4901_IredellMSWLF_2nd2015WQMR_DIN25853_20160324

Iredell County Closed Unlined MSWLF
Statesville, North Carolina
July 2015
Permit Number: 49-01
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G15014.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

y Monitoring Report
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Groundwater Samples Above Standards Page 2
Surface Water Samples Above Standards Page 2
Groundwater and Surface Water Characterization Page 2
Findings Page 2
Closing Page 3
FIGURES
Topographic Map with Site Location Figure 1
Superimposed Aerial Photograph of Facility Figure 2
Histograms of Total VOC Concentrations Figure 3
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, 2B or MCL Table 5
APPENDICIES
Laboratory Analysis Reports and Chains of Custody Appendix A
Field Sampling Data Sheet Appendix B
March 23, 2016
Mr. Ervin Lane
Solid Waste Section (SWS)
NC DEQ Division of Waste Management
217 West Jones Street
Raleigh, NC 27603
Re: Semi-Annual Water Quality Monitoring Report
Iredell County Closed Unlined Landfill
Permit No. 49-01
MESC0 Project No. G15014.0
Event Date(s): July 11, 2015

Dear Mr. Lane:
Introduction
On behalf of Iredell County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Report for the summer 2015 event performed at the Iredell County Closed Unlined
Landfill. NCDENR Solid Waste Rules 15A NCAC 13B.0601 requires that Iredell County provide this report to the
SWS on a semi-annual basis. This report documents the quality of the ground and surface waters during the
monitoring event performed July 11, 2015. Laboratory analytical results indicate the surficial aquifer monitored by
monitoring wells MW-1, MW-3, MW-6, MW-6R and MW-7S contained between one and five volatile organic
compound(s) [VOC(s)] in concentrations above their respective North Carolina Groundwater Standard (2L).
Background
The Iredell County Closed Unlined MSWLF, permit #49-01, is located at 243 Twin Oaks Road, Statesville, North
Carolina. The site location topographic map is depicted in the attached Figure 1.
Water quality monitoring was initiated in 1989 and the facility has been continuously monitored on at least a semi-
annual basis since 1995. Current data was compared to all historical data compiled since 1995.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and a recent SWS
memorandum this report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization. Well construction summary table, sampling and analysis summary table, detections compared to
Standards table, histograms of historical detections, potentiometric map, field parameters, laboratory analytical
reports with quality assurance/quality control data and chains-of-custody (C-O-C) are also included in this report.
Sampling Procedure
MESCO personnel collected water samples utilizing portable monitoring methodology from locations indicated in
the site-specific Sampling and Analysis Plan (SAP) contained in the previously approved Transition Plan.
Additional, water samples were collected from MW-3R, MW-6R, MW-7S, and MW-7D which have been installed
since initiation of the SAP. Water quality monitoring locations consist of six downgradient groundwater monitoring
wells (MW-2, MW-3, MW-3R, MW-4, MW-6, MW-6R), three hydraulically upgradient wells (MW-1, MW-7S,
MW-7D), an upstream surface water location (SW-1) and a downstream surface water point (SW-2). The water
supply wells designated in the SAP, which previously served the ANIMAL SHELTER and MENTAL HEALTH
CENTER, were inspected during this event and remain disconnected; therefore, neither supply well was sampled.
Monitoring locations are shown on the enclosed aerial photograph (Figure 2).

A groundwater monitoring well construction table is presented as Table 1. The function and integrity of all
monitoring locations were visually evaluated and no deficiencies observed as documented on Table 2. The depth to
water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low-flow
pumping methodology or bailing was utilized to adequately purge the wells to a minimum of three times the volume
of standing water in the well or until dry. Surface water samples were collected from Fourth Creek tributary
discharge feature at previously designated locations. During well purging and surface water sample collection the
required field parameters were recorded. The samples were then placed into laboratory-prepared, pre-preserved
containers via a new disposable polyethylene bailer. Samples were kept on ice and transported to a NC-certified
laboratory under proper C-O-C protocols within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters recorded included pH, specific conductance, temperature, total dissolved solids (TDS),
and turbidity. A summary of the field parameter data is presented in Table 3 and the field sampling data sheet is
enclosed in Appendix B. The field parameter data appears to be generally consistent relative to each other and
congruent with data historically reported.
Laboratory Results
Pace Analytical Laboratories, Inc. of Huntersville, NC, performed lab analysis targeting the parameters listed in 40
CFR Subpart 258 Appendix I using EPA 8260B for volatile organic compounds (VOCs) and EPA 6000/7000 for total
metals. A summary of the locations, target parameters and analytical methods are shown in Table 4.
Water samples were analyzed to laboratory-established Method Detection Limits (MDL) set at or below current Solid
Waste Section Limits (SWSL). Table 5 summarizes constituents detected in water samples in concentrations equal
to or exceeding the current SWSL, Groundwater Protection Standards (GWP), North Carolina Groundwater
Standards (2L), the North Carolina Surface Water Standards (2B) for Class C water bodies and maximum
contaminant level (MCL) also referenced as “Primary Drinking Water Standards”. Laboratory results and COCs are
presented in Appendix A.
Groundwater Samples Above Standards
Total cadmium was detected in samples MW-3R (2.1 µg/L) and MW-6 (2.3 µg/L) above the 2L Standard (2.0 µg/L)
but below the MCL (5.0 µg/L).
VOCs were reported in quantifiable concentrations above their respective 2L Standard in samples collected from
downgradient wells MW-3 (1,1-DCA, PCE, TCE), MW-6 (1,2-DCP, 1,2-DCA, VCM, benzene) and MW-6R (PCE,
TCE). VOCs were also detected at quantifiable levels in exceedance of their respective 2L Standard in wells MW-1
(PCE, TCE, 1,1-DCA, VCM, benzene) and MW-7S (PCE) which appear to be located hydraulically upgradient from
the landfill.
Surface Water Samples Above Standards
No contaminants were detected in concentrations above SWSL or 2B Standards in samples collected upstream (SW-
1) or downstream (SW-2) of the landfill.
Groundwater and Surface Water Characterization
Groundwater in the surficial aquifer flows from a hydrological high at MW-7S, upgradient of the MSWLF, in a
general northeast direction towards the Fourth Creek discharge feature. Fourth Creek tributary was visually observed
to have moderate flow and gage height with low turbidity.
Findings
The surficial aquifer monitored by down/cross gradient monitoring wells MW-3, MW-6, MW-6R, and hydraulically
upgradient wells MW-1 and MW-7S contained VOCs with some concentrations above their respective 2L Standards
and fewer above EPA Drinking Water Standards. All total cumulative VOC concentrations remain within their own
respective historically identified range (Figure 3). Landfill gas is suspected to be the transport mechanism for the
VOCs detected in groundwater especially in the area hydraulically upgradient of the landfill monitored by MW-1 and
MW-7S/D. Actions have been initiated to reduce landfill gas migration at the closed landfill with an emphasis on the
area near the closed animal shelter building which may improve groundwater quality upgradient of the landfill.
2
Figures
Closed C&D
Lined MSWLF
34 21
C&D
Closed Unlined MSWLF
STATESVILLE
Topographic Map with Site Location
Iredell County Landfill
Figure 102.5 2.5 MILES
STATESVILLE EAST QUADRANGLE
N
354 Twin Oaks Rd
Statesville, NC 28625
Lat:35-46-17.8012
Long:-80-49-22.2973
Northing:740719.35
Easting:1459306.76
MW-6R MW-3R
MW-3
MW-6
MW-7D
SUBDIVISION ON CITY WATER
ANIMAL
SHELTER
TWIN OAKS GOLF
COURSE
OWNED BY IREDELL
COUNTY
SUPPLY WELL FOR 3
BUILDINGS (NOT IN
SERVICE)
SW-1
SW-2
FOU
RT
H C
RE
E
K
MW-4
SUBDIVISION ON
WELL WATER
Closed MSWLF
<10/9/93
Closed MSWLF <10/9/91
MW-2
MW-1
MW-7S
Figure 2. Superimposed Aerial Photograph
Property Line
General Groundwater Contours Ephemeral Ditch
Perennial Stream
Waste Limit
Iredell County Closed Unlined MSWLF
Monitoring Locations Not Surveyed
N
Iredell County Closed Unlined MSWLF Page 1 of 1
Figure 3
Histograms of Total VOC Concentrations
December 21, 1995 – July 11, 2015
= July 11, 2015
Tables
Iredell County Closed Unlined MSWLF Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
July 11, 2015
Latitude Longitude
MW-1 06/19/89 2 60 50 10 Sandy Clay 843.83 841.92 799.62 44.21 35º46'31.5087"80º49'31.0952"
MW-2 06/19/89 2 49 39 10 Sandy Clay 797.44 795.33 777.78 19.66 35º46'46.0504"80º49'30.3965"
MW-3R 06/21/02 2 23 13 10 Sandy Clay 752.69 753.93 745.71 6.98 35º46'46.7602"80º49'8.4510"
MW-3 06/19/89 2 20 5 15 Sandy Silt 756.09 749.46 746.28 9.81 35º46'49.1493"80º49'7.0950"
MW-4 06/19/89 2 30 20 10 Sandy Clay 764.87 762.67 752.60 12.27 35º46'31.5087"80º49'7.4321"
MW-6 01/21/92 2 33 18 15 Sandy Silt 782.49 781.49 755.81 26.68 35º46'46.7528"80º49'20.8301"
MW-6R 06/21/02 2 20.5 5.5 15 Sandy Silt 753.13 750.24 749.65 3.48 35º46'49.6883"80º49'19.0478"
MW-7S 07/01/06 2 54.37 39.37 15 Sandy Clay 846.77 843.77 800.69 46.08 35º46'37.9363"80º49'31.2640"
MW-7D 07/01/06 2 132.1 122.1 10 Rock 846.60 843.60 800.44 46.16 35º46'37.9281"80º49'31.2202"
NOTE:
Monitoring
Well
Date
Installed
Well
Diameter
(inches)
Total
Well
Depth
(ft bgs)
Top of
Screen
Depth
(ft bgs)
Screen
Interval
(ft bgs)
Geology of
Screened
Interval
Top of
Casing
Elevation
(ft amsl)
Ground
Elevation
(ft amsl)
Groundwater
Elevation
(ft amsl)
Depth
to
Water
(ft btoc)
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Iredell County Closed Unlined MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
July 11, 2015
Locked Comments
MW-1 Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes Yes
MW-3 Yes Yes Yes Yes Yes Yes
MW-3R Yes Yes Yes Yes Yes Yes Field dry.
MW-4 Yes Yes Yes Yes Yes Yes
MW-6 Yes Yes Yes Yes Yes Yes
MW-6R Yes Yes Yes Yes Yes Yes
MW-7S Yes Yes Yes Yes Yes Yes
MW-7D Yes Yes Yes Yes Yes Yes
SW-1 Yes Yes Yes Yes Yes Yes Low Volume & Flow
SW-2 Yes Yes Yes Yes Yes Yes Low Volume & Flow
No Yes WSW. Not in Use
No Yes WSW. Not in Use Wiring Disconnected
Any unusual field conditions, observations, or events:
Animal Shelter permanently closed on July 6, 2011. MW-1 is located inside animal shelter's fence.
All steel protective well cases painted yellow by County since July 2011.
Field in which MW-3R is located was dry. Flooding observed in January 2015 was caused by beaver dam(s).
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears
Effective
Mental
Health Center na na na na
Animal
Shelter na na na na
Iredell County Closed Unlined MSWLF Page 1 of 1
Table 3
Sampling and Analysis Summary
July 11, 2015
Field Parameter
Re
a
s
o
n

N
o
t

S
a
m
p
l
e
d
To
t
a
l

M
e
t
a
l
s

Te
m
p
e
r
a
t
u
r
e
Co
n
d
u
c
t
i
v
i
t
y
To
t
a
l

D
i
s
s
o
l
v
e
d

S
o
l
i
d
s

(
T
D
S
)
pH Tu
r
b
i
d
i
t
y
La
b

E
P
A

8
2
6
0
B
L
a
b

E
P
A

6
0
0
0
/
7
0
0
0
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

V
i
s
u
a
l
MW-1 x x x x x x x
MW-2 x x x x x x x
MW-3 x x x x x x x
MW-3R x x x x x x x
MW-4 x x x x x x x
MW-6 x x x x x x x
MW-6R x x x x x x x
MW-7S x x x x x x x
MW-7D x x x x x x x
SW-1 x x x x x x x
SW-2 x x x x x x x
All locations listed in the water quality monitoring plan are shown
Appendix I List taken from current 40 CFR 258
App. I
V OC
s
Iredell County Closed Unlined MSWLF Page 1 of 1
Table 4
Field Parameter Data Summary
July 11, 2015
Sample ID Temp.ORP DO pH TDS
Units C mg/L SU Visual
MW-1 44.21 799.62 843.83 18.5 NR NR 5.03 10 0 Clear
MW-2 19.66 777.78 797.44 18.1 NR NR 6.38 310 150 Clear
MW-3R 6.98 745.71 752.69 16.2 NR NR 6.38 80 30 Slight
MW-3 9.81 746.28 756.09 15.5 NR NR 7.09 70 30 Slight
MW-4 12.27 752.6 764.87 15.8 NR NR 6.35 460 230 Clear
MW-6 26.68 755.81 782.49 17.1 NR NR 6.35 1280 630 Slight
MW-6R 3.48 749.65 753.13 15.1 NR NR 6.20 180 80 Clear
MW-7S 46.08 800.69 846.77 19.1 NR NR 5.11 60 30 Clear
MW-7D 46.16 800.44 846.60 20.9 NR NR 6.99 110 50 Clear
Minimum 3.48 745.71 752.69 15.1 NR NR 5.03 10 0 Clear
Average 23.93 769.84 793.77 17.4 NR NR 6.21 284 137 Clear
Maximum 46.16 800.69 846.77 20.9 NR NR 7.09 1280 630 Slight
SW-1 ---26.2 NR NR 7.01 110 50 Clear
SW-2 ---25.8 NR NR 7.03 90 40 Clear
Minimum ---25.8 NR NR 7.01 90 40 Clear
Average ---26.0 NR NR 7.02 100 45 Clear
Maximum ---26.2 NR NR 7.03 110 50 Clear
NR = No reading attempted and not required
Water
Depth
Water
Elevation
TOC
Elevation
Specific
Conductance
Turbidity
of Metal
Sample
ft (btoc)ft (amsl)ft (amsl)mV цs/cm ppt
Iredell County Closed Unlined MSWLF Page 1 of 2
Table 5
Detections that Attain or are Above SWSL, GWP, 2L, 2B or MCL
July 11, 2015
Result Unit
MW-1 7/11/15 17.7 0.32 5 6 7 LFG
MW-1 7/11/15 1.3 0.33 1 6 75
MW-1 Benzene 7/11/15 1.6 0.25 1 1 5 LFG
MW-1 7/11/15 11.8 0.19 5 70 70
MW-1 Methylene Chloride 7/11/15 2.7 0.97 1 4.6 5
MW-1 7/11/15 7.3 0.46 1 0.7 5 LFG
MW-1 7/11/15 11.2 0.47 1 3 5 LFG
MW-1 Vinyl chloride 7/11/15 1.5 0.62 1 0.03 2 LFG
MW-1 Zinc, total 7/11/15 19.7 5 10 1000 5000
MW-2 Barium, total 7/11/15 451 2.5 100 700 1300
MW-2 7/11/15 7J 3.1 10 NE NE NE
MW-2 Zinc, total 7/11/15 12.1 5 10 1000 5000
MW-3 7/11/15 21.3 0.32 5 6 7 L &/or LFG
MW-3 7/11/15 8 0.19 1 70 70
MW-3 7/11/15 3.8 0.46 1 0.7 5 L &/or LFG
MW-3 7/11/15 4.7 0.47 1 3 5 L &/or LFG
MW-3R Barium, total 7/11/15 102 2.5 100 700 1300
MW-3R Cadmium, total 7/11/15 2.1 0.5 1 2 5 N
MW-3R Vanadium, total 7/11/15 5.5J 2.5 25 NE 3.5 NE
MW-6 7/11/15 0.8J 0.3 5 24 NE
MW-6 7/11/15 2.1 0.12 1 0.4 5 L &/or LFG
MW-6 7/11/15 1.3 0.27 1 0.6 5 L &/or LFG
MW-6 7/11/15 2.3 0.33 1 6 75
MW-6 Barium, total 7/11/15 503 2.5 100 700 1300
MW-6 Benzene 7/11/15 4.7 0.25 1 1 5 L &/or LFG
MW-6 Cadmium, total 7/11/15 2.3 0.5 1 2 5 N
MW-6 7/11/15 21.8 0.19 5 70 70
MW-6 Cobalt, total 7/11/15 42.6 2.5 10 NE 70 NE
MW-6 Methylene Chloride 7/11/15 1 0.97 1 4.6 5 A
MW-6 7/11/15 72.7 3.1 10 NE NE NE
MW-6 Thallium, total 7/11/15 5.1J 5 5.5 NE 0.28 2
MW-6 Vinyl chloride 7/11/15 4.4 0.62 1 0.03 2 L &/or LFG
MW-6R 7/11/15 2.2 0.46 1 0.7 5 L &/or LFG
MW-6R 7/11/15 3.4 0.47 1 3 5 L &/or LFG
MW-6R Zinc, total 7/11/15 20.9 5 10 1000 5000
MW-7D Vanadium, total 7/11/15 19J 2.5 25 NE 3.5 NE
MW-7S 7/11/15 8 0.46 1 0.7 5 LFG
MW-7S 7/11/15 1.9 0.47 1 3 5
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
1,1-Dichloroethane ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
ug/L
ug/L
ug/L
Tetrahydrofuran ug/L
ug/L
1,1-Dichloroethane ug/L
cis-1,2-Dichloroethene ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
ug/L
ug/L
ug/L
1,2-Dichlorobenzene ug/L
1,2-Dichloroethane ug/L
1,2-Dichloropropane ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
Tetrahydrofuran ug/L
ug/L
ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
ug/L
ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
Iredell County Closed Unlined MSWLF Page 2 of 2
Result UnitSample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
FB Methylene Chloride 7/23/15 0.99J 0.97 1 4.6 5 A
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
N = Natural. Not anthropogenic
L = Leachate
LFG = Landfill Gas
A = Artifact laboratory or field induced as detected in blank(s) and flagged by the lab as “(C9) common laboratory contaminant”
Concentration > 2L, 2B, GWP or MCL Standard
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
BOLD =
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
July 20, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92258575
92258575
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
IREDELL CLOSED MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 14, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 37
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 37
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92258575001 MW-1 Water 07/11/15 16:05 07/14/15 14:40
92258575002 MW-2 Water 07/11/15 12:05 07/14/15 14:40
92258575003 MW-3 Water 07/11/15 10:55 07/14/15 14:40
92258575004 MW-3R Water 07/11/15 10:00 07/14/15 14:40
92258575005 MW-4 Water 07/11/15 11:30 07/14/15 14:40
92258575006 MW-6 Water 07/11/15 14:30 07/14/15 14:40
92258575007 MW-6R Water 07/11/15 13:40 07/14/15 14:40
92258575008 MW-7S Water 07/11/15 15:40 07/14/15 14:40
92258575009 MW-7D Water 07/11/15 15:10 07/14/15 14:40
92258575010 SW-1 Water 07/11/15 09:15 07/14/15 14:40
92258575011 SW-2 Water 07/11/15 10:20 07/14/15 14:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 37
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92258575001 MW-1 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575002 MW-2 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575003 MW-3 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575004 MW-3R EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575005 MW-4 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575006 MW-6 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575007 MW-6R EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575008 MW-7S EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575009 MW-7D EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575010 SW-1 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92258575011 SW-2 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-1 Lab ID:92258575001 Collected:07/11/15 16:05 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 18:52 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 18:52 7440-38-207/15/15 17:0010.0 2.5 1
Barium 79.2J ug/L 07/16/15 18:52 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 18:52 7440-41-707/15/15 17:001.0 0.50 1
Cadmium ND ug/L 07/16/15 18:52 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 18:52 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt 8.6J ug/L 07/16/15 18:52 7440-48-407/15/15 17:0010.0 2.5 1
Copper 6.5J ug/L 07/16/15 18:52 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 18:52 7439-92-107/15/15 17:0010.0 2.5 1
Nickel 6.4J ug/L 07/16/15 18:52 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 18:52 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 18:52 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 18:52 7440-28-007/15/15 17:005.5 5.0 1
Vanadium ND ug/L 07/16/15 18:52 7440-62-207/15/15 17:0025.0 2.5 1
Zinc 19.7 ug/L 07/16/15 18:52 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 19:21 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 19:21 107-13-12001.9 1
Benzene 1.6 ug/L 07/16/15 19:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 19:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 19:21 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 19:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/16/15 19:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 19:21 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 19:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 19:21 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 19:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 19:21 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 19:21 67-66-35.0 0.14 1
Chloromethane 0.12J ug/L 07/16/15 19:21 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 19:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 19:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 19:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 19:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 19:21 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.3 ug/L 07/16/15 19:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 19:21 110-57-61001.0 1
1,1-Dichloroethane 17.7 ug/L 07/16/15 19:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/16/15 19:21 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 19:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 11.8 ug/L 07/16/15 19:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 19:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/16/15 19:21 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 19:21 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 19:21 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-1 Lab ID:92258575001 Collected:07/11/15 16:05 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 19:21 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 19:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 19:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/16/15 19:21 74-88-410.0 0.32 1
Methylene Chloride 2.7 ug/L 07/16/15 19:21 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 19:21 108-10-11000.33 1
Styrene ND ug/L 07/16/15 19:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 19:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 19:21 79-34-53.0 0.40 1
Tetrachloroethene 7.3 ug/L 07/16/15 19:21 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/16/15 19:21 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 19:21 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 19:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 19:21 79-00-51.0 0.29 1
Trichloroethene 11.2 ug/L 07/16/15 19:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 19:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 19:21 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 19:21 108-05-450.0 0.35 1
Vinyl chloride 1.5 ug/L 07/16/15 19:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 19:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)87 %07/16/15 19:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %07/16/15 19:21 17060-07-070-130 1
Toluene-d8 (S)100 %07/16/15 19:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-2 Lab ID:92258575002 Collected:07/11/15 12:05 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 19:24 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 19:24 7440-38-207/15/15 17:0010.0 2.5 1
Barium 451 ug/L 07/16/15 19:24 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 19:24 7440-41-707/15/15 17:001.0 0.50 1
Cadmium ND ug/L 07/16/15 19:24 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 19:24 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt ND ug/L 07/16/15 19:24 7440-48-407/15/15 17:0010.0 2.5 1
Copper ND ug/L 07/16/15 19:24 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 19:24 7439-92-107/15/15 17:0010.0 2.5 1
Nickel ND ug/L 07/16/15 19:24 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 19:24 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 19:24 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 19:24 7440-28-007/15/15 17:005.5 5.0 1
Vanadium ND ug/L 07/16/15 19:24 7440-62-207/15/15 17:0025.0 2.5 1
Zinc 12.1 ug/L 07/16/15 19:24 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 19:40 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 19:40 107-13-12001.9 1
Benzene ND ug/L 07/16/15 19:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 19:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 19:40 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 19:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/16/15 19:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 19:40 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 19:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 19:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 19:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 19:40 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 19:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/16/15 19:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 19:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 19:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 19:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 19:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 19:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/16/15 19:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 19:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/16/15 19:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/16/15 19:40 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 19:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/16/15 19:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 19:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/16/15 19:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 19:40 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 19:40 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-2 Lab ID:92258575002 Collected:07/11/15 12:05 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 19:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 19:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 19:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/16/15 19:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/16/15 19:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 19:40 108-10-11000.33 1
Styrene ND ug/L 07/16/15 19:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 19:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 19:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/16/15 19:40 127-18-41.0 0.46 1
Tetrahydrofuran 7.0J ug/L 07/16/15 19:40 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 19:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 19:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 19:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/16/15 19:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 19:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 19:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 19:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/16/15 19:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 19:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)88 %07/16/15 19:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %07/16/15 19:40 17060-07-070-130 1
Toluene-d8 (S)102 %07/16/15 19:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-3 Lab ID:92258575003 Collected:07/11/15 10:55 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 19:28 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 19:28 7440-38-207/15/15 17:0010.0 2.5 1
Barium 79.4J ug/L 07/16/15 19:28 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 19:28 7440-41-707/15/15 17:001.0 0.50 1
Cadmium ND ug/L 07/16/15 19:28 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 19:28 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt ND ug/L 07/16/15 19:28 7440-48-407/15/15 17:0010.0 2.5 1
Copper ND ug/L 07/16/15 19:28 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 19:28 7439-92-107/15/15 17:0010.0 2.5 1
Nickel ND ug/L 07/16/15 19:28 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 19:28 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 19:28 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 19:28 7440-28-007/15/15 17:005.5 5.0 1
Vanadium ND ug/L 07/16/15 19:28 7440-62-207/15/15 17:0025.0 2.5 1
Zinc ND ug/L 07/16/15 19:28 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 19:58 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 19:58 107-13-12001.9 1
Benzene ND ug/L 07/16/15 19:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 19:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 19:58 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 19:58 75-25-23.0 0.26 1
Bromomethane 3.5J ug/L 07/16/15 19:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 19:58 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 19:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 19:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 19:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 19:58 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 19:58 67-66-35.0 0.14 1
Chloromethane 0.11J ug/L 07/16/15 19:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 19:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 19:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 19:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 19:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 19:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/16/15 19:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 19:58 110-57-61001.0 1
1,1-Dichloroethane 21.3 ug/L 07/16/15 19:58 75-34-35.0 0.32 1
1,2-Dichloroethane 0.18J ug/L 07/16/15 19:58 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 19:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 8.0 ug/L 07/16/15 19:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 19:58 156-60-55.0 0.49 1
1,2-Dichloropropane 0.44J ug/L 07/16/15 19:58 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 19:58 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 19:58 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-3 Lab ID:92258575003 Collected:07/11/15 10:55 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 19:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 19:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 19:58 591-78-650.0 0.46 1
Iodomethane 4.3J ug/L 07/16/15 19:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/16/15 19:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 19:58 108-10-11000.33 1
Styrene ND ug/L 07/16/15 19:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 19:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 19:58 79-34-53.0 0.40 1
Tetrachloroethene 3.8 ug/L 07/16/15 19:58 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/16/15 19:58 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 19:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 19:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 19:58 79-00-51.0 0.29 1
Trichloroethene 4.7 ug/L 07/16/15 19:58 79-01-61.0 0.47 1
Trichlorofluoromethane 0.36J ug/L 07/16/15 19:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 19:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 19:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/16/15 19:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 19:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)88 %07/16/15 19:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %07/16/15 19:58 17060-07-070-130 1
Toluene-d8 (S)101 %07/16/15 19:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-3R Lab ID:92258575004 Collected:07/11/15 10:00 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 19:33 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 19:33 7440-38-207/15/15 17:0010.0 2.5 1
Barium 102 ug/L 07/16/15 19:33 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 19:33 7440-41-707/15/15 17:001.0 0.50 1
Cadmium 2.1 ug/L 07/16/15 19:33 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 19:33 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt ND ug/L 07/16/15 19:33 7440-48-407/15/15 17:0010.0 2.5 1
Copper ND ug/L 07/16/15 19:33 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 19:33 7439-92-107/15/15 17:0010.0 2.5 1
Nickel ND ug/L 07/16/15 19:33 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 19:33 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 19:33 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 19:33 7440-28-007/15/15 17:005.5 5.0 1
Vanadium 5.5J ug/L 07/16/15 19:33 7440-62-207/15/15 17:0025.0 2.5 1
Zinc 6.0J ug/L 07/16/15 19:33 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 20:16 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 20:16 107-13-12001.9 1
Benzene ND ug/L 07/16/15 20:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 20:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 20:16 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 20:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/16/15 20:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 20:16 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 20:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 20:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 20:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 20:16 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 20:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/16/15 20:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 20:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 20:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 20:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 20:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 20:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/16/15 20:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 20:16 110-57-61001.0 1
1,1-Dichloroethane 0.61J ug/L 07/16/15 20:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/16/15 20:16 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 20:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/16/15 20:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 20:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/16/15 20:16 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 20:16 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 20:16 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-3R Lab ID:92258575004 Collected:07/11/15 10:00 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 20:16 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 20:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 20:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/16/15 20:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/16/15 20:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 20:16 108-10-11000.33 1
Styrene ND ug/L 07/16/15 20:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 20:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 20:16 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/16/15 20:16 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/16/15 20:16 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 20:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 20:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 20:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/16/15 20:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 20:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 20:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 20:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/16/15 20:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 20:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)89 %07/16/15 20:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %07/16/15 20:16 17060-07-070-130 1
Toluene-d8 (S)101 %07/16/15 20:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-4 Lab ID:92258575005 Collected:07/11/15 11:30 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 19:39 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 19:39 7440-38-207/15/15 17:0010.0 2.5 1
Barium 20.7J ug/L 07/16/15 19:39 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 19:39 7440-41-707/15/15 17:001.0 0.50 1
Cadmium ND ug/L 07/16/15 19:39 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 19:39 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt ND ug/L 07/16/15 19:39 7440-48-407/15/15 17:0010.0 2.5 1
Copper ND ug/L 07/16/15 19:39 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 19:39 7439-92-107/15/15 17:0010.0 2.5 1
Nickel ND ug/L 07/16/15 19:39 7440-02-007/15/15 17:0050.0 2.5 1
Selenium 5.3J ug/L 07/16/15 19:39 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 19:39 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 19:39 7440-28-007/15/15 17:005.5 5.0 1
Vanadium ND ug/L 07/16/15 19:39 7440-62-207/15/15 17:0025.0 2.5 1
Zinc ND ug/L 07/16/15 19:39 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 20:34 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 20:34 107-13-12001.9 1
Benzene ND ug/L 07/16/15 20:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 20:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 20:34 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 20:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/16/15 20:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 20:34 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 20:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 20:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 20:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 20:34 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 20:34 67-66-35.0 0.14 1
Chloromethane 0.14J ug/L 07/16/15 20:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 20:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 20:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 20:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 20:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 20:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/16/15 20:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 20:34 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/16/15 20:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/16/15 20:34 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 20:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/16/15 20:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 20:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/16/15 20:34 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 20:34 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 20:34 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-4 Lab ID:92258575005 Collected:07/11/15 11:30 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 20:34 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 20:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 20:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/16/15 20:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/16/15 20:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 20:34 108-10-11000.33 1
Styrene ND ug/L 07/16/15 20:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 20:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 20:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/16/15 20:34 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/16/15 20:34 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 20:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 20:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 20:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/16/15 20:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 20:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 20:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 20:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/16/15 20:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 20:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)90 %07/16/15 20:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %07/16/15 20:34 17060-07-070-130 1
Toluene-d8 (S)103 %07/16/15 20:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-6 Lab ID:92258575006 Collected:07/11/15 14:30 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 19:45 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 19:45 7440-38-207/15/15 17:0010.0 2.5 1
Barium 503 ug/L 07/16/15 19:45 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 19:45 7440-41-707/15/15 17:001.0 0.50 1
Cadmium 2.3 ug/L 07/16/15 19:45 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 19:45 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt 42.6 ug/L 07/16/15 19:45 7440-48-407/15/15 17:0010.0 2.5 1
Copper ND ug/L 07/16/15 19:45 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 19:45 7439-92-107/15/15 17:0010.0 2.5 1
Nickel 2.8J ug/L 07/16/15 19:45 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 19:45 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 19:45 7440-22-407/15/15 17:0010.0 2.5 1
Thallium 5.1J ug/L 07/16/15 19:45 7440-28-007/15/15 17:005.5 5.0 1
Vanadium ND ug/L 07/16/15 19:45 7440-62-207/15/15 17:0025.0 2.5 1
Zinc ND ug/L 07/16/15 19:45 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 20:52 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 20:52 107-13-12001.9 1
Benzene 4.7 ug/L 07/16/15 20:52 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 20:52 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 20:52 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 20:52 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/16/15 20:52 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 20:52 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 20:52 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 20:52 56-23-51.0 0.25 1
Chlorobenzene 1.4J ug/L 07/16/15 20:52 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 20:52 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 20:52 67-66-35.0 0.14 1
Chloromethane 0.18J ug/L 07/16/15 20:52 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 20:52 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 20:52 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 20:52 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 20:52 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.80J ug/L 07/16/15 20:52 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.3 ug/L 07/16/15 20:52 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 20:52 110-57-61001.0 1
1,1-Dichloroethane 4.0J ug/L 07/16/15 20:52 75-34-35.0 0.32 1
1,2-Dichloroethane 2.1 ug/L 07/16/15 20:52 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 20:52 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 21.8 ug/L 07/16/15 20:52 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 20:52 156-60-55.0 0.49 1
1,2-Dichloropropane 1.3 ug/L 07/16/15 20:52 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 20:52 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 20:52 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-6 Lab ID:92258575006 Collected:07/11/15 14:30 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 20:52 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 20:52 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 20:52 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/16/15 20:52 74-88-410.0 0.32 1
Methylene Chloride 1.0 ug/L 07/16/15 20:52 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 20:52 108-10-11000.33 1
Styrene ND ug/L 07/16/15 20:52 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 20:52 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 20:52 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/16/15 20:52 127-18-41.0 0.46 1
Tetrahydrofuran 72.7 ug/L 07/16/15 20:52 109-99-910.0 3.1 1
Toluene 0.50J ug/L 07/16/15 20:52 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 20:52 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 20:52 79-00-51.0 0.29 1
Trichloroethene 0.70J ug/L 07/16/15 20:52 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 20:52 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 20:52 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 20:52 108-05-450.0 0.35 1
Vinyl chloride 4.4 ug/L 07/16/15 20:52 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 20:52 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)86 %07/16/15 20:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %07/16/15 20:52 17060-07-070-130 1
Toluene-d8 (S)102 %07/16/15 20:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-6R Lab ID:92258575007 Collected:07/11/15 13:40 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 19:51 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 19:51 7440-38-207/15/15 17:0010.0 2.5 1
Barium 76.0J ug/L 07/16/15 19:51 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 19:51 7440-41-707/15/15 17:001.0 0.50 1
Cadmium ND ug/L 07/16/15 19:51 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 19:51 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt ND ug/L 07/16/15 19:51 7440-48-407/15/15 17:0010.0 2.5 1
Copper 2.8J ug/L 07/16/15 19:51 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 19:51 7439-92-107/15/15 17:0010.0 2.5 1
Nickel ND ug/L 07/16/15 19:51 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 19:51 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 19:51 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 19:51 7440-28-007/15/15 17:005.5 5.0 1
Vanadium ND ug/L 07/16/15 19:51 7440-62-207/15/15 17:0025.0 2.5 1
Zinc 20.9 ug/L 07/16/15 19:51 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 21:10 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 21:10 107-13-12001.9 1
Benzene ND ug/L 07/16/15 21:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 21:10 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 21:10 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 21:10 75-25-23.0 0.26 1
Bromomethane 3.6J ug/L 07/16/15 21:10 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 21:10 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 21:10 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 21:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 21:10 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 21:10 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 21:10 67-66-35.0 0.14 1
Chloromethane 0.17J ug/L 07/16/15 21:10 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 21:10 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 21:10 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 21:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 21:10 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 21:10 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.63J ug/L 07/16/15 21:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 21:10 110-57-61001.0 1
1,1-Dichloroethane 1.8J ug/L 07/16/15 21:10 75-34-35.0 0.32 1
1,2-Dichloroethane 0.27J ug/L 07/16/15 21:10 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 21:10 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.7J ug/L 07/16/15 21:10 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 21:10 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/16/15 21:10 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 21:10 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 21:10 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-6R Lab ID:92258575007 Collected:07/11/15 13:40 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 21:10 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 21:10 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 21:10 591-78-650.0 0.46 1
Iodomethane 4.5J ug/L 07/16/15 21:10 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/16/15 21:10 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 21:10 108-10-11000.33 1
Styrene ND ug/L 07/16/15 21:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 21:10 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 21:10 79-34-53.0 0.40 1
Tetrachloroethene 2.2 ug/L 07/16/15 21:10 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/16/15 21:10 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 21:10 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 21:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 21:10 79-00-51.0 0.29 1
Trichloroethene 3.4 ug/L 07/16/15 21:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 21:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 21:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 21:10 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/16/15 21:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 21:10 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)88 %07/16/15 21:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %07/16/15 21:10 17060-07-070-130 1
Toluene-d8 (S)102 %07/16/15 21:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-7S Lab ID:92258575008 Collected:07/11/15 15:40 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 19:59 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 19:59 7440-38-207/15/15 17:0010.0 2.5 1
Barium 72.5J ug/L 07/16/15 19:59 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 19:59 7440-41-707/15/15 17:001.0 0.50 1
Cadmium ND ug/L 07/16/15 19:59 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 19:59 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt ND ug/L 07/16/15 19:59 7440-48-407/15/15 17:0010.0 2.5 1
Copper ND ug/L 07/16/15 19:59 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 19:59 7439-92-107/15/15 17:0010.0 2.5 1
Nickel ND ug/L 07/16/15 19:59 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 19:59 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 19:59 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 19:59 7440-28-007/15/15 17:005.5 5.0 1
Vanadium ND ug/L 07/16/15 19:59 7440-62-207/15/15 17:0025.0 2.5 1
Zinc 9.1J ug/L 07/16/15 19:59 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 21:28 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 21:28 107-13-12001.9 1
Benzene ND ug/L 07/16/15 21:28 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 21:28 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 21:28 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 21:28 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/16/15 21:28 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 21:28 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 21:28 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 21:28 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 21:28 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 21:28 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 21:28 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/16/15 21:28 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 21:28 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 21:28 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 21:28 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 21:28 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 21:28 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/16/15 21:28 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 21:28 110-57-61001.0 1
1,1-Dichloroethane 1.9J ug/L 07/16/15 21:28 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/16/15 21:28 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 21:28 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/16/15 21:28 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 21:28 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/16/15 21:28 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 21:28 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 21:28 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-7S Lab ID:92258575008 Collected:07/11/15 15:40 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 21:28 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 21:28 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 21:28 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/16/15 21:28 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/16/15 21:28 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 21:28 108-10-11000.33 1
Styrene ND ug/L 07/16/15 21:28 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 21:28 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 21:28 79-34-53.0 0.40 1
Tetrachloroethene 8.0 ug/L 07/16/15 21:28 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/16/15 21:28 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 21:28 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 21:28 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 21:28 79-00-51.0 0.29 1
Trichloroethene 1.9 ug/L 07/16/15 21:28 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 21:28 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 21:28 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 21:28 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/16/15 21:28 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 21:28 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)88 %07/16/15 21:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %07/16/15 21:28 17060-07-070-130 1
Toluene-d8 (S)103 %07/16/15 21:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-7D Lab ID:92258575009 Collected:07/11/15 15:10 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 20:02 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 20:02 7440-38-207/15/15 17:0010.0 2.5 1
Barium 19.2J ug/L 07/16/15 20:02 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 20:02 7440-41-707/15/15 17:001.0 0.50 1
Cadmium ND ug/L 07/16/15 20:02 7440-43-907/15/15 17:001.0 0.50 1
Chromium 8.2J ug/L 07/16/15 20:02 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt ND ug/L 07/16/15 20:02 7440-48-407/15/15 17:0010.0 2.5 1
Copper ND ug/L 07/16/15 20:02 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 20:02 7439-92-107/15/15 17:0010.0 2.5 1
Nickel ND ug/L 07/16/15 20:02 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 20:02 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 20:02 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 20:02 7440-28-007/15/15 17:005.5 5.0 1
Vanadium 19.0J ug/L 07/16/15 20:02 7440-62-207/15/15 17:0025.0 2.5 1
Zinc ND ug/L 07/16/15 20:02 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 21:46 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 21:46 107-13-12001.9 1
Benzene ND ug/L 07/16/15 21:46 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 21:46 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 21:46 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 21:46 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/16/15 21:46 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 21:46 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 21:46 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 21:46 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 21:46 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 21:46 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 21:46 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/16/15 21:46 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 21:46 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 21:46 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 21:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 21:46 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 21:46 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/16/15 21:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 21:46 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/16/15 21:46 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/16/15 21:46 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 21:46 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/16/15 21:46 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 21:46 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/16/15 21:46 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 21:46 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 21:46 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:MW-7D Lab ID:92258575009 Collected:07/11/15 15:10 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 21:46 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 21:46 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 21:46 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/16/15 21:46 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/16/15 21:46 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 21:46 108-10-11000.33 1
Styrene ND ug/L 07/16/15 21:46 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 21:46 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 21:46 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/16/15 21:46 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/16/15 21:46 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 21:46 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 21:46 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 21:46 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/16/15 21:46 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 21:46 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 21:46 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 21:46 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/16/15 21:46 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 21:46 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)90 %07/16/15 21:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %07/16/15 21:46 17060-07-070-130 1
Toluene-d8 (S)101 %07/16/15 21:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:SW-1 Lab ID:92258575010 Collected:07/11/15 09:15 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 20:18 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 20:18 7440-38-207/15/15 17:0010.0 2.5 1
Barium 44.5J ug/L 07/16/15 20:18 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 20:18 7440-41-707/15/15 17:001.0 0.50 1
Cadmium ND ug/L 07/16/15 20:18 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 20:18 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt ND ug/L 07/16/15 20:18 7440-48-407/15/15 17:0010.0 2.5 1
Copper ND ug/L 07/16/15 20:18 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 20:18 7439-92-107/15/15 17:0010.0 2.5 1
Nickel ND ug/L 07/16/15 20:18 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 20:18 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 20:18 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 20:18 7440-28-007/15/15 17:005.5 5.0 1
Vanadium ND ug/L 07/16/15 20:18 7440-62-207/15/15 17:0025.0 2.5 1
Zinc ND ug/L 07/16/15 20:18 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 22:04 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 22:04 107-13-12001.9 1
Benzene ND ug/L 07/16/15 22:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 22:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 22:04 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 22:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/16/15 22:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 22:04 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 22:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 22:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 22:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 22:04 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 22:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/16/15 22:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 22:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 22:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 22:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 22:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 22:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/16/15 22:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 22:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/16/15 22:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/16/15 22:04 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 22:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/16/15 22:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 22:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/16/15 22:04 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 22:04 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 22:04 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
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[phone]
Page 23 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:SW-1 Lab ID:92258575010 Collected:07/11/15 09:15 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 22:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 22:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 22:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/16/15 22:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/16/15 22:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 22:04 108-10-11000.33 1
Styrene ND ug/L 07/16/15 22:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 22:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 22:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/16/15 22:04 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/16/15 22:04 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 22:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 22:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 22:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/16/15 22:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 22:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 22:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 22:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/16/15 22:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 22:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)91 %07/16/15 22:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %07/16/15 22:04 17060-07-070-130 1
Toluene-d8 (S)104 %07/16/15 22:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
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[phone]
Page 24 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:SW-2 Lab ID:92258575011 Collected:07/11/15 10:20 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/16/15 20:22 7440-36-007/15/15 17:006.0 3.8 1
Arsenic ND ug/L 07/16/15 20:22 7440-38-207/15/15 17:0010.0 2.5 1
Barium 44.5J ug/L 07/16/15 20:22 7440-39-307/15/15 17:001002.5 1
Beryllium ND ug/L 07/16/15 20:22 7440-41-707/15/15 17:001.0 0.50 1
Cadmium ND ug/L 07/16/15 20:22 7440-43-907/15/15 17:001.0 0.50 1
Chromium ND ug/L 07/16/15 20:22 7440-47-307/15/15 17:0010.0 2.5 1
Cobalt ND ug/L 07/16/15 20:22 7440-48-407/15/15 17:0010.0 2.5 1
Copper ND ug/L 07/16/15 20:22 7440-50-807/15/15 17:0010.0 2.5 1
Lead ND ug/L 07/16/15 20:22 7439-92-107/15/15 17:0010.0 2.5 1
Nickel 3.0J ug/L 07/16/15 20:22 7440-02-007/15/15 17:0050.0 2.5 1
Selenium ND ug/L 07/16/15 20:22 7782-49-207/15/15 17:0010.0 5.0 1
Silver ND ug/L 07/16/15 20:22 7440-22-407/15/15 17:0010.0 2.5 1
Thallium ND ug/L 07/16/15 20:22 7440-28-007/15/15 17:005.5 5.0 1
Vanadium ND ug/L 07/16/15 20:22 7440-62-207/15/15 17:0025.0 2.5 1
Zinc ND ug/L 07/16/15 20:22 7440-66-607/15/15 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/16/15 22:40 67-64-110010.0 1
Acrylonitrile ND ug/L 07/16/15 22:40 107-13-12001.9 1
Benzene ND ug/L 07/16/15 22:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/16/15 22:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/16/15 22:40 75-27-41.0 0.18 1
Bromoform ND ug/L 07/16/15 22:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/16/15 22:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/16/15 22:40 78-93-31000.96 1
Carbon disulfide ND ug/L 07/16/15 22:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/16/15 22:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/16/15 22:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/16/15 22:40 75-00-310.0 0.54 1
Chloroform ND ug/L 07/16/15 22:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/16/15 22:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/15 22:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/16/15 22:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/15 22:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/16/15 22:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/16/15 22:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/16/15 22:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/16/15 22:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/16/15 22:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/16/15 22:40 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 07/16/15 22:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/16/15 22:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/16/15 22:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/16/15 22:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/16/15 22:40 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/16/15 22:40 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Sample:SW-2 Lab ID:92258575011 Collected:07/11/15 10:20 Received:07/14/15 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/16/15 22:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/16/15 22:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/16/15 22:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/16/15 22:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/16/15 22:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/15 22:40 108-10-11000.33 1
Styrene ND ug/L 07/16/15 22:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/15 22:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/15 22:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/16/15 22:40 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/16/15 22:40 109-99-910.0 3.1 1
Toluene ND ug/L 07/16/15 22:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/16/15 22:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/16/15 22:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/16/15 22:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/16/15 22:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/16/15 22:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/16/15 22:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/16/15 22:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/16/15 22:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)89 %07/16/15 22:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %07/16/15 22:40 17060-07-070-130 1
Toluene-d8 (S)102 %07/16/15 22:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19003
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92258575001, 92258575002, 92258575003, 92258575004, 92258575005, 92258575006, 92258575007,
92258575008, 92258575009, 92258575010, 92258575011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1509905
Associated Lab Samples:92258575001, 92258575002, 92258575003, 92258575004, 92258575005, 92258575006, 92258575007,
92258575008, 92258575009, 92258575010, 92258575011
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 07/16/15 18:41
Arsenic ug/L ND 10.0 07/16/15 18:41
Barium ug/L ND 100 07/16/15 18:41
Beryllium ug/L ND 1.0 07/16/15 18:41
Cadmium ug/L ND 1.0 07/16/15 18:41
Chromium ug/L ND 10.0 07/16/15 18:41
Cobalt ug/L ND 10.0 07/16/15 18:41
Copper ug/L ND 10.0 07/16/15 18:41
Lead ug/L ND 10.0 07/16/15 18:41
Nickel ug/L ND 50.0 07/16/15 18:41
Selenium ug/L ND 10.0 07/16/15 18:41
Silver ug/L ND 10.0 07/16/15 18:41
Thallium ug/L ND 5.5 07/16/15 18:41
Vanadium ug/L ND 25.0 07/16/15 18:41
Zinc ug/L ND 10.0 07/16/15 18:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1509906LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 447500 89 80-120
Arsenic ug/L 430500 86 80-120
Barium ug/L 434500 87 80-120
Beryllium ug/L 436500 87 80-120
Cadmium ug/L 424500 85 80-120
Chromium ug/L 435500 87 80-120
Cobalt ug/L 447500 89 80-120
Copper ug/L 439500 88 80-120
Lead ug/L 436500 87 80-120
Nickel ug/L 433500 87 80-120
Selenium ug/L 430500 86 80-120
Silver ug/L 221250 88 80-120
Thallium ug/L 428500 86 80-120
Vanadium ug/L 441500 88 80-120
Zinc ug/L 432500 86 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1509907MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92258575001
1509908
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 100 75-12589 12 25500ND499444
Arsenic ug/L 500 96 75-12586 11 25500ND480428
Barium ug/L 500 97 75-12586 10 2550079.2J 562 510
Beryllium ug/L 500 98 75-12587 12 25500ND491434
Cadmium ug/L 500 95 75-12584 12 25500ND476420
Chromium ug/L 500 98 75-12587 12 25500ND489434
Cobalt ug/L 500 100 75-12589 11 255008.6J 508 453
Copper ug/L 500 99 75-12588 12 255006.5J 500 444
Lead ug/L 500 97 75-12586 12 25500ND485428
Nickel ug/L 500 96 75-12586 11 255006.4J 486 435
Selenium ug/L 500 96 75-12585 13 25500ND481423
Silver ug/L 250 98 75-12588 11 25250ND245220
Thallium ug/L 500 95 75-12584 12 25500ND474422
Vanadium ug/L 500 99 75-12588 12 25500ND497440
Zinc ug/L 500 95 75-12586 10 2550019.7 497 449
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32615
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92258575001, 92258575002, 92258575003, 92258575004, 92258575005, 92258575006, 92258575007,
92258575008, 92258575009, 92258575010, 92258575011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1511711
Associated Lab Samples:92258575001, 92258575002, 92258575003, 92258575004, 92258575005, 92258575006, 92258575007,
92258575008, 92258575009, 92258575010, 92258575011
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/16/15 18:45
1,1,1-Trichloroethane ug/L ND 1.0 07/16/15 18:45
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/16/15 18:45
1,1,2-Trichloroethane ug/L ND 1.0 07/16/15 18:45
1,1-Dichloroethane ug/L ND 5.0 07/16/15 18:45
1,1-Dichloroethene ug/L ND 5.0 07/16/15 18:45
1,2,3-Trichloropropane ug/L ND 1.0 07/16/15 18:45
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/16/15 18:45
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/16/15 18:45
1,2-Dichlorobenzene ug/L ND 5.0 07/16/15 18:45
1,2-Dichloroethane ug/L ND 1.0 07/16/15 18:45
1,2-Dichloropropane ug/L ND 1.0 07/16/15 18:45
1,3-Dichloropropane ug/L ND 1.0 07/16/15 18:45
1,4-Dichlorobenzene ug/L ND 1.0 07/16/15 18:45
2-Butanone (MEK)ug/L ND 100 07/16/15 18:45
2-Hexanone ug/L ND 50.0 07/16/15 18:45
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/16/15 18:45
Acetone ug/L ND 100 07/16/15 18:45
Acrylonitrile ug/L ND 200 07/16/15 18:45
Benzene ug/L ND 1.0 07/16/15 18:45
Bromochloromethane ug/L ND 3.0 07/16/15 18:45
Bromodichloromethane ug/L ND 1.0 07/16/15 18:45
Bromoform ug/L ND 3.0 07/16/15 18:45
Bromomethane ug/L ND 10.0 07/16/15 18:45
Carbon disulfide ug/L ND 100 07/16/15 18:45
Carbon tetrachloride ug/L ND 1.0 07/16/15 18:45
Chlorobenzene ug/L ND 3.0 07/16/15 18:45
Chloroethane ug/L ND 10.0 07/16/15 18:45
Chloroform ug/L ND 5.0 07/16/15 18:45
Chloromethane ug/L ND 1.0 07/16/15 18:45
cis-1,2-Dichloroethene ug/L ND 5.0 07/16/15 18:45
cis-1,3-Dichloropropene ug/L ND 1.0 07/16/15 18:45
Dibromochloromethane ug/L ND 3.0 07/16/15 18:45
Dibromomethane ug/L ND 10.0 07/16/15 18:45
Ethylbenzene ug/L ND 1.0 07/16/15 18:45
Iodomethane ug/L ND 10.0 07/16/15 18:45
Methylene Chloride ug/L ND 1.0 07/16/15 18:45
Styrene ug/L ND 1.0 07/16/15 18:45
Tetrachloroethene ug/L ND 1.0 07/16/15 18:45
Tetrahydrofuran ug/L ND 10.0 07/16/15 18:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/20/2015 05:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1511711
Associated Lab Samples:92258575001, 92258575002, 92258575003, 92258575004, 92258575005, 92258575006, 92258575007,
92258575008, 92258575009, 92258575010, 92258575011
Matrix:Water
Analyzed
Toluene ug/L ND 1.0 07/16/15 18:45
trans-1,2-Dichloroethene ug/L ND 5.0 07/16/15 18:45
trans-1,3-Dichloropropene ug/L ND 1.0 07/16/15 18:45
trans-1,4-Dichloro-2-butene ug/L ND 100 07/16/15 18:45
Trichloroethene ug/L ND 1.0 07/16/15 18:45
Trichlorofluoromethane ug/L ND 1.0 07/16/15 18:45
Vinyl acetate ug/L ND 50.0 07/16/15 18:45
Vinyl chloride ug/L ND 1.0 07/16/15 18:45
Xylene (Total)ug/L ND 5.0 07/16/15 18:45
1,2-Dichloroethane-d4 (S)%99 70-130 07/16/15 18:45
4-Bromofluorobenzene (S)%90 70-130 07/16/15 18:45
Toluene-d8 (S)%102 70-130 07/16/15 18:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1511712LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.950 106 80-125
1,1,1-Trichloroethane ug/L 51.450 103 71-129
1,1,2,2-Tetrachloroethane ug/L 52.550 105 79-124
1,1,2-Trichloroethane ug/L 49.650 99 85-125
1,1-Dichloroethane ug/L 48.950 98 73-126
1,1-Dichloroethene ug/L 51.050 102 66-135
1,2,3-Trichloropropane ug/L 50.450 101 75-130
1,2-Dibromo-3-chloropropane ug/L 50.850 102 71-133
1,2-Dibromoethane (EDB)ug/L 52.950 106 83-124
1,2-Dichlorobenzene ug/L 53.750 107 80-133
1,2-Dichloroethane ug/L 47.050 94 67-128
1,2-Dichloropropane ug/L 50.250 100 75-132
1,3-Dichloropropane ug/L 52.550 105 76-131
1,4-Dichlorobenzene ug/L 53.450 107 78-130
2-Butanone (MEK)ug/L 102100 102 61-144
2-Hexanone ug/L 106100 106 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 91.6J100 92 48-146
Acrylonitrile ug/L 237250 95 40-160
Benzene ug/L 52.450 105 80-125
Bromochloromethane ug/L 49.750 99 71-125
Bromodichloromethane ug/L 52.950 106 78-124
Bromoform ug/L 53.350 107 71-128
Bromomethane ug/L 47.350 95 40-160
Carbon disulfide ug/L 52.2J50 104 50-160
Carbon tetrachloride ug/L 53.250 106 69-131
Chlorobenzene ug/L 53.750 107 81-122
REPORT OF LABORATORY ANALYSIS
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Page 30 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1511712LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroethane ug/L 45.250 90 39-148
Chloroform ug/L 49.350 99 73-127
Chloromethane ug/L 44.250 88 44-146
cis-1,2-Dichloroethene ug/L 49.450 99 74-124
cis-1,3-Dichloropropene ug/L 52.250 104 72-132
Dibromochloromethane ug/L 54.450 109 78-125
Dibromomethane ug/L 49.550 99 82-120
Ethylbenzene ug/L 53.550 107 79-121
Iodomethane ug/L 109100 109 39-154
Methylene Chloride ug/L 48.850 98 64-133
Styrene ug/L 53.050 106 84-126
Tetrachloroethene ug/L 51.550 103 78-122
Tetrahydrofuran ug/L 501500 100 69-148
Toluene ug/L 51.750 103 80-121
trans-1,2-Dichloroethene ug/L 51.350 103 71-127
trans-1,3-Dichloropropene ug/L 52.550 105 69-141
trans-1,4-Dichloro-2-butene ug/L 57.6J50 115 40-160
Trichloroethene ug/L 51.750 103 78-122
Trichlorofluoromethane ug/L 45.150 90 53-137
Vinyl acetate ug/L 104100 104 40-160
Vinyl chloride ug/L 48.050 96 58-137
Xylene (Total)ug/L 148150 99 81-126
1,2-Dichloroethane-d4 (S)%109 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1511714MATRIX SPIKE SAMPLE:
MSSpike
Result
92258575011
1,1,1,2-Tetrachloroethane ug/L 19.620 98 70-130ND
1,1,1-Trichloroethane ug/L 20.720 104 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.320 101 70-130ND
1,1,2-Trichloroethane ug/L 20.020 100 70-130ND
1,1-Dichloroethane ug/L 21.520 107 70-130ND
1,1-Dichloroethene ug/L 22.820 114 70-166ND
1,2,3-Trichloropropane ug/L 19.120 95 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.420 82 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130ND
1,2-Dichlorobenzene ug/L 20.820 104 70-130ND
1,2-Dichloroethane ug/L 17.520 87 70-130ND
1,2-Dichloropropane ug/L 20.920 104 70-130ND
1,3-Dichloropropane ug/L 19.920 100 70-130ND
1,4-Dichlorobenzene ug/L 20.820 104 70-130ND
2-Butanone (MEK)ug/L 40.8J40 102 70-130ND
2-Hexanone ug/L 38.9J40 97 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 31 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1511714MATRIX SPIKE SAMPLE:
MSSpike
Result
92258575011
4-Methyl-2-pentanone (MIBK)ug/L 38.1J40 95 70-130ND
Acetone ug/L 42.8J40 98 70-130ND
Acrylonitrile ug/L 103J100 103 70-130ND
Benzene ug/L 22.220 111 70-148ND
Bromochloromethane ug/L 21.620 108 70-130ND
Bromodichloromethane ug/L 19.920 99 70-130ND
Bromoform ug/L 16.820 84 70-130ND
Bromomethane ug/L 22.020 110 70-130ND
Carbon disulfide ug/L 23.0J20 115 70-130ND
Carbon tetrachloride ug/L 20.720 103 70-130ND
Chlorobenzene ug/L 20.820 104 70-146ND
Chloroethane ug/L 21.320 107 70-130ND
Chloroform ug/L 21.020 105 70-130ND
Chloromethane ug/L 21.420 107 70-130ND
cis-1,2-Dichloroethene ug/L 21.220 106 70-130ND
cis-1,3-Dichloropropene ug/L 19.720 98 70-130ND
Dibromochloromethane ug/L 19.220 96 70-130ND
Dibromomethane ug/L 20.820 104 70-130ND
Ethylbenzene ug/L 20.720 103 70-130ND
Iodomethane ug/L 40.240 101 70-130ND
Methylene Chloride ug/L 21.620 108 70-130ND
Styrene ug/L 21.120 105 70-130ND
Tetrachloroethene ug/L 20.020 100 70-130ND
Tetrahydrofuran ug/L 198200 99 70-130ND
Toluene ug/L 22.120 110 70-155ND
trans-1,2-Dichloroethene ug/L 21.320 107 70-130ND
trans-1,3-Dichloropropene ug/L 19.020 95 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.3J20 91 70-130ND
Trichloroethene ug/L 21.520 108 69-151ND
Trichlorofluoromethane ug/L 19.220 96 70-130ND
Vinyl acetate ug/L 30.5J40 76 70-130ND
Vinyl chloride ug/L 22.820 114 70-130ND
1,2-Dichloroethane-d4 (S)%88 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92258575010
1511713SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 32 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92258575010
1511713SAMPLE DUPLICATE:
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.11J 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%98 199
4-Bromofluorobenzene (S)%88 391
Toluene-d8 (S)%103 2104
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
REPORT OF LABORATORY ANALYSIS
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Page 34 of 37
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92258575
IREDELL CLOSED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92258575001 MPRP/19003 ICP/17078MW-1 EPA 3010 EPA 6010
92258575002 MPRP/19003 ICP/17078MW-2 EPA 3010 EPA 6010
92258575003 MPRP/19003 ICP/17078MW-3 EPA 3010 EPA 6010
92258575004 MPRP/19003 ICP/17078MW-3R EPA 3010 EPA 6010
92258575005 MPRP/19003 ICP/17078MW-4 EPA 3010 EPA 6010
92258575006 MPRP/19003 ICP/17078MW-6 EPA 3010 EPA 6010
92258575007 MPRP/19003 ICP/17078MW-6R EPA 3010 EPA 6010
92258575008 MPRP/19003 ICP/17078MW-7S EPA 3010 EPA 6010
92258575009 MPRP/19003 ICP/17078MW-7D EPA 3010 EPA 6010
92258575010 MPRP/19003 ICP/17078SW-1 EPA 3010 EPA 6010
92258575011 MPRP/19003 ICP/17078SW-2 EPA 3010 EPA 6010
92258575001 MSV/32615MW-1 EPA 8260
92258575002 MSV/32615MW-2 EPA 8260
92258575003 MSV/32615MW-3 EPA 8260
92258575004 MSV/32615MW-3R EPA 8260
92258575005 MSV/32615MW-4 EPA 8260
92258575006 MSV/32615MW-6 EPA 8260
92258575007 MSV/32615MW-6R EPA 8260
92258575008 MSV/32615MW-7S EPA 8260
92258575009 MSV/32615MW-7D EPA 8260
92258575010 MSV/32615SW-1 EPA 8260
92258575011 MSV/32615SW-2 EPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 35 of 37
Page 36 of 37
Page 37 of 37
#=CL#
August 04, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92260267
92260267
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
IREDELL BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
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Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
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Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92260267001 EB Water 07/23/15 17:35 07/24/15 11:49
92260267002 FB Water 07/23/15 17:40 07/24/15 11:49
92260267003 TB Water 07/23/15 00:00 07/24/15 11:49
REPORT OF LABORATORY ANALYSIS
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Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92260267001 EB EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CSNP
92260267002 FB EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CSNP
92260267003 TB EPA 8260 52 PASI-CSNP
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:EB Lab ID:92260267001 Collected:07/23/15 17:35 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:36 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:36 7440-38-207/27/15 19:0010.0 2.5 1
Barium ND ug/L 08/04/15 03:36 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:36 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:36 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:36 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:36 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:36 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:36 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:36 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:36 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:36 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:36 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:36 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:36 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 19:48 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 19:48 107-13-12001.9 1
Benzene ND ug/L 07/28/15 19:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 19:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 19:48 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 19:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 19:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 19:48 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 19:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 19:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 19:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 19:48 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 19:48 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 19:48 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 19:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 19:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 19:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 19:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 19:48 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 19:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 19:48 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 19:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 19:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 19:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 19:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 19:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 19:48 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 19:48 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 19:48 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:EB Lab ID:92260267001 Collected:07/23/15 17:35 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 19:48 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 19:48 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 19:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 19:48 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 19:48 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 19:48 108-10-11000.33 1
Styrene ND ug/L 07/28/15 19:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 19:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 19:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 19:48 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/28/15 19:48 109-99-910.0 3.1 1
Toluene ND ug/L 07/28/15 19:48 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 19:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 19:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 19:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 19:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 19:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 19:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 19:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 19:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %07/28/15 19:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %07/28/15 19:48 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/15 19:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
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Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:FB Lab ID:92260267002 Collected:07/23/15 17:40 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:39 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:39 7440-38-207/27/15 19:0010.0 2.5 1
Barium ND ug/L 08/04/15 03:39 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:39 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:39 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:39 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:39 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:39 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:39 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:39 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:39 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:39 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:39 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:39 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:39 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 20:04 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 20:04 107-13-12001.9 1
Benzene ND ug/L 07/28/15 20:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 20:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 20:04 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 20:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 20:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 20:04 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 20:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 20:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 20:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 20:04 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 20:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 20:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 20:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 20:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 20:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 20:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 20:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 20:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 20:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 20:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 20:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 20:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 20:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 20:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 20:04 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 20:04 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 20:04 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
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Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:FB Lab ID:92260267002 Collected:07/23/15 17:40 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 20:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 20:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 20:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 20:04 74-88-410.0 0.32 1
Methylene Chloride 0.99J ug/L 07/28/15 20:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 20:04 108-10-11000.33 1
Styrene ND ug/L 07/28/15 20:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 20:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 20:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 20:04 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/28/15 20:04 109-99-910.0 3.1 1
Toluene ND ug/L 07/28/15 20:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 20:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 20:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 20:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 20:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 20:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 20:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 20:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 20:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %07/28/15 20:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %07/28/15 20:04 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 20:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:TB Lab ID:92260267003 Collected:07/23/15 00:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 20:21 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 20:21 107-13-12001.9 1
Benzene ND ug/L 07/28/15 20:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 20:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 20:21 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 20:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 20:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 20:21 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 20:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 20:21 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 20:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 20:21 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 20:21 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 20:21 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 20:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 20:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 20:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 20:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 20:21 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 20:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 20:21 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 20:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 20:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 20:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 20:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 20:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 20:21 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 20:21 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 20:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/28/15 20:21 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 20:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 20:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 20:21 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 20:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 20:21 108-10-11000.33 1
Styrene ND ug/L 07/28/15 20:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 20:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 20:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 20:21 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/28/15 20:21 109-99-910.0 3.1 1
Toluene ND ug/L 07/28/15 20:21 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 20:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 20:21 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 20:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 20:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 20:21 96-18-41.0 0.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:TB Lab ID:92260267003 Collected:07/23/15 00:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl acetate ND ug/L 07/28/15 20:21 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 20:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 20:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %07/28/15 20:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %07/28/15 20:21 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 20:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19105
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92260267001, 92260267002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519047
Associated Lab Samples:92260267001, 92260267002
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 08/04/15 02:28
Arsenic ug/L ND 10.0 08/04/15 02:28
Barium ug/L ND 100 08/04/15 02:28
Beryllium ug/L ND 1.0 08/04/15 02:28
Cadmium ug/L ND 1.0 08/04/15 02:28
Chromium ug/L ND 10.0 08/04/15 02:28
Cobalt ug/L ND 10.0 08/04/15 02:28
Copper ug/L ND 10.0 08/04/15 02:28
Lead ug/L ND 10.0 08/04/15 02:28
Nickel ug/L ND 50.0 08/04/15 02:28
Selenium ug/L ND 10.0 08/04/15 02:28
Silver ug/L ND 10.0 08/04/15 02:28
Thallium ug/L ND 5.5 08/04/15 02:28
Vanadium ug/L ND 25.0 08/04/15 02:28
Zinc ug/L ND 10.0 08/04/15 02:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519048LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 468500 94 80-120
Arsenic ug/L 455500 91 80-120
Barium ug/L 469500 94 80-120
Beryllium ug/L 476500 95 80-120
Cadmium ug/L 464500 93 80-120
Chromium ug/L 479500 96 80-120
Cobalt ug/L 466500 93 80-120
Copper ug/L 470500 94 80-120
Lead ug/L 460500 92 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 447500 89 80-120
Silver ug/L 228250 91 80-120
Thallium ug/L 466500 93 80-120
Vanadium ug/L 473500 95 80-120
Zinc ug/L 464500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1519049MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260261001
1519050
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12595 1 2550016.0 486 492
Arsenic ug/L 500 95 75-12596 1 2550016.4 492 496
Barium ug/L 500 93 75-125101 3 2550082312901330
Beryllium ug/L 500 94 75-12595 0 25500ND472474
Cadmium ug/L 500 94 75-12595 1 25500ND471475
Chromium ug/L 500 94 75-12595 1 2550038.8 508 515
Cobalt ug/L 500 88 75-12589 1 2550016.0 457 460
Copper ug/L 500 96 75-12599 2 2550029.9 512 524
Lead ug/L 500 85 75-12586 1 255003.5J 430 434
Nickel ug/L 500 86 75-12587 1 25500137569573
Selenium ug/L 500 89 75-12591 2 25500ND447454
Silver ug/L 250 94 75-12595 1 25250ND236239
Thallium ug/L 500 83 75-12583 1 25500ND413417
Vanadium ug/L 500 95 75-12596 1 2550019.9J 495 501
Zinc ug/L 500 89 75-12591 2 2550021.8 469 476
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32735
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92260267001, 92260267002, 92260267003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519691
Associated Lab Samples:92260267001, 92260267002, 92260267003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/28/15 13:58
1,1,1-Trichloroethane ug/L ND 1.0 07/28/15 13:58
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/28/15 13:58
1,1,2-Trichloroethane ug/L ND 1.0 07/28/15 13:58
1,1-Dichloroethane ug/L ND 5.0 07/28/15 13:58
1,1-Dichloroethene ug/L ND 5.0 07/28/15 13:58
1,2,3-Trichloropropane ug/L ND 1.0 07/28/15 13:58
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/28/15 13:58
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/28/15 13:58
1,2-Dichlorobenzene ug/L ND 5.0 07/28/15 13:58
1,2-Dichloroethane ug/L ND 1.0 07/28/15 13:58
1,2-Dichloropropane ug/L ND 1.0 07/28/15 13:58
1,3-Dichloropropane ug/L ND 1.0 07/28/15 13:58
1,4-Dichlorobenzene ug/L ND 1.0 07/28/15 13:58
2-Butanone (MEK)ug/L ND 100 07/28/15 13:58
2-Hexanone ug/L ND 50.0 07/28/15 13:58
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/28/15 13:58
Acetone ug/L ND 100 07/28/15 13:58
Acrylonitrile ug/L ND 200 07/28/15 13:58
Benzene ug/L ND 1.0 07/28/15 13:58
Bromochloromethane ug/L ND 3.0 07/28/15 13:58
Bromodichloromethane ug/L ND 1.0 07/28/15 13:58
Bromoform ug/L ND 3.0 07/28/15 13:58
Bromomethane ug/L ND 10.0 07/28/15 13:58
Carbon disulfide ug/L ND 100 07/28/15 13:58
Carbon tetrachloride ug/L ND 1.0 07/28/15 13:58
Chlorobenzene ug/L ND 3.0 07/28/15 13:58
Chloroethane ug/L ND 10.0 07/28/15 13:58
Chloroform ug/L ND 5.0 07/28/15 13:58
Chloromethane ug/L ND 1.0 07/28/15 13:58
cis-1,2-Dichloroethene ug/L ND 5.0 07/28/15 13:58
cis-1,3-Dichloropropene ug/L ND 1.0 07/28/15 13:58
Dibromochloromethane ug/L ND 3.0 07/28/15 13:58
Dibromomethane ug/L ND 10.0 07/28/15 13:58
Ethylbenzene ug/L ND 1.0 07/28/15 13:58
Iodomethane ug/L ND 10.0 07/28/15 13:58
Methylene Chloride ug/L ND 1.0 07/28/15 13:58
Styrene ug/L ND 1.0 07/28/15 13:58
Tetrachloroethene ug/L ND 1.0 07/28/15 13:58
Tetrahydrofuran ug/L ND 10.0 07/28/15 13:58
Toluene ug/L ND 1.0 07/28/15 13:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519691
Associated Lab Samples:92260267001, 92260267002, 92260267003
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 5.0 07/28/15 13:58
trans-1,3-Dichloropropene ug/L ND 1.0 07/28/15 13:58
trans-1,4-Dichloro-2-butene ug/L ND 100 07/28/15 13:58
Trichloroethene ug/L ND 1.0 07/28/15 13:58
Trichlorofluoromethane ug/L ND 1.0 07/28/15 13:58
Vinyl acetate ug/L ND 50.0 07/28/15 13:58
Vinyl chloride ug/L ND 1.0 07/28/15 13:58
Xylene (Total)ug/L ND 5.0 07/28/15 13:58
1,2-Dichloroethane-d4 (S)%104 70-130 07/28/15 13:58
4-Bromofluorobenzene (S)%102 70-130 07/28/15 13:58
Toluene-d8 (S)%100 70-130 07/28/15 13:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519692LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.550 101 80-125
1,1,1-Trichloroethane ug/L 50.150 100 71-129
1,1,2,2-Tetrachloroethane ug/L 52.550 105 79-124
1,1,2-Trichloroethane ug/L 50.850 102 85-125
1,1-Dichloroethane ug/L 46.350 93 73-126
1,1-Dichloroethene ug/L 49.050 98 66-135
1,2,3-Trichloropropane ug/L 53.150 106 75-130
1,2-Dibromo-3-chloropropane ug/L 46.950 94 71-133
1,2-Dibromoethane (EDB)ug/L 51.850 104 83-124
1,2-Dichlorobenzene ug/L 51.850 104 80-133
1,2-Dichloroethane ug/L 46.750 93 67-128
1,2-Dichloropropane ug/L 48.050 96 75-132
1,3-Dichloropropane ug/L 51.250 102 76-131
1,4-Dichlorobenzene ug/L 50.950 102 78-130
2-Butanone (MEK)ug/L 91.9J100 92 61-144
2-Hexanone ug/L 99.9100 100 68-143
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 72-135
Acetone ug/L 87.3J100 87 48-146
Acrylonitrile ug/L 221250 89 40-160
Benzene ug/L 49.650 99 80-125
Bromochloromethane ug/L 53.250 106 71-125
Bromodichloromethane ug/L 53.450 107 78-124
Bromoform ug/L 48.850 98 71-128
Bromomethane ug/L 41.050 82 40-160
Carbon disulfide ug/L 44.4J50 89 50-160
Carbon tetrachloride ug/L 52.850 106 69-131
Chlorobenzene ug/L 50.850 102 81-122
Chloroethane ug/L 44.050 88 39-148
Chloroform ug/L 49.650 99 73-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519692LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 41.050 82 44-146
cis-1,2-Dichloroethene ug/L 47.850 96 74-124
cis-1,3-Dichloropropene ug/L 51.050 102 72-132
Dibromochloromethane ug/L 51.950 104 78-125
Dibromomethane ug/L 52.050 104 82-120
Ethylbenzene ug/L 51.550 103 79-121
Iodomethane ug/L 86.0100 86 39-154
Methylene Chloride ug/L 48.150 96 64-133
Styrene ug/L 50.650 101 84-126
Tetrachloroethene ug/L 49.950 100 78-122
Tetrahydrofuran ug/L 457500 91 69-148
Toluene ug/L 50.950 102 80-121
trans-1,2-Dichloroethene ug/L 46.350 93 71-127
trans-1,3-Dichloropropene ug/L 51.550 103 69-141
trans-1,4-Dichloro-2-butene ug/L 52.2J50 104 40-160
Trichloroethene ug/L 47.050 94 78-122
Trichlorofluoromethane ug/L 49.850 100 53-137
Vinyl acetate ug/L 97.7100 98 40-160
Vinyl chloride ug/L 44.750 89 58-137
Xylene (Total)ug/L 150150 100 81-126
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92260267001 MPRP/19105 ICP/17174EBEPA 3010 EPA 6010
92260267002 MPRP/19105 ICP/17174FBEPA 3010 EPA 6010
92260267001 MSV/32735EBEPA 8260
92260267002 MSV/32735FBEPA 8260
92260267003 MSV/32735TBEPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 19
Page 18 of 19
Page 19 of 19
Appendix B
Field Sampling Parameter Data Sheet(s)