182 193 168 170 174 142 142 141 153 157
15 3 µg/L bis(2-Ethylhexyl)phthalate 13
NE 250000 µg/L Chloride 4710 4290 3610 3610 3950 4300 356010 10 µg/L Chromium
10 70 µg/L Cyanide 4.7
5 1000 µg/L Dichlorodifluoromethane 0.76 0.28 0.28
300 300 µg/L Iron 55.9 136 867
10 15 µg/L Lead50 50 µg/L Manganese 4 3.5 7.6 6.9 16.6
10 20 µg/L Silver 0.43
NE NE µg/L Sodium 14500 14500 14600 12400 13500 12900 13100 12600 11900
250000 250000 µg/L Sulfate 1110 2030 2100 3200NE 500000 µg/L Total Dissolved Solids 142000 134000 141000 107000 124000 100000 118000 123000 128000
1 2000 µg/L Trichlorofluoromethane 1.1 0.98 0.96 0.47 0.69 0.36 0.49 0.42 0.26
10 1000 µg/L Zinc 5.3
MW-1050 NE µg/L 2-Hexanone 0.69 0.96
100 NE µg/L 4-Methyl-2-pentanone (MIBK) 2.6 5.6 2.2
100 6000 µg/L Acetone 11.8
NE NE µg/L Alkalinity, Total as CaCO3 48200 47300 42200 31400 26700 32100 25500 413000 21700100 700 µg/L Barium 241 660 262 132 112 115 101 96.5 91.3 80.7 38.9
1 1 µg/L Benzene 0.46 0.44
1 4000 µg/L Beryllium 1.9 2.8 1.4
100 700 µg/L Carbon disulfideNE 250000 µg/L Chloride 47400 51800 2220 1820 1790 2040 1800
10 10 µg/L Chromium 3.5 6.7 0.63
5 70 µg/L cis-1,2-Dichloroethene 0.35
10 1000 µg/L Cobalt 3.1 4.810 1000 µg/L Copper 6.3 3.8
10 70 µg/L Cyanide 9.8
0.1 40 µg/L Endosulfan I 0.17
1 600 µg/L Ethylbenzene 0.4 1 0.73
0.05 0.008 µg/L Heptachlor 0.120.075 0.004 µg/L Heptachlor epoxide 0.093
300 300 µg/L Iron 3690 3650 1160 84.3 92.8 218 55.1 424
10 15 µg/L Lead 8.5 11.6 4.1
5 500 µg/L m&p-Xylene 0.68 1.2 1.150 50 µg/L Manganese 587 736 130 10.9 7.9 5.1 6.8
0.2 1 µg/L Mercury 0.12 0.29 0.33 0.51
1 5 µg/L Methylene chloride 1.2
50 100 µg/L Nickel 3.9 5.9NE NE µg/L o-Xylene 0.43 0.85 0.65
10 20 µg/L Selenium
10 20 µg/L Silver 0.12
NE NE µg/L Sodium 19800 14100 6860 5280250000 250000 µg/L Sulfate 63600 8770
1000 NE µg/L Sulfide 260
NS NS µg/L Tetrahydrofuran 120 145 106 18.6 5
100 2E+06 µg/L Tin 8.51 600 µg/L Toluene 0.63
NE 500000 µg/L Total Dissolved Solids 403000 279000 86000 63000 66000 46000 63000 49000 89000
1 2000 µg/L Trichlorofluoromethane 0.2 0.33 0.38 0.49 0.68 0.52
25 300 µg/L Vanadium 5.6 4.910 1000 µg/L Zinc 27.2 21.2 6.2
c:\pwworking\tpa\d0269489\W-S GW Revised
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Ma
r
-
1
0
Se
p
-
0
9
Ma
r
-
0
9
De
c
-
0
8
Ma
r
-
0
8
No
v
-
0
7
Ap
r
-
0
7
No
v
-
0
6
Ap
r
-
0
6
No
v
-
0
5
Ju
n
-
0
5
No
v
-
0
4
Au
g
-
0
4
Ma
y
-
0
4
No
v
-
0
3
Ma
y
-
0
3
De
c
-
0
2
Ap
r
-
0
2
No
v
-
0
1
Ju
l
-
0
1
De
c
-
0
0
Ju
n
-
0
0
No
v
-
9
9
Ju
n
-
9
9
No
v
-
9
8
Ma
y
-
9
8
Oc
t
-
9
7
Ma
y
-
9
7
Oc
t
-
9
6
Ja
n
-
9
6
6 36 46 8928.8 27.2 25 32.8 24 26.6 30 29 29 26 25 30 480 52 77 48 150 2700 2600 4200
1.4 0.78 0.97 0.42 2.4 28 3.2 3.8 2 23 94 92 240
41 6.7 150 210 400
0.1 0.26
0.16 0.15 0.13 0.16
134 128 173 124 124 117 140 140 100 100 85 95 240
7.6 0.47 14
14
0.27 0.32 0.18 0.36 0.22 0.32
46.6 39.1 38.9 41.9 42 40.8 52 71 48 46 82 55 98
13
0.65 13
6.8
0.2
6.2
0.19
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels No
v
-
1
5
Ma
y
-
1
5
No
v
-
1
4
Ma
y
-
1
4
No
v
-
1
3
Ma
y
-
1
3
No
v
-
1
2
Ap
r
-
1
2
De
c
-
1
1
No
v
-
1
1
Ju
n
-
1
1
Ma
y
-
1
1
No
v
-
1
0
Ap
r
-
1
0
MCL
MW-11
0.1 0.1 µg/L 4,4'-DDT 0.05
NE NE µg/L Alkalinity, Total as CaCO3 127000 132000 143000 175000 161000 189000 153000 120000 122000
100 700 µg/L Barium 97.2 93.7 96.8 94.3 87.8 87 76.8 70.3 57.5 56.2 48.110 200 µg/L Benzo(g,h,i)perylene 1.3
NE 250000 µg/L Chloride 14900 14400 15000 12400 14000 14200 12900 10800 8480
10 10 µg/L Chromium
10 1000 µg/L Cobalt 2.9 2.5 2.6 47.5 65.110 1000 µg/L Copper 2.8
10 70 µg/L Cyanide 4.2
300 300 µg/L Iron 34600 31400 35700 33400 32100 30700 29000 26300 23000
10 15 µg/L Lead 2.9 3.650 50 µg/L Manganese 2020 1990 2030 1960 1920 1890 1740 1580 1250
10 20 µg/L Selenium 5.6
10 20 µg/L Silver 1.2
NE NE µg/L Sodium 12000 9460 10000 8490 9070 8290 8770 7460 6480250000 250000 µg/L Sulfate 19100 15300 12800 10700 10400 11000 10400 9700 7590
1000 NE µg/L Sulfide 130
NS NS µg/L Tetrahydrofuran 4.4 12.1
5.5 200 µg/L Thallium 8.8NE 500000 µg/L Total Dissolved Solids 281000 239000 228000 207000 236000 228000 220000 161000 165000
25 300 µg/L Vanadium 3.5 3.2 3.6
10 1000 µg/L Zinc 92
MW-12NE NE µg/L Alkalinity, Total as CaCO3 41000 19200 40500 45500 39300 29600 40200 37200 40200
10 10 µg/L Arsenic
100 700 µg/L Barium 95.7 60.9 59.2 61.1 47.6 50.1 50.5 46.9 60.1 39.1 44.9
10 200 µg/L Benzo(g,h,i)perylene 1.2
NE 250000 µg/L Chloride 9000 8070 8240 6180 6230 5820 4900 8200 80301 3 µg/L Chloromethane 0.21
10 10 µg/L Chromium 2.6 1.1
10 70 µg/L Cyanide 5.3
5 1000 µg/L Dichlorodifluoromethane 0.2310 100 µg/L Di-n-octylphthalate 5.6
10 0.05 µg/L Indeno(1,2,3-cd)pyrene 1.2
300 300 µg/L Iron 523 524 758 348 253 324 1430 539 3030
50 50 µg/L Manganese 49.6 9.7 199 14.6 86.1 13.2 33.6 15.7 58.31 5 µg/L Methylene chloride 2
50 100 µg/L Nickel 3.2 4.1
10 20 µg/L Silver 0.7
NE NE µg/L Sodium 13700 11200 12800 11000 10500 11100 11000 11600 9980250000 250000 µg/L Sulfate 70800 73600 32800 48000 27400 51800 24200 20500 15300
NE 500000 µg/L Total Dissolved Solids 234000 163000 135000 149000 126000 138000 127000 130000 124000
1 2000 µg/L Trichlorofluoromethane 0.82 0.22 0.32
10 1000 µg/L Zinc 30.8MW-13
5 350 µg/L 1,1-Dichloroethene
NE NE µg/L Alkalinity, Total as CaCO3 37100 36900 36200 46400 43200 58700 43900 52200 44500
10 10 µg/L Arsenic 2.6100 700 µg/L Barium 71.5 89.3 130 77.1 106 176 279 144 139 164 176
10 0.005 µg/L Benzo(a)pyrene 1.1
10 0.05 µg/L Benzo(b)fluoranthene 1
10 200 µg/L Benzo(g,h,i)perylene 1.5
1 4000 µg/L Beryllium 0.68 0.66 1.2 2.4 3.5 1.4 2.3NE 250000 µg/L Chloride 3270 3760 5870 3880 5700 3820 6150 5380
10 10 µg/L Chromium 2.9 3 7.1 11.8 5.5 3.9 4
10 1000 µg/L Cobalt 6.6
10 1000 µg/L Copper 3.8 7.6 6.9 6.110 70 µg/L Cyanide 5
10 0.005 µg/L Dibenz(a,h)anthracene 1.2
10 0.05 µg/L Indeno(1,2,3-cd)pyrene 1.5
300 300 µg/L Iron 790 1400 2720 232 1330 8610 11300 3760 614010 15 µg/L Lead 2.9 5.4 6.5 7.5 6.4 4.3
50 50 µg/L Manganese 62.1 41.2 55.6 34.1 48.8 158 301 91.5 140
10 20 µg/L Silver 0.72
NE NE µg/L Sodium 12200 10700 10700 11200 11700 19100 14600 16700 20200250000 250000 µg/L Sulfate 10100 9330 8660 8680 9360 7820 9770 9420 9460
1000 NE µg/L Sulfide 151 106 178
NS NS µg/L Tetrahydrofuran 18.6
NE 500000 µg/L Total Dissolved Solids 110000 107000 119000 113000 114000 87000 144000 110000 1590001 2000 µg/L Trichlorofluoromethane
25 300 µg/L Vanadium 2.6 3.4 7.1 14.6 18.7 7.2 10.8
10 1000 µg/L Zinc 8.6 7.9 13.7 17.2 37.3 51 20 31.6
c:\pwworking\tpa\d0269489\W-S GW Revised
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Ma
r
-
1
0
Se
p
-
0
9
Ma
r
-
0
9
De
c
-
0
8
Ma
r
-
0
8
No
v
-
0
7
Ap
r
-
0
7
No
v
-
0
6
Ap
r
-
0
6
No
v
-
0
5
Ju
n
-
0
5
No
v
-
0
4
Au
g
-
0
4
Ma
y
-
0
4
No
v
-
0
3
Ma
y
-
0
3
De
c
-
0
2
Ap
r
-
0
2
No
v
-
0
1
Ju
l
-
0
1
De
c
-
0
0
Ju
n
-
0
0
No
v
-
9
9
Ju
n
-
9
9
No
v
-
9
8
Ma
y
-
9
8
Oc
t
-
9
7
Ma
y
-
9
7
Oc
t
-
9
6
Ja
n
-
9
6
37.6 31.8 28.4 28.6 29.2 23.1 25 24 26 27 24 28 47
3.9 3.3
8.7
0.48 0.5 0.79 0.41 0.39
2.7
40.6 38 34.5 57.9 60.5 47.3 31 66 55 77 50 77 74
2.4 2 1.8 4 2.1
0.2 0.39 0.37 0.15 0.26
19.8
126 117 79.2 88.7 64.6 85.6 79 62 65 59 46 57 160
1.7 0.8 1.6 2.2 1.1 2 4.8 9.2
11
0.4 0.41 0.44 0.21
18.6
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels No
v
-
1
5
Ma
y
-
1
5
No
v
-
1
4
Ma
y
-
1
4
No
v
-
1
3
Ma
y
-
1
3
No
v
-
1
2
Ap
r
-
1
2
De
c
-
1
1
No
v
-
1
1
Ju
n
-
1
1
Ma
y
-
1
1
No
v
-
1
0
Ap
r
-
1
0
MCL
MW-14
NE NE µg/L Alkalinity, Total as CaCO3 51500 45200 42300 37400 32800 35600 28900 30100 30400
10 10 µg/L Arsenic
100 700 µg/L Barium 183 179 193 163 140 254 160 122 143 125 1291 4000 µg/L Beryllium 0.63 0.54 0.6
15 3 µg/L bis(2-Ethylhexyl)phthalate 9.8
NE 250000 µg/L Chloride 3930 3510 3720 3630 4100 4290 4790
1 3 µg/L Chloromethane 0.2410 10 µg/L Chromium 4.5 6.6 6 1.8 2.3
10 1000 µg/L Copper 4.8 9.5 5.8
10 70 µg/L Cyanide 5.3 6
5 1000 µg/L Dichlorodifluoromethane 2.1300 300 µg/L Iron 466 695 2620 142 915 5820 4520 1140 2050
10 15 µg/L Lead
50 50 µg/L Manganese 69.3 25.7 120 40.2 110 240 251 170 71
0.2 1 µg/L Mercury50 100 µg/L Nickel 2.8 2.8 5.3 8.6 13.7 12.5
10 20 µg/L Silver 0.74
NE NE µg/L Sodium 15800 14500 14400 12800 12300 13500 15000 14300 12700
250000 250000 µg/L Sulfate 1080 1790NE 500000 µg/L Total Dissolved Solids 135000 131000 119000 124000 123000 102000 127000 145000 138000
1 2000 µg/L Trichlorofluoromethane 0.54 0.59 0.57 0.34
25 300 µg/L Vanadium 5.5 9.9 8
10 1000 µg/L Zinc 6.3 13.3 11.7 27.4 23 12MW-15
5 350 µg/L 1,1-Dichloroethene 3.1
0.1 0.1 µg/L 4,4'-DDD 0.062
NE NE µg/L Alkalinity, Total as CaCO3 103000 91500 54700 96600 64300 78900 77600 75300
10 10 µg/L Arsenic 4.5 7.1 5.7100 700 µg/L Barium 74 105 41.5 8.6 23.8 59.6 143 115
NE 250000 µg/L Chloride 113000 98200 146000 83400 124000 124000 143000 60600
5 70 µg/L Chloroform 0.44 0.26 0.49 0.77 0.63 0.49 1.4
10 10 µg/L Chromium 5.4 7.6 6.7 7.210 1000 µg/L Copper 7.1 8.8 10.5
10 70 µg/L Cyanide 5.2
300 300 µg/L Iron 8180 10600 233 292 239 4140 12300 10000
10 15 µg/L Lead 6 6.8 9.5 7.650 50 µg/L Manganese 297 271 33 34.7 14 160 317 327
50 100 µg/L Nickel 3.9 4.3
NE NE µg/L Sodium 21800 20300 24000 24200 25300 26700 21200 16300
250000 250000 µg/L Sulfate 70000 65400 43800 59500 53200 41200 35600 258001000 NE µg/L Sulfide 100
NS NS µg/L Tetrahydrofuran 19.8 16.9 15.5 21.4 14.7 7.4 6.3
NE 500000 µg/L Total Dissolved Solids 362000 360000 464000 373000 410000 442000 298000 260000
1 2000 µg/L Trichlorofluoromethane 4.8 4.4 3.9 5.3 7.6 4.3 8.1 7.325 300 µg/L Vanadium 18.9 24.7 8.6 28.6 23.4
10 1000 µg/L Zinc 35.4 49 5.3 17.1 22.7 45.6 51.1
SW-1
100 6000 µg/L Acetone 2.2NE NE µg/L Alkalinity, Total as CaCO3 35100 44500 63700 45200 72700 58000 79700 47200 19600
10 10 µg/L Arsenic 5.9
100 700 µg/L Barium 65 72.2 276 65.8 71.1 58.9 63.3 70.4 42.5 69.9 61.9
1 4000 µg/L Beryllium 1.1
1 2 µg/L Cadmium 0.7NE 250000 µg/L Chloride 21600 31500 19500 23700 18100 20600 19700 25300 19100
10 10 µg/L Chromium 13
10 1000 µg/L Cobalt 9 14.6
10 1000 µg/L Copper 3.9 16.40.1 2 µg/L Endrin 0.08
300 300 µg/L Iron 9830 8870 155000 8210 22800 6900 25500 11400 2290
10 15 µg/L Lead 18.3
50 50 µg/L Manganese 688 1160 1760 749 1530 855 1720 1040 1300.2 1 µg/L Mercury
50 100 µg/L Nickel 8.7
10 20 µg/L Selenium 7
10 20 µg/L Silver 0.4NE NE µg/L Sodium 12800 16000 12500 14500 13000 12400 15500 14300 9390
250000 250000 µg/L Sulfate 4460 3690 3130 2820 2190 2700 2090
NE 500000 µg/L Total Dissolved Solids 113000 140000 122000 126000 125000 104000 131000 98000 140000
25 300 µg/L Vanadium 4.3 3710 1000 µg/L Zinc 7.5 69.8
c:\pwworking\tpa\d0269489\W-S GW Revised
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Ma
r
-
1
0
Se
p
-
0
9
Ma
r
-
0
9
De
c
-
0
8
Ma
r
-
0
8
No
v
-
0
7
Ap
r
-
0
7
No
v
-
0
6
Ap
r
-
0
6
No
v
-
0
5
Ju
n
-
0
5
No
v
-
0
4
Au
g
-
0
4
Ma
y
-
0
4
No
v
-
0
3
Ma
y
-
0
3
De
c
-
0
2
Ap
r
-
0
2
No
v
-
0
1
Ju
l
-
0
1
De
c
-
0
0
Ju
n
-
0
0
No
v
-
9
9
Ju
n
-
9
9
No
v
-
9
8
Ma
y
-
9
8
Oc
t
-
9
7
Ma
y
-
9
7
Oc
t
-
9
6
Ja
n
-
9
6
7.3 8.3
130 242 97.9 583 186 130 210 460 250 120 69 66 170
3 10.7 0.4 40.2 4.1 1.7 6.6 35 15 3.9 3.2
7.2 26.2 5.2 23 13 5.9 8
0.098 0.44
0.39 0.54 0.46 0.56 0.48
22.7
3.7 23 20
92.5 77.7 45.6 78.2 79.7 70.3 88 54 120 73 750 53 500
0.61 0.67 1.2 0.61 4.2 52 3.2 36
17.5 57 38
1.1
0.28 0.62 0.39 0.37 0.51
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels No
v
-
1
5
Ma
y
-
1
5
No
v
-
1
4
Ma
y
-
1
4
No
v
-
1
3
Ma
y
-
1
3
No
v
-
1
2
Ap
r
-
1
2
De
c
-
1
1
No
v
-
1
1
Ju
n
-
1
1
Ma
y
-
1
1
No
v
-
1
0
Ap
r
-
1
0
MCL
SW-2
50 NE µg/L 2-Hexanone 1.8
20 NE µg/L 3,3'-Dichlorobenzidine 3.6
10 NE µg/L 3-Methylcholanthrene 2.9100 6000 µg/L Acetone 4
NE NE µg/L Alkalinity, Total as CaCO3 43200 33200 2390 41300 48900 48600 44700 44200 26100
10 10 µg/L Arsenic 17 6.2
100 700 µg/L Barium 70 700 171 59.7 50.1 51.7 46.5 53.4 81 49.2 57.610 0.05 µg/L Benzo(a)anthracene 1.1
10 0.005 µg/L Benzo(a)pyrene 2.5
10 0.05 µg/L Benzo(b)fluoranthene 2.8
10 200 µg/L Benzo(g,h,i)perylene 1.810 0.5 µg/L Benzo(k)fluoranthene 2.5
1 4000 µg/L Beryllium 3.7 0.64
15 3 µg/L bis(2-Ethylhexyl)phthalate 1.1
NE 250000 µg/L Chloride 12500 4050 28200 10700 11600 10800 10300 11300 1090010 10 µg/L Chromium 40.3 3.2
10 5 µg/L Chrysene 1.1
10 1000 µg/L Cobalt 5.9 4.4
10 1000 µg/L Copper 81.6 3.210 0.005 µg/L Dibenz(a,h)anthracene 2.1
10 0.05 µg/L Indeno(1,2,3-cd)pyrene 2.2
300 300 µg/L Iron 2070 226000 75000 2130 3360 1400 1280 1720 4170
10 15 µg/L Lead 75 7.450 50 µg/L Manganese 291 1020 1010 219 152 153 106 157 280
0.2 1 µg/L Mercury 0.2
50 100 µg/L Nickel 16.4 3.1
10 20 µg/L Selenium
10 20 µg/L Silver 0.2NE NE µg/L Sodium 11300 8390 17600 9840 10300 9160 9990 9890 8650
250000 250000 µg/L Sulfate 11600 7280 5620 12700 5490 5090 4240 6180 38300
1000 NE µg/L Sulfide 142
NS NS µg/L Tetrahydrofuran 18.4NE 500000 µg/L Total Dissolved Solids 105000 125000 117000 120000 114000 91000 101000 101000 189000
25 300 µg/L Vanadium 127 11.6 7.5
10 1000 µg/L Zinc 249 28 13.5
SW-310 40 µg/L 3&4-Methylphenol(m&p Cresol) 3.6
0.1 0.1 µg/L 4,4'-DDD 0.079
0.1 0.1 µg/L 4,4'-DDT 0.09
NE NE µg/L Alkalinity, Total as CaCO3 210000 118000 389000 259000 516000 293000 317000 221000 160000100 700 µg/L Barium 152 105 206 181 348 185 315 179 123
1 1 µg/L Benzene 0.54 0.32 0.88 0.34 0.25
NE 250000 µg/L Chloride 16300 27000 27000 16900 34800 20000 24300 22800 20900
10 10 µg/L Chromium 3.410 1000 µg/L Cobalt 3.4 14.8 14.4 25.3 13 5.5
10 1000 µg/L Copper 4.4
0.1 42 µg/L Endosulfan II 0.071 0.085
300 300 µg/L Iron 4160 4940 5270 8890 11700 9560 16500 9370 323010 15 µg/L Lead 2.7
50 50 µg/L Manganese 3860 1420 5080 4320 8930 3990 5200 3760 1890
50 100 µg/L Nickel 2.8 2.8 4.8 12
NE NE µg/L Sodium 20900 18200 29900 29900 41100 25000 33800 21300 18500
250000 250000 µg/L Sulfate 27000 17000 16800 26300 62500 20100 36400 26400 19800NS NS µg/L Tetrahydrofuran 3.3 10.2 9.7 18.9 5.1 4.8 4.5
NE 500000 µg/L Total Dissolved Solids 300000 233000 473000 319000 705000 327000 432000 329000 237000
25 300 µg/L Vanadium 5.6 9.7 9.8
10 1000 µg/L Zinc 13.6 10.8SW-4
5 350 µg/L 1,1-Dichloroethene 0.58
50 NE µg/L 2-Hexanone 3.1
0.1 0.1 µg/L 4,4'-DDD 0.11 0.0620.1 0.1 µg/L 4,4'-DDT 0.054
NE NE µg/L Alkalinity, Total as CaCO3 187000 242000 140000 158000 152000 147000 220000 158000 131000
100 700 µg/L Barium 115 187 82.8 126 101 106 151 136 105
NE 250000 µg/L Chloride 19800 19000 24300 30800 31000 26900 28800 30900 236005 70 µg/L Chloroform 0.97
10 1000 µg/L Cobalt 5.9 10.4
0.1 42 µg/L Endosulfan II 0.066
0.1 2 µg/L Endrin aldehyde 0.061300 300 µg/L Iron 2240 9220 638 2520 1790 4180 1640 2140 1060
50 50 µg/L Manganese 2550 5050 739 2250 1080 1650 2430 2420 1290
50 100 µg/L Nickel 3.6
NE NE µg/L Sodium 20200 23800 17800 24400 20100 18200 29000 20000 17900250000 250000 µg/L Sulfate 24900 23500 17600 23500 23000 13200 32300 23600 19500
NS NS µg/L Tetrahydrofuran 4.1 4.4
NE 500000 µg/L Total Dissolved Solids 267000 371000 222000 257000 270000 255000 349000 272000 234000
1 2000 µg/L Trichlorofluoromethane 0.27 0.25 1.4
c:\pwworking\tpa\d0269489\W-S GW Revised
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Ma
r
-
1
0
Se
p
-
0
9
Ma
r
-
0
9
De
c
-
0
8
Ma
r
-
0
8
No
v
-
0
7
Ap
r
-
0
7
No
v
-
0
6
Ap
r
-
0
6
No
v
-
0
5
Ju
n
-
0
5
No
v
-
0
4
Au
g
-
0
4
Ma
y
-
0
4
No
v
-
0
3
Ma
y
-
0
3
De
c
-
0
2
Ap
r
-
0
2
No
v
-
0
1
Ju
l
-
0
1
De
c
-
0
0
Ju
n
-
0
0
No
v
-
9
9
Ju
n
-
9
9
No
v
-
9
8
Ma
y
-
9
8
Oc
t
-
9
7
Ma
y
-
9
7
Oc
t
-
9
6
Ja
n
-
9
6
5.5
59.4 52.1 46.3 50.6 50.6 49.4 300 44 150 51 47 65 63
0.42 17 4.7
11 7.6
0.081
21
0.2 0.36 0.5 0.26 0.26
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels No
v
-
1
5
Ma
y
-
1
5
No
v
-
1
4
Ma
y
-
1
4
No
v
-
1
3
Ma
y
-
1
3
No
v
-
1
2
Ap
r
-
1
2
De
c
-
1
1
No
v
-
1
1
Ju
n
-
1
1
Ma
y
-
1
1
No
v
-
1
0
Ap
r
-
1
0
MCL
25 300 µg/L Vanadium 3.5 5.9
c:\pwworking\tpa\d0269489\W-S GW Revised
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Ma
r
-
1
0
Se
p
-
0
9
Ma
r
-
0
9
De
c
-
0
8
Ma
r
-
0
8
No
v
-
0
7
Ap
r
-
0
7
No
v
-
0
6
Ap
r
-
0
6
No
v
-
0
5
Ju
n
-
0
5
No
v
-
0
4
Au
g
-
0
4
Ma
y
-
0
4
No
v
-
0
3
Ma
y
-
0
3
De
c
-
0
2
Ap
r
-
0
2
No
v
-
0
1
Ju
l
-
0
1
De
c
-
0
0
Ju
n
-
0
0
No
v
-
9
9
Ju
n
-
9
9
No
v
-
9
8
Ma
y
-
9
8
Oc
t
-
9
7
Ma
y
-
9
7
Oc
t
-
9
6
Ja
n
-
9
6
c:\pwworking\tpa\d0269489\W-S GW Revised
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
December-15Field
feet
Static Water Level 20.86
Total Well Depth 27
mg/L
Oxygen, Dissolved 1NTU
Turbidity 7.8
Std. Units
Field pH 6
mV
REDOX -71.6
µmhos/cm
Field Specific Conductance 365.6
°C
Field Temperature 13.6
November-15
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 1070 115000 2200 70300 7430 10100 1350
EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 207 279 271 184 92.7 140 34.4
1 4000 µg/L Beryllium
10 10 µg/L Chromium
10 1000 µg/L Cobalt 17.4 9.1 28.3 2.5
10 1000 µg/L Copper 6.2
300 300 µg/L Iron 82.8 3080 68200 312 32600 48.6
10 15 µg/L Lead 3.8
50 50 µg/L Manganese 2.8 9010 7100 407 1890 33.6 3.350 100 µg/L Nickel 18 3.7
10 20 µg/L Selenium
NE NE µg/L Sodium 13200 61400 2590 23800 11300 15700 7940
5.5 200 µg/L Thallium
100 2000000 µg/L Tin
25 300 µg/L Vanadium 11.9 9.9 3.7
10 1000 µg/L Zinc 5.6 5.8 8.7 5.9 7.1EPA 7470
µg/L
0.2 1 µg/L Mercury
EPA 8081
µg/L
0.1 40 µg/L Endosulfan I
0.05 0.008 µg/L Heptachlor
0.075 0.004 µg/L Heptachlor epoxide
MCL
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
1110 63600 19100 70800 10100 1080 70000 4460 11600 27000 24900
2.6 4.5
186 241 97.2 95.7 71.5 183 74 65 70 152 115
1.9 0.68 0.63
3.5 5.4
3.1 2.9
6.3 2.8 7.1 3.9
3690 34600 523 790 466 8180 9830 2070 4160 2240
8.5 6
4 587 2020 49.6 62.1 69.3 297 688 291 3860 25503.9 3.2 2.8 3.9 2.8
5.6
14500 19800 12000 13700 12200 15800 21800 12800 11300 20900 20200
8.8
8.5
5.6 3.5 2.6 18.9 4.3 5.6 3.5
27.2 8.6 6.3 35.4 7.5
0.12
0.17
0.12
0.093
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 0.91
1 6 µg/L 1,4-Dichlorobenzene 0.38
50 NE µg/L 2-Hexanone
100 NE µg/L 4-Methyl-2-pentanone (MIB
100 6000 µg/L Acetone
1 1 µg/L Benzene 1.5
5 70 µg/L Chloroform
1 3 µg/L Chloromethane 0.25
5 70 µg/L cis-1,2-Dichloroethene 0.26 0.8
5 1000 µg/L Dichlorodifluoromethane 0.26 1
1 600 µg/L Ethylbenzene
5 500 µg/L m&p-Xylene 0.84
1 5 µg/L Methylene chloride 1.3 2.3 3.9
NE NE µg/L o-Xylene 0.27
1 0.7 µg/L Tetrachloroethene 0.95
NS NS µg/L Tetrahydrofuran 35.8 7 17.7
1 600 µg/L Toluene 0.27
1 3 µg/L Trichloroethene 0.66
1 2000 µg/L Trichlorofluoromethane 1 1.4
1 0.03 µg/L Vinyl chloride 0.75
EPA 8270
µg/L
10 NE µg/L 2,4-Dinitrotoluene 5.9
10 NE µg/L 2,6-Dinitrotoluene 8.1
10 200 µg/L Benzo(g,h,i)perylene 1
10 0.005 µg/L Dibenz(a,h)anthracene 1
10 100 µg/L Di-n-octylphthalate 5.6
10 0.05 µg/L Indeno(1,2,3-cd)pyrene 1.1
SM 2320B
µg/LNE NE µg/L Alkalinity, Total as CaCO3 48100 440000 102000 144000 32300 67300 23200
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 78000 806000 137000 161000 104000 78000 79000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 8510 48700 2990 16900 16200 6050 2040
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 7.5 5.1
Field
feet
Static Water Level 72.25 16.3 43.76 20.31 23.2 76.9 36.73
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 2.2 2 0.2 3.3 5.9 0.7 4.4
NTU
Turbidity 1 5.6 3 9.6 1 1 1.6
Std. Units
Field pH 5.4 6.1 6.3 5.8 5.8 5.5 5.4
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
0.69
2.6
11.8
0.44
0.76 0.23 2.1
0.4
0.68
1.2 2 1.1
0.43
120 19.8 3.3
1.1 0.82 0.54 4.8
5.6
23400 48200 127000 41000 37100 51500 103000 35100 43200 210000 187000
142000 403000 281000 234000 110000 135000 362000 113000 105000 300000 267000
4710 47400 14900 9000 3270 3930 113000 21600 12500 16300 19800
4.7 9.8 4.2 5.3 5 5.3
107.71 24.15 7.17 9.51 17.47 104.89 78.88
60 21 20 15.58 20 60 50.85
6.3 0.2 0.1 3.4 1.2 4.8 2.8 5.5 3.5 3.2 7.6
2.6 295 9.3 8.9 51.6 5.9 154.9 48.7 20.5 9.1 3.2
5.3 5.4 5.9 5.8 5.5 5.4 6.2 6.7 6.6 6.4 7
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
mV
REDOX 34.8 -35.2 -91.6 48.8 52.6 30.9 4
µmhos/cm
Field Specific Conductance 163.2 1044 211.4 395.9 164.5 196.6 58.4
°C
Field Temperature 16 15.9 15.2 15.5 15.9 15.3 15.6
May-15EPA 300.0
µg/L
250000 250000 µg/L Sulfate 1700 98400 3000 72700 8000 1850 1860
EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 164 287 214 306 54 122 30
1 4000 µg/L Beryllium
10 10 µg/L Chromium 4.8
10 1000 µg/L Cobalt 20.3 10.1 15.2
10 1000 µg/L Copper 6.3
300 300 µg/L Iron 9560 56000 292 113 54
10 15 µg/L Lead 3.3 2.7
50 50 µg/L Manganese 11900 7980 315 27.1 3.4
50 100 µg/L Nickel 17 2.8
NE NE µg/L Sodium 11600 51400 23000 13100 16300 6940
5.5 200 µg/L Thallium 5.1
25 300 µg/L Vanadium 11.4 8.8 4.3
10 1000 µg/L Zinc 8.7 7.5 6.8EPA 7470
µg/L
0.2 1 µg/L Mercury
EPA 8151
µg/L
2 50 µg/L 2,4,5-TP (Silvex) 0.142 70 µg/L 2,4-D 0.43
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 0.49 1.1
50 NE µg/L 2-Hexanone
100 NE µg/L 4-Methyl-2-pentanone (MIB
1 1 µg/L Benzene 1.7 0.29
5 70 µg/L Chloroform
1 3 µg/L Chloromethane 0.13
5 70 µg/L cis-1,2-Dichloroethene 0.73
1 600 µg/L Ethylbenzene
5 500 µg/L m&p-Xylene 1.5
1 5 µg/L Methylene chloride 2.3 2.1
NE NE µg/L o-Xylene 0.4
1 0.7 µg/L Tetrachloroethene 1.2
NS NS µg/L Tetrahydrofuran 34.6 5.8 14.1
1 600 µg/L Toluene
1 3 µg/L Trichloroethene 0.79
1 2000 µg/L Trichlorofluoromethane 1.5 0.79
1 0.03 µg/L Vinyl chloride 0.7
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
54.3 -77.7 -38.7 -23.3 5.2 49.6 34.8 -78.3 -84.6 -90 -87.1
151.5 365.1 400.8 281.5 108.9 152.1 596.2 92.6 88.6 274.8 247.9
15.9 16.5 15.8 16.2 16.2 16.3 15.6 9.4 11.9 8.2 9
2030 8770 15300 73600 9330 1790 65400 3690 7280 17000 23500
17
182 660 93.7 60.9 89.3 179 105 72.2 700 105 187
2.8 0.66 0.54 3.7
6.7 2.9 7.6 40.3 3.4
4.8 2.5 5.9 5.9
3.8 8.8 81.6 4.4
3650 31400 524 1400 695 10600 8870 226000 4940 9220
11.6 2.9 2.9 6.8 75 2.7
3.5 736 1990 9.7 41.2 25.7 271 1160 1020 1420 5050
5.9 2.8 4.3 16.4 2.8 3.6
14500 14100 9460 11200 10700 14500 20300 16000 8390 18200 23800
4.9 3.2 3.4 24.7 127 9.7 5.9
21.2 7.9 49 249 13.6
0.29 0.2
0.96 1.8 3.1
5.6
0.46
0.26
1
1.2
1.5 1.8
0.85
145 16.9 4.1
0.63
0.98 0.22 0.59 4.4
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 39600 358000 107000 117000 28600 64100 20000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 133000 632000 182000 304000 166000 145000 61000
SM 4500-Cl-Eµg/L
NE 250000 µg/L Chloride 7640 44200 2990 22200 15700 4340 1960
Field
feet
Static Water Level 71.44 16.32 42.18 18.28 21.85 75.46 16.85
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 4.5 1.6 2 2.5 6.8 0.4 5.7
NTU
Turbidity 1.2 8.8 6.2 12.2 2.2 1.2 2.3
Std. Units
Field pH 5.5 6.1 6.1 5.9 5.9 5.6 5.7
mV
REDOX 265.1 15.4 -1.1 262.8 244.4 228.8 255.2
µmhos/cm
Field Specific Conductance 153.1 985 363.4 422 175.1 194.8 50.9
°C
Field Temperature 18 13.7 15 13.3 14.7 16.7 16.1
November-14EPA 300.0
µg/L
250000 250000 µg/L Sulfate 1720 117000 3740 143000 8180 1360
EPA 6010
µg/L
10 10 µg/L Arsenic 2.6100 700 µg/L Barium 142 339 221 305 58.2 111 38
1 4000 µg/L Beryllium
1 2 µg/L Cadmium
10 10 µg/L Chromium 3.4 4.8
10 1000 µg/L Cobalt 25 13.3 82
10 1000 µg/L Copper 9.6
300 300 µg/L Iron 85.8 2580 49700 126 221 76.5 529
10 15 µg/L Lead 2.7
50 50 µg/L Manganese 2.9 9880 9380 1040 2.6 22.9 19.9
50 100 µg/L Nickel 25.9 7.2
10 20 µg/L Selenium
NE NE µg/L Sodium 10600 58300 2770 55400 13700 16600 7810
25 300 µg/L Vanadium 2.8 2.7 5.6
10 1000 µg/L Zinc 16.8 7.2
EPA 7470
µg/L
0.2 1 µg/L Mercury
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
18900 47300 132000 19200 36900 45200 91500 44500 33200 118000 242000
134000 279000 239000 163000 107000 131000 360000 140000 125000 233000 371000
4290 51800 14400 8070 3760 3510 98200 31500 4050 27000 19000
53.36 23.35 8.07 9.8 8.98 52.23 39.21
60 21 20 15.58 20 60 50.85
6.3 1.5 0.3 5.4 2.7 5.2 2 4.5 0.2 6.9 3.5
1.4 246.4 8 7.7 32.7 26.1 81.7 26.5 385.5 42.7 18.6
5.5 5.2 6 6 5.7 5.6 6.2 6.3 6.5 6.9 6.5
206.8 244.7 -34.3 230.6 218.9 221.2 176 11 -79.4 -15.8 -25.5
148.3 297.2 407.8 234.3 115 150.1 611 228.7 185.9 364.2 603
17.5 17.1 13.4 14.9 18.7 17.1 17.3 20.4 19.7 17.5 18.2
2100 12800 32800 8660 43800 3130 5620 16800 17600
3.5 5.9 6.2193 262 96.8 59.2 130 193 41.5 276 171 206 82.8
1.4 1.2 0.6 1.1 0.64
0.7
3 4.5 13 3.2
2.6 4.4 3.4
3.8 4.8 16.4 3.2
55.9 1160 35700 758 2720 2620 233 155000 75000 5270 638
4.1 3.6 5.4 18.3 7.4
7.6 130 2030 199 55.6 120 33 1760 1010 5080 739
4.1 5.3 8.7 3.1 4.8
7
14600 6860 10000 12800 10700 14400 24000 12500 17600 29900 17800
3.6 7.1 5.5 37 11.6
5.3 6.2 13.7 13.3 5.3 69.8 28
0.33
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.1 1.3
1 6 µg/L 1,4-Dichlorobenzene 0.4
100 NE µg/L 4-Methyl-2-pentanone (MIB
1 1 µg/L Benzene 2.5 0.42
10 3000 µg/L Chloroethane 2.15 70 µg/L cis-1,2-Dichloroethene 0.5 0.73
1 600 µg/L Ethylbenzene
5 500 µg/L m&p-Xylene 1.1
1 5 µg/L Methylene chloride 3.7 2.9
NE NE µg/L o-Xylene 0.33 0.36
1 0.7 µg/L Tetrachloroethene 2
NS NS µg/L Tetrahydrofuran 79.2 15.9 8.8
1 3 µg/L Trichloroethene 0.85
1 2000 µg/L Trichlorofluoromethane 2.4 1.2
1 0.03 µg/L Vinyl chloride 1.2
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 37600 453000 177000 286000 24000 62400 22800SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 120000 769000 191000 692000 163000 138000 64000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 7090 49800 2940 50500 15500 4300 1350SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 4.4 4.2 10.4 4.3 5.1
SM 4500-S2D
µg/L
1000 NE µg/L SulfideField
feet
Static Water Level 69.7 17.18 21.87 18.4 22.36 36.9 37.58
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 1 0.5 6.3 0.5 5 0.5 2.3
NTU
Turbidity 1.7 3.53 5.2 10 3.6 1.2 9.1
Std. Units
Field pH 5.6 6.1 6 5.9 6 5.6 5.7
mV
REDOX 194 38 13 158 198 184 224
µmhos/cm
Field Specific Conductance 138 1150 363 971 184 186 59
°C
Field Temperature 14.8 13.2 13.2 13.7 12.9 13.7 13
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
2.2
0.44 0.54
0.35
0.73
1.1
0.65
106 15.5 18.4 10.2
0.96 0.57 3.9 0.27
18300 42200 143000 40500 36200 42300 54700 63700 2390 389000 140000
141000 86000 228000 135000 119000 119000 464000 122000 117000 473000 222000
3610 2220 15000 8240 5870 3720 146000 19500 28200 27000 24300
260 130 151 142
104.74 24.68 5.4 10.76 18.48 103.8 79
60 21 20 15.58 20 60 50.85
8.3 0.5 0.5 0.5 3.8 1.25 0.5 2.11 4.5 8.18
2 98 9.9 5.2 152 7.8 20.1 363.9 136.9 16.6 28.3
5.5 5.1 5.9 5.9 5.6 5.6 6.2 6.1 6.3 6.6 6.7
252 198 -61 101 232 242 182 7 -36 -45 27
161 106 440 203 120 159 647 247 324 885 344
12.4 15.3 15.4 15.4 13.8 11.9 16.7 10.8 11.2 12.5 10
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
May-14EPA 300.0
µg/L
250000 250000 µg/L Sulfate 136000 4230 85200 8060
EPA 6010
µg/L
6 1000 µg/L Antimony 5.410 10 µg/L Arsenic 8.9
100 700 µg/L Barium 124 324 205 264 54.4 90.8 30.7
10 10 µg/L Chromium 5.6
10 1000 µg/L Cobalt 22.8 46.6
300 300 µg/L Iron 52.9 1650 38200 123
50 50 µg/L Manganese 7950 9260 641 6.1 15.5
50 100 µg/L Nickel 20.6
10 20 µg/L Selenium 16.5 11.5
NE NE µg/L Sodium 10800 59700 39700 13600 14200 6160
10 1000 µg/L Zinc 11.4
EPA 7470
µg/L
0.2 1 µg/L MercuryEPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 0.83 0.81
1 1 µg/L Benzene 1.8 0.28
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.38 0.37
1 5 µg/L Methylene chloride 3.7
NE NE µg/L o-Xylene 0.31
1 0.7 µg/L Tetrachloroethene 1.8
NS NS µg/L Tetrahydrofuran 72.6 11.8 5.2
1 3 µg/L Trichloroethene 0.71
1 2000 µg/L Trichlorofluoromethane 3.7 0.62SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 30000 344000 155000 222000 31900 51900 21300
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 91000 549000 187000 445000 167000 126000 50000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 5600 50500 3260 29700 13900 3600 1800
Field
feet
Static Water Level 70.78 14.24 37.86 14.47 20.22 74.12 26.82
Total Well Depth 60 21 27 20 30 37.05 27
mg/L
Oxygen, Dissolved 5.3 4.8 6.3 6.2 8.6 3.8 8.4
NTU
Turbidity 3 11 6 17 10 6 8
Std. Units
Field pH 5.6 5.8 6 5.7 5.7 5.3 5
mV
REDOX 411 243 146 374 389 363 389
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
10700 48000 8680 59500 2820 12700 26300 23500
168 132 94.3 61.1 77.1 163 8.6 65.8 59.7 181 126
9 14.8
33400 348 232 142 292 8210 2130 8890 2520
10.9 1960 14.6 34.1 40.2 34.7 749 219 4320 2250
12400 8490 11000 11200 12800 24200 14500 9840 29900 24400
17.2 11.7
0.51
0.32
0.49
1.1
18.6 21.4 9.7 4.4
0.47 0.2 0.32 0.34 5.3
18300 31400 175000 45500 46400 37400 96600 45200 41300 259000 158000
107000 63000 207000 149000 113000 124000 373000 126000 120000 319000 257000
3610 1820 12400 6180 3880 3630 83400 23700 10700 16900 30800
52.72 11.34 8.55 9.77 17.91 103.61 76.95
60 21 20 15.58 20 60 50.85
8.7 8.3 7.5 8.4 6.8 8.1 5.4 5.5 7.3 2.9 7
5 4 22 15 147 118 50 51 23 14 33
5.2 5 6 5.9 5.6 5.5 6.3 6.4 6.8 6.5 6.8
436 436 27 315 367 437 406 284 252 127 262
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
µmhos/cm
Field Specific Conductance 137 1040 367 715 194 171 64
°C
Field Temperature 18.4 19.6 18.7 14.8 14.7 17.2 16
November-13
EPA 300.0
µg/L250000 250000 µg/L Sulfate 128000 3400 113000 8310
EPA 6010
µg/L
100 700 µg/L Barium 106 311 201 296 53.9 98.8 25.4
10 1000 µg/L Cobalt 19.2 53.5 49.4
300 300 µg/L Iron 766 31300 89.5 136
50 50 µg/L Manganese 8710 9990 688 19.4 6.8
50 100 µg/L Nickel 27.1 5.3
NE NE µg/L Sodium 9940 46200 42600 13800 13000 5580
25 300 µg/L Vanadium 5.5
10 1000 µg/L Zinc 12.2
EPA 8151
µg/L
2 50 µg/L 2,4,5-TP (Silvex) 0.23
2 70 µg/L 2,4-D 1.1
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.3 0.9
1 1 µg/L Benzene 1.9 0.27
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.41 0.54
5 1000 µg/L Dichlorodifluoromethane
1 5 µg/L Methylene chloride 3
10 6 µg/L Naphthalene 0.86
NE NE µg/L o-Xylene 0.541 0.7 µg/L Tetrachloroethene 2.2
NS NS µg/L Tetrahydrofuran 99.6 11.7 13.7
1 3 µg/L Trichloroethene 0.89
1 2000 µg/L Trichlorofluoromethane 12 0.47
1 0.03 µg/L Vinyl chloride 0.95
EPA 8270
µg/L
10 40 µg/L 3&4-Methylphenol(m&p Cre
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 28100 349000 155000 224000 31700 51600 19700
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 103000 654000 193000 496000 154000 116000 61000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 5880 56700 3620 36500 15200 5160 1510
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 7.1 5.9
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
155 86 430 243 149 156 623 205 183 649 478
17.7 15 14.4 15 16.6 17.7 17.8 21.2 19.7 18.9 19.3
10400 27400 9360 53200 2190 5490 62500 23000
170 112 87.8 47.6 106 140 23.8 71.1 50.1 348 101
47.5 14.4
136 84.3 32100 253 1330 915 239 22800 3360 11700 1790
6.9 7.9 1920 86.1 48.8 110 14 1530 152 8930 1080
12
13500 9070 10500 11700 12300 25300 13000 10300 41100 20100
9.8
17.1 10.8
0.88
0.77
0.28
5 14.7 18.9
0.69 0.33 7.6 0.25
3.6
18400 26700 161000 39300 43200 32800 64300 72700 48900 516000 152000
124000 66000 236000 126000 114000 123000 410000 125000 114000 705000 270000
3950 1790 14000 6230 5700 4100 124000 18100 11600 34800 31000
6 5.2
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
Field
feet
Static Water Level 71.87 16.65 45.08 18.63 22.73 76.44 36.08
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 8.7 0.9 0.7 7.5 5.6 0.5 10.2
NTUTurbidity 1 3 1 12 3 2 5
Std. Units
Field pH 5.6 5.6 5.9 5.8 5.9 5.5 5.4
mV
REDOX 228 68 -8 207 239 200 357
µmhos/cm
Field Specific Conductance 104 840 316 678 168 144 48
°C
Field Temperature 18.3 13.8 15.9 17.2 17.4 16.5 15.1
May-13
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 115000 5070 97600 11200 2100EPA 6010
µg/L
100 700 µg/L Barium 109 324 216 375 57.7 115 28.5
1 4000 µg/L Beryllium
10 10 µg/L Chromium
10 1000 µg/L Cobalt 18.2 64.1 35.3
10 1000 µg/L Copper
300 300 µg/L Iron 877 34100 158 126 61.5
10 15 µg/L Lead
50 50 µg/L Manganese 7880 9630 496 24.9
50 100 µg/L Nickel 20.7
NE NE µg/L Sodium 9080 45700 42600 13000 14300 6120100 2000000 µg/L Tin 5.8
25 300 µg/L Vanadium
10 1000 µg/L Zinc 21.1 10.5 13.6
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.2 0.84
50 NE µg/L 2-Hexanone 0.48
100 6000 µg/L Acetone 20.3
1 1 µg/L Benzene 1.4
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.26 0.72
5 500 µg/L m&p-Xylene 0.96
1 5 µg/L Methylene chloride 4.2
10 6 µg/L Naphthalene 1.3
NE NE µg/L o-Xylene 0.54 0.27
1 0.7 µg/L Tetrachloroethene 1.5
NS NS µg/L Tetrahydrofuran 111 8.5 24.2
1 3 µg/L Trichloroethene 0.68
1 2000 µg/L Trichlorofluoromethane 12.1 0.25
5 500 µg/L Xylenes (Total) 1.2
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
106.03 24.77 9.1 10.56 18.83 104.66 79.28
60 21 20 15.58 20 60 50.85
9.2 2.2 0.5 6.5 1.3 6.5 2.8 3 4 2.5 4.3
11 4 8 9 123 250 21 35 2 57 4
5.2 5.2 5.9 5.8 5.4 5.4 6.2 6.2 6.7 6.2 6.8
363 327 -66 189 280 355 241 -31 -12 -15 61
138 63 385 153 115 123 614 246 134 899 369
16.3 16.7 16.7 17.1 14.8 16.7 17 13.7 12.7 15.1 12.8
3200 11000 51800 7820 41200 2700 5090 20100 13200
174 115 87 50.1 176 254 59.6 58.9 51.7 185 106
2.4
7.1 6.6
65.1 6.6 14.6 25.3 10.4
7.6 9.5
867 92.8 30700 324 8610 5820 4140 6900 1400 9560 4180
6.5
16.6 1890 13.2 158 240 160 855 153 3990 1650
8.6
12900 8290 11100 19100 13500 26700 12400 9160 25000 18200
14.6 9.9 8.6
37.3 27.4 22.7
0.63
7.4 5.1
0.36 0.38 4.3
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 29800 363000 175000 203000 34800 63500 22800
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 84000 589000 175000 413000 131000 108000 51000
SM 4500-Cl-Eµg/L
NE 250000 µg/L Chloride 5910 50000 3860 33700 16200 5340 2070
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 8.1 5
Field
feet
Static Water Level 73 15.54 21.94 17.53 21.44 38.62 31.43
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 8.3 1.9 6 2.7 7.1 0.9 7.2
NTU
Turbidity 1 1 1 36 1 1 1
Std. Units
Field pH 5.6 5.8 5.8 5.6 6 5.3 5.5
mV
REDOX 263 10 21 246 274 211 260
µmhos/cm
Field Specific Conductance 68 802 217 382 116 106 31
°C
Field Temperature 20.9 19.7 15.7 15.6 15.2 16.3 17.5
November-12
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 79500 5420 73600 8400 2090EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 91.7 335 173 400 53.4 95.1 26.9
1 4000 µg/L Beryllium
10 10 µg/L Chromium
10 1000 µg/L Cobalt 15.2 35.5
10 1000 µg/L Copper
300 300 µg/L Iron 1730 25300 344 102 60.8
10 15 µg/L Lead
50 50 µg/L Manganese 8400 11600 541 17.4
50 100 µg/L Nickel 21.8
NE NE µg/L Sodium 9180 43400 43600 14500 13900 6980
25 300 µg/L Vanadium
10 1000 µg/L Zinc 24.5 15.2
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
21700 32100 189000 29600 58700 35600 78900 58000 48600 293000 147000
100000 46000 228000 138000 87000 102000 442000 104000 91000 327000 255000
4300 2040 14200 5820 3820 4290 124000 20600 10800 20000 26900
106.24 23.65 8.13 9.59 17.62 104.48 78.61
60 21 20 15.58 20 60 50.85
7.4 3.1 6.4 9.3 1.3 6.4 2.5 5 9.5 1.9 5.8
44 1 6 5 587 446 190 45 11 13 15
5 5.2 6.2 5.8 5.6 5.5 6.1 6.4 7 6.3 6.9
282 267 -22 185 204 254 224 -13 -10 -53 -31
88 43 400 197 136 81 403 208 144 575 367
18.1 16.3 14.7 14.7 16.5 18.2 17.9 22.4 23 22.4 23.3
10400 24200 9770 35600 2090 4240 36400 32300
7.1
142 101 76.8 50.5 279 160 143 63.3 46.5 315 151
3.5
11.8 6 6.7
13
6.9 5.8 10.5
218 29000 1430 11300 4520 12300 25500 1280 16500 1640
7.5 9.5
5.1 1740 33.6 301 251 317 1720 106 5200 2430
13.7
13100 5280 8770 11000 14600 15000 21200 15500 9990 33800 29000
18.7 8 28.6
92 30.8 51 23 45.6
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
EPA 8081
µg/L
0.1 0.1 µg/L 4,4'-DDD
0.002 0.002 µg/L Dieldrin 0.11
0.1 42 µg/L Endosulfan II 0.12
0.1 2 µg/L Endrin 0.27
0.1 2 µg/L Endrin aldehyde 0.230.075 0.004 µg/L Heptachlor epoxide 0.12
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.2 1.2
1 1 µg/L Benzene 1.3
10 3000 µg/L Chloroethane 1.3
5 70 µg/L Chloroform 0.16
5 70 µg/L cis-1,2-Dichloroethene 0.25 0.62
5 1000 µg/L Dichlorodifluoromethane
1 5 µg/L Methylene chloride 4.5
10 6 µg/L Naphthalene 1.6
NE NE µg/L o-Xylene 0.63
1 0.7 µg/L Tetrachloroethene 1.8
NS NS µg/L Tetrahydrofuran 93.2 13.5 26
1 3 µg/L Trichloroethene 0.77
1 2000 µg/L Trichlorofluoromethane 16.9 0.29
5 500 µg/L Xylenes (Total) 0.98 0.79
EPA 8270
µg/L
10 0.05 µg/L Benzo(a)anthracene 1.4
15 3 µg/L bis(2-Ethylhexyl)phthalate 2.4 1.1 1
10 5 µg/L Chrysene 1.5
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 26300 277000 142000 174000 31200 51900 19500SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 95000 564000 172000 435000 157000 111000 58000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 5320 64000 3920 34500 16100 3810 1860
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 9.1
SM 4500-S2D
µg/L
1000 NE µg/L Sulfide
Field
feet
Static Water Level 72.24 17.78 45.36 19.26 22.81 77.49 37.56
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 5.5 1.5 1.2 2.3 6.4 1.8 9.8
NTU
Turbidity 1 1 25 14 14 7 1
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
0.062 0.079 0.11
0.071
0.08
0.34
0.49
0.28
6.3 4.8
0.49 0.49 8.1
13 9.8
17200 25500 153000 40200 43900 28900 77600 79700 44700 317000 220000
118000 63000 220000 127000 144000 127000 298000 131000 101000 432000 349000
3560 1800 12900 4900 6150 4790 143000 19700 10300 24300 28800
106 100
105.53 25.13 8.94 10.71 18.71 104.68 79.91
60 21 20 15.58 20 60 50.85
7.3 4.4 0.9 3 2.3 6.4 2.3 8.7 6.7 2.1 6.7
1 1 25 1 605 329 456 3 1 14 92
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
Std. Units
Field pH 5.7 5.8 5.6 5.7 5.8 5.4 5.7
mV
REDOX 236 77 16 181 245 197 260
µmhos/cm
Field Specific Conductance 100 842 283 655 175 147 49
°CField Temperature 16 14 15.2 13.3 15.9 14.5 15.6
April-12
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 95000 6860 98700 7910
EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 93.8 366 228 407 57.5 100 27.5
1 4000 µg/L Beryllium
10 10 µg/L Chromium 5.2
10 1000 µg/L Cobalt 14.8 16.4 21.5
300 300 µg/L Iron 3190 41500 145 209 57.8
10 15 µg/L Lead
50 50 µg/L Manganese 8280 9310 370 10.2
50 100 µg/L Nickel 22.3
10 20 µg/L Silver 5.2
NE NE µg/L Sodium 9440 38400 40400 14200 13700 6250
25 300 µg/L Vanadium
10 1000 µg/L Zinc 35.2
EPA 8081
µg/L
0.1 0.1 µg/L 4,4'-DDD 0.13
0.1 0.1 µg/L 4,4'-DDT 0.54 0.14
0.05 2 µg/L Aldrin 0.120.05 0.006 µg/L alpha-BHC 0.12
0.05 0.019 µg/L beta-BHC 0.1
0.05 0.019 µg/L delta-BHC 0.18 0.069
0.002 0.002 µg/L Dieldrin 0.081
0.1 42 µg/L Endosulfan II
0.1 2 µg/L Endrin aldehyde 0.28
0.05 0.008 µg/L Heptachlor 0.48
0.075 0.004 µg/L Heptachlor epoxide 0.066
1 40 µg/L Methoxychlor 0.83
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
5.5 5 6.1 5.9 5.5 5.5 6.5 6.1 6.7 6.2 6.8
352 366 -61 150 246 365 160 -21 -21 -26 83
134 63 354 158 136 137 434 261 135 700 523
16 16.3 16 16.1 15.8 15.8 15.5 14.7 12.7 10 12.4
9700 20500 9420 25800 6180 26400 23600
5.7
142 96.5 70.3 46.9 144 122 115 70.4 53.4 179 136
1.4
7.2
5.5
55.1 26300 539 3760 1140 10000 11400 1720 9370 2140
7.6
1580 15.7 91.5 170 327 1040 157 3760 2420
12.5
12600 7460 11600 16700 14300 16300 14300 9890 21300 20000
7.2 23.4
20 51.1
0.062
0.05 0.09 0.054
0.085 0.066
0.061
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.1 1.2
5 350 µg/L 1,1-Dichloroethene 36.6
1 1 µg/L Benzene 1.5
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.33 0.51 5 µg/L Methylene chloride 3.2
10 6 µg/L Naphthalene 1.9
NE NE µg/L o-Xylene 1
1 0.7 µg/L Tetrachloroethene 1.7
NS NS µg/L Tetrahydrofuran 152 8.8 18.9
1 3 µg/L Trichloroethene 0.82
1 2000 µg/L Trichlorofluoromethane 20.9
5 500 µg/L Xylenes (Total) 1.6
EPA 8270
µg/L
20 NE µg/L 3,3'-Dichlorobenzidine
10 NE µg/L 3-Methylcholanthrene
10 0.05 µg/L Benzo(a)anthracene
10 0.005 µg/L Benzo(a)pyrene
10 0.05 µg/L Benzo(b)fluoranthene
10 200 µg/L Benzo(g,h,i)perylene
10 0.5 µg/L Benzo(k)fluoranthene
15 3 µg/L bis(2-Ethylhexyl)phthalate 5.5
10 5 µg/L Chrysene
10 0.005 µg/L Dibenz(a,h)anthracene
10 0.05 µg/L Indeno(1,2,3-cd)pyrene
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 27100 196000 150000 64300 134000 50200 20100
SM 2540Cµg/L
NE 500000 µg/L Total Dissolved Solids 93000 531000 168000 374000 149000 109000 52000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 5350 61500 33200 16100
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 6.5
SM 4500-S2D
µg/L
1000 NE µg/L Sulfide
Field
feet
Static Water Level 36.43 7.99 21.01 8.24 10.55 38.23 15.03
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 5 2.9 0.8 0.7 8.7 0.8 6.7
NTU
Turbidity 1 4 3 7 2 1 7
Std. Units
Field pH 5.2 5.8 5.8 5.5 5.4 5.5 5.5
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
3.1
0.25
1.4 0.97
4.4 4.5
7.3 1.4
3.6
2.9
1.1
1.1 2.5
1 2.8
1.3 1.2 1.5 1.8
2.5
1.1
1.1
1.2 2.1
1.2 1.5 2.2
20100 413000 120000 37200 52200 30100 75300 47200 44200 221000 158000
123000 49000 161000 130000 110000 145000 260000 98000 101000 329000 272000
10800 8200 5380 60600 25300 11300 22800 30900
178
52.4 11.92 4.13 5.04 8.92 52.03 39.39
60 21 20 15.58 20 60 50.85
7.2 4.8 0.5 5.4 1.6 6.9 2.5 7.1 8.5 4.1 7.7
2 2 14 8 150 32 112 21 16 12 10
5.2 5.2 5.5 6.1 5.9 5.8 6.4 6.5 7.1 6.4 6.5
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
mV
REDOX 166 43 -24 156 189 185 176
µmhos/cm
Field Specific Conductance 102 809 329 568 182 149 52
°C
Field Temperature 16.7 15.2 13.8 13 13.9 14.7 14.4
December-11EPA 300.0
µg/L
250000 250000 µg/L Sulfate 61800 7020
EPA 6010
µg/L
100 700 µg/L Barium 82.6 328 85.2
10 10 µg/L Chromium 14.7
10 1000 µg/L Cobalt 15
300 300 µg/L Iron 368 3540
50 50 µg/L Manganese 257 43.5
NE NE µg/L Sodium 7670 35300 13300
25 300 µg/L Vanadium 13
10 1000 µg/L Zinc 15.3EPA 8260
µg/L
5 350 µg/L 1,1-Dichloroethene
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 27500 143000 32800SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 95000 345000 139000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 29200 16400Field
feet
Static Water Level 36.8 9.33 11.2
Total Well Depth 60 20 30
mg/L
Oxygen, Dissolved 5.4 2.3 6.2
NTU
Turbidity 2 40 90
Std. Units
Field pH 5.8 5.9 5.7
mV
REDOX 218 175 200
µmhos/cm
Field Specific Conductance 97 490 177
°C
Field Temperature 15.4 12.5 15.2
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
180 196 -78 166 189 177 121 -6 -36 -62 -23
140 66 325 176 144 150 404 194 142 570 454
16 14.5 14.2 15.1 15 16.4 16.7 19.9 18 18.5 18.9
19800 19500
123 105
3230 1060
1890 1290
18500 17900
0.58
160000 131000
237000 234000
20900 23600
5.1 8.3
14 7
6.4 6.7
-1 66
415 370
11.4 11.5
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
November-11EPA 300.0
µg/L
250000 250000 µg/L Sulfate 96300
EPA 6010
µg/L
100 700 µg/L Barium 351 237 97.1 24.41 4000 µg/L Beryllium
10 10 µg/L Chromium
10 1000 µg/L Cobalt 11.8
10 1000 µg/L Copper
300 300 µg/L Iron 2980 40300 151
10 15 µg/L Lead
50 50 µg/L Manganese 7920 7310 12.7 7
50 100 µg/L Nickel 20.9
10 20 µg/L Silver 5
NE NE µg/L Sodium 31800 12000 5410
25 300 µg/L Vanadium
10 1000 µg/L Zinc 33.3 45.4
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.2 1.9
5 350 µg/L 1,1-Dichloroethene 38.7
100 6000 µg/L Acetone 3.7
1 1 µg/L Benzene 2
5 70 µg/L Chloroform 0.26
5 70 µg/L cis-1,2-Dichloroethene 0.46 0.67
5 500 µg/L m&p-Xylene 0.66
1 5 µg/L Methylene chloride 3.5
NE NE µg/L o-Xylene 1.2
1 0.7 µg/L Tetrachloroethene 1.8
NS NS µg/L Tetrahydrofuran 1971 3 µg/L Trichloroethene 0.88
1 2000 µg/L Trichlorofluoromethane 20.1 0.34
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 219000 155000 47700 19600
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 498000 180000 124000 81000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 62400
Field
feet
Static Water Level 36.52 16.58 44.06 9.04 11.1 77.6 17.03
Total Well Depth 21 27 48 27
mg/L
Oxygen, Dissolved 1.7 3.1 4 5.8
NTU
Turbidity 1 4 3 4
Std. Units
Field pH 5.9 6 5.8 5.6
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
7590 15300 9460 38300
141 91.3 57.5 60.1 139 143 42.5 812.3
5.5
6.1
424 23000 3030 6140 2050 2290 4170
6.4
6.8 1250 58.3 140 71 130 280
11900 6480 9980 20200 12700 9390 8650
10.8 7.5
31.6 12 13.5
2.2 4 6.6 5.5
3.2
0.42 0.68
17400 21700 122000 40200 44500 30400 19600 26100
128000 89000 165000 124000 159000 138000 140000 189000
8480 8030 19100 10900
52.19 12.24 7.38 9.19 17.83 52.08
60 21 20 15.58 20 60
6.8 4.5 0.6 2 6.9 6.2 7.7 7.3
1 2 37 54 223 154 36 103
5.6 5.6 6.3 6 5.9 5.8 6.4 6.6
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
mV
REDOX 95 71 207 206
µmhos/cm
Field Specific Conductance 762 306 158 48
°C
Field Temperature 12.7 13.8 12.3 15.2
June-11EPA 350.1
µg/L
NS NS µg/L Nitrogen, Ammonia 0.12
EPA 6010
µg/L
NE NE µg/L Sodium 27200
EPA 8260
µg/L
1 1 µg/L Benzene 1.6
1 0.7 µg/L Tetrachloroethene 1.6
NS NS µg/L Tetrahydrofuran 274
RSK 175
µg/L
NS NS µg/L Methane 1280
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 165000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 39900
Field
feet
Static Water Level 8.31
Total Well Depth 21
mg/LOxygen, Dissolved 4.2
NTU
Turbidity 3
Std. Units
Field pH 5.8
mV
REDOX 88
µmhos/cm
Field Specific Conductance 698
°C
Field Temperature 19.1
May-11
EPA 6010
µg/L
100 700 µg/L Barium 84.7 273 301 126 63.7 104 27.3
10 10 µg/L Chromium 1.4 5.4 1.3 7.6 0.96
10 20 µg/L Silver 0.51 2.5 0.6 0.88 0.57 0.84 0.1
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
205 223 -148 216 239 218 112 88
141 58 289 155 127 139 116 177
14.9 14.2 13.5 13 13.3 14.3 10.9 11.5
153 80.7 56.2 39.1 164 125 69.9 49.2
0.63 2.6 3.9 1.8
0.43 0.12 1.2 0.7 0.72 0.74 0.4 0.2
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
EPA 8260
µg/L
1 200 µg/L 1,1,1-Trichloroethane 0.82
5 6 µg/L 1,1-Dichloroethane 1.1 3.8
100 6000 µg/L Acetone 3.8
1 1 µg/L Benzene 1.3
5 70 µg/L Chloroform 0.361 3 µg/L Chloromethane 0.15
5 70 µg/L cis-1,2-Dichloroethene 0.26 0.71
5 500 µg/L m&p-Xylene 0.74 1.4
1 5 µg/L Methylene chloride 4.1
NE NE µg/L o-Xylene 0.84 0.39
1 0.7 µg/L Tetrachloroethene 1.4
NS NS µg/L Tetrahydrofuran 226
1 3 µg/L Trichloroethene 0.65
1 2000 µg/L Trichlorofluoromethane 31.6 0.48
Field
feet
Static Water Level 35.93 8.17 20.56 8.34 10.44 37.99 15.08
Total Well Depth 60 21 27 20 19.56 48 27
mg/L
Oxygen, Dissolved 6.3 3.9 6.3 5.3 9 3.2 8.7
NTU
Turbidity 55 57 70 96 85 40 18
Std. Units
Field pH 5.8 5.9 6.2 5.7 6.1 5.6 5.1
mV
REDOX 263 71 -43 271 141 245 272
µmhos/cm
Field Specific Conductance 110 687 409 174 208 193 10
°C
Field Temperature 17 16 14.6 14.3 15.5 16.2 16.6November-10
EPA 6010
µg/L
100 700 µg/L Barium 85.4 223 302 335 53 100 26.8
10 10 µg/L Chromium 0.96 0.49 0.68 5.8 0.55 0.62
10 15 µg/L Lead
10 20 µg/L Silver 0.85 1.3 0.16 0.23EPA 8260
µg/L
1 5 µg/L Methylene chloride 4.2
1 2000 µg/L Trichlorofluoromethane 36.1
Field
feet
Static Water Level 35.62 8.39 19.97 8.49 10.5 37.48 16.12
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 6.8 4.3 4.8 3.6 8.1 4 7.9
NTU
Turbidity 3 6 99 40 3 1.5 1
Std. Units
Field pH 5.13 5.05 5.22 6.16 5.13 5.81 5.56
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
0.21 0.24
12.1 18.6
0.26 0.52
51.11 11.72 4 4.91 8.85 51.45
60 21 20 15.58 20 60
7.3 7.1 4.3 7.4 5.2 7.8 6.6 9.1
1 4 23 25 177 39 50 52
5.6 5.5 6.2 6 5.6 5.5 6.4 6.5
265 279 -36 188 245 272 -15 23
153 55 321 179 171 140 295 129
18.7 16.6 15.6 15 15 17.1 19.7 18.6
157 38.9 48.1 44.9 176 129 61.9 57.6
1.1 4 2.3
4.3
50.02 12.04 4.03 4.97 9.04 51
60 21 20 15.58 20 60
7.8 7.8 5.1 4.9 5.2 7.7 6.7 8.8
1 0.5 80 7 200 24 7 8
5.38 5.31 5.91 5.82 5.45 5.42 6.37 6.09
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
mV
REDOX 282 99 -14 260 212 261 329
µmhos/cm
Field Specific Conductance 109 543 369 562 204 191 60
°C
Field Temperature 16.8 16.3 15.9 16.4 16.2 15.1 17.5
April-10EPA 8260
µg/L
1 2000 µg/L Trichlorofluoromethane 21.9
Field
feet
Static Water Level 7.15
Total Well Depth 21
mg/L
Oxygen, Dissolved 2.7
NTU
Turbidity 2
Std. Units
Field pH 5.46
mV
REDOX -7
µmhos/cm
Field Specific Conductance 255
°C
Field Temperature 14.3March-10
EPA 6010
µg/L
10 10 µg/L Arsenic 4 4.2 3.4
100 700 µg/L Barium 85.3 103 314 55.9 54.3 99.3 28.8
1 2 µg/L Cadmium 0.8210 10 µg/L Chromium 1.4 1.2 1.3 5 1.4
10 20 µg/L Silver 0.29 0.67 0.45 0.46 0.56
EPA 8260
µg/L
1 2000 µg/L Trichlorofluoromethane 22.2
Field
feet
Static Water Level 36.62 7.16 18.22 8.22 9.99 38.71 13.23
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 5.9 4.8 3.7 4.4 6.1 2.2 7.2
NTU
Turbidity 2 4 6 45 3 2 7
Std. Units
Field pH 5.74 5.31 5.61 5.56 5.96 5.55 5.21
mV
REDOX 262 191 31 262 260 213 303
µmhos/cm
Field Specific Conductance 90 230 330 90 170 160 60
°C
Field Temperature 20.7 14.8 16.4 14.6 19.2 16.8 13.7
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
334 329 -27 183 251 335 9 60
193 42 267 183 168 167 307 183
16.2 18.5 17 18.1 17.2 17.2 14 13.4
2.7 3.7
134 46.6 37.6 40.6 126 130 92.5 59.4
2.4 1.7 3
0.27 0.48 0.2 0.4 0.39 0.28 0.2
51.31 11.18 3.55 4.15 8.05 51.21
60 21 20 15.58 20 60
8.5 7.4 1.9 6.8 5.4 7.9 6.8 8.8
6 2 13 31 11 29 8 13
5.32 5.18 5.97 5.73 5.5 5.35 7.05 6.77
309 300 -60 197 237 292 53 82
140 40 190 140 120 150 230 170
14.6 17.1 13.4 13 13.6 14.4 17.1 17.9
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
November-09Field
feet
Static Water Level
Total Well Depth
mg/L
Oxygen, DissolvedNTU
Turbidity
Std. Units
Field pH
mV
REDOX
µmhos/cm
Field Specific Conductance
°C
Field Temperature
September-09
EPA 6010
µg/L
100 700 µg/L Barium 92.8 80.7 289 334 66.8 104 27.2
10 10 µg/L Chromium 2 5.4 8.6 0.65
10 15 µg/L Lead 4.8
10 20 µg/L Silver 0.48 0.68 1 2.4 0.6 0.88 0.16
EPA 7470
µg/L
0.2 1 µg/L Mercury
EPA 8260
µg/L
5 350 µg/L 1,1-Dichloroethene
100 700 µg/L Carbon disulfide 26.1 12.5
1 5 µg/L Methylene chloride1 2000 µg/L Trichlorofluoromethane
Field
feet
Static Water Level 37.16 8.89 22.73 9.59 11.33 39.87 16.7
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 3.6 1 0.5 1.8 6.3 1 5.4
NTU
Turbidity 38 12 40 247 62 21 27
Std. Units
Field pH 5.61 5.65 5.88 5.77 6.11 5.47 5.43
mV
REDOX 334 175 37 259 362 292 342
µmhos/cm
Field Specific Conductance 107 228 366 391 195 170 60
°C
Field Temperature 18.1 18.8 17.6 19.2 16.6 18.9 16.1
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
8.55
20
2.6
65
5.23
386
105
15.9
128 39.1 31.8 38 117 242 77.7 52.1
0.8 10.7
7.2 17.5
0.32 0.19 0.5 0.39 0.41 0.54 0.62 0.36
0.081
19.8
13
2.618.6
51.52 12.36 4.48 4.85 9.35 51.28
60 21 20 15.58 20 60
6.1 6.9 1 2.4 4.1 6 0.6 8.4
28 2 13 19 63 598 65 30
5.45 5.35 6.15 5.83 5.56 5.53 6.16 6.55
353 371 -22 197 290 364 28 111
141 42 171 139 124 147 255 148
16.9 18.9 19.3 19.5 17.9 16.8 19.8 20.9
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
March-09EPA 6010
µg/L
100 700 µg/L Barium 74.3 88.5 252 58.3 52.6 86.9 25
10 10 µg/L Chromium 0.88 1.6 1.2 5.2 0.78
10 20 µg/L Silver 0.58 0.29 0.28 0.42
EPA 8260µg/L
100 700 µg/L Carbon disulfide 3.3
Field
feet
Static Water Level 38.27 8.14 22.29 10.07 11.14 40.61 15.86
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 4.5 2.6 1.3 4.9 6.6 0.9 7.8
Std. Units
Field pH 5.7 5.59 5.92 5.51 6.01 5.62 5.38
mV
REDOX 585 198 1 433 517 355 523
µmhos/cm
Field Specific Conductance 94 222 349 60 175 152 54
°C
Field Temperature 15.4 13 14.7 11 13.6 15 14.8
December-08
EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 85 98.8 231 263 56.1 99 32.8
10 10 µg/L Chromium 0.64 0.5 0.58 5.3 0.91 0.97
10 15 µg/L Lead
10 20 µg/L Selenium 11.8
10 20 µg/L Silver 0.62 1.2 1.5 2.6 0.78 0.96 0.15EPA 8260
µg/L
5 70 µg/L Chloroform 3.4
Field
feet
Static Water Level 38.39 9.13 22.72 11.18 11.78 40.61 17.8
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 4.43 0.64 0.62 0.81 6.83 1.88 6.01
Std. Units
Field pH 5.79 5.76 5.79 5.88 6.08 5.64 5.85
mV
REDOX 217 185 45 178 197 220 199
µmhos/cm
Field Specific Conductance 93 218 268 422 176 152 53
°C
Field Temperature 14.8 13.3 14.6 14.7 15 12.8 15.3
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
173 38.9 28.4 34.5 79.2 97.9 45.6 46.3
7.6 0.65 2 1.6 0.4 0.61 0.42
0.18
52.36 11.7 3.73 4.13 8.34 51.52
60 21 20 15.58 20 60
6.4 7.2 2.4 7.1 4.2 8.3 6.4 8.6
5.37 5.58 5.84 5.79 5.4 5.5 6.07 7.01
466 353 -122 181 241 390 53 117
115 37 137 114 89 140 146 126
15.5 13.9 13.5 12.4 12.8 15 15.5 15.9
7.3
124 41.9 28.6 57.9 88.7 583 78.2 50.6
0.47 2.2 40.2 0.67
26.2
8.7
0.36 0.79 0.37 0.44 0.46 0.39 0.5
52.11 12.33 4.24 4.51 8.91 51.81
60 21 20 15.58 20 60
6.19 6.73 0.35 2.52 4.2 6.68 5.58 8.4
5.7 5.73 6.33 5.98 5.68 5.81 5.04 6.19
203 222 -79 -30 190 215 145 88
117 35 133 118 84 135 196 130
15 15.6 14.7 14.3 14.5 14.8 8.1 7
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
March-08EPA 6010
µg/L
100 700 µg/L Barium 90.3 102 293 172 57.5 95.7 24
10 10 µg/L Chromium 0.49 0.79 0.63 0.4 5.6 7.3 0.42
10 20 µg/L Selenium 4.9
10 20 µg/L Silver 0.43 0.93 0.87 0.94 0.56 0.66 0.13EPA 7470
µg/L
0.2 1 µg/L Mercury 0.1
EPA 8260
µg/L
100 4000 µg/L 2-Butanone (MEK)
100 6000 µg/L AcetoneField
feet
Static Water Level 38.28 8.83 22.71 10.49 11.13 40.6 15.22
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 4.61 1.46 3.08 3.69 6.77 3.04 6.44
Std. Units
Field pH 6.04 6.14 6.08 6.75 6.56 5.84 7.39
mV
REDOX 56 29 -43 24 33 52 50
µmhos/cm
Field Specific Conductance 91 234 258 254 172 141 51
°C
Field Temperature 16.62 16.47 14.41 11.87 14.15 15.59 14
November-07
(blank)
µg/L
100 6000 µg/L Acetone100 700 µg/L Barium 105 107 273 287 70.6 101 26.6
10 10 µg/L Chromium 8.4
0.2 1 µg/L Mercury
10 20 µg/L Selenium 18.1
10 20 µg/L Silver 0.16
Field
feet
Static Water Level 38.12 9.32 22.72 10.65 11.65 40.4 16.78
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 5.08 0.72 1.69 1.32 6.5 0.85 7.12
Std. Units
Field pH 6.52 6.67 6.21 6.35 7 6.07 6.27
mV
REDOX 59 61 66 43 61 53 66
µmhos/cm
Field Specific Conductance 85 176 217 394 161 126 51
°C
Field Temperature 15.42 14.08 13.22 16.04 14.9 14.16 15.48
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
124 42 29.2 60.5 64.6 186 79.7 50.6
1.8 1.1 4.1 1.2
0.22 0.41 0.15 0.21 0.56 0.37 0.26
0.26
4.6
15
51.33 11.77 4.08 4.47 8.78 51.11
60 21 20 15.58 20 60
7.8 7.08 0.33 5.27 5.85 6.69 7.5 7.28
5.66 6.81 7.12 7.22 6.45 5.82 7.69 8.54
191 123 -172 18 74 124 197 195
123 36 125 99 72 136 194 122
17.68 14.52 13.95 12.86 15.63 16.47 14.74 13.5
22.7117 40.8 23.1 47.3 85.6 130 70.3 49.4
1.7 0.61
0.098
0.32 0.39 0.26 0.48 0.51 0.26
50.38 12.34 4.33 4.95 9.27 50.78
60 21 20 15.58 20 60
7.32 6.59 1.02 2.01 5.16 7.33 5 6.93
5.73 5.95 6.67 6.48 6.83 5.82 6.18 7.35
56 73 -80 21 73 58 34 48
121 36 121 114 65 140 218 112
15.75 16.38 16.33 16.3 15.32 15.75 15.64 17.53
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
April-07(blank)
µg/L
100 4000 µg/L 2-Butanone (MEK)
10 10 µg/L Arsenic
100 700 µg/L Barium 81 79 310 200 58 89 30
10 10 µg/L Chromium 6.410 15 µg/L Lead
10 20 µg/L Selenium 24
Field
feet
Static Water Level 37.43 8.58 20.12 8.71 10.33 39.81 14.14
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 3.82 0.48 290 1.07 5.55 0.67 5.14
Std. Units
Field pH 5.86 5.59 5.81 6 6.17 5.66 5.03
mV
REDOX 58 50 -3 -8 36 30 48
µmhos/cm
Field Specific Conductance 91 151 324 333 171 139 52
°C
Field Temperature 15.4 12.4 14.2 12.1 13.5 15.4 14.3
November-06
(blank)
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 94 90 230 220 58 76 29
1 2 µg/L Cadmium 2
10 10 µg/L Chromium 6.2
10 15 µg/L Lead
Fieldfeet
Static Water Level 38.17 8.74 22.3 9.81 11.17 40.13 16.19
Total Well Depth 60 21 27 20 30 48 27
mg/L
Oxygen, Dissolved 4.28 0.31 1.15 0.42 5.88 1.21 6.2
Std. Units
Field pH 6.29 5.97 5.94 6.16 6.49 5.94 6.15
mV
REDOX -13 114 160 59 59 95 35
µmhos/cm
Field Specific Conductance 104 235 266 196 196 155 60
°F
Field Temperature 58.8 59.3 59.5 59.9 60.2 58.1 59.9April-06
(blank)
µg/L
100 700 µg/L Barium 82 52 290 220 57 74 29
10 10 µg/L Chromium 6.2
10 15 µg/L Lead
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
11
5.5
140 52 25 31 79 210 88 300
6.6 175.2 11
21
49.98 11.43 2.66 4.21 8.67 49.43
60 21 20 15.7 20 60
5.35 5.53 280 6.57 4.59 5.7 5.5 6.16
5.86 5.62 5.96 6.02 5.72 5.79 6.63 6.32
90 124 -114 87 110 99 27 86
115 39 125 105 72 140 314 130
15.5 14 13.9 13.5 12.9 15.4 22.3 20.8
8.3
140 71 24 66 62 460 54 44
35
23
49.85 11.94 3.41 4.65 8.92 40.93
60 21 20 15.6 20 60
5.44 5.67 0.31 0.85 4.54 6.41 7.91 5.26
5.94 5.84 6.64 6.24 5.84 6 7.28 6.65
90 221 67 132 235 171 130 233
136 45 145 127 80 152 66 140
59.7 60.7 60.4 60.3 60.7 59.2 55.4 62.2
100 48 26 55 65 250 120 150
4215 4.2 4.7
13 7.6
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
November-05EPA 6010
µg/L
100 700 µg/L Barium 78 62 300 180 54 60 26
10 10 µg/L Chromium 3.5
10 15 µg/L Lead
EPA 7470µg/L
0.2 1 µg/L Mercury 0.34 0.4 0.24 0.26
EPA 8260
µg/L
1 3 µg/L Chloromethane 5.4
June-05
(blank)
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 48 43 300 150 53 53 25
10 10 µg/L Chromium 5.6
10 15 µg/L Lead
10 20 µg/L Selenium 5.5November-04
(blank)
µg/L
10 10 µg/L Arsenic 5.1
100 700 µg/L Barium 95 52 340 140 80 63 30
10 10 µg/L Chromium 2 2.3 14 4.4 2.4August-04
(blank)
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium
10 10 µg/L Chromium10 15 µg/L Lead
10 20 µg/L Selenium
May-04
(blank)
µg/L
10 10 µg/L Arsenic 9.2 5 6
100 700 µg/L Barium 96.3 55 270 380 76 28 180 480
10 10 µg/L Chromium 3.5 3.7 14 7.3 2.2 26 28
10 15 µg/L Lead 14 18 5.1 41
November-03
(blank)
µg/L
10 10 µg/L Arsenic 8.6
100 700 µg/L Barium 460 60 200 97 65 25 820 52
10 10 µg/L Chromium 2.2 2.3 2.6 8.7 2.4 150 3.2
10 15 µg/L Lead 22 24
1/8/2016
Summary of Detected Constituents
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equip
ment
Blank
100 46 27 77 59 120 73 51
3.9
5.9
0.2 0.44 1.1
23
85 82 24 50 46 69 750 47
52
57
95 55 28 77 57 66 53 65
3.9 2.1 4.8 3.2
20
240 98 47 74 160 170 500 63
14 13 3.3 9.2 3.2 3614 6.8 11 8 38
6.2
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
May-03(blank)
µg/L
100 700 µg/L Barium 120 56 220 94 72 24 130 77
1 2 µg/L Cadmium 2.7
10 10 µg/L Chromium 4.3 5.5 9.5 17 3.8
10 15 µg/L Lead 5.3 5.3 6.7December-02
(blank)
µg/L
100 700 µg/L Barium 100 140 13 86 65 41 210 48
1 2 µg/L Cadmium 1.9
10 10 µg/L Chromium 2.3 2.1 5 7.4 3.2 32 2
10 15 µg/L Lead 6 6April-02
(blank)
µg/L
10 10 µg/L Arsenic 7.4
100 700 µg/L Barium 130 100 370 61 150 180 84 150
10 10 µg/L Chromium 5 15 23 26 6.8 23
10 15 µg/L Lead 21 7.6
10 20 µg/L Silver 2.6
November-01
(blank)
µg/L
10 10 µg/L Arsenic 5.8 8.4 12 7 16 17 36
100 700 µg/L Barium 280 160 400 900 610 530 1300 2700
10 10 µg/L Chromium 22 16 19 95 140 95 270 94
10 15 µg/L Lead 10 7 35 36 13 38 36 150
1 600 µg/L Toluene 21
July-01
(blank)µg/L
10 10 µg/L Arsenic 18 5.6 16 46
100 700 µg/L Barium 87 280 950 550 270 62 1300 2600
10 10 µg/L Chromium 6.6 16 50 38 49 4.1 210 92
10 15 µg/L Lead 8.9 53 14 7.6 26 210
December-00
(blank)
µg/L
10 10 µg/L Arsenic 31 5 45 89
100 700 µg/L Barium 150 61 1500 350 400 41 2600 4200
10 10 µg/L Chromium 6.6 3.9 100 28 82 2.6 580 240
10 15 µg/L Lead 80 8.1 7.6 65 400
June-00(blank)
µg/L
100 700 µg/L Barium 110 180 300 570 200 82 360
10 10 µg/L Chromium 3 8.1 2.5
10 15 µg/L Lead 6.5 9.5 5.8 8.7
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
November-99(blank)
µg/L
10 10 µg/L Arsenic 5.9 7.5
100 700 µg/L Barium 130 120 52 860 200 59 390
10 10 µg/L Chromium 5.2 14 24 60 29 2.8 62
10 15 µg/L Lead 6.9 40 40 8.2 120.2 1 µg/L Mercury 0.36
June-99
(blank)
µg/L
10 10 µg/L Arsenic 9.8
100 700 µg/L Barium 150 150 950 240 960
10 10 µg/L Chromium 7.8 7.8 110 38 190
10 15 µg/L Lead 50 16 30
1 5 µg/L Methylene chloride 13 13 10 10 10
November-98
(blank)
µg/L
100 6000 µg/L Acetone 150
10 10 µg/L Arsenic 11
100 700 µg/L Barium 160 1100 1400 2000 480 160 1300
100 700 µg/L Carbon disulfide 28 25 9
10 10 µg/L Chromium 12 210 77 300 96 12 350
10 15 µg/L Lead 68 39 76 29 36
0.2 1 µg/L Mercury 0.21May-98
(blank)
µg/L
10 10 µg/L Arsenic 5
100 700 µg/L Barium 100 190 860 850 820 360 1200
10 10 µg/L Chromium 49 34 25 130 170 33 43010 15 µg/L Lead 19 32 43 69 20 38
October-97
(blank)
µg/L
100 700 µg/L Barium 290 340 620 650 610 260 1800
10 10 µg/L Chromium 11 43 16 55 16 14 410
10 15 µg/L Lead 12 31 26 29 31 14 53
0.2 1 µg/L Mercury 0.2 0.2
May-97
(blank)
µg/L
100 700 µg/L Barium 100 200 800 280 330 300 750
1 2 µg/L Cadmium 3
10 10 µg/L Chromium 3 4 28 70 21 180
10 15 µg/L Lead 14 27 12 14 14 23
10 20 µg/L Silver 6 6
1/8/2016
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8
MCL
October-96(blank)
µg/L
100 700 µg/L Barium 180 160 790 720 620 590 970
10 10 µg/L Chromium 6 9 20 47 43 10 21
10 15 µg/L Lead 8 15 16 20 11 6
0.2 1 µg/L Mercury 0.2 0.3 0.4January-96
(blank)
µg/L
100 4000 µg/L 2-Butanone (MEK) 86
100 700 µg/L Barium 224 350 1230 595 1000 1400 1930
1 2 µg/L Cadmium 7
100 700 µg/L Carbon disulfide 23
10 10 µg/L Chromium 12 9 21 96 12 28
10 15 µg/L Lead 6 26 15 17 19 18 17
0.2 1 µg/L Mercury 1.8 0.4 0.7 1.7 0.8 1.4 1.4
1/8/2016
Winston-Salem City/County Utilities | Assessment Monitoring Report
APPENDIX B – LABORATORY GROUNDWATER REPORT
B.

B
Appendix B –
Laboratory
Groundwater Report

B-1

This page intentionally left blank.
#=CL#
December 30, 2015
LIMS USE: FR - ERIC WRIGHT
LIMS OBJECT ID: 92276295
92276295
Project:
Pace Project No.:
RE:
Mr. Eric Wright
HDR Engineering
440 South Church Street
Suite 1000
Charlotte, NC 28202
OSR
Dear Mr. Wright:
Enclosed are the analytical results for sample(s) received by the laboratory between November 16,
2015 and December 22, 2015. The results relate only to the samples included in this report.
Results reported herein conform to the most current TNI standards and the laboratory's Quality
Assurance Manual, where applicable, unless otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 265
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92276295
OSR
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North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 265
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92276295001 3412-SW1 EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295002 3412-SW2 EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295003 3412-SW3 EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295004 3412-SW4 EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295005 3412-MW3R EPA 8081 21 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 265
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8082 8 PASI-CSWB
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295006 3412-EQUIPMENT BLANK EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OLJM
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 105 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 4500-S2D 1 PASI-AMJP
SM 4500-CN-E 1 PASI-ASER
92276295007 3412-MW4R EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OLJM
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295008 3412-MW7 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OLJM
EPA 6010 19 PASI-ACDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 265
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295009 3412-MW5R EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OLJM
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295010 3412-MW1R EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OLJM
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295011 3412-MW15 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 265
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8151 5 PASI-OLJM
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295012 3412-MW2R EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OJTJ
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295013 3412-MW8 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OJTJ
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 265
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92276295014 3412-MW10 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OJTJ
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295015 3412-MW11 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OJTJ
EPA 6010 19 PASI-AJMW
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295016 3412-MW12 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OJTJ
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 265
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295017 3412-TRIP BLANK EPA 8260 69 PASI-CNB
92276295018 3412-MW9 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OJTJ
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295019 3412-MW13 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OJTJ
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92276295020 3412-MW14 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 5 PASI-OJTJ
EPA 6010 19 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 69 PASI-CNB
SM 2320B 1 PASI-AMLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 265
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 2540C 1 PASI-ASAM
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92280822001 3412-MW3R EPA 8151 5 PASI-OLJM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW1 Lab ID:92276295001 Collected:11/16/15 10:10 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/16/15 10:101
Field pH 6.7 Std. Units 11/16/15 10:100.10 1
Field Temperature 9.4 deg C 11/16/15 10:100.50 1
Field Specific Conductance 92.6 umhos/cm 11/16/15 10:101.0 1
Oxygen, Dissolved 5.5 mg/L 11/16/15 10:10 7782-44-71
REDOX -78.3 mV 11/16/15 10:101
Turbidity 48.7 NTU 11/16/15 10:101.0 1
Odor none 11/16/15 10:101
Appearance murky 11/16/15 10:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/23/15 21:34 7440-36-011/18/15 20:305.0 1
Arsenic ND ug/L 11/23/15 21:34 7440-38-211/18/15 20:3010.0 1
Barium 65.0 ug/L 11/23/15 21:34 7440-39-311/18/15 20:305.0 1
Beryllium ND ug/L 11/23/15 21:34 7440-41-711/18/15 20:301.0 1
Cadmium ND ug/L 11/23/15 21:34 7440-43-911/18/15 20:301.0 1
Chromium ND ug/L 11/23/15 21:34 7440-47-311/18/15 20:305.0 1
Cobalt ND ug/L 11/23/15 21:34 7440-48-411/18/15 20:305.0 1
Copper 3.9J ug/L 11/23/15 21:34 7440-50-811/18/15 20:305.0 1
Iron 9830 ug/L 11/23/15 21:34 7439-89-611/18/15 20:3050.0 1
Lead ND ug/L 11/23/15 21:34 7439-92-111/18/15 20:305.0 1
Manganese 688 ug/L 11/23/15 21:34 7439-96-511/18/15 20:305.0 1
Nickel ND ug/L 11/23/15 21:34 7440-02-011/18/15 20:305.0 1
Selenium ND ug/L 11/23/15 21:34 7782-49-211/18/15 20:3010.0 1
Silver ND ug/L 11/23/15 21:34 7440-22-411/18/15 20:305.0 1
Sodium 12800 ug/L 11/23/15 21:34 7440-23-511/18/15 20:3050001
Thallium ND ug/L 11/23/15 21:34 7440-28-011/18/15 20:305.4 1
Tin ND ug/L 11/23/15 21:34 7440-31-511/18/15 20:305.0 1
Vanadium 4.3J ug/L 11/23/15 21:34 7440-62-211/18/15 20:305.0 1
Zinc 7.5J ug/L 11/23/15 21:34 7440-66-611/18/15 20:3010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 13:31 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 05:59 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 05:59 75-05-850.0 1
Acrolein ND ug/L 11/20/15 05:59 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 05:59 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 05:59 107-05-12.0 1
Benzene ND ug/L 11/20/15 05:59 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 05:59 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 05:59 75-27-41.0 1
Bromoform ND ug/L 11/20/15 05:59 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 05:59 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 05:59 78-93-35.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW1 Lab ID:92276295001 Collected:11/16/15 10:10 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon disulfide ND ug/L 11/20/15 05:59 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 05:59 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 05:59 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 05:59 75-00-31.0 1
Chloroform ND ug/L 11/20/15 05:59 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 05:59 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 05:59 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 05:59 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 05:59 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 05:59 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 05:59 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 05:59 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 05:59 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 05:59 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 05:59 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 05:59 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 05:59 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 05:59 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 05:59 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 05:59 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 05:59 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 05:59 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 05:59 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 05:59 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 05:59 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 05:59 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 05:59 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 05:59 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 05:59 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/20/15 05:59 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 05:59 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 05:59 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 05:59 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 05:59 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 05:59 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 05:59 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 05:59 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 05:59 107-12-020.0 1
Styrene ND ug/L 11/20/15 05:59 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 05:59 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 05:59 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 05:59 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 05:59 109-99-910.0 1
Toluene ND ug/L 11/20/15 05:59 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 05:59 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 05:59 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 05:59 79-00-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW1 Lab ID:92276295001 Collected:11/16/15 10:10 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Trichloroethene ND ug/L 11/20/15 05:59 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 05:59 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 05:59 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 05:59 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 05:59 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 05:59 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 05:59 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 05:59 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %11/20/15 05:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/20/15 05:59 17060-07-070-130 1
Toluene-d8 (S)99 %11/20/15 05:59 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 35100 ug/L 11/24/15 20:0750001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 113000 ug/L 11/18/15 14:51250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/18/15 17:45 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 4460 ug/L 11/18/15 13:33 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 21600 ug/L 11/19/15 19:00 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/18/15 22:25 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW2 Lab ID:92276295002 Collected:11/16/15 11:25 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/16/15 11:251
Field pH 6.6 Std. Units 11/16/15 11:250.10 1
Field Temperature 11.9 deg C 11/16/15 11:250.50 1
Field Specific Conductance 88.6 umhos/cm 11/16/15 11:251.0 1
Oxygen, Dissolved 3.5 mg/L 11/16/15 11:25 7782-44-71
REDOX -84.6 mV 11/16/15 11:251
Turbidity 20.5 NTU 11/16/15 11:251.0 1
Odor none 11/16/15 11:251
Appearance murky 11/16/15 11:251
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/23/15 21:37 7440-36-011/18/15 20:305.0 1
Arsenic ND ug/L 11/23/15 21:37 7440-38-211/18/15 20:3010.0 1
Barium 70.0 ug/L 11/23/15 21:37 7440-39-311/18/15 20:305.0 1
Beryllium ND ug/L 11/23/15 21:37 7440-41-711/18/15 20:301.0 1
Cadmium ND ug/L 11/23/15 21:37 7440-43-911/18/15 20:301.0 1
Chromium ND ug/L 11/23/15 21:37 7440-47-311/18/15 20:305.0 1
Cobalt ND ug/L 11/23/15 21:37 7440-48-411/18/15 20:305.0 1
Copper ND ug/L 11/23/15 21:37 7440-50-811/18/15 20:305.0 1
Iron 2070 ug/L 11/23/15 21:37 7439-89-611/18/15 20:3050.0 1
Lead ND ug/L 11/23/15 21:37 7439-92-111/18/15 20:305.0 1
Manganese 291 ug/L 11/23/15 21:37 7439-96-511/18/15 20:305.0 1
Nickel ND ug/L 11/23/15 21:37 7440-02-011/18/15 20:305.0 1
Selenium ND ug/L 11/23/15 21:37 7782-49-211/18/15 20:3010.0 1
Silver ND ug/L 11/23/15 21:37 7440-22-411/18/15 20:305.0 1
Sodium 11300 ug/L 11/23/15 21:37 7440-23-511/18/15 20:3050001
Thallium ND ug/L 11/23/15 21:37 7440-28-011/18/15 20:305.4 1
Tin ND ug/L 11/23/15 21:37 7440-31-511/18/15 20:305.0 1
Vanadium ND ug/L 11/23/15 21:37 7440-62-211/18/15 20:305.0 1
Zinc ND ug/L 11/23/15 21:37 7440-66-611/18/15 20:3010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 13:33 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 06:16 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 06:16 75-05-850.0 1
Acrolein ND ug/L 11/20/15 06:16 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 06:16 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 06:16 107-05-12.0 1
Benzene ND ug/L 11/20/15 06:16 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 06:16 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 06:16 75-27-41.0 1
Bromoform ND ug/L 11/20/15 06:16 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 06:16 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 06:16 78-93-35.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW2 Lab ID:92276295002 Collected:11/16/15 11:25 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon disulfide ND ug/L 11/20/15 06:16 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 06:16 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 06:16 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 06:16 75-00-31.0 1
Chloroform ND ug/L 11/20/15 06:16 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 06:16 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 06:16 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 06:16 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 06:16 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 06:16 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 06:16 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 06:16 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 06:16 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 06:16 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 06:16 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 06:16 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 06:16 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 06:16 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 06:16 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 06:16 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 06:16 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 06:16 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 06:16 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 06:16 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 06:16 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 06:16 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 06:16 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 06:16 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 06:16 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/20/15 06:16 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 06:16 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 06:16 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 06:16 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 06:16 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 06:16 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 06:16 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 06:16 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 06:16 107-12-020.0 1
Styrene ND ug/L 11/20/15 06:16 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 06:16 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 06:16 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 06:16 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 06:16 109-99-910.0 1
Toluene ND ug/L 11/20/15 06:16 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 06:16 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 06:16 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 06:16 79-00-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW2 Lab ID:92276295002 Collected:11/16/15 11:25 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Trichloroethene ND ug/L 11/20/15 06:16 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 06:16 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 06:16 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 06:16 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 06:16 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 06:16 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 06:16 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 06:16 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/20/15 06:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/20/15 06:16 17060-07-070-130 1
Toluene-d8 (S)102 %11/20/15 06:16 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 43200 ug/L 11/24/15 21:08 M1,R150001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 105000 ug/L 11/18/15 14:51250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/18/15 17:45 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 11600 ug/L 11/18/15 14:14 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 12500 ug/L 11/19/15 19:01 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/18/15 22:26 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW3 Lab ID:92276295003 Collected:11/16/15 09:10 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/16/15 09:101
Field pH 6.4 Std. Units 11/16/15 09:100.10 1
Field Temperature 8.2 deg C 11/16/15 09:100.50 1
Field Specific Conductance 274.8 umhos/cm 11/16/15 09:101.0 1
Oxygen, Dissolved 3.2 mg/L 11/16/15 09:10 7782-44-71
REDOX -90.0 mV 11/16/15 09:101
Turbidity 9.1 NTU 11/16/15 09:101.0 1
Odor sulfurous 11/16/15 09:101
Appearance clear 11/16/15 09:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/23/15 21:41 7440-36-011/18/15 20:305.0 1
Arsenic ND ug/L 11/23/15 21:41 7440-38-211/18/15 20:3010.0 1
Barium 152 ug/L 11/23/15 21:41 7440-39-311/18/15 20:305.0 1
Beryllium ND ug/L 11/23/15 21:41 7440-41-711/18/15 20:301.0 1
Cadmium ND ug/L 11/23/15 21:41 7440-43-911/18/15 20:301.0 1
Chromium ND ug/L 11/23/15 21:41 7440-47-311/18/15 20:305.0 1
Cobalt ND ug/L 11/23/15 21:41 7440-48-411/18/15 20:305.0 1
Copper ND ug/L 11/23/15 21:41 7440-50-811/18/15 20:305.0 1
Iron 4160 ug/L 11/23/15 21:41 7439-89-611/18/15 20:3050.0 1
Lead ND ug/L 11/23/15 21:41 7439-92-111/18/15 20:305.0 1
Manganese 3860 ug/L 11/23/15 21:41 7439-96-511/18/15 20:305.0 1
Nickel 2.8J ug/L 11/23/15 21:41 7440-02-011/18/15 20:305.0 1
Selenium ND ug/L 11/23/15 21:41 7782-49-211/18/15 20:3010.0 1
Silver ND ug/L 11/23/15 21:41 7440-22-411/18/15 20:305.0 1
Sodium 20900 ug/L 11/23/15 21:41 7440-23-511/18/15 20:3050001
Thallium ND ug/L 11/23/15 21:41 7440-28-011/18/15 20:305.4 1
Tin ND ug/L 11/23/15 21:41 7440-31-511/18/15 20:305.0 1
Vanadium 5.6 ug/L 11/23/15 21:41 7440-62-211/18/15 20:305.0 1
Zinc ND ug/L 11/23/15 21:41 7440-66-611/18/15 20:3010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 13:36 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 06:33 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 06:33 75-05-850.0 1
Acrolein ND ug/L 11/20/15 06:33 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 06:33 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 06:33 107-05-12.0 1
Benzene ND ug/L 11/20/15 06:33 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 06:33 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 06:33 75-27-41.0 1
Bromoform ND ug/L 11/20/15 06:33 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 06:33 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 06:33 78-93-35.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW3 Lab ID:92276295003 Collected:11/16/15 09:10 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon disulfide ND ug/L 11/20/15 06:33 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 06:33 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 06:33 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 06:33 75-00-31.0 1
Chloroform ND ug/L 11/20/15 06:33 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 06:33 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 06:33 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 06:33 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 06:33 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 06:33 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 06:33 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 06:33 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 06:33 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 06:33 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 06:33 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 06:33 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 06:33 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 06:33 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 06:33 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 06:33 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 06:33 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 06:33 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 06:33 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 06:33 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 06:33 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 06:33 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 06:33 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 06:33 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 06:33 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/20/15 06:33 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 06:33 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 06:33 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 06:33 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 06:33 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 06:33 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 06:33 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 06:33 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 06:33 107-12-020.0 1
Styrene ND ug/L 11/20/15 06:33 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 06:33 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 06:33 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 06:33 127-18-41.0 1
Tetrahydrofuran 3.3J ug/L 11/20/15 06:33 109-99-910.0 1
Toluene ND ug/L 11/20/15 06:33 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 06:33 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 06:33 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 06:33 79-00-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW3 Lab ID:92276295003 Collected:11/16/15 09:10 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Trichloroethene ND ug/L 11/20/15 06:33 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 06:33 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 06:33 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 06:33 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 06:33 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 06:33 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 06:33 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 06:33 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %11/20/15 06:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %11/20/15 06:33 17060-07-070-130 1
Toluene-d8 (S)100 %11/20/15 06:33 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 210000 ug/L 11/24/15 21:3950001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 300000 ug/L 11/18/15 14:52250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/18/15 17:45 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 27000 ug/L 11/18/15 14:28 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 16300 ug/L 11/19/15 19:02 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/18/15 22:27 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW4 Lab ID:92276295004 Collected:11/16/15 09:35 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/16/15 09:351
Field pH 7.0 Std. Units 11/16/15 09:350.10 1
Field Temperature 9.0 deg C 11/16/15 09:350.50 1
Field Specific Conductance 247.9 umhos/cm 11/16/15 09:351.0 1
Oxygen, Dissolved 7.6 mg/L 11/16/15 09:35 7782-44-71
REDOX -87.1 mV 11/16/15 09:351
Turbidity 3.2 NTU 11/16/15 09:351.0 1
Odor none 11/16/15 09:351
Appearance clear 11/16/15 09:351
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/23/15 21:44 7440-36-011/18/15 20:305.0 1
Arsenic ND ug/L 11/23/15 21:44 7440-38-211/18/15 20:3010.0 1
Barium 115 ug/L 11/23/15 21:44 7440-39-311/18/15 20:305.0 1
Beryllium ND ug/L 11/23/15 21:44 7440-41-711/18/15 20:301.0 1
Cadmium ND ug/L 11/23/15 21:44 7440-43-911/18/15 20:301.0 1
Chromium ND ug/L 11/23/15 21:44 7440-47-311/18/15 20:305.0 1
Cobalt ND ug/L 11/23/15 21:44 7440-48-411/18/15 20:305.0 1
Copper ND ug/L 11/23/15 21:44 7440-50-811/18/15 20:305.0 1
Iron 2240 ug/L 11/23/15 21:44 7439-89-611/18/15 20:3050.0 1
Lead ND ug/L 11/23/15 21:44 7439-92-111/18/15 20:305.0 1
Manganese 2550 ug/L 11/23/15 21:44 7439-96-511/18/15 20:305.0 1
Nickel ND ug/L 11/23/15 21:44 7440-02-011/18/15 20:305.0 1
Selenium ND ug/L 11/23/15 21:44 7782-49-211/18/15 20:3010.0 1
Silver ND ug/L 11/23/15 21:44 7440-22-411/18/15 20:305.0 1
Sodium 20200 ug/L 11/23/15 21:44 7440-23-511/18/15 20:3050001
Thallium ND ug/L 11/23/15 21:44 7440-28-011/18/15 20:305.4 1
Tin ND ug/L 11/23/15 21:44 7440-31-511/18/15 20:305.0 1
Vanadium 3.5J ug/L 11/23/15 21:44 7440-62-211/18/15 20:305.0 1
Zinc ND ug/L 11/23/15 21:44 7440-66-611/18/15 20:3010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 13:38 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 06:50 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 06:50 75-05-850.0 1
Acrolein ND ug/L 11/20/15 06:50 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 06:50 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 06:50 107-05-12.0 1
Benzene ND ug/L 11/20/15 06:50 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 06:50 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 06:50 75-27-41.0 1
Bromoform ND ug/L 11/20/15 06:50 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 06:50 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 06:50 78-93-35.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW4 Lab ID:92276295004 Collected:11/16/15 09:35 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon disulfide ND ug/L 11/20/15 06:50 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 06:50 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 06:50 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 06:50 75-00-31.0 1
Chloroform ND ug/L 11/20/15 06:50 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 06:50 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 06:50 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 06:50 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 06:50 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 06:50 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 06:50 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 06:50 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 06:50 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 06:50 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 06:50 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 06:50 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 06:50 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 06:50 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 06:50 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 06:50 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 06:50 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 06:50 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 06:50 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 06:50 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 06:50 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 06:50 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 06:50 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 06:50 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 06:50 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/20/15 06:50 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 06:50 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 06:50 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 06:50 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 06:50 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 06:50 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 06:50 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 06:50 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 06:50 107-12-020.0 1
Styrene ND ug/L 11/20/15 06:50 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 06:50 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 06:50 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 06:50 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 06:50 109-99-910.0 1
Toluene ND ug/L 11/20/15 06:50 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 06:50 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 06:50 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 06:50 79-00-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-SW4 Lab ID:92276295004 Collected:11/16/15 09:35 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Trichloroethene ND ug/L 11/20/15 06:50 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 06:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 06:50 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 06:50 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 06:50 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 06:50 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 06:50 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 06:50 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/20/15 06:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/20/15 06:50 17060-07-070-130 1
Toluene-d8 (S)101 %11/20/15 06:50 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 187000 ug/L 11/24/15 21:5250001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 267000 ug/L 11/18/15 14:52250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/18/15 17:45 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 24900 ug/L 11/18/15 14:42 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 19800 ug/L 11/19/15 19:06 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/18/15 22:28 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW3R Lab ID:92276295005 Collected:11/16/15 15:30 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/16/15 15:201
Field pH 6.3 Std. Units 11/16/15 15:200.10 1
Field Temperature 15.2 deg C 11/16/15 15:200.50 1
Static Water Level 21.88 feet 11/16/15 15:201
Field Specific Conductance 211.4 umhos/cm 11/16/15 15:201.0 1
Oxygen, Dissolved 0.2 mg/L 11/16/15 15:20 7782-44-71
Total Well Depth 27 feet 11/16/15 15:201
REDOX -91.6 mV 11/16/15 15:201
Turbidity 3.0 NTU 11/16/15 15:201.0 1
Odor none 11/16/15 15:201
Appearance clear 11/16/15 15:201
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/20/15 21:26 309-00-211/19/15 14:090.050 1
alpha-BHC ND ug/L 11/20/15 21:26 319-84-611/19/15 14:090.050 1
beta-BHC ND ug/L 11/20/15 21:26 319-85-711/19/15 14:090.050 1
delta-BHC ND ug/L 11/20/15 21:26 319-86-811/19/15 14:090.050 1
gamma-BHC (Lindane)ND ug/L 11/20/15 21:26 58-89-911/19/15 14:090.050 1
Chlordane (Technical)ND ug/L 11/20/15 21:26 57-74-911/19/15 14:090.20 1
4,4'-DDD ND ug/L 11/20/15 21:26 72-54-811/19/15 14:090.050 1
4,4'-DDE ND ug/L 11/20/15 21:26 72-55-911/19/15 14:090.050 1
4,4'-DDT ND ug/L 11/20/15 21:26 50-29-311/19/15 14:090.050 1
Dieldrin ND ug/L 11/20/15 21:26 60-57-111/19/15 14:090.050 1
Endosulfan I ND ug/L 11/20/15 21:26 959-98-811/19/15 14:090.050 1
Endosulfan II ND ug/L 11/20/15 21:26 33213-65-911/19/15 14:090.050 1
Endosulfan sulfate ND ug/L 11/20/15 21:26 1031-07-811/19/15 14:090.050 1
Endrin ND ug/L 11/20/15 21:26 72-20-811/19/15 14:090.050 1
Endrin aldehyde ND ug/L 11/20/15 21:26 7421-93-411/19/15 14:090.050 1
Heptachlor ND ug/L 11/20/15 21:26 76-44-811/19/15 14:090.050 1
Heptachlor epoxide ND ug/L 11/20/15 21:26 1024-57-311/19/15 14:090.050 1
Methoxychlor ND ug/L 11/20/15 21:26 72-43-511/19/15 14:090.15 1
Toxaphene ND ug/L 11/20/15 21:26 8001-35-211/19/15 14:090.20 1
Surrogates
Tetrachloro-m-xylene (S)71 %11/20/15 21:26 877-09-811/19/15 14:0920-130 1
Decachlorobiphenyl (S)78 %11/20/15 21:26 2051-24-311/19/15 14:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/20/15 17:36 12674-11-211/19/15 14:090.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/20/15 17:36 11104-28-211/19/15 14:090.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/20/15 17:36 11141-16-511/19/15 14:090.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/20/15 17:36 53469-21-911/19/15 14:090.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/20/15 17:36 12672-29-611/19/15 14:090.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/20/15 17:36 11097-69-111/19/15 14:090.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/20/15 17:36 11096-82-511/19/15 14:090.50 1
Surrogates
Decachlorobiphenyl (S)83 %11/20/15 17:36 2051-24-311/19/15 14:0910-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW3R Lab ID:92276295005 Collected:11/16/15 15:30 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/23/15 21:47 7440-36-011/18/15 20:305.0 1
Arsenic ND ug/L 11/23/15 21:47 7440-38-211/18/15 20:3010.0 1
Barium 271 ug/L 11/23/15 21:47 7440-39-311/18/15 20:305.0 1
Beryllium ND ug/L 11/23/15 21:47 7440-41-711/18/15 20:301.0 1
Cadmium ND ug/L 11/23/15 21:47 7440-43-911/18/15 20:301.0 1
Chromium ND ug/L 11/23/15 21:47 7440-47-311/18/15 20:305.0 1
Cobalt 9.1 ug/L 11/23/15 21:47 7440-48-411/18/15 20:305.0 1
Copper 6.2 ug/L 11/23/15 21:47 7440-50-811/18/15 20:305.0 1
Iron 68200 ug/L 11/23/15 21:47 7439-89-611/18/15 20:3050.0 1
Lead 3.8J ug/L 11/23/15 21:47 7439-92-111/18/15 20:305.0 1
Manganese 7100 ug/L 11/23/15 21:47 7439-96-511/18/15 20:305.0 1
Nickel ND ug/L 11/23/15 21:47 7440-02-011/18/15 20:305.0 1
Selenium ND ug/L 11/23/15 21:47 7782-49-211/18/15 20:3010.0 1
Silver ND ug/L 11/23/15 21:47 7440-22-411/18/15 20:305.0 1
Sodium 2590J ug/L 11/23/15 21:47 7440-23-511/18/15 20:3050001
Thallium ND ug/L 11/23/15 21:47 7440-28-011/18/15 20:305.4 1
Tin ND ug/L 11/23/15 21:47 7440-31-511/18/15 20:305.0 1
Vanadium 9.9 ug/L 11/23/15 21:47 7440-62-211/18/15 20:305.0 1
Zinc 8.7J ug/L 11/23/15 21:47 7440-66-611/18/15 20:3010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 13:41 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 11/23/15 17:59 83-32-911/17/15 13:4010.0 1
Acenaphthylene ND ug/L 11/23/15 17:59 208-96-811/17/15 13:4010.0 1
Acetophenone ND ug/L 11/23/15 17:59 98-86-211/17/15 13:4010.0 1
2-Acetylaminofluorene ND ug/L 11/23/15 17:59 53-96-311/17/15 13:4020.0 1
4-Aminobiphenyl ND ug/L 11/23/15 17:59 92-67-111/17/15 13:4010.0 1
Anthracene ND ug/L 11/23/15 17:59 120-12-711/17/15 13:4010.0 1
Benzo(a)anthracene ND ug/L 11/23/15 17:59 56-55-311/17/15 13:4010.0 1
Benzo(a)pyrene ND ug/L 11/23/15 17:59 50-32-811/17/15 13:4010.0 1
Benzo(b)fluoranthene ND ug/L 11/23/15 17:59 205-99-211/17/15 13:4010.0 1
Benzo(g,h,i)perylene 1.0J ug/L 11/23/15 17:59 191-24-211/17/15 13:4010.0 1
Benzo(k)fluoranthene ND ug/L 11/23/15 17:59 207-08-911/17/15 13:4010.0 1
Benzyl alcohol ND ug/L 11/23/15 17:59 100-51-611/17/15 13:4020.0 1
4-Bromophenylphenyl ether ND ug/L 11/23/15 17:59 101-55-311/17/15 13:4010.0 1
Butylbenzylphthalate ND ug/L 11/23/15 17:59 85-68-711/17/15 13:4010.0 1
4-Chloro-3-methylphenol ND ug/L 11/23/15 17:59 59-50-711/17/15 13:4020.0 1
4-Chloroaniline ND ug/L 11/23/15 17:59 106-47-811/17/15 13:4020.0 1
Chlorobenzilate ND ug/L 11/23/15 17:59 510-15-611/17/15 13:4010.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/23/15 17:59 111-91-111/17/15 13:4010.0 1
bis(2-Chloroethyl) ether ND ug/L 11/23/15 17:59 111-44-411/17/15 13:4010.0 1
bis(2-Chloroisopropyl) ether ND ug/L 11/23/15 17:59 108-60-111/17/15 13:4010.0 1
2-Chloronaphthalene ND ug/L 11/23/15 17:59 91-58-711/17/15 13:4010.0 1
2-Chlorophenol ND ug/L 11/23/15 17:59 95-57-811/17/15 13:4010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW3R Lab ID:92276295005 Collected:11/16/15 15:30 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 11/23/15 17:59 7005-72-311/17/15 13:4010.0 1
Chrysene ND ug/L 11/23/15 17:59 218-01-911/17/15 13:4010.0 1
Diallate ND ug/L 11/23/15 17:59 2303-16-411/17/15 13:4010.0 1
Dibenz(a,h)anthracene 1.0J ug/L 11/23/15 17:59 53-70-311/17/15 13:4010.0 1
Dibenzofuran ND ug/L 11/23/15 17:59 132-64-911/17/15 13:4010.0 1
3,3'-Dichlorobenzidine ND ug/L 11/23/15 17:59 91-94-111/17/15 13:4020.0 1
2,4-Dichlorophenol ND ug/L 11/23/15 17:59 120-83-211/17/15 13:4010.0 1
2,6-Dichlorophenol ND ug/L 11/23/15 17:59 87-65-011/17/15 13:4010.0 1
Diethylphthalate ND ug/L 11/23/15 17:59 84-66-211/17/15 13:4010.0 1
Dimethoate ND ug/L 11/23/15 17:59 60-51-511/17/15 13:4010.0 1
P-Dimethylaminoazobenzene ND ug/L 11/23/15 17:59 60-11-711/17/15 13:405.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 11/23/15 17:59 57-97-611/17/15 13:4010.0 1
3,3'-Dimethylbenzidine ND ug/L 11/23/15 17:59 119-93-711/17/15 13:4010.0 1
2,4-Dimethylphenol ND ug/L 11/23/15 17:59 105-67-911/17/15 13:4010.0 1
Dimethylphthalate ND ug/L 11/23/15 17:59 131-11-311/17/15 13:4010.0 1
Di-n-butylphthalate ND ug/L 11/23/15 17:59 84-74-211/17/15 13:4010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/23/15 17:59 534-52-111/17/15 13:4020.0 1
1,3-Dinitrobenzene ND ug/L 11/23/15 17:59 99-65-011/17/15 13:4020.0 1
2,4-Dinitrophenol ND ug/L 11/23/15 17:59 51-28-511/17/15 13:4050.0 1
2,4-Dinitrotoluene ND ug/L 11/23/15 17:59 121-14-211/17/15 13:4010.0 1
2,6-Dinitrotoluene ND ug/L 11/23/15 17:59 606-20-211/17/15 13:4010.0 1
Di-n-octylphthalate ND ug/L 11/23/15 17:59 117-84-011/17/15 13:4010.0 1
Diphenylamine ND ug/L 11/23/15 17:59 122-39-411/17/15 13:4010.0 1
Disulfoton ND ug/L 11/23/15 17:59 298-04-411/17/15 13:4010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/23/15 17:59 117-81-711/17/15 13:406.0 1
Ethyl methanesulfonate ND ug/L 11/23/15 17:59 62-50-011/17/15 13:4020.0 1
Famphur ND ug/L 11/23/15 17:59 52-85-711/17/15 13:4010.0 1
Fluoranthene ND ug/L 11/23/15 17:59 206-44-011/17/15 13:4010.0 1
Fluorene ND ug/L 11/23/15 17:59 86-73-711/17/15 13:4010.0 1
Hexachlorobenzene ND ug/L 11/23/15 17:59 118-74-111/17/15 13:4010.0 1
Hexachlorocyclopentadiene ND ug/L 11/23/15 17:59 77-47-411/17/15 13:4010.0 1
Hexachloroethane ND ug/L 11/23/15 17:59 67-72-111/17/15 13:4010.0 1
Hexachlorophene ND ug/L 11/23/15 17:59 70-30-411/17/15 13:401001
Indeno(1,2,3-cd)pyrene 1.1J ug/L 11/23/15 17:59 193-39-511/17/15 13:4010.0 1
Isodrin ND ug/L 11/23/15 17:59 465-73-611/17/15 13:4020.0 1
Isophorone ND ug/L 11/23/15 17:59 78-59-111/17/15 13:4010.0 1
Isosafrole ND ug/L 11/23/15 17:59 120-58-111/17/15 13:4010.0 1
Kepone ND ug/L 11/23/15 17:59 143-50-011/17/15 13:4010.0 1
Methapyrilene ND ug/L 11/23/15 17:59 91-80-511/17/15 13:4050.0 1
3-Methylcholanthrene ND ug/L 11/23/15 17:59 56-49-511/17/15 13:4010.0 1
Methyl methanesulfonate ND ug/L 11/23/15 17:59 66-27-311/17/15 13:405.0 1
2-Methylnaphthalene ND ug/L 11/23/15 17:59 91-57-611/17/15 13:4010.0 1
Methyl parathion ND ug/L 11/23/15 17:59 298-00-011/17/15 13:4010.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/23/15 17:59 95-48-711/17/15 13:4010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/23/15 17:5911/17/15 13:4010.0 1
1-Naphthalenamine ND ug/L 11/23/15 17:59 134-32-711/17/15 13:405.0 1
2-Naphthalenamine ND ug/L 11/23/15 17:59 91-59-811/17/15 13:405.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
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Page 24 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW3R Lab ID:92276295005 Collected:11/16/15 15:30 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1,4-Naphthoquinone ND ug/L 11/23/15 17:59 130-15-411/17/15 13:405.0 1
2-Nitroaniline ND ug/L 11/23/15 17:59 88-74-411/17/15 13:4050.0 1
3-Nitroaniline ND ug/L 11/23/15 17:59 99-09-211/17/15 13:4050.0 1
4-Nitroaniline ND ug/L 11/23/15 17:59 100-01-611/17/15 13:4020.0 1
Nitrobenzene ND ug/L 11/23/15 17:59 98-95-311/17/15 13:4010.0 1
2-Nitrophenol ND ug/L 11/23/15 17:59 88-75-511/17/15 13:4010.0 1
4-Nitrophenol ND ug/L 11/23/15 17:59 100-02-711/17/15 13:4050.0 1
5-Nitro-o-toluidine ND ug/L 11/23/15 17:59 99-55-811/17/15 13:4010.0 1
N-Nitrosodiethylamine ND ug/L 11/23/15 17:59 55-18-511/17/15 13:4020.0 1
N-Nitrosodimethylamine ND ug/L 11/23/15 17:59 62-75-911/17/15 13:4010.0 1
N-Nitroso-di-n-butylamine ND ug/L 11/23/15 17:59 924-16-311/17/15 13:4010.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/23/15 17:59 621-64-711/17/15 13:4010.0 1
N-Nitrosodiphenylamine ND ug/L 11/23/15 17:59 86-30-611/17/15 13:4010.0 1
N-Nitrosomethylethylamine ND ug/L 11/23/15 17:59 10595-95-611/17/15 13:4010.0 1
N-Nitrosopiperidine ND ug/L 11/23/15 17:59 100-75-411/17/15 13:4020.0 1
N-Nitrosopyrrolidine ND ug/L 11/23/15 17:59 930-55-211/17/15 13:4010.0 1
O,O,O-Triethylphosphorothioate ND ug/L 11/23/15 17:59 126-68-111/17/15 13:4010.0 1
Parathion (Ethyl parathion)ND ug/L 11/23/15 17:59 56-38-211/17/15 13:4010.0 1
Pentachlorobenzene ND ug/L 11/23/15 17:59 608-93-511/17/15 13:4010.0 1
Pentachloronitrobenzene ND ug/L 11/23/15 17:59 82-68-811/17/15 13:4020.0 1
Pentachlorophenol ND ug/L 11/23/15 17:59 87-86-511/17/15 13:4025.0 1
Phenacetin ND ug/L 11/23/15 17:59 62-44-211/17/15 13:4020.0 1
Phenanthrene ND ug/L 11/23/15 17:59 85-01-811/17/15 13:4010.0 1
Phenol ND ug/L 11/23/15 17:59 108-95-211/17/15 13:4010.0 1
p-Phenylenediamine ND ug/L 11/23/15 17:59 106-50-311/17/15 13:4010.0 1
Phorate ND ug/L 11/23/15 17:59 298-02-2 L311/17/15 13:4010.0 1
Pronamide ND ug/L 11/23/15 17:59 23950-58-511/17/15 13:4010.0 1
Pyrene ND ug/L 11/23/15 17:59 129-00-011/17/15 13:4010.0 1
Safrole ND ug/L 11/23/15 17:59 94-59-711/17/15 13:4010.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 11/23/15 17:59 95-94-311/17/15 13:4010.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 11/23/15 17:59 58-90-211/17/15 13:4010.0 1
Thionazin ND ug/L 11/23/15 17:59 297-97-211/17/15 13:4020.0 1
O-Toluidine ND ug/L 11/23/15 17:59 95-53-411/17/15 13:4010.0 1
2,4,5-Trichlorophenol ND ug/L 11/23/15 17:59 95-95-411/17/15 13:4010.0 1
2,4,6-Trichlorophenol ND ug/L 11/23/15 17:59 88-06-211/17/15 13:4010.0 1
1,3,5-Trinitrobenzene ND ug/L 11/23/15 17:59 99-35-4 L311/17/15 13:4010.0 1
Surrogates
Nitrobenzene-d5 (S)72 %11/23/15 17:59 4165-60-011/17/15 13:4021-110 1
2-Fluorobiphenyl (S)78 %11/23/15 17:59 321-60-811/17/15 13:4027-110 1
Terphenyl-d14 (S)77 %11/23/15 17:59 1718-51-011/17/15 13:4031-107 1
Phenol-d6 (S)21 %11/23/15 17:59 13127-88-311/17/15 13:4010-110 1
2-Fluorophenol (S)34 %11/23/15 17:59 367-12-411/17/15 13:4012-110 1
2,4,6-Tribromophenol (S)78 %11/23/15 17:59 118-79-611/17/15 13:4027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 07:08 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 07:08 75-05-850.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Huntersville, NC 28078
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Page 25 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW3R Lab ID:92276295005 Collected:11/16/15 15:30 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrolein ND ug/L 11/20/15 07:08 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 07:08 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 07:08 107-05-12.0 1
Benzene ND ug/L 11/20/15 07:08 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 07:08 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 07:08 75-27-41.0 1
Bromoform ND ug/L 11/20/15 07:08 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 07:08 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 07:08 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 07:08 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 07:08 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 07:08 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 07:08 75-00-31.0 1
Chloroform ND ug/L 11/20/15 07:08 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 07:08 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 07:08 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 07:08 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 07:08 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 07:08 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 07:08 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 07:08 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 07:08 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 07:08 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 07:08 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 07:08 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 07:08 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 07:08 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 07:08 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 07:08 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 07:08 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 07:08 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 07:08 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 07:08 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 07:08 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 07:08 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 07:08 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 07:08 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 07:08 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/20/15 07:08 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 07:08 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 07:08 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 07:08 126-98-710.0 1
Methylene Chloride 2.3 ug/L 11/20/15 07:08 75-09-2 C91.0 1
Methyl methacrylate ND ug/L 11/20/15 07:08 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 07:08 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 07:08 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 07:08 107-12-020.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW3R Lab ID:92276295005 Collected:11/16/15 15:30 Received:11/16/15 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Styrene ND ug/L 11/20/15 07:08 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 07:08 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 07:08 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 07:08 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 07:08 109-99-910.0 1
Toluene ND ug/L 11/20/15 07:08 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 07:08 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 07:08 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 07:08 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 07:08 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 07:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 07:08 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 07:08 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 07:08 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 07:08 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 07:08 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 07:08 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %11/20/15 07:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/20/15 07:08 17060-07-070-130 1
Toluene-d8 (S)101 %11/20/15 07:08 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 102000 ug/L 11/24/15 22:0450001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 137000 ug/L 11/18/15 14:52250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/18/15 17:45 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2200 ug/L 11/18/15 14:55 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 2990 ug/L 11/19/15 19:07 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/18/15 22:30 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-EQUIPMENT BLANK Lab ID:92276295006 Collected:11/17/15 08:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/20/15 21:44 309-00-211/19/15 14:090.050 1
alpha-BHC ND ug/L 11/20/15 21:44 319-84-611/19/15 14:090.050 1
beta-BHC ND ug/L 11/20/15 21:44 319-85-711/19/15 14:090.050 1
delta-BHC ND ug/L 11/20/15 21:44 319-86-811/19/15 14:090.050 1
gamma-BHC (Lindane)ND ug/L 11/20/15 21:44 58-89-911/19/15 14:090.050 1
Chlordane (Technical)ND ug/L 11/20/15 21:44 57-74-911/19/15 14:090.20 1
4,4'-DDD ND ug/L 11/20/15 21:44 72-54-811/19/15 14:090.050 1
4,4'-DDE ND ug/L 11/20/15 21:44 72-55-911/19/15 14:090.050 1
4,4'-DDT ND ug/L 11/20/15 21:44 50-29-311/19/15 14:090.050 1
Dieldrin ND ug/L 11/20/15 21:44 60-57-111/19/15 14:090.050 1
Endosulfan I ND ug/L 11/20/15 21:44 959-98-811/19/15 14:090.050 1
Endosulfan II ND ug/L 11/20/15 21:44 33213-65-911/19/15 14:090.050 1
Endosulfan sulfate ND ug/L 11/20/15 21:44 1031-07-811/19/15 14:090.050 1
Endrin ND ug/L 11/20/15 21:44 72-20-811/19/15 14:090.050 1
Endrin aldehyde ND ug/L 11/20/15 21:44 7421-93-411/19/15 14:090.050 1
Heptachlor ND ug/L 11/20/15 21:44 76-44-811/19/15 14:090.050 1
Heptachlor epoxide ND ug/L 11/20/15 21:44 1024-57-311/19/15 14:090.050 1
Methoxychlor ND ug/L 11/20/15 21:44 72-43-511/19/15 14:090.15 1
Toxaphene ND ug/L 11/20/15 21:44 8001-35-211/19/15 14:090.20 1
Surrogates
Tetrachloro-m-xylene (S)89 %11/20/15 21:44 877-09-811/19/15 14:0920-130 1
Decachlorobiphenyl (S)53 %11/20/15 21:44 2051-24-311/19/15 14:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/20/15 17:56 12674-11-211/19/15 14:090.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/20/15 17:56 11104-28-211/19/15 14:090.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/20/15 17:56 11141-16-511/19/15 14:090.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/20/15 17:56 53469-21-911/19/15 14:090.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/20/15 17:56 12672-29-611/19/15 14:090.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/20/15 17:56 11097-69-111/19/15 14:090.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/20/15 17:56 11096-82-511/19/15 14:090.50 1
Surrogates
Decachlorobiphenyl (S)53 %11/20/15 17:56 2051-24-311/19/15 14:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/24/15 20:01 94-75-711/23/15 16:350.94 1
Dinoseb ND ug/L 11/24/15 20:01 88-85-711/23/15 16:350.19 1
2,4,5-T ND ug/L 11/24/15 20:01 93-76-511/23/15 16:350.19 1
2,4,5-TP (Silvex)ND ug/L 11/24/15 20:01 93-72-111/23/15 16:350.19 1
Surrogates
2,4-DCAA (S)97 %11/24/15 20:01 19719-28-911/23/15 16:3536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/24/15 08:40 7440-36-011/20/15 18:005.0 1
Arsenic ND ug/L 11/24/15 08:40 7440-38-211/20/15 18:0010.0 1
Barium ND ug/L 11/24/15 08:40 7440-39-311/20/15 18:005.0 1
Beryllium ND ug/L 11/24/15 08:40 7440-41-711/20/15 18:001.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-EQUIPMENT BLANK Lab ID:92276295006 Collected:11/17/15 08:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Cadmium ND ug/L 11/24/15 08:40 7440-43-911/20/15 18:001.0 1
Chromium ND ug/L 11/24/15 08:40 7440-47-311/20/15 18:005.0 1
Cobalt ND ug/L 11/24/15 08:40 7440-48-411/20/15 18:005.0 1
Copper ND ug/L 11/24/15 08:40 7440-50-811/20/15 18:005.0 1
Iron ND ug/L 11/24/15 08:40 7439-89-611/20/15 18:0050.0 1
Lead ND ug/L 11/24/15 08:40 7439-92-111/20/15 18:005.0 1
Manganese ND ug/L 11/24/15 08:40 7439-96-511/20/15 18:005.0 1
Nickel ND ug/L 11/24/15 08:40 7440-02-011/20/15 18:005.0 1
Selenium ND ug/L 11/24/15 08:40 7782-49-211/20/15 18:0010.0 1
Silver ND ug/L 11/24/15 08:40 7440-22-411/20/15 18:005.0 1
Sodium ND ug/L 11/24/15 08:40 7440-23-511/20/15 18:0050001
Thallium ND ug/L 11/24/15 08:40 7440-28-011/20/15 18:005.4 1
Tin ND ug/L 11/24/15 08:40 7440-31-511/20/15 18:005.0 1
Vanadium ND ug/L 11/24/15 08:40 7440-62-211/20/15 18:005.0 1
Zinc ND ug/L 11/24/15 08:40 7440-66-611/20/15 18:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 14:04 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 11/30/15 18:29 83-32-911/20/15 19:3210.0 1
Acenaphthylene ND ug/L 11/30/15 18:29 208-96-811/20/15 19:3210.0 1
Acetophenone ND ug/L 11/30/15 18:29 98-86-211/20/15 19:3210.0 1
2-Acetylaminofluorene ND ug/L 11/30/15 18:29 53-96-311/20/15 19:3220.0 1
4-Aminobiphenyl ND ug/L 11/30/15 18:29 92-67-111/20/15 19:3210.0 1
Anthracene ND ug/L 11/30/15 18:29 120-12-711/20/15 19:3210.0 1
Benzo(a)anthracene ND ug/L 11/30/15 18:29 56-55-311/20/15 19:3210.0 1
Benzo(a)pyrene ND ug/L 11/30/15 18:29 50-32-811/20/15 19:3210.0 1
Benzo(b)fluoranthene ND ug/L 11/30/15 18:29 205-99-211/20/15 19:3210.0 1
Benzo(g,h,i)perylene ND ug/L 11/30/15 18:29 191-24-211/20/15 19:3210.0 1
Benzo(k)fluoranthene ND ug/L 11/30/15 18:29 207-08-911/20/15 19:3210.0 1
Benzyl alcohol ND ug/L 11/30/15 18:29 100-51-611/20/15 19:3220.0 1
4-Bromophenylphenyl ether ND ug/L 11/30/15 18:29 101-55-311/20/15 19:3210.0 1
Butylbenzylphthalate ND ug/L 11/30/15 18:29 85-68-711/20/15 19:3210.0 1
4-Chloro-3-methylphenol ND ug/L 11/30/15 18:29 59-50-711/20/15 19:3220.0 1
4-Chloroaniline ND ug/L 11/30/15 18:29 106-47-811/20/15 19:3220.0 1
Chlorobenzilate ND ug/L 11/30/15 18:29 510-15-611/20/15 19:3210.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/30/15 18:29 111-91-111/20/15 19:3210.0 1
bis(2-Chloroethyl) ether ND ug/L 11/30/15 18:29 111-44-411/20/15 19:3210.0 1
bis(2-Chloroisopropyl) ether ND ug/L 11/30/15 18:29 108-60-111/20/15 19:3210.0 1
2-Chloronaphthalene ND ug/L 11/30/15 18:29 91-58-711/20/15 19:3210.0 1
2-Chlorophenol ND ug/L 11/30/15 18:29 95-57-811/20/15 19:3210.0 1
4-Chlorophenylphenyl ether ND ug/L 11/30/15 18:29 7005-72-311/20/15 19:3210.0 1
Chrysene ND ug/L 11/30/15 18:29 218-01-911/20/15 19:3210.0 1
Diallate ND ug/L 11/30/15 18:29 2303-16-411/20/15 19:3210.0 1
Dibenz(a,h)anthracene ND ug/L 11/30/15 18:29 53-70-311/20/15 19:3210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-EQUIPMENT BLANK Lab ID:92276295006 Collected:11/17/15 08:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 11/30/15 18:29 132-64-911/20/15 19:3210.0 1
3,3'-Dichlorobenzidine ND ug/L 11/30/15 18:29 91-94-111/20/15 19:3220.0 1
2,4-Dichlorophenol ND ug/L 11/30/15 18:29 120-83-211/20/15 19:3210.0 1
2,6-Dichlorophenol ND ug/L 11/30/15 18:29 87-65-011/20/15 19:3210.0 1
Diethylphthalate ND ug/L 11/30/15 18:29 84-66-211/20/15 19:3210.0 1
Dimethoate ND ug/L 11/30/15 18:29 60-51-511/20/15 19:3210.0 1
P-Dimethylaminoazobenzene ND ug/L 11/30/15 18:29 60-11-711/20/15 19:325.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 11/30/15 18:29 57-97-611/20/15 19:3210.0 1
3,3'-Dimethylbenzidine ND ug/L 11/30/15 18:29 119-93-711/20/15 19:3210.0 1
2,4-Dimethylphenol ND ug/L 11/30/15 18:29 105-67-911/20/15 19:3210.0 1
Dimethylphthalate ND ug/L 11/30/15 18:29 131-11-311/20/15 19:3210.0 1
Di-n-butylphthalate ND ug/L 11/30/15 18:29 84-74-211/20/15 19:3210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/30/15 18:29 534-52-111/20/15 19:3220.0 1
1,3-Dinitrobenzene ND ug/L 11/30/15 18:29 99-65-011/20/15 19:3220.0 1
2,4-Dinitrophenol ND ug/L 11/30/15 18:29 51-28-511/20/15 19:3250.0 1
2,4-Dinitrotoluene ND ug/L 11/30/15 18:29 121-14-211/20/15 19:3210.0 1
2,6-Dinitrotoluene ND ug/L 11/30/15 18:29 606-20-211/20/15 19:3210.0 1
Di-n-octylphthalate ND ug/L 11/30/15 18:29 117-84-011/20/15 19:3210.0 1
Diphenylamine ND ug/L 11/30/15 18:29 122-39-411/20/15 19:3210.0 1
Disulfoton ND ug/L 11/30/15 18:29 298-04-411/20/15 19:3210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/30/15 18:29 117-81-711/20/15 19:326.0 1
Ethyl methanesulfonate ND ug/L 11/30/15 18:29 62-50-011/20/15 19:3220.0 1
Famphur ND ug/L 11/30/15 18:29 52-85-711/20/15 19:3210.0 1
Fluoranthene ND ug/L 11/30/15 18:29 206-44-011/20/15 19:3210.0 1
Fluorene ND ug/L 11/30/15 18:29 86-73-711/20/15 19:3210.0 1
Hexachlorobenzene ND ug/L 11/30/15 18:29 118-74-111/20/15 19:3210.0 1
Hexachlorocyclopentadiene ND ug/L 11/30/15 18:29 77-47-411/20/15 19:3210.0 1
Hexachloroethane ND ug/L 11/30/15 18:29 67-72-111/20/15 19:3210.0 1
Hexachlorophene ND ug/L 11/30/15 18:29 70-30-411/20/15 19:321001
Indeno(1,2,3-cd)pyrene ND ug/L 11/30/15 18:29 193-39-511/20/15 19:3210.0 1
Isodrin ND ug/L 11/30/15 18:29 465-73-611/20/15 19:3220.0 1
Isophorone ND ug/L 11/30/15 18:29 78-59-111/20/15 19:3210.0 1
Isosafrole ND ug/L 11/30/15 18:29 120-58-111/20/15 19:3210.0 1
Kepone ND ug/L 11/30/15 18:29 143-50-011/20/15 19:3210.0 1
Methapyrilene ND ug/L 11/30/15 18:29 91-80-511/20/15 19:3250.0 1
3-Methylcholanthrene ND ug/L 11/30/15 18:29 56-49-511/20/15 19:3210.0 1
Methyl methanesulfonate ND ug/L 11/30/15 18:29 66-27-311/20/15 19:325.0 1
2-Methylnaphthalene ND ug/L 11/30/15 18:29 91-57-611/20/15 19:3210.0 1
Methyl parathion ND ug/L 11/30/15 18:29 298-00-011/20/15 19:3210.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/30/15 18:29 95-48-711/20/15 19:3210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/30/15 18:2911/20/15 19:3210.0 1
1-Naphthalenamine ND ug/L 11/30/15 18:29 134-32-711/20/15 19:325.0 1
2-Naphthalenamine ND ug/L 11/30/15 18:29 91-59-811/20/15 19:325.0 1
1,4-Naphthoquinone ND ug/L 11/30/15 18:29 130-15-411/20/15 19:325.0 1
2-Nitroaniline ND ug/L 11/30/15 18:29 88-74-411/20/15 19:3250.0 1
3-Nitroaniline ND ug/L 11/30/15 18:29 99-09-211/20/15 19:3250.0 1
4-Nitroaniline ND ug/L 11/30/15 18:29 100-01-611/20/15 19:3220.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-EQUIPMENT BLANK Lab ID:92276295006 Collected:11/17/15 08:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Nitrobenzene ND ug/L 11/30/15 18:29 98-95-311/20/15 19:3210.0 1
2-Nitrophenol ND ug/L 11/30/15 18:29 88-75-511/20/15 19:3210.0 1
4-Nitrophenol ND ug/L 11/30/15 18:29 100-02-711/20/15 19:3250.0 1
5-Nitro-o-toluidine ND ug/L 11/30/15 18:29 99-55-811/20/15 19:3210.0 1
N-Nitrosodiethylamine ND ug/L 11/30/15 18:29 55-18-511/20/15 19:3220.0 1
N-Nitrosodimethylamine ND ug/L 11/30/15 18:29 62-75-911/20/15 19:3210.0 1
N-Nitroso-di-n-butylamine ND ug/L 11/30/15 18:29 924-16-311/20/15 19:3210.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/30/15 18:29 621-64-711/20/15 19:3210.0 1
N-Nitrosodiphenylamine ND ug/L 11/30/15 18:29 86-30-611/20/15 19:3210.0 1
N-Nitrosomethylethylamine ND ug/L 11/30/15 18:29 10595-95-611/20/15 19:3210.0 1
N-Nitrosopiperidine ND ug/L 11/30/15 18:29 100-75-411/20/15 19:3220.0 1
N-Nitrosopyrrolidine ND ug/L 11/30/15 18:29 930-55-211/20/15 19:3210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 11/30/15 18:29 126-68-111/20/15 19:3210.0 1
Parathion (Ethyl parathion)ND ug/L 11/30/15 18:29 56-38-211/20/15 19:3210.0 1
Pentachlorobenzene ND ug/L 11/30/15 18:29 608-93-511/20/15 19:3210.0 1
Pentachloronitrobenzene ND ug/L 11/30/15 18:29 82-68-811/20/15 19:3220.0 1
Pentachlorophenol ND ug/L 11/30/15 18:29 87-86-511/20/15 19:3225.0 1
Phenacetin ND ug/L 11/30/15 18:29 62-44-211/20/15 19:3220.0 1
Phenanthrene ND ug/L 11/30/15 18:29 85-01-811/20/15 19:3210.0 1
Phenol ND ug/L 11/30/15 18:29 108-95-211/20/15 19:3210.0 1
p-Phenylenediamine ND ug/L 11/30/15 18:29 106-50-311/20/15 19:3210.0 1
Phorate ND ug/L 11/30/15 18:29 298-02-211/20/15 19:3210.0 1
Pronamide ND ug/L 11/30/15 18:29 23950-58-511/20/15 19:3210.0 1
Pyrene ND ug/L 11/30/15 18:29 129-00-011/20/15 19:3210.0 1
Safrole ND ug/L 11/30/15 18:29 94-59-711/20/15 19:3210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 11/30/15 18:29 95-94-311/20/15 19:3210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 11/30/15 18:29 58-90-211/20/15 19:3210.0 1
Thionazin ND ug/L 11/30/15 18:29 297-97-211/20/15 19:3220.0 1
O-Toluidine ND ug/L 11/30/15 18:29 95-53-411/20/15 19:3210.0 1
2,4,5-Trichlorophenol ND ug/L 11/30/15 18:29 95-95-411/20/15 19:3210.0 1
2,4,6-Trichlorophenol ND ug/L 11/30/15 18:29 88-06-211/20/15 19:3210.0 1
1,3,5-Trinitrobenzene ND ug/L 11/30/15 18:29 99-35-411/20/15 19:3210.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 07:59 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 07:59 75-05-850.0 1
Acrolein ND ug/L 11/20/15 07:59 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 07:59 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 07:59 107-05-12.0 1
Benzene ND ug/L 11/20/15 07:59 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 07:59 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 07:59 75-27-41.0 1
Bromoform ND ug/L 11/20/15 07:59 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 07:59 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 07:59 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 07:59 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 07:59 56-23-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-EQUIPMENT BLANK Lab ID:92276295006 Collected:11/17/15 08:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Chlorobenzene ND ug/L 11/20/15 07:59 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 07:59 75-00-31.0 1
Chloroform ND ug/L 11/20/15 07:59 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 07:59 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 07:59 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 07:59 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 07:59 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 07:59 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 07:59 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 07:59 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 07:59 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 07:59 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 07:59 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 07:59 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 07:59 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 07:59 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 07:59 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 07:59 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 07:59 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 07:59 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 07:59 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 07:59 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 07:59 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 07:59 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 07:59 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 07:59 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 07:59 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/20/15 07:59 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 07:59 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 07:59 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 07:59 126-98-710.0 1
Methylene Chloride 1.1 ug/L 11/20/15 07:59 75-09-2 C91.0 1
Methyl methacrylate ND ug/L 11/20/15 07:59 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 07:59 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 07:59 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 07:59 107-12-020.0 1
Styrene ND ug/L 11/20/15 07:59 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 07:59 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 07:59 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 07:59 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 07:59 109-99-910.0 1
Toluene ND ug/L 11/20/15 07:59 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 07:59 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 07:59 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 07:59 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 07:59 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 07:59 75-69-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-EQUIPMENT BLANK Lab ID:92276295006 Collected:11/17/15 08:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2,3-Trichloropropane ND ug/L 11/20/15 07:59 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 07:59 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 07:59 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 07:59 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 07:59 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 07:59 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %11/20/15 07:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %11/20/15 07:59 17060-07-070-130 1
Toluene-d8 (S)101 %11/20/15 07:59 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/19/15 23:00 18496-25-81001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/19/15 04:38 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW4R Lab ID:92276295007 Collected:11/17/15 09:45 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/17/15 09:451
Field pH 5.8 Std. Units 11/17/15 09:450.10 1
Field Temperature 15.5 deg C 11/17/15 09:450.50 1
Static Water Level 10.20 feet 11/17/15 09:451
Field Specific Conductance 395.9 umhos/cm 11/17/15 09:451.0 1
Oxygen, Dissolved 3.3 mg/L 11/17/15 09:45 7782-44-71
Total Well Depth 20 feet 11/17/15 09:451
REDOX 48.8 mV 11/17/15 09:451
Turbidity 9.6 NTU 11/17/15 09:451.0 1
Odor none 11/17/15 09:451
Appearance clear 11/17/15 09:451
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/20/15 22:02 309-00-211/19/15 14:090.050 1
alpha-BHC ND ug/L 11/20/15 22:02 319-84-611/19/15 14:090.050 1
beta-BHC ND ug/L 11/20/15 22:02 319-85-711/19/15 14:090.050 1
delta-BHC ND ug/L 11/20/15 22:02 319-86-811/19/15 14:090.050 1
gamma-BHC (Lindane)ND ug/L 11/20/15 22:02 58-89-911/19/15 14:090.050 1
Chlordane (Technical)ND ug/L 11/20/15 22:02 57-74-911/19/15 14:090.20 1
4,4'-DDD ND ug/L 11/20/15 22:02 72-54-811/19/15 14:090.050 1
4,4'-DDE ND ug/L 11/20/15 22:02 72-55-911/19/15 14:090.050 1
4,4'-DDT ND ug/L 11/20/15 22:02 50-29-311/19/15 14:090.050 1
Dieldrin ND ug/L 11/20/15 22:02 60-57-111/19/15 14:090.050 1
Endosulfan I ND ug/L 11/20/15 22:02 959-98-811/19/15 14:090.050 1
Endosulfan II ND ug/L 11/20/15 22:02 33213-65-911/19/15 14:090.050 1
Endosulfan sulfate ND ug/L 11/20/15 22:02 1031-07-811/19/15 14:090.050 1
Endrin ND ug/L 11/20/15 22:02 72-20-811/19/15 14:090.050 1
Endrin aldehyde ND ug/L 11/20/15 22:02 7421-93-411/19/15 14:090.050 1
Heptachlor ND ug/L 11/20/15 22:02 76-44-811/19/15 14:090.050 1
Heptachlor epoxide ND ug/L 11/20/15 22:02 1024-57-311/19/15 14:090.050 1
Methoxychlor ND ug/L 11/20/15 22:02 72-43-511/19/15 14:090.15 1
Toxaphene ND ug/L 11/20/15 22:02 8001-35-211/19/15 14:090.20 1
Surrogates
Tetrachloro-m-xylene (S)72 %11/20/15 22:02 877-09-811/19/15 14:0920-130 1
Decachlorobiphenyl (S)64 %11/20/15 22:02 2051-24-311/19/15 14:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/20/15 18:17 12674-11-211/19/15 14:090.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/20/15 18:17 11104-28-211/19/15 14:090.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/20/15 18:17 11141-16-511/19/15 14:090.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/20/15 18:17 53469-21-911/19/15 14:090.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/20/15 18:17 12672-29-611/19/15 14:090.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/20/15 18:17 11097-69-111/19/15 14:090.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/20/15 18:17 11096-82-511/19/15 14:090.50 1
Surrogates
Decachlorobiphenyl (S)74 %11/20/15 18:17 2051-24-311/19/15 14:0910-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW4R Lab ID:92276295007 Collected:11/17/15 09:45 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/24/15 01:24 94-75-711/22/15 16:350.94 1
Dinoseb ND ug/L 11/24/15 01:24 88-85-711/22/15 16:350.19 1
2,4,5-T ND ug/L 11/24/15 01:24 93-76-511/22/15 16:350.19 1
2,4,5-TP (Silvex)ND ug/L 11/24/15 01:24 93-72-111/22/15 16:350.19 1
Surrogates
2,4-DCAA (S)94 %11/24/15 01:24 19719-28-911/22/15 16:3536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/24/15 08:43 7440-36-011/20/15 18:005.0 1
Arsenic ND ug/L 11/24/15 08:43 7440-38-211/20/15 18:0010.0 1
Barium 184 ug/L 11/24/15 08:43 7440-39-311/20/15 18:005.0 1
Beryllium ND ug/L 11/24/15 08:43 7440-41-711/20/15 18:001.0 1
Cadmium ND ug/L 11/24/15 08:43 7440-43-911/20/15 18:001.0 1
Chromium ND ug/L 11/24/15 08:43 7440-47-311/20/15 18:005.0 1
Cobalt 28.3 ug/L 11/24/15 08:43 7440-48-411/20/15 18:005.0 1
Copper ND ug/L 11/24/15 08:43 7440-50-811/20/15 18:005.0 1
Iron 312 ug/L 11/24/15 08:43 7439-89-611/20/15 18:0050.0 1
Lead ND ug/L 11/24/15 08:43 7439-92-111/20/15 18:005.0 1
Manganese 407 ug/L 11/24/15 08:43 7439-96-511/20/15 18:005.0 1
Nickel 3.7J ug/L 11/24/15 08:43 7440-02-011/20/15 18:005.0 1
Selenium ND ug/L 11/24/15 08:43 7782-49-211/20/15 18:0010.0 1
Silver ND ug/L 11/24/15 08:43 7440-22-411/20/15 18:005.0 1
Sodium 23800 ug/L 11/24/15 08:43 7440-23-511/20/15 18:0050001
Thallium ND ug/L 11/24/15 08:43 7440-28-011/20/15 18:005.4 1
Tin ND ug/L 11/24/15 08:43 7440-31-511/20/15 18:005.0 1
Vanadium ND ug/L 11/24/15 08:43 7440-62-211/20/15 18:005.0 1
Zinc 5.9J ug/L 11/24/15 08:43 7440-66-611/20/15 18:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 14:07 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/01/15 12:02 83-32-911/20/15 19:3210.0 1
Acenaphthylene ND ug/L 12/01/15 12:02 208-96-811/20/15 19:3210.0 1
Acetophenone ND ug/L 12/01/15 12:02 98-86-211/20/15 19:3210.0 1
2-Acetylaminofluorene ND ug/L 12/01/15 12:02 53-96-311/20/15 19:3220.0 1
4-Aminobiphenyl ND ug/L 12/01/15 12:02 92-67-111/20/15 19:3210.0 1
Anthracene ND ug/L 12/01/15 12:02 120-12-711/20/15 19:3210.0 1
Benzo(a)anthracene ND ug/L 12/01/15 12:02 56-55-311/20/15 19:3210.0 1
Benzo(a)pyrene ND ug/L 12/01/15 12:02 50-32-811/20/15 19:3210.0 1
Benzo(b)fluoranthene ND ug/L 12/01/15 12:02 205-99-211/20/15 19:3210.0 1
Benzo(g,h,i)perylene ND ug/L 12/01/15 12:02 191-24-211/20/15 19:3210.0 1
Benzo(k)fluoranthene ND ug/L 12/01/15 12:02 207-08-911/20/15 19:3210.0 1
Benzyl alcohol ND ug/L 12/01/15 12:02 100-51-611/20/15 19:3220.0 1
4-Bromophenylphenyl ether ND ug/L 12/01/15 12:02 101-55-311/20/15 19:3210.0 1
Butylbenzylphthalate ND ug/L 12/01/15 12:02 85-68-711/20/15 19:3210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW4R Lab ID:92276295007 Collected:11/17/15 09:45 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/01/15 12:02 59-50-711/20/15 19:3220.0 1
4-Chloroaniline ND ug/L 12/01/15 12:02 106-47-811/20/15 19:3220.0 1
Chlorobenzilate ND ug/L 12/01/15 12:02 510-15-611/20/15 19:3210.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/01/15 12:02 111-91-111/20/15 19:3210.0 1
bis(2-Chloroethyl) ether ND ug/L 12/01/15 12:02 111-44-411/20/15 19:3210.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/01/15 12:02 108-60-111/20/15 19:3210.0 1
2-Chloronaphthalene ND ug/L 12/01/15 12:02 91-58-711/20/15 19:3210.0 1
2-Chlorophenol ND ug/L 12/01/15 12:02 95-57-811/20/15 19:3210.0 1
4-Chlorophenylphenyl ether ND ug/L 12/01/15 12:02 7005-72-311/20/15 19:3210.0 1
Chrysene ND ug/L 12/01/15 12:02 218-01-911/20/15 19:3210.0 1
Diallate ND ug/L 12/01/15 12:02 2303-16-411/20/15 19:3210.0 1
Dibenz(a,h)anthracene ND ug/L 12/01/15 12:02 53-70-311/20/15 19:3210.0 1
Dibenzofuran ND ug/L 12/01/15 12:02 132-64-911/20/15 19:3210.0 1
3,3'-Dichlorobenzidine ND ug/L 12/01/15 12:02 91-94-111/20/15 19:3220.0 1
2,4-Dichlorophenol ND ug/L 12/01/15 12:02 120-83-211/20/15 19:3210.0 1
2,6-Dichlorophenol ND ug/L 12/01/15 12:02 87-65-011/20/15 19:3210.0 1
Diethylphthalate ND ug/L 12/01/15 12:02 84-66-211/20/15 19:3210.0 1
Dimethoate ND ug/L 12/01/15 12:02 60-51-511/20/15 19:3210.0 1
P-Dimethylaminoazobenzene ND ug/L 12/01/15 12:02 60-11-711/20/15 19:325.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/01/15 12:02 57-97-611/20/15 19:3210.0 1
3,3'-Dimethylbenzidine ND ug/L 12/01/15 12:02 119-93-711/20/15 19:3210.0 1
2,4-Dimethylphenol ND ug/L 12/01/15 12:02 105-67-911/20/15 19:3210.0 1
Dimethylphthalate ND ug/L 12/01/15 12:02 131-11-311/20/15 19:3210.0 1
Di-n-butylphthalate ND ug/L 12/01/15 12:02 84-74-211/20/15 19:3210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/01/15 12:02 534-52-111/20/15 19:3220.0 1
1,3-Dinitrobenzene ND ug/L 12/01/15 12:02 99-65-011/20/15 19:3220.0 1
2,4-Dinitrophenol ND ug/L 12/01/15 12:02 51-28-511/20/15 19:3250.0 1
2,4-Dinitrotoluene ND ug/L 12/01/15 12:02 121-14-211/20/15 19:3210.0 1
2,6-Dinitrotoluene ND ug/L 12/01/15 12:02 606-20-211/20/15 19:3210.0 1
Di-n-octylphthalate ND ug/L 12/01/15 12:02 117-84-011/20/15 19:3210.0 1
Diphenylamine ND ug/L 12/01/15 12:02 122-39-411/20/15 19:3210.0 1
Disulfoton ND ug/L 12/01/15 12:02 298-04-411/20/15 19:3210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/01/15 12:02 117-81-711/20/15 19:326.0 1
Ethyl methanesulfonate ND ug/L 12/01/15 12:02 62-50-011/20/15 19:3220.0 1
Famphur ND ug/L 12/01/15 12:02 52-85-711/20/15 19:3210.0 1
Fluoranthene ND ug/L 12/01/15 12:02 206-44-011/20/15 19:3210.0 1
Fluorene ND ug/L 12/01/15 12:02 86-73-711/20/15 19:3210.0 1
Hexachlorobenzene ND ug/L 12/01/15 12:02 118-74-111/20/15 19:3210.0 1
Hexachlorocyclopentadiene ND ug/L 12/01/15 12:02 77-47-411/20/15 19:3210.0 1
Hexachloroethane ND ug/L 12/01/15 12:02 67-72-111/20/15 19:3210.0 1
Hexachlorophene ND ug/L 12/01/15 12:02 70-30-411/20/15 19:321001
Indeno(1,2,3-cd)pyrene ND ug/L 12/01/15 12:02 193-39-511/20/15 19:3210.0 1
Isodrin ND ug/L 12/01/15 12:02 465-73-611/20/15 19:3220.0 1
Isophorone ND ug/L 12/01/15 12:02 78-59-111/20/15 19:3210.0 1
Isosafrole ND ug/L 12/01/15 12:02 120-58-111/20/15 19:3210.0 1
Kepone ND ug/L 12/01/15 12:02 143-50-011/20/15 19:3210.0 1
Methapyrilene ND ug/L 12/01/15 12:02 91-80-511/20/15 19:3250.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW4R Lab ID:92276295007 Collected:11/17/15 09:45 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/01/15 12:02 56-49-511/20/15 19:3210.0 1
Methyl methanesulfonate ND ug/L 12/01/15 12:02 66-27-311/20/15 19:325.0 1
2-Methylnaphthalene ND ug/L 12/01/15 12:02 91-57-611/20/15 19:3210.0 1
Methyl parathion ND ug/L 12/01/15 12:02 298-00-011/20/15 19:3210.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/01/15 12:02 95-48-711/20/15 19:3210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/01/15 12:0211/20/15 19:3210.0 1
1-Naphthalenamine ND ug/L 12/01/15 12:02 134-32-711/20/15 19:325.0 1
2-Naphthalenamine ND ug/L 12/01/15 12:02 91-59-811/20/15 19:325.0 1
1,4-Naphthoquinone ND ug/L 12/01/15 12:02 130-15-411/20/15 19:325.0 1
2-Nitroaniline ND ug/L 12/01/15 12:02 88-74-411/20/15 19:3250.0 1
3-Nitroaniline ND ug/L 12/01/15 12:02 99-09-211/20/15 19:3250.0 1
4-Nitroaniline ND ug/L 12/01/15 12:02 100-01-611/20/15 19:3220.0 1
Nitrobenzene ND ug/L 12/01/15 12:02 98-95-311/20/15 19:3210.0 1
2-Nitrophenol ND ug/L 12/01/15 12:02 88-75-511/20/15 19:3210.0 1
4-Nitrophenol ND ug/L 12/01/15 12:02 100-02-711/20/15 19:3250.0 1
5-Nitro-o-toluidine ND ug/L 12/01/15 12:02 99-55-811/20/15 19:3210.0 1
N-Nitrosodiethylamine ND ug/L 12/01/15 12:02 55-18-511/20/15 19:3220.0 1
N-Nitrosodimethylamine ND ug/L 12/01/15 12:02 62-75-911/20/15 19:3210.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/01/15 12:02 924-16-311/20/15 19:3210.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/01/15 12:02 621-64-711/20/15 19:3210.0 1
N-Nitrosodiphenylamine ND ug/L 12/01/15 12:02 86-30-611/20/15 19:3210.0 1
N-Nitrosomethylethylamine ND ug/L 12/01/15 12:02 10595-95-611/20/15 19:3210.0 1
N-Nitrosopiperidine ND ug/L 12/01/15 12:02 100-75-411/20/15 19:3220.0 1
N-Nitrosopyrrolidine ND ug/L 12/01/15 12:02 930-55-211/20/15 19:3210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/01/15 12:02 126-68-111/20/15 19:3210.0 1
Parathion (Ethyl parathion)ND ug/L 12/01/15 12:02 56-38-211/20/15 19:3210.0 1
Pentachlorobenzene ND ug/L 12/01/15 12:02 608-93-511/20/15 19:3210.0 1
Pentachloronitrobenzene ND ug/L 12/01/15 12:02 82-68-811/20/15 19:3220.0 1
Pentachlorophenol ND ug/L 12/01/15 12:02 87-86-511/20/15 19:3225.0 1
Phenacetin ND ug/L 12/01/15 12:02 62-44-211/20/15 19:3220.0 1
Phenanthrene ND ug/L 12/01/15 12:02 85-01-811/20/15 19:3210.0 1
Phenol ND ug/L 12/01/15 12:02 108-95-211/20/15 19:3210.0 1
p-Phenylenediamine ND ug/L 12/01/15 12:02 106-50-311/20/15 19:3210.0 1
Phorate ND ug/L 12/01/15 12:02 298-02-211/20/15 19:3210.0 1
Pronamide ND ug/L 12/01/15 12:02 23950-58-511/20/15 19:3210.0 1
Pyrene ND ug/L 12/01/15 12:02 129-00-011/20/15 19:3210.0 1
Safrole ND ug/L 12/01/15 12:02 94-59-711/20/15 19:3210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/01/15 12:02 95-94-311/20/15 19:3210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/01/15 12:02 58-90-211/20/15 19:3210.0 1
Thionazin ND ug/L 12/01/15 12:02 297-97-211/20/15 19:3220.0 1
O-Toluidine ND ug/L 12/01/15 12:02 95-53-411/20/15 19:3210.0 1
2,4,5-Trichlorophenol ND ug/L 12/01/15 12:02 95-95-411/20/15 19:3210.0 1
2,4,6-Trichlorophenol ND ug/L 12/01/15 12:02 88-06-211/20/15 19:3210.0 1
1,3,5-Trinitrobenzene ND ug/L 12/01/15 12:02 99-35-411/20/15 19:3210.0 1
Surrogates
Nitrobenzene-d5 (S)75 %12/01/15 12:02 4165-60-011/20/15 19:3221-110 1
2-Fluorobiphenyl (S)78 %12/01/15 12:02 321-60-811/20/15 19:3227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW4R Lab ID:92276295007 Collected:11/17/15 09:45 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)91 %12/01/15 12:02 1718-51-011/20/15 19:3231-107 1
Phenol-d6 (S)26 %12/01/15 12:02 13127-88-311/20/15 19:3210-110 1
2-Fluorophenol (S)38 %12/01/15 12:02 367-12-411/20/15 19:3212-110 1
2,4,6-Tribromophenol (S)88 %12/01/15 12:02 118-79-611/20/15 19:3227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 08:16 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 08:16 75-05-850.0 1
Acrolein ND ug/L 11/20/15 08:16 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 08:16 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 08:16 107-05-12.0 1
Benzene ND ug/L 11/20/15 08:16 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 08:16 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 08:16 75-27-41.0 1
Bromoform ND ug/L 11/20/15 08:16 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 08:16 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 08:16 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 08:16 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 08:16 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 08:16 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 08:16 75-00-31.0 1
Chloroform ND ug/L 11/20/15 08:16 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 08:16 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 08:16 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 08:16 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 08:16 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 08:16 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 08:16 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 08:16 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 08:16 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 08:16 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 08:16 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 08:16 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 08:16 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 08:16 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 08:16 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 08:16 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 08:16 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 08:16 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 08:16 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 08:16 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 08:16 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 08:16 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 08:16 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 08:16 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 08:16 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW4R Lab ID:92276295007 Collected:11/17/15 09:45 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 08:16 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 08:16 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 08:16 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 08:16 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 08:16 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 08:16 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 08:16 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 08:16 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 08:16 107-12-020.0 1
Styrene ND ug/L 11/20/15 08:16 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 08:16 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 08:16 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 08:16 127-18-41.0 1
Tetrahydrofuran 7.0J ug/L 11/20/15 08:16 109-99-910.0 1
Toluene ND ug/L 11/20/15 08:16 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 08:16 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 08:16 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 08:16 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 08:16 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 08:16 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 08:16 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 08:16 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 08:16 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 08:16 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 08:16 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 08:16 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %11/20/15 08:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/20/15 08:16 17060-07-070-130 1
Toluene-d8 (S)100 %11/20/15 08:16 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 144000 ug/L 11/29/15 14:0950001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 161000 ug/L 11/19/15 10:20250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/19/15 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 70300 ug/L 11/24/15 19:04 14808-79-8100005
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 16900 ug/L 11/19/15 19:12 16887-00-610001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW4R Lab ID:92276295007 Collected:11/17/15 09:45 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/19/15 04:39 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW7 Lab ID:92276295008 Collected:11/17/15 10:50 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/17/15 10:501
Field pH 5.5 Std. Units 11/17/15 10:500.10 1
Field Temperature 15.3 deg C 11/17/15 10:500.50 1
Static Water Level 38.49 feet 11/17/15 10:501
Field Specific Conductance 196.6 umhos/cm 11/17/15 10:501.0 1
Oxygen, Dissolved 0.7 mg/L 11/17/15 10:50 7782-44-71
Total Well Depth 48.00 feet 11/17/15 10:501
REDOX 30.9 mV 11/17/15 10:501
Turbidity 1.0 NTU 11/17/15 10:501.0 1
Odor none 11/17/15 10:501
Appearance clear 11/17/15 10:501
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/20/15 22:20 309-00-211/19/15 14:090.050 1
alpha-BHC ND ug/L 11/20/15 22:20 319-84-611/19/15 14:090.050 1
beta-BHC ND ug/L 11/20/15 22:20 319-85-711/19/15 14:090.050 1
delta-BHC ND ug/L 11/20/15 22:20 319-86-811/19/15 14:090.050 1
gamma-BHC (Lindane)ND ug/L 11/20/15 22:20 58-89-911/19/15 14:090.050 1
Chlordane (Technical)ND ug/L 11/20/15 22:20 57-74-911/19/15 14:090.20 1
4,4'-DDD ND ug/L 11/20/15 22:20 72-54-811/19/15 14:090.050 1
4,4'-DDE ND ug/L 11/20/15 22:20 72-55-911/19/15 14:090.050 1
4,4'-DDT ND ug/L 11/20/15 22:20 50-29-311/19/15 14:090.050 1
Dieldrin ND ug/L 11/20/15 22:20 60-57-111/19/15 14:090.050 1
Endosulfan I ND ug/L 11/20/15 22:20 959-98-811/19/15 14:090.050 1
Endosulfan II ND ug/L 11/20/15 22:20 33213-65-911/19/15 14:090.050 1
Endosulfan sulfate ND ug/L 11/20/15 22:20 1031-07-811/19/15 14:090.050 1
Endrin ND ug/L 11/20/15 22:20 72-20-811/19/15 14:090.050 1
Endrin aldehyde ND ug/L 11/20/15 22:20 7421-93-411/19/15 14:090.050 1
Heptachlor ND ug/L 11/20/15 22:20 76-44-811/19/15 14:090.050 1
Heptachlor epoxide ND ug/L 11/20/15 22:20 1024-57-311/19/15 14:090.050 1
Methoxychlor ND ug/L 11/20/15 22:20 72-43-511/19/15 14:090.15 1
Toxaphene ND ug/L 11/20/15 22:20 8001-35-211/19/15 14:090.20 1
Surrogates
Tetrachloro-m-xylene (S)97 %11/20/15 22:20 877-09-811/19/15 14:0920-130 1
Decachlorobiphenyl (S)76 %11/20/15 22:20 2051-24-311/19/15 14:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/20/15 18:37 12674-11-211/19/15 14:090.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/20/15 18:37 11104-28-211/19/15 14:090.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/20/15 18:37 11141-16-511/19/15 14:090.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/20/15 18:37 53469-21-911/19/15 14:090.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/20/15 18:37 12672-29-611/19/15 14:090.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/20/15 18:37 11097-69-111/19/15 14:090.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/20/15 18:37 11096-82-511/19/15 14:090.50 1
Surrogates
Decachlorobiphenyl (S)93 %11/20/15 18:37 2051-24-311/19/15 14:0910-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW7 Lab ID:92276295008 Collected:11/17/15 10:50 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/24/15 20:31 94-75-711/23/15 16:350.94 1
Dinoseb ND ug/L 11/24/15 20:31 88-85-711/23/15 16:350.19 1
2,4,5-T ND ug/L 11/24/15 20:31 93-76-511/23/15 16:350.19 1
2,4,5-TP (Silvex)ND ug/L 11/24/15 20:31 93-72-111/23/15 16:350.19 1
Surrogates
2,4-DCAA (S)79 %11/24/15 20:31 19719-28-911/23/15 16:3536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/24/15 08:55 7440-36-011/20/15 18:005.0 1
Arsenic ND ug/L 11/24/15 08:55 7440-38-211/20/15 18:0010.0 1
Barium 140 ug/L 11/24/15 08:55 7440-39-311/20/15 18:005.0 1
Beryllium ND ug/L 11/24/15 08:55 7440-41-711/20/15 18:001.0 1
Cadmium ND ug/L 11/24/15 08:55 7440-43-911/20/15 18:001.0 1
Chromium ND ug/L 11/24/15 08:55 7440-47-311/20/15 18:005.0 1
Cobalt ND ug/L 11/24/15 08:55 7440-48-411/20/15 18:005.0 1
Copper ND ug/L 11/24/15 08:55 7440-50-811/20/15 18:005.0 1
Iron ND ug/L 11/24/15 08:55 7439-89-611/20/15 18:0050.0 1
Lead ND ug/L 11/24/15 08:55 7439-92-111/20/15 18:005.0 1
Manganese 33.6 ug/L 11/24/15 08:55 7439-96-511/20/15 18:005.0 1
Nickel ND ug/L 11/24/15 08:55 7440-02-011/20/15 18:005.0 1
Selenium ND ug/L 11/24/15 08:55 7782-49-211/20/15 18:0010.0 1
Silver ND ug/L 11/24/15 08:55 7440-22-411/20/15 18:005.0 1
Sodium 15700 ug/L 11/24/15 08:55 7440-23-511/20/15 18:0050001
Thallium ND ug/L 11/24/15 08:55 7440-28-011/20/15 18:005.4 1
Tin ND ug/L 11/24/15 08:55 7440-31-511/20/15 18:005.0 1
Vanadium ND ug/L 11/24/15 08:55 7440-62-211/20/15 18:005.0 1
Zinc ND ug/L 11/24/15 08:55 7440-66-611/20/15 18:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 14:09 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/01/15 12:30 83-32-911/20/15 19:3210.0 1
Acenaphthylene ND ug/L 12/01/15 12:30 208-96-811/20/15 19:3210.0 1
Acetophenone ND ug/L 12/01/15 12:30 98-86-211/20/15 19:3210.0 1
2-Acetylaminofluorene ND ug/L 12/01/15 12:30 53-96-311/20/15 19:3220.0 1
4-Aminobiphenyl ND ug/L 12/01/15 12:30 92-67-111/20/15 19:3210.0 1
Anthracene ND ug/L 12/01/15 12:30 120-12-711/20/15 19:3210.0 1
Benzo(a)anthracene ND ug/L 12/01/15 12:30 56-55-311/20/15 19:3210.0 1
Benzo(a)pyrene ND ug/L 12/01/15 12:30 50-32-811/20/15 19:3210.0 1
Benzo(b)fluoranthene ND ug/L 12/01/15 12:30 205-99-211/20/15 19:3210.0 1
Benzo(g,h,i)perylene ND ug/L 12/01/15 12:30 191-24-211/20/15 19:3210.0 1
Benzo(k)fluoranthene ND ug/L 12/01/15 12:30 207-08-911/20/15 19:3210.0 1
Benzyl alcohol ND ug/L 12/01/15 12:30 100-51-611/20/15 19:3220.0 1
4-Bromophenylphenyl ether ND ug/L 12/01/15 12:30 101-55-311/20/15 19:3210.0 1
Butylbenzylphthalate ND ug/L 12/01/15 12:30 85-68-711/20/15 19:3210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW7 Lab ID:92276295008 Collected:11/17/15 10:50 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/01/15 12:30 59-50-711/20/15 19:3220.0 1
4-Chloroaniline ND ug/L 12/01/15 12:30 106-47-811/20/15 19:3220.0 1
Chlorobenzilate ND ug/L 12/01/15 12:30 510-15-611/20/15 19:3210.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/01/15 12:30 111-91-111/20/15 19:3210.0 1
bis(2-Chloroethyl) ether ND ug/L 12/01/15 12:30 111-44-411/20/15 19:3210.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/01/15 12:30 108-60-111/20/15 19:3210.0 1
2-Chloronaphthalene ND ug/L 12/01/15 12:30 91-58-711/20/15 19:3210.0 1
2-Chlorophenol ND ug/L 12/01/15 12:30 95-57-811/20/15 19:3210.0 1
4-Chlorophenylphenyl ether ND ug/L 12/01/15 12:30 7005-72-311/20/15 19:3210.0 1
Chrysene ND ug/L 12/01/15 12:30 218-01-911/20/15 19:3210.0 1
Diallate ND ug/L 12/01/15 12:30 2303-16-411/20/15 19:3210.0 1
Dibenz(a,h)anthracene ND ug/L 12/01/15 12:30 53-70-311/20/15 19:3210.0 1
Dibenzofuran ND ug/L 12/01/15 12:30 132-64-911/20/15 19:3210.0 1
3,3'-Dichlorobenzidine ND ug/L 12/01/15 12:30 91-94-111/20/15 19:3220.0 1
2,4-Dichlorophenol ND ug/L 12/01/15 12:30 120-83-211/20/15 19:3210.0 1
2,6-Dichlorophenol ND ug/L 12/01/15 12:30 87-65-011/20/15 19:3210.0 1
Diethylphthalate ND ug/L 12/01/15 12:30 84-66-211/20/15 19:3210.0 1
Dimethoate ND ug/L 12/01/15 12:30 60-51-511/20/15 19:3210.0 1
P-Dimethylaminoazobenzene ND ug/L 12/01/15 12:30 60-11-711/20/15 19:325.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/01/15 12:30 57-97-611/20/15 19:3210.0 1
3,3'-Dimethylbenzidine ND ug/L 12/01/15 12:30 119-93-711/20/15 19:3210.0 1
2,4-Dimethylphenol ND ug/L 12/01/15 12:30 105-67-911/20/15 19:3210.0 1
Dimethylphthalate ND ug/L 12/01/15 12:30 131-11-311/20/15 19:3210.0 1
Di-n-butylphthalate ND ug/L 12/01/15 12:30 84-74-211/20/15 19:3210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/01/15 12:30 534-52-111/20/15 19:3220.0 1
1,3-Dinitrobenzene ND ug/L 12/01/15 12:30 99-65-011/20/15 19:3220.0 1
2,4-Dinitrophenol ND ug/L 12/01/15 12:30 51-28-511/20/15 19:3250.0 1
2,4-Dinitrotoluene ND ug/L 12/01/15 12:30 121-14-211/20/15 19:3210.0 1
2,6-Dinitrotoluene ND ug/L 12/01/15 12:30 606-20-211/20/15 19:3210.0 1
Di-n-octylphthalate ND ug/L 12/01/15 12:30 117-84-011/20/15 19:3210.0 1
Diphenylamine ND ug/L 12/01/15 12:30 122-39-411/20/15 19:3210.0 1
Disulfoton ND ug/L 12/01/15 12:30 298-04-411/20/15 19:3210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/01/15 12:30 117-81-711/20/15 19:326.0 1
Ethyl methanesulfonate ND ug/L 12/01/15 12:30 62-50-011/20/15 19:3220.0 1
Famphur ND ug/L 12/01/15 12:30 52-85-711/20/15 19:3210.0 1
Fluoranthene ND ug/L 12/01/15 12:30 206-44-011/20/15 19:3210.0 1
Fluorene ND ug/L 12/01/15 12:30 86-73-711/20/15 19:3210.0 1
Hexachlorobenzene ND ug/L 12/01/15 12:30 118-74-111/20/15 19:3210.0 1
Hexachlorocyclopentadiene ND ug/L 12/01/15 12:30 77-47-411/20/15 19:3210.0 1
Hexachloroethane ND ug/L 12/01/15 12:30 67-72-111/20/15 19:3210.0 1
Hexachlorophene ND ug/L 12/01/15 12:30 70-30-411/20/15 19:321001
Indeno(1,2,3-cd)pyrene ND ug/L 12/01/15 12:30 193-39-511/20/15 19:3210.0 1
Isodrin ND ug/L 12/01/15 12:30 465-73-611/20/15 19:3220.0 1
Isophorone ND ug/L 12/01/15 12:30 78-59-111/20/15 19:3210.0 1
Isosafrole ND ug/L 12/01/15 12:30 120-58-111/20/15 19:3210.0 1
Kepone ND ug/L 12/01/15 12:30 143-50-011/20/15 19:3210.0 1
Methapyrilene ND ug/L 12/01/15 12:30 91-80-511/20/15 19:3250.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW7 Lab ID:92276295008 Collected:11/17/15 10:50 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/01/15 12:30 56-49-511/20/15 19:3210.0 1
Methyl methanesulfonate ND ug/L 12/01/15 12:30 66-27-311/20/15 19:325.0 1
2-Methylnaphthalene ND ug/L 12/01/15 12:30 91-57-611/20/15 19:3210.0 1
Methyl parathion ND ug/L 12/01/15 12:30 298-00-011/20/15 19:3210.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/01/15 12:30 95-48-711/20/15 19:3210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/01/15 12:3011/20/15 19:3210.0 1
1-Naphthalenamine ND ug/L 12/01/15 12:30 134-32-711/20/15 19:325.0 1
2-Naphthalenamine ND ug/L 12/01/15 12:30 91-59-811/20/15 19:325.0 1
1,4-Naphthoquinone ND ug/L 12/01/15 12:30 130-15-411/20/15 19:325.0 1
2-Nitroaniline ND ug/L 12/01/15 12:30 88-74-411/20/15 19:3250.0 1
3-Nitroaniline ND ug/L 12/01/15 12:30 99-09-211/20/15 19:3250.0 1
4-Nitroaniline ND ug/L 12/01/15 12:30 100-01-611/20/15 19:3220.0 1
Nitrobenzene ND ug/L 12/01/15 12:30 98-95-311/20/15 19:3210.0 1
2-Nitrophenol ND ug/L 12/01/15 12:30 88-75-511/20/15 19:3210.0 1
4-Nitrophenol ND ug/L 12/01/15 12:30 100-02-711/20/15 19:3250.0 1
5-Nitro-o-toluidine ND ug/L 12/01/15 12:30 99-55-811/20/15 19:3210.0 1
N-Nitrosodiethylamine ND ug/L 12/01/15 12:30 55-18-511/20/15 19:3220.0 1
N-Nitrosodimethylamine ND ug/L 12/01/15 12:30 62-75-911/20/15 19:3210.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/01/15 12:30 924-16-311/20/15 19:3210.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/01/15 12:30 621-64-711/20/15 19:3210.0 1
N-Nitrosodiphenylamine ND ug/L 12/01/15 12:30 86-30-611/20/15 19:3210.0 1
N-Nitrosomethylethylamine ND ug/L 12/01/15 12:30 10595-95-611/20/15 19:3210.0 1
N-Nitrosopiperidine ND ug/L 12/01/15 12:30 100-75-411/20/15 19:3220.0 1
N-Nitrosopyrrolidine ND ug/L 12/01/15 12:30 930-55-211/20/15 19:3210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/01/15 12:30 126-68-111/20/15 19:3210.0 1
Parathion (Ethyl parathion)ND ug/L 12/01/15 12:30 56-38-211/20/15 19:3210.0 1
Pentachlorobenzene ND ug/L 12/01/15 12:30 608-93-511/20/15 19:3210.0 1
Pentachloronitrobenzene ND ug/L 12/01/15 12:30 82-68-811/20/15 19:3220.0 1
Pentachlorophenol ND ug/L 12/01/15 12:30 87-86-511/20/15 19:3225.0 1
Phenacetin ND ug/L 12/01/15 12:30 62-44-211/20/15 19:3220.0 1
Phenanthrene ND ug/L 12/01/15 12:30 85-01-811/20/15 19:3210.0 1
Phenol ND ug/L 12/01/15 12:30 108-95-211/20/15 19:3210.0 1
p-Phenylenediamine ND ug/L 12/01/15 12:30 106-50-311/20/15 19:3210.0 1
Phorate ND ug/L 12/01/15 12:30 298-02-211/20/15 19:3210.0 1
Pronamide ND ug/L 12/01/15 12:30 23950-58-511/20/15 19:3210.0 1
Pyrene ND ug/L 12/01/15 12:30 129-00-011/20/15 19:3210.0 1
Safrole ND ug/L 12/01/15 12:30 94-59-711/20/15 19:3210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/01/15 12:30 95-94-311/20/15 19:3210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/01/15 12:30 58-90-211/20/15 19:3210.0 1
Thionazin ND ug/L 12/01/15 12:30 297-97-211/20/15 19:3220.0 1
O-Toluidine ND ug/L 12/01/15 12:30 95-53-411/20/15 19:3210.0 1
2,4,5-Trichlorophenol ND ug/L 12/01/15 12:30 95-95-411/20/15 19:3210.0 1
2,4,6-Trichlorophenol ND ug/L 12/01/15 12:30 88-06-211/20/15 19:3210.0 1
1,3,5-Trinitrobenzene ND ug/L 12/01/15 12:30 99-35-411/20/15 19:3210.0 1
Surrogates
Nitrobenzene-d5 (S)79 %12/01/15 12:30 4165-60-011/20/15 19:3221-110 1
2-Fluorobiphenyl (S)77 %12/01/15 12:30 321-60-811/20/15 19:3227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW7 Lab ID:92276295008 Collected:11/17/15 10:50 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)86 %12/01/15 12:30 1718-51-011/20/15 19:3231-107 1
Phenol-d6 (S)25 %12/01/15 12:30 13127-88-311/20/15 19:3210-110 1
2-Fluorophenol (S)36 %12/01/15 12:30 367-12-411/20/15 19:3212-110 1
2,4,6-Tribromophenol (S)89 %12/01/15 12:30 118-79-611/20/15 19:3227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 07:25 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 07:25 75-05-850.0 1
Acrolein ND ug/L 11/20/15 07:25 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 07:25 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 07:25 107-05-12.0 1
Benzene ND ug/L 11/20/15 07:25 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 07:25 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 07:25 75-27-41.0 1
Bromoform ND ug/L 11/20/15 07:25 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 07:25 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 07:25 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 07:25 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 07:25 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 07:25 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 07:25 75-00-31.0 1
Chloroform ND ug/L 11/20/15 07:25 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 07:25 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 07:25 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 07:25 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 07:25 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 07:25 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 07:25 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 07:25 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 07:25 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 07:25 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 07:25 110-57-61.0 1
Dichlorodifluoromethane 1.0 ug/L 11/20/15 07:25 75-71-81.0 1
1,1-Dichloroethane 0.91J ug/L 11/20/15 07:25 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 07:25 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 07:25 75-35-41.0 1
cis-1,2-Dichloroethene 0.80J ug/L 11/20/15 07:25 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 07:25 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 07:25 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 07:25 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 07:25 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 07:25 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 07:25 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 07:25 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 07:25 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 07:25 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW7 Lab ID:92276295008 Collected:11/17/15 10:50 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 07:25 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 07:25 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 07:25 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 07:25 126-98-710.0 1
Methylene Chloride 3.9 ug/L 11/20/15 07:25 75-09-2 C91.0 1
Methyl methacrylate ND ug/L 11/20/15 07:25 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 07:25 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 07:25 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 07:25 107-12-020.0 1
Styrene ND ug/L 11/20/15 07:25 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 07:25 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 07:25 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 07:25 127-18-41.0 1
Tetrahydrofuran 17.7 ug/L 11/20/15 07:25 109-99-910.0 1
Toluene ND ug/L 11/20/15 07:25 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 07:25 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 07:25 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 07:25 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 07:25 79-01-61.0 1
Trichlorofluoromethane 1.4 ug/L 11/20/15 07:25 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 07:25 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 07:25 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 07:25 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 07:25 1330-20-72.0 1
m&p-Xylene 0.84J ug/L 11/20/15 07:25 179601-23-12.0 1
o-Xylene 0.27J ug/L 11/20/15 07:25 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %11/20/15 07:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/20/15 07:25 17060-07-070-130 1
Toluene-d8 (S)99 %11/20/15 07:25 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 67300 ug/L 11/29/15 14:2250001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 78000 ug/L 11/19/15 10:20250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/19/15 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 10100 ug/L 11/24/15 19:18 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 6050 ug/L 11/19/15 19:13 16887-00-610001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW7 Lab ID:92276295008 Collected:11/17/15 10:50 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/19/15 04:40 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW5R Lab ID:92276295009 Collected:11/17/15 12:20 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/17/15 12:201
Field pH 5.8 Std. Units 11/17/15 12:200.10 1
Field Temperature 15.9 deg C 11/17/15 12:200.50 1
Static Water Level 11.62 feet 11/17/15 12:201
Field Specific Conductance 164.5 umhos/cm 11/17/15 12:201.0 1
Oxygen, Dissolved 5.9 mg/L 11/17/15 12:20 7782-44-71
Total Well Depth 30 feet 11/17/15 12:201
REDOX 52.6 mV 11/17/15 12:201
Turbidity 1.0 NTU 11/17/15 12:201.0 1
Odor none 11/17/15 12:201
Appearance clear 11/17/15 12:201
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/20/15 22:37 309-00-211/19/15 14:090.050 1
alpha-BHC ND ug/L 11/20/15 22:37 319-84-611/19/15 14:090.050 1
beta-BHC ND ug/L 11/20/15 22:37 319-85-711/19/15 14:090.050 1
delta-BHC ND ug/L 11/20/15 22:37 319-86-811/19/15 14:090.050 1
gamma-BHC (Lindane)ND ug/L 11/20/15 22:37 58-89-911/19/15 14:090.050 1
Chlordane (Technical)ND ug/L 11/20/15 22:37 57-74-911/19/15 14:090.20 1
4,4'-DDD ND ug/L 11/20/15 22:37 72-54-811/19/15 14:090.050 1
4,4'-DDE ND ug/L 11/20/15 22:37 72-55-911/19/15 14:090.050 1
4,4'-DDT ND ug/L 11/20/15 22:37 50-29-311/19/15 14:090.050 1
Dieldrin ND ug/L 11/20/15 22:37 60-57-111/19/15 14:090.050 1
Endosulfan I ND ug/L 11/20/15 22:37 959-98-811/19/15 14:090.050 1
Endosulfan II ND ug/L 11/20/15 22:37 33213-65-911/19/15 14:090.050 1
Endosulfan sulfate ND ug/L 11/20/15 22:37 1031-07-811/19/15 14:090.050 1
Endrin ND ug/L 11/20/15 22:37 72-20-811/19/15 14:090.050 1
Endrin aldehyde ND ug/L 11/20/15 22:37 7421-93-411/19/15 14:090.050 1
Heptachlor ND ug/L 11/20/15 22:37 76-44-811/19/15 14:090.050 1
Heptachlor epoxide ND ug/L 11/20/15 22:37 1024-57-311/19/15 14:090.050 1
Methoxychlor ND ug/L 11/20/15 22:37 72-43-511/19/15 14:090.15 1
Toxaphene ND ug/L 11/20/15 22:37 8001-35-211/19/15 14:090.20 1
Surrogates
Tetrachloro-m-xylene (S)70 %11/20/15 22:37 877-09-811/19/15 14:0920-130 1
Decachlorobiphenyl (S)79 %11/20/15 22:37 2051-24-311/19/15 14:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/20/15 18:58 12674-11-211/19/15 14:090.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/20/15 18:58 11104-28-211/19/15 14:090.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/20/15 18:58 11141-16-511/19/15 14:090.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/20/15 18:58 53469-21-911/19/15 14:090.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/20/15 18:58 12672-29-611/19/15 14:090.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/20/15 18:58 11097-69-111/19/15 14:090.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/20/15 18:58 11096-82-511/19/15 14:090.50 1
Surrogates
Decachlorobiphenyl (S)83 %11/20/15 18:58 2051-24-311/19/15 14:0910-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW5R Lab ID:92276295009 Collected:11/17/15 12:20 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/24/15 21:02 94-75-711/23/15 16:350.94 1
Dinoseb ND ug/L 11/24/15 21:02 88-85-711/23/15 16:350.19 1
2,4,5-T ND ug/L 11/24/15 21:02 93-76-511/23/15 16:350.19 1
2,4,5-TP (Silvex)ND ug/L 11/24/15 21:02 93-72-111/23/15 16:350.19 1
Surrogates
2,4-DCAA (S)98 %11/24/15 21:02 19719-28-911/23/15 16:3536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/30/15 17:57 7440-36-011/25/15 22:005.0 1
Arsenic ND ug/L 11/30/15 17:57 7440-38-211/25/15 22:0010.0 1
Barium 92.7 ug/L 11/30/15 17:57 7440-39-311/25/15 22:005.0 1
Beryllium ND ug/L 11/30/15 17:57 7440-41-711/25/15 22:001.0 1
Cadmium ND ug/L 11/30/15 17:57 7440-43-911/25/15 22:001.0 1
Chromium ND ug/L 11/30/15 17:57 7440-47-311/25/15 22:005.0 1
Cobalt 2.5J ug/L 11/30/15 17:57 7440-48-411/25/15 22:005.0 1
Copper ND ug/L 11/30/15 17:57 7440-50-811/25/15 22:005.0 1
Iron 32600 ug/L 11/30/15 17:57 7439-89-611/25/15 22:0050.0 1
Lead ND ug/L 11/30/15 17:57 7439-92-111/25/15 22:005.0 1
Manganese 1890 ug/L 11/30/15 17:57 7439-96-511/25/15 22:005.0 1
Nickel ND ug/L 11/30/15 17:57 7440-02-011/25/15 22:005.0 1
Selenium ND ug/L 11/30/15 17:57 7782-49-211/25/15 22:0010.0 1
Silver ND ug/L 11/30/15 17:57 7440-22-411/25/15 22:005.0 1
Sodium 11300 ug/L 11/30/15 17:57 7440-23-511/25/15 22:0050001
Thallium ND ug/L 12/01/15 17:48 7440-28-011/25/15 22:005.4 1
Tin ND ug/L 11/30/15 17:57 7440-31-511/25/15 22:005.0 1
Vanadium 3.7J ug/L 11/30/15 17:57 7440-62-211/25/15 22:005.0 1
Zinc ND ug/L 11/30/15 17:57 7440-66-611/25/15 22:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 14:16 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 11/30/15 19:52 83-32-911/20/15 19:3210.0 1
Acenaphthylene ND ug/L 11/30/15 19:52 208-96-811/20/15 19:3210.0 1
Acetophenone ND ug/L 11/30/15 19:52 98-86-211/20/15 19:3210.0 1
2-Acetylaminofluorene ND ug/L 11/30/15 19:52 53-96-311/20/15 19:3220.0 1
4-Aminobiphenyl ND ug/L 11/30/15 19:52 92-67-111/20/15 19:3210.0 1
Anthracene ND ug/L 11/30/15 19:52 120-12-711/20/15 19:3210.0 1
Benzo(a)anthracene ND ug/L 11/30/15 19:52 56-55-311/20/15 19:3210.0 1
Benzo(a)pyrene ND ug/L 11/30/15 19:52 50-32-811/20/15 19:3210.0 1
Benzo(b)fluoranthene ND ug/L 11/30/15 19:52 205-99-211/20/15 19:3210.0 1
Benzo(g,h,i)perylene ND ug/L 11/30/15 19:52 191-24-211/20/15 19:3210.0 1
Benzo(k)fluoranthene ND ug/L 11/30/15 19:52 207-08-911/20/15 19:3210.0 1
Benzyl alcohol ND ug/L 11/30/15 19:52 100-51-611/20/15 19:3220.0 1
4-Bromophenylphenyl ether ND ug/L 11/30/15 19:52 101-55-311/20/15 19:3210.0 1
Butylbenzylphthalate ND ug/L 11/30/15 19:52 85-68-711/20/15 19:3210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW5R Lab ID:92276295009 Collected:11/17/15 12:20 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 11/30/15 19:52 59-50-711/20/15 19:3220.0 1
4-Chloroaniline ND ug/L 11/30/15 19:52 106-47-811/20/15 19:3220.0 1
Chlorobenzilate ND ug/L 11/30/15 19:52 510-15-611/20/15 19:3210.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/30/15 19:52 111-91-111/20/15 19:3210.0 1
bis(2-Chloroethyl) ether ND ug/L 11/30/15 19:52 111-44-411/20/15 19:3210.0 1
bis(2-Chloroisopropyl) ether ND ug/L 11/30/15 19:52 108-60-111/20/15 19:3210.0 1
2-Chloronaphthalene ND ug/L 11/30/15 19:52 91-58-711/20/15 19:3210.0 1
2-Chlorophenol ND ug/L 11/30/15 19:52 95-57-811/20/15 19:3210.0 1
4-Chlorophenylphenyl ether ND ug/L 11/30/15 19:52 7005-72-311/20/15 19:3210.0 1
Chrysene ND ug/L 11/30/15 19:52 218-01-911/20/15 19:3210.0 1
Diallate ND ug/L 11/30/15 19:52 2303-16-411/20/15 19:3210.0 1
Dibenz(a,h)anthracene ND ug/L 11/30/15 19:52 53-70-311/20/15 19:3210.0 1
Dibenzofuran ND ug/L 11/30/15 19:52 132-64-911/20/15 19:3210.0 1
3,3'-Dichlorobenzidine ND ug/L 11/30/15 19:52 91-94-111/20/15 19:3220.0 1
2,4-Dichlorophenol ND ug/L 11/30/15 19:52 120-83-211/20/15 19:3210.0 1
2,6-Dichlorophenol ND ug/L 11/30/15 19:52 87-65-011/20/15 19:3210.0 1
Diethylphthalate ND ug/L 11/30/15 19:52 84-66-211/20/15 19:3210.0 1
Dimethoate ND ug/L 11/30/15 19:52 60-51-511/20/15 19:3210.0 1
P-Dimethylaminoazobenzene ND ug/L 11/30/15 19:52 60-11-711/20/15 19:325.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 11/30/15 19:52 57-97-611/20/15 19:3210.0 1
3,3'-Dimethylbenzidine ND ug/L 11/30/15 19:52 119-93-711/20/15 19:3210.0 1
2,4-Dimethylphenol ND ug/L 11/30/15 19:52 105-67-911/20/15 19:3210.0 1
Dimethylphthalate ND ug/L 11/30/15 19:52 131-11-311/20/15 19:3210.0 1
Di-n-butylphthalate ND ug/L 11/30/15 19:52 84-74-211/20/15 19:3210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/30/15 19:52 534-52-111/20/15 19:3220.0 1
1,3-Dinitrobenzene ND ug/L 11/30/15 19:52 99-65-011/20/15 19:3220.0 1
2,4-Dinitrophenol ND ug/L 11/30/15 19:52 51-28-511/20/15 19:3250.0 1
2,4-Dinitrotoluene ND ug/L 11/30/15 19:52 121-14-211/20/15 19:3210.0 1
2,6-Dinitrotoluene ND ug/L 11/30/15 19:52 606-20-211/20/15 19:3210.0 1
Di-n-octylphthalate ND ug/L 11/30/15 19:52 117-84-011/20/15 19:3210.0 1
Diphenylamine ND ug/L 11/30/15 19:52 122-39-411/20/15 19:3210.0 1
Disulfoton ND ug/L 11/30/15 19:52 298-04-411/20/15 19:3210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/30/15 19:52 117-81-711/20/15 19:326.0 1
Ethyl methanesulfonate ND ug/L 11/30/15 19:52 62-50-011/20/15 19:3220.0 1
Famphur ND ug/L 11/30/15 19:52 52-85-711/20/15 19:3210.0 1
Fluoranthene ND ug/L 11/30/15 19:52 206-44-011/20/15 19:3210.0 1
Fluorene ND ug/L 11/30/15 19:52 86-73-711/20/15 19:3210.0 1
Hexachlorobenzene ND ug/L 11/30/15 19:52 118-74-111/20/15 19:3210.0 1
Hexachlorocyclopentadiene ND ug/L 11/30/15 19:52 77-47-411/20/15 19:3210.0 1
Hexachloroethane ND ug/L 11/30/15 19:52 67-72-111/20/15 19:3210.0 1
Hexachlorophene ND ug/L 11/30/15 19:52 70-30-411/20/15 19:321001
Indeno(1,2,3-cd)pyrene ND ug/L 11/30/15 19:52 193-39-511/20/15 19:3210.0 1
Isodrin ND ug/L 11/30/15 19:52 465-73-611/20/15 19:3220.0 1
Isophorone ND ug/L 11/30/15 19:52 78-59-111/20/15 19:3210.0 1
Isosafrole ND ug/L 11/30/15 19:52 120-58-111/20/15 19:3210.0 1
Kepone ND ug/L 11/30/15 19:52 143-50-011/20/15 19:3210.0 1
Methapyrilene ND ug/L 11/30/15 19:52 91-80-511/20/15 19:3250.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW5R Lab ID:92276295009 Collected:11/17/15 12:20 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 11/30/15 19:52 56-49-511/20/15 19:3210.0 1
Methyl methanesulfonate ND ug/L 11/30/15 19:52 66-27-311/20/15 19:325.0 1
2-Methylnaphthalene ND ug/L 11/30/15 19:52 91-57-611/20/15 19:3210.0 1
Methyl parathion ND ug/L 11/30/15 19:52 298-00-011/20/15 19:3210.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/30/15 19:52 95-48-711/20/15 19:3210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/30/15 19:5211/20/15 19:3210.0 1
1-Naphthalenamine ND ug/L 11/30/15 19:52 134-32-711/20/15 19:325.0 1
2-Naphthalenamine ND ug/L 11/30/15 19:52 91-59-811/20/15 19:325.0 1
1,4-Naphthoquinone ND ug/L 11/30/15 19:52 130-15-411/20/15 19:325.0 1
2-Nitroaniline ND ug/L 11/30/15 19:52 88-74-411/20/15 19:3250.0 1
3-Nitroaniline ND ug/L 11/30/15 19:52 99-09-211/20/15 19:3250.0 1
4-Nitroaniline ND ug/L 11/30/15 19:52 100-01-611/20/15 19:3220.0 1
Nitrobenzene ND ug/L 11/30/15 19:52 98-95-311/20/15 19:3210.0 1
2-Nitrophenol ND ug/L 11/30/15 19:52 88-75-511/20/15 19:3210.0 1
4-Nitrophenol ND ug/L 11/30/15 19:52 100-02-711/20/15 19:3250.0 1
5-Nitro-o-toluidine ND ug/L 11/30/15 19:52 99-55-811/20/15 19:3210.0 1
N-Nitrosodiethylamine ND ug/L 11/30/15 19:52 55-18-511/20/15 19:3220.0 1
N-Nitrosodimethylamine ND ug/L 11/30/15 19:52 62-75-911/20/15 19:3210.0 1
N-Nitroso-di-n-butylamine ND ug/L 11/30/15 19:52 924-16-311/20/15 19:3210.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/30/15 19:52 621-64-711/20/15 19:3210.0 1
N-Nitrosodiphenylamine ND ug/L 11/30/15 19:52 86-30-611/20/15 19:3210.0 1
N-Nitrosomethylethylamine ND ug/L 11/30/15 19:52 10595-95-611/20/15 19:3210.0 1
N-Nitrosopiperidine ND ug/L 11/30/15 19:52 100-75-411/20/15 19:3220.0 1
N-Nitrosopyrrolidine ND ug/L 11/30/15 19:52 930-55-211/20/15 19:3210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 11/30/15 19:52 126-68-111/20/15 19:3210.0 1
Parathion (Ethyl parathion)ND ug/L 11/30/15 19:52 56-38-211/20/15 19:3210.0 1
Pentachlorobenzene ND ug/L 11/30/15 19:52 608-93-511/20/15 19:3210.0 1
Pentachloronitrobenzene ND ug/L 11/30/15 19:52 82-68-811/20/15 19:3220.0 1
Pentachlorophenol ND ug/L 11/30/15 19:52 87-86-511/20/15 19:3225.0 1
Phenacetin ND ug/L 11/30/15 19:52 62-44-211/20/15 19:3220.0 1
Phenanthrene ND ug/L 11/30/15 19:52 85-01-811/20/15 19:3210.0 1
Phenol ND ug/L 11/30/15 19:52 108-95-211/20/15 19:3210.0 1
p-Phenylenediamine ND ug/L 11/30/15 19:52 106-50-311/20/15 19:3210.0 1
Phorate ND ug/L 11/30/15 19:52 298-02-211/20/15 19:3210.0 1
Pronamide ND ug/L 11/30/15 19:52 23950-58-511/20/15 19:3210.0 1
Pyrene ND ug/L 11/30/15 19:52 129-00-011/20/15 19:3210.0 1
Safrole ND ug/L 11/30/15 19:52 94-59-711/20/15 19:3210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 11/30/15 19:52 95-94-311/20/15 19:3210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 11/30/15 19:52 58-90-211/20/15 19:3210.0 1
Thionazin ND ug/L 11/30/15 19:52 297-97-211/20/15 19:3220.0 1
O-Toluidine ND ug/L 11/30/15 19:52 95-53-411/20/15 19:3210.0 1
2,4,5-Trichlorophenol ND ug/L 11/30/15 19:52 95-95-411/20/15 19:3210.0 1
2,4,6-Trichlorophenol ND ug/L 11/30/15 19:52 88-06-211/20/15 19:3210.0 1
1,3,5-Trinitrobenzene ND ug/L 11/30/15 19:52 99-35-411/20/15 19:3210.0 1
Surrogates
Nitrobenzene-d5 (S)71 %11/30/15 19:52 4165-60-011/20/15 19:3221-110 1
2-Fluorobiphenyl (S)74 %11/30/15 19:52 321-60-811/20/15 19:3227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW5R Lab ID:92276295009 Collected:11/17/15 12:20 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)86 %11/30/15 19:52 1718-51-011/20/15 19:3231-107 1
Phenol-d6 (S)20 %11/30/15 19:52 13127-88-311/20/15 19:3210-110 1
2-Fluorophenol (S)31 %11/30/15 19:52 367-12-411/20/15 19:3212-110 1
2,4,6-Tribromophenol (S)78 %11/30/15 19:52 118-79-611/20/15 19:3227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 07:42 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 07:42 75-05-850.0 1
Acrolein ND ug/L 11/20/15 07:42 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 07:42 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 07:42 107-05-12.0 1
Benzene ND ug/L 11/20/15 07:42 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 07:42 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 07:42 75-27-41.0 1
Bromoform ND ug/L 11/20/15 07:42 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 07:42 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 07:42 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 07:42 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 07:42 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 07:42 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 07:42 75-00-31.0 1
Chloroform ND ug/L 11/20/15 07:42 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 07:42 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 07:42 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 07:42 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 07:42 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 07:42 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 07:42 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 07:42 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 07:42 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 07:42 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 07:42 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 07:42 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 07:42 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 07:42 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 07:42 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 07:42 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 07:42 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 07:42 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 07:42 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 07:42 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 07:42 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 07:42 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 07:42 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 07:42 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 07:42 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW5R Lab ID:92276295009 Collected:11/17/15 12:20 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 07:42 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 07:42 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 07:42 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 07:42 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 07:42 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 07:42 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 07:42 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 07:42 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 07:42 107-12-020.0 1
Styrene ND ug/L 11/20/15 07:42 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 07:42 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 07:42 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 07:42 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 07:42 109-99-910.0 1
Toluene ND ug/L 11/20/15 07:42 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 07:42 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 07:42 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 07:42 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 07:42 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 07:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 07:42 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 07:42 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 07:42 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 07:42 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 07:42 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 07:42 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %11/20/15 07:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %11/20/15 07:42 17060-07-070-130 1
Toluene-d8 (S)101 %11/20/15 07:42 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 32300 ug/L 11/29/15 14:5350001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 104000 ug/L 11/19/15 10:21250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/19/15 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 7430 ug/L 11/24/15 19:31 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 16200 ug/L 11/19/15 19:13 16887-00-610001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW5R Lab ID:92276295009 Collected:11/17/15 12:20 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/19/15 04:40 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW1R Lab ID:92276295010 Collected:11/17/15 14:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/17/15 14:101
Field pH 5.4 Std. Units 11/17/15 14:100.10 1
Field Temperature 16.0 deg C 11/17/15 14:100.50 1
Static Water Level 36.15 feet 11/17/15 14:101
Field Specific Conductance 163.2 umhos/cm 11/17/15 14:101.0 1
Oxygen, Dissolved 2.2 mg/L 11/17/15 14:10 7782-44-71
Total Well Depth 60 feet 11/17/15 14:101
REDOX 34.8 mV 11/17/15 14:101
Turbidity 1.0 NTU 11/17/15 14:101.0 1
Odor none 11/17/15 14:101
Appearance clear 11/17/15 14:101
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/20/15 22:55 309-00-211/19/15 14:090.050 1
alpha-BHC ND ug/L 11/20/15 22:55 319-84-611/19/15 14:090.050 1
beta-BHC ND ug/L 11/20/15 22:55 319-85-711/19/15 14:090.050 1
delta-BHC ND ug/L 11/20/15 22:55 319-86-811/19/15 14:090.050 1
gamma-BHC (Lindane)ND ug/L 11/20/15 22:55 58-89-911/19/15 14:090.050 1
Chlordane (Technical)ND ug/L 11/20/15 22:55 57-74-911/19/15 14:090.20 1
4,4'-DDD ND ug/L 11/20/15 22:55 72-54-811/19/15 14:090.050 1
4,4'-DDE ND ug/L 11/20/15 22:55 72-55-911/19/15 14:090.050 1
4,4'-DDT ND ug/L 11/20/15 22:55 50-29-311/19/15 14:090.050 1
Dieldrin ND ug/L 11/20/15 22:55 60-57-111/19/15 14:090.050 1
Endosulfan I ND ug/L 11/20/15 22:55 959-98-811/19/15 14:090.050 1
Endosulfan II ND ug/L 11/20/15 22:55 33213-65-911/19/15 14:090.050 1
Endosulfan sulfate ND ug/L 11/20/15 22:55 1031-07-811/19/15 14:090.050 1
Endrin ND ug/L 11/20/15 22:55 72-20-811/19/15 14:090.050 1
Endrin aldehyde ND ug/L 11/20/15 22:55 7421-93-411/19/15 14:090.050 1
Heptachlor ND ug/L 11/20/15 22:55 76-44-811/19/15 14:090.050 1
Heptachlor epoxide ND ug/L 11/20/15 22:55 1024-57-311/19/15 14:090.050 1
Methoxychlor ND ug/L 11/20/15 22:55 72-43-511/19/15 14:090.15 1
Toxaphene ND ug/L 11/20/15 22:55 8001-35-211/19/15 14:090.20 1
Surrogates
Tetrachloro-m-xylene (S)89 %11/20/15 22:55 877-09-811/19/15 14:0920-130 1
Decachlorobiphenyl (S)85 %11/20/15 22:55 2051-24-311/19/15 14:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/20/15 19:18 12674-11-211/19/15 14:090.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/20/15 19:18 11104-28-211/19/15 14:090.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/20/15 19:18 11141-16-511/19/15 14:090.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/20/15 19:18 53469-21-911/19/15 14:090.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/20/15 19:18 12672-29-611/19/15 14:090.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/20/15 19:18 11097-69-111/19/15 14:090.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/20/15 19:18 11096-82-511/19/15 14:090.50 1
Surrogates
Decachlorobiphenyl (S)86 %11/20/15 19:18 2051-24-311/19/15 14:0910-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW1R Lab ID:92276295010 Collected:11/17/15 14:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/24/15 21:32 94-75-711/23/15 16:350.94 1
Dinoseb ND ug/L 11/24/15 21:32 88-85-711/23/15 16:350.19 1
2,4,5-T ND ug/L 11/24/15 21:32 93-76-511/23/15 16:350.19 1
2,4,5-TP (Silvex)ND ug/L 11/24/15 21:32 93-72-111/23/15 16:350.19 1
Surrogates
2,4-DCAA (S)90 %11/24/15 21:32 19719-28-911/23/15 16:3536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/24/15 08:58 7440-36-011/20/15 18:005.0 1
Arsenic ND ug/L 11/24/15 08:58 7440-38-211/20/15 18:0010.0 1
Barium 207 ug/L 11/24/15 08:58 7440-39-311/20/15 18:005.0 1
Beryllium ND ug/L 11/24/15 08:58 7440-41-711/20/15 18:001.0 1
Cadmium ND ug/L 11/24/15 08:58 7440-43-911/20/15 18:001.0 1
Chromium ND ug/L 11/24/15 08:58 7440-47-311/20/15 18:005.0 1
Cobalt ND ug/L 11/24/15 08:58 7440-48-411/20/15 18:005.0 1
Copper ND ug/L 11/24/15 08:58 7440-50-811/20/15 18:005.0 1
Iron 82.8 ug/L 11/24/15 08:58 7439-89-611/20/15 18:0050.0 1
Lead ND ug/L 11/24/15 08:58 7439-92-111/20/15 18:005.0 1
Manganese 2.8J ug/L 11/24/15 08:58 7439-96-511/20/15 18:005.0 1
Nickel ND ug/L 11/24/15 08:58 7440-02-011/20/15 18:005.0 1
Selenium ND ug/L 11/24/15 08:58 7782-49-211/20/15 18:0010.0 1
Silver ND ug/L 11/24/15 08:58 7440-22-411/20/15 18:005.0 1
Sodium 13200 ug/L 11/24/15 08:58 7440-23-511/20/15 18:0050001
Thallium ND ug/L 11/24/15 08:58 7440-28-011/20/15 18:005.4 1
Tin ND ug/L 11/24/15 08:58 7440-31-511/20/15 18:005.0 1
Vanadium ND ug/L 11/24/15 08:58 7440-62-211/20/15 18:005.0 1
Zinc 5.6J ug/L 11/24/15 08:58 7440-66-611/20/15 18:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 14:18 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 11/30/15 20:20 83-32-911/20/15 19:3210.0 1
Acenaphthylene ND ug/L 11/30/15 20:20 208-96-811/20/15 19:3210.0 1
Acetophenone ND ug/L 11/30/15 20:20 98-86-211/20/15 19:3210.0 1
2-Acetylaminofluorene ND ug/L 11/30/15 20:20 53-96-311/20/15 19:3220.0 1
4-Aminobiphenyl ND ug/L 11/30/15 20:20 92-67-111/20/15 19:3210.0 1
Anthracene ND ug/L 11/30/15 20:20 120-12-711/20/15 19:3210.0 1
Benzo(a)anthracene ND ug/L 11/30/15 20:20 56-55-311/20/15 19:3210.0 1
Benzo(a)pyrene ND ug/L 11/30/15 20:20 50-32-811/20/15 19:3210.0 1
Benzo(b)fluoranthene ND ug/L 11/30/15 20:20 205-99-211/20/15 19:3210.0 1
Benzo(g,h,i)perylene ND ug/L 11/30/15 20:20 191-24-211/20/15 19:3210.0 1
Benzo(k)fluoranthene ND ug/L 11/30/15 20:20 207-08-911/20/15 19:3210.0 1
Benzyl alcohol ND ug/L 11/30/15 20:20 100-51-611/20/15 19:3220.0 1
4-Bromophenylphenyl ether ND ug/L 11/30/15 20:20 101-55-311/20/15 19:3210.0 1
Butylbenzylphthalate ND ug/L 11/30/15 20:20 85-68-711/20/15 19:3210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW1R Lab ID:92276295010 Collected:11/17/15 14:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 11/30/15 20:20 59-50-711/20/15 19:3220.0 1
4-Chloroaniline ND ug/L 11/30/15 20:20 106-47-811/20/15 19:3220.0 1
Chlorobenzilate ND ug/L 11/30/15 20:20 510-15-611/20/15 19:3210.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/30/15 20:20 111-91-111/20/15 19:3210.0 1
bis(2-Chloroethyl) ether ND ug/L 11/30/15 20:20 111-44-411/20/15 19:3210.0 1
bis(2-Chloroisopropyl) ether ND ug/L 11/30/15 20:20 108-60-111/20/15 19:3210.0 1
2-Chloronaphthalene ND ug/L 11/30/15 20:20 91-58-711/20/15 19:3210.0 1
2-Chlorophenol ND ug/L 11/30/15 20:20 95-57-811/20/15 19:3210.0 1
4-Chlorophenylphenyl ether ND ug/L 11/30/15 20:20 7005-72-311/20/15 19:3210.0 1
Chrysene ND ug/L 11/30/15 20:20 218-01-911/20/15 19:3210.0 1
Diallate ND ug/L 11/30/15 20:20 2303-16-411/20/15 19:3210.0 1
Dibenz(a,h)anthracene ND ug/L 11/30/15 20:20 53-70-311/20/15 19:3210.0 1
Dibenzofuran ND ug/L 11/30/15 20:20 132-64-911/20/15 19:3210.0 1
3,3'-Dichlorobenzidine ND ug/L 11/30/15 20:20 91-94-111/20/15 19:3220.0 1
2,4-Dichlorophenol ND ug/L 11/30/15 20:20 120-83-211/20/15 19:3210.0 1
2,6-Dichlorophenol ND ug/L 11/30/15 20:20 87-65-011/20/15 19:3210.0 1
Diethylphthalate ND ug/L 11/30/15 20:20 84-66-211/20/15 19:3210.0 1
Dimethoate ND ug/L 11/30/15 20:20 60-51-511/20/15 19:3210.0 1
P-Dimethylaminoazobenzene ND ug/L 11/30/15 20:20 60-11-711/20/15 19:325.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 11/30/15 20:20 57-97-611/20/15 19:3210.0 1
3,3'-Dimethylbenzidine ND ug/L 11/30/15 20:20 119-93-711/20/15 19:3210.0 1
2,4-Dimethylphenol ND ug/L 11/30/15 20:20 105-67-911/20/15 19:3210.0 1
Dimethylphthalate ND ug/L 11/30/15 20:20 131-11-311/20/15 19:3210.0 1
Di-n-butylphthalate ND ug/L 11/30/15 20:20 84-74-211/20/15 19:3210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/30/15 20:20 534-52-111/20/15 19:3220.0 1
1,3-Dinitrobenzene ND ug/L 11/30/15 20:20 99-65-011/20/15 19:3220.0 1
2,4-Dinitrophenol ND ug/L 11/30/15 20:20 51-28-511/20/15 19:3250.0 1
2,4-Dinitrotoluene ND ug/L 11/30/15 20:20 121-14-211/20/15 19:3210.0 1
2,6-Dinitrotoluene ND ug/L 11/30/15 20:20 606-20-211/20/15 19:3210.0 1
Di-n-octylphthalate ND ug/L 11/30/15 20:20 117-84-011/20/15 19:3210.0 1
Diphenylamine ND ug/L 11/30/15 20:20 122-39-411/20/15 19:3210.0 1
Disulfoton ND ug/L 11/30/15 20:20 298-04-411/20/15 19:3210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/30/15 20:20 117-81-711/20/15 19:326.0 1
Ethyl methanesulfonate ND ug/L 11/30/15 20:20 62-50-011/20/15 19:3220.0 1
Famphur ND ug/L 11/30/15 20:20 52-85-711/20/15 19:3210.0 1
Fluoranthene ND ug/L 11/30/15 20:20 206-44-011/20/15 19:3210.0 1
Fluorene ND ug/L 11/30/15 20:20 86-73-711/20/15 19:3210.0 1
Hexachlorobenzene ND ug/L 11/30/15 20:20 118-74-111/20/15 19:3210.0 1
Hexachlorocyclopentadiene ND ug/L 11/30/15 20:20 77-47-411/20/15 19:3210.0 1
Hexachloroethane ND ug/L 11/30/15 20:20 67-72-111/20/15 19:3210.0 1
Hexachlorophene ND ug/L 11/30/15 20:20 70-30-411/20/15 19:321001
Indeno(1,2,3-cd)pyrene ND ug/L 11/30/15 20:20 193-39-511/20/15 19:3210.0 1
Isodrin ND ug/L 11/30/15 20:20 465-73-611/20/15 19:3220.0 1
Isophorone ND ug/L 11/30/15 20:20 78-59-111/20/15 19:3210.0 1
Isosafrole ND ug/L 11/30/15 20:20 120-58-111/20/15 19:3210.0 1
Kepone ND ug/L 11/30/15 20:20 143-50-011/20/15 19:3210.0 1
Methapyrilene ND ug/L 11/30/15 20:20 91-80-511/20/15 19:3250.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 57 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW1R Lab ID:92276295010 Collected:11/17/15 14:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 11/30/15 20:20 56-49-511/20/15 19:3210.0 1
Methyl methanesulfonate ND ug/L 11/30/15 20:20 66-27-311/20/15 19:325.0 1
2-Methylnaphthalene ND ug/L 11/30/15 20:20 91-57-611/20/15 19:3210.0 1
Methyl parathion ND ug/L 11/30/15 20:20 298-00-011/20/15 19:3210.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/30/15 20:20 95-48-711/20/15 19:3210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/30/15 20:2011/20/15 19:3210.0 1
1-Naphthalenamine ND ug/L 11/30/15 20:20 134-32-711/20/15 19:325.0 1
2-Naphthalenamine ND ug/L 11/30/15 20:20 91-59-811/20/15 19:325.0 1
1,4-Naphthoquinone ND ug/L 11/30/15 20:20 130-15-411/20/15 19:325.0 1
2-Nitroaniline ND ug/L 11/30/15 20:20 88-74-411/20/15 19:3250.0 1
3-Nitroaniline ND ug/L 11/30/15 20:20 99-09-211/20/15 19:3250.0 1
4-Nitroaniline ND ug/L 11/30/15 20:20 100-01-611/20/15 19:3220.0 1
Nitrobenzene ND ug/L 11/30/15 20:20 98-95-311/20/15 19:3210.0 1
2-Nitrophenol ND ug/L 11/30/15 20:20 88-75-511/20/15 19:3210.0 1
4-Nitrophenol ND ug/L 11/30/15 20:20 100-02-711/20/15 19:3250.0 1
5-Nitro-o-toluidine ND ug/L 11/30/15 20:20 99-55-811/20/15 19:3210.0 1
N-Nitrosodiethylamine ND ug/L 11/30/15 20:20 55-18-511/20/15 19:3220.0 1
N-Nitrosodimethylamine ND ug/L 11/30/15 20:20 62-75-911/20/15 19:3210.0 1
N-Nitroso-di-n-butylamine ND ug/L 11/30/15 20:20 924-16-311/20/15 19:3210.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/30/15 20:20 621-64-711/20/15 19:3210.0 1
N-Nitrosodiphenylamine ND ug/L 11/30/15 20:20 86-30-611/20/15 19:3210.0 1
N-Nitrosomethylethylamine ND ug/L 11/30/15 20:20 10595-95-611/20/15 19:3210.0 1
N-Nitrosopiperidine ND ug/L 11/30/15 20:20 100-75-411/20/15 19:3220.0 1
N-Nitrosopyrrolidine ND ug/L 11/30/15 20:20 930-55-211/20/15 19:3210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 11/30/15 20:20 126-68-111/20/15 19:3210.0 1
Parathion (Ethyl parathion)ND ug/L 11/30/15 20:20 56-38-211/20/15 19:3210.0 1
Pentachlorobenzene ND ug/L 11/30/15 20:20 608-93-511/20/15 19:3210.0 1
Pentachloronitrobenzene ND ug/L 11/30/15 20:20 82-68-811/20/15 19:3220.0 1
Pentachlorophenol ND ug/L 11/30/15 20:20 87-86-511/20/15 19:3225.0 1
Phenacetin ND ug/L 11/30/15 20:20 62-44-211/20/15 19:3220.0 1
Phenanthrene ND ug/L 11/30/15 20:20 85-01-811/20/15 19:3210.0 1
Phenol ND ug/L 11/30/15 20:20 108-95-211/20/15 19:3210.0 1
p-Phenylenediamine ND ug/L 11/30/15 20:20 106-50-311/20/15 19:3210.0 1
Phorate ND ug/L 11/30/15 20:20 298-02-211/20/15 19:3210.0 1
Pronamide ND ug/L 11/30/15 20:20 23950-58-511/20/15 19:3210.0 1
Pyrene ND ug/L 11/30/15 20:20 129-00-011/20/15 19:3210.0 1
Safrole ND ug/L 11/30/15 20:20 94-59-711/20/15 19:3210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 11/30/15 20:20 95-94-311/20/15 19:3210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 11/30/15 20:20 58-90-211/20/15 19:3210.0 1
Thionazin ND ug/L 11/30/15 20:20 297-97-211/20/15 19:3220.0 1
O-Toluidine ND ug/L 11/30/15 20:20 95-53-411/20/15 19:3210.0 1
2,4,5-Trichlorophenol ND ug/L 11/30/15 20:20 95-95-411/20/15 19:3210.0 1
2,4,6-Trichlorophenol ND ug/L 11/30/15 20:20 88-06-211/20/15 19:3210.0 1
1,3,5-Trinitrobenzene ND ug/L 11/30/15 20:20 99-35-411/20/15 19:3210.0 1
Surrogates
Nitrobenzene-d5 (S)69 %11/30/15 20:20 4165-60-011/20/15 19:3221-110 1
2-Fluorobiphenyl (S)74 %11/30/15 20:20 321-60-811/20/15 19:3227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW1R Lab ID:92276295010 Collected:11/17/15 14:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)83 %11/30/15 20:20 1718-51-011/20/15 19:3231-107 1
Phenol-d6 (S)22 %11/30/15 20:20 13127-88-311/20/15 19:3210-110 1
2-Fluorophenol (S)33 %11/30/15 20:20 367-12-411/20/15 19:3212-110 1
2,4,6-Tribromophenol (S)70 %11/30/15 20:20 118-79-611/20/15 19:3227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 17:53 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 17:53 75-05-850.0 1
Acrolein ND ug/L 11/20/15 17:53 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 17:53 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 17:53 107-05-12.0 1
Benzene ND ug/L 11/20/15 17:53 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 17:53 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 17:53 75-27-41.0 1
Bromoform ND ug/L 11/20/15 17:53 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 17:53 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 17:53 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 17:53 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 17:53 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 17:53 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 17:53 75-00-31.0 1
Chloroform ND ug/L 11/20/15 17:53 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 17:53 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 17:53 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 17:53 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 17:53 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 17:53 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 17:53 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 17:53 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 17:53 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 17:53 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 17:53 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 17:53 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 17:53 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 17:53 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 17:53 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 17:53 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 17:53 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 17:53 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 17:53 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 17:53 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 17:53 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 17:53 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 17:53 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 17:53 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 17:53 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW1R Lab ID:92276295010 Collected:11/17/15 14:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 17:53 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 17:53 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 17:53 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 17:53 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 17:53 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 17:53 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 17:53 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 17:53 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 17:53 107-12-020.0 1
Styrene ND ug/L 11/20/15 17:53 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 17:53 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 17:53 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 17:53 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 17:53 109-99-910.0 1
Toluene ND ug/L 11/20/15 17:53 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 17:53 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 17:53 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 17:53 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 17:53 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 17:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 17:53 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 17:53 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 17:53 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 17:53 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 17:53 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 17:53 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %11/20/15 17:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/20/15 17:53 17060-07-070-130 1
Toluene-d8 (S)102 %11/20/15 17:53 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 48100 ug/L 11/29/15 15:0550001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 78000 ug/L 11/19/15 10:22250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/19/15 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1070J ug/L 11/24/15 19:45 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 8510 ug/L 11/19/15 19:18 16887-00-610001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW1R Lab ID:92276295010 Collected:11/17/15 14:10 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/19/15 04:43 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW15 Lab ID:92276295011 Collected:11/17/15 16:30 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/17/15 16:301
Field pH 6.2 Std. Units 11/17/15 16:300.10 1
Field Temperature 15.6 deg C 11/17/15 16:300.50 1
Static Water Level 39.44 feet 11/17/15 16:301
Field Specific Conductance 596.2 umhos/cm 11/17/15 16:301.0 1
Oxygen, Dissolved 2.8 mg/L 11/17/15 16:30 7782-44-71
Total Well Depth 50.85 feet 11/17/15 16:301
REDOX 34.8 mV 11/17/15 16:301
Turbidity 154.9 NTU 11/17/15 16:301.0 1
Odor none 11/17/15 16:301
Appearance murky 11/17/15 16:301
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/20/15 23:13 309-00-211/19/15 14:090.050 1
alpha-BHC ND ug/L 11/20/15 23:13 319-84-611/19/15 14:090.050 1
beta-BHC ND ug/L 11/20/15 23:13 319-85-711/19/15 14:090.050 1
delta-BHC ND ug/L 11/20/15 23:13 319-86-811/19/15 14:090.050 1
gamma-BHC (Lindane)ND ug/L 11/20/15 23:13 58-89-911/19/15 14:090.050 1
Chlordane (Technical)ND ug/L 11/20/15 23:13 57-74-911/19/15 14:090.20 1
4,4'-DDD ND ug/L 11/20/15 23:13 72-54-811/19/15 14:090.050 1
4,4'-DDE ND ug/L 11/20/15 23:13 72-55-911/19/15 14:090.050 1
4,4'-DDT ND ug/L 11/20/15 23:13 50-29-311/19/15 14:090.050 1
Dieldrin ND ug/L 11/20/15 23:13 60-57-111/19/15 14:090.050 1
Endosulfan I ND ug/L 11/20/15 23:13 959-98-811/19/15 14:090.050 1
Endosulfan II ND ug/L 11/20/15 23:13 33213-65-911/19/15 14:090.050 1
Endosulfan sulfate ND ug/L 11/20/15 23:13 1031-07-811/19/15 14:090.050 1
Endrin ND ug/L 11/20/15 23:13 72-20-811/19/15 14:090.050 1
Endrin aldehyde ND ug/L 11/20/15 23:13 7421-93-411/19/15 14:090.050 1
Heptachlor ND ug/L 11/20/15 23:13 76-44-811/19/15 14:090.050 1
Heptachlor epoxide ND ug/L 11/20/15 23:13 1024-57-311/19/15 14:090.050 1
Methoxychlor ND ug/L 11/20/15 23:13 72-43-511/19/15 14:090.15 1
Toxaphene ND ug/L 11/20/15 23:13 8001-35-211/19/15 14:090.20 1
Surrogates
Tetrachloro-m-xylene (S)91 %11/20/15 23:13 877-09-811/19/15 14:0920-130 1
Decachlorobiphenyl (S)97 %11/20/15 23:13 2051-24-311/19/15 14:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/20/15 19:39 12674-11-211/19/15 14:090.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/20/15 19:39 11104-28-211/19/15 14:090.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/20/15 19:39 11141-16-511/19/15 14:090.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/20/15 19:39 53469-21-911/19/15 14:090.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/20/15 19:39 12672-29-611/19/15 14:090.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/20/15 19:39 11097-69-111/19/15 14:090.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/20/15 19:39 11096-82-511/19/15 14:090.50 1
Surrogates
Decachlorobiphenyl (S)75 %11/20/15 19:39 2051-24-311/19/15 14:0910-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW15 Lab ID:92276295011 Collected:11/17/15 16:30 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/24/15 22:02 94-75-711/23/15 16:350.94 1
Dinoseb ND ug/L 11/24/15 22:02 88-85-711/23/15 16:350.19 1
2,4,5-T ND ug/L 11/24/15 22:02 93-76-511/23/15 16:350.19 1
2,4,5-TP (Silvex)ND ug/L 11/24/15 22:02 93-72-111/23/15 16:350.19 1
Surrogates
2,4-DCAA (S)125 %11/24/15 22:02 19719-28-911/23/15 16:3536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/24/15 09:01 7440-36-011/20/15 18:005.0 1
Arsenic 4.5J ug/L 11/24/15 09:01 7440-38-211/20/15 18:0010.0 1
Barium 74.0 ug/L 11/24/15 09:01 7440-39-311/20/15 18:005.0 1
Beryllium ND ug/L 11/24/15 09:01 7440-41-711/20/15 18:001.0 1
Cadmium ND ug/L 11/24/15 09:01 7440-43-911/20/15 18:001.0 1
Chromium 5.4 ug/L 11/24/15 09:01 7440-47-311/20/15 18:005.0 1
Cobalt ND ug/L 11/24/15 09:01 7440-48-411/20/15 18:005.0 1
Copper 7.1 ug/L 11/24/15 09:01 7440-50-811/20/15 18:005.0 1
Iron 8180 ug/L 11/24/15 09:01 7439-89-611/20/15 18:0050.0 1
Lead 6.0 ug/L 11/24/15 09:01 7439-92-111/20/15 18:005.0 1
Manganese 297 ug/L 11/24/15 09:01 7439-96-511/20/15 18:005.0 1
Nickel 3.9J ug/L 11/24/15 09:01 7440-02-011/20/15 18:005.0 1
Selenium ND ug/L 11/24/15 09:01 7782-49-211/20/15 18:0010.0 1
Silver ND ug/L 11/24/15 09:01 7440-22-411/20/15 18:005.0 1
Sodium 21800 ug/L 11/24/15 09:01 7440-23-511/20/15 18:0050001
Thallium ND ug/L 11/24/15 09:01 7440-28-011/20/15 18:005.4 1
Tin ND ug/L 11/24/15 09:01 7440-31-511/20/15 18:005.0 1
Vanadium 18.9 ug/L 11/24/15 09:01 7440-62-211/20/15 18:005.0 1
Zinc 35.4 ug/L 11/24/15 09:01 7440-66-611/20/15 18:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 14:21 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 11/30/15 20:48 83-32-911/20/15 19:3210.0 1
Acenaphthylene ND ug/L 11/30/15 20:48 208-96-811/20/15 19:3210.0 1
Acetophenone ND ug/L 11/30/15 20:48 98-86-211/20/15 19:3210.0 1
2-Acetylaminofluorene ND ug/L 11/30/15 20:48 53-96-311/20/15 19:3220.0 1
4-Aminobiphenyl ND ug/L 11/30/15 20:48 92-67-111/20/15 19:3210.0 1
Anthracene ND ug/L 11/30/15 20:48 120-12-711/20/15 19:3210.0 1
Benzo(a)anthracene ND ug/L 11/30/15 20:48 56-55-311/20/15 19:3210.0 1
Benzo(a)pyrene ND ug/L 11/30/15 20:48 50-32-811/20/15 19:3210.0 1
Benzo(b)fluoranthene ND ug/L 11/30/15 20:48 205-99-211/20/15 19:3210.0 1
Benzo(g,h,i)perylene ND ug/L 11/30/15 20:48 191-24-211/20/15 19:3210.0 1
Benzo(k)fluoranthene ND ug/L 11/30/15 20:48 207-08-911/20/15 19:3210.0 1
Benzyl alcohol ND ug/L 11/30/15 20:48 100-51-611/20/15 19:3220.0 1
4-Bromophenylphenyl ether ND ug/L 11/30/15 20:48 101-55-311/20/15 19:3210.0 1
Butylbenzylphthalate ND ug/L 11/30/15 20:48 85-68-711/20/15 19:3210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW15 Lab ID:92276295011 Collected:11/17/15 16:30 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 11/30/15 20:48 59-50-711/20/15 19:3220.0 1
4-Chloroaniline ND ug/L 11/30/15 20:48 106-47-811/20/15 19:3220.0 1
Chlorobenzilate ND ug/L 11/30/15 20:48 510-15-611/20/15 19:3210.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/30/15 20:48 111-91-111/20/15 19:3210.0 1
bis(2-Chloroethyl) ether ND ug/L 11/30/15 20:48 111-44-411/20/15 19:3210.0 1
bis(2-Chloroisopropyl) ether ND ug/L 11/30/15 20:48 108-60-111/20/15 19:3210.0 1
2-Chloronaphthalene ND ug/L 11/30/15 20:48 91-58-711/20/15 19:3210.0 1
2-Chlorophenol ND ug/L 11/30/15 20:48 95-57-811/20/15 19:3210.0 1
4-Chlorophenylphenyl ether ND ug/L 11/30/15 20:48 7005-72-311/20/15 19:3210.0 1
Chrysene ND ug/L 11/30/15 20:48 218-01-911/20/15 19:3210.0 1
Diallate ND ug/L 11/30/15 20:48 2303-16-411/20/15 19:3210.0 1
Dibenz(a,h)anthracene ND ug/L 11/30/15 20:48 53-70-311/20/15 19:3210.0 1
Dibenzofuran ND ug/L 11/30/15 20:48 132-64-911/20/15 19:3210.0 1
3,3'-Dichlorobenzidine ND ug/L 11/30/15 20:48 91-94-111/20/15 19:3220.0 1
2,4-Dichlorophenol ND ug/L 11/30/15 20:48 120-83-211/20/15 19:3210.0 1
2,6-Dichlorophenol ND ug/L 11/30/15 20:48 87-65-011/20/15 19:3210.0 1
Diethylphthalate ND ug/L 11/30/15 20:48 84-66-211/20/15 19:3210.0 1
Dimethoate ND ug/L 11/30/15 20:48 60-51-511/20/15 19:3210.0 1
P-Dimethylaminoazobenzene ND ug/L 11/30/15 20:48 60-11-711/20/15 19:325.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 11/30/15 20:48 57-97-611/20/15 19:3210.0 1
3,3'-Dimethylbenzidine ND ug/L 11/30/15 20:48 119-93-711/20/15 19:3210.0 1
2,4-Dimethylphenol ND ug/L 11/30/15 20:48 105-67-911/20/15 19:3210.0 1
Dimethylphthalate ND ug/L 11/30/15 20:48 131-11-311/20/15 19:3210.0 1
Di-n-butylphthalate ND ug/L 11/30/15 20:48 84-74-211/20/15 19:3210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/30/15 20:48 534-52-111/20/15 19:3220.0 1
1,3-Dinitrobenzene ND ug/L 11/30/15 20:48 99-65-011/20/15 19:3220.0 1
2,4-Dinitrophenol ND ug/L 11/30/15 20:48 51-28-511/20/15 19:3250.0 1
2,4-Dinitrotoluene ND ug/L 11/30/15 20:48 121-14-211/20/15 19:3210.0 1
2,6-Dinitrotoluene ND ug/L 11/30/15 20:48 606-20-211/20/15 19:3210.0 1
Di-n-octylphthalate ND ug/L 11/30/15 20:48 117-84-011/20/15 19:3210.0 1
Diphenylamine ND ug/L 11/30/15 20:48 122-39-411/20/15 19:3210.0 1
Disulfoton ND ug/L 11/30/15 20:48 298-04-411/20/15 19:3210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/30/15 20:48 117-81-711/20/15 19:326.0 1
Ethyl methanesulfonate ND ug/L 11/30/15 20:48 62-50-011/20/15 19:3220.0 1
Famphur ND ug/L 11/30/15 20:48 52-85-711/20/15 19:3210.0 1
Fluoranthene ND ug/L 11/30/15 20:48 206-44-011/20/15 19:3210.0 1
Fluorene ND ug/L 11/30/15 20:48 86-73-711/20/15 19:3210.0 1
Hexachlorobenzene ND ug/L 11/30/15 20:48 118-74-111/20/15 19:3210.0 1
Hexachlorocyclopentadiene ND ug/L 11/30/15 20:48 77-47-411/20/15 19:3210.0 1
Hexachloroethane ND ug/L 11/30/15 20:48 67-72-111/20/15 19:3210.0 1
Hexachlorophene ND ug/L 11/30/15 20:48 70-30-411/20/15 19:321001
Indeno(1,2,3-cd)pyrene ND ug/L 11/30/15 20:48 193-39-511/20/15 19:3210.0 1
Isodrin ND ug/L 11/30/15 20:48 465-73-611/20/15 19:3220.0 1
Isophorone ND ug/L 11/30/15 20:48 78-59-111/20/15 19:3210.0 1
Isosafrole ND ug/L 11/30/15 20:48 120-58-111/20/15 19:3210.0 1
Kepone ND ug/L 11/30/15 20:48 143-50-011/20/15 19:3210.0 1
Methapyrilene ND ug/L 11/30/15 20:48 91-80-511/20/15 19:3250.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW15 Lab ID:92276295011 Collected:11/17/15 16:30 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 11/30/15 20:48 56-49-511/20/15 19:3210.0 1
Methyl methanesulfonate ND ug/L 11/30/15 20:48 66-27-311/20/15 19:325.0 1
2-Methylnaphthalene ND ug/L 11/30/15 20:48 91-57-611/20/15 19:3210.0 1
Methyl parathion ND ug/L 11/30/15 20:48 298-00-011/20/15 19:3210.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/30/15 20:48 95-48-711/20/15 19:3210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/30/15 20:4811/20/15 19:3210.0 1
1-Naphthalenamine ND ug/L 11/30/15 20:48 134-32-711/20/15 19:325.0 1
2-Naphthalenamine ND ug/L 11/30/15 20:48 91-59-811/20/15 19:325.0 1
1,4-Naphthoquinone ND ug/L 11/30/15 20:48 130-15-411/20/15 19:325.0 1
2-Nitroaniline ND ug/L 11/30/15 20:48 88-74-411/20/15 19:3250.0 1
3-Nitroaniline ND ug/L 11/30/15 20:48 99-09-211/20/15 19:3250.0 1
4-Nitroaniline ND ug/L 11/30/15 20:48 100-01-611/20/15 19:3220.0 1
Nitrobenzene ND ug/L 11/30/15 20:48 98-95-311/20/15 19:3210.0 1
2-Nitrophenol ND ug/L 11/30/15 20:48 88-75-511/20/15 19:3210.0 1
4-Nitrophenol ND ug/L 11/30/15 20:48 100-02-711/20/15 19:3250.0 1
5-Nitro-o-toluidine ND ug/L 11/30/15 20:48 99-55-811/20/15 19:3210.0 1
N-Nitrosodiethylamine ND ug/L 11/30/15 20:48 55-18-511/20/15 19:3220.0 1
N-Nitrosodimethylamine ND ug/L 11/30/15 20:48 62-75-911/20/15 19:3210.0 1
N-Nitroso-di-n-butylamine ND ug/L 11/30/15 20:48 924-16-311/20/15 19:3210.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/30/15 20:48 621-64-711/20/15 19:3210.0 1
N-Nitrosodiphenylamine ND ug/L 11/30/15 20:48 86-30-611/20/15 19:3210.0 1
N-Nitrosomethylethylamine ND ug/L 11/30/15 20:48 10595-95-611/20/15 19:3210.0 1
N-Nitrosopiperidine ND ug/L 11/30/15 20:48 100-75-411/20/15 19:3220.0 1
N-Nitrosopyrrolidine ND ug/L 11/30/15 20:48 930-55-211/20/15 19:3210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 11/30/15 20:48 126-68-111/20/15 19:3210.0 1
Parathion (Ethyl parathion)ND ug/L 11/30/15 20:48 56-38-211/20/15 19:3210.0 1
Pentachlorobenzene ND ug/L 11/30/15 20:48 608-93-511/20/15 19:3210.0 1
Pentachloronitrobenzene ND ug/L 11/30/15 20:48 82-68-811/20/15 19:3220.0 1
Pentachlorophenol ND ug/L 11/30/15 20:48 87-86-511/20/15 19:3225.0 1
Phenacetin ND ug/L 11/30/15 20:48 62-44-211/20/15 19:3220.0 1
Phenanthrene ND ug/L 11/30/15 20:48 85-01-811/20/15 19:3210.0 1
Phenol ND ug/L 11/30/15 20:48 108-95-211/20/15 19:3210.0 1
p-Phenylenediamine ND ug/L 11/30/15 20:48 106-50-311/20/15 19:3210.0 1
Phorate ND ug/L 11/30/15 20:48 298-02-211/20/15 19:3210.0 1
Pronamide ND ug/L 11/30/15 20:48 23950-58-511/20/15 19:3210.0 1
Pyrene ND ug/L 11/30/15 20:48 129-00-011/20/15 19:3210.0 1
Safrole ND ug/L 11/30/15 20:48 94-59-711/20/15 19:3210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 11/30/15 20:48 95-94-311/20/15 19:3210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 11/30/15 20:48 58-90-211/20/15 19:3210.0 1
Thionazin ND ug/L 11/30/15 20:48 297-97-211/20/15 19:3220.0 1
O-Toluidine ND ug/L 11/30/15 20:48 95-53-411/20/15 19:3210.0 1
2,4,5-Trichlorophenol ND ug/L 11/30/15 20:48 95-95-411/20/15 19:3210.0 1
2,4,6-Trichlorophenol ND ug/L 11/30/15 20:48 88-06-211/20/15 19:3210.0 1
1,3,5-Trinitrobenzene ND ug/L 11/30/15 20:48 99-35-411/20/15 19:3210.0 1
Surrogates
Nitrobenzene-d5 (S)68 %11/30/15 20:48 4165-60-011/20/15 19:3221-110 1
2-Fluorobiphenyl (S)77 %11/30/15 20:48 321-60-811/20/15 19:3227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW15 Lab ID:92276295011 Collected:11/17/15 16:30 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)74 %11/30/15 20:48 1718-51-011/20/15 19:3231-107 1
Phenol-d6 (S)21 %11/30/15 20:48 13127-88-311/20/15 19:3210-110 1
2-Fluorophenol (S)33 %11/30/15 20:48 367-12-411/20/15 19:3212-110 1
2,4,6-Tribromophenol (S)79 %11/30/15 20:48 118-79-611/20/15 19:3227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 18:10 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 18:10 75-05-850.0 1
Acrolein ND ug/L 11/20/15 18:10 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 18:10 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 18:10 107-05-12.0 1
Benzene ND ug/L 11/20/15 18:10 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 18:10 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 18:10 75-27-41.0 1
Bromoform ND ug/L 11/20/15 18:10 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 18:10 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 18:10 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 18:10 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 18:10 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 18:10 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 18:10 75-00-31.0 1
Chloroform 0.44J ug/L 11/20/15 18:10 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 18:10 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 18:10 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 18:10 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 18:10 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 18:10 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 18:10 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 18:10 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 18:10 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 18:10 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 18:10 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 18:10 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 18:10 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 18:10 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 18:10 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 18:10 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 18:10 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 18:10 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 18:10 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 18:10 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 18:10 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 18:10 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 18:10 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 18:10 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 18:10 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW15 Lab ID:92276295011 Collected:11/17/15 16:30 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 18:10 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 18:10 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 18:10 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 18:10 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 18:10 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 18:10 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 18:10 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 18:10 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 18:10 107-12-020.0 1
Styrene ND ug/L 11/20/15 18:10 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 18:10 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 18:10 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 18:10 127-18-41.0 1
Tetrahydrofuran 19.8 ug/L 11/20/15 18:10 109-99-910.0 1
Toluene ND ug/L 11/20/15 18:10 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 18:10 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 18:10 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 18:10 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 18:10 79-01-61.0 1
Trichlorofluoromethane 4.8 ug/L 11/20/15 18:10 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 18:10 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 18:10 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 18:10 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 18:10 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 18:10 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 18:10 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %11/20/15 18:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/20/15 18:10 17060-07-070-130 1
Toluene-d8 (S)101 %11/20/15 18:10 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 103000 ug/L 11/29/15 15:1750001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 362000 ug/L 11/19/15 10:23250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/19/15 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 70000 ug/L 11/24/15 20:25 14808-79-8 M140002
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 113000 ug/L 11/19/15 19:19 16887-00-650005
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW15 Lab ID:92276295011 Collected:11/17/15 16:30 Received:11/17/15 19:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/19/15 04:46 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW2R Lab ID:92276295012 Collected:11/18/15 09:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/18/15 09:001
Field pH 6.1 Std. Units 11/18/15 09:000.10 1
Field Temperature 15.9 deg C 11/18/15 09:000.50 1
Static Water Level 8.17 feet 11/18/15 09:001
Field Specific Conductance 1044 umhos/cm 11/18/15 09:001.0 1
Oxygen, Dissolved 2.0 mg/L 11/18/15 09:00 7782-44-71
Total Well Depth 21.0 feet 11/18/15 09:001
REDOX -35.2 mV 11/18/15 09:001
Turbidity 5.6 NTU 11/18/15 09:001.0 1
Odor none 11/18/15 09:001
Appearance clear 11/18/15 09:001
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/25/15 16:19 309-00-211/24/15 11:000.050 1
alpha-BHC ND ug/L 11/25/15 16:19 319-84-611/24/15 11:000.050 1
beta-BHC ND ug/L 11/25/15 16:19 319-85-711/24/15 11:000.050 1
delta-BHC ND ug/L 11/25/15 16:19 319-86-811/24/15 11:000.050 1
gamma-BHC (Lindane)ND ug/L 11/25/15 16:19 58-89-911/24/15 11:000.050 1
Chlordane (Technical)ND ug/L 11/25/15 16:19 57-74-911/24/15 11:000.20 1
4,4'-DDD ND ug/L 11/25/15 16:19 72-54-811/24/15 11:000.050 1
4,4'-DDE ND ug/L 11/25/15 16:19 72-55-911/24/15 11:000.050 1
4,4'-DDT ND ug/L 11/25/15 16:19 50-29-311/24/15 11:000.050 1
Dieldrin ND ug/L 11/25/15 16:19 60-57-111/24/15 11:000.050 1
Endosulfan I ND ug/L 11/25/15 16:19 959-98-811/24/15 11:000.050 1
Endosulfan II ND ug/L 11/25/15 16:19 33213-65-911/24/15 11:000.050 1
Endosulfan sulfate ND ug/L 11/25/15 16:19 1031-07-811/24/15 11:000.050 1
Endrin ND ug/L 11/25/15 16:19 72-20-811/24/15 11:000.050 1
Endrin aldehyde ND ug/L 11/25/15 16:19 7421-93-411/24/15 11:000.050 1
Heptachlor ND ug/L 11/25/15 16:19 76-44-811/24/15 11:000.050 1
Heptachlor epoxide ND ug/L 11/25/15 16:19 1024-57-311/24/15 11:000.050 1
Methoxychlor ND ug/L 11/25/15 16:19 72-43-511/24/15 11:000.15 1
Toxaphene ND ug/L 11/25/15 16:19 8001-35-211/24/15 11:000.20 1
Surrogates
Tetrachloro-m-xylene (S)68 %11/25/15 16:19 877-09-811/24/15 11:0020-130 1
Decachlorobiphenyl (S)65 %11/25/15 16:19 2051-24-311/24/15 11:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/25/15 16:40 12674-11-211/24/15 11:000.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/25/15 16:40 11104-28-211/24/15 11:000.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/25/15 16:40 11141-16-511/24/15 11:000.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/25/15 16:40 53469-21-911/24/15 11:000.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/25/15 16:40 12672-29-611/24/15 11:000.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/25/15 16:40 11097-69-111/24/15 11:000.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/25/15 16:40 11096-82-511/24/15 11:000.50 1
Surrogates
Decachlorobiphenyl (S)69 %11/25/15 16:40 2051-24-311/24/15 11:0010-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW2R Lab ID:92276295012 Collected:11/18/15 09:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/26/15 00:18 94-75-711/24/15 16:550.94 1
Dinoseb ND ug/L 11/26/15 00:18 88-85-711/24/15 16:550.19 1
2,4,5-T ND ug/L 11/26/15 00:18 93-76-511/24/15 16:550.19 1
2,4,5-TP (Silvex)ND ug/L 11/26/15 00:18 93-72-111/24/15 16:550.19 1
Surrogates
2,4-DCAA (S)105 %11/26/15 00:18 19719-28-911/24/15 16:5536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/24/15 09:48 7440-36-011/20/15 18:005.0 1
Arsenic ND ug/L 11/24/15 09:48 7440-38-211/20/15 18:0010.0 1
Barium 279 ug/L 11/24/15 09:48 7440-39-311/20/15 18:005.0 1
Beryllium ND ug/L 11/24/15 09:48 7440-41-711/20/15 18:001.0 1
Cadmium ND ug/L 11/24/15 09:48 7440-43-911/20/15 18:001.0 1
Chromium ND ug/L 11/24/15 09:48 7440-47-311/20/15 18:005.0 1
Cobalt 17.4 ug/L 11/24/15 09:48 7440-48-411/20/15 18:005.0 1
Copper ND ug/L 11/24/15 09:48 7440-50-811/20/15 18:005.0 1
Iron 3080 ug/L 11/24/15 09:48 7439-89-611/20/15 18:0050.0 1
Lead ND ug/L 11/24/15 09:48 7439-92-111/20/15 18:005.0 1
Manganese 9010 ug/L 11/24/15 09:48 7439-96-511/20/15 18:005.0 1
Nickel 18.0 ug/L 11/24/15 09:48 7440-02-011/20/15 18:005.0 1
Selenium ND ug/L 11/24/15 09:48 7782-49-211/20/15 18:0010.0 1
Silver ND ug/L 11/24/15 09:48 7440-22-411/20/15 18:005.0 1
Sodium 61400 ug/L 11/24/15 09:48 7440-23-511/20/15 18:0050001
Thallium ND ug/L 11/24/15 09:48 7440-28-011/20/15 18:005.4 1
Tin ND ug/L 11/24/15 09:48 7440-31-511/20/15 18:005.0 1
Vanadium 11.9 ug/L 11/24/15 09:48 7440-62-211/20/15 18:005.0 1
Zinc 5.8J ug/L 11/24/15 09:48 7440-66-611/20/15 18:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 15:08 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/02/15 13:01 83-32-911/25/15 10:3610.0 1
Acenaphthylene ND ug/L 12/02/15 13:01 208-96-811/25/15 10:3610.0 1
Acetophenone ND ug/L 12/02/15 13:01 98-86-211/25/15 10:3610.0 1
2-Acetylaminofluorene ND ug/L 12/02/15 13:01 53-96-3 L211/25/15 10:3620.0 1
4-Aminobiphenyl ND ug/L 12/02/15 13:01 92-67-111/25/15 10:3610.0 1
Anthracene ND ug/L 12/02/15 13:01 120-12-711/25/15 10:3610.0 1
Benzo(a)anthracene ND ug/L 12/02/15 13:01 56-55-311/25/15 10:3610.0 1
Benzo(a)pyrene ND ug/L 12/02/15 13:01 50-32-811/25/15 10:3610.0 1
Benzo(b)fluoranthene ND ug/L 12/02/15 13:01 205-99-2 M111/25/15 10:3610.0 1
Benzo(g,h,i)perylene ND ug/L 12/02/15 13:01 191-24-211/25/15 10:3610.0 1
Benzo(k)fluoranthene ND ug/L 12/02/15 13:01 207-08-9 M111/25/15 10:3610.0 1
Benzyl alcohol ND ug/L 12/02/15 13:01 100-51-611/25/15 10:3620.0 1
4-Bromophenylphenyl ether ND ug/L 12/02/15 13:01 101-55-311/25/15 10:3610.0 1
Butylbenzylphthalate ND ug/L 12/02/15 13:01 85-68-7 M111/25/15 10:3610.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW2R Lab ID:92276295012 Collected:11/18/15 09:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/02/15 13:01 59-50-711/25/15 10:3620.0 1
4-Chloroaniline ND ug/L 12/02/15 13:01 106-47-811/25/15 10:3620.0 1
Chlorobenzilate ND ug/L 12/02/15 13:01 510-15-611/25/15 10:3610.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/02/15 13:01 111-91-111/25/15 10:3610.0 1
bis(2-Chloroethyl) ether ND ug/L 12/02/15 13:01 111-44-411/25/15 10:3610.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/02/15 13:01 108-60-111/25/15 10:3610.0 1
2-Chloronaphthalene ND ug/L 12/02/15 13:01 91-58-711/25/15 10:3610.0 1
2-Chlorophenol ND ug/L 12/02/15 13:01 95-57-811/25/15 10:3610.0 1
4-Chlorophenylphenyl ether ND ug/L 12/02/15 13:01 7005-72-311/25/15 10:3610.0 1
Chrysene ND ug/L 12/02/15 13:01 218-01-911/25/15 10:3610.0 1
Diallate ND ug/L 12/02/15 13:01 2303-16-411/25/15 10:3610.0 1
Dibenz(a,h)anthracene ND ug/L 12/02/15 13:01 53-70-311/25/15 10:3610.0 1
Dibenzofuran ND ug/L 12/02/15 13:01 132-64-911/25/15 10:3610.0 1
3,3'-Dichlorobenzidine ND ug/L 12/02/15 13:01 91-94-1 M111/25/15 10:3620.0 1
2,4-Dichlorophenol ND ug/L 12/02/15 13:01 120-83-211/25/15 10:3610.0 1
2,6-Dichlorophenol ND ug/L 12/02/15 13:01 87-65-011/25/15 10:3610.0 1
Diethylphthalate ND ug/L 12/02/15 13:01 84-66-211/25/15 10:3610.0 1
Dimethoate ND ug/L 12/02/15 13:01 60-51-511/25/15 10:3610.0 1
P-Dimethylaminoazobenzene ND ug/L 12/02/15 13:01 60-11-7 M111/25/15 10:365.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/02/15 13:01 57-97-611/25/15 10:3610.0 1
3,3'-Dimethylbenzidine ND ug/L 12/02/15 13:01 119-93-7 M111/25/15 10:3610.0 1
2,4-Dimethylphenol ND ug/L 12/02/15 13:01 105-67-911/25/15 10:3610.0 1
Dimethylphthalate ND ug/L 12/02/15 13:01 131-11-311/25/15 10:3610.0 1
Di-n-butylphthalate ND ug/L 12/02/15 13:01 84-74-2 M111/25/15 10:3610.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/02/15 13:01 534-52-111/25/15 10:3620.0 1
1,3-Dinitrobenzene ND ug/L 12/02/15 13:01 99-65-011/25/15 10:3620.0 1
2,4-Dinitrophenol ND ug/L 12/02/15 13:01 51-28-511/25/15 10:3650.0 1
2,4-Dinitrotoluene 5.9J ug/L 12/02/15 13:01 121-14-211/25/15 10:3610.0 1
2,6-Dinitrotoluene 8.1J ug/L 12/02/15 13:01 606-20-211/25/15 10:3610.0 1
Di-n-octylphthalate ND ug/L 12/02/15 13:01 117-84-011/25/15 10:3610.0 1
Diphenylamine ND ug/L 12/02/15 13:01 122-39-411/25/15 10:3610.0 1
Disulfoton ND ug/L 12/02/15 13:01 298-04-411/25/15 10:3610.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/02/15 13:01 117-81-7 M111/25/15 10:366.0 1
Ethyl methanesulfonate ND ug/L 12/02/15 13:01 62-50-011/25/15 10:3620.0 1
Famphur ND ug/L 12/02/15 13:01 52-85-711/25/15 10:3610.0 1
Fluoranthene ND ug/L 12/02/15 13:01 206-44-011/25/15 10:3610.0 1
Fluorene ND ug/L 12/02/15 13:01 86-73-711/25/15 10:3610.0 1
Hexachlorobenzene ND ug/L 12/02/15 13:01 118-74-111/25/15 10:3610.0 1
Hexachlorocyclopentadiene ND ug/L 12/02/15 13:01 77-47-411/25/15 10:3610.0 1
Hexachloroethane ND ug/L 12/02/15 13:01 67-72-111/25/15 10:3610.0 1
Hexachlorophene ND ug/L 12/02/15 13:01 70-30-4 M111/25/15 10:361001
Indeno(1,2,3-cd)pyrene ND ug/L 12/02/15 13:01 193-39-511/25/15 10:3610.0 1
Isodrin ND ug/L 12/02/15 13:01 465-73-611/25/15 10:3620.0 1
Isophorone ND ug/L 12/02/15 13:01 78-59-111/25/15 10:3610.0 1
Isosafrole ND ug/L 12/02/15 13:01 120-58-111/25/15 10:3610.0 1
Kepone ND ug/L 12/02/15 13:01 143-50-011/25/15 10:3610.0 1
Methapyrilene ND ug/L 12/02/15 13:01 91-80-511/25/15 10:3650.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW2R Lab ID:92276295012 Collected:11/18/15 09:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/02/15 13:01 56-49-511/25/15 10:3610.0 1
Methyl methanesulfonate ND ug/L 12/02/15 13:01 66-27-311/25/15 10:365.0 1
2-Methylnaphthalene ND ug/L 12/02/15 13:01 91-57-611/25/15 10:3610.0 1
Methyl parathion ND ug/L 12/02/15 13:01 298-00-011/25/15 10:3610.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/02/15 13:01 95-48-711/25/15 10:3610.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/02/15 13:01 M111/25/15 10:3610.0 1
1-Naphthalenamine ND ug/L 12/02/15 13:01 134-32-711/25/15 10:365.0 1
2-Naphthalenamine ND ug/L 12/02/15 13:01 91-59-811/25/15 10:365.0 1
1,4-Naphthoquinone ND ug/L 12/02/15 13:01 130-15-411/25/15 10:365.0 1
2-Nitroaniline ND ug/L 12/02/15 13:01 88-74-411/25/15 10:3650.0 1
3-Nitroaniline ND ug/L 12/02/15 13:01 99-09-211/25/15 10:3650.0 1
4-Nitroaniline ND ug/L 12/02/15 13:01 100-01-611/25/15 10:3620.0 1
Nitrobenzene ND ug/L 12/02/15 13:01 98-95-311/25/15 10:3610.0 1
2-Nitrophenol ND ug/L 12/02/15 13:01 88-75-511/25/15 10:3610.0 1
4-Nitrophenol ND ug/L 12/02/15 13:01 100-02-711/25/15 10:3650.0 1
5-Nitro-o-toluidine ND ug/L 12/02/15 13:01 99-55-811/25/15 10:3610.0 1
N-Nitrosodiethylamine ND ug/L 12/02/15 13:01 55-18-511/25/15 10:3620.0 1
N-Nitrosodimethylamine ND ug/L 12/02/15 13:01 62-75-911/25/15 10:3610.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/02/15 13:01 924-16-311/25/15 10:3610.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/02/15 13:01 621-64-711/25/15 10:3610.0 1
N-Nitrosodiphenylamine ND ug/L 12/02/15 13:01 86-30-611/25/15 10:3610.0 1
N-Nitrosomethylethylamine ND ug/L 12/02/15 13:01 10595-95-611/25/15 10:3610.0 1
N-Nitrosopiperidine ND ug/L 12/02/15 13:01 100-75-411/25/15 10:3620.0 1
N-Nitrosopyrrolidine ND ug/L 12/02/15 13:01 930-55-211/25/15 10:3610.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/02/15 13:01 126-68-111/25/15 10:3610.0 1
Parathion (Ethyl parathion)ND ug/L 12/02/15 13:01 56-38-211/25/15 10:3610.0 1
Pentachlorobenzene ND ug/L 12/02/15 13:01 608-93-511/25/15 10:3610.0 1
Pentachloronitrobenzene ND ug/L 12/02/15 13:01 82-68-811/25/15 10:3620.0 1
Pentachlorophenol ND ug/L 12/02/15 13:01 87-86-511/25/15 10:3625.0 1
Phenacetin ND ug/L 12/02/15 13:01 62-44-211/25/15 10:3620.0 1
Phenanthrene ND ug/L 12/02/15 13:01 85-01-811/25/15 10:3610.0 1
Phenol ND ug/L 12/02/15 13:01 108-95-211/25/15 10:3610.0 1
p-Phenylenediamine ND ug/L 12/02/15 13:01 106-50-311/25/15 10:3610.0 1
Phorate ND ug/L 12/02/15 13:01 298-02-211/25/15 10:3610.0 1
Pronamide ND ug/L 12/02/15 13:01 23950-58-511/25/15 10:3610.0 1
Pyrene ND ug/L 12/02/15 13:01 129-00-011/25/15 10:3610.0 1
Safrole ND ug/L 12/02/15 13:01 94-59-711/25/15 10:3610.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/02/15 13:01 95-94-311/25/15 10:3610.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/02/15 13:01 58-90-2 M111/25/15 10:3610.0 1
Thionazin ND ug/L 12/02/15 13:01 297-97-211/25/15 10:3620.0 1
O-Toluidine ND ug/L 12/02/15 13:01 95-53-411/25/15 10:3610.0 1
2,4,5-Trichlorophenol ND ug/L 12/02/15 13:01 95-95-411/25/15 10:3610.0 1
2,4,6-Trichlorophenol ND ug/L 12/02/15 13:01 88-06-211/25/15 10:3610.0 1
1,3,5-Trinitrobenzene ND ug/L 12/02/15 13:01 99-35-4 L311/25/15 10:3610.0 1
Surrogates
Nitrobenzene-d5 (S)77 %12/02/15 13:01 4165-60-011/25/15 10:3621-110 1
2-Fluorobiphenyl (S)82 %12/02/15 13:01 321-60-811/25/15 10:3627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW2R Lab ID:92276295012 Collected:11/18/15 09:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)79 %12/02/15 13:01 1718-51-011/25/15 10:3631-107 1
Phenol-d6 (S)30 %12/02/15 13:01 13127-88-311/25/15 10:3610-110 1
2-Fluorophenol (S)43 %12/02/15 13:01 367-12-411/25/15 10:3612-110 1
2,4,6-Tribromophenol (S)93 %12/02/15 13:01 118-79-611/25/15 10:3627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 18:28 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 18:28 75-05-850.0 1
Acrolein ND ug/L 11/20/15 18:28 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 18:28 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 18:28 107-05-12.0 1
Benzene 1.5 ug/L 11/20/15 18:28 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 18:28 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 18:28 75-27-41.0 1
Bromoform ND ug/L 11/20/15 18:28 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 18:28 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 18:28 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 18:28 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 18:28 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 18:28 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 18:28 75-00-31.0 1
Chloroform ND ug/L 11/20/15 18:28 67-66-31.0 1
Chloromethane 0.25J ug/L 11/20/15 18:28 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 18:28 126-99-8 M15.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 18:28 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 18:28 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 18:28 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 18:28 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 18:28 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 18:28 541-73-11.0 1
1,4-Dichlorobenzene 0.38J ug/L 11/20/15 18:28 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 18:28 110-57-6 M11.0 1
Dichlorodifluoromethane 0.26J ug/L 11/20/15 18:28 75-71-8 M11.0 1
1,1-Dichloroethane ND ug/L 11/20/15 18:28 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 18:28 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 18:28 75-35-41.0 1
cis-1,2-Dichloroethene 0.26J ug/L 11/20/15 18:28 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 18:28 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 18:28 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 18:28 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 18:28 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 18:28 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 18:28 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 18:28 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 18:28 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 18:28 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 73 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW2R Lab ID:92276295012 Collected:11/18/15 09:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 18:28 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 18:28 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 18:28 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 18:28 126-98-710.0 1
Methylene Chloride 1.3 ug/L 11/20/15 18:28 75-09-2 C91.0 1
Methyl methacrylate ND ug/L 11/20/15 18:28 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 18:28 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 18:28 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 18:28 107-12-020.0 1
Styrene ND ug/L 11/20/15 18:28 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 18:28 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 18:28 79-34-51.0 1
Tetrachloroethene 0.95J ug/L 11/20/15 18:28 127-18-41.0 1
Tetrahydrofuran 35.8 ug/L 11/20/15 18:28 109-99-910.0 1
Toluene 0.27J ug/L 11/20/15 18:28 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 18:28 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 18:28 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 18:28 79-00-51.0 1
Trichloroethene 0.66J ug/L 11/20/15 18:28 79-01-61.0 1
Trichlorofluoromethane 1.0 ug/L 11/20/15 18:28 75-69-4 M11.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 18:28 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 18:28 108-05-42.0 1
Vinyl chloride 0.75J ug/L 11/20/15 18:28 75-01-4 M11.0 1
Xylene (Total)ND ug/L 11/20/15 18:28 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 18:28 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 18:28 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/20/15 18:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/20/15 18:28 17060-07-070-130 1
Toluene-d8 (S)101 %11/20/15 18:28 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 440000 ug/L 11/29/15 20:1350001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 806000 ug/L 11/22/15 11:03500001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/23/15 23:30 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 115000 ug/L 11/24/15 23:08 14808-79-8100005
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 48700 ug/L 11/30/15 19:16 16887-00-650005
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW2R Lab ID:92276295012 Collected:11/18/15 09:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 7.5J ug/L 11/25/15 02:45 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW8 Lab ID:92276295013 Collected:11/18/15 11:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/18/15 11:001
Field pH 5.4 Std. Units 11/18/15 11:000.10 1
Field Temperature 15.6 deg C 11/18/15 11:000.50 1
Static Water Level 18.28 feet 11/18/15 11:001
Field Specific Conductance 58.4 umhos/cm 11/18/15 11:001.0 1
Oxygen, Dissolved 4.4 mg/L 11/18/15 11:00 7782-44-71
Total Well Depth 27 feet 11/18/15 11:001
REDOX 4.0 mV 11/18/15 11:001
Turbidity 1.6 NTU 11/18/15 11:001.0 1
Odor none 11/18/15 11:001
Appearance clear 11/18/15 11:001
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/25/15 16:37 309-00-211/24/15 11:000.050 1
alpha-BHC ND ug/L 11/25/15 16:37 319-84-611/24/15 11:000.050 1
beta-BHC ND ug/L 11/25/15 16:37 319-85-711/24/15 11:000.050 1
delta-BHC ND ug/L 11/25/15 16:37 319-86-811/24/15 11:000.050 1
gamma-BHC (Lindane)ND ug/L 11/25/15 16:37 58-89-911/24/15 11:000.050 1
Chlordane (Technical)ND ug/L 11/25/15 16:37 57-74-911/24/15 11:000.20 1
4,4'-DDD ND ug/L 11/25/15 16:37 72-54-811/24/15 11:000.050 1
4,4'-DDE ND ug/L 11/25/15 16:37 72-55-911/24/15 11:000.050 1
4,4'-DDT ND ug/L 11/25/15 16:37 50-29-311/24/15 11:000.050 1
Dieldrin ND ug/L 11/25/15 16:37 60-57-111/24/15 11:000.050 1
Endosulfan I ND ug/L 11/25/15 16:37 959-98-811/24/15 11:000.050 1
Endosulfan II ND ug/L 11/25/15 16:37 33213-65-911/24/15 11:000.050 1
Endosulfan sulfate ND ug/L 11/25/15 16:37 1031-07-811/24/15 11:000.050 1
Endrin ND ug/L 11/25/15 16:37 72-20-811/24/15 11:000.050 1
Endrin aldehyde ND ug/L 11/25/15 16:37 7421-93-411/24/15 11:000.050 1
Heptachlor ND ug/L 11/25/15 16:37 76-44-811/24/15 11:000.050 1
Heptachlor epoxide ND ug/L 11/25/15 16:37 1024-57-311/24/15 11:000.050 1
Methoxychlor ND ug/L 11/25/15 16:37 72-43-511/24/15 11:000.15 1
Toxaphene ND ug/L 11/25/15 16:37 8001-35-211/24/15 11:000.20 1
Surrogates
Tetrachloro-m-xylene (S)75 %11/25/15 16:37 877-09-811/24/15 11:0020-130 1
Decachlorobiphenyl (S)57 %11/25/15 16:37 2051-24-311/24/15 11:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/25/15 17:01 12674-11-211/24/15 11:000.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/25/15 17:01 11104-28-211/24/15 11:000.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/25/15 17:01 11141-16-511/24/15 11:000.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/25/15 17:01 53469-21-911/24/15 11:000.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/25/15 17:01 12672-29-611/24/15 11:000.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/25/15 17:01 11097-69-111/24/15 11:000.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/25/15 17:01 11096-82-511/24/15 11:000.50 1
Surrogates
Decachlorobiphenyl (S)57 %11/25/15 17:01 2051-24-311/24/15 11:0010-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW8 Lab ID:92276295013 Collected:11/18/15 11:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/26/15 00:48 94-75-711/24/15 16:550.94 1
Dinoseb ND ug/L 11/26/15 00:48 88-85-711/24/15 16:550.19 1
2,4,5-T ND ug/L 11/26/15 00:48 93-76-511/24/15 16:550.19 1
2,4,5-TP (Silvex)ND ug/L 11/26/15 00:48 93-72-111/24/15 16:550.19 1
Surrogates
2,4-DCAA (S)79 %11/26/15 00:48 19719-28-911/24/15 16:5536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/24/15 09:52 7440-36-011/20/15 18:005.0 1
Arsenic ND ug/L 11/24/15 09:52 7440-38-211/20/15 18:0010.0 1
Barium 34.4 ug/L 11/24/15 09:52 7440-39-311/20/15 18:005.0 1
Beryllium ND ug/L 11/24/15 09:52 7440-41-711/20/15 18:001.0 1
Cadmium ND ug/L 11/24/15 09:52 7440-43-911/20/15 18:001.0 1
Chromium ND ug/L 11/24/15 09:52 7440-47-311/20/15 18:005.0 1
Cobalt ND ug/L 11/24/15 09:52 7440-48-411/20/15 18:005.0 1
Copper ND ug/L 11/24/15 09:52 7440-50-811/20/15 18:005.0 1
Iron 48.6J ug/L 11/24/15 09:52 7439-89-611/20/15 18:0050.0 1
Lead ND ug/L 11/24/15 09:52 7439-92-111/20/15 18:005.0 1
Manganese 3.3J ug/L 11/24/15 09:52 7439-96-511/20/15 18:005.0 1
Nickel ND ug/L 11/24/15 09:52 7440-02-011/20/15 18:005.0 1
Selenium ND ug/L 11/24/15 09:52 7782-49-211/20/15 18:0010.0 1
Silver ND ug/L 11/24/15 09:52 7440-22-411/20/15 18:005.0 1
Sodium 7940 ug/L 11/24/15 09:52 7440-23-511/20/15 18:0050001
Thallium ND ug/L 11/24/15 09:52 7440-28-011/20/15 18:005.4 1
Tin ND ug/L 11/24/15 09:52 7440-31-511/20/15 18:005.0 1
Vanadium ND ug/L 11/24/15 09:52 7440-62-211/20/15 18:005.0 1
Zinc 7.1J ug/L 11/24/15 09:52 7440-66-611/20/15 18:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 15:11 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/02/15 13:28 83-32-911/25/15 10:3610.0 1
Acenaphthylene ND ug/L 12/02/15 13:28 208-96-811/25/15 10:3610.0 1
Acetophenone ND ug/L 12/02/15 13:28 98-86-211/25/15 10:3610.0 1
2-Acetylaminofluorene ND ug/L 12/02/15 13:28 53-96-3 L211/25/15 10:3620.0 1
4-Aminobiphenyl ND ug/L 12/02/15 13:28 92-67-111/25/15 10:3610.0 1
Anthracene ND ug/L 12/02/15 13:28 120-12-711/25/15 10:3610.0 1
Benzo(a)anthracene ND ug/L 12/02/15 13:28 56-55-311/25/15 10:3610.0 1
Benzo(a)pyrene ND ug/L 12/02/15 13:28 50-32-811/25/15 10:3610.0 1
Benzo(b)fluoranthene ND ug/L 12/02/15 13:28 205-99-211/25/15 10:3610.0 1
Benzo(g,h,i)perylene ND ug/L 12/02/15 13:28 191-24-211/25/15 10:3610.0 1
Benzo(k)fluoranthene ND ug/L 12/02/15 13:28 207-08-911/25/15 10:3610.0 1
Benzyl alcohol ND ug/L 12/02/15 13:28 100-51-611/25/15 10:3620.0 1
4-Bromophenylphenyl ether ND ug/L 12/02/15 13:28 101-55-311/25/15 10:3610.0 1
Butylbenzylphthalate ND ug/L 12/02/15 13:28 85-68-711/25/15 10:3610.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW8 Lab ID:92276295013 Collected:11/18/15 11:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/02/15 13:28 59-50-711/25/15 10:3620.0 1
4-Chloroaniline ND ug/L 12/02/15 13:28 106-47-811/25/15 10:3620.0 1
Chlorobenzilate ND ug/L 12/02/15 13:28 510-15-611/25/15 10:3610.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/02/15 13:28 111-91-111/25/15 10:3610.0 1
bis(2-Chloroethyl) ether ND ug/L 12/02/15 13:28 111-44-411/25/15 10:3610.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/02/15 13:28 108-60-111/25/15 10:3610.0 1
2-Chloronaphthalene ND ug/L 12/02/15 13:28 91-58-711/25/15 10:3610.0 1
2-Chlorophenol ND ug/L 12/02/15 13:28 95-57-811/25/15 10:3610.0 1
4-Chlorophenylphenyl ether ND ug/L 12/02/15 13:28 7005-72-311/25/15 10:3610.0 1
Chrysene ND ug/L 12/02/15 13:28 218-01-911/25/15 10:3610.0 1
Diallate ND ug/L 12/02/15 13:28 2303-16-411/25/15 10:3610.0 1
Dibenz(a,h)anthracene ND ug/L 12/02/15 13:28 53-70-311/25/15 10:3610.0 1
Dibenzofuran ND ug/L 12/02/15 13:28 132-64-911/25/15 10:3610.0 1
3,3'-Dichlorobenzidine ND ug/L 12/02/15 13:28 91-94-111/25/15 10:3620.0 1
2,4-Dichlorophenol ND ug/L 12/02/15 13:28 120-83-211/25/15 10:3610.0 1
2,6-Dichlorophenol ND ug/L 12/02/15 13:28 87-65-011/25/15 10:3610.0 1
Diethylphthalate ND ug/L 12/02/15 13:28 84-66-211/25/15 10:3610.0 1
Dimethoate ND ug/L 12/02/15 13:28 60-51-511/25/15 10:3610.0 1
P-Dimethylaminoazobenzene ND ug/L 12/02/15 13:28 60-11-711/25/15 10:365.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/02/15 13:28 57-97-611/25/15 10:3610.0 1
3,3'-Dimethylbenzidine ND ug/L 12/02/15 13:28 119-93-711/25/15 10:3610.0 1
2,4-Dimethylphenol ND ug/L 12/02/15 13:28 105-67-911/25/15 10:3610.0 1
Dimethylphthalate ND ug/L 12/02/15 13:28 131-11-311/25/15 10:3610.0 1
Di-n-butylphthalate ND ug/L 12/02/15 13:28 84-74-211/25/15 10:3610.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/02/15 13:28 534-52-111/25/15 10:3620.0 1
1,3-Dinitrobenzene ND ug/L 12/02/15 13:28 99-65-011/25/15 10:3620.0 1
2,4-Dinitrophenol ND ug/L 12/02/15 13:28 51-28-511/25/15 10:3650.0 1
2,4-Dinitrotoluene ND ug/L 12/02/15 13:28 121-14-211/25/15 10:3610.0 1
2,6-Dinitrotoluene ND ug/L 12/02/15 13:28 606-20-211/25/15 10:3610.0 1
Di-n-octylphthalate 5.6J ug/L 12/02/15 13:28 117-84-011/25/15 10:3610.0 1
Diphenylamine ND ug/L 12/02/15 13:28 122-39-411/25/15 10:3610.0 1
Disulfoton ND ug/L 12/02/15 13:28 298-04-411/25/15 10:3610.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/02/15 13:28 117-81-711/25/15 10:366.0 1
Ethyl methanesulfonate ND ug/L 12/02/15 13:28 62-50-011/25/15 10:3620.0 1
Famphur ND ug/L 12/02/15 13:28 52-85-711/25/15 10:3610.0 1
Fluoranthene ND ug/L 12/02/15 13:28 206-44-011/25/15 10:3610.0 1
Fluorene ND ug/L 12/02/15 13:28 86-73-711/25/15 10:3610.0 1
Hexachlorobenzene ND ug/L 12/02/15 13:28 118-74-111/25/15 10:3610.0 1
Hexachlorocyclopentadiene ND ug/L 12/02/15 13:28 77-47-411/25/15 10:3610.0 1
Hexachloroethane ND ug/L 12/02/15 13:28 67-72-111/25/15 10:3610.0 1
Hexachlorophene ND ug/L 12/02/15 13:28 70-30-411/25/15 10:361001
Indeno(1,2,3-cd)pyrene ND ug/L 12/02/15 13:28 193-39-511/25/15 10:3610.0 1
Isodrin ND ug/L 12/02/15 13:28 465-73-611/25/15 10:3620.0 1
Isophorone ND ug/L 12/02/15 13:28 78-59-111/25/15 10:3610.0 1
Isosafrole ND ug/L 12/02/15 13:28 120-58-111/25/15 10:3610.0 1
Kepone ND ug/L 12/02/15 13:28 143-50-011/25/15 10:3610.0 1
Methapyrilene ND ug/L 12/02/15 13:28 91-80-511/25/15 10:3650.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW8 Lab ID:92276295013 Collected:11/18/15 11:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/02/15 13:28 56-49-511/25/15 10:3610.0 1
Methyl methanesulfonate ND ug/L 12/02/15 13:28 66-27-311/25/15 10:365.0 1
2-Methylnaphthalene ND ug/L 12/02/15 13:28 91-57-611/25/15 10:3610.0 1
Methyl parathion ND ug/L 12/02/15 13:28 298-00-011/25/15 10:3610.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/02/15 13:28 95-48-711/25/15 10:3610.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/02/15 13:2811/25/15 10:3610.0 1
1-Naphthalenamine ND ug/L 12/02/15 13:28 134-32-711/25/15 10:365.0 1
2-Naphthalenamine ND ug/L 12/02/15 13:28 91-59-811/25/15 10:365.0 1
1,4-Naphthoquinone ND ug/L 12/02/15 13:28 130-15-411/25/15 10:365.0 1
2-Nitroaniline ND ug/L 12/02/15 13:28 88-74-411/25/15 10:3650.0 1
3-Nitroaniline ND ug/L 12/02/15 13:28 99-09-211/25/15 10:3650.0 1
4-Nitroaniline ND ug/L 12/02/15 13:28 100-01-611/25/15 10:3620.0 1
Nitrobenzene ND ug/L 12/02/15 13:28 98-95-311/25/15 10:3610.0 1
2-Nitrophenol ND ug/L 12/02/15 13:28 88-75-511/25/15 10:3610.0 1
4-Nitrophenol ND ug/L 12/02/15 13:28 100-02-711/25/15 10:3650.0 1
5-Nitro-o-toluidine ND ug/L 12/02/15 13:28 99-55-811/25/15 10:3610.0 1
N-Nitrosodiethylamine ND ug/L 12/02/15 13:28 55-18-511/25/15 10:3620.0 1
N-Nitrosodimethylamine ND ug/L 12/02/15 13:28 62-75-911/25/15 10:3610.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/02/15 13:28 924-16-311/25/15 10:3610.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/02/15 13:28 621-64-711/25/15 10:3610.0 1
N-Nitrosodiphenylamine ND ug/L 12/02/15 13:28 86-30-611/25/15 10:3610.0 1
N-Nitrosomethylethylamine ND ug/L 12/02/15 13:28 10595-95-611/25/15 10:3610.0 1
N-Nitrosopiperidine ND ug/L 12/02/15 13:28 100-75-411/25/15 10:3620.0 1
N-Nitrosopyrrolidine ND ug/L 12/02/15 13:28 930-55-211/25/15 10:3610.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/02/15 13:28 126-68-111/25/15 10:3610.0 1
Parathion (Ethyl parathion)ND ug/L 12/02/15 13:28 56-38-211/25/15 10:3610.0 1
Pentachlorobenzene ND ug/L 12/02/15 13:28 608-93-511/25/15 10:3610.0 1
Pentachloronitrobenzene ND ug/L 12/02/15 13:28 82-68-811/25/15 10:3620.0 1
Pentachlorophenol ND ug/L 12/02/15 13:28 87-86-511/25/15 10:3625.0 1
Phenacetin ND ug/L 12/02/15 13:28 62-44-211/25/15 10:3620.0 1
Phenanthrene ND ug/L 12/02/15 13:28 85-01-811/25/15 10:3610.0 1
Phenol ND ug/L 12/02/15 13:28 108-95-211/25/15 10:3610.0 1
p-Phenylenediamine ND ug/L 12/02/15 13:28 106-50-311/25/15 10:3610.0 1
Phorate ND ug/L 12/02/15 13:28 298-02-211/25/15 10:3610.0 1
Pronamide ND ug/L 12/02/15 13:28 23950-58-511/25/15 10:3610.0 1
Pyrene ND ug/L 12/02/15 13:28 129-00-011/25/15 10:3610.0 1
Safrole ND ug/L 12/02/15 13:28 94-59-711/25/15 10:3610.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/02/15 13:28 95-94-311/25/15 10:3610.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/02/15 13:28 58-90-211/25/15 10:3610.0 1
Thionazin ND ug/L 12/02/15 13:28 297-97-211/25/15 10:3620.0 1
O-Toluidine ND ug/L 12/02/15 13:28 95-53-411/25/15 10:3610.0 1
2,4,5-Trichlorophenol ND ug/L 12/02/15 13:28 95-95-411/25/15 10:3610.0 1
2,4,6-Trichlorophenol ND ug/L 12/02/15 13:28 88-06-211/25/15 10:3610.0 1
1,3,5-Trinitrobenzene ND ug/L 12/02/15 13:28 99-35-4 L311/25/15 10:3610.0 1
Surrogates
Nitrobenzene-d5 (S)75 %12/02/15 13:28 4165-60-011/25/15 10:3621-110 1
2-Fluorobiphenyl (S)74 %12/02/15 13:28 321-60-811/25/15 10:3627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 79 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW8 Lab ID:92276295013 Collected:11/18/15 11:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)92 %12/02/15 13:28 1718-51-011/25/15 10:3631-107 1
Phenol-d6 (S)23 %12/02/15 13:28 13127-88-311/25/15 10:3610-110 1
2-Fluorophenol (S)35 %12/02/15 13:28 367-12-411/25/15 10:3612-110 1
2,4,6-Tribromophenol (S)84 %12/02/15 13:28 118-79-611/25/15 10:3627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 18:45 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 18:45 75-05-850.0 1
Acrolein ND ug/L 11/20/15 18:45 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 18:45 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 18:45 107-05-12.0 1
Benzene ND ug/L 11/20/15 18:45 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 18:45 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 18:45 75-27-41.0 1
Bromoform ND ug/L 11/20/15 18:45 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 18:45 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 18:45 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 18:45 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 18:45 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 18:45 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 18:45 75-00-31.0 1
Chloroform ND ug/L 11/20/15 18:45 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 18:45 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 18:45 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 18:45 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 18:45 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 18:45 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 18:45 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 18:45 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 18:45 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 18:45 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 18:45 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 18:45 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 18:45 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 18:45 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 18:45 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 18:45 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 18:45 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 18:45 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 18:45 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 18:45 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 18:45 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 18:45 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 18:45 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 18:45 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 18:45 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW8 Lab ID:92276295013 Collected:11/18/15 11:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 18:45 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 18:45 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 18:45 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 18:45 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 18:45 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 18:45 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 18:45 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 18:45 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 18:45 107-12-020.0 1
Styrene ND ug/L 11/20/15 18:45 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 18:45 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 18:45 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 18:45 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 18:45 109-99-910.0 1
Toluene ND ug/L 11/20/15 18:45 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 18:45 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 18:45 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 18:45 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 18:45 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 18:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 18:45 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 18:45 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 18:45 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 18:45 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 18:45 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 18:45 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %11/20/15 18:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/20/15 18:45 17060-07-070-130 1
Toluene-d8 (S)101 %11/20/15 18:45 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 23200 ug/L 11/29/15 20:3250001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 79000 ug/L 11/22/15 11:07250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/23/15 23:30 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1350J ug/L 11/24/15 23:22 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 2040 ug/L 11/30/15 19:17 16887-00-610001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW8 Lab ID:92276295013 Collected:11/18/15 11:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.1J ug/L 11/25/15 02:46 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW10 Lab ID:92276295014 Collected:11/18/15 14:10 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/18/15 14:101
Field pH 5.4 Std. Units 11/18/15 14:100.10 1
Field Temperature 16.5 deg C 11/18/15 14:100.50 1
Static Water Level 12.05 feet 11/18/15 14:101
Field Specific Conductance 365.1 umhos/cm 11/18/15 14:101.0 1
Oxygen, Dissolved 0.2 mg/L 11/18/15 14:10 7782-44-71
Total Well Depth 21.0 feet 11/18/15 14:101
REDOX -77.7 mV 11/18/15 14:101
Turbidity 295.0 NTU 11/18/15 14:101.0 1
Odor none 11/18/15 14:101
Appearance murky 11/18/15 14:101
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/25/15 16:55 309-00-211/24/15 11:000.050 1
alpha-BHC ND ug/L 11/25/15 16:55 319-84-611/24/15 11:000.050 1
beta-BHC ND ug/L 11/25/15 16:55 319-85-711/24/15 11:000.050 1
delta-BHC ND ug/L 11/25/15 16:55 319-86-811/24/15 11:000.050 1
gamma-BHC (Lindane)ND ug/L 11/25/15 16:55 58-89-911/24/15 11:000.050 1
Chlordane (Technical)ND ug/L 11/25/15 16:55 57-74-911/24/15 11:000.20 1
4,4'-DDD ND ug/L 11/25/15 16:55 72-54-811/24/15 11:000.050 1
4,4'-DDE ND ug/L 11/25/15 16:55 72-55-911/24/15 11:000.050 1
4,4'-DDT ND ug/L 11/25/15 16:55 50-29-311/24/15 11:000.050 1
Dieldrin ND ug/L 11/25/15 16:55 60-57-111/24/15 11:000.050 1
Endosulfan I 0.17 ug/L 11/25/15 16:55 959-98-811/24/15 11:000.050 1
Endosulfan II ND ug/L 11/25/15 16:55 33213-65-911/24/15 11:000.050 1
Endosulfan sulfate ND ug/L 11/25/15 16:55 1031-07-811/24/15 11:000.050 1
Endrin ND ug/L 11/25/15 16:55 72-20-811/24/15 11:000.050 1
Endrin aldehyde ND ug/L 11/25/15 16:55 7421-93-411/24/15 11:000.050 1
Heptachlor 0.12 ug/L 11/25/15 16:55 76-44-811/24/15 11:000.050 1
Heptachlor epoxide 0.093 ug/L 11/25/15 16:55 1024-57-311/24/15 11:000.050 1
Methoxychlor ND ug/L 11/25/15 16:55 72-43-511/24/15 11:000.15 1
Toxaphene ND ug/L 11/25/15 16:55 8001-35-211/24/15 11:000.20 1
Surrogates
Tetrachloro-m-xylene (S)89 %11/25/15 16:55 877-09-811/24/15 11:0020-130 1
Decachlorobiphenyl (S)89 %11/25/15 16:55 2051-24-311/24/15 11:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/25/15 17:22 12674-11-211/24/15 11:000.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/25/15 17:22 11104-28-211/24/15 11:000.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/25/15 17:22 11141-16-511/24/15 11:000.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/25/15 17:22 53469-21-911/24/15 11:000.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/25/15 17:22 12672-29-611/24/15 11:000.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/25/15 17:22 11097-69-111/24/15 11:000.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/25/15 17:22 11096-82-511/24/15 11:000.50 1
Surrogates
Decachlorobiphenyl (S)60 %11/25/15 17:22 2051-24-311/24/15 11:0010-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW10 Lab ID:92276295014 Collected:11/18/15 14:10 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/26/15 01:18 94-75-711/24/15 16:550.94 1
Dinoseb ND ug/L 11/26/15 01:18 88-85-711/24/15 16:550.19 1
2,4,5-T ND ug/L 11/26/15 01:18 93-76-511/24/15 16:550.19 1
2,4,5-TP (Silvex)ND ug/L 11/26/15 01:18 93-72-111/24/15 16:550.19 1
Surrogates
2,4-DCAA (S)93 %11/26/15 01:18 19719-28-911/24/15 16:5536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/24/15 09:55 7440-36-011/20/15 18:005.0 1
Arsenic ND ug/L 11/24/15 09:55 7440-38-211/20/15 18:0010.0 1
Barium 241 ug/L 11/24/15 09:55 7440-39-311/20/15 18:005.0 1
Beryllium 1.9 ug/L 11/24/15 09:55 7440-41-711/20/15 18:001.0 1
Cadmium ND ug/L 11/24/15 09:55 7440-43-911/20/15 18:001.0 1
Chromium 3.5J ug/L 11/24/15 09:55 7440-47-311/20/15 18:005.0 1
Cobalt 3.1J ug/L 11/24/15 09:55 7440-48-411/20/15 18:005.0 1
Copper 6.3 ug/L 11/24/15 09:55 7440-50-811/20/15 18:005.0 1
Iron 3690 ug/L 11/24/15 09:55 7439-89-611/20/15 18:0050.0 1
Lead 8.5 ug/L 11/24/15 09:55 7439-92-111/20/15 18:005.0 1
Manganese 587 ug/L 11/24/15 09:55 7439-96-511/20/15 18:005.0 1
Nickel 3.9J ug/L 11/24/15 09:55 7440-02-011/20/15 18:005.0 1
Selenium ND ug/L 11/24/15 09:55 7782-49-211/20/15 18:0010.0 1
Silver ND ug/L 11/24/15 09:55 7440-22-411/20/15 18:005.0 1
Sodium 19800 ug/L 11/24/15 09:55 7440-23-511/20/15 18:0050001
Thallium ND ug/L 11/24/15 09:55 7440-28-011/20/15 18:005.4 1
Tin 8.5 ug/L 11/24/15 09:55 7440-31-511/20/15 18:005.0 1
Vanadium 5.6 ug/L 11/24/15 09:55 7440-62-211/20/15 18:005.0 1
Zinc 27.2 ug/L 11/24/15 09:55 7440-66-611/20/15 18:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.12J ug/L 12/02/15 15:13 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/02/15 13:56 83-32-911/25/15 10:3610.0 1
Acenaphthylene ND ug/L 12/02/15 13:56 208-96-811/25/15 10:3610.0 1
Acetophenone ND ug/L 12/02/15 13:56 98-86-211/25/15 10:3610.0 1
2-Acetylaminofluorene ND ug/L 12/02/15 13:56 53-96-3 L211/25/15 10:3620.0 1
4-Aminobiphenyl ND ug/L 12/02/15 13:56 92-67-111/25/15 10:3610.0 1
Anthracene ND ug/L 12/02/15 13:56 120-12-711/25/15 10:3610.0 1
Benzo(a)anthracene ND ug/L 12/02/15 13:56 56-55-311/25/15 10:3610.0 1
Benzo(a)pyrene ND ug/L 12/02/15 13:56 50-32-811/25/15 10:3610.0 1
Benzo(b)fluoranthene ND ug/L 12/02/15 13:56 205-99-211/25/15 10:3610.0 1
Benzo(g,h,i)perylene ND ug/L 12/02/15 13:56 191-24-211/25/15 10:3610.0 1
Benzo(k)fluoranthene ND ug/L 12/02/15 13:56 207-08-911/25/15 10:3610.0 1
Benzyl alcohol ND ug/L 12/02/15 13:56 100-51-611/25/15 10:3620.0 1
4-Bromophenylphenyl ether ND ug/L 12/02/15 13:56 101-55-311/25/15 10:3610.0 1
Butylbenzylphthalate ND ug/L 12/02/15 13:56 85-68-711/25/15 10:3610.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW10 Lab ID:92276295014 Collected:11/18/15 14:10 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/02/15 13:56 59-50-711/25/15 10:3620.0 1
4-Chloroaniline ND ug/L 12/02/15 13:56 106-47-811/25/15 10:3620.0 1
Chlorobenzilate ND ug/L 12/02/15 13:56 510-15-611/25/15 10:3610.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/02/15 13:56 111-91-111/25/15 10:3610.0 1
bis(2-Chloroethyl) ether ND ug/L 12/02/15 13:56 111-44-411/25/15 10:3610.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/02/15 13:56 108-60-111/25/15 10:3610.0 1
2-Chloronaphthalene ND ug/L 12/02/15 13:56 91-58-711/25/15 10:3610.0 1
2-Chlorophenol ND ug/L 12/02/15 13:56 95-57-811/25/15 10:3610.0 1
4-Chlorophenylphenyl ether ND ug/L 12/02/15 13:56 7005-72-311/25/15 10:3610.0 1
Chrysene ND ug/L 12/02/15 13:56 218-01-911/25/15 10:3610.0 1
Diallate ND ug/L 12/02/15 13:56 2303-16-411/25/15 10:3610.0 1
Dibenz(a,h)anthracene ND ug/L 12/02/15 13:56 53-70-311/25/15 10:3610.0 1
Dibenzofuran ND ug/L 12/02/15 13:56 132-64-911/25/15 10:3610.0 1
3,3'-Dichlorobenzidine ND ug/L 12/02/15 13:56 91-94-111/25/15 10:3620.0 1
2,4-Dichlorophenol ND ug/L 12/02/15 13:56 120-83-211/25/15 10:3610.0 1
2,6-Dichlorophenol ND ug/L 12/02/15 13:56 87-65-011/25/15 10:3610.0 1
Diethylphthalate ND ug/L 12/02/15 13:56 84-66-211/25/15 10:3610.0 1
Dimethoate ND ug/L 12/02/15 13:56 60-51-511/25/15 10:3610.0 1
P-Dimethylaminoazobenzene ND ug/L 12/02/15 13:56 60-11-711/25/15 10:365.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/02/15 13:56 57-97-611/25/15 10:3610.0 1
3,3'-Dimethylbenzidine ND ug/L 12/02/15 13:56 119-93-711/25/15 10:3610.0 1
2,4-Dimethylphenol ND ug/L 12/02/15 13:56 105-67-911/25/15 10:3610.0 1
Dimethylphthalate ND ug/L 12/02/15 13:56 131-11-311/25/15 10:3610.0 1
Di-n-butylphthalate ND ug/L 12/02/15 13:56 84-74-211/25/15 10:3610.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/02/15 13:56 534-52-111/25/15 10:3620.0 1
1,3-Dinitrobenzene ND ug/L 12/02/15 13:56 99-65-011/25/15 10:3620.0 1
2,4-Dinitrophenol ND ug/L 12/02/15 13:56 51-28-511/25/15 10:3650.0 1
2,4-Dinitrotoluene ND ug/L 12/02/15 13:56 121-14-211/25/15 10:3610.0 1
2,6-Dinitrotoluene ND ug/L 12/02/15 13:56 606-20-211/25/15 10:3610.0 1
Di-n-octylphthalate ND ug/L 12/02/15 13:56 117-84-011/25/15 10:3610.0 1
Diphenylamine ND ug/L 12/02/15 13:56 122-39-411/25/15 10:3610.0 1
Disulfoton ND ug/L 12/02/15 13:56 298-04-411/25/15 10:3610.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/02/15 13:56 117-81-711/25/15 10:366.0 1
Ethyl methanesulfonate ND ug/L 12/02/15 13:56 62-50-011/25/15 10:3620.0 1
Famphur ND ug/L 12/02/15 13:56 52-85-711/25/15 10:3610.0 1
Fluoranthene ND ug/L 12/02/15 13:56 206-44-011/25/15 10:3610.0 1
Fluorene ND ug/L 12/02/15 13:56 86-73-711/25/15 10:3610.0 1
Hexachlorobenzene ND ug/L 12/02/15 13:56 118-74-111/25/15 10:3610.0 1
Hexachlorocyclopentadiene ND ug/L 12/02/15 13:56 77-47-411/25/15 10:3610.0 1
Hexachloroethane ND ug/L 12/02/15 13:56 67-72-111/25/15 10:3610.0 1
Hexachlorophene ND ug/L 12/02/15 13:56 70-30-411/25/15 10:361001
Indeno(1,2,3-cd)pyrene ND ug/L 12/02/15 13:56 193-39-511/25/15 10:3610.0 1
Isodrin ND ug/L 12/02/15 13:56 465-73-611/25/15 10:3620.0 1
Isophorone ND ug/L 12/02/15 13:56 78-59-111/25/15 10:3610.0 1
Isosafrole ND ug/L 12/02/15 13:56 120-58-111/25/15 10:3610.0 1
Kepone ND ug/L 12/02/15 13:56 143-50-011/25/15 10:3610.0 1
Methapyrilene ND ug/L 12/02/15 13:56 91-80-511/25/15 10:3650.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 85 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW10 Lab ID:92276295014 Collected:11/18/15 14:10 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/02/15 13:56 56-49-511/25/15 10:3610.0 1
Methyl methanesulfonate ND ug/L 12/02/15 13:56 66-27-311/25/15 10:365.0 1
2-Methylnaphthalene ND ug/L 12/02/15 13:56 91-57-611/25/15 10:3610.0 1
Methyl parathion ND ug/L 12/02/15 13:56 298-00-011/25/15 10:3610.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/02/15 13:56 95-48-711/25/15 10:3610.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/02/15 13:5611/25/15 10:3610.0 1
1-Naphthalenamine ND ug/L 12/02/15 13:56 134-32-711/25/15 10:365.0 1
2-Naphthalenamine ND ug/L 12/02/15 13:56 91-59-811/25/15 10:365.0 1
1,4-Naphthoquinone ND ug/L 12/02/15 13:56 130-15-411/25/15 10:365.0 1
2-Nitroaniline ND ug/L 12/02/15 13:56 88-74-411/25/15 10:3650.0 1
3-Nitroaniline ND ug/L 12/02/15 13:56 99-09-211/25/15 10:3650.0 1
4-Nitroaniline ND ug/L 12/02/15 13:56 100-01-611/25/15 10:3620.0 1
Nitrobenzene ND ug/L 12/02/15 13:56 98-95-311/25/15 10:3610.0 1
2-Nitrophenol ND ug/L 12/02/15 13:56 88-75-511/25/15 10:3610.0 1
4-Nitrophenol ND ug/L 12/02/15 13:56 100-02-711/25/15 10:3650.0 1
5-Nitro-o-toluidine ND ug/L 12/02/15 13:56 99-55-811/25/15 10:3610.0 1
N-Nitrosodiethylamine ND ug/L 12/02/15 13:56 55-18-511/25/15 10:3620.0 1
N-Nitrosodimethylamine ND ug/L 12/02/15 13:56 62-75-911/25/15 10:3610.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/02/15 13:56 924-16-311/25/15 10:3610.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/02/15 13:56 621-64-711/25/15 10:3610.0 1
N-Nitrosodiphenylamine ND ug/L 12/02/15 13:56 86-30-611/25/15 10:3610.0 1
N-Nitrosomethylethylamine ND ug/L 12/02/15 13:56 10595-95-611/25/15 10:3610.0 1
N-Nitrosopiperidine ND ug/L 12/02/15 13:56 100-75-411/25/15 10:3620.0 1
N-Nitrosopyrrolidine ND ug/L 12/02/15 13:56 930-55-211/25/15 10:3610.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/02/15 13:56 126-68-111/25/15 10:3610.0 1
Parathion (Ethyl parathion)ND ug/L 12/02/15 13:56 56-38-211/25/15 10:3610.0 1
Pentachlorobenzene ND ug/L 12/02/15 13:56 608-93-511/25/15 10:3610.0 1
Pentachloronitrobenzene ND ug/L 12/02/15 13:56 82-68-811/25/15 10:3620.0 1
Pentachlorophenol ND ug/L 12/02/15 13:56 87-86-511/25/15 10:3625.0 1
Phenacetin ND ug/L 12/02/15 13:56 62-44-211/25/15 10:3620.0 1
Phenanthrene ND ug/L 12/02/15 13:56 85-01-811/25/15 10:3610.0 1
Phenol ND ug/L 12/02/15 13:56 108-95-211/25/15 10:3610.0 1
p-Phenylenediamine ND ug/L 12/02/15 13:56 106-50-311/25/15 10:3610.0 1
Phorate ND ug/L 12/02/15 13:56 298-02-211/25/15 10:3610.0 1
Pronamide ND ug/L 12/02/15 13:56 23950-58-511/25/15 10:3610.0 1
Pyrene ND ug/L 12/02/15 13:56 129-00-011/25/15 10:3610.0 1
Safrole ND ug/L 12/02/15 13:56 94-59-711/25/15 10:3610.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/02/15 13:56 95-94-311/25/15 10:3610.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/02/15 13:56 58-90-211/25/15 10:3610.0 1
Thionazin ND ug/L 12/02/15 13:56 297-97-211/25/15 10:3620.0 1
O-Toluidine ND ug/L 12/02/15 13:56 95-53-411/25/15 10:3610.0 1
2,4,5-Trichlorophenol ND ug/L 12/02/15 13:56 95-95-411/25/15 10:3610.0 1
2,4,6-Trichlorophenol ND ug/L 12/02/15 13:56 88-06-211/25/15 10:3610.0 1
1,3,5-Trinitrobenzene ND ug/L 12/02/15 13:56 99-35-4 L311/25/15 10:3610.0 1
Surrogates
Nitrobenzene-d5 (S)81 %12/02/15 13:56 4165-60-011/25/15 10:3621-110 1
2-Fluorobiphenyl (S)76 %12/02/15 13:56 321-60-811/25/15 10:3627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW10 Lab ID:92276295014 Collected:11/18/15 14:10 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)69 %12/02/15 13:56 1718-51-011/25/15 10:3631-107 1
Phenol-d6 (S)31 %12/02/15 13:56 13127-88-311/25/15 10:3610-110 1
2-Fluorophenol (S)44 %12/02/15 13:56 367-12-411/25/15 10:3612-110 1
2,4,6-Tribromophenol (S)92 %12/02/15 13:56 118-79-611/25/15 10:3627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 11.8J ug/L 11/20/15 19:19 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 19:19 75-05-850.0 1
Acrolein ND ug/L 11/20/15 19:19 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 19:19 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 19:19 107-05-12.0 1
Benzene ND ug/L 11/20/15 19:19 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 19:19 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 19:19 75-27-41.0 1
Bromoform ND ug/L 11/20/15 19:19 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 19:19 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 19:19 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 19:19 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 19:19 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 19:19 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 19:19 75-00-31.0 1
Chloroform ND ug/L 11/20/15 19:19 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 19:19 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 19:19 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 19:19 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 19:19 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 19:19 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 19:19 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 19:19 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 19:19 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 19:19 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 19:19 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 19:19 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 19:19 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 19:19 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 19:19 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 19:19 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 19:19 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 19:19 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 19:19 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 19:19 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 19:19 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 19:19 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 19:19 10061-02-61.0 1
Ethylbenzene 0.40J ug/L 11/20/15 19:19 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 19:19 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW10 Lab ID:92276295014 Collected:11/18/15 14:10 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 19:19 87-68-31.0 1
2-Hexanone 0.69J ug/L 11/20/15 19:19 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 19:19 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 19:19 126-98-710.0 1
Methylene Chloride 1.2 ug/L 11/20/15 19:19 75-09-2 C91.0 1
Methyl methacrylate ND ug/L 11/20/15 19:19 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)2.6J ug/L 11/20/15 19:19 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 19:19 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 19:19 107-12-020.0 1
Styrene ND ug/L 11/20/15 19:19 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 19:19 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 19:19 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 19:19 127-18-41.0 1
Tetrahydrofuran 120 ug/L 11/20/15 19:19 109-99-910.0 1
Toluene ND ug/L 11/20/15 19:19 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 19:19 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 19:19 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 19:19 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 19:19 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 19:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 19:19 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 19:19 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 19:19 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 19:19 1330-20-72.0 1
m&p-Xylene 0.68J ug/L 11/20/15 19:19 179601-23-12.0 1
o-Xylene 0.43J ug/L 11/20/15 19:19 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %11/20/15 19:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/20/15 19:19 17060-07-070-130 1
Toluene-d8 (S)100 %11/20/15 19:19 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 48200 ug/L 11/29/15 20:4350001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 403000 ug/L 11/22/15 11:07250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/23/15 23:30 18496-25-8100010
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 63600 ug/L 11/25/15 08:38 14808-79-8 M140002
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 47400 ug/L 11/30/15 19:22 16887-00-640004
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW10 Lab ID:92276295014 Collected:11/18/15 14:10 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 9.8 ug/L 11/25/15 02:47 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW11 Lab ID:92276295015 Collected:11/18/15 15:40 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/18/15 15:401
Field pH 5.9 Std. Units 11/18/15 15:400.10 1
Field Temperature 15.8 deg C 11/18/15 15:400.50 1
Static Water Level 3.58 feet 11/18/15 15:401
Field Specific Conductance 400.8 umhos/cm 11/18/15 15:401.0 1
Oxygen, Dissolved 0.1 mg/L 11/18/15 15:40 7782-44-71
Total Well Depth 20 feet 11/18/15 15:401
REDOX -38.7 mV 11/18/15 15:401
Turbidity 9.3 NTU 11/18/15 15:401.0 1
Odor sulfurous 11/18/15 15:401
Appearance clear 11/18/15 15:401
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/25/15 17:13 309-00-211/24/15 11:000.050 1
alpha-BHC ND ug/L 11/25/15 17:13 319-84-611/24/15 11:000.050 1
beta-BHC ND ug/L 11/25/15 17:13 319-85-711/24/15 11:000.050 1
delta-BHC ND ug/L 11/25/15 17:13 319-86-811/24/15 11:000.050 1
gamma-BHC (Lindane)ND ug/L 11/25/15 17:13 58-89-911/24/15 11:000.050 1
Chlordane (Technical)ND ug/L 11/25/15 17:13 57-74-911/24/15 11:000.20 1
4,4'-DDD ND ug/L 11/25/15 17:13 72-54-811/24/15 11:000.050 1
4,4'-DDE ND ug/L 11/25/15 17:13 72-55-911/24/15 11:000.050 1
4,4'-DDT ND ug/L 11/25/15 17:13 50-29-311/24/15 11:000.050 1
Dieldrin ND ug/L 11/25/15 17:13 60-57-111/24/15 11:000.050 1
Endosulfan I ND ug/L 11/25/15 17:13 959-98-811/24/15 11:000.050 1
Endosulfan II ND ug/L 11/25/15 17:13 33213-65-911/24/15 11:000.050 1
Endosulfan sulfate ND ug/L 11/25/15 17:13 1031-07-811/24/15 11:000.050 1
Endrin ND ug/L 11/25/15 17:13 72-20-811/24/15 11:000.050 1
Endrin aldehyde ND ug/L 11/25/15 17:13 7421-93-411/24/15 11:000.050 1
Heptachlor ND ug/L 11/25/15 17:13 76-44-811/24/15 11:000.050 1
Heptachlor epoxide ND ug/L 11/25/15 17:13 1024-57-311/24/15 11:000.050 1
Methoxychlor ND ug/L 11/25/15 17:13 72-43-511/24/15 11:000.15 1
Toxaphene ND ug/L 11/25/15 17:13 8001-35-211/24/15 11:000.20 1
Surrogates
Tetrachloro-m-xylene (S)77 %11/25/15 17:13 877-09-811/24/15 11:0020-130 1
Decachlorobiphenyl (S)79 %11/25/15 17:13 2051-24-311/24/15 11:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/25/15 17:42 12674-11-211/24/15 11:000.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/25/15 17:42 11104-28-211/24/15 11:000.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/25/15 17:42 11141-16-511/24/15 11:000.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/25/15 17:42 53469-21-911/24/15 11:000.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/25/15 17:42 12672-29-611/24/15 11:000.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/25/15 17:42 11097-69-111/24/15 11:000.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/25/15 17:42 11096-82-511/24/15 11:000.50 1
Surrogates
Decachlorobiphenyl (S)89 %11/25/15 17:42 2051-24-311/24/15 11:0010-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW11 Lab ID:92276295015 Collected:11/18/15 15:40 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/26/15 01:48 94-75-711/24/15 16:550.94 1
Dinoseb ND ug/L 11/26/15 01:48 88-85-711/24/15 16:550.19 1
2,4,5-T ND ug/L 11/26/15 01:48 93-76-511/24/15 16:550.19 1
2,4,5-TP (Silvex)ND ug/L 11/26/15 01:48 93-72-111/24/15 16:550.19 1
Surrogates
2,4-DCAA (S)91 %11/26/15 01:48 19719-28-911/24/15 16:5536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/03/15 16:48 7440-36-012/02/15 17:305.0 1
Arsenic ND ug/L 12/03/15 16:48 7440-38-212/02/15 17:3010.0 1
Barium 97.2 ug/L 12/03/15 16:48 7440-39-312/02/15 17:305.0 1
Beryllium ND ug/L 12/03/15 16:48 7440-41-712/02/15 17:301.0 1
Cadmium ND ug/L 12/03/15 16:48 7440-43-912/02/15 17:301.0 1
Chromium ND ug/L 12/03/15 16:48 7440-47-312/02/15 17:305.0 1
Cobalt 2.9J ug/L 12/03/15 16:48 7440-48-412/02/15 17:305.0 1
Copper 2.8J ug/L 12/03/15 16:48 7440-50-812/02/15 17:305.0 1
Iron 34600 ug/L 12/03/15 16:48 7439-89-612/02/15 17:3050.0 1
Lead ND ug/L 12/03/15 16:48 7439-92-112/02/15 17:305.0 1
Manganese 2020 ug/L 12/03/15 16:48 7439-96-512/02/15 17:305.0 1
Nickel ND ug/L 12/03/15 16:48 7440-02-012/02/15 17:305.0 1
Selenium 5.6J ug/L 12/03/15 16:48 7782-49-212/02/15 17:3010.0 1
Silver ND ug/L 12/03/15 16:48 7440-22-412/02/15 17:305.0 1
Sodium 12000 ug/L 12/03/15 16:48 7440-23-512/02/15 17:3050001
Thallium 8.8 ug/L 12/03/15 16:48 7440-28-012/02/15 17:305.4 1
Tin ND ug/L 12/03/15 16:48 7440-31-512/02/15 17:305.0 1
Vanadium 3.5J ug/L 12/03/15 16:48 7440-62-212/02/15 17:305.0 1
Zinc ND ug/L 12/03/15 16:48 7440-66-612/02/15 17:3010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 15:15 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/01/15 15:41 83-32-911/25/15 10:3610.0 1
Acenaphthylene ND ug/L 12/01/15 15:41 208-96-811/25/15 10:3610.0 1
Acetophenone ND ug/L 12/01/15 15:41 98-86-211/25/15 10:3610.0 1
2-Acetylaminofluorene ND ug/L 12/01/15 15:41 53-96-3 L211/25/15 10:3620.0 1
4-Aminobiphenyl ND ug/L 12/01/15 15:41 92-67-111/25/15 10:3610.0 1
Anthracene ND ug/L 12/01/15 15:41 120-12-711/25/15 10:3610.0 1
Benzo(a)anthracene ND ug/L 12/01/15 15:41 56-55-311/25/15 10:3610.0 1
Benzo(a)pyrene ND ug/L 12/01/15 15:41 50-32-811/25/15 10:3610.0 1
Benzo(b)fluoranthene ND ug/L 12/01/15 15:41 205-99-211/25/15 10:3610.0 1
Benzo(g,h,i)perylene ND ug/L 12/01/15 15:41 191-24-211/25/15 10:3610.0 1
Benzo(k)fluoranthene ND ug/L 12/01/15 15:41 207-08-911/25/15 10:3610.0 1
Benzyl alcohol ND ug/L 12/01/15 15:41 100-51-611/25/15 10:3620.0 1
4-Bromophenylphenyl ether ND ug/L 12/01/15 15:41 101-55-311/25/15 10:3610.0 1
Butylbenzylphthalate ND ug/L 12/01/15 15:41 85-68-711/25/15 10:3610.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW11 Lab ID:92276295015 Collected:11/18/15 15:40 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/01/15 15:41 59-50-711/25/15 10:3620.0 1
4-Chloroaniline ND ug/L 12/01/15 15:41 106-47-811/25/15 10:3620.0 1
Chlorobenzilate ND ug/L 12/01/15 15:41 510-15-611/25/15 10:3610.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/01/15 15:41 111-91-111/25/15 10:3610.0 1
bis(2-Chloroethyl) ether ND ug/L 12/01/15 15:41 111-44-411/25/15 10:3610.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/01/15 15:41 108-60-111/25/15 10:3610.0 1
2-Chloronaphthalene ND ug/L 12/01/15 15:41 91-58-711/25/15 10:3610.0 1
2-Chlorophenol ND ug/L 12/01/15 15:41 95-57-811/25/15 10:3610.0 1
4-Chlorophenylphenyl ether ND ug/L 12/01/15 15:41 7005-72-311/25/15 10:3610.0 1
Chrysene ND ug/L 12/01/15 15:41 218-01-911/25/15 10:3610.0 1
Diallate ND ug/L 12/01/15 15:41 2303-16-411/25/15 10:3610.0 1
Dibenz(a,h)anthracene ND ug/L 12/01/15 15:41 53-70-311/25/15 10:3610.0 1
Dibenzofuran ND ug/L 12/01/15 15:41 132-64-911/25/15 10:3610.0 1
3,3'-Dichlorobenzidine ND ug/L 12/01/15 15:41 91-94-111/25/15 10:3620.0 1
2,4-Dichlorophenol ND ug/L 12/01/15 15:41 120-83-211/25/15 10:3610.0 1
2,6-Dichlorophenol ND ug/L 12/01/15 15:41 87-65-011/25/15 10:3610.0 1
Diethylphthalate ND ug/L 12/01/15 15:41 84-66-211/25/15 10:3610.0 1
Dimethoate ND ug/L 12/01/15 15:41 60-51-511/25/15 10:3610.0 1
P-Dimethylaminoazobenzene ND ug/L 12/01/15 15:41 60-11-711/25/15 10:365.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/01/15 15:41 57-97-611/25/15 10:3610.0 1
3,3'-Dimethylbenzidine ND ug/L 12/01/15 15:41 119-93-711/25/15 10:3610.0 1
2,4-Dimethylphenol ND ug/L 12/01/15 15:41 105-67-911/25/15 10:3610.0 1
Dimethylphthalate ND ug/L 12/01/15 15:41 131-11-311/25/15 10:3610.0 1
Di-n-butylphthalate ND ug/L 12/01/15 15:41 84-74-211/25/15 10:3610.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/01/15 15:41 534-52-111/25/15 10:3620.0 1
1,3-Dinitrobenzene ND ug/L 12/01/15 15:41 99-65-011/25/15 10:3620.0 1
2,4-Dinitrophenol ND ug/L 12/01/15 15:41 51-28-511/25/15 10:3650.0 1
2,4-Dinitrotoluene ND ug/L 12/01/15 15:41 121-14-211/25/15 10:3610.0 1
2,6-Dinitrotoluene ND ug/L 12/01/15 15:41 606-20-211/25/15 10:3610.0 1
Di-n-octylphthalate ND ug/L 12/01/15 15:41 117-84-011/25/15 10:3610.0 1
Diphenylamine ND ug/L 12/01/15 15:41 122-39-411/25/15 10:3610.0 1
Disulfoton ND ug/L 12/01/15 15:41 298-04-411/25/15 10:3610.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/01/15 15:41 117-81-711/25/15 10:366.0 1
Ethyl methanesulfonate ND ug/L 12/01/15 15:41 62-50-011/25/15 10:3620.0 1
Famphur ND ug/L 12/01/15 15:41 52-85-711/25/15 10:3610.0 1
Fluoranthene ND ug/L 12/01/15 15:41 206-44-011/25/15 10:3610.0 1
Fluorene ND ug/L 12/01/15 15:41 86-73-711/25/15 10:3610.0 1
Hexachlorobenzene ND ug/L 12/01/15 15:41 118-74-111/25/15 10:3610.0 1
Hexachlorocyclopentadiene ND ug/L 12/01/15 15:41 77-47-411/25/15 10:3610.0 1
Hexachloroethane ND ug/L 12/01/15 15:41 67-72-111/25/15 10:3610.0 1
Hexachlorophene ND ug/L 12/01/15 15:41 70-30-411/25/15 10:361001
Indeno(1,2,3-cd)pyrene ND ug/L 12/01/15 15:41 193-39-511/25/15 10:3610.0 1
Isodrin ND ug/L 12/01/15 15:41 465-73-611/25/15 10:3620.0 1
Isophorone ND ug/L 12/01/15 15:41 78-59-111/25/15 10:3610.0 1
Isosafrole ND ug/L 12/01/15 15:41 120-58-111/25/15 10:3610.0 1
Kepone ND ug/L 12/01/15 15:41 143-50-011/25/15 10:3610.0 1
Methapyrilene ND ug/L 12/01/15 15:41 91-80-511/25/15 10:3650.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW11 Lab ID:92276295015 Collected:11/18/15 15:40 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/01/15 15:41 56-49-511/25/15 10:3610.0 1
Methyl methanesulfonate ND ug/L 12/01/15 15:41 66-27-311/25/15 10:365.0 1
2-Methylnaphthalene ND ug/L 12/01/15 15:41 91-57-611/25/15 10:3610.0 1
Methyl parathion ND ug/L 12/01/15 15:41 298-00-011/25/15 10:3610.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/01/15 15:41 95-48-711/25/15 10:3610.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/01/15 15:4111/25/15 10:3610.0 1
1-Naphthalenamine ND ug/L 12/01/15 15:41 134-32-711/25/15 10:365.0 1
2-Naphthalenamine ND ug/L 12/01/15 15:41 91-59-811/25/15 10:365.0 1
1,4-Naphthoquinone ND ug/L 12/01/15 15:41 130-15-411/25/15 10:365.0 1
2-Nitroaniline ND ug/L 12/01/15 15:41 88-74-411/25/15 10:3650.0 1
3-Nitroaniline ND ug/L 12/01/15 15:41 99-09-211/25/15 10:3650.0 1
4-Nitroaniline ND ug/L 12/01/15 15:41 100-01-611/25/15 10:3620.0 1
Nitrobenzene ND ug/L 12/01/15 15:41 98-95-311/25/15 10:3610.0 1
2-Nitrophenol ND ug/L 12/01/15 15:41 88-75-511/25/15 10:3610.0 1
4-Nitrophenol ND ug/L 12/01/15 15:41 100-02-711/25/15 10:3650.0 1
5-Nitro-o-toluidine ND ug/L 12/01/15 15:41 99-55-811/25/15 10:3610.0 1
N-Nitrosodiethylamine ND ug/L 12/01/15 15:41 55-18-511/25/15 10:3620.0 1
N-Nitrosodimethylamine ND ug/L 12/01/15 15:41 62-75-911/25/15 10:3610.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/01/15 15:41 924-16-311/25/15 10:3610.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/01/15 15:41 621-64-711/25/15 10:3610.0 1
N-Nitrosodiphenylamine ND ug/L 12/01/15 15:41 86-30-611/25/15 10:3610.0 1
N-Nitrosomethylethylamine ND ug/L 12/01/15 15:41 10595-95-611/25/15 10:3610.0 1
N-Nitrosopiperidine ND ug/L 12/01/15 15:41 100-75-411/25/15 10:3620.0 1
N-Nitrosopyrrolidine ND ug/L 12/01/15 15:41 930-55-211/25/15 10:3610.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/01/15 15:41 126-68-111/25/15 10:3610.0 1
Parathion (Ethyl parathion)ND ug/L 12/01/15 15:41 56-38-211/25/15 10:3610.0 1
Pentachlorobenzene ND ug/L 12/01/15 15:41 608-93-511/25/15 10:3610.0 1
Pentachloronitrobenzene ND ug/L 12/01/15 15:41 82-68-811/25/15 10:3620.0 1
Pentachlorophenol ND ug/L 12/01/15 15:41 87-86-511/25/15 10:3625.0 1
Phenacetin ND ug/L 12/01/15 15:41 62-44-211/25/15 10:3620.0 1
Phenanthrene ND ug/L 12/01/15 15:41 85-01-811/25/15 10:3610.0 1
Phenol ND ug/L 12/01/15 15:41 108-95-211/25/15 10:3610.0 1
p-Phenylenediamine ND ug/L 12/01/15 15:41 106-50-311/25/15 10:3610.0 1
Phorate ND ug/L 12/01/15 15:41 298-02-211/25/15 10:3610.0 1
Pronamide ND ug/L 12/01/15 15:41 23950-58-511/25/15 10:3610.0 1
Pyrene ND ug/L 12/01/15 15:41 129-00-011/25/15 10:3610.0 1
Safrole ND ug/L 12/01/15 15:41 94-59-711/25/15 10:3610.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/01/15 15:41 95-94-311/25/15 10:3610.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/01/15 15:41 58-90-211/25/15 10:3610.0 1
Thionazin ND ug/L 12/01/15 15:41 297-97-211/25/15 10:3620.0 1
O-Toluidine ND ug/L 12/01/15 15:41 95-53-411/25/15 10:3610.0 1
2,4,5-Trichlorophenol ND ug/L 12/01/15 15:41 95-95-411/25/15 10:3610.0 1
2,4,6-Trichlorophenol ND ug/L 12/01/15 15:41 88-06-211/25/15 10:3610.0 1
1,3,5-Trinitrobenzene ND ug/L 12/01/15 15:41 99-35-4 L311/25/15 10:3610.0 1
Surrogates
Nitrobenzene-d5 (S)70 %12/01/15 15:41 4165-60-011/25/15 10:3621-110 1
2-Fluorobiphenyl (S)72 %12/01/15 15:41 321-60-811/25/15 10:3627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW11 Lab ID:92276295015 Collected:11/18/15 15:40 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)80 %12/01/15 15:41 1718-51-011/25/15 10:3631-107 1
Phenol-d6 (S)23 %12/01/15 15:41 13127-88-311/25/15 10:3610-110 1
2-Fluorophenol (S)35 %12/01/15 15:41 367-12-411/25/15 10:3612-110 1
2,4,6-Tribromophenol (S)81 %12/01/15 15:41 118-79-611/25/15 10:3627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 19:36 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 19:36 75-05-850.0 1
Acrolein ND ug/L 11/20/15 19:36 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 19:36 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 19:36 107-05-12.0 1
Benzene ND ug/L 11/20/15 19:36 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 19:36 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 19:36 75-27-41.0 1
Bromoform ND ug/L 11/20/15 19:36 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 19:36 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 19:36 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 19:36 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 19:36 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 19:36 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 19:36 75-00-31.0 1
Chloroform ND ug/L 11/20/15 19:36 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 19:36 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 19:36 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 19:36 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 19:36 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 19:36 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 19:36 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 19:36 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 19:36 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 19:36 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 19:36 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/20/15 19:36 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 19:36 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 19:36 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 19:36 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 19:36 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 19:36 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 19:36 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 19:36 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 19:36 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 19:36 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 19:36 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 19:36 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 19:36 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 19:36 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW11 Lab ID:92276295015 Collected:11/18/15 15:40 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 19:36 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 19:36 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 19:36 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 19:36 126-98-710.0 1
Methylene Chloride ND ug/L 11/20/15 19:36 75-09-21.0 1
Methyl methacrylate ND ug/L 11/20/15 19:36 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 19:36 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 19:36 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 19:36 107-12-020.0 1
Styrene ND ug/L 11/20/15 19:36 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 19:36 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 19:36 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 19:36 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 19:36 109-99-910.0 1
Toluene ND ug/L 11/20/15 19:36 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 19:36 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 19:36 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 19:36 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 19:36 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/20/15 19:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 19:36 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 19:36 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 19:36 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 19:36 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 19:36 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 19:36 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %11/20/15 19:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/20/15 19:36 17060-07-070-130 1
Toluene-d8 (S)99 %11/20/15 19:36 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 127000 ug/L 11/29/15 21:1550001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 281000 ug/L 11/22/15 11:07250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/23/15 23:30 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 19100 ug/L 11/25/15 00:44 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 14900 ug/L 11/30/15 19:23 16887-00-610001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW11 Lab ID:92276295015 Collected:11/18/15 15:40 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.2J ug/L 11/25/15 02:49 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW12 Lab ID:92276295016 Collected:11/18/15 17:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/18/15 17:001
Field pH 5.8 Std. Units 11/18/15 17:000.10 1
Field Temperature 16.2 deg C 11/18/15 17:000.50 1
Static Water Level 4.77 feet 11/18/15 17:001
Field Specific Conductance 281.5 umhos/cm 11/18/15 17:001.0 1
Oxygen, Dissolved 3.4 mg/L 11/18/15 17:00 7782-44-71
Total Well Depth 15.58 feet 11/18/15 17:001
REDOX -23.3 mV 11/18/15 17:001
Turbidity 8.9 NTU 11/18/15 17:001.0 1
Odor none 11/18/15 17:001
Appearance clear 11/18/15 17:001
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/25/15 17:31 309-00-211/24/15 11:000.050 1
alpha-BHC ND ug/L 11/25/15 17:31 319-84-611/24/15 11:000.050 1
beta-BHC ND ug/L 11/25/15 17:31 319-85-711/24/15 11:000.050 1
delta-BHC ND ug/L 11/25/15 17:31 319-86-811/24/15 11:000.050 1
gamma-BHC (Lindane)ND ug/L 11/25/15 17:31 58-89-911/24/15 11:000.050 1
Chlordane (Technical)ND ug/L 11/25/15 17:31 57-74-911/24/15 11:000.20 1
4,4'-DDD ND ug/L 11/25/15 17:31 72-54-811/24/15 11:000.050 1
4,4'-DDE ND ug/L 11/25/15 17:31 72-55-911/24/15 11:000.050 1
4,4'-DDT ND ug/L 11/25/15 17:31 50-29-311/24/15 11:000.050 1
Dieldrin ND ug/L 11/25/15 17:31 60-57-111/24/15 11:000.050 1
Endosulfan I ND ug/L 11/25/15 17:31 959-98-811/24/15 11:000.050 1
Endosulfan II ND ug/L 11/25/15 17:31 33213-65-911/24/15 11:000.050 1
Endosulfan sulfate ND ug/L 11/25/15 17:31 1031-07-811/24/15 11:000.050 1
Endrin ND ug/L 11/25/15 17:31 72-20-811/24/15 11:000.050 1
Endrin aldehyde ND ug/L 11/25/15 17:31 7421-93-411/24/15 11:000.050 1
Heptachlor ND ug/L 11/25/15 17:31 76-44-811/24/15 11:000.050 1
Heptachlor epoxide ND ug/L 11/25/15 17:31 1024-57-311/24/15 11:000.050 1
Methoxychlor ND ug/L 11/25/15 17:31 72-43-511/24/15 11:000.15 1
Toxaphene ND ug/L 11/25/15 17:31 8001-35-211/24/15 11:000.20 1
Surrogates
Tetrachloro-m-xylene (S)76 %11/25/15 17:31 877-09-811/24/15 11:0020-130 1
Decachlorobiphenyl (S)76 %11/25/15 17:31 2051-24-311/24/15 11:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/25/15 18:03 12674-11-211/24/15 11:000.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/25/15 18:03 11104-28-211/24/15 11:000.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/25/15 18:03 11141-16-511/24/15 11:000.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/25/15 18:03 53469-21-911/24/15 11:000.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/25/15 18:03 12672-29-611/24/15 11:000.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/25/15 18:03 11097-69-111/24/15 11:000.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/25/15 18:03 11096-82-511/24/15 11:000.50 1
Surrogates
Decachlorobiphenyl (S)72 %11/25/15 18:03 2051-24-311/24/15 11:0010-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW12 Lab ID:92276295016 Collected:11/18/15 17:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/26/15 02:19 94-75-711/24/15 16:550.94 1
Dinoseb ND ug/L 11/26/15 02:19 88-85-711/24/15 16:550.19 1
2,4,5-T ND ug/L 11/26/15 02:19 93-76-511/24/15 16:550.19 1
2,4,5-TP (Silvex)ND ug/L 11/26/15 02:19 93-72-111/24/15 16:550.19 1
Surrogates
2,4-DCAA (S)75 %11/26/15 02:19 19719-28-911/24/15 16:5536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/30/15 18:35 7440-36-011/25/15 22:005.0 1
Arsenic ND ug/L 11/30/15 18:35 7440-38-211/25/15 22:0010.0 1
Barium 95.7 ug/L 11/30/15 18:35 7440-39-311/25/15 22:005.0 1
Beryllium ND ug/L 11/30/15 18:35 7440-41-711/25/15 22:001.0 1
Cadmium ND ug/L 11/30/15 18:35 7440-43-911/25/15 22:001.0 1
Chromium ND ug/L 11/30/15 18:35 7440-47-311/25/15 22:005.0 1
Cobalt ND ug/L 11/30/15 18:35 7440-48-411/25/15 22:005.0 1
Copper ND ug/L 11/30/15 18:35 7440-50-811/25/15 22:005.0 1
Iron 523 ug/L 11/30/15 18:35 7439-89-611/25/15 22:0050.0 1
Lead ND ug/L 11/30/15 18:35 7439-92-111/25/15 22:005.0 1
Manganese 49.6 ug/L 11/30/15 18:35 7439-96-511/25/15 22:005.0 1
Nickel 3.2J ug/L 11/30/15 18:35 7440-02-011/25/15 22:005.0 1
Selenium ND ug/L 11/30/15 18:35 7782-49-211/25/15 22:0010.0 1
Silver ND ug/L 11/30/15 18:35 7440-22-411/25/15 22:005.0 1
Sodium 13700 ug/L 11/30/15 18:35 7440-23-511/25/15 22:0050001
Thallium ND ug/L 12/01/15 18:29 7440-28-011/25/15 22:005.4 1
Tin ND ug/L 11/30/15 18:35 7440-31-511/25/15 22:005.0 1
Vanadium ND ug/L 11/30/15 18:35 7440-62-211/25/15 22:005.0 1
Zinc ND ug/L 11/30/15 18:35 7440-66-611/25/15 22:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 15:18 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/01/15 16:09 83-32-911/25/15 10:3610.0 1
Acenaphthylene ND ug/L 12/01/15 16:09 208-96-811/25/15 10:3610.0 1
Acetophenone ND ug/L 12/01/15 16:09 98-86-211/25/15 10:3610.0 1
2-Acetylaminofluorene ND ug/L 12/01/15 16:09 53-96-3 L211/25/15 10:3620.0 1
4-Aminobiphenyl ND ug/L 12/01/15 16:09 92-67-111/25/15 10:3610.0 1
Anthracene ND ug/L 12/01/15 16:09 120-12-711/25/15 10:3610.0 1
Benzo(a)anthracene ND ug/L 12/01/15 16:09 56-55-311/25/15 10:3610.0 1
Benzo(a)pyrene ND ug/L 12/01/15 16:09 50-32-811/25/15 10:3610.0 1
Benzo(b)fluoranthene ND ug/L 12/01/15 16:09 205-99-211/25/15 10:3610.0 1
Benzo(g,h,i)perylene ND ug/L 12/01/15 16:09 191-24-211/25/15 10:3610.0 1
Benzo(k)fluoranthene ND ug/L 12/01/15 16:09 207-08-911/25/15 10:3610.0 1
Benzyl alcohol ND ug/L 12/01/15 16:09 100-51-611/25/15 10:3620.0 1
4-Bromophenylphenyl ether ND ug/L 12/01/15 16:09 101-55-311/25/15 10:3610.0 1
Butylbenzylphthalate ND ug/L 12/01/15 16:09 85-68-711/25/15 10:3610.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW12 Lab ID:92276295016 Collected:11/18/15 17:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/01/15 16:09 59-50-711/25/15 10:3620.0 1
4-Chloroaniline ND ug/L 12/01/15 16:09 106-47-811/25/15 10:3620.0 1
Chlorobenzilate ND ug/L 12/01/15 16:09 510-15-611/25/15 10:3610.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/01/15 16:09 111-91-111/25/15 10:3610.0 1
bis(2-Chloroethyl) ether ND ug/L 12/01/15 16:09 111-44-411/25/15 10:3610.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/01/15 16:09 108-60-111/25/15 10:3610.0 1
2-Chloronaphthalene ND ug/L 12/01/15 16:09 91-58-711/25/15 10:3610.0 1
2-Chlorophenol ND ug/L 12/01/15 16:09 95-57-811/25/15 10:3610.0 1
4-Chlorophenylphenyl ether ND ug/L 12/01/15 16:09 7005-72-311/25/15 10:3610.0 1
Chrysene ND ug/L 12/01/15 16:09 218-01-911/25/15 10:3610.0 1
Diallate ND ug/L 12/01/15 16:09 2303-16-411/25/15 10:3610.0 1
Dibenz(a,h)anthracene ND ug/L 12/01/15 16:09 53-70-311/25/15 10:3610.0 1
Dibenzofuran ND ug/L 12/01/15 16:09 132-64-911/25/15 10:3610.0 1
3,3'-Dichlorobenzidine ND ug/L 12/01/15 16:09 91-94-111/25/15 10:3620.0 1
2,4-Dichlorophenol ND ug/L 12/01/15 16:09 120-83-211/25/15 10:3610.0 1
2,6-Dichlorophenol ND ug/L 12/01/15 16:09 87-65-011/25/15 10:3610.0 1
Diethylphthalate ND ug/L 12/01/15 16:09 84-66-211/25/15 10:3610.0 1
Dimethoate ND ug/L 12/01/15 16:09 60-51-511/25/15 10:3610.0 1
P-Dimethylaminoazobenzene ND ug/L 12/01/15 16:09 60-11-711/25/15 10:365.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/01/15 16:09 57-97-611/25/15 10:3610.0 1
3,3'-Dimethylbenzidine ND ug/L 12/01/15 16:09 119-93-711/25/15 10:3610.0 1
2,4-Dimethylphenol ND ug/L 12/01/15 16:09 105-67-911/25/15 10:3610.0 1
Dimethylphthalate ND ug/L 12/01/15 16:09 131-11-311/25/15 10:3610.0 1
Di-n-butylphthalate ND ug/L 12/01/15 16:09 84-74-211/25/15 10:3610.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/01/15 16:09 534-52-111/25/15 10:3620.0 1
1,3-Dinitrobenzene ND ug/L 12/01/15 16:09 99-65-011/25/15 10:3620.0 1
2,4-Dinitrophenol ND ug/L 12/01/15 16:09 51-28-511/25/15 10:3650.0 1
2,4-Dinitrotoluene ND ug/L 12/01/15 16:09 121-14-211/25/15 10:3610.0 1
2,6-Dinitrotoluene ND ug/L 12/01/15 16:09 606-20-211/25/15 10:3610.0 1
Di-n-octylphthalate 5.6J ug/L 12/01/15 16:09 117-84-011/25/15 10:3610.0 1
Diphenylamine ND ug/L 12/01/15 16:09 122-39-411/25/15 10:3610.0 1
Disulfoton ND ug/L 12/01/15 16:09 298-04-411/25/15 10:3610.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/01/15 16:09 117-81-711/25/15 10:366.0 1
Ethyl methanesulfonate ND ug/L 12/01/15 16:09 62-50-011/25/15 10:3620.0 1
Famphur ND ug/L 12/01/15 16:09 52-85-711/25/15 10:3610.0 1
Fluoranthene ND ug/L 12/01/15 16:09 206-44-011/25/15 10:3610.0 1
Fluorene ND ug/L 12/01/15 16:09 86-73-711/25/15 10:3610.0 1
Hexachlorobenzene ND ug/L 12/01/15 16:09 118-74-111/25/15 10:3610.0 1
Hexachlorocyclopentadiene ND ug/L 12/01/15 16:09 77-47-411/25/15 10:3610.0 1
Hexachloroethane ND ug/L 12/01/15 16:09 67-72-111/25/15 10:3610.0 1
Hexachlorophene ND ug/L 12/01/15 16:09 70-30-411/25/15 10:361001
Indeno(1,2,3-cd)pyrene ND ug/L 12/01/15 16:09 193-39-511/25/15 10:3610.0 1
Isodrin ND ug/L 12/01/15 16:09 465-73-611/25/15 10:3620.0 1
Isophorone ND ug/L 12/01/15 16:09 78-59-111/25/15 10:3610.0 1
Isosafrole ND ug/L 12/01/15 16:09 120-58-111/25/15 10:3610.0 1
Kepone ND ug/L 12/01/15 16:09 143-50-011/25/15 10:3610.0 1
Methapyrilene ND ug/L 12/01/15 16:09 91-80-511/25/15 10:3650.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW12 Lab ID:92276295016 Collected:11/18/15 17:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/01/15 16:09 56-49-511/25/15 10:3610.0 1
Methyl methanesulfonate ND ug/L 12/01/15 16:09 66-27-311/25/15 10:365.0 1
2-Methylnaphthalene ND ug/L 12/01/15 16:09 91-57-611/25/15 10:3610.0 1
Methyl parathion ND ug/L 12/01/15 16:09 298-00-011/25/15 10:3610.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/01/15 16:09 95-48-711/25/15 10:3610.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/01/15 16:0911/25/15 10:3610.0 1
1-Naphthalenamine ND ug/L 12/01/15 16:09 134-32-711/25/15 10:365.0 1
2-Naphthalenamine ND ug/L 12/01/15 16:09 91-59-811/25/15 10:365.0 1
1,4-Naphthoquinone ND ug/L 12/01/15 16:09 130-15-411/25/15 10:365.0 1
2-Nitroaniline ND ug/L 12/01/15 16:09 88-74-411/25/15 10:3650.0 1
3-Nitroaniline ND ug/L 12/01/15 16:09 99-09-211/25/15 10:3650.0 1
4-Nitroaniline ND ug/L 12/01/15 16:09 100-01-611/25/15 10:3620.0 1
Nitrobenzene ND ug/L 12/01/15 16:09 98-95-311/25/15 10:3610.0 1
2-Nitrophenol ND ug/L 12/01/15 16:09 88-75-511/25/15 10:3610.0 1
4-Nitrophenol ND ug/L 12/01/15 16:09 100-02-711/25/15 10:3650.0 1
5-Nitro-o-toluidine ND ug/L 12/01/15 16:09 99-55-811/25/15 10:3610.0 1
N-Nitrosodiethylamine ND ug/L 12/01/15 16:09 55-18-511/25/15 10:3620.0 1
N-Nitrosodimethylamine ND ug/L 12/01/15 16:09 62-75-911/25/15 10:3610.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/01/15 16:09 924-16-311/25/15 10:3610.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/01/15 16:09 621-64-711/25/15 10:3610.0 1
N-Nitrosodiphenylamine ND ug/L 12/01/15 16:09 86-30-611/25/15 10:3610.0 1
N-Nitrosomethylethylamine ND ug/L 12/01/15 16:09 10595-95-611/25/15 10:3610.0 1
N-Nitrosopiperidine ND ug/L 12/01/15 16:09 100-75-411/25/15 10:3620.0 1
N-Nitrosopyrrolidine ND ug/L 12/01/15 16:09 930-55-211/25/15 10:3610.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/01/15 16:09 126-68-111/25/15 10:3610.0 1
Parathion (Ethyl parathion)ND ug/L 12/01/15 16:09 56-38-211/25/15 10:3610.0 1
Pentachlorobenzene ND ug/L 12/01/15 16:09 608-93-511/25/15 10:3610.0 1
Pentachloronitrobenzene ND ug/L 12/01/15 16:09 82-68-811/25/15 10:3620.0 1
Pentachlorophenol ND ug/L 12/01/15 16:09 87-86-511/25/15 10:3625.0 1
Phenacetin ND ug/L 12/01/15 16:09 62-44-211/25/15 10:3620.0 1
Phenanthrene ND ug/L 12/01/15 16:09 85-01-811/25/15 10:3610.0 1
Phenol ND ug/L 12/01/15 16:09 108-95-211/25/15 10:3610.0 1
p-Phenylenediamine ND ug/L 12/01/15 16:09 106-50-311/25/15 10:3610.0 1
Phorate ND ug/L 12/01/15 16:09 298-02-211/25/15 10:3610.0 1
Pronamide ND ug/L 12/01/15 16:09 23950-58-511/25/15 10:3610.0 1
Pyrene ND ug/L 12/01/15 16:09 129-00-011/25/15 10:3610.0 1
Safrole ND ug/L 12/01/15 16:09 94-59-711/25/15 10:3610.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/01/15 16:09 95-94-311/25/15 10:3610.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/01/15 16:09 58-90-211/25/15 10:3610.0 1
Thionazin ND ug/L 12/01/15 16:09 297-97-211/25/15 10:3620.0 1
O-Toluidine ND ug/L 12/01/15 16:09 95-53-411/25/15 10:3610.0 1
2,4,5-Trichlorophenol ND ug/L 12/01/15 16:09 95-95-411/25/15 10:3610.0 1
2,4,6-Trichlorophenol ND ug/L 12/01/15 16:09 88-06-211/25/15 10:3610.0 1
1,3,5-Trinitrobenzene ND ug/L 12/01/15 16:09 99-35-4 L311/25/15 10:3610.0 1
Surrogates
Nitrobenzene-d5 (S)79 %12/01/15 16:09 4165-60-011/25/15 10:3621-110 1
2-Fluorobiphenyl (S)81 %12/01/15 16:09 321-60-811/25/15 10:3627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW12 Lab ID:92276295016 Collected:11/18/15 17:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)92 %12/01/15 16:09 1718-51-011/25/15 10:3631-107 1
Phenol-d6 (S)26 %12/01/15 16:09 13127-88-311/25/15 10:3610-110 1
2-Fluorophenol (S)39 %12/01/15 16:09 367-12-411/25/15 10:3612-110 1
2,4,6-Tribromophenol (S)85 %12/01/15 16:09 118-79-611/25/15 10:3627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/20/15 19:53 67-64-125.0 1
Acetonitrile ND ug/L 11/20/15 19:53 75-05-850.0 1
Acrolein ND ug/L 11/20/15 19:53 107-02-810.0 1
Acrylonitrile ND ug/L 11/20/15 19:53 107-13-110.0 1
Allyl chloride ND ug/L 11/20/15 19:53 107-05-12.0 1
Benzene ND ug/L 11/20/15 19:53 71-43-21.0 1
Bromochloromethane ND ug/L 11/20/15 19:53 74-97-51.0 1
Bromodichloromethane ND ug/L 11/20/15 19:53 75-27-41.0 1
Bromoform ND ug/L 11/20/15 19:53 75-25-21.0 1
Bromomethane ND ug/L 11/20/15 19:53 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/20/15 19:53 78-93-35.0 1
Carbon disulfide ND ug/L 11/20/15 19:53 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/20/15 19:53 56-23-51.0 1
Chlorobenzene ND ug/L 11/20/15 19:53 108-90-71.0 1
Chloroethane ND ug/L 11/20/15 19:53 75-00-31.0 1
Chloroform ND ug/L 11/20/15 19:53 67-66-31.0 1
Chloromethane ND ug/L 11/20/15 19:53 74-87-31.0 1
Chloroprene ND ug/L 11/20/15 19:53 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/20/15 19:53 96-12-82.0 1
Dibromochloromethane ND ug/L 11/20/15 19:53 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/20/15 19:53 106-93-41.0 1
Dibromomethane ND ug/L 11/20/15 19:53 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/20/15 19:53 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/20/15 19:53 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/20/15 19:53 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/20/15 19:53 110-57-61.0 1
Dichlorodifluoromethane 0.23J ug/L 11/20/15 19:53 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/20/15 19:53 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/20/15 19:53 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/20/15 19:53 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/20/15 19:53 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/20/15 19:53 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/20/15 19:53 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/20/15 19:53 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/20/15 19:53 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/20/15 19:53 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/20/15 19:53 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/20/15 19:53 10061-02-61.0 1
Ethylbenzene ND ug/L 11/20/15 19:53 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/20/15 19:53 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 101 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW12 Lab ID:92276295016 Collected:11/18/15 17:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/20/15 19:53 87-68-31.0 1
2-Hexanone ND ug/L 11/20/15 19:53 591-78-65.0 1
Isobutanol ND ug/L 11/20/15 19:53 78-83-11001
Methacrylonitrile ND ug/L 11/20/15 19:53 126-98-710.0 1
Methylene Chloride 2.0 ug/L 11/20/15 19:53 75-09-2 C91.0 1
Methyl methacrylate ND ug/L 11/20/15 19:53 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/20/15 19:53 108-10-15.0 1
Naphthalene ND ug/L 11/20/15 19:53 91-20-31.0 1
Propionitrile ND ug/L 11/20/15 19:53 107-12-020.0 1
Styrene ND ug/L 11/20/15 19:53 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/20/15 19:53 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/20/15 19:53 79-34-51.0 1
Tetrachloroethene ND ug/L 11/20/15 19:53 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/20/15 19:53 109-99-910.0 1
Toluene ND ug/L 11/20/15 19:53 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/20/15 19:53 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/20/15 19:53 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/20/15 19:53 79-00-51.0 1
Trichloroethene ND ug/L 11/20/15 19:53 79-01-61.0 1
Trichlorofluoromethane 0.82J ug/L 11/20/15 19:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/20/15 19:53 96-18-41.0 1
Vinyl acetate ND ug/L 11/20/15 19:53 108-05-42.0 1
Vinyl chloride ND ug/L 11/20/15 19:53 75-01-41.0 1
Xylene (Total)ND ug/L 11/20/15 19:53 1330-20-72.0 1
m&p-Xylene ND ug/L 11/20/15 19:53 179601-23-12.0 1
o-Xylene ND ug/L 11/20/15 19:53 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)106 %11/20/15 19:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %11/20/15 19:53 17060-07-070-130 1
Toluene-d8 (S)100 %11/20/15 19:53 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 41000 ug/L 11/29/15 21:2850001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 234000 ug/L 11/22/15 11:08250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/23/15 23:30 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 70800 ug/L 11/25/15 00:57 14808-79-840002
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 9000 ug/L 12/01/15 22:52 16887-00-610001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 102 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW12 Lab ID:92276295016 Collected:11/18/15 17:00 Received:11/18/15 20:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.3J ug/L 11/25/15 02:50 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
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Page 103 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-TRIP BLANK Lab ID:92276295017 Collected:11/16/15 08:00 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/21/15 14:35 67-64-125.0 1
Acetonitrile ND ug/L 11/21/15 14:35 75-05-850.0 1
Acrolein ND ug/L 11/21/15 14:35 107-02-810.0 1
Acrylonitrile ND ug/L 11/21/15 14:35 107-13-110.0 1
Allyl chloride ND ug/L 11/21/15 14:35 107-05-12.0 1
Benzene ND ug/L 11/21/15 14:35 71-43-21.0 1
Bromochloromethane ND ug/L 11/21/15 14:35 74-97-51.0 1
Bromodichloromethane ND ug/L 11/21/15 14:35 75-27-41.0 1
Bromoform ND ug/L 11/21/15 14:35 75-25-21.0 1
Bromomethane ND ug/L 11/21/15 14:35 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/21/15 14:35 78-93-35.0 1
Carbon disulfide ND ug/L 11/21/15 14:35 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/21/15 14:35 56-23-51.0 1
Chlorobenzene ND ug/L 11/21/15 14:35 108-90-71.0 1
Chloroethane ND ug/L 11/21/15 14:35 75-00-31.0 1
Chloroform ND ug/L 11/21/15 14:35 67-66-31.0 1
Chloromethane ND ug/L 11/21/15 14:35 74-87-31.0 1
Chloroprene ND ug/L 11/21/15 14:35 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/21/15 14:35 96-12-82.0 1
Dibromochloromethane ND ug/L 11/21/15 14:35 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/21/15 14:35 106-93-41.0 1
Dibromomethane ND ug/L 11/21/15 14:35 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/21/15 14:35 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/21/15 14:35 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/21/15 14:35 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/21/15 14:35 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/21/15 14:35 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/21/15 14:35 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/21/15 14:35 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/21/15 14:35 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/21/15 14:35 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/21/15 14:35 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/21/15 14:35 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/21/15 14:35 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/21/15 14:35 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/21/15 14:35 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/21/15 14:35 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/21/15 14:35 10061-02-61.0 1
Ethylbenzene ND ug/L 11/21/15 14:35 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/21/15 14:35 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/21/15 14:35 87-68-31.0 1
2-Hexanone ND ug/L 11/21/15 14:35 591-78-65.0 1
Isobutanol ND ug/L 11/21/15 14:35 78-83-11001
Methacrylonitrile ND ug/L 11/21/15 14:35 126-98-710.0 1
Methylene Chloride ND ug/L 11/21/15 14:35 75-09-21.0 1
Methyl methacrylate ND ug/L 11/21/15 14:35 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/21/15 14:35 108-10-15.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 104 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-TRIP BLANK Lab ID:92276295017 Collected:11/16/15 08:00 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Naphthalene ND ug/L 11/21/15 14:35 91-20-31.0 1
Propionitrile ND ug/L 11/21/15 14:35 107-12-020.0 1
Styrene ND ug/L 11/21/15 14:35 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/21/15 14:35 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/21/15 14:35 79-34-51.0 1
Tetrachloroethene ND ug/L 11/21/15 14:35 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/21/15 14:35 109-99-910.0 1
Toluene ND ug/L 11/21/15 14:35 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/21/15 14:35 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/21/15 14:35 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/21/15 14:35 79-00-51.0 1
Trichloroethene ND ug/L 11/21/15 14:35 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/21/15 14:35 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/21/15 14:35 96-18-41.0 1
Vinyl acetate ND ug/L 11/21/15 14:35 108-05-42.0 1
Vinyl chloride ND ug/L 11/21/15 14:35 75-01-41.0 1
Xylene (Total)ND ug/L 11/21/15 14:35 1330-20-72.0 1
m&p-Xylene ND ug/L 11/21/15 14:35 179601-23-12.0 1
o-Xylene ND ug/L 11/21/15 14:35 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)106 %11/21/15 14:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/21/15 14:35 17060-07-070-130 1
Toluene-d8 (S)100 %11/21/15 14:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 105 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW9 Lab ID:92276295018 Collected:11/19/15 09:40 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/19/15 09:401
Field pH 5.3 Std. Units 11/19/15 09:400.10 1
Field Temperature 15.9 deg C 11/19/15 09:400.50 1
Static Water Level 53.86 feet 11/19/15 09:401
Field Specific Conductance 151.5 umhos/cm 11/19/15 09:401.0 1
Oxygen, Dissolved 6.3 mg/L 11/19/15 09:40 7782-44-71
Total Well Depth 60.0 feet 11/19/15 09:401
REDOX 54.3 mV 11/19/15 09:401
Turbidity 2.6 NTU 11/19/15 09:401.0 1
Odor none 11/19/15 09:401
Appearance clear 11/19/15 09:401
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/25/15 17:48 309-00-211/24/15 11:000.050 1
alpha-BHC ND ug/L 11/25/15 17:48 319-84-611/24/15 11:000.050 1
beta-BHC ND ug/L 11/25/15 17:48 319-85-711/24/15 11:000.050 1
delta-BHC ND ug/L 11/25/15 17:48 319-86-811/24/15 11:000.050 1
gamma-BHC (Lindane)ND ug/L 11/25/15 17:48 58-89-911/24/15 11:000.050 1
Chlordane (Technical)ND ug/L 11/25/15 17:48 57-74-911/24/15 11:000.20 1
4,4'-DDD ND ug/L 11/25/15 17:48 72-54-811/24/15 11:000.050 1
4,4'-DDE ND ug/L 11/25/15 17:48 72-55-911/24/15 11:000.050 1
4,4'-DDT ND ug/L 11/25/15 17:48 50-29-311/24/15 11:000.050 1
Dieldrin ND ug/L 11/25/15 17:48 60-57-111/24/15 11:000.050 1
Endosulfan I ND ug/L 11/25/15 17:48 959-98-811/24/15 11:000.050 1
Endosulfan II ND ug/L 11/25/15 17:48 33213-65-911/24/15 11:000.050 1
Endosulfan sulfate ND ug/L 11/25/15 17:48 1031-07-811/24/15 11:000.050 1
Endrin ND ug/L 11/25/15 17:48 72-20-811/24/15 11:000.050 1
Endrin aldehyde ND ug/L 11/25/15 17:48 7421-93-411/24/15 11:000.050 1
Heptachlor ND ug/L 11/25/15 17:48 76-44-811/24/15 11:000.050 1
Heptachlor epoxide ND ug/L 11/25/15 17:48 1024-57-311/24/15 11:000.050 1
Methoxychlor ND ug/L 11/25/15 17:48 72-43-511/24/15 11:000.15 1
Toxaphene ND ug/L 11/25/15 17:48 8001-35-211/24/15 11:000.20 1
Surrogates
Tetrachloro-m-xylene (S)78 %11/25/15 17:48 877-09-811/24/15 11:0020-130 1
Decachlorobiphenyl (S)70 %11/25/15 17:48 2051-24-311/24/15 11:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/25/15 18:23 12674-11-211/24/15 11:000.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/25/15 18:23 11104-28-211/24/15 11:000.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/25/15 18:23 11141-16-511/24/15 11:000.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/25/15 18:23 53469-21-911/24/15 11:000.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/25/15 18:23 12672-29-611/24/15 11:000.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/25/15 18:23 11097-69-111/24/15 11:000.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/25/15 18:23 11096-82-511/24/15 11:000.50 1
Surrogates
Decachlorobiphenyl (S)73 %11/25/15 18:23 2051-24-311/24/15 11:0010-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 106 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW9 Lab ID:92276295018 Collected:11/19/15 09:40 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/26/15 02:49 94-75-711/24/15 16:550.94 1
Dinoseb ND ug/L 11/26/15 02:49 88-85-711/24/15 16:550.19 1
2,4,5-T ND ug/L 11/26/15 02:49 93-76-511/24/15 16:550.19 1
2,4,5-TP (Silvex)ND ug/L 11/26/15 02:49 93-72-111/24/15 16:550.19 1
Surrogates
2,4-DCAA (S)80 %11/26/15 02:49 19719-28-911/24/15 16:5536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/30/15 19:09 7440-36-011/25/15 22:005.0 1
Arsenic ND ug/L 11/30/15 19:09 7440-38-211/25/15 22:0010.0 1
Barium 186 ug/L 11/30/15 19:09 7440-39-311/25/15 22:005.0 1
Beryllium ND ug/L 11/30/15 19:09 7440-41-711/25/15 22:001.0 1
Cadmium ND ug/L 11/30/15 19:09 7440-43-911/25/15 22:001.0 1
Chromium ND ug/L 11/30/15 19:09 7440-47-311/25/15 22:005.0 1
Cobalt ND ug/L 11/30/15 19:09 7440-48-411/25/15 22:005.0 1
Copper ND ug/L 11/30/15 19:09 7440-50-811/25/15 22:005.0 1
Iron ND ug/L 11/30/15 19:09 7439-89-611/25/15 22:0050.0 1
Lead ND ug/L 11/30/15 19:09 7439-92-111/25/15 22:005.0 1
Manganese 4.0J ug/L 11/30/15 19:09 7439-96-511/25/15 22:005.0 1
Nickel ND ug/L 11/30/15 19:09 7440-02-011/25/15 22:005.0 1
Selenium ND ug/L 11/30/15 19:09 7782-49-211/25/15 22:0010.0 1
Silver ND ug/L 11/30/15 19:09 7440-22-411/25/15 22:005.0 1
Sodium 14500 ug/L 11/30/15 19:09 7440-23-511/25/15 22:0050001
Thallium ND ug/L 12/01/15 19:03 7440-28-011/25/15 22:005.4 1
Tin ND ug/L 11/30/15 19:09 7440-31-511/25/15 22:005.0 1
Vanadium ND ug/L 11/30/15 19:09 7440-62-211/25/15 22:005.0 1
Zinc ND ug/L 11/30/15 19:09 7440-66-611/25/15 22:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 16:03 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/01/15 16:36 83-32-911/25/15 10:3610.0 1
Acenaphthylene ND ug/L 12/01/15 16:36 208-96-811/25/15 10:3610.0 1
Acetophenone ND ug/L 12/01/15 16:36 98-86-211/25/15 10:3610.0 1
2-Acetylaminofluorene ND ug/L 12/01/15 16:36 53-96-3 L211/25/15 10:3620.0 1
4-Aminobiphenyl ND ug/L 12/01/15 16:36 92-67-111/25/15 10:3610.0 1
Anthracene ND ug/L 12/01/15 16:36 120-12-711/25/15 10:3610.0 1
Benzo(a)anthracene ND ug/L 12/01/15 16:36 56-55-311/25/15 10:3610.0 1
Benzo(a)pyrene ND ug/L 12/01/15 16:36 50-32-811/25/15 10:3610.0 1
Benzo(b)fluoranthene ND ug/L 12/01/15 16:36 205-99-211/25/15 10:3610.0 1
Benzo(g,h,i)perylene ND ug/L 12/01/15 16:36 191-24-211/25/15 10:3610.0 1
Benzo(k)fluoranthene ND ug/L 12/01/15 16:36 207-08-911/25/15 10:3610.0 1
Benzyl alcohol ND ug/L 12/01/15 16:36 100-51-611/25/15 10:3620.0 1
4-Bromophenylphenyl ether ND ug/L 12/01/15 16:36 101-55-311/25/15 10:3610.0 1
Butylbenzylphthalate ND ug/L 12/01/15 16:36 85-68-711/25/15 10:3610.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 107 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW9 Lab ID:92276295018 Collected:11/19/15 09:40 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/01/15 16:36 59-50-711/25/15 10:3620.0 1
4-Chloroaniline ND ug/L 12/01/15 16:36 106-47-811/25/15 10:3620.0 1
Chlorobenzilate ND ug/L 12/01/15 16:36 510-15-611/25/15 10:3610.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/01/15 16:36 111-91-111/25/15 10:3610.0 1
bis(2-Chloroethyl) ether ND ug/L 12/01/15 16:36 111-44-411/25/15 10:3610.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/01/15 16:36 108-60-111/25/15 10:3610.0 1
2-Chloronaphthalene ND ug/L 12/01/15 16:36 91-58-711/25/15 10:3610.0 1
2-Chlorophenol ND ug/L 12/01/15 16:36 95-57-811/25/15 10:3610.0 1
4-Chlorophenylphenyl ether ND ug/L 12/01/15 16:36 7005-72-311/25/15 10:3610.0 1
Chrysene ND ug/L 12/01/15 16:36 218-01-911/25/15 10:3610.0 1
Diallate ND ug/L 12/01/15 16:36 2303-16-411/25/15 10:3610.0 1
Dibenz(a,h)anthracene ND ug/L 12/01/15 16:36 53-70-311/25/15 10:3610.0 1
Dibenzofuran ND ug/L 12/01/15 16:36 132-64-911/25/15 10:3610.0 1
3,3'-Dichlorobenzidine ND ug/L 12/01/15 16:36 91-94-111/25/15 10:3620.0 1
2,4-Dichlorophenol ND ug/L 12/01/15 16:36 120-83-211/25/15 10:3610.0 1
2,6-Dichlorophenol ND ug/L 12/01/15 16:36 87-65-011/25/15 10:3610.0 1
Diethylphthalate ND ug/L 12/01/15 16:36 84-66-211/25/15 10:3610.0 1
Dimethoate ND ug/L 12/01/15 16:36 60-51-511/25/15 10:3610.0 1
P-Dimethylaminoazobenzene ND ug/L 12/01/15 16:36 60-11-711/25/15 10:365.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/01/15 16:36 57-97-611/25/15 10:3610.0 1
3,3'-Dimethylbenzidine ND ug/L 12/01/15 16:36 119-93-711/25/15 10:3610.0 1
2,4-Dimethylphenol ND ug/L 12/01/15 16:36 105-67-911/25/15 10:3610.0 1
Dimethylphthalate ND ug/L 12/01/15 16:36 131-11-311/25/15 10:3610.0 1
Di-n-butylphthalate ND ug/L 12/01/15 16:36 84-74-211/25/15 10:3610.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/01/15 16:36 534-52-111/25/15 10:3620.0 1
1,3-Dinitrobenzene ND ug/L 12/01/15 16:36 99-65-011/25/15 10:3620.0 1
2,4-Dinitrophenol ND ug/L 12/01/15 16:36 51-28-511/25/15 10:3650.0 1
2,4-Dinitrotoluene ND ug/L 12/01/15 16:36 121-14-211/25/15 10:3610.0 1
2,6-Dinitrotoluene ND ug/L 12/01/15 16:36 606-20-211/25/15 10:3610.0 1
Di-n-octylphthalate ND ug/L 12/01/15 16:36 117-84-011/25/15 10:3610.0 1
Diphenylamine ND ug/L 12/01/15 16:36 122-39-411/25/15 10:3610.0 1
Disulfoton ND ug/L 12/01/15 16:36 298-04-411/25/15 10:3610.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/01/15 16:36 117-81-711/25/15 10:366.0 1
Ethyl methanesulfonate ND ug/L 12/01/15 16:36 62-50-011/25/15 10:3620.0 1
Famphur ND ug/L 12/01/15 16:36 52-85-711/25/15 10:3610.0 1
Fluoranthene ND ug/L 12/01/15 16:36 206-44-011/25/15 10:3610.0 1
Fluorene ND ug/L 12/01/15 16:36 86-73-711/25/15 10:3610.0 1
Hexachlorobenzene ND ug/L 12/01/15 16:36 118-74-111/25/15 10:3610.0 1
Hexachlorocyclopentadiene ND ug/L 12/01/15 16:36 77-47-411/25/15 10:3610.0 1
Hexachloroethane ND ug/L 12/01/15 16:36 67-72-111/25/15 10:3610.0 1
Hexachlorophene ND ug/L 12/01/15 16:36 70-30-411/25/15 10:361001
Indeno(1,2,3-cd)pyrene ND ug/L 12/01/15 16:36 193-39-511/25/15 10:3610.0 1
Isodrin ND ug/L 12/01/15 16:36 465-73-611/25/15 10:3620.0 1
Isophorone ND ug/L 12/01/15 16:36 78-59-111/25/15 10:3610.0 1
Isosafrole ND ug/L 12/01/15 16:36 120-58-111/25/15 10:3610.0 1
Kepone ND ug/L 12/01/15 16:36 143-50-011/25/15 10:3610.0 1
Methapyrilene ND ug/L 12/01/15 16:36 91-80-511/25/15 10:3650.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 108 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW9 Lab ID:92276295018 Collected:11/19/15 09:40 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/01/15 16:36 56-49-511/25/15 10:3610.0 1
Methyl methanesulfonate ND ug/L 12/01/15 16:36 66-27-311/25/15 10:365.0 1
2-Methylnaphthalene ND ug/L 12/01/15 16:36 91-57-611/25/15 10:3610.0 1
Methyl parathion ND ug/L 12/01/15 16:36 298-00-011/25/15 10:3610.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/01/15 16:36 95-48-711/25/15 10:3610.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/01/15 16:3611/25/15 10:3610.0 1
1-Naphthalenamine ND ug/L 12/01/15 16:36 134-32-711/25/15 10:365.0 1
2-Naphthalenamine ND ug/L 12/01/15 16:36 91-59-811/25/15 10:365.0 1
1,4-Naphthoquinone ND ug/L 12/01/15 16:36 130-15-411/25/15 10:365.0 1
2-Nitroaniline ND ug/L 12/01/15 16:36 88-74-411/25/15 10:3650.0 1
3-Nitroaniline ND ug/L 12/01/15 16:36 99-09-211/25/15 10:3650.0 1
4-Nitroaniline ND ug/L 12/01/15 16:36 100-01-611/25/15 10:3620.0 1
Nitrobenzene ND ug/L 12/01/15 16:36 98-95-311/25/15 10:3610.0 1
2-Nitrophenol ND ug/L 12/01/15 16:36 88-75-511/25/15 10:3610.0 1
4-Nitrophenol ND ug/L 12/01/15 16:36 100-02-711/25/15 10:3650.0 1
5-Nitro-o-toluidine ND ug/L 12/01/15 16:36 99-55-811/25/15 10:3610.0 1
N-Nitrosodiethylamine ND ug/L 12/01/15 16:36 55-18-511/25/15 10:3620.0 1
N-Nitrosodimethylamine ND ug/L 12/01/15 16:36 62-75-911/25/15 10:3610.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/01/15 16:36 924-16-311/25/15 10:3610.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/01/15 16:36 621-64-711/25/15 10:3610.0 1
N-Nitrosodiphenylamine ND ug/L 12/01/15 16:36 86-30-611/25/15 10:3610.0 1
N-Nitrosomethylethylamine ND ug/L 12/01/15 16:36 10595-95-611/25/15 10:3610.0 1
N-Nitrosopiperidine ND ug/L 12/01/15 16:36 100-75-411/25/15 10:3620.0 1
N-Nitrosopyrrolidine ND ug/L 12/01/15 16:36 930-55-211/25/15 10:3610.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/01/15 16:36 126-68-111/25/15 10:3610.0 1
Parathion (Ethyl parathion)ND ug/L 12/01/15 16:36 56-38-211/25/15 10:3610.0 1
Pentachlorobenzene ND ug/L 12/01/15 16:36 608-93-511/25/15 10:3610.0 1
Pentachloronitrobenzene ND ug/L 12/01/15 16:36 82-68-811/25/15 10:3620.0 1
Pentachlorophenol ND ug/L 12/01/15 16:36 87-86-511/25/15 10:3625.0 1
Phenacetin ND ug/L 12/01/15 16:36 62-44-211/25/15 10:3620.0 1
Phenanthrene ND ug/L 12/01/15 16:36 85-01-811/25/15 10:3610.0 1
Phenol ND ug/L 12/01/15 16:36 108-95-211/25/15 10:3610.0 1
p-Phenylenediamine ND ug/L 12/01/15 16:36 106-50-311/25/15 10:3610.0 1
Phorate ND ug/L 12/01/15 16:36 298-02-211/25/15 10:3610.0 1
Pronamide ND ug/L 12/01/15 16:36 23950-58-511/25/15 10:3610.0 1
Pyrene ND ug/L 12/01/15 16:36 129-00-011/25/15 10:3610.0 1
Safrole ND ug/L 12/01/15 16:36 94-59-711/25/15 10:3610.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/01/15 16:36 95-94-311/25/15 10:3610.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/01/15 16:36 58-90-211/25/15 10:3610.0 1
Thionazin ND ug/L 12/01/15 16:36 297-97-211/25/15 10:3620.0 1
O-Toluidine ND ug/L 12/01/15 16:36 95-53-411/25/15 10:3610.0 1
2,4,5-Trichlorophenol ND ug/L 12/01/15 16:36 95-95-411/25/15 10:3610.0 1
2,4,6-Trichlorophenol ND ug/L 12/01/15 16:36 88-06-211/25/15 10:3610.0 1
1,3,5-Trinitrobenzene ND ug/L 12/01/15 16:36 99-35-4 L311/25/15 10:3610.0 1
Surrogates
Nitrobenzene-d5 (S)72 %12/01/15 16:36 4165-60-011/25/15 10:3621-110 1
2-Fluorobiphenyl (S)75 %12/01/15 16:36 321-60-811/25/15 10:3627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW9 Lab ID:92276295018 Collected:11/19/15 09:40 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)85 %12/01/15 16:36 1718-51-011/25/15 10:3631-107 1
Phenol-d6 (S)21 %12/01/15 16:36 13127-88-311/25/15 10:3610-110 1
2-Fluorophenol (S)32 %12/01/15 16:36 367-12-411/25/15 10:3612-110 1
2,4,6-Tribromophenol (S)72 %12/01/15 16:36 118-79-611/25/15 10:3627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/21/15 14:52 67-64-125.0 1
Acetonitrile ND ug/L 11/21/15 14:52 75-05-850.0 1
Acrolein ND ug/L 11/21/15 14:52 107-02-810.0 1
Acrylonitrile ND ug/L 11/21/15 14:52 107-13-110.0 1
Allyl chloride ND ug/L 11/21/15 14:52 107-05-12.0 1
Benzene ND ug/L 11/21/15 14:52 71-43-21.0 1
Bromochloromethane ND ug/L 11/21/15 14:52 74-97-51.0 1
Bromodichloromethane ND ug/L 11/21/15 14:52 75-27-41.0 1
Bromoform ND ug/L 11/21/15 14:52 75-25-21.0 1
Bromomethane ND ug/L 11/21/15 14:52 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/21/15 14:52 78-93-35.0 1
Carbon disulfide ND ug/L 11/21/15 14:52 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/21/15 14:52 56-23-51.0 1
Chlorobenzene ND ug/L 11/21/15 14:52 108-90-71.0 1
Chloroethane ND ug/L 11/21/15 14:52 75-00-31.0 1
Chloroform ND ug/L 11/21/15 14:52 67-66-31.0 1
Chloromethane ND ug/L 11/21/15 14:52 74-87-31.0 1
Chloroprene ND ug/L 11/21/15 14:52 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/21/15 14:52 96-12-82.0 1
Dibromochloromethane ND ug/L 11/21/15 14:52 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/21/15 14:52 106-93-41.0 1
Dibromomethane ND ug/L 11/21/15 14:52 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/21/15 14:52 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/21/15 14:52 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/21/15 14:52 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/21/15 14:52 110-57-61.0 1
Dichlorodifluoromethane 0.76J ug/L 11/21/15 14:52 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/21/15 14:52 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/21/15 14:52 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/21/15 14:52 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/21/15 14:52 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/21/15 14:52 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/21/15 14:52 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/21/15 14:52 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/21/15 14:52 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/21/15 14:52 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/21/15 14:52 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/21/15 14:52 10061-02-61.0 1
Ethylbenzene ND ug/L 11/21/15 14:52 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/21/15 14:52 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW9 Lab ID:92276295018 Collected:11/19/15 09:40 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/21/15 14:52 87-68-31.0 1
2-Hexanone ND ug/L 11/21/15 14:52 591-78-65.0 1
Isobutanol ND ug/L 11/21/15 14:52 78-83-11001
Methacrylonitrile ND ug/L 11/21/15 14:52 126-98-710.0 1
Methylene Chloride ND ug/L 11/21/15 14:52 75-09-21.0 1
Methyl methacrylate ND ug/L 11/21/15 14:52 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/21/15 14:52 108-10-15.0 1
Naphthalene ND ug/L 11/21/15 14:52 91-20-31.0 1
Propionitrile ND ug/L 11/21/15 14:52 107-12-020.0 1
Styrene ND ug/L 11/21/15 14:52 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/21/15 14:52 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/21/15 14:52 79-34-51.0 1
Tetrachloroethene ND ug/L 11/21/15 14:52 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/21/15 14:52 109-99-910.0 1
Toluene ND ug/L 11/21/15 14:52 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/21/15 14:52 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/21/15 14:52 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/21/15 14:52 79-00-51.0 1
Trichloroethene ND ug/L 11/21/15 14:52 79-01-61.0 1
Trichlorofluoromethane 1.1 ug/L 11/21/15 14:52 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/21/15 14:52 96-18-41.0 1
Vinyl acetate ND ug/L 11/21/15 14:52 108-05-42.0 1
Vinyl chloride ND ug/L 11/21/15 14:52 75-01-41.0 1
Xylene (Total)ND ug/L 11/21/15 14:52 1330-20-72.0 1
m&p-Xylene ND ug/L 11/21/15 14:52 179601-23-12.0 1
o-Xylene ND ug/L 11/21/15 14:52 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)106 %11/21/15 14:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/21/15 14:52 17060-07-070-130 1
Toluene-d8 (S)101 %11/21/15 14:52 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 23400 ug/L 12/01/15 18:5050001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 142000 ug/L 11/24/15 18:33250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/23/15 23:30 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1110J ug/L 11/25/15 01:51 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4710 ug/L 12/01/15 23:00 16887-00-610001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW9 Lab ID:92276295018 Collected:11/19/15 09:40 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.7J ug/L 11/25/15 03:13 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW13 Lab ID:92276295019 Collected:11/19/15 13:20 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/19/15 13:201
Field pH 5.5 Std. Units 11/19/15 13:200.10 1
Field Temperature 16.2 deg C 11/19/15 13:200.50 1
Static Water Level 8.66 feet 11/19/15 13:201
Field Specific Conductance 108.9 umhos/cm 11/19/15 13:201.0 1
Oxygen, Dissolved 1.2 mg/L 11/19/15 13:20 7782-44-71
Total Well Depth 20 feet 11/19/15 13:201
REDOX 5.2 mV 11/19/15 13:201
Turbidity 51.6 NTU 11/19/15 13:201.0 1
Odor none 11/19/15 13:201
Appearance clear 11/19/15 13:201
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/25/15 18:06 309-00-211/24/15 11:000.050 1
alpha-BHC ND ug/L 11/25/15 18:06 319-84-611/24/15 11:000.050 1
beta-BHC ND ug/L 11/25/15 18:06 319-85-711/24/15 11:000.050 1
delta-BHC ND ug/L 11/25/15 18:06 319-86-811/24/15 11:000.050 1
gamma-BHC (Lindane)ND ug/L 11/25/15 18:06 58-89-911/24/15 11:000.050 1
Chlordane (Technical)ND ug/L 11/25/15 18:06 57-74-911/24/15 11:000.20 1
4,4'-DDD ND ug/L 11/25/15 18:06 72-54-811/24/15 11:000.050 1
4,4'-DDE ND ug/L 11/25/15 18:06 72-55-911/24/15 11:000.050 1
4,4'-DDT ND ug/L 11/25/15 18:06 50-29-311/24/15 11:000.050 1
Dieldrin ND ug/L 11/25/15 18:06 60-57-111/24/15 11:000.050 1
Endosulfan I ND ug/L 11/25/15 18:06 959-98-811/24/15 11:000.050 1
Endosulfan II ND ug/L 11/25/15 18:06 33213-65-911/24/15 11:000.050 1
Endosulfan sulfate ND ug/L 11/25/15 18:06 1031-07-811/24/15 11:000.050 1
Endrin ND ug/L 11/25/15 18:06 72-20-811/24/15 11:000.050 1
Endrin aldehyde ND ug/L 11/25/15 18:06 7421-93-411/24/15 11:000.050 1
Heptachlor ND ug/L 11/25/15 18:06 76-44-811/24/15 11:000.050 1
Heptachlor epoxide ND ug/L 11/25/15 18:06 1024-57-311/24/15 11:000.050 1
Methoxychlor ND ug/L 11/25/15 18:06 72-43-511/24/15 11:000.15 1
Toxaphene ND ug/L 11/25/15 18:06 8001-35-211/24/15 11:000.20 1
Surrogates
Tetrachloro-m-xylene (S)75 %11/25/15 18:06 877-09-811/24/15 11:0020-130 1
Decachlorobiphenyl (S)51 %11/25/15 18:06 2051-24-311/24/15 11:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/25/15 18:44 12674-11-211/24/15 11:000.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/25/15 18:44 11104-28-211/24/15 11:000.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/25/15 18:44 11141-16-511/24/15 11:000.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/25/15 18:44 53469-21-911/24/15 11:000.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/25/15 18:44 12672-29-611/24/15 11:000.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/25/15 18:44 11097-69-111/24/15 11:000.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/25/15 18:44 11096-82-511/24/15 11:000.50 1
Surrogates
Decachlorobiphenyl (S)52 %11/25/15 18:44 2051-24-311/24/15 11:0010-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW13 Lab ID:92276295019 Collected:11/19/15 13:20 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/26/15 03:19 94-75-711/24/15 16:550.94 1
Dinoseb ND ug/L 11/26/15 03:19 88-85-711/24/15 16:550.19 1
2,4,5-T ND ug/L 11/26/15 03:19 93-76-511/24/15 16:550.19 1
2,4,5-TP (Silvex)ND ug/L 11/26/15 03:19 93-72-111/24/15 16:550.19 1
Surrogates
2,4-DCAA (S)81 %11/26/15 03:19 19719-28-911/24/15 16:5536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 11/30/15 19:12 7440-36-011/25/15 22:005.0 1
Arsenic 2.6J ug/L 11/30/15 19:12 7440-38-211/25/15 22:0010.0 1
Barium 71.5 ug/L 11/30/15 19:12 7440-39-311/25/15 22:005.0 1
Beryllium 0.68J ug/L 11/30/15 19:12 7440-41-711/25/15 22:001.0 1
Cadmium ND ug/L 11/30/15 19:12 7440-43-911/25/15 22:001.0 1
Chromium ND ug/L 11/30/15 19:12 7440-47-311/25/15 22:005.0 1
Cobalt ND ug/L 11/30/15 19:12 7440-48-411/25/15 22:005.0 1
Copper ND ug/L 11/30/15 19:12 7440-50-811/25/15 22:005.0 1
Iron 790 ug/L 11/30/15 19:12 7439-89-611/25/15 22:0050.0 1
Lead ND ug/L 11/30/15 19:12 7439-92-111/25/15 22:005.0 1
Manganese 62.1 ug/L 11/30/15 19:12 7439-96-511/25/15 22:005.0 1
Nickel ND ug/L 11/30/15 19:12 7440-02-011/25/15 22:005.0 1
Selenium ND ug/L 11/30/15 19:12 7782-49-211/25/15 22:0010.0 1
Silver ND ug/L 11/30/15 19:12 7440-22-411/25/15 22:005.0 1
Sodium 12200 ug/L 11/30/15 19:12 7440-23-511/25/15 22:0050001
Thallium ND ug/L 12/01/15 19:06 7440-28-011/25/15 22:005.4 1
Tin ND ug/L 11/30/15 19:12 7440-31-511/25/15 22:005.0 1
Vanadium 2.6J ug/L 11/30/15 19:12 7440-62-211/25/15 22:005.0 1
Zinc 8.6J ug/L 11/30/15 19:12 7440-66-611/25/15 22:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 16:05 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/01/15 17:04 83-32-911/25/15 10:3610.0 1
Acenaphthylene ND ug/L 12/01/15 17:04 208-96-811/25/15 10:3610.0 1
Acetophenone ND ug/L 12/01/15 17:04 98-86-211/25/15 10:3610.0 1
2-Acetylaminofluorene ND ug/L 12/01/15 17:04 53-96-3 L211/25/15 10:3620.0 1
4-Aminobiphenyl ND ug/L 12/01/15 17:04 92-67-111/25/15 10:3610.0 1
Anthracene ND ug/L 12/01/15 17:04 120-12-711/25/15 10:3610.0 1
Benzo(a)anthracene ND ug/L 12/01/15 17:04 56-55-311/25/15 10:3610.0 1
Benzo(a)pyrene ND ug/L 12/01/15 17:04 50-32-811/25/15 10:3610.0 1
Benzo(b)fluoranthene ND ug/L 12/01/15 17:04 205-99-211/25/15 10:3610.0 1
Benzo(g,h,i)perylene ND ug/L 12/01/15 17:04 191-24-211/25/15 10:3610.0 1
Benzo(k)fluoranthene ND ug/L 12/01/15 17:04 207-08-911/25/15 10:3610.0 1
Benzyl alcohol ND ug/L 12/01/15 17:04 100-51-611/25/15 10:3620.0 1
4-Bromophenylphenyl ether ND ug/L 12/01/15 17:04 101-55-311/25/15 10:3610.0 1
Butylbenzylphthalate ND ug/L 12/01/15 17:04 85-68-711/25/15 10:3610.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW13 Lab ID:92276295019 Collected:11/19/15 13:20 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/01/15 17:04 59-50-711/25/15 10:3620.0 1
4-Chloroaniline ND ug/L 12/01/15 17:04 106-47-811/25/15 10:3620.0 1
Chlorobenzilate ND ug/L 12/01/15 17:04 510-15-611/25/15 10:3610.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/01/15 17:04 111-91-111/25/15 10:3610.0 1
bis(2-Chloroethyl) ether ND ug/L 12/01/15 17:04 111-44-411/25/15 10:3610.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/01/15 17:04 108-60-111/25/15 10:3610.0 1
2-Chloronaphthalene ND ug/L 12/01/15 17:04 91-58-711/25/15 10:3610.0 1
2-Chlorophenol ND ug/L 12/01/15 17:04 95-57-811/25/15 10:3610.0 1
4-Chlorophenylphenyl ether ND ug/L 12/01/15 17:04 7005-72-311/25/15 10:3610.0 1
Chrysene ND ug/L 12/01/15 17:04 218-01-911/25/15 10:3610.0 1
Diallate ND ug/L 12/01/15 17:04 2303-16-411/25/15 10:3610.0 1
Dibenz(a,h)anthracene ND ug/L 12/01/15 17:04 53-70-311/25/15 10:3610.0 1
Dibenzofuran ND ug/L 12/01/15 17:04 132-64-911/25/15 10:3610.0 1
3,3'-Dichlorobenzidine ND ug/L 12/01/15 17:04 91-94-111/25/15 10:3620.0 1
2,4-Dichlorophenol ND ug/L 12/01/15 17:04 120-83-211/25/15 10:3610.0 1
2,6-Dichlorophenol ND ug/L 12/01/15 17:04 87-65-011/25/15 10:3610.0 1
Diethylphthalate ND ug/L 12/01/15 17:04 84-66-211/25/15 10:3610.0 1
Dimethoate ND ug/L 12/01/15 17:04 60-51-511/25/15 10:3610.0 1
P-Dimethylaminoazobenzene ND ug/L 12/01/15 17:04 60-11-711/25/15 10:365.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/01/15 17:04 57-97-611/25/15 10:3610.0 1
3,3'-Dimethylbenzidine ND ug/L 12/01/15 17:04 119-93-711/25/15 10:3610.0 1
2,4-Dimethylphenol ND ug/L 12/01/15 17:04 105-67-911/25/15 10:3610.0 1
Dimethylphthalate ND ug/L 12/01/15 17:04 131-11-311/25/15 10:3610.0 1
Di-n-butylphthalate ND ug/L 12/01/15 17:04 84-74-211/25/15 10:3610.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/01/15 17:04 534-52-111/25/15 10:3620.0 1
1,3-Dinitrobenzene ND ug/L 12/01/15 17:04 99-65-011/25/15 10:3620.0 1
2,4-Dinitrophenol ND ug/L 12/01/15 17:04 51-28-511/25/15 10:3650.0 1
2,4-Dinitrotoluene ND ug/L 12/01/15 17:04 121-14-211/25/15 10:3610.0 1
2,6-Dinitrotoluene ND ug/L 12/01/15 17:04 606-20-211/25/15 10:3610.0 1
Di-n-octylphthalate ND ug/L 12/01/15 17:04 117-84-011/25/15 10:3610.0 1
Diphenylamine ND ug/L 12/01/15 17:04 122-39-411/25/15 10:3610.0 1
Disulfoton ND ug/L 12/01/15 17:04 298-04-411/25/15 10:3610.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/01/15 17:04 117-81-711/25/15 10:366.0 1
Ethyl methanesulfonate ND ug/L 12/01/15 17:04 62-50-011/25/15 10:3620.0 1
Famphur ND ug/L 12/01/15 17:04 52-85-711/25/15 10:3610.0 1
Fluoranthene ND ug/L 12/01/15 17:04 206-44-011/25/15 10:3610.0 1
Fluorene ND ug/L 12/01/15 17:04 86-73-711/25/15 10:3610.0 1
Hexachlorobenzene ND ug/L 12/01/15 17:04 118-74-111/25/15 10:3610.0 1
Hexachlorocyclopentadiene ND ug/L 12/01/15 17:04 77-47-411/25/15 10:3610.0 1
Hexachloroethane ND ug/L 12/01/15 17:04 67-72-111/25/15 10:3610.0 1
Hexachlorophene ND ug/L 12/01/15 17:04 70-30-411/25/15 10:361001
Indeno(1,2,3-cd)pyrene ND ug/L 12/01/15 17:04 193-39-511/25/15 10:3610.0 1
Isodrin ND ug/L 12/01/15 17:04 465-73-611/25/15 10:3620.0 1
Isophorone ND ug/L 12/01/15 17:04 78-59-111/25/15 10:3610.0 1
Isosafrole ND ug/L 12/01/15 17:04 120-58-111/25/15 10:3610.0 1
Kepone ND ug/L 12/01/15 17:04 143-50-011/25/15 10:3610.0 1
Methapyrilene ND ug/L 12/01/15 17:04 91-80-511/25/15 10:3650.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW13 Lab ID:92276295019 Collected:11/19/15 13:20 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/01/15 17:04 56-49-511/25/15 10:3610.0 1
Methyl methanesulfonate ND ug/L 12/01/15 17:04 66-27-311/25/15 10:365.0 1
2-Methylnaphthalene ND ug/L 12/01/15 17:04 91-57-611/25/15 10:3610.0 1
Methyl parathion ND ug/L 12/01/15 17:04 298-00-011/25/15 10:3610.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/01/15 17:04 95-48-711/25/15 10:3610.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/01/15 17:0411/25/15 10:3610.0 1
1-Naphthalenamine ND ug/L 12/01/15 17:04 134-32-711/25/15 10:365.0 1
2-Naphthalenamine ND ug/L 12/01/15 17:04 91-59-811/25/15 10:365.0 1
1,4-Naphthoquinone ND ug/L 12/01/15 17:04 130-15-411/25/15 10:365.0 1
2-Nitroaniline ND ug/L 12/01/15 17:04 88-74-411/25/15 10:3650.0 1
3-Nitroaniline ND ug/L 12/01/15 17:04 99-09-211/25/15 10:3650.0 1
4-Nitroaniline ND ug/L 12/01/15 17:04 100-01-611/25/15 10:3620.0 1
Nitrobenzene ND ug/L 12/01/15 17:04 98-95-311/25/15 10:3610.0 1
2-Nitrophenol ND ug/L 12/01/15 17:04 88-75-511/25/15 10:3610.0 1
4-Nitrophenol ND ug/L 12/01/15 17:04 100-02-711/25/15 10:3650.0 1
5-Nitro-o-toluidine ND ug/L 12/01/15 17:04 99-55-811/25/15 10:3610.0 1
N-Nitrosodiethylamine ND ug/L 12/01/15 17:04 55-18-511/25/15 10:3620.0 1
N-Nitrosodimethylamine ND ug/L 12/01/15 17:04 62-75-911/25/15 10:3610.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/01/15 17:04 924-16-311/25/15 10:3610.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/01/15 17:04 621-64-711/25/15 10:3610.0 1
N-Nitrosodiphenylamine ND ug/L 12/01/15 17:04 86-30-611/25/15 10:3610.0 1
N-Nitrosomethylethylamine ND ug/L 12/01/15 17:04 10595-95-611/25/15 10:3610.0 1
N-Nitrosopiperidine ND ug/L 12/01/15 17:04 100-75-411/25/15 10:3620.0 1
N-Nitrosopyrrolidine ND ug/L 12/01/15 17:04 930-55-211/25/15 10:3610.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/01/15 17:04 126-68-111/25/15 10:3610.0 1
Parathion (Ethyl parathion)ND ug/L 12/01/15 17:04 56-38-211/25/15 10:3610.0 1
Pentachlorobenzene ND ug/L 12/01/15 17:04 608-93-511/25/15 10:3610.0 1
Pentachloronitrobenzene ND ug/L 12/01/15 17:04 82-68-811/25/15 10:3620.0 1
Pentachlorophenol ND ug/L 12/01/15 17:04 87-86-511/25/15 10:3625.0 1
Phenacetin ND ug/L 12/01/15 17:04 62-44-211/25/15 10:3620.0 1
Phenanthrene ND ug/L 12/01/15 17:04 85-01-811/25/15 10:3610.0 1
Phenol ND ug/L 12/01/15 17:04 108-95-211/25/15 10:3610.0 1
p-Phenylenediamine ND ug/L 12/01/15 17:04 106-50-311/25/15 10:3610.0 1
Phorate ND ug/L 12/01/15 17:04 298-02-211/25/15 10:3610.0 1
Pronamide ND ug/L 12/01/15 17:04 23950-58-511/25/15 10:3610.0 1
Pyrene ND ug/L 12/01/15 17:04 129-00-011/25/15 10:3610.0 1
Safrole ND ug/L 12/01/15 17:04 94-59-711/25/15 10:3610.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/01/15 17:04 95-94-311/25/15 10:3610.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/01/15 17:04 58-90-211/25/15 10:3610.0 1
Thionazin ND ug/L 12/01/15 17:04 297-97-211/25/15 10:3620.0 1
O-Toluidine ND ug/L 12/01/15 17:04 95-53-411/25/15 10:3610.0 1
2,4,5-Trichlorophenol ND ug/L 12/01/15 17:04 95-95-411/25/15 10:3610.0 1
2,4,6-Trichlorophenol ND ug/L 12/01/15 17:04 88-06-211/25/15 10:3610.0 1
1,3,5-Trinitrobenzene ND ug/L 12/01/15 17:04 99-35-4 L311/25/15 10:3610.0 1
Surrogates
Nitrobenzene-d5 (S)78 %12/01/15 17:04 4165-60-011/25/15 10:3621-110 1
2-Fluorobiphenyl (S)84 %12/01/15 17:04 321-60-811/25/15 10:3627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW13 Lab ID:92276295019 Collected:11/19/15 13:20 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)89 %12/01/15 17:04 1718-51-011/25/15 10:3631-107 1
Phenol-d6 (S)26 %12/01/15 17:04 13127-88-311/25/15 10:3610-110 1
2-Fluorophenol (S)42 %12/01/15 17:04 367-12-411/25/15 10:3612-110 1
2,4,6-Tribromophenol (S)85 %12/01/15 17:04 118-79-611/25/15 10:3627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/21/15 15:09 67-64-125.0 1
Acetonitrile ND ug/L 11/21/15 15:09 75-05-850.0 1
Acrolein ND ug/L 11/21/15 15:09 107-02-810.0 1
Acrylonitrile ND ug/L 11/21/15 15:09 107-13-110.0 1
Allyl chloride ND ug/L 11/21/15 15:09 107-05-12.0 1
Benzene ND ug/L 11/21/15 15:09 71-43-21.0 1
Bromochloromethane ND ug/L 11/21/15 15:09 74-97-51.0 1
Bromodichloromethane ND ug/L 11/21/15 15:09 75-27-41.0 1
Bromoform ND ug/L 11/21/15 15:09 75-25-21.0 1
Bromomethane ND ug/L 11/21/15 15:09 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/21/15 15:09 78-93-35.0 1
Carbon disulfide ND ug/L 11/21/15 15:09 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/21/15 15:09 56-23-51.0 1
Chlorobenzene ND ug/L 11/21/15 15:09 108-90-71.0 1
Chloroethane ND ug/L 11/21/15 15:09 75-00-31.0 1
Chloroform ND ug/L 11/21/15 15:09 67-66-31.0 1
Chloromethane ND ug/L 11/21/15 15:09 74-87-31.0 1
Chloroprene ND ug/L 11/21/15 15:09 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/21/15 15:09 96-12-82.0 1
Dibromochloromethane ND ug/L 11/21/15 15:09 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/21/15 15:09 106-93-41.0 1
Dibromomethane ND ug/L 11/21/15 15:09 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/21/15 15:09 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/21/15 15:09 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/21/15 15:09 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/21/15 15:09 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/21/15 15:09 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/21/15 15:09 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/21/15 15:09 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/21/15 15:09 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/21/15 15:09 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/21/15 15:09 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/21/15 15:09 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/21/15 15:09 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/21/15 15:09 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/21/15 15:09 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/21/15 15:09 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/21/15 15:09 10061-02-61.0 1
Ethylbenzene ND ug/L 11/21/15 15:09 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/21/15 15:09 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW13 Lab ID:92276295019 Collected:11/19/15 13:20 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/21/15 15:09 87-68-31.0 1
2-Hexanone ND ug/L 11/21/15 15:09 591-78-65.0 1
Isobutanol ND ug/L 11/21/15 15:09 78-83-11001
Methacrylonitrile ND ug/L 11/21/15 15:09 126-98-710.0 1
Methylene Chloride ND ug/L 11/21/15 15:09 75-09-21.0 1
Methyl methacrylate ND ug/L 11/21/15 15:09 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/21/15 15:09 108-10-15.0 1
Naphthalene ND ug/L 11/21/15 15:09 91-20-31.0 1
Propionitrile ND ug/L 11/21/15 15:09 107-12-020.0 1
Styrene ND ug/L 11/21/15 15:09 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/21/15 15:09 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/21/15 15:09 79-34-51.0 1
Tetrachloroethene ND ug/L 11/21/15 15:09 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/21/15 15:09 109-99-910.0 1
Toluene ND ug/L 11/21/15 15:09 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/21/15 15:09 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/21/15 15:09 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/21/15 15:09 79-00-51.0 1
Trichloroethene ND ug/L 11/21/15 15:09 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/21/15 15:09 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/21/15 15:09 96-18-41.0 1
Vinyl acetate ND ug/L 11/21/15 15:09 108-05-42.0 1
Vinyl chloride ND ug/L 11/21/15 15:09 75-01-41.0 1
Xylene (Total)ND ug/L 11/21/15 15:09 1330-20-72.0 1
m&p-Xylene ND ug/L 11/21/15 15:09 179601-23-12.0 1
o-Xylene ND ug/L 11/21/15 15:09 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %11/21/15 15:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/21/15 15:09 17060-07-070-130 1
Toluene-d8 (S)101 %11/21/15 15:09 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 37100 ug/L 12/01/15 19:0150001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 110000 ug/L 11/24/15 18:33250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/23/15 23:30 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 10100 ug/L 11/25/15 02:05 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3270 ug/L 12/01/15 23:00 16887-00-610001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW13 Lab ID:92276295019 Collected:11/19/15 13:20 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.0J ug/L 11/25/15 03:14 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW14 Lab ID:92276295020 Collected:11/19/15 10:55 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 11/19/15 10:551
Field pH 5.4 Std. Units 11/19/15 10:550.10 1
Field Temperature 16.3 deg C 11/19/15 10:550.50 1
Static Water Level 52.43 feet 11/19/15 10:551
Field Specific Conductance 152.1 umhos/cm 11/19/15 10:551.0 1
Oxygen, Dissolved 4.8 mg/L 11/19/15 10:55 7782-44-71
Total Well Depth 60 feet 11/19/15 10:551
REDOX 49.6 mV 11/19/15 10:551
Turbidity 5.9 NTU 11/19/15 10:551.0 1
Odor none 11/19/15 10:551
Appearance clear 11/19/15 10:551
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/25/15 18:24 309-00-211/24/15 11:000.050 1
alpha-BHC ND ug/L 11/25/15 18:24 319-84-611/24/15 11:000.050 1
beta-BHC ND ug/L 11/25/15 18:24 319-85-711/24/15 11:000.050 1
delta-BHC ND ug/L 11/25/15 18:24 319-86-811/24/15 11:000.050 1
gamma-BHC (Lindane)ND ug/L 11/25/15 18:24 58-89-911/24/15 11:000.050 1
Chlordane (Technical)ND ug/L 11/25/15 18:24 57-74-911/24/15 11:000.20 1
4,4'-DDD ND ug/L 11/25/15 18:24 72-54-811/24/15 11:000.050 1
4,4'-DDE ND ug/L 11/25/15 18:24 72-55-911/24/15 11:000.050 1
4,4'-DDT ND ug/L 11/25/15 18:24 50-29-311/24/15 11:000.050 1
Dieldrin ND ug/L 11/25/15 18:24 60-57-111/24/15 11:000.050 1
Endosulfan I ND ug/L 11/25/15 18:24 959-98-811/24/15 11:000.050 1
Endosulfan II ND ug/L 11/25/15 18:24 33213-65-911/24/15 11:000.050 1
Endosulfan sulfate ND ug/L 11/25/15 18:24 1031-07-811/24/15 11:000.050 1
Endrin ND ug/L 11/25/15 18:24 72-20-811/24/15 11:000.050 1
Endrin aldehyde ND ug/L 11/25/15 18:24 7421-93-411/24/15 11:000.050 1
Heptachlor ND ug/L 11/25/15 18:24 76-44-811/24/15 11:000.050 1
Heptachlor epoxide ND ug/L 11/25/15 18:24 1024-57-311/24/15 11:000.050 1
Methoxychlor ND ug/L 11/25/15 18:24 72-43-511/24/15 11:000.15 1
Toxaphene ND ug/L 11/25/15 18:24 8001-35-211/24/15 11:000.20 1
Surrogates
Tetrachloro-m-xylene (S)85 %11/25/15 18:24 877-09-811/24/15 11:0020-130 1
Decachlorobiphenyl (S)81 %11/25/15 18:24 2051-24-311/24/15 11:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/25/15 19:04 12674-11-211/24/15 11:000.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/25/15 19:04 11104-28-211/24/15 11:000.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/25/15 19:04 11141-16-511/24/15 11:000.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/25/15 19:04 53469-21-911/24/15 11:000.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/25/15 19:04 12672-29-611/24/15 11:000.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/25/15 19:04 11097-69-111/24/15 11:000.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/25/15 19:04 11096-82-511/24/15 11:000.50 1
Surrogates
Decachlorobiphenyl (S)84 %11/25/15 19:04 2051-24-311/24/15 11:0010-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW14 Lab ID:92276295020 Collected:11/19/15 10:55 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/26/15 03:49 94-75-711/24/15 16:550.94 1
Dinoseb ND ug/L 11/26/15 03:49 88-85-711/24/15 16:550.19 1
2,4,5-T ND ug/L 11/26/15 03:49 93-76-511/24/15 16:550.19 1
2,4,5-TP (Silvex)ND ug/L 11/26/15 03:49 93-72-111/24/15 16:550.19 1
Surrogates
2,4-DCAA (S)89 %11/26/15 03:49 19719-28-911/24/15 16:5536-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/01/15 19:09 7440-36-011/25/15 22:005.0 1
Arsenic ND ug/L 12/01/15 19:09 7440-38-211/25/15 22:0010.0 1
Barium 183 ug/L 12/01/15 19:09 7440-39-311/25/15 22:005.0 1
Beryllium 0.63J ug/L 12/01/15 19:09 7440-41-711/25/15 22:001.0 1
Cadmium ND ug/L 12/01/15 19:09 7440-43-911/25/15 22:001.0 1
Chromium ND ug/L 12/01/15 19:09 7440-47-311/25/15 22:005.0 1
Cobalt ND ug/L 12/01/15 19:09 7440-48-411/25/15 22:005.0 1
Copper ND ug/L 12/01/15 19:09 7440-50-811/25/15 22:005.0 1
Iron 466 ug/L 12/01/15 19:09 7439-89-611/25/15 22:0050.0 1
Lead ND ug/L 12/01/15 19:09 7439-92-111/25/15 22:005.0 1
Manganese 69.3 ug/L 12/01/15 19:09 7439-96-511/25/15 22:005.0 1
Nickel 2.8J ug/L 12/01/15 19:09 7440-02-011/25/15 22:005.0 1
Selenium ND ug/L 12/01/15 19:09 7782-49-211/25/15 22:0010.0 1
Silver ND ug/L 12/01/15 19:09 7440-22-411/25/15 22:005.0 1
Sodium 15800 ug/L 12/01/15 19:09 7440-23-511/25/15 22:0050001
Thallium ND ug/L 12/01/15 19:09 7440-28-011/25/15 22:005.4 1
Tin ND ug/L 12/01/15 19:09 7440-31-511/25/15 22:005.0 1
Vanadium ND ug/L 12/01/15 19:09 7440-62-211/25/15 22:005.0 1
Zinc 6.3J ug/L 12/01/15 19:09 7440-66-611/25/15 22:0010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/02/15 16:07 7439-97-612/02/15 10:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 12/02/15 14:24 83-32-911/25/15 10:3610.0 1
Acenaphthylene ND ug/L 12/02/15 14:24 208-96-811/25/15 10:3610.0 1
Acetophenone ND ug/L 12/02/15 14:24 98-86-211/25/15 10:3610.0 1
2-Acetylaminofluorene ND ug/L 12/02/15 14:24 53-96-3 L211/25/15 10:3620.0 1
4-Aminobiphenyl ND ug/L 12/02/15 14:24 92-67-111/25/15 10:3610.0 1
Anthracene ND ug/L 12/02/15 14:24 120-12-711/25/15 10:3610.0 1
Benzo(a)anthracene ND ug/L 12/02/15 14:24 56-55-311/25/15 10:3610.0 1
Benzo(a)pyrene ND ug/L 12/02/15 14:24 50-32-811/25/15 10:3610.0 1
Benzo(b)fluoranthene ND ug/L 12/02/15 14:24 205-99-211/25/15 10:3610.0 1
Benzo(g,h,i)perylene ND ug/L 12/02/15 14:24 191-24-211/25/15 10:3610.0 1
Benzo(k)fluoranthene ND ug/L 12/02/15 14:24 207-08-911/25/15 10:3610.0 1
Benzyl alcohol ND ug/L 12/02/15 14:24 100-51-611/25/15 10:3620.0 1
4-Bromophenylphenyl ether ND ug/L 12/02/15 14:24 101-55-311/25/15 10:3610.0 1
Butylbenzylphthalate ND ug/L 12/02/15 14:24 85-68-711/25/15 10:3610.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW14 Lab ID:92276295020 Collected:11/19/15 10:55 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloro-3-methylphenol ND ug/L 12/02/15 14:24 59-50-711/25/15 10:3620.0 1
4-Chloroaniline ND ug/L 12/02/15 14:24 106-47-811/25/15 10:3620.0 1
Chlorobenzilate ND ug/L 12/02/15 14:24 510-15-611/25/15 10:3610.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/02/15 14:24 111-91-111/25/15 10:3610.0 1
bis(2-Chloroethyl) ether ND ug/L 12/02/15 14:24 111-44-411/25/15 10:3610.0 1
bis(2-Chloroisopropyl) ether ND ug/L 12/02/15 14:24 108-60-111/25/15 10:3610.0 1
2-Chloronaphthalene ND ug/L 12/02/15 14:24 91-58-711/25/15 10:3610.0 1
2-Chlorophenol ND ug/L 12/02/15 14:24 95-57-811/25/15 10:3610.0 1
4-Chlorophenylphenyl ether ND ug/L 12/02/15 14:24 7005-72-311/25/15 10:3610.0 1
Chrysene ND ug/L 12/02/15 14:24 218-01-911/25/15 10:3610.0 1
Diallate ND ug/L 12/02/15 14:24 2303-16-411/25/15 10:3610.0 1
Dibenz(a,h)anthracene ND ug/L 12/02/15 14:24 53-70-311/25/15 10:3610.0 1
Dibenzofuran ND ug/L 12/02/15 14:24 132-64-911/25/15 10:3610.0 1
3,3'-Dichlorobenzidine ND ug/L 12/02/15 14:24 91-94-111/25/15 10:3620.0 1
2,4-Dichlorophenol ND ug/L 12/02/15 14:24 120-83-211/25/15 10:3610.0 1
2,6-Dichlorophenol ND ug/L 12/02/15 14:24 87-65-011/25/15 10:3610.0 1
Diethylphthalate ND ug/L 12/02/15 14:24 84-66-211/25/15 10:3610.0 1
Dimethoate ND ug/L 12/02/15 14:24 60-51-511/25/15 10:3610.0 1
P-Dimethylaminoazobenzene ND ug/L 12/02/15 14:24 60-11-711/25/15 10:365.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 12/02/15 14:24 57-97-611/25/15 10:3610.0 1
3,3'-Dimethylbenzidine ND ug/L 12/02/15 14:24 119-93-711/25/15 10:3610.0 1
2,4-Dimethylphenol ND ug/L 12/02/15 14:24 105-67-911/25/15 10:3610.0 1
Dimethylphthalate ND ug/L 12/02/15 14:24 131-11-311/25/15 10:3610.0 1
Di-n-butylphthalate ND ug/L 12/02/15 14:24 84-74-211/25/15 10:3610.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/02/15 14:24 534-52-111/25/15 10:3620.0 1
1,3-Dinitrobenzene ND ug/L 12/02/15 14:24 99-65-011/25/15 10:3620.0 1
2,4-Dinitrophenol ND ug/L 12/02/15 14:24 51-28-511/25/15 10:3650.0 1
2,4-Dinitrotoluene ND ug/L 12/02/15 14:24 121-14-211/25/15 10:3610.0 1
2,6-Dinitrotoluene ND ug/L 12/02/15 14:24 606-20-211/25/15 10:3610.0 1
Di-n-octylphthalate ND ug/L 12/02/15 14:24 117-84-011/25/15 10:3610.0 1
Diphenylamine ND ug/L 12/02/15 14:24 122-39-411/25/15 10:3610.0 1
Disulfoton ND ug/L 12/02/15 14:24 298-04-411/25/15 10:3610.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/02/15 14:24 117-81-711/25/15 10:366.0 1
Ethyl methanesulfonate ND ug/L 12/02/15 14:24 62-50-011/25/15 10:3620.0 1
Famphur ND ug/L 12/02/15 14:24 52-85-711/25/15 10:3610.0 1
Fluoranthene ND ug/L 12/02/15 14:24 206-44-011/25/15 10:3610.0 1
Fluorene ND ug/L 12/02/15 14:24 86-73-711/25/15 10:3610.0 1
Hexachlorobenzene ND ug/L 12/02/15 14:24 118-74-111/25/15 10:3610.0 1
Hexachlorocyclopentadiene ND ug/L 12/02/15 14:24 77-47-411/25/15 10:3610.0 1
Hexachloroethane ND ug/L 12/02/15 14:24 67-72-111/25/15 10:3610.0 1
Hexachlorophene ND ug/L 12/02/15 14:24 70-30-411/25/15 10:361001
Indeno(1,2,3-cd)pyrene ND ug/L 12/02/15 14:24 193-39-511/25/15 10:3610.0 1
Isodrin ND ug/L 12/02/15 14:24 465-73-611/25/15 10:3620.0 1
Isophorone ND ug/L 12/02/15 14:24 78-59-111/25/15 10:3610.0 1
Isosafrole ND ug/L 12/02/15 14:24 120-58-111/25/15 10:3610.0 1
Kepone ND ug/L 12/02/15 14:24 143-50-011/25/15 10:3610.0 1
Methapyrilene ND ug/L 12/02/15 14:24 91-80-511/25/15 10:3650.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW14 Lab ID:92276295020 Collected:11/19/15 10:55 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Methylcholanthrene ND ug/L 12/02/15 14:24 56-49-511/25/15 10:3610.0 1
Methyl methanesulfonate ND ug/L 12/02/15 14:24 66-27-311/25/15 10:365.0 1
2-Methylnaphthalene ND ug/L 12/02/15 14:24 91-57-611/25/15 10:3610.0 1
Methyl parathion ND ug/L 12/02/15 14:24 298-00-011/25/15 10:3610.0 1
2-Methylphenol(o-Cresol)ND ug/L 12/02/15 14:24 95-48-711/25/15 10:3610.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/02/15 14:2411/25/15 10:3610.0 1
1-Naphthalenamine ND ug/L 12/02/15 14:24 134-32-711/25/15 10:365.0 1
2-Naphthalenamine ND ug/L 12/02/15 14:24 91-59-811/25/15 10:365.0 1
1,4-Naphthoquinone ND ug/L 12/02/15 14:24 130-15-411/25/15 10:365.0 1
2-Nitroaniline ND ug/L 12/02/15 14:24 88-74-411/25/15 10:3650.0 1
3-Nitroaniline ND ug/L 12/02/15 14:24 99-09-211/25/15 10:3650.0 1
4-Nitroaniline ND ug/L 12/02/15 14:24 100-01-611/25/15 10:3620.0 1
Nitrobenzene ND ug/L 12/02/15 14:24 98-95-311/25/15 10:3610.0 1
2-Nitrophenol ND ug/L 12/02/15 14:24 88-75-511/25/15 10:3610.0 1
4-Nitrophenol ND ug/L 12/02/15 14:24 100-02-711/25/15 10:3650.0 1
5-Nitro-o-toluidine ND ug/L 12/02/15 14:24 99-55-811/25/15 10:3610.0 1
N-Nitrosodiethylamine ND ug/L 12/02/15 14:24 55-18-511/25/15 10:3620.0 1
N-Nitrosodimethylamine ND ug/L 12/02/15 14:24 62-75-911/25/15 10:3610.0 1
N-Nitroso-di-n-butylamine ND ug/L 12/02/15 14:24 924-16-311/25/15 10:3610.0 1
N-Nitroso-di-n-propylamine ND ug/L 12/02/15 14:24 621-64-711/25/15 10:3610.0 1
N-Nitrosodiphenylamine ND ug/L 12/02/15 14:24 86-30-611/25/15 10:3610.0 1
N-Nitrosomethylethylamine ND ug/L 12/02/15 14:24 10595-95-611/25/15 10:3610.0 1
N-Nitrosopiperidine ND ug/L 12/02/15 14:24 100-75-411/25/15 10:3620.0 1
N-Nitrosopyrrolidine ND ug/L 12/02/15 14:24 930-55-211/25/15 10:3610.0 1
O,O,O-Triethylphosphorothioate ND ug/L 12/02/15 14:24 126-68-111/25/15 10:3610.0 1
Parathion (Ethyl parathion)ND ug/L 12/02/15 14:24 56-38-211/25/15 10:3610.0 1
Pentachlorobenzene ND ug/L 12/02/15 14:24 608-93-511/25/15 10:3610.0 1
Pentachloronitrobenzene ND ug/L 12/02/15 14:24 82-68-811/25/15 10:3620.0 1
Pentachlorophenol ND ug/L 12/02/15 14:24 87-86-511/25/15 10:3625.0 1
Phenacetin ND ug/L 12/02/15 14:24 62-44-211/25/15 10:3620.0 1
Phenanthrene ND ug/L 12/02/15 14:24 85-01-811/25/15 10:3610.0 1
Phenol ND ug/L 12/02/15 14:24 108-95-211/25/15 10:3610.0 1
p-Phenylenediamine ND ug/L 12/02/15 14:24 106-50-311/25/15 10:3610.0 1
Phorate ND ug/L 12/02/15 14:24 298-02-211/25/15 10:3610.0 1
Pronamide ND ug/L 12/02/15 14:24 23950-58-511/25/15 10:3610.0 1
Pyrene ND ug/L 12/02/15 14:24 129-00-011/25/15 10:3610.0 1
Safrole ND ug/L 12/02/15 14:24 94-59-711/25/15 10:3610.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 12/02/15 14:24 95-94-311/25/15 10:3610.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 12/02/15 14:24 58-90-211/25/15 10:3610.0 1
Thionazin ND ug/L 12/02/15 14:24 297-97-211/25/15 10:3620.0 1
O-Toluidine ND ug/L 12/02/15 14:24 95-53-411/25/15 10:3610.0 1
2,4,5-Trichlorophenol ND ug/L 12/02/15 14:24 95-95-411/25/15 10:3610.0 1
2,4,6-Trichlorophenol ND ug/L 12/02/15 14:24 88-06-211/25/15 10:3610.0 1
1,3,5-Trinitrobenzene ND ug/L 12/02/15 14:24 99-35-4 L311/25/15 10:3610.0 1
Surrogates
Nitrobenzene-d5 (S)71 %12/02/15 14:24 4165-60-011/25/15 10:3621-110 1
2-Fluorobiphenyl (S)76 %12/02/15 14:24 321-60-811/25/15 10:3627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW14 Lab ID:92276295020 Collected:11/19/15 10:55 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)85 %12/02/15 14:24 1718-51-011/25/15 10:3631-107 1
Phenol-d6 (S)26 %12/02/15 14:24 13127-88-311/25/15 10:3610-110 1
2-Fluorophenol (S)38 %12/02/15 14:24 367-12-411/25/15 10:3612-110 1
2,4,6-Tribromophenol (S)83 %12/02/15 14:24 118-79-611/25/15 10:3627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/21/15 15:26 67-64-125.0 1
Acetonitrile ND ug/L 11/21/15 15:26 75-05-850.0 1
Acrolein ND ug/L 11/21/15 15:26 107-02-810.0 1
Acrylonitrile ND ug/L 11/21/15 15:26 107-13-110.0 1
Allyl chloride ND ug/L 11/21/15 15:26 107-05-12.0 1
Benzene ND ug/L 11/21/15 15:26 71-43-21.0 1
Bromochloromethane ND ug/L 11/21/15 15:26 74-97-51.0 1
Bromodichloromethane ND ug/L 11/21/15 15:26 75-27-41.0 1
Bromoform ND ug/L 11/21/15 15:26 75-25-21.0 1
Bromomethane ND ug/L 11/21/15 15:26 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/21/15 15:26 78-93-35.0 1
Carbon disulfide ND ug/L 11/21/15 15:26 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/21/15 15:26 56-23-51.0 1
Chlorobenzene ND ug/L 11/21/15 15:26 108-90-71.0 1
Chloroethane ND ug/L 11/21/15 15:26 75-00-31.0 1
Chloroform ND ug/L 11/21/15 15:26 67-66-31.0 1
Chloromethane ND ug/L 11/21/15 15:26 74-87-31.0 1
Chloroprene ND ug/L 11/21/15 15:26 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/21/15 15:26 96-12-82.0 1
Dibromochloromethane ND ug/L 11/21/15 15:26 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/21/15 15:26 106-93-41.0 1
Dibromomethane ND ug/L 11/21/15 15:26 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/21/15 15:26 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/21/15 15:26 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/21/15 15:26 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/21/15 15:26 110-57-61.0 1
Dichlorodifluoromethane 2.1 ug/L 11/21/15 15:26 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/21/15 15:26 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/21/15 15:26 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/21/15 15:26 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/21/15 15:26 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/21/15 15:26 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/21/15 15:26 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/21/15 15:26 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/21/15 15:26 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/21/15 15:26 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/21/15 15:26 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/21/15 15:26 10061-02-61.0 1
Ethylbenzene ND ug/L 11/21/15 15:26 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/21/15 15:26 97-63-21.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 124 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW14 Lab ID:92276295020 Collected:11/19/15 10:55 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 11/21/15 15:26 87-68-31.0 1
2-Hexanone ND ug/L 11/21/15 15:26 591-78-65.0 1
Isobutanol ND ug/L 11/21/15 15:26 78-83-11001
Methacrylonitrile ND ug/L 11/21/15 15:26 126-98-710.0 1
Methylene Chloride ND ug/L 11/21/15 15:26 75-09-21.0 1
Methyl methacrylate ND ug/L 11/21/15 15:26 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/21/15 15:26 108-10-15.0 1
Naphthalene ND ug/L 11/21/15 15:26 91-20-31.0 1
Propionitrile ND ug/L 11/21/15 15:26 107-12-020.0 1
Styrene ND ug/L 11/21/15 15:26 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/21/15 15:26 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/21/15 15:26 79-34-51.0 1
Tetrachloroethene ND ug/L 11/21/15 15:26 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/21/15 15:26 109-99-910.0 1
Toluene ND ug/L 11/21/15 15:26 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/21/15 15:26 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/21/15 15:26 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/21/15 15:26 79-00-51.0 1
Trichloroethene ND ug/L 11/21/15 15:26 79-01-61.0 1
Trichlorofluoromethane 0.54J ug/L 11/21/15 15:26 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/21/15 15:26 96-18-41.0 1
Vinyl acetate ND ug/L 11/21/15 15:26 108-05-42.0 1
Vinyl chloride ND ug/L 11/21/15 15:26 75-01-41.0 1
Xylene (Total)ND ug/L 11/21/15 15:26 1330-20-72.0 1
m&p-Xylene ND ug/L 11/21/15 15:26 179601-23-12.0 1
o-Xylene ND ug/L 11/21/15 15:26 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)106 %11/21/15 15:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/21/15 15:26 17060-07-070-130 1
Toluene-d8 (S)102 %11/21/15 15:26 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 51500 ug/L 12/01/15 20:2550001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 135000 ug/L 11/24/15 18:34250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/25/15 17:30 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1080J ug/L 11/25/15 02:46 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3930 ug/L 12/01/15 23:01 16887-00-610001
REPORT OF LABORATORY ANALYSIS
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Page 125 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW14 Lab ID:92276295020 Collected:11/19/15 10:55 Received:11/19/15 17:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.3J ug/L 11/25/15 03:15 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
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Page 126 of 265
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276295
OSR
Sample:3412-MW3R Lab ID:92280822001 Collected:12/22/15 10:00 Received:12/22/15 13:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/22/15 10:001
Field pH 6.0 Std. Units 12/22/15 10:000.10 1
Field Temperature 13.6 deg C 12/22/15 10:000.50 1
Static Water Level 20.86 feet 12/22/15 10:001
Field Specific Conductance 365.6 umhos/cm 12/22/15 10:001.0 1
Oxygen, Dissolved 1.0 mg/L 12/22/15 10:00 7782-44-71
Total Well Depth 27 feet 12/22/15 10:001
REDOX -71.6 mV 12/22/15 10:001
Turbidity 7.8 NTU 12/22/15 10:001.0 1
Odor NONE 12/22/15 10:001
Appearance CLEAR 12/22/15 10:001
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 12/28/15 16:09 94-75-712/23/15 15:100.94 1
Dinoseb ND ug/L 12/28/15 16:09 88-85-712/23/15 15:100.19 1
2,4,5-T ND ug/L 12/28/15 16:09 93-76-512/23/15 15:100.19 1
2,4,5-TP (Silvex)ND ug/L 12/28/15 16:09 93-72-112/23/15 15:100.19 1
Surrogates
2,4-DCAA (S)98 %12/28/15 16:09 19719-28-912/23/15 15:1036-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 127 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/8709
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005, 92276295006, 92276295007,
92276295008, 92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617067
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005, 92276295006, 92276295007,
92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 12/02/15 13:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617068LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617069MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276562003
1617070
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 97 75-125103 62.5ND 2.5 2.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/8711
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617079
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 12/02/15 14:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617080LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.72.5 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617081MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276534004
1617082
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 82 75-12582 02.5ND 2.1 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/8712
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92276295018, 92276295019, 92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617083
Associated Lab Samples:92276295018, 92276295019, 92276295020
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 12/02/15 15:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617084LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617085MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277227005
1617086
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 104 75-125106 12.5ND 2.6 2.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 130 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20064
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1610065
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 11/23/15 20:55
Arsenic ug/L ND 10.0 11/23/15 20:55
Barium ug/L ND 5.0 11/23/15 20:55
Beryllium ug/L ND 1.0 11/23/15 20:55
Cadmium ug/L ND 1.0 11/23/15 20:55
Chromium ug/L ND 5.0 11/23/15 20:55
Cobalt ug/L ND 5.0 11/23/15 20:55
Copper ug/L ND 5.0 11/23/15 20:55
Iron ug/L ND 50.0 11/23/15 20:55
Lead ug/L ND 5.0 11/23/15 20:55
Manganese ug/L ND 5.0 11/23/15 20:55
Nickel ug/L ND 5.0 11/23/15 20:55
Selenium ug/L ND 10.0 11/23/15 20:55
Silver ug/L ND 5.0 11/23/15 20:55
Sodium ug/L ND 5000 11/23/15 20:55
Thallium ug/L ND 5.4 11/23/15 20:55
Tin ug/L ND 5.0 11/23/15 20:55
Vanadium ug/L ND 5.0 11/23/15 20:55
Zinc ug/L ND 10.0 11/23/15 20:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1610066LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 485500 97 80-120
Arsenic ug/L 485500 97 80-120
Barium ug/L 482500 96 80-120
Beryllium ug/L 483500 97 80-120
Cadmium ug/L 481500 96 80-120
Chromium ug/L 470500 94 80-120
Cobalt ug/L 488500 98 80-120
Copper ug/L 485500 97 80-120
Iron ug/L 48505000 97 80-120
Lead ug/L 480500 96 80-120
Manganese ug/L 466500 93 80-120
Nickel ug/L 481500 96 80-120
Selenium ug/L 480500 96 80-120
Silver ug/L 231250 92 80-120
Sodium ug/L 4740J5000 95 80-120
Thallium ug/L 474500 95 80-120
Tin ug/L 485500 97 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 131 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1610066LABORATORY CONTROL SAMPLE:
LCSSpike
Vanadium ug/L 473500 95 80-120
Zinc ug/L 487500 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1610067MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275640003
1610068
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 106 75-12596 10500ND533481
Arsenic ug/L 500 106 75-12597 10500ND532483
Barium ug/L 500 108 75-12598 950046.5 587 535
Beryllium ug/L 500 108 75-12597 11500ND542487
Cadmium ug/L 500 106 75-12595 11500ND530477
Chromium ug/L 500 104 75-12594 11500ND523470
Cobalt ug/L 500 108 75-12597 10500ND538485
Copper ug/L 500 108 75-12597 10500ND539486
Iron ug/L 5000 114 75-125104 8500079064805970
Lead ug/L 500 105 75-12595 10500ND529476
Manganese ug/L 500 104 75-12594 950040.0 561 511
Nickel ug/L 500 106 75-12596 10500ND530478
Selenium ug/L 500 105 75-12594 11500ND526472
Silver ug/L 250 102 75-12592 11250ND256230
Sodium ug/L 5000 107 75-12597 550004550J98809380
Thallium ug/L 500 105 75-12596 95005.1J 531 484
Tin ug/L 500 108 75-12597 11500ND539484
Vanadium ug/L 500 105 75-12595 10500ND529476
Zinc ug/L 500 108 75-12597 10500ND542489
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 132 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20085
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295010, 92276295011, 92276295012, 92276295013,
92276295014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1612393
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295010, 92276295011, 92276295012, 92276295013,
92276295014
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 11/24/15 08:21
Arsenic ug/L ND 10.0 11/24/15 08:21
Barium ug/L ND 5.0 11/24/15 08:21
Beryllium ug/L ND 1.0 11/24/15 08:21
Cadmium ug/L ND 1.0 11/24/15 08:21
Chromium ug/L ND 5.0 11/24/15 08:21
Cobalt ug/L ND 5.0 11/24/15 08:21
Copper ug/L ND 5.0 11/24/15 08:21
Iron ug/L ND 50.0 11/24/15 08:21
Lead ug/L ND 5.0 11/24/15 08:21
Manganese ug/L ND 5.0 11/24/15 08:21
Nickel ug/L ND 5.0 11/24/15 08:21
Selenium ug/L ND 10.0 11/24/15 08:21
Silver ug/L ND 5.0 11/24/15 08:21
Sodium ug/L ND 5000 11/24/15 08:21
Thallium ug/L ND 5.4 11/24/15 16:28
Tin ug/L ND 5.0 11/24/15 08:21
Vanadium ug/L ND 5.0 11/24/15 08:21
Zinc ug/L ND 10.0 11/24/15 08:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612394LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 512500 102 80-120
Arsenic ug/L 497500 99 80-120
Barium ug/L 483500 97 80-120
Beryllium ug/L 488500 98 80-120
Cadmium ug/L 483500 97 80-120
Chromium ug/L 466500 93 80-120
Cobalt ug/L 491500 98 80-120
Copper ug/L 483500 97 80-120
Iron ug/L 50505000 101 80-120
Lead ug/L 485500 97 80-120
Manganese ug/L 469500 94 80-120
Nickel ug/L 481500 96 80-120
Selenium ug/L 490500 98 80-120
Silver ug/L 242250 97 80-120
Sodium ug/L 4880J5000 98 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 133 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612394LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 480500 96 80-120
Tin ug/L 511500 102 80-120
Vanadium ug/L 476500 95 80-120
Zinc ug/L 500500 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1612395MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276562005
1612396
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 95 75-12597 2500ND476484
Arsenic ug/L 500 93 75-12594 2500ND463471
Barium ug/L 500 89 75-12591 250088.9 533 546
Beryllium ug/L 500 91 75-12593 25001.6 457 468
Cadmium ug/L 500 90 75-12591 2500ND448456
Chromium ug/L 500 86 75-12588 3500ND430441
Cobalt ug/L 500 90 75-12592 2500186634646
Copper ug/L 500 89 75-12592 3500ND448461
Iron ug/L 5000 93 75-12596 35000150061306310
Lead ug/L 500 88 75-12590 2500ND442453
Manganese ug/L M15003975-12571 3500570059006050
Nickel ug/L 500 88 75-12590 250025.0 464 473
Selenium ug/L 500 90 75-12592 2500ND451458
Silver ug/L 250 90 75-12592 3250ND224231
Sodium ug/L 5000 81 75-12593 35000152001920019800
Thallium ug/L 500 89 75-12593 5500ND444465
Tin ug/L 500 95 75-12597 2500ND477485
Vanadium ug/L 500 87 75-12590 35007.3J 444 457
Zinc ug/L 500 91 75-12593 250076.8 532 544
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1612513MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276534004
1612514
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12599 1500ND490497
Arsenic ug/L 500 96 75-12597 1500ND478484
Barium ug/L 500 92 75-12593 150081.0 540 545
Beryllium ug/L 500 94 75-12595 1500ND470476
Cadmium ug/L 500 93 75-12594 1500ND463469
Chromium ug/L 500 88 75-12590 2500ND442450
Cobalt ug/L 500 91 75-12592 150046.4 502 507
Copper ug/L 500 93 75-12595 2500ND464474
Iron ug/L 5000 95 75-12597 2500012748804960
Lead ug/L 500 90 75-12592 2500ND450458
Manganese ug/L M15008575-12567 1500576061806090
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
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[phone]
Page 134 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1612513MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276534004
1612514
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nickel ug/L 500 89 75-12590 150031.1 475 481
Selenium ug/L 500 93 75-12594 1500ND464470
Silver ug/L 250 93 75-12595 2250ND233237
Sodium ug/L 5000 94 75-12590 15000160002070020500
Thallium ug/L 500 90 75-12593 3500ND452466
Tin ug/L 500 97 75-12598 1500ND484490
Vanadium ug/L 500 91 75-12593 250020.6 476 484
Zinc ug/L 500 92 75-12593 150047.0 508 514
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 135 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20122
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92276295009, 92276295016, 92276295018, 92276295019, 92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1615891
Associated Lab Samples:92276295009, 92276295016, 92276295018, 92276295019, 92276295020
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 12/01/15 16:21
Arsenic ug/L ND 10.0 12/01/15 16:21
Barium ug/L ND 5.0 12/01/15 16:21
Beryllium ug/L ND 1.0 12/01/15 16:21
Cadmium ug/L ND 1.0 12/01/15 16:21
Chromium ug/L ND 5.0 12/01/15 16:21
Cobalt ug/L ND 5.0 12/01/15 16:21
Copper ug/L ND 5.0 12/01/15 16:21
Iron ug/L ND 50.0 12/01/15 16:21
Lead ug/L ND 5.0 12/01/15 16:21
Manganese ug/L ND 5.0 12/01/15 16:21
Nickel ug/L ND 5.0 12/01/15 16:21
Selenium ug/L ND 10.0 12/01/15 16:21
Silver ug/L ND 5.0 12/01/15 16:21
Sodium ug/L ND 5000 12/01/15 16:21
Thallium ug/L ND 5.4 12/01/15 17:42
Tin ug/L ND 5.0 12/01/15 16:21
Vanadium ug/L ND 5.0 12/01/15 16:21
Zinc ug/L ND 10.0 12/01/15 16:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1615892LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 485500 97 80-120
Arsenic ug/L 463500 93 80-120
Barium ug/L 479500 96 80-120
Beryllium ug/L 480500 96 80-120
Cadmium ug/L 477500 95 80-120
Chromium ug/L 474500 95 80-120
Cobalt ug/L 479500 96 80-120
Copper ug/L 484500 97 80-120
Iron ug/L 47805000 96 80-120
Lead ug/L 474500 95 80-120
Manganese ug/L 466500 93 80-120
Nickel ug/L 478500 96 80-120
Selenium ug/L 468500 94 80-120
Silver ug/L 228250 91 80-120
Sodium ug/L 4740J5000 95 80-120
Thallium ug/L 465500 93 80-120
Tin ug/L 487500 97 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 136 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1615892LABORATORY CONTROL SAMPLE:
LCSSpike
Vanadium ug/L 475500 95 80-120
Zinc ug/L 474500 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1615893MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276295009
1615894
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12592 7500ND493461
Arsenic ug/L 500 96 75-12589 7500ND480447
Barium ug/L 500 97 75-12592 450092.7 578 554
Beryllium ug/L 500 98 75-12592 6500ND489461
Cadmium ug/L 500 97 75-12591 7500ND487453
Chromium ug/L 500 96 75-12591 5500ND481457
Cobalt ug/L 500 95 75-12589 65002.5J 478 449
Copper ug/L 500 99 75-12593 6500ND498467
Iron ug/L 5000 92 75-125105 25000326003720037900
Lead ug/L 500 94 75-12588 7500ND473442
Manganese ug/L 500 94 75-12599 1500189023602390
Nickel ug/L 500 95 75-12589 6500ND476447
Selenium ug/L 500 95 75-12589 7500ND478445
Silver ug/L 250 94 75-12588 7250ND236220
Sodium ug/L 5000 98 75-12597 05000113001620016100
Thallium ug/L 500 97 75-12590 8500ND488453
Tin ug/L 500 98 75-12592 7500ND492461
Vanadium ug/L 500 98 75-12592 65003.7J 491 462
Zinc ug/L 500 94 75-12588 6500ND468442
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 137 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20153
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92276295015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1618438
Associated Lab Samples:92276295015
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 12/03/15 16:42
Arsenic ug/L ND 10.0 12/03/15 16:42
Barium ug/L ND 5.0 12/03/15 16:42
Beryllium ug/L ND 1.0 12/03/15 16:42
Cadmium ug/L ND 1.0 12/03/15 16:42
Chromium ug/L ND 5.0 12/03/15 16:42
Cobalt ug/L ND 5.0 12/03/15 16:42
Copper ug/L ND 5.0 12/03/15 16:42
Iron ug/L ND 50.0 12/03/15 16:42
Lead ug/L ND 5.0 12/03/15 16:42
Manganese ug/L ND 5.0 12/03/15 16:42
Nickel ug/L ND 5.0 12/03/15 16:42
Selenium ug/L ND 10.0 12/03/15 16:42
Silver ug/L ND 5.0 12/03/15 16:42
Sodium ug/L ND 5000 12/03/15 16:42
Thallium ug/L ND 5.4 12/03/15 16:42
Tin ug/L ND 5.0 12/03/15 16:42
Vanadium ug/L ND 5.0 12/03/15 16:42
Zinc ug/L ND 10.0 12/03/15 16:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1618439LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 472500 94 80-120
Arsenic ug/L 450500 90 80-120
Barium ug/L 474500 95 80-120
Beryllium ug/L 479500 96 80-120
Cadmium ug/L 469500 94 80-120
Chromium ug/L 475500 95 80-120
Cobalt ug/L 471500 94 80-120
Copper ug/L 471500 94 80-120
Iron ug/L 48605000 97 80-120
Lead ug/L 463500 93 80-120
Manganese ug/L 473500 95 80-120
Nickel ug/L 472500 94 80-120
Selenium ug/L 457500 91 80-120
Silver ug/L 234250 94 80-120
Sodium ug/L 4860J5000 97 80-120
Thallium ug/L 462500 92 80-120
Tin ug/L 480500 96 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 138 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1618439LABORATORY CONTROL SAMPLE:
LCSSpike
Vanadium ug/L 479500 96 80-120
Zinc ug/L 468500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1618440MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276295015
1618441
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 101 75-12596 6500ND508479
Arsenic ug/L 500 98 75-12592 7500ND491460
Barium ug/L 500 103 75-12597 550097.2 610 581
Beryllium ug/L 500 104 75-12598 6500ND521490
Cadmium ug/L 500 101 75-12594 6500ND504472
Chromium ug/L 500 102 75-12595 7500ND510477
Cobalt ug/L 500 99 75-12593 75002.9J 500 469
Copper ug/L 500 103 75-12597 65002.8J 516 486
Iron ug/L 5000 105 75-125116 15000346003980040400
Lead ug/L 500 98 75-12592 6500ND490459
Manganese ug/L 500 103 75-125105 0500202025402540
Nickel ug/L 500 100 75-12593 7500ND499467
Selenium ug/L 500 97 75-12591 75005.6J 492 460
Silver ug/L 250 101 75-12595 6250ND253237
Sodium ug/L 5000 106 75-125106 05000120001730017300
Thallium ug/L 500 96 75-12593 35008.8 490 474
Tin ug/L 500 103 75-12597 6500ND513484
Vanadium ug/L 500 104 75-12598 65003.5J 524 491
Zinc ug/L 500 99 75-12593 7500ND498465
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 139 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34361
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005, 92276295006, 92276295007,
92276295008, 92276295009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1611084
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005, 92276295006, 92276295007,
92276295008, 92276295009
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/19/15 22:51
1,1,1-Trichloroethane ug/L ND 1.0 11/19/15 22:51
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/19/15 22:51
1,1,2-Trichloroethane ug/L ND 1.0 11/19/15 22:51
1,1-Dichloroethane ug/L ND 1.0 11/19/15 22:51
1,1-Dichloroethene ug/L ND 1.0 11/19/15 22:51
1,1-Dichloropropene ug/L ND 1.0 11/19/15 22:51
1,2,3-Trichloropropane ug/L ND 1.0 11/19/15 22:51
1,2,4-Trichlorobenzene ug/L ND 1.0 11/19/15 22:51
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/19/15 22:51
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/19/15 22:51
1,2-Dichlorobenzene ug/L ND 1.0 11/19/15 22:51
1,2-Dichloroethane ug/L ND 1.0 11/19/15 22:51
1,2-Dichloropropane ug/L ND 1.0 11/19/15 22:51
1,3-Dichlorobenzene ug/L ND 1.0 11/19/15 22:51
1,3-Dichloropropane ug/L ND 1.0 11/19/15 22:51
1,4-Dichlorobenzene ug/L ND 1.0 11/19/15 22:51
2,2-Dichloropropane ug/L ND 1.0 11/19/15 22:51
2-Butanone (MEK)ug/L ND 5.0 11/19/15 22:51
2-Hexanone ug/L ND 5.0 11/19/15 22:51
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/19/15 22:51
Acetone ug/L ND 25.0 11/19/15 22:51
Acetonitrile ug/L ND 50.0 11/19/15 22:51
Acrolein ug/L ND 10.0 11/19/15 22:51
Acrylonitrile ug/L ND 10.0 11/19/15 22:51
Allyl chloride ug/L ND 2.0 11/19/15 22:51
Benzene ug/L ND 1.0 11/19/15 22:51
Bromochloromethane ug/L ND 1.0 11/19/15 22:51
Bromodichloromethane ug/L ND 1.0 11/19/15 22:51
Bromoform ug/L ND 1.0 11/19/15 22:51
Bromomethane ug/L ND 2.0 11/19/15 22:51
Carbon disulfide ug/L ND 2.0 11/19/15 22:51
Carbon tetrachloride ug/L ND 1.0 11/19/15 22:51
Chlorobenzene ug/L ND 1.0 11/19/15 22:51
Chloroethane ug/L ND 1.0 11/19/15 22:51
Chloroform ug/L ND 1.0 11/19/15 22:51
Chloromethane ug/L ND 1.0 11/19/15 22:51
Chloroprene ug/L ND 5.0 11/19/15 22:51
cis-1,2-Dichloroethene ug/L ND 1.0 11/19/15 22:51
cis-1,3-Dichloropropene ug/L ND 1.0 11/19/15 22:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 140 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1611084
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005, 92276295006, 92276295007,
92276295008, 92276295009
Matrix:Water
Analyzed
Dibromochloromethane ug/L ND 1.0 11/19/15 22:51
Dibromomethane ug/L ND 1.0 11/19/15 22:51
Dichlorodifluoromethane ug/L ND 1.0 11/19/15 22:51
Ethyl methacrylate ug/L ND 1.0 11/19/15 22:51
Ethylbenzene ug/L ND 1.0 11/19/15 22:51
Hexachloro-1,3-butadiene ug/L ND 1.0 11/19/15 22:51
Isobutanol ug/L ND 100 11/19/15 22:51
m&p-Xylene ug/L ND 2.0 11/19/15 22:51
Methacrylonitrile ug/L ND 10.0 11/19/15 22:51
Methyl methacrylate ug/L ND 2.0 11/19/15 22:51
Methylene Chloride ug/L ND 1.0 11/19/15 22:51
Naphthalene ug/L ND 1.0 11/19/15 22:51
o-Xylene ug/L ND 1.0 11/19/15 22:51
Propionitrile ug/L ND 20.0 11/19/15 22:51
Styrene ug/L ND 1.0 11/19/15 22:51
Tetrachloroethene ug/L ND 1.0 11/19/15 22:51
Tetrahydrofuran ug/L ND 10.0 11/19/15 22:51
Toluene ug/L ND 1.0 11/19/15 22:51
trans-1,2-Dichloroethene ug/L ND 1.0 11/19/15 22:51
trans-1,3-Dichloropropene ug/L ND 1.0 11/19/15 22:51
trans-1,4-Dichloro-2-butene ug/L ND 1.0 11/19/15 22:51
Trichloroethene ug/L ND 1.0 11/19/15 22:51
Trichlorofluoromethane ug/L ND 1.0 11/19/15 22:51
Vinyl acetate ug/L ND 2.0 11/19/15 22:51
Vinyl chloride ug/L ND 1.0 11/19/15 22:51
Xylene (Total)ug/L ND 2.0 11/19/15 22:51
1,2-Dichloroethane-d4 (S)%100 70-130 11/19/15 22:51
4-Bromofluorobenzene (S)%103 70-130 11/19/15 22:51
Toluene-d8 (S)%101 70-130 11/19/15 22:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1611085LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 45.850 92 80-125
1,1,1-Trichloroethane ug/L 47.250 94 71-129
1,1,2,2-Tetrachloroethane ug/L 44.250 88 79-124
1,1,2-Trichloroethane ug/L 47.450 95 85-125
1,1-Dichloroethane ug/L 48.350 97 73-126
1,1-Dichloroethene ug/L 52.350 105 66-135
1,1-Dichloropropene ug/L 50.250 100 74-135
1,2,3-Trichloropropane ug/L 48.050 96 75-130
1,2,4-Trichlorobenzene ug/L 45.450 91 75-134
1,2-Dibromo-3-chloropropane ug/L 44.450 89 71-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 141 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1611085LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromoethane (EDB)ug/L 46.850 94 83-124
1,2-Dichlorobenzene ug/L 47.850 96 80-133
1,2-Dichloroethane ug/L 45.750 91 67-128
1,2-Dichloropropane ug/L 45.750 91 75-132
1,3-Dichlorobenzene ug/L 48.050 96 77-130
1,3-Dichloropropane ug/L 44.750 89 76-131
1,4-Dichlorobenzene ug/L 46.350 93 78-130
2,2-Dichloropropane ug/L 45.550 91 40-160
2-Butanone (MEK)ug/L 99.8100 100 61-144
2-Hexanone ug/L 92.1100 92 68-143
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 72-135
Acetone ug/L 98.8100 99 48-146
Acetonitrile ug/L 477500 95 62-150
Acrolein ug/L 244250 98 24-160
Acrylonitrile ug/L 255250 102 40-160
Allyl chloride ug/L 44.650 89 66-137
Benzene ug/L 49.550 99 80-125
Bromochloromethane ug/L 51.150 102 71-125
Bromodichloromethane ug/L 45.350 91 78-124
Bromoform ug/L 40.450 81 71-128
Bromomethane ug/L 43.250 86 40-160
Carbon disulfide ug/L 51.550 103 50-160
Carbon tetrachloride ug/L 49.850 100 69-131
Chlorobenzene ug/L 45.850 92 81-122
Chloroethane ug/L 50.150 100 39-148
Chloroform ug/L 47.850 96 73-127
Chloromethane ug/L 51.550 103 44-146
Chloroprene ug/L 52.050 104 75-145
cis-1,2-Dichloroethene ug/L 50.650 101 74-124
cis-1,3-Dichloropropene ug/L 46.550 93 72-132
Dibromochloromethane ug/L 43.150 86 78-125
Dibromomethane ug/L 50.550 101 82-120
Dichlorodifluoromethane ug/L 58.550 117 34-157
Ethyl methacrylate ug/L 43.850 88 82-121
Ethylbenzene ug/L 45.650 91 79-121
Hexachloro-1,3-butadiene ug/L 48.150 96 72-131
Isobutanol ug/L 9771000 98 34-160
m&p-Xylene ug/L 91.8100 92 81-124
Methacrylonitrile ug/L 485500 97 74-134
Methyl methacrylate ug/L 44.950 90 84-124
Methylene Chloride ug/L 51.450 103 64-133
Naphthalene ug/L 44.850 90 73-133
o-Xylene ug/L 45.150 90 79-131
Propionitrile ug/L 486500 97 73-140
Styrene ug/L 46.050 92 84-126
Tetrachloroethene ug/L 48.450 97 78-122
Tetrahydrofuran ug/L 497500 99 69-148
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 142 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1611085LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene ug/L 47.650 95 80-121
trans-1,2-Dichloroethene ug/L 50.850 102 71-127
trans-1,3-Dichloropropene ug/L 46.150 92 69-141
trans-1,4-Dichloro-2-butene ug/L 39.250 78 40-160
Trichloroethene ug/L 46.350 93 78-122
Trichlorofluoromethane ug/L 54.550 109 53-137
Vinyl acetate ug/L 95.2100 95 40-160
Vinyl chloride ug/L 56.050 112 58-137
Xylene (Total)ug/L 137150 91 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1611086MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276562003
1611087
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 104 70-130103 120ND20.9 20.7
1,1,1-Trichloroethane ug/L 20 114 70-130115 120ND22.8 23.1
1,1,2,2-Tetrachloroethane ug/L 20 99 70-13097 320ND19.9 19.3
1,1,2-Trichloroethane ug/L 20 107 70-130108 120ND21.3 21.5
1,1-Dichloroethane ug/L 20 118 70-130115 220ND23.6 23.1
1,1-Dichloroethene ug/L 20 126 70-166127 120ND25.2 25.3
1,1-Dichloropropene ug/L 20 123 70-130121 120ND24.5 24.2
1,2,3-Trichloropropane ug/L 20 105 70-130108 320ND21.1 21.7
1,2,4-Trichlorobenzene ug/L 20 96 70-13096 120ND19.1 19.3
1,2-Dibromo-3-chloropropane ug/L 20 94 70-13098 420ND18.9 19.6
1,2-Dibromoethane (EDB)ug/L 20 109 70-130106 320ND21.9 21.2
1,2-Dichlorobenzene ug/L 20 105 70-130108 320ND20.9 21.5
1,2-Dichloroethane ug/L 20 108 70-130106 220ND21.6 21.2
1,2-Dichloropropane ug/L 20 109 70-130105 420ND21.8 21.0
1,3-Dichlorobenzene ug/L 20 107 70-130109 220ND21.4 21.8
1,3-Dichloropropane ug/L 20 100 70-130100 020ND20.0 20.0
1,4-Dichlorobenzene ug/L 20 103 70-130105 220ND20.6 21.0
2,2-Dichloropropane ug/L 20 92 70-13097 620ND18.3 19.4
2-Butanone (MEK)ug/L 40 110 70-130116 540ND44.1 46.4
2-Hexanone ug/L 40 104 70-130106 240ND41.6 42.5
4-Methyl-2-pentanone (MIBK)ug/L 40 112 70-130114 240ND44.9 45.7
Acetone ug/L 40 121 70-130120 140ND48.4 48.0
Acetonitrile ug/L 200 105 70-130117 11200ND210234
Acrolein ug/L 100 95 70-13096 1100ND94.9 95.8
Acrylonitrile ug/L 100 114 70-130115 0100ND114115
Allyl chloride ug/L 20 106 70-130107 120ND21.3 21.4
Benzene ug/L 20 116 70-148117 120ND23.1 23.4
Bromochloromethane ug/L 20 120 70-130117 220ND23.9 23.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 143 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1611086MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276562003
1611087
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 20 102 70-130104 120ND20.4 20.7
Bromoform ug/L 20 86 70-13088 220ND17.3 17.6
Bromomethane ug/L 20 92 70-130100 820ND18.4 19.9
Carbon disulfide ug/L 20 120 70-130121 120ND24.0 24.2
Carbon tetrachloride ug/L 20 119 70-130118 120ND23.8 23.6
Chlorobenzene ug/L 20 105 70-146104 120ND21.1 20.9
Chloroethane ug/L 20 119 70-130114 420ND23.8 22.7
Chloroform ug/L 20 116 70-130115 120ND23.3 23.0
Chloromethane ug/L 20 121 70-130122 120ND24.3 24.5
Chloroprene ug/L 20 126 70-130124 220ND25.3 24.8
cis-1,2-Dichloroethene ug/L 20 119 70-130121 220ND23.8 24.2
cis-1,3-Dichloropropene ug/L 20 103 70-130102 020ND20.5 20.5
Dibromochloromethane ug/L 20 96 70-13098 220ND19.3 19.7
Dibromomethane ug/L 20 116 70-130115 120ND23.3 23.0
Dichlorodifluoromethane ug/L M12013870-130141 220ND27.6 28.1
Ethyl methacrylate ug/L 20 103 70-130100 320ND20.5 20.0
Ethylbenzene ug/L 20 107 70-130103 420ND21.5 20.7
Hexachloro-1,3-butadiene ug/L 20 103 70-130107 420ND20.6 21.4
Isobutanol ug/L 400 111 70-130117 5400ND446467
m&p-Xylene ug/L 40 104 70-130104 040ND41.7 41.7
Methacrylonitrile ug/L 200 112 70-130112 0200ND224224
Methyl methacrylate ug/L 20 100 70-13099 120ND20.0 19.9
Methylene Chloride ug/L 20 120 70-130123 220ND24.1 24.6
Naphthalene ug/L 20 94 70-13098 420ND18.9 19.6
o-Xylene ug/L 20 105 70-130104 120ND21.1 20.8
Propionitrile ug/L 200 109 70-130118 8200ND217235
Styrene ug/L 20 104 70-130101 320ND20.8 20.3
Tetrachloroethene ug/L 20 115 70-130112 320ND23.0 22.4
Tetrahydrofuran ug/L 200 107 70-130115 7200ND215229
Toluene ug/L 20 111 70-155110 120ND22.1 21.9
trans-1,2-Dichloroethene ug/L 20 125 70-130124 120ND25.1 24.9
trans-1,3-Dichloropropene ug/L 20 101 70-130102 120ND20.2 20.3
trans-1,4-Dichloro-2-butene ug/L 20 78 70-13080 320ND15.6 16.1
Trichloroethene ug/L 20 109 69-151112 220ND21.8 22.3
Trichlorofluoromethane ug/L M12013370-130131 220ND26.7 26.2
Vinyl acetate ug/L 40 82 70-13084 240ND32.9 33.7
Vinyl chloride ug/L M12013570-130134 020ND27.0 26.9
1,2-Dichloroethane-d4 (S)%99 70-130103
4-Bromofluorobenzene (S)%106 70-130104
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 144 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34364
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92276295010, 92276295011, 92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1611724
Associated Lab Samples:92276295010, 92276295011, 92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/20/15 11:55
1,1,1-Trichloroethane ug/L ND 1.0 11/20/15 11:55
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/20/15 11:55
1,1,2-Trichloroethane ug/L ND 1.0 11/20/15 11:55
1,1-Dichloroethane ug/L ND 1.0 11/20/15 11:55
1,1-Dichloroethene ug/L ND 1.0 11/20/15 11:55
1,1-Dichloropropene ug/L ND 1.0 11/20/15 11:55
1,2,3-Trichloropropane ug/L ND 1.0 11/20/15 11:55
1,2,4-Trichlorobenzene ug/L ND 1.0 11/20/15 11:55
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/20/15 11:55
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/20/15 11:55
1,2-Dichlorobenzene ug/L ND 1.0 11/20/15 11:55
1,2-Dichloroethane ug/L ND 1.0 11/20/15 11:55
1,2-Dichloropropane ug/L ND 1.0 11/20/15 11:55
1,3-Dichlorobenzene ug/L ND 1.0 11/20/15 11:55
1,3-Dichloropropane ug/L ND 1.0 11/20/15 11:55
1,4-Dichlorobenzene ug/L ND 1.0 11/20/15 11:55
2,2-Dichloropropane ug/L ND 1.0 11/20/15 11:55
2-Butanone (MEK)ug/L ND 5.0 11/20/15 11:55
2-Hexanone ug/L ND 5.0 11/20/15 11:55
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/20/15 11:55
Acetone ug/L ND 25.0 11/20/15 11:55
Acetonitrile ug/L ND 50.0 11/20/15 11:55
Acrolein ug/L ND 10.0 11/20/15 11:55
Acrylonitrile ug/L ND 10.0 11/20/15 11:55
Allyl chloride ug/L ND 2.0 11/20/15 11:55
Benzene ug/L ND 1.0 11/20/15 11:55
Bromochloromethane ug/L ND 1.0 11/20/15 11:55
Bromodichloromethane ug/L ND 1.0 11/20/15 11:55
Bromoform ug/L ND 1.0 11/20/15 11:55
Bromomethane ug/L ND 2.0 11/20/15 11:55
Carbon disulfide ug/L ND 2.0 11/20/15 11:55
Carbon tetrachloride ug/L ND 1.0 11/20/15 11:55
Chlorobenzene ug/L ND 1.0 11/20/15 11:55
Chloroethane ug/L ND 1.0 11/20/15 11:55
Chloroform ug/L ND 1.0 11/20/15 11:55
Chloromethane ug/L ND 1.0 11/20/15 11:55
Chloroprene ug/L ND 5.0 11/20/15 11:55
cis-1,2-Dichloroethene ug/L ND 1.0 11/20/15 11:55
cis-1,3-Dichloropropene ug/L ND 1.0 11/20/15 11:55
Dibromochloromethane ug/L ND 1.0 11/20/15 11:55
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 145 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1611724
Associated Lab Samples:92276295010, 92276295011, 92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Matrix:Water
Analyzed
Dibromomethane ug/L ND 1.0 11/20/15 11:55
Dichlorodifluoromethane ug/L ND 1.0 11/20/15 11:55
Ethyl methacrylate ug/L ND 1.0 11/20/15 11:55
Ethylbenzene ug/L ND 1.0 11/20/15 11:55
Hexachloro-1,3-butadiene ug/L ND 1.0 11/20/15 11:55
Isobutanol ug/L ND 100 11/20/15 11:55
m&p-Xylene ug/L ND 2.0 11/20/15 11:55
Methacrylonitrile ug/L ND 10.0 11/20/15 11:55
Methyl methacrylate ug/L ND 2.0 11/20/15 11:55
Methylene Chloride ug/L ND 1.0 11/20/15 11:55
Naphthalene ug/L ND 1.0 11/20/15 11:55
o-Xylene ug/L ND 1.0 11/20/15 11:55
Propionitrile ug/L ND 20.0 11/20/15 11:55
Styrene ug/L ND 1.0 11/20/15 11:55
Tetrachloroethene ug/L ND 1.0 11/20/15 11:55
Tetrahydrofuran ug/L ND 10.0 11/20/15 11:55
Toluene ug/L ND 1.0 11/20/15 11:55
trans-1,2-Dichloroethene ug/L ND 1.0 11/20/15 11:55
trans-1,3-Dichloropropene ug/L ND 1.0 11/20/15 11:55
trans-1,4-Dichloro-2-butene ug/L ND 1.0 11/20/15 11:55
Trichloroethene ug/L ND 1.0 11/20/15 11:55
Trichlorofluoromethane ug/L ND 1.0 11/20/15 11:55
Vinyl acetate ug/L ND 2.0 11/20/15 11:55
Vinyl chloride ug/L ND 1.0 11/20/15 11:55
Xylene (Total)ug/L ND 2.0 11/20/15 11:55
1,2-Dichloroethane-d4 (S)%100 70-130 11/20/15 11:55
4-Bromofluorobenzene (S)%103 70-130 11/20/15 11:55
Toluene-d8 (S)%100 70-130 11/20/15 11:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1611725LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.350 95 80-125
1,1,1-Trichloroethane ug/L 48.650 97 71-129
1,1,2,2-Tetrachloroethane ug/L 42.750 85 79-124
1,1,2-Trichloroethane ug/L 49.050 98 85-125
1,1-Dichloroethane ug/L 48.250 96 73-126
1,1-Dichloroethene ug/L 52.950 106 66-135
1,1-Dichloropropene ug/L 52.550 105 74-135
1,2,3-Trichloropropane ug/L 45.450 91 75-130
1,2,4-Trichlorobenzene ug/L 47.450 95 75-134
1,2-Dibromo-3-chloropropane ug/L 44.750 89 71-133
1,2-Dibromoethane (EDB)ug/L 45.650 91 83-124
1,2-Dichlorobenzene ug/L 47.950 96 80-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 146 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1611725LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 48.450 97 67-128
1,2-Dichloropropane ug/L 46.850 94 75-132
1,3-Dichlorobenzene ug/L 48.850 98 77-130
1,3-Dichloropropane ug/L 44.150 88 76-131
1,4-Dichlorobenzene ug/L 48.750 97 78-130
2,2-Dichloropropane ug/L 49.350 99 40-160
2-Butanone (MEK)ug/L 99.5100 100 61-144
2-Hexanone ug/L 88.8100 89 68-143
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 72-135
Acetone ug/L 99.0100 99 48-146
Acetonitrile ug/L 474500 95 62-150
Acrolein ug/L 253250 101 24-160
Acrylonitrile ug/L 246250 98 40-160
Allyl chloride ug/L 47.050 94 66-137
Benzene ug/L 49.550 99 80-125
Bromochloromethane ug/L 52.050 104 71-125
Bromodichloromethane ug/L 45.950 92 78-124
Bromoform ug/L 40.150 80 71-128
Bromomethane ug/L 47.850 96 40-160
Carbon disulfide ug/L 53.150 106 50-160
Carbon tetrachloride ug/L 50.750 101 69-131
Chlorobenzene ug/L 46.450 93 81-122
Chloroethane ug/L 52.950 106 39-148
Chloroform ug/L 49.950 100 73-127
Chloromethane ug/L 50.350 101 44-146
Chloroprene ug/L 54.150 108 75-145
cis-1,2-Dichloroethene ug/L 51.650 103 74-124
cis-1,3-Dichloropropene ug/L 47.650 95 72-132
Dibromochloromethane ug/L 44.650 89 78-125
Dibromomethane ug/L 52.850 106 82-120
Dichlorodifluoromethane ug/L 58.650 117 34-157
Ethyl methacrylate ug/L 45.250 90 82-121
Ethylbenzene ug/L 45.550 91 79-121
Hexachloro-1,3-butadiene ug/L 46.650 93 72-131
Isobutanol ug/L 9921000 99 34-160
m&p-Xylene ug/L 90.5100 91 81-124
Methacrylonitrile ug/L 488500 98 74-134
Methyl methacrylate ug/L 45.350 91 84-124
Methylene Chloride ug/L 52.250 104 64-133
Naphthalene ug/L 45.050 90 73-133
o-Xylene ug/L 44.750 89 79-131
Propionitrile ug/L 479500 96 73-140
Styrene ug/L 45.550 91 84-126
Tetrachloroethene ug/L 47.750 95 78-122
Tetrahydrofuran ug/L 490500 98 69-148
Toluene ug/L 48.750 97 80-121
trans-1,2-Dichloroethene ug/L 53.550 107 71-127
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Huntersville, NC 28078
[phone]
Page 147 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1611725LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/L 47.750 95 69-141
trans-1,4-Dichloro-2-butene ug/L 37.950 76 40-160
Trichloroethene ug/L 48.950 98 78-122
Trichlorofluoromethane ug/L 52.850 106 53-137
Vinyl acetate ug/L 98.7100 99 40-160
Vinyl chloride ug/L 58.750 117 58-137
Xylene (Total)ug/L 135150 90 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1611726MATRIX SPIKE SAMPLE:
MSSpike
Result
92276295012
1,1,1,2-Tetrachloroethane ug/L 20.820 104 70-130ND
1,1,1-Trichloroethane ug/L 23.320 116 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.720 98 70-130ND
1,1,2-Trichloroethane ug/L 22.120 110 70-130ND
1,1-Dichloroethane ug/L 24.120 120 70-130ND
1,1-Dichloroethene ug/L 25.520 127 70-166ND
1,1-Dichloropropene ug/L 25.520 128 70-130ND
1,2,3-Trichloropropane ug/L 21.320 107 70-130ND
1,2,4-Trichlorobenzene ug/L 20.520 102 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.420 97 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.220 106 70-130ND
1,2-Dichlorobenzene ug/L 22.220 111 70-130ND
1,2-Dichloroethane ug/L 21.720 108 70-130ND
1,2-Dichloropropane ug/L 21.620 108 70-130ND
1,3-Dichlorobenzene ug/L 21.820 109 70-130ND
1,3-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 21.920 108 70-1300.38J
2,2-Dichloropropane ug/L 20.420 102 70-130ND
2-Butanone (MEK)ug/L 45.240 113 70-130ND
2-Hexanone ug/L 43.040 108 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 46.040 115 70-130ND
Acetone ug/L 48.340 111 70-130ND
Acetonitrile ug/L 223200 112 70-130ND
Acrolein ug/L 100100 100 70-130ND
Acrylonitrile ug/L 112100 112 70-130ND
Allyl chloride ug/L 21.620 108 70-130ND
Benzene ug/L 25.420 120 70-1481.5
Bromochloromethane ug/L 24.520 122 70-130ND
Bromodichloromethane ug/L 20.720 103 70-130ND
Bromoform ug/L 16.520 82 70-130ND
Bromomethane ug/L 18.920 94 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
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Page 148 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1611726MATRIX SPIKE SAMPLE:
MSSpike
Result
92276295012
Carbon disulfide ug/L 24.420 122 70-130ND
Carbon tetrachloride ug/L 24.720 123 70-130ND
Chlorobenzene ug/L 21.520 107 70-146ND
Chloroethane ug/L 25.720 129 70-130ND
Chloroform ug/L 23.520 118 70-130ND
Chloromethane ug/L 24.620 122 70-1300.25J
Chloroprene ug/L 26.4 M12013270-130ND
cis-1,2-Dichloroethene ug/L 25.220 124 70-1300.26J
cis-1,3-Dichloropropene ug/L 21.020 105 70-130ND
Dibromochloromethane ug/L 19.120 96 70-130ND
Dibromomethane ug/L 22.720 113 70-130ND
Dichlorodifluoromethane ug/L 28.8 M12014370-1300.26J
Ethyl methacrylate ug/L 19.920 100 70-130ND
Ethylbenzene ug/L 21.820 109 70-130ND
Hexachloro-1,3-butadiene ug/L 21.920 110 70-130ND
Isobutanol ug/L 423400 106 70-130ND
m&p-Xylene ug/L 43.340 108 70-130ND
Methacrylonitrile ug/L 219200 109 70-130ND
Methyl methacrylate ug/L 20.620 103 70-130ND
Methylene Chloride ug/L 25.620 122 70-1301.3
Naphthalene ug/L 20.220 101 70-130ND
o-Xylene ug/L 21.520 108 70-130ND
Propionitrile ug/L 214200 107 70-130ND
Styrene ug/L 22.020 110 70-130ND
Tetrachloroethene ug/L 24.420 117 70-1300.95J
Tetrahydrofuran ug/L 259200 111 70-13035.8
Toluene ug/L 22.920 113 70-1550.27J
trans-1,2-Dichloroethene ug/L 25.220 126 70-130ND
trans-1,3-Dichloropropene ug/L 20.720 104 70-130ND
trans-1,4-Dichloro-2-butene ug/L 13.4 M1206770-130ND
Trichloroethene ug/L 23.820 116 69-1510.66J
Trichlorofluoromethane ug/L 27.9 M12013570-1301.0
Vinyl acetate ug/L 37.340 93 70-130ND
Vinyl chloride ug/L 28.5 M12013970-1300.75J
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92276295013
1611727SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 149 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276295013
1611727SAMPLE DUPLICATE:
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acetonitrile ug/L NDND
Acrolein ug/L NDND
Acrylonitrile ug/L NDND
Allyl chloride ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
Chloroprene ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethyl methacrylate ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
Isobutanol ug/L NDND
m&p-Xylene ug/L NDND
Methacrylonitrile ug/L NDND
Methyl methacrylate ug/L NDND
Methylene Chloride ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 150 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276295013
1611727SAMPLE DUPLICATE:
Naphthalene ug/L NDND
o-Xylene ug/L NDND
Propionitrile ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%100 2102
4-Bromofluorobenzene (S)%107 3104
Toluene-d8 (S)%101 0101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 151 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34379
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92276295017, 92276295018, 92276295019, 92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1612653
Associated Lab Samples:92276295017, 92276295018, 92276295019, 92276295020
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/21/15 11:45
1,1,1-Trichloroethane ug/L ND 1.0 11/21/15 11:45
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/21/15 11:45
1,1,2-Trichloroethane ug/L ND 1.0 11/21/15 11:45
1,1-Dichloroethane ug/L ND 1.0 11/21/15 11:45
1,1-Dichloroethene ug/L ND 1.0 11/21/15 11:45
1,1-Dichloropropene ug/L ND 1.0 11/21/15 11:45
1,2,3-Trichloropropane ug/L ND 1.0 11/21/15 11:45
1,2,4-Trichlorobenzene ug/L ND 1.0 11/21/15 11:45
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/21/15 11:45
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/21/15 11:45
1,2-Dichlorobenzene ug/L ND 1.0 11/21/15 11:45
1,2-Dichloroethane ug/L ND 1.0 11/21/15 11:45
1,2-Dichloropropane ug/L ND 1.0 11/21/15 11:45
1,3-Dichlorobenzene ug/L ND 1.0 11/21/15 11:45
1,3-Dichloropropane ug/L ND 1.0 11/21/15 11:45
1,4-Dichlorobenzene ug/L ND 1.0 11/21/15 11:45
2,2-Dichloropropane ug/L ND 1.0 11/21/15 11:45
2-Butanone (MEK)ug/L ND 5.0 11/21/15 11:45
2-Hexanone ug/L ND 5.0 11/21/15 11:45
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/21/15 11:45
Acetone ug/L ND 25.0 11/21/15 11:45
Acetonitrile ug/L ND 50.0 11/21/15 11:45
Acrolein ug/L ND 10.0 11/21/15 11:45
Acrylonitrile ug/L ND 10.0 11/21/15 11:45
Allyl chloride ug/L ND 2.0 11/21/15 11:45
Benzene ug/L ND 1.0 11/21/15 11:45
Bromochloromethane ug/L ND 1.0 11/21/15 11:45
Bromodichloromethane ug/L ND 1.0 11/21/15 11:45
Bromoform ug/L ND 1.0 11/21/15 11:45
Bromomethane ug/L ND 2.0 11/21/15 11:45
Carbon disulfide ug/L ND 2.0 11/21/15 11:45
Carbon tetrachloride ug/L ND 1.0 11/21/15 11:45
Chlorobenzene ug/L ND 1.0 11/21/15 11:45
Chloroethane ug/L ND 1.0 11/21/15 11:45
Chloroform ug/L ND 1.0 11/21/15 11:45
Chloromethane ug/L ND 1.0 11/21/15 11:45
Chloroprene ug/L ND 5.0 11/21/15 11:45
cis-1,2-Dichloroethene ug/L ND 1.0 11/21/15 11:45
cis-1,3-Dichloropropene ug/L ND 1.0 11/21/15 11:45
Dibromochloromethane ug/L ND 1.0 11/21/15 11:45
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 152 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1612653
Associated Lab Samples:92276295017, 92276295018, 92276295019, 92276295020
Matrix:Water
Analyzed
Dibromomethane ug/L ND 1.0 11/21/15 11:45
Dichlorodifluoromethane ug/L ND 1.0 11/21/15 11:45
Ethyl methacrylate ug/L ND 1.0 11/21/15 11:45
Ethylbenzene ug/L ND 1.0 11/21/15 11:45
Hexachloro-1,3-butadiene ug/L ND 1.0 11/21/15 11:45
Isobutanol ug/L ND 100 11/21/15 11:45
m&p-Xylene ug/L ND 2.0 11/21/15 11:45
Methacrylonitrile ug/L ND 10.0 11/21/15 11:45
Methyl methacrylate ug/L ND 2.0 11/21/15 11:45
Methylene Chloride ug/L ND 1.0 11/21/15 11:45
Naphthalene ug/L ND 1.0 11/21/15 11:45
o-Xylene ug/L ND 1.0 11/21/15 11:45
Propionitrile ug/L ND 20.0 11/21/15 11:45
Styrene ug/L ND 1.0 11/21/15 11:45
Tetrachloroethene ug/L ND 1.0 11/21/15 11:45
Tetrahydrofuran ug/L ND 10.0 11/21/15 11:45
Toluene ug/L ND 1.0 11/21/15 11:45
trans-1,2-Dichloroethene ug/L ND 1.0 11/21/15 11:45
trans-1,3-Dichloropropene ug/L ND 1.0 11/21/15 11:45
trans-1,4-Dichloro-2-butene ug/L ND 1.0 11/21/15 11:45
Trichloroethene ug/L ND 1.0 11/21/15 11:45
Trichlorofluoromethane ug/L ND 1.0 11/21/15 11:45
Vinyl acetate ug/L ND 2.0 11/21/15 11:45
Vinyl chloride ug/L ND 1.0 11/21/15 11:45
Xylene (Total)ug/L ND 2.0 11/21/15 11:45
1,2-Dichloroethane-d4 (S)%100 70-130 11/21/15 11:45
4-Bromofluorobenzene (S)%105 70-130 11/21/15 11:45
Toluene-d8 (S)%99 70-130 11/21/15 11:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612654LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.150 92 80-125
1,1,1-Trichloroethane ug/L 49.050 98 71-129
1,1,2,2-Tetrachloroethane ug/L 43.250 86 79-124
1,1,2-Trichloroethane ug/L 49.650 99 85-125
1,1-Dichloroethane ug/L 49.050 98 73-126
1,1-Dichloroethene ug/L 54.250 108 66-135
1,1-Dichloropropene ug/L 52.450 105 74-135
1,2,3-Trichloropropane ug/L 47.950 96 75-130
1,2,4-Trichlorobenzene ug/L 46.350 93 75-134
1,2-Dibromo-3-chloropropane ug/L 41.850 84 71-133
1,2-Dibromoethane (EDB)ug/L 45.750 91 83-124
1,2-Dichlorobenzene ug/L 46.750 93 80-133
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 153 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612654LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 47.250 94 67-128
1,2-Dichloropropane ug/L 46.850 94 75-132
1,3-Dichlorobenzene ug/L 46.750 93 77-130
1,3-Dichloropropane ug/L 44.550 89 76-131
1,4-Dichlorobenzene ug/L 46.850 94 78-130
2,2-Dichloropropane ug/L 49.850 100 40-160
2-Butanone (MEK)ug/L 105100 105 61-144
2-Hexanone ug/L 90.2100 90 68-143
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 72-135
Acetone ug/L 107100 107 48-146
Acetonitrile ug/L 529500 106 62-150
Acrolein ug/L 246250 99 24-160
Acrylonitrile ug/L 254250 102 40-160
Allyl chloride ug/L 47.050 94 66-137
Benzene ug/L 50.150 100 80-125
Bromochloromethane ug/L 51.350 103 71-125
Bromodichloromethane ug/L 45.750 91 78-124
Bromoform ug/L 39.950 80 71-128
Bromomethane ug/L 49.350 99 40-160
Carbon disulfide ug/L 53.350 107 50-160
Carbon tetrachloride ug/L 51.550 103 69-131
Chlorobenzene ug/L 45.550 91 81-122
Chloroethane ug/L 53.650 107 39-148
Chloroform ug/L 50.850 102 73-127
Chloromethane ug/L 51.750 103 44-146
Chloroprene ug/L 53.950 108 75-145
cis-1,2-Dichloroethene ug/L 51.250 102 74-124
cis-1,3-Dichloropropene ug/L 47.850 96 72-132
Dibromochloromethane ug/L 44.450 89 78-125
Dibromomethane ug/L 52.550 105 82-120
Dichlorodifluoromethane ug/L 58.650 117 34-157
Ethyl methacrylate ug/L 44.450 89 82-121
Ethylbenzene ug/L 45.150 90 79-121
Hexachloro-1,3-butadiene ug/L 46.350 93 72-131
Isobutanol ug/L 10501000 105 34-160
m&p-Xylene ug/L 91.2100 91 81-124
Methacrylonitrile ug/L 498500 100 74-134
Methyl methacrylate ug/L 46.950 94 84-124
Methylene Chloride ug/L 51.550 103 64-133
Naphthalene ug/L 42.850 86 73-133
o-Xylene ug/L 43.950 88 79-131
Propionitrile ug/L 504500 101 73-140
Styrene ug/L 46.550 93 84-126
Tetrachloroethene ug/L 48.450 97 78-122
Tetrahydrofuran ug/L 506500 101 69-148
Toluene ug/L 48.050 96 80-121
trans-1,2-Dichloroethene ug/L 54.050 108 71-127
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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[phone]
Page 154 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612654LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/L 46.250 92 69-141
trans-1,4-Dichloro-2-butene ug/L 36.950 74 40-160
Trichloroethene ug/L 49.750 99 78-122
Trichlorofluoromethane ug/L 53.150 106 53-137
Vinyl acetate ug/L 97.7100 98 40-160
Vinyl chloride ug/L 60.150 120 58-137
Xylene (Total)ug/L 135150 90 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1612655MATRIX SPIKE SAMPLE:
MSSpike
Result
92277056001
1,1,1,2-Tetrachloroethane ug/L 19.420 97 70-130ND
1,1,1-Trichloroethane ug/L 22.520 113 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.120 91 70-130ND
1,1,2-Trichloroethane ug/L 21.120 106 70-130ND
1,1-Dichloroethane ug/L 43.520 114 70-13020.7
1,1-Dichloroethene ug/L 25.120 124 70-166ND
1,1-Dichloropropene ug/L 24.220 121 70-130ND
1,2,3-Trichloropropane ug/L 19.420 97 70-130ND
1,2,4-Trichlorobenzene ug/L 18.520 93 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.720 93 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.320 97 70-130ND
1,2-Dichlorobenzene ug/L 20.220 100 70-130ND
1,2-Dichloroethane ug/L 22.420 108 70-1300.86J
1,2-Dichloropropane ug/L 24.520 101 70-1304.3
1,3-Dichlorobenzene ug/L 19.820 99 70-130ND
1,3-Dichloropropane ug/L 19.320 97 70-130ND
1,4-Dichlorobenzene ug/L 25.520 104 70-1304.8
2,2-Dichloropropane ug/L 19.620 98 70-130ND
2-Butanone (MEK)ug/L 45.040 113 70-130ND
2-Hexanone ug/L 38.740 97 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 44.440 111 70-130ND
Acetone ug/L 43.140 108 70-130ND
Acetonitrile ug/L 208200 104 70-130ND
Acrolein ug/L 94.5100 95 70-130ND
Acrylonitrile ug/L 109100 109 70-130ND
Allyl chloride ug/L 21.620 108 70-130ND
Benzene ug/L 28.920 114 70-1486.0
Bromochloromethane ug/L 22.920 115 70-130ND
Bromodichloromethane ug/L 20.120 101 70-130ND
Bromoform ug/L 16.320 82 70-130ND
Bromomethane ug/L 19.520 97 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 155 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1612655MATRIX SPIKE SAMPLE:
MSSpike
Result
92277056001
Carbon disulfide ug/L 24.020 120 70-130ND
Carbon tetrachloride ug/L 23.420 117 70-130ND
Chlorobenzene ug/L 20.220 99 70-1460.31J
Chloroethane ug/L 23.820 119 70-130ND
Chloroform ug/L 23.020 115 70-130ND
Chloromethane ug/L 22.520 113 70-130ND
Chloroprene ug/L 24.920 125 70-130ND
cis-1,2-Dichloroethene ug/L 68.120 119 70-13044.4
cis-1,3-Dichloropropene ug/L 20.320 101 70-130ND
Dibromochloromethane ug/L 18.820 94 70-130ND
Dibromomethane ug/L 22.420 112 70-130ND
Dichlorodifluoromethane ug/L 28.3 M12013670-1301.1J
Ethyl methacrylate ug/L 18.520 93 70-130ND
Ethylbenzene ug/L 19.920 100 70-130ND
Hexachloro-1,3-butadiene ug/L 19.020 95 70-130ND
Isobutanol ug/L 425400 106 70-130ND
m&p-Xylene ug/L 39.340 98 70-130ND
Methacrylonitrile ug/L 217200 108 70-130ND
Methyl methacrylate ug/L 20.120 100 70-130ND
Methylene Chloride ug/L 24.320 122 70-130ND
Naphthalene ug/L 18.220 90 70-1300.31J
o-Xylene ug/L 19.620 98 70-130ND
Propionitrile ug/L 211200 105 70-130ND
Styrene ug/L 19.820 99 70-130ND
Tetrachloroethene ug/L 21.920 105 70-1300.90J
Tetrahydrofuran ug/L 224200 109 70-1304.7J
Toluene ug/L 21.820 109 70-155ND
trans-1,2-Dichloroethene ug/L 26.020 123 70-1301.5J
trans-1,3-Dichloropropene ug/L 20.020 100 70-130ND
trans-1,4-Dichloro-2-butene ug/L 13.1 M1206570-130ND
Trichloroethene ug/L 27.120 112 69-1514.7
Trichlorofluoromethane ug/L 25.320 124 70-1300.41J
Vinyl acetate ug/L 37.440 93 70-130ND
Vinyl chloride ug/L 35.0 M12013770-1307.7
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92277056002
1612656SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 156 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92277056002
1612656SAMPLE DUPLICATE:
1,1-Dichloroethane ug/L 0.85J0.82J
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L ND0.40J
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L 1.2 111.4
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acetonitrile ug/L NDND
Acrolein ug/L NDND
Acrylonitrile ug/L NDND
Allyl chloride ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L 0.81J0.81J
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
Chloroprene ug/L NDND
cis-1,2-Dichloroethene ug/L 5.3 45.6
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethyl methacrylate ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
Isobutanol ug/L NDND
m&p-Xylene ug/L NDND
Methacrylonitrile ug/L NDND
Methyl methacrylate ug/L NDND
Methylene Chloride ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 157 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92277056002
1612656SAMPLE DUPLICATE:
Naphthalene ug/L NDND
o-Xylene ug/L NDND
Propionitrile ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L 1.9 22.0
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%101 1102
4-Bromofluorobenzene (S)%105 0105
Toluene-d8 (S)%100 1101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 158 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39187
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92276295005, 92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1610834
Associated Lab Samples:92276295005, 92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 11/20/15 23:31
4,4'-DDE ug/L ND 0.050 11/20/15 23:31
4,4'-DDT ug/L ND 0.050 11/20/15 23:31
Aldrin ug/L ND 0.050 11/20/15 23:31
alpha-BHC ug/L ND 0.050 11/20/15 23:31
beta-BHC ug/L ND 0.050 11/20/15 23:31
Chlordane (Technical)ug/L ND 0.20 11/20/15 23:31
delta-BHC ug/L ND 0.050 11/20/15 23:31
Dieldrin ug/L ND 0.050 11/20/15 23:31
Endosulfan I ug/L ND 0.050 11/20/15 23:31
Endosulfan II ug/L ND 0.050 11/20/15 23:31
Endosulfan sulfate ug/L ND 0.050 11/20/15 23:31
Endrin ug/L ND 0.050 11/20/15 23:31
Endrin aldehyde ug/L ND 0.050 11/20/15 23:31
gamma-BHC (Lindane)ug/L ND 0.050 11/20/15 23:31
Heptachlor ug/L ND 0.050 11/20/15 23:31
Heptachlor epoxide ug/L ND 0.050 11/20/15 23:31
Methoxychlor ug/L ND 0.15 11/20/15 23:31
Toxaphene ug/L ND 0.20 11/20/15 23:31
Decachlorobiphenyl (S)%61 20-130 11/20/15 23:31
Tetrachloro-m-xylene (S)%81 20-130 11/20/15 23:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1610835LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1610836
4,4'-DDD ug/L 0.28.25 111 20-1501110.27 0 30
4,4'-DDE ug/L 0.26.25 106 20-1501050.26 0 30
4,4'-DDT ug/L 0.30.25 121 20-1501210.30 1 30
Aldrin ug/L 0.21.25 83 20-150830.21 0 30
alpha-BHC ug/L 0.25.25 103 20-1501020.25 1 30
beta-BHC ug/L 0.27.25 108 20-1501080.27 1 30
delta-BHC ug/L 0.30.25 122 20-1501210.30 1 30
Dieldrin ug/L 0.28.25 112 20-1501120.28 0 30
Endosulfan I ug/L 0.27.25 109 20-1501090.27 0 30
Endosulfan II ug/L 0.28.25 112 20-1501130.28 0 30
Endosulfan sulfate ug/L 0.29.25 116 20-1501160.29 0 30
Endrin ug/L 0.30.25 121 20-1501200.30 0 30
Endrin aldehyde ug/L 0.25.25 102 20-1501020.25 1 30
gamma-BHC (Lindane)ug/L 0.26.25 107 20-1501050.26 1 30
Heptachlor ug/L 0.24.25 97 20-150960.24 1 30
REPORT OF LABORATORY ANALYSIS
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Page 159 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1610835LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1610836
Heptachlor epoxide ug/L 0.27.25 109 20-1501080.27 0 30
Methoxychlor ug/L 0.89.74 120 20-1501190.89 0 30
Decachlorobiphenyl (S)%94 20-13094
Tetrachloro-m-xylene (S)%106 20-130105
REPORT OF LABORATORY ANALYSIS
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Page 160 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39285
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1613806
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 11/25/15 13:04
4,4'-DDE ug/L ND 0.050 11/25/15 13:04
4,4'-DDT ug/L ND 0.050 11/25/15 13:04
Aldrin ug/L ND 0.050 11/25/15 13:04
alpha-BHC ug/L ND 0.050 11/25/15 13:04
beta-BHC ug/L ND 0.050 11/25/15 13:04
Chlordane (Technical)ug/L ND 0.20 11/25/15 13:04
delta-BHC ug/L ND 0.050 11/25/15 13:04
Dieldrin ug/L ND 0.050 11/25/15 13:04
Endosulfan I ug/L ND 0.050 11/25/15 13:04
Endosulfan II ug/L ND 0.050 11/25/15 13:04
Endosulfan sulfate ug/L ND 0.050 11/25/15 13:04
Endrin ug/L ND 0.050 11/25/15 13:04
Endrin aldehyde ug/L ND 0.050 11/25/15 13:04
gamma-BHC (Lindane)ug/L ND 0.050 11/25/15 13:04
Heptachlor ug/L ND 0.050 11/25/15 13:04
Heptachlor epoxide ug/L ND 0.050 11/25/15 13:04
Methoxychlor ug/L ND 0.15 11/25/15 13:04
Toxaphene ug/L ND 0.20 11/25/15 13:04
Decachlorobiphenyl (S)%88 20-130 11/25/15 13:04
Tetrachloro-m-xylene (S)%120 20-130 11/25/15 13:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613807LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1613808
4,4'-DDD ug/L 0.26.25 106 20-1501170.29 10 30
4,4'-DDE ug/L 0.23.25 93 20-1501030.25 10 30
4,4'-DDT ug/L 0.27.25 109 20-1501250.31 14 30
Aldrin ug/L 0.22.25 91 20-1501000.25 10 30
alpha-BHC ug/L 0.25.25 103 20-1501240.31 18 30
beta-BHC ug/L 0.27.25 107 20-1501210.30 12 30
delta-BHC ug/L 0.27.25 111 20-1501320.33 17 30
Dieldrin ug/L 0.27.25 109 20-1501220.30 11 30
Endosulfan I ug/L 0.24.25 97 20-150930.23 4 30
Endosulfan II ug/L 0.26.25 106 20-1501190.29 11 30
Endosulfan sulfate ug/L 0.25.25 103 20-1501180.29 14 30
Endrin ug/L 0.27.25 111 20-1501290.32 15 30
Endrin aldehyde ug/L 0.21.25 86 20-150990.24 13 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 161 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613807LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1613808
gamma-BHC (Lindane)ug/L 0.26.25 104 20-1501160.29 10 30
Heptachlor ug/L 0.24.25 95 20-1501120.28 16 30
Heptachlor epoxide ug/L 0.26.25 107 20-1501190.30 11 30
Methoxychlor ug/L 0.81.74 109 20-1501190.89 9 30
Decachlorobiphenyl (S)%89 20-13094
Tetrachloro-m-xylene (S)%113 20-130129
REPORT OF LABORATORY ANALYSIS
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Page 162 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39186
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92276295005, 92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1610827
Associated Lab Samples:92276295005, 92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
PCB-1016 (Aroclor 1016)ug/L ND 0.50 11/21/15 14:11
PCB-1221 (Aroclor 1221)ug/L ND 0.50 11/21/15 14:11
PCB-1232 (Aroclor 1232)ug/L ND 0.50 11/21/15 14:11
PCB-1242 (Aroclor 1242)ug/L ND 0.50 11/21/15 14:11
PCB-1248 (Aroclor 1248)ug/L ND 0.50 11/21/15 14:11
PCB-1254 (Aroclor 1254)ug/L ND 0.50 11/21/15 14:11
PCB-1260 (Aroclor 1260)ug/L ND 0.50 11/21/15 14:11
Decachlorobiphenyl (S)%63 10-132 11/21/15 14:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1610828LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1610829
PCB-1016 (Aroclor 1016)ug/L 3.45 69 50-150603.0 13 30
PCB-1260 (Aroclor 1260)ug/L 4.25 84 50-150723.6 16 30
Decachlorobiphenyl (S)%68 10-13253
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 163 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39292
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1614010
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Matrix:Water
Analyzed
PCB-1016 (Aroclor 1016)ug/L ND 0.50 11/25/15 19:25
PCB-1221 (Aroclor 1221)ug/L ND 0.50 11/25/15 19:25
PCB-1232 (Aroclor 1232)ug/L ND 0.50 11/25/15 19:25
PCB-1242 (Aroclor 1242)ug/L ND 0.50 11/25/15 19:25
PCB-1248 (Aroclor 1248)ug/L ND 0.50 11/25/15 19:25
PCB-1254 (Aroclor 1254)ug/L ND 0.50 11/25/15 19:25
PCB-1260 (Aroclor 1260)ug/L ND 0.50 11/25/15 19:25
Decachlorobiphenyl (S)%87 10-132 11/25/15 19:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1614011LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1614012
PCB-1016 (Aroclor 1016)ug/L 4.65 91 50-150854.2 7 30
PCB-1260 (Aroclor 1260)ug/L 4.55 90 50-150964.8 6 30
Decachlorobiphenyl (S)%81 10-13283
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Huntersville, NC 28078
[phone]
Page 164 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/25401
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92276295007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1400190
Associated Lab Samples:92276295007
Matrix:Water
Analyzed
2,4,5-T ug/L ND 0.19 11/23/15 20:51
2,4,5-TP (Silvex)ug/L ND 0.19 11/23/15 20:51
2,4-D ug/L ND 0.94 11/23/15 20:51
Dinoseb ug/L ND 0.19 11/23/15 20:51
2,4-DCAA (S)%81 36-130 11/23/15 20:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1400191LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1401006
2,4,5-T ug/L 0.981.2 81 40-130770.92 6 40
2,4,5-TP (Silvex)ug/L 0.981.2 82 58-130780.94 4 40
2,4-D ug/L 4.46 74 42-134714.3 5 40
Dinoseb ug/L 0.961.2 80 10-157720.86 10 40
2,4-DCAA (S)%77 36-13074 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 165 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/25403
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92276295006, 92276295008, 92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1400211
Associated Lab Samples:92276295006, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
2,4,5-T ug/L ND 0.19 11/24/15 11:58
2,4,5-TP (Silvex)ug/L ND 0.19 11/24/15 11:58
2,4-D ug/L ND 0.94 11/24/15 11:58
Dinoseb ug/L ND 0.19 11/24/15 11:58
2,4-DCAA (S)%78 36-130 11/24/15 11:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1400212LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.11.2 95 40-130
2,4,5-TP (Silvex)ug/L 1.31.2 105 58-130
2,4-D ug/L 5.66 93 42-134
Dinoseb ug/L 1.21.2 102 10-157
2,4-DCAA (S)%91 36-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1401936MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35217261001
1401937
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4,5-T ug/L 1.2 102 40-130112 91.20.041U 1.2 1.3
2,4,5-TP (Silvex)ug/L 1.2 106 58-130112 51.20.048U 1.3 1.3
2,4-D ug/L 5.9 102 42-134106 25.90.22U 6.1 6.2
Dinoseb ug/L 1.2 104 10-157122 151.20.056U 1.2 1.4
2,4-DCAA (S)%94 36-130101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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[phone]
Page 166 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/25425
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1401789
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Matrix:Water
Analyzed
2,4,5-T ug/L ND 0.19 11/25/15 12:04
2,4,5-TP (Silvex)ug/L ND 0.19 11/25/15 12:04
2,4-D ug/L ND 0.94 11/25/15 12:04
Dinoseb ug/L ND 0.19 11/25/15 12:04
2,4-DCAA (S)%77 36-130 11/25/15 12:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1401790LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.21.2 103 40-130
2,4,5-TP (Silvex)ug/L 1.31.2 111 58-130
2,4-D ug/L 5.96 98 42-134
Dinoseb ug/L 1.11.2 95 10-157
2,4-DCAA (S)%95 36-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1401791MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276534004
1401792
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4,5-T ug/L 2.2 88 40-13080 102.2ND 1.9 1.8
2,4,5-TP (Silvex)ug/L M12.2 141 58-130103 322.2ND 3.1 2.2
2,4-D ug/L M1,R110.9 74 42-13429 8710.9ND 8.1 3.2
Dinoseb ug/L R12.2 56 10-15736 452.2ND 1.2 0.78
2,4-DCAA (S)%S024436-130144
REPORT OF LABORATORY ANALYSIS
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Page 167 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/25834
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92280822001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1427014
Associated Lab Samples:92280822001
Matrix:Water
Analyzed
2,4,5-T ug/L ND 0.19 12/24/15 02:03
2,4,5-TP (Silvex)ug/L ND 0.19 12/24/15 02:03
2,4-D ug/L ND 0.94 12/24/15 02:03
Dinoseb ug/L ND 0.19 12/24/15 02:03
2,4-DCAA (S)%31 36-130 S012/24/15 02:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1427015LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1429740
2,4,5-T ug/L 0.701.2 59 40-130650.78 10 40
2,4,5-TP (Silvex)ug/L 0.921.2 77 58-130861.0 11 40
2,4-D ug/L 3.26 53 42-134563.4 6 40
Dinoseb ug/L 0.721.2 60 10-157760.92 24 40
2,4-DCAA (S)%74 36-13073 40
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 168 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39107
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92276295005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608360
Associated Lab Samples:92276295005
Matrix:Water
Analyzed
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 11/20/15 13:54
1,3,5-Trinitrobenzene ug/L ND 10.0 11/20/15 13:54
1,3-Dinitrobenzene ug/L ND 20.0 11/20/15 13:54
1,4-Naphthoquinone ug/L ND 5.0 11/20/15 13:54
1-Naphthalenamine ug/L ND 5.0 11/20/15 13:54
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 11/24/15 09:29
2,4,5-Trichlorophenol ug/L ND 10.0 11/24/15 09:29
2,4,6-Trichlorophenol ug/L ND 10.0 11/24/15 09:29
2,4-Dichlorophenol ug/L ND 10.0 11/24/15 09:29
2,4-Dimethylphenol ug/L ND 10.0 11/24/15 09:29
2,4-Dinitrophenol ug/L ND 50.0 11/24/15 09:29
2,4-Dinitrotoluene ug/L ND 10.0 11/24/15 09:29
2,6-Dichlorophenol ug/L ND 10.0 11/20/15 13:54
2,6-Dinitrotoluene ug/L ND 10.0 11/24/15 09:29
2-Acetylaminofluorene ug/L 8.0J 20.0 11/20/15 13:54
2-Chloronaphthalene ug/L ND 10.0 11/24/15 09:29
2-Chlorophenol ug/L ND 10.0 11/24/15 09:29
2-Methylnaphthalene ug/L ND 10.0 11/24/15 09:29
2-Methylphenol(o-Cresol)ug/L ND 10.0 11/24/15 09:29
2-Naphthalenamine ug/L ND 5.0 11/20/15 13:54
2-Nitroaniline ug/L ND 50.0 11/24/15 09:29
2-Nitrophenol ug/L ND 10.0 11/24/15 09:29
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 11/24/15 09:29
3,3'-Dichlorobenzidine ug/L ND 20.0 11/24/15 09:29
3,3'-Dimethylbenzidine ug/L ND 10.0 11/20/15 13:54
3-Methylcholanthrene ug/L 2.2J 10.0 11/20/15 13:54
3-Nitroaniline ug/L ND 50.0 11/24/15 09:29
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/24/15 09:29
4-Aminobiphenyl ug/L ND 10.0 11/20/15 13:54
4-Bromophenylphenyl ether ug/L ND 10.0 11/24/15 09:29
4-Chloro-3-methylphenol ug/L ND 20.0 11/24/15 09:29
4-Chloroaniline ug/L ND 20.0 11/24/15 09:29
4-Chlorophenylphenyl ether ug/L ND 10.0 11/24/15 09:29
4-Nitroaniline ug/L ND 20.0 11/24/15 09:29
4-Nitrophenol ug/L ND 50.0 11/24/15 09:29
5-Nitro-o-toluidine ug/L ND 10.0 11/20/15 13:54
7,12-Dimethylbenz(a)anthracene ug/L 1.5J 10.0 11/20/15 13:54
Acenaphthene ug/L ND 10.0 11/24/15 09:29
Acenaphthylene ug/L ND 10.0 11/24/15 09:29
Acetophenone ug/L ND 10.0 11/24/15 09:29
Anthracene ug/L ND 10.0 11/24/15 09:29
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 169 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608360
Associated Lab Samples:92276295005
Matrix:Water
Analyzed
Benzo(a)anthracene ug/L ND 10.0 11/24/15 09:29
Benzo(a)pyrene ug/L ND 10.0 11/24/15 09:29
Benzo(b)fluoranthene ug/L ND 10.0 11/24/15 09:29
Benzo(g,h,i)perylene ug/L ND 10.0 11/24/15 09:29
Benzo(k)fluoranthene ug/L ND 10.0 11/24/15 09:29
Benzyl alcohol ug/L ND 20.0 11/24/15 09:29
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/24/15 09:29
bis(2-Chloroethyl) ether ug/L ND 10.0 11/24/15 09:29
bis(2-Chloroisopropyl) ether ug/L ND 10.0 11/24/15 09:29
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/24/15 09:29
Butylbenzylphthalate ug/L ND 10.0 11/24/15 09:29
Chlorobenzilate ug/L ND 10.0 11/20/15 13:54
Chrysene ug/L ND 10.0 11/24/15 09:29
Di-n-butylphthalate ug/L ND 10.0 11/24/15 09:29
Di-n-octylphthalate ug/L ND 10.0 11/24/15 09:29
Diallate ug/L ND 10.0 11/20/15 13:54
Dibenz(a,h)anthracene ug/L ND 10.0 11/24/15 09:29
Dibenzofuran ug/L ND 10.0 11/24/15 09:29
Diethylphthalate ug/L ND 10.0 11/24/15 09:29
Dimethoate ug/L ND 10.0 11/20/15 13:54
Dimethylphthalate ug/L ND 10.0 11/24/15 09:29
Diphenylamine ug/L ND 10.0 11/24/15 09:29
Disulfoton ug/L ND 10.0 11/20/15 13:54
Ethyl methanesulfonate ug/L ND 20.0 11/20/15 13:54
Famphur ug/L ND 10.0 11/20/15 13:54
Fluoranthene ug/L ND 10.0 11/24/15 09:29
Fluorene ug/L ND 10.0 11/24/15 09:29
Hexachlorobenzene ug/L ND 10.0 11/24/15 09:29
Hexachlorocyclopentadiene ug/L ND 10.0 11/24/15 09:29
Hexachloroethane ug/L ND 10.0 11/24/15 09:29
Hexachlorophene ug/L ND 100 11/20/15 13:54
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/24/15 09:29
Isodrin ug/L ND 20.0 11/20/15 13:54
Isophorone ug/L ND 10.0 11/24/15 09:29
Isosafrole ug/L ND 10.0 11/20/15 13:54
Kepone ug/L ND 10.0 11/20/15 13:54
Methapyrilene ug/L ND 50.0 11/20/15 13:54
Methyl methanesulfonate ug/L ND 5.0 11/20/15 13:54
Methyl parathion ug/L ND 10.0 11/20/15 13:54
N-Nitroso-di-n-butylamine ug/L ND 10.0 11/20/15 13:54
N-Nitroso-di-n-propylamine ug/L ND 10.0 11/24/15 09:29
N-Nitrosodiethylamine ug/L ND 20.0 11/20/15 13:54
N-Nitrosodimethylamine ug/L ND 10.0 11/24/15 09:29
N-Nitrosodiphenylamine ug/L ND 10.0 11/24/15 09:29
N-Nitrosomethylethylamine ug/L ND 10.0 11/20/15 13:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 170 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608360
Associated Lab Samples:92276295005
Matrix:Water
Analyzed
N-Nitrosopiperidine ug/L ND 20.0 11/20/15 13:54
N-Nitrosopyrrolidine ug/L ND 10.0 11/20/15 13:54
Nitrobenzene ug/L ND 10.0 11/24/15 09:29
O,O,O-Triethylphosphorothioate ug/L ND 10.0 11/20/15 13:54
O-Toluidine ug/L ND 10.0 11/20/15 13:54
P-Dimethylaminoazobenzene ug/L ND 5.0 11/20/15 13:54
p-Phenylenediamine ug/L ND 10.0 11/20/15 13:54
Parathion (Ethyl parathion)ug/L ND 10.0 11/20/15 13:54
Pentachlorobenzene ug/L ND 10.0 11/20/15 13:54
Pentachloronitrobenzene ug/L ND 20.0 11/20/15 13:54
Pentachlorophenol ug/L ND 25.0 11/24/15 09:29
Phenacetin ug/L ND 20.0 11/20/15 13:54
Phenanthrene ug/L ND 10.0 11/24/15 09:29
Phenol ug/L ND 10.0 11/24/15 09:29
Phorate ug/L ND 10.0 11/20/15 13:54
Pronamide ug/L ND 10.0 11/20/15 13:54
Pyrene ug/L ND 10.0 11/24/15 09:29
Safrole ug/L ND 10.0 11/20/15 13:54
Thionazin ug/L ND 20.0 11/20/15 13:54
2,4,6-Tribromophenol (S)%65 27-110 11/24/15 09:29
2-Fluorobiphenyl (S)%68 27-110 11/24/15 09:29
2-Fluorophenol (S)%32 12-110 11/24/15 09:29
Nitrobenzene-d5 (S)%59 21-110 11/24/15 09:29
Phenol-d6 (S)%21 10-110 11/24/15 09:29
Terphenyl-d14 (S)%83 31-107 11/24/15 09:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608361LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 34.750 69 16-129
1,3,5-Trinitrobenzene ug/L 65.4 L05013155-125
1,3-Dinitrobenzene ug/L 45.650 91 30-122
1,4-Naphthoquinone ug/L 38.750 77 31-120
1-Naphthalenamine ug/L 32.350 65 37-126
2,3,4,6-Tetrachlorophenol ug/L 91.750 183 54-276
2,4,5-Trichlorophenol ug/L 46.150 92 43-113
2,4,6-Trichlorophenol ug/L 42.650 85 42-120
2,4-Dichlorophenol ug/L 38.450 77 30-120
2,4-Dimethylphenol ug/L 35.450 71 29-111
2,4-Dinitrophenol ug/L 194250 78 19-132
2,4-Dinitrotoluene ug/L 46.350 93 58-128
2,6-Dichlorophenol ug/L 36.050 72 54-128
2,6-Dinitrotoluene ug/L 47.050 94 54-129
2-Acetylaminofluorene ug/L 46.350 93 81-160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 171 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608361LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chloronaphthalene ug/L 45.350 91 43-117
2-Chlorophenol ug/L 31.050 62 37-120
2-Methylnaphthalene ug/L 34.350 69 33-120
2-Methylphenol(o-Cresol)ug/L 30.450 61 31-120
2-Naphthalenamine ug/L 40.650 81 41-136
2-Nitroaniline ug/L 76.5100 76 48-121
2-Nitrophenol ug/L 40.250 80 25-116
3&4-Methylphenol(m&p Cresol)ug/L 25.450 51 23-120
3,3'-Dichlorobenzidine ug/L 86.5250 35 10-154
3,3'-Dimethylbenzidine ug/L 70.9100 71 10-157
3-Methylcholanthrene ug/L 47.350 95 65-130
3-Nitroaniline ug/L 82.8100 83 43-115
4,6-Dinitro-2-methylphenol ug/L 95.5100 96 44-124
4-Aminobiphenyl ug/L 42.350 85 21-125
4-Bromophenylphenyl ether ug/L 41.150 82 34-113
4-Chloro-3-methylphenol ug/L 79.2100 79 31-110
4-Chloroaniline ug/L 65.1100 65 20-120
4-Chlorophenylphenyl ether ug/L 38.650 77 34-116
4-Nitroaniline ug/L 88.7100 89 46-128
4-Nitrophenol ug/L 96.8250 39 11-120
5-Nitro-o-toluidine ug/L 49.250 98 78-160
7,12-Dimethylbenz(a)anthracene ug/L 48.250 96 47-124
Acenaphthene ug/L 40.550 81 48-114
Acenaphthylene ug/L 42.650 85 48-112
Acetophenone ug/L 33.650 67 24-120
Anthracene ug/L 46.450 93 57-118
Benzo(a)anthracene ug/L 47.050 94 56-121
Benzo(a)pyrene ug/L 47.750 95 55-127
Benzo(b)fluoranthene ug/L 50.250 100 53-128
Benzo(g,h,i)perylene ug/L 43.450 87 54-125
Benzo(k)fluoranthene ug/L 56.850 114 51-123
Benzyl alcohol ug/L 56.2100 56 27-120
bis(2-Chloroethoxy)methane ug/L 33.650 67 32-120
bis(2-Chloroethyl) ether ug/L 30.850 62 33-111
bis(2-Chloroisopropyl) ether ug/L 27.350 55 15-120
bis(2-Ethylhexyl)phthalate ug/L 51.850 104 50-145
Butylbenzylphthalate ug/L 54.250 108 54-138
Chlorobenzilate ug/L 52.250 104 65-132
Chrysene ug/L 46.250 92 58-127
Di-n-butylphthalate ug/L 52.050 104 56-125
Di-n-octylphthalate ug/L 46.750 93 50-134
Diallate ug/L 48.650 97 47-123
Dibenz(a,h)anthracene ug/L 44.750 89 53-129
Dibenzofuran ug/L 39.650 79 45-120
Diethylphthalate ug/L 43.750 87 53-120
Dimethoate ug/L 44.950 90 57-139
Dimethylphthalate ug/L 43.050 86 55-116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 172 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608361LABORATORY CONTROL SAMPLE:
LCSSpike
Diphenylamine ug/L 41.150 82 42-120
Disulfoton ug/L 42.850 86 49-156
Ethyl methanesulfonate ug/L 36.550 73 43-120
Famphur ug/L 40.7100 41 40-160
Fluoranthene ug/L 48.850 98 57-125
Fluorene ug/L 43.250 86 53-118
Hexachlorobenzene ug/L 47.250 94 49-116
Hexachlorocyclopentadiene ug/L 34.450 69 26-158
Hexachloroethane ug/L 33.650 67 30-114
Hexachlorophene ug/L 246500 49 10-130
Indeno(1,2,3-cd)pyrene ug/L 44.750 89 55-128
Isodrin ug/L 47.350 95 68-129
Isophorone ug/L 36.350 73 31-118
Isosafrole ug/L 40.350 81 48-107
Kepone ug/L 61.0100 61 10-124
Methapyrilene ug/L 20.5J50 41 40-160
Methyl methanesulfonate ug/L 25.650 51 25-114
Methyl parathion ug/L 48.550 97 58-137
N-Nitroso-di-n-butylamine ug/L 31.350 63 36-115
N-Nitroso-di-n-propylamine ug/L 32.550 65 32-119
N-Nitrosodiethylamine ug/L 40.750 81 47-115
N-Nitrosodimethylamine ug/L 19.550 39 13-120
N-Nitrosodiphenylamine ug/L 41.150 82 43-120
N-Nitrosomethylethylamine ug/L 36.150 72 39-120
N-Nitrosopiperidine ug/L 35.850 72 43-113
N-Nitrosopyrrolidine ug/L 35.950 72 32-110
Nitrobenzene ug/L 35.050 70 33-110
O,O,O-Triethylphosphorothioate ug/L 35.050 70 51-127
O-Toluidine ug/L 31.550 63 27-120
P-Dimethylaminoazobenzene ug/L 24.6100 25 10-120
p-Phenylenediamine ug/L 43.850 88 72-143
Parathion (Ethyl parathion)ug/L 47.550 95 56-140
Pentachlorobenzene ug/L 38.450 77 30-137
Pentachloronitrobenzene ug/L 52.750 105 70-124
Pentachlorophenol ug/L 90.2250 36 10-137
Phenacetin ug/L 50.350 101 60-130
Phenanthrene ug/L 42.250 84 57-117
Phenol ug/L 15.350 31 10-120
Phorate ug/L 64.7 L05012955-126
Pronamide ug/L 51.550 103 75-124
Pyrene ug/L 49.750 99 55-122
Safrole ug/L 32.750 65 41-120
Thionazin ug/L 43.650 87 63-137
2,4,6-Tribromophenol (S)%92 27-110
2-Fluorobiphenyl (S)%74 27-110
2-Fluorophenol (S)%38 12-110
Nitrobenzene-d5 (S)%72 21-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 173 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608361LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol-d6 (S)%26 10-110
Terphenyl-d14 (S)%89 31-107
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1608362MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275855005
1608363
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4,5-Tetrachlorobenzene ug/L M1,R11007950-15047 50100ND79.1 47.3
1,3,5-Trinitrobenzene ug/L 100 132 50-150130 2100ND132130
1,3-Dinitrobenzene ug/L 100 100 50-15096 4100ND10096.1
1,4-Naphthoquinone ug/L 100 83 50-15077 8100ND83.3 76.7
1-Naphthalenamine ug/L 100 74 50-15070 5100ND73.5 69.7
2,3,4,6-Tetrachlorophenol ug/L M110020550-150197 4100ND205197
2,4,5-Trichlorophenol ug/L 100 100 19-10589 11100ND99.8 89.4
2,4,6-Trichlorophenol ug/L 100 90 13-10877 16100ND90.3 76.7
2,4-Dichlorophenol ug/L R11008029-11157 35100ND80.3 56.7
2,4-Dimethylphenol ug/L R11007421-10353 33100ND73.8 52.8
2,4-Dinitrophenol ug/L 500 102 10-109100 2500ND511499
2,4-Dinitrotoluene ug/L 100 103 27-104100 3100ND10399.8
2,6-Dichlorophenol ug/L 100 76 50-15059 25100ND76.0 58.8
2,6-Dinitrotoluene ug/L 100 100 28-10195 5100ND10095.3
2-Acetylaminofluorene ug/L 100 81 50-15085 51007.1J 87.8 92.0
2-Chloronaphthalene ug/L M1,R110010414-10271 37100ND10471.0
2-Chlorophenol ug/L R11007516-11041 59100ND75.1 40.7
2-Methylnaphthalene ug/L R11007213-11050 37100ND72.4 49.6
2-Methylphenol(o-Cresol)ug/L R11007919-11043 59100ND78.5 42.5
2-Naphthalenamine ug/L 100 87 50-15080 9100ND87.1 80.0
2-Nitroaniline ug/L 200 82 26-10376 7200ND164152
2-Nitrophenol ug/L R11008120-11052 44100ND80.9 51.8
3&4-Methylphenol(m&p
Cresol)ug/L R11007120-11040 56100ND70.6 39.6
3,3'-Dichlorobenzidine ug/L 500 33 25-11234 3500ND164168
3,3'-Dimethylbenzidine ug/L 200 67 50-15067 1200ND134133
3-Methylcholanthrene ug/L 100 94 50-15092 1100ND94.1 92.8
3-Nitroaniline ug/L 200 93 29-11089 4200ND186179
4,6-Dinitro-2-methylphenol ug/L 200 96 10-11797 1200ND192194
4-Aminobiphenyl ug/L 100 86 50-15086 0100ND85.6 85.6
4-Bromophenylphenyl ether ug/L 100 80 20-10576 5100ND80.0 76.1
4-Chloro-3-methylphenol ug/L 200 84 22-11082 2200ND167165
4-Chloroaniline ug/L 200 68 20-10053 26200ND136105
4-Chlorophenylphenyl ether ug/L 100 83 19-10274 11100ND83.2 74.3
4-Nitroaniline ug/L 200 104 29-110100 4200ND207200
4-Nitrophenol ug/L 500 74 10-11065 12500ND369326
5-Nitro-o-toluidine ug/L 100 116 50-150111 4100ND116111
7,12-
Dimethylbenz(a)anthracene ug/L 100 99 50-15098 1100ND98.8 97.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 174 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1608362MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275855005
1608363
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Acenaphthene ug/L 100 88 17-10072 20100ND87.5 71.5
Acenaphthylene ug/L 100 92 21-10075 20100ND91.8 74.7
Acetophenone ug/L M1,R11007650-15042 57100ND75.8 42.2
Anthracene ug/L 100 93 24-10992 2100ND93.4 91.7
Benzo(a)anthracene ug/L 100 95 22-11792 3100ND94.8 92.3
Benzo(a)pyrene ug/L 100 97 23-10495 2100ND97.4 95.1
Benzo(b)fluoranthene ug/L 100 101 23-103102 1100ND101102
Benzo(g,h,i)perylene ug/L 100 89 18-11185 4100ND88.5 85.0
Benzo(k)fluoranthene ug/L M110011522-113114 2100ND115114
Benzyl alcohol ug/L R12007419-10140 59200ND14780.4
bis(2-Chloroethoxy)methane ug/L R11006922-11044 45100ND69.4 44.1
bis(2-Chloroethyl) ether ug/L R11007016-11039 56100ND70.1 39.4
bis(2-Chloroisopropyl) ether ug/L R11006314-11034 59100ND62.7 34.3
bis(2-Ethylhexyl)phthalate ug/L M110010523-102104 2100ND105104
Butylbenzylphthalate ug/L M110011225-110109 3100ND112109
Chlorobenzilate ug/L 100 109 50-150106 2100ND109106
Chrysene ug/L 100 92 23-11592 0100ND91.9 92.1
Di-n-butylphthalate ug/L 100 109 26-110107 2100ND109107
Di-n-octylphthalate ug/L 100 89 22-11094 5100ND89.1 93.9
Diallate ug/L 100 94 50-15090 4100ND93.9 90.0
Dibenz(a,h)anthracene ug/L 100 90 21-11287 3100ND90.2 87.5
Dibenzofuran ug/L 100 86 19-10274 16100ND86.1 73.6
Diethylphthalate ug/L 100 97 29-11093 4100ND96.5 92.9
Dimethoate ug/L 100 100 50-15097 4100ND10096.6
Dimethylphthalate ug/L 100 92 27-11087 6100ND91.7 86.6
Diphenylamine ug/L 100 78 50-15076 3100ND78.5 75.9
Disulfoton ug/L 100 87 50-15086 2100ND87.2 85.7
Ethyl methanesulfonate ug/L M1,R11008750-15047 59100ND86.8 47.4
Famphur ug/L M1,R12004650-15028 48200ND91.6 56.3
Fluoranthene ug/L 100 103 23-112102 1100ND103102
Fluorene ug/L 100 95 22-10486 10100ND94.9 86.2
Hexachlorobenzene ug/L 100 91 21-11688 3100ND90.7 88.0
Hexachlorocyclopentadiene ug/L R11007710-11041 61100ND76.6 40.7
Hexachloroethane ug/L R11008410-11047 56100ND83.9 47.1
Hexachlorophene ug/L M110004850-15052 91000ND478524
Indeno(1,2,3-cd)pyrene ug/L 100 91 20-11388 4100ND91.0 87.6
Isodrin ug/L 100 99 50-15095 3100ND98.6 95.5
Isophorone ug/L R11007450-15053 32100ND73.8 53.5
Isosafrole ug/L 100 88 50-15065 29100ND87.6 65.2
Kepone ug/L 200 79 50-15070 12200ND158140
Methapyrilene ug/L M11005550-15036100ND55.1J 36.4J
Methyl methanesulfonate ug/L M1,R11007150-15039 59100ND71.0 38.8
Methyl parathion ug/L 100 104 50-150102 2100ND104102
N-Nitroso-di-n-butylamine ug/L 100 63 50-15060 5100ND63.4 60.1
N-Nitroso-di-n-propylamine ug/L R11007421-10541 57100ND73.7 40.9
N-Nitrosodiethylamine ug/L R11009350-15050 59100ND92.6 50.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 175 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1608362MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275855005
1608363
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/L R11006210-11033 61100ND61.8 32.9
N-Nitrosodiphenylamine ug/L 100 78 23-10776 3100ND78.5 75.9
N-Nitrosomethylethylamine ug/L M1,R11009050-15048 61100ND89.8 48.0
N-Nitrosopiperidine ug/L 100 75 50-15059 24100ND74.8 58.6
N-Nitrosopyrrolidine ug/L R11008950-15056 46100ND88.9 55.5
Nitrobenzene ug/L R11007020-11045 43100ND69.8 45.1
O,O,O-
Triethylphosphorothioate ug/L R11007350-15050 38100ND73.2 50.1
O-Toluidine ug/L M1,R11007650-15044 54100ND75.8 43.7
P-Dimethylaminoazobenzene ug/L M12002550-15025 2200ND49.8 50.7
p-Phenylenediamine ug/L 100 106 50-150126 17100ND106126
Parathion (Ethyl parathion)ug/L 100 101 50-150100 1100ND101100
Pentachlorobenzene ug/L 100 83 50-15070 17100ND83.5 70.4
Pentachloronitrobenzene ug/L 100 106 50-150105 1100ND106105
Pentachlorophenol ug/L 500 36 10-11838 3500ND182189
Phenacetin ug/L 100 109 50-150107 3100ND109107
Phenanthrene ug/L 100 85 24-10683 3100ND84.9 82.6
Phenol ug/L R11005312-11027 66100ND52.8 26.7
Phorate ug/L 100 131 50-150128 2100ND131128
Pronamide ug/L 100 110 50-150108 2100ND110108
Pyrene ug/L 100 99 24-11498 2100ND99.5 97.8
Safrole ug/L 100 69 50-15051 30100ND68.9 51.1
Thionazin ug/L 100 97 50-15095 2100ND97.1 95.2
2,4,6-Tribromophenol (S)%91 27-11088
2-Fluorobiphenyl (S)%81 27-11054
2-Fluorophenol (S)%60 12-11031
Nitrobenzene-d5 (S)%73 21-11046
Phenol-d6 (S)%47 10-11023
Terphenyl-d14 (S)%90 31-10789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 176 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39238
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1612612
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 11/23/15 21:12
1,3,5-Trinitrobenzene ug/L ND 10.0 11/23/15 21:12
1,3-Dinitrobenzene ug/L ND 20.0 11/23/15 21:12
1,4-Naphthoquinone ug/L ND 5.0 11/23/15 21:12
1-Naphthalenamine ug/L ND 5.0 11/23/15 21:12
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 11/23/15 21:12
2,4,5-Trichlorophenol ug/L ND 10.0 11/23/15 21:12
2,4,6-Trichlorophenol ug/L ND 10.0 11/23/15 21:12
2,4-Dichlorophenol ug/L ND 10.0 11/23/15 21:12
2,4-Dimethylphenol ug/L ND 10.0 11/23/15 21:12
2,4-Dinitrophenol ug/L ND 50.0 11/23/15 21:12
2,4-Dinitrotoluene ug/L ND 10.0 11/23/15 21:12
2,6-Dichlorophenol ug/L ND 10.0 11/23/15 21:12
2,6-Dinitrotoluene ug/L ND 10.0 11/23/15 21:12
2-Acetylaminofluorene ug/L ND 20.0 11/23/15 21:12
2-Chloronaphthalene ug/L ND 10.0 11/23/15 21:12
2-Chlorophenol ug/L ND 10.0 11/23/15 21:12
2-Methylnaphthalene ug/L ND 10.0 11/23/15 21:12
2-Methylphenol(o-Cresol)ug/L ND 10.0 11/23/15 21:12
2-Naphthalenamine ug/L ND 5.0 11/23/15 21:12
2-Nitroaniline ug/L ND 50.0 11/23/15 21:12
2-Nitrophenol ug/L ND 10.0 11/23/15 21:12
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 11/23/15 21:12
3,3'-Dichlorobenzidine ug/L ND 20.0 11/23/15 21:12
3,3'-Dimethylbenzidine ug/L ND 10.0 11/23/15 21:12
3-Methylcholanthrene ug/L ND 10.0 11/23/15 21:12
3-Nitroaniline ug/L ND 50.0 11/23/15 21:12
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/23/15 21:12
4-Aminobiphenyl ug/L ND 10.0 11/23/15 21:12
4-Bromophenylphenyl ether ug/L ND 10.0 11/23/15 21:12
4-Chloro-3-methylphenol ug/L ND 20.0 11/23/15 21:12
4-Chloroaniline ug/L ND 20.0 11/23/15 21:12
4-Chlorophenylphenyl ether ug/L ND 10.0 11/23/15 21:12
4-Nitroaniline ug/L ND 20.0 11/23/15 21:12
4-Nitrophenol ug/L ND 50.0 11/23/15 21:12
5-Nitro-o-toluidine ug/L ND 10.0 11/23/15 21:12
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 11/23/15 21:12
Acenaphthene ug/L ND 10.0 11/23/15 21:12
Acenaphthylene ug/L ND 10.0 11/23/15 21:12
Acetophenone ug/L ND 10.0 11/23/15 21:12
Anthracene ug/L ND 10.0 11/23/15 21:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 177 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1612612
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
Benzo(a)anthracene ug/L ND 10.0 11/23/15 21:12
Benzo(a)pyrene ug/L ND 10.0 11/23/15 21:12
Benzo(b)fluoranthene ug/L ND 10.0 11/23/15 21:12
Benzo(g,h,i)perylene ug/L ND 10.0 11/23/15 21:12
Benzo(k)fluoranthene ug/L ND 10.0 11/23/15 21:12
Benzyl alcohol ug/L ND 20.0 11/23/15 21:12
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/23/15 21:12
bis(2-Chloroethyl) ether ug/L ND 10.0 11/23/15 21:12
bis(2-Chloroisopropyl) ether ug/L ND 10.0 11/23/15 21:12
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/23/15 21:12
Butylbenzylphthalate ug/L ND 10.0 11/23/15 21:12
Chlorobenzilate ug/L ND 10.0 11/23/15 21:12
Chrysene ug/L ND 10.0 11/23/15 21:12
Di-n-butylphthalate ug/L ND 10.0 11/23/15 21:12
Di-n-octylphthalate ug/L ND 10.0 11/23/15 21:12
Diallate ug/L ND 10.0 11/23/15 21:12
Dibenz(a,h)anthracene ug/L ND 10.0 11/23/15 21:12
Dibenzofuran ug/L ND 10.0 11/23/15 21:12
Diethylphthalate ug/L ND 10.0 11/23/15 21:12
Dimethoate ug/L ND 10.0 11/23/15 21:12
Dimethylphthalate ug/L ND 10.0 11/23/15 21:12
Diphenylamine ug/L ND 10.0 11/23/15 21:12
Disulfoton ug/L ND 10.0 11/23/15 21:12
Ethyl methanesulfonate ug/L ND 20.0 11/23/15 21:12
Famphur ug/L ND 10.0 11/23/15 21:12
Fluoranthene ug/L ND 10.0 11/23/15 21:12
Fluorene ug/L ND 10.0 11/23/15 21:12
Hexachlorobenzene ug/L ND 10.0 11/23/15 21:12
Hexachlorocyclopentadiene ug/L ND 10.0 11/23/15 21:12
Hexachloroethane ug/L ND 10.0 11/23/15 21:12
Hexachlorophene ug/L ND 100 11/23/15 21:12
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/23/15 21:12
Isodrin ug/L ND 20.0 11/23/15 21:12
Isophorone ug/L ND 10.0 11/23/15 21:12
Isosafrole ug/L ND 10.0 11/23/15 21:12
Kepone ug/L ND 10.0 11/23/15 21:12
Methapyrilene ug/L ND 50.0 11/23/15 21:12
Methyl methanesulfonate ug/L ND 5.0 11/23/15 21:12
Methyl parathion ug/L ND 10.0 11/23/15 21:12
N-Nitroso-di-n-butylamine ug/L ND 10.0 11/23/15 21:12
N-Nitroso-di-n-propylamine ug/L ND 10.0 11/23/15 21:12
N-Nitrosodiethylamine ug/L ND 20.0 11/23/15 21:12
N-Nitrosodimethylamine ug/L ND 10.0 11/23/15 21:12
N-Nitrosodiphenylamine ug/L ND 10.0 11/23/15 21:12
N-Nitrosomethylethylamine ug/L ND 10.0 11/23/15 21:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 178 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1612612
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
N-Nitrosopiperidine ug/L ND 20.0 11/23/15 21:12
N-Nitrosopyrrolidine ug/L ND 10.0 11/23/15 21:12
Nitrobenzene ug/L ND 10.0 11/23/15 21:12
O,O,O-Triethylphosphorothioate ug/L ND 10.0 11/23/15 21:12
O-Toluidine ug/L ND 10.0 11/23/15 21:12
P-Dimethylaminoazobenzene ug/L ND 5.0 11/23/15 21:12
p-Phenylenediamine ug/L ND 10.0 11/23/15 21:12
Parathion (Ethyl parathion)ug/L ND 10.0 11/23/15 21:12
Pentachlorobenzene ug/L ND 10.0 11/23/15 21:12
Pentachloronitrobenzene ug/L ND 20.0 11/23/15 21:12
Pentachlorophenol ug/L ND 25.0 11/23/15 21:12
Phenacetin ug/L ND 20.0 11/23/15 21:12
Phenanthrene ug/L ND 10.0 11/23/15 21:12
Phenol ug/L ND 10.0 11/23/15 21:12
Phorate ug/L ND 10.0 11/23/15 21:12
Pronamide ug/L ND 10.0 11/23/15 21:12
Pyrene ug/L ND 10.0 11/23/15 21:12
Safrole ug/L ND 10.0 11/23/15 21:12
Thionazin ug/L ND 20.0 11/23/15 21:12
2,4,6-Tribromophenol (S)%79 27-110 11/23/15 21:12
2-Fluorobiphenyl (S)%74 27-110 11/23/15 21:12
2-Fluorophenol (S)%39 12-110 11/23/15 21:12
Nitrobenzene-d5 (S)%75 21-110 11/23/15 21:12
Phenol-d6 (S)%25 10-110 11/23/15 21:12
Terphenyl-d14 (S)%81 31-107 11/23/15 21:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612613LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 37.850 76 16-129
1,3,5-Trinitrobenzene ug/L 62.650 125 55-125
1,3-Dinitrobenzene ug/L 44.450 89 30-122
1,4-Naphthoquinone ug/L 38.450 77 31-120
1-Naphthalenamine ug/L 29.850 60 37-126
2,3,4,6-Tetrachlorophenol ug/L 87.750 175 54-276
2,4,5-Trichlorophenol ug/L 45.850 92 43-113
2,4,6-Trichlorophenol ug/L 41.150 82 42-120
2,4-Dichlorophenol ug/L 36.850 74 30-120
2,4-Dimethylphenol ug/L 34.050 68 29-111
2,4-Dinitrophenol ug/L 158250 63 19-132
2,4-Dinitrotoluene ug/L 46.050 92 58-128
2,6-Dichlorophenol ug/L 31.950 64 54-128
2,6-Dinitrotoluene ug/L 46.250 92 54-129
2-Acetylaminofluorene ug/L 41.450 83 81-160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 179 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612613LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chloronaphthalene ug/L 48.750 97 43-117
2-Chlorophenol ug/L 31.250 62 37-120
2-Methylnaphthalene ug/L 34.550 69 33-120
2-Methylphenol(o-Cresol)ug/L 29.350 59 31-120
2-Naphthalenamine ug/L 37.050 74 41-136
2-Nitroaniline ug/L 77.7100 78 48-121
2-Nitrophenol ug/L 39.950 80 25-116
3&4-Methylphenol(m&p Cresol)ug/L 51.850 104 23-120
3,3'-Dichlorobenzidine ug/L 77.7250 31 10-154
3,3'-Dimethylbenzidine ug/L 48.1100 48 10-157
3-Methylcholanthrene ug/L 36.850 74 65-130
3-Nitroaniline ug/L 80.7100 81 43-115
4,6-Dinitro-2-methylphenol ug/L 79.6100 80 44-124
4-Aminobiphenyl ug/L 37.250 74 21-125
4-Bromophenylphenyl ether ug/L 39.850 80 34-113
4-Chloro-3-methylphenol ug/L 73.8100 74 31-110
4-Chloroaniline ug/L 60.2100 60 20-120
4-Chlorophenylphenyl ether ug/L 38.650 77 34-116
4-Nitroaniline ug/L 90.0100 90 46-128
4-Nitrophenol ug/L 92.4250 37 11-120
5-Nitro-o-toluidine ug/L 49.250 98 78-160
7,12-Dimethylbenz(a)anthracene ug/L 39.150 78 47-124
Acenaphthene ug/L 40.850 82 48-114
Acenaphthylene ug/L 42.950 86 48-112
Acetophenone ug/L 32.550 65 24-120
Anthracene ug/L 45.650 91 57-118
Benzo(a)anthracene ug/L 45.550 91 56-121
Benzo(a)pyrene ug/L 39.950 80 55-127
Benzo(b)fluoranthene ug/L 40.350 81 53-128
Benzo(g,h,i)perylene ug/L 36.850 74 54-125
Benzo(k)fluoranthene ug/L 48.050 96 51-123
Benzyl alcohol ug/L 53.9100 54 27-120
bis(2-Chloroethoxy)methane ug/L 34.550 69 32-120
bis(2-Chloroethyl) ether ug/L 31.350 63 33-111
bis(2-Chloroisopropyl) ether ug/L 27.950 56 15-120
bis(2-Ethylhexyl)phthalate ug/L 49.350 99 50-145
Butylbenzylphthalate ug/L 51.950 104 54-138
Chlorobenzilate ug/L 49.650 99 65-132
Chrysene ug/L 44.950 90 58-127
Di-n-butylphthalate ug/L 50.050 100 56-125
Di-n-octylphthalate ug/L 43.050 86 50-134
Diallate ug/L 46.350 93 47-123
Dibenz(a,h)anthracene ug/L 37.350 75 53-129
Dibenzofuran ug/L 40.250 80 45-120
Diethylphthalate ug/L 43.750 87 53-120
Dimethoate ug/L 42.950 86 57-139
Dimethylphthalate ug/L 42.750 85 55-116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 180 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612613LABORATORY CONTROL SAMPLE:
LCSSpike
Diphenylamine ug/L 39.750 79 42-120
Disulfoton ug/L 41.050 82 49-156
Ethyl methanesulfonate ug/L 35.650 71 43-120
Famphur ug/L 66.6100 67 40-160
Fluoranthene ug/L 48.450 97 57-125
Fluorene ug/L 43.950 88 53-118
Hexachlorobenzene ug/L 45.850 92 49-116
Hexachlorocyclopentadiene ug/L 36.650 73 26-158
Hexachloroethane ug/L 34.650 69 30-114
Hexachlorophene ug/L 146500 29 10-130
Indeno(1,2,3-cd)pyrene ug/L 37.450 75 55-128
Isodrin ug/L 45.250 90 68-129
Isophorone ug/L 35.750 71 31-118
Isosafrole ug/L 40.550 81 48-107
Kepone ug/L 91.7100 92 10-124
Methapyrilene ug/L 25.7J50 51 40-160
Methyl methanesulfonate ug/L 26.850 54 25-114
Methyl parathion ug/L 46.750 93 58-137
N-Nitroso-di-n-butylamine ug/L 26.050 52 36-115
N-Nitroso-di-n-propylamine ug/L 29.650 59 32-119
N-Nitrosodiethylamine ug/L 38.850 78 47-115
N-Nitrosodimethylamine ug/L 22.250 44 13-120
N-Nitrosodiphenylamine ug/L 39.750 79 43-120
N-Nitrosomethylethylamine ug/L 36.350 73 39-120
N-Nitrosopiperidine ug/L 31.850 64 43-113
N-Nitrosopyrrolidine ug/L 29.050 58 32-110
Nitrobenzene ug/L 35.850 72 33-110
O,O,O-Triethylphosphorothioate ug/L 32.550 65 51-127
O-Toluidine ug/L 28.750 57 27-120
P-Dimethylaminoazobenzene ug/L 23.9100 24 10-120
p-Phenylenediamine ug/L 37.450 75 72-143
Parathion (Ethyl parathion)ug/L 45.650 91 56-140
Pentachlorobenzene ug/L 38.850 78 30-137
Pentachloronitrobenzene ug/L 51.450 103 70-124
Pentachlorophenol ug/L 82.0250 33 10-137
Phenacetin ug/L 47.950 96 60-130
Phenanthrene ug/L 41.450 83 57-117
Phenol ug/L 15.150 30 10-120
Phorate ug/L 61.950 124 55-126
Pronamide ug/L 49.950 100 75-124
Pyrene ug/L 47.850 96 55-122
Safrole ug/L 29.850 60 41-120
Thionazin ug/L 42.950 86 63-137
2,4,6-Tribromophenol (S)%88 27-110
2-Fluorobiphenyl (S)%77 27-110
2-Fluorophenol (S)%41 12-110
Nitrobenzene-d5 (S)%75 21-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 181 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612613LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol-d6 (S)%26 10-110
Terphenyl-d14 (S)%87 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1612614MATRIX SPIKE SAMPLE:
MSSpike
Result
92276747001
1,2,4,5-Tetrachlorobenzene ug/L 39.150 78 50-150ND
1,3,5-Trinitrobenzene ug/L 63.450 127 50-150ND
1,3-Dinitrobenzene ug/L 42.150 84 50-150ND
1,4-Naphthoquinone ug/L 36.650 73 50-150ND
1-Naphthalenamine ug/L 30.450 61 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 83.0 M15016650-150ND
2,4,5-Trichlorophenol ug/L 43.650 87 19-105ND
2,4,6-Trichlorophenol ug/L 40.050 80 13-108ND
2,4-Dichlorophenol ug/L 34.950 70 29-111ND
2,4-Dimethylphenol ug/L 32.050 64 21-103ND
2,4-Dinitrophenol ug/L 138250 55 10-109ND
2,4-Dinitrotoluene ug/L 45.450 91 27-104ND
2,6-Dichlorophenol ug/L 36.750 73 50-150ND
2,6-Dinitrotoluene ug/L 45.150 90 28-101ND
2-Acetylaminofluorene ug/L 43.950 88 50-150ND
2-Chloronaphthalene ug/L 49.450 99 14-102ND
2-Chlorophenol ug/L 31.850 64 16-110ND
2-Methylnaphthalene ug/L 33.950 68 13-110ND
2-Methylphenol(o-Cresol)ug/L 29.650 59 19-110ND
2-Naphthalenamine ug/L 33.750 67 50-150ND
2-Nitroaniline ug/L 74.9100 75 26-103ND
2-Nitrophenol ug/L 36.950 74 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 23.350 47 20-110ND
3,3'-Dichlorobenzidine ug/L 85.7250 34 25-112ND
3,3'-Dimethylbenzidine ug/L 51.5100 51 50-150ND
3-Methylcholanthrene ug/L 40.050 80 50-150ND
3-Nitroaniline ug/L 76.2100 76 29-110ND
4,6-Dinitro-2-methylphenol ug/L 81.3100 81 10-117ND
4-Aminobiphenyl ug/L 35.950 72 50-150ND
4-Bromophenylphenyl ether ug/L 39.650 79 20-105ND
4-Chloro-3-methylphenol ug/L 68.0100 68 22-110ND
4-Chloroaniline ug/L 56.9100 57 20-100ND
4-Chlorophenylphenyl ether ug/L 38.950 78 19-102ND
4-Nitroaniline ug/L 90.6100 91 29-110ND
4-Nitrophenol ug/L 92.9250 37 10-110ND
5-Nitro-o-toluidine ug/L 48.250 96 50-150ND
7,12-Dimethylbenz(a)anthracene ug/L 41.550 83 50-150ND
Acenaphthene ug/L 40.950 82 17-100ND
Acenaphthylene ug/L 43.050 86 21-100ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 182 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1612614MATRIX SPIKE SAMPLE:
MSSpike
Result
92276747001
Acetophenone ug/L 34.450 69 50-150ND
Anthracene ug/L 45.650 91 24-109ND
Benzo(a)anthracene ug/L 45.050 90 22-117ND
Benzo(a)pyrene ug/L 41.950 84 23-104ND
Benzo(b)fluoranthene ug/L 43.550 87 23-103ND
Benzo(g,h,i)perylene ug/L 40.350 81 18-111ND
Benzo(k)fluoranthene ug/L 51.550 103 22-113ND
Benzyl alcohol ug/L 51.7100 52 19-101ND
bis(2-Chloroethoxy)methane ug/L 33.150 66 22-110ND
bis(2-Chloroethyl) ether ug/L 33.050 66 16-110ND
bis(2-Chloroisopropyl) ether ug/L 30.450 61 14-110ND
bis(2-Ethylhexyl)phthalate ug/L 47.450 95 23-102ND
Butylbenzylphthalate ug/L 49.750 99 25-110ND
Chlorobenzilate ug/L 44.650 89 50-150ND
Chrysene ug/L 45.250 90 23-115ND
Di-n-butylphthalate ug/L 51.150 102 26-110ND
Di-n-octylphthalate ug/L 42.650 85 22-110ND
Diallate ug/L 47.750 95 50-150ND
Dibenz(a,h)anthracene ug/L 40.750 81 21-112ND
Dibenzofuran ug/L 40.350 81 19-102ND
Diethylphthalate ug/L 44.350 89 29-110ND
Dimethoate ug/L 45.750 91 50-150ND
Dimethylphthalate ug/L 42.550 85 27-110ND
Diphenylamine ug/L 39.750 79 50-150ND
Disulfoton ug/L 41.450 83 50-150ND
Ethyl methanesulfonate ug/L 38.250 76 50-150ND
Famphur ug/L 79.1100 79 50-150ND
Fluoranthene ug/L 51.050 102 23-112ND
Fluorene ug/L 43.650 87 22-104ND
Hexachlorobenzene ug/L 46.150 92 21-116ND
Hexachlorocyclopentadiene ug/L 37.250 74 10-110ND
Hexachloroethane ug/L 39.850 80 10-110ND
Hexachlorophene ug/L 165 M15003350-150ND
Indeno(1,2,3-cd)pyrene ug/L 40.750 81 20-113ND
Isodrin ug/L 45.850 92 50-150ND
Isophorone ug/L 34.150 68 50-150ND
Isosafrole ug/L 40.950 82 50-150ND
Kepone ug/L 88.3100 88 50-150ND
Methapyrilene ug/L 25.8J50 52 50-150ND
Methyl methanesulfonate ug/L 27.950 56 50-150ND
Methyl parathion ug/L 46.950 94 50-150ND
N-Nitroso-di-n-butylamine ug/L 30.050 60 50-150ND
N-Nitroso-di-n-propylamine ug/L 33.150 66 21-105ND
N-Nitrosodiethylamine ug/L 41.650 83 50-150ND
N-Nitrosodimethylamine ug/L 19.450 39 10-110ND
N-Nitrosodiphenylamine ug/L 39.750 79 23-107ND
N-Nitrosomethylethylamine ug/L 37.550 75 50-150ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1612614MATRIX SPIKE SAMPLE:
MSSpike
Result
92276747001
N-Nitrosopiperidine ug/L 37.150 74 50-150ND
N-Nitrosopyrrolidine ug/L 32.950 66 50-150ND
Nitrobenzene ug/L 34.050 68 20-110ND
O,O,O-Triethylphosphorothioate ug/L 38.750 77 50-150ND
O-Toluidine ug/L 30.250 60 50-150ND
P-Dimethylaminoazobenzene ug/L 21.2 M11002150-150ND
p-Phenylenediamine ug/L 41.550 83 50-150ND
Parathion (Ethyl parathion)ug/L 46.050 92 50-150ND
Pentachlorobenzene ug/L 39.650 79 50-150ND
Pentachloronitrobenzene ug/L 50.350 101 50-150ND
Pentachlorophenol ug/L 73.6250 29 10-118ND
Phenacetin ug/L 47.550 95 50-150ND
Phenanthrene ug/L 42.250 84 24-106ND
Phenol ug/L 14.850 30 12-110ND
Phorate ug/L 62.750 125 50-150ND
Pronamide ug/L 51.250 102 50-150ND
Pyrene ug/L 40.850 82 24-114ND
Safrole ug/L 35.150 70 50-150ND
Thionazin ug/L 42.350 85 50-150ND
2,4,6-Tribromophenol (S)%85 27-110
2-Fluorobiphenyl (S)%78 27-110
2-Fluorophenol (S)%38 12-110
Nitrobenzene-d5 (S)%69 21-110
Phenol-d6 (S)%24 10-110
Terphenyl-d14 (S)%64 31-107
Parameter Units
Dup
Result QualifiersRPDResult
92276747004
1612615SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L NDND
1,3,5-Trinitrobenzene ug/L NDND
1,3-Dinitrobenzene ug/L NDND
1,4-Naphthoquinone ug/L NDND
1-Naphthalenamine ug/L NDND
2,3,4,6-Tetrachlorophenol ug/L NDND
2,4,5-Trichlorophenol ug/L NDND
2,4,6-Trichlorophenol ug/L NDND
2,4-Dichlorophenol ug/L NDND
2,4-Dimethylphenol ug/L NDND
2,4-Dinitrophenol ug/L NDND
2,4-Dinitrotoluene ug/L NDND
2,6-Dichlorophenol ug/L NDND
2,6-Dinitrotoluene ug/L NDND
2-Acetylaminofluorene ug/L NDND
2-Chloronaphthalene ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 184 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276747004
1612615SAMPLE DUPLICATE:
2-Chlorophenol ug/L NDND
2-Methylnaphthalene ug/L NDND
2-Methylphenol(o-Cresol)ug/L NDND
2-Naphthalenamine ug/L NDND
2-Nitroaniline ug/L NDND
2-Nitrophenol ug/L NDND
3&4-Methylphenol(m&p Cresol)ug/L NDND
3,3'-Dichlorobenzidine ug/L NDND
3,3'-Dimethylbenzidine ug/L NDND
3-Methylcholanthrene ug/L NDND
3-Nitroaniline ug/L NDND
4,6-Dinitro-2-methylphenol ug/L NDND
4-Aminobiphenyl ug/L NDND
4-Bromophenylphenyl ether ug/L NDND
4-Chloro-3-methylphenol ug/L NDND
4-Chloroaniline ug/L NDND
4-Chlorophenylphenyl ether ug/L NDND
4-Nitroaniline ug/L NDND
4-Nitrophenol ug/L NDND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L NDND
Acenaphthene ug/L NDND
Acenaphthylene ug/L NDND
Acetophenone ug/L NDND
Anthracene ug/L NDND
Benzo(a)anthracene ug/L NDND
Benzo(a)pyrene ug/L NDND
Benzo(b)fluoranthene ug/L NDND
Benzo(g,h,i)perylene ug/L NDND
Benzo(k)fluoranthene ug/L NDND
Benzyl alcohol ug/L NDND
bis(2-Chloroethoxy)methane ug/L NDND
bis(2-Chloroethyl) ether ug/L NDND
bis(2-Chloroisopropyl) ether ug/L NDND
bis(2-Ethylhexyl)phthalate ug/L NDND
Butylbenzylphthalate ug/L NDND
Chlorobenzilate ug/L NDND
Chrysene ug/L NDND
Di-n-butylphthalate ug/L NDND
Di-n-octylphthalate ug/L NDND
Diallate ug/L NDND
Dibenz(a,h)anthracene ug/L NDND
Dibenzofuran ug/L NDND
Diethylphthalate ug/L NDND
Dimethoate ug/L NDND
Dimethylphthalate ug/L NDND
Diphenylamine ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 185 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276747004
1612615SAMPLE DUPLICATE:
Disulfoton ug/L NDND
Ethyl methanesulfonate ug/L NDND
Famphur ug/L NDND
Fluoranthene ug/L NDND
Fluorene ug/L NDND
Hexachlorobenzene ug/L NDND
Hexachlorocyclopentadiene ug/L NDND
Hexachloroethane ug/L NDND
Hexachlorophene ug/L NDND
Indeno(1,2,3-cd)pyrene ug/L NDND
Isodrin ug/L NDND
Isophorone ug/L NDND
Isosafrole ug/L NDND
Kepone ug/L NDND
Methapyrilene ug/L NDND
Methyl methanesulfonate ug/L NDND
Methyl parathion ug/L NDND
N-Nitroso-di-n-butylamine ug/L NDND
N-Nitroso-di-n-propylamine ug/L NDND
N-Nitrosodiethylamine ug/L NDND
N-Nitrosodimethylamine ug/L NDND
N-Nitrosodiphenylamine ug/L NDND
N-Nitrosomethylethylamine ug/L NDND
N-Nitrosopiperidine ug/L NDND
N-Nitrosopyrrolidine ug/L NDND
Nitrobenzene ug/L NDND
O,O,O-Triethylphosphorothioate ug/L NDND
O-Toluidine ug/L NDND
P-Dimethylaminoazobenzene ug/L NDND
p-Phenylenediamine ug/L NDND
Parathion (Ethyl parathion)ug/L NDND
Pentachlorobenzene ug/L NDND
Pentachloronitrobenzene ug/L NDND
Pentachlorophenol ug/L NDND
Phenacetin ug/L NDND
Phenanthrene ug/L NDND
Phenol ug/L NDND
Phorate ug/L NDND
Pronamide ug/L NDND
Pyrene ug/L NDND
Safrole ug/L NDND
Thionazin ug/L NDND
2,4,6-Tribromophenol (S)%74 1166
2-Fluorobiphenyl (S)%75 1664
2-Fluorophenol (S)%35 1730
Nitrobenzene-d5 (S)%70 1560
Phenol-d6 (S)%22 2418
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 186 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276747004
1612615SAMPLE DUPLICATE:
Terphenyl-d14 (S)%79 873
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 187 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39320
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1615017
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Matrix:Water
Analyzed
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 11/30/15 21:15
1,3,5-Trinitrobenzene ug/L ND 10.0 11/30/15 21:15
1,3-Dinitrobenzene ug/L ND 20.0 11/30/15 21:15
1,4-Naphthoquinone ug/L ND 5.0 11/30/15 21:15
1-Naphthalenamine ug/L ND 5.0 11/30/15 21:15
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 11/29/15 16:27
2,4,5-Trichlorophenol ug/L ND 10.0 11/29/15 16:27
2,4,6-Trichlorophenol ug/L ND 10.0 11/29/15 16:27
2,4-Dichlorophenol ug/L ND 10.0 11/29/15 16:27
2,4-Dimethylphenol ug/L ND 10.0 11/29/15 16:27
2,4-Dinitrophenol ug/L ND 50.0 11/29/15 16:27
2,4-Dinitrotoluene ug/L ND 10.0 11/29/15 16:27
2,6-Dichlorophenol ug/L ND 10.0 11/30/15 21:15
2,6-Dinitrotoluene ug/L ND 10.0 11/29/15 16:27
2-Acetylaminofluorene ug/L ND 20.0 11/30/15 21:15
2-Chloronaphthalene ug/L ND 10.0 11/29/15 16:27
2-Chlorophenol ug/L ND 10.0 11/29/15 16:27
2-Methylnaphthalene ug/L ND 10.0 11/29/15 16:27
2-Methylphenol(o-Cresol)ug/L ND 10.0 11/29/15 16:27
2-Naphthalenamine ug/L ND 5.0 11/30/15 21:15
2-Nitroaniline ug/L ND 50.0 11/29/15 16:27
2-Nitrophenol ug/L ND 10.0 11/29/15 16:27
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 11/29/15 16:27
3,3'-Dichlorobenzidine ug/L ND 20.0 11/29/15 16:27
3,3'-Dimethylbenzidine ug/L ND 10.0 11/30/15 21:15
3-Methylcholanthrene ug/L ND 10.0 11/30/15 21:15
3-Nitroaniline ug/L ND 50.0 11/29/15 16:27
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/29/15 16:27
4-Aminobiphenyl ug/L ND 10.0 11/30/15 21:15
4-Bromophenylphenyl ether ug/L ND 10.0 11/29/15 16:27
4-Chloro-3-methylphenol ug/L ND 20.0 11/29/15 16:27
4-Chloroaniline ug/L ND 20.0 11/29/15 16:27
4-Chlorophenylphenyl ether ug/L ND 10.0 11/29/15 16:27
4-Nitroaniline ug/L ND 20.0 11/29/15 16:27
4-Nitrophenol ug/L ND 50.0 11/29/15 16:27
5-Nitro-o-toluidine ug/L ND 10.0 11/30/15 21:15
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 11/30/15 21:15
Acenaphthene ug/L ND 10.0 11/29/15 16:27
Acenaphthylene ug/L ND 10.0 11/29/15 16:27
Acetophenone ug/L ND 10.0 11/29/15 16:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 188 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1615017
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Matrix:Water
Analyzed
Anthracene ug/L ND 10.0 11/29/15 16:27
Benzo(a)anthracene ug/L ND 10.0 11/29/15 16:27
Benzo(a)pyrene ug/L ND 10.0 11/29/15 16:27
Benzo(b)fluoranthene ug/L ND 10.0 11/29/15 16:27
Benzo(g,h,i)perylene ug/L ND 10.0 11/29/15 16:27
Benzo(k)fluoranthene ug/L ND 10.0 11/29/15 16:27
Benzyl alcohol ug/L ND 20.0 11/29/15 16:27
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/29/15 16:27
bis(2-Chloroethyl) ether ug/L ND 10.0 11/29/15 16:27
bis(2-Chloroisopropyl) ether ug/L ND 10.0 11/29/15 16:27
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/29/15 16:27
Butylbenzylphthalate ug/L ND 10.0 11/29/15 16:27
Chlorobenzilate ug/L ND 10.0 11/30/15 21:15
Chrysene ug/L ND 10.0 11/29/15 16:27
Di-n-butylphthalate ug/L ND 10.0 11/29/15 16:27
Di-n-octylphthalate ug/L ND 10.0 11/29/15 16:27
Diallate ug/L ND 10.0 11/30/15 21:15
Dibenz(a,h)anthracene ug/L ND 10.0 11/29/15 16:27
Dibenzofuran ug/L ND 10.0 11/29/15 16:27
Diethylphthalate ug/L ND 10.0 11/29/15 16:27
Dimethoate ug/L ND 10.0 11/30/15 21:15
Dimethylphthalate ug/L ND 10.0 11/29/15 16:27
Diphenylamine ug/L ND 10.0 11/29/15 16:27
Disulfoton ug/L ND 10.0 11/30/15 21:15
Ethyl methanesulfonate ug/L ND 20.0 11/30/15 21:15
Famphur ug/L ND 10.0 11/30/15 21:15
Fluoranthene ug/L ND 10.0 11/29/15 16:27
Fluorene ug/L ND 10.0 11/29/15 16:27
Hexachlorobenzene ug/L ND 10.0 11/29/15 16:27
Hexachlorocyclopentadiene ug/L ND 10.0 11/29/15 16:27
Hexachloroethane ug/L ND 10.0 11/29/15 16:27
Hexachlorophene ug/L ND 100 11/30/15 21:15
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/29/15 16:27
Isodrin ug/L ND 20.0 11/30/15 21:15
Isophorone ug/L ND 10.0 11/29/15 16:27
Isosafrole ug/L ND 10.0 11/30/15 21:15
Kepone ug/L ND 10.0 11/30/15 21:15
Methapyrilene ug/L ND 50.0 11/30/15 21:15
Methyl methanesulfonate ug/L ND 5.0 11/30/15 21:15
Methyl parathion ug/L ND 10.0 11/30/15 21:15
N-Nitroso-di-n-butylamine ug/L ND 10.0 11/30/15 21:15
N-Nitroso-di-n-propylamine ug/L ND 10.0 11/29/15 16:27
N-Nitrosodiethylamine ug/L ND 20.0 11/30/15 21:15
N-Nitrosodimethylamine ug/L ND 10.0 11/29/15 16:27
N-Nitrosodiphenylamine ug/L ND 10.0 11/29/15 16:27
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 189 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1615017
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019,
92276295020
Matrix:Water
Analyzed
N-Nitrosomethylethylamine ug/L ND 10.0 11/30/15 21:15
N-Nitrosopiperidine ug/L ND 20.0 11/30/15 21:15
N-Nitrosopyrrolidine ug/L ND 10.0 11/30/15 21:15
Nitrobenzene ug/L ND 10.0 11/29/15 16:27
O,O,O-Triethylphosphorothioate ug/L ND 10.0 11/30/15 21:15
O-Toluidine ug/L ND 10.0 11/30/15 21:15
P-Dimethylaminoazobenzene ug/L ND 5.0 11/30/15 21:15
p-Phenylenediamine ug/L ND 10.0 11/30/15 21:15
Parathion (Ethyl parathion)ug/L ND 10.0 11/30/15 21:15
Pentachlorobenzene ug/L ND 10.0 11/30/15 21:15
Pentachloronitrobenzene ug/L ND 20.0 11/30/15 21:15
Pentachlorophenol ug/L ND 25.0 11/29/15 16:27
Phenacetin ug/L ND 20.0 11/30/15 21:15
Phenanthrene ug/L ND 10.0 11/29/15 16:27
Phenol ug/L ND 10.0 11/29/15 16:27
Phorate ug/L ND 10.0 11/30/15 21:15
Pronamide ug/L ND 10.0 11/30/15 21:15
Pyrene ug/L ND 10.0 11/29/15 16:27
Safrole ug/L ND 10.0 11/30/15 21:15
Thionazin ug/L ND 20.0 11/30/15 21:15
2,4,6-Tribromophenol (S)%73 27-110 11/29/15 16:27
2-Fluorobiphenyl (S)%73 27-110 11/29/15 16:27
2-Fluorophenol (S)%35 12-110 11/29/15 16:27
Nitrobenzene-d5 (S)%71 21-110 11/29/15 16:27
Phenol-d6 (S)%23 10-110 11/29/15 16:27
Terphenyl-d14 (S)%93 31-107 11/29/15 16:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1615018LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 32.650 65 16-129
1,3,5-Trinitrobenzene ug/L 63.7 L05012755-125
1,3-Dinitrobenzene ug/L 43.550 87 30-122
1,4-Naphthoquinone ug/L 35.950 72 31-120
1-Naphthalenamine ug/L 31.150 62 37-126
2,3,4,6-Tetrachlorophenol ug/L 77.950 156 54-276
2,4,5-Trichlorophenol ug/L 39.150 78 43-113
2,4,6-Trichlorophenol ug/L 35.350 71 42-120
2,4-Dichlorophenol ug/L 33.550 67 30-120
2,4-Dimethylphenol ug/L 31.750 63 29-111
2,4-Dinitrophenol ug/L 141250 56 19-132
2,4-Dinitrotoluene ug/L 42.150 84 58-128
2,6-Dichlorophenol ug/L 33.150 66 54-128
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 190 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1615018LABORATORY CONTROL SAMPLE:
LCSSpike
2,6-Dinitrotoluene ug/L 42.050 84 54-129
2-Acetylaminofluorene ug/L 39.4 L0507981-160
2-Chloronaphthalene ug/L 45.950 92 43-117
2-Chlorophenol ug/L 28.850 58 37-120
2-Methylnaphthalene ug/L 32.950 66 33-120
2-Methylphenol(o-Cresol)ug/L 27.950 56 31-120
2-Naphthalenamine ug/L 38.150 76 41-136
2-Nitroaniline ug/L 70.1100 70 48-121
2-Nitrophenol ug/L 33.650 67 25-116
3&4-Methylphenol(m&p Cresol)ug/L 21.250 42 23-120
3,3'-Dichlorobenzidine ug/L 74.9250 30 10-154
3,3'-Dimethylbenzidine ug/L 56.9100 57 10-157
3-Methylcholanthrene ug/L 36.850 74 65-130
3-Nitroaniline ug/L 73.8100 74 43-115
4,6-Dinitro-2-methylphenol ug/L 68.9100 69 44-124
4-Aminobiphenyl ug/L 35.150 70 21-125
4-Bromophenylphenyl ether ug/L 36.250 72 34-113
4-Chloro-3-methylphenol ug/L 70.8100 71 31-110
4-Chloroaniline ug/L 60.0100 60 20-120
4-Chlorophenylphenyl ether ug/L 34.550 69 34-116
4-Nitroaniline ug/L 82.9100 83 46-128
4-Nitrophenol ug/L 83.6250 33 11-120
5-Nitro-o-toluidine ug/L 51.050 102 78-160
7,12-Dimethylbenz(a)anthracene ug/L 41.150 82 47-124
Acenaphthene ug/L 38.750 77 48-114
Acenaphthylene ug/L 40.150 80 48-112
Acetophenone ug/L 32.150 64 24-120
Anthracene ug/L 41.950 84 57-118
Benzo(a)anthracene ug/L 40.850 82 56-121
Benzo(a)pyrene ug/L 39.050 78 55-127
Benzo(b)fluoranthene ug/L 39.950 80 53-128
Benzo(g,h,i)perylene ug/L 33.850 68 54-125
Benzo(k)fluoranthene ug/L 49.450 99 51-123
Benzyl alcohol ug/L 51.0100 51 27-120
bis(2-Chloroethoxy)methane ug/L 31.450 63 32-120
bis(2-Chloroethyl) ether ug/L 29.650 59 33-111
bis(2-Chloroisopropyl) ether ug/L 26.350 53 15-120
bis(2-Ethylhexyl)phthalate ug/L 44.450 89 50-145
Butylbenzylphthalate ug/L 46.750 93 54-138
Chlorobenzilate ug/L 47.150 94 65-132
Chrysene ug/L 40.850 82 58-127
Di-n-butylphthalate ug/L 46.350 93 56-125
Di-n-octylphthalate ug/L 36.450 73 50-134
Diallate ug/L 46.950 94 47-123
Dibenz(a,h)anthracene ug/L 35.050 70 53-129
Dibenzofuran ug/L 38.150 76 45-120
Diethylphthalate ug/L 41.350 83 53-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 191 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1615018LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethoate ug/L 43.550 87 57-139
Dimethylphthalate ug/L 39.950 80 55-116
Diphenylamine ug/L 37.750 75 42-120
Disulfoton ug/L 41.050 82 49-156
Ethyl methanesulfonate ug/L 37.750 75 43-120
Famphur ug/L 50.0100 50 40-160
Fluoranthene ug/L 43.450 87 57-125
Fluorene ug/L 41.450 83 53-118
Hexachlorobenzene ug/L 41.250 82 49-116
Hexachlorocyclopentadiene ug/L 28.550 57 26-158
Hexachloroethane ug/L 33.250 66 30-114
Hexachlorophene ug/L 142500 28 10-130
Indeno(1,2,3-cd)pyrene ug/L 34.950 70 55-128
Isodrin ug/L 43.150 86 68-129
Isophorone ug/L 32.850 66 31-118
Isosafrole ug/L 39.050 78 48-107
Kepone ug/L 70.9100 71 10-124
Methapyrilene ug/L 23.9J50 48 40-160
Methyl methanesulfonate ug/L 26.450 53 25-114
Methyl parathion ug/L 45.950 92 58-137
N-Nitroso-di-n-butylamine ug/L 30.150 60 36-115
N-Nitroso-di-n-propylamine ug/L 31.350 63 32-119
N-Nitrosodiethylamine ug/L 41.050 82 47-115
N-Nitrosodimethylamine ug/L 19.350 39 13-120
N-Nitrosodiphenylamine ug/L 37.750 75 43-120
N-Nitrosomethylethylamine ug/L 35.150 70 39-120
N-Nitrosopiperidine ug/L 33.350 67 43-113
N-Nitrosopyrrolidine ug/L 41.350 83 32-110
Nitrobenzene ug/L 32.450 65 33-110
O,O,O-Triethylphosphorothioate ug/L 30.150 60 51-127
O-Toluidine ug/L 33.150 66 27-120
P-Dimethylaminoazobenzene ug/L 22.3100 22 10-120
p-Phenylenediamine ug/L 43.850 88 72-143
Parathion (Ethyl parathion)ug/L 44.750 89 56-140
Pentachlorobenzene ug/L 37.150 74 30-137
Pentachloronitrobenzene ug/L 48.750 97 70-124
Pentachlorophenol ug/L 66.0250 26 10-137
Phenacetin ug/L 47.750 95 60-130
Phenanthrene ug/L 38.550 77 57-117
Phenol ug/L 14.150 28 10-120
Phorate ug/L 63.050 126 55-126
Pronamide ug/L 50.650 101 75-124
Pyrene ug/L 43.650 87 55-122
Safrole ug/L 31.850 64 41-120
Thionazin ug/L 43.550 87 63-137
2,4,6-Tribromophenol (S)%80 27-110
2-Fluorobiphenyl (S)%70 27-110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 192 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1615018LABORATORY CONTROL SAMPLE:
LCSSpike
2-Fluorophenol (S)%36 12-110
Nitrobenzene-d5 (S)%68 21-110
Phenol-d6 (S)%24 10-110
Terphenyl-d14 (S)%80 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1615019MATRIX SPIKE SAMPLE:
MSSpike
Result
92276295012
1,2,4,5-Tetrachlorobenzene ug/L 39.850 80 50-150ND
1,3,5-Trinitrobenzene ug/L 73.950 148 50-150ND
1,3-Dinitrobenzene ug/L 49.250 98 50-150ND
1,4-Naphthoquinone ug/L 39.950 80 50-150ND
1-Naphthalenamine ug/L 27.350 55 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 94.9 M15019050-150ND
2,4,5-Trichlorophenol ug/L 47.050 94 19-105ND
2,4,6-Trichlorophenol ug/L 44.850 90 13-108ND
2,4-Dichlorophenol ug/L 41.550 83 29-111ND
2,4-Dimethylphenol ug/L 38.550 77 21-103ND
2,4-Dinitrophenol ug/L 216250 87 10-109ND
2,4-Dinitrotoluene ug/L 49.750 88 27-1045.9J
2,6-Dichlorophenol ug/L 38.050 76 50-150ND
2,6-Dinitrotoluene ug/L 49.950 84 28-1018.1J
2-Acetylaminofluorene ug/L 46.650 93 50-150ND
2-Chloronaphthalene ug/L 50.850 102 14-102ND
2-Chlorophenol ug/L 35.350 71 16-110ND
2-Methylnaphthalene ug/L 38.950 78 13-110ND
2-Methylphenol(o-Cresol)ug/L 36.950 74 19-110ND
2-Naphthalenamine ug/L 27.650 55 50-150ND
2-Nitroaniline ug/L 84.1100 84 26-103ND
2-Nitrophenol ug/L 41.650 83 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 65.6 M15013120-110ND
3,3'-Dichlorobenzidine ug/L 57.8 M12502325-112ND
3,3'-Dimethylbenzidine ug/L 2.7J M1100350-150ND
3-Methylcholanthrene ug/L 47.050 94 50-150ND
3-Nitroaniline ug/L 86.6100 87 29-110ND
4,6-Dinitro-2-methylphenol ug/L 95.5100 95 10-117ND
4-Aminobiphenyl ug/L 34.950 70 50-150ND
4-Bromophenylphenyl ether ug/L 43.950 88 20-105ND
4-Chloro-3-methylphenol ug/L 85.3100 85 22-110ND
4-Chloroaniline ug/L 66.0100 66 20-100ND
4-Chlorophenylphenyl ether ug/L 40.350 81 19-102ND
4-Nitroaniline ug/L 95.1100 95 29-110ND
4-Nitrophenol ug/L 121250 48 10-110ND
5-Nitro-o-toluidine ug/L 53.650 107 50-150ND
7,12-Dimethylbenz(a)anthracene ug/L 51.850 104 50-150ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Page 193 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1615019MATRIX SPIKE SAMPLE:
MSSpike
Result
92276295012
Acenaphthene ug/L 47.050 94 17-100ND
Acenaphthylene ug/L 48.750 97 21-100ND
Acetophenone ug/L 38.950 78 50-150ND
Anthracene ug/L 51.050 102 24-109ND
Benzo(a)anthracene ug/L 49.250 98 22-117ND
Benzo(a)pyrene ug/L 51.050 102 23-104ND
Benzo(b)fluoranthene ug/L 52.6 M15010523-103ND
Benzo(g,h,i)perylene ug/L 42.150 84 18-111ND
Benzo(k)fluoranthene ug/L 61.4 M15012322-113ND
Benzyl alcohol ug/L 65.7100 66 19-101ND
bis(2-Chloroethoxy)methane ug/L 36.650 73 22-110ND
bis(2-Chloroethyl) ether ug/L 35.050 70 16-110ND
bis(2-Chloroisopropyl) ether ug/L 31.650 63 14-110ND
bis(2-Ethylhexyl)phthalate ug/L 55.9 M15011223-102ND
Butylbenzylphthalate ug/L 58.3 M15011725-110ND
Chlorobenzilate ug/L 54.850 110 50-150ND
Chrysene ug/L 48.850 98 23-115ND
Di-n-butylphthalate ug/L 56.9 M15011426-110ND
Di-n-octylphthalate ug/L 47.050 94 22-110ND
Diallate ug/L 55.150 110 50-150ND
Dibenz(a,h)anthracene ug/L 43.350 87 21-112ND
Dibenzofuran ug/L 45.250 90 19-102ND
Diethylphthalate ug/L 48.450 97 29-110ND
Dimethoate ug/L 52.450 105 50-150ND
Dimethylphthalate ug/L 46.050 92 27-110ND
Diphenylamine ug/L 46.350 93 50-150ND
Disulfoton ug/L 48.750 96 50-150ND
Ethyl methanesulfonate ug/L 43.050 86 50-150ND
Famphur ug/L 66.2100 66 50-150ND
Fluoranthene ug/L 51.850 104 23-112ND
Fluorene ug/L 49.150 98 22-104ND
Hexachlorobenzene ug/L 48.750 97 21-116ND
Hexachlorocyclopentadiene ug/L 33.650 67 10-110ND
Hexachloroethane ug/L 41.450 83 10-110ND
Hexachlorophene ug/L 237 M15004750-150ND
Indeno(1,2,3-cd)pyrene ug/L 43.250 86 20-113ND
Isodrin ug/L 50.050 100 50-150ND
Isophorone ug/L 38.350 77 50-150ND
Isosafrole ug/L 46.650 93 50-150ND
Kepone ug/L 67.8100 68 50-150ND
Methapyrilene ug/L 27.3J50 55 50-150ND
Methyl methanesulfonate ug/L 31.650 63 50-150ND
Methyl parathion ug/L 53.650 107 50-150ND
N-Nitroso-di-n-butylamine ug/L 32.950 66 50-150ND
N-Nitroso-di-n-propylamine ug/L 39.450 79 21-105ND
N-Nitrosodiethylamine ug/L 47.750 95 50-150ND
N-Nitrosodimethylamine ug/L 24.850 50 10-110ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 194 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1615019MATRIX SPIKE SAMPLE:
MSSpike
Result
92276295012
N-Nitrosodiphenylamine ug/L 46.350 93 23-107ND
N-Nitrosomethylethylamine ug/L 44.250 88 50-150ND
N-Nitrosopiperidine ug/L 37.750 75 50-150ND
N-Nitrosopyrrolidine ug/L 46.850 94 50-150ND
Nitrobenzene ug/L 37.750 75 20-110ND
O,O,O-Triethylphosphorothioate ug/L 34.950 70 50-150ND
O-Toluidine ug/L 35.350 71 50-150ND
P-Dimethylaminoazobenzene ug/L 25.2 M11002550-150ND
p-Phenylenediamine ug/L 45.550 91 50-150ND
Parathion (Ethyl parathion)ug/L 51.750 103 50-150ND
Pentachlorobenzene ug/L 42.150 84 50-150ND
Pentachloronitrobenzene ug/L 57.450 115 50-150ND
Pentachlorophenol ug/L 95.0250 38 10-118ND
Phenacetin ug/L 58.050 116 50-150ND
Phenanthrene ug/L 46.850 94 24-106ND
Phenol ug/L 18.350 37 12-110ND
Phorate ug/L 73.150 146 50-150ND
Pronamide ug/L 57.850 115 50-150ND
Pyrene ug/L 54.350 109 24-114ND
Safrole ug/L 35.350 71 50-150ND
Thionazin ug/L 49.850 100 50-150ND
2,4,6-Tribromophenol (S)%96 27-110
2-Fluorobiphenyl (S)%83 27-110
2-Fluorophenol (S)%45 12-110
Nitrobenzene-d5 (S)%78 21-110
Phenol-d6 (S)%32 10-110
Terphenyl-d14 (S)%73 31-107
Parameter Units
Dup
Result QualifiersRPDResult
92276295013
1615020SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L NDND
1,3,5-Trinitrobenzene ug/L NDND
1,3-Dinitrobenzene ug/L NDND
1,4-Naphthoquinone ug/L NDND
1-Naphthalenamine ug/L NDND
2,3,4,6-Tetrachlorophenol ug/L NDND
2,4,5-Trichlorophenol ug/L NDND
2,4,6-Trichlorophenol ug/L NDND
2,4-Dichlorophenol ug/L NDND
2,4-Dimethylphenol ug/L NDND
2,4-Dinitrophenol ug/L NDND
2,4-Dinitrotoluene ug/L NDND
2,6-Dichlorophenol ug/L NDND
2,6-Dinitrotoluene ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 195 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276295013
1615020SAMPLE DUPLICATE:
2-Acetylaminofluorene ug/L NDND
2-Chloronaphthalene ug/L NDND
2-Chlorophenol ug/L NDND
2-Methylnaphthalene ug/L NDND
2-Methylphenol(o-Cresol)ug/L NDND
2-Naphthalenamine ug/L NDND
2-Nitroaniline ug/L NDND
2-Nitrophenol ug/L NDND
3&4-Methylphenol(m&p Cresol)ug/L NDND
3,3'-Dichlorobenzidine ug/L NDND
3,3'-Dimethylbenzidine ug/L NDND
3-Methylcholanthrene ug/L NDND
3-Nitroaniline ug/L NDND
4,6-Dinitro-2-methylphenol ug/L NDND
4-Aminobiphenyl ug/L NDND
4-Bromophenylphenyl ether ug/L NDND
4-Chloro-3-methylphenol ug/L NDND
4-Chloroaniline ug/L NDND
4-Chlorophenylphenyl ether ug/L NDND
4-Nitroaniline ug/L NDND
4-Nitrophenol ug/L NDND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L NDND
Acenaphthene ug/L NDND
Acenaphthylene ug/L NDND
Acetophenone ug/L NDND
Anthracene ug/L NDND
Benzo(a)anthracene ug/L NDND
Benzo(a)pyrene ug/L NDND
Benzo(b)fluoranthene ug/L NDND
Benzo(g,h,i)perylene ug/L NDND
Benzo(k)fluoranthene ug/L NDND
Benzyl alcohol ug/L NDND
bis(2-Chloroethoxy)methane ug/L NDND
bis(2-Chloroethyl) ether ug/L NDND
bis(2-Chloroisopropyl) ether ug/L NDND
bis(2-Ethylhexyl)phthalate ug/L NDND
Butylbenzylphthalate ug/L NDND
Chlorobenzilate ug/L NDND
Chrysene ug/L NDND
Di-n-butylphthalate ug/L NDND
Di-n-octylphthalate ug/L ND5.6J
Diallate ug/L NDND
Dibenz(a,h)anthracene ug/L NDND
Dibenzofuran ug/L NDND
Diethylphthalate ug/L NDND
Dimethoate ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 196 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276295013
1615020SAMPLE DUPLICATE:
Dimethylphthalate ug/L NDND
Diphenylamine ug/L NDND
Disulfoton ug/L NDND
Ethyl methanesulfonate ug/L NDND
Famphur ug/L NDND
Fluoranthene ug/L NDND
Fluorene ug/L NDND
Hexachlorobenzene ug/L NDND
Hexachlorocyclopentadiene ug/L NDND
Hexachloroethane ug/L NDND
Hexachlorophene ug/L NDND
Indeno(1,2,3-cd)pyrene ug/L NDND
Isodrin ug/L NDND
Isophorone ug/L NDND
Isosafrole ug/L NDND
Kepone ug/L NDND
Methapyrilene ug/L NDND
Methyl methanesulfonate ug/L NDND
Methyl parathion ug/L NDND
N-Nitroso-di-n-butylamine ug/L NDND
N-Nitroso-di-n-propylamine ug/L NDND
N-Nitrosodiethylamine ug/L NDND
N-Nitrosodimethylamine ug/L NDND
N-Nitrosodiphenylamine ug/L NDND
N-Nitrosomethylethylamine ug/L NDND
N-Nitrosopiperidine ug/L NDND
N-Nitrosopyrrolidine ug/L NDND
Nitrobenzene ug/L NDND
O,O,O-Triethylphosphorothioate ug/L NDND
O-Toluidine ug/L NDND
P-Dimethylaminoazobenzene ug/L NDND
p-Phenylenediamine ug/L NDND
Parathion (Ethyl parathion)ug/L NDND
Pentachlorobenzene ug/L NDND
Pentachloronitrobenzene ug/L NDND
Pentachlorophenol ug/L NDND
Phenacetin ug/L NDND
Phenanthrene ug/L NDND
Phenol ug/L NDND
Phorate ug/L NDND
Pronamide ug/L NDND
Pyrene ug/L NDND
Safrole ug/L NDND
Thionazin ug/L NDND
2,4,6-Tribromophenol (S)%87 484
2-Fluorobiphenyl (S)%86 1474
2-Fluorophenol (S)%40 1335
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 197 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276295013
1615020SAMPLE DUPLICATE:
Nitrobenzene-d5 (S)%83 1175
Phenol-d6 (S)%25 723
Terphenyl-d14 (S)%93 292
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
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Huntersville, NC 28078
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Page 198 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41581
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92276295001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1613709
Associated Lab Samples:92276295001
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 11/24/15 15:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613710LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 5040050000 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613711MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276764001
1613712
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M150000102080-1201030 150000311
mg/L 818000 826000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613738MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276984001
1613739
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500007280-12085 350000172
mg/L 208000 214000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 199 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41582
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92276295002, 92276295003, 92276295004, 92276295005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1613715
Associated Lab Samples:92276295002, 92276295003, 92276295004, 92276295005
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 11/24/15 20:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613716LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 5000050000 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613717MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276295002
1613718
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1,R1500009480-12085 550000432009000085700
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 200 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41638
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616021
Associated Lab Samples:92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 11/29/15 12:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616022LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4910050000 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616023MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277024001
1616024
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 102 80-12097 35000047.9
mg/L 99100 96400
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616025MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276534009
1616026
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 95 80-12092 050000274
mg/L 322000 320000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 201 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41641
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616045
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 11/29/15 19:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616046LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4980050000 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616047MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276524004
1616048
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 101 80-120101 1500008.7
mg/L 59400 59000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616049MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276855003
1616050
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 101 80-120100 1500009.3
mg/L 59700 59200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 202 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41659
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92276295018, 92276295019, 92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616790
Associated Lab Samples:92276295018, 92276295019, 92276295020
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 12/01/15 14:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616791LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4990050000 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616792MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277119005
1616793
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 100 80-120100 050000ND5070050600
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616798MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277515002
1616799
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 98 80-120103 25000070.3
mg/L 119000 122000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 203 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41465
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609584
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Matrix:Water
Analyzed
Total Dissolved Solids ug/L ND 25000 11/18/15 14:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609585LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 244000250000 98 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92276182001
1609586SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 169000 0169 mg/L
Parameter Units
Dup
Result QualifiersRPDResult
92276405002
1609587SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 387000 D663202 mg/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 204 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41488
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1610306
Associated Lab Samples:92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
Total Dissolved Solids ug/L ND 25000 11/19/15 10:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1610307LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 236000250000 94 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92276498005
1610308SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 94000 D610629.0 mg/L
Parameter Units
Dup
Result QualifiersRPDResult
92276513004
1610309SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 132000 D618110 mg/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 205 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41557
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1612809
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Matrix:Water
Analyzed
Total Dissolved Solids ug/L ND 25000 11/22/15 11:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612810LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 250000250000 100 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92276728003
1612811SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 136000 D612120 mg/L
Parameter Units
Dup
Result QualifiersRPDResult
92276295015
1612812SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 283000 1281000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 206 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41589
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92276295018, 92276295019, 92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1613762
Associated Lab Samples:92276295018, 92276295019, 92276295020
Matrix:Water
Analyzed
Total Dissolved Solids ug/L ND 25000 11/24/15 16:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613763LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 131000125000 105 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92276570001
1613764SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 218000 0217 mg/L
Parameter Units
Dup
Result QualifiersRPDResult
92277140006
1613765SAMPLE DUPLICATE:
Total Dissolved Solids ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 207 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41472
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609858
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Matrix:Water
Analyzed
Sulfide ug/L ND 100 11/18/15 17:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609859LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 485500 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1609860MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276433001
1609861
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 100 90-110100 0500ND499499
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1609862MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276295005
1609863
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 99 90-11099 0500ND493493
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 208 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41513
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1611295
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
Sulfide ug/L ND 100 11/19/15 23:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1611296LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 499500 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1611297MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276507001
1611298
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 101 90-110101 0500ND505505
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1611299MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276443002
1611300
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 95 90-11095 0500ND474474
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 209 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41571
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1613121
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018, 92276295019
Matrix:Water
Analyzed
Sulfide ug/L ND 100 11/23/15 23:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613122LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 511500 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613123MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276764001
1613124
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 96 90-11096 0500ND479479
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613125MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276295016
1613126
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 92 90-11092 0500ND460460
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 210 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41615
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1615410
Associated Lab Samples:92276295020
Matrix:Water
Analyzed
Sulfide ug/L ND 100 11/25/15 17:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1615411LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 514500 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1615412MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277023002
1615413
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 96 90-11096 0500ND480480
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1615414MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277119010
1615415
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L M15005790-11057 0500ND356356
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 211 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25452
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609094
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Matrix:Water
Analyzed
Sulfate ug/L ND 2000 11/18/15 11:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609095LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 1870020000 93 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1609096MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276097013
1609097
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 20000 99 90-11098 020000ND1970019700
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 212 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25522
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92276295007, 92276295008, 92276295009, 92276295010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1613692
Associated Lab Samples:92276295007, 92276295008, 92276295009, 92276295010
Matrix:Water
Analyzed
Sulfate ug/L ND 2000 11/24/15 13:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613693LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 1940020000 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613694MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276750001
1613695
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M6200004090-11040 020000313
mg/L 321000 321000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613696MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276750011
1613697
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M1200007990-11081 12000045.1
mg/L 61000 61400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 213 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25523
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92276295011, 92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018,
92276295019, 92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1613698
Associated Lab Samples:92276295011, 92276295012, 92276295013, 92276295014, 92276295015, 92276295016, 92276295018,
92276295019, 92276295020
Matrix:Water
Analyzed
Sulfate ug/L ND 2000 11/24/15 19:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613699LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 1890020000 95 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613700MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276295011
1613701
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M1200006390-11060 120000700008260082000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613702MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276295014
1613703
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M1200006690-11069 120000636007680077500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 214 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25476
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005, 92276295007, 92276295008,
92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1611074
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005, 92276295007, 92276295008,
92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
Chloride ug/L ND 1000 11/19/15 18:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1611075LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2010020000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1611076MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276097024
1611077
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 600000 99 90-11099 0600000236
mg/L 828000 827000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1611078MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276097025
1611079
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 20000 102 90-110102 0200003.7
mg/L 24000 24000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 215 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25570
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616551
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015
Matrix:Water
Analyzed
Chloride ug/L ND 1000 11/30/15 18:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616552LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 1950020000 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616553MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276538002
1616554
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 20000 101 90-11099 12000014.0
mg/L 34100 33800
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616555MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276534008
1616556
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 200000 95 90-11093 120000090.7
mg/L 280000 276000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 216 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25594
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92276295016, 92276295018, 92276295019, 92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617466
Associated Lab Samples:92276295016, 92276295018, 92276295019, 92276295020
Matrix:Water
Analyzed
Chloride ug/L ND 1000 12/01/15 22:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617467LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 1970020000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617468MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277478001
1617469
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 80000 101 90-110101 08000036.0
mg/L 117000 117000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617470MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277478002
1617471
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 100000 90 90-11090 010000070.6
mg/L 161000 160000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 217 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25449
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609000
Associated Lab Samples:92276295001, 92276295002, 92276295003, 92276295004, 92276295005
Matrix:Water
Analyzed
Cyanide ug/L ND 8.0 11/18/15 22:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609001LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 119100 119 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1609002MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275034002
1609003
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L R110010275-125117 13100ND105120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 218 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25466
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1610191
Associated Lab Samples:92276295006, 92276295007, 92276295008, 92276295009, 92276295010, 92276295011
Matrix:Water
Analyzed
Cyanide ug/L ND 8.0 11/19/15 04:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1610192LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 111100 111 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1610193MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276650003
1610194
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 100 103 75-12598 4100ND105100
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1610195MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276295009
1610196
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 100 101 75-125100 1100ND103101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 219 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25510
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1613285
Associated Lab Samples:92276295012, 92276295013, 92276295014, 92276295015, 92276295016
Matrix:Water
Analyzed
Cyanide ug/L ND 8.0 11/25/15 03:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613286LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 97.4100 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613287MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276911005
1613288
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 200 77 75-12581 5200ND161170
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613289MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276893002
1613290
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L M12007575-12572 4200ND157151
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 220 of 265
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276295
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25511
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92276295018, 92276295019, 92276295020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1613329
Associated Lab Samples:92276295018, 92276295019, 92276295020
Matrix:Water
Analyzed
Cyanide ug/L ND 8.0 11/25/15 03:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1613330LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 115100 115 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613331MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276889005
1613332
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L M12006575-12568 5200ND137144
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1613658MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277122001
1613659
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L M12005675-12552 520063.7 176 168
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 221 of 265
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92276295
OSR
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 222 of 265
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92276295001 FLD/3412-SW1
92276295002 FLD/3412-SW2
92276295003 FLD/3412-SW3
92276295004 FLD/3412-SW4
92276295005 FLD/3412-MW3R
92276295007 FLD/3412-MW4R
92276295008 FLD/3412-MW7
92276295009 FLD/3412-MW5R
92276295010 FLD/3412-MW1R
92276295011 FLD/3412-MW15
92276295012 FLD/3412-MW2R
92276295013 FLD/3412-MW8
92276295014 FLD/3412-MW10
92276295015 FLD/3412-MW11
92276295016 FLD/3412-MW12
92276295018 FLD/3412-MW9
92276295019 FLD/3412-MW13
92276295020 FLD/3412-MW14
92280822001 FLD/3412-MW3R
92276295005 OEXT/39187 GCSV/232783412-MW3R EPA 3510 EPA 8081
92276295006 OEXT/39187 GCSV/232783412-EQUIPMENT BLANK EPA 3510 EPA 8081
92276295007 OEXT/39187 GCSV/232783412-MW4R EPA 3510 EPA 8081
92276295008 OEXT/39187 GCSV/232783412-MW7 EPA 3510 EPA 8081
92276295009 OEXT/39187 GCSV/232783412-MW5R EPA 3510 EPA 8081
92276295010 OEXT/39187 GCSV/232783412-MW1R EPA 3510 EPA 8081
92276295011 OEXT/39187 GCSV/232783412-MW15 EPA 3510 EPA 8081
92276295012 OEXT/39285 GCSV/233343412-MW2R EPA 3510 EPA 8081
92276295013 OEXT/39285 GCSV/233343412-MW8 EPA 3510 EPA 8081
92276295014 OEXT/39285 GCSV/233343412-MW10 EPA 3510 EPA 8081
92276295015 OEXT/39285 GCSV/233343412-MW11 EPA 3510 EPA 8081
92276295016 OEXT/39285 GCSV/233343412-MW12 EPA 3510 EPA 8081
92276295018 OEXT/39285 GCSV/233343412-MW9 EPA 3510 EPA 8081
92276295019 OEXT/39285 GCSV/233343412-MW13 EPA 3510 EPA 8081
92276295020 OEXT/39285 GCSV/233343412-MW14 EPA 3510 EPA 8081
92276295005 OEXT/39186 GCSV/232773412-MW3R EPA 3510 EPA 8082
92276295006 OEXT/39186 GCSV/232773412-EQUIPMENT BLANK EPA 3510 EPA 8082
92276295007 OEXT/39186 GCSV/232773412-MW4R EPA 3510 EPA 8082
92276295008 OEXT/39186 GCSV/232773412-MW7 EPA 3510 EPA 8082
92276295009 OEXT/39186 GCSV/232773412-MW5R EPA 3510 EPA 8082
92276295010 OEXT/39186 GCSV/232773412-MW1R EPA 3510 EPA 8082
92276295011 OEXT/39186 GCSV/232773412-MW15 EPA 3510 EPA 8082
92276295012 OEXT/39292 GCSV/233363412-MW2R EPA 3510 EPA 8082
92276295013 OEXT/39292 GCSV/233363412-MW8 EPA 3510 EPA 8082
92276295014 OEXT/39292 GCSV/233363412-MW10 EPA 3510 EPA 8082
92276295015 OEXT/39292 GCSV/233363412-MW11 EPA 3510 EPA 8082
92276295016 OEXT/39292 GCSV/233363412-MW12 EPA 3510 EPA 8082
92276295018 OEXT/39292 GCSV/233363412-MW9 EPA 3510 EPA 8082
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 223 of 265
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92276295019 OEXT/39292 GCSV/233363412-MW13 EPA 3510 EPA 8082
92276295020 OEXT/39292 GCSV/233363412-MW14 EPA 3510 EPA 8082
92276295006 OEXT/25403 GCSV/165343412-EQUIPMENT BLANK EPA 8151 EPA 8151
92276295007 OEXT/25401 GCSV/165313412-MW4R EPA 8151 EPA 8151
92276295008 OEXT/25403 GCSV/165343412-MW7 EPA 8151 EPA 8151
92276295009 OEXT/25403 GCSV/165343412-MW5R EPA 8151 EPA 8151
92276295010 OEXT/25403 GCSV/165343412-MW1R EPA 8151 EPA 8151
92276295011 OEXT/25403 GCSV/165343412-MW15 EPA 8151 EPA 8151
92276295012 OEXT/25425 GCSV/165533412-MW2R EPA 8151 EPA 8151
92276295013 OEXT/25425 GCSV/165533412-MW8 EPA 8151 EPA 8151
92276295014 OEXT/25425 GCSV/165533412-MW10 EPA 8151 EPA 8151
92276295015 OEXT/25425 GCSV/165533412-MW11 EPA 8151 EPA 8151
92276295016 OEXT/25425 GCSV/165533412-MW12 EPA 8151 EPA 8151
92276295018 OEXT/25425 GCSV/165533412-MW9 EPA 8151 EPA 8151
92276295019 OEXT/25425 GCSV/165533412-MW13 EPA 8151 EPA 8151
92276295020 OEXT/25425 GCSV/165533412-MW14 EPA 8151 EPA 8151
92280822001 OEXT/25834 GCSV/168153412-MW3R EPA 8151 EPA 8151
92276295001 MPRP/20064 ICP/180963412-SW1 EPA 3010A EPA 6010
92276295002 MPRP/20064 ICP/180963412-SW2 EPA 3010A EPA 6010
92276295003 MPRP/20064 ICP/180963412-SW3 EPA 3010A EPA 6010
92276295004 MPRP/20064 ICP/180963412-SW4 EPA 3010A EPA 6010
92276295005 MPRP/20064 ICP/180963412-MW3R EPA 3010A EPA 6010
92276295006 MPRP/20085 ICP/181193412-EQUIPMENT BLANK EPA 3010A EPA 6010
92276295007 MPRP/20085 ICP/181193412-MW4R EPA 3010A EPA 6010
92276295008 MPRP/20085 ICP/181193412-MW7 EPA 3010A EPA 6010
92276295009 MPRP/20122 ICP/181513412-MW5R EPA 3010A EPA 6010
92276295010 MPRP/20085 ICP/181193412-MW1R EPA 3010A EPA 6010
92276295011 MPRP/20085 ICP/181193412-MW15 EPA 3010A EPA 6010
92276295012 MPRP/20085 ICP/181193412-MW2R EPA 3010A EPA 6010
92276295013 MPRP/20085 ICP/181193412-MW8 EPA 3010A EPA 6010
92276295014 MPRP/20085 ICP/181193412-MW10 EPA 3010A EPA 6010
92276295015 MPRP/20153 ICP/181803412-MW11 EPA 3010A EPA 6010
92276295016 MPRP/20122 ICP/181513412-MW12 EPA 3010A EPA 6010
92276295018 MPRP/20122 ICP/181513412-MW9 EPA 3010A EPA 6010
92276295019 MPRP/20122 ICP/181513412-MW13 EPA 3010A EPA 6010
92276295020 MPRP/20122 ICP/181513412-MW14 EPA 3010A EPA 6010
92276295001 MERP/8709 MERC/83693412-SW1 EPA 7470 EPA 7470
92276295002 MERP/8709 MERC/83693412-SW2 EPA 7470 EPA 7470
92276295003 MERP/8709 MERC/83693412-SW3 EPA 7470 EPA 7470
92276295004 MERP/8709 MERC/83693412-SW4 EPA 7470 EPA 7470
92276295005 MERP/8709 MERC/83693412-MW3R EPA 7470 EPA 7470
92276295006 MERP/8709 MERC/83693412-EQUIPMENT BLANK EPA 7470 EPA 7470
92276295007 MERP/8709 MERC/83693412-MW4R EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 224 of 265
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92276295008 MERP/8709 MERC/83693412-MW7 EPA 7470 EPA 7470
92276295009 MERP/8709 MERC/83693412-MW5R EPA 7470 EPA 7470
92276295010 MERP/8709 MERC/83693412-MW1R EPA 7470 EPA 7470
92276295011 MERP/8709 MERC/83693412-MW15 EPA 7470 EPA 7470
92276295012 MERP/8711 MERC/83703412-MW2R EPA 7470 EPA 7470
92276295013 MERP/8711 MERC/83703412-MW8 EPA 7470 EPA 7470
92276295014 MERP/8711 MERC/83703412-MW10 EPA 7470 EPA 7470
92276295015 MERP/8711 MERC/83703412-MW11 EPA 7470 EPA 7470
92276295016 MERP/8711 MERC/83703412-MW12 EPA 7470 EPA 7470
92276295018 MERP/8712 MERC/83713412-MW9 EPA 7470 EPA 7470
92276295019 MERP/8712 MERC/83713412-MW13 EPA 7470 EPA 7470
92276295020 MERP/8712 MERC/83713412-MW14 EPA 7470 EPA 7470
92276295005 OEXT/39107 MSSV/115433412-MW3R EPA 3510 EPA 8270
92276295006 OEXT/39238 MSSV/115583412-EQUIPMENT BLANK EPA 3510 EPA 8270
92276295007 OEXT/39238 MSSV/115583412-MW4R EPA 3510 EPA 8270
92276295008 OEXT/39238 MSSV/115583412-MW7 EPA 3510 EPA 8270
92276295009 OEXT/39238 MSSV/115583412-MW5R EPA 3510 EPA 8270
92276295010 OEXT/39238 MSSV/115583412-MW1R EPA 3510 EPA 8270
92276295011 OEXT/39238 MSSV/115583412-MW15 EPA 3510 EPA 8270
92276295012 OEXT/39320 MSSV/115723412-MW2R EPA 3510 EPA 8270
92276295013 OEXT/39320 MSSV/115723412-MW8 EPA 3510 EPA 8270
92276295014 OEXT/39320 MSSV/115723412-MW10 EPA 3510 EPA 8270
92276295015 OEXT/39320 MSSV/115723412-MW11 EPA 3510 EPA 8270
92276295016 OEXT/39320 MSSV/115723412-MW12 EPA 3510 EPA 8270
92276295018 OEXT/39320 MSSV/115723412-MW9 EPA 3510 EPA 8270
92276295019 OEXT/39320 MSSV/115723412-MW13 EPA 3510 EPA 8270
92276295020 OEXT/39320 MSSV/115723412-MW14 EPA 3510 EPA 8270
92276295001 MSV/343613412-SW1 EPA 8260
92276295002 MSV/343613412-SW2 EPA 8260
92276295003 MSV/343613412-SW3 EPA 8260
92276295004 MSV/343613412-SW4 EPA 8260
92276295005 MSV/343613412-MW3R EPA 8260
92276295006 MSV/343613412-EQUIPMENT BLANK EPA 8260
92276295007 MSV/343613412-MW4R EPA 8260
92276295008 MSV/343613412-MW7 EPA 8260
92276295009 MSV/343613412-MW5R EPA 8260
92276295010 MSV/343643412-MW1R EPA 8260
92276295011 MSV/343643412-MW15 EPA 8260
92276295012 MSV/343643412-MW2R EPA 8260
92276295013 MSV/343643412-MW8 EPA 8260
92276295014 MSV/343643412-MW10 EPA 8260
92276295015 MSV/343643412-MW11 EPA 8260
92276295016 MSV/343643412-MW12 EPA 8260
92276295017 MSV/343793412-TRIP BLANK EPA 8260
92276295018 MSV/343793412-MW9 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 225 of 265
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92276295019 MSV/343793412-MW13 EPA 8260
92276295020 MSV/343793412-MW14 EPA 8260
92276295001 WET/415813412-SW1 SM 2320B
92276295002 WET/415823412-SW2 SM 2320B
92276295003 WET/415823412-SW3 SM 2320B
92276295004 WET/415823412-SW4 SM 2320B
92276295005 WET/415823412-MW3R SM 2320B
92276295007 WET/416383412-MW4R SM 2320B
92276295008 WET/416383412-MW7 SM 2320B
92276295009 WET/416383412-MW5R SM 2320B
92276295010 WET/416383412-MW1R SM 2320B
92276295011 WET/416383412-MW15 SM 2320B
92276295012 WET/416413412-MW2R SM 2320B
92276295013 WET/416413412-MW8 SM 2320B
92276295014 WET/416413412-MW10 SM 2320B
92276295015 WET/416413412-MW11 SM 2320B
92276295016 WET/416413412-MW12 SM 2320B
92276295018 WET/416593412-MW9 SM 2320B
92276295019 WET/416593412-MW13 SM 2320B
92276295020 WET/416593412-MW14 SM 2320B
92276295001 WET/414653412-SW1 SM 2540C
92276295002 WET/414653412-SW2 SM 2540C
92276295003 WET/414653412-SW3 SM 2540C
92276295004 WET/414653412-SW4 SM 2540C
92276295005 WET/414653412-MW3R SM 2540C
92276295007 WET/414883412-MW4R SM 2540C
92276295008 WET/414883412-MW7 SM 2540C
92276295009 WET/414883412-MW5R SM 2540C
92276295010 WET/414883412-MW1R SM 2540C
92276295011 WET/414883412-MW15 SM 2540C
92276295012 WET/415573412-MW2R SM 2540C
92276295013 WET/415573412-MW8 SM 2540C
92276295014 WET/415573412-MW10 SM 2540C
92276295015 WET/415573412-MW11 SM 2540C
92276295016 WET/415573412-MW12 SM 2540C
92276295018 WET/415893412-MW9 SM 2540C
92276295019 WET/415893412-MW13 SM 2540C
92276295020 WET/415893412-MW14 SM 2540C
92276295001 WET/414723412-SW1 SM 4500-S2D
92276295002 WET/414723412-SW2 SM 4500-S2D
92276295003 WET/414723412-SW3 SM 4500-S2D
92276295004 WET/414723412-SW4 SM 4500-S2D
92276295005 WET/414723412-MW3R SM 4500-S2D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 226 of 265
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92276295006 WET/415133412-EQUIPMENT BLANK SM 4500-S2D
92276295007 WET/415133412-MW4R SM 4500-S2D
92276295008 WET/415133412-MW7 SM 4500-S2D
92276295009 WET/415133412-MW5R SM 4500-S2D
92276295010 WET/415133412-MW1R SM 4500-S2D
92276295011 WET/415133412-MW15 SM 4500-S2D
92276295012 WET/415713412-MW2R SM 4500-S2D
92276295013 WET/415713412-MW8 SM 4500-S2D
92276295014 WET/415713412-MW10 SM 4500-S2D
92276295015 WET/415713412-MW11 SM 4500-S2D
92276295016 WET/415713412-MW12 SM 4500-S2D
92276295018 WET/415713412-MW9 SM 4500-S2D
92276295019 WET/415713412-MW13 SM 4500-S2D
92276295020 WET/416153412-MW14 SM 4500-S2D
92276295001 WETA/254523412-SW1 EPA 300.0
92276295002 WETA/254523412-SW2 EPA 300.0
92276295003 WETA/254523412-SW3 EPA 300.0
92276295004 WETA/254523412-SW4 EPA 300.0
92276295005 WETA/254523412-MW3R EPA 300.0
92276295007 WETA/255223412-MW4R EPA 300.0
92276295008 WETA/255223412-MW7 EPA 300.0
92276295009 WETA/255223412-MW5R EPA 300.0
92276295010 WETA/255223412-MW1R EPA 300.0
92276295011 WETA/255233412-MW15 EPA 300.0
92276295012 WETA/255233412-MW2R EPA 300.0
92276295013 WETA/255233412-MW8 EPA 300.0
92276295014 WETA/255233412-MW10 EPA 300.0
92276295015 WETA/255233412-MW11 EPA 300.0
92276295016 WETA/255233412-MW12 EPA 300.0
92276295018 WETA/255233412-MW9 EPA 300.0
92276295019 WETA/255233412-MW13 EPA 300.0
92276295020 WETA/255233412-MW14 EPA 300.0
92276295001 WETA/254763412-SW1 SM 4500-Cl-E
92276295002 WETA/254763412-SW2 SM 4500-Cl-E
92276295003 WETA/254763412-SW3 SM 4500-Cl-E
92276295004 WETA/254763412-SW4 SM 4500-Cl-E
92276295005 WETA/254763412-MW3R SM 4500-Cl-E
92276295007 WETA/254763412-MW4R SM 4500-Cl-E
92276295008 WETA/254763412-MW7 SM 4500-Cl-E
92276295009 WETA/254763412-MW5R SM 4500-Cl-E
92276295010 WETA/254763412-MW1R SM 4500-Cl-E
92276295011 WETA/254763412-MW15 SM 4500-Cl-E
92276295012 WETA/255703412-MW2R SM 4500-Cl-E
92276295013 WETA/255703412-MW8 SM 4500-Cl-E
92276295014 WETA/255703412-MW10 SM 4500-Cl-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 227 of 265
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92276295
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92276295015 WETA/255703412-MW11 SM 4500-Cl-E
92276295016 WETA/255943412-MW12 SM 4500-Cl-E
92276295018 WETA/255943412-MW9 SM 4500-Cl-E
92276295019 WETA/255943412-MW13 SM 4500-Cl-E
92276295020 WETA/255943412-MW14 SM 4500-Cl-E
92276295001 WETA/254493412-SW1 SM 4500-CN-E
92276295002 WETA/254493412-SW2 SM 4500-CN-E
92276295003 WETA/254493412-SW3 SM 4500-CN-E
92276295004 WETA/254493412-SW4 SM 4500-CN-E
92276295005 WETA/254493412-MW3R SM 4500-CN-E
92276295006 WETA/254663412-EQUIPMENT BLANK SM 4500-CN-E
92276295007 WETA/254663412-MW4R SM 4500-CN-E
92276295008 WETA/254663412-MW7 SM 4500-CN-E
92276295009 WETA/254663412-MW5R SM 4500-CN-E
92276295010 WETA/254663412-MW1R SM 4500-CN-E
92276295011 WETA/254663412-MW15 SM 4500-CN-E
92276295012 WETA/255103412-MW2R SM 4500-CN-E
92276295013 WETA/255103412-MW8 SM 4500-CN-E
92276295014 WETA/255103412-MW10 SM 4500-CN-E
92276295015 WETA/255103412-MW11 SM 4500-CN-E
92276295016 WETA/255103412-MW12 SM 4500-CN-E
92276295018 WETA/255113412-MW9 SM 4500-CN-E
92276295019 WETA/255113412-MW13 SM 4500-CN-E
92276295020 WETA/255113412-MW14 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/30/2015 08:05 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 228 of 265
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Winston-Salem City/County Utilities | Assessment Monitoring Report
APPENDIX C – FIELD DATA
C.

C
Appendix C – Field
Data

C-1

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Winston-Salem City/County Utilities | Assessment Monitoring Report
APPENDIX D – ELECTRONIC FILES
D.

D
Appendix D –
Electronic Files

Portable Document Format (PDF) of this Report
Electronic Data Deliverable (EDD) of Groundwater Results

D-1

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