1306_CabarrusCoHWY49_2017WQMR_DIN28601_20170803

SPRING 2017 SEMI-ANNUAL WATER QUALITY MONITORING REPORT GREENWAY WASTE SOLUTIONS OF HARRISBURG, LLC (FORMERLY HIGHWAY 49 C&D LANDFILL FACILITY) 2105 SPEEDRAIL COURT HARRISBURG, NORTH CAROLINA SOLID WASTE FACILITY PERMIT NUMBER 13-06 Prepared For: GREENWAY WASTE SOLUTIONS OF HARRISBURG, LLC 19109 W. CATAWBA AVENUE, SUITE 200 CORNELIUS, NORTH CAROLINA 28031 Prepared By: CIVIL & ENVIRONMENTAL CONSULTANTS, INC. 1900 CENTER PARK DRIVE, SUITE A CHARLOTTE NORTH CAROLINA 28217 CEC PROJECT 111-370.002 AUGUST 3, 2017

Edward H. Stephens, L.G. Bruce D. Reilly Project Manager Senior Project Manager

-i- Spring 2017 Water Quality Monitoring Report August 2017
TABLE OF CONTENTS
1.0 PURPOSE ...........................................................................................................................1
2.0 SITE DESCRIPTION AND BACKGROUND ................................................................2
3.0 RECENT MODIFICATIONS TO THE MONITORING SYSTEM ............................4
4.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES ...............................................5 4.1 Well Water Level Gauging ..................................................................................... 5 4.2 Well Purging ........................................................................................................... 6
4.3 Groundwater Sample Collection ............................................................................. 6
5.0 GROUNDWATER FLOW EVALUATION ...................................................................7
6.0 GROUNDWATER SAMPLE ANALYTICAL PARAMETERS ..................................8
7.0 GROUNDWATER SAMPLE ANALYTICAL DATA EVALUATION .......................9 7.1 Vinyl Chloride (VC) Data ....................................................................................... 9
7.2 Metal Analytes Detected at Concentrations Exceeding the 2L Standards ............ 11
7.3 Inorganic Leachate Indicator Parameters .............................................................. 12
8.0 SURFACE WATER SAMPLING DATA ......................................................................14
9.0 DEMONSTRATION LETTERS ON VINYL CHLORIDE AND METALS .............15
10.0 OTHER WATER QUALITY MONITORING ACTIVITIES ....................................16
11.0 CONCLUSIONS AND RECOMMENDATIONS .........................................................17
11.1 Conclusions ........................................................................................................... 17 11.2 Recommendations ................................................................................................. 18 FIGURES Figure 1 – Site Location Map Figure 2 – Site Map TABLES Table 1 – Summary of Monitoring Well Gauging Data Table 2 – Summary of Recent Site Groundwater Sample Analytical Detections Table 3 – Historical Groundwater Data Summary
APPENDIX Appendix A – Groundwater Sampling Field Logs Appendix B – Laboratory Data Reports Appendix C – Demonstration of Error in Sample Analyses

-1- Spring 2017 Water Quality Monitoring Report August 2017
1.0 PURPOSE

On behalf of Greenway Waste Solutions of Harrisburg, LLC (GWS), Civil & Environmental
Consultants, Inc. (CEC) has prepared this Spring 2017 Semi-Annual Water Quality Monitoring
Report for the GWS landfill (formerly Highway 49 C&D Landfill) located at 2105 Speedrail Court
in Harrisburg, North Carolina. This report describes the well gauging and field sampling activities,
and provides a summary of the site groundwater conditions and acquired groundwater sample data.

-2- Spring 2017 Water Quality Monitoring Report August 2017
2.0 SITE DESCRIPTION AND BACKGROUND

Greenway Waste Solutions of Harrisburg, LLC (GWS) operates the subject landfill facility under
Solid Waste Facility Permit Number 13-06. The facility address is 2105 Speedrail Court,
Harrisburg, North Carolina. A Site Location Map is attached as Figure 1. The active Phase I/II
C&D disposal area is located in the northwest portion of the site. It is bounded by Coddle Creek
to the north; an adjacent permitted Phase I Expansion C&D Landfill to the east; private industrial
and residential properties to the south; and Speedrail Court to the west. Waste placement in the
active disposal area has generally occurred from 2000 to present. A Site Map is attached as Figure
2.

The North Carolina Department of Environment and Natural Resources (now Department of
Environmental Quality) – Solid Waste Section (NCDEQ-SWS) permitted the landfill facility to
operate in 2000. As a part of the landfill permit, routine semi-annual groundwater detection
monitoring is performed for one background (MW-21) and three downgradient monitoring wells
(MW-55, MW-56 and MW-57) with reports submitted to the NCDEQ-SWS. The landfill facility
and approximate landfill monitoring well locations are depicted in Figure 2.

During the Spring 2013 semi-annual water quality monitoring event conducted by Enviro-Pro,
P.C. (EP), benzene and/or vinyl chloride (VC) were detected in groundwater samples collected
from monitoring wells MW-56 and MW-57. These analytes were detected at low concentrations
that exceeded their respective 15A NCAC 2L .0202 ground water protection standards (2L
Standards) of 1.0 and 0.03 micrograms per liter (µg/L). EP conducted a confirmation-resampling
event on May 31, 2013 that verified the presence of these volatile organic compounds (VOCs) at
similar concentrations in the same monitoring wells.

At the request of the NCDEQ-SWS, EP prepared a Proposed Assessment Monitoring Work Plan
dated August 5, 2013 to further assess groundwater impacts at the Phase I Landfill. Additional
assessment monitoring wells (MW-56A, MW-56D, and MW-57D) were installed hydraulically
downgradient of the landfill. These new wells and the existing detection monitoring wells were
sampled on October 21, 2013 as part of this initial groundwater assessment. Wells MW-55, MW-

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56, MW-57, and MW-57D were re-sampled on November 19, 2013 for confirmatory analyses.
These sampling events confirmed the presence of VC in the saprolite and upper bedrock aquifer
horizons downgradient of the landfill.

-4- Spring 2017 Water Quality Monitoring Report August 2017
3.0 RECENT MODIFICATIONS TO THE MONITORING SYSTEM

The NCDEQ-SWS requested a characterization of the nature and extent of the groundwater
contamination at the active Phase I Landfill. This request was made in response to the detection
of VC at concentrations above the 2L Standards in several monitoring wells at the subject landfill
as reported in May 2013.

In addition to the installation of the three new groundwater monitoring wells in 2013, the facility
owner has continued an on-going contaminant delineation since September 2013, which has
included the following activities:

1) As required by the operating permit for the landfill, groundwater assessment
monitoring wells installed after 2013 have been routinely monitored and sampled along with the originally permitted groundwater monitoring wells for the Appendix II parameter list;
2) Installation of four landfill gas probes and subsequent gas sampling to evaluate the
potential for landfill gas to impact site groundwater; and 3) Evaluation of analytical leachate/landfill gas ‟indicator” parameters including alkalinity, chloride, iron, manganese, sulfate, and total dissolved solids to characterize
the source of the groundwater impacts.

-5- Spring 2017 Water Quality Monitoring Report August 2017
4.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES

CEC personnel conducted field activities associated with the Spring 2017 semi-annual water
quality monitoring on April 26, 2017. Project oversight was provided by an NC-licensed geologist.
Monitoring well water levels were gauged, static well water was purged, and groundwater samples
were collected from six wells including MW-55, MW-56, MW-56A, MW-56D, MW-57, and MW-
57D. During the site visit, background monitoring well MW-21 was observed to be damaged as a
result of on-site activities and could not be gauged or sampled. (This well is scheduled to be
replaced in August 2017.) The approximate locations of these monitoring points are shown on
Figure 2.

In accordance with assessment monitoring requirements, groundwater samples collected from the
six monitoring wells were analyzed for listed Appendix II parameters including volatile organic
compounds (VOCs), semi-volatile organic compounds (SVOCs), pesticides, herbicides,
polychlorinated biphenyls (PCBs), metals, and cyanide. Samples were also collected for leachate
indicator parameters including bicarbonate alkalinity, chloride, sulfate, and total dissolved solids
(TDS). For quality control purposes, CEC personnel collected split samples from wells MW-55,
MW-56, MW-57, and MW-57D for VOC analyses by an independent analytical laboratory.

Two surface water samples (SW-1 and SW-2) were collected from upstream and downstream
points along Coddle Creek. The approximate creek sampling locations are depicted on Figure 2.
Surface water samples were analyzed for listed Appendix I VOCs and metals.

Laboratory analytical methods and sample analytical results are discussed in Sections 6.0 and 7.0.

4.1 WELL WATER LEVEL GAUGING

Prior to well purging/sampling, the water level in each accessible monitoring well was gauged
using an electronic water level meter. The depth-to-groundwater as measured from a reference
point on the well top-of-casing was recorded to the nearest 0.01-inch on the well sampling field

-6- Spring 2017 Water Quality Monitoring Report August 2017
log (see Appendix A). The water level probe was decontaminated between well measurements.
Well gauging data are presented in Table 1.

4.2 WELL PURGING

The water levels in the site monitoring wells were sufficiently shallow to employ a peristaltic pump
to purge the wells at a low-flow rate until targeted analytical parameters were observed to stabilize.
During the well purge, specific conductance, pH, dissolved oxygen, and oxidation-reduction
potential were frequently measured with an YSI 556 Water Quality Meter in a flow-through cell
to observe and document the chemical stability of the formation water entering the monitoring
well. When parameter values indicated stable water chemistry as defined by USEPA Groundwater
Sampling Guidelines for Superfund and RCRA Project Managers (EPA 542-S-02-001, May 2002),
the well purge was considered complete and groundwater samples were then collected. Well purge
data was recorded on the well sampling field logs provided in Appendix A.

4.3 GROUNDWATER SAMPLE COLLECTION

Following the above-described well purging procedures, CEC collected groundwater samples
from each well employing the same peristaltic pump operated at a low-flow rate. Groundwater
samples were collected in laboratory-supplied sample containers that were labeled and packed on
ice in insulated coolers. The sample coolers were transported back to the CEC Charlotte office
where they were picked up by the laboratory courier and shipped overnight to the selected
analytical laboratory. Samples were handled under chain-of-custody protocol.

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5.0 GROUNDWATER FLOW EVALUATION

A depth-to-water level measurement was performed relative to the well top-of-well casing in each
accessible groundwater monitoring well prior to well purging. A water level elevation was
calculated by subtracting the depth-to-water from the respective surveyed top-of-well casing
elevation datum. Monitoring well gauging data are summarized in Table 1.

The water level elevation data indicate that horizontal groundwater movement away from the
landfill is toward Coddle Creek to the north.

A vertical gradient of 0.038 feet/foot downward was calculated for well cluster MW-56A/56D
located south of Coddle Creek. This recently observed downward vertical gradient at MW-
56A/56D is in contrast to upward vertical gradients observed in recent data since October 2014 as
presented in Table 1. A period of heavy precipitation occurred prior to the most recent monitoring
event that appears to have resulted in a temporal reversal of hydraulic gradient direction. A vertical
hydraulic gradient of 0.025 feet/foot upward was calculated for well cluster MW-57/57D that is
located adjacent to Coddle Creek. This upward hydraulic gradient indicates local groundwater
discharge to Coddle Creek, which is consistent with typical Piedmont hydrogeology.

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6.0 GROUNDWATER SAMPLE ANALYTICAL PARAMETERS

CEC submitted the collected groundwater samples to the prime analytical laboratory TestAmerica
for the target analyses. CEC submitted the split samples that were collected from four selected
wells to Pace Analytical Services, Inc. (Pace) laboratory for VOC analyses.

Six monitoring well samples were analyzed for the following Appendix II parameters:

Volatile Organic Compounds (VOCs) plus Tetrahydrofuran (THF) [EPA 8260B]
Semi-VOCs [EPA 8270D]
Organochlorine Pesticides [EPA 8081B]
Polychlorinated Biphenyls (PCBs) [EPA 8082A]
Herbicides [EPA 8151A]
Metals [EPA 200.8]
Mercury [EPA 245.1]
Cyanide [EPA 9014]

Monitoring well samples were also tested for leachate indicator parameters including the
following:

Chloride and Sulfate [EPA 9056A]
Alkalinity [SM 2320B]
Total Dissolved Solids (TDS) [SM 2540C]

-9- Spring 2017 Water Quality Monitoring Report August 2017
7.0 GROUNDWATER SAMPLE ANALYTICAL DATA EVALUATION

Summaries of Appendix II VOCs, SVOCs, organochlorine pesticides, herbicides, PCBs, metals,
and inorganic analytes detected in the collected groundwater samples at concentrations above their
respective laboratory-specific method detection limits are provided in Tables 2 and 3. The
laboratory analytical data reports are provided in Appendix B.

7.1 VINYL CHLORIDE (VC) DATA

Data discussed in this section draw inferences to historical well sampling data acquired at the
active Phase I Landfill since Spring 2013. Enviro-Pro, PC conducted the water quality monitoring
activities from at least 2004 to October 2016. Pace performed the sample analyses from 2004 to
November 2012. Beginning in April 2013 through October 2016, Shealy Environmental Services,
Inc. (Shealy) performed the sample analyses for the semi-annual monitoring events. CEC
performed the sampling and engaged TestAmerica to analyze the water samples for the most
recently conducted Spring 2017 monitoring event, and also submitted split samples from four wells
to Pace for VOC analyses.

Prior to the April 2013 monitoring event, Pace performed the groundwater sample analyses, and
no VOCs were detected in any sample. Shealy reported the initial detections of VOCs in site wells
MW-56 and MW-57 during the April 2013 monitoring event. Shealy consistently reported VC in
wells MW-55, MW-56, MW-57, and MW-57D up through October 2016.

As presented in Table 7.1 below, April 2017 split samples between TestAmerica and Pace
confirmed the presence of VC in MW-56 only.

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Table 7.1 – Recent Reported Vinyl Chloride Data

Units in micrograms per liter (µg/L) cn = case narrative refers to laboratory error BOLD indicates exceedance of the 2L Standard

For the Spring 2017 groundwater sampling event, CEC obtained split samples and these were
delivered to TestAmerica and Pace. For certain samples, higher than expected values of VC were
reported by TestAmerica compared to the Pace results. CEC asked TestAmerica to review the
results, analysis methodology, instruments used, and interviewed the analysts in an effort to either
validate or discount this first round of 2017 results. TestAmerica brought in their Senior Technical
Services Group to review their process. In late May, TestAmerica informed CEC of the following
results of their investigation:

1. Search indicated a possibility of conversion of a Freon refrigerant (Freon 151) to VC in the
gas chromatograph (GC);
2. Confirmation of this occurred after TestAmerica obtained and ran a Freon 151 standard
through their Chicago GCs, resulting in only one of the GCs not converting the Freon 151
to VC;
3. A TestAmerica company-wide program was implemented and identified most of their GCs
converting the Freon 151 to VC; and
4. TestAmerica started, and is continuing, a corrective-action program to identify and change
the component(s) of the GCs converting the Freon. (It is reported that the likely cause is
the Purge and Trap mechanism.)

Well I.D. October 2016 Vinyl Chloride Shealy
April 2017 Vinyl Chloride TestAmerica
April 2017 Vinyl Chloride Pace
June 2017 Vinyl Chloride
TestAmerica
MW-55 0.78 <0.5 <1.0 NA
MW-56 13 6.6 cn 3.3 9.6
MW-57 4.8 3.3 cn <1.0 0.59
MW-57D 2.5 1.1 cn <1.0 <0.5

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On June 15, 2017, CEC re-sampled MW-56, MW-57, and MW-57D and submitted these
confirmatory samples to TestAmerica for VOCs analysis. The confirmatory samples were
analyzed by TestAmerica using a GC instrument that they previous tested and cleared to provide
artifact-free VC data. VC was detected in MW-56 at 9.6 µg/L and in MW-57 at 0.59 µg/L. VC
was not detected in the MW-57D re-sample at a concentration above the laboratory reporting limit
of <0.5 µg/L.

Following the June 2017 confirmation-resampling event, CEC received a letter from Shealy regarding
in-house testing of their GC instruments documenting the results of their independent testing, which
confirmed TestAmerica’s findings. Shealy also provided a letter from the supplier of the silica gel
component in the GC purge and trap mechanisms (OI Analytical) that indicated the silica gel
component may be the “active” Freon 151 to VC conversion location. The documentation from
TestAmerica, Shealy, and OI Analytical can be found in Appendix C.

While the confirmed conversion of Freon 151 to VC explains the spike in VC at the Highway 49
Landfill, the groundwater as measured in MW-56 and MW-57 still exhibits VC at concentrations
above the 2L Standards. Confirmation of these second-round results from the Spring 2017
sampling will continue to take place for the near future as part of the approved water quality
monitoring plan. CEC will continue to obtain and analyze split samples and blind duplicates from
selected groundwater monitoring wells. TestAmerica and Pace are continuing to conduct reviews
of their GCs to eliminate the issue(s) converting the Freon to VC.

The presented data and supporting correspondence from the analytical laboratories directly
working on the project clearly show that the VC analytical data prior to the Spring 2017 sampling
event have to be considered invalid. Any remedial efforts to address VC impacts above the 2L
Standards will be based on sample data from the Spring 2017 event and future sampling events.

7.2 METAL ANALYTES DETECTED AT CONCENTRATIONS EXCEEDING
THE 2L STANDARDS
As highlighted in Table 2, the laboratory test results for the monitoring event show that detected
iron and manganese concentrations exceed their respective 2L Standards in the majority of the

-12- Spring 2017 Water Quality Monitoring Report August 2017
landfill monitoring well samples. Elevated iron concentrations of 4,100 and 47,000 µg/L were
detected in downgradient wells MW-56 and MW-57, respectively. Elevated manganese
concentrations of 11,000 and 10,000 µg/L were detected in downgradient wells MW-56 and MW-
57, respectively. Manganese levels ranged from 690 to 1,800 µg/L in upgradient well MW-21.
Reducing groundwater conditions in the vicinity of wells MW-56 and MW-57 may be causing
iron and manganese to solubilize from the natural formations into the groundwater. Low dissolved
oxygen (DO) and negative oxidation-reduction potential (ORP) indicative of reducing conditions
were measured in MW-56 and MW-57 during the monitoring event.

Cobalt concentrations exceed its NC Interim Maximum Allowable Concentration (IMAC) of 1
µg/L in the majority of the landfill wells. In particular, elevated cobalt levels of 66 and 17 µg/L
were detected in downgradient wells MW-56 and MW-57. The historical cobalt levels in
upgradient well MW-21 range from 1.1 to 11 µg/L. Reducing conditions in these areas may be
causing cobalt to solubilize from the natural formations into the groundwater.

Nickel was detected at 100 µg/L in MW-57D. The 2L Standard for nickel is 100 µg/L.
Historically, nickel levels have been detected in the range of 69 to 100 µg/L in MW-57D. The
historical nickel levels in upgradient well MW-21 range from 2.6 to 5.3 µg/L. Reducing conditions
in this area may be causing nickel to solubilize from the natural formations into the groundwater.

Vanadium concentrations of 6.8 and 21 µg/L were detected in MW-55 and MW-57D, respectively,
which exceed its IMAC of 0.3 µg/L. The historical vanadium levels in upgradient well MW-21
range from 1.4 to 15 µg/L. Vanadium was detected in the two surface water samples at
concentrations of 9.8 and 9.9 µg/L. When compared to background data, the detected vanadium
levels in MW-55 and MW-57D appear to be in the range of naturally occurring concentrations.

7.3 INORGANIC LEACHATE INDICATOR PARAMETERS

The detections of inorganic parameters are summarized in Table 2. Sulfate was detected in MW-
57D at 330 mg/L, which exceeds its 2L Standard of 250 mg/L. Historical sulfate levels in
upgradient well MW-21 range from 12 to 32 mg/L. Total dissolved solids (TDS) concentrations

-13- Spring 2017 Water Quality Monitoring Report August 2017
of 1,300 and 1,500 mg/L in MW-57 and MW-57D, respectively, exceeded its 2L Standard of 500
mg/L. Historical TDS levels in upgradient well MW-21 range from 221 to 310 mg/L. These data
suggest that leachate may be affecting downgradient groundwater quality near the well pair.

-14- Spring 2017 Water Quality Monitoring Report August 2017
8.0 SURFACE WATER SAMPLING DATA

CEC personnel collected two surface water samples (SW-1 and SW-2) from upstream and
downstream points along Coddle Creek. The approximate creek sampling locations are depicted
on Figure 2. Surface water samples were analyzed for the constituents listed in Appendix I of 40
CFR Part 258. The stream sample analytical results are summarized in Tables 2 and 3.

No Appendix I VOCs were detected above the laboratory reporting limits in the surface water
samples. Several Appendix I metals including cobalt, iron, manganese, and vanadium were
detected in both surface water samples. Cobalt was detected in SW-1 and SW-2 at 2.4 and 2.7
µg/L, respectively. The NC Protection Standard for cobalt is 4 µg/L. Iron and manganese were
detected in both surface water samples at levels within the range of published naturally occurring
stream concentrations. Vanadium was detected in SW-1 and SW-2 at 9.9 and 9.8 µg/L,
respectively. Detected vanadium levels are also within the range of published naturally occurring
stream concentrations.

-15- Spring 2017 Water Quality Monitoring Report August 2017
9.0 DEMONSTRATION LETTERS ON VINYL CHLORIDE AND METALS

Per 15A NCAC 13B .0544 (b) (1) (I), on behalf of Greenway Waste Solutions of Harrisburg, LLC,
CEC prepared and submitted letters under separate cover to the NCDEQ-SWS Compliance Unit
presenting historical data and recent technical findings regarding the laboratory detections of VC and
on the presence of background metals in the groundwater underlying the landfill. Copies of these
letters and supporting documentation are included in Appendix C. Both letters present and discuss
data on laboratory error in falsely reporting VC due to the Freon conversion and on the presence of
naturally occurring metals in geology and hydrogeology at the landfill.

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10.0 OTHER WATER QUALITY MONITORING ACTIVITIES

Recently, CEC field personnel noted that upgradient detection monitoring well MW-21 had been
damaged by on-site landfill activities. This well is scheduled to be replaced in August 2017. An
attempt will be made to install the replacement well in close proximity to the original well. Should
there be a need to re-locate the replacement well out of landfill traffic, CEC will consult with the
NCDEQ-SWS for siting approval. In accordance with regulations in 15A NCAC 02C .0113 (d),
the damaged well will be abandoned concurrent with the well replacement.

-17- Spring 2017 Water Quality Monitoring Report August 2017
11.0 CONCLUSIONS AND RECOMMENDATIONS

11.1 CONCLUSIONS

CEC personnel conducted field activities associated with the Spring 2017 semi-annual water
quality monitoring at the GWS Landfill on April 26, 2017. Well water levels were gauged, static
well water was purged, and groundwater samples were collected from six monitoring wells
including shallow wells MW-55, MW-56, MW-56A, and MW-57, and deeper wells MW-56D and
MW-57D. In addition, surface water samples (SW-1 and SW-2) were collected from upstream
and downstream locations within Coddle Creek.

Due to a laboratory issue involving the conversion of Freon 151 to VC, CEC re-sampled MW-56,
MW-57, and MW-57D on June 15, 2017 and submitted these confirmatory samples to
TestAmerica for VOCs analysis. Vinyl chloride was detected in MW-56 at 9.6 µg/L and in MW-
57 at 0.59 µg/L. Vinyl chloride was not detected in the MW-57D re-sample at a concentration
above the laboratory reporting limit of <0.5 µg/L.

Cobalt, iron, and manganese were detected at higher than background levels in MW-56 and MW-
57. Field measurement data for dissolved oxygen and oxidation-reduction potential indicate
reducing groundwater conditions in these areas. It is not known whether the reducing conditions
are naturally occurring or a result of leachate impact.

Analytical testing detected leachate indicator parameters in downgradient wells MW-57 and MW-
57D including sulfate and/or TDS at elevated concentrations above the 2L Standards and compared
to the upgradient groundwater well MW-21. These data suggest that leachate may be affecting
downgradient groundwater quality in the vicinity of the well pair MW-57/57D.

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11.2 RECOMMENDATIONS

It is CEC’s technical opinion based on the quality assurance sampling and analytical data obtained
during the Spring 2017 monitoring event that recent historical vinyl chloride detections in site
monitoring wells are largely the result of laboratory artifacts. Laboratory instrumentation reviews
have determined that when present Freon 151 will degrade to VC in GC instruments operating
with purge and trap equipment with a silica gel component. The well re-sample analyses in June
2017 is the only reported vinyl chloride data that should be representative of site groundwater
quality. Confirmation of these second-round results from the Spring 2017 sampling will continue
to take place for the near future as part of the approved groundwater monitoring plan. CEC will
continue to obtain and analyze split samples and blind duplicates from selected groundwater
monitoring wells. TestAmerica and Pace are continuing to conduct reviews of their GCs to
eliminate the issue(s) converting the Freon to vinyl chloride.

To minimize sampling artifacts and validate certain metals, sulfate and TDS data, CEC will
carefully monitor turbidity in the site monitoring wells during the well purge process. CEC will
collect samples after achieving turbidity levels of 20 Nephelometric Turbidity Units (NTUs) or
less, if practical.

Recently, CEC field personnel noted that upgradient detection monitoring well MW-21 had been
damaged by on-site landfill activities. This well is scheduled to be replaced in August 2017. An
attempt will be made to install the replacement well in close proximity to the original well. Should
there be a need to re-locate the replacement well out of landfill traffic, CEC will consult with the
NCDEQ-SWS for siting approval. In accordance with regulations in 15A NCAC 02C .0113 (d),
the damaged well will be abandoned concurrent with the well replacement.

FIGURES

REFERENCE
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE LOCATION MAP
111-370.0021"=1000'AUGUST 2017
PNP EHS EHS 1
HIGHWAY 49 C&D LANDFILL
GREENWAY WASTE SOLUTIONS OF
HARRISBURG, LLC
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE MAP
111-370.0021" = 400'AUGUST 2017
JKS PNP EHS 2
GREENWAY WASTE SOLUTIONS OF
HARRISBURG, LLC
HARRISBURG, NORTH CAROLINA
REFERENCE
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
LEGEND

TABLES

Table 1
Summary of Monitoring Well Gauging Data
Spring Semi-Annual Groundwater Monitoring
Highway 49 Landfill
CEC Project No. 111-370.002
August 2017
MW ID Well
Depth
Screen
Interval TOC Elev.
Depth to
Water
(TOC)
April 2017
WT Elev.
Depth to
Water
(TOC)
June 2017
WT Elev.
MW-21 50 35 - 50 627.89 NM * NM NM * NM
MW-55 23 5 - 20 545.28 12.18 533.1 NM NM
MW-56 25 10 - 25 NM 5.52 NM 5.75 NM
MW-56A 20 10 - 20 541.79 5.92 535.87 NM NM
MW-56D 50 40 - 50 542.01 7.29 534.72 NM NM
MW-57 20 10 - 20 543.11 9.87 533.24 10.65 532.46
MW-57D 50 40 - 50 543.69 9.64 534.05 10.09 533.6
All units given in feet NM = Not measured.
TOC = Top of Casing Elevation * = Well damaged and not accessible.
WT = Groundwater Table
Table 2
Summary of April/June 2017 Sampling Events
Highway 49 Landfill
CEC Project: 111-370.002
Well I.D. MW-55 MW-56A MW-56D
Sampling Date 4/26/17 4/26/17 6/16/17 4/26/17 4/26/17
Organics (µg/L)2L Std.
Benzene 1 <0.5 1.7 1.3 <0.5 <0.5
Bis(2-ethylhexyl)phthalate 3 <7.5 <7.5 NA <7.5 <7.8
Carbon Disulfide 700 <2 <2 <2 <2 <2
cis-1,2-Dichloroethene 70 <1 2.1 5.2 <1 <1
2,4-Dimethylphenol 100 <7.5 <7.5 NA <7.5 <7.8
Diethylphthalate 6,000 <5 <5 NA <5 <5
2,4 -D 70 <2 <2 NA <2 <2
4-4'-DDT 0.1 <0.04 <0.04 NA <0.04 <0.04
Dieldrin 0 <0.04 <0.04 NA <0.04 <0.04
Dinoseb 7 <2.4 <2.3 NA <2.2 <2.2
Endosulfan II 40 <0.04 <0.04 NA <0.04 <0.04
Endosulfan sulfate 40 <0.04 <0.04 NA <0.04 <0.04
Endrin 2 <0.04 <0.04 NA <0.04 <0.04
Endrin aldehyde 2 <0.04 <0.04 NA <0.04 <0.04
Methylene Chloride 5 <5 <5 <5 <5 <5
Trichloroethene 3 <0.5 <0.5 <0.5 <0.5 <0.5
Vinyl Chloride 0.03 <0.5 6.6 cn 9.6 <0.5 <0.5
Toluene 600 <0.5 <0.5 <0.5 <0.5 <0.5
Xylenes 500 <1 <1 <1 <1 <1
beta-BHC NS <0.037 <0.037 NA <0.038 <0.04
1,1-Dichloroethane 6 <1 <1 <1 <1 <1
1,2-Dichloroethane 0.4 <1 <1 0.51 J <1 <1
1,1-Dichloroethene 350 <1 <1 <1 <1 <1
Tetrachloroethene 0.7 <1 <1 <1 <1 <1
Tetrahydrofuran NS <10 <10 <10 <10 <10
Naphthalene 6 <0.75 <0.75 NA <0.75 <0.78
Acetophenone 700 <3.7 <3.7 NA <3.8 <3.9
Metals (µg/L)
Antimony 1 <3 <3 NA <3 <3
Arsenic 10 0.18 J 0.28 J NA <1 0.41 J
Barium 700 120 170 NA 51 31
Beryllium 4 <1 <1 NA <1 <1
Cadmium 2 <0.5 <0.5 NA <0.5 <0.5
Calcium NS NA NA NA NA NA
Chromium 10 <5 <5 NA <5 <5
Cobalt 1 5.8 66 NA <1 0.55 J
Copper 1,000 5.3 4 NA 1.3 J 1.7 J
Iron 300 810 4100 NA <100 540
Lead 15 0.31 J 0.17 J NA <0.5 0.78
Manganese 50 98 11000 NA 16 37
Nickel 100 21 9.7 NA <2 1.7 J
Selenium 20 <2.5 <2.5 NA <2.5 <2.5
Thallium 0.2 <2 <2 NA <2 <2
Vanadium 0.3 6.8 <5 NA <5 <5
Zinc 1,000 10 J <20 NA <20 <20
Indicator Parameters (mg/L)NA
Alkalinity NS 150 340 NA 86 180
Ammonia- N 1.5 NA NA NA NA NA
Carbon Dioxide NS NA NA NA NA NA
Chloride 250 14 11 NA 19 14
Cyanide 70 <0.01 <0.01 NA <0.01 <0.01
Sulfate 250 95 67 NA 63 74
Sulfide NS NA NA NA NA NA
TDS 500 350 450 NA 230 330
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
Bold values exceed the NCDEQ Standards
Bold and highlighted values exceed the NCDEQ
Standards yet the analyte concentrations are
within the range of naturally-occurring levels.
NA = Not Analyzed
NS = Not Specified
J = Method Detection Limit < Reporting Limit
cn = Case Narrative
MW-56
Table 2 (cont.)
Summary of April/June 2017 Sampling Events
Highway 49 Landfill
CEC Project: 111-370.002
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Selenium 20
Thallium 0.2
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
Bold values exceed the NCDEQ Standards
Bold and highlighted values exceed the NCDEQ
Standards yet the analyte concentrations are
within the range of naturally-occurring levels.
NA = Not Analyzed
NS = Not Specified
J = Method Detection Limit < Reporting Limit
cn = Case Narrative
SW-1 SW-2
4/26/17 6/16/17 4/26/17 6/16/17 4/26/17 4/26/17
<0.5 0.7 0.6 <0.5 <0.5 <0.5
<7.4 NA <7.5 NA NA NA
<2 <2 <2 <2 <2 <2
<1 <1 <1 <1 <1 <1
<7.4 NA <7.5 NA NA NA
<5 NA <5 NA NA NA
<2 NA <2 NA NA NA
<0.04 NA <0.04 NA NA NA
<0.04 NA <0.04 NA NA NA
<2.3 NA <2.4 NA NA NA
<0.04 NA <0.04 NA NA NA
<0.04 NA <0.04 NA NA NA
<0.04 NA <0.04 NA NA NA
<0.04 NA <0.04 NA NA NA
<5 <5 <5 <5 <5 <5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5
3.3 cn 0.59 1.1 cn <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<1 <1 <1 <1 <1 <1
<0.037 NA <0.037 NA NA NA
<1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10
<0.74 NA <0.75 NA NA NA
<3.7 NA <3.8 NA NA NA
<3 NA <3 NA <1 <1
1.2 NA 0.18 J NA 0.46 J 0.47 J
450 NA 93 NA 56 61
<1 NA <1 NA <0.4 <0.4
<0.5 NA 0.38 J NA <0.5 <0.5
NA NA NA NA NA NA
<5 NA <5 NA <5 <5
17 NA 1.1 NA 2.4 2.7
0.68 J NA 16 NA 4 4
47,000 NA 300 NA 3000 3100
0.4 J NA 0.2 J NA 1.2 1.3
10,000 NA 220 NA 230 260
15 NA 100 NA 1.5 J 1.6 J
<2.5 NA <2.5 NA <2.5 <2.5
<2 NA <2 NA <2 <2
<5 NA 21 NA 9.9 9.8
17 J NA 8.4 J NA 9.8 J 15 J
NA NA
880 NA 920 NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
73 NA 75 NA NA NA
<0.10 NA <0.01 NA NA NA
150 NA 330 NA NA NA
NA NA NA NA NA NA
1300 NA 1500 NA NA NA
MW-57 MW-57D
Table 3Summary of Recent Site Groundwater Monitoring DataHighway 49 LandfillCEC Project: 111-370.002Well I.D.Sampling Date10/18/11 10/23/12 4/22/13 10/21/13 4/3/14 10/17/14 4/15/15 10/20/15 4/16/16 10/21/16 4/26/17Organics (µg/L)2L Std.Benzene 1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1Bis(2-ethylhexyl)phthalate 3 NA NA NA <525<5 2.1 J 2.7 J 1.9 J <5Carbon Disulfide 700 <2 <2 <1 <1 <1 <1 <1 <1 <1 <1cis-1,2-Dichloroethene 70 <1 <1 <1 <1 <1 <1 <1 <1 <1 <12,4-Dimethylphenol 100 NA NA NA <1 <1 <1 <1 <1 <1 <1Diethylphthalate 6,000 NA NA NA <5 <5 <5 <5 <5 <5 <52,4 -D 70 NA NA NA <2 <2 <2 <2 <2 <2 <24-4'-DDT 0.1 NA NA NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04Dieldrin 0 NA NA NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04Dinoseb 7 NA NA NA <1 <1 <1 <1 <1 <1 <1Endosulfan II 40 NA NA NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04<0.04Endosulfan sulfate 40 NA NA NA <0.04 <0.04 <0.04 <0.04 <0.04<0.04 <0.04Endrin 2 NA NA NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04Endrin aldehyde 2 NA NA NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04Methylene Chloride 5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1Trichloroethene 3 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1Vinyl Chloride 0.03 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1Toluene 600 <1 <1 <1 <1 <1 <1 2.5 1 <1 0.71 JXylenes 500 <2 <2 <1 <1 <1 <1 2.7 1.1 < 1.2beta-BHC NS NA NA NA <0.025 <0.025 <0.025 <0.04 <0.04 <0.04 <0.041,1-Dichloroethane 6 <1 <1 <1 <1 <1 <1 <1 <1 <1 <11,2-Dichloroethane 0.4 <1 <1 <1 <1 <1 <1 <1 <1 <1 <11,1-Dichloroethene 350 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1Tetrachloroethene 0.7 <1 <1 < <1 <1 <1 <1 <1 <1 <1Tetrahydrofuran NS <10 <10 <5 <5 <5 <5 <5 <5 <5 <5Naphthalene 6 NA NA NA <1 <1 <1 0.21 J 0.12 J <1 <1Acetophenone 700 NA NA NA <1 <1 <1 0.39 J 2.9 <1 <1Metals (µg/L)Antimony 1 <6 <6 <1 <1 <1 <1 <1 0.32 J1.5 B0.83 JArsenic 10 <10 <10 <10 <1 <1 <1 1.4 B 11 0.54 J 0.68 JBarium 700 54.3 J 137 140 120 120 43 50 140 170 110Beryllium 4 <1 <1 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 0.12 J <0.4Cadmium 2 <1 <1 <2 <0.1 <0.1 <0.1 0.052 J 0.33 0.15 0.055 JCalcium NS NA NA NA NA NA NA NA 31,000 22,000 18,000Chromium 10 <10 <10 <5 <5 <5 <5 <5 2.6 J 4.3 J <5Cobalt 1 <10 <10 <259.9 6.6<51.1 J 11 8 3.9 JCopper 1,000 <10 <10 5.6 6.8 3.3 370 5 39 B 28 B 6.2Iron300 NA NA NA NA NA NA NA NA NA NALead15 <10 <10 <10 <1 <1 <1 0.24 J 1.8 2.1 0.15 JManganese 50 NA NA NA NA NA NA NA1,800 1,200 690Nickel 100 <50 <50 <40 <5 <5 <5 2.8 J 5.2 5.3 2.6 JSelenium 20 <10 <10 <10 <1 <1 <1 1.3 <1 <1 <1Thallium 0.2 <5.5 <5.5 NA <0.50.57<0.5 <5 <0.5 <0.5 <0.5Vanadium 0.3 <25 <25 <50 <5 <5 <52.1 J 8.1 15 B 1.4 JZinc 1,000 159 15.4 50 62 61 48 41 190 64 40Indicator Parameters (mg/L)Alkalinity NS 125 156 180 NA NA NA NA 160 160 160Ammonia- N 1.5 NA NA NA NA NA NA NA 4.8 B 0.56 0.41Carbon Dioxide NS NA NA NA NA NA NA NA 200 230 400Chloride 250 11.4 14.8 11 NA NA NA NA 10 4.6 8.3Cyanide 70 NA NA NA NA NA NA NA NA 0.0071 J <0.01Sulfate 250 12 J 30.9 32 NA NA NA NA NA NA NASulfide NS NA NA NA <1 <1 <1 <1 1.5 2 0.7 JTDS500 221 242 270 NA NA NA NA 310 B 210 B 2602L Std. = 15A NCAC 02L .0202 Groundwater Standards or Interim Maximum Allowable Concentrations (IMACs) (Eff. April 1, 2013)Bold values exceed the NCDEQ StandardsBold and highlighted values exceed the NCDEQ Standards yet the analyte concentrations are within the range of naturally-occurring levels.NA = Not AnalyzedNS = Not SpecifiedJ = Method Detection Limit < Reporting Limitcn = Case NarrativeWell Damaged - No Sample CollectedMW-21 (Background Well)
Table 3Summary of Recent Site Groundwater Monitoring DataHighway 49 LandfillCEC Project: 111-370.002Well I.D.Sampling DateOrganics (µg/L)2L Std.Benzene 1Bis(2-ethylhexyl)phthalate 3Carbon Disulfide 700cis-1,2-Dichloroethene 702,4-Dimethylphenol 100Diethylphthalate 6,0002,4 -D 704-4'-DDT 0.1Dieldrin 0Dinoseb 7Endosulfan II 40Endosulfan sulfate 40Endrin 2Endrin aldehyde 2Methylene Chloride 5Trichloroethene 3Vinyl Chloride 0.03Toluene 600Xylenes 500beta-BHC NS1,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350Tetrachloroethene 0.7Tetrahydrofuran NSNaphthalene 6Acetophenone 700Metals (µg/L)Antimony 1Arsenic 10Barium 700Beryllium 4Cadmium 2Calcium NSChromium 10Cobalt 1Copper 1,000Iron300Lead15Manganese 50Nickel 100Selenium 20Thallium 0.2Vanadium 0.3Zinc 1,000Indicator Parameters (mg/L)Alkalinity NSAmmonia- N 1.5Carbon Dioxide NSChloride 250Cyanide 70Sulfate 250Sulfide NSTDS5002L Std. = 15A NCAC 02L .0202 Groundwater Standards or Interim Maximum Allowable Concentrations (IMACs) (Eff. April 1, 2013)Bold values exceed the NCDEQ StandardsBold and highlighted values exceed the NCDEQ Standards yet the analyte concentrations are within the range of naturally-occurring levels.NA = Not AnalyzedNS = Not SpecifiedJ = Method Detection Limit < Reporting Limitcn = Case Narrative10/18/11 10/23/12 4/22/13 10/21/13 11/19/13 4/3/14 10/17/14 4/15/15 10/20/15 4/16/16 10/21/16 4/26/17 10/18/11 10/23/12 4/22/13 10/21/13 11/19/13 4/3/14 10/17/14 4/15/15 10/20/15 4/16/16 10/21/16 4/26/17 6/16/17<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 <1 <12 2 1.4 2.1 1.10.48 J1.30.59 J1.9 1.7 1.3NA NA NA <5 NA <5 <5 <5 4.4 J 0.98 J <5 <7.5 NA ND NA <5.1 NA <5 <510<5 2.5 J <5 <7.5 NA<2 <2 ND <1 <1 <1 <1 <1 <1 <1 <1 <2 <2 <2 <1 <1 <1 <1 <1 <1 1.4 <1 <1 <2 <2<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 < <1 12 8.4 5.4 8 3.9 4.9 3.8 6.8 3.32.1 5.2NA NA NA <1 NA <1 <1 <1 <1 <1 <1 <7.5 NA NA NA <1 NA <1 <1 <1 <1 <1 <1 <7.5 NANA NA NA <5 <5 <5 <5 <5 <5 <5 0.36 J <5 NA NA NA <5 NA <5 <5 <5 <5 <5 <5 <5 NANA NA NA <2 NA <2 <2 <2 <2 <2 <2 <2 NA NA NA <2 NA <2 <2 <2 <2 0.69 J <2 <2 NANA NA NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04NA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NANA NA NA <1 NA <1 <1 <1 <1 <1 <1 <2.4 NA NA NA <1 NA <1 <1 <1 <1 <1 <1 <2.3 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 0.94 J <1 0.79 J <1 <5 <5<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 <1 <1 1.2 <1 <1 <1 <1 0.46 J 0.27 J 0.92 J <1 <0.5 <0.5<1 <1 <11.7 1.5<12.1 0.66 J 1.1<10.78 J<0.5 <1 <114 24 18 26 27 8.2 6.3 20 13 6.6 cn 9.6<1 <1 <1 <1 <1 <1 <1 2.2 1.3 <1 1.1 <0.5 <1 < <1 <1 <1 <1 <1 1.4 0.71 J<1 0.87 J <0.5 <0.5<2 <2 < <1 <1 <1 <1 2.1 1.2 <1 1.6 <1 <2 <2 <1 <1 <1 <1 <1 1.7 0.92 J <11.3 <1 <1NA NA NA <0.025 NA <0.025 <0.025 <0.04 <0.04 <0.04 <0.04 <0.037 NA NA NA <0.025 NA <0.025 <0.025 <0.04 <0.04 <0.04 <0.04 <0.037 NA<1 <1 <1 < <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.29 J <1 <1 <1 <1<1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10.51 J<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.31 J <1 <1 <1 <1 <1< <1 <1 <1 <1 < <1 <1 <1 <1 <1 <1 <1 <1 < <1 <1 <1 <1 0.43 J <1 <1 <1 <1 <1<10 <10 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 <10 <5 <5 <5 <5 <5 <5 <5 2.7 J <5 <10 <10NA NA NA <1 NA <1 <1 0.13 J <1 <1 <1 <0.75 NA NA NA ND NA <1 <1 0.15 J0.098 J <1 <1 <0.75 NANA NA NA <1 NA <1 <1 <1 6 0.49 J <1 <3.7 ND NA NA <1 NA <1 <1 <1 1.5 0.35 J <1 <3.7 NA<6 <6 <1 <1 <1 <1 <1 <1 <1 0.89 BJ 0.72 BJ <3 <6 <6 <1 <1 <1 <1 <1 <1 0.34 J 0.51 BJ 0.42 BJ <3 NA<10 <10 <10 1 NA <1 <1 0.97 BJ 9.7 1.4 J 0.86 J 0.18 J <10 <10 <10 <1 NA <5 <1 0.74 BJ 2.9 <1 <1 0.28 J NA132 150 190 150 NA 210 130 170 170 310 180 120 102 145 70 68 NA 130 15 98 45 510 130 170 NA<1 <1 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 0.36 J <0.4 <1 <1 <1 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <1 NA<1 <1 <2 <0.1 NA <0.1 <0.1 0.054 J <0.1 0.5 0.053 J <0.5 <1 <1 <2 <0.1 NA <0.1 <0.1 <0.1 <0.1 0.07 J <0.1 <0.5 NANA NA NA NA NA NA NA NA 51,000 69,000 50,000 NA NA NA NA NA NA NA NA NA 17,000 110,000 56,000 NA NA<10 <10 <5 <5 NA <5 <5 0.99 J 4.5 J324.2 J <5 <10 <10 <5 <5 NA <5 <5 <5 0.85 J 1.0 J 0.66 J <5 NA8.2 J 9.6 J<2513NA9.1 6.6 6.1 11 62 12 5.8 9.8 J 7.2 J 27 23NA33<535 9.1 77 34 66NA<10 26.1 17 55 NA 10 7.1 17 32 B 160 B 24 5.3 <10 32.4 <5 3.7 NA 4 6.2 1.1 9.3 B 4.5 B 3 4 NANA NA NA NA NA NA NA NA NA NA NA810NA NA NA NA NA NA NA NA NA NA NA4100NA<10 <10 <10 <1 NA <1 <1 0.18 J 0.4 J 3.9 0.47 0.31 J <10 <10 <10 <1 NA <1 <1 <1 0.68 J 0.46 J 0.23 J 0.17 J NANA NA NA NA NA NA NA NA260 590 240 98NA NA NA NA NA NA NA NA950 13,000 7,600 11,000NA8.5 J 21.2 J <40 35 NA 28 18 22 2112029 21 <50 15.5 J <40 <5 NA <5 <5 9.8 3.3 J 67 5 9.7 NA<10 <10 <10 <1 NA <1 1.1 1.8 <1 <5 <1 <2.5 <10 <10 <10 <1 NA <5 <1 1.7<1 <1 <1 <2.5 NA<5.5 <5.5 NA <0.5 NA0.54<0.5 <0.5 <0.50.21 J<0.5 <2 <5.5 <5.5 NA <0.5 NA1.3<0.5 <0.5 <0.5 <0.5 <0.5 <2 NA<2515.5 J<5025NA14 13 7.5 13 69 B 22 6.8<2515.1 J<506.7NA34<5 <512 14 B 2.8 J<5 NA<10 10.5 <20 79 NA 86 55 38 42 110 17 10 J 12.4 10.4 62 74 NA 71 18 3160 29 8.4 J <20 NANA216 145 220 NA NA NA NA NA 180 190 170 150 224 152 130 NA NA NA NA NA 190 420 310 340 NANA NA NA NA NA NA NA NA 0.057 BJ 0.052 J 0.054 J NA NA NA NA NA NA NA NA NA 0.18 B 0.15 0.25 NA NANA NA NA NA NA NA NA NA 270 380 310 NA NA NA NA NA NA NA NA NA 440 870 910 NA NA13.1 14.9 13 NA NA NA NA NA 23 24 18 14 13.8 14.9 8.2 NA NA NA NA NA 8.5 59 11 11 NANA NA NA NA NA NA NA NA NA <0.01 <0.01 <0.01 NA NA NA NA NA NA NA NA NA<0.01 <0.01 <0.01 NA24.7 J 29.4 55 NA NA NA NA NA NA NA NA 95 18.7 J 32 63 NA NA NA NA NA NA NA NA 67 NANA NA NA NA NA <1 <1 <1 0.90 J <1 <1 NA NA NA NA <1 NA <1 <1 <1 <1 <1 <1 NA NA315 249 350 NA NA NA NA NA 340 B 380 B 320 350 325 284 260 NA NA NA NA NA 390 B640 B480 450 NAMW-55MW-56
Table 3Summary of Recent Site Groundwater Monitoring DataHighway 49 LandfillCEC Project: 111-370.002Well I.D.Sampling DateOrganics (µg/L)2L Std.Benzene 1Bis(2-ethylhexyl)phthalate 3Carbon Disulfide 700cis-1,2-Dichloroethene 702,4-Dimethylphenol 100Diethylphthalate 6,0002,4 -D 704-4'-DDT 0.1Dieldrin 0Dinoseb 7Endosulfan II 40Endosulfan sulfate 40Endrin 2Endrin aldehyde 2Methylene Chloride 5Trichloroethene 3Vinyl Chloride 0.03Toluene 600Xylenes 500beta-BHC NS1,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350Tetrachloroethene 0.7Tetrahydrofuran NSNaphthalene 6Acetophenone 700Metals (µg/L)Antimony 1Arsenic 10Barium 700Beryllium 4Cadmium 2Calcium NSChromium 10Cobalt 1Copper 1,000Iron300Lead15Manganese 50Nickel 100Selenium 20Thallium 0.2Vanadium 0.3Zinc 1,000Indicator Parameters (mg/L)Alkalinity NSAmmonia- N 1.5Carbon Dioxide NSChloride 250Cyanide 70Sulfate 250Sulfide NSTDS5002L Std. = 15A NCAC 02L .0202 Groundwater Standards or Interim Maximum Allowable Concentrations (IMACs) (Eff. April 1, 2013)Bold values exceed the NCDEQ StandardsBold and highlighted values exceed the NCDEQ Standards yet the analyte concentrations are within the range of naturally-occurring levels.NA = Not AnalyzedNS = Not SpecifiedJ = Method Detection Limit < Reporting Limitcn = Case Narrative10/21/13 4/3/14 10/17/14 4/15/15 10/20/15 4/16/16 10/21/16 4/26/17 10/21/13 4/3/14 10/17/14 4/15/15 10/20/15 4/16/16 10/21/16 4/26/17<1 <1 <1 <1 <1 <1 <1 <0.5 <1 <1 <1 <1 <1 <1 <1 <0.5<5.1 ND30<5 <5 0.52 J <5 <7.5 <5 <5 <5 <5 <5 4.9 J <5 <7.8<1 <1 <1 <1 <1 <1 <1 <2 <1 <1 <1 <1 1 <1 <1 <2<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <7.5 <1 <1 <1 <1 <1 <1 <1 <7.8<5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 0.26 J <5<2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04<1 <1 <1 <1 <1 <1 <1 <2.2 <1 <1 <1 <1 <1 <1 <1 <2.2<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04<1 <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <5<1 <1 <1 <1 <1 <1 <1 <0.5 <1 <1 <1 <1 <1 <1 <1 <0.5<1 <1 <1 <1 <1 <1 <1 <0.5 <1 <1 <1 <1 <1 <1 <1 <0.5<1 <1 <1 1.2 0.71 J <1 0.92 J <0.5 <1 <1 <1 1.7 0.75 J <1 0.56 J <0.5<1 <1 <1 1.5 0.86 J <1 1.3 <1 <1 <1 <1 1.6 1 <1 <1 <1<0.025 <0.025 <0.025 <0.04 <0.04 <0.04 <0.04 <0.038 <0.025 <0.025 <0.025 <0.04 0.018 J <0.04 <0.04 <0.04<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<5 <5 <5 <5 <5 <5 <5 <10 <5 <5 <5 2.2 J <5 <5 5.4 <10<1 <1 <1 0.12 J 0.087 J <1 <1 <0.75 <1 <1 <1 0.12 J 0.10 J <1 <1 <0.78<1 <1 <1 <1 2 <1 <1 <3.8 <1 <1 <1 <1 1.8 <1 <1 <3.9<1 <1 <1 <1 <1 0.17 BJ <1 <3 <1 <1 <1 <1 <1 0.5 BJ 0.32 BJ <3<1 1 <1 0.70 BJ 2.7 <1 0.34 J <1 <1 <1 <1 0.89 J 0.59 J 0.37 J <10.41 J28 37 40 48 64 32 54 51 19 30 17 30 33 31 26 31<0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <1 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <1<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.5 <0.1 <0.1 <0.1 <0.1 <1 0.065 J <0.1 <0.5NA NA NA NA 27,000 18,000 28,000 NA NA NA NA NA 62,000 59,000 59,000 NA<5 <5 <5 <5 2.2 J 0.88 J 0.91 J <5 <5 <5 <5 <5 <5 <5 <5 <5<5 <5 <5 <52.3 J0.44 J 0.83 J <1 <5 <5 <5 <5 0.60 J 0.58 J <5 0.55 J1.8 2 1.4 0.54 J 8.8 B 2.8 B 3.5 1.3 J 1.1 1.1 1.9 1.4 1.1 B 2.6 B 0.98 J 1.7 JNA NA NA NA NA NA NA <100 NA NA NA NA NA NA NA540<1 <1 <1 <1 0.70 J <1 0.41 J <0.5 <1 <1 <1 <1 <1 <1 <1 0.78NA NA NA NA83177916 NA NA NA NA73 799.9 37<5 <5 <5 1.6 J 2.6 J 0.77 J 1.7 J <2 <5 <5 <5 3.1 J 2.5 J 3.0 J 1.6 J 1.7 J<1 <1 1.3 1.9 <1 <1 <1 <2.5 1.1 1 <1 <1 <1 <1 <1 <2.5<0.50.52<0.5 <0.5 <0.5 <0.5 <0.5 <2 <0.50.51<0.5 <0.5 <0.5 <0.5 <0.5 <2<5 <5 <5 <57.6 2.6 BJ 3.5 J<5 <5 <5 <5 <52.1 J 3.4 BJ<5 <513 18 20 9.6 J 22 3.4 J 5.5 J <20 11 15 14 8.3 J 8.7 J 17 5.7 J <20NA NA NA NA 82 24 76 86 NA NA NA NA 150 180 170 180NA NA NA NA <0.1 <0.1 <0.1 NA NA NA NA NA <0.1 <0.1 <0.1 NANA NA NA NA 120 90 170 NA NA NA NA NA 140 170 170 NANA NA NA NA 20 6.5 16 19 NA NA NA NA 7.5 9.1 9.8 14NA NA NA NA NA <0.01 <0.01 <0.01 NA NA NA NA NA <0.01 <0.01 <0.01NA NA NA NA NA NA NA 63 NA NA NA NA NA NA NA 74<1 <1 <1 <1 <1 1.4 <1 NA <1 <1 <1 <1 <1 <1 <1 NANA NA NA NA 230 B 200 B 210 230 NA NA NA NA 320 B 320 B 320 330MW-56AMW-56D
Table 3Summary of Recent Site Groundwater Monitoring DataHighway 49 LandfillCEC Project: 111-370.002Well I.D.Sampling DateOrganics (µg/L)2L Std.Benzene 1Bis(2-ethylhexyl)phthalate 3Carbon Disulfide 700cis-1,2-Dichloroethene 702,4-Dimethylphenol 100Diethylphthalate 6,0002,4 -D 704-4'-DDT 0.1Dieldrin 0Dinoseb 7Endosulfan II 40Endosulfan sulfate 40Endrin 2Endrin aldehyde 2Methylene Chloride 5Trichloroethene 3Vinyl Chloride 0.03Toluene 600Xylenes 500beta-BHC NS1,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350Tetrachloroethene 0.7Tetrahydrofuran NSNaphthalene 6Acetophenone 700Metals (µg/L)Antimony 1Arsenic 10Barium 700Beryllium 4Cadmium 2Calcium NSChromium 10Cobalt 1Copper 1,000Iron300Lead15Manganese 50Nickel 100Selenium 20Thallium 0.2Vanadium 0.3Zinc 1,000Indicator Parameters (mg/L)Alkalinity NSAmmonia- N 1.5Carbon Dioxide NSChloride 250Cyanide 70Sulfate 250Sulfide NSTDS5002L Std. = 15A NCAC 02L .0202 Groundwater Standards or Interim Maximum Allowable Concentrations (IMACs) (Eff. April 1, 2013)Bold values exceed the NCDEQ StandardsBold and highlighted values exceed the NCDEQ Standards yet the analyte concentrations are within the range of naturally-occurring levels.NA = Not AnalyzedNS = Not SpecifiedJ = Method Detection Limit < Reporting Limitcn = Case Narrative10/18/11 10/23/12 4/22/13 10/21/13 11/19/13 4/3/14 10/17/14 4/15/15 10/20/15 4/16/16 10/21/16 4/26/17 6/16/17<1 <1 <1 <1 <1 <1 <1 0.89 J 0.76 J 0.31 J <1 <0.5 0.7NA NA NA <5 NA <5 <5 <5 <5 <5 <5 <7.4 NA<2 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <2<1 <11.2<1 <1 <1 <1 0.61 J 0.39 J <1 <1 <1 <1NA NA NA <1 NA <1 <1 <1 0.29 J 0.24 J <1 <7.4 NANA NA NA <5 NA <5 <5 <5 <5 <5 <5 <5 NANA NA NA <2 NA <2 <2 <2 <2 <2 <2 <2 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NANA NA NA <1 NA 3.2 P <1 <1 <1 <1 0.66 JP <2.3 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NANA NA NA <0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA<1 <1 1.1 <1 1 <1 <1 0.71 J <1 <1 <1 <5 <5<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 <0.5<1 <17.2 13 13 16 11 3.9 3.2 4.6 4.8 3.3 cn 0.59<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 <0.5<2 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1NA NA NA 0.25 NA <0.25 <0.025 <0.04 0.032 J <0.04 <0.04 <0.037NA<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<10 <10 <5 <5 <5 <5 <5 <5 1.6 J <5 1.1 J <10 <10NA NA NA <1 NA <1 <1 <1 <1 <1 <1 <0.74 NANA NA NA <1 NA <1 <1 <1 <1 <1 <1 <3.7 NA<6 <6 <1 <1 <1 <1 <1 <1 <1 0.2 BJ 0.2 BJ <3 NA<10 <10 <10 5 NA <5 1.7 <10 1.8 1.5 1.5 1.2 NA74.1 J 152 79 380 NA 600 410 310 410 440 430 450 NA<1 <1 <0.4 <0.4 <0.4 0.46 <0.4 <0.4 <0.4 <0.4 <0.4 <1 NA<1 <1 <2 <0.1 ND <0.1 <0.1 <0.1 <0.1 0.058 J <0.1 <0.5 NANA NA NA NA NA NA NA NA 130,000 120,000 120,000 NA NA<10 <10 <5 <5 NA13<5 <5 1.8 J 1.4 J 2.2 J <5 NA<10 <10 <2524NA23 64 11 47 46 63 17NA<10 <10 <5 3.3 NA 16 14 8.3 J 2.7 B 3.8 B 8.9 0.68 J NANA NA NA NA NA NA NA NA NA NA NA47,000NA<10 <10 <10 <1 NA 6 <1 <1 0.40 J 0.63 J 0.90 J 0.4 J NANA NA NA NA NA NA NA NA19,000 19,000 27,000 10,000NA<50 <50 <40 13 NA 21 7.2 20 8.9 10 8.3 15 NA<10 <10 <10 5.7 NA <5 1.8 <10 2.5 <1 <1 <2.5 NA<5.5 <5.5 NA <0.5 NA0.56<0.5 <0.5 <0.5 <0.5 <0.5 <2 NA<256.2 J<50 <5 NA51<5 <54.8 J 7.6 B 9.1<5 NA117 <10 <20 180 NA 200 170 0.046 93 10 28 17 J NANA153 692 700 NA NA NA NA NA 500 700 630 880 NANA NA NA NA NA NA NA NA 1.7 1.5 2.2 NA NANA NA NA NA NA NA NA NA 700 1200 1100 NA NA13.5 15.4 63 NA NA NA NA NA 39 41 61 73 NANA NA NA NA NA NA NA NA NA <0.01 <0.02 <0.10 NA12.1 J 31.4 120 NA NA NA NA NA NA NA NA 150 NANA NA NA <1 NA <1 <1 <1 <1 <1 <1 NA NA2301020 1100NA NA NA NA NA890 B 850 B 1100 1300NAMW-57
Table 3Summary of Recent Site Groundwater Monitoring DataHighway 49 LandfillCEC Project: 111-370.002Well I.D.Sampling DateOrganics (µg/L)2L Std.Benzene 1Bis(2-ethylhexyl)phthalate 3Carbon Disulfide 700cis-1,2-Dichloroethene 702,4-Dimethylphenol 100Diethylphthalate 6,0002,4 -D 704-4'-DDT 0.1Dieldrin 0Dinoseb 7Endosulfan II 40Endosulfan sulfate 40Endrin 2Endrin aldehyde 2Methylene Chloride 5Trichloroethene 3Vinyl Chloride 0.03Toluene 600Xylenes 500beta-BHC NS1,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350Tetrachloroethene 0.7Tetrahydrofuran NSNaphthalene 6Acetophenone 700Metals (µg/L)Antimony 1Arsenic 10Barium 700Beryllium 4Cadmium 2Calcium NSChromium 10Cobalt 1Copper 1,000Iron300Lead15Manganese 50Nickel 100Selenium 20Thallium 0.2Vanadium 0.3Zinc 1,000Indicator Parameters (mg/L)Alkalinity NSAmmonia- N 1.5Carbon Dioxide NSChloride 250Cyanide 70Sulfate 250Sulfide NSTDS5002L Std. = 15A NCAC 02L .0202 Groundwater Standards or Interim Maximum Allowable Concentrations (IMACs) (Eff. April 1, 2013)Bold values exceed the NCDEQ StandardsBold and highlighted values exceed the NCDEQ Standards yet the analyte concentrations are within the range of naturally-occurring levels.NA = Not AnalyzedNS = Not SpecifiedJ = Method Detection Limit < Reporting Limitcn = Case Narrative10/21/13 11/19/13 4/3/14 10/17/14 4/15/15 10/20/15 4/16/16 10/21/16 4/26/17 6/16/17 4/16/16 10/21/16 4/26/17 4/16/16 10/21/16 4/26/17<1 <1 <1 <1 0.16 J <1 <1 <1 0.6 <0.5 <1 <1 <0.5 <1 <1 <0.5<5.2 NA <5 <5 <5 <5 1.7 J <5 <7.5 NA NA NA NA NA NA NA<1 <1 <1 <1 <1 <1 <1 <1 <2 <2 <1 <1 <2 <1 <1 <2<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 NA <1 1.5 <1 <1 <1 <1 <7.5 NA NA NA NA NA NA NA<5 NA <5 <5 <5 <5 <5 <5 <5 NA NA NA NA NA NA NA<2 NA <2 <2 <2 <2 <2 <2 <2 NA NA NA NA NA NA NA<0.04 NA <0.04 <0.04 <0.04 <0.04 0.021 J <0.04 <0.04 NA NA NA NA NA NA NA<0.04 NA <0.04 <0.04 <0.040.016 J<0.04 <0.04 <0.04 NA NA NA NA NA NA NA3.4 NA 3.1 <1 <1 <1 <1 0.78 J <2.4 NA NA NA NA NA NA NA<0.04 NA <0.04 <0.04 <0.04 0.011 JP <0.04 <0.04 <0.04 NA NA NANA NA NA NA<0.04 NA <0.04 <0.04 <0.04 <0.04 <0.04 0.016 JP <0.04 NA NA NANA NA NA NA<0.04 NA <0.04 <0.04 <0.04 0.012 JP 0.029 J 0.018 JP <0.04 NA NA NA NA NA NA NA<0.04 NA <0.04 <0.04 <0.04 0.013 J 0.024 J <0.04 <0.04 NA NA NA NA NA NA NA<1 <1 <1 <1 <1 <1 <1 <1 <5 <5 <1 <1 <5 <1 <1 <5<1 <1 <1 <1 <1 <1 <1 <1 <0.5 <0.5 <1 <1 <0.5 <1 <1 <0.54.5 4.5 3.3 4.5 1.1 1.5 1.9 2.5 1.1 cn<0.5 <1 <1 <0.5 <1 <1 <0.5<1 <1 <1 <1 1.5 0.78 J <1 0.62 J <0.5 <0.5 <1 <1 <0.5 <1 <1 <0.5<1 <1 <1 <1 1.9 0.99 J <1 1.1 <1 <1 <1 <1 <1 <1 <1 <10.25 NA <0.25 <0.025 0.071 <0.04 <0.04 <0.04 <0.037 NA NA NA NANA NA NA<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1<5 <5 <5 <5 2.2 J 4.4 J <5 5.9 <10 <10 <5 <5 <10 <5 <5 <10<1 NA <1 <1 0.15 J 0.14 J <1 <1 <0.75 NA NA NA NA NA NA NA<1 NA <1 <1 <1 2.5 0.34 J <1 <3.8 NA NA NA NA NA NA NA<1 <1 <1 <1 <1 <1 0.7 BJ 0.26 BJ <3 NA <1 <1 <1 <1 <1 <15.9 NA <1 <1 1.5 B 1.3 <1 <1 0.18 J NA <1 0.39 J 0.46 J <1 0.32 J0.47 J230 NA 170 110 100 68 90 81 93 NA 40 49 56 41 50 61<0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <1 NA <0.4 <0.4 <0.4 <0.4 <0.4 <0.4<0.1 ND <0.1 <0.1 0.052 J <0.1 0.31 <0.1 0.38 J NA <0.1 <0.1 <0.5 <0.1 <0.1 <0.5NA NA NA NA NA 220,000 240,000 240,000 NA NA 14,000 18,000 NA 15,000 19,000 NA<5 NA <5 <5 <5 1.0 J 1.7 J 0.72 J <5 NA <5 <5 <5 <5 <5 <517NA <5 <5 0.33 J1.5 J 1.5 J<51.1NA 0.29 J <52.40.38 J <52.72.9 NA 5.7 3.2 6.3 3.1 B 15 B 2.1 16 NA 0.8 BJ 1.3 4 1.1 B 0.84 J4NA NA NA NA NA NA NA NA300NA NA NA3000NA NA3100<1 NA <1 <1 <1 <1 0.27 J <1 0.2 J NA <1 <1 1.2 <1 <1 1.3NA NA NA NA NA130 160 310 220NA130 170 230 130 170 260100NA 76 69 83 78 89 82100NA <5 0.71 J 1.5 J <5 0.71 J 1.6 J4.7 NA 3.4 3.2 5.2 2.5 <1 <1 <2.5 NA <1 <1 <2.5 <1 <1 <2.5<0.5 NA0.54<0.5 <0.5 <0.5 <0.5 <0.5 <2 NA NA NA <2 NA NA <2<5 NA5.8 11 12 10 12 B 7.9 21NA2.3 BJ 1.7 J 9.9 2.1 BJ 1.6 J 9.896 NA 69 48 15 14 10 3.3 J 8.4 J NA <10 4.3 J 9.8 J <10 1.6 J 15 JNANA NA NA NA NA 740 850 870 920 NA NA NA NA NA NA NANA NA NA NA NA 0.17 <0.1 0.075 J NA NA NA NA NA NA NA NANA NA NA NA NA 970 940 1400 NA NA NA NA NA NA NA NANA NA NA NA NA 57 59 76 75 NA NA NA NA NA NA NANA NA NA NA NA NA <0.01 <0.01 <0.01 NA NA NA NA NA NA NANA NA NA NA NA NA NA NA330NA NA NA NA NA NA NA<1 NA <1 <1 <1 1.1 <1 0.74 J NA NA NA NA NA NA NA NANA NA NA NA NA1400 B 1400 B 1500 1500NANANANANANANAMW-57DSW-1SW-2

APPENDIX A

APPENDIX B

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
TestAmerica Job ID: 500-127325-1
Client Project/Site: NC Highway 49 Landfill
Revision: 1
For:
Civil & Environmental Consultants Inc
1900 Center Park Drive
Suite A
Charlotte, North Carolina 28217
Attn: Phillip Pressley
Authorized for release by:
6/5/2017 9:26:17 AM
Robin Kintz, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
TestAmerica Job ID: 500-127325-1
Page 2 of 90 TestAmerica Chicago6/5/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .58
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .60
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .79
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .84
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .85
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .90
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Case Narrative
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-127325-1
Project/Site: NC Highway 49 Landfill
Job ID: 500-127325-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-127325-1
Comments
The report was revised because samples were submitted for 2 sites, separate chains of custody, but these were logged in a single job.
The sites need to be divided into separate jobs and invoices. Also, the lab needed to add flags to the data, see the GC/MS VOA section for
details.
No additional comments.
Receipt
The samples were received on 4/28/2017 9:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperatures of the 8 coolers at receipt time were 0.0º C, 0.1º C, 1.9º C, 2.0º C, 2.1º C, 2.4º C, 3.3º C and 3.4º C.
Receipt Exceptions
Only received Metals and VOAs vials for sample SW-1 (500-127325-7), logged in only for Metals and VOAs analysis.
GC/MS VOA
Method(s) 8260B: All positive detects for Vinyl Chloride correlate with the presences of a non-target analyte, Freon 151, which is present in
the samples. It has been demonstrated that Freon 151 degrades to Vinyl Chloride on the GC/MS instrument used for analysis of these
samples, most likely due to the presence of active sites on the instrument that have developed over time. The results for Vinyl Chloride
have been flagged with a "cn" flag to denote the high bias associated with the reported results for Vinyl Chloride in the samples: MW-56
(500-127325-2), MW-57 (500-127325-5), MW-57D (500-127325-6) and Duplicate (500-127325-9). In the absence of high bias due to
degradation of Freon 151, it is possible that some or most samples would be non-detect (ND) for Vinyl Chloride.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
Method(s) 8081B: The continuing calibration verification (CCV) associated with batch 500-383721 recovered low and outside control limit
for surrogate DCB Decachlorobiphenyl (25.1%D). The samples associated with this CCV had surrogate recoveries within control limits;
therefore, the data have been reported. The following sample is impacted: (CCV 500-383721/30).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Detection Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Client Sample ID: MW-55 Lab Sample ID: 500-127325-1
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.18 200.8
Barium 2.5 ug/L0.37 Total/NA1120200.8
Cobalt 1.0 ug/L0.27 Total/NA15.8 200.8
Copper 2.0 ug/L0.63 Total/NA15.3 200.8
Iron 100 ug/L38 Total/NA1810200.8
Lead 0.50 ug/L0.16 Total/NA10.31 J 200.8
Manganese 2.5 ug/L1.1 Total/NA198200.8
Nickel 2.0 ug/L0.92 Total/NA121200.8
Vanadium 5.0 ug/L2.0 Total/NA16.8 200.8
Zinc 20 ug/L8.1 Total/NA110J200.8
Chloride 2.0 mg/L1.7 Total/NA10149056A
Sulfate 4.0 mg/L1.9 Total/NA20959056A
Alkalinity 5.0 mg/L3.7 Total/NA1150SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1350SM 2540C
Client Sample ID: MW-56 Lab Sample ID: 500-127325-2
Acetone
RL
5.0 ug/L
MDL
1.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1168260B
Benzene 0.50 ug/L0.15 Total/NA11.7 8260B
cis-1,2-Dichloroethene 1.0 ug/L0.41 Total/NA12.1 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA16.6 cn 8260B
Arsenic 1.0 ug/L0.15 Total/NA10.28 J 200.8
Barium 2.5 ug/L0.37 Total/NA1170200.8
Cobalt 1.0 ug/L0.27 Total/NA166200.8
Copper 2.0 ug/L0.63 Total/NA14.0 200.8
Iron 100 ug/L38 Total/NA14100200.8
Lead 0.50 ug/L0.16 Total/NA10.17 J 200.8
Manganese 25 ug/L11 Total/NA1011000200.8
Nickel 2.0 ug/L0.92 Total/NA19.7 200.8
Chloride 2.0 mg/L1.7 Total/NA10119056A
Sulfate 2.0 mg/L0.95 Total/NA10679056A
Alkalinity 5.0 mg/L3.7 Total/NA1340SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1450SM 2540C
Client Sample ID: MW-56A Lab Sample ID: 500-127325-3
Barium
RL
2.5 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA151200.8
Copper 2.0 ug/L0.63 Total/NA11.3 J 200.8
Manganese 2.5 ug/L1.1 Total/NA116200.8
Chloride 2.0 mg/L1.7 Total/NA10199056A
Sulfate 2.0 mg/L0.95 Total/NA10639056A
Alkalinity 5.0 mg/L3.7 Total/NA186SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1230SM 2540C
Client Sample ID: MW-56D Lab Sample ID: 500-127325-4
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.41 200.8
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Client Sample ID: MW-56D (Continued)Lab Sample ID: 500-127325-4
Barium
RL
2.5 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA131200.8
Cobalt 1.0 ug/L0.27 Total/NA10.55 J 200.8
Copper 2.0 ug/L0.63 Total/NA11.7 J 200.8
Iron 100 ug/L38 Total/NA1540200.8
Lead 0.50 ug/L0.16 Total/NA10.78 200.8
Manganese 2.5 ug/L1.1 Total/NA137200.8
Nickel 2.0 ug/L0.92 Total/NA11.7 J 200.8
Chloride 2.0 mg/L1.7 Total/NA10149056A
Sulfate 2.0 mg/L0.95 Total/NA10749056A
Alkalinity 5.0 mg/L3.7 Total/NA1180SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1330SM 2540C
Client Sample ID: MW-57 Lab Sample ID: 500-127325-5
Vinyl chloride
RL
0.50 ug/L
MDL
0.20
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1cn3.3 8260B
Arsenic 1.0 ug/L0.15 Total/NA11.2 200.8
Barium 2.5 ug/L0.37 Total/NA1450200.8
Cobalt 1.0 ug/L0.27 Total/NA117200.8
Copper 2.0 ug/L0.63 Total/NA10.68 J 200.8
Iron 100 ug/L38 Total/NA147000200.8
Lead 0.50 ug/L0.16 Total/NA10.40 J 200.8
Manganese 25 ug/L11 Total/NA1010000200.8
Nickel 2.0 ug/L0.92 Total/NA115200.8
Zinc 20 ug/L8.1 Total/NA117J200.8
Chloride 4.0 mg/L3.4 Total/NA20739056A
Sulfate 4.0 mg/L1.9 Total/NA201509056A
Alkalinity 5.0 mg/L3.7 Total/NA1880SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA11300SM 2540C
Client Sample ID: MW-57D Lab Sample ID: 500-127325-6
Acetone
RL
5.0 ug/L
MDL
1.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA15.5 8260B
Benzene 0.50 ug/L0.15 Total/NA10.60 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA11.1 cn 8260B
Arsenic 1.0 ug/L0.15 Total/NA10.18 J 200.8
Barium 2.5 ug/L0.37 Total/NA193200.8
Cadmium 0.50 ug/L0.15 Total/NA10.38 J 200.8
Cobalt 1.0 ug/L0.27 Total/NA11.1 200.8
Copper 2.0 ug/L0.63 Total/NA116200.8
Iron 100 ug/L38 Total/NA1300200.8
Lead 0.50 ug/L0.16 Total/NA10.20 J 200.8
Manganese 2.5 ug/L1.1 Total/NA1220200.8
Nickel 2.0 ug/L0.92 Total/NA1100200.8
Vanadium 5.0 ug/L2.0 Total/NA121200.8
Zinc 20 ug/L8.1 Total/NA18.4 J 200.8
Chloride 10 mg/L8.5 Total/NA50759056A
Sulfate 10 mg/L4.8 Total/NA503309056A
Alkalinity 5.0 mg/L3.7 Total/NA1920SM 2320B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Client Sample ID: MW-57D (Continued)Lab Sample ID: 500-127325-6
Total Dissolved Solids
RL
10 mg/L
MDL
4.3
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11500SM 2540C
Client Sample ID: SW-1 Lab Sample ID: 500-127325-7
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.46 200.8
Barium 2.5 ug/L0.37 Total/NA156200.8
Cobalt 1.0 ug/L0.27 Total/NA12.4 200.8
Copper 2.0 ug/L0.63 Total/NA14.0 200.8
Iron 100 ug/L38 Total/NA13000200.8
Manganese 2.5 ug/L1.1 Total/NA1230200.8
Nickel 2.0 ug/L0.92 Total/NA11.5 J 200.8
Lead 0.50 ug/L0.16 Total/NA11.2 200.8
Vanadium 5.0 ug/L2.0 Total/NA19.9 200.8
Zinc 20 ug/L8.1 Total/NA19.8 J 200.8
Client Sample ID: SW-2 Lab Sample ID: 500-127325-8
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.47 200.8
Barium 2.5 ug/L0.37 Total/NA161200.8
Cobalt 1.0 ug/L0.27 Total/NA12.7 200.8
Copper 2.0 ug/L0.63 Total/NA14.0 200.8
Iron 100 ug/L38 Total/NA13100200.8
Manganese 2.5 ug/L1.1 Total/NA1260200.8
Nickel 2.0 ug/L0.92 Total/NA11.6 J 200.8
Lead 0.50 ug/L0.16 Total/NA11.3 200.8
Vanadium 5.0 ug/L2.0 Total/NA19.8 200.8
Zinc 20 ug/L8.1 Total/NA115J200.8
Client Sample ID: Duplicate Lab Sample ID: 500-127325-9
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.68 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA13.3 cn 8260B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Method Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL CHI
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL CHI
SW8468081BOrganochlorine Pesticides (GC)TAL CHI
SW8468082APolychlorinated Biphenyls (PCBs) by Gas Chromatography TAL CHI
SW8468151AHerbicides (GC)TAL CHI
EPA200.8 Metals (ICP/MS)TAL CHI
EPA245.1 Mercury (CVAA)TAL CHI
SW8469014Cyanide TAL CHI
SW8469056AAnions, Ion Chromatography TAL CHI
SMSM 2320B Alkalinity TAL CHI
SMSM 2540C Solids, Total Dissolved (TDS)TAL CHI
Protocol References:
EPA = US Environmental Protection Agency
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Sample Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-127325-1 MW-55 Water 04/26/17 12:10 04/28/17 09:00
500-127325-2 MW-56 Water 04/26/17 12:10 04/28/17 09:00
500-127325-3 MW-56A Water 04/26/17 08:45 04/28/17 09:00
500-127325-4 MW-56D Water 04/26/17 08:30 04/28/17 09:00
500-127325-5 MW-57 Water 04/26/17 09:45 04/28/17 09:00
500-127325-6 MW-57D Water 04/26/17 09:50 04/28/17 09:00
500-127325-7 SW-1 Water 04/26/17 12:10 04/28/17 09:00
500-127325-8 SW-2 Water 04/26/17 13:10 04/28/17 09:00
500-127325-9 Duplicate Water 04/26/17 00:00 04/28/17 09:00
TestAmerica Chicago
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-1Client Sample ID: MW-55
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <5.0 5.0 1.7 ug/L 05/07/17 22:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 4.2 ug/L 05/07/17 22:59 1Acetonitrile<10
100 23 ug/L 05/07/17 22:59 1Acrolein<100
20 4.5 ug/L 05/07/17 22:59 1Acrylonitrile<20
0.50 0.15 ug/L 05/07/17 22:59 1Benzene<0.50
1.0 0.43 ug/L 05/07/17 22:59 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/07/17 22:59 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/07/17 22:59 1Bromoform<1.0
2.0 0.80 ug/L 05/07/17 22:59 1Bromomethane<2.0
5.0 2.1 ug/L 05/07/17 22:59 12-Butanone (MEK)<5.0
2.0 0.45 ug/L 05/07/17 22:59 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/07/17 22:59 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/07/17 22:59 1Chlorobenzene<1.0
1.0 0.23 ug/L 05/07/17 22:59 12-Chloro-1,3-butadiene <1.0
1.0 0.51 ug/L 05/07/17 22:59 1Chloroethane<1.0
2.0 0.37 ug/L 05/07/17 22:59 1Chloroform<2.0
1.0 0.32 ug/L 05/07/17 22:59 1Chloromethane<1.0
2.5 0.86 ug/L 05/07/17 22:59 13-Chloropropene <2.5
1.0 0.41 ug/L 05/07/17 22:59 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/07/17 22:59 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/07/17 22:59 1Dibromochloromethane<1.0
5.0 2.0 ug/L 05/07/17 22:59 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/07/17 22:59 11,2-Dibromoethane <1.0
1.0 0.27 ug/L 05/07/17 22:59 1Dibromomethane<1.0
1.0 0.40 ug/L 05/07/17 22:59 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 05/07/17 22:59 11,4-Dichlorobenzene <1.0
1.0 0.33 ug/L 05/07/17 22:59 11,2-Dichlorobenzene <1.0
2.0 0.67 ug/L 05/07/17 22:59 1Dichlorodifluoromethane<2.0
1.0 0.41 ug/L 05/07/17 22:59 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/07/17 22:59 11,2-Dichloroethane <1.0
1.0 0.39 ug/L 05/07/17 22:59 11,1-Dichloroethene <1.0
1.0 0.44 ug/L 05/07/17 22:59 12,2-Dichloropropane <1.0
1.0 0.43 ug/L 05/07/17 22:59 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/07/17 22:59 11,3-Dichloropropane <1.0
1.0 0.30 ug/L 05/07/17 22:59 11,1-Dichloropropene <1.0
0.50 0.18 ug/L 05/07/17 22:59 1Ethylbenzene<0.50
2.5 0.53 ug/L 05/07/17 22:59 1Ethyl methacrylate <2.5
1.0 0.45 ug/L 05/07/17 22:59 1Hexachlorobutadiene<1.0
5.0 1.6 ug/L 05/07/17 22:59 12-Hexanone <5.0
2.5 0.66 ug/L 05/07/17 22:59 1Iodomethane<2.5
100 36 ug/L 05/07/17 22:59 1Isobutyl alcohol <100
10 2.5 ug/L 05/07/17 22:59 1Methacrylonitrile<10
5.0 1.6 ug/L 05/07/17 22:59 1Methylene Chloride <5.0
2.5 0.55 ug/L 05/07/17 22:59 1Methyl methacrylate <2.5
5.0 2.2 ug/L 05/07/17 22:59 14-Methyl-2-pentanone (MIBK)<5.0
10 4.8 ug/L 05/07/17 22:59 1Propionitrile<10
1.0 0.39 ug/L 05/07/17 22:59 1Styrene<1.0
1.0 0.46 ug/L 05/07/17 22:59 11,1,1,2-Tetrachloroethane <1.0
1.0 0.40 ug/L 05/07/17 22:59 11,1,2,2-Tetrachloroethane <1.0
TestAmerica Chicago
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-1Client Sample ID: MW-55
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Tetrachloroethene <1.0 1.0 0.37 ug/L 05/07/17 22:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 1.9 ug/L 05/07/17 22:59 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/07/17 22:59 1Toluene<0.50
5.0 1.2 ug/L 05/07/17 22:59 1trans-1,4-Dichloro-2-butene <5.0
1.0 0.35 ug/L 05/07/17 22:59 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/07/17 22:59 1trans-1,3-Dichloropropene <1.0
1.0 0.34 ug/L 05/07/17 22:59 11,2,4-Trichlorobenzene <1.0
1.0 0.38 ug/L 05/07/17 22:59 11,1,1-Trichloroethane <1.0
1.0 0.35 ug/L 05/07/17 22:59 11,1,2-Trichloroethane <1.0
0.50 0.16 ug/L 05/07/17 22:59 1Trichloroethene<0.50
1.0 0.43 ug/L 05/07/17 22:59 1Trichlorofluoromethane<1.0
1.0 0.41 ug/L 05/07/17 22:59 11,2,3-Trichloropropane <1.0
2.0 0.91 ug/L 05/07/17 22:59 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/07/17 22:59 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/07/17 22:59 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)104 75-126 05/07/17 22:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)103 05/07/17 22:59 175-120
4-Bromofluorobenzene (Surr)110 05/07/17 22:59 172-124
Dibromofluoromethane 90 05/07/17 22:59 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.75 0.75 0.23 ug/L 05/01/17 15:19 05/05/17 14:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.75 0.20 ug/L 05/01/17 15:19 05/05/17 14:46 1Acenaphthylene<0.75
3.7 0.49 ug/L 05/01/17 15:19 05/05/17 14:46 1Acetophenone<3.7
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 14:46 12-Acetylaminofluorene <7.5
7.5 2.8 ug/L 05/01/17 15:19 05/05/17 14:46 14-Aminobiphenyl <7.5
0.75 0.25 ug/L 05/01/17 15:19 05/05/17 14:46 1Anthracene<0.75
0.15 0.042 ug/L 05/01/17 15:19 05/05/17 14:46 1Benzo[a]anthracene <0.15
0.15 0.074 ug/L 05/01/17 15:19 05/05/17 14:46 1Benzo[a]pyrene <0.15
0.15 0.060 ug/L 05/01/17 15:19 05/05/17 14:46 1Benzo[b]fluoranthene <0.15
0.75 0.28 ug/L 05/01/17 15:19 05/05/17 14:46 1Benzo[g,h,i]perylene <0.75
0.15 0.048 ug/L 05/01/17 15:19 05/05/17 14:46 1Benzo[k]fluoranthene <0.15
15 4.5 ug/L 05/01/17 15:19 05/05/17 14:46 1Benzyl alcohol <15
1.5 0.21 ug/L 05/01/17 15:19 05/05/17 14:46 1Bis(2-chloroethoxy)methane <1.5
1.5 0.22 ug/L 05/01/17 15:19 05/05/17 14:46 1Bis(2-chloroethyl)ether <1.5
7.5 1.3 ug/L 05/01/17 15:19 05/05/17 14:46 1Bis(2-ethylhexyl) phthalate <7.5
3.7 0.40 ug/L 05/01/17 15:19 05/05/17 14:46 14-Bromophenyl phenyl ether <3.7
1.5 0.36 ug/L 05/01/17 15:19 05/05/17 14:46 1Butyl benzyl phthalate <1.5
7.5 1.5 ug/L 05/01/17 15:19 05/05/17 14:46 14-Chloroaniline <7.5
7.5 2.5 ug/L 05/01/17 15:19 05/05/17 14:46 1Chlorobenzilate<7.5
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 14:46 14-Chloro-3-methylphenol <7.5
1.5 0.18 ug/L 05/01/17 15:19 05/05/17 14:46 12-Chloronaphthalene <1.5
3.7 0.42 ug/L 05/01/17 15:19 05/05/17 14:46 12-Chlorophenol <3.7
3.7 0.47 ug/L 05/01/17 15:19 05/05/17 14:46 14-Chlorophenyl phenyl ether <3.7
0.15 0.051 ug/L 05/01/17 15:19 05/05/17 14:46 1Chrysene<0.15
7.5 4.1 ug/L 05/01/17 15:19 05/05/17 14:46 1Diallate<7.5
0.22 0.038 ug/L 05/01/17 15:19 05/05/17 14:46 1Dibenz(a,h)anthracene <0.22
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-1Client Sample ID: MW-55
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.5 1.5 0.20 ug/L 05/01/17 15:19 05/05/17 14:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.7 1.3 ug/L 05/01/17 15:19 05/05/17 14:46 13,3'-Dichlorobenzidine <3.7
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 14:46 12,4-Dichlorophenol <7.5
7.5 2.6 ug/L 05/01/17 15:19 05/05/17 14:46 12,6-Dichlorophenol <7.5
1.5 0.27 ug/L 05/01/17 15:19 05/05/17 14:46 1Diethyl phthalate <1.5
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 14:46 1Dimethoate<7.5
30 2.2 ug/L 05/01/17 15:19 05/05/17 14:46 17,12-Dimethylbenz(a)anthracene <30
30 13 ug/L 05/01/17 15:19 05/05/17 14:46 13,3'-Dimethylbenzidine <30
7.5 1.3 ug/L 05/01/17 15:19 05/05/17 14:46 12,4-Dimethylphenol <7.5
1.5 0.23 ug/L 05/01/17 15:19 05/05/17 14:46 1Dimethyl phthalate <1.5
3.7 0.54 ug/L 05/01/17 15:19 05/05/17 14:46 1Di-n-butyl phthalate <3.7
15 4.4 ug/L 05/01/17 15:19 05/05/17 14:46 14,6-Dinitro-2-methylphenol <15
15 6.4 ug/L 05/01/17 15:19 05/05/17 14:46 12,4-Dinitrophenol <15
0.75 0.055 ug/L 05/01/17 15:19 05/05/17 14:46 12,6-Dinitrotoluene <0.75
0.75 0.18 ug/L 05/01/17 15:19 05/05/17 14:46 12,4-Dinitrotoluene <0.75
7.5 0.78 ug/L 05/01/17 15:19 05/05/17 14:46 1Di-n-octyl phthalate <7.5
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 14:46 1Diphenylamine<7.5
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 14:46 1Disulfoton<7.5
15 2.8 ug/L 05/01/17 15:19 05/05/17 14:46 1Ethyl methanesulfonate <15
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 14:46 1Ethyl Parathion <7.5
30 22 ug/L 05/01/17 15:19 05/05/17 14:46 1Famphur<30
0.75 0.34 ug/L 05/01/17 15:19 05/05/17 14:46 1Fluoranthene<0.75
0.75 0.18 ug/L 05/01/17 15:19 05/05/17 14:46 1Fluorene<0.75
0.37 0.059 ug/L 05/01/17 15:19 05/05/17 14:46 1Hexachlorobenzene<0.37
15 4.8 ug/L 05/01/17 15:19 05/05/17 14:46 1Hexachlorocyclopentadiene<15
3.7 0.45 ug/L 05/01/17 15:19 05/05/17 14:46 1Hexachloroethane<3.7
15 3.5 ug/L 05/01/17 15:19 05/05/17 14:46 1Hexachloropropene<15
0.15 0.056 ug/L 05/01/17 15:19 05/05/17 14:46 1Indeno[1,2,3-cd]pyrene <0.15
15 5.1 ug/L 05/01/17 15:19 05/05/17 14:46 1Isodrin<15
1.5 0.28 ug/L 05/01/17 15:19 05/05/17 14:46 1Isophorone<1.5
7.5 2.9 ug/L 05/01/17 15:19 05/05/17 14:46 1Isosafrole<7.5
7.5 1.2 ug/L 05/01/17 15:19 05/05/17 14:46 1Kepone<7.5
3.7 0.99 ug/L 05/01/17 15:19 05/05/17 14:46 1m-Dinitrobenzene <3.7
30 7.6 ug/L 05/01/17 15:19 05/05/17 14:46 1Methapyrilene<30
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 14:46 13-Methylcholanthrene <7.5
30 4.4 ug/L 05/01/17 15:19 05/05/17 14:46 1Methyl methanesulfonate <30
1.5 0.049 ug/L 05/01/17 15:19 05/05/17 14:46 12-Methylnaphthalene <1.5
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 14:46 1Methyl parathion <7.5
1.5 0.23 ug/L 05/01/17 15:19 05/05/17 14:46 12-Methylphenol <1.5
1.5 0.33 ug/L 05/01/17 15:19 05/05/17 14:46 13 & 4 Methylphenol <1.5
0.75 0.23 ug/L 05/01/17 15:19 05/05/17 14:46 1Naphthalene<0.75
30 29 ug/L 05/01/17 15:19 05/05/17 14:46 11,4-Naphthoquinone <30
15 4.4 ug/L 05/01/17 15:19 05/05/17 14:46 11-Naphthylamine <15
15 6.8 ug/L 05/01/17 15:19 05/05/17 14:46 12-Naphthylamine <15
3.7 0.96 ug/L 05/01/17 15:19 05/05/17 14:46 12-Nitroaniline <3.7
7.5 1.3 ug/L 05/01/17 15:19 05/05/17 14:46 13-Nitroaniline <7.5
7.5 1.2 ug/L 05/01/17 15:19 05/05/17 14:46 14-Nitroaniline <7.5
0.75 0.33 ug/L 05/01/17 15:19 05/05/17 14:46 1Nitrobenzene<0.75
7.5 2.3 ug/L 05/01/17 15:19 05/05/17 14:46 15-Nitro-o-toluidine <7.5
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-1Client Sample ID: MW-55
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.5 7.5 1.9 ug/L 05/01/17 15:19 05/05/17 14:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 5.5 ug/L 05/01/17 15:19 05/05/17 14:46 14-Nitrophenol <15
15 6.4 ug/L 05/01/17 15:19 05/05/17 14:46 1N-Nitrosodiethylamine <15
7.5 3.5 ug/L 05/01/17 15:19 05/05/17 14:46 1N-Nitrosodimethylamine <7.5
7.5 3.1 ug/L 05/01/17 15:19 05/05/17 14:46 1N-Nitrosodi-n-butylamine <7.5
0.37 0.11 ug/L 05/01/17 15:19 05/05/17 14:46 1N-Nitrosodi-n-propylamine <0.37
1.5 0.28 ug/L 05/01/17 15:19 05/05/17 14:46 1N-Nitrosodiphenylamine <1.5
15 5.6 ug/L 05/01/17 15:19 05/05/17 14:46 1N-Nitrosomethylethylamine <15
7.5 2.6 ug/L 05/01/17 15:19 05/05/17 14:46 1N-Nitrosopiperidine <7.5
7.5 2.5 ug/L 05/01/17 15:19 05/05/17 14:46 1N-Nitrosopyrrolidine <7.5
15 4.1 ug/L 05/01/17 15:19 05/05/17 14:46 1o,o',o''-Triethylphosphorothioate <15
30 5.9 ug/L 05/01/17 15:19 05/05/17 14:46 1o-Toluidine <30
1.5 0.28 ug/L 05/01/17 15:19 05/05/17 14:46 12,2'-oxybis[1-chloropropane]<1.5
7.5 2.2 ug/L 05/01/17 15:19 05/05/17 14:46 1p-Dimethylamino azobenzene <7.5
7.5 2.1 ug/L 05/01/17 15:19 05/05/17 14:46 1Pentachlorobenzene<7.5
7.5 2.7 ug/L 05/01/17 15:19 05/05/17 14:46 1Pentachloronitrobenzene<7.5
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 14:46 1Phenacetin<7.5
0.75 0.22 ug/L 05/01/17 15:19 05/05/17 14:46 1Phenanthrene<0.75
3.7 0.50 ug/L 05/01/17 15:19 05/05/17 14:46 1Phenol<3.7
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 14:46 1Phorate<7.5
60 12 ug/L 05/01/17 15:19 05/05/17 14:46 1p-Phenylene diamine <60
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 14:46 1Pronamide<7.5
0.75 0.32 ug/L 05/01/17 15:19 05/05/17 14:46 1Pyrene<0.75
7.5 3.0 ug/L 05/01/17 15:19 05/05/17 14:46 1Safrole<7.5
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 14:46 1sym-Trinitrobenzene <7.5
7.5 7.5 ug/L 05/01/17 15:19 05/05/17 14:46 12,3,7,8-TCDD (Screen)<7.5
3.7 0.43 ug/L 05/01/17 15:19 05/05/17 14:46 11,2,4,5-Tetrachlorobenzene <3.7
3.7 0.56 ug/L 05/01/17 15:19 05/05/17 14:46 12,3,4,6-Tetrachlorophenol <3.7
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 14:46 1Thionazin<7.5
3.7 0.53 ug/L 05/01/17 15:19 05/05/17 14:46 12,4,6-Trichlorophenol <3.7
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 14:46 12,4,5-Trichlorophenol <7.5
2-Fluorophenol 57 27-110 05/01/17 15:19 05/05/17 14:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Phenol-d5 43 05/01/17 15:19 05/05/17 14:46 120-100
Nitrobenzene-d5 58 05/01/17 15:19 05/05/17 14:46 136-120
2-Fluorobiphenyl 58 05/01/17 15:19 05/05/17 14:46 134-110
2,4,6-Tribromophenol 85 05/01/17 15:19 05/05/17 14:46 140-145
Terphenyl-d14 83 05/01/17 15:19 05/05/17 14:46 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.037 0.037 0.0024 ug/L 05/01/17 10:27 05/05/17 00:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0094 ug/L 05/01/17 10:27 05/05/17 00:30 1beta-BHC <0.037
0.037 0.0095 ug/L 05/01/17 10:27 05/05/17 00:30 1delta-BHC <0.037
0.037 0.0052 ug/L 05/01/17 10:27 05/05/17 00:30 1gamma-BHC (Lindane)<0.037
0.037 0.012 ug/L 05/01/17 10:27 05/05/17 00:30 1Heptachlor<0.037
0.037 0.0049 ug/L 05/01/17 10:27 05/05/17 00:30 1Aldrin<0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 00:30 1Heptachlor epoxide <0.037
0.037 0.0038 ug/L 05/01/17 10:27 05/05/17 00:30 1Endosulfan I <0.037
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-1Client Sample ID: MW-55
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.037 0.037 0.012 ug/L 05/01/17 10:27 05/05/17 00:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0035 ug/L 05/01/17 10:27 05/05/17 00:30 14,4'-DDE <0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 00:30 1Endrin<0.037
0.037 0.0026 ug/L 05/01/17 10:27 05/05/17 00:30 1Endosulfan II <0.037
0.037 0.012 ug/L 05/01/17 10:27 05/05/17 00:30 14,4'-DDD <0.037
0.037 0.011 ug/L 05/01/17 10:27 05/05/17 00:30 1Endosulfan sulfate <0.037
0.037 0.0030 ug/L 05/01/17 10:27 05/05/17 00:30 14,4'-DDT <0.037
0.074 0.021 ug/L 05/01/17 10:27 05/05/17 00:30 1Methoxychlor<0.074
0.37 0.18 ug/L 05/01/17 10:27 05/05/17 00:30 1Toxaphene<0.37
0.037 0.0076 ug/L 05/01/17 10:27 05/05/17 00:30 1Endrin aldehyde <0.037
0.074 0.037 ug/L 05/01/17 10:27 05/05/17 00:30 1Chlordane (technical)<0.074
DCB Decachlorobiphenyl 57 30-130 05/01/17 10:27 05/05/17 00:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 69 05/01/17 10:27 05/05/17 00:30 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.37 0.37 0.062 ug/L 05/01/17 10:27 05/02/17 12:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 12:50 1PCB-1221 <0.37
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 12:50 1PCB-1232 <0.37
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 12:50 1PCB-1242 <0.37
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 12:50 1PCB-1248 <0.37
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 12:50 1PCB-1254 <0.37
0.37 0.065 ug/L 05/01/17 10:27 05/02/17 12:50 1PCB-1260 <0.37
Tetrachloro-m-xylene 72 30-120 05/01/17 10:27 05/02/17 12:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 86 05/01/17 10:27 05/02/17 12:50 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <1.2 1.2 0.55 ug/L 05/02/17 10:54 05/09/17 00:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.59 0.11 ug/L 05/02/17 10:54 05/09/17 00:39 1Pentachlorophenol<0.59
1.2 0.34 ug/L 05/02/17 10:54 05/09/17 00:39 1Silvex (2,4,5-TP)<1.2
1.2 0.51 ug/L 05/02/17 10:54 05/09/17 00:39 12,4,5-T <1.2
2.4 0.19 ug/L 05/02/17 10:54 05/09/17 00:39 1Dinoseb<2.4
DCAA 59 25-130 05/02/17 10:54 05/09/17 00:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 05/01/17 10:50 05/01/17 15:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 05/01/17 10:50 05/03/17 12:07 1Arsenic0.18 J
2.5 0.37 ug/L 05/01/17 10:50 05/01/17 15:54 1Barium120
1.0 0.43 ug/L 05/01/17 10:50 05/01/17 15:54 1Beryllium<1.0
0.50 0.15 ug/L 05/01/17 10:50 05/01/17 15:54 1Cadmium<0.50
5.0 2.3 ug/L 05/01/17 10:50 05/01/17 15:54 1Chromium<5.0
1.0 0.27 ug/L 05/01/17 10:50 05/01/17 15:54 1Cobalt5.8
2.0 0.63 ug/L 05/01/17 10:50 05/03/17 12:07 1Copper5.3
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-1Client Sample ID: MW-55
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 810 100 38 ug/L 05/01/17 10:50 05/01/17 15:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 05/01/17 10:50 05/01/17 15:54 1Lead0.31 J
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 15:54 1Manganese98
2.0 0.92 ug/L 05/01/17 10:50 05/01/17 15:54 1Nickel21
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 15:54 1Selenium<2.5
0.50 0.078 ug/L 05/01/17 10:50 05/01/17 15:54 1Silver<0.50
2.0 0.65 ug/L 05/01/17 10:50 05/01/17 15:54 1Thallium<2.0
10 4.2 ug/L 05/01/17 10:50 05/01/17 15:54 1Tin<10
5.0 2.0 ug/L 05/01/17 10:50 05/01/17 15:54 1Vanadium6.8
20 8.1 ug/L 05/01/17 10:50 05/03/17 12:07 1Zinc10J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 05/03/17 12:50 05/04/17 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 05/08/17 14:00 05/08/17 16:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 1.7 mg/L 05/05/17 19:40 10Chloride14
4.0 1.9 mg/L 05/08/17 11:41 20Sulfate95
5.0 3.7 mg/L 05/05/17 15:38 1Alkalinity150
10 4.3 mg/L 05/02/17 04:30 1Total Dissolved Solids 350
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-2Client Sample ID: MW-56
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 16 5.0 1.7 ug/L 05/07/17 23:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 4.2 ug/L 05/07/17 23:26 1Acetonitrile<10
100 23 ug/L 05/07/17 23:26 1Acrolein<100
20 4.5 ug/L 05/07/17 23:26 1Acrylonitrile<20
0.50 0.15 ug/L 05/07/17 23:26 1Benzene1.7
1.0 0.43 ug/L 05/07/17 23:26 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/07/17 23:26 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/07/17 23:26 1Bromoform<1.0
2.0 0.80 ug/L 05/07/17 23:26 1Bromomethane<2.0
5.0 2.1 ug/L 05/07/17 23:26 12-Butanone (MEK)<5.0
2.0 0.45 ug/L 05/07/17 23:26 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/07/17 23:26 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/07/17 23:26 1Chlorobenzene<1.0
1.0 0.23 ug/L 05/07/17 23:26 12-Chloro-1,3-butadiene <1.0
1.0 0.51 ug/L 05/07/17 23:26 1Chloroethane<1.0
2.0 0.37 ug/L 05/07/17 23:26 1Chloroform<2.0
1.0 0.32 ug/L 05/07/17 23:26 1Chloromethane<1.0
2.5 0.86 ug/L 05/07/17 23:26 13-Chloropropene <2.5
1.0 0.41 ug/L 05/07/17 23:26 1cis-1,2-Dichloroethene 2.1
1.0 0.42 ug/L 05/07/17 23:26 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/07/17 23:26 1Dibromochloromethane<1.0
5.0 2.0 ug/L 05/07/17 23:26 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/07/17 23:26 11,2-Dibromoethane <1.0
1.0 0.27 ug/L 05/07/17 23:26 1Dibromomethane<1.0
1.0 0.40 ug/L 05/07/17 23:26 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 05/07/17 23:26 11,4-Dichlorobenzene <1.0
1.0 0.33 ug/L 05/07/17 23:26 11,2-Dichlorobenzene <1.0
2.0 0.67 ug/L 05/07/17 23:26 1Dichlorodifluoromethane<2.0
1.0 0.41 ug/L 05/07/17 23:26 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/07/17 23:26 11,2-Dichloroethane <1.0
1.0 0.39 ug/L 05/07/17 23:26 11,1-Dichloroethene <1.0
1.0 0.44 ug/L 05/07/17 23:26 12,2-Dichloropropane <1.0
1.0 0.43 ug/L 05/07/17 23:26 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/07/17 23:26 11,3-Dichloropropane <1.0
1.0 0.30 ug/L 05/07/17 23:26 11,1-Dichloropropene <1.0
0.50 0.18 ug/L 05/07/17 23:26 1Ethylbenzene<0.50
2.5 0.53 ug/L 05/07/17 23:26 1Ethyl methacrylate <2.5
1.0 0.45 ug/L 05/07/17 23:26 1Hexachlorobutadiene<1.0
5.0 1.6 ug/L 05/07/17 23:26 12-Hexanone <5.0
2.5 0.66 ug/L 05/07/17 23:26 1Iodomethane<2.5
100 36 ug/L 05/07/17 23:26 1Isobutyl alcohol <100
10 2.5 ug/L 05/07/17 23:26 1Methacrylonitrile<10
5.0 1.6 ug/L 05/07/17 23:26 1Methylene Chloride <5.0
2.5 0.55 ug/L 05/07/17 23:26 1Methyl methacrylate <2.5
5.0 2.2 ug/L 05/07/17 23:26 14-Methyl-2-pentanone (MIBK)<5.0
10 4.8 ug/L 05/07/17 23:26 1Propionitrile<10
1.0 0.39 ug/L 05/07/17 23:26 1Styrene<1.0
1.0 0.46 ug/L 05/07/17 23:26 11,1,1,2-Tetrachloroethane <1.0
1.0 0.40 ug/L 05/07/17 23:26 11,1,2,2-Tetrachloroethane <1.0
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-2Client Sample ID: MW-56
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Tetrachloroethene <1.0 1.0 0.37 ug/L 05/07/17 23:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 1.9 ug/L 05/07/17 23:26 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/07/17 23:26 1Toluene<0.50
5.0 1.2 ug/L 05/07/17 23:26 1trans-1,4-Dichloro-2-butene <5.0
1.0 0.35 ug/L 05/07/17 23:26 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/07/17 23:26 1trans-1,3-Dichloropropene <1.0
1.0 0.34 ug/L 05/07/17 23:26 11,2,4-Trichlorobenzene <1.0
1.0 0.38 ug/L 05/07/17 23:26 11,1,1-Trichloroethane <1.0
1.0 0.35 ug/L 05/07/17 23:26 11,1,2-Trichloroethane <1.0
0.50 0.16 ug/L 05/07/17 23:26 1Trichloroethene<0.50
1.0 0.43 ug/L 05/07/17 23:26 1Trichlorofluoromethane<1.0
1.0 0.41 ug/L 05/07/17 23:26 11,2,3-Trichloropropane <1.0
2.0 0.91 ug/L 05/07/17 23:26 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/07/17 23:26 1Vinyl chloride 6.6 cn
1.0 0.22 ug/L 05/07/17 23:26 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)101 75-126 05/07/17 23:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)100 05/07/17 23:26 175-120
4-Bromofluorobenzene (Surr)112 05/07/17 23:26 172-124
Dibromofluoromethane 90 05/07/17 23:26 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.75 0.75 0.23 ug/L 05/01/17 15:19 05/05/17 15:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.75 0.20 ug/L 05/01/17 15:19 05/05/17 15:11 1Acenaphthylene<0.75
3.7 0.50 ug/L 05/01/17 15:19 05/05/17 15:11 1Acetophenone<3.7
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 15:11 12-Acetylaminofluorene <7.5
7.5 2.8 ug/L 05/01/17 15:19 05/05/17 15:11 14-Aminobiphenyl <7.5
0.75 0.25 ug/L 05/01/17 15:19 05/05/17 15:11 1Anthracene<0.75
0.15 0.042 ug/L 05/01/17 15:19 05/05/17 15:11 1Benzo[a]anthracene <0.15
0.15 0.074 ug/L 05/01/17 15:19 05/05/17 15:11 1Benzo[a]pyrene <0.15
0.15 0.060 ug/L 05/01/17 15:19 05/05/17 15:11 1Benzo[b]fluoranthene <0.15
0.75 0.28 ug/L 05/01/17 15:19 05/05/17 15:11 1Benzo[g,h,i]perylene <0.75
0.15 0.048 ug/L 05/01/17 15:19 05/05/17 15:11 1Benzo[k]fluoranthene <0.15
15 4.5 ug/L 05/01/17 15:19 05/05/17 15:11 1Benzyl alcohol <15
1.5 0.21 ug/L 05/01/17 15:19 05/05/17 15:11 1Bis(2-chloroethoxy)methane <1.5
1.5 0.22 ug/L 05/01/17 15:19 05/05/17 15:11 1Bis(2-chloroethyl)ether <1.5
7.5 1.3 ug/L 05/01/17 15:19 05/05/17 15:11 1Bis(2-ethylhexyl) phthalate <7.5
3.7 0.40 ug/L 05/01/17 15:19 05/05/17 15:11 14-Bromophenyl phenyl ether <3.7
1.5 0.36 ug/L 05/01/17 15:19 05/05/17 15:11 1Butyl benzyl phthalate <1.5
7.5 1.5 ug/L 05/01/17 15:19 05/05/17 15:11 14-Chloroaniline <7.5
7.5 2.5 ug/L 05/01/17 15:19 05/05/17 15:11 1Chlorobenzilate<7.5
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 15:11 14-Chloro-3-methylphenol <7.5
1.5 0.18 ug/L 05/01/17 15:19 05/05/17 15:11 12-Chloronaphthalene <1.5
3.7 0.42 ug/L 05/01/17 15:19 05/05/17 15:11 12-Chlorophenol <3.7
3.7 0.48 ug/L 05/01/17 15:19 05/05/17 15:11 14-Chlorophenyl phenyl ether <3.7
0.15 0.051 ug/L 05/01/17 15:19 05/05/17 15:11 1Chrysene<0.15
7.5 4.1 ug/L 05/01/17 15:19 05/05/17 15:11 1Diallate<7.5
0.22 0.038 ug/L 05/01/17 15:19 05/05/17 15:11 1Dibenz(a,h)anthracene <0.22
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-2Client Sample ID: MW-56
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.5 1.5 0.20 ug/L 05/01/17 15:19 05/05/17 15:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.7 1.3 ug/L 05/01/17 15:19 05/05/17 15:11 13,3'-Dichlorobenzidine <3.7
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 15:11 12,4-Dichlorophenol <7.5
7.5 2.6 ug/L 05/01/17 15:19 05/05/17 15:11 12,6-Dichlorophenol <7.5
1.5 0.27 ug/L 05/01/17 15:19 05/05/17 15:11 1Diethyl phthalate <1.5
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 15:11 1Dimethoate<7.5
30 2.3 ug/L 05/01/17 15:19 05/05/17 15:11 17,12-Dimethylbenz(a)anthracene <30
30 13 ug/L 05/01/17 15:19 05/05/17 15:11 13,3'-Dimethylbenzidine <30
7.5 1.3 ug/L 05/01/17 15:19 05/05/17 15:11 12,4-Dimethylphenol <7.5
1.5 0.23 ug/L 05/01/17 15:19 05/05/17 15:11 1Dimethyl phthalate <1.5
3.7 0.55 ug/L 05/01/17 15:19 05/05/17 15:11 1Di-n-butyl phthalate <3.7
15 4.4 ug/L 05/01/17 15:19 05/05/17 15:11 14,6-Dinitro-2-methylphenol <15
15 6.4 ug/L 05/01/17 15:19 05/05/17 15:11 12,4-Dinitrophenol <15
0.75 0.055 ug/L 05/01/17 15:19 05/05/17 15:11 12,6-Dinitrotoluene <0.75
0.75 0.18 ug/L 05/01/17 15:19 05/05/17 15:11 12,4-Dinitrotoluene <0.75
7.5 0.79 ug/L 05/01/17 15:19 05/05/17 15:11 1Di-n-octyl phthalate <7.5
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 15:11 1Diphenylamine<7.5
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 15:11 1Disulfoton<7.5
15 2.8 ug/L 05/01/17 15:19 05/05/17 15:11 1Ethyl methanesulfonate <15
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 15:11 1Ethyl Parathion <7.5
30 23 ug/L 05/01/17 15:19 05/05/17 15:11 1Famphur<30
0.75 0.34 ug/L 05/01/17 15:19 05/05/17 15:11 1Fluoranthene<0.75
0.75 0.18 ug/L 05/01/17 15:19 05/05/17 15:11 1Fluorene<0.75
0.37 0.059 ug/L 05/01/17 15:19 05/05/17 15:11 1Hexachlorobenzene<0.37
15 4.8 ug/L 05/01/17 15:19 05/05/17 15:11 1Hexachlorocyclopentadiene<15
3.7 0.45 ug/L 05/01/17 15:19 05/05/17 15:11 1Hexachloroethane<3.7
15 3.5 ug/L 05/01/17 15:19 05/05/17 15:11 1Hexachloropropene<15
0.15 0.056 ug/L 05/01/17 15:19 05/05/17 15:11 1Indeno[1,2,3-cd]pyrene <0.15
15 5.2 ug/L 05/01/17 15:19 05/05/17 15:11 1Isodrin<15
1.5 0.28 ug/L 05/01/17 15:19 05/05/17 15:11 1Isophorone<1.5
7.5 2.9 ug/L 05/01/17 15:19 05/05/17 15:11 1Isosafrole<7.5
7.5 1.2 ug/L 05/01/17 15:19 05/05/17 15:11 1Kepone<7.5
3.7 0.99 ug/L 05/01/17 15:19 05/05/17 15:11 1m-Dinitrobenzene <3.7
30 7.6 ug/L 05/01/17 15:19 05/05/17 15:11 1Methapyrilene<30
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 15:11 13-Methylcholanthrene <7.5
30 4.4 ug/L 05/01/17 15:19 05/05/17 15:11 1Methyl methanesulfonate <30
1.5 0.049 ug/L 05/01/17 15:19 05/05/17 15:11 12-Methylnaphthalene <1.5
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 15:11 1Methyl parathion <7.5
1.5 0.23 ug/L 05/01/17 15:19 05/05/17 15:11 12-Methylphenol <1.5
1.5 0.34 ug/L 05/01/17 15:19 05/05/17 15:11 13 & 4 Methylphenol <1.5
0.75 0.23 ug/L 05/01/17 15:19 05/05/17 15:11 1Naphthalene<0.75
30 29 ug/L 05/01/17 15:19 05/05/17 15:11 11,4-Naphthoquinone <30
15 4.4 ug/L 05/01/17 15:19 05/05/17 15:11 11-Naphthylamine <15
15 6.8 ug/L 05/01/17 15:19 05/05/17 15:11 12-Naphthylamine <15
3.7 0.96 ug/L 05/01/17 15:19 05/05/17 15:11 12-Nitroaniline <3.7
7.5 1.3 ug/L 05/01/17 15:19 05/05/17 15:11 13-Nitroaniline <7.5
7.5 1.2 ug/L 05/01/17 15:19 05/05/17 15:11 14-Nitroaniline <7.5
0.75 0.34 ug/L 05/01/17 15:19 05/05/17 15:11 1Nitrobenzene<0.75
7.5 2.3 ug/L 05/01/17 15:19 05/05/17 15:11 15-Nitro-o-toluidine <7.5
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-2Client Sample ID: MW-56
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.5 7.5 1.9 ug/L 05/01/17 15:19 05/05/17 15:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 5.6 ug/L 05/01/17 15:19 05/05/17 15:11 14-Nitrophenol <15
15 6.4 ug/L 05/01/17 15:19 05/05/17 15:11 1N-Nitrosodiethylamine <15
7.5 3.6 ug/L 05/01/17 15:19 05/05/17 15:11 1N-Nitrosodimethylamine <7.5
7.5 3.1 ug/L 05/01/17 15:19 05/05/17 15:11 1N-Nitrosodi-n-butylamine <7.5
0.37 0.12 ug/L 05/01/17 15:19 05/05/17 15:11 1N-Nitrosodi-n-propylamine <0.37
1.5 0.28 ug/L 05/01/17 15:19 05/05/17 15:11 1N-Nitrosodiphenylamine <1.5
15 5.6 ug/L 05/01/17 15:19 05/05/17 15:11 1N-Nitrosomethylethylamine <15
7.5 2.6 ug/L 05/01/17 15:19 05/05/17 15:11 1N-Nitrosopiperidine <7.5
7.5 2.5 ug/L 05/01/17 15:19 05/05/17 15:11 1N-Nitrosopyrrolidine <7.5
15 4.1 ug/L 05/01/17 15:19 05/05/17 15:11 1o,o',o''-Triethylphosphorothioate <15
30 5.9 ug/L 05/01/17 15:19 05/05/17 15:11 1o-Toluidine <30
1.5 0.28 ug/L 05/01/17 15:19 05/05/17 15:11 12,2'-oxybis[1-chloropropane]<1.5
7.5 2.2 ug/L 05/01/17 15:19 05/05/17 15:11 1p-Dimethylamino azobenzene <7.5
7.5 2.1 ug/L 05/01/17 15:19 05/05/17 15:11 1Pentachlorobenzene<7.5
7.5 2.7 ug/L 05/01/17 15:19 05/05/17 15:11 1Pentachloronitrobenzene<7.5
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 15:11 1Phenacetin<7.5
0.75 0.23 ug/L 05/01/17 15:19 05/05/17 15:11 1Phenanthrene<0.75
3.7 0.50 ug/L 05/01/17 15:19 05/05/17 15:11 1Phenol<3.7
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 15:11 1Phorate<7.5
60 12 ug/L 05/01/17 15:19 05/05/17 15:11 1p-Phenylene diamine <60
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 15:11 1Pronamide<7.5
0.75 0.32 ug/L 05/01/17 15:19 05/05/17 15:11 1Pyrene<0.75
7.5 3.0 ug/L 05/01/17 15:19 05/05/17 15:11 1Safrole<7.5
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 15:11 1sym-Trinitrobenzene <7.5
7.5 7.5 ug/L 05/01/17 15:19 05/05/17 15:11 12,3,7,8-TCDD (Screen)<7.5
3.7 0.43 ug/L 05/01/17 15:19 05/05/17 15:11 11,2,4,5-Tetrachlorobenzene <3.7
3.7 0.56 ug/L 05/01/17 15:19 05/05/17 15:11 12,3,4,6-Tetrachlorophenol <3.7
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 15:11 1Thionazin<7.5
3.7 0.54 ug/L 05/01/17 15:19 05/05/17 15:11 12,4,6-Trichlorophenol <3.7
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 15:11 12,4,5-Trichlorophenol <7.5
2-Fluorophenol 71 27-110 05/01/17 15:19 05/05/17 15:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Phenol-d5 51 05/01/17 15:19 05/05/17 15:11 120-100
Nitrobenzene-d5 77 05/01/17 15:19 05/05/17 15:11 136-120
2-Fluorobiphenyl 76 05/01/17 15:19 05/05/17 15:11 134-110
2,4,6-Tribromophenol 113 05/01/17 15:19 05/05/17 15:11 140-145
Terphenyl-d14 99 05/01/17 15:19 05/05/17 15:11 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.037 0.037 0.0024 ug/L 05/01/17 10:27 05/05/17 00:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0095 ug/L 05/01/17 10:27 05/05/17 00:49 1beta-BHC <0.037
0.037 0.0096 ug/L 05/01/17 10:27 05/05/17 00:49 1delta-BHC <0.037
0.037 0.0052 ug/L 05/01/17 10:27 05/05/17 00:49 1gamma-BHC (Lindane)<0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 00:49 1Heptachlor<0.037
0.037 0.0050 ug/L 05/01/17 10:27 05/05/17 00:49 1Aldrin<0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 00:49 1Heptachlor epoxide <0.037
0.037 0.0038 ug/L 05/01/17 10:27 05/05/17 00:49 1Endosulfan I <0.037
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-2Client Sample ID: MW-56
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.037 0.037 0.012 ug/L 05/01/17 10:27 05/05/17 00:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0036 ug/L 05/01/17 10:27 05/05/17 00:49 14,4'-DDE <0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 00:49 1Endrin<0.037
0.037 0.0026 ug/L 05/01/17 10:27 05/05/17 00:49 1Endosulfan II <0.037
0.037 0.012 ug/L 05/01/17 10:27 05/05/17 00:49 14,4'-DDD <0.037
0.037 0.011 ug/L 05/01/17 10:27 05/05/17 00:49 1Endosulfan sulfate <0.037
0.037 0.0030 ug/L 05/01/17 10:27 05/05/17 00:49 14,4'-DDT <0.037
0.075 0.021 ug/L 05/01/17 10:27 05/05/17 00:49 1Methoxychlor<0.075
0.37 0.19 ug/L 05/01/17 10:27 05/05/17 00:49 1Toxaphene<0.37
0.037 0.0077 ug/L 05/01/17 10:27 05/05/17 00:49 1Endrin aldehyde <0.037
0.075 0.037 ug/L 05/01/17 10:27 05/05/17 00:49 1Chlordane (technical)<0.075
DCB Decachlorobiphenyl 63 30-130 05/01/17 10:27 05/05/17 00:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 71 05/01/17 10:27 05/05/17 00:49 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.37 0.37 0.063 ug/L 05/01/17 10:27 05/02/17 13:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:06 1PCB-1221 <0.37
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:06 1PCB-1232 <0.37
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:06 1PCB-1242 <0.37
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:06 1PCB-1248 <0.37
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:06 1PCB-1254 <0.37
0.37 0.065 ug/L 05/01/17 10:27 05/02/17 13:06 1PCB-1260 <0.37
Tetrachloro-m-xylene 77 30-120 05/01/17 10:27 05/02/17 13:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 66 05/01/17 10:27 05/02/17 13:06 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <1.1 1.1 0.53 ug/L 05/02/17 10:54 05/09/17 01:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.57 0.10 ug/L 05/02/17 10:54 05/09/17 01:04 1Pentachlorophenol<0.57
1.1 0.33 ug/L 05/02/17 10:54 05/09/17 01:04 1Silvex (2,4,5-TP)<1.1
1.1 0.50 ug/L 05/02/17 10:54 05/09/17 01:04 12,4,5-T <1.1
2.3 0.19 ug/L 05/02/17 10:54 05/09/17 01:04 1Dinoseb<2.3
DCAA 70 25-130 05/02/17 10:54 05/09/17 01:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 05/01/17 10:50 05/01/17 16:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 05/01/17 10:50 05/03/17 12:22 1Arsenic0.28 J
2.5 0.37 ug/L 05/01/17 10:50 05/01/17 16:17 1Barium170
1.0 0.43 ug/L 05/01/17 10:50 05/01/17 16:17 1Beryllium<1.0
0.50 0.15 ug/L 05/01/17 10:50 05/01/17 16:17 1Cadmium<0.50
5.0 2.3 ug/L 05/01/17 10:50 05/01/17 16:17 1Chromium<5.0
1.0 0.27 ug/L 05/01/17 10:50 05/01/17 16:17 1Cobalt66
2.0 0.63 ug/L 05/01/17 10:50 05/03/17 12:22 1Copper4.0
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-2Client Sample ID: MW-56
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 4100 100 38 ug/L 05/01/17 10:50 05/01/17 16:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 05/01/17 10:50 05/01/17 16:17 1Lead0.17 J
25 11 ug/L 05/01/17 10:50 05/03/17 14:19 10Manganese11000
2.0 0.92 ug/L 05/01/17 10:50 05/01/17 16:17 1Nickel9.7
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:17 1Selenium<2.5
0.50 0.078 ug/L 05/01/17 10:50 05/01/17 16:17 1Silver<0.50
2.0 0.65 ug/L 05/01/17 10:50 05/01/17 16:17 1Thallium<2.0
10 4.2 ug/L 05/01/17 10:50 05/01/17 16:17 1Tin<10
5.0 2.0 ug/L 05/01/17 10:50 05/01/17 16:17 1Vanadium<5.0
20 8.1 ug/L 05/01/17 10:50 05/03/17 12:22 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 05/03/17 12:50 05/04/17 08:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 05/08/17 14:00 05/08/17 16:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 1.7 mg/L 05/05/17 19:53 10Chloride11
2.0 0.95 mg/L 05/05/17 19:53 10Sulfate67
5.0 3.7 mg/L 05/05/17 15:45 1Alkalinity340
10 4.3 mg/L 05/02/17 04:37 1Total Dissolved Solids 450
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-3Client Sample ID: MW-56A
Matrix: WaterDate Collected: 04/26/17 08:45
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <5.0 5.0 1.7 ug/L 05/07/17 23:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 4.2 ug/L 05/07/17 23:52 1Acetonitrile<10
100 23 ug/L 05/07/17 23:52 1Acrolein<100
20 4.5 ug/L 05/07/17 23:52 1Acrylonitrile<20
0.50 0.15 ug/L 05/07/17 23:52 1Benzene<0.50
1.0 0.43 ug/L 05/07/17 23:52 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/07/17 23:52 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/07/17 23:52 1Bromoform<1.0
2.0 0.80 ug/L 05/07/17 23:52 1Bromomethane<2.0
5.0 2.1 ug/L 05/07/17 23:52 12-Butanone (MEK)<5.0
2.0 0.45 ug/L 05/07/17 23:52 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/07/17 23:52 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/07/17 23:52 1Chlorobenzene<1.0
1.0 0.23 ug/L 05/07/17 23:52 12-Chloro-1,3-butadiene <1.0
1.0 0.51 ug/L 05/07/17 23:52 1Chloroethane<1.0
2.0 0.37 ug/L 05/07/17 23:52 1Chloroform<2.0
1.0 0.32 ug/L 05/07/17 23:52 1Chloromethane<1.0
2.5 0.86 ug/L 05/07/17 23:52 13-Chloropropene <2.5
1.0 0.41 ug/L 05/07/17 23:52 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/07/17 23:52 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/07/17 23:52 1Dibromochloromethane<1.0
5.0 2.0 ug/L 05/07/17 23:52 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/07/17 23:52 11,2-Dibromoethane <1.0
1.0 0.27 ug/L 05/07/17 23:52 1Dibromomethane<1.0
1.0 0.40 ug/L 05/07/17 23:52 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 05/07/17 23:52 11,4-Dichlorobenzene <1.0
1.0 0.33 ug/L 05/07/17 23:52 11,2-Dichlorobenzene <1.0
2.0 0.67 ug/L 05/07/17 23:52 1Dichlorodifluoromethane<2.0
1.0 0.41 ug/L 05/07/17 23:52 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/07/17 23:52 11,2-Dichloroethane <1.0
1.0 0.39 ug/L 05/07/17 23:52 11,1-Dichloroethene <1.0
1.0 0.44 ug/L 05/07/17 23:52 12,2-Dichloropropane <1.0
1.0 0.43 ug/L 05/07/17 23:52 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/07/17 23:52 11,3-Dichloropropane <1.0
1.0 0.30 ug/L 05/07/17 23:52 11,1-Dichloropropene <1.0
0.50 0.18 ug/L 05/07/17 23:52 1Ethylbenzene<0.50
2.5 0.53 ug/L 05/07/17 23:52 1Ethyl methacrylate <2.5
1.0 0.45 ug/L 05/07/17 23:52 1Hexachlorobutadiene<1.0
5.0 1.6 ug/L 05/07/17 23:52 12-Hexanone <5.0
2.5 0.66 ug/L 05/07/17 23:52 1Iodomethane<2.5
100 36 ug/L 05/07/17 23:52 1Isobutyl alcohol <100
10 2.5 ug/L 05/07/17 23:52 1Methacrylonitrile<10
5.0 1.6 ug/L 05/07/17 23:52 1Methylene Chloride <5.0
2.5 0.55 ug/L 05/07/17 23:52 1Methyl methacrylate <2.5
5.0 2.2 ug/L 05/07/17 23:52 14-Methyl-2-pentanone (MIBK)<5.0
10 4.8 ug/L 05/07/17 23:52 1Propionitrile<10
1.0 0.39 ug/L 05/07/17 23:52 1Styrene<1.0
1.0 0.46 ug/L 05/07/17 23:52 11,1,1,2-Tetrachloroethane <1.0
1.0 0.40 ug/L 05/07/17 23:52 11,1,2,2-Tetrachloroethane <1.0
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-3Client Sample ID: MW-56A
Matrix: WaterDate Collected: 04/26/17 08:45
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Tetrachloroethene <1.0 1.0 0.37 ug/L 05/07/17 23:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 1.9 ug/L 05/07/17 23:52 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/07/17 23:52 1Toluene<0.50
5.0 1.2 ug/L 05/07/17 23:52 1trans-1,4-Dichloro-2-butene <5.0
1.0 0.35 ug/L 05/07/17 23:52 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/07/17 23:52 1trans-1,3-Dichloropropene <1.0
1.0 0.34 ug/L 05/07/17 23:52 11,2,4-Trichlorobenzene <1.0
1.0 0.38 ug/L 05/07/17 23:52 11,1,1-Trichloroethane <1.0
1.0 0.35 ug/L 05/07/17 23:52 11,1,2-Trichloroethane <1.0
0.50 0.16 ug/L 05/07/17 23:52 1Trichloroethene<0.50
1.0 0.43 ug/L 05/07/17 23:52 1Trichlorofluoromethane<1.0
1.0 0.41 ug/L 05/07/17 23:52 11,2,3-Trichloropropane <1.0
2.0 0.91 ug/L 05/07/17 23:52 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/07/17 23:52 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/07/17 23:52 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)103 75-126 05/07/17 23:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)103 05/07/17 23:52 175-120
4-Bromofluorobenzene (Surr)114 05/07/17 23:52 172-124
Dibromofluoromethane 89 05/07/17 23:52 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.75 0.75 0.23 ug/L 05/01/17 15:19 05/05/17 15:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.75 0.20 ug/L 05/01/17 15:19 05/05/17 15:36 1Acenaphthylene<0.75
3.8 0.50 ug/L 05/01/17 15:19 05/05/17 15:36 1Acetophenone<3.8
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 15:36 12-Acetylaminofluorene <7.5
7.5 2.8 ug/L 05/01/17 15:19 05/05/17 15:36 14-Aminobiphenyl <7.5
0.75 0.25 ug/L 05/01/17 15:19 05/05/17 15:36 1Anthracene<0.75
0.15 0.043 ug/L 05/01/17 15:19 05/05/17 15:36 1Benzo[a]anthracene <0.15
0.15 0.074 ug/L 05/01/17 15:19 05/05/17 15:36 1Benzo[a]pyrene <0.15
0.15 0.061 ug/L 05/01/17 15:19 05/05/17 15:36 1Benzo[b]fluoranthene <0.15
0.75 0.28 ug/L 05/01/17 15:19 05/05/17 15:36 1Benzo[g,h,i]perylene <0.75
0.15 0.048 ug/L 05/01/17 15:19 05/05/17 15:36 1Benzo[k]fluoranthene <0.15
15 4.5 ug/L 05/01/17 15:19 05/05/17 15:36 1Benzyl alcohol <15
1.5 0.21 ug/L 05/01/17 15:19 05/05/17 15:36 1Bis(2-chloroethoxy)methane <1.5
1.5 0.22 ug/L 05/01/17 15:19 05/05/17 15:36 1Bis(2-chloroethyl)ether <1.5
7.5 1.3 ug/L 05/01/17 15:19 05/05/17 15:36 1Bis(2-ethylhexyl) phthalate <7.5
3.8 0.41 ug/L 05/01/17 15:19 05/05/17 15:36 14-Bromophenyl phenyl ether <3.8
1.5 0.36 ug/L 05/01/17 15:19 05/05/17 15:36 1Butyl benzyl phthalate <1.5
7.5 1.5 ug/L 05/01/17 15:19 05/05/17 15:36 14-Chloroaniline <7.5
7.5 2.6 ug/L 05/01/17 15:19 05/05/17 15:36 1Chlorobenzilate<7.5
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 15:36 14-Chloro-3-methylphenol <7.5
1.5 0.18 ug/L 05/01/17 15:19 05/05/17 15:36 12-Chloronaphthalene <1.5
3.8 0.42 ug/L 05/01/17 15:19 05/05/17 15:36 12-Chlorophenol <3.8
3.8 0.48 ug/L 05/01/17 15:19 05/05/17 15:36 14-Chlorophenyl phenyl ether <3.8
0.15 0.051 ug/L 05/01/17 15:19 05/05/17 15:36 1Chrysene<0.15
7.5 4.1 ug/L 05/01/17 15:19 05/05/17 15:36 1Diallate<7.5
0.23 0.038 ug/L 05/01/17 15:19 05/05/17 15:36 1Dibenz(a,h)anthracene <0.23
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-3Client Sample ID: MW-56A
Matrix: WaterDate Collected: 04/26/17 08:45
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.5 1.5 0.20 ug/L 05/01/17 15:19 05/05/17 15:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.8 1.3 ug/L 05/01/17 15:19 05/05/17 15:36 13,3'-Dichlorobenzidine <3.8
7.5 2.0 ug/L 05/01/17 15:19 05/05/17 15:36 12,4-Dichlorophenol <7.5
7.5 2.6 ug/L 05/01/17 15:19 05/05/17 15:36 12,6-Dichlorophenol <7.5
1.5 0.27 ug/L 05/01/17 15:19 05/05/17 15:36 1Diethyl phthalate <1.5
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 15:36 1Dimethoate<7.5
30 2.3 ug/L 05/01/17 15:19 05/05/17 15:36 17,12-Dimethylbenz(a)anthracene <30
30 13 ug/L 05/01/17 15:19 05/05/17 15:36 13,3'-Dimethylbenzidine <30
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 15:36 12,4-Dimethylphenol <7.5
1.5 0.24 ug/L 05/01/17 15:19 05/05/17 15:36 1Dimethyl phthalate <1.5
3.8 0.55 ug/L 05/01/17 15:19 05/05/17 15:36 1Di-n-butyl phthalate <3.8
15 4.4 ug/L 05/01/17 15:19 05/05/17 15:36 14,6-Dinitro-2-methylphenol <15
15 6.5 ug/L 05/01/17 15:19 05/05/17 15:36 12,4-Dinitrophenol <15
0.75 0.056 ug/L 05/01/17 15:19 05/05/17 15:36 12,6-Dinitrotoluene <0.75
0.75 0.18 ug/L 05/01/17 15:19 05/05/17 15:36 12,4-Dinitrotoluene <0.75
7.5 0.79 ug/L 05/01/17 15:19 05/05/17 15:36 1Di-n-octyl phthalate <7.5
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 15:36 1Diphenylamine<7.5
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 15:36 1Disulfoton<7.5
15 2.9 ug/L 05/01/17 15:19 05/05/17 15:36 1Ethyl methanesulfonate <15
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 15:36 1Ethyl Parathion <7.5
30 23 ug/L 05/01/17 15:19 05/05/17 15:36 1Famphur<30
0.75 0.34 ug/L 05/01/17 15:19 05/05/17 15:36 1Fluoranthene<0.75
0.75 0.18 ug/L 05/01/17 15:19 05/05/17 15:36 1Fluorene<0.75
0.38 0.060 ug/L 05/01/17 15:19 05/05/17 15:36 1Hexachlorobenzene<0.38
15 4.8 ug/L 05/01/17 15:19 05/05/17 15:36 1Hexachlorocyclopentadiene<15
3.8 0.45 ug/L 05/01/17 15:19 05/05/17 15:36 1Hexachloroethane<3.8
15 3.5 ug/L 05/01/17 15:19 05/05/17 15:36 1Hexachloropropene<15
0.15 0.056 ug/L 05/01/17 15:19 05/05/17 15:36 1Indeno[1,2,3-cd]pyrene <0.15
15 5.2 ug/L 05/01/17 15:19 05/05/17 15:36 1Isodrin<15
1.5 0.28 ug/L 05/01/17 15:19 05/05/17 15:36 1Isophorone<1.5
7.5 2.9 ug/L 05/01/17 15:19 05/05/17 15:36 1Isosafrole<7.5
7.5 1.2 ug/L 05/01/17 15:19 05/05/17 15:36 1Kepone<7.5
3.8 1.0 ug/L 05/01/17 15:19 05/05/17 15:36 1m-Dinitrobenzene <3.8
30 7.6 ug/L 05/01/17 15:19 05/05/17 15:36 1Methapyrilene<30
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 15:36 13-Methylcholanthrene <7.5
30 4.5 ug/L 05/01/17 15:19 05/05/17 15:36 1Methyl methanesulfonate <30
1.5 0.049 ug/L 05/01/17 15:19 05/05/17 15:36 12-Methylnaphthalene <1.5
7.5 1.8 ug/L 05/01/17 15:19 05/05/17 15:36 1Methyl parathion <7.5
1.5 0.23 ug/L 05/01/17 15:19 05/05/17 15:36 12-Methylphenol <1.5
1.5 0.34 ug/L 05/01/17 15:19 05/05/17 15:36 13 & 4 Methylphenol <1.5
0.75 0.23 ug/L 05/01/17 15:19 05/05/17 15:36 1Naphthalene<0.75
30 29 ug/L 05/01/17 15:19 05/05/17 15:36 11,4-Naphthoquinone <30
15 4.5 ug/L 05/01/17 15:19 05/05/17 15:36 11-Naphthylamine <15
15 6.9 ug/L 05/01/17 15:19 05/05/17 15:36 12-Naphthylamine <15
3.8 0.97 ug/L 05/01/17 15:19 05/05/17 15:36 12-Nitroaniline <3.8
7.5 1.3 ug/L 05/01/17 15:19 05/05/17 15:36 13-Nitroaniline <7.5
7.5 1.3 ug/L 05/01/17 15:19 05/05/17 15:36 14-Nitroaniline <7.5
0.75 0.34 ug/L 05/01/17 15:19 05/05/17 15:36 1Nitrobenzene<0.75
7.5 2.3 ug/L 05/01/17 15:19 05/05/17 15:36 15-Nitro-o-toluidine <7.5
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-3Client Sample ID: MW-56A
Matrix: WaterDate Collected: 04/26/17 08:45
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.5 7.5 1.9 ug/L 05/01/17 15:19 05/05/17 15:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 5.6 ug/L 05/01/17 15:19 05/05/17 15:36 14-Nitrophenol <15
15 6.5 ug/L 05/01/17 15:19 05/05/17 15:36 1N-Nitrosodiethylamine <15
7.5 3.6 ug/L 05/01/17 15:19 05/05/17 15:36 1N-Nitrosodimethylamine <7.5
7.5 3.2 ug/L 05/01/17 15:19 05/05/17 15:36 1N-Nitrosodi-n-butylamine <7.5
0.38 0.12 ug/L 05/01/17 15:19 05/05/17 15:36 1N-Nitrosodi-n-propylamine <0.38
1.5 0.28 ug/L 05/01/17 15:19 05/05/17 15:36 1N-Nitrosodiphenylamine <1.5
15 5.6 ug/L 05/01/17 15:19 05/05/17 15:36 1N-Nitrosomethylethylamine <15
7.5 2.6 ug/L 05/01/17 15:19 05/05/17 15:36 1N-Nitrosopiperidine <7.5
7.5 2.5 ug/L 05/01/17 15:19 05/05/17 15:36 1N-Nitrosopyrrolidine <7.5
15 4.1 ug/L 05/01/17 15:19 05/05/17 15:36 1o,o',o''-Triethylphosphorothioate <15
30 6.0 ug/L 05/01/17 15:19 05/05/17 15:36 1o-Toluidine <30
1.5 0.29 ug/L 05/01/17 15:19 05/05/17 15:36 12,2'-oxybis[1-chloropropane]<1.5
7.5 2.3 ug/L 05/01/17 15:19 05/05/17 15:36 1p-Dimethylamino azobenzene <7.5
7.5 2.1 ug/L 05/01/17 15:19 05/05/17 15:36 1Pentachlorobenzene<7.5
7.5 2.7 ug/L 05/01/17 15:19 05/05/17 15:36 1Pentachloronitrobenzene<7.5
7.5 1.7 ug/L 05/01/17 15:19 05/05/17 15:36 1Phenacetin<7.5
0.75 0.23 ug/L 05/01/17 15:19 05/05/17 15:36 1Phenanthrene<0.75
3.8 0.51 ug/L 05/01/17 15:19 05/05/17 15:36 1Phenol<3.8
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 15:36 1Phorate<7.5
60 12 ug/L 05/01/17 15:19 05/05/17 15:36 1p-Phenylene diamine <60
7.5 1.6 ug/L 05/01/17 15:19 05/05/17 15:36 1Pronamide<7.5
0.75 0.32 ug/L 05/01/17 15:19 05/05/17 15:36 1Pyrene<0.75
7.5 3.0 ug/L 05/01/17 15:19 05/05/17 15:36 1Safrole<7.5
7.5 1.4 ug/L 05/01/17 15:19 05/05/17 15:36 1sym-Trinitrobenzene <7.5
7.5 7.5 ug/L 05/01/17 15:19 05/05/17 15:36 12,3,7,8-TCDD (Screen)<7.5
3.8 0.43 ug/L 05/01/17 15:19 05/05/17 15:36 11,2,4,5-Tetrachlorobenzene <3.8
3.8 0.56 ug/L 05/01/17 15:19 05/05/17 15:36 12,3,4,6-Tetrachlorophenol <3.8
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 15:36 1Thionazin<7.5
3.8 0.54 ug/L 05/01/17 15:19 05/05/17 15:36 12,4,6-Trichlorophenol <3.8
7.5 1.9 ug/L 05/01/17 15:19 05/05/17 15:36 12,4,5-Trichlorophenol <7.5
2-Fluorophenol 87 27-110 05/01/17 15:19 05/05/17 15:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Phenol-d5 58 05/01/17 15:19 05/05/17 15:36 120-100
Nitrobenzene-d5 86 05/01/17 15:19 05/05/17 15:36 136-120
2-Fluorobiphenyl 82 05/01/17 15:19 05/05/17 15:36 134-110
2,4,6-Tribromophenol 106 05/01/17 15:19 05/05/17 15:36 140-145
Terphenyl-d14 103 05/01/17 15:19 05/05/17 15:36 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.038 0.038 0.0024 ug/L 05/01/17 10:27 05/05/17 01:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.038 0.0096 ug/L 05/01/17 10:27 05/05/17 01:08 1beta-BHC <0.038
0.038 0.0097 ug/L 05/01/17 10:27 05/05/17 01:08 1delta-BHC <0.038
0.038 0.0053 ug/L 05/01/17 10:27 05/05/17 01:08 1gamma-BHC (Lindane)<0.038
0.038 0.013 ug/L 05/01/17 10:27 05/05/17 01:08 1Heptachlor<0.038
0.038 0.0050 ug/L 05/01/17 10:27 05/05/17 01:08 1Aldrin<0.038
0.038 0.013 ug/L 05/01/17 10:27 05/05/17 01:08 1Heptachlor epoxide <0.038
0.038 0.0038 ug/L 05/01/17 10:27 05/05/17 01:08 1Endosulfan I <0.038
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-3Client Sample ID: MW-56A
Matrix: WaterDate Collected: 04/26/17 08:45
Date Received: 04/28/17 09:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.038 0.038 0.012 ug/L 05/01/17 10:27 05/05/17 01:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.038 0.0036 ug/L 05/01/17 10:27 05/05/17 01:08 14,4'-DDE <0.038
0.038 0.013 ug/L 05/01/17 10:27 05/05/17 01:08 1Endrin<0.038
0.038 0.0026 ug/L 05/01/17 10:27 05/05/17 01:08 1Endosulfan II <0.038
0.038 0.012 ug/L 05/01/17 10:27 05/05/17 01:08 14,4'-DDD <0.038
0.038 0.011 ug/L 05/01/17 10:27 05/05/17 01:08 1Endosulfan sulfate <0.038
0.038 0.0030 ug/L 05/01/17 10:27 05/05/17 01:08 14,4'-DDT <0.038
0.075 0.022 ug/L 05/01/17 10:27 05/05/17 01:08 1Methoxychlor<0.075
0.38 0.19 ug/L 05/01/17 10:27 05/05/17 01:08 1Toxaphene<0.38
0.038 0.0077 ug/L 05/01/17 10:27 05/05/17 01:08 1Endrin aldehyde <0.038
0.075 0.038 ug/L 05/01/17 10:27 05/05/17 01:08 1Chlordane (technical)<0.075
DCB Decachlorobiphenyl 88 30-130 05/01/17 10:27 05/05/17 01:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 79 05/01/17 10:27 05/05/17 01:08 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.38 0.38 0.063 ug/L 05/01/17 10:27 05/02/17 13:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.38 0.19 ug/L 05/01/17 10:27 05/02/17 13:21 1PCB-1221 <0.38
0.38 0.19 ug/L 05/01/17 10:27 05/02/17 13:21 1PCB-1232 <0.38
0.38 0.19 ug/L 05/01/17 10:27 05/02/17 13:21 1PCB-1242 <0.38
0.38 0.19 ug/L 05/01/17 10:27 05/02/17 13:21 1PCB-1248 <0.38
0.38 0.19 ug/L 05/01/17 10:27 05/02/17 13:21 1PCB-1254 <0.38
0.38 0.066 ug/L 05/01/17 10:27 05/02/17 13:21 1PCB-1260 <0.38
Tetrachloro-m-xylene 82 30-120 05/01/17 10:27 05/02/17 13:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 88 05/01/17 10:27 05/02/17 13:21 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <1.1 1.1 0.51 ug/L 05/02/17 10:54 05/09/17 01:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.55 0.099 ug/L 05/02/17 10:54 05/09/17 01:28 1Pentachlorophenol<0.55
1.1 0.32 ug/L 05/02/17 10:54 05/09/17 01:28 1Silvex (2,4,5-TP)<1.1
1.1 0.48 ug/L 05/02/17 10:54 05/09/17 01:28 12,4,5-T <1.1
2.2 0.18 ug/L 05/02/17 10:54 05/09/17 01:28 1Dinoseb<2.2
DCAA 49 25-130 05/02/17 10:54 05/09/17 01:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 05/01/17 10:50 05/01/17 16:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 05/01/17 10:50 05/03/17 12:26 1Arsenic<1.0
2.5 0.37 ug/L 05/01/17 10:50 05/01/17 16:21 1Barium51
1.0 0.43 ug/L 05/01/17 10:50 05/01/17 16:21 1Beryllium<1.0
0.50 0.15 ug/L 05/01/17 10:50 05/01/17 16:21 1Cadmium<0.50
5.0 2.3 ug/L 05/01/17 10:50 05/01/17 16:21 1Chromium<5.0
1.0 0.27 ug/L 05/01/17 10:50 05/01/17 16:21 1Cobalt<1.0
2.0 0.63 ug/L 05/01/17 10:50 05/03/17 12:26 1Copper1.3 J
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-3Client Sample ID: MW-56A
Matrix: WaterDate Collected: 04/26/17 08:45
Date Received: 04/28/17 09:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron <100 100 38 ug/L 05/01/17 10:50 05/01/17 16:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 05/01/17 10:50 05/01/17 16:21 1Lead<0.50
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:21 1Manganese16
2.0 0.92 ug/L 05/01/17 10:50 05/01/17 16:21 1Nickel<2.0
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:21 1Selenium<2.5
0.50 0.078 ug/L 05/01/17 10:50 05/01/17 16:21 1Silver<0.50
2.0 0.65 ug/L 05/01/17 10:50 05/01/17 16:21 1Thallium<2.0
10 4.2 ug/L 05/01/17 10:50 05/01/17 16:21 1Tin<10
5.0 2.0 ug/L 05/01/17 10:50 05/01/17 16:21 1Vanadium<5.0
20 8.1 ug/L 05/01/17 10:50 05/03/17 12:26 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 05/03/17 12:50 05/04/17 08:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 05/08/17 14:00 05/08/17 16:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 1.7 mg/L 05/05/17 20:06 10Chloride19
2.0 0.95 mg/L 05/05/17 20:06 10Sulfate63
5.0 3.7 mg/L 05/05/17 15:51 1Alkalinity86
10 4.3 mg/L 05/02/17 04:40 1Total Dissolved Solids 230
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-4Client Sample ID: MW-56D
Matrix: WaterDate Collected: 04/26/17 08:30
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <5.0 5.0 1.7 ug/L 05/08/17 00:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 4.2 ug/L 05/08/17 00:17 1Acetonitrile<10
100 23 ug/L 05/08/17 00:17 1Acrolein<100
20 4.5 ug/L 05/08/17 00:17 1Acrylonitrile<20
0.50 0.15 ug/L 05/08/17 00:17 1Benzene<0.50
1.0 0.43 ug/L 05/08/17 00:17 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/08/17 00:17 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/08/17 00:17 1Bromoform<1.0
2.0 0.80 ug/L 05/08/17 00:17 1Bromomethane<2.0
5.0 2.1 ug/L 05/08/17 00:17 12-Butanone (MEK)<5.0
2.0 0.45 ug/L 05/08/17 00:17 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/08/17 00:17 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/08/17 00:17 1Chlorobenzene<1.0
1.0 0.23 ug/L 05/08/17 00:17 12-Chloro-1,3-butadiene <1.0
1.0 0.51 ug/L 05/08/17 00:17 1Chloroethane<1.0
2.0 0.37 ug/L 05/08/17 00:17 1Chloroform<2.0
1.0 0.32 ug/L 05/08/17 00:17 1Chloromethane<1.0
2.5 0.86 ug/L 05/08/17 00:17 13-Chloropropene <2.5
1.0 0.41 ug/L 05/08/17 00:17 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/08/17 00:17 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/08/17 00:17 1Dibromochloromethane<1.0
5.0 2.0 ug/L 05/08/17 00:17 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/08/17 00:17 11,2-Dibromoethane <1.0
1.0 0.27 ug/L 05/08/17 00:17 1Dibromomethane<1.0
1.0 0.40 ug/L 05/08/17 00:17 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 05/08/17 00:17 11,4-Dichlorobenzene <1.0
1.0 0.33 ug/L 05/08/17 00:17 11,2-Dichlorobenzene <1.0
2.0 0.67 ug/L 05/08/17 00:17 1Dichlorodifluoromethane<2.0
1.0 0.41 ug/L 05/08/17 00:17 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/08/17 00:17 11,2-Dichloroethane <1.0
1.0 0.39 ug/L 05/08/17 00:17 11,1-Dichloroethene <1.0
1.0 0.44 ug/L 05/08/17 00:17 12,2-Dichloropropane <1.0
1.0 0.43 ug/L 05/08/17 00:17 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/08/17 00:17 11,3-Dichloropropane <1.0
1.0 0.30 ug/L 05/08/17 00:17 11,1-Dichloropropene <1.0
0.50 0.18 ug/L 05/08/17 00:17 1Ethylbenzene<0.50
2.5 0.53 ug/L 05/08/17 00:17 1Ethyl methacrylate <2.5
1.0 0.45 ug/L 05/08/17 00:17 1Hexachlorobutadiene<1.0
5.0 1.6 ug/L 05/08/17 00:17 12-Hexanone <5.0
2.5 0.66 ug/L 05/08/17 00:17 1Iodomethane<2.5
100 36 ug/L 05/08/17 00:17 1Isobutyl alcohol <100
10 2.5 ug/L 05/08/17 00:17 1Methacrylonitrile<10
5.0 1.6 ug/L 05/08/17 00:17 1Methylene Chloride <5.0
2.5 0.55 ug/L 05/08/17 00:17 1Methyl methacrylate <2.5
5.0 2.2 ug/L 05/08/17 00:17 14-Methyl-2-pentanone (MIBK)<5.0
10 4.8 ug/L 05/08/17 00:17 1Propionitrile<10
1.0 0.39 ug/L 05/08/17 00:17 1Styrene<1.0
1.0 0.46 ug/L 05/08/17 00:17 11,1,1,2-Tetrachloroethane <1.0
1.0 0.40 ug/L 05/08/17 00:17 11,1,2,2-Tetrachloroethane <1.0
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-4Client Sample ID: MW-56D
Matrix: WaterDate Collected: 04/26/17 08:30
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Tetrachloroethene <1.0 1.0 0.37 ug/L 05/08/17 00:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 1.9 ug/L 05/08/17 00:17 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/08/17 00:17 1Toluene<0.50
5.0 1.2 ug/L 05/08/17 00:17 1trans-1,4-Dichloro-2-butene <5.0
1.0 0.35 ug/L 05/08/17 00:17 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/08/17 00:17 1trans-1,3-Dichloropropene <1.0
1.0 0.34 ug/L 05/08/17 00:17 11,2,4-Trichlorobenzene <1.0
1.0 0.38 ug/L 05/08/17 00:17 11,1,1-Trichloroethane <1.0
1.0 0.35 ug/L 05/08/17 00:17 11,1,2-Trichloroethane <1.0
0.50 0.16 ug/L 05/08/17 00:17 1Trichloroethene<0.50
1.0 0.43 ug/L 05/08/17 00:17 1Trichlorofluoromethane<1.0
1.0 0.41 ug/L 05/08/17 00:17 11,2,3-Trichloropropane <1.0
2.0 0.91 ug/L 05/08/17 00:17 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/08/17 00:17 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/08/17 00:17 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)104 75-126 05/08/17 00:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)101 05/08/17 00:17 175-120
4-Bromofluorobenzene (Surr)109 05/08/17 00:17 172-124
Dibromofluoromethane 91 05/08/17 00:17 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.78 0.78 0.24 ug/L 05/01/17 15:19 05/07/17 16:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.78 0.21 ug/L 05/01/17 15:19 05/07/17 16:42 1Acenaphthylene<0.78
3.9 0.52 ug/L 05/01/17 15:19 05/07/17 16:42 1Acetophenone<3.9
7.8 1.7 ug/L 05/01/17 15:19 05/07/17 16:42 12-Acetylaminofluorene <7.8
7.8 2.9 ug/L 05/01/17 15:19 05/07/17 16:42 14-Aminobiphenyl <7.8
0.78 0.26 ug/L 05/01/17 15:19 05/07/17 16:42 1Anthracene<0.78
0.16 0.044 ug/L 05/01/17 15:19 05/07/17 16:42 1Benzo[a]anthracene <0.16
0.16 0.077 ug/L 05/01/17 15:19 05/07/17 16:42 1Benzo[a]pyrene <0.16
0.16 0.063 ug/L 05/01/17 15:19 05/07/17 16:42 1Benzo[b]fluoranthene <0.16
0.78 0.29 ug/L 05/01/17 15:19 05/07/17 16:42 1Benzo[g,h,i]perylene <0.78
0.16 0.050 ug/L 05/01/17 15:19 05/07/17 16:42 1Benzo[k]fluoranthene <0.16
16 4.7 ug/L 05/01/17 15:19 05/07/17 16:42 1Benzyl alcohol <16
1.6 0.22 ug/L 05/01/17 15:19 05/07/17 16:42 1Bis(2-chloroethoxy)methane <1.6
1.6 0.23 ug/L 05/01/17 15:19 05/07/17 16:42 1Bis(2-chloroethyl)ether <1.6
7.8 1.3 ug/L 05/01/17 15:19 05/07/17 16:42 1Bis(2-ethylhexyl) phthalate <7.8
3.9 0.42 ug/L 05/01/17 15:19 05/07/17 16:42 14-Bromophenyl phenyl ether <3.9
1.6 0.37 ug/L 05/01/17 15:19 05/07/17 16:42 1Butyl benzyl phthalate <1.6
7.8 1.6 ug/L 05/01/17 15:19 05/07/17 16:42 14-Chloroaniline <7.8
7.8 2.7 ug/L 05/01/17 15:19 05/07/17 16:42 1Chlorobenzilate<7.8
7.8 1.8 ug/L 05/01/17 15:19 05/07/17 16:42 14-Chloro-3-methylphenol <7.8
1.6 0.18 ug/L 05/01/17 15:19 05/07/17 16:42 12-Chloronaphthalene <1.6
3.9 0.44 ug/L 05/01/17 15:19 05/07/17 16:42 12-Chlorophenol <3.9
3.9 0.50 ug/L 05/01/17 15:19 05/07/17 16:42 14-Chlorophenyl phenyl ether <3.9
0.16 0.053 ug/L 05/01/17 15:19 05/07/17 16:42 1Chrysene<0.16
7.8 4.3 ug/L 05/01/17 15:19 05/07/17 16:42 1Diallate<7.8
0.23 0.040 ug/L 05/01/17 15:19 05/07/17 16:42 1Dibenz(a,h)anthracene <0.23
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-4Client Sample ID: MW-56D
Matrix: WaterDate Collected: 04/26/17 08:30
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.6 1.6 0.20 ug/L 05/01/17 15:19 05/07/17 16:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.9 1.3 ug/L 05/01/17 15:19 05/07/17 16:42 13,3'-Dichlorobenzidine <3.9
7.8 2.0 ug/L 05/01/17 15:19 05/07/17 16:42 12,4-Dichlorophenol <7.8
7.8 2.7 ug/L 05/01/17 15:19 05/07/17 16:42 12,6-Dichlorophenol <7.8
1.6 0.28 ug/L 05/01/17 15:19 05/07/17 16:42 1Diethyl phthalate <1.6
7.8 1.5 ug/L 05/01/17 15:19 05/07/17 16:42 1Dimethoate<7.8
31 2.3 ug/L 05/01/17 15:19 05/07/17 16:42 17,12-Dimethylbenz(a)anthracene <31
31 14 ug/L 05/01/17 15:19 05/07/17 16:42 13,3'-Dimethylbenzidine <31
7.8 1.4 ug/L 05/01/17 15:19 05/07/17 16:42 12,4-Dimethylphenol <7.8
1.6 0.24 ug/L 05/01/17 15:19 05/07/17 16:42 1Dimethyl phthalate <1.6
3.9 0.57 ug/L 05/01/17 15:19 05/07/17 16:42 1Di-n-butyl phthalate <3.9
16 4.6 ug/L 05/01/17 15:19 05/07/17 16:42 14,6-Dinitro-2-methylphenol <16
16 6.7 ug/L 05/01/17 15:19 05/07/17 16:42 12,4-Dinitrophenol <16
0.78 0.058 ug/L 05/01/17 15:19 05/07/17 16:42 12,6-Dinitrotoluene <0.78
0.78 0.19 ug/L 05/01/17 15:19 05/07/17 16:42 12,4-Dinitrotoluene <0.78
7.8 0.82 ug/L 05/01/17 15:19 05/07/17 16:42 1Di-n-octyl phthalate <7.8
7.8 2.0 ug/L 05/01/17 15:19 05/07/17 16:42 1Diphenylamine<7.8
7.8 1.5 ug/L 05/01/17 15:19 05/07/17 16:42 1Disulfoton<7.8
16 3.0 ug/L 05/01/17 15:19 05/07/17 16:42 1Ethyl methanesulfonate <16
7.8 1.6 ug/L 05/01/17 15:19 05/07/17 16:42 1Ethyl Parathion <7.8
31 23 ug/L 05/01/17 15:19 05/07/17 16:42 1Famphur<31
0.78 0.35 ug/L 05/01/17 15:19 05/07/17 16:42 1Fluoranthene<0.78
0.78 0.19 ug/L 05/01/17 15:19 05/07/17 16:42 1Fluorene<0.78
0.39 0.062 ug/L 05/01/17 15:19 05/07/17 16:42 1Hexachlorobenzene<0.39
16 5.0 ug/L 05/01/17 15:19 05/07/17 16:42 1Hexachlorocyclopentadiene<16
3.9 0.47 ug/L 05/01/17 15:19 05/07/17 16:42 1Hexachloroethane<3.9
16 3.7 ug/L 05/01/17 15:19 05/07/17 16:42 1Hexachloropropene<16
0.16 0.058 ug/L 05/01/17 15:19 05/07/17 16:42 1Indeno[1,2,3-cd]pyrene <0.16
16 5.4 ug/L 05/01/17 15:19 05/07/17 16:42 1Isodrin<16
1.6 0.29 ug/L 05/01/17 15:19 05/07/17 16:42 1Isophorone<1.6
7.8 3.0 ug/L 05/01/17 15:19 05/07/17 16:42 1Isosafrole<7.8
7.8 1.3 ug/L 05/01/17 15:19 05/07/17 16:42 1Kepone<7.8
3.9 1.0 ug/L 05/01/17 15:19 05/07/17 16:42 1m-Dinitrobenzene <3.9
31 7.9 ug/L 05/01/17 15:19 05/07/17 16:42 1Methapyrilene<31
7.8 1.8 ug/L 05/01/17 15:19 05/07/17 16:42 13-Methylcholanthrene <7.8
31 4.6 ug/L 05/01/17 15:19 05/07/17 16:42 1Methyl methanesulfonate <31
1.6 0.051 ug/L 05/01/17 15:19 05/07/17 16:42 12-Methylnaphthalene <1.6
7.8 1.8 ug/L 05/01/17 15:19 05/07/17 16:42 1Methyl parathion <7.8
1.6 0.24 ug/L 05/01/17 15:19 05/07/17 16:42 12-Methylphenol <1.6
1.6 0.35 ug/L 05/01/17 15:19 05/07/17 16:42 13 & 4 Methylphenol <1.6
0.78 0.24 ug/L 05/01/17 15:19 05/07/17 16:42 1Naphthalene<0.78
31 30 ug/L 05/01/17 15:19 05/07/17 16:42 11,4-Naphthoquinone <31
16 4.6 ug/L 05/01/17 15:19 05/07/17 16:42 11-Naphthylamine <16
16 7.1 ug/L 05/01/17 15:19 05/07/17 16:42 12-Naphthylamine <16
3.9 1.0 ug/L 05/01/17 15:19 05/07/17 16:42 12-Nitroaniline <3.9
7.8 1.4 ug/L 05/01/17 15:19 05/07/17 16:42 13-Nitroaniline <7.8
7.8 1.3 ug/L 05/01/17 15:19 05/07/17 16:42 14-Nitroaniline <7.8
0.78 0.35 ug/L 05/01/17 15:19 05/07/17 16:42 1Nitrobenzene<0.78
7.8 2.4 ug/L 05/01/17 15:19 05/07/17 16:42 15-Nitro-o-toluidine <7.8
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-4Client Sample ID: MW-56D
Matrix: WaterDate Collected: 04/26/17 08:30
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.8 7.8 2.0 ug/L 05/01/17 15:19 05/07/17 16:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
16 5.8 ug/L 05/01/17 15:19 05/07/17 16:42 14-Nitrophenol <16
16 6.7 ug/L 05/01/17 15:19 05/07/17 16:42 1N-Nitrosodiethylamine <16
7.8 3.7 ug/L 05/01/17 15:19 05/07/17 16:42 1N-Nitrosodimethylamine <7.8
7.8 3.3 ug/L 05/01/17 15:19 05/07/17 16:42 1N-Nitrosodi-n-butylamine <7.8
0.39 0.12 ug/L 05/01/17 15:19 05/07/17 16:42 1N-Nitrosodi-n-propylamine <0.39
1.6 0.29 ug/L 05/01/17 15:19 05/07/17 16:42 1N-Nitrosodiphenylamine <1.6
16 5.8 ug/L 05/01/17 15:19 05/07/17 16:42 1N-Nitrosomethylethylamine <16
7.8 2.7 ug/L 05/01/17 15:19 05/07/17 16:42 1N-Nitrosopiperidine <7.8
7.8 2.6 ug/L 05/01/17 15:19 05/07/17 16:42 1N-Nitrosopyrrolidine <7.8
16 4.3 ug/L 05/01/17 15:19 05/07/17 16:42 1o,o',o''-Triethylphosphorothioate <16
31 6.2 ug/L 05/01/17 15:19 05/07/17 16:42 1o-Toluidine <31
1.6 0.30 ug/L 05/01/17 15:19 05/07/17 16:42 12,2'-oxybis[1-chloropropane]<1.6
7.8 2.3 ug/L 05/01/17 15:19 05/07/17 16:42 1p-Dimethylamino azobenzene <7.8
7.8 2.2 ug/L 05/01/17 15:19 05/07/17 16:42 1Pentachlorobenzene<7.8
7.8 2.8 ug/L 05/01/17 15:19 05/07/17 16:42 1Pentachloronitrobenzene<7.8
7.8 1.8 ug/L 05/01/17 15:19 05/07/17 16:42 1Phenacetin<7.8
0.78 0.23 ug/L 05/01/17 15:19 05/07/17 16:42 1Phenanthrene<0.78
3.9 0.52 ug/L 05/01/17 15:19 05/07/17 16:42 1Phenol<3.9
7.8 1.7 ug/L 05/01/17 15:19 05/07/17 16:42 1Phorate<7.8
62 13 ug/L 05/01/17 15:19 05/07/17 16:42 1p-Phenylene diamine <62
7.8 1.7 ug/L 05/01/17 15:19 05/07/17 16:42 1Pronamide<7.8
0.78 0.33 ug/L 05/01/17 15:19 05/07/17 16:42 1Pyrene<0.78
7.8 3.1 ug/L 05/01/17 15:19 05/07/17 16:42 1Safrole<7.8
7.8 1.5 ug/L 05/01/17 15:19 05/07/17 16:42 1sym-Trinitrobenzene <7.8
7.8 7.8 ug/L 05/01/17 15:19 05/07/17 16:42 12,3,7,8-TCDD (Screen)<7.8
3.9 0.45 ug/L 05/01/17 15:19 05/07/17 16:42 11,2,4,5-Tetrachlorobenzene <3.9
3.9 0.58 ug/L 05/01/17 15:19 05/07/17 16:42 12,3,4,6-Tetrachlorophenol <3.9
7.8 2.0 ug/L 05/01/17 15:19 05/07/17 16:42 1Thionazin<7.8
3.9 0.56 ug/L 05/01/17 15:19 05/07/17 16:42 12,4,6-Trichlorophenol <3.9
7.8 2.0 ug/L 05/01/17 15:19 05/07/17 16:42 12,4,5-Trichlorophenol <7.8
2-Fluorophenol 70 27-110 05/01/17 15:19 05/07/17 16:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Phenol-d5 51 05/01/17 15:19 05/07/17 16:42 120-100
Nitrobenzene-d5 74 05/01/17 15:19 05/07/17 16:42 136-120
2-Fluorobiphenyl 71 05/01/17 15:19 05/07/17 16:42 134-110
2,4,6-Tribromophenol 107 05/01/17 15:19 05/07/17 16:42 140-145
Terphenyl-d14 96 05/01/17 15:19 05/07/17 16:42 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.040 0.040 0.0026 ug/L 05/01/17 10:27 05/05/17 01:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.040 0.010 ug/L 05/01/17 10:27 05/05/17 01:27 1beta-BHC <0.040
0.040 0.010 ug/L 05/01/17 10:27 05/05/17 01:27 1delta-BHC <0.040
0.040 0.0056 ug/L 05/01/17 10:27 05/05/17 01:27 1gamma-BHC (Lindane)<0.040
0.040 0.014 ug/L 05/01/17 10:27 05/05/17 01:27 1Heptachlor<0.040
0.040 0.0053 ug/L 05/01/17 10:27 05/05/17 01:27 1Aldrin<0.040
0.040 0.014 ug/L 05/01/17 10:27 05/05/17 01:27 1Heptachlor epoxide <0.040
0.040 0.0041 ug/L 05/01/17 10:27 05/05/17 01:27 1Endosulfan I <0.040
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-4Client Sample ID: MW-56D
Matrix: WaterDate Collected: 04/26/17 08:30
Date Received: 04/28/17 09:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.040 0.040 0.013 ug/L 05/01/17 10:27 05/05/17 01:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.040 0.0038 ug/L 05/01/17 10:27 05/05/17 01:27 14,4'-DDE <0.040
0.040 0.014 ug/L 05/01/17 10:27 05/05/17 01:27 1Endrin<0.040
0.040 0.0028 ug/L 05/01/17 10:27 05/05/17 01:27 1Endosulfan II <0.040
0.040 0.013 ug/L 05/01/17 10:27 05/05/17 01:27 14,4'-DDD <0.040
0.040 0.012 ug/L 05/01/17 10:27 05/05/17 01:27 1Endosulfan sulfate <0.040
0.040 0.0032 ug/L 05/01/17 10:27 05/05/17 01:27 14,4'-DDT <0.040
0.081 0.023 ug/L 05/01/17 10:27 05/05/17 01:27 1Methoxychlor<0.081
0.40 0.20 ug/L 05/01/17 10:27 05/05/17 01:27 1Toxaphene<0.40
0.040 0.0083 ug/L 05/01/17 10:27 05/05/17 01:27 1Endrin aldehyde <0.040
0.081 0.040 ug/L 05/01/17 10:27 05/05/17 01:27 1Chlordane (technical)<0.081
DCB Decachlorobiphenyl 75 30-130 05/01/17 10:27 05/05/17 01:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 83 05/01/17 10:27 05/05/17 01:27 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.40 0.40 0.067 ug/L 05/01/17 10:27 05/02/17 13:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.20 ug/L 05/01/17 10:27 05/02/17 13:37 1PCB-1221 <0.40
0.40 0.20 ug/L 05/01/17 10:27 05/02/17 13:37 1PCB-1232 <0.40
0.40 0.20 ug/L 05/01/17 10:27 05/02/17 13:37 1PCB-1242 <0.40
0.40 0.20 ug/L 05/01/17 10:27 05/02/17 13:37 1PCB-1248 <0.40
0.40 0.20 ug/L 05/01/17 10:27 05/02/17 13:37 1PCB-1254 <0.40
0.40 0.070 ug/L 05/01/17 10:27 05/02/17 13:37 1PCB-1260 <0.40
Tetrachloro-m-xylene 75 30-120 05/01/17 10:27 05/02/17 13:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 87 05/01/17 10:27 05/02/17 13:37 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <1.1 1.1 0.52 ug/L 05/02/17 10:54 05/09/17 01:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.56 0.10 ug/L 05/02/17 10:54 05/09/17 01:52 1Pentachlorophenol<0.56
1.1 0.32 ug/L 05/02/17 10:54 05/09/17 01:52 1Silvex (2,4,5-TP)<1.1
1.1 0.48 ug/L 05/02/17 10:54 05/09/17 01:52 12,4,5-T <1.1
2.2 0.18 ug/L 05/02/17 10:54 05/09/17 01:52 1Dinoseb<2.2
DCAA 65 25-130 05/02/17 10:54 05/09/17 01:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 05/01/17 10:50 05/01/17 16:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 05/01/17 10:50 05/03/17 12:29 1Arsenic0.41 J
2.5 0.37 ug/L 05/01/17 10:50 05/01/17 16:24 1Barium31
1.0 0.43 ug/L 05/01/17 10:50 05/01/17 16:24 1Beryllium<1.0
0.50 0.15 ug/L 05/01/17 10:50 05/01/17 16:24 1Cadmium<0.50
5.0 2.3 ug/L 05/01/17 10:50 05/01/17 16:24 1Chromium<5.0
1.0 0.27 ug/L 05/01/17 10:50 05/01/17 16:24 1Cobalt0.55 J
2.0 0.63 ug/L 05/01/17 10:50 05/03/17 12:29 1Copper1.7 J
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-4Client Sample ID: MW-56D
Matrix: WaterDate Collected: 04/26/17 08:30
Date Received: 04/28/17 09:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 540 100 38 ug/L 05/01/17 10:50 05/01/17 16:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 05/01/17 10:50 05/01/17 16:24 1Lead0.78
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:24 1Manganese37
2.0 0.92 ug/L 05/01/17 10:50 05/01/17 16:24 1Nickel1.7 J
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:24 1Selenium<2.5
0.50 0.078 ug/L 05/01/17 10:50 05/01/17 16:24 1Silver<0.50
2.0 0.65 ug/L 05/01/17 10:50 05/01/17 16:24 1Thallium<2.0
10 4.2 ug/L 05/01/17 10:50 05/01/17 16:24 1Tin<10
5.0 2.0 ug/L 05/01/17 10:50 05/01/17 16:24 1Vanadium<5.0
20 8.1 ug/L 05/01/17 10:50 05/03/17 12:29 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 05/03/17 12:50 05/04/17 08:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 05/08/17 14:00 05/08/17 16:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 1.7 mg/L 05/05/17 20:18 10Chloride14
2.0 0.95 mg/L 05/05/17 20:18 10Sulfate74
5.0 3.7 mg/L 05/05/17 15:57 1Alkalinity180
10 4.3 mg/L 05/02/17 04:42 1Total Dissolved Solids 330
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-5Client Sample ID: MW-57
Matrix: WaterDate Collected: 04/26/17 09:45
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <5.0 5.0 1.7 ug/L 05/08/17 00:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 4.2 ug/L 05/08/17 00:43 1Acetonitrile<10
100 23 ug/L 05/08/17 00:43 1Acrolein<100
20 4.5 ug/L 05/08/17 00:43 1Acrylonitrile<20
0.50 0.15 ug/L 05/08/17 00:43 1Benzene<0.50
1.0 0.43 ug/L 05/08/17 00:43 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/08/17 00:43 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/08/17 00:43 1Bromoform<1.0
2.0 0.80 ug/L 05/08/17 00:43 1Bromomethane<2.0
5.0 2.1 ug/L 05/08/17 00:43 12-Butanone (MEK)<5.0
2.0 0.45 ug/L 05/08/17 00:43 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/08/17 00:43 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/08/17 00:43 1Chlorobenzene<1.0
1.0 0.23 ug/L 05/08/17 00:43 12-Chloro-1,3-butadiene <1.0
1.0 0.51 ug/L 05/08/17 00:43 1Chloroethane<1.0
2.0 0.37 ug/L 05/08/17 00:43 1Chloroform<2.0
1.0 0.32 ug/L 05/08/17 00:43 1Chloromethane<1.0
2.5 0.86 ug/L 05/08/17 00:43 13-Chloropropene <2.5
1.0 0.41 ug/L 05/08/17 00:43 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/08/17 00:43 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/08/17 00:43 1Dibromochloromethane<1.0
5.0 2.0 ug/L 05/08/17 00:43 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/08/17 00:43 11,2-Dibromoethane <1.0
1.0 0.27 ug/L 05/08/17 00:43 1Dibromomethane<1.0
1.0 0.40 ug/L 05/08/17 00:43 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 05/08/17 00:43 11,4-Dichlorobenzene <1.0
1.0 0.33 ug/L 05/08/17 00:43 11,2-Dichlorobenzene <1.0
2.0 0.67 ug/L 05/08/17 00:43 1Dichlorodifluoromethane<2.0
1.0 0.41 ug/L 05/08/17 00:43 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/08/17 00:43 11,2-Dichloroethane <1.0
1.0 0.39 ug/L 05/08/17 00:43 11,1-Dichloroethene <1.0
1.0 0.44 ug/L 05/08/17 00:43 12,2-Dichloropropane <1.0
1.0 0.43 ug/L 05/08/17 00:43 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/08/17 00:43 11,3-Dichloropropane <1.0
1.0 0.30 ug/L 05/08/17 00:43 11,1-Dichloropropene <1.0
0.50 0.18 ug/L 05/08/17 00:43 1Ethylbenzene<0.50
2.5 0.53 ug/L 05/08/17 00:43 1Ethyl methacrylate <2.5
1.0 0.45 ug/L 05/08/17 00:43 1Hexachlorobutadiene<1.0
5.0 1.6 ug/L 05/08/17 00:43 12-Hexanone <5.0
2.5 0.66 ug/L 05/08/17 00:43 1Iodomethane<2.5
100 36 ug/L 05/08/17 00:43 1Isobutyl alcohol <100
10 2.5 ug/L 05/08/17 00:43 1Methacrylonitrile<10
5.0 1.6 ug/L 05/08/17 00:43 1Methylene Chloride <5.0
2.5 0.55 ug/L 05/08/17 00:43 1Methyl methacrylate <2.5
5.0 2.2 ug/L 05/08/17 00:43 14-Methyl-2-pentanone (MIBK)<5.0
10 4.8 ug/L 05/08/17 00:43 1Propionitrile<10
1.0 0.39 ug/L 05/08/17 00:43 1Styrene<1.0
1.0 0.46 ug/L 05/08/17 00:43 11,1,1,2-Tetrachloroethane <1.0
1.0 0.40 ug/L 05/08/17 00:43 11,1,2,2-Tetrachloroethane <1.0
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-5Client Sample ID: MW-57
Matrix: WaterDate Collected: 04/26/17 09:45
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Tetrachloroethene <1.0 1.0 0.37 ug/L 05/08/17 00:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 1.9 ug/L 05/08/17 00:43 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/08/17 00:43 1Toluene<0.50
5.0 1.2 ug/L 05/08/17 00:43 1trans-1,4-Dichloro-2-butene <5.0
1.0 0.35 ug/L 05/08/17 00:43 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/08/17 00:43 1trans-1,3-Dichloropropene <1.0
1.0 0.34 ug/L 05/08/17 00:43 11,2,4-Trichlorobenzene <1.0
1.0 0.38 ug/L 05/08/17 00:43 11,1,1-Trichloroethane <1.0
1.0 0.35 ug/L 05/08/17 00:43 11,1,2-Trichloroethane <1.0
0.50 0.16 ug/L 05/08/17 00:43 1Trichloroethene<0.50
1.0 0.43 ug/L 05/08/17 00:43 1Trichlorofluoromethane<1.0
1.0 0.41 ug/L 05/08/17 00:43 11,2,3-Trichloropropane <1.0
2.0 0.91 ug/L 05/08/17 00:43 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/08/17 00:43 1Vinyl chloride 3.3 cn
1.0 0.22 ug/L 05/08/17 00:43 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)104 75-126 05/08/17 00:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)100 05/08/17 00:43 175-120
4-Bromofluorobenzene (Surr)108 05/08/17 00:43 172-124
Dibromofluoromethane 89 05/08/17 00:43 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.74 0.74 0.23 ug/L 05/01/17 15:19 05/07/17 17:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.74 0.20 ug/L 05/01/17 15:19 05/07/17 17:07 1Acenaphthylene<0.74
3.7 0.49 ug/L 05/01/17 15:19 05/07/17 17:07 1Acetophenone<3.7
7.4 1.6 ug/L 05/01/17 15:19 05/07/17 17:07 12-Acetylaminofluorene <7.4
7.4 2.8 ug/L 05/01/17 15:19 05/07/17 17:07 14-Aminobiphenyl <7.4
0.74 0.25 ug/L 05/01/17 15:19 05/07/17 17:07 1Anthracene<0.74
0.15 0.042 ug/L 05/01/17 15:19 05/07/17 17:07 1Benzo[a]anthracene <0.15
0.15 0.074 ug/L 05/01/17 15:19 05/07/17 17:07 1Benzo[a]pyrene <0.15
0.15 0.060 ug/L 05/01/17 15:19 05/07/17 17:07 1Benzo[b]fluoranthene <0.15
0.74 0.28 ug/L 05/01/17 15:19 05/07/17 17:07 1Benzo[g,h,i]perylene <0.74
0.15 0.048 ug/L 05/01/17 15:19 05/07/17 17:07 1Benzo[k]fluoranthene <0.15
15 4.5 ug/L 05/01/17 15:19 05/07/17 17:07 1Benzyl alcohol <15
1.5 0.21 ug/L 05/01/17 15:19 05/07/17 17:07 1Bis(2-chloroethoxy)methane <1.5
1.5 0.22 ug/L 05/01/17 15:19 05/07/17 17:07 1Bis(2-chloroethyl)ether <1.5
7.4 1.3 ug/L 05/01/17 15:19 05/07/17 17:07 1Bis(2-ethylhexyl) phthalate <7.4
3.7 0.40 ug/L 05/01/17 15:19 05/07/17 17:07 14-Bromophenyl phenyl ether <3.7
1.5 0.36 ug/L 05/01/17 15:19 05/07/17 17:07 1Butyl benzyl phthalate <1.5
7.4 1.5 ug/L 05/01/17 15:19 05/07/17 17:07 14-Chloroaniline <7.4
7.4 2.5 ug/L 05/01/17 15:19 05/07/17 17:07 1Chlorobenzilate<7.4
7.4 1.7 ug/L 05/01/17 15:19 05/07/17 17:07 14-Chloro-3-methylphenol <7.4
1.5 0.18 ug/L 05/01/17 15:19 05/07/17 17:07 12-Chloronaphthalene <1.5
3.7 0.42 ug/L 05/01/17 15:19 05/07/17 17:07 12-Chlorophenol <3.7
3.7 0.47 ug/L 05/01/17 15:19 05/07/17 17:07 14-Chlorophenyl phenyl ether <3.7
0.15 0.051 ug/L 05/01/17 15:19 05/07/17 17:07 1Chrysene<0.15
7.4 4.1 ug/L 05/01/17 15:19 05/07/17 17:07 1Diallate<7.4
0.22 0.038 ug/L 05/01/17 15:19 05/07/17 17:07 1Dibenz(a,h)anthracene <0.22
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-5Client Sample ID: MW-57
Matrix: WaterDate Collected: 04/26/17 09:45
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.5 1.5 0.20 ug/L 05/01/17 15:19 05/07/17 17:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.7 1.3 ug/L 05/01/17 15:19 05/07/17 17:07 13,3'-Dichlorobenzidine <3.7
7.4 1.9 ug/L 05/01/17 15:19 05/07/17 17:07 12,4-Dichlorophenol <7.4
7.4 2.6 ug/L 05/01/17 15:19 05/07/17 17:07 12,6-Dichlorophenol <7.4
1.5 0.27 ug/L 05/01/17 15:19 05/07/17 17:07 1Diethyl phthalate <1.5
7.4 1.4 ug/L 05/01/17 15:19 05/07/17 17:07 1Dimethoate<7.4
30 2.2 ug/L 05/01/17 15:19 05/07/17 17:07 17,12-Dimethylbenz(a)anthracene <30
30 13 ug/L 05/01/17 15:19 05/07/17 17:07 13,3'-Dimethylbenzidine <30
7.4 1.3 ug/L 05/01/17 15:19 05/07/17 17:07 12,4-Dimethylphenol <7.4
1.5 0.23 ug/L 05/01/17 15:19 05/07/17 17:07 1Dimethyl phthalate <1.5
3.7 0.54 ug/L 05/01/17 15:19 05/07/17 17:07 1Di-n-butyl phthalate <3.7
15 4.4 ug/L 05/01/17 15:19 05/07/17 17:07 14,6-Dinitro-2-methylphenol <15
15 6.4 ug/L 05/01/17 15:19 05/07/17 17:07 12,4-Dinitrophenol <15
0.74 0.055 ug/L 05/01/17 15:19 05/07/17 17:07 12,6-Dinitrotoluene <0.74
0.74 0.18 ug/L 05/01/17 15:19 05/07/17 17:07 12,4-Dinitrotoluene <0.74
7.4 0.78 ug/L 05/01/17 15:19 05/07/17 17:07 1Di-n-octyl phthalate <7.4
7.4 1.9 ug/L 05/01/17 15:19 05/07/17 17:07 1Diphenylamine<7.4
7.4 1.4 ug/L 05/01/17 15:19 05/07/17 17:07 1Disulfoton<7.4
15 2.8 ug/L 05/01/17 15:19 05/07/17 17:07 1Ethyl methanesulfonate <15
7.4 1.6 ug/L 05/01/17 15:19 05/07/17 17:07 1Ethyl Parathion <7.4
30 22 ug/L 05/01/17 15:19 05/07/17 17:07 1Famphur<30
0.74 0.34 ug/L 05/01/17 15:19 05/07/17 17:07 1Fluoranthene<0.74
0.74 0.18 ug/L 05/01/17 15:19 05/07/17 17:07 1Fluorene<0.74
0.37 0.059 ug/L 05/01/17 15:19 05/07/17 17:07 1Hexachlorobenzene<0.37
15 4.7 ug/L 05/01/17 15:19 05/07/17 17:07 1Hexachlorocyclopentadiene<15
3.7 0.45 ug/L 05/01/17 15:19 05/07/17 17:07 1Hexachloroethane<3.7
15 3.5 ug/L 05/01/17 15:19 05/07/17 17:07 1Hexachloropropene<15
0.15 0.056 ug/L 05/01/17 15:19 05/07/17 17:07 1Indeno[1,2,3-cd]pyrene <0.15
15 5.1 ug/L 05/01/17 15:19 05/07/17 17:07 1Isodrin<15
1.5 0.28 ug/L 05/01/17 15:19 05/07/17 17:07 1Isophorone<1.5
7.4 2.9 ug/L 05/01/17 15:19 05/07/17 17:07 1Isosafrole<7.4
7.4 1.2 ug/L 05/01/17 15:19 05/07/17 17:07 1Kepone<7.4
3.7 0.99 ug/L 05/01/17 15:19 05/07/17 17:07 1m-Dinitrobenzene <3.7
30 7.6 ug/L 05/01/17 15:19 05/07/17 17:07 1Methapyrilene<30
7.4 1.7 ug/L 05/01/17 15:19 05/07/17 17:07 13-Methylcholanthrene <7.4
30 4.4 ug/L 05/01/17 15:19 05/07/17 17:07 1Methyl methanesulfonate <30
1.5 0.049 ug/L 05/01/17 15:19 05/07/17 17:07 12-Methylnaphthalene <1.5
7.4 1.7 ug/L 05/01/17 15:19 05/07/17 17:07 1Methyl parathion <7.4
1.5 0.23 ug/L 05/01/17 15:19 05/07/17 17:07 12-Methylphenol <1.5
1.5 0.33 ug/L 05/01/17 15:19 05/07/17 17:07 13 & 4 Methylphenol <1.5
0.74 0.23 ug/L 05/01/17 15:19 05/07/17 17:07 1Naphthalene<0.74
30 29 ug/L 05/01/17 15:19 05/07/17 17:07 11,4-Naphthoquinone <30
15 4.4 ug/L 05/01/17 15:19 05/07/17 17:07 11-Naphthylamine <15
15 6.8 ug/L 05/01/17 15:19 05/07/17 17:07 12-Naphthylamine <15
3.7 0.96 ug/L 05/01/17 15:19 05/07/17 17:07 12-Nitroaniline <3.7
7.4 1.3 ug/L 05/01/17 15:19 05/07/17 17:07 13-Nitroaniline <7.4
7.4 1.2 ug/L 05/01/17 15:19 05/07/17 17:07 14-Nitroaniline <7.4
0.74 0.33 ug/L 05/01/17 15:19 05/07/17 17:07 1Nitrobenzene<0.74
7.4 2.3 ug/L 05/01/17 15:19 05/07/17 17:07 15-Nitro-o-toluidine <7.4
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-5Client Sample ID: MW-57
Matrix: WaterDate Collected: 04/26/17 09:45
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.4 7.4 1.9 ug/L 05/01/17 15:19 05/07/17 17:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 5.5 ug/L 05/01/17 15:19 05/07/17 17:07 14-Nitrophenol <15
15 6.4 ug/L 05/01/17 15:19 05/07/17 17:07 1N-Nitrosodiethylamine <15
7.4 3.5 ug/L 05/01/17 15:19 05/07/17 17:07 1N-Nitrosodimethylamine <7.4
7.4 3.1 ug/L 05/01/17 15:19 05/07/17 17:07 1N-Nitrosodi-n-butylamine <7.4
0.37 0.11 ug/L 05/01/17 15:19 05/07/17 17:07 1N-Nitrosodi-n-propylamine <0.37
1.5 0.28 ug/L 05/01/17 15:19 05/07/17 17:07 1N-Nitrosodiphenylamine <1.5
15 5.6 ug/L 05/01/17 15:19 05/07/17 17:07 1N-Nitrosomethylethylamine <15
7.4 2.6 ug/L 05/01/17 15:19 05/07/17 17:07 1N-Nitrosopiperidine <7.4
7.4 2.5 ug/L 05/01/17 15:19 05/07/17 17:07 1N-Nitrosopyrrolidine <7.4
15 4.1 ug/L 05/01/17 15:19 05/07/17 17:07 1o,o',o''-Triethylphosphorothioate <15
30 5.9 ug/L 05/01/17 15:19 05/07/17 17:07 1o-Toluidine <30
1.5 0.28 ug/L 05/01/17 15:19 05/07/17 17:07 12,2'-oxybis[1-chloropropane]<1.5
7.4 2.2 ug/L 05/01/17 15:19 05/07/17 17:07 1p-Dimethylamino azobenzene <7.4
7.4 2.1 ug/L 05/01/17 15:19 05/07/17 17:07 1Pentachlorobenzene<7.4
7.4 2.7 ug/L 05/01/17 15:19 05/07/17 17:07 1Pentachloronitrobenzene<7.4
7.4 1.7 ug/L 05/01/17 15:19 05/07/17 17:07 1Phenacetin<7.4
0.74 0.22 ug/L 05/01/17 15:19 05/07/17 17:07 1Phenanthrene<0.74
3.7 0.50 ug/L 05/01/17 15:19 05/07/17 17:07 1Phenol<3.7
7.4 1.6 ug/L 05/01/17 15:19 05/07/17 17:07 1Phorate<7.4
60 12 ug/L 05/01/17 15:19 05/07/17 17:07 1p-Phenylene diamine <60
7.4 1.6 ug/L 05/01/17 15:19 05/07/17 17:07 1Pronamide<7.4
0.74 0.32 ug/L 05/01/17 15:19 05/07/17 17:07 1Pyrene<0.74
7.4 3.0 ug/L 05/01/17 15:19 05/07/17 17:07 1Safrole<7.4
7.4 1.4 ug/L 05/01/17 15:19 05/07/17 17:07 1sym-Trinitrobenzene <7.4
7.4 7.4 ug/L 05/01/17 15:19 05/07/17 17:07 12,3,7,8-TCDD (Screen)<7.4
3.7 0.43 ug/L 05/01/17 15:19 05/07/17 17:07 11,2,4,5-Tetrachlorobenzene <3.7
3.7 0.56 ug/L 05/01/17 15:19 05/07/17 17:07 12,3,4,6-Tetrachlorophenol <3.7
7.4 1.9 ug/L 05/01/17 15:19 05/07/17 17:07 1Thionazin<7.4
3.7 0.53 ug/L 05/01/17 15:19 05/07/17 17:07 12,4,6-Trichlorophenol <3.7
7.4 1.9 ug/L 05/01/17 15:19 05/07/17 17:07 12,4,5-Trichlorophenol <7.4
2-Fluorophenol 69 27-110 05/01/17 15:19 05/07/17 17:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Phenol-d5 52 05/01/17 15:19 05/07/17 17:07 120-100
Nitrobenzene-d5 71 05/01/17 15:19 05/07/17 17:07 136-120
2-Fluorobiphenyl 77 05/01/17 15:19 05/07/17 17:07 134-110
2,4,6-Tribromophenol 120 05/01/17 15:19 05/07/17 17:07 140-145
Terphenyl-d14 88 05/01/17 15:19 05/07/17 17:07 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.037 0.037 0.0024 ug/L 05/01/17 10:27 05/05/17 01:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0095 ug/L 05/01/17 10:27 05/05/17 01:47 1beta-BHC <0.037
0.037 0.0096 ug/L 05/01/17 10:27 05/05/17 01:47 1delta-BHC <0.037
0.037 0.0052 ug/L 05/01/17 10:27 05/05/17 01:47 1gamma-BHC (Lindane)<0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 01:47 1Heptachlor<0.037
0.037 0.0049 ug/L 05/01/17 10:27 05/05/17 01:47 1Aldrin<0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 01:47 1Heptachlor epoxide <0.037
0.037 0.0038 ug/L 05/01/17 10:27 05/05/17 01:47 1Endosulfan I <0.037
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-5Client Sample ID: MW-57
Matrix: WaterDate Collected: 04/26/17 09:45
Date Received: 04/28/17 09:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.037 0.037 0.012 ug/L 05/01/17 10:27 05/05/17 01:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0035 ug/L 05/01/17 10:27 05/05/17 01:47 14,4'-DDE <0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 01:47 1Endrin<0.037
0.037 0.0026 ug/L 05/01/17 10:27 05/05/17 01:47 1Endosulfan II <0.037
0.037 0.012 ug/L 05/01/17 10:27 05/05/17 01:47 14,4'-DDD <0.037
0.037 0.011 ug/L 05/01/17 10:27 05/05/17 01:47 1Endosulfan sulfate <0.037
0.037 0.0030 ug/L 05/01/17 10:27 05/05/17 01:47 14,4'-DDT <0.037
0.075 0.021 ug/L 05/01/17 10:27 05/05/17 01:47 1Methoxychlor<0.075
0.37 0.19 ug/L 05/01/17 10:27 05/05/17 01:47 1Toxaphene<0.37
0.037 0.0076 ug/L 05/01/17 10:27 05/05/17 01:47 1Endrin aldehyde <0.037
0.075 0.037 ug/L 05/01/17 10:27 05/05/17 01:47 1Chlordane (technical)<0.075
DCB Decachlorobiphenyl 63 30-130 05/01/17 10:27 05/05/17 01:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 76 05/01/17 10:27 05/05/17 01:47 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.37 0.37 0.063 ug/L 05/01/17 10:27 05/02/17 13:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:52 1PCB-1221 <0.37
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:52 1PCB-1232 <0.37
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:52 1PCB-1242 <0.37
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:52 1PCB-1248 <0.37
0.37 0.19 ug/L 05/01/17 10:27 05/02/17 13:52 1PCB-1254 <0.37
0.37 0.065 ug/L 05/01/17 10:27 05/02/17 13:52 1PCB-1260 <0.37
Tetrachloro-m-xylene 82 30-120 05/01/17 10:27 05/02/17 13:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 82 05/01/17 10:27 05/02/17 13:52 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <1.1 1.1 0.53 ug/L 05/02/17 10:54 05/09/17 02:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.57 0.10 ug/L 05/02/17 10:54 05/09/17 02:17 1Pentachlorophenol<0.57
1.1 0.33 ug/L 05/02/17 10:54 05/09/17 02:17 1Silvex (2,4,5-TP)<1.1
1.1 0.49 ug/L 05/02/17 10:54 05/09/17 02:17 12,4,5-T <1.1
2.3 0.19 ug/L 05/02/17 10:54 05/09/17 02:17 1Dinoseb<2.3
DCAA 69 25-130 05/02/17 10:54 05/09/17 02:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 05/01/17 10:50 05/01/17 16:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 05/01/17 10:50 05/03/17 12:41 1Arsenic1.2
2.5 0.37 ug/L 05/01/17 10:50 05/01/17 16:28 1Barium450
1.0 0.43 ug/L 05/01/17 10:50 05/01/17 16:28 1Beryllium<1.0
0.50 0.15 ug/L 05/01/17 10:50 05/01/17 16:28 1Cadmium<0.50
5.0 2.3 ug/L 05/01/17 10:50 05/01/17 16:28 1Chromium<5.0
1.0 0.27 ug/L 05/01/17 10:50 05/01/17 16:28 1Cobalt17
2.0 0.63 ug/L 05/01/17 10:50 05/03/17 12:41 1Copper0.68 J
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-5Client Sample ID: MW-57
Matrix: WaterDate Collected: 04/26/17 09:45
Date Received: 04/28/17 09:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 47000 100 38 ug/L 05/01/17 10:50 05/01/17 16:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 05/01/17 10:50 05/01/17 16:28 1Lead0.40 J
25 11 ug/L 05/01/17 10:50 05/03/17 14:23 10Manganese10000
2.0 0.92 ug/L 05/01/17 10:50 05/01/17 16:28 1Nickel15
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:28 1Selenium<2.5
0.50 0.078 ug/L 05/01/17 10:50 05/01/17 16:28 1Silver<0.50
2.0 0.65 ug/L 05/01/17 10:50 05/01/17 16:28 1Thallium<2.0
10 4.2 ug/L 05/01/17 10:50 05/01/17 16:28 1Tin<10
5.0 2.0 ug/L 05/01/17 10:50 05/01/17 16:28 1Vanadium<5.0
20 8.1 ug/L 05/01/17 10:50 05/03/17 12:41 1Zinc17J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 05/03/17 12:50 05/04/17 08:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 05/08/17 14:00 05/08/17 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.0 3.4 mg/L 05/05/17 20:31 20Chloride73
4.0 1.9 mg/L 05/05/17 20:31 20Sulfate150
5.0 3.7 mg/L 05/05/17 15:32 1Alkalinity880
10 4.3 mg/L 05/02/17 04:45 1Total Dissolved Solids 1300
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-6Client Sample ID: MW-57D
Matrix: WaterDate Collected: 04/26/17 09:50
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.5 5.0 1.7 ug/L 05/08/17 01:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 4.2 ug/L 05/08/17 01:09 1Acetonitrile<10
100 23 ug/L 05/08/17 01:09 1Acrolein<100
20 4.5 ug/L 05/08/17 01:09 1Acrylonitrile<20
0.50 0.15 ug/L 05/08/17 01:09 1Benzene0.60
1.0 0.43 ug/L 05/08/17 01:09 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/08/17 01:09 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/08/17 01:09 1Bromoform<1.0
2.0 0.80 ug/L 05/08/17 01:09 1Bromomethane<2.0
5.0 2.1 ug/L 05/08/17 01:09 12-Butanone (MEK)<5.0
2.0 0.45 ug/L 05/08/17 01:09 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/08/17 01:09 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/08/17 01:09 1Chlorobenzene<1.0
1.0 0.23 ug/L 05/08/17 01:09 12-Chloro-1,3-butadiene <1.0
1.0 0.51 ug/L 05/08/17 01:09 1Chloroethane<1.0
2.0 0.37 ug/L 05/08/17 01:09 1Chloroform<2.0
1.0 0.32 ug/L 05/08/17 01:09 1Chloromethane<1.0
2.5 0.86 ug/L 05/08/17 01:09 13-Chloropropene <2.5
1.0 0.41 ug/L 05/08/17 01:09 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/08/17 01:09 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/08/17 01:09 1Dibromochloromethane<1.0
5.0 2.0 ug/L 05/08/17 01:09 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/08/17 01:09 11,2-Dibromoethane <1.0
1.0 0.27 ug/L 05/08/17 01:09 1Dibromomethane<1.0
1.0 0.40 ug/L 05/08/17 01:09 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 05/08/17 01:09 11,4-Dichlorobenzene <1.0
1.0 0.33 ug/L 05/08/17 01:09 11,2-Dichlorobenzene <1.0
2.0 0.67 ug/L 05/08/17 01:09 1Dichlorodifluoromethane<2.0
1.0 0.41 ug/L 05/08/17 01:09 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/08/17 01:09 11,2-Dichloroethane <1.0
1.0 0.39 ug/L 05/08/17 01:09 11,1-Dichloroethene <1.0
1.0 0.44 ug/L 05/08/17 01:09 12,2-Dichloropropane <1.0
1.0 0.43 ug/L 05/08/17 01:09 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/08/17 01:09 11,3-Dichloropropane <1.0
1.0 0.30 ug/L 05/08/17 01:09 11,1-Dichloropropene <1.0
0.50 0.18 ug/L 05/08/17 01:09 1Ethylbenzene<0.50
2.5 0.53 ug/L 05/08/17 01:09 1Ethyl methacrylate <2.5
1.0 0.45 ug/L 05/08/17 01:09 1Hexachlorobutadiene<1.0
5.0 1.6 ug/L 05/08/17 01:09 12-Hexanone <5.0
2.5 0.66 ug/L 05/08/17 01:09 1Iodomethane<2.5
100 36 ug/L 05/08/17 01:09 1Isobutyl alcohol <100
10 2.5 ug/L 05/08/17 01:09 1Methacrylonitrile<10
5.0 1.6 ug/L 05/08/17 01:09 1Methylene Chloride <5.0
2.5 0.55 ug/L 05/08/17 01:09 1Methyl methacrylate <2.5
5.0 2.2 ug/L 05/08/17 01:09 14-Methyl-2-pentanone (MIBK)<5.0
10 4.8 ug/L 05/08/17 01:09 1Propionitrile<10
1.0 0.39 ug/L 05/08/17 01:09 1Styrene<1.0
1.0 0.46 ug/L 05/08/17 01:09 11,1,1,2-Tetrachloroethane <1.0
1.0 0.40 ug/L 05/08/17 01:09 11,1,2,2-Tetrachloroethane <1.0
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-6Client Sample ID: MW-57D
Matrix: WaterDate Collected: 04/26/17 09:50
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Tetrachloroethene <1.0 1.0 0.37 ug/L 05/08/17 01:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 1.9 ug/L 05/08/17 01:09 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/08/17 01:09 1Toluene<0.50
5.0 1.2 ug/L 05/08/17 01:09 1trans-1,4-Dichloro-2-butene <5.0
1.0 0.35 ug/L 05/08/17 01:09 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/08/17 01:09 1trans-1,3-Dichloropropene <1.0
1.0 0.34 ug/L 05/08/17 01:09 11,2,4-Trichlorobenzene <1.0
1.0 0.38 ug/L 05/08/17 01:09 11,1,1-Trichloroethane <1.0
1.0 0.35 ug/L 05/08/17 01:09 11,1,2-Trichloroethane <1.0
0.50 0.16 ug/L 05/08/17 01:09 1Trichloroethene<0.50
1.0 0.43 ug/L 05/08/17 01:09 1Trichlorofluoromethane<1.0
1.0 0.41 ug/L 05/08/17 01:09 11,2,3-Trichloropropane <1.0
2.0 0.91 ug/L 05/08/17 01:09 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/08/17 01:09 1Vinyl chloride 1.1 cn
1.0 0.22 ug/L 05/08/17 01:09 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)106 75-126 05/08/17 01:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)100 05/08/17 01:09 175-120
4-Bromofluorobenzene (Surr)109 05/08/17 01:09 172-124
Dibromofluoromethane 90 05/08/17 01:09 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.75 0.75 0.23 ug/L 05/01/17 15:19 05/07/17 17:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.75 0.20 ug/L 05/01/17 15:19 05/07/17 17:31 1Acenaphthylene<0.75
3.8 0.50 ug/L 05/01/17 15:19 05/07/17 17:31 1Acetophenone<3.8
7.5 1.6 ug/L 05/01/17 15:19 05/07/17 17:31 12-Acetylaminofluorene <7.5
7.5 2.8 ug/L 05/01/17 15:19 05/07/17 17:31 14-Aminobiphenyl <7.5
0.75 0.25 ug/L 05/01/17 15:19 05/07/17 17:31 1Anthracene<0.75
0.15 0.043 ug/L 05/01/17 15:19 05/07/17 17:31 1Benzo[a]anthracene <0.15
0.15 0.075 ug/L 05/01/17 15:19 05/07/17 17:31 1Benzo[a]pyrene <0.15
0.15 0.061 ug/L 05/01/17 15:19 05/07/17 17:31 1Benzo[b]fluoranthene <0.15
0.75 0.28 ug/L 05/01/17 15:19 05/07/17 17:31 1Benzo[g,h,i]perylene <0.75
0.15 0.048 ug/L 05/01/17 15:19 05/07/17 17:31 1Benzo[k]fluoranthene <0.15
15 4.6 ug/L 05/01/17 15:19 05/07/17 17:31 1Benzyl alcohol <15
1.5 0.21 ug/L 05/01/17 15:19 05/07/17 17:31 1Bis(2-chloroethoxy)methane <1.5
1.5 0.22 ug/L 05/01/17 15:19 05/07/17 17:31 1Bis(2-chloroethyl)ether <1.5
7.5 1.3 ug/L 05/01/17 15:19 05/07/17 17:31 1Bis(2-ethylhexyl) phthalate <7.5
3.8 0.41 ug/L 05/01/17 15:19 05/07/17 17:31 14-Bromophenyl phenyl ether <3.8
1.5 0.36 ug/L 05/01/17 15:19 05/07/17 17:31 1Butyl benzyl phthalate <1.5
7.5 1.5 ug/L 05/01/17 15:19 05/07/17 17:31 14-Chloroaniline <7.5
7.5 2.6 ug/L 05/01/17 15:19 05/07/17 17:31 1Chlorobenzilate<7.5
7.5 1.7 ug/L 05/01/17 15:19 05/07/17 17:31 14-Chloro-3-methylphenol <7.5
1.5 0.18 ug/L 05/01/17 15:19 05/07/17 17:31 12-Chloronaphthalene <1.5
3.8 0.42 ug/L 05/01/17 15:19 05/07/17 17:31 12-Chlorophenol <3.8
3.8 0.48 ug/L 05/01/17 15:19 05/07/17 17:31 14-Chlorophenyl phenyl ether <3.8
0.15 0.051 ug/L 05/01/17 15:19 05/07/17 17:31 1Chrysene<0.15
7.5 4.2 ug/L 05/01/17 15:19 05/07/17 17:31 1Diallate<7.5
0.23 0.038 ug/L 05/01/17 15:19 05/07/17 17:31 1Dibenz(a,h)anthracene <0.23
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-6Client Sample ID: MW-57D
Matrix: WaterDate Collected: 04/26/17 09:50
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.5 1.5 0.20 ug/L 05/01/17 15:19 05/07/17 17:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.8 1.3 ug/L 05/01/17 15:19 05/07/17 17:31 13,3'-Dichlorobenzidine <3.8
7.5 2.0 ug/L 05/01/17 15:19 05/07/17 17:31 12,4-Dichlorophenol <7.5
7.5 2.6 ug/L 05/01/17 15:19 05/07/17 17:31 12,6-Dichlorophenol <7.5
1.5 0.27 ug/L 05/01/17 15:19 05/07/17 17:31 1Diethyl phthalate <1.5
7.5 1.4 ug/L 05/01/17 15:19 05/07/17 17:31 1Dimethoate<7.5
30 2.3 ug/L 05/01/17 15:19 05/07/17 17:31 17,12-Dimethylbenz(a)anthracene <30
30 13 ug/L 05/01/17 15:19 05/07/17 17:31 13,3'-Dimethylbenzidine <30
7.5 1.4 ug/L 05/01/17 15:19 05/07/17 17:31 12,4-Dimethylphenol <7.5
1.5 0.24 ug/L 05/01/17 15:19 05/07/17 17:31 1Dimethyl phthalate <1.5
3.8 0.55 ug/L 05/01/17 15:19 05/07/17 17:31 1Di-n-butyl phthalate <3.8
15 4.5 ug/L 05/01/17 15:19 05/07/17 17:31 14,6-Dinitro-2-methylphenol <15
15 6.5 ug/L 05/01/17 15:19 05/07/17 17:31 12,4-Dinitrophenol <15
0.75 0.056 ug/L 05/01/17 15:19 05/07/17 17:31 12,6-Dinitrotoluene <0.75
0.75 0.18 ug/L 05/01/17 15:19 05/07/17 17:31 12,4-Dinitrotoluene <0.75
7.5 0.79 ug/L 05/01/17 15:19 05/07/17 17:31 1Di-n-octyl phthalate <7.5
7.5 1.9 ug/L 05/01/17 15:19 05/07/17 17:31 1Diphenylamine<7.5
7.5 1.4 ug/L 05/01/17 15:19 05/07/17 17:31 1Disulfoton<7.5
15 2.9 ug/L 05/01/17 15:19 05/07/17 17:31 1Ethyl methanesulfonate <15
7.5 1.6 ug/L 05/01/17 15:19 05/07/17 17:31 1Ethyl Parathion <7.5
30 23 ug/L 05/01/17 15:19 05/07/17 17:31 1Famphur<30
0.75 0.34 ug/L 05/01/17 15:19 05/07/17 17:31 1Fluoranthene<0.75
0.75 0.18 ug/L 05/01/17 15:19 05/07/17 17:31 1Fluorene<0.75
0.38 0.060 ug/L 05/01/17 15:19 05/07/17 17:31 1Hexachlorobenzene<0.38
15 4.8 ug/L 05/01/17 15:19 05/07/17 17:31 1Hexachlorocyclopentadiene<15
3.8 0.45 ug/L 05/01/17 15:19 05/07/17 17:31 1Hexachloroethane<3.8
15 3.5 ug/L 05/01/17 15:19 05/07/17 17:31 1Hexachloropropene<15
0.15 0.056 ug/L 05/01/17 15:19 05/07/17 17:31 1Indeno[1,2,3-cd]pyrene <0.15
15 5.2 ug/L 05/01/17 15:19 05/07/17 17:31 1Isodrin<15
1.5 0.28 ug/L 05/01/17 15:19 05/07/17 17:31 1Isophorone<1.5
7.5 2.9 ug/L 05/01/17 15:19 05/07/17 17:31 1Isosafrole<7.5
7.5 1.2 ug/L 05/01/17 15:19 05/07/17 17:31 1Kepone<7.5
3.8 1.0 ug/L 05/01/17 15:19 05/07/17 17:31 1m-Dinitrobenzene <3.8
30 7.6 ug/L 05/01/17 15:19 05/07/17 17:31 1Methapyrilene<30
7.5 1.7 ug/L 05/01/17 15:19 05/07/17 17:31 13-Methylcholanthrene <7.5
30 4.5 ug/L 05/01/17 15:19 05/07/17 17:31 1Methyl methanesulfonate <30
1.5 0.049 ug/L 05/01/17 15:19 05/07/17 17:31 12-Methylnaphthalene <1.5
7.5 1.8 ug/L 05/01/17 15:19 05/07/17 17:31 1Methyl parathion <7.5
1.5 0.23 ug/L 05/01/17 15:19 05/07/17 17:31 12-Methylphenol <1.5
1.5 0.34 ug/L 05/01/17 15:19 05/07/17 17:31 13 & 4 Methylphenol <1.5
0.75 0.23 ug/L 05/01/17 15:19 05/07/17 17:31 1Naphthalene<0.75
30 29 ug/L 05/01/17 15:19 05/07/17 17:31 11,4-Naphthoquinone <30
15 4.5 ug/L 05/01/17 15:19 05/07/17 17:31 11-Naphthylamine <15
15 6.9 ug/L 05/01/17 15:19 05/07/17 17:31 12-Naphthylamine <15
3.8 0.97 ug/L 05/01/17 15:19 05/07/17 17:31 12-Nitroaniline <3.8
7.5 1.3 ug/L 05/01/17 15:19 05/07/17 17:31 13-Nitroaniline <7.5
7.5 1.3 ug/L 05/01/17 15:19 05/07/17 17:31 14-Nitroaniline <7.5
0.75 0.34 ug/L 05/01/17 15:19 05/07/17 17:31 1Nitrobenzene<0.75
7.5 2.3 ug/L 05/01/17 15:19 05/07/17 17:31 15-Nitro-o-toluidine <7.5
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-6Client Sample ID: MW-57D
Matrix: WaterDate Collected: 04/26/17 09:50
Date Received: 04/28/17 09:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.5 7.5 1.9 ug/L 05/01/17 15:19 05/07/17 17:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 5.6 ug/L 05/01/17 15:19 05/07/17 17:31 14-Nitrophenol <15
15 6.5 ug/L 05/01/17 15:19 05/07/17 17:31 1N-Nitrosodiethylamine <15
7.5 3.6 ug/L 05/01/17 15:19 05/07/17 17:31 1N-Nitrosodimethylamine <7.5
7.5 3.2 ug/L 05/01/17 15:19 05/07/17 17:31 1N-Nitrosodi-n-butylamine <7.5
0.38 0.12 ug/L 05/01/17 15:19 05/07/17 17:31 1N-Nitrosodi-n-propylamine <0.38
1.5 0.28 ug/L 05/01/17 15:19 05/07/17 17:31 1N-Nitrosodiphenylamine <1.5
15 5.6 ug/L 05/01/17 15:19 05/07/17 17:31 1N-Nitrosomethylethylamine <15
7.5 2.6 ug/L 05/01/17 15:19 05/07/17 17:31 1N-Nitrosopiperidine <7.5
7.5 2.5 ug/L 05/01/17 15:19 05/07/17 17:31 1N-Nitrosopyrrolidine <7.5
15 4.2 ug/L 05/01/17 15:19 05/07/17 17:31 1o,o',o''-Triethylphosphorothioate <15
30 6.0 ug/L 05/01/17 15:19 05/07/17 17:31 1o-Toluidine <30
1.5 0.29 ug/L 05/01/17 15:19 05/07/17 17:31 12,2'-oxybis[1-chloropropane]<1.5
7.5 2.3 ug/L 05/01/17 15:19 05/07/17 17:31 1p-Dimethylamino azobenzene <7.5
7.5 2.1 ug/L 05/01/17 15:19 05/07/17 17:31 1Pentachlorobenzene<7.5
7.5 2.7 ug/L 05/01/17 15:19 05/07/17 17:31 1Pentachloronitrobenzene<7.5
7.5 1.7 ug/L 05/01/17 15:19 05/07/17 17:31 1Phenacetin<7.5
0.75 0.23 ug/L 05/01/17 15:19 05/07/17 17:31 1Phenanthrene<0.75
3.8 0.51 ug/L 05/01/17 15:19 05/07/17 17:31 1Phenol<3.8
7.5 1.6 ug/L 05/01/17 15:19 05/07/17 17:31 1Phorate<7.5
60 12 ug/L 05/01/17 15:19 05/07/17 17:31 1p-Phenylene diamine <60
7.5 1.6 ug/L 05/01/17 15:19 05/07/17 17:31 1Pronamide<7.5
0.75 0.32 ug/L 05/01/17 15:19 05/07/17 17:31 1Pyrene<0.75
7.5 3.0 ug/L 05/01/17 15:19 05/07/17 17:31 1Safrole<7.5
7.5 1.4 ug/L 05/01/17 15:19 05/07/17 17:31 1sym-Trinitrobenzene <7.5
7.5 7.5 ug/L 05/01/17 15:19 05/07/17 17:31 12,3,7,8-TCDD (Screen)<7.5
3.8 0.43 ug/L 05/01/17 15:19 05/07/17 17:31 11,2,4,5-Tetrachlorobenzene <3.8
3.8 0.56 ug/L 05/01/17 15:19 05/07/17 17:31 12,3,4,6-Tetrachlorophenol <3.8
7.5 2.0 ug/L 05/01/17 15:19 05/07/17 17:31 1Thionazin<7.5
3.8 0.54 ug/L 05/01/17 15:19 05/07/17 17:31 12,4,6-Trichlorophenol <3.8
7.5 1.9 ug/L 05/01/17 15:19 05/07/17 17:31 12,4,5-Trichlorophenol <7.5
2-Fluorophenol 75 27-110 05/01/17 15:19 05/07/17 17:31 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Phenol-d5 55 05/01/17 15:19 05/07/17 17:31 120-100
Nitrobenzene-d5 75 05/01/17 15:19 05/07/17 17:31 136-120
2-Fluorobiphenyl 79 05/01/17 15:19 05/07/17 17:31 134-110
2,4,6-Tribromophenol 129 05/01/17 15:19 05/07/17 17:31 140-145
Terphenyl-d14 92 05/01/17 15:19 05/07/17 17:31 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.037 0.037 0.0024 ug/L 05/01/17 10:27 05/05/17 02:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0094 ug/L 05/01/17 10:27 05/05/17 02:06 1beta-BHC <0.037
0.037 0.0095 ug/L 05/01/17 10:27 05/05/17 02:06 1delta-BHC <0.037
0.037 0.0052 ug/L 05/01/17 10:27 05/05/17 02:06 1gamma-BHC (Lindane)<0.037
0.037 0.012 ug/L 05/01/17 10:27 05/05/17 02:06 1Heptachlor<0.037
0.037 0.0049 ug/L 05/01/17 10:27 05/05/17 02:06 1Aldrin<0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 02:06 1Heptachlor epoxide <0.037
0.037 0.0038 ug/L 05/01/17 10:27 05/05/17 02:06 1Endosulfan I <0.037
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-6Client Sample ID: MW-57D
Matrix: WaterDate Collected: 04/26/17 09:50
Date Received: 04/28/17 09:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.037 0.037 0.012 ug/L 05/01/17 10:27 05/05/17 02:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0035 ug/L 05/01/17 10:27 05/05/17 02:06 14,4'-DDE <0.037
0.037 0.013 ug/L 05/01/17 10:27 05/05/17 02:06 1Endrin<0.037
0.037 0.0026 ug/L 05/01/17 10:27 05/05/17 02:06 1Endosulfan II <0.037
0.037 0.012 ug/L 05/01/17 10:27 05/05/17 02:06 14,4'-DDD <0.037
0.037 0.011 ug/L 05/01/17 10:27 05/05/17 02:06 1Endosulfan sulfate <0.037
0.037 0.0029 ug/L 05/01/17 10:27 05/05/17 02:06 14,4'-DDT <0.037
0.074 0.021 ug/L 05/01/17 10:27 05/05/17 02:06 1Methoxychlor<0.074
0.37 0.18 ug/L 05/01/17 10:27 05/05/17 02:06 1Toxaphene<0.37
0.037 0.0076 ug/L 05/01/17 10:27 05/05/17 02:06 1Endrin aldehyde <0.037
0.074 0.037 ug/L 05/01/17 10:27 05/05/17 02:06 1Chlordane (technical)<0.074
DCB Decachlorobiphenyl 72 30-130 05/01/17 10:27 05/05/17 02:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 70 05/01/17 10:27 05/05/17 02:06 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.37 0.37 0.062 ug/L 05/01/17 10:27 05/02/17 14:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 14:07 1PCB-1221 <0.37
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 14:07 1PCB-1232 <0.37
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 14:07 1PCB-1242 <0.37
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 14:07 1PCB-1248 <0.37
0.37 0.18 ug/L 05/01/17 10:27 05/02/17 14:07 1PCB-1254 <0.37
0.37 0.064 ug/L 05/01/17 10:27 05/02/17 14:07 1PCB-1260 <0.37
Tetrachloro-m-xylene 84 30-120 05/01/17 10:27 05/02/17 14:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 95 05/01/17 10:27 05/02/17 14:07 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <1.2 1.2 0.55 ug/L 05/02/17 10:54 05/09/17 03:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.59 0.11 ug/L 05/02/17 10:54 05/09/17 03:55 1Pentachlorophenol<0.59
1.2 0.34 ug/L 05/02/17 10:54 05/09/17 03:55 1Silvex (2,4,5-TP)<1.2
1.2 0.51 ug/L 05/02/17 10:54 05/09/17 03:55 12,4,5-T <1.2
2.4 0.19 ug/L 05/02/17 10:54 05/09/17 03:55 1Dinoseb<2.4
DCAA 58 25-130 05/02/17 10:54 05/09/17 03:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 05/01/17 10:50 05/01/17 16:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 05/01/17 10:50 05/03/17 12:56 1Arsenic0.18 J
2.5 0.37 ug/L 05/01/17 10:50 05/01/17 16:43 1Barium93
1.0 0.43 ug/L 05/01/17 10:50 05/01/17 16:43 1Beryllium<1.0
0.50 0.15 ug/L 05/01/17 10:50 05/01/17 16:43 1Cadmium0.38 J
5.0 2.3 ug/L 05/01/17 10:50 05/01/17 16:43 1Chromium<5.0
1.0 0.27 ug/L 05/01/17 10:50 05/01/17 16:43 1Cobalt1.1
2.0 0.63 ug/L 05/01/17 10:50 05/03/17 12:56 1Copper16
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-6Client Sample ID: MW-57D
Matrix: WaterDate Collected: 04/26/17 09:50
Date Received: 04/28/17 09:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 300 100 38 ug/L 05/01/17 10:50 05/01/17 16:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 05/01/17 10:50 05/01/17 16:43 1Lead0.20 J
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:43 1Manganese220
2.0 0.92 ug/L 05/01/17 10:50 05/01/17 16:43 1Nickel100
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:43 1Selenium<2.5
0.50 0.078 ug/L 05/01/17 10:50 05/01/17 16:43 1Silver<0.50
2.0 0.65 ug/L 05/01/17 10:50 05/01/17 16:43 1Thallium<2.0
10 4.2 ug/L 05/01/17 10:50 05/01/17 16:43 1Tin<10
5.0 2.0 ug/L 05/01/17 10:50 05/01/17 16:43 1Vanadium21
20 8.1 ug/L 05/01/17 10:50 05/03/17 12:56 1Zinc8.4 J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 05/03/17 12:50 05/04/17 08:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 05/08/17 14:00 05/08/17 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 8.5 mg/L 05/05/17 20:44 50Chloride75
10 4.8 mg/L 05/05/17 20:44 50Sulfate330
5.0 3.7 mg/L 05/05/17 16:20 1Alkalinity920
10 4.3 mg/L 05/02/17 04:47 1Total Dissolved Solids 1500
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-7Client Sample ID: SW-1
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Benzene <0.50 0.50 0.15 ug/L 05/08/17 01:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.67 ug/L 05/08/17 01:35 1Dichlorodifluoromethane<2.0
1.0 0.32 ug/L 05/08/17 01:35 1Chloromethane<1.0
0.50 0.20 ug/L 05/08/17 01:35 1Vinyl chloride <0.50
2.0 0.80 ug/L 05/08/17 01:35 1Bromomethane<2.0
1.0 0.51 ug/L 05/08/17 01:35 1Chloroethane<1.0
1.0 0.43 ug/L 05/08/17 01:35 1Trichlorofluoromethane<1.0
100 23 ug/L 05/08/17 01:35 1Acrolein<100
1.0 0.39 ug/L 05/08/17 01:35 11,1-Dichloroethene <1.0
2.5 0.66 ug/L 05/08/17 01:35 1Iodomethane<2.5
2.0 0.45 ug/L 05/08/17 01:35 1Carbon disulfide <2.0
5.0 1.7 ug/L 05/08/17 01:35 1Acetone<5.0
10 4.2 ug/L 05/08/17 01:35 1Acetonitrile<10
5.0 1.6 ug/L 05/08/17 01:35 1Methylene Chloride <5.0
1.0 0.35 ug/L 05/08/17 01:35 1trans-1,2-Dichloroethene <1.0
20 4.5 ug/L 05/08/17 01:35 1Acrylonitrile<20
1.0 0.41 ug/L 05/08/17 01:35 11,1-Dichloroethane <1.0
2.0 0.91 ug/L 05/08/17 01:35 1Vinyl acetate <2.0
1.0 0.44 ug/L 05/08/17 01:35 12,2-Dichloropropane <1.0
1.0 0.41 ug/L 05/08/17 01:35 1cis-1,2-Dichloroethene <1.0
5.0 2.1 ug/L 05/08/17 01:35 12-Butanone (MEK)<5.0
10 4.8 ug/L 05/08/17 01:35 1Propionitrile<10
1.0 0.43 ug/L 05/08/17 01:35 1Bromochloromethane<1.0
10 1.9 ug/L 05/08/17 01:35 1Tetrahydrofuran<10
2.0 0.37 ug/L 05/08/17 01:35 1Chloroform<2.0
1.0 0.38 ug/L 05/08/17 01:35 11,1,1-Trichloroethane <1.0
1.0 0.30 ug/L 05/08/17 01:35 11,1-Dichloropropene <1.0
1.0 0.38 ug/L 05/08/17 01:35 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/08/17 01:35 11,2-Dichloroethane <1.0
0.50 0.16 ug/L 05/08/17 01:35 1Trichloroethene<0.50
1.0 0.43 ug/L 05/08/17 01:35 11,2-Dichloropropane <1.0
1.0 0.27 ug/L 05/08/17 01:35 1Dibromomethane<1.0
1.0 0.37 ug/L 05/08/17 01:35 1Bromodichloromethane<1.0
1.0 0.42 ug/L 05/08/17 01:35 1cis-1,3-Dichloropropene <1.0
5.0 2.2 ug/L 05/08/17 01:35 14-Methyl-2-pentanone (MIBK)<5.0
0.50 0.15 ug/L 05/08/17 01:35 1Toluene<0.50
1.0 0.36 ug/L 05/08/17 01:35 1trans-1,3-Dichloropropene <1.0
1.0 0.35 ug/L 05/08/17 01:35 11,1,2-Trichloroethane <1.0
1.0 0.37 ug/L 05/08/17 01:35 1Tetrachloroethene<1.0
1.0 0.36 ug/L 05/08/17 01:35 11,3-Dichloropropane <1.0
5.0 1.6 ug/L 05/08/17 01:35 12-Hexanone <5.0
1.0 0.49 ug/L 05/08/17 01:35 1Dibromochloromethane<1.0
1.0 0.39 ug/L 05/08/17 01:35 11,2-Dibromoethane <1.0
1.0 0.39 ug/L 05/08/17 01:35 1Chlorobenzene<1.0
1.0 0.46 ug/L 05/08/17 01:35 11,1,1,2-Tetrachloroethane <1.0
0.50 0.18 ug/L 05/08/17 01:35 1Ethylbenzene<0.50
1.0 0.39 ug/L 05/08/17 01:35 1Styrene<1.0
1.0 0.48 ug/L 05/08/17 01:35 1Bromoform<1.0
5.0 1.2 ug/L 05/08/17 01:35 1trans-1,4-Dichloro-2-butene <5.0
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-7Client Sample ID: SW-1
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane <1.0 1.0 0.40 ug/L 05/08/17 01:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.41 ug/L 05/08/17 01:35 11,2,3-Trichloropropane <1.0
1.0 0.22 ug/L 05/08/17 01:35 1Xylenes, Total <1.0
1.0 0.40 ug/L 05/08/17 01:35 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 05/08/17 01:35 11,4-Dichlorobenzene <1.0
1.0 0.33 ug/L 05/08/17 01:35 11,2-Dichlorobenzene <1.0
5.0 2.0 ug/L 05/08/17 01:35 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.34 ug/L 05/08/17 01:35 11,2,4-Trichlorobenzene <1.0
1.0 0.45 ug/L 05/08/17 01:35 1Hexachlorobutadiene<1.0
2.5 0.86 ug/L 05/08/17 01:35 13-Chloropropene <2.5
1.0 0.23 ug/L 05/08/17 01:35 12-Chloro-1,3-butadiene <1.0
10 2.5 ug/L 05/08/17 01:35 1Methacrylonitrile<10
100 36 ug/L 05/08/17 01:35 1Isobutyl alcohol <100
2.5 0.55 ug/L 05/08/17 01:35 1Methyl methacrylate <2.5
2.5 0.53 ug/L 05/08/17 01:35 1Ethyl methacrylate <2.5
1,2-Dichloroethane-d4 (Surr)103 75-126 05/08/17 01:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)102 05/08/17 01:35 175-120
4-Bromofluorobenzene (Surr)108 05/08/17 01:35 172-124
Dibromofluoromethane 89 05/08/17 01:35 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Silver <0.50 0.50 0.078 ug/L 05/01/17 10:50 05/01/17 16:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 05/01/17 10:50 05/03/17 13:00 1Arsenic0.46 J
2.5 0.37 ug/L 05/01/17 10:50 05/01/17 16:47 1Barium56
1.0 0.43 ug/L 05/01/17 10:50 05/01/17 16:47 1Beryllium<1.0
0.50 0.15 ug/L 05/01/17 10:50 05/01/17 16:47 1Cadmium<0.50
1.0 0.27 ug/L 05/01/17 10:50 05/01/17 16:47 1Cobalt2.4
5.0 2.3 ug/L 05/01/17 10:50 05/01/17 16:47 1Chromium<5.0
2.0 0.63 ug/L 05/01/17 10:50 05/03/17 13:00 1Copper4.0
100 38 ug/L 05/01/17 10:50 05/01/17 16:47 1Iron3000
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:47 1Manganese230
2.0 0.92 ug/L 05/01/17 10:50 05/01/17 16:47 1Nickel1.5 J
0.50 0.16 ug/L 05/01/17 10:50 05/01/17 16:47 1Lead1.2
3.0 1.3 ug/L 05/01/17 10:50 05/01/17 16:47 1Antimony<3.0
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:47 1Selenium<2.5
10 4.2 ug/L 05/01/17 10:50 05/01/17 16:47 1Tin<10
2.0 0.65 ug/L 05/01/17 10:50 05/01/17 16:47 1Thallium<2.0
5.0 2.0 ug/L 05/01/17 10:50 05/01/17 16:47 1Vanadium9.9
20 8.1 ug/L 05/01/17 10:50 05/03/17 13:00 1Zinc9.8 J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 05/03/17 12:50 05/04/17 08:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-8Client Sample ID: SW-2
Matrix: WaterDate Collected: 04/26/17 13:10
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Benzene <0.50 0.50 0.15 ug/L 05/08/17 02:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.67 ug/L 05/08/17 02:01 1Dichlorodifluoromethane<2.0
1.0 0.32 ug/L 05/08/17 02:01 1Chloromethane<1.0
0.50 0.20 ug/L 05/08/17 02:01 1Vinyl chloride <0.50
2.0 0.80 ug/L 05/08/17 02:01 1Bromomethane<2.0
1.0 0.51 ug/L 05/08/17 02:01 1Chloroethane<1.0
1.0 0.43 ug/L 05/08/17 02:01 1Trichlorofluoromethane<1.0
100 23 ug/L 05/08/17 02:01 1Acrolein<100
1.0 0.39 ug/L 05/08/17 02:01 11,1-Dichloroethene <1.0
2.5 0.66 ug/L 05/08/17 02:01 1Iodomethane<2.5
2.0 0.45 ug/L 05/08/17 02:01 1Carbon disulfide <2.0
5.0 1.7 ug/L 05/08/17 02:01 1Acetone<5.0
10 4.2 ug/L 05/08/17 02:01 1Acetonitrile<10
5.0 1.6 ug/L 05/08/17 02:01 1Methylene Chloride <5.0
1.0 0.35 ug/L 05/08/17 02:01 1trans-1,2-Dichloroethene <1.0
20 4.5 ug/L 05/08/17 02:01 1Acrylonitrile<20
1.0 0.41 ug/L 05/08/17 02:01 11,1-Dichloroethane <1.0
2.0 0.91 ug/L 05/08/17 02:01 1Vinyl acetate <2.0
1.0 0.44 ug/L 05/08/17 02:01 12,2-Dichloropropane <1.0
1.0 0.41 ug/L 05/08/17 02:01 1cis-1,2-Dichloroethene <1.0
5.0 2.1 ug/L 05/08/17 02:01 12-Butanone (MEK)<5.0
10 4.8 ug/L 05/08/17 02:01 1Propionitrile<10
1.0 0.43 ug/L 05/08/17 02:01 1Bromochloromethane<1.0
10 1.9 ug/L 05/08/17 02:01 1Tetrahydrofuran<10
2.0 0.37 ug/L 05/08/17 02:01 1Chloroform<2.0
1.0 0.38 ug/L 05/08/17 02:01 11,1,1-Trichloroethane <1.0
1.0 0.30 ug/L 05/08/17 02:01 11,1-Dichloropropene <1.0
1.0 0.38 ug/L 05/08/17 02:01 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/08/17 02:01 11,2-Dichloroethane <1.0
0.50 0.16 ug/L 05/08/17 02:01 1Trichloroethene<0.50
1.0 0.43 ug/L 05/08/17 02:01 11,2-Dichloropropane <1.0
1.0 0.27 ug/L 05/08/17 02:01 1Dibromomethane<1.0
1.0 0.37 ug/L 05/08/17 02:01 1Bromodichloromethane<1.0
1.0 0.42 ug/L 05/08/17 02:01 1cis-1,3-Dichloropropene <1.0
5.0 2.2 ug/L 05/08/17 02:01 14-Methyl-2-pentanone (MIBK)<5.0
0.50 0.15 ug/L 05/08/17 02:01 1Toluene<0.50
1.0 0.36 ug/L 05/08/17 02:01 1trans-1,3-Dichloropropene <1.0
1.0 0.35 ug/L 05/08/17 02:01 11,1,2-Trichloroethane <1.0
1.0 0.37 ug/L 05/08/17 02:01 1Tetrachloroethene<1.0
1.0 0.36 ug/L 05/08/17 02:01 11,3-Dichloropropane <1.0
5.0 1.6 ug/L 05/08/17 02:01 12-Hexanone <5.0
1.0 0.49 ug/L 05/08/17 02:01 1Dibromochloromethane<1.0
1.0 0.39 ug/L 05/08/17 02:01 11,2-Dibromoethane <1.0
1.0 0.39 ug/L 05/08/17 02:01 1Chlorobenzene<1.0
1.0 0.46 ug/L 05/08/17 02:01 11,1,1,2-Tetrachloroethane <1.0
0.50 0.18 ug/L 05/08/17 02:01 1Ethylbenzene<0.50
1.0 0.39 ug/L 05/08/17 02:01 1Styrene<1.0
1.0 0.48 ug/L 05/08/17 02:01 1Bromoform<1.0
5.0 1.2 ug/L 05/08/17 02:01 1trans-1,4-Dichloro-2-butene <5.0
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-8Client Sample ID: SW-2
Matrix: WaterDate Collected: 04/26/17 13:10
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane <1.0 1.0 0.40 ug/L 05/08/17 02:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.41 ug/L 05/08/17 02:01 11,2,3-Trichloropropane <1.0
1.0 0.22 ug/L 05/08/17 02:01 1Xylenes, Total <1.0
1.0 0.40 ug/L 05/08/17 02:01 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 05/08/17 02:01 11,4-Dichlorobenzene <1.0
1.0 0.33 ug/L 05/08/17 02:01 11,2-Dichlorobenzene <1.0
5.0 2.0 ug/L 05/08/17 02:01 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.34 ug/L 05/08/17 02:01 11,2,4-Trichlorobenzene <1.0
1.0 0.45 ug/L 05/08/17 02:01 1Hexachlorobutadiene<1.0
2.5 0.86 ug/L 05/08/17 02:01 13-Chloropropene <2.5
1.0 0.23 ug/L 05/08/17 02:01 12-Chloro-1,3-butadiene <1.0
10 2.5 ug/L 05/08/17 02:01 1Methacrylonitrile<10
100 36 ug/L 05/08/17 02:01 1Isobutyl alcohol <100
2.5 0.55 ug/L 05/08/17 02:01 1Methyl methacrylate <2.5
2.5 0.53 ug/L 05/08/17 02:01 1Ethyl methacrylate <2.5
1,2-Dichloroethane-d4 (Surr)105 75-126 05/08/17 02:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)101 05/08/17 02:01 175-120
4-Bromofluorobenzene (Surr)113 05/08/17 02:01 172-124
Dibromofluoromethane 91 05/08/17 02:01 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Silver <0.50 0.50 0.078 ug/L 05/01/17 10:50 05/01/17 16:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 05/01/17 10:50 05/03/17 13:04 1Arsenic0.47 J
2.5 0.37 ug/L 05/01/17 10:50 05/01/17 16:51 1Barium61
1.0 0.43 ug/L 05/01/17 10:50 05/01/17 16:51 1Beryllium<1.0
0.50 0.15 ug/L 05/01/17 10:50 05/01/17 16:51 1Cadmium<0.50
1.0 0.27 ug/L 05/01/17 10:50 05/01/17 16:51 1Cobalt2.7
5.0 2.3 ug/L 05/01/17 10:50 05/01/17 16:51 1Chromium<5.0
2.0 0.63 ug/L 05/01/17 10:50 05/03/17 13:04 1Copper4.0
100 38 ug/L 05/01/17 10:50 05/01/17 16:51 1Iron3100
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:51 1Manganese260
2.0 0.92 ug/L 05/01/17 10:50 05/01/17 16:51 1Nickel1.6 J
0.50 0.16 ug/L 05/01/17 10:50 05/01/17 16:51 1Lead1.3
3.0 1.3 ug/L 05/01/17 10:50 05/01/17 16:51 1Antimony<3.0
2.5 1.1 ug/L 05/01/17 10:50 05/01/17 16:51 1Selenium<2.5
10 4.2 ug/L 05/01/17 10:50 05/01/17 16:51 1Tin<10
2.0 0.65 ug/L 05/01/17 10:50 05/01/17 16:51 1Thallium<2.0
5.0 2.0 ug/L 05/01/17 10:50 05/01/17 16:51 1Vanadium9.8
20 8.1 ug/L 05/01/17 10:50 05/03/17 13:04 1Zinc15J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 05/03/17 12:50 05/04/17 08:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-9Client Sample ID: Duplicate
Matrix: WaterDate Collected: 04/26/17 00:00
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Benzene 0.68 0.50 0.15 ug/L 05/08/17 02:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.67 ug/L 05/08/17 02:27 1Dichlorodifluoromethane<2.0
1.0 0.32 ug/L 05/08/17 02:27 1Chloromethane<1.0
0.50 0.20 ug/L 05/08/17 02:27 1Vinyl chloride 3.3 cn
2.0 0.80 ug/L 05/08/17 02:27 1Bromomethane<2.0
1.0 0.51 ug/L 05/08/17 02:27 1Chloroethane<1.0
1.0 0.43 ug/L 05/08/17 02:27 1Trichlorofluoromethane<1.0
100 23 ug/L 05/08/17 02:27 1Acrolein<100
1.0 0.39 ug/L 05/08/17 02:27 11,1-Dichloroethene <1.0
2.5 0.66 ug/L 05/08/17 02:27 1Iodomethane<2.5
2.0 0.45 ug/L 05/08/17 02:27 1Carbon disulfide <2.0
5.0 1.7 ug/L 05/08/17 02:27 1Acetone<5.0
10 4.2 ug/L 05/08/17 02:27 1Acetonitrile<10
5.0 1.6 ug/L 05/08/17 02:27 1Methylene Chloride <5.0
1.0 0.35 ug/L 05/08/17 02:27 1trans-1,2-Dichloroethene <1.0
20 4.5 ug/L 05/08/17 02:27 1Acrylonitrile<20
1.0 0.41 ug/L 05/08/17 02:27 11,1-Dichloroethane <1.0
2.0 0.91 ug/L 05/08/17 02:27 1Vinyl acetate <2.0
1.0 0.44 ug/L 05/08/17 02:27 12,2-Dichloropropane <1.0
1.0 0.41 ug/L 05/08/17 02:27 1cis-1,2-Dichloroethene <1.0
5.0 2.1 ug/L 05/08/17 02:27 12-Butanone (MEK)<5.0
10 4.8 ug/L 05/08/17 02:27 1Propionitrile<10
1.0 0.43 ug/L 05/08/17 02:27 1Bromochloromethane<1.0
10 1.9 ug/L 05/08/17 02:27 1Tetrahydrofuran<10
2.0 0.37 ug/L 05/08/17 02:27 1Chloroform<2.0
1.0 0.38 ug/L 05/08/17 02:27 11,1,1-Trichloroethane <1.0
1.0 0.30 ug/L 05/08/17 02:27 11,1-Dichloropropene <1.0
1.0 0.38 ug/L 05/08/17 02:27 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/08/17 02:27 11,2-Dichloroethane <1.0
0.50 0.16 ug/L 05/08/17 02:27 1Trichloroethene<0.50
1.0 0.43 ug/L 05/08/17 02:27 11,2-Dichloropropane <1.0
1.0 0.27 ug/L 05/08/17 02:27 1Dibromomethane<1.0
1.0 0.37 ug/L 05/08/17 02:27 1Bromodichloromethane<1.0
1.0 0.42 ug/L 05/08/17 02:27 1cis-1,3-Dichloropropene <1.0
5.0 2.2 ug/L 05/08/17 02:27 14-Methyl-2-pentanone (MIBK)<5.0
0.50 0.15 ug/L 05/08/17 02:27 1Toluene<0.50
1.0 0.36 ug/L 05/08/17 02:27 1trans-1,3-Dichloropropene <1.0
1.0 0.35 ug/L 05/08/17 02:27 11,1,2-Trichloroethane <1.0
1.0 0.37 ug/L 05/08/17 02:27 1Tetrachloroethene<1.0
1.0 0.36 ug/L 05/08/17 02:27 11,3-Dichloropropane <1.0
5.0 1.6 ug/L 05/08/17 02:27 12-Hexanone <5.0
1.0 0.49 ug/L 05/08/17 02:27 1Dibromochloromethane<1.0
1.0 0.39 ug/L 05/08/17 02:27 11,2-Dibromoethane <1.0
1.0 0.39 ug/L 05/08/17 02:27 1Chlorobenzene<1.0
1.0 0.46 ug/L 05/08/17 02:27 11,1,1,2-Tetrachloroethane <1.0
0.50 0.18 ug/L 05/08/17 02:27 1Ethylbenzene<0.50
1.0 0.39 ug/L 05/08/17 02:27 1Styrene<1.0
1.0 0.48 ug/L 05/08/17 02:27 1Bromoform<1.0
5.0 1.2 ug/L 05/08/17 02:27 1trans-1,4-Dichloro-2-butene <5.0
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Client Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Lab Sample ID: 500-127325-9Client Sample ID: Duplicate
Matrix: WaterDate Collected: 04/26/17 00:00
Date Received: 04/28/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane <1.0 1.0 0.40 ug/L 05/08/17 02:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.41 ug/L 05/08/17 02:27 11,2,3-Trichloropropane <1.0
1.0 0.22 ug/L 05/08/17 02:27 1Xylenes, Total <1.0
1.0 0.40 ug/L 05/08/17 02:27 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 05/08/17 02:27 11,4-Dichlorobenzene <1.0
1.0 0.33 ug/L 05/08/17 02:27 11,2-Dichlorobenzene <1.0
5.0 2.0 ug/L 05/08/17 02:27 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.34 ug/L 05/08/17 02:27 11,2,4-Trichlorobenzene <1.0
1.0 0.45 ug/L 05/08/17 02:27 1Hexachlorobutadiene<1.0
2.5 0.86 ug/L 05/08/17 02:27 13-Chloropropene <2.5
1.0 0.23 ug/L 05/08/17 02:27 12-Chloro-1,3-butadiene <1.0
10 2.5 ug/L 05/08/17 02:27 1Methacrylonitrile<10
100 36 ug/L 05/08/17 02:27 1Isobutyl alcohol <100
2.5 0.55 ug/L 05/08/17 02:27 1Methyl methacrylate <2.5
2.5 0.53 ug/L 05/08/17 02:27 1Ethyl methacrylate <2.5
1,2-Dichloroethane-d4 (Surr)105 75-126 05/08/17 02:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)101 05/08/17 02:27 175-120
4-Bromofluorobenzene (Surr)108 05/08/17 02:27 172-124
Dibromofluoromethane 91 05/08/17 02:27 175-120
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Definitions/Glossary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Qualifiers
GC/MS VOA
Qualifier Description
cn Refer to Case Narrative for further detail
Qualifier
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
F3 Duplicate RPD exceeds the control limit
F5 Duplicate RPD exceeds limit, and one or both sample results are less than 5 times RL. The data are considered valid because the
absolute difference is less than the RL.
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
GC/MS VOA
Analysis Batch: 384124
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-127325-1 MW-55 Total/NA
Water 8260B500-127325-2 MW-56 Total/NA
Water 8260B500-127325-3 MW-56A Total/NA
Water 8260B500-127325-4 MW-56D Total/NA
Water 8260B500-127325-5 MW-57 Total/NA
Water 8260B500-127325-6 MW-57D Total/NA
Water 8260B500-127325-7 SW-1 Total/NA
Water 8260B500-127325-8 SW-2 Total/NA
Water 8260B500-127325-9 Duplicate Total/NA
Water 8260BMB 500-384124/6 Method Blank Total/NA
Water 8260BLCS 500-384124/4 Lab Control Sample Total/NA
GC/MS Semi VOA
Prep Batch: 383173
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C500-127325-1 MW-55 Total/NA
Water 3510C500-127325-2 MW-56 Total/NA
Water 3510C500-127325-3 MW-56A Total/NA
Water 3510C500-127325-4 MW-56D Total/NA
Water 3510C500-127325-5 MW-57 Total/NA
Water 3510C500-127325-6 MW-57D Total/NA
Water 3510CMB 500-383173/1-A Method Blank Total/NA
Water 3510CLCS 500-383173/2-A Lab Control Sample Total/NA
Water 3510CLCSD 500-383173/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 383899
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 383173500-127325-1 MW-55 Total/NA
Water 8270D 383173500-127325-2 MW-56 Total/NA
Water 8270D 383173500-127325-3 MW-56A Total/NA
Water 8270D 383173MB 500-383173/1-A Method Blank Total/NA
Water 8270D 383173LCS 500-383173/2-A Lab Control Sample Total/NA
Water 8270D 383173LCSD 500-383173/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 384111
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 383173500-127325-4 MW-56D Total/NA
Water 8270D 383173500-127325-5 MW-57 Total/NA
Water 8270D 383173500-127325-6 MW-57D Total/NA
GC Semi VOA
Prep Batch: 383107
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C500-127325-1 MW-55 Total/NA
Water 3510C500-127325-2 MW-56 Total/NA
Water 3510C500-127325-3 MW-56A Total/NA
Water 3510C500-127325-4 MW-56D Total/NA
Water 3510C500-127325-5 MW-57 Total/NA
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QC Association Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
GC Semi VOA (Continued)
Prep Batch: 383107 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C500-127325-6 MW-57D Total/NA
Water 3510CMB 500-383107/1-A Method Blank Total/NA
Water 3510CLCS 500-383107/2-A Lab Control Sample Total/NA
Water 3510CLCS 500-383107/4-A Lab Control Sample Total/NA
Water 3510CLCSD 500-383107/3-A Lab Control Sample Dup Total/NA
Water 3510CLCSD 500-383107/5-A Lab Control Sample Dup Total/NA
Prep Batch: 383303
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8151A500-127325-1 MW-55 Total/NA
Water 8151A500-127325-2 MW-56 Total/NA
Water 8151A500-127325-3 MW-56A Total/NA
Water 8151A500-127325-4 MW-56D Total/NA
Water 8151A500-127325-5 MW-57 Total/NA
Water 8151A500-127325-6 MW-57D Total/NA
Water 8151AMB 500-383303/1-A Method Blank Total/NA
Water 8151ALCS 500-383303/2-A Lab Control Sample Total/NA
Water 8151ALCSD 500-383303/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 383316
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8082A 383107500-127325-1 MW-55 Total/NA
Water 8082A 383107500-127325-2 MW-56 Total/NA
Water 8082A 383107500-127325-3 MW-56A Total/NA
Water 8082A 383107500-127325-4 MW-56D Total/NA
Water 8082A 383107500-127325-5 MW-57 Total/NA
Water 8082A 383107500-127325-6 MW-57D Total/NA
Water 8082A 383107MB 500-383107/1-A Method Blank Total/NA
Water 8082A 383107LCS 500-383107/4-A Lab Control Sample Total/NA
Water 8082A 383107LCSD 500-383107/5-A Lab Control Sample Dup Total/NA
Analysis Batch: 383721
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B 383107500-127325-1 MW-55 Total/NA
Water 8081B 383107500-127325-2 MW-56 Total/NA
Water 8081B 383107500-127325-3 MW-56A Total/NA
Water 8081B 383107500-127325-4 MW-56D Total/NA
Water 8081B 383107500-127325-5 MW-57 Total/NA
Water 8081B 383107500-127325-6 MW-57D Total/NA
Water 8081B 383107MB 500-383107/1-A Method Blank Total/NA
Water 8081B 383107LCS 500-383107/2-A Lab Control Sample Total/NA
Water 8081B 383107LCSD 500-383107/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 384274
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8151A 383303500-127325-1 MW-55 Total/NA
Water 8151A 383303500-127325-2 MW-56 Total/NA
Water 8151A 383303500-127325-3 MW-56A Total/NA
Water 8151A 383303500-127325-4 MW-56D Total/NA
Water 8151A 383303500-127325-5 MW-57 Total/NA
Water 8151A 383303500-127325-6 MW-57D Total/NA
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QC Association Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
GC Semi VOA (Continued)
Analysis Batch: 384274 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8151A 383303MB 500-383303/1-A Method Blank Total/NA
Water 8151A 383303LCS 500-383303/2-A Lab Control Sample Total/NA
Water 8151A 383303LCSD 500-383303/3-A Lab Control Sample Dup Total/NA
Metals
Prep Batch: 383120
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-127325-1 MW-55 Total/NA
Water 200.8500-127325-2 MW-56 Total/NA
Water 200.8500-127325-3 MW-56A Total/NA
Water 200.8500-127325-4 MW-56D Total/NA
Water 200.8500-127325-5 MW-57 Total/NA
Water 200.8500-127325-6 MW-57D Total/NA
Water 200.8500-127325-7 SW-1 Total/NA
Water 200.8500-127325-8 SW-2 Total/NA
Water 200.8MB 500-383120/1-A Method Blank Total/NA
Water 200.8LCS 500-383120/2-A Lab Control Sample Total/NA
Water 200.8500-127325-1 MS MW-55 Total/NA
Water 200.8500-127325-5 MS MW-57 Total/NA
Water 200.8500-127325-1 DU MW-55 Total/NA
Water 200.8500-127325-5 DU MW-57 Total/NA
Analysis Batch: 383287
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 383120500-127325-1 MW-55 Total/NA
Water 200.8 383120500-127325-2 MW-56 Total/NA
Water 200.8 383120500-127325-3 MW-56A Total/NA
Water 200.8 383120500-127325-4 MW-56D Total/NA
Water 200.8 383120500-127325-5 MW-57 Total/NA
Water 200.8 383120500-127325-6 MW-57D Total/NA
Water 200.8 383120500-127325-7 SW-1 Total/NA
Water 200.8 383120500-127325-8 SW-2 Total/NA
Water 200.8 383120MB 500-383120/1-A Method Blank Total/NA
Water 200.8 383120LCS 500-383120/2-A Lab Control Sample Total/NA
Water 200.8 383120500-127325-1 MS MW-55 Total/NA
Water 200.8 383120500-127325-5 MS MW-57 Total/NA
Water 200.8 383120500-127325-1 DU MW-55 Total/NA
Water 200.8 383120500-127325-5 DU MW-57 Total/NA
Prep Batch: 383544
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1500-127325-1 MW-55 Total/NA
Water 245.1500-127325-2 MW-56 Total/NA
Water 245.1500-127325-3 MW-56A Total/NA
Water 245.1500-127325-4 MW-56D Total/NA
Water 245.1500-127325-5 MW-57 Total/NA
Water 245.1500-127325-6 MW-57D Total/NA
Water 245.1500-127325-7 SW-1 Total/NA
Water 245.1500-127325-8 SW-2 Total/NA
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QC Association Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Metals (Continued)
Prep Batch: 383544 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1MB 500-383544/12-A Method Blank Total/NA
Water 245.1LCS 500-383544/13-A Lab Control Sample Total/NA
Water 245.1500-127325-1 MS MW-55 Total/NA
Water 245.1500-127325-1 DU MW-55 Total/NA
Analysis Batch: 383705
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 383120500-127325-1 MW-55 Total/NA
Water 200.8 383120500-127325-2 MW-56 Total/NA
Water 200.8 383120500-127325-2 MW-56 Total/NA
Water 200.8 383120500-127325-3 MW-56A Total/NA
Water 200.8 383120500-127325-4 MW-56D Total/NA
Water 200.8 383120500-127325-5 MW-57 Total/NA
Water 200.8 383120500-127325-5 MW-57 Total/NA
Water 200.8 383120500-127325-6 MW-57D Total/NA
Water 200.8 383120500-127325-7 SW-1 Total/NA
Water 200.8 383120500-127325-8 SW-2 Total/NA
Water 200.8 383120MB 500-383120/1-A Method Blank Total/NA
Water 200.8 383120LCS 500-383120/2-A Lab Control Sample Total/NA
Water 200.8 383120500-127325-1 MS MW-55 Total/NA
Water 200.8 383120500-127325-5 MS MW-57 Total/NA
Water 200.8 383120500-127325-5 MS MW-57 Total/NA
Water 200.8 383120500-127325-1 DU MW-55 Total/NA
Water 200.8 383120500-127325-5 DU MW-57 Total/NA
Water 200.8 383120500-127325-5 DU MW-57 Total/NA
Analysis Batch: 383786
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1 383544500-127325-1 MW-55 Total/NA
Water 245.1 383544500-127325-2 MW-56 Total/NA
Water 245.1 383544500-127325-3 MW-56A Total/NA
Water 245.1 383544500-127325-4 MW-56D Total/NA
Water 245.1 383544500-127325-5 MW-57 Total/NA
Water 245.1 383544500-127325-6 MW-57D Total/NA
Water 245.1 383544500-127325-7 SW-1 Total/NA
Water 245.1 383544500-127325-8 SW-2 Total/NA
Water 245.1 383544MB 500-383544/12-A Method Blank Total/NA
Water 245.1 383544LCS 500-383544/13-A Lab Control Sample Total/NA
Water 245.1 383544500-127325-1 MS MW-55 Total/NA
Water 245.1 383544500-127325-1 DU MW-55 Total/NA
General Chemistry
Analysis Batch: 383234
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C500-127325-1 MW-55 Total/NA
Water SM 2540C500-127325-2 MW-56 Total/NA
Water SM 2540C500-127325-3 MW-56A Total/NA
Water SM 2540C500-127325-4 MW-56D Total/NA
Water SM 2540C500-127325-5 MW-57 Total/NA
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QC Association Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
General Chemistry (Continued)
Analysis Batch: 383234 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C500-127325-6 MW-57D Total/NA
Water SM 2540CMB 500-383234/1 Method Blank Total/NA
Water SM 2540CLCS 500-383234/2 Lab Control Sample Total/NA
Water SM 2540C500-127325-1 MS MW-55 Total/NA
Water SM 2540C500-127325-1 DU MW-55 Total/NA
Analysis Batch: 384190
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-127325-1 MW-55 Total/NA
Water 9056A500-127325-2 MW-56 Total/NA
Water 9056A500-127325-3 MW-56A Total/NA
Water 9056A500-127325-4 MW-56D Total/NA
Water 9056A500-127325-5 MW-57 Total/NA
Water 9056A500-127325-6 MW-57D Total/NA
Water 9056AMB 500-384190/36 Method Blank Total/NA
Water 9056ALCS 500-384190/37 Lab Control Sample Total/NA
Prep Batch: 384259
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9010B500-127325-1 MW-55 Total/NA
Water 9010B500-127325-2 MW-56 Total/NA
Water 9010B500-127325-3 MW-56A Total/NA
Water 9010B500-127325-4 MW-56D Total/NA
Water 9010B500-127325-5 MW-57 Total/NA
Water 9010B500-127325-6 MW-57D Total/NA
Water 9010BMB 500-384259/1-A Method Blank Total/NA
Water 9010BLCS 500-384259/2-A Lab Control Sample Total/NA
Water 9010B500-127325-1 MS MW-55 Total/NA
Water 9010B500-127325-1 MSD MW-55 Total/NA
Analysis Batch: 384336
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-127325-1 MW-55 Total/NA
Water 9056AMB 500-384336/4 Method Blank Total/NA
Water 9056ALCS 500-384336/5 Lab Control Sample Total/NA
Analysis Batch: 384364
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B500-127325-1 MW-55 Total/NA
Water SM 2320B500-127325-2 MW-56 Total/NA
Water SM 2320B500-127325-3 MW-56A Total/NA
Water SM 2320B500-127325-4 MW-56D Total/NA
Water SM 2320B500-127325-5 MW-57 Total/NA
Water SM 2320B500-127325-6 MW-57D Total/NA
Water SM 2320BMB 500-384364/3 Method Blank Total/NA
Water SM 2320BLCS 500-384364/5 Lab Control Sample Total/NA
Water SM 2320B500-127325-4 DU MW-56D Total/NA
Analysis Batch: 384368
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9014 384259500-127325-1 MW-55 Total/NA
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QC Association Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
General Chemistry (Continued)
Analysis Batch: 384368 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9014 384259500-127325-2 MW-56 Total/NA
Water 9014 384259500-127325-3 MW-56A Total/NA
Water 9014 384259500-127325-4 MW-56D Total/NA
Water 9014 384259500-127325-5 MW-57 Total/NA
Water 9014 384259500-127325-6 MW-57D Total/NA
Water 9014 384259MB 500-384259/1-A Method Blank Total/NA
Water 9014 384259LCS 500-384259/2-A Lab Control Sample Total/NA
Water 9014 384259500-127325-1 MS MW-55 Total/NA
Water 9014 384259500-127325-1 MSD MW-55 Total/NA
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Surrogate Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (75-126)(75-120)(72-124)(75-120)
12DCE TOL BFB DBFM
104 103 110 90500-127325-1
Percent Surrogate Recovery (Acceptance Limits)
MW-55
101 100 112 90500-127325-2 MW-56
103 103 114 89500-127325-3 MW-56A
104 101 109 91500-127325-4 MW-56D
104 100 108 89500-127325-5 MW-57
106 100 109 90500-127325-6 MW-57D
103 102 108 89500-127325-7 SW-1
105 101 113 91500-127325-8 SW-2
105 101 108 91500-127325-9 Duplicate
105 101 108 96LCS 500-384124/4 Lab Control Sample
105 101 109 91MB 500-384124/6 Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
TOL = Toluene-d8 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (27-110)(20-100)(36-120)(34-110)(40-145)(40-145)
2FP PHL NBZ FBP TBP TPH
57 43 58 58 85 83500-127325-1
Percent Surrogate Recovery (Acceptance Limits)
MW-55
71 51 77 11376 99500-127325-2 MW-56
87 58 86 10682 103500-127325-3 MW-56A
70 51 74 10771 96500-127325-4 MW-56D
69 52 71 12077 88500-127325-5 MW-57
75 55 75 12979 92500-127325-6 MW-57D
92 69 98 12790 111LCS 500-383173/2-A Lab Control Sample
85 65 91 12690 108LCSD 500-383173/3-A Lab Control Sample Dup
91 69 89 10286 107MB 500-383173/1-A Method Blank
Surrogate Legend
2FP = 2-Fluorophenol
PHL = Phenol-d5
NBZ = Nitrobenzene-d5
FBP = 2-Fluorobiphenyl
TBP = 2,4,6-Tribromophenol
TPH = Terphenyl-d14
Method: 8081B - Organochlorine Pesticides (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-130)(30-120)
DCB1 TCX1
57 69500-127325-1
Percent Surrogate Recovery (Acceptance Limits)
MW-55
63 71500-127325-2 MW-56
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Surrogate Summary
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-130)(30-120)
DCB1 TCX1
88 79500-127325-3
Percent Surrogate Recovery (Acceptance Limits)
MW-56A
75 83500-127325-4 MW-56D
63 76500-127325-5 MW-57
72 70500-127325-6 MW-57D
80 68LCS 500-383107/2-A Lab Control Sample
87 68LCSD 500-383107/3-A Lab Control Sample Dup
64 62MB 500-383107/1-A Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-120)(30-140)
TCX1 DCB1
72 86500-127325-1
Percent Surrogate Recovery (Acceptance Limits)
MW-55
77 66500-127325-2 MW-56
82 88500-127325-3 MW-56A
75 87500-127325-4 MW-56D
82 82500-127325-5 MW-57
84 95500-127325-6 MW-57D
74 76LCS 500-383107/4-A Lab Control Sample
70 90LCSD 500-383107/5-A Lab Control Sample Dup
75 80MB 500-383107/1-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
Method: 8151A - Herbicides (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (25-130)
DCPA1
59500-127325-1
Percent Surrogate Recovery (Acceptance Limits)
MW-55
70500-127325-2 MW-56
49500-127325-3 MW-56A
65500-127325-4 MW-56D
69500-127325-5 MW-57
58500-127325-6 MW-57D
54LCS 500-383303/2-A Lab Control Sample
54LCSD 500-383303/3-A Lab Control Sample Dup
53MB 500-383303/1-A Method Blank
Surrogate Legend
DCPA = DCAA
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-384124/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384124
RL MDL
Benzene <0.50 0.50 0.15 ug/L 05/07/17 21:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<100 23100 ug/L 05/07/17 21:41 1Acrolein
<2.0 0.802.0 ug/L 05/07/17 21:41 1Bromomethane
<2.0 0.452.0 ug/L 05/07/17 21:41 1Carbon disulfide
<5.0 1.75.0 ug/L 05/07/17 21:41 1Acetone
<10 4.210 ug/L 05/07/17 21:41 1Acetonitrile
<1.0 0.511.0 ug/L 05/07/17 21:41 1Chloroethane
<20 4.520 ug/L 05/07/17 21:41 1Acrylonitrile
<1.0 0.321.0 ug/L 05/07/17 21:41 1Chloromethane
<1.0 0.411.0 ug/L 05/07/17 21:41 1cis-1,2-Dichloroethene
<5.0 2.15.0 ug/L 05/07/17 21:41 12-Butanone (MEK)
<1.0 0.431.0 ug/L 05/07/17 21:41 1Bromochloromethane
<2.0 0.372.0 ug/L 05/07/17 21:41 1Chloroform
<1.0 0.381.0 ug/L 05/07/17 21:41 1Carbon tetrachloride
<2.0 0.672.0 ug/L 05/07/17 21:41 1Dichlorodifluoromethane
<1.0 0.411.0 ug/L 05/07/17 21:41 11,1-Dichloroethane
<1.0 0.391.0 ug/L 05/07/17 21:41 11,2-Dichloroethane
<1.0 0.391.0 ug/L 05/07/17 21:41 11,1-Dichloroethene
<1.0 0.441.0 ug/L 05/07/17 21:41 12,2-Dichloropropane
<1.0 0.271.0 ug/L 05/07/17 21:41 1Dibromomethane
<1.0 0.431.0 ug/L 05/07/17 21:41 11,2-Dichloropropane
<1.0 0.371.0 ug/L 05/07/17 21:41 1Bromodichloromethane
<1.0 0.421.0 ug/L 05/07/17 21:41 1cis-1,3-Dichloropropene
<1.0 0.301.0 ug/L 05/07/17 21:41 11,1-Dichloropropene
<1.0 0.361.0 ug/L 05/07/17 21:41 11,3-Dichloropropane
<2.5 0.662.5 ug/L 05/07/17 21:41 1Iodomethane
<5.0 1.65.0 ug/L 05/07/17 21:41 12-Hexanone
<1.0 0.491.0 ug/L 05/07/17 21:41 1Dibromochloromethane
<1.0 0.391.0 ug/L 05/07/17 21:41 11,2-Dibromoethane
<5.0 1.65.0 ug/L 05/07/17 21:41 1Methylene Chloride
<1.0 0.391.0 ug/L 05/07/17 21:41 1Chlorobenzene
<5.0 2.25.0 ug/L 05/07/17 21:41 14-Methyl-2-pentanone (MIBK)
<0.50 0.180.50 ug/L 05/07/17 21:41 1Ethylbenzene
<10 4.810 ug/L 05/07/17 21:41 1Propionitrile
<1.0 0.391.0 ug/L 05/07/17 21:41 1Styrene
<1.0 0.461.0 ug/L 05/07/17 21:41 11,1,1,2-Tetrachloroethane
<1.0 0.481.0 ug/L 05/07/17 21:41 1Bromoform
<1.0 0.401.0 ug/L 05/07/17 21:41 11,1,2,2-Tetrachloroethane
<1.0 0.371.0 ug/L 05/07/17 21:41 1Tetrachloroethene
<10 1.910 ug/L 05/07/17 21:41 1Tetrahydrofuran
<0.50 0.150.50 ug/L 05/07/17 21:41 1Toluene
<1.0 0.401.0 ug/L 05/07/17 21:41 11,3-Dichlorobenzene
<5.0 1.25.0 ug/L 05/07/17 21:41 1trans-1,4-Dichloro-2-butene
<1.0 0.361.0 ug/L 05/07/17 21:41 11,4-Dichlorobenzene
<1.0 0.351.0 ug/L 05/07/17 21:41 1trans-1,2-Dichloroethene
<1.0 0.331.0 ug/L 05/07/17 21:41 11,2-Dichlorobenzene
<1.0 0.361.0 ug/L 05/07/17 21:41 1trans-1,3-Dichloropropene
<5.0 2.05.0 ug/L 05/07/17 21:41 11,2-Dibromo-3-Chloropropane
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-384124/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384124
RL MDL
1,1,1-Trichloroethane <1.0 1.0 0.38 ug/L 05/07/17 21:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.341.0 ug/L 05/07/17 21:41 11,2,4-Trichlorobenzene
<1.0 0.351.0 ug/L 05/07/17 21:41 11,1,2-Trichloroethane
<1.0 0.451.0 ug/L 05/07/17 21:41 1Hexachlorobutadiene
<2.5 0.862.5 ug/L 05/07/17 21:41 13-Chloropropene
<0.50 0.160.50 ug/L 05/07/17 21:41 1Trichloroethene
<1.0 0.231.0 ug/L 05/07/17 21:41 12-Chloro-1,3-butadiene
<1.0 0.431.0 ug/L 05/07/17 21:41 1Trichlorofluoromethane
<1.0 0.411.0 ug/L 05/07/17 21:41 11,2,3-Trichloropropane
<10 2.510 ug/L 05/07/17 21:41 1Methacrylonitrile
<100 36100 ug/L 05/07/17 21:41 1Isobutyl alcohol
<2.0 0.912.0 ug/L 05/07/17 21:41 1Vinyl acetate
<2.5 0.552.5 ug/L 05/07/17 21:41 1Methyl methacrylate
<0.50 0.200.50 ug/L 05/07/17 21:41 1Vinyl chloride
<2.5 0.532.5 ug/L 05/07/17 21:41 1Ethyl methacrylate
<1.0 0.221.0 ug/L 05/07/17 21:41 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)105 75-126 05/07/17 21:41 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
101 05/07/17 21:41 1Toluene-d8 (Surr)75-120
109 05/07/17 21:41 14-Bromofluorobenzene (Surr)72-124
91 05/07/17 21:41 1Dibromofluoromethane75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-384124/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384124
Benzene 50.0 50.9 ug/L 102 70-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Bromomethane 50.0 34.5 ug/L 69 40-130
Carbon disulfide 50.0 47.7 ug/L 95 66-120
Acetone 50.0 43.5 ug/L 87 40-143
Chloroethane 50.0 28.9 ug/L 58 45-127
Chloromethane 50.0 48.6 ug/L 97 54-147
cis-1,2-Dichloroethene 50.0 50.6 ug/L 101 70-125
2-Butanone (MEK)50.0 57.5 ug/L 115 53-141
Bromochloromethane 50.0 47.5 ug/L 95 65-122
Chloroform 50.0 48.7 ug/L 97 70-120
Carbon tetrachloride 50.0 49.6 ug/L 99 65-122
Dichlorodifluoromethane 50.0 48.0 ug/L 96 40-150
1,1-Dichloroethane 50.0 51.2 ug/L 102 70-125
1,2-Dichloroethane 50.0 53.7 ug/L 107 68-127
1,1-Dichloroethene 50.0 49.3 ug/L 99 67-122
2,2-Dichloropropane 50.0 49.4 ug/L 99 58-129
Dibromomethane 50.0 50.0 ug/L 100 70-120
1,2-Dichloropropane 50.0 53.8 ug/L 108 67-130
Bromodichloromethane 50.0 48.4 ug/L 97 69-120
cis-1,3-Dichloropropene 50.0 51.4 ug/L 103 64-127
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-384124/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384124
1,1-Dichloropropene 50.0 52.1 ug/L 104 70-121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,3-Dichloropropane 50.0 52.9 ug/L 106 62-136
Iodomethane 50.0 46.5 ug/L 93 61-136
2-Hexanone 50.0 52.4 ug/L 105 56-135
Dibromochloromethane 50.0 48.2 ug/L 96 68-125
1,2-Dibromoethane 50.0 48.4 ug/L 97 70-125
Methylene Chloride 50.0 45.8 ug/L 92 69-125
Chlorobenzene 50.0 52.9 ug/L 106 70-120
4-Methyl-2-pentanone (MIBK)50.0 55.9 ug/L 112 56-133
Ethylbenzene 50.0 51.0 ug/L 102 70-120
m&p-Xylene 50.0 53.8 ug/L 108 70-125
o-Xylene 50.0 50.7 ug/L 101 70-120
Styrene 50.0 49.7 ug/L 99 70-120
1,1,1,2-Tetrachloroethane 50.0 50.6 ug/L 101 70-125
Bromoform 50.0 54.7 ug/L 109 56-132
1,1,2,2-Tetrachloroethane 50.0 48.0 ug/L 96 67-127
Tetrachloroethene 50.0 56.1 ug/L 112 70-128
Tetrahydrofuran 100 96.9 ug/L 97 59-139
Toluene 50.0 53.7 ug/L 107 70-125
1,3-Dichlorobenzene 50.0 51.5 ug/L 103 70-125
1,4-Dichlorobenzene 50.0 50.4 ug/L 101 70-120
trans-1,2-Dichloroethene 50.0 48.6 ug/L 97 70-125
1,2-Dichlorobenzene 50.0 50.7 ug/L 101 70-125
trans-1,3-Dichloropropene 50.0 50.5 ug/L 101 62-128
1,2-Dibromo-3-Chloropropane 50.0 44.7 ug/L 89 56-123
1,1,1-Trichloroethane 50.0 49.1 ug/L 98 70-125
1,2,4-Trichlorobenzene 50.0 42.9 ug/L 86 66-127
1,1,2-Trichloroethane 50.0 52.2 ug/L 104 70-122
Hexachlorobutadiene 50.0 56.6 ug/L 113 51-150
Trichloroethene 50.0 51.6 ug/L 103 70-125
Trichlorofluoromethane 50.0 45.6 ug/L 91 70-126
1,2,3-Trichloropropane 50.0 49.1 ug/L 98 50-133
Vinyl acetate 50.0 52.1 ug/L 104 43-133
Vinyl chloride 50.0 47.5 ug/L 95 64-126
Xylenes, Total 100 105 ug/L 105 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
101Toluene-d8 (Surr)75 -120
1084-Bromofluorobenzene (Surr)72 -124
96Dibromofluoromethane 75 -120
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-383173/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383899 Prep Batch: 383173
RL MDL
Acenaphthene <0.80 0.80 0.25 ug/L 05/01/17 15:19 05/05/17 13:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.80 0.210.80 ug/L 05/01/17 15:19 05/05/17 13:57 1Acenaphthylene
<4.0 0.534.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Acetophenone
<8.0 1.78.0 ug/L 05/01/17 15:19 05/05/17 13:57 12-Acetylaminofluorene
<8.0 3.08.0 ug/L 05/01/17 15:19 05/05/17 13:57 14-Aminobiphenyl
<0.80 0.270.80 ug/L 05/01/17 15:19 05/05/17 13:57 1Anthracene
<0.16 0.0450.16 ug/L 05/01/17 15:19 05/05/17 13:57 1Benzo[a]anthracene
<0.16 0.0790.16 ug/L 05/01/17 15:19 05/05/17 13:57 1Benzo[a]pyrene
<0.16 0.0650.16 ug/L 05/01/17 15:19 05/05/17 13:57 1Benzo[b]fluoranthene
<0.80 0.300.80 ug/L 05/01/17 15:19 05/05/17 13:57 1Benzo[g,h,i]perylene
<0.16 0.0510.16 ug/L 05/01/17 15:19 05/05/17 13:57 1Benzo[k]fluoranthene
<16 4.816 ug/L 05/01/17 15:19 05/05/17 13:57 1Benzyl alcohol
<1.6 0.231.6 ug/L 05/01/17 15:19 05/05/17 13:57 1Bis(2-chloroethoxy)methane
<1.6 0.231.6 ug/L 05/01/17 15:19 05/05/17 13:57 1Bis(2-chloroethyl)ether
<8.0 1.48.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Bis(2-ethylhexyl) phthalate
<4.0 0.434.0 ug/L 05/01/17 15:19 05/05/17 13:57 14-Bromophenyl phenyl ether
<1.6 0.381.6 ug/L 05/01/17 15:19 05/05/17 13:57 1Butyl benzyl phthalate
<8.0 1.68.0 ug/L 05/01/17 15:19 05/05/17 13:57 14-Chloroaniline
<8.0 2.78.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Chlorobenzilate
<8.0 1.88.0 ug/L 05/01/17 15:19 05/05/17 13:57 14-Chloro-3-methylphenol
<1.6 0.191.6 ug/L 05/01/17 15:19 05/05/17 13:57 12-Chloronaphthalene
<4.0 0.454.0 ug/L 05/01/17 15:19 05/05/17 13:57 12-Chlorophenol
<4.0 0.514.0 ug/L 05/01/17 15:19 05/05/17 13:57 14-Chlorophenyl phenyl ether
<0.16 0.0550.16 ug/L 05/01/17 15:19 05/05/17 13:57 1Chrysene
<8.0 4.48.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Diallate
<0.24 0.0410.24 ug/L 05/01/17 15:19 05/05/17 13:57 1Dibenz(a,h)anthracene
<1.6 0.211.6 ug/L 05/01/17 15:19 05/05/17 13:57 1Dibenzofuran
<4.0 1.44.0 ug/L 05/01/17 15:19 05/05/17 13:57 13,3'-Dichlorobenzidine
<8.0 2.18.0 ug/L 05/01/17 15:19 05/05/17 13:57 12,4-Dichlorophenol
<8.0 2.88.0 ug/L 05/01/17 15:19 05/05/17 13:57 12,6-Dichlorophenol
<1.6 0.291.6 ug/L 05/01/17 15:19 05/05/17 13:57 1Diethyl phthalate
<8.0 1.58.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Dimethoate
<32 2.432 ug/L 05/01/17 15:19 05/05/17 13:57 17,12-Dimethylbenz(a)anthracene
<32 1432 ug/L 05/01/17 15:19 05/05/17 13:57 13,3'-Dimethylbenzidine
<8.0 1.48.0 ug/L 05/01/17 15:19 05/05/17 13:57 12,4-Dimethylphenol
<1.6 0.251.6 ug/L 05/01/17 15:19 05/05/17 13:57 1Dimethyl phthalate
<4.0 0.584.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Di-n-butyl phthalate
<16 4.716 ug/L 05/01/17 15:19 05/05/17 13:57 14,6-Dinitro-2-methylphenol
<16 6.916 ug/L 05/01/17 15:19 05/05/17 13:57 12,4-Dinitrophenol
<0.80 0.0590.80 ug/L 05/01/17 15:19 05/05/17 13:57 12,6-Dinitrotoluene
<0.80 0.200.80 ug/L 05/01/17 15:19 05/05/17 13:57 12,4-Dinitrotoluene
<8.0 0.848.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Di-n-octyl phthalate
<8.0 2.08.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Diphenylamine
<8.0 1.58.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Disulfoton
<16 3.016 ug/L 05/01/17 15:19 05/05/17 13:57 1Ethyl methanesulfonate
<8.0 1.78.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Ethyl Parathion
<32 2432 ug/L 05/01/17 15:19 05/05/17 13:57 1Famphur
<0.80 0.360.80 ug/L 05/01/17 15:19 05/05/17 13:57 1Fluoranthene
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-383173/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383899 Prep Batch: 383173
RL MDL
Fluorene <0.80 0.80 0.20 ug/L 05/01/17 15:19 05/05/17 13:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.40 0.0640.40 ug/L 05/01/17 15:19 05/05/17 13:57 1Hexachlorobenzene
<16 5.116 ug/L 05/01/17 15:19 05/05/17 13:57 1Hexachlorocyclopentadiene
<4.0 0.484.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Hexachloroethane
<16 3.816 ug/L 05/01/17 15:19 05/05/17 13:57 1Hexachloropropene
<0.16 0.0600.16 ug/L 05/01/17 15:19 05/05/17 13:57 1Indeno[1,2,3-cd]pyrene
<16 5.516 ug/L 05/01/17 15:19 05/05/17 13:57 1Isodrin
<1.6 0.301.6 ug/L 05/01/17 15:19 05/05/17 13:57 1Isophorone
<8.0 3.18.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Isosafrole
<8.0 1.38.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Kepone
<4.0 1.14.0 ug/L 05/01/17 15:19 05/05/17 13:57 1m-Dinitrobenzene
<32 8.132 ug/L 05/01/17 15:19 05/05/17 13:57 1Methapyrilene
<8.0 1.88.0 ug/L 05/01/17 15:19 05/05/17 13:57 13-Methylcholanthrene
<32 4.832 ug/L 05/01/17 15:19 05/05/17 13:57 1Methyl methanesulfonate
<1.6 0.0521.6 ug/L 05/01/17 15:19 05/05/17 13:57 12-Methylnaphthalene
<8.0 1.98.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Methyl parathion
<1.6 0.241.6 ug/L 05/01/17 15:19 05/05/17 13:57 12-Methylphenol
<1.6 0.361.6 ug/L 05/01/17 15:19 05/05/17 13:57 13 & 4 Methylphenol
<0.80 0.250.80 ug/L 05/01/17 15:19 05/05/17 13:57 1Naphthalene
<32 3132 ug/L 05/01/17 15:19 05/05/17 13:57 11,4-Naphthoquinone
<16 4.716 ug/L 05/01/17 15:19 05/05/17 13:57 11-Naphthylamine
<16 7.316 ug/L 05/01/17 15:19 05/05/17 13:57 12-Naphthylamine
<4.0 1.04.0 ug/L 05/01/17 15:19 05/05/17 13:57 12-Nitroaniline
<8.0 1.48.0 ug/L 05/01/17 15:19 05/05/17 13:57 13-Nitroaniline
<8.0 1.38.0 ug/L 05/01/17 15:19 05/05/17 13:57 14-Nitroaniline
<0.80 0.360.80 ug/L 05/01/17 15:19 05/05/17 13:57 1Nitrobenzene
<8.0 2.58.0 ug/L 05/01/17 15:19 05/05/17 13:57 15-Nitro-o-toluidine
<8.0 2.08.0 ug/L 05/01/17 15:19 05/05/17 13:57 12-Nitrophenol
<16 5.916 ug/L 05/01/17 15:19 05/05/17 13:57 14-Nitrophenol
<16 6.916 ug/L 05/01/17 15:19 05/05/17 13:57 1N-Nitrosodiethylamine
<8.0 3.88.0 ug/L 05/01/17 15:19 05/05/17 13:57 1N-Nitrosodimethylamine
<8.0 3.48.0 ug/L 05/01/17 15:19 05/05/17 13:57 1N-Nitrosodi-n-butylamine
<0.40 0.120.40 ug/L 05/01/17 15:19 05/05/17 13:57 1N-Nitrosodi-n-propylamine
<1.6 0.301.6 ug/L 05/01/17 15:19 05/05/17 13:57 1N-Nitrosodiphenylamine
<16 6.016 ug/L 05/01/17 15:19 05/05/17 13:57 1N-Nitrosomethylethylamine
<8.0 2.88.0 ug/L 05/01/17 15:19 05/05/17 13:57 1N-Nitrosopiperidine
<8.0 2.78.0 ug/L 05/01/17 15:19 05/05/17 13:57 1N-Nitrosopyrrolidine
<16 4.416 ug/L 05/01/17 15:19 05/05/17 13:57 1o,o',o''-Triethylphosphorothioate
<32 6.332 ug/L 05/01/17 15:19 05/05/17 13:57 1o-Toluidine
<1.6 0.301.6 ug/L 05/01/17 15:19 05/05/17 13:57 12,2'-oxybis[1-chloropropane]
<8.0 2.48.0 ug/L 05/01/17 15:19 05/05/17 13:57 1p-Dimethylamino azobenzene
<8.0 2.28.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Pentachlorobenzene
<8.0 2.98.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Pentachloronitrobenzene
<8.0 1.88.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Phenacetin
<0.80 0.240.80 ug/L 05/01/17 15:19 05/05/17 13:57 1Phenanthrene
<4.0 0.544.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Phenol
<8.0 1.78.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Phorate
<64 1364 ug/L 05/01/17 15:19 05/05/17 13:57 1p-Phenylene diamine
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-383173/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383899 Prep Batch: 383173
RL MDL
Pronamide <8.0 8.0 1.7 ug/L 05/01/17 15:19 05/05/17 13:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.80 0.340.80 ug/L 05/01/17 15:19 05/05/17 13:57 1Pyrene
<8.0 3.28.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Safrole
<8.0 1.58.0 ug/L 05/01/17 15:19 05/05/17 13:57 1sym-Trinitrobenzene
<8.0 8.08.0 ug/L 05/01/17 15:19 05/05/17 13:57 12,3,7,8-TCDD (Screen)
<4.0 0.464.0 ug/L 05/01/17 15:19 05/05/17 13:57 11,2,4,5-Tetrachlorobenzene
<4.0 0.604.0 ug/L 05/01/17 15:19 05/05/17 13:57 12,3,4,6-Tetrachlorophenol
<8.0 2.18.0 ug/L 05/01/17 15:19 05/05/17 13:57 1Thionazin
<4.0 0.574.0 ug/L 05/01/17 15:19 05/05/17 13:57 12,4,6-Trichlorophenol
<8.0 2.18.0 ug/L 05/01/17 15:19 05/05/17 13:57 12,4,5-Trichlorophenol
2-Fluorophenol 91 27-110 05/05/17 13:57 1
MB MB
Surrogate
05/01/17 15:19
Dil FacPreparedAnalyzedQualifierLimits%Recovery
69 05/01/17 15:19 05/05/17 13:57 1Phenol-d5 20-100
89 05/01/17 15:19 05/05/17 13:57 1Nitrobenzene-d5 36-120
86 05/01/17 15:19 05/05/17 13:57 12-Fluorobiphenyl 34-110
102 05/01/17 15:19 05/05/17 13:57 12,4,6-Tribromophenol 40-145
107 05/01/17 15:19 05/05/17 13:57 1Terphenyl-d14 40-145
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383173/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383899 Prep Batch: 383173
Acenaphthene 32.0 29.4 ug/L 92 46-110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 32.0 27.3 ug/L 85 47-110
Acetophenone 32.0 30.1 ug/L 94 60-110
Anthracene 32.0 31.4 ug/L 98 67-110
Benzo[a]anthracene 32.0 32.6 ug/L 102 70-120
Benzo[a]pyrene 32.0 35.7 ug/L 112 70-120
Benzo[b]fluoranthene 32.0 37.4 ug/L 117 69-123
Benzo[g,h,i]perylene 32.0 35.7 ug/L 112 70-120
Benzo[k]fluoranthene 32.0 35.7 ug/L 112 70-120
Benzyl alcohol 32.0 31.4 ug/L 98 33-127
Bis(2-chloroethoxy)methane 32.0 30.2 ug/L 94 60-110
Bis(2-chloroethyl)ether 32.0 29.7 ug/L 93 49-110
Bis(2-ethylhexyl) phthalate 32.0 31.6 ug/L 99 69-120
4-Bromophenyl phenyl ether 32.0 34.1 ug/L 106 58-120
Butyl benzyl phthalate 32.0 30.9 ug/L 96 68-120
4-Chloroaniline 32.0 26.9 ug/L 84 35-128
4-Chloro-3-methylphenol 32.0 31.1 ug/L 97 64-120
2-Chloronaphthalene 32.0 28.7 ug/L 90 39-110
2-Chlorophenol 32.0 30.2 ug/L 94 59-110
4-Chlorophenyl phenyl ether 32.0 31.6 ug/L 99 47-112
Chrysene 32.0 32.4 ug/L 101 68-120
Dibenz(a,h)anthracene 32.0 37.3 ug/L 117 70-127
Dibenzofuran 32.0 29.7 ug/L 93 51-110
3,3'-Dichlorobenzidine 32.0 34.9 ug/L 109 60-132
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383173/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383899 Prep Batch: 383173
2,4-Dichlorophenol 32.0 31.9 ug/L 100 62-110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
2,6-Dichlorophenol 32.0 31.7 ug/L 99 60-110
Diethyl phthalate 32.0 31.9 ug/L 100 62-120
2,4-Dimethylphenol 32.0 24.4 ug/L 76 51-110
Dimethyl phthalate 32.0 31.9 ug/L 100 63-120
Di-n-butyl phthalate 32.0 31.8 ug/L 100 70-120
4,6-Dinitro-2-methylphenol 64.0 73.2 ug/L 114 50-117
2,4-Dinitrophenol 64.0 69.2 ug/L 108 37-130
2,6-Dinitrotoluene 32.0 33.4 ug/L 104 63-119
2,4-Dinitrotoluene 32.0 32.6 ug/L 102 63-122
Di-n-octyl phthalate 32.0 33.2 ug/L 104 70-122
Fluoranthene 32.0 33.0 ug/L 103 68-120
Fluorene 32.0 31.0 ug/L 97 53-120
Hexachlorobenzene 32.0 33.9 ug/L 106 61-120
Hexachlorocyclopentadiene 32.0 16.7 ug/L 52 10-100
Hexachloroethane 32.0 22.7 ug/L 71 20-100
Indeno[1,2,3-cd]pyrene 32.0 36.7 ug/L 115 65-133
Isophorone 32.0 29.3 ug/L 92 57-110
2-Methylnaphthalene 32.0 27.0 ug/L 85 34-110
2-Methylphenol 32.0 28.3 ug/L 88 53-110
3 & 4 Methylphenol 32.0 29.7 ug/L 93 53-110
Naphthalene 32.0 26.6 ug/L 83 36-110
2-Nitroaniline 32.0 29.5 ug/L 92 59-122
3-Nitroaniline 32.0 25.6 ug/L 80 47-123
4-Nitroaniline 32.0 25.6 ug/L 80 52-147
Nitrobenzene 32.0 30.4 ug/L 95 53-110
2-Nitrophenol 32.0 31.5 ug/L 98 58-110
4-Nitrophenol 64.0 49.1 ug/L 77 20-110
N-Nitrosodimethylamine 32.0 23.3 ug/L 73 41-110
N-Nitrosodi-n-propylamine 32.0 29.5 ug/L 92 58-110
N-Nitrosodiphenylamine 32.0 31.7 ug/L 99 66-110
2,2'-oxybis[1-chloropropane]32.0 26.8 ug/L 84 38-110
Phenanthrene 32.0 31.4 ug/L 98 65-120
Phenol 32.0 22.3 ug/L 70 33-100
Pyrene 32.0 32.4 ug/L 101 70-110
1,2,4,5-Tetrachlorobenzene 32.0 28.5 ug/L 89 30-110
2,3,4,6-Tetrachlorophenol 32.0 35.9 ug/L 112 44-118
2,4,6-Trichlorophenol 32.0 34.2 ug/L 107 62-110
2,4,5-Trichlorophenol 32.0 34.7 ug/L 108 63-120
2-Fluorophenol 27 -110
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
69Phenol-d5 20 -100
98Nitrobenzene-d5 36 -120
902-Fluorobiphenyl 34 -110
1272,4,6-Tribromophenol 40 -145
111Terphenyl-d14 40 -145
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-383173/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383899 Prep Batch: 383173
Acenaphthene 32.0 29.5 ug/L 92 46-110 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 32.0 27.7 ug/L 87 47-110 1 20
Acetophenone 32.0 29.3 ug/L 92 60-110 3 20
Anthracene 32.0 30.5 ug/L 95 67-110 3 20
Benzo[a]anthracene 32.0 32.0 ug/L 100 70-120 2 20
Benzo[a]pyrene 32.0 34.2 ug/L 107 70-120 4 20
Benzo[b]fluoranthene 32.0 36.2 ug/L 113 69-123 3 20
Benzo[g,h,i]perylene 32.0 34.4 ug/L 108 70-120 4 20
Benzo[k]fluoranthene 32.0 35.5 ug/L 111 70-120 1 20
Benzyl alcohol 32.0 30.3 ug/L 95 33-127 3 20
Bis(2-chloroethoxy)methane 32.0 29.6 ug/L 93 60-110 2 20
Bis(2-chloroethyl)ether 32.0 29.5 ug/L 92 49-110 1 20
Bis(2-ethylhexyl) phthalate 32.0 30.9 ug/L 97 69-120 2 20
4-Bromophenyl phenyl ether 32.0 32.8 ug/L 103 58-120 4 20
Butyl benzyl phthalate 32.0 30.4 ug/L 95 68-120 1 20
4-Chloroaniline 32.0 26.8 ug/L 84 35-128 1 20
4-Chloro-3-methylphenol 32.0 29.3 ug/L 91 64-120 6 20
2-Chloronaphthalene 32.0 28.6 ug/L 90 39-110 0 20
2-Chlorophenol 32.0 30.0 ug/L 94 59-110 1 20
4-Chlorophenyl phenyl ether 32.0 31.5 ug/L 98 47-112 0 20
Chrysene 32.0 31.8 ug/L 99 68-120 2 20
Dibenz(a,h)anthracene 32.0 36.6 ug/L 114 70-127 2 20
Dibenzofuran 32.0 30.0 ug/L 94 51-110 1 20
3,3'-Dichlorobenzidine 32.0 36.3 ug/L 113 60-132 4 20
2,4-Dichlorophenol 32.0 30.7 ug/L 96 62-110 4 20
2,6-Dichlorophenol 32.0 30.8 ug/L 96 60-110 3 20
Diethyl phthalate 32.0 31.9 ug/L 100 62-120 0 20
2,4-Dimethylphenol 32.0 24.3 ug/L 76 51-110 1 20
Dimethyl phthalate 32.0 31.8 ug/L 100 63-120 0 20
Di-n-butyl phthalate 32.0 30.9 ug/L 97 70-120 3 20
4,6-Dinitro-2-methylphenol 64.0 70.7 ug/L 110 50-117 3 20
2,4-Dinitrophenol 64.0 69.3 ug/L 108 37-130 0 20
2,6-Dinitrotoluene 32.0 32.9 ug/L 103 63-119 1 20
2,4-Dinitrotoluene 32.0 32.7 ug/L 102 63-122 0 20
Di-n-octyl phthalate 32.0 32.2 ug/L 101 70-122 3 20
Fluoranthene 32.0 31.9 ug/L 100 68-120 3 20
Fluorene 32.0 31.4 ug/L 98 53-120 1 20
Hexachlorobenzene 32.0 32.6 ug/L 102 61-120 4 20
Hexachlorocyclopentadiene 32.0 17.8 ug/L 56 10-100 6 20
Hexachloroethane 32.0 22.8 ug/L 71 20-100 0 20
Indeno[1,2,3-cd]pyrene 32.0 35.8 ug/L 112 65-133 3 20
Isophorone 32.0 29.0 ug/L 91 57-110 1 20
2-Methylnaphthalene 32.0 26.0 ug/L 81 34-110 4 20
2-Methylphenol 32.0 28.2 ug/L 88 53-110 0 20
3 & 4 Methylphenol 32.0 29.4 ug/L 92 53-110 1 20
Naphthalene 32.0 26.8 ug/L 84 36-110 1 20
2-Nitroaniline 32.0 29.7 ug/L 93 59-122 1 20
3-Nitroaniline 32.0 26.9 ug/L 84 47-123 5 20
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-383173/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383899 Prep Batch: 383173
4-Nitroaniline 32.0 25.0 ug/L 78 52-147 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Nitrobenzene 32.0 28.6 ug/L 89 53-110 6 20
2-Nitrophenol 32.0 30.5 ug/L 95 58-110 3 20
4-Nitrophenol 64.0 48.0 ug/L 75 20-110 2 20
N-Nitrosodimethylamine 32.0 23.0 ug/L 72 41-110 1 20
N-Nitrosodi-n-propylamine 32.0 28.9 ug/L 90 58-110 2 20
N-Nitrosodiphenylamine 32.0 31.5 ug/L 98 66-110 1 20
2,2'-oxybis[1-chloropropane]32.0 27.4 ug/L 86 38-110 2 20
Phenanthrene 32.0 30.5 ug/L 95 65-120 3 20
Phenol 32.0 21.1 ug/L 66 33-100 6 20
Pyrene 32.0 31.8 ug/L 99 70-110 2 20
1,2,4,5-Tetrachlorobenzene 32.0 28.8 ug/L 90 30-110 1 20
2,3,4,6-Tetrachlorophenol 32.0 35.9 ug/L 112 44-118 0 20
2,4,6-Trichlorophenol 32.0 34.5 ug/L 108 62-110 1 20
2,4,5-Trichlorophenol 32.0 34.6 ug/L 108 63-120 0 20
2-Fluorophenol 27 -110
Surrogate
85
LCSD LCSD
Qualifier Limits%Recovery
65Phenol-d5 20 -100
91Nitrobenzene-d5 36 -120
902-Fluorobiphenyl 34 -110
1262,4,6-Tribromophenol 40 -145
108Terphenyl-d14 40 -145
Method: 8081B - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 500-383107/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383721 Prep Batch: 383107
RL MDL
alpha-BHC <0.040 0.040 0.0026 ug/L 05/01/17 10:27 05/04/17 23:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.040 0.0100.040 ug/L 05/01/17 10:27 05/04/17 23:32 1beta-BHC
<0.040 0.0100.040 ug/L 05/01/17 10:27 05/04/17 23:32 1delta-BHC
<0.040 0.00560.040 ug/L 05/01/17 10:27 05/04/17 23:32 1gamma-BHC (Lindane)
<0.040 0.0140.040 ug/L 05/01/17 10:27 05/04/17 23:32 1Heptachlor
<0.040 0.00530.040 ug/L 05/01/17 10:27 05/04/17 23:32 1Aldrin
<0.040 0.0140.040 ug/L 05/01/17 10:27 05/04/17 23:32 1Heptachlor epoxide
<0.040 0.00410.040 ug/L 05/01/17 10:27 05/04/17 23:32 1Endosulfan I
<0.040 0.0130.040 ug/L 05/01/17 10:27 05/04/17 23:32 1Dieldrin
<0.040 0.00380.040 ug/L 05/01/17 10:27 05/04/17 23:32 14,4'-DDE
<0.040 0.0140.040 ug/L 05/01/17 10:27 05/04/17 23:32 1Endrin
<0.040 0.00280.040 ug/L 05/01/17 10:27 05/04/17 23:32 1Endosulfan II
<0.040 0.0130.040 ug/L 05/01/17 10:27 05/04/17 23:32 14,4'-DDD
<0.040 0.0120.040 ug/L 05/01/17 10:27 05/04/17 23:32 1Endosulfan sulfate
<0.040 0.00320.040 ug/L 05/01/17 10:27 05/04/17 23:32 14,4'-DDT
<0.080 0.0230.080 ug/L 05/01/17 10:27 05/04/17 23:32 1Methoxychlor
<0.40 0.200.40 ug/L 05/01/17 10:27 05/04/17 23:32 1Toxaphene
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-383107/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383721 Prep Batch: 383107
RL MDL
Endrin aldehyde <0.040 0.040 0.0082 ug/L 05/01/17 10:27 05/04/17 23:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.080 0.0400.080 ug/L 05/01/17 10:27 05/04/17 23:32 1Chlordane (technical)
DCB Decachlorobiphenyl 64 30-130 05/04/17 23:32 1
MB MB
Surrogate
05/01/17 10:27
Dil FacPreparedAnalyzedQualifierLimits%Recovery
62 05/01/17 10:27 05/04/17 23:32 1Tetrachloro-m-xylene 30-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383107/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383721 Prep Batch: 383107
alpha-BHC 0.320 0.314 ug/L 98 65-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
beta-BHC 0.320 0.302 ug/L 94 65-120
delta-BHC 0.320 0.339 ug/L 106 70-122
gamma-BHC (Lindane)0.320 0.320 ug/L 100 68-120
Heptachlor 0.320 0.278 ug/L 87 40-120
Aldrin 0.320 0.268 ug/L 84 34-120
Heptachlor epoxide 0.320 0.314 ug/L 98 64-120
Endosulfan I 0.320 0.280 ug/L 88 35-110
Dieldrin 0.320 0.310 ug/L 97 68-120
4,4'-DDE 0.320 0.310 ug/L 97 58-122
Endrin 0.320 0.307 ug/L 96 60-132
Endosulfan II 0.320 0.285 ug/L 89 53-110
4,4'-DDD 0.320 0.318 ug/L 99 69-124
Endosulfan sulfate 0.320 0.349 ug/L 109 70-133
4,4'-DDT 0.320 0.305 ug/L 95 62-127
Methoxychlor 0.320 0.309 ug/L 97 63-135
Endrin aldehyde 0.320 0.314 ug/L 98 66-120
DCB Decachlorobiphenyl 30 -130
Surrogate
80
LCS LCS
Qualifier Limits%Recovery
68Tetrachloro-m-xylene 30 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-383107/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383721 Prep Batch: 383107
alpha-BHC 0.320 0.335 ug/L 105 65-120 6 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
beta-BHC 0.320 0.321 ug/L 100 65-120 6 20
delta-BHC 0.320 0.358 ug/L 112 70-122 6 20
gamma-BHC (Lindane)0.320 0.337 ug/L 105 68-120 5 20
Heptachlor 0.320 0.306 ug/L 96 40-120 10 20
Aldrin 0.320 0.314 ug/L 98 34-120 16 20
Heptachlor epoxide 0.320 0.332 ug/L 104 64-120 5 20
Endosulfan I 0.320 0.309 ug/L 97 35-110 10 20
Dieldrin 0.320 0.346 ug/L 108 68-120 11 20
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-383107/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383721 Prep Batch: 383107
4,4'-DDE 0.320 0.324 ug/L 101 58-122 4 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Endrin 0.320 0.338 ug/L 106 60-132 10 20
Endosulfan II 0.320 0.314 ug/L 98 53-110 10 20
4,4'-DDD 0.320 0.356 ug/L 111 69-124 11 20
Endosulfan sulfate 0.320 0.378 ug/L 118 70-133 8 20
4,4'-DDT 0.320 0.342 ug/L 107 62-127 11 20
Methoxychlor 0.320 0.359 ug/L 112 63-135 15 20
Endrin aldehyde 0.320 0.359 ug/L 112 66-120 13 20
DCB Decachlorobiphenyl 30 -130
Surrogate
87
LCSD LCSD
Qualifier Limits%Recovery
68Tetrachloro-m-xylene 30 -120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 500-383107/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383316 Prep Batch: 383107
RL MDL
PCB-1016 <0.40 0.40 0.067 ug/L 05/01/17 10:27 05/02/17 12:04 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.40 0.200.40 ug/L 05/01/17 10:27 05/02/17 12:04 1PCB-1221
<0.40 0.200.40 ug/L 05/01/17 10:27 05/02/17 12:04 1PCB-1232
<0.40 0.200.40 ug/L 05/01/17 10:27 05/02/17 12:04 1PCB-1242
<0.40 0.200.40 ug/L 05/01/17 10:27 05/02/17 12:04 1PCB-1248
<0.40 0.200.40 ug/L 05/01/17 10:27 05/02/17 12:04 1PCB-1254
<0.40 0.0700.40 ug/L 05/01/17 10:27 05/02/17 12:04 1PCB-1260
Tetrachloro-m-xylene 75 30-120 05/02/17 12:04 1
MB MB
Surrogate
05/01/17 10:27
Dil FacPreparedAnalyzedQualifierLimits%Recovery
80 05/01/17 10:27 05/02/17 12:04 1DCB Decachlorobiphenyl 30-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383107/4-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383316 Prep Batch: 383107
PCB-1016 4.00 3.43 ug/L 86 56-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
PCB-1260 4.00 3.30 ug/L 83 53-137
Tetrachloro-m-xylene 30 -120
Surrogate
74
LCS LCS
Qualifier Limits%Recovery
76DCB Decachlorobiphenyl 30 -140
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-383107/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383316 Prep Batch: 383107
PCB-1016 4.00 3.33 ug/L 83 56-120 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
PCB-1260 4.00 3.38 ug/L 84 53-137 2 20
Tetrachloro-m-xylene 30 -120
Surrogate
70
LCSD LCSD
Qualifier Limits%Recovery
90DCB Decachlorobiphenyl 30 -140
Method: 8151A - Herbicides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 500-383303/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384274 Prep Batch: 383303
RL MDL
2,4-D <1.0 1.0 0.47 ug/L 05/02/17 10:54 05/08/17 23:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.50 0.0900.50 ug/L 05/02/17 10:54 05/08/17 23:26 1Pentachlorophenol
<1.0 0.291.0 ug/L 05/02/17 10:54 05/08/17 23:26 1Silvex (2,4,5-TP)
<1.0 0.431.0 ug/L 05/02/17 10:54 05/08/17 23:26 12,4,5-T
<2.0 0.162.0 ug/L 05/02/17 10:54 05/08/17 23:26 1Dinoseb
DCAA 53 25-130 05/08/17 23:26 1
MB MB
Surrogate
05/02/17 10:54
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383303/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384274 Prep Batch: 383303
2,4-D 10.0 6.62 ug/L 66 30-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Pentachlorophenol 2.50 1.40 ug/L 56 40-122
Silvex (2,4,5-TP)2.50 1.70 ug/L 68 32-115
2,4,5-T 2.50 1.48 ug/L 59 30-115
Dinoseb 10.1 4.42 ug/L 44 30-110
DCAA 25 -130
Surrogate
54
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-383303/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384274 Prep Batch: 383303
2,4-D 10.0 6.54 ug/L 65 30-115 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Pentachlorophenol 2.50 1.50 ug/L 60 40-122 7 20
Silvex (2,4,5-TP)2.50 1.69 ug/L 68 32-115 0 20
2,4,5-T 2.50 1.46 ug/L 58 30-115 1 20
Dinoseb 10.1 3.91 ug/L 39 30-110 12 20
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
DCAA 25 -130
Surrogate
54
LCSD LCSD
Qualifier Limits%Recovery
Method: 200.8 - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-383120/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383287 Prep Batch: 383120
RL MDL
Barium <2.5 2.5 0.37 ug/L 05/01/17 10:50 05/01/17 15:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.431.0 ug/L 05/01/17 10:50 05/01/17 15:35 1Beryllium
<0.50 0.150.50 ug/L 05/01/17 10:50 05/01/17 15:35 1Cadmium
<5.0 2.35.0 ug/L 05/01/17 10:50 05/01/17 15:35 1Chromium
<1.0 0.271.0 ug/L 05/01/17 10:50 05/01/17 15:35 1Cobalt
<100 38100 ug/L 05/01/17 10:50 05/01/17 15:35 1Iron
<2.5 1.12.5 ug/L 05/01/17 10:50 05/01/17 15:35 1Manganese
<0.50 0.160.50 ug/L 05/01/17 10:50 05/01/17 15:35 1Lead
<2.0 0.922.0 ug/L 05/01/17 10:50 05/01/17 15:35 1Nickel
<3.0 1.33.0 ug/L 05/01/17 10:50 05/01/17 15:35 1Antimony
<2.5 1.12.5 ug/L 05/01/17 10:50 05/01/17 15:35 1Selenium
<0.50 0.0780.50 ug/L 05/01/17 10:50 05/01/17 15:35 1Silver
<2.0 0.652.0 ug/L 05/01/17 10:50 05/01/17 15:35 1Thallium
<10 4.210 ug/L 05/01/17 10:50 05/01/17 15:35 1Tin
<5.0 2.05.0 ug/L 05/01/17 10:50 05/01/17 15:35 1Vanadium
Client Sample ID: Method BlankLab Sample ID: MB 500-383120/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383705 Prep Batch: 383120
RL MDL
Arsenic <1.0 1.0 0.15 ug/L 05/01/17 10:50 05/03/17 11:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<2.0 0.632.0 ug/L 05/01/17 10:50 05/03/17 11:55 1Copper
<20 8.120 ug/L 05/01/17 10:50 05/03/17 11:55 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383120/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383287 Prep Batch: 383120
Barium 500 547 ug/L 109 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 50.0 49.5 ug/L 99 85-115
Cadmium 50.0 52.2 ug/L 104 85-115
Chromium 200 208 ug/L 104 85-115
Cobalt 500 512 ug/L 102 85-115
Iron 1000 1020 ug/L 102 85-115
Manganese 500 521 ug/L 104 85-115
Lead 100 105 ug/L 105 85-115
Nickel 500 523 ug/L 105 85-115
Antimony 500 526 ug/L 105 85-115
Selenium 100 108 ug/L 108 85-115
Silver 50.0 51.9 ug/L 104 85-115
Thallium 100 103 ug/L 103 85-115
Tin 1000 1000 ug/L 100 85-115
Vanadium 500 515 ug/L 103 85-115
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383120/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383705 Prep Batch: 383120
Arsenic 100 102 ug/L 102 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Copper 250 262 ug/L 105 85-115
Zinc 500 521 ug/L 104 85-115
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383287 Prep Batch: 383120
Barium 120 500 654 ug/L 107 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <1.0 50.0 46.0 ug/L 92 70-130
Cadmium <0.50 50.0 51.5 ug/L 103 70-130
Chromium <5.0 200 189 ug/L 94 70-130
Cobalt 5.8 500 461 ug/L 91 70-130
Iron 810 1000 1680 ug/L 87 70-130
Manganese 98 500 568 ug/L 94 70-130
Lead 0.31 J 100 99.3 ug/L 99 70-130
Nickel 21 500 478 ug/L 91 70-130
Antimony <3.0 500 530 ug/L 106 70-130
Selenium <2.5 100 110 ug/L 110 70-130
Silver <0.50 50.0 50.5 ug/L 101 70-130
Thallium <2.0 100 97.8 ug/L 98 70-130
Tin <10 1000 1010 ug/L 101 70-130
Vanadium 6.8 500 476 ug/L 94 70-130
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383705 Prep Batch: 383120
Arsenic 0.18 J 100 103 ug/L 103 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Copper 5.3 250 263 ug/L 103 70-130
Zinc 10 J 500 518 ug/L 102 70-130
Client Sample ID: MW-57Lab Sample ID: 500-127325-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383287 Prep Batch: 383120
Barium 450 500 994 ug/L 110 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <1.0 50.0 47.1 ug/L 94 70-130
Cadmium <0.50 50.0 51.9 ug/L 104 70-130
Chromium <5.0 200 191 ug/L 96 70-130
Cobalt 17 500 470 ug/L 91 70-130
Iron 47000 1000 48400 4 ug/L 161 70-130
Lead 0.40 J 100 104 ug/L 103 70-130
Nickel 15 500 472 ug/L 91 70-130
Antimony <3.0 500 543 ug/L 109 70-130
Selenium <2.5 100 113 ug/L 113 70-130
Silver <0.50 50.0 51.2 ug/L 102 70-130
Thallium <2.0 100 102 ug/L 102 70-130
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: MW-57Lab Sample ID: 500-127325-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383287 Prep Batch: 383120
Tin <10 1000 1030 ug/L 103 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Vanadium <5.0 500 482 ug/L 96 70-130
Client Sample ID: MW-57Lab Sample ID: 500-127325-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383705 Prep Batch: 383120
Arsenic 1.2 100 105 ug/L 104 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Copper 0.68 J 250 252 ug/L 101 70-130
Zinc 17 J 500 502 ug/L 97 70-130
Client Sample ID: MW-57Lab Sample ID: 500-127325-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383705 Prep Batch: 383120
Manganese 10000 500 10700 4 ug/L 117 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383287 Prep Batch: 383120
Barium 120 118 ug/L 0.4 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Beryllium <1.0 <1.0 ug/L NC 20
Cadmium <0.50 <0.50 ug/L NC 20
Chromium <5.0 <5.0 ug/L NC 20
Cobalt 5.8 5.68 ug/L 2 20
Iron 810 628 F3 ug/L 25 20
Manganese 98 97.9 ug/L 0.4 20
Lead 0.31 J 0.195 J F5 ug/L 47 20
Nickel 21 20.7 ug/L 2 20
Antimony <3.0 <3.0 ug/L NC 20
Selenium <2.5 <2.5 ug/L NC 20
Silver <0.50 <0.50 ug/L NC 20
Thallium <2.0 <2.0 ug/L NC 20
Tin <10 <10 ug/L NC 20
Vanadium 6.8 6.49 ug/L 5 20
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383705 Prep Batch: 383120
Arsenic 0.18 J 0.200 J ug/L 13 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Copper 5.3 5.04 ug/L 6 20
Zinc 10 J <20 ug/L NC 20
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: MW-57Lab Sample ID: 500-127325-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383287 Prep Batch: 383120
Barium 450 464 ug/L 4 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Beryllium <1.0 <1.0 ug/L NC 20
Cadmium <0.50 <0.50 ug/L NC 20
Chromium <5.0 <5.0 ug/L NC 20
Cobalt 17 16.5 ug/L 0.9 20
Iron 47000 48000 ug/L 3 20
Lead 0.40 J <0.50 ug/L NC 20
Nickel 15 15.4 ug/L 0 20
Antimony <3.0 <3.0 ug/L NC 20
Selenium <2.5 <2.5 ug/L NC 20
Silver <0.50 <0.50 ug/L NC 20
Thallium <2.0 <2.0 ug/L NC 20
Tin <10 <10 ug/L NC 20
Vanadium <5.0 <5.0 ug/L NC 20
Client Sample ID: MW-57Lab Sample ID: 500-127325-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383705 Prep Batch: 383120
Arsenic 1.2 1.36 ug/L 12 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Copper 0.68 J <2.0 ug/L NC 20
Zinc 17 J <20 ug/L NC 20
Client Sample ID: MW-57Lab Sample ID: 500-127325-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383705 Prep Batch: 383120
Manganese 10000 10400 ug/L 2 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 245.1 - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-383544/12-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383786 Prep Batch: 383544
RL MDL
Mercury <0.20 0.20 0.091 ug/L 05/03/17 12:50 05/04/17 08:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383544/13-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383786 Prep Batch: 383544
Mercury 2.00 2.01 ug/L 101 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 245.1 - Mercury (CVAA) (Continued)
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383786 Prep Batch: 383544
Mercury <0.20 1.00 0.951 ug/L 95 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383786 Prep Batch: 383544
Mercury <0.20 <0.20 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 9014 - Cyanide
Client Sample ID: Method BlankLab Sample ID: MB 500-384259/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384368 Prep Batch: 384259
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 05/08/17 14:00 05/08/17 16:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-384259/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384368 Prep Batch: 384259
Cyanide, Total 0.100 0.101 mg/L 101 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384368 Prep Batch: 384259
Cyanide, Total <0.010 0.0400 0.0396 mg/L 99 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384368 Prep Batch: 384259
Cyanide, Total <0.010 0.0400 0.0349 mg/L 87 75-125 13 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 9056A - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 500-384190/36
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384190
RL MDL
Chloride <0.20 0.20 0.17 mg/L 05/05/17 19:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.20 0.0950.20 mg/L 05/05/17 19:15 1Sulfate
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: 9056A - Anions, Ion Chromatography (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-384190/37
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384190
Chloride 3.00 2.91 mg/L 97 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 5.00 5.43 mg/L 109 80-120
Client Sample ID: Method BlankLab Sample ID: MB 500-384336/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384336
RL MDL
Chloride <0.20 0.20 0.17 mg/L 05/08/17 11:04 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.20 0.0950.20 mg/L 05/08/17 11:04 1Sulfate
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-384336/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384336
Chloride 3.00 2.82 mg/L 94 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 5.00 4.78 mg/L 96 80-120
Method: SM 2320B - Alkalinity
Client Sample ID: Method BlankLab Sample ID: MB 500-384364/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384364
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 05/05/17 13:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-384364/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384364
Alkalinity 100 88.7 mg/L 89 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-56DLab Sample ID: 500-127325-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384364
Alkalinity 180 186 mg/L 1 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 500-127325-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49 Landfill
Method: SM 2540C - Solids, Total Dissolved (TDS)
Client Sample ID: Method BlankLab Sample ID: MB 500-383234/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383234
RL MDL
Total Dissolved Solids <10 10 4.3 mg/L 05/02/17 04:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383234/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383234
Total Dissolved Solids 250 288 mg/L 115 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383234
Total Dissolved Solids 350 250 652 mg/L 122 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-55Lab Sample ID: 500-127325-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383234
Total Dissolved Solids 350 336 mg/L 4 5
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-127325-1
Project/Site: NC Highway 49 Landfill
Client Sample ID: MW-55 Lab Sample ID: 500-127325-1
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Analysis 8260B 05/07/17 22:59 TCT1384124 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 383173 05/01/17 15:19 DAK TAL CHITotal/NA
Analysis 8270D 1 383899 05/05/17 14:46 AJD TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8081B 1 383721 05/05/17 00:30 PJG TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8082A 1 383316 05/02/17 12:50 BJH TAL CHITotal/NA
Prep 8151A 383303 05/02/17 10:54 JJH TAL CHITotal/NA
Analysis 8151A 1 384274 05/09/17 00:39 SAW TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383287 05/01/17 15:54 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383705 05/03/17 12:07 FXG TAL CHITotal/NA
Prep 245.1 383544 05/03/17 12:50 MJD TAL CHITotal/NA
Analysis 245.1 1 383786 05/04/17 08:42 MJD TAL CHITotal/NA
Prep 9010B 384259 05/08/17 14:00 MAN TAL CHITotal/NA
Analysis 9014 1 384368 MAN TAL CHITotal/NA
05/08/17 16:46
05/08/17 16:46
(Start)
(End)
Analysis 9056A 20 384336 05/08/17 11:41 PMF TAL CHITotal/NA
Analysis 9056A 10 384190 05/05/17 19:40 PMF TAL CHITotal/NA
Analysis SM 2320B 1 384364 05/05/17 15:38 SMO TAL CHITotal/NA
Analysis SM 2540C 1 383234 05/02/17 04:30 CLB TAL CHITotal/NA
Client Sample ID: MW-56 Lab Sample ID: 500-127325-2
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Analysis 8260B 05/07/17 23:26 TCT1384124 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 383173 05/01/17 15:19 DAK TAL CHITotal/NA
Analysis 8270D 1 383899 05/05/17 15:11 AJD TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8081B 1 383721 05/05/17 00:49 PJG TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8082A 1 383316 05/02/17 13:06 BJH TAL CHITotal/NA
Prep 8151A 383303 05/02/17 10:54 JJH TAL CHITotal/NA
Analysis 8151A 1 384274 05/09/17 01:04 SAW TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383287 05/01/17 16:17 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383705 05/03/17 12:22 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-127325-1
Project/Site: NC Highway 49 Landfill
Client Sample ID: MW-56 Lab Sample ID: 500-127325-2
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Analysis 200.8 05/03/17 14:19 FXG10383705 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 245.1 383544 05/03/17 12:50 MJD TAL CHITotal/NA
Analysis 245.1 1 383786 05/04/17 08:46 MJD TAL CHITotal/NA
Prep 9010B 384259 05/08/17 14:00 MAN TAL CHITotal/NA
Analysis 9014 1 384368 MAN TAL CHITotal/NA
05/08/17 16:47
05/08/17 16:47
(Start)
(End)
Analysis 9056A 10 384190 05/05/17 19:53 PMF TAL CHITotal/NA
Analysis SM 2320B 1 384364 05/05/17 15:45 SMO TAL CHITotal/NA
Analysis SM 2540C 1 383234 05/02/17 04:37 CLB TAL CHITotal/NA
Client Sample ID: MW-56A Lab Sample ID: 500-127325-3
Matrix: WaterDate Collected: 04/26/17 08:45
Date Received: 04/28/17 09:00
Analysis 8260B 05/07/17 23:52 TCT1384124 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 383173 05/01/17 15:19 DAK TAL CHITotal/NA
Analysis 8270D 1 383899 05/05/17 15:36 AJD TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8081B 1 383721 05/05/17 01:08 PJG TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8082A 1 383316 05/02/17 13:21 BJH TAL CHITotal/NA
Prep 8151A 383303 05/02/17 10:54 JJH TAL CHITotal/NA
Analysis 8151A 1 384274 05/09/17 01:28 SAW TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383287 05/01/17 16:21 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383705 05/03/17 12:26 FXG TAL CHITotal/NA
Prep 245.1 383544 05/03/17 12:50 MJD TAL CHITotal/NA
Analysis 245.1 1 383786 05/04/17 08:51 MJD TAL CHITotal/NA
Prep 9010B 384259 05/08/17 14:00 MAN TAL CHITotal/NA
Analysis 9014 1 384368 MAN TAL CHITotal/NA
05/08/17 16:47
05/08/17 16:47
(Start)
(End)
Analysis 9056A 10 384190 05/05/17 20:06 PMF TAL CHITotal/NA
Analysis SM 2320B 1 384364 05/05/17 15:51 SMO TAL CHITotal/NA
Analysis SM 2540C 1 383234 05/02/17 04:40 CLB TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-127325-1
Project/Site: NC Highway 49 Landfill
Client Sample ID: MW-56D Lab Sample ID: 500-127325-4
Matrix: WaterDate Collected: 04/26/17 08:30
Date Received: 04/28/17 09:00
Analysis 8260B 05/08/17 00:17 TCT1384124 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 383173 05/01/17 15:19 DAK TAL CHITotal/NA
Analysis 8270D 1 384111 05/07/17 16:42 GES TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8081B 1 383721 05/05/17 01:27 PJG TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8082A 1 383316 05/02/17 13:37 BJH TAL CHITotal/NA
Prep 8151A 383303 05/02/17 10:54 JJH TAL CHITotal/NA
Analysis 8151A 1 384274 05/09/17 01:52 SAW TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383287 05/01/17 16:24 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383705 05/03/17 12:29 FXG TAL CHITotal/NA
Prep 245.1 383544 05/03/17 12:50 MJD TAL CHITotal/NA
Analysis 245.1 1 383786 05/04/17 08:52 MJD TAL CHITotal/NA
Prep 9010B 384259 05/08/17 14:00 MAN TAL CHITotal/NA
Analysis 9014 1 384368 MAN TAL CHITotal/NA
05/08/17 16:47
05/08/17 16:48
(Start)
(End)
Analysis 9056A 10 384190 05/05/17 20:18 PMF TAL CHITotal/NA
Analysis SM 2320B 1 384364 05/05/17 15:57 SMO TAL CHITotal/NA
Analysis SM 2540C 1 383234 05/02/17 04:42 CLB TAL CHITotal/NA
Client Sample ID: MW-57 Lab Sample ID: 500-127325-5
Matrix: WaterDate Collected: 04/26/17 09:45
Date Received: 04/28/17 09:00
Analysis 8260B 05/08/17 00:43 TCT1384124 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 383173 05/01/17 15:19 DAK TAL CHITotal/NA
Analysis 8270D 1 384111 05/07/17 17:07 GES TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8081B 1 383721 05/05/17 01:47 PJG TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8082A 1 383316 05/02/17 13:52 BJH TAL CHITotal/NA
Prep 8151A 383303 05/02/17 10:54 JJH TAL CHITotal/NA
Analysis 8151A 1 384274 05/09/17 02:17 SAW TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383287 05/01/17 16:28 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383705 05/03/17 12:41 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 10 383705 05/03/17 14:23 FXG TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-127325-1
Project/Site: NC Highway 49 Landfill
Client Sample ID: MW-57 Lab Sample ID: 500-127325-5
Matrix: WaterDate Collected: 04/26/17 09:45
Date Received: 04/28/17 09:00
Prep 245.1 05/03/17 12:50 MJD383544 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 245.1 1 383786 05/04/17 08:54 MJD TAL CHITotal/NA
Prep 9010B 384259 05/08/17 14:00 MAN TAL CHITotal/NA
Analysis 9014 1 384368 MAN TAL CHITotal/NA
05/08/17 16:48
05/08/17 16:48
(Start)
(End)
Analysis 9056A 20 384190 05/05/17 20:31 PMF TAL CHITotal/NA
Analysis SM 2320B 1 384364 05/05/17 15:32 SMO TAL CHITotal/NA
Analysis SM 2540C 1 383234 05/02/17 04:45 CLB TAL CHITotal/NA
Client Sample ID: MW-57D Lab Sample ID: 500-127325-6
Matrix: WaterDate Collected: 04/26/17 09:50
Date Received: 04/28/17 09:00
Analysis 8260B 05/08/17 01:09 TCT1384124 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 383173 05/01/17 15:19 DAK TAL CHITotal/NA
Analysis 8270D 1 384111 05/07/17 17:31 GES TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8081B 1 383721 05/05/17 02:06 PJG TAL CHITotal/NA
Prep 3510C 383107 05/01/17 10:27 JJH TAL CHITotal/NA
Analysis 8082A 1 383316 05/02/17 14:07 BJH TAL CHITotal/NA
Prep 8151A 383303 05/02/17 10:54 JJH TAL CHITotal/NA
Analysis 8151A 1 384274 05/09/17 03:55 SAW TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383287 05/01/17 16:43 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383705 05/03/17 12:56 FXG TAL CHITotal/NA
Prep 245.1 383544 05/03/17 12:50 MJD TAL CHITotal/NA
Analysis 245.1 1 383786 05/04/17 08:55 MJD TAL CHITotal/NA
Prep 9010B 384259 05/08/17 14:00 MAN TAL CHITotal/NA
Analysis 9014 1 384368 MAN TAL CHITotal/NA
05/08/17 16:48
05/08/17 16:48
(Start)
(End)
Analysis 9056A 50 384190 05/05/17 20:44 PMF TAL CHITotal/NA
Analysis SM 2320B 1 384364 05/05/17 16:20 SMO TAL CHITotal/NA
Analysis SM 2540C 1 383234 05/02/17 04:47 CLB TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-127325-1
Project/Site: NC Highway 49 Landfill
Client Sample ID: SW-1 Lab Sample ID: 500-127325-7
Matrix: WaterDate Collected: 04/26/17 12:10
Date Received: 04/28/17 09:00
Analysis 8260B 05/08/17 01:35 TCT1384124 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383287 05/01/17 16:47 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383705 05/03/17 13:00 FXG TAL CHITotal/NA
Prep 245.1 383544 05/03/17 12:50 MJD TAL CHITotal/NA
Analysis 245.1 1 383786 05/04/17 08:57 MJD TAL CHITotal/NA
Client Sample ID: SW-2 Lab Sample ID: 500-127325-8
Matrix: WaterDate Collected: 04/26/17 13:10
Date Received: 04/28/17 09:00
Analysis 8260B 05/08/17 02:01 TCT1384124 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383287 05/01/17 16:51 FXG TAL CHITotal/NA
Prep 200.8 383120 05/01/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 383705 05/03/17 13:04 FXG TAL CHITotal/NA
Prep 245.1 383544 05/03/17 12:50 MJD TAL CHITotal/NA
Analysis 245.1 1 383786 05/04/17 08:58 MJD TAL CHITotal/NA
Client Sample ID: Duplicate Lab Sample ID: 500-127325-9
Matrix: WaterDate Collected: 04/26/17 00:00
Date Received: 04/28/17 09:00
Analysis 8260B 05/08/17 02:27 TCT1384124 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-127325-1
Project/Site: NC Highway 49 Landfill
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)2914State Program 12-31-17
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but are not accredited/certified under this accreditation/certification:
8270D 3510C Water Methyl parathion
8270D 3510C Water Phorate
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
200.8 200.8 Water Tin
8260B Water trans-1,4-Dichloro-2-butene
8270D 3510C Water 2,3,7,8-TCDD (Screen)
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 500-127325-1
Login Number: 127325
Question Answer Comment
Creator: Scott, Sherri L
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.2.1,3.3,2.4,3.4,0.1,1.9,2.0,0.0
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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#=CL#
May 02, 2017
LIMS USE: FR - ED STEPHENS
LIMS OBJECT ID: 92338704
92338704
Project:
Pace Project No.:
RE:
Ed Stephens
Civil & Environmental Consultants
1900 Center Park Drive
Charlotte, NC 28217
HIGHWAY 49 LANDFILL
Dear Ed Stephens:
Enclosed are the analytical results for sample(s) received by the laboratory on April 27, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92338704001 MW-55 SPLIT EPA 8260 63 PASI-CZDO
92338704002 MW-56 SPLIT EPA 8260 63 PASI-CZDO
92338704003 MW-57 SPLIT EPA 8260 63 PASI-CZDO
92338704004 MW-57D SPLIT EPA 8260 63 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 23
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92338704002 MW-56 SPLIT
Benzene 1.4 ug/L 04/30/17 02:461.0EPA 8260
cis-1,2-Dichloroethene 2.7 ug/L 04/30/17 02:461.0EPA 8260
Vinyl chloride 3.3 ug/L 04/30/17 02:461.0EPA 8260
92338704004 MW-57D SPLIT
Methyl-tert-butyl ether 2.0 ug/L 04/30/17 03:381.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Sample:MW-55 SPLIT Lab ID:92338704001 Collected:04/26/17 10:45 Received:04/27/17 14:21 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 04/30/17 02:29 67-64-125.0 1
Benzene ND ug/L 04/30/17 02:29 71-43-21.0 1
Bromobenzene ND ug/L 04/30/17 02:29 108-86-11.0 1
Bromochloromethane ND ug/L 04/30/17 02:29 74-97-51.0 1
Bromodichloromethane ND ug/L 04/30/17 02:29 75-27-41.0 1
Bromoform ND ug/L 04/30/17 02:29 75-25-21.0 1
Bromomethane ND ug/L 04/30/17 02:29 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/30/17 02:29 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/30/17 02:29 56-23-51.0 1
Chlorobenzene ND ug/L 04/30/17 02:29 108-90-71.0 1
Chloroethane ND ug/L 04/30/17 02:29 75-00-31.0 1
Chloroform ND ug/L 04/30/17 02:29 67-66-31.0 1
Chloromethane ND ug/L 04/30/17 02:29 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/30/17 02:29 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/30/17 02:29 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/30/17 02:29 96-12-82.0 1
Dibromochloromethane ND ug/L 04/30/17 02:29 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 04/30/17 02:29 106-93-41.0 1
Dibromomethane ND ug/L 04/30/17 02:29 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/30/17 02:29 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/30/17 02:29 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 04/30/17 02:29 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/30/17 02:29 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/30/17 02:29 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/30/17 02:29 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/30/17 02:29 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/30/17 02:29 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/30/17 02:29 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/30/17 02:29 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/30/17 02:29 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/30/17 02:29 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/30/17 02:29 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/30/17 02:29 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/30/17 02:29 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/30/17 02:29 108-20-31.0 1
Ethylbenzene ND ug/L 04/30/17 02:29 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/30/17 02:29 87-68-31.0 1
2-Hexanone ND ug/L 04/30/17 02:29 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/30/17 02:29 99-87-61.0 1
Methylene Chloride ND ug/L 04/30/17 02:29 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/30/17 02:29 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 04/30/17 02:29 1634-04-41.0 1
Naphthalene ND ug/L 04/30/17 02:29 91-20-31.0 1
Styrene ND ug/L 04/30/17 02:29 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/30/17 02:29 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/30/17 02:29 79-34-51.0 1
Tetrachloroethene ND ug/L 04/30/17 02:29 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Sample:MW-55 SPLIT Lab ID:92338704001 Collected:04/26/17 10:45 Received:04/27/17 14:21 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Toluene ND ug/L 04/30/17 02:29 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/30/17 02:29 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/30/17 02:29 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/30/17 02:29 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/30/17 02:29 79-00-51.0 1
Trichloroethene ND ug/L 04/30/17 02:29 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/30/17 02:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/30/17 02:29 96-18-41.0 1
Vinyl acetate ND ug/L 04/30/17 02:29 108-05-42.0 1
Vinyl chloride ND ug/L 04/30/17 02:29 75-01-41.0 1
Xylene (Total)ND ug/L 04/30/17 02:29 1330-20-71.0 1
m&p-Xylene ND ug/L 04/30/17 02:29 179601-23-12.0 1
o-Xylene ND ug/L 04/30/17 02:29 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %04/30/17 02:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %04/30/17 02:29 17060-07-070-130 1
Toluene-d8 (S)107 %04/30/17 02:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Sample:MW-56 SPLIT Lab ID:92338704002 Collected:04/26/17 12:10 Received:04/27/17 14:21 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 04/30/17 02:46 67-64-125.0 1
Benzene 1.4 ug/L 04/30/17 02:46 71-43-21.0 1
Bromobenzene ND ug/L 04/30/17 02:46 108-86-11.0 1
Bromochloromethane ND ug/L 04/30/17 02:46 74-97-51.0 1
Bromodichloromethane ND ug/L 04/30/17 02:46 75-27-41.0 1
Bromoform ND ug/L 04/30/17 02:46 75-25-21.0 1
Bromomethane ND ug/L 04/30/17 02:46 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/30/17 02:46 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/30/17 02:46 56-23-51.0 1
Chlorobenzene ND ug/L 04/30/17 02:46 108-90-71.0 1
Chloroethane ND ug/L 04/30/17 02:46 75-00-31.0 1
Chloroform ND ug/L 04/30/17 02:46 67-66-31.0 1
Chloromethane ND ug/L 04/30/17 02:46 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/30/17 02:46 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/30/17 02:46 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/30/17 02:46 96-12-82.0 1
Dibromochloromethane ND ug/L 04/30/17 02:46 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 04/30/17 02:46 106-93-41.0 1
Dibromomethane ND ug/L 04/30/17 02:46 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/30/17 02:46 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/30/17 02:46 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 04/30/17 02:46 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/30/17 02:46 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/30/17 02:46 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/30/17 02:46 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/30/17 02:46 75-35-41.0 1
cis-1,2-Dichloroethene 2.7 ug/L 04/30/17 02:46 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/30/17 02:46 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/30/17 02:46 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/30/17 02:46 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/30/17 02:46 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/30/17 02:46 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/30/17 02:46 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/30/17 02:46 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/30/17 02:46 108-20-31.0 1
Ethylbenzene ND ug/L 04/30/17 02:46 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/30/17 02:46 87-68-31.0 1
2-Hexanone ND ug/L 04/30/17 02:46 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/30/17 02:46 99-87-61.0 1
Methylene Chloride ND ug/L 04/30/17 02:46 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/30/17 02:46 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 04/30/17 02:46 1634-04-41.0 1
Naphthalene ND ug/L 04/30/17 02:46 91-20-31.0 1
Styrene ND ug/L 04/30/17 02:46 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/30/17 02:46 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/30/17 02:46 79-34-51.0 1
Tetrachloroethene ND ug/L 04/30/17 02:46 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
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Page 7 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Sample:MW-56 SPLIT Lab ID:92338704002 Collected:04/26/17 12:10 Received:04/27/17 14:21 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Toluene ND ug/L 04/30/17 02:46 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/30/17 02:46 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/30/17 02:46 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/30/17 02:46 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/30/17 02:46 79-00-51.0 1
Trichloroethene ND ug/L 04/30/17 02:46 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/30/17 02:46 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/30/17 02:46 96-18-41.0 1
Vinyl acetate ND ug/L 04/30/17 02:46 108-05-42.0 1
Vinyl chloride 3.3 ug/L 04/30/17 02:46 75-01-41.0 1
Xylene (Total)ND ug/L 04/30/17 02:46 1330-20-71.0 1
m&p-Xylene ND ug/L 04/30/17 02:46 179601-23-12.0 1
o-Xylene ND ug/L 04/30/17 02:46 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %04/30/17 02:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %04/30/17 02:46 17060-07-070-130 1
Toluene-d8 (S)106 %04/30/17 02:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Sample:MW-57 SPLIT Lab ID:92338704003 Collected:04/26/17 09:45 Received:04/27/17 14:21 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 04/30/17 03:21 67-64-125.0 1
Benzene ND ug/L 04/30/17 03:21 71-43-21.0 1
Bromobenzene ND ug/L 04/30/17 03:21 108-86-11.0 1
Bromochloromethane ND ug/L 04/30/17 03:21 74-97-51.0 1
Bromodichloromethane ND ug/L 04/30/17 03:21 75-27-41.0 1
Bromoform ND ug/L 04/30/17 03:21 75-25-21.0 1
Bromomethane ND ug/L 04/30/17 03:21 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/30/17 03:21 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/30/17 03:21 56-23-51.0 1
Chlorobenzene ND ug/L 04/30/17 03:21 108-90-71.0 1
Chloroethane ND ug/L 04/30/17 03:21 75-00-31.0 1
Chloroform ND ug/L 04/30/17 03:21 67-66-31.0 1
Chloromethane ND ug/L 04/30/17 03:21 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/30/17 03:21 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/30/17 03:21 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/30/17 03:21 96-12-82.0 1
Dibromochloromethane ND ug/L 04/30/17 03:21 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 04/30/17 03:21 106-93-41.0 1
Dibromomethane ND ug/L 04/30/17 03:21 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/30/17 03:21 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/30/17 03:21 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 04/30/17 03:21 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/30/17 03:21 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/30/17 03:21 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/30/17 03:21 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/30/17 03:21 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/30/17 03:21 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/30/17 03:21 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/30/17 03:21 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/30/17 03:21 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/30/17 03:21 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/30/17 03:21 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/30/17 03:21 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/30/17 03:21 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/30/17 03:21 108-20-31.0 1
Ethylbenzene ND ug/L 04/30/17 03:21 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/30/17 03:21 87-68-31.0 1
2-Hexanone ND ug/L 04/30/17 03:21 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/30/17 03:21 99-87-61.0 1
Methylene Chloride ND ug/L 04/30/17 03:21 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/30/17 03:21 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 04/30/17 03:21 1634-04-41.0 1
Naphthalene ND ug/L 04/30/17 03:21 91-20-31.0 1
Styrene ND ug/L 04/30/17 03:21 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/30/17 03:21 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/30/17 03:21 79-34-51.0 1
Tetrachloroethene ND ug/L 04/30/17 03:21 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
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Page 9 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Sample:MW-57 SPLIT Lab ID:92338704003 Collected:04/26/17 09:45 Received:04/27/17 14:21 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Toluene ND ug/L 04/30/17 03:21 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/30/17 03:21 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/30/17 03:21 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/30/17 03:21 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/30/17 03:21 79-00-51.0 1
Trichloroethene ND ug/L 04/30/17 03:21 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/30/17 03:21 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/30/17 03:21 96-18-41.0 1
Vinyl acetate ND ug/L 04/30/17 03:21 108-05-42.0 1
Vinyl chloride ND ug/L 04/30/17 03:21 75-01-41.0 1
Xylene (Total)ND ug/L 04/30/17 03:21 1330-20-71.0 1
m&p-Xylene ND ug/L 04/30/17 03:21 179601-23-12.0 1
o-Xylene ND ug/L 04/30/17 03:21 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %04/30/17 03:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %04/30/17 03:21 17060-07-070-130 1
Toluene-d8 (S)109 %04/30/17 03:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Sample:MW-57D SPLIT Lab ID:92338704004 Collected:04/26/17 09:50 Received:04/27/17 14:21 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 04/30/17 03:38 67-64-125.0 1
Benzene ND ug/L 04/30/17 03:38 71-43-21.0 1
Bromobenzene ND ug/L 04/30/17 03:38 108-86-11.0 1
Bromochloromethane ND ug/L 04/30/17 03:38 74-97-51.0 1
Bromodichloromethane ND ug/L 04/30/17 03:38 75-27-41.0 1
Bromoform ND ug/L 04/30/17 03:38 75-25-21.0 1
Bromomethane ND ug/L 04/30/17 03:38 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/30/17 03:38 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/30/17 03:38 56-23-51.0 1
Chlorobenzene ND ug/L 04/30/17 03:38 108-90-71.0 1
Chloroethane ND ug/L 04/30/17 03:38 75-00-31.0 1
Chloroform ND ug/L 04/30/17 03:38 67-66-31.0 1
Chloromethane ND ug/L 04/30/17 03:38 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/30/17 03:38 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/30/17 03:38 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/30/17 03:38 96-12-82.0 1
Dibromochloromethane ND ug/L 04/30/17 03:38 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 04/30/17 03:38 106-93-41.0 1
Dibromomethane ND ug/L 04/30/17 03:38 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/30/17 03:38 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/30/17 03:38 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 04/30/17 03:38 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/30/17 03:38 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/30/17 03:38 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/30/17 03:38 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/30/17 03:38 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/30/17 03:38 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/30/17 03:38 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/30/17 03:38 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/30/17 03:38 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/30/17 03:38 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/30/17 03:38 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/30/17 03:38 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/30/17 03:38 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/30/17 03:38 108-20-31.0 1
Ethylbenzene ND ug/L 04/30/17 03:38 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/30/17 03:38 87-68-31.0 1
2-Hexanone ND ug/L 04/30/17 03:38 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/30/17 03:38 99-87-61.0 1
Methylene Chloride ND ug/L 04/30/17 03:38 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/30/17 03:38 108-10-15.0 1
Methyl-tert-butyl ether 2.0 ug/L 04/30/17 03:38 1634-04-41.0 1
Naphthalene ND ug/L 04/30/17 03:38 91-20-31.0 1
Styrene ND ug/L 04/30/17 03:38 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/30/17 03:38 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/30/17 03:38 79-34-51.0 1
Tetrachloroethene ND ug/L 04/30/17 03:38 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Sample:MW-57D SPLIT Lab ID:92338704004 Collected:04/26/17 09:50 Received:04/27/17 14:21 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Toluene ND ug/L 04/30/17 03:38 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/30/17 03:38 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/30/17 03:38 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/30/17 03:38 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/30/17 03:38 79-00-51.0 1
Trichloroethene ND ug/L 04/30/17 03:38 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/30/17 03:38 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/30/17 03:38 96-18-41.0 1
Vinyl acetate ND ug/L 04/30/17 03:38 108-05-42.0 1
Vinyl chloride ND ug/L 04/30/17 03:38 75-01-41.0 1
Xylene (Total)ND ug/L 04/30/17 03:38 1330-20-71.0 1
m&p-Xylene ND ug/L 04/30/17 03:38 179601-23-12.0 1
o-Xylene ND ug/L 04/30/17 03:38 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %04/30/17 03:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %04/30/17 03:38 17060-07-070-130 1
Toluene-d8 (S)106 %04/30/17 03:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
358559
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92338704001, 92338704002, 92338704003, 92338704004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1988737
Associated Lab Samples:92338704001, 92338704002, 92338704003, 92338704004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 04/30/17 01:37
1,1,1-Trichloroethane ug/L ND 1.0 04/30/17 01:37
1,1,2,2-Tetrachloroethane ug/L ND 1.0 04/30/17 01:37
1,1,2-Trichloroethane ug/L ND 1.0 04/30/17 01:37
1,1-Dichloroethane ug/L ND 1.0 04/30/17 01:37
1,1-Dichloroethene ug/L ND 1.0 04/30/17 01:37
1,1-Dichloropropene ug/L ND 1.0 04/30/17 01:37
1,2,3-Trichlorobenzene ug/L ND 1.0 04/30/17 01:37
1,2,3-Trichloropropane ug/L ND 1.0 04/30/17 01:37
1,2,4-Trichlorobenzene ug/L ND 1.0 04/30/17 01:37
1,2-Dibromo-3-chloropropane ug/L ND 2.0 04/30/17 01:37
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/30/17 01:37
1,2-Dichlorobenzene ug/L ND 1.0 04/30/17 01:37
1,2-Dichloroethane ug/L ND 1.0 04/30/17 01:37
1,2-Dichloropropane ug/L ND 1.0 04/30/17 01:37
1,3-Dichlorobenzene ug/L ND 1.0 04/30/17 01:37
1,3-Dichloropropane ug/L ND 1.0 04/30/17 01:37
1,4-Dichlorobenzene ug/L ND 1.0 04/30/17 01:37
2,2-Dichloropropane ug/L ND 1.0 04/30/17 01:37
2-Butanone (MEK)ug/L ND 5.0 04/30/17 01:37
2-Chlorotoluene ug/L ND 1.0 04/30/17 01:37
2-Hexanone ug/L ND 5.0 04/30/17 01:37
4-Chlorotoluene ug/L ND 1.0 04/30/17 01:37
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 04/30/17 01:37
Acetone ug/L ND 25.0 04/30/17 01:37
Benzene ug/L ND 1.0 04/30/17 01:37
Bromobenzene ug/L ND 1.0 04/30/17 01:37
Bromochloromethane ug/L ND 1.0 04/30/17 01:37
Bromodichloromethane ug/L ND 1.0 04/30/17 01:37
Bromoform ug/L ND 1.0 04/30/17 01:37
Bromomethane ug/L ND 2.0 04/30/17 01:37
Carbon tetrachloride ug/L ND 1.0 04/30/17 01:37
Chlorobenzene ug/L ND 1.0 04/30/17 01:37
Chloroethane ug/L ND 1.0 04/30/17 01:37
Chloroform ug/L ND 1.0 04/30/17 01:37
Chloromethane ug/L ND 1.0 04/30/17 01:37
cis-1,2-Dichloroethene ug/L ND 1.0 04/30/17 01:37
cis-1,3-Dichloropropene ug/L ND 1.0 04/30/17 01:37
Dibromochloromethane ug/L ND 1.0 04/30/17 01:37
Dibromomethane ug/L ND 1.0 04/30/17 01:37
Dichlorodifluoromethane ug/L ND 1.0 04/30/17 01:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1988737
Associated Lab Samples:92338704001, 92338704002, 92338704003, 92338704004
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 04/30/17 01:37
Ethylbenzene ug/L ND 1.0 04/30/17 01:37
Hexachloro-1,3-butadiene ug/L ND 1.0 04/30/17 01:37
m&p-Xylene ug/L ND 2.0 04/30/17 01:37
Methyl-tert-butyl ether ug/L ND 1.0 04/30/17 01:37
Methylene Chloride ug/L ND 2.0 04/30/17 01:37
Naphthalene ug/L ND 1.0 04/30/17 01:37
o-Xylene ug/L ND 1.0 04/30/17 01:37
p-Isopropyltoluene ug/L ND 1.0 04/30/17 01:37
Styrene ug/L ND 1.0 04/30/17 01:37
Tetrachloroethene ug/L ND 1.0 04/30/17 01:37
Toluene ug/L ND 1.0 04/30/17 01:37
trans-1,2-Dichloroethene ug/L ND 1.0 04/30/17 01:37
trans-1,3-Dichloropropene ug/L ND 1.0 04/30/17 01:37
Trichloroethene ug/L ND 1.0 04/30/17 01:37
Trichlorofluoromethane ug/L ND 1.0 04/30/17 01:37
Vinyl acetate ug/L ND 2.0 04/30/17 01:37
Vinyl chloride ug/L ND 1.0 04/30/17 01:37
Xylene (Total)ug/L ND 1.0 04/30/17 01:37
1,2-Dichloroethane-d4 (S)%96 70-130 04/30/17 01:37
4-Bromofluorobenzene (S)%101 70-130 04/30/17 01:37
Toluene-d8 (S)%107 70-130 04/30/17 01:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1988738LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.750 99 70-130
1,1,1-Trichloroethane ug/L 49.050 98 70-130
1,1,2,2-Tetrachloroethane ug/L 49.350 99 70-130
1,1,2-Trichloroethane ug/L 50.250 100 70-130
1,1-Dichloroethane ug/L 47.350 95 70-130
1,1-Dichloroethene ug/L 49.450 99 70-132
1,1-Dichloropropene ug/L 51.550 103 70-130
1,2,3-Trichlorobenzene ug/L 44.950 90 70-135
1,2,3-Trichloropropane ug/L 49.950 100 70-130
1,2,4-Trichlorobenzene ug/L 44.950 90 70-134
1,2-Dibromo-3-chloropropane ug/L 48.050 96 70-130
1,2-Dibromoethane (EDB)ug/L 50.250 100 70-130
1,2-Dichlorobenzene ug/L 46.650 93 70-130
1,2-Dichloroethane ug/L 47.850 96 70-130
1,2-Dichloropropane ug/L 51.050 102 70-130
1,3-Dichlorobenzene ug/L 47.050 94 70-130
1,3-Dichloropropane ug/L 51.550 103 70-130
1,4-Dichlorobenzene ug/L 47.850 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1988738LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 41.050 82 58-145
2-Butanone (MEK)ug/L 101100 101 70-145
2-Chlorotoluene ug/L 47.450 95 70-130
2-Hexanone ug/L 96.5100 96 70-144
4-Chlorotoluene ug/L 47.750 95 70-130
4-Methyl-2-pentanone (MIBK)ug/L 100100 100 70-140
Acetone ug/L 101100 101 50-175
Benzene ug/L 49.950 100 70-130
Bromobenzene ug/L 47.650 95 70-130
Bromochloromethane ug/L 49.650 99 70-130
Bromodichloromethane ug/L 49.450 99 70-130
Bromoform ug/L 42.150 84 70-130
Bromomethane ug/L 58.150 116 54-130
Carbon tetrachloride ug/L 47.550 95 70-132
Chlorobenzene ug/L 47.950 96 70-130
Chloroethane ug/L 46.350 93 64-134
Chloroform ug/L 48.050 96 70-130
Chloromethane ug/L 55.150 110 64-130
cis-1,2-Dichloroethene ug/L 48.650 97 70-131
cis-1,3-Dichloropropene ug/L 51.350 103 70-130
Dibromochloromethane ug/L 51.250 102 70-130
Dibromomethane ug/L 47.050 94 70-131
Dichlorodifluoromethane ug/L 42.350 85 56-130
Diisopropyl ether ug/L 51.350 103 70-130
Ethylbenzene ug/L 48.050 96 70-130
Hexachloro-1,3-butadiene ug/L 42.450 85 70-130
m&p-Xylene ug/L 95.3100 95 70-130
Methyl-tert-butyl ether ug/L 54.550 109 70-130
Methylene Chloride ug/L 51.750 103 63-130
Naphthalene ug/L 47.550 95 70-138
o-Xylene ug/L 47.650 95 70-130
p-Isopropyltoluene ug/L 47.250 94 70-130
Styrene ug/L 47.750 95 70-130
Tetrachloroethene ug/L 46.750 93 70-130
Toluene ug/L 48.850 98 70-130
trans-1,2-Dichloroethene ug/L 48.250 96 70-130
trans-1,3-Dichloropropene ug/L 49.950 100 70-132
Trichloroethene ug/L 50.250 100 70-130
Trichlorofluoromethane ug/L 49.250 98 62-133
Vinyl acetate ug/L 110100 110 66-157
Vinyl chloride ug/L 46.650 93 50-150
Xylene (Total)ug/L 143150 95 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1988739MATRIX SPIKE SAMPLE:
MSSpike
Result
92338704001
1,1,1,2-Tetrachloroethane ug/L 20.420 102 70-130ND
1,1,1-Trichloroethane ug/L 22.720 113 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,2-Trichloroethane ug/L 21.820 109 70-130ND
1,1-Dichloroethane ug/L 22.620 113 70-130ND
1,1-Dichloroethene ug/L 27.820 139 70-166ND
1,1-Dichloropropene ug/L 24.520 123 70-130ND
1,2,3-Trichlorobenzene ug/L 17.420 87 70-130ND
1,2,3-Trichloropropane ug/L 19.420 97 70-130ND
1,2,4-Trichlorobenzene ug/L 17.820 89 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.320 92 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.720 99 70-130ND
1,2-Dichlorobenzene ug/L 19.920 99 70-130ND
1,2-Dichloroethane ug/L 21.920 110 70-130ND
1,2-Dichloropropane ug/L 22.320 111 70-130ND
1,3-Dichlorobenzene ug/L 19.920 99 70-130ND
1,3-Dichloropropane ug/L 20.320 102 70-130ND
1,4-Dichlorobenzene ug/L 20.220 101 70-130ND
2,2-Dichloropropane ug/L 16.420 82 70-130ND
2-Butanone (MEK)ug/L 44.340 111 70-130ND
2-Chlorotoluene ug/L 20.220 101 70-130ND
2-Hexanone ug/L 39.340 98 70-130ND
4-Chlorotoluene ug/L 20.020 100 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.740 107 70-130ND
Acetone ug/L 45.340 102 70-130ND
Benzene ug/L 22.920 114 70-148ND
Bromobenzene ug/L 20.120 100 70-130ND
Bromochloromethane ug/L 23.520 117 70-130ND
Bromodichloromethane ug/L 22.320 112 70-130ND
Bromoform ug/L 17.720 89 70-130ND
Bromomethane ug/L 19.020 95 70-130ND
Carbon tetrachloride ug/L 21.620 108 70-130ND
Chlorobenzene ug/L 21.220 106 70-146ND
Chloroethane ug/L 24.620 123 70-130ND
Chloroform ug/L 22.220 111 70-130ND
Chloromethane ug/L 25.420 127 70-130ND
cis-1,2-Dichloroethene ug/L 23.020 115 70-130ND
cis-1,3-Dichloropropene ug/L 24.120 121 70-130ND
Dibromochloromethane ug/L 19.820 99 70-130ND
Dibromomethane ug/L 21.220 106 70-130ND
Dichlorodifluoromethane ug/L 22.520 113 70-130ND
Diisopropyl ether ug/L 22.120 111 70-130ND
Ethylbenzene ug/L 21.320 106 70-130ND
Hexachloro-1,3-butadiene ug/L 16.220 81 70-130ND
m&p-Xylene ug/L 42.040 105 70-130ND
Methyl-tert-butyl ether ug/L 22.120 110 70-130ND
Methylene Chloride ug/L 22.820 114 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1988739MATRIX SPIKE SAMPLE:
MSSpike
Result
92338704001
Naphthalene ug/L 18.020 90 70-130ND
o-Xylene ug/L 20.720 103 70-130ND
p-Isopropyltoluene ug/L 18.920 95 70-130ND
Styrene ug/L 20.820 104 70-130ND
Tetrachloroethene ug/L 22.820 114 70-130ND
Toluene ug/L 27.920 140 70-155ND
trans-1,2-Dichloroethene ug/L 23.220 116 70-130ND
trans-1,3-Dichloropropene ug/L 19.920 100 70-130ND
Trichloroethene ug/L 21.820 109 69-151ND
Trichlorofluoromethane ug/L 25.520 128 70-130ND
Vinyl acetate ug/L 40.840 102 70-130ND
Vinyl chloride ug/L 24.220 121 70-130ND
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%110 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92338704002
1988740SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L 23.1JND
Benzene ug/L 1.4 31.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92338704002
1988740SAMPLE DUPLICATE:
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L 2.7 12.7
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L 3.1 43.3
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%98 396
4-Bromofluorobenzene (S)%101 0102
Toluene-d8 (S)%105 0106
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92338704
HIGHWAY 49 LANDFILL
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92338704001 358559MW-55 SPLIT EPA 8260
92338704002 358559MW-56 SPLIT EPA 8260
92338704003 358559MW-57 SPLIT EPA 8260
92338704004 358559MW-57D SPLIT EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2017 03:49 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 23
Page 21 of 23
Page 22 of 23
Page 23 of 23
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
TestAmerica Job ID: 500-129772-1
Client Project/Site: NC Highway 49
Revision: 1
For:
Civil & Environmental Consultants Inc
1900 Center Park Drive
Suite A
Charlotte, North Carolina 28217
Attn: Phillip Pressley
Authorized for release by:
7/7/2017 3:52:14 PM
Robin Kintz, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
TestAmerica Job ID: 500-129772-1
Page 2 of 25 TestAmerica Chicago7/7/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
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Case Narrative
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-129772-1
Project/Site: NC Highway 49
Job ID: 500-129772-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-129772-1
Comments
The report was revised to separate out samples on the chain of custody MW-8 and MW-56, MW-57, and MW-57D into separate reports.
No additional comments.
Receipt
The samples were received on 6/17/2017 10:20 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 2.0º C.
GC/MS VOA
Method(s) 8260B: The laboratory control sample (LCS) for batch 390457 recovered outside control limits for Bromomethane. This analyte
was biased high in the LCS and was not detected in the associated samples: MW-56 (500-129772-2) ; therefore, the data has been
reported.
Method(s) 8260B: The samples with positive detects for Vinyl Chloride in the presence of freon 151 were re-collected and the lab
re-analyzed these on Instrument 25. The lab had determined this instrument to be "inert" to the degradation of freon 151 to Vinyl chloride.
The results for Vinyl Chloride were significantly lower from the original samples. The lab analyzed the Freon 151 standard on this
instrument before and after these samples were analyzed to confirm vinyl chloride was not detected and the instrument continues to be
"inert". The following samples were re-collected and analyzed: MW-56 (500-129772-2), MW-57 (500-129772-3) and MW-57D
(500-129772-4).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica ChicagoPage 3 of 25 7/7/2017
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Detection Summary
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Client Sample ID: MW-56 Lab Sample ID: 500-129772-2
1,2-Dichloroethane
RL
1.0 ug/L
MDL
0.39
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.51 8260B
Benzene 0.50 ug/L0.15 Total/NA11.3 8260B
Chloroethane 1.0 ug/L0.51 Total/NA11.0 8260B
cis-1,2-Dichloroethene 1.0 ug/L0.41 Total/NA15.2 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA19.6 8260B
Client Sample ID: MW-57 Lab Sample ID: 500-129772-3
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.70 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA10.59 8260B
Client Sample ID: MW-57D Lab Sample ID: 500-129772-4
Acetone
RL
5.0 ug/L
MDL
1.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA16.6 8260B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
Page 4 of 25 7/7/2017
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Method Summary
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL CHI
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Sample Summary
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-129772-2 MW-56 Water 06/16/17 12:45 06/17/17 10:20
500-129772-3 MW-57 Water 06/16/17 12:45 06/17/17 10:20
500-129772-4 MW-57D Water 06/16/17 12:36 06/17/17 10:20
TestAmerica Chicago
Page 6 of 25 7/7/2017
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Client Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Lab Sample ID: 500-129772-2Client Sample ID: MW-56
Matrix: WaterDate Collected: 06/16/17 12:45
Date Received: 06/17/17 10:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 06/22/17 12:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 06/22/17 12:54 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 06/22/17 12:54 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 06/22/17 12:54 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 06/22/17 12:54 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 06/22/17 12:54 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 06/22/17 12:54 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 06/22/17 12:54 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 06/22/17 12:54 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 06/22/17 12:54 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 06/22/17 12:54 11,2-Dichloroethane 0.51 J
1.0 0.43 ug/L 06/22/17 12:54 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 06/22/17 12:54 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 06/22/17 12:54 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 06/22/17 12:54 12-Hexanone <5.0
5.0 2.2 ug/L 06/22/17 12:54 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 06/22/17 12:54 1Acetone<5.0
20 4.5 ug/L 06/22/17 12:54 1Acrylonitrile<20
0.50 0.15 ug/L 06/22/17 12:54 1Benzene1.3
1.0 0.43 ug/L 06/22/17 12:54 1Bromochloromethane<1.0
1.0 0.37 ug/L 06/22/17 12:54 1Bromodichloromethane<1.0
1.0 0.48 ug/L 06/22/17 12:54 1Bromoform<1.0
2.0 0.80 ug/L 06/22/17 12:54 1Bromomethane<2.0 *
2.0 0.45 ug/L 06/22/17 12:54 1Carbon disulfide <2.0
1.0 0.38 ug/L 06/22/17 12:54 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 06/22/17 12:54 1Chlorobenzene<1.0
1.0 0.51 ug/L 06/22/17 12:54 1Chloroethane1.0
2.0 0.37 ug/L 06/22/17 12:54 1Chloroform<2.0
1.0 0.32 ug/L 06/22/17 12:54 1Chloromethane<1.0
1.0 0.41 ug/L 06/22/17 12:54 1cis-1,2-Dichloroethene 5.2
1.0 0.42 ug/L 06/22/17 12:54 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 06/22/17 12:54 1Dibromochloromethane<1.0
1.0 0.27 ug/L 06/22/17 12:54 1Dibromomethane<1.0
0.50 0.18 ug/L 06/22/17 12:54 1Ethylbenzene<0.50
2.5 0.66 ug/L 06/22/17 12:54 1Iodomethane<2.5
5.0 1.6 ug/L 06/22/17 12:54 1Methylene Chloride <5.0
1.0 0.39 ug/L 06/22/17 12:54 1Styrene<1.0
1.0 0.37 ug/L 06/22/17 12:54 1Tetrachloroethene<1.0
10 1.9 ug/L 06/22/17 12:54 1Tetrahydrofuran<10
0.50 0.15 ug/L 06/22/17 12:54 1Toluene<0.50
1.0 0.35 ug/L 06/22/17 12:54 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 06/22/17 12:54 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 06/22/17 12:54 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 06/22/17 12:54 1Trichloroethene<0.50
1.0 0.43 ug/L 06/22/17 12:54 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 06/22/17 12:54 1Vinyl acetate <2.0
0.50 0.20 ug/L 06/22/17 12:54 1Vinyl chloride 9.6
1.0 0.22 ug/L 06/22/17 12:54 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Lab Sample ID: 500-129772-2Client Sample ID: MW-56
Matrix: WaterDate Collected: 06/16/17 12:45
Date Received: 06/17/17 10:20
1,2-Dichloroethane-d4 (Surr)105 75-126 06/22/17 12:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 06/22/17 12:54 172-124
Dibromofluoromethane 96 06/22/17 12:54 175-120
Toluene-d8 (Surr)97 06/22/17 12:54 175-120
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Client Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Lab Sample ID: 500-129772-3Client Sample ID: MW-57
Matrix: WaterDate Collected: 06/16/17 12:45
Date Received: 06/17/17 10:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 06/20/17 01:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 06/20/17 01:15 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 06/20/17 01:15 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 06/20/17 01:15 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 06/20/17 01:15 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 06/20/17 01:15 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 06/20/17 01:15 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 06/20/17 01:15 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 06/20/17 01:15 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 06/20/17 01:15 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 06/20/17 01:15 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 06/20/17 01:15 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 06/20/17 01:15 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 06/20/17 01:15 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 06/20/17 01:15 12-Hexanone <5.0
5.0 2.2 ug/L 06/20/17 01:15 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 06/20/17 01:15 1Acetone<5.0
20 4.5 ug/L 06/20/17 01:15 1Acrylonitrile<20
0.50 0.15 ug/L 06/20/17 01:15 1Benzene0.70
1.0 0.43 ug/L 06/20/17 01:15 1Bromochloromethane<1.0
1.0 0.37 ug/L 06/20/17 01:15 1Bromodichloromethane<1.0
1.0 0.48 ug/L 06/20/17 01:15 1Bromoform<1.0
2.0 0.80 ug/L 06/20/17 01:15 1Bromomethane<2.0
2.0 0.45 ug/L 06/20/17 01:15 1Carbon disulfide <2.0
1.0 0.38 ug/L 06/20/17 01:15 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 06/20/17 01:15 1Chlorobenzene<1.0
1.0 0.51 ug/L 06/20/17 01:15 1Chloroethane<1.0
2.0 0.37 ug/L 06/20/17 01:15 1Chloroform<2.0
1.0 0.32 ug/L 06/20/17 01:15 1Chloromethane<1.0
1.0 0.41 ug/L 06/20/17 01:15 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 06/20/17 01:15 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 06/20/17 01:15 1Dibromochloromethane<1.0
1.0 0.27 ug/L 06/20/17 01:15 1Dibromomethane<1.0
0.50 0.18 ug/L 06/20/17 01:15 1Ethylbenzene<0.50
2.5 0.66 ug/L 06/20/17 01:15 1Iodomethane<2.5
5.0 1.6 ug/L 06/20/17 01:15 1Methylene Chloride <5.0
1.0 0.39 ug/L 06/20/17 01:15 1Styrene<1.0
1.0 0.37 ug/L 06/20/17 01:15 1Tetrachloroethene<1.0
10 1.9 ug/L 06/20/17 01:15 1Tetrahydrofuran<10
0.50 0.15 ug/L 06/20/17 01:15 1Toluene<0.50
1.0 0.35 ug/L 06/20/17 01:15 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 06/20/17 01:15 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 06/20/17 01:15 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 06/20/17 01:15 1Trichloroethene<0.50
1.0 0.43 ug/L 06/20/17 01:15 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 06/20/17 01:15 1Vinyl acetate <2.0
0.50 0.20 ug/L 06/20/17 01:15 1Vinyl chloride 0.59
1.0 0.22 ug/L 06/20/17 01:15 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Lab Sample ID: 500-129772-3Client Sample ID: MW-57
Matrix: WaterDate Collected: 06/16/17 12:45
Date Received: 06/17/17 10:20
1,2-Dichloroethane-d4 (Surr)102 75-126 06/20/17 01:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)88 06/20/17 01:15 172-124
Dibromofluoromethane 107 06/20/17 01:15 175-120
Toluene-d8 (Surr)92 06/20/17 01:15 175-120
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Client Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Lab Sample ID: 500-129772-4Client Sample ID: MW-57D
Matrix: WaterDate Collected: 06/16/17 12:36
Date Received: 06/17/17 10:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 06/21/17 14:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 06/21/17 14:21 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 06/21/17 14:21 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 06/21/17 14:21 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 06/21/17 14:21 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 06/21/17 14:21 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 06/21/17 14:21 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 06/21/17 14:21 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 06/21/17 14:21 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 06/21/17 14:21 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 06/21/17 14:21 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 06/21/17 14:21 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 06/21/17 14:21 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 06/21/17 14:21 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 06/21/17 14:21 12-Hexanone <5.0
5.0 2.2 ug/L 06/21/17 14:21 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 06/21/17 14:21 1Acetone6.6
20 4.5 ug/L 06/21/17 14:21 1Acrylonitrile<20
0.50 0.15 ug/L 06/21/17 14:21 1Benzene<0.50
1.0 0.43 ug/L 06/21/17 14:21 1Bromochloromethane<1.0
1.0 0.37 ug/L 06/21/17 14:21 1Bromodichloromethane<1.0
1.0 0.48 ug/L 06/21/17 14:21 1Bromoform<1.0
2.0 0.80 ug/L 06/21/17 14:21 1Bromomethane<2.0
2.0 0.45 ug/L 06/21/17 14:21 1Carbon disulfide <2.0
1.0 0.38 ug/L 06/21/17 14:21 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 06/21/17 14:21 1Chlorobenzene<1.0
1.0 0.51 ug/L 06/21/17 14:21 1Chloroethane<1.0
2.0 0.37 ug/L 06/21/17 14:21 1Chloroform<2.0
1.0 0.32 ug/L 06/21/17 14:21 1Chloromethane<1.0
1.0 0.41 ug/L 06/21/17 14:21 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 06/21/17 14:21 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 06/21/17 14:21 1Dibromochloromethane<1.0
1.0 0.27 ug/L 06/21/17 14:21 1Dibromomethane<1.0
0.50 0.18 ug/L 06/21/17 14:21 1Ethylbenzene<0.50
2.5 0.66 ug/L 06/21/17 14:21 1Iodomethane<2.5
5.0 1.6 ug/L 06/21/17 14:21 1Methylene Chloride <5.0
1.0 0.39 ug/L 06/21/17 14:21 1Styrene<1.0
1.0 0.37 ug/L 06/21/17 14:21 1Tetrachloroethene<1.0
10 1.9 ug/L 06/21/17 14:21 1Tetrahydrofuran<10
0.50 0.15 ug/L 06/21/17 14:21 1Toluene<0.50
1.0 0.35 ug/L 06/21/17 14:21 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 06/21/17 14:21 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 06/21/17 14:21 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 06/21/17 14:21 1Trichloroethene<0.50
1.0 0.43 ug/L 06/21/17 14:21 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 06/21/17 14:21 1Vinyl acetate <2.0
0.50 0.20 ug/L 06/21/17 14:21 1Vinyl chloride <0.50
1.0 0.22 ug/L 06/21/17 14:21 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Lab Sample ID: 500-129772-4Client Sample ID: MW-57D
Matrix: WaterDate Collected: 06/16/17 12:36
Date Received: 06/17/17 10:20
1,2-Dichloroethane-d4 (Surr)105 75-126 06/21/17 14:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)99 06/21/17 14:21 172-124
Dibromofluoromethane 95 06/21/17 14:21 175-120
Toluene-d8 (Surr)98 06/21/17 14:21 175-120
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Definitions/Glossary
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
*LCS or LCSD is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association Summary
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
GC/MS VOA
Analysis Batch: 389940
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-129772-3 MW-57 Total/NA
Analysis Batch: 390300
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-129772-4 MW-57D Total/NA
Water 8260BMB 500-390300/6 Method Blank Total/NA
Water 8260BLCS 500-390300/4 Lab Control Sample Total/NA
Analysis Batch: 390457
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-129772-2 MW-56 Total/NA
Water 8260BMB 500-390457/6 Method Blank Total/NA
Water 8260BLCS 500-390457/4 Lab Control Sample Total/NA
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Surrogate Summary
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (75-126)(72-124)(75-120)(75-120)
12DCE BFB DBFM TOL
105 97 96 97500-129772-2
Percent Surrogate Recovery (Acceptance Limits)
MW-56
102 88 107 92500-129772-3 MW-57
105 99 95 98500-129772-4 MW-57D
102 98 94 97LCS 500-390300/4 Lab Control Sample
99 100 93 101LCS 500-390457/4 Lab Control Sample
104 99 94 95MB 500-390300/6 Method Blank
109 98 98 93MB 500-390457/6 Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
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QC Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-390300/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390300
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 06/21/17 12:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.381.0 ug/L 06/21/17 12:58 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 06/21/17 12:58 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 06/21/17 12:58 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 06/21/17 12:58 11,1-Dichloroethane
<1.0 0.391.0 ug/L 06/21/17 12:58 11,1-Dichloroethene
<1.0 0.411.0 ug/L 06/21/17 12:58 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 06/21/17 12:58 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 06/21/17 12:58 11,2-Dibromoethane
<1.0 0.331.0 ug/L 06/21/17 12:58 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 06/21/17 12:58 11,2-Dichloroethane
<1.0 0.431.0 ug/L 06/21/17 12:58 11,2-Dichloropropane
<1.0 0.361.0 ug/L 06/21/17 12:58 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 06/21/17 12:58 12-Butanone (MEK)
<5.0 1.65.0 ug/L 06/21/17 12:58 12-Hexanone
<5.0 2.25.0 ug/L 06/21/17 12:58 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 06/21/17 12:58 1Acetone
<20 4.520 ug/L 06/21/17 12:58 1Acrylonitrile
<0.50 0.150.50 ug/L 06/21/17 12:58 1Benzene
<1.0 0.431.0 ug/L 06/21/17 12:58 1Bromochloromethane
<1.0 0.371.0 ug/L 06/21/17 12:58 1Bromodichloromethane
<1.0 0.481.0 ug/L 06/21/17 12:58 1Bromoform
<2.0 0.802.0 ug/L 06/21/17 12:58 1Bromomethane
<2.0 0.452.0 ug/L 06/21/17 12:58 1Carbon disulfide
<1.0 0.381.0 ug/L 06/21/17 12:58 1Carbon tetrachloride
<1.0 0.391.0 ug/L 06/21/17 12:58 1Chlorobenzene
<1.0 0.511.0 ug/L 06/21/17 12:58 1Chloroethane
<2.0 0.372.0 ug/L 06/21/17 12:58 1Chloroform
<1.0 0.321.0 ug/L 06/21/17 12:58 1Chloromethane
<1.0 0.411.0 ug/L 06/21/17 12:58 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 06/21/17 12:58 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 06/21/17 12:58 1Dibromochloromethane
<1.0 0.271.0 ug/L 06/21/17 12:58 1Dibromomethane
<0.50 0.180.50 ug/L 06/21/17 12:58 1Ethylbenzene
<2.5 0.662.5 ug/L 06/21/17 12:58 1Iodomethane
<5.0 1.65.0 ug/L 06/21/17 12:58 1Methylene Chloride
<1.0 0.391.0 ug/L 06/21/17 12:58 1Styrene
<1.0 0.371.0 ug/L 06/21/17 12:58 1Tetrachloroethene
<10 1.910 ug/L 06/21/17 12:58 1Tetrahydrofuran
<0.50 0.150.50 ug/L 06/21/17 12:58 1Toluene
<1.0 0.351.0 ug/L 06/21/17 12:58 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 06/21/17 12:58 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 06/21/17 12:58 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 06/21/17 12:58 1Trichloroethene
<1.0 0.431.0 ug/L 06/21/17 12:58 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 06/21/17 12:58 1Vinyl acetate
<0.50 0.200.50 ug/L 06/21/17 12:58 1Vinyl chloride
<1.0 0.221.0 ug/L 06/21/17 12:58 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
1,2-Dichloroethane-d4 (Surr)104 75-126 06/21/17 12:58 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 06/21/17 12:58 14-Bromofluorobenzene (Surr)72-124
94 06/21/17 12:58 1Dibromofluoromethane75-120
95 06/21/17 12:58 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-390300/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390300
1,1,1,2-Tetrachloroethane 50.0 44.9 ug/L 90 70-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 42.6 ug/L 85 70-125
1,1,2,2-Tetrachloroethane 50.0 50.2 ug/L 100 67-127
1,1,2-Trichloroethane 50.0 45.5 ug/L 91 70-122
1,1-Dichloroethane 50.0 48.7 ug/L 97 70-125
1,1-Dichloroethene 50.0 42.0 ug/L 84 67-122
1,2,3-Trichloropropane 50.0 46.9 ug/L 94 50-133
1,2-Dibromo-3-Chloropropane 50.0 44.6 ug/L 89 56-123
1,2-Dibromoethane 50.0 46.9 ug/L 94 70-125
1,2-Dichlorobenzene 50.0 44.0 ug/L 88 70-125
1,2-Dichloroethane 50.0 46.1 ug/L 92 68-127
1,2-Dichloropropane 50.0 53.4 ug/L 107 67-130
1,4-Dichlorobenzene 50.0 44.1 ug/L 88 70-120
2-Butanone (MEK)50.0 48.1 ug/L 96 53-141
2-Hexanone 50.0 50.5 ug/L 101 56-135
4-Methyl-2-pentanone (MIBK)50.0 50.5 ug/L 101 56-133
Acetone 50.0 50.4 ug/L 101 40-143
Acrylonitrile 500 524 ug/L 105 67-140
Benzene 50.0 43.3 ug/L 87 70-120
Bromochloromethane 50.0 44.4 ug/L 89 65-122
Bromodichloromethane 50.0 43.7 ug/L 87 69-120
Bromoform 50.0 48.4 ug/L 97 56-132
Bromomethane 50.0 61.0 ug/L 122 40-130
Carbon disulfide 50.0 41.9 ug/L 84 66-120
Carbon tetrachloride 50.0 41.9 ug/L 84 65-122
Chlorobenzene 50.0 43.6 ug/L 87 70-120
Chloroethane 50.0 47.0 ug/L 94 45-127
Chloroform 50.0 43.2 ug/L 86 70-120
Chloromethane 50.0 41.5 ug/L 83 54-147
cis-1,2-Dichloroethene 50.0 43.2 ug/L 86 70-125
cis-1,3-Dichloropropene 50.0 45.1 ug/L 90 64-127
Dibromochloromethane 50.0 44.9 ug/L 90 68-125
Dibromomethane 50.0 45.8 ug/L 92 70-120
Ethylbenzene 50.0 43.6 ug/L 87 70-120
Iodomethane 50.0 32.6 ug/L 65 61-136
Methylene Chloride 50.0 42.4 ug/L 85 69-125
Styrene 50.0 44.3 ug/L 89 70-120
Tetrachloroethene 50.0 42.9 ug/L 86 70-128
Tetrahydrofuran 100 81.6 ug/L 82 59-139
Toluene 50.0 42.6 ug/L 85 70-125
trans-1,2-Dichloroethene 50.0 42.6 ug/L 85 70-125
trans-1,3-Dichloropropene 50.0 45.2 ug/L 90 62-128
trans-1,4-Dichloro-2-butene 50.0 41.1 ug/L 82 60-130
Trichloroethene 50.0 43.0 ug/L 86 70-125
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QC Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-390300/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390300
Trichlorofluoromethane 50.0 41.0 ug/L 82 70-126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 50.0 42.8 ug/L 86 43-133
Vinyl chloride 50.0 49.1 ug/L 98 64-126
Xylenes, Total 100 85.2 ug/L 85 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)72 -124
94Dibromofluoromethane 75 -120
97Toluene-d8 (Surr)75 -120
Client Sample ID: Method BlankLab Sample ID: MB 500-390457/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390457
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 06/22/17 12:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.381.0 ug/L 06/22/17 12:24 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 06/22/17 12:24 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 06/22/17 12:24 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 06/22/17 12:24 11,1-Dichloroethane
<1.0 0.391.0 ug/L 06/22/17 12:24 11,1-Dichloroethene
<1.0 0.411.0 ug/L 06/22/17 12:24 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 06/22/17 12:24 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 06/22/17 12:24 11,2-Dibromoethane
<1.0 0.331.0 ug/L 06/22/17 12:24 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 06/22/17 12:24 11,2-Dichloroethane
<1.0 0.431.0 ug/L 06/22/17 12:24 11,2-Dichloropropane
<1.0 0.361.0 ug/L 06/22/17 12:24 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 06/22/17 12:24 12-Butanone (MEK)
<5.0 1.65.0 ug/L 06/22/17 12:24 12-Hexanone
<5.0 2.25.0 ug/L 06/22/17 12:24 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 06/22/17 12:24 1Acetone
<20 4.520 ug/L 06/22/17 12:24 1Acrylonitrile
<0.50 0.150.50 ug/L 06/22/17 12:24 1Benzene
<1.0 0.431.0 ug/L 06/22/17 12:24 1Bromochloromethane
<1.0 0.371.0 ug/L 06/22/17 12:24 1Bromodichloromethane
<1.0 0.481.0 ug/L 06/22/17 12:24 1Bromoform
<2.0 0.802.0 ug/L 06/22/17 12:24 1Bromomethane
<2.0 0.452.0 ug/L 06/22/17 12:24 1Carbon disulfide
<1.0 0.381.0 ug/L 06/22/17 12:24 1Carbon tetrachloride
<1.0 0.391.0 ug/L 06/22/17 12:24 1Chlorobenzene
<1.0 0.511.0 ug/L 06/22/17 12:24 1Chloroethane
<2.0 0.372.0 ug/L 06/22/17 12:24 1Chloroform
<1.0 0.321.0 ug/L 06/22/17 12:24 1Chloromethane
<1.0 0.411.0 ug/L 06/22/17 12:24 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 06/22/17 12:24 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 06/22/17 12:24 1Dibromochloromethane
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QC Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-390457/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390457
RL MDL
Dibromomethane <1.0 1.0 0.27 ug/L 06/22/17 12:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.50 0.180.50 ug/L 06/22/17 12:24 1Ethylbenzene
<2.5 0.662.5 ug/L 06/22/17 12:24 1Iodomethane
<5.0 1.65.0 ug/L 06/22/17 12:24 1Methylene Chloride
<1.0 0.391.0 ug/L 06/22/17 12:24 1Styrene
<1.0 0.371.0 ug/L 06/22/17 12:24 1Tetrachloroethene
<10 1.910 ug/L 06/22/17 12:24 1Tetrahydrofuran
<0.50 0.150.50 ug/L 06/22/17 12:24 1Toluene
<1.0 0.351.0 ug/L 06/22/17 12:24 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 06/22/17 12:24 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 06/22/17 12:24 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 06/22/17 12:24 1Trichloroethene
<1.0 0.431.0 ug/L 06/22/17 12:24 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 06/22/17 12:24 1Vinyl acetate
<0.50 0.200.50 ug/L 06/22/17 12:24 1Vinyl chloride
<1.0 0.221.0 ug/L 06/22/17 12:24 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)109 75-126 06/22/17 12:24 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
98 06/22/17 12:24 14-Bromofluorobenzene (Surr)72-124
98 06/22/17 12:24 1Dibromofluoromethane75-120
93 06/22/17 12:24 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-390457/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390457
1,1,1,2-Tetrachloroethane 50.0 49.3 ug/L 99 70-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 46.7 ug/L 93 70-125
1,1,2,2-Tetrachloroethane 50.0 55.3 ug/L 111 67-127
1,1,2-Trichloroethane 50.0 50.8 ug/L 102 70-122
1,1-Dichloroethane 50.0 54.9 ug/L 110 70-125
1,1-Dichloroethene 50.0 49.6 ug/L 99 67-122
1,2,3-Trichloropropane 50.0 52.0 ug/L 104 50-133
1,2-Dibromo-3-Chloropropane 50.0 46.9 ug/L 94 56-123
1,2-Dibromoethane 50.0 50.5 ug/L 101 70-125
1,2-Dichlorobenzene 50.0 49.5 ug/L 99 70-125
1,2-Dichloroethane 50.0 49.5 ug/L 99 68-127
1,2-Dichloropropane 50.0 58.2 ug/L 116 67-130
1,4-Dichlorobenzene 50.0 49.1 ug/L 98 70-120
2-Butanone (MEK)50.0 39.8 ug/L 80 53-141
2-Hexanone 50.0 43.8 ug/L 88 56-135
4-Methyl-2-pentanone (MIBK)50.0 44.5 ug/L 89 56-133
Acetone 50.0 43.2 ug/L 86 40-143
Acrylonitrile 500 575 ug/L 115 67-140
Benzene 50.0 48.6 ug/L 97 70-120
Bromochloromethane 50.0 47.7 ug/L 95 65-122
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QC Sample Results
TestAmerica Job ID: 500-129772-1Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 49
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-390457/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390457
Bromodichloromethane 50.0 48.1 ug/L 96 69-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Bromoform 50.0 51.3 ug/L 103 56-132
Bromomethane 50.0 68.0 *ug/L 136 40-130
Carbon disulfide 50.0 52.5 ug/L 105 66-120
Carbon tetrachloride 50.0 46.2 ug/L 92 65-122
Chlorobenzene 50.0 49.1 ug/L 98 70-120
Chloroethane 50.0 56.1 ug/L 112 45-127
Chloroform 50.0 48.4 ug/L 97 70-120
Chloromethane 50.0 53.0 ug/L 106 54-147
cis-1,2-Dichloroethene 50.0 48.0 ug/L 96 70-125
cis-1,3-Dichloropropene 50.0 49.4 ug/L 99 64-127
Dibromochloromethane 50.0 49.4 ug/L 99 68-125
Dibromomethane 50.0 48.7 ug/L 97 70-120
Ethylbenzene 50.0 48.1 ug/L 96 70-120
Iodomethane 50.0 37.8 ug/L 76 61-136
Methylene Chloride 50.0 47.1 ug/L 94 69-125
Styrene 50.0 48.7 ug/L 97 70-120
Tetrachloroethene 50.0 47.7 ug/L 95 70-128
Tetrahydrofuran 100 90.4 ug/L 90 59-139
Toluene 50.0 48.7 ug/L 97 70-125
trans-1,2-Dichloroethene 50.0 48.5 ug/L 97 70-125
trans-1,3-Dichloropropene 50.0 49.5 ug/L 99 62-128
trans-1,4-Dichloro-2-butene 50.0 46.7 ug/L 93 60-130
Trichloroethene 50.0 47.5 ug/L 95 70-125
Trichlorofluoromethane 50.0 48.8 ug/L 98 70-126
Vinyl acetate 50.0 38.7 ug/L 77 43-133
Vinyl chloride 50.0 59.1 ug/L 118 64-126
Xylenes, Total 100 96.0 ug/L 96 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
1004-Bromofluorobenzene (Surr)72 -124
93Dibromofluoromethane 75 -120
101Toluene-d8 (Surr)75 -120
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-129772-1
Project/Site: NC Highway 49
Client Sample ID: MW-56 Lab Sample ID: 500-129772-2
Matrix: WaterDate Collected: 06/16/17 12:45
Date Received: 06/17/17 10:20
Analysis 8260B 06/22/17 12:54 PJH1390457 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-57 Lab Sample ID: 500-129772-3
Matrix: WaterDate Collected: 06/16/17 12:45
Date Received: 06/17/17 10:20
Analysis 8260B 06/20/17 01:15 EMA1389940 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-57D Lab Sample ID: 500-129772-4
Matrix: WaterDate Collected: 06/16/17 12:36
Date Received: 06/17/17 10:20
Analysis 8260B 06/21/17 14:21 EMA1390300 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-129772-1
Project/Site: NC Highway 49
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)2914State Program 12-31-17
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
8260B Water trans-1,4-Dichloro-2-butene
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 500-129772-1
Login Number: 129772
Question Answer Comment
Creator: Sanchez, Ariel M
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
FalseContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Refer to Job Narrative for details.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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APPENDIX C

August 2, 2017

Ms. Jackie Drummond Compliance Hydrogeologist Division of Waste Management - Solid Waste Section North Carolina Department of Environmental Quality
Asheville Regional Office
2090 US Highway 70 Swannanoa, NC 28778 Dear Jackie:

Subject: Highway 49 C&D Landfill – Permit 13-06 Greenway Waste Solutions of Harrisburg, LLC Demonstration Letter on Background Metals in Groundwater Samples CEC Project 111-370.0002

Per 15A NCAC 13B .0544 (b) (1) (I), Civil & Environmental Consultants, Inc. (CEC) on behalf of Greenway Waste Solutions of Harrisburg, LLC, is submitting this Demonstration Letter to establish that a natural variation in groundwater quality has caused contamination at the aforementioned facility. Certain metals have been detected in the groundwater that is sampled and analyzed per the
approved Groundwater Monitoring Plan. These metals are regularly detected at concentrations
exceeding their respective cleanup standards as published in 15A NCAC 02L .0202 (Standards), or published Interim Maximum Contaminant Levels (IMCL). This letter presents:
• Statistical analysis used to determine metals of concern;
• Condensed historical information on the detection of metals in groundwater at the landfill;
• Information on the presence of reducing groundwater conditions and its impact on metal
solubility and mobility;
• Summary of published information on the background presence of selected metals in groundwater and stream sediments.
Attachments include a site plan depicting groundwater monitoring well locations, selected field data
sheets on the latest sampling event; and figures on published groundwater and/or stream sediment concentration data for selected metals.
Ms. Jackie Drummond - NCDEQ
CEC Project 111-370.0002
Page 2 August 2, 2017

Statistical Analyses and Metals of Concern
Semi-annual groundwater monitoring has been performed at the landfill for an extended period. CEC tabulated and statistically analyzed historical groundwater data for the Facility for the period 2007 thru 2017 to determine metals of concern. The criteria for selection of metals of concern are:
• Any constituent must have a minimum of two detections within 2007 and 2017 above
method detection limit (MDL);
• The geometric mean (GM) of the data for each constituent is then determined using only
values greater than MDL;
• A comparison is made between the GM against the Standard or IMCL (Standard/IMCL);
and
• If the comparison indicates the GM is greater than the Standard/IMCL, then the constituent
is a metal of concern.

Using the monitored wells, the analyses yielded six metals of concern:

1) Chromium (10 µg/L) – GM of 20.4 µg/L, 2 samples above MDL;
2) Cobalt (1 µg/L) – GM of 17.6 µg/L, 30 samples above MDL;
3) Iron (300 µg/L) – GM of 1,908 µg/L, 5 samples above the MDL;
4) Manganese (50 µg/L) – GM of 483 µg/L, 27 samples above the MDL;
5) Thallium (0.2 µg/L) – GM of 0.6 µg/L, 7 samples above the MDL; and
6) Vanadium (0.3 µg/L) – GM of 12.3 µg/L, 20 samples above the MDL.

Condensed Historical Information The groundwater-monitoring program at the Highway 49 C&D Landfill currently consists of 7 groundwater monitoring wells. Semi-annual sampling and analysis is conducted per the approved Groundwater Monitoring Plan. Initial metal analyses included the RCRA 8 metals until 2011.
Between 2011 and 2012, Appendix I metals were analyzed. From 2013 on, Appendix II metal
analyses were added. The first available data (2007) show that barium was the first and most prevalent metal detected. Barium, cadmium, copper and selenium were observed in the historical records at levels less than their applicable current Standard. Various semi-annual reports submitted by others state that the detected values represent background concentrations in the Piedmont.

Groundwater Conditions and Its Impact on Bedrock Metal Mobility Two of the metals of concern, iron and manganese, are well recognized as being part of the Piedmont bedrock/saprolite. Both of these metals are easily mobilized from the bedrock/saprolite when
reducing groundwater conditions are present. Field sampling logs generated by CEC personnel
during the last two low-flow groundwater-sampling events identified a majority of the groundwater
Ms. Jackie Drummond - NCDEQ
CEC Project 111-370.0002
Page 3 August 2, 2017

wells as having a negative Oxidation-Reduction Potential (ORP) measurement. This negative ORP
indicates a reducing environment. A reducing environment allows for the converting insoluble forms
of iron and manganese in the bedrock to soluble salts resulting in elevated concentrations of these metals in the groundwater. CEC has also reviewed the historical field notes from 2007 to 2016. There are notations of high turbidity in some collected samples. Similar to the solubilizing of the iron and manganese in reducing conditions, high-turbidity in Piedmont groundwater is well understood to
increase the total metal concentrations compared to a low-turbidity sample. The revised groundwater
sampling process of low-sampling now in practice should reduce the likelihood of high turbidity samples going forwards. Published Information on Selected Metals in Background
Chromium, cobalt and vanadium are also well understood to be present in the Piedmont geology. The Energy, Land and Natural Resources Division of NCDEQ published maps(1) on the measured concentrations of these metals in stream sediments. These maps can be found in the Attachments. In these maps, significant concentrations of these three metals are observed in sediments. For example,
chromium has been identified through sampling to be detected in the range of 15 to 20 milligrams per
liter in stream sediments in the general area of the Facility. Likewise, for cobalt, stream sediments have been observed to have concentrations ranging from 15 to 20 milligrams per liter in the general area of the Facility. Vanadium is similar with greater than 180 milligrams per liter being detected in sediments in the general area of the Facility. CEC has also included a publication and map from the
United States Geological Survey (USGS) showing the presence and history of cobalt in the central
North Carolina in the Attachments. Comparing these detected stream sediment concentrations to the GM concentrations of 20.4, 17.6 and 12.3 µg/L of chromium, cobalt and vanadium, the presence of these metals due to naturally occurring background bedrock/saprolite is concluded.
Thallium is the last metal of concern then that needs to be evaluated with respect to its presence in the
background bedrock and saprolite at the Facility. Thallium has been reported in gold deposits and non-gold bearing quartz deposits by the United States Geological Society. Gold mining has been in-place in the Cabarrus and Mecklenburg County areas since the mid-19th century. It has been detected above its method detection limit in all sampled wells ranging from 0.5 to 1.3 µg/L. It has also been
detected in the background well MW-21 at the same value range (0.6 µg/L). The presence of the
thallium in the background well; its known association with gold bearing quartz; and the presence of historical gold mining operations throughout the area supports the conclusion that the thallium is a naturally occurring background metal.
(1) Hoffman, J.D., and Buttleman, Kim, 1994. National Geochemical Data Base: National Uranium Resource
Evaluation Data for the Conterminous United States, U.S. Geological Survey Digital Data Series DDS-18-
A.

Ms. Jackie Drummond - NCDEQ
CEC Project 111-370.0002
Page 4 August 2, 2017

Conclusion
The presented data clearly supports the position that each of the six metals of concern detected in the Facility groundwater are due to their presence in the natural geology. These metals should then be removed from the Contaminants of Concern for the Facility at this time. If you have any questions or comments, please feel free to contact me at [phone].

Sincerely, CIVIL & ENVIRONMENTAL CONSULTANTS, INC.
Bruce D. Reilly, P.E. Scott L. Brown, P.E. Senior Project Manager Vice President
Attachments Cc: Mr. John Brown – Greenway Waste Solutions

ATTACHMENTS

DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
CHROMIUM STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 1
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
IRON IN STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 2
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
IRON IN STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 3
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
MANGANESE IN STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 4
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
VANADIUM IN STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 5
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
UNITED STATES DEPARTMENT OF THE INTERIOR
GEOLOGICAL SURVEY
Distribution of cobalt in heavy-mineral-concentrate samples
from the Charlotte 1° x 2° quadrangle,
North Carolina and South Carolina
by
W. R. Griffitts, J. W. Whitlow, D. F. Siems,
K. A. Duttweiler, and J. D. Hoffman
Open-File Report 84-843-L
This report is preliminary and has not been reviewed for conformity with U.S.
Geological Survey editorial standards and stratigraphic nomenclature. Use of
brand or manufacturer's names is for descriptive purposes only and does not
constitute endorsement by the U.S. Geological Survey.
1984
This map is a product of a geochemical survey of the Charlotte 1° x 2°
quadrangle, North Carolina and South Carolina, begun in 1978 that is part of a
multidisciplinary study to determine the mineral potential of the area.
Correlative studies are the completion of a geologic map of the quadrangle and
aeromagnetic, aeroradiation, and gravity surveys (Uilson and Daniels, 1981).
The Charlotte quadrangle provides a nearly complete section across the
Piedmont: its northwestern corner is in the Blue Ridge, its southeastern
corner is over a basin of Triassic sedimentary rocks only a few miles from the
Coastal Plain. All of the quadrangle except the southeastern corner is
underlain by crystalline rocks of Precambrian and Paleozoic age metamorphosed
to greenschist facies in the Carolina Slate Belt and to amphibolite facies
farther west. Both premetamorphic and post metamorphic intrusive rocks are
present. The rocks have been weathered to permeable saprolite reaching depths
of 200 feet (60 meters) in the Inner Piedmont. Because of the thorough
leaching, most soils are acidic.
In making the geochemical survey, we took samples of sediment within a
few miles of the heads of major streams and of the tributaries of these
streams, keeping the size of the drainage basin small. By doing so, we
usually reduce the variety of rocks that contribute detritus to the sample,
thus facilitating a correlation between sample composition and the geology of
the drainage basin. At the same time, we reduce the chance that a localized
cloudburst has buried the sample site with sediment from a small part of the
drainage basin, thus reducing the validity of the sample as an approximate
composite of the rocks of the whole basin. Nevertheless, the samples are not
all geologically and geochemically equivalent. For instance, at some sites in
the mountainous area in the northwestern part of the quadrangle, many clasts
in the stream sediment are several yards (meters) across and collection of
fine detritus suitable for a sample required a 1/2-hour search. Not far to
the east, the finer sediment was abundant.
In the Piedmont, the usual procedure was to sample rather coarse
sediment pebble- or cobble-containing gravel and to dig deeply to the bottom
of the alluvial bed or to a compact clay layer. The coarsest particles in the
gravel boulders, cobbles, and coarse pebbles were excluded from the sample,
which then consisted of about 10 Ibs (4 1/2 kg) of clay to granule or fine
gravel sized material. The heavy minerals were extracted from this unsifted
material at the sample site with a gold pan. Samples taken in the same manner
on earlier projects were also used to get better coverage of the Inner
Piedmont than we would have had otherwise.
The quartz, feldspar, and other minerals of specific gravity below 2.89
were removed from the pan concentrate by floating them with bromoform. The
heavy-mineral concentrate cleaned in that way was then separated magnetically
into four fractions. The first was removed with a hand magnet, or an
equivalent instrument, and not studied. The remaining concentrate was passed
through a Frantz Isodynamic Separator at successive current settings of 0.5
ampere and 1 ampere with 15° side slope and 25° forward slope. The material
removed from the sample at 0.5 ampere and 1 ampere will be referred to as the
M-5 and Ml concentrates or fractions, respectively, and the nonmagnetic
material at 1 ampere will be referred to as the NM concentrate or fraction.
Most common ore minerals occur mainly in the NM fraction, making them and
their contained metals easier to find and to identify. The NM fraction also
1
contains zircon, sillimanite, kyanite, spinel, apatite, sphene, and the TiC^
minerals. It is generally the most useful fraction. The Ml fraction is
largely monazite in the Inner Piedmont. Because of interferences caused by
cerium during spectrographic analysis and the high content of radiogenic lead
in the monazite, it was necessary to remove it from the bulk concentrates to
improve the quality of analyses and to permit recognition of lead, possibly
derived from mineral deposits, in the NM and M-5 fraction. East of the Inner
Piedmont the Ml concentrate contained very abundant epidote, clinozoisite,
mixed mineral grains, including ilmenite partly converted to leucoxene,
staurolite, and locally abundant spinel. The M-5 concentrate contains
abundant garnet in the Inner Piedmont, dark ferromagnesian minerals in the
Charlotte Belt, and ilmenite in most provinces.
Mineral proportions in each magnetic fraction were estimated using a
binocular microscope. Minerals of special interest were identified optically
or by X-ray diffraction. The time available did not permit a thorough
mineralogic study of all concentrates. Metal-rich minerals were sought in all
samples that were shown by the spectrograph to contain metal in unusually high
concentrations. After establishing the presence of a metal-rich mineral, the
variations in metal contents among the concentrates were inferred to indicate
variations in the content of metalliferous minerals.
Each fraction was analyzed semiquantitatively for 31 elements using a
six-step, D.C. arc, optical-emission spectrographic method (Grimes and
Marranzino, 1968). The semiquantitative spectrographic values are reported as
one of six steps per order of magnitude (1, 0.7, 0.5, 0.3, 0.2, 0.15, and
multiples of 10 of these numbers) and the values are the approximate geometric
midpoints of the concentration ranges. The precision of the method has been
shown to be within one adjoining reporting interval on each side of the
reported values 83 percent of the time and within two adjoining intervals on
each side of the reported value 96 percent of the time (Motooka and Grimes,
1976).
The lower limits of spectrographic determination for the 5 elements that
are mentioned in this report are, in parts per million: cobalt, 10; gold, 20;
niobium, 50; and tin, 20.
All analytical data for sample material other than concentrates are taken
from a report by Ferguson (1979). Such sample material is referred to as
"silt" in this report.
Most samples were taken by J. W. Whitlow and W. R. Griffitts. Lesser
numbers were taken by D. F. Siems, A. L. Meier, and K. A. Duttweiler. The
mineral analyses were made by W. R. Griffitts, K. A. Duttweiler, J. W.
Whitlow, and C. L. Bigelow, with special mineral determinations by Theodore
Botinelly. All spectrographic analyses were made by D. F. Siems, in part from
plates prepared by K. A. Duttweiler. Steve McDanal and Christine McDougal
were responsible for entering and editing the locality and spectrographic data
in the RASS computer file. Many maps were subsequently plotted from this file
by H. V. Alminas, L. 0. Wilch, and J. D. Hoffman. Most mineral distribution
maps were plotted by K. A. Duttweiler.
Cobalt is widespread in rather high concentrations in the M-5
concentrates and common but less widespread in the NM concentrates. It is
2
particularly widespread in the Carolina Slate Belt. In much of the
quadrangle, cobalt is so commonly associated with gold as to indicate that
both were involved in common episodes of mineralization. Cobalt is not
closely associated with mafic rocks, as is indicated by the high cobalt
contents of magnesium-poor M-5 concentrates (plate 1). The M-5 magnetic
fraction contains the dark silicate minerals in our concentrates; most of
those minerals have magnesium as a major component, so their scarcity
indicates that mafic rocks, rich in ferromagnesian minerals cannot be
prominent in the drainage basins.
No cobalt minerals were recognized in our investigation. The abundance
of manganese in the M-5 concentrates collected near Salisbury suggests that
the cobalt may now be in black manganese oxide minerals, some of which are
known to be cobalt accumulators.
A row of clusters of cobalt-rich sample sites passes west-northwest from
near the southeastern corner of the quadrangle to the vicinity of Charlotte.
The mineralized area near Charlotte has long been known and exploited for
gold. The area near the southeastern corner of the quadrangle, in eastern
Union County, has not been exploited for any minerals.
A cluster of cobalt-rich sample sites near Blacksburg also yields gold
and high-zinc values. That general area contains gold-quartz veins and
several kinds of iron deposits: gossans; layered quartz-hematite iron
formation; and black oxides in skarn. The cobalt concentrations may be
related to one or more of these types of deposit.
A series of 4 cobalt-rich samples were collected along a line that trends
north-northeast about 5 miles southeast of Lexington. The trend is similar to
the trends of faults at the northern end of the Gold Hill fault in the
vicinity, so the cobalt may have been deposited in minor, unmapped, faults
related to the major ones. The Gold Hill fault itself does not yield cobalt-
rich samples.
An unusually large group of sites is found over and around a granite
pluton south of Salisbury and extends as far west as Kannopolis. The cobalt
here is associated with gold, as in most places in the quadrangle, but it also
is accompanied by niobium and tin. The granite pluton is the source for the
niobium and tin, but the sources of the cobalt and gold is unknown.
The cobalt content of nonmagnetic concentrates calls attention to some of
the same areas as that of M-5 concentrates. The area south of Salisbury is
not prominent in the values in nonmagnetic concentrates; the area near
Blacksburg remains prominent.
The cobalt content of minus-100-mesh sediment is rather high in parts of
the eastern Charlotte Belt and eastern and northern Carolina Slate Belt.
Unlike the cobalt in M-5 concentrates, the high values in silt are not
generally in gold areas, but are between gold areas.
References
Ferguson, R. B., 1979, Athens, Charlotte, Greenville, and Spartanburg NTMS
1° x 2° quadrangle areas: Supplemental data release: U.S. Department of
Energy, Grand Junction, Colorado, Open-File Report GJBX 73(79), 124 p.
Grimes, D. J., and Marranzino, A. P., 1968, Direct-current arc and alternating
current spark emission spectrographic field methods for the
semiquantitative analysis of geologic materials: U.S. Geological Survey
Circular 591, 6 p.
Heffner, J. D., and Ferguson, R. B., 1978, Charlotte NTMS area, North Carolina
and South Carolina: Preliminary Data Release: U.S. Department of
Energy, Grand Junction, Colorado, Open-File Report GJBX 40(78).
Motooka, J. M., and Grimes, D. M., 1976, Analytical precision of one-sixth
order semiquantitative spectrographic analysis: U.S. Geological Survey
Circular 738, 25 p.
Wilson, F. A., and Daniels, D. L., 1980, Simple Bouguer gravity map of the
Charlotte 1° x 2° quadrangle, North Carolina and South Carolina: U.S.
Geological Survey Miscellaneous Investigations Series Map I-1251-A.
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
MONITORING WELL LOCATION MAP
111-370.0021" = 400'MAY 2017
JKS PNP EHS 1
GREENWAY WASTE SOLUTIONS OF
HARRISBURG, LLC
HARRISBURG, NORTH CAROLINA
REFERENCE
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
LEGEND

August 2, 2017

Ms. Jackie Drummond Compliance Hydrogeologist Division of Waste Management - Solid Waste Section North Carolina Department of Environmental Quality
Asheville Regional Office
2090 US Highway 70 Swannanoa, NC 28778 Dear Jackie:

Subject: Highway 49 C&D Landfill – Permit 13-06 Greenway Waste Solutions of Harrisburg, LLC Demonstration Letter on Laboratory Analyses for Vinyl Chloride CEC Project 111-370.002

Per 15A NCAC 13B .0544 (b) (1) (I), Civil & Environmental Consultants, Inc. (CEC) on behalf of Greenway Waste Solutions of Harrisburg, LLC has prepared and is submitting this Demonstration Letter presenting history and recently discovered facts regarding the detections of vinyl chloride in groundwater that is sampled and analyzed per the conditions in the above permit. Vinyl chloride is
groundwater contaminant 145 as listed in 15A NCAC 02L .0202 and has a cleanup standard of 0.03
micrograms per liter or the practical quantitation limit whichever is greater. This letter presents condensed historical information on the detection of vinyl chloride in groundwater at the landfill and then provides a timeline and facts generated during the investigation of higher than expected detection of vinyl chloride. Attachments include selected monitoring well vinyl chloride historical charts, site
plan showing well locations and correspondence from analytical laboratories certified by the state to
perform groundwater organic analyses. Condensed Historical Information
The groundwater-monitoring program at the Highway 49 C&D Landfill consists of a network
groundwater monitoring wells and has been ongoing since December 2004. Semi-annual sampling takes place and the samples analyzed per the approved groundwater-monitoring plan. Vinyl chloride was first detected in the facility’s groundwater in the spring sampling event in 2013.
Three monitoring wells at the facility contained vinyl chloride at concentrations above the practical
quantitation limit during the spring 2016 sampling. In 2013, the first detections of vinyl chloride occurred in three monitoring wells. (Charts for several of the monitoring well historical vinyl chloride concentrations can be found in the Attachment.) At a permitted facility operated by Greenway Waste Solutions of North Meck a similar vinyl chloride data history exists. As part of CEC’s review of the
Ms. Jackie Drummond - NCDEQ
CEC Project 111-370.0002
Page 2 August 2, 2017

North Meck vinyl chloride history and after detailed review of the historical data for the Highway 49
C&D Landfill, CEC was tasked with sampling the groundwater monitoring wells in 2017.
For the spring 2017 groundwater-sampling event, CEC obtained split samples and these were delivered to TestAmerica and Pace Analytical Laboratories. For certain samples, higher than expected values of vinyl chloride were reported by TestAmerica compared against the Pace results.

CEC asked TestAmerica to review the results, analysis methodology, instruments used and interview the analysts in an effort to either validate or discount this first round of 2017 results. TestAmerica brought in their Senior Technical Services Group to review their process. In late May, TestAmerica informed CEC of the following results of their investigation:

1. Search indicated a possibility of conversion of a Freon refrigerant (Freon 151) to vinyl chloride in the GC; 2. Confirmation of this occurred after TestAmerica obtained and ran a Freon 151 standard through their Chicago GCs, resulting only one of the GCs not converting the Freon 151 to
vinyl chloride;
3. A TestAmerica company-wide program was implemented and identified most of their GCs converting the Freon 151 to vinyl chloride; and 4. TestAmerica started, and is continuing, a corrective-action program to identify and change the component(s) of the GCs converting the Freon. (It is reported that the likely cause is the
Purge and Trap mechanism.)
After receiving the information that the analytical procedure and equipment were the cause of the higher than expected groundwater vinyl chloride results, CEC resampled the monitoring wells with spring 2017 vinyl chloride detections at the Highway 49 C&D Landfill in June 2017. The comparison
of the recent historical vinyl chloride results are shown in the following table:

Table 1 – Vinyl Chloride Results Fall 2016 to Spring 2017

Results are shown in µg/L * = POC Well NS = Not Sampled BOLD = value exceeds the PQL or Standard of 0.03 µg/L for vinyl chloride
Well I.D. October 2016 Vinyl Chloride
Shealy
April 2017 Vinyl Chloride
TestAmerica
April 2017 Vinyl Chloride
Pace
June 2017 Vinyl Chloride
TestAmerica
MW-55* 0.78 <0.5 <1.0 NS
MW-56* 13 6.6 3.3 9.6
MW-57* 4.8 3.3 <1.0 0.59
MW-57D* 2.5 1.1 <1.0 <0.5
Ms. Jackie Drummond - NCDEQ
CEC Project 111-370.0002
Page 3 August 2, 2017

The results of the second round of spring 2017 sampling showed two point of compliance wells
exhibiting vinyl chloride concentrations above the practical quantitation limit. A figure showing the facility’s wells can be found in the Attachment. CEC also received from Shealy and their supplier of the silica gel (OI Analytical) in the Purge and
Trap mechanisms that are part of the GC letters documenting the results of their independent testing
confirming TestAmerica’s results. The various pieces of correspondence from TestAmerica, Shealy and OI Analytical can be found in the Attachment. Impacts on Compliance Status
While the confirmed conversion of Freon 151 to vinyl chloride explains the higher than expected historical data on vinyl chloride at the Highway 49 C&D Landfill, the groundwater as measured at the POC wells still exhibits vinyl chloride and other constituents either above the applicable standard or above the practical quantitation limit. Confirmation of these second round results from the spring
2017 sampling will continue to take place for the near future as part of the approved groundwater-
monitoring plan. CEC will continue to obtain an analyze split samples and blind duplicates from selected groundwater monitoring wells as we have recently done. TestAmerica and Pace are continuing to work through reviews of their GCs to eliminate the issue(s) converting the Freon to vinyl chloride.

Conclusion CEC on behalf of our client is requesting that NCDEQ discount the vinyl chloride analytical data when reviewing historical information from prior to 2017.

If you have any questions or comments, please feel free to contact me at [phone]. Sincerely,
CIVIL & ENVIRONMENTAL CONSULTANTS, INC.
Bruce D. Reilly, P.E. Scott L. Brown, P.E.
Senior Project Manager Vice President
Attachments Cc: Mr. John Brown – Greenway Waste Solutions

ATTACHMENTS

0
5
10
15
20
25
30
MW-56
Vinyl Chloride Trend (ug/l)
0
5
10
15
20
MW-57
Vinyl Chloride Trend (ug/l)
1
Reilly, Bruce
From:Stephens, Ed
Sent:Wednesday, July 19, 2017 8:46 AM
To:Reilly, Bruce
Subject:FW: Vinyl chloride
fyi

Ed Stephens, P.G.
Civil & Environmental Consultants, Inc.
1900 Center Park Drive · Suite A · Charlotte, NC 28217
Toll-Free: 855-859-9932· Fax: [phone]
Mobile: [phone] · http://www.cecinc.com
Senior Leadership · Integrated Services · Personal Business Relationships

From: Dan Wright [mailto:[e-mail]]
Sent: Tuesday, January 10, 2017 8:58 AM
To: Stephens, Ed <[e-mail]>
Cc: Michael Kilpatrick <[e-mail]>; Grant Wilton <[e-mail]>
Subject: Vinyl chloride

Morning Ed,

We have solved the vinyl chloride mystery. All the samples that we are detecting vinyl chloride have the tentatively
identified compound 1-chloro-1-fluoroethane (molecular weight 82.5 aka Freon 151) which is breaking down in the
autosampler metal sample pathway to vinyl chloride (molecular weight 62.5). This is likely occurring in the 6 port valve
of the autosampler where actives site are catalyzing HF which accounts for 20 AMUs. I discussed this with Test America
staff since they had the large discrepancy between the two labs. It appears that some autosamplers are most likely to
have the active sites that cause this degradation of Freon 151. They have witnessed this specific issue first hand at Test
America as well.

We have ordered a single standard of Freon 151 which we will run on several instruments to determine if any do not
cause the degradation. This situation is fairly rare, but due to the presence of Freon 151 in these samples the conditions
were right to form vinyl chloride. I will call you to discuss, but wanted to get you in the loop now so you can pass this on
to your client and the applicable regulators.

Once we analyze the Freon 151 standard we should be able to switch out some components in our autosamplers to
remove the active site thus preventing the formation of vinyl chloride. If we demonstrate we can eliminate the
degradation issue we certainly want to talk to you about systematically getting this groundwater work back. We have
supported these sites for many years and appreciate the scope or requirements.

Thanks,

Dan

NOTICE: The information contained in this email and any document attached hereto is intended only for the
2
named recipient(s). If you are not the intended recipient, nor the employee or agent responsible for delivering
this message in confidence to the intended recipient(s), you are hereby notified that you have received this
transmittal in error, and any review, dissemination, distribution or copying of this transmittal or its attachments
is strictly prohibited. If you have received this transmittal and/or attachments in error, please notify me
immediately by reply e-mail and then delete this message, including any attachments.

Page 1 of 3
TestAmerica Chicago

Corrective Action Report
Client: Civil and Environmental Consultants Inc.
Project: NC Landfills
Site: NC North Mecklenburg Landfill, NC Highway 49 Landifll, NC Apex Landfill, NC
Responsible Parties: TestAmerica Chicago
Date Initiated: 05/24/17
Initiator: JoAnn Petruszak-Kmetty
Description of Problem: The client requested that the vinyl chloride (VC) data for job 500-127404 from the North Mecklenburg Landfill - Infill be re-reviewed because the results were “an
order of magnitude greater than the split samples results”. During the review, it
was observed that each sample that had a positive detect for vinyl chloride also had a tentatively identified compound (TIC) identified as 1-chloro-1-fluoroethane (Freon 151). An inquiry was made of the other TestAmerica laboratories and the technical support personnel within TestAmerica to see if others have seen this
correlation.
After a preliminary investigation was performed at three TestAmerica laboratories, the TestAmerica Technical Support Organization (TSO) determined that false positive or high-biased results for vinyl chloride can occur due to the
degradation of 1-chloro-1-fluoroethane (Freon 151) on some VOA GC/MS
instruments. Freon 151 is not a VOA target analyte and it is not commonly found in the environment, but it is present more frequently in landfill leachates and monitoring wells. All of the vinyl chloride artifacts attributable to Freon 151 that we have identified to date are associated with landfill operations.

When samples containing Freon 151 are analyzed on certain VOA GC/MS instruments that ‘activate’ or promote its degradation, vinyl chloride artifacts will

Page 2 of 3
TestAmerica Chicago

be generated. Some VOA instruments are highly ‘activated’ towards Freon 151 degradation, while others are quite ‘inert’. Freon 151 degradation is believed to
occur on active sites in the VOA instrument ‘sample pathway’ that have
developed over time, and may be difficult to reverse. Freon 151 has a characteristic mass spectrum and is easy to identify by library search. It will usually be evident as a significant peak eluting shortly after vinyl chloride.
Corrective Action Plan:
To correct the immediate problem, the following actions were taken: 1) Analyze a Freon 151 standard at ~ 300 ppb concentration on all VOC instruments.
2) Identify VOC instruments as ‘activated’ if VC is > RL, and ‘inert’ if VC is < RL,
in the analysis of the Freon 151 standard. 3) Monitor each presumptive positive detect for VC on an activated instrument for the presence of Freon 151. If Freon 151 is present, re-analyze samples with presumptive positives for VC on an inert instrument.
4) When/where possible, perform maintenance on activated instruments to
eliminate active sites and ensure inert status. 5) Review previous jobs that were analyzed from these sites and identify samples that had Freon 151 and VC detects.
Status as of 6-12-17: The TestAmerica Chicago laboratory has analyzed a Freon 151 standard on each VOA instrument in the laboratory and has identified which instruments are
‘activated’ and which instruments are ‘inert’.
All analysts have been informed of the situation and instructed to re-analyze samples with positive detects for VC and Freon 151 on an instrument which has been determined to be ‘inert’. The laboratory project manager will be informed of
the situation and the client will be notified if data is impacted.
The project manager will flag each known project site that historically has had Freon 151 with a method comment in TALs computer system so that it will appear on the analyst’s backlog upon arrival of samples to the laboratory.

The following jobs have been reviewed and samples containing VC and Freon 151 have been identified: 500-127325, -127370, -127404, -127480, -127268, and -126939. The results have been flagged with a ‘cn’ flag and narrated.

Page 3 of 3
TestAmerica Chicago

The TestAmerica Chicago laboratory is in the process of performing maintenance on the activated instruments to minimize or eliminate the active sites to ensure
an inert status.
Further Corrective Action Needed: 1. Systematically clean or replace sample pathway to identify location of
active site within the instrumentation.
2. 3.

Reviewed by: _____________
JoAnn Petruszak-Kmetty, GC/MS VOA Supervisor Date Reviewed by: _____________ Robin Kintz, Project Manager Date

Reviewed by: Terese A. Preston, QA Manager Date Reviewed by:
Michael J. Healy, Laboratory Director Date

DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
MONITORING WELL LOCATION MAP
111-370.0021" = 400'MAY 2017
JKS PNP EHS 1
GREENWAY WASTE SOLUTIONS OF
HARRISBURG, LLC
HARRISBURG, NORTH CAROLINA
REFERENCE
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
LEGEND