2608_FortBragg_GWMR_DIN28240_20141114

FINAL
November 2014 (N=29) GROUNDWATER AND METHANE MONITORING REPORT
FOR

THE LAMONT ROAD LCID (CLOSED) AND C&D LANDFILLS
NCDENR LANDFILL PERMIT #26-08

FORT BRAGG, NORTH CAROLINA

Prepared by:

US Army Corps of Engineers
Savannah District
Hazardous, Toxic & Radioactive Waste Section
CESAS-EN-GH
100 W. Oglethorpe Avenue
Savannah, GA 31401
March 2015

FINAL
November 2014 (N=29) GROUNDWATER AND
METHANE MONITORING REPORT

FOR
THE LAMONT ROAD LCID (CLOSED) AND C&D LANDFILLS NCDENR LANDFILL PERMIT #26-08

FORT BRAGG, NORTH CAROLINA

Prepared by:
US Army Corps of Engineers Savannah District Hazardous, Toxic & Radioactive Waste Section
CESAS-EN-GH
100 W. Oglethorpe Avenue
Savannah, GA 31401

March 2015

Prepared by: Date

_____________________ 3/13/15 Kevin Haborak, P.G.

TABLE OF CONTENTS
SECTION PAGE

1.0 INTRODUCTION .......................................................................................................................... 1
1.1 Project Background ............................................................................................. 1
1.2 Project Scope ...................................................................................................... 2
2.0 PROJECT HISTORY .................................................................................................................... 3
2.1 Site Description and History ............................................................................... 3
2.2 General Site Geology and Hydrology ................................................................. 3
2.3 Previous Investigation and Results ..................................................................... 4
3.0 METHODS ..................................................................................................................................... 5
3.1 Methane Monitoring ........................................................................................... 5
3.2 Water-Level Gauging.......................................................................................... 5
3.3 Groundwater Sampling ....................................................................................... 5
3.4 Investigation Derived Wastes Handling ............................................................. 6
4.0 ANALYTICAL RESULTS AND STATISTICAL ANALYSIS ................................................. 8
4.1 Analytical Data Summary ................................................................................... 8
4.2 Statistical Analysis Results ................................................................................. 9
4.3 Methane Monitoring Results ............................................................................. 10
CONCLUSIONS AND RECOMMENATIONS .......................................................................................11
5.0 REFERENCES ..............................................................................................................................12
In Order
Following Page 11

ii
FIGURES

Figure 1 Site Map – Ft. Bragg, NC
Figure 2 Location Map – Lamont Road Landfill, Ft. Bragg, NC
Figure 3 Methane Monitoring Results
Figure 4 Potentiometric Map
Figure 5 Groundwater Analytical Results
TABLES
Table 1 Methane Monitoring Results

Table 2 Groundwater Elevation Data
Table 3 Field Parameter Measurements Table 4 Summary of Groundwater Detections

APPENDICES

Appendix A – Groundwater Sampling Logs
Appendix B – Chains of Custody and Laboratory Analytical Reports
Appendix C – Statistical Reports
Appendix D – Historical Data

iii
LIST OF ACRONYMS

C&D Construction and Demolition COCs Chemicals of Concern
DPW Directorate of Public Works
IDW Investigation Derived Waste
LCID Land Clearing and Inert Debris
µg/L Micrograms Per Liter
MSWLF Municipal Solid Waste Landfill Facility
NC2L North Carolina Administrative Code, Title 15A, Subchapter 2L
NCDENR North Carolina Department of Environmental and Natural Resources RCRA Resource Conservation and Recovery Act SAP Sampling and Analysis Plan
SSI Statistically Significant Increase
USACE US Army Corps of Engineers
VOCs Volatile Organic Compounds

1
FINAL November 2014 (N=29) GROUNDWATER AND
METHANE MONITORING REPORT FOR
THE LAMONT ROAD LCID (CLOSED) AND C&D LANDFILLS NCDENR LANDFILL PERMIT #26-08 FORT BRAGG, NORTH CAROLINA

1.0 INTRODUCTION
This is the Report for the November 2014 groundwater and methane monitoring
at the Lamont Road Landfills (Figure 1) performed by the United States Army Corps of
Engineers (USACE), Savannah District in November 2014. The monitoring is required
by the North Carolina Department of Environmental and Natural Resources (NCDENR)
Solid Waste Management Division. This was the twenty-ninth (N=29) event performed
for the Site. This report summarizes the methods used for the groundwater and methane
monitoring and presents the results of the sampling event.

1.1 Project Background The USACE was contracted by the Directorate of Public Works (DPW), Fort
Bragg, North Carolina to perform groundwater sampling and methane monitoring. The
original groundwater monitoring well network for the land clearing and inert debris
(LCID) and construction and demolition (C&D) landfills consisted of 12 wells. Four of
the original eleven monitoring wells have been permanently abandoned and replaced with
new wells at different locations. An additional two wells have also been installed. The
current Sampling and Analysis Plan (SAP), approved by NCDENR, includes sampling
these 13 monitoring wells. The monitoring wells are LMW-3, LMW-3S, LMW-4R,
LMW-6, LMW-7, LMW-8, LMW-9, LMW-9S, LMW-9D, LMW-10, LMW-14R, LMW-
15R, and LMW-16. Groundwater monitoring locations are shown on Figure 2. Only 11
of the 13 wells could be sampled during this event, all sampling was conducted according
to North Carolina Solid Waste Management Guidelines.

2
1.2 Project Scope
The scope for this project included collecting groundwater samples from 12
monitoring wells at the Lamont Road LCID and C&D Landfill for analyses of Appendix
I constituents, sampling for methane at 13 selected methane monitoring wells and at three
additional buildings, evaluating the analytical results, and reporting the results of the
investigation. The groundwater sampling and data analyses included obtaining field
parameter measurements (i.e. pH, temperature, etc.), measuring water levels at the
monitoring well locations, determining groundwater flow directions, validating
laboratory analytical data, performing statistical analysis for each detected constituent as
required by NC regulations, and determining the concentration changes of chemicals of
concern (COCs) with time.

3
2.0 PROJECT HISTORY
2.1 Site Description and History

The Lamont Road LCID and C&D Landfills are on the west side of Cooleyconch
Mountain (Figure 2). The site was previously utilized as a maneuver training area
(conducted continuously for 50 years), a borrow pit for sands and clays, and a repository
for unclassified debris from land clearing and construction demolition. The LCID
Landfill started as an uncontrolled dump site which was associated with reclaiming
borrow excavation. Its initial operation pre-dated Federal and State regulations
governing waste disposal. The LCID Landfill has been operated as a controlled
repository for C&D debris as well as for land clearing and inert debris since its permitting
under NCDENR Permit No. 26C on August 28, 1987. From February 1993 to date of
closure, C&D debris was diverted to the Longstreet Road Sanitary Landfill, and only
LCID has been accepted at the LCID Landfill site. It is presumed that asbestos materials
are disposed of in this landfill.

Cooleyconch Mountain is the prominent terrain feature west of the main post.
The LCID Landfill site is 1.5 miles west of the Longstreet Road municipal solid waste
landfill (MSWLF) (closed January 1, 1998) and 200 yards northwest of the Lamont Road
C&D Landfill. The area adjacent and east of the LCID Landfill has been excavated to be
used as a borrow pit for sandy fill material. To the south of the LCID Landfill, in the
C&D Landfill site, petroleum contaminated soils have been spread, dried, and stored for
subsequent removal. To the east of the LCID Landfill, petroleum contaminated sludge
has been stored in earthen impoundments for subsequent removal. The LCID Landfill
drains north to Cypress Creek, which intersects the Little River a mile upstream of the
Fort Bragg Water Plant intake.

2.2 General Site Geology and Hydrology

Lithologic descriptions of soil borings and monitoring well borings from previous
investigations at Fort Bragg indicate that in general Fort Bragg is underlain by alternating
sands, silty sands, clayey sands, sandy clays, and clays, likely belonging to the

4
Middendorf Formation. The sands and silty sands range in thickness from
approximately 2 to 22 ft and are coarse grained. The clay units range in thickness from
approximately 2 to 7 ft and are typically plastic.

2.3 Previous Investigation and Results

Several sampling events have been conducted at the landfills. Initially, four
monthly sampling events were conducted in July, August, September, and October 1996
by R,S & H Architect, Engineering, & Planning, Inc. Law & Company, Inc. conducted
two sampling events in March and September, 1999 in conjunction with the installation
of new wells. Then until 2005, sampling events were conducted by BPA Environmental
& Engineering, Inc. The USACE has monitored the site since 2005.

The previous sampling event, held in May of 2014 for Lamont Landfill, was
conducted by the USACE, Savannah District. Low levels of Appendix I VOCs and
metals were detected. All of the detections were below their respective NC2L standards
and according to the statistical analysis there was no evidence that showed an increasing
contaminant concentration trend.

5
METHODS

2.4 Methane Monitoring

Methane monitoring was performed at 12 wells and at two additional buildings.
The monitoring included measuring levels of methane, carbon dioxide, and oxygen at
each location. The results of the monitoring are summarized in Table 1 and are also
presented on Figure 3.

2.5 Water-Level Gauging During this sampling event, USACE personnel measured the water levels in 10
monitoring wells. Observed water levels and calculated groundwater elevations are
presented in Table 2. A potentiometric map was developed based on the groundwater
elevations; the map is presented as Figure 4. The map shows that the general direction of
the groundwater flow at the Lamont Landfill is towards the west-northwest.

2.6 Groundwater Sampling
The groundwater sampling was conducted in accordance with the SAP for the
Lamont Road LCID and C&D Landfills (NCDENR Landfill Permits # 26G and #26-08
dated April 2005, which have been updated to reflect the most recent SAP).
Groundwater samples were collected from 10 wells, monitoring wells LMW-7 and
LMW-8 were not sampled due to the wells being dry. Water quality parameters pH,
specific conductivity, temperature, turbidity, dissolved oxygen (DO), and oxidation-
reduction potential (ORP) were measured during the purge cycle of each well. The
measurements are summarized in Table 3.

Groundwater samples were collected using a low-flow purge method with either a
bladder pump or a peristaltic pump. Immediately before purging a well, the static water
level below the top of the well casing and the total depth of the well were measured to the
nearest 0.01 foot and recorded in the field notebook. The volume of water in the well
was calculated based on the static water level and the well construction information.

6
Well volume calculations were placed in the field notebook. The inlet of the sampling
pump was placed at the mid-point of the screened interval. This level was adjusted for
wells where the static water level is within the well screen. The monitoring wells were
purged using a variable-flow bladder pump or peristaltic pump at a rate of 500 ml/min or
less.

The wells were purged until the water quality had stabilized or five purge volumes
were removed. The wells were considered stable when the following requirements were
met for three consecutive readings: turbidity values within 10% or lower than 10
Nephelometric Turbidity Units (NTUs), temperature values within a range of 0.5 degrees
Celcius, pH readings within 0.1 Standard Units (SU), ORP values within a range of 10
milivolts (mV), and conductivity values within 3%, and DO values within 10%.

The rate of pumping was determined and noted in the field notebook. The purge
rate was adjusted, as necessary, to avoid purging any well to dryness and to equal the
recharge of the aquifer. All sampling equipment was protected from contaminated soil
surfaces to prevent contamination of the samples (e.g., equipment may be placed on
disposable polyethylene plastic sheeting). Groundwater samples were collected after
purging was complete. The tubing was disconnected from the flow through cell, and the
samples were collected from the pump outlet. The samples were labeled and placed into
an ice-filled cooler for preservation.

Groundwater sampling data (including sample number, location, quantity of water
purged, field parameters, site conditions, etc.) were documented in the field notebook.
Water samples for Resource Conservation and Recovery Act (RCRA) metal analyses
were un-filtered. The results of the groundwater sampling are presented in Table 4 and
on Figure 5. The groundwater sampling field data logs are presented in Appendix A.

2.7 Investigation Derived Wastes Handling

The investigation derived wastes (IDW), including the waste water from well
purging and decontamination water, were containerized in 55-gallon drums. Those

7
drums were appropriately labeled, sealed, and staged within designated areas until
analytical results had been received and reviewed. Based on the analytical results of the
groundwater samples, the IDW was classified as non-hazardous. With the concurrence of
the Fort Bragg Installation Restoration Program Manager, the IDW was disposed of at an
appropriate disposal facility.

8
3.0 ANALYTICAL RESULTS AND STATISTICAL ANALYSIS
3.1 Analytical Data Summary Groundwater samples collected in November 2014 were analyzed for Appendix I
VOCs and metals. The summary of detections of the COCs is presented in Table 4.
Figure 5 shows the distribution of the detections and their concentrations from this
sampling event. The laboratory reports of analytical results are included as Appendix B.
The Statistical Analyses Summary Report included in Appendix C. For comparison,
the analytical results of previous investigations are presented in Appendix D.

In accordance with North Carolina guidance, analytical results are compared to
North Carolina Groundwater 2L Standards (NC2L standards). The analytical data of the
second 2014 sampling event indicated that some VOCs were detected at low levels. Two
sampling locations had detections exceeding the NC2L standards: wells LMW-6 and
LMW-15R (Table 4). The analytical results for each of those wells are shown below:

• Well LMW-6
One compound was detected above the 2L standard as listed below:
Compound 2L Concentration Nitrate 1,000 J µg/L 2,200 J µg/L
No other constituents were above their 2L standards.

• Well LMW-15R
One compound was detected above the 2L standard as listed below:
Compound 2L Concentration Nitrate 1,000 µg/L 1,100 µg/L

These exceedances are new detections and will be confirmed in the May 2015
sampling event. No other constituents were above their 2L standards.

9
3.2 Statistical Analysis Results
A statistical test predicts the average behavior (distribution) of a random variable
by comparing the means (normal distribution) or medians (lognormal and non-parametric
distributions) of the compliance well data to background well data. Different statistical
tests were used as appropriate for the different distributional patterns that occur within
the data. Prior to testing for statistical significance, the distribution of each parameter
was determined to be normal, lognormal, or non-normal.

If the data were non-normally distributed, or the fraction of nondetects exceeded
15% but were less than 90%, then the Kruskal-Wallis Test was applied. If the fraction of
non-detects exceeded 90%, then the Non-Parametric Prediction Limit was applied. For
these tests to be sufficiently sensitive, the sample size for any group must be at least 4. A
Kruskal-Wallis Test can be used in any situation that the parametric analysis of variance
can be used. This test computes the H-statistic, adjusts it for ties, and compares it to the
appropriate chi-square critical value. If the H-statistic is less than the critical value, the
null-hypothesis is accepted, and it is concluded that there are no differences between
median background and compliance well concentrations. If the H-statistic is greater than
the critical value, it is concluded that at least one pair of well groups is statistically
different. However, the Kruskal-Wallis test is prone to false positives. Therefore,
additional statistical analyses were used to determine the validity of the positive results.
Intra-well comparisons of data from a single well to previous data from the same well
were performed to determine if a trend of increasing concentration is occurring. The
Mann-Kendall Trend Analysis and the Shewhart-CUSUM Control Chart statistical tests
were selected for these additional analyses.

A detailed discussion of the statistical methods is presented in Appendix D. The
results of the statistical analysis indicate that there are no SSIs in the concentrations of
the detected constituents.

10
3.3 Methane Monitoring Results
The methane levels were measured at 14 locations at Lamont Landfill. The
results of the monitoring are summarized in Table 1 and are also presented on Figure 3.
No methane monitoring wells contained a high level of methane (> 5% Methane by
Volume).

11
4.0 CONCLUSIONS AND RECOMMENATIONS
The annual monitoring program consists of two sampling events conducted six
months apart. This was the November 2014 sampling event for groundwater and
methane monitoring performed by the USACE, Savannah District. It was the N=29
sampling event for the Lamont Road Landfills. Low levels of Appendix I VOCs and
metals were detected. Wells LMW-6 and LMW-15R contained nitrate above the NC2L
standard. These exceedances are new detections and will be confirmed in the May 2015
sampling event. No other constituents were above their 2L standards.
According to the Statistical Analysis of groundwater Data (Appendix D), there is
no evidence of an upward trend in constituent concentrations. The statistical findings at
the Lamont Road Landfill demonstrated that any statistical abnormalities were due to
natural variation in the results. Long-term monitoring should continue at the Lamont
Road Landfill because it is still an active site and NC Solid Waste Regulations require it.
The methane levels were measured at 14 locations around Lamont landfill. No
methane monitoring wells contained a high level of methane (> 5% Methane by Volume).

12
REFERENCES

North Carolina Administrative Code, Title 15A, Department of Environment, Health, and
Natural Resources, Division of Solid Waste, Management, Subchapter 13B, Solid
Waste Management, Section .1600 (January 4, 1994).

North Carolina Administrative Code, Title 15A, Department of Environment, Health, and
Natural Resources, Division of Solid Waste, Management, SubchapterNC2L,
Classifications and Water Quality Standards Applicable to the Ground Waters of
North Carolina, Sections .0100, .0200, and .0300 (November 8, 1993): from the
Environmental Management Commission, Raleigh, North Carolina.

FIGURES
West Virginia
Virginia
Kentucky
Tennessee
Georgia South Carolina
North Carolina
$
Moore
Harnett
Scotland
Richmond
Hoke
Cumberland
FORT BRAGG
Southern Pines
Raeford
Fayetteville
MACKALL
$5 0 5 102.5 Miles
50 0 50 100 15025Miles
C a p e F e a r R i v e r
Rockfish Creek
Figure 1
Site Map -- Ft. Bragg, NC
U.S. ARMY ENGINEER DISTRICTCORPS OF ENGINEERSSAVANNAH, GEORGIA
Lamont Street Landfill
Longstreet Road
Landfill
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
LMW-6
LMW-5
LMW-4
LMW-9DLMW-9S
LMW-16
LMW-3S
LMW-10
LMW-09
LMW-08
LMW-15R
LMW-14R
DATE: MARCH 2015 FIGURE: 2
LAMONT STREET LANDFILL
LOCATION MAP
FORT BRAGG, NC
$0 250 500125'
1 inch = 250 feet
Legend
&<Groundwater Monitoring Wells
&§M Methane Monitoring Wells
Buildings
U.S. ARMY CORPS OF ENGINEERSSAVANNAH DISTRICTSAVANNAH, GEORGIA
L
A
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O
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T

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T
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&§M GP-12
GP-11
GP-09
GP-08
GP-07
GP-06
GP-05
GP-04
GP-03
GP-02
GP-01
GP-10R
GP-13R
DATE: MARCH 2015 FIGURE: 3
LAMONT STREET LANDFILL
METHANE MONITORING RESULTSNOVEMBER 2013
FORT BRAGG, NC
$0 200 400100'
1 inch = 200 feet
Legend
&§M Methane Monitoring Wells
Buildings
Streams
U.S. ARMY CORPS OF ENGINEERSSAVANNAH DISTRICTSAVANNAH, GEORGIA
0.0% Methane
0.0% Methane
0.0% Methane
0.0% Methane
Scale House0.0% Methane
1.2% Methane
0.0% Methane
0.0% Methane
0.0% Methane
0.0% Methane
0..0% Methane
0.0% Methane
Office0.0% Methane
O-35330.0% Methane
0.0% Methane
0.0% Methane
&<
&<
&<
&<
&<
&<
&<
&<
330
320
310
300
290
340
3 5 0
3 3 0 3 2 0 3 1 0340
LMW-09(281.7)
LMW-10(351.12)
LMW-08(308.34)
LMW-06(350.07)
LMW-16(340.205)
LMW-04R(352.77)
LMW-03S(345.182)
LMW-14R(349.408)
@A
@A
@A @A
@A @A
@A
@A
@A@A
@A
@A
@A
DATE: JULY 2014 FIGURE: 4
LAMONT STREET LANDFILL
POTENTIOMETRIC SURFACE MAPNOVEMBER 2013FORT BRAGG, NC
$0 250 500125'
1 inch = 247 feet
U.S. ARMY CORPS OF ENGINEERSSAVANNAH DISTRICTSAVANNAH, GEORGIA
Note: Monitoring wells used forpotentiometric surface are displayedwith elevations in feet above MSL inparenthesis below the label.
Arrows point in direction of groundwater flow.
Legend
&<Groundwater Monitoring Wells
Groundwater Contour Line

TABLES

Table 1. Methane Monitoring Results
Lamont Landfills, Fort Bragg, NC

Well
ID

Date
Sampled

Time
Sampled

%Methane
by Volume

%Oxygen

%CO2
Gas-GP-1 15 Nov 2014 1339 0.0 19.6 0.6
Gas- GP -2 15 Nov 2014 1044 0.0 12.8 9.8
Gas- GP -3 15 Nov 2014 1405 0.0 19.1 1.3
Gas- GP -4 15 Nov 2014 1259 0.0 19.1 1.0
Gas- GP -5 15 Nov 2014 1301 0.0 19.3 0.6
Gas- GP -6 15 Nov 2014 1304 0.0 18.1 2.1
Gas- GP -7 15 Nov 2014 1308 0.0 16.7 3.3
Gas- GP -8 15 Nov 2014 1312 0.0 18.7 0.2
Gas- GP -9 15 Nov 2014 1320 0.0 16.2 5.1
Gas- GP -10R 15 Nov 2014 1322 1.2 18.3 3.9
Gas- GP -11 15 Nov 2014 1350 0.0 19.8 0.0
Gas- GP -12 15 Nov 2014 1344 0.0 19.9 0.1
Gas- GP -13R 15 Nov 2014 1247 0.0 12.0 5.0
Office 15 Nov 2014 1406 0.0 19.8 0.6
Scale House 15 Nov 2014 1412 0.0 20.0 0.1
O-3533 15 Nov 2014 1415 0.0 19.8 0.2

Note:
TOC – Top of casing, btoc – Below top of casing, NA – Not Available
bgs – Below ground surface, amsl – Above mean sea level
 --- Selected Well for Long Term Monitoring
TOC elevation is based on vertical datum NGVD29 (source: USGS RFI, Aug. 1999)
* Erroneous reading not reported in table.
**No well cover
***Not Sampled - Inaccessible due to dense vegetation
Table 2
Groundwater Elevation Data
Lamont Street Landfill, Fort Bragg NC
Nov-08 Nov-08 Jun-09 Jun-09 Nov-09 Nov-09 Jun-10 Jun-10 Nov-10 Nov-10 Jun-11 Jun-11 Nov-11 Nov-11 May-12 May-12 Nov-12 Nov-12 May-13 May-13 Nov-13 Nov-13 May-14 May-14 Nov-14 Nov-14
LMW-3 408.32 102.18 306.14 103.2 305.12 102.21 306.11 87.27 321.05 102.13 306.19 102.79 305.56 104 304.32 106.22 302.1 105.72 302.6 106.27 199.87 105.6 302.72 104.82 303.5 104.25 304.07
LMW-3s 405.89 59.19 NA 60.4 NA 59.12 NA 59.61 NA 58.91 NA 59.64 NA 61.26 NA 62.8 NA 63.17 NA 63.57 NA 61.7 344.19 60.71 345.182 59.95 345.94
LMW-4R **441.79 75.42 366.37 74.65 367.14 74.74 367.05 75.39 366.4 74.83 366.96 75.33 366.46 75.81 365.98 75.71 366.08 80.34 361.45 79.85 286.52 79.39 351.61 78.23 352.77 77.1 364.69
LMW-6 431.45 80.3 351.15 81.65 349.8 80.15 351.3 80.75 350.7 80.04 351.41 80.93 350.52 82.7 348.75 84.38 347.07 84.81 346.64 85.05 266.1 84.81 346.64 81.38 350.07 80.95 350.5
LMW-7R***436.62 125.87 310.75 125.63 310.99 124.78 311.84 128.8 307.82 124.54 312.08 124.78 311.84 125 311.62 125.2 311.42 125.11 311.51 125.41 185.34 130.4 304.6 130.16 304.84 Dry NA
LMW-8 354.07 48.68 305.39 76.66 277.41 46.85 307.22 304.86 49.21 46.86 307.21 48.95 305.12 51.02 303.05 50.84 303.23 49.97 304.1 NA NA 46.93 307.17 45.73 308.34 NM NA
LMW-9 364.79 82.16 282.63 80 284.79 80.71 284.08 87.27 277.52 80.73 284.06 82.43 282.36 85 279.79 86.64 278.15 87.43 277.36 87.95 194.68 83.8 280.99 83.09 281.7 83.2 281.59
LMW-9S *52.46 NA 49.01 NA 51.01 NA 53.35 NA 51 NA 52.89 NA 55.05 NA 54.83 NA 53.95 NA 55.43 NA 51.3 NA NA NA 61.31 NA
LMW-9D *76.95 NA 76.66 NA 75.41 NA 77.03 NA 75.48 NA 77.29 NA 79.73 NA 81.11 NA 82.07 NA 82.61 NA 78.4 NA NA NA 77.98 NA
LMW-10 428.68 76.81 351.87 76.48 352.2 76.38 352.3 72.11 356.57 NA NA 76.89 NA 78.84 349.84 79.87 348.81 79.87 348.81 80.25 271.62 77.9 350.78 77.56 351.12 77 351.68
LMW-14R 398.42 50.07 NA 49 NA 48.97 NA 50.06 NA 48.99 NA 50.25 NA 51.53 NA 52.02 NA 51.67 NA 52.28 NA 49.08 349.34 49.01 349.408 49.44 348.98
LMW-15R *40.89 NA 37 NA 37.55 NA 40.31 NA 38.19 NA 40.28 NA 41.68 NA 40.81 NA 40.35 NA 40.82 NA 36.4 NA NA NA 39.22 NA
LMW-16 374.69 86.02 NA 36.48 NA 37.5 NA 37.28 NA 36.61 NA 36 NA 36.8 NA 37.36 NA 37.22 NA 36.91 NA 36.8 337.89 34.48 340.205 43.75 330.94
Note:
TOC – Top of casing,
bgs – Below ground surface,
∆ --- Selected Well for Long Term Monitoring
TOC elevation is based on vertical datum NGVD29 (source: USGS RFI, Aug. 1999)
btoc – Below top of casing,
amsl – Above mean sea level
*Well & ground-water elevations unavailable at this time.
** Data are for LMW-4 up through May 2013
*** Data are for LMW-7 up through May 2013
NA – Not Available
NS – Not Surveyed
NM- Not Measured
Water Level
Elev. (ft.
amsl)
Water
Level (ft.
BTOC)
Water Level
Elev. (ft.
amsl)
Water
Level Elev.
(ft. amsl)
Water
Level (ft.
BTOC)
Water
Level Elev.
(ft. amsl)
Water
Level (ft.
BTOC)
Water
Level Elev.
(ft. amsl)
Water
Level (ft.
BTOC)
Water
Level Elev.
(ft. amsl)
Water
Level
(ft. BTOC)
Water Level
Elev. (ft.
amsl)
Water
Level
(ft. BTOC)
Water Level
Elev. (ft.
amsl)
Water
Level (ft.
BTOC)Well ID
Water
Level Elev.
(ft. amsl)
Water
Level (ft.
BTOC)
Water
Level Elev.
(ft. amsl)TOC Elev.
(ft. amsl)
Water
Level
(ft. BTOC)
Water
Level (ft.
BTOC)
Water
Level Elev.
(ft. amsl)
Water
Level
(ft. BTOC)
Water Level
Elev. (ft.
amsl)
Water
Level
(ft.
BTOC)
Water
Level
Elev. (ft.
l)
Water
Level
(ft. BTOC)
Table 3. Field Parameter Measurements Lamont Landfills, Fort Bragg, NC

Monitoring Sample Specific Temperature Turbidity Dissolved
Well Identification pH Conductivity
(µs/cm) (°C) (N.T.U.) Oxygen
(mg/L) ORP
LMW-3 LMW-3-11-15 4.36 0.005 6.93 12 2.44 166
LMW-3S LMW-3S-11-15 5.06 0.014 11.02 45 1.75 23
LMW-4R LMW-4R-11-15 4.9 0.006 16.62 228 2.55 152
LMW-6 LMW-6-11-15 5.13 0.07 11.44 18.5 1.45 111
LMW-7* -- -- -- -- -- -- --
LMW-8* -- -- -- -- -- -- --
LMW-9 LMW-9-11-15 4.7 0.008 15.42 23 7.95 203
LMW-9S LMW-9S-11-15 5.98 0.173 17.29 8 2.21 -0.8
LMW-9D LMW-9D-11-15 6.09 0.017 16.69 15 6.38 146
LMW-10 LMW-10-11-15 4.9 0.013 15.72 14 6.9 136
LMW-14R LMW-14R-11-15 4.48 0.006 15.11 12 6.2 205
LMW-15R LMW-15R-11-15 4.64 0.014 17.51 >800 1.72 170
LMW-16 LMW-16-11-15 6.46 0.136 15.79 15 0.88 2
Note: N.T.U. --- Nephelometric Turbidity Unit ORP --- Oxidation Reduction Potential
* – Not Sampled
Table 4
Analytical Data Summary
Lamont Road Landfill, Fort Bragg NC
Notes:
All results are ug/L
* Primary MCL used instead of NC2L
#NA - No established NC2L or MCL
Analyte NC2L Standard LMW-10 LMW-14R LMW-15R LMW-16 LMW-3 LMW-3S LMW-4R LMW-6 LMW-9 LMW-9D LMW-9S
VOCs
1,2-cis-Dichloroethylene 70 0.17 J ND ND ND ND ND ND ND 0.30 J 0.29 J 0.34 J
Chloroform 70 ND ND ND ND 0.25 J ND ND ND ND ND ND
Dichlorodifluoromethane 1000 2.8 ND ND ND ND 2.3 ND ND ND ND ND
Trichloroethene 3 1.8 ND ND ND ND ND ND ND ND ND ND
Trichlorofluoromethane 2000 4 ND ND ND 0.33 J 0.83 J ND 0.38 J ND ND ND
Metals
Arsenic 10 ND ND 0.53 J 3.3 ND 0.94 J 0.48 J ND ND 1.9 1.4
Barium 700 17 17 33 6.2 5.5 8 6.9 28 3.8 3.2 51
Beryllium 4*ND ND 0.15 J ND ND ND ND ND 0.11 J ND ND
Chromium 10 0.65 J 0.54 J 1.4 0.28 J 0.70 J 0.74 J 1.4 0.36 J 0.37 J 0.80 J ND
Cobalt 1000 0.16 J 0.23 0.68 0.19 J 0.21 0.56 0.19 J 0.33 0.19 J ND 1.8
Copper 1000 0.27 J 0.30 J 0.45 J 0.51 J 1.6 1.6 0.49 J 0.65 J 0.84 J 1.1 0.65 J
Lead 15 1.1 0.11 J 0.20 J 0.20 J 0.12 J 0.25 J 1.2 ND ND 0.61 ND
Nickel 100 0.64 J 0.88 J 1.3 0.41 J 0.90 J 1.5 0.81 J 0.97 J 0.70 J 1 0.45 J
Selenium 20 1.2 ND 0.23 J 0.31 J ND ND 0.45 J 1.1 ND 0.35 J 0.38 J
Vanadium #N/A ND ND ND ND 1.90 J 1.50 J 2.00 J ND ND 3.10 J ND
Zinc 1000 3.30 J 2.90 J 2.60 J ND 6.00 J 5.30 J ND 3.70 J 3.00 J 4.00 J ND
Other Inorganics
Nitrate 1000 390 40.00 J 1100 ND 190 110 57 2200 J 110 120 ND

APPENDIX A
GROUNDWATER SAMPLING LOGS

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 16 Nov 2014
SAMPLED BY: R. Hill & C. Poston TIME : 0953
WEATHER CONDITIONS: Cloudy, 42

Location: Lamont Landfill Sample ID: LMW-9D-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):87 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):77.98 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.48 (gallons)
Flow Rate:250 (ml/min)Purge Vol:2.4 (gallons)
Length of Time Purged:36 (minutes)Purge Time:945
Amount Purged:2.5 (gallons)Pump Depth:85.5
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 0951 0956 1001 1006 1011
pH 5.83 6.07 6.06 6.03 6.09
Sp. Cond 0.023 0.018 0.017 0.016 0.017
Temp. °C 14.63 16.46 16.55 16.72 16.69
Turbidity 12 15 16 18 15
DO 8.01 6.76 6.56 6.30 6.38
ORP 139 169 152 148 146
Water Level 78.0 78.3 78.6 78.9 77.7

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 16 Nov 2014
SAMPLED BY: R. Hill & C. Poston TIME :1114
WEATHER CONDITIONS: Cloudy 38˚

Location: Lamont Landfill Sample ID: LMW-9S-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):61.31 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):53 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.36 (gallons)
Flow Rate:330.75 (ml/min)Purge Vol:3.5 (gallons)
Length of Time Purged:40 (minutes)Purge Time:1034
Amount Purged:3.5 (gallons)Pump Depth:59
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1044 1049 1054 1059 1104
pH 5.99 5.98 5.98 5.97 5.98
Sp. Cond 0.162 0.169 0.171 0.172 0.173
Temp. °C 16.91 17.10 17.10 17.12 17.29
Turbidity 12.6 8.8 9.3 8.9 8.0
DO 4.09 3.21 3.08 2.53 2.21
ORP -2.6 -2.9 -2.6 -1.0 -0.8
Water Level 53.1 53.1 53.1 53.1 53.1

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 16 Nov 2014
SAMPLED BY: R. Hill & C. Poston TIME : 1220
WEATHER CONDITIONS: Cloudy 48˚

Location: Lamont Landfill Sample ID: LMW-9-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):135.5 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):83.2 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =8.58 (gallons)
Flow Rate:429.55 (ml/min)Purge Vol:5.0 (gallons)
Length of Time Purged:44 (minutes)Purge Time:1124
Amount Purged:5 (gallons)Pump Depth:132
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1150 1155 1200 1205 1210
pH 4.71 4.70 4.71 4.69 4.70
Sp. Cond 0.009 0.009 0.009 0.008 0.008
Temp. °C 15.07 15.33 15.47 15.45 15.42
Turbidity 28 21 22 25 23
DO 7.73 7.81 7.92 7.92 7.95
ORP 214 210 210 207 203
Water Level 83.4 83.4 83.4 83.4 83.4

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 16 Nov-14
SAMPLED BY: R. Hill & C. Poston TIME : 1417
WEATHER CONDITIONS: Cloudy, 39˚

Location: Lamont Landfill Sample ID: LMW-16-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):43.75 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):36.95 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.12 (gallons)
Flow Rate:336 (ml/min)Purge Vol:4.0 (gallons)
Length of Time Purged:45 (minutes)Purge Time:1332
Amount Purged:4 (gallons)Pump Depth:41.5
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1347 1352 1657 1402 1409
pH 6.6 6.42 6.43 6.46 6.46
Sp. Cond 0.132 0.133 0.133 0.136 0.136
Temp. °C 15.95 15.99 15.94 15.81 15.79
Turbidity 29 22 24 18 15
DO 0.99 0.194 0.191 0.99 0.88
ORP 77 43 30 21 2
Water Level 37.2 37.2 37.2 37.2 37.2

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 17 Nov 2014
SAMPLED BY: R. Hill & C. Poston TIME : 0950
WEATHER CONDITIONS: Cloudy, 52˚

Location: Lamont Landfill Sample ID: LMW-10-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):82.62 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):77 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =0.92 (gallons)
Flow Rate:283.5 (ml/min)Purge Vol:3.0 (gallons)
Length of Time Purged:40 (minutes)Purge Time:910
Amount Purged:3 (gallons)Pump Depth:81
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 0920 0925 0930 0935 0940
pH 4.99 4.97 4.95 4.92 4.90
Sp. Cond 0.015 0.015 0.018 0.013 0.013
Temp. °C 15.14 15.40 15.62 15.75 15.72
Turbidity 22 18 16 15 14
DO 7.26 7.00 7.05 6.99 6.90
ORP 146 141 137 137 136
Water Level 77.1 77.1 77.1 77.1 77.1

5. NOTES

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 17 Nov 2014
SAMPLED BY: R. Hill & C. Poston TIME : 1112
WEATHER CONDITIONS: Rain, 54˚

Location: Lamont Landfill Sample ID: LMW-4R-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):89.15 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):77.1 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.98 (gallons)
Flow Rate:348.92 (ml/min)Purge Vol:6.0 (gallons)
Length of Time Purged:65 (minutes)Purge Time:1007
Amount Purged:6 (gallons)Pump Depth:88
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1042 1047 1052 1057 1102
pH 4.97 4.92 4.90 4.93 4.90
Sp. Cond 0.006 0.006 0.006 0.006 0.006
Temp. °C 16.45 16.53 16.55 16.58 16.62
Turbidity - - - - 228
DO 2.58 2.59 2.45 2.37 2.55
ORP 168 158 153 152 152
Water Level 77.2 77.2 77.2 77.2 77.2

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 18 Nov 2014
SAMPLED BY: R. Hill & C. Poston TIME : 1001
WEATHER CONDITIONS: Clear, Windy 30˚

Location: Lamont Landfill Sample ID: LMW-6-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):94.53 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):80.95 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =2.23 (gallons)
Flow Rate:309.84 (ml/min)Purge Vol:5.0 (gallons)
Length of Time Purged:61 (minutes)Purge Time:900
Amount Purged:5 (gallons)Pump Depth:93
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 0931 0936 0941 0946 0951
pH 5.09 5.10 5.13 5.11 5.13
Sp. Cond 0.066 0.067 0.068 0.069 0.070
Temp. °C 11.32 11.46 11.28 11.06 11.44
Turbidity 38.4 28.9 23.4 20.6 18.5
DO 1.88 1.69 1.67 1.49 1.45
ORP 107 109 109 112 111
Water Level 80.9 80.9 80.9 80.9 80.9

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 18 Nov-14
SAMPLED BY: R. Hill & C. Poston TIME : 1130
WEATHER CONDITIONS: LMW-9-5-14

Location: Lamont Landfill Sample ID: LMW-3S-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):69.75 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):59.95 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.61 (gallons)
Flow Rate:343.64 (ml/min)Purge Vol:5.0 (gallons)
Length of Time Purged:55 (minutes)Purge Time:1035
Amount Purged:5 (gallons)Pump Depth:68
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1100 1105 1110 1115 1120
pH 5.65 5.56 5.38 5..22 5.06
Sp. Cond 0.030 0.028 0.019 0.016 0.014
Temp. °C 1087 11.51 10.96 10.69 11.02
Turbidity 52 46 32 38 45
DO 1.22 1.31 1.51 1.63 1.75
ORP -62 -45 -23 -1 23
Water Level 60.1 60.1 60.1 60.1 60.1

5. NOTES: MS/MSD collected

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 18 Nov-14
SAMPLED BY: R. Hill & C. Poston TIME : 1234
WEATHER CONDITIONS: Clear 34˚

Location: Lamont Landfill Sample ID: LMW-3-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):123 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):104.25 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =3.08 (gallons)
Flow Rate:133.1 (ml/min)Purge Vol:2.5 (gallons)
Length of Time Purged:71 (minutes)Purge Time:1123
Amount Purged:2.5 (gallons)Pump Depth:121
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1204 1209 1214 1219 1224
pH 4.48 4.43 4.34 4.37 4.36
Sp. Cond 0.006 0.006 0.006 0.006 0.005
Temp. °C 7.58 7.13 6.93 6.95 6.93
Turbidity 13 12 11 10 12
DO 4.41 3.84 3.26 2.81 2.44
ORP 191 174 168 166 166
Water Level 104.3 104.3 104.3 104.3 104.3

5. NOTES: Blank taken at 1400

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 21 Nov-14
SAMPLED BY: R. Hill & C. Poston TIME : 1341
WEATHER CONDITIONS: Sunny 36˚

Location: Lamont Landfill Sample ID: LMW-15R-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):46.31 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):39.22 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.16 (gallons)
Flow Rate:275.63 (ml/min)Purge Vol:3.5 (gallons)
Length of Time Purged:48 (minutes)Purge Time:1253
Amount Purged:3.5 (gallons)Pump Depth:45
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1311 1316 1321 1326 1331
pH 4.60 4.61 4.64 4.65 4.64
Sp. Cond 0.015 0.014 0.014 0.014 0.014
Temp. °C 17.52 17.46 17.36 17.55 17.51
Turbidity >800 >800 >800 >800 >800
DO 1.73 1.71 1.64 1.71 1.72
ORP 188 182 176 172 170
Water Level 39.3 39.3 39.3 39.3 39.3

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 20 Nov-14
SAMPLED BY: R. Hill & C. Poston TIME : 1438
WEATHER CONDITIONS: Sunny, 58˚

Location: Lamont Landfill Sample ID: LMW-14R-5-14

PRESERVATIVE: Ice, HCL &HNO3
ANALYSES REQUESTED: EPA 8260B, EPA 6020 App. I EPA 300_Nitrate
# OF CONTAINERS: 5
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):57.34 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):49.44 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.30 (gallons)
Flow Rate:321.7 (ml/min)Purge Vol:4.0 (gallons)
Length of Time Purged:47 (minutes)Purge Time:1351
Amount Purged:4 (gallons)Pump Depth:55
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1408 1413 1418 1423 1428
pH 4.54 4.53 4.50 4.49 4.48
Sp. Cond 0.006 0.006 0.006 0.006 0.006
Temp. °C 15.08 15.07 15.06 15.09 15.11
Turbidity 32 24 22 18 12
DO 5.72 5.83 6.05 6.09 6.20
ORP 203 207 208 205 205
Water Level 49.5 49.5 49.5 49.5 49.5

5. NOTES:

APPENDIX B

CHAINS OF CUSTODY & LAB ANALYTICAL REPORTS
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-107343-1
Client Project/Site: Ft.Bragg - Lamont Landfill
For:
U.S. Army Corps of Engineers
100 West Oglethorpe Ave
Savannah, Georgia 31401
Attn: Mr. Kevin Haborak
Authorized for release by:
11/26/2014 4:56:52 PM
Linda Wolfe, Project Manager II
[phone] e.3005
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
TestAmerica Job ID: 680-107343-1
Page 2 of 46 TestAmerica Savannah11/26/2014
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .40
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .45
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-107343-1
Project/Site: Ft.Bragg - Lamont Landfill
Job ID: 680-107343-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: U.S. Army Corps of Engineers
Project: Ft.Bragg - Lamont Landfill
Report Number: 680-107343-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 11/18/2014; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.3 C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples LMW-9D-11-14 (680-107343-1), Trip Blank (680-107343-2), LMW-9S-11-14 (680-107343-3), LMW-9-11-14 (680-107343-4),
LMW-16-11-14 (680-107343-5), LMW-10-11-14 (680-107343-6) and LMW-4R-11-14 (680-107343-7) were analyzed for Volatile Organic
Compounds (GC-MS) in accordance with EPA SW-846 Method 8260B. The samples were analyzed on 11/25/2014 and 11/26/2014.
1,2,4-Trichlorobenzene and Hexachlorobutadiene were detected in method blank MB 680-360309/9 at levels that were above the method
detection limit but below the reporting limit. The values should be considered estimates, and have been flagged. If the associated
sample reported a result above the MDL and/or RL, the result has been flagged. 1,2,3-Trichlorobenzene and Hexachlorobutadiene were
detected in method blank MB 680-360546/11 at levels that were above the method detection limit but below the reporting limit. The values
should be considered estimates, and have been flagged. If the associated sample reported a result above the MDL and/or RL, the result
has been flagged. Refer to the QC report for details.
Surrogate recovery for the following sample was outside of acceptance limits: Trip Blank (680-107343-2). There was insufficient sample
to perform another analysis, because the remaining vial was analyzed against an invalid calibration.
Methylene Chloride and trans-1,2-Dichloroethene failed the recovery criteria low for LCS 680-360309/4. Chloroethane and Vinyl chloride
exceeded the RPD limit for LCSD 680-360309/11. Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
METALS (ICPMS)
Samples LMW-9D-11-14 (680-107343-8), LMW-9S-11-14 (680-107343-9), LMW-9-11-14 (680-107343-10), LMW-16-11-14
(680-107343-11), LMW-10-11-14 (680-107343-12) and LMW-4R-11-14 (680-107343-13) were analyzed for Metals (ICPMS) in accordance
with EPA SW-846 Method 6020A. The samples were prepared on 11/18/2014 and analyzed on 11/19/2014.
Chromium was detected in method blank MB 680-359308/1-A at a level that was above the method detection limit but below the reporting
limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the MDL
and/or RL, the result has been flagged.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-107343-1
Project/Site: Ft.Bragg - Lamont Landfill
Job ID: 680-107343-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
ANIONS BY ION CHROMATOGRAPHY (Nitrate )
Samples LMW-9D-11-14 (680-107343-8), LMW-9S-11-14 (680-107343-9), LMW-9-11-14 (680-107343-10), LMW-16-11-14
(680-107343-11), LMW-10-11-14 (680-107343-12) and LMW-4R-11-14 (680-107343-13) were analyzed for Anions by Ion Chromatography
(48 Hour) in accordance with EPA Method 300.0. The samples were analyzed on 11/18/2014.
Sample LMW-9S-11-14 (680-107343-9)[2X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Sample Summary
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-107343-1 LMW-9D-11-14 Water 11/16/14 10:21 11/18/14 10:05
680-107343-2 Trip Blank Water 11/16/14 08:30 11/18/14 10:05
680-107343-3 LMW-9S-11-14 Water 11/16/14 11:14 11/18/14 10:05
680-107343-4 LMW-9-11-14 Water 11/16/14 12:20 11/18/14 10:05
680-107343-5 LMW-16-11-14 Water 11/16/14 14:17 11/18/14 10:05
680-107343-6 LMW-10-11-14 Water 11/17/14 09:50 11/18/14 10:05
680-107343-7 LMW-4R-11-14 Water 11/17/14 11:12 11/18/14 10:05
680-107343-8 LMW-9D-11-14 Water 11/17/14 07:30 11/18/14 10:05
680-107343-9 LMW-9S-11-14 Water 11/17/14 07:45 11/18/14 10:05
680-107343-10 LMW-9-11-14 Water 11/17/14 07:55 11/18/14 10:05
680-107343-11 LMW-16-11-14 Water 11/17/14 08:10 11/18/14 10:05
680-107343-12 LMW-10-11-14 Water 11/17/14 09:50 11/18/14 10:05
680-107343-13 LMW-4R-11-14 Water 11/17/14 11:12 11/18/14 10:05
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Method Summary
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL SAV
MCAWW300.0 Anions, Ion Chromatography TAL SAV
SW8466020AMetals (ICP/MS)TAL SAV
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Definitions/Glossary
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Qualifiers
GC/MS VOA
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
Q One or more quality control criteria failed.
HPLC/IC
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
Metals
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Detection Summary
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-9D-11-14 Lab Sample ID: 680-107343-1
cis-1,2-Dichloroethene
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.29 8260B
Client Sample ID: Trip Blank Lab Sample ID: 680-107343-2
Hexachlorobutadiene
RL
5.0 ug/L
MDL
0.40
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J1.7 8260B
Client Sample ID: LMW-9S-11-14 Lab Sample ID: 680-107343-3
cis-1,2-Dichloroethene
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.34 8260B
Client Sample ID: LMW-9-11-14 Lab Sample ID: 680-107343-4
cis-1,2-Dichloroethene
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.30 8260B
Client Sample ID: LMW-16-11-14 Lab Sample ID: 680-107343-5
No Detections.
Client Sample ID: LMW-10-11-14 Lab Sample ID: 680-107343-6
cis-1,2-Dichloroethene
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.17 8260B
Dichlorodifluoromethane 1.0 ug/L0.25 Total/NA12.8 8260B
Trichloroethene 1.0 ug/L0.13 Total/NA11.8 8260B
Trichlorofluoromethane 1.0 ug/L0.25 Total/NA14.0 8260B
Client Sample ID: LMW-4R-11-14 Lab Sample ID: 680-107343-7
No Detections.
Client Sample ID: LMW-9D-11-14 Lab Sample ID: 680-107343-8
Nitrate as N
RL
0.050 mg/L
MDL
0.023
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.12 300.0
Arsenic 1.0 ug/L0.40 Total/NA11.9 6020A
Barium 1.0 ug/L0.15 Total/NA13.2 6020A
Chromium 1.0 ug/L0.16 Total/NA10.80 J 6020A
Copper 1.0 ug/L0.21 Total/NA11.1 6020A
Lead 0.30 ug/L0.080 Total/NA10.61 6020A
Nickel 1.0 ug/L0.40 Total/NA11.0 6020A
Selenium 0.50 ug/L0.21 Total/NA10.35 J 6020A
Vanadium 5.0 ug/L1.4 Total/NA13.1 J 6020A
Zinc 10 ug/L2.6 Total/NA14.0 J 6020A
Client Sample ID: LMW-9S-11-14 Lab Sample ID: 680-107343-9
Arsenic
RL
1.0 ug/L
MDL
0.40
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.4 6020A
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-9S-11-14 (Continued)Lab Sample ID: 680-107343-9
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1516020A
Cobalt 0.20 ug/L0.078 Total/NA11.8 6020A
Copper 1.0 ug/L0.21 Total/NA10.65 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.45 J 6020A
Selenium 0.50 ug/L0.21 Total/NA10.38 J 6020A
Client Sample ID: LMW-9-11-14 Lab Sample ID: 680-107343-10
Nitrate as N
RL
0.050 mg/L
MDL
0.023
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.11 300.0
Barium 1.0 ug/L0.15 Total/NA13.8 6020A
Beryllium 0.20 ug/L0.070 Total/NA10.11 J 6020A
Chromium 1.0 ug/L0.16 Total/NA10.37 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.19 J 6020A
Copper 1.0 ug/L0.21 Total/NA10.84 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.70 J 6020A
Zinc 10 ug/L2.6 Total/NA13.0 J 6020A
Client Sample ID: LMW-16-11-14 Lab Sample ID: 680-107343-11
Arsenic
RL
1.0 ug/L
MDL
0.40
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.3 6020A
Barium 1.0 ug/L0.15 Total/NA16.2 6020A
Chromium 1.0 ug/L0.16 Total/NA10.28 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.19 J 6020A
Copper 1.0 ug/L0.21 Total/NA10.51 J 6020A
Lead 0.30 ug/L0.080 Total/NA10.20 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.41 J 6020A
Selenium 0.50 ug/L0.21 Total/NA10.31 J 6020A
Client Sample ID: LMW-10-11-14 Lab Sample ID: 680-107343-12
Nitrate as N
RL
0.050 mg/L
MDL
0.023
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.39 300.0
Barium 1.0 ug/L0.15 Total/NA1176020A
Chromium 1.0 ug/L0.16 Total/NA10.65 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.16 J 6020A
Copper 1.0 ug/L0.21 Total/NA10.27 J 6020A
Lead 0.30 ug/L0.080 Total/NA11.1 6020A
Nickel 1.0 ug/L0.40 Total/NA10.64 J 6020A
Selenium 0.50 ug/L0.21 Total/NA11.2 6020A
Zinc 10 ug/L2.6 Total/NA13.3 J 6020A
Client Sample ID: LMW-4R-11-14 Lab Sample ID: 680-107343-13
Nitrate as N
RL
0.050 mg/L
MDL
0.023
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.057 300.0
Arsenic 1.0 ug/L0.40 Total/NA10.48 J 6020A
Barium 1.0 ug/L0.15 Total/NA16.9 6020A
Chromium 1.0 ug/L0.16 Total/NA11.4 6020A
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
Page 9 of 46 11/26/2014
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Detection Summary
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-4R-11-14 (Continued)Lab Sample ID: 680-107343-13
Cobalt
RL
0.20 ug/L
MDL
0.078
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.19 6020A
Copper 1.0 ug/L0.21 Total/NA10.49 J 6020A
Lead 0.30 ug/L0.080 Total/NA11.2 6020A
Nickel 1.0 ug/L0.40 Total/NA10.81 J 6020A
Selenium 0.50 ug/L0.21 Total/NA10.45 J 6020A
Vanadium 5.0 ug/L1.4 Total/NA12.0 J 6020A
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
Page 10 of 46 11/26/2014
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-1Client Sample ID: LMW-9D-11-14
Matrix: WaterDate Collected: 11/16/14 10:21
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 13:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/26/14 13:00 1Benzene0.25 U
1.0 0.16 ug/L 11/26/14 13:00 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/26/14 13:00 1Bromoform0.50 U
5.0 2.0 ug/L 11/26/14 13:00 1Bromomethane2.0 U
10 1.0 ug/L 11/26/14 13:00 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/26/14 13:00 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/26/14 13:00 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/26/14 13:00 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/26/14 13:00 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/26/14 13:00 1Chloroethane2.0 U
1.0 0.14 ug/L 11/26/14 13:00 1Chloroform0.14 U
5.0 0.27 ug/L 11/26/14 13:00 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/26/14 13:00 1Chloromethane0.33 U
1.0 0.17 ug/L 11/26/14 13:00 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/26/14 13:00 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/26/14 13:00 1cis-1,2-Dichloroethene 0.29 J
1.0 0.11 ug/L 11/26/14 13:00 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/26/14 13:00 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/26/14 13:00 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/26/14 13:00 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/26/14 13:00 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/26/14 13:00 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/26/14 13:00 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 11/26/14 13:00 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 11/26/14 13:00 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/26/14 13:00 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/26/14 13:00 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/26/14 13:00 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/26/14 13:00 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/26/14 13:00 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/26/14 13:00 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/26/14 13:00 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/26/14 13:00 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/26/14 13:00 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/26/14 13:00 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/26/14 13:00 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/26/14 13:00 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/26/14 13:00 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/26/14 13:00 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/26/14 13:00 1Naphthalene1.0 U
1.0 0.10 ug/L 11/26/14 13:00 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/26/14 13:00 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/26/14 13:00 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/26/14 13:00 1Styrene0.11 U
1.0 0.12 ug/L 11/26/14 13:00 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/26/14 13:00 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/26/14 13:00 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/26/14 13:00 1Tetrachloroethene0.15 U
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-1Client Sample ID: LMW-9D-11-14
Matrix: WaterDate Collected: 11/16/14 10:21
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene 0.33 U 1.0 0.33 ug/L 11/26/14 13:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.20 ug/L 11/26/14 13:00 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/26/14 13:00 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/26/14 13:00 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/26/14 13:00 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/26/14 13:00 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/26/14 13:00 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/26/14 13:00 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/26/14 13:00 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 11/26/14 13:00 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/26/14 13:00 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/26/14 13:00 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/26/14 13:00 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)97 70-130 11/26/14 13:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)81 11/26/14 13:00 170-130
Dibromofluoromethane (Surr)91 11/26/14 13:00 170-130
4-Bromofluorobenzene (Surr)101 11/26/14 13:00 170-130
Lab Sample ID: 680-107343-2Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 11/16/14 08:30
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/25/14 15:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/25/14 15:56 1Benzene0.25 U
1.0 0.16 ug/L 11/25/14 15:56 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/25/14 15:56 1Bromoform0.50 U
5.0 2.0 ug/L 11/25/14 15:56 1Bromomethane2.0 U
10 1.0 ug/L 11/25/14 15:56 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/25/14 15:56 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/25/14 15:56 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/25/14 15:56 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/25/14 15:56 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/25/14 15:56 1Chloroethane2.0 U Q
1.0 0.14 ug/L 11/25/14 15:56 1Chloroform0.14 U
5.0 0.27 ug/L 11/25/14 15:56 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/25/14 15:56 1Chloromethane0.33 U
1.0 0.17 ug/L 11/25/14 15:56 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/25/14 15:56 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/25/14 15:56 1cis-1,2-Dichloroethene 0.15 U
1.0 0.11 ug/L 11/25/14 15:56 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/25/14 15:56 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/25/14 15:56 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/25/14 15:56 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/25/14 15:56 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/25/14 15:56 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/25/14 15:56 1Dichlorodifluoromethane0.25 U
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-2Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 11/16/14 08:30
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloroethane 0.25 U 1.0 0.25 ug/L 11/25/14 15:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.10 ug/L 11/25/14 15:56 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/25/14 15:56 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/25/14 15:56 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/25/14 15:56 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/25/14 15:56 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/25/14 15:56 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/25/14 15:56 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/25/14 15:56 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/25/14 15:56 1Hexachlorobutadiene1.7 J
1.0 0.10 ug/L 11/25/14 15:56 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/25/14 15:56 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/25/14 15:56 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/25/14 15:56 1Methylene Chloride 1.0 U Q
10 1.0 ug/L 11/25/14 15:56 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/25/14 15:56 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/25/14 15:56 1Naphthalene1.0 U
1.0 0.10 ug/L 11/25/14 15:56 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/25/14 15:56 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/25/14 15:56 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/25/14 15:56 1Styrene0.11 U
1.0 0.12 ug/L 11/25/14 15:56 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/25/14 15:56 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/25/14 15:56 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/25/14 15:56 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 11/25/14 15:56 1Toluene0.33 U
1.0 0.20 ug/L 11/25/14 15:56 1trans-1,2-Dichloroethene 0.20 U Q
1.0 0.21 ug/L 11/25/14 15:56 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/25/14 15:56 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/25/14 15:56 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/25/14 15:56 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/25/14 15:56 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/25/14 15:56 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/25/14 15:56 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 11/25/14 15:56 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/25/14 15:56 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/25/14 15:56 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/25/14 15:56 1Vinyl chloride 0.18 U Q
Toluene-d8 (Surr)101 70-130 11/25/14 15:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)71 11/25/14 15:56 170-130
Dibromofluoromethane (Surr)91 11/25/14 15:56 170-130
4-Bromofluorobenzene (Surr)156 J 11/25/14 15:56 170-130
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-3Client Sample ID: LMW-9S-11-14
Matrix: WaterDate Collected: 11/16/14 11:14
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/25/14 20:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/25/14 20:43 1Benzene0.25 U
1.0 0.16 ug/L 11/25/14 20:43 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/25/14 20:43 1Bromoform0.50 U
5.0 2.0 ug/L 11/25/14 20:43 1Bromomethane2.0 U
10 1.0 ug/L 11/25/14 20:43 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/25/14 20:43 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/25/14 20:43 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/25/14 20:43 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/25/14 20:43 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/25/14 20:43 1Chloroethane2.0 U Q
1.0 0.14 ug/L 11/25/14 20:43 1Chloroform0.14 U
5.0 0.27 ug/L 11/25/14 20:43 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/25/14 20:43 1Chloromethane0.33 U
1.0 0.17 ug/L 11/25/14 20:43 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/25/14 20:43 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/25/14 20:43 1cis-1,2-Dichloroethene 0.34 J
1.0 0.11 ug/L 11/25/14 20:43 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/25/14 20:43 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/25/14 20:43 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/25/14 20:43 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/25/14 20:43 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/25/14 20:43 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/25/14 20:43 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 11/25/14 20:43 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 11/25/14 20:43 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/25/14 20:43 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/25/14 20:43 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/25/14 20:43 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/25/14 20:43 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/25/14 20:43 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/25/14 20:43 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/25/14 20:43 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/25/14 20:43 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/25/14 20:43 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/25/14 20:43 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/25/14 20:43 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/25/14 20:43 1Methylene Chloride 1.0 U Q
10 1.0 ug/L 11/25/14 20:43 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/25/14 20:43 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/25/14 20:43 1Naphthalene1.0 U
1.0 0.10 ug/L 11/25/14 20:43 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/25/14 20:43 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/25/14 20:43 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/25/14 20:43 1Styrene0.11 U
1.0 0.12 ug/L 11/25/14 20:43 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/25/14 20:43 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/25/14 20:43 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/25/14 20:43 1Tetrachloroethene0.15 U
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-3Client Sample ID: LMW-9S-11-14
Matrix: WaterDate Collected: 11/16/14 11:14
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene 0.33 U 1.0 0.33 ug/L 11/25/14 20:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.20 ug/L 11/25/14 20:43 1trans-1,2-Dichloroethene 0.20 U Q
1.0 0.21 ug/L 11/25/14 20:43 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/25/14 20:43 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/25/14 20:43 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/25/14 20:43 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/25/14 20:43 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/25/14 20:43 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/25/14 20:43 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 11/25/14 20:43 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/25/14 20:43 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/25/14 20:43 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/25/14 20:43 1Vinyl chloride 0.18 U Q
Toluene-d8 (Surr)96 70-130 11/25/14 20:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)88 11/25/14 20:43 170-130
Dibromofluoromethane (Surr)91 11/25/14 20:43 170-130
4-Bromofluorobenzene (Surr)98 11/25/14 20:43 170-130
Lab Sample ID: 680-107343-4Client Sample ID: LMW-9-11-14
Matrix: WaterDate Collected: 11/16/14 12:20
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/25/14 21:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/25/14 21:05 1Benzene0.25 U
1.0 0.16 ug/L 11/25/14 21:05 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/25/14 21:05 1Bromoform0.50 U
5.0 2.0 ug/L 11/25/14 21:05 1Bromomethane2.0 U
10 1.0 ug/L 11/25/14 21:05 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/25/14 21:05 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/25/14 21:05 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/25/14 21:05 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/25/14 21:05 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/25/14 21:05 1Chloroethane2.0 U Q
1.0 0.14 ug/L 11/25/14 21:05 1Chloroform0.14 U
5.0 0.27 ug/L 11/25/14 21:05 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/25/14 21:05 1Chloromethane0.33 U
1.0 0.17 ug/L 11/25/14 21:05 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/25/14 21:05 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/25/14 21:05 1cis-1,2-Dichloroethene 0.30 J
1.0 0.11 ug/L 11/25/14 21:05 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/25/14 21:05 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/25/14 21:05 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/25/14 21:05 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/25/14 21:05 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/25/14 21:05 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/25/14 21:05 1Dichlorodifluoromethane0.25 U
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-4Client Sample ID: LMW-9-11-14
Matrix: WaterDate Collected: 11/16/14 12:20
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloroethane 0.25 U 1.0 0.25 ug/L 11/25/14 21:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.10 ug/L 11/25/14 21:05 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/25/14 21:05 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/25/14 21:05 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/25/14 21:05 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/25/14 21:05 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/25/14 21:05 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/25/14 21:05 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/25/14 21:05 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/25/14 21:05 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/25/14 21:05 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/25/14 21:05 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/25/14 21:05 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/25/14 21:05 1Methylene Chloride 1.0 U Q
10 1.0 ug/L 11/25/14 21:05 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/25/14 21:05 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/25/14 21:05 1Naphthalene1.0 U
1.0 0.10 ug/L 11/25/14 21:05 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/25/14 21:05 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/25/14 21:05 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/25/14 21:05 1Styrene0.11 U
1.0 0.12 ug/L 11/25/14 21:05 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/25/14 21:05 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/25/14 21:05 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/25/14 21:05 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 11/25/14 21:05 1Toluene0.33 U
1.0 0.20 ug/L 11/25/14 21:05 1trans-1,2-Dichloroethene 0.20 U Q
1.0 0.21 ug/L 11/25/14 21:05 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/25/14 21:05 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/25/14 21:05 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/25/14 21:05 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/25/14 21:05 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/25/14 21:05 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/25/14 21:05 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 11/25/14 21:05 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/25/14 21:05 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/25/14 21:05 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/25/14 21:05 1Vinyl chloride 0.18 U Q
Toluene-d8 (Surr)92 70-130 11/25/14 21:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)74 11/25/14 21:05 170-130
Dibromofluoromethane (Surr)91 11/25/14 21:05 170-130
4-Bromofluorobenzene (Surr)127 11/25/14 21:05 170-130
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-5Client Sample ID: LMW-16-11-14
Matrix: WaterDate Collected: 11/16/14 14:17
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 13:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/26/14 13:21 1Benzene0.25 U
1.0 0.16 ug/L 11/26/14 13:21 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/26/14 13:21 1Bromoform0.50 U
5.0 2.0 ug/L 11/26/14 13:21 1Bromomethane2.0 U
10 1.0 ug/L 11/26/14 13:21 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/26/14 13:21 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/26/14 13:21 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/26/14 13:21 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/26/14 13:21 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/26/14 13:21 1Chloroethane2.0 U
1.0 0.14 ug/L 11/26/14 13:21 1Chloroform0.14 U
5.0 0.27 ug/L 11/26/14 13:21 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/26/14 13:21 1Chloromethane0.33 U
1.0 0.17 ug/L 11/26/14 13:21 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/26/14 13:21 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/26/14 13:21 1cis-1,2-Dichloroethene 0.15 U
1.0 0.11 ug/L 11/26/14 13:21 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/26/14 13:21 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/26/14 13:21 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/26/14 13:21 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/26/14 13:21 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/26/14 13:21 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/26/14 13:21 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 11/26/14 13:21 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 11/26/14 13:21 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/26/14 13:21 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/26/14 13:21 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/26/14 13:21 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/26/14 13:21 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/26/14 13:21 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/26/14 13:21 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/26/14 13:21 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/26/14 13:21 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/26/14 13:21 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/26/14 13:21 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/26/14 13:21 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/26/14 13:21 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/26/14 13:21 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/26/14 13:21 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/26/14 13:21 1Naphthalene1.0 U
1.0 0.10 ug/L 11/26/14 13:21 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/26/14 13:21 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/26/14 13:21 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/26/14 13:21 1Styrene0.11 U
1.0 0.12 ug/L 11/26/14 13:21 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/26/14 13:21 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/26/14 13:21 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/26/14 13:21 1Tetrachloroethene0.15 U
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-5Client Sample ID: LMW-16-11-14
Matrix: WaterDate Collected: 11/16/14 14:17
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene 0.33 U 1.0 0.33 ug/L 11/26/14 13:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.20 ug/L 11/26/14 13:21 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/26/14 13:21 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/26/14 13:21 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/26/14 13:21 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/26/14 13:21 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/26/14 13:21 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/26/14 13:21 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/26/14 13:21 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 11/26/14 13:21 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/26/14 13:21 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/26/14 13:21 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/26/14 13:21 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)95 70-130 11/26/14 13:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)80 11/26/14 13:21 170-130
Dibromofluoromethane (Surr)88 11/26/14 13:21 170-130
4-Bromofluorobenzene (Surr)100 11/26/14 13:21 170-130
Lab Sample ID: 680-107343-6Client Sample ID: LMW-10-11-14
Matrix: WaterDate Collected: 11/17/14 09:50
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 13:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/26/14 13:42 1Benzene0.25 U
1.0 0.16 ug/L 11/26/14 13:42 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/26/14 13:42 1Bromoform0.50 U
5.0 2.0 ug/L 11/26/14 13:42 1Bromomethane2.0 U
10 1.0 ug/L 11/26/14 13:42 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/26/14 13:42 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/26/14 13:42 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/26/14 13:42 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/26/14 13:42 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/26/14 13:42 1Chloroethane2.0 U
1.0 0.14 ug/L 11/26/14 13:42 1Chloroform0.14 U
5.0 0.27 ug/L 11/26/14 13:42 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/26/14 13:42 1Chloromethane0.33 U
1.0 0.17 ug/L 11/26/14 13:42 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/26/14 13:42 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/26/14 13:42 1cis-1,2-Dichloroethene 0.17 J
1.0 0.11 ug/L 11/26/14 13:42 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/26/14 13:42 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/26/14 13:42 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/26/14 13:42 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/26/14 13:42 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/26/14 13:42 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/26/14 13:42 1Dichlorodifluoromethane2.8
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-6Client Sample ID: LMW-10-11-14
Matrix: WaterDate Collected: 11/17/14 09:50
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloroethane 0.25 U 1.0 0.25 ug/L 11/26/14 13:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.10 ug/L 11/26/14 13:42 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/26/14 13:42 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/26/14 13:42 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/26/14 13:42 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/26/14 13:42 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/26/14 13:42 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/26/14 13:42 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/26/14 13:42 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/26/14 13:42 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/26/14 13:42 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/26/14 13:42 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/26/14 13:42 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/26/14 13:42 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/26/14 13:42 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/26/14 13:42 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/26/14 13:42 1Naphthalene1.0 U
1.0 0.10 ug/L 11/26/14 13:42 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/26/14 13:42 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/26/14 13:42 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/26/14 13:42 1Styrene0.11 U
1.0 0.12 ug/L 11/26/14 13:42 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/26/14 13:42 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/26/14 13:42 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/26/14 13:42 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 11/26/14 13:42 1Toluene0.33 U
1.0 0.20 ug/L 11/26/14 13:42 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/26/14 13:42 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/26/14 13:42 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/26/14 13:42 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/26/14 13:42 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/26/14 13:42 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/26/14 13:42 1Trichloroethene1.8
1.0 0.25 ug/L 11/26/14 13:42 1Trichlorofluoromethane4.0
1.0 0.41 ug/L 11/26/14 13:42 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/26/14 13:42 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/26/14 13:42 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/26/14 13:42 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)95 70-130 11/26/14 13:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)78 11/26/14 13:42 170-130
Dibromofluoromethane (Surr)93 11/26/14 13:42 170-130
4-Bromofluorobenzene (Surr)108 11/26/14 13:42 170-130
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-7Client Sample ID: LMW-4R-11-14
Matrix: WaterDate Collected: 11/17/14 11:12
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 14:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/26/14 14:03 1Benzene0.25 U
1.0 0.16 ug/L 11/26/14 14:03 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/26/14 14:03 1Bromoform0.50 U
5.0 2.0 ug/L 11/26/14 14:03 1Bromomethane2.0 U
10 1.0 ug/L 11/26/14 14:03 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/26/14 14:03 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/26/14 14:03 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/26/14 14:03 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/26/14 14:03 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/26/14 14:03 1Chloroethane2.0 U
1.0 0.14 ug/L 11/26/14 14:03 1Chloroform0.14 U
5.0 0.27 ug/L 11/26/14 14:03 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/26/14 14:03 1Chloromethane0.33 U
1.0 0.17 ug/L 11/26/14 14:03 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/26/14 14:03 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/26/14 14:03 1cis-1,2-Dichloroethene 0.15 U
1.0 0.11 ug/L 11/26/14 14:03 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/26/14 14:03 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/26/14 14:03 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/26/14 14:03 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/26/14 14:03 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/26/14 14:03 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/26/14 14:03 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 11/26/14 14:03 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 11/26/14 14:03 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/26/14 14:03 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/26/14 14:03 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/26/14 14:03 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/26/14 14:03 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/26/14 14:03 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/26/14 14:03 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/26/14 14:03 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/26/14 14:03 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/26/14 14:03 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/26/14 14:03 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/26/14 14:03 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/26/14 14:03 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/26/14 14:03 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/26/14 14:03 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/26/14 14:03 1Naphthalene1.0 U
1.0 0.10 ug/L 11/26/14 14:03 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/26/14 14:03 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/26/14 14:03 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/26/14 14:03 1Styrene0.11 U
1.0 0.12 ug/L 11/26/14 14:03 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/26/14 14:03 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/26/14 14:03 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/26/14 14:03 1Tetrachloroethene0.15 U
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-7Client Sample ID: LMW-4R-11-14
Matrix: WaterDate Collected: 11/17/14 11:12
Date Received: 11/18/14 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene 0.33 U 1.0 0.33 ug/L 11/26/14 14:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.20 ug/L 11/26/14 14:03 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/26/14 14:03 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/26/14 14:03 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/26/14 14:03 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/26/14 14:03 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/26/14 14:03 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/26/14 14:03 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/26/14 14:03 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 11/26/14 14:03 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/26/14 14:03 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/26/14 14:03 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/26/14 14:03 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)79 70-130 11/26/14 14:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)70 11/26/14 14:03 170-130
Dibromofluoromethane (Surr)87 11/26/14 14:03 170-130
4-Bromofluorobenzene (Surr)89 11/26/14 14:03 170-130
Lab Sample ID: 680-107343-8Client Sample ID: LMW-9D-11-14
Matrix: WaterDate Collected: 11/17/14 07:30
Date Received: 11/18/14 10:05
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.12 0.050 0.023 mg/L 11/18/14 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/18/14 14:08 11/19/14 00:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 00:19 1Arsenic1.9
1.0 0.15 ug/L 11/18/14 14:08 11/19/14 00:19 1Barium3.2
0.20 0.070 ug/L 11/18/14 14:08 11/19/14 00:19 1Beryllium0.070 U
0.50 0.20 ug/L 11/18/14 14:08 11/19/14 00:19 1Cadmium0.20 U
1.0 0.16 ug/L 11/18/14 14:08 11/19/14 00:19 1Chromium0.80 J
0.20 0.078 ug/L 11/18/14 14:08 11/19/14 00:19 1Cobalt0.078 U
1.0 0.21 ug/L 11/18/14 14:08 11/19/14 00:19 1Copper1.1
0.30 0.080 ug/L 11/18/14 14:08 11/19/14 00:19 1Lead0.61
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 00:19 1Nickel1.0
0.50 0.21 ug/L 11/18/14 14:08 11/19/14 00:19 1Selenium0.35 J
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 00:19 1Silver0.10 U
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 00:19 1Thallium0.10 U
5.0 1.4 ug/L 11/18/14 14:08 11/19/14 00:19 1Vanadium3.1 J
10 2.6 ug/L 11/18/14 14:08 11/19/14 00:19 1Zinc4.0 J
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-9Client Sample ID: LMW-9S-11-14
Matrix: WaterDate Collected: 11/17/14 07:45
Date Received: 11/18/14 10:05
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.046 U 0.10 0.046 mg/L 11/18/14 18:56 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/18/14 14:08 11/19/14 00:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 00:46 1Arsenic1.4
1.0 0.15 ug/L 11/18/14 14:08 11/19/14 00:46 1Barium51
0.20 0.070 ug/L 11/18/14 14:08 11/19/14 00:46 1Beryllium0.070 U
0.50 0.20 ug/L 11/18/14 14:08 11/19/14 00:46 1Cadmium0.20 U
1.0 0.16 ug/L 11/18/14 14:08 11/19/14 00:46 1Chromium0.16 U
0.20 0.078 ug/L 11/18/14 14:08 11/19/14 00:46 1Cobalt1.8
1.0 0.21 ug/L 11/18/14 14:08 11/19/14 00:46 1Copper0.65 J
0.30 0.080 ug/L 11/18/14 14:08 11/19/14 00:46 1Lead0.080 U
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 00:46 1Nickel0.45 J
0.50 0.21 ug/L 11/18/14 14:08 11/19/14 00:46 1Selenium0.38 J
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 00:46 1Silver0.10 U
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 00:46 1Thallium0.10 U
5.0 1.4 ug/L 11/18/14 14:08 11/19/14 00:46 1Vanadium1.4 U
10 2.6 ug/L 11/18/14 14:08 11/19/14 00:46 1Zinc2.6 U
Lab Sample ID: 680-107343-10Client Sample ID: LMW-9-11-14
Matrix: WaterDate Collected: 11/17/14 07:55
Date Received: 11/18/14 10:05
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.11 0.050 0.023 mg/L 11/18/14 19:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/18/14 14:08 11/19/14 00:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 00:51 1Arsenic0.40 U
1.0 0.15 ug/L 11/18/14 14:08 11/19/14 00:51 1Barium3.8
0.20 0.070 ug/L 11/18/14 14:08 11/19/14 00:51 1Beryllium0.11 J
0.50 0.20 ug/L 11/18/14 14:08 11/19/14 00:51 1Cadmium0.20 U
1.0 0.16 ug/L 11/18/14 14:08 11/19/14 00:51 1Chromium0.37 J
0.20 0.078 ug/L 11/18/14 14:08 11/19/14 00:51 1Cobalt0.19 J
1.0 0.21 ug/L 11/18/14 14:08 11/19/14 00:51 1Copper0.84 J
0.30 0.080 ug/L 11/18/14 14:08 11/19/14 00:51 1Lead0.080 U
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 00:51 1Nickel0.70 J
0.50 0.21 ug/L 11/18/14 14:08 11/19/14 00:51 1Selenium0.21 U
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 00:51 1Silver0.10 U
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 00:51 1Thallium0.10 U
5.0 1.4 ug/L 11/18/14 14:08 11/19/14 00:51 1Vanadium1.4 U
10 2.6 ug/L 11/18/14 14:08 11/19/14 00:51 1Zinc3.0 J
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-11Client Sample ID: LMW-16-11-14
Matrix: WaterDate Collected: 11/17/14 08:10
Date Received: 11/18/14 10:05
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.023 U 0.050 0.023 mg/L 11/18/14 19:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/18/14 14:08 11/19/14 00:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 00:56 1Arsenic3.3
1.0 0.15 ug/L 11/18/14 14:08 11/19/14 00:56 1Barium6.2
0.20 0.070 ug/L 11/18/14 14:08 11/19/14 00:56 1Beryllium0.070 U
0.50 0.20 ug/L 11/18/14 14:08 11/19/14 00:56 1Cadmium0.20 U
1.0 0.16 ug/L 11/18/14 14:08 11/19/14 00:56 1Chromium0.28 J
0.20 0.078 ug/L 11/18/14 14:08 11/19/14 00:56 1Cobalt0.19 J
1.0 0.21 ug/L 11/18/14 14:08 11/19/14 00:56 1Copper0.51 J
0.30 0.080 ug/L 11/18/14 14:08 11/19/14 00:56 1Lead0.20 J
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 00:56 1Nickel0.41 J
0.50 0.21 ug/L 11/18/14 14:08 11/19/14 00:56 1Selenium0.31 J
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 00:56 1Silver0.10 U
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 00:56 1Thallium0.10 U
5.0 1.4 ug/L 11/18/14 14:08 11/19/14 00:56 1Vanadium1.4 U
10 2.6 ug/L 11/18/14 14:08 11/19/14 00:56 1Zinc2.6 U
Lab Sample ID: 680-107343-12Client Sample ID: LMW-10-11-14
Matrix: WaterDate Collected: 11/17/14 09:50
Date Received: 11/18/14 10:05
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.39 0.050 0.023 mg/L 11/18/14 19:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/18/14 14:08 11/19/14 01:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 01:12 1Arsenic0.40 U
1.0 0.15 ug/L 11/18/14 14:08 11/19/14 01:12 1Barium17
0.20 0.070 ug/L 11/18/14 14:08 11/19/14 01:12 1Beryllium0.070 U
0.50 0.20 ug/L 11/18/14 14:08 11/19/14 01:12 1Cadmium0.20 U
1.0 0.16 ug/L 11/18/14 14:08 11/19/14 01:12 1Chromium0.65 J
0.20 0.078 ug/L 11/18/14 14:08 11/19/14 01:12 1Cobalt0.16 J
1.0 0.21 ug/L 11/18/14 14:08 11/19/14 01:12 1Copper0.27 J
0.30 0.080 ug/L 11/18/14 14:08 11/19/14 01:12 1Lead1.1
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 01:12 1Nickel0.64 J
0.50 0.21 ug/L 11/18/14 14:08 11/19/14 01:12 1Selenium1.2
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 01:12 1Silver0.10 U
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 01:12 1Thallium0.10 U
5.0 1.4 ug/L 11/18/14 14:08 11/19/14 01:12 1Vanadium1.4 U
10 2.6 ug/L 11/18/14 14:08 11/19/14 01:12 1Zinc3.3 J
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Client Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107343-13Client Sample ID: LMW-4R-11-14
Matrix: WaterDate Collected: 11/17/14 11:12
Date Received: 11/18/14 10:05
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.057 0.050 0.023 mg/L 11/18/14 21:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/18/14 14:08 11/19/14 01:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 01:18 1Arsenic0.48 J
1.0 0.15 ug/L 11/18/14 14:08 11/19/14 01:18 1Barium6.9
0.20 0.070 ug/L 11/18/14 14:08 11/19/14 01:18 1Beryllium0.070 U
0.50 0.20 ug/L 11/18/14 14:08 11/19/14 01:18 1Cadmium0.20 U
1.0 0.16 ug/L 11/18/14 14:08 11/19/14 01:18 1Chromium1.4
0.20 0.078 ug/L 11/18/14 14:08 11/19/14 01:18 1Cobalt0.19 J
1.0 0.21 ug/L 11/18/14 14:08 11/19/14 01:18 1Copper0.49 J
0.30 0.080 ug/L 11/18/14 14:08 11/19/14 01:18 1Lead1.2
1.0 0.40 ug/L 11/18/14 14:08 11/19/14 01:18 1Nickel0.81 J
0.50 0.21 ug/L 11/18/14 14:08 11/19/14 01:18 1Selenium0.45 J
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 01:18 1Silver0.10 U
0.20 0.10 ug/L 11/18/14 14:08 11/19/14 01:18 1Thallium0.10 U
5.0 1.4 ug/L 11/18/14 14:08 11/19/14 01:18 1Vanadium2.0 J
10 2.6 ug/L 11/18/14 14:08 11/19/14 01:18 1Zinc2.6 U
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Surrogate Summary
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-130)(70-130)(70-130)(70-130)
TOL 12DCE DBFM BFB
97 81 91 101680-107343-1
Percent Surrogate Recovery (Acceptance Limits)
LMW-9D-11-14
101 71 91 156 J680-107343-2 Trip Blank
96 88 91 98680-107343-3 LMW-9S-11-14
92 74 91 127680-107343-4 LMW-9-11-14
95 80 88 100680-107343-5 LMW-16-11-14
95 78 93 108680-107343-6 LMW-10-11-14
79 70 87 89680-107343-7 LMW-4R-11-14
75 79 81 77LCS 680-360309/4 Lab Control Sample
104 91 92 75LCS 680-360546/6 Lab Control Sample
103 86 95 92LCSD 680-360309/11 Lab Control Sample Dup
104 77 77 89LCSD 680-360546/7 Lab Control Sample Dup
72 94 108 104MB 680-360309/9 Method Blank
97 78 87 104MB 680-360546/11 Method Blank
Surrogate Legend
TOL = Toluene-d8 (Surr)
12DCE = 1,2-Dichloroethane-d4 (Surr)
DBFM = Dibromofluoromethane (Surr)
BFB = 4-Bromofluorobenzene (Surr)
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-360309/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360309
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/25/14 13:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.25 U 0.251.0 ug/L 11/25/14 13:57 1Benzene
0.16 U 0.161.0 ug/L 11/25/14 13:57 1Bromobenzene
0.50 U 0.501.0 ug/L 11/25/14 13:57 1Bromoform
2.0 U 2.05.0 ug/L 11/25/14 13:57 1Bromomethane
1.0 U 1.010 ug/L 11/25/14 13:57 12-Butanone (MEK)
0.50 U 0.501.0 ug/L 11/25/14 13:57 1Carbon tetrachloride
0.25 U 0.251.0 ug/L 11/25/14 13:57 1Chlorobenzene
0.14 U 0.141.0 ug/L 11/25/14 13:57 1Chlorobromomethane
0.10 U 0.101.0 ug/L 11/25/14 13:57 1Chlorodibromomethane
2.0 U 2.05.0 ug/L 11/25/14 13:57 1Chloroethane
0.14 U 0.141.0 ug/L 11/25/14 13:57 1Chloroform
0.27 U 0.275.0 ug/L 11/25/14 13:57 11-Chlorohexane
0.33 U 0.331.0 ug/L 11/25/14 13:57 1Chloromethane
0.17 U 0.171.0 ug/L 11/25/14 13:57 12-Chlorotoluene
0.27 U 0.271.0 ug/L 11/25/14 13:57 14-Chlorotoluene
0.15 U 0.151.0 ug/L 11/25/14 13:57 1cis-1,2-Dichloroethene
0.11 U 0.111.0 ug/L 11/25/14 13:57 1cis-1,3-Dichloropropene
0.44 U 0.445.0 ug/L 11/25/14 13:57 11,2-Dibromo-3-Chloropropane
0.21 U 0.211.0 ug/L 11/25/14 13:57 11,2-Dichlorobenzene
0.25 U 0.251.0 ug/L 11/25/14 13:57 11,3-Dichlorobenzene
0.28 U 0.281.0 ug/L 11/25/14 13:57 11,4-Dichlorobenzene
0.25 U 0.251.0 ug/L 11/25/14 13:57 1Dichlorobromomethane
0.25 U 0.251.0 ug/L 11/25/14 13:57 1Dichlorodifluoromethane
0.25 U 0.251.0 ug/L 11/25/14 13:57 11,1-Dichloroethane
0.10 U 0.101.0 ug/L 11/25/14 13:57 11,2-Dichloroethane
0.11 U 0.111.0 ug/L 11/25/14 13:57 11,1-Dichloroethene
0.13 U 0.131.0 ug/L 11/25/14 13:57 11,2-Dichloropropane
0.13 U 0.131.0 ug/L 11/25/14 13:57 11,3-Dichloropropane
0.12 U 0.121.0 ug/L 11/25/14 13:57 12,2-Dichloropropane
0.25 U 0.251.0 ug/L 11/25/14 13:57 11,1-Dichloropropene
0.11 U 0.111.0 ug/L 11/25/14 13:57 1Ethylbenzene
0.25 U 0.251.0 ug/L 11/25/14 13:57 1Ethylene Dibromide
0.741 J 0.405.0 ug/L 11/25/14 13:57 1Hexachlorobutadiene
0.10 U 0.101.0 ug/L 11/25/14 13:57 1Isopropylbenzene
0.24 U 0.2410 ug/L 11/25/14 13:57 1Isopropyl ether
0.13 U 0.131.0 ug/L 11/25/14 13:57 14-Isopropyltoluene
1.0 U 1.05.0 ug/L 11/25/14 13:57 1Methylene Chloride
1.0 U 1.010 ug/L 11/25/14 13:57 14-Methyl-2-pentanone (MIBK)
0.20 U 0.2010 ug/L 11/25/14 13:57 1Methyl tert-butyl ether
1.0 U 1.05.0 ug/L 11/25/14 13:57 1Naphthalene
0.10 U 0.101.0 ug/L 11/25/14 13:57 1n-Butylbenzene
0.15 U 0.151.0 ug/L 11/25/14 13:57 1N-Propylbenzene
0.16 U 0.161.0 ug/L 11/25/14 13:57 1sec-Butylbenzene
0.11 U 0.111.0 ug/L 11/25/14 13:57 1Styrene
0.12 U 0.121.0 ug/L 11/25/14 13:57 1tert-Butylbenzene
0.33 U 0.331.0 ug/L 11/25/14 13:57 11,1,1,2-Tetrachloroethane
0.18 U 0.181.0 ug/L 11/25/14 13:57 11,1,2,2-Tetrachloroethane
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-360309/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360309
RL MDL
Tetrachloroethene 0.15 U 1.0 0.15 ug/L 11/25/14 13:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.33 U 0.331.0 ug/L 11/25/14 13:57 1Toluene
0.20 U 0.201.0 ug/L 11/25/14 13:57 1trans-1,2-Dichloroethene
0.21 U 0.211.0 ug/L 11/25/14 13:57 1trans-1,3-Dichloropropene
0.35 U 0.355.0 ug/L 11/25/14 13:57 11,2,3-Trichlorobenzene
0.295 J 0.255.0 ug/L 11/25/14 13:57 11,2,4-Trichlorobenzene
0.50 U 0.501.0 ug/L 11/25/14 13:57 11,1,1-Trichloroethane
0.13 U 0.131.0 ug/L 11/25/14 13:57 11,1,2-Trichloroethane
0.13 U 0.131.0 ug/L 11/25/14 13:57 1Trichloroethene
0.25 U 0.251.0 ug/L 11/25/14 13:57 1Trichlorofluoromethane
0.41 U 0.411.0 ug/L 11/25/14 13:57 11,2,3-Trichloropropane
0.33 U 0.331.0 ug/L 11/25/14 13:57 11,2,4-Trimethylbenzene
0.33 U 0.331.0 ug/L 11/25/14 13:57 11,3,5-Trimethylbenzene
0.18 U 0.181.0 ug/L 11/25/14 13:57 1Vinyl chloride
Toluene-d8 (Surr)72 70-130 11/25/14 13:57 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
94 11/25/14 13:57 11,2-Dichloroethane-d4 (Surr)70-130
108 11/25/14 13:57 1Dibromofluoromethane (Surr)70-130
104 11/25/14 13:57 14-Bromofluorobenzene (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-360309/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360309
Acetone 250 196 ug/L 78 39 -162
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 41.1 ug/L 82 74 -123
Bromobenzene 50.0 47.2 ug/L 94 79 -125
Bromoform 50.0 44.1 ug/L 88 60 -134
Bromomethane 50.0 36.4 ug/L 73 10 -171
2-Butanone (MEK)250 202 ug/L 81 55 -142
Carbon tetrachloride 50.0 41.5 ug/L 83 70 -131
Chlorobenzene 50.0 43.7 ug/L 87 79 -120
Chlorobromomethane 50.0 40.3 ug/L 81 60 -136
Chlorodibromomethane 50.0 43.6 ug/L 87 63 -134
Chloroethane 50.0 36.9 ug/L 74 47 -148
Chloroform 50.0 40.2 ug/L 80 76 -128
Chloromethane 50.0 36.9 ug/L 74 47 -151
2-Chlorotoluene 50.0 45.6 ug/L 91 78 -126
4-Chlorotoluene 50.0 45.1 ug/L 90 79 -124
cis-1,2-Dichloroethene 50.0 40.9 ug/L 82 78 -127
cis-1,3-Dichloropropene 50.0 44.4 ug/L 89 73 -128
1,2-Dibromo-3-Chloropropane 50.0 42.4 ug/L 85 57 -126
1,2-Dichlorobenzene 50.0 44.5 ug/L 89 77 -124
1,3-Dichlorobenzene 50.0 42.2 ug/L 84 79 -123
1,4-Dichlorobenzene 50.0 42.6 ug/L 85 76 -124
Dichlorobromomethane 50.0 44.4 ug/L 89 72 -129
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-360309/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360309
Dichlorodifluoromethane 50.0 39.8 ug/L 80 41 -165
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1-Dichloroethane 50.0 39.7 ug/L 79 69 -132
1,2-Dichloroethane 50.0 43.2 ug/L 86 75 -120
1,1-Dichloroethene 50.0 39.6 ug/L 79 73 -134
1,2-Dichloropropane 50.0 45.8 ug/L 92 71 -126
1,3-Dichloropropane 50.0 43.7 ug/L 87 73 -125
2,2-Dichloropropane 50.0 39.4 ug/L 79 72 -147
1,1-Dichloropropene 50.0 39.9 ug/L 80 74 -130
Ethylbenzene 50.0 42.6 ug/L 85 78 -125
Ethylene Dibromide 50.0 42.7 ug/L 85 75 -127
Hexachlorobutadiene 50.0 47.5 ug/L 95 62 -145
Isopropylbenzene 50.0 44.0 ug/L 88 72 -129
4-Isopropyltoluene 50.0 42.0 ug/L 84 69 -129
Methylene Chloride 50.0 39.2 Q ug/L 78 79 -124
4-Methyl-2-pentanone (MIBK)250 221 ug/L 89 51 -143
Methyl tert-butyl ether 50.0 43.9 ug/L 88 76 -126
Naphthalene 50.0 52.5 ug/L 105 56 -136
n-Butylbenzene 50.0 43.6 ug/L 87 72 -128
N-Propylbenzene 50.0 46.5 ug/L 93 74 -130
sec-Butylbenzene 50.0 43.9 ug/L 88 71 -130
Styrene 50.0 47.0 ug/L 94 75 -129
tert-Butylbenzene 50.0 45.0 ug/L 90 72 -130
1,1,1,2-Tetrachloroethane 50.0 44.3 ug/L 89 68 -132
1,1,2,2-Tetrachloroethane 50.0 43.2 ug/L 86 71 -127
Tetrachloroethene 50.0 43.2 ug/L 86 77 -128
Toluene 50.0 43.4 ug/L 87 77 -125
trans-1,2-Dichloroethene 50.0 38.2 Q ug/L 76 78 -130
trans-1,3-Dichloropropene 50.0 42.5 ug/L 85 72 -127
1,2,3-Trichlorobenzene 50.0 52.6 ug/L 105 63 -136
1,2,4-Trichlorobenzene 50.0 53.7 ug/L 107 67 -134
1,1,1-Trichloroethane 50.0 40.6 ug/L 81 76 -126
1,1,2-Trichloroethane 50.0 45.2 ug/L 90 69 -127
Trichloroethene 50.0 43.2 ug/L 86 80 -120
Trichlorofluoromethane 50.0 39.7 ug/L 79 66 -144
1,2,3-Trichloropropane 50.0 44.9 ug/L 90 74 -126
1,2,4-Trimethylbenzene 50.0 46.9 ug/L 94 72 -129
1,3,5-Trimethylbenzene 50.0 46.3 ug/L 93 72 -130
Vinyl chloride 50.0 37.6 ug/L 75 58 -141
Toluene-d8 (Surr)70 -130
Surrogate
75
LCS LCS
Qualifier Limits%Recovery
791,2-Dichloroethane-d4 (Surr)70 -130
81Dibromofluoromethane (Surr)70 -130
774-Bromofluorobenzene (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-360309/11
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360309
Acetone 250 232 ug/L 93 39 -162 17 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 50.0 48.0 ug/L 96 74 -123 15 30
Bromobenzene 50.0 49.0 ug/L 98 79 -125 4 30
Bromoform 50.0 50.4 ug/L 101 60 -134 13 30
Bromomethane 50.0 59.1 ug/L 118 10 -171 48 50
2-Butanone (MEK)250 256 ug/L 102 55 -142 24 30
Carbon tetrachloride 50.0 47.5 ug/L 95 70 -131 13 30
Chlorobenzene 50.0 54.8 ug/L 110 79 -120 22 30
Chlorobromomethane 50.0 46.9 ug/L 94 60 -136 15 30
Chlorodibromomethane 50.0 47.7 ug/L 95 63 -134 9 50
Chloroethane 50.0 58.6 Q ug/L 117 47 -148 45 40
Chloroform 50.0 46.9 ug/L 94 76 -128 15 30
Chloromethane 50.0 47.5 ug/L 95 47 -151 25 30
2-Chlorotoluene 50.0 47.8 ug/L 96 78 -126 5 30
4-Chlorotoluene 50.0 52.9 ug/L 106 79 -124 16 30
cis-1,2-Dichloroethene 50.0 48.5 ug/L 97 78 -127 17 30
cis-1,3-Dichloropropene 50.0 51.7 ug/L 103 73 -128 15 30
1,2-Dibromo-3-Chloropropane 50.0 50.3 ug/L 101 57 -126 17 50
1,2-Dichlorobenzene 50.0 50.5 ug/L 101 77 -124 13 30
1,3-Dichlorobenzene 50.0 51.7 ug/L 103 79 -123 20 30
1,4-Dichlorobenzene 50.0 52.8 ug/L 106 76 -124 21 30
Dichlorobromomethane 50.0 49.8 ug/L 100 72 -129 12 30
Dichlorodifluoromethane 50.0 49.1 ug/L 98 41 -165 21 50
1,1-Dichloroethane 50.0 46.3 ug/L 93 69 -132 15 30
1,2-Dichloroethane 50.0 45.8 ug/L 92 75 -120 6 30
1,1-Dichloroethene 50.0 51.9 ug/L 104 73 -134 27 30
1,2-Dichloropropane 50.0 53.5 ug/L 107 71 -126 15 30
1,3-Dichloropropane 50.0 49.5 ug/L 99 73 -125 12 30
2,2-Dichloropropane 50.0 46.8 ug/L 94 72 -147 17 30
1,1-Dichloropropene 50.0 50.2 ug/L 100 74 -130 23 30
Ethylbenzene 50.0 55.1 ug/L 110 78 -125 26 30
Ethylene Dibromide 50.0 48.8 ug/L 98 75 -127 13 30
Hexachlorobutadiene 50.0 56.1 ug/L 112 62 -145 17 30
Isopropylbenzene 50.0 52.6 ug/L 105 72 -129 18 30
4-Isopropyltoluene 50.0 54.6 ug/L 109 69 -129 26 50
Methylene Chloride 50.0 48.2 ug/L 96 79 -124 21 30
4-Methyl-2-pentanone (MIBK)250 257 ug/L 103 51 -143 15 30
Methyl tert-butyl ether 50.0 50.8 ug/L 102 76 -126 15 30
Naphthalene 50.0 58.7 ug/L 117 56 -136 11 30
n-Butylbenzene 50.0 53.1 ug/L 106 72 -128 20 30
N-Propylbenzene 50.0 48.1 ug/L 96 74 -130 3 30
sec-Butylbenzene 50.0 52.9 ug/L 106 71 -130 18 30
Styrene 50.0 56.3 ug/L 113 75 -129 18 30
tert-Butylbenzene 50.0 54.5 ug/L 109 72 -130 19 30
1,1,1,2-Tetrachloroethane 50.0 54.2 ug/L 108 68 -132 20 30
1,1,2,2-Tetrachloroethane 50.0 42.2 ug/L 84 71 -127 2 30
Tetrachloroethene 50.0 52.1 ug/L 104 77 -128 19 30
Toluene 50.0 51.9 ug/L 104 77 -125 18 30
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-360309/11
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360309
trans-1,2-Dichloroethene 50.0 46.7 ug/L 93 78 -130 20 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
trans-1,3-Dichloropropene 50.0 49.0 ug/L 98 72 -127 14 50
1,2,3-Trichlorobenzene 50.0 56.3 ug/L 113 63 -136 7 30
1,2,4-Trichlorobenzene 50.0 57.1 ug/L 114 67 -134 6 30
1,1,1-Trichloroethane 50.0 46.5 ug/L 93 76 -126 14 30
1,1,2-Trichloroethane 50.0 52.3 ug/L 105 69 -127 15 30
Trichloroethene 50.0 50.6 ug/L 101 80 -120 16 30
Trichlorofluoromethane 50.0 49.2 ug/L 98 66 -144 21 30
1,2,3-Trichloropropane 50.0 46.9 ug/L 94 74 -126 4 30
1,2,4-Trimethylbenzene 50.0 53.0 ug/L 106 72 -129 12 50
1,3,5-Trimethylbenzene 50.0 51.8 ug/L 104 72 -130 11 50
Vinyl chloride 50.0 54.2 Q ug/L 108 58 -141 36 30
Toluene-d8 (Surr)70 -130
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
861,2-Dichloroethane-d4 (Surr)70 -130
95Dibromofluoromethane (Surr)70 -130
924-Bromofluorobenzene (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-360546/11
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360546
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 11:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.25 U 0.251.0 ug/L 11/26/14 11:49 1Benzene
0.16 U 0.161.0 ug/L 11/26/14 11:49 1Bromobenzene
0.50 U 0.501.0 ug/L 11/26/14 11:49 1Bromoform
2.0 U 2.05.0 ug/L 11/26/14 11:49 1Bromomethane
1.0 U 1.010 ug/L 11/26/14 11:49 12-Butanone (MEK)
0.50 U 0.501.0 ug/L 11/26/14 11:49 1Carbon tetrachloride
0.25 U 0.251.0 ug/L 11/26/14 11:49 1Chlorobenzene
0.14 U 0.141.0 ug/L 11/26/14 11:49 1Chlorobromomethane
0.10 U 0.101.0 ug/L 11/26/14 11:49 1Chlorodibromomethane
2.0 U 2.05.0 ug/L 11/26/14 11:49 1Chloroethane
0.14 U 0.141.0 ug/L 11/26/14 11:49 1Chloroform
0.27 U 0.275.0 ug/L 11/26/14 11:49 11-Chlorohexane
0.33 U 0.331.0 ug/L 11/26/14 11:49 1Chloromethane
0.17 U 0.171.0 ug/L 11/26/14 11:49 12-Chlorotoluene
0.27 U 0.271.0 ug/L 11/26/14 11:49 14-Chlorotoluene
0.15 U 0.151.0 ug/L 11/26/14 11:49 1cis-1,2-Dichloroethene
0.11 U 0.111.0 ug/L 11/26/14 11:49 1cis-1,3-Dichloropropene
0.44 U 0.445.0 ug/L 11/26/14 11:49 11,2-Dibromo-3-Chloropropane
0.21 U 0.211.0 ug/L 11/26/14 11:49 11,2-Dichlorobenzene
0.25 U 0.251.0 ug/L 11/26/14 11:49 11,3-Dichlorobenzene
0.28 U 0.281.0 ug/L 11/26/14 11:49 11,4-Dichlorobenzene
0.25 U 0.251.0 ug/L 11/26/14 11:49 1Dichlorobromomethane
0.25 U 0.251.0 ug/L 11/26/14 11:49 1Dichlorodifluoromethane
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-360546/11
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360546
RL MDL
1,1-Dichloroethane 0.25 U 1.0 0.25 ug/L 11/26/14 11:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.10 U 0.101.0 ug/L 11/26/14 11:49 11,2-Dichloroethane
0.11 U 0.111.0 ug/L 11/26/14 11:49 11,1-Dichloroethene
0.13 U 0.131.0 ug/L 11/26/14 11:49 11,2-Dichloropropane
0.13 U 0.131.0 ug/L 11/26/14 11:49 11,3-Dichloropropane
0.12 U 0.121.0 ug/L 11/26/14 11:49 12,2-Dichloropropane
0.25 U 0.251.0 ug/L 11/26/14 11:49 11,1-Dichloropropene
0.11 U 0.111.0 ug/L 11/26/14 11:49 1Ethylbenzene
0.25 U 0.251.0 ug/L 11/26/14 11:49 1Ethylene Dibromide
1.09 J 0.405.0 ug/L 11/26/14 11:49 1Hexachlorobutadiene
0.10 U 0.101.0 ug/L 11/26/14 11:49 1Isopropylbenzene
0.24 U 0.2410 ug/L 11/26/14 11:49 1Isopropyl ether
0.13 U 0.131.0 ug/L 11/26/14 11:49 14-Isopropyltoluene
1.0 U 1.05.0 ug/L 11/26/14 11:49 1Methylene Chloride
1.0 U 1.010 ug/L 11/26/14 11:49 14-Methyl-2-pentanone (MIBK)
0.20 U 0.2010 ug/L 11/26/14 11:49 1Methyl tert-butyl ether
1.0 U 1.05.0 ug/L 11/26/14 11:49 1Naphthalene
0.10 U 0.101.0 ug/L 11/26/14 11:49 1n-Butylbenzene
0.15 U 0.151.0 ug/L 11/26/14 11:49 1N-Propylbenzene
0.16 U 0.161.0 ug/L 11/26/14 11:49 1sec-Butylbenzene
0.11 U 0.111.0 ug/L 11/26/14 11:49 1Styrene
0.12 U 0.121.0 ug/L 11/26/14 11:49 1tert-Butylbenzene
0.33 U 0.331.0 ug/L 11/26/14 11:49 11,1,1,2-Tetrachloroethane
0.18 U 0.181.0 ug/L 11/26/14 11:49 11,1,2,2-Tetrachloroethane
0.15 U 0.151.0 ug/L 11/26/14 11:49 1Tetrachloroethene
0.33 U 0.331.0 ug/L 11/26/14 11:49 1Toluene
0.20 U 0.201.0 ug/L 11/26/14 11:49 1trans-1,2-Dichloroethene
0.21 U 0.211.0 ug/L 11/26/14 11:49 1trans-1,3-Dichloropropene
0.368 J 0.355.0 ug/L 11/26/14 11:49 11,2,3-Trichlorobenzene
0.25 U 0.255.0 ug/L 11/26/14 11:49 11,2,4-Trichlorobenzene
0.50 U 0.501.0 ug/L 11/26/14 11:49 11,1,1-Trichloroethane
0.13 U 0.131.0 ug/L 11/26/14 11:49 11,1,2-Trichloroethane
0.13 U 0.131.0 ug/L 11/26/14 11:49 1Trichloroethene
0.25 U 0.251.0 ug/L 11/26/14 11:49 1Trichlorofluoromethane
0.41 U 0.411.0 ug/L 11/26/14 11:49 11,2,3-Trichloropropane
0.33 U 0.331.0 ug/L 11/26/14 11:49 11,2,4-Trimethylbenzene
0.33 U 0.331.0 ug/L 11/26/14 11:49 11,3,5-Trimethylbenzene
0.18 U 0.181.0 ug/L 11/26/14 11:49 1Vinyl chloride
Toluene-d8 (Surr)97 70-130 11/26/14 11:49 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
78 11/26/14 11:49 11,2-Dichloroethane-d4 (Surr)70-130
87 11/26/14 11:49 1Dibromofluoromethane (Surr)70-130
104 11/26/14 11:49 14-Bromofluorobenzene (Surr)70-130
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-360546/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360546
Acetone 250 276 ug/L 110 39 -162
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 47.1 ug/L 94 74 -123
Bromobenzene 50.0 51.4 ug/L 103 79 -125
Bromoform 50.0 51.7 ug/L 103 60 -134
Bromomethane 50.0 54.4 ug/L 109 10 -171
2-Butanone (MEK)250 249 ug/L 100 55 -142
Carbon tetrachloride 50.0 45.0 ug/L 90 70 -131
Chlorobenzene 50.0 51.2 ug/L 102 79 -120
Chlorobromomethane 50.0 46.6 ug/L 93 60 -136
Chlorodibromomethane 50.0 42.8 ug/L 86 63 -134
Chloroethane 50.0 45.2 ug/L 90 47 -148
Chloroform 50.0 46.0 ug/L 92 76 -128
Chloromethane 50.0 55.9 ug/L 112 47 -151
2-Chlorotoluene 50.0 50.5 ug/L 101 78 -126
4-Chlorotoluene 50.0 51.7 ug/L 103 79 -124
cis-1,2-Dichloroethene 50.0 48.1 ug/L 96 78 -127
cis-1,3-Dichloropropene 50.0 52.6 ug/L 105 73 -128
1,2-Dibromo-3-Chloropropane 50.0 46.7 ug/L 93 57 -126
1,2-Dichlorobenzene 50.0 46.5 ug/L 93 77 -124
1,3-Dichlorobenzene 50.0 46.8 ug/L 94 79 -123
1,4-Dichlorobenzene 50.0 47.8 ug/L 96 76 -124
Dichlorobromomethane 50.0 50.8 ug/L 102 72 -129
Dichlorodifluoromethane 50.0 54.6 ug/L 109 41 -165
1,1-Dichloroethane 50.0 45.6 ug/L 91 69 -132
1,2-Dichloroethane 50.0 47.5 ug/L 95 75 -120
1,1-Dichloroethene 50.0 57.0 ug/L 114 73 -134
1,2-Dichloropropane 50.0 52.2 ug/L 104 71 -126
1,3-Dichloropropane 50.0 43.5 ug/L 87 73 -125
2,2-Dichloropropane 50.0 46.5 ug/L 93 72 -147
1,1-Dichloropropene 50.0 46.0 ug/L 92 74 -130
Ethylbenzene 50.0 48.1 ug/L 96 78 -125
Ethylene Dibromide 50.0 43.9 ug/L 88 75 -127
Hexachlorobutadiene 50.0 49.8 ug/L 100 62 -145
Isopropylbenzene 50.0 50.1 ug/L 100 72 -129
4-Isopropyltoluene 50.0 47.6 ug/L 95 69 -129
Methylene Chloride 50.0 56.2 ug/L 112 79 -124
4-Methyl-2-pentanone (MIBK)250 259 ug/L 104 51 -143
Methyl tert-butyl ether 50.0 61.7 ug/L 123 76 -126
Naphthalene 50.0 53.0 ug/L 106 56 -136
n-Butylbenzene 50.0 47.3 ug/L 95 72 -128
N-Propylbenzene 50.0 50.8 ug/L 102 74 -130
sec-Butylbenzene 50.0 61.2 ug/L 122 71 -130
Styrene 50.0 51.0 ug/L 102 75 -129
tert-Butylbenzene 50.0 55.0 ug/L 110 72 -130
1,1,1,2-Tetrachloroethane 50.0 50.7 ug/L 101 68 -132
1,1,2,2-Tetrachloroethane 50.0 49.6 ug/L 99 71 -127
Tetrachloroethene 50.0 43.1 ug/L 86 77 -128
Toluene 50.0 51.0 ug/L 102 77 -125
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-360546/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360546
trans-1,2-Dichloroethene 50.0 54.5 ug/L 109 78 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
trans-1,3-Dichloropropene 50.0 47.3 ug/L 95 72 -127
1,2,3-Trichlorobenzene 50.0 54.1 ug/L 108 63 -136
1,2,4-Trichlorobenzene 50.0 53.6 ug/L 107 67 -134
1,1,1-Trichloroethane 50.0 45.3 ug/L 91 76 -126
1,1,2-Trichloroethane 50.0 46.0 ug/L 92 69 -127
Trichloroethene 50.0 48.8 ug/L 98 80 -120
Trichlorofluoromethane 50.0 52.7 ug/L 105 66 -144
1,2,3-Trichloropropane 50.0 49.8 ug/L 100 74 -126
1,2,4-Trimethylbenzene 50.0 62.5 ug/L 125 72 -129
1,3,5-Trimethylbenzene 50.0 52.9 ug/L 106 72 -130
Vinyl chloride 50.0 61.8 ug/L 124 58 -141
Toluene-d8 (Surr)70 -130
Surrogate
104
LCS LCS
Qualifier Limits%Recovery
911,2-Dichloroethane-d4 (Surr)70 -130
92Dibromofluoromethane (Surr)70 -130
754-Bromofluorobenzene (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-360546/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360546
Acetone 250 250 ug/L 100 39 -162 10 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 50.0 41.2 ug/L 82 74 -123 13 30
Bromobenzene 50.0 56.0 ug/L 112 79 -125 9 30
Bromoform 50.0 56.4 ug/L 113 60 -134 9 30
Bromomethane 50.0 53.9 ug/L 108 10 -171 1 50
2-Butanone (MEK)250 236 ug/L 94 55 -142 6 30
Carbon tetrachloride 50.0 40.1 ug/L 80 70 -131 11 30
Chlorobenzene 50.0 50.8 ug/L 102 79 -120 1 30
Chlorobromomethane 50.0 37.0 ug/L 74 60 -136 23 30
Chlorodibromomethane 50.0 45.5 ug/L 91 63 -134 6 50
Chloroethane 50.0 39.6 ug/L 79 47 -148 13 40
Chloroform 50.0 37.8 ug/L 76 76 -128 20 30
Chloromethane 50.0 49.6 ug/L 99 47 -151 12 30
2-Chlorotoluene 50.0 54.8 ug/L 110 78 -126 8 30
4-Chlorotoluene 50.0 56.3 ug/L 113 79 -124 9 30
cis-1,2-Dichloroethene 50.0 44.4 ug/L 89 78 -127 8 30
cis-1,3-Dichloropropene 50.0 48.4 ug/L 97 73 -128 8 30
1,2-Dibromo-3-Chloropropane 50.0 35.3 ug/L 71 57 -126 28 50
1,2-Dichlorobenzene 50.0 45.9 ug/L 92 77 -124 1 30
1,3-Dichlorobenzene 50.0 48.1 ug/L 96 79 -123 3 30
1,4-Dichlorobenzene 50.0 48.6 ug/L 97 76 -124 2 30
Dichlorobromomethane 50.0 50.4 ug/L 101 72 -129 1 30
Dichlorodifluoromethane 50.0 49.3 ug/L 99 41 -165 10 50
1,1-Dichloroethane 50.0 44.6 ug/L 89 69 -132 2 30
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-360546/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360546
1,2-Dichloroethane 50.0 41.3 ug/L 83 75 -120 14 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1-Dichloroethene 50.0 53.2 ug/L 106 73 -134 7 30
1,2-Dichloropropane 50.0 45.8 ug/L 92 71 -126 13 30
1,3-Dichloropropane 50.0 47.1 ug/L 94 73 -125 8 30
2,2-Dichloropropane 50.0 42.5 ug/L 85 72 -147 9 30
1,1-Dichloropropene 50.0 38.7 ug/L 77 74 -130 17 30
Ethylbenzene 50.0 52.9 ug/L 106 78 -125 9 30
Ethylene Dibromide 50.0 46.6 ug/L 93 75 -127 6 30
Hexachlorobutadiene 50.0 54.1 ug/L 108 62 -145 8 30
Isopropylbenzene 50.0 44.5 ug/L 89 72 -129 12 30
4-Isopropyltoluene 50.0 48.9 ug/L 98 69 -129 3 50
Methylene Chloride 50.0 52.8 ug/L 106 79 -124 6 30
4-Methyl-2-pentanone (MIBK)250 249 ug/L 99 51 -143 4 30
Methyl tert-butyl ether 50.0 56.7 ug/L 113 76 -126 8 30
Naphthalene 50.0 58.7 ug/L 117 56 -136 10 30
n-Butylbenzene 50.0 45.2 ug/L 90 72 -128 5 30
N-Propylbenzene 50.0 53.8 ug/L 108 74 -130 6 30
sec-Butylbenzene 50.0 56.6 ug/L 113 71 -130 8 30
Styrene 50.0 57.6 ug/L 115 75 -129 12 30
tert-Butylbenzene 50.0 56.5 ug/L 113 72 -130 3 30
1,1,1,2-Tetrachloroethane 50.0 52.4 ug/L 105 68 -132 3 30
1,1,2,2-Tetrachloroethane 50.0 53.3 ug/L 107 71 -127 7 30
Tetrachloroethene 50.0 47.5 ug/L 95 77 -128 10 30
Toluene 50.0 40.3 ug/L 81 77 -125 23 30
trans-1,2-Dichloroethene 50.0 49.5 ug/L 99 78 -130 10 30
trans-1,3-Dichloropropene 50.0 45.5 ug/L 91 72 -127 4 50
1,2,3-Trichlorobenzene 50.0 58.8 ug/L 118 63 -136 8 30
1,2,4-Trichlorobenzene 50.0 55.5 ug/L 111 67 -134 4 30
1,1,1-Trichloroethane 50.0 38.8 ug/L 78 76 -126 15 30
1,1,2-Trichloroethane 50.0 49.4 ug/L 99 69 -127 7 30
Trichloroethene 50.0 46.9 ug/L 94 80 -120 4 30
Trichlorofluoromethane 50.0 49.1 ug/L 98 66 -144 7 30
1,2,3-Trichloropropane 50.0 52.8 ug/L 106 74 -126 6 30
1,2,4-Trimethylbenzene 50.0 58.4 ug/L 117 72 -129 7 50
1,3,5-Trimethylbenzene 50.0 57.4 ug/L 115 72 -130 8 50
Vinyl chloride 50.0 56.8 ug/L 114 58 -141 8 30
Toluene-d8 (Surr)70 -130
Surrogate
104
LCSD LCSD
Qualifier Limits%Recovery
771,2-Dichloroethane-d4 (Surr)70 -130
77Dibromofluoromethane (Surr)70 -130
894-Bromofluorobenzene (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 680-359409/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359409
RL MDL
Nitrate as N 0.023 U 0.050 0.023 mg/L 11/18/14 17:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-359409/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359409
Nitrate as N 0.999 0.995 mg/L 100 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-359409/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359409
Nitrate as N 0.999 0.994 mg/L 99 90 -110 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: LMW-10-11-14Lab Sample ID: 680-107343-12 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359409
Nitrate as N 0.39 0.999 1.52 mg/L 113 80 -120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: LMW-10-11-14Lab Sample ID: 680-107343-12 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359409
Nitrate as N 0.39 0.999 1.47 mg/L 109 80 -120 3 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: LMW-4R-11-14Lab Sample ID: 680-107343-13 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359409
Nitrate as N 0.057 0.0566 mg/L 0.7 30
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 6020A - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-359308/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359518 Prep Batch: 359308
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/18/14 14:08 11/19/14 00:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.40 U 0.401.0 ug/L 11/18/14 14:08 11/19/14 00:09 1Arsenic
0.15 U 0.151.0 ug/L 11/18/14 14:08 11/19/14 00:09 1Barium
0.070 U 0.0700.20 ug/L 11/18/14 14:08 11/19/14 00:09 1Beryllium
0.20 U 0.200.50 ug/L 11/18/14 14:08 11/19/14 00:09 1Cadmium
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-359308/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359518 Prep Batch: 359308
RL MDL
Chromium 0.222 J 1.0 0.16 ug/L 11/18/14 14:08 11/19/14 00:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.078 U 0.0780.20 ug/L 11/18/14 14:08 11/19/14 00:09 1Cobalt
0.21 U 0.211.0 ug/L 11/18/14 14:08 11/19/14 00:09 1Copper
0.080 U 0.0800.30 ug/L 11/18/14 14:08 11/19/14 00:09 1Lead
0.40 U 0.401.0 ug/L 11/18/14 14:08 11/19/14 00:09 1Nickel
0.21 U 0.210.50 ug/L 11/18/14 14:08 11/19/14 00:09 1Selenium
0.10 U 0.100.20 ug/L 11/18/14 14:08 11/19/14 00:09 1Silver
0.10 U 0.100.20 ug/L 11/18/14 14:08 11/19/14 00:09 1Thallium
1.4 U 1.45.0 ug/L 11/18/14 14:08 11/19/14 00:09 1Vanadium
2.6 U 2.610 ug/L 11/18/14 14:08 11/19/14 00:09 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-359308/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359518 Prep Batch: 359308
Antimony 20.0 20.0 ug/L 100 75 -125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 40.0 42.0 ug/L 105 75 -125
Barium 40.0 40.2 ug/L 100 75 -125
Beryllium 20.0 19.8 ug/L 99 75 -125
Cadmium 20.0 20.0 ug/L 100 75 -125
Chromium 40.0 41.5 ug/L 104 75 -125
Cobalt 20.0 20.4 ug/L 102 75 -125
Copper 40.0 42.9 ug/L 107 75 -125
Lead 200 197 ug/L 99 75 -125
Nickel 40.0 41.6 ug/L 104 75 -125
Selenium 40.0 40.1 ug/L 100 75 -125
Silver 20.0 20.3 ug/L 101 75 -125
Thallium 16.0 15.9 ug/L 99 75 -125
Vanadium 40.0 41.1 ug/L 103 75 -125
Zinc 40.0 42.7 ug/L 107 75 -125
Client Sample ID: LMW-9D-11-14Lab Sample ID: 680-107343-8 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359518 Prep Batch: 359308
Antimony 0.99 U 20.0 20.1 ug/L 101 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 1.9 40.0 42.8 ug/L 102 75 -125
Barium 3.2 40.0 43.0 ug/L 100 75 -125
Beryllium 0.070 U 20.0 19.7 ug/L 99 75 -125
Cadmium 0.20 U 20.0 20.0 ug/L 100 75 -125
Chromium 0.80 J 40.0 40.1 ug/L 98 75 -125
Cobalt 0.078 U 20.0 19.5 ug/L 97 75 -125
Copper 1.1 40.0 40.7 ug/L 99 75 -125
Lead 0.61 200 195 ug/L 97 75 -125
Nickel 1.0 40.0 40.4 ug/L 98 75 -125
Selenium 0.35 J 40.0 39.2 ug/L 97 75 -125
Silver 0.10 U 20.0 20.4 ug/L 102 75 -125
TestAmerica Savannah
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QC Sample Results
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: LMW-9D-11-14Lab Sample ID: 680-107343-8 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359518 Prep Batch: 359308
Thallium 0.10 U 16.0 15.3 ug/L 96 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Vanadium 3.1 J 40.0 41.7 ug/L 96 75 -125
Zinc 4.0 J 40.0 43.0 ug/L 97 75 -125
Client Sample ID: LMW-9D-11-14Lab Sample ID: 680-107343-8 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 359518 Prep Batch: 359308
Antimony 0.99 U 20.0 19.6 ug/L 98 75 -125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 1.9 40.0 42.0 ug/L 100 75 -125 2 20
Barium 3.2 40.0 42.1 ug/L 97 75 -125 2 20
Beryllium 0.070 U 20.0 18.7 ug/L 93 75 -125 5 20
Cadmium 0.20 U 20.0 19.5 ug/L 98 75 -125 2 20
Chromium 0.80 J 40.0 39.5 ug/L 97 75 -125 2 20
Cobalt 0.078 U 20.0 19.1 ug/L 96 75 -125 2 20
Copper 1.1 40.0 40.0 ug/L 97 75 -125 2 20
Lead 0.61 200 190 ug/L 95 75 -125 3 20
Nickel 1.0 40.0 39.7 ug/L 97 75 -125 2 20
Selenium 0.35 J 40.0 37.4 ug/L 93 75 -125 5 20
Silver 0.10 U 20.0 19.8 ug/L 99 75 -125 3 20
Thallium 0.10 U 16.0 14.8 ug/L 93 75 -125 3 20
Vanadium 3.1 J 40.0 41.1 ug/L 95 75 -125 1 20
Zinc 4.0 J 40.0 42.6 ug/L 96 75 -125 1 20
TestAmerica Savannah
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QC Association Summary
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
GC/MS VOA
Analysis Batch: 360309
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B680-107343-2 Trip Blank Total/NA
Water 8260B680-107343-3 LMW-9S-11-14 Total/NA
Water 8260B680-107343-4 LMW-9-11-14 Total/NA
Water 8260BLCS 680-360309/4 Lab Control Sample Total/NA
Water 8260BLCSD 680-360309/11 Lab Control Sample Dup Total/NA
Water 8260BMB 680-360309/9 Method Blank Total/NA
Analysis Batch: 360546
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B680-107343-1 LMW-9D-11-14 Total/NA
Water 8260B680-107343-5 LMW-16-11-14 Total/NA
Water 8260B680-107343-6 LMW-10-11-14 Total/NA
Water 8260B680-107343-7 LMW-4R-11-14 Total/NA
Water 8260BLCS 680-360546/6 Lab Control Sample Total/NA
Water 8260BLCSD 680-360546/7 Lab Control Sample Dup Total/NA
Water 8260BMB 680-360546/11 Method Blank Total/NA
HPLC/IC
Analysis Batch: 359409
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0680-107343-8 LMW-9D-11-14 Total/NA
Water 300.0680-107343-9 LMW-9S-11-14 Total/NA
Water 300.0680-107343-10 LMW-9-11-14 Total/NA
Water 300.0680-107343-11 LMW-16-11-14 Total/NA
Water 300.0680-107343-12 LMW-10-11-14 Total/NA
Water 300.0680-107343-12 MS LMW-10-11-14 Total/NA
Water 300.0680-107343-12 MSD LMW-10-11-14 Total/NA
Water 300.0680-107343-13 LMW-4R-11-14 Total/NA
Water 300.0680-107343-13 DU LMW-4R-11-14 Total/NA
Water 300.0LCS 680-359409/6 Lab Control Sample Total/NA
Water 300.0LCSD 680-359409/7 Lab Control Sample Dup Total/NA
Water 300.0MB 680-359409/5 Method Blank Total/NA
Metals
Prep Batch: 359308
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3030C680-107343-8 LMW-9D-11-14 Total/NA
Water 3030C680-107343-8 MS LMW-9D-11-14 Total/NA
Water 3030C680-107343-8 MSD LMW-9D-11-14 Total/NA
Water 3030C680-107343-9 LMW-9S-11-14 Total/NA
Water 3030C680-107343-10 LMW-9-11-14 Total/NA
Water 3030C680-107343-11 LMW-16-11-14 Total/NA
Water 3030C680-107343-12 LMW-10-11-14 Total/NA
Water 3030C680-107343-13 LMW-4R-11-14 Total/NA
Water 3030CLCS 680-359308/2-A Lab Control Sample Total/NA
Water 3030CMB 680-359308/1-A Method Blank Total/NA
TestAmerica Savannah
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QC Association Summary
TestAmerica Job ID: 680-107343-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Metals (Continued)
Analysis Batch: 359518
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 359308680-107343-8 LMW-9D-11-14 Total/NA
Water 6020A 359308680-107343-8 MS LMW-9D-11-14 Total/NA
Water 6020A 359308680-107343-8 MSD LMW-9D-11-14 Total/NA
Water 6020A 359308680-107343-9 LMW-9S-11-14 Total/NA
Water 6020A 359308680-107343-10 LMW-9-11-14 Total/NA
Water 6020A 359308680-107343-11 LMW-16-11-14 Total/NA
Water 6020A 359308680-107343-12 LMW-10-11-14 Total/NA
Water 6020A 359308680-107343-13 LMW-4R-11-14 Total/NA
Water 6020A 359308LCS 680-359308/2-A Lab Control Sample Total/NA
Water 6020A 359308MB 680-359308/1-A Method Blank Total/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-107343-1
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-9D-11-14 Lab Sample ID: 680-107343-1
Matrix: WaterDate Collected: 11/16/14 10:21
Date Received: 11/18/14 10:05
Analysis 8260B 11/26/14 13:00 MMT1360546 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: Trip Blank Lab Sample ID: 680-107343-2
Matrix: WaterDate Collected: 11/16/14 08:30
Date Received: 11/18/14 10:05
Analysis 8260B 11/25/14 15:56 RWB1360309 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-9S-11-14 Lab Sample ID: 680-107343-3
Matrix: WaterDate Collected: 11/16/14 11:14
Date Received: 11/18/14 10:05
Analysis 8260B 11/25/14 20:43 RWB1360309 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-9-11-14 Lab Sample ID: 680-107343-4
Matrix: WaterDate Collected: 11/16/14 12:20
Date Received: 11/18/14 10:05
Analysis 8260B 11/25/14 21:05 RWB1360309 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-16-11-14 Lab Sample ID: 680-107343-5
Matrix: WaterDate Collected: 11/16/14 14:17
Date Received: 11/18/14 10:05
Analysis 8260B 11/26/14 13:21 MMT1360546 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-10-11-14 Lab Sample ID: 680-107343-6
Matrix: WaterDate Collected: 11/17/14 09:50
Date Received: 11/18/14 10:05
Analysis 8260B 11/26/14 13:42 MMT1360546 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-107343-1
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-4R-11-14 Lab Sample ID: 680-107343-7
Matrix: WaterDate Collected: 11/17/14 11:12
Date Received: 11/18/14 10:05
Analysis 8260B 11/26/14 14:03 MMT1360546 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-9D-11-14 Lab Sample ID: 680-107343-8
Matrix: WaterDate Collected: 11/17/14 07:30
Date Received: 11/18/14 10:05
Analysis 300.0 11/18/14 18:41 CMB1359409 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 359308 11/18/14 14:08 SP TAL SAVTotal/NA
Analysis 6020A 1 359518 11/19/14 00:19 BWR TAL SAVTotal/NA
Client Sample ID: LMW-9S-11-14 Lab Sample ID: 680-107343-9
Matrix: WaterDate Collected: 11/17/14 07:45
Date Received: 11/18/14 10:05
Analysis 300.0 11/18/14 18:56 CMB2359409 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 359308 11/18/14 14:08 SP TAL SAVTotal/NA
Analysis 6020A 1 359518 11/19/14 00:46 BWR TAL SAVTotal/NA
Client Sample ID: LMW-9-11-14 Lab Sample ID: 680-107343-10
Matrix: WaterDate Collected: 11/17/14 07:55
Date Received: 11/18/14 10:05
Analysis 300.0 11/18/14 19:12 CMB1359409 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 359308 11/18/14 14:08 SP TAL SAVTotal/NA
Analysis 6020A 1 359518 11/19/14 00:51 BWR TAL SAVTotal/NA
Client Sample ID: LMW-16-11-14 Lab Sample ID: 680-107343-11
Matrix: WaterDate Collected: 11/17/14 08:10
Date Received: 11/18/14 10:05
Analysis 300.0 11/18/14 19:27 CMB1359409 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 359308 11/18/14 14:08 SP TAL SAVTotal/NA
Analysis 6020A 1 359518 11/19/14 00:56 BWR TAL SAVTotal/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-107343-1
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-10-11-14 Lab Sample ID: 680-107343-12
Matrix: WaterDate Collected: 11/17/14 09:50
Date Received: 11/18/14 10:05
Analysis 300.0 11/18/14 19:43 CMB1359409 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 359308 11/18/14 14:08 SP TAL SAVTotal/NA
Analysis 6020A 1 359518 11/19/14 01:12 BWR TAL SAVTotal/NA
Client Sample ID: LMW-4R-11-14 Lab Sample ID: 680-107343-13
Matrix: WaterDate Collected: 11/17/14 11:12
Date Received: 11/18/14 10:05
Analysis 300.0 11/18/14 21:00 CMB1359409 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 359308 11/18/14 14:08 SP TAL SAVTotal/NA
Analysis 6020A 1 359518 11/19/14 01:18 BWR TAL SAVTotal/NA
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Login Sample Receipt Checklist
Client: U.S. Army Corps of Engineers Job Number: 680-107343-1
Login Number: 107343
Question Answer Comment
Creator: White, Menica R
List Source: TestAmerica Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Savannah
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Certification Summary
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-107343-1
Project/Site: Ft.Bragg - Lamont Landfill
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
A2LA 399.01DoD ELAP 02-28-15
North Carolina (DW)State Program 4 13701 07-31-15
TestAmerica Savannah
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-107398-1
Client Project/Site: Ft.Bragg - Lamont Landfill
For:
U.S. Army Corps of Engineers
100 West Oglethorpe Ave
Savannah, Georgia 31401
Attn: Mr. Kevin Haborak
Authorized for release by:
12/3/2014 12:27:38 PM
Linda Wolfe, Project Manager II
[phone] e.3005
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
TestAmerica Job ID: 680-107398-1
Page 2 of 50 TestAmerica Savannah12/3/2014
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .45
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .49
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-107398-1
Project/Site: Ft.Bragg - Lamont Landfill
Job ID: 680-107398-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: U.S. Army Corps of Engineers
Project: Ft.Bragg - Lamont Landfill
Report Number: 680-107398-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 11/19/2014; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.9 C.
Except:
The container label for the following sample did not match the information listed on the Chain-of-Custody: LMW-6-11-14 (680-107398-2).
Per the client the ID on the label is correct as LMW-6-11-14, COC ID was incorrect.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples Trip Blank (680-107398-1), LMW-6-11-14 (680-107398-2), Dup-1-11-14 (680-107398-3), LMW-3S-11-14 (680-107398-4),
LMW-3-11-14 (680-107398-5) and BLK-1-11-14 (680-107398-6) were analyzed for Volatile Organic Compounds (GC-MS) in accordance
with EPA SW-846 Method 8260B. The samples were analyzed on 11/26/2014 and 11/27/2014.
The reference method requires a continuing calibration verification (CCV) to be analyzed every 12 hours. The following laboratory control
spike duplicate (LCSD) associated with batch 360702 was analyzed one minute outside this method-defined frequency: (LCSD
680-360702/33).
1,2,3-Trichlorobenzene and Hexachlorobutadiene were detected in method blank MB 680-360702/10 at levels that were above the method
detection limit but below the reporting limit. The values should be considered estimates, and have been flagged. If the associated
sample reported a result above the MDL and/or RL, the result has been flagged. Refer to the QC report for details.
The laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for batch 680-360579 recovered outside control
limits for the following analyte: 1,2-dichloroethane. This analyte was biased high in the LCS and was not detected in the associated
samples; therefore, the data has been reported.
The laboratory control sample (LCS) for batch 360702 recovered outside control limits for the following analyte: 1,2,3-trichlorobenzene.
This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data has been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
METALS (ICPMS)
Samples LMW-6-11-14 (680-107398-2), Dup-1-11-14 (680-107398-3), LMW-3S-11-14 (680-107398-4), LMW-3-11-14 (680-107398-5) and
BLK-1-11-14 (680-107398-6) were analyzed for Metals (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were
prepared on 11/19/2014 and analyzed on 11/21/2014.
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-107398-1
Project/Site: Ft.Bragg - Lamont Landfill
Job ID: 680-107398-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
Chromium was detected in method blank MB 680-359553/1-A at a level that was above the method detection limit but below the reporting
limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the MDL
and/or RL, the result has been flagged. Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ANIONS BY ION CHROMATOGRAPHY (48 HOUR)
Samples LMW-6-11-14 (680-107398-2), Dup-1-11-14 (680-107398-3), LMW-3S-11-14 (680-107398-4), LMW-3-11-14 (680-107398-5) and
BLK-1-11-14 (680-107398-6) were analyzed for Anions by Ion Chromatography (48 Hour) in accordance with EPA Method 300.0. The
samples were analyzed on 11/19/2014 and 11/27/2014.
The following samples required a dilution, that were analyzed out of hold in analytical batch 360731: Dup-1-11-14 (680-107398-3),
LMW-6-11-14 (680-107398-2). Both sets of data are reported.
Samples LMW-6-11-14 (680-107398-2)[2X], Dup-1-11-14 (680-107398-3)[2X] and LMW-3S-11-14 (680-107398-4)[2X] required dilution
prior to analysis. The reporting limits have been adjusted accordingly.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Sample Summary
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-107398-1 Trip Blank Water 11/18/14 08:30 11/19/14 09:56
680-107398-2 LMW-6-11-14 Water 11/18/14 10:01 11/19/14 09:56
680-107398-3 Dup-1-11-14 Water 11/18/14 08:00 11/19/14 09:56
680-107398-4 LMW-3S-11-14 Water 11/18/14 11:30 11/19/14 09:56
680-107398-5 LMW-3-11-14 Water 11/18/14 12:34 11/19/14 09:56
680-107398-6 BLK-1-11-14 Water 11/18/14 14:00 11/19/14 09:56
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Method Summary
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL SAV
MCAWW300.0 Anions, Ion Chromatography TAL SAV
SW8466020AMetals (ICP/MS)TAL SAV
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
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Definitions/Glossary
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Qualifiers
GC/MS VOA
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
Q One or more quality control criteria failed.
HPLC/IC
Qualifier Description
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
Qualifier
H Sample was prepped or analyzed beyond the specified holding time
U Undetected at the Limit of Detection.
Metals
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Detection Summary
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: Trip Blank Lab Sample ID: 680-107398-1
No Detections.
Client Sample ID: LMW-6-11-14 Lab Sample ID: 680-107398-2
Trichlorofluoromethane
RL
1.0 ug/L
MDL
0.25
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.38 8260B
Nitrate as N 0.050 mg/L0.023 Total/NA12.2 J 300.0
Nitrate as N 0.10 mg/L0.046 Total/NA21.9 H 300.0
Barium 1.0 ug/L0.15 Total/NA1286020A
Chromium 1.0 ug/L0.16 Total/NA10.36 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.33 6020A
Copper 1.0 ug/L0.21 Total/NA10.65 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.97 J 6020A
Selenium 0.50 ug/L0.21 Total/NA11.1 6020A
Zinc 10 ug/L2.6 Total/NA13.7 J 6020A
Client Sample ID: Dup-1-11-14 Lab Sample ID: 680-107398-3
Dichlorodifluoromethane
RL
1.0 ug/L
MDL
0.25
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.49 8260B
Trichlorofluoromethane 1.0 ug/L0.25 Total/NA10.37 J 8260B
Nitrate as N 0.050 mg/L0.023 Total/NA12.2 J 300.0
Nitrate as N 0.10 mg/L0.046 Total/NA21.9 H 300.0
Barium 1.0 ug/L0.15 Total/NA1286020A
Chromium 1.0 ug/L0.16 Total/NA10.39 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.32 6020A
Copper 1.0 ug/L0.21 Total/NA10.73 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.80 J 6020A
Selenium 0.50 ug/L0.21 Total/NA11.3 6020A
Vanadium 5.0 ug/L1.4 Total/NA11.4 J 6020A
Zinc 10 ug/L2.6 Total/NA14.4 J 6020A
Client Sample ID: LMW-3S-11-14 Lab Sample ID: 680-107398-4
Dichlorodifluoromethane
RL
1.0 ug/L
MDL
0.25
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA12.3 8260B
Trichlorofluoromethane 1.0 ug/L0.25 Total/NA10.83 J 8260B
Nitrate as N 0.10 mg/L0.046 Total/NA20.11 300.0
Arsenic 1.0 ug/L0.40 Total/NA10.94 J 6020A
Barium 1.0 ug/L0.15 Total/NA18.0 6020A
Chromium 1.0 ug/L0.16 Total/NA10.74 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.56 6020A
Copper 1.0 ug/L0.21 Total/NA11.6 6020A
Lead 0.30 ug/L0.080 Total/NA10.25 J 6020A
Nickel 1.0 ug/L0.40 Total/NA11.5 6020A
Vanadium 5.0 ug/L1.4 Total/NA11.5 J 6020A
Zinc 10 ug/L2.6 Total/NA15.3 J 6020A
Client Sample ID: LMW-3-11-14 Lab Sample ID: 680-107398-5
Chloroform
RL
1.0 ug/L
MDL
0.14
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.25 8260B
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-3-11-14 (Continued)Lab Sample ID: 680-107398-5
Trichlorofluoromethane
RL
1.0 ug/L
MDL
0.25
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.33 8260B
Nitrate as N 0.050 mg/L0.023 Total/NA10.19 300.0
Barium 1.0 ug/L0.15 Total/NA15.5 6020A
Chromium 1.0 ug/L0.16 Total/NA10.70 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.21 6020A
Copper 1.0 ug/L0.21 Total/NA11.6 6020A
Lead 0.30 ug/L0.080 Total/NA10.12 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.90 J 6020A
Vanadium 5.0 ug/L1.4 Total/NA11.9 J 6020A
Zinc 10 ug/L2.6 Total/NA16.0 J 6020A
Client Sample ID: BLK-1-11-14 Lab Sample ID: 680-107398-6
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.47 6020A
Copper 1.0 ug/L0.21 Total/NA10.27 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.63 J 6020A
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-1Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 11/18/14 08:30
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 23:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/26/14 23:14 1Benzene0.25 U
1.0 0.16 ug/L 11/26/14 23:14 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/26/14 23:14 1Bromoform0.50 U
5.0 2.0 ug/L 11/26/14 23:14 1Bromomethane2.0 U
10 1.0 ug/L 11/26/14 23:14 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/26/14 23:14 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/26/14 23:14 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/26/14 23:14 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/26/14 23:14 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/26/14 23:14 1Chloroethane2.0 U
1.0 0.14 ug/L 11/26/14 23:14 1Chloroform0.14 U
5.0 0.27 ug/L 11/26/14 23:14 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/26/14 23:14 1Chloromethane0.33 U
1.0 0.17 ug/L 11/26/14 23:14 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/26/14 23:14 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/26/14 23:14 1cis-1,2-Dichloroethene 0.15 U
1.0 0.11 ug/L 11/26/14 23:14 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/26/14 23:14 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/26/14 23:14 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/26/14 23:14 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/26/14 23:14 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/26/14 23:14 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/26/14 23:14 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 11/26/14 23:14 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 11/26/14 23:14 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/26/14 23:14 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/26/14 23:14 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/26/14 23:14 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/26/14 23:14 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/26/14 23:14 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/26/14 23:14 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/26/14 23:14 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/26/14 23:14 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/26/14 23:14 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/26/14 23:14 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/26/14 23:14 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/26/14 23:14 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/26/14 23:14 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/26/14 23:14 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/26/14 23:14 1Naphthalene1.0 U
1.0 0.10 ug/L 11/26/14 23:14 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/26/14 23:14 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/26/14 23:14 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/26/14 23:14 1Styrene0.11 U
1.0 0.12 ug/L 11/26/14 23:14 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/26/14 23:14 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/26/14 23:14 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/26/14 23:14 1Tetrachloroethene0.15 U
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-1Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 11/18/14 08:30
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene 0.33 U 1.0 0.33 ug/L 11/26/14 23:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.20 ug/L 11/26/14 23:14 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/26/14 23:14 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/26/14 23:14 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/26/14 23:14 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/26/14 23:14 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/26/14 23:14 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/26/14 23:14 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/26/14 23:14 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 11/26/14 23:14 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/26/14 23:14 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/26/14 23:14 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/26/14 23:14 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)98 70-130 11/26/14 23:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)81 11/26/14 23:14 170-130
Dibromofluoromethane (Surr)90 11/26/14 23:14 170-130
4-Bromofluorobenzene (Surr)92 11/26/14 23:14 170-130
Lab Sample ID: 680-107398-2Client Sample ID: LMW-6-11-14
Matrix: WaterDate Collected: 11/18/14 10:01
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/27/14 04:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/27/14 04:10 1Benzene0.25 U
1.0 0.16 ug/L 11/27/14 04:10 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/27/14 04:10 1Bromoform0.50 U
5.0 2.0 ug/L 11/27/14 04:10 1Bromomethane2.0 U
10 1.0 ug/L 11/27/14 04:10 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/27/14 04:10 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/27/14 04:10 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/27/14 04:10 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/27/14 04:10 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/27/14 04:10 1Chloroethane2.0 U
1.0 0.14 ug/L 11/27/14 04:10 1Chloroform0.14 U
5.0 0.27 ug/L 11/27/14 04:10 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/27/14 04:10 1Chloromethane0.33 U
1.0 0.17 ug/L 11/27/14 04:10 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/27/14 04:10 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/27/14 04:10 1cis-1,2-Dichloroethene 0.15 U
1.0 0.11 ug/L 11/27/14 04:10 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/27/14 04:10 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/27/14 04:10 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/27/14 04:10 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/27/14 04:10 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/27/14 04:10 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/27/14 04:10 1Dichlorodifluoromethane0.25 U
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-2Client Sample ID: LMW-6-11-14
Matrix: WaterDate Collected: 11/18/14 10:01
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloroethane 0.25 U 1.0 0.25 ug/L 11/27/14 04:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.10 ug/L 11/27/14 04:10 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/27/14 04:10 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/27/14 04:10 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/27/14 04:10 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/27/14 04:10 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/27/14 04:10 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/27/14 04:10 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/27/14 04:10 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/27/14 04:10 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/27/14 04:10 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/27/14 04:10 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/27/14 04:10 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/27/14 04:10 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/27/14 04:10 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/27/14 04:10 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/27/14 04:10 1Naphthalene1.0 U
1.0 0.10 ug/L 11/27/14 04:10 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/27/14 04:10 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/27/14 04:10 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/27/14 04:10 1Styrene0.11 U
1.0 0.12 ug/L 11/27/14 04:10 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/27/14 04:10 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/27/14 04:10 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/27/14 04:10 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 11/27/14 04:10 1Toluene0.33 U
1.0 0.20 ug/L 11/27/14 04:10 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/27/14 04:10 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/27/14 04:10 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/27/14 04:10 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/27/14 04:10 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/27/14 04:10 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/27/14 04:10 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/27/14 04:10 1Trichlorofluoromethane0.38 J
1.0 0.41 ug/L 11/27/14 04:10 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/27/14 04:10 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/27/14 04:10 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/27/14 04:10 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)96 70-130 11/27/14 04:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)85 11/27/14 04:10 170-130
Dibromofluoromethane (Surr)91 11/27/14 04:10 170-130
4-Bromofluorobenzene (Surr)92 11/27/14 04:10 170-130
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 2.2 J 0.050 0.023 mg/L 11/19/14 21:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.10 0.046 mg/L 11/27/14 12:33 2Nitrate as N 1.9 H
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-2Client Sample ID: LMW-6-11-14
Matrix: WaterDate Collected: 11/18/14 10:01
Date Received: 11/19/14 09:56
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/19/14 15:24 11/21/14 10:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 10:10 1Arsenic0.40 U
1.0 0.15 ug/L 11/19/14 15:24 11/21/14 10:10 1Barium28
0.20 0.070 ug/L 11/19/14 15:24 11/21/14 10:10 1Beryllium0.070 U
0.50 0.20 ug/L 11/19/14 15:24 11/21/14 10:10 1Cadmium0.20 U
1.0 0.16 ug/L 11/19/14 15:24 11/21/14 10:10 1Chromium0.36 J
0.20 0.078 ug/L 11/19/14 15:24 11/21/14 10:10 1Cobalt0.33
1.0 0.21 ug/L 11/19/14 15:24 11/21/14 10:10 1Copper0.65 J
0.30 0.080 ug/L 11/19/14 15:24 11/21/14 10:10 1Lead0.080 U
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 10:10 1Nickel0.97 J
0.50 0.21 ug/L 11/19/14 15:24 11/21/14 10:10 1Selenium1.1
0.20 0.10 ug/L 11/19/14 15:24 11/21/14 10:10 1Silver0.10 U
0.20 0.10 ug/L 11/19/14 15:24 11/21/14 10:10 1Thallium0.10 U
5.0 1.4 ug/L 11/19/14 15:24 11/21/14 10:10 1Vanadium1.4 U
10 2.6 ug/L 11/19/14 15:24 11/21/14 10:10 1Zinc3.7 J
Lab Sample ID: 680-107398-3Client Sample ID: Dup-1-11-14
Matrix: WaterDate Collected: 11/18/14 08:00
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/27/14 03:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/27/14 03:28 1Benzene0.25 U
1.0 0.16 ug/L 11/27/14 03:28 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/27/14 03:28 1Bromoform0.50 U
5.0 2.0 ug/L 11/27/14 03:28 1Bromomethane2.0 U
10 1.0 ug/L 11/27/14 03:28 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/27/14 03:28 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/27/14 03:28 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/27/14 03:28 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/27/14 03:28 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/27/14 03:28 1Chloroethane2.0 U
1.0 0.14 ug/L 11/27/14 03:28 1Chloroform0.14 U
5.0 0.27 ug/L 11/27/14 03:28 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/27/14 03:28 1Chloromethane0.33 U
1.0 0.17 ug/L 11/27/14 03:28 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/27/14 03:28 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/27/14 03:28 1cis-1,2-Dichloroethene 0.15 U
1.0 0.11 ug/L 11/27/14 03:28 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/27/14 03:28 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/27/14 03:28 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/27/14 03:28 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/27/14 03:28 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/27/14 03:28 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/27/14 03:28 1Dichlorodifluoromethane0.49 J
1.0 0.25 ug/L 11/27/14 03:28 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 11/27/14 03:28 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/27/14 03:28 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/27/14 03:28 11,2-Dichloropropane 0.13 U
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-3Client Sample ID: Dup-1-11-14
Matrix: WaterDate Collected: 11/18/14 08:00
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,3-Dichloropropane 0.13 U 1.0 0.13 ug/L 11/27/14 03:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.12 ug/L 11/27/14 03:28 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/27/14 03:28 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/27/14 03:28 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/27/14 03:28 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/27/14 03:28 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/27/14 03:28 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/27/14 03:28 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/27/14 03:28 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/27/14 03:28 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/27/14 03:28 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/27/14 03:28 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/27/14 03:28 1Naphthalene1.0 U
1.0 0.10 ug/L 11/27/14 03:28 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/27/14 03:28 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/27/14 03:28 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/27/14 03:28 1Styrene0.11 U
1.0 0.12 ug/L 11/27/14 03:28 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/27/14 03:28 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/27/14 03:28 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/27/14 03:28 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 11/27/14 03:28 1Toluene0.33 U
1.0 0.20 ug/L 11/27/14 03:28 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/27/14 03:28 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/27/14 03:28 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/27/14 03:28 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/27/14 03:28 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/27/14 03:28 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/27/14 03:28 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/27/14 03:28 1Trichlorofluoromethane0.37 J
1.0 0.41 ug/L 11/27/14 03:28 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/27/14 03:28 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/27/14 03:28 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/27/14 03:28 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)97 70-130 11/27/14 03:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)85 11/27/14 03:28 170-130
Dibromofluoromethane (Surr)92 11/27/14 03:28 170-130
4-Bromofluorobenzene (Surr)93 11/27/14 03:28 170-130
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 2.2 J 0.050 0.023 mg/L 11/19/14 21:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.10 0.046 mg/L 11/27/14 12:48 2Nitrate as N 1.9 H
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/19/14 15:24 11/21/14 10:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 10:15 1Arsenic0.40 U
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-3Client Sample ID: Dup-1-11-14
Matrix: WaterDate Collected: 11/18/14 08:00
Date Received: 11/19/14 09:56
Method: 6020A - Metals (ICP/MS) (Continued)
RL MDL
Barium 28 1.0 0.15 ug/L 11/19/14 15:24 11/21/14 10:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.20 0.070 ug/L 11/19/14 15:24 11/21/14 10:15 1Beryllium0.070 U
0.50 0.20 ug/L 11/19/14 15:24 11/21/14 10:15 1Cadmium0.20 U
1.0 0.16 ug/L 11/19/14 15:24 11/21/14 10:15 1Chromium0.39 J
0.20 0.078 ug/L 11/19/14 15:24 11/21/14 10:15 1Cobalt0.32
1.0 0.21 ug/L 11/19/14 15:24 11/21/14 10:15 1Copper0.73 J
0.30 0.080 ug/L 11/19/14 15:24 11/21/14 10:15 1Lead0.080 U
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 10:15 1Nickel0.80 J
0.50 0.21 ug/L 11/19/14 15:24 11/21/14 10:15 1Selenium1.3
0.20 0.10 ug/L 11/19/14 15:24 11/21/14 10:15 1Silver0.10 U
0.20 0.10 ug/L 11/19/14 15:24 11/21/14 10:15 1Thallium0.10 U
5.0 1.4 ug/L 11/19/14 15:24 11/21/14 10:15 1Vanadium1.4 J
10 2.6 ug/L 11/19/14 15:24 11/21/14 10:15 1Zinc4.4 J
Lab Sample ID: 680-107398-4Client Sample ID: LMW-3S-11-14
Matrix: WaterDate Collected: 11/18/14 11:30
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/27/14 03:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/27/14 03:49 1Benzene0.25 U
1.0 0.16 ug/L 11/27/14 03:49 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/27/14 03:49 1Bromoform0.50 U
5.0 2.0 ug/L 11/27/14 03:49 1Bromomethane2.0 U
10 1.0 ug/L 11/27/14 03:49 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/27/14 03:49 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/27/14 03:49 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/27/14 03:49 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/27/14 03:49 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/27/14 03:49 1Chloroethane2.0 U
1.0 0.14 ug/L 11/27/14 03:49 1Chloroform0.14 U
5.0 0.27 ug/L 11/27/14 03:49 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/27/14 03:49 1Chloromethane0.33 U
1.0 0.17 ug/L 11/27/14 03:49 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/27/14 03:49 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/27/14 03:49 1cis-1,2-Dichloroethene 0.15 U
1.0 0.11 ug/L 11/27/14 03:49 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/27/14 03:49 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/27/14 03:49 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/27/14 03:49 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/27/14 03:49 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/27/14 03:49 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/27/14 03:49 1Dichlorodifluoromethane2.3
1.0 0.25 ug/L 11/27/14 03:49 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 11/27/14 03:49 11,2-Dichloroethane 0.10 U
1.0 0.11 ug/L 11/27/14 03:49 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/27/14 03:49 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/27/14 03:49 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/27/14 03:49 12,2-Dichloropropane 0.12 U
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-4Client Sample ID: LMW-3S-11-14
Matrix: WaterDate Collected: 11/18/14 11:30
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloropropene 0.25 U 1.0 0.25 ug/L 11/27/14 03:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.11 ug/L 11/27/14 03:49 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/27/14 03:49 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/27/14 03:49 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/27/14 03:49 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/27/14 03:49 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/27/14 03:49 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/27/14 03:49 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/27/14 03:49 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/27/14 03:49 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/27/14 03:49 1Naphthalene1.0 U
1.0 0.10 ug/L 11/27/14 03:49 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/27/14 03:49 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/27/14 03:49 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/27/14 03:49 1Styrene0.11 U
1.0 0.12 ug/L 11/27/14 03:49 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/27/14 03:49 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/27/14 03:49 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/27/14 03:49 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 11/27/14 03:49 1Toluene0.33 U
1.0 0.20 ug/L 11/27/14 03:49 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/27/14 03:49 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/27/14 03:49 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/27/14 03:49 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/27/14 03:49 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/27/14 03:49 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/27/14 03:49 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/27/14 03:49 1Trichlorofluoromethane0.83 J
1.0 0.41 ug/L 11/27/14 03:49 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/27/14 03:49 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/27/14 03:49 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/27/14 03:49 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)98 70-130 11/27/14 03:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)83 11/27/14 03:49 170-130
Dibromofluoromethane (Surr)91 11/27/14 03:49 170-130
4-Bromofluorobenzene (Surr)91 11/27/14 03:49 170-130
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.11 0.10 0.046 mg/L 11/19/14 22:07 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/19/14 15:24 11/21/14 09:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 09:43 1Arsenic0.94 J
1.0 0.15 ug/L 11/19/14 15:24 11/21/14 09:43 1Barium8.0
0.20 0.070 ug/L 11/19/14 15:24 11/21/14 09:43 1Beryllium0.070 U
0.50 0.20 ug/L 11/19/14 15:24 11/21/14 09:43 1Cadmium0.20 U
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-4Client Sample ID: LMW-3S-11-14
Matrix: WaterDate Collected: 11/18/14 11:30
Date Received: 11/19/14 09:56
Method: 6020A - Metals (ICP/MS) (Continued)
RL MDL
Chromium 0.74 J 1.0 0.16 ug/L 11/19/14 15:24 11/21/14 09:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.20 0.078 ug/L 11/19/14 15:24 11/21/14 09:43 1Cobalt0.56
1.0 0.21 ug/L 11/19/14 15:24 11/21/14 09:43 1Copper1.6
0.30 0.080 ug/L 11/19/14 15:24 11/21/14 09:43 1Lead0.25 J
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 09:43 1Nickel1.5
0.50 0.21 ug/L 11/19/14 15:24 11/21/14 09:43 1Selenium0.21 U
0.20 0.10 ug/L 11/19/14 15:24 11/21/14 09:43 1Silver0.10 U J
0.20 0.10 ug/L 11/19/14 15:24 11/21/14 09:43 1Thallium0.10 U
5.0 1.4 ug/L 11/19/14 15:24 11/21/14 09:43 1Vanadium1.5 J
10 2.6 ug/L 11/19/14 15:24 11/21/14 09:43 1Zinc5.3 J
Lab Sample ID: 680-107398-5Client Sample ID: LMW-3-11-14
Matrix: WaterDate Collected: 11/18/14 12:34
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 16:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/26/14 16:28 1Benzene0.25 U
1.0 0.16 ug/L 11/26/14 16:28 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/26/14 16:28 1Bromoform0.50 U
5.0 2.0 ug/L 11/26/14 16:28 1Bromomethane2.0 U
10 1.0 ug/L 11/26/14 16:28 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/26/14 16:28 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/26/14 16:28 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/26/14 16:28 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/26/14 16:28 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/26/14 16:28 1Chloroethane2.0 U
1.0 0.14 ug/L 11/26/14 16:28 1Chloroform0.25 J
5.0 0.27 ug/L 11/26/14 16:28 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/26/14 16:28 1Chloromethane0.33 U
1.0 0.17 ug/L 11/26/14 16:28 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/26/14 16:28 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/26/14 16:28 1cis-1,2-Dichloroethene 0.15 U
1.0 0.11 ug/L 11/26/14 16:28 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/26/14 16:28 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/26/14 16:28 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/26/14 16:28 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/26/14 16:28 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/26/14 16:28 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/26/14 16:28 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 11/26/14 16:28 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 11/26/14 16:28 11,2-Dichloroethane 0.10 U Q
1.0 0.11 ug/L 11/26/14 16:28 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/26/14 16:28 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/26/14 16:28 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/26/14 16:28 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/26/14 16:28 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/26/14 16:28 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/26/14 16:28 1Ethylene Dibromide 0.25 U
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-5Client Sample ID: LMW-3-11-14
Matrix: WaterDate Collected: 11/18/14 12:34
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Hexachlorobutadiene 0.40 U 5.0 0.40 ug/L 11/26/14 16:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.10 ug/L 11/26/14 16:28 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/26/14 16:28 1Isopropyl ether 0.24 U
1.0 0.13 ug/L 11/26/14 16:28 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 11/26/14 16:28 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/26/14 16:28 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/26/14 16:28 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/26/14 16:28 1Naphthalene1.0 U
1.0 0.10 ug/L 11/26/14 16:28 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/26/14 16:28 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/26/14 16:28 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/26/14 16:28 1Styrene0.11 U
1.0 0.12 ug/L 11/26/14 16:28 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/26/14 16:28 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/26/14 16:28 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/26/14 16:28 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 11/26/14 16:28 1Toluene0.33 U
1.0 0.20 ug/L 11/26/14 16:28 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/26/14 16:28 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/26/14 16:28 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/26/14 16:28 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/26/14 16:28 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/26/14 16:28 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/26/14 16:28 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/26/14 16:28 1Trichlorofluoromethane0.33 J
1.0 0.41 ug/L 11/26/14 16:28 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/26/14 16:28 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/26/14 16:28 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/26/14 16:28 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)95 70-130 11/26/14 16:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)117 11/26/14 16:28 170-130
Dibromofluoromethane (Surr)103 11/26/14 16:28 170-130
4-Bromofluorobenzene (Surr)102 11/26/14 16:28 170-130
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.19 0.050 0.023 mg/L 11/19/14 22:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/19/14 15:24 11/21/14 10:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 10:20 1Arsenic0.40 U
1.0 0.15 ug/L 11/19/14 15:24 11/21/14 10:20 1Barium5.5
0.20 0.070 ug/L 11/19/14 15:24 11/21/14 10:20 1Beryllium0.070 U
0.50 0.20 ug/L 11/19/14 15:24 11/21/14 10:20 1Cadmium0.20 U
1.0 0.16 ug/L 11/19/14 15:24 11/21/14 10:20 1Chromium0.70 J
0.20 0.078 ug/L 11/19/14 15:24 11/21/14 10:20 1Cobalt0.21
1.0 0.21 ug/L 11/19/14 15:24 11/21/14 10:20 1Copper1.6
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-5Client Sample ID: LMW-3-11-14
Matrix: WaterDate Collected: 11/18/14 12:34
Date Received: 11/19/14 09:56
Method: 6020A - Metals (ICP/MS) (Continued)
RL MDL
Lead 0.12 J 0.30 0.080 ug/L 11/19/14 15:24 11/21/14 10:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 10:20 1Nickel0.90 J
0.50 0.21 ug/L 11/19/14 15:24 11/21/14 10:20 1Selenium0.21 U
0.20 0.10 ug/L 11/19/14 15:24 11/21/14 10:20 1Silver0.10 U
0.20 0.10 ug/L 11/19/14 15:24 11/21/14 10:20 1Thallium0.10 U
5.0 1.4 ug/L 11/19/14 15:24 11/21/14 10:20 1Vanadium1.9 J
10 2.6 ug/L 11/19/14 15:24 11/21/14 10:20 1Zinc6.0 J
Lab Sample ID: 680-107398-6Client Sample ID: BLK-1-11-14
Matrix: WaterDate Collected: 11/18/14 14:00
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 16:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 11/26/14 16:51 1Benzene0.25 U
1.0 0.16 ug/L 11/26/14 16:51 1Bromobenzene0.16 U
1.0 0.50 ug/L 11/26/14 16:51 1Bromoform0.50 U
5.0 2.0 ug/L 11/26/14 16:51 1Bromomethane2.0 U
10 1.0 ug/L 11/26/14 16:51 12-Butanone (MEK)1.0 U
1.0 0.50 ug/L 11/26/14 16:51 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 11/26/14 16:51 1Chlorobenzene0.25 U
1.0 0.14 ug/L 11/26/14 16:51 1Chlorobromomethane0.14 U
1.0 0.10 ug/L 11/26/14 16:51 1Chlorodibromomethane0.10 U
5.0 2.0 ug/L 11/26/14 16:51 1Chloroethane2.0 U
1.0 0.14 ug/L 11/26/14 16:51 1Chloroform0.14 U
5.0 0.27 ug/L 11/26/14 16:51 11-Chlorohexane 0.27 U
1.0 0.33 ug/L 11/26/14 16:51 1Chloromethane0.33 U
1.0 0.17 ug/L 11/26/14 16:51 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 11/26/14 16:51 14-Chlorotoluene 0.27 U
1.0 0.15 ug/L 11/26/14 16:51 1cis-1,2-Dichloroethene 0.15 U
1.0 0.11 ug/L 11/26/14 16:51 1cis-1,3-Dichloropropene 0.11 U
5.0 0.44 ug/L 11/26/14 16:51 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.21 ug/L 11/26/14 16:51 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 11/26/14 16:51 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 11/26/14 16:51 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 11/26/14 16:51 1Dichlorobromomethane0.25 U
1.0 0.25 ug/L 11/26/14 16:51 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 11/26/14 16:51 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 11/26/14 16:51 11,2-Dichloroethane 0.10 U Q
1.0 0.11 ug/L 11/26/14 16:51 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 11/26/14 16:51 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 11/26/14 16:51 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 11/26/14 16:51 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 11/26/14 16:51 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 11/26/14 16:51 1Ethylbenzene0.11 U
1.0 0.25 ug/L 11/26/14 16:51 1Ethylene Dibromide 0.25 U
5.0 0.40 ug/L 11/26/14 16:51 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 11/26/14 16:51 1Isopropylbenzene0.10 U
10 0.24 ug/L 11/26/14 16:51 1Isopropyl ether 0.24 U
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-6Client Sample ID: BLK-1-11-14
Matrix: WaterDate Collected: 11/18/14 14:00
Date Received: 11/19/14 09:56
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
4-Isopropyltoluene 0.13 U 1.0 0.13 ug/L 11/26/14 16:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.0 ug/L 11/26/14 16:51 1Methylene Chloride 1.0 U
10 1.0 ug/L 11/26/14 16:51 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 11/26/14 16:51 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 11/26/14 16:51 1Naphthalene1.0 U
1.0 0.10 ug/L 11/26/14 16:51 1n-Butylbenzene 0.10 U
1.0 0.15 ug/L 11/26/14 16:51 1N-Propylbenzene 0.15 U
1.0 0.16 ug/L 11/26/14 16:51 1sec-Butylbenzene 0.16 U
1.0 0.11 ug/L 11/26/14 16:51 1Styrene0.11 U
1.0 0.12 ug/L 11/26/14 16:51 1tert-Butylbenzene 0.12 U
1.0 0.33 ug/L 11/26/14 16:51 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 11/26/14 16:51 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 11/26/14 16:51 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 11/26/14 16:51 1Toluene0.33 U
1.0 0.20 ug/L 11/26/14 16:51 1trans-1,2-Dichloroethene 0.20 U
1.0 0.21 ug/L 11/26/14 16:51 1trans-1,3-Dichloropropene 0.21 U
5.0 0.35 ug/L 11/26/14 16:51 11,2,3-Trichlorobenzene 0.35 U
5.0 0.25 ug/L 11/26/14 16:51 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 11/26/14 16:51 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 11/26/14 16:51 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 11/26/14 16:51 1Trichloroethene0.13 U
1.0 0.25 ug/L 11/26/14 16:51 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 11/26/14 16:51 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 11/26/14 16:51 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 11/26/14 16:51 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 11/26/14 16:51 1Vinyl chloride 0.18 U
Toluene-d8 (Surr)94 70-130 11/26/14 16:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)116 11/26/14 16:51 170-130
Dibromofluoromethane (Surr)104 11/26/14 16:51 170-130
4-Bromofluorobenzene (Surr)102 11/26/14 16:51 170-130
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.023 U 0.050 0.023 mg/L 11/19/14 23:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 11/19/14 15:24 11/21/14 10:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 10:39 1Arsenic0.40 U
1.0 0.15 ug/L 11/19/14 15:24 11/21/14 10:39 1Barium0.47 J
0.20 0.070 ug/L 11/19/14 15:24 11/21/14 10:39 1Beryllium0.070 U
0.50 0.20 ug/L 11/19/14 15:24 11/21/14 10:39 1Cadmium0.20 U
1.0 0.16 ug/L 11/19/14 15:24 11/21/14 10:39 1Chromium0.16 U
0.20 0.078 ug/L 11/19/14 15:24 11/21/14 10:39 1Cobalt0.078 U
1.0 0.21 ug/L 11/19/14 15:24 11/21/14 10:39 1Copper0.27 J
0.30 0.080 ug/L 11/19/14 15:24 11/21/14 10:39 1Lead0.080 U
1.0 0.40 ug/L 11/19/14 15:24 11/21/14 10:39 1Nickel0.63 J
0.50 0.21 ug/L 11/19/14 15:24 11/21/14 10:39 1Selenium0.21 U
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Client Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-107398-6Client Sample ID: BLK-1-11-14
Matrix: WaterDate Collected: 11/18/14 14:00
Date Received: 11/19/14 09:56
Method: 6020A - Metals (ICP/MS) (Continued)
RL MDL
Silver 0.10 U 0.20 0.10 ug/L 11/19/14 15:24 11/21/14 10:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.20 0.10 ug/L 11/19/14 15:24 11/21/14 10:39 1Thallium0.10 U
5.0 1.4 ug/L 11/19/14 15:24 11/21/14 10:39 1Vanadium1.4 U
10 2.6 ug/L 11/19/14 15:24 11/21/14 10:39 1Zinc2.6 U
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Surrogate Summary
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-130)(70-130)(70-130)(70-130)
TOL 12DCE DBFM BFB
98 81 90 92680-107398-1
Percent Surrogate Recovery (Acceptance Limits)
Trip Blank
96 85 91 92680-107398-2 LMW-6-11-14
97 85 92 93680-107398-3 Dup-1-11-14
98 83 91 91680-107398-4 LMW-3S-11-14
96 98 97 97680-107398-4 MS LMW-3S-11-14
94 95 97 95680-107398-4 MSD LMW-3S-11-14
95 117 103 102680-107398-5 LMW-3-11-14
94 116 104 102680-107398-6 BLK-1-11-14
90 123 103 100LCS 680-360579/4 Lab Control Sample
94 96 97 81LCS 680-360702/5 Lab Control Sample
97 102 103 101LCS 680-360983/4 Lab Control Sample
88 121 106 101LCSD 680-360579/5 Lab Control Sample Dup
93 98 94 90LCSD 680-360702/33 Lab Control Sample Dup
93 100 100 97LCSD 680-360983/5 Lab Control Sample Dup
91 123 103 102MB 680-360579/9 Method Blank
99 80 90 93MB 680-360702/10 Method Blank
99 98 101 98MB 680-360983/10 Method Blank
Surrogate Legend
TOL = Toluene-d8 (Surr)
12DCE = 1,2-Dichloroethane-d4 (Surr)
DBFM = Dibromofluoromethane (Surr)
BFB = 4-Bromofluorobenzene (Surr)
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QC Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-360579/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360579
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 13:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.25 U 0.251.0 ug/L 11/26/14 13:00 1Benzene
0.16 U 0.161.0 ug/L 11/26/14 13:00 1Bromobenzene
0.50 U 0.501.0 ug/L 11/26/14 13:00 1Bromoform
2.0 U 2.05.0 ug/L 11/26/14 13:00 1Bromomethane
1.0 U 1.010 ug/L 11/26/14 13:00 12-Butanone (MEK)
0.50 U 0.501.0 ug/L 11/26/14 13:00 1Carbon tetrachloride
0.25 U 0.251.0 ug/L 11/26/14 13:00 1Chlorobenzene
0.14 U 0.141.0 ug/L 11/26/14 13:00 1Chlorobromomethane
0.10 U 0.101.0 ug/L 11/26/14 13:00 1Chlorodibromomethane
2.0 U 2.05.0 ug/L 11/26/14 13:00 1Chloroethane
0.14 U 0.141.0 ug/L 11/26/14 13:00 1Chloroform
0.27 U 0.275.0 ug/L 11/26/14 13:00 11-Chlorohexane
0.33 U 0.331.0 ug/L 11/26/14 13:00 1Chloromethane
0.17 U 0.171.0 ug/L 11/26/14 13:00 12-Chlorotoluene
0.27 U 0.271.0 ug/L 11/26/14 13:00 14-Chlorotoluene
0.15 U 0.151.0 ug/L 11/26/14 13:00 1cis-1,2-Dichloroethene
0.11 U 0.111.0 ug/L 11/26/14 13:00 1cis-1,3-Dichloropropene
0.44 U 0.445.0 ug/L 11/26/14 13:00 11,2-Dibromo-3-Chloropropane
0.21 U 0.211.0 ug/L 11/26/14 13:00 11,2-Dichlorobenzene
0.25 U 0.251.0 ug/L 11/26/14 13:00 11,3-Dichlorobenzene
0.28 U 0.281.0 ug/L 11/26/14 13:00 11,4-Dichlorobenzene
0.25 U 0.251.0 ug/L 11/26/14 13:00 1Dichlorobromomethane
0.25 U 0.251.0 ug/L 11/26/14 13:00 1Dichlorodifluoromethane
0.25 U 0.251.0 ug/L 11/26/14 13:00 11,1-Dichloroethane
0.10 U 0.101.0 ug/L 11/26/14 13:00 11,2-Dichloroethane
0.11 U 0.111.0 ug/L 11/26/14 13:00 11,1-Dichloroethene
0.13 U 0.131.0 ug/L 11/26/14 13:00 11,2-Dichloropropane
0.13 U 0.131.0 ug/L 11/26/14 13:00 11,3-Dichloropropane
0.12 U 0.121.0 ug/L 11/26/14 13:00 12,2-Dichloropropane
0.25 U 0.251.0 ug/L 11/26/14 13:00 11,1-Dichloropropene
0.11 U 0.111.0 ug/L 11/26/14 13:00 1Ethylbenzene
0.25 U 0.251.0 ug/L 11/26/14 13:00 1Ethylene Dibromide
0.40 U 0.405.0 ug/L 11/26/14 13:00 1Hexachlorobutadiene
0.10 U 0.101.0 ug/L 11/26/14 13:00 1Isopropylbenzene
0.24 U 0.2410 ug/L 11/26/14 13:00 1Isopropyl ether
0.13 U 0.131.0 ug/L 11/26/14 13:00 14-Isopropyltoluene
1.0 U 1.05.0 ug/L 11/26/14 13:00 1Methylene Chloride
1.0 U 1.010 ug/L 11/26/14 13:00 14-Methyl-2-pentanone (MIBK)
0.20 U 0.2010 ug/L 11/26/14 13:00 1Methyl tert-butyl ether
1.0 U 1.05.0 ug/L 11/26/14 13:00 1Naphthalene
0.10 U 0.101.0 ug/L 11/26/14 13:00 1n-Butylbenzene
0.15 U 0.151.0 ug/L 11/26/14 13:00 1N-Propylbenzene
0.16 U 0.161.0 ug/L 11/26/14 13:00 1sec-Butylbenzene
0.11 U 0.111.0 ug/L 11/26/14 13:00 1Styrene
0.12 U 0.121.0 ug/L 11/26/14 13:00 1tert-Butylbenzene
0.33 U 0.331.0 ug/L 11/26/14 13:00 11,1,1,2-Tetrachloroethane
0.18 U 0.181.0 ug/L 11/26/14 13:00 11,1,2,2-Tetrachloroethane
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QC Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-360579/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360579
RL MDL
Tetrachloroethene 0.15 U 1.0 0.15 ug/L 11/26/14 13:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.33 U 0.331.0 ug/L 11/26/14 13:00 1Toluene
0.20 U 0.201.0 ug/L 11/26/14 13:00 1trans-1,2-Dichloroethene
0.21 U 0.211.0 ug/L 11/26/14 13:00 1trans-1,3-Dichloropropene
0.35 U 0.355.0 ug/L 11/26/14 13:00 11,2,3-Trichlorobenzene
0.25 U 0.255.0 ug/L 11/26/14 13:00 11,2,4-Trichlorobenzene
0.50 U 0.501.0 ug/L 11/26/14 13:00 11,1,1-Trichloroethane
0.13 U 0.131.0 ug/L 11/26/14 13:00 11,1,2-Trichloroethane
0.13 U 0.131.0 ug/L 11/26/14 13:00 1Trichloroethene
0.25 U 0.251.0 ug/L 11/26/14 13:00 1Trichlorofluoromethane
0.41 U 0.411.0 ug/L 11/26/14 13:00 11,2,3-Trichloropropane
0.33 U 0.331.0 ug/L 11/26/14 13:00 11,2,4-Trimethylbenzene
0.33 U 0.331.0 ug/L 11/26/14 13:00 11,3,5-Trimethylbenzene
0.18 U 0.181.0 ug/L 11/26/14 13:00 1Vinyl chloride
Toluene-d8 (Surr)91 70-130 11/26/14 13:00 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
123 11/26/14 13:00 11,2-Dichloroethane-d4 (Surr)70-130
103 11/26/14 13:00 1Dibromofluoromethane (Surr)70-130
102 11/26/14 13:00 14-Bromofluorobenzene (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-360579/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360579
Acetone 250 286 ug/L 114 39 -162
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 49.7 ug/L 99 74 -123
Bromobenzene 50.0 48.1 ug/L 96 79 -125
Bromoform 50.0 56.1 ug/L 112 60 -134
Bromomethane 50.0 59.6 ug/L 119 10 -171
2-Butanone (MEK)250 269 ug/L 108 55 -142
Carbon tetrachloride 50.0 58.0 ug/L 116 70 -131
Chlorobenzene 50.0 44.5 ug/L 89 79 -120
Chlorobromomethane 50.0 52.7 ug/L 105 60 -136
Chlorodibromomethane 50.0 57.5 ug/L 115 63 -134
Chloroethane 50.0 66.4 ug/L 133 47 -148
Chloroform 50.0 56.8 ug/L 114 76 -128
Chloromethane 50.0 56.3 ug/L 113 47 -151
2-Chlorotoluene 50.0 48.1 ug/L 96 78 -126
4-Chlorotoluene 50.0 49.1 ug/L 98 79 -124
cis-1,2-Dichloroethene 50.0 57.4 ug/L 115 78 -127
cis-1,3-Dichloropropene 50.0 55.4 ug/L 111 73 -128
1,2-Dibromo-3-Chloropropane 50.0 55.9 ug/L 112 57 -126
1,2-Dichlorobenzene 50.0 51.3 ug/L 103 77 -124
1,3-Dichlorobenzene 50.0 49.7 ug/L 99 79 -123
1,4-Dichlorobenzene 50.0 48.0 ug/L 96 76 -124
Dichlorobromomethane 50.0 59.7 ug/L 119 72 -129
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QC Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-360579/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360579
Dichlorodifluoromethane 50.0 57.6 ug/L 115 41 -165
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1-Dichloroethane 50.0 55.8 ug/L 112 69 -132
1,2-Dichloroethane 50.0 61.4 Q ug/L 123 75 -120
1,1-Dichloroethene 50.0 50.1 ug/L 100 73 -134
1,2-Dichloropropane 50.0 51.3 ug/L 103 71 -126
1,3-Dichloropropane 50.0 52.8 ug/L 106 73 -125
2,2-Dichloropropane 50.0 61.9 ug/L 124 72 -147
1,1-Dichloropropene 50.0 48.9 ug/L 98 74 -130
Ethylbenzene 50.0 47.2 ug/L 94 78 -125
Ethylene Dibromide 50.0 52.3 ug/L 105 75 -127
Hexachlorobutadiene 50.0 48.4 ug/L 97 62 -145
Isopropylbenzene 50.0 47.6 ug/L 95 72 -129
4-Isopropyltoluene 50.0 50.2 ug/L 100 69 -129
Methylene Chloride 50.0 51.7 ug/L 103 79 -124
4-Methyl-2-pentanone (MIBK)250 309 ug/L 124 51 -143
Methyl tert-butyl ether 50.0 62.5 ug/L 125 76 -126
Naphthalene 50.0 55.7 ug/L 111 56 -136
n-Butylbenzene 50.0 48.7 ug/L 97 72 -128
N-Propylbenzene 50.0 46.5 ug/L 93 74 -130
sec-Butylbenzene 50.0 45.4 ug/L 91 71 -130
Styrene 50.0 49.9 ug/L 100 75 -129
tert-Butylbenzene 50.0 47.9 ug/L 96 72 -130
1,1,1,2-Tetrachloroethane 50.0 51.9 ug/L 104 68 -132
1,1,2,2-Tetrachloroethane 50.0 45.4 ug/L 91 71 -127
Tetrachloroethene 50.0 46.5 ug/L 93 77 -128
Toluene 50.0 50.0 ug/L 100 77 -125
trans-1,2-Dichloroethene 50.0 49.8 ug/L 100 78 -130
trans-1,3-Dichloropropene 50.0 56.4 ug/L 113 72 -127
1,2,3-Trichlorobenzene 50.0 52.5 ug/L 105 63 -136
1,2,4-Trichlorobenzene 50.0 52.5 ug/L 105 67 -134
1,1,1-Trichloroethane 50.0 60.2 ug/L 120 76 -126
1,1,2-Trichloroethane 50.0 50.4 ug/L 101 69 -127
Trichloroethene 50.0 48.9 ug/L 98 80 -120
Trichlorofluoromethane 50.0 58.2 ug/L 116 66 -144
1,2,3-Trichloropropane 50.0 50.6 ug/L 101 74 -126
1,2,4-Trimethylbenzene 50.0 50.6 ug/L 101 72 -129
1,3,5-Trimethylbenzene 50.0 49.1 ug/L 98 72 -130
Vinyl chloride 50.0 59.8 ug/L 120 58 -141
Toluene-d8 (Surr)70 -130
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
1231,2-Dichloroethane-d4 (Surr)70 -130
103Dibromofluoromethane (Surr)70 -130
1004-Bromofluorobenzene (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-360579/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360579
Acetone 250 278 ug/L 111 39 -162 3 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 50.0 49.8 ug/L 100 74 -123 0 30
Bromobenzene 50.0 47.3 ug/L 95 79 -125 2 30
Bromoform 50.0 55.3 ug/L 111 60 -134 1 30
Bromomethane 50.0 66.9 ug/L 134 10 -171 12 50
2-Butanone (MEK)250 258 ug/L 103 55 -142 4 30
Carbon tetrachloride 50.0 57.2 ug/L 114 70 -131 1 30
Chlorobenzene 50.0 44.2 ug/L 88 79 -120 1 30
Chlorobromomethane 50.0 52.8 ug/L 106 60 -136 0 30
Chlorodibromomethane 50.0 58.3 ug/L 117 63 -134 1 50
Chloroethane 50.0 67.0 ug/L 134 47 -148 1 40
Chloroform 50.0 56.4 ug/L 113 76 -128 1 30
Chloromethane 50.0 56.4 ug/L 113 47 -151 0 30
2-Chlorotoluene 50.0 47.6 ug/L 95 78 -126 1 30
4-Chlorotoluene 50.0 48.6 ug/L 97 79 -124 1 30
cis-1,2-Dichloroethene 50.0 56.9 ug/L 114 78 -127 1 30
cis-1,3-Dichloropropene 50.0 55.5 ug/L 111 73 -128 0 30
1,2-Dibromo-3-Chloropropane 50.0 56.7 ug/L 113 57 -126 1 50
1,2-Dichlorobenzene 50.0 50.8 ug/L 102 77 -124 1 30
1,3-Dichlorobenzene 50.0 49.8 ug/L 100 79 -123 0 30
1,4-Dichlorobenzene 50.0 49.3 ug/L 99 76 -124 3 30
Dichlorobromomethane 50.0 60.1 ug/L 120 72 -129 1 30
Dichlorodifluoromethane 50.0 58.0 ug/L 116 41 -165 1 50
1,1-Dichloroethane 50.0 55.8 ug/L 112 69 -132 0 30
1,2-Dichloroethane 50.0 61.2 Q ug/L 122 75 -120 0 30
1,1-Dichloroethene 50.0 51.8 ug/L 104 73 -134 3 30
1,2-Dichloropropane 50.0 51.9 ug/L 104 71 -126 1 30
1,3-Dichloropropane 50.0 52.2 ug/L 104 73 -125 1 30
2,2-Dichloropropane 50.0 61.5 ug/L 123 72 -147 1 30
1,1-Dichloropropene 50.0 50.3 ug/L 101 74 -130 3 30
Ethylbenzene 50.0 47.0 ug/L 94 78 -125 0 30
Ethylene Dibromide 50.0 51.0 ug/L 102 75 -127 2 30
Hexachlorobutadiene 50.0 50.3 ug/L 101 62 -145 4 30
Isopropylbenzene 50.0 47.3 ug/L 95 72 -129 1 30
4-Isopropyltoluene 50.0 51.5 ug/L 103 69 -129 3 50
Methylene Chloride 50.0 50.3 ug/L 101 79 -124 3 30
4-Methyl-2-pentanone (MIBK)250 306 ug/L 122 51 -143 1 30
Methyl tert-butyl ether 50.0 62.3 ug/L 125 76 -126 0 30
Naphthalene 50.0 56.2 ug/L 112 56 -136 1 30
n-Butylbenzene 50.0 48.6 ug/L 97 72 -128 0 30
N-Propylbenzene 50.0 46.4 ug/L 93 74 -130 0 30
sec-Butylbenzene 50.0 45.1 ug/L 90 71 -130 1 30
Styrene 50.0 49.4 ug/L 99 75 -129 1 30
tert-Butylbenzene 50.0 47.1 ug/L 94 72 -130 2 30
1,1,1,2-Tetrachloroethane 50.0 51.2 ug/L 102 68 -132 1 30
1,1,2,2-Tetrachloroethane 50.0 45.4 ug/L 91 71 -127 0 30
Tetrachloroethene 50.0 47.0 ug/L 94 77 -128 1 30
Toluene 50.0 49.7 ug/L 99 77 -125 1 30
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QC Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-360579/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360579
trans-1,2-Dichloroethene 50.0 49.5 ug/L 99 78 -130 1 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
trans-1,3-Dichloropropene 50.0 57.3 ug/L 115 72 -127 2 50
1,2,3-Trichlorobenzene 50.0 52.5 ug/L 105 63 -136 0 30
1,2,4-Trichlorobenzene 50.0 53.2 ug/L 106 67 -134 1 30
1,1,1-Trichloroethane 50.0 60.3 ug/L 121 76 -126 0 30
1,1,2-Trichloroethane 50.0 50.2 ug/L 100 69 -127 0 30
Trichloroethene 50.0 49.3 ug/L 99 80 -120 1 30
Trichlorofluoromethane 50.0 59.3 ug/L 119 66 -144 2 30
1,2,3-Trichloropropane 50.0 50.3 ug/L 101 74 -126 1 30
1,2,4-Trimethylbenzene 50.0 50.1 ug/L 100 72 -129 1 50
1,3,5-Trimethylbenzene 50.0 49.1 ug/L 98 72 -130 0 50
Vinyl chloride 50.0 61.7 ug/L 123 58 -141 3 30
Toluene-d8 (Surr)70 -130
Surrogate
88
LCSD LCSD
Qualifier Limits%Recovery
1211,2-Dichloroethane-d4 (Surr)70 -130
106Dibromofluoromethane (Surr)70 -130
1014-Bromofluorobenzene (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-360702/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360702
RL MDL
Acetone 5.0 U 10 5.0 ug/L 11/26/14 22:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.25 U 0.251.0 ug/L 11/26/14 22:32 1Benzene
0.16 U 0.161.0 ug/L 11/26/14 22:32 1Bromobenzene
0.50 U 0.501.0 ug/L 11/26/14 22:32 1Bromoform
2.0 U 2.05.0 ug/L 11/26/14 22:32 1Bromomethane
1.0 U 1.010 ug/L 11/26/14 22:32 12-Butanone (MEK)
0.50 U 0.501.0 ug/L 11/26/14 22:32 1Carbon tetrachloride
0.25 U 0.251.0 ug/L 11/26/14 22:32 1Chlorobenzene
0.14 U 0.141.0 ug/L 11/26/14 22:32 1Chlorobromomethane
0.10 U 0.101.0 ug/L 11/26/14 22:32 1Chlorodibromomethane
2.0 U 2.05.0 ug/L 11/26/14 22:32 1Chloroethane
0.14 U 0.141.0 ug/L 11/26/14 22:32 1Chloroform
0.27 U 0.275.0 ug/L 11/26/14 22:32 11-Chlorohexane
0.33 U 0.331.0 ug/L 11/26/14 22:32 1Chloromethane
0.17 U 0.171.0 ug/L 11/26/14 22:32 12-Chlorotoluene
0.27 U 0.271.0 ug/L 11/26/14 22:32 14-Chlorotoluene
0.15 U 0.151.0 ug/L 11/26/14 22:32 1cis-1,2-Dichloroethene
0.11 U 0.111.0 ug/L 11/26/14 22:32 1cis-1,3-Dichloropropene
0.44 U 0.445.0 ug/L 11/26/14 22:32 11,2-Dibromo-3-Chloropropane
0.21 U 0.211.0 ug/L 11/26/14 22:32 11,2-Dichlorobenzene
0.25 U 0.251.0 ug/L 11/26/14 22:32 11,3-Dichlorobenzene
0.28 U 0.281.0 ug/L 11/26/14 22:32 11,4-Dichlorobenzene
0.25 U 0.251.0 ug/L 11/26/14 22:32 1Dichlorobromomethane
0.25 U 0.251.0 ug/L 11/26/14 22:32 1Dichlorodifluoromethane
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QC Sample Results
TestAmerica Job ID: 680-107398-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-360702/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 360702
RL MDL
1,1-Dichloroethane 0.25 U 1.0 0.25 ug/L 11/26/14 22:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.10 U 0.101.0 ug/L 11/26/14 22:32 11,2-Dichloroethane
0.11 U 0.111.0 ug/L 11/26/14 22:32 11,1-Dichloroethene
0.13 U 0.131.0 ug/L 11/26/14 22:32 11,2-Dichloropropane
0.13 U 0.131.0 ug/L 11/26/14 22:32 11,3-Dichloropropane
0.12 U 0.121.0 ug/L 11/26/14 22:32 12,2-Dichloropropane
0.25 U 0.251.0 ug/L 11/26/14 22:32 11,1-Dichloropropene
0.11 U 0.111.0 ug/L 11/26/14 22:32 1Ethylbenzene
0.25 U 0.251.0 ug/L 11/26/14 22:32 1Ethylene Dibromide
0.534 J 0.405.0 ug/L 11/26/14 22:32 1Hexachlorobutadiene
0.10 U 0.101.0 ug/L 11/26/14 22:32 1Isopropylbenzene
0.24 U 0.2410 ug/L 11/26/14 22:32 1Isopropyl ether
0.13 U 0.131.0 ug/L 11/26/14 22:32 14-Isopropyltoluene
1.0 U 1.05.0 ug/L 11/26/14 22:32 1Methylene Chloride
1.0 U 1.010 ug/L 11/26/14 22:32 14-Methyl-2-pentanone (MIBK)
0.20 U 0.2010 ug/L 11/26/14 22:32 1Methyl tert-butyl ether
1.0 U 1.05.0 ug/L 11/26/14 22:32 1Naphthalene
0.10 U 0.101.0 ug/L 11/26/14 22:32 1n-Butylbenzene
0.15 U 0.151.0 ug/L 11/26/14 22:32 1N-Propylbenzene
0.16 U 0.161.0 ug/L 11/26/14 22:32 1sec-Butylbenzene
0.11 U 0.111.0 ug/L 11/26/14 22:32 1Styrene
0.12 U 0.121.0 ug/L 11/26/14 22:32 1tert-Butylbenzene
0.33 U 0.331.0 ug/L 11/26/14 22:32 11,1,1,2-Tetrachloroethane
0.18 U 0.181.0 ug/L 11/26/14 22:32 11,1,2,2-Tetrachloroethane
0.15 U 0.151.0 ug/L 11/26/14 22:32 1Tetrachloroethene
0.33 U 0.331.0 ug/L 11/26/14 22:32 1Toluene
0.20 U 0.201.0 ug/L 11/26/14 22:32 1trans-1,2-Dichloroethene
0.21 U 0.211.0 ug/L 11/26/14 22:32 1trans-1,3-Dichloropropene
0.389 J 0.355.0 ug/L 11/26/14 22:32 11,2,3-Trichlorobenzene
0.25 U 0.255.0 ug/L 11/26/14 22:32 11,2,4-Trichlorobenzene
0.50 U 0.501.0 ug/L 11/26/14 22:32 11,1,1-Trichloroethane
0.13 U 0.131.0 ug/L 11/26/14 22:32 11,1,2-Trichloroethane
0.13 U 0.131.0 ug/L 11/26/14 22:32 1Trichloroethene
0.25 U 0.251.0 ug/L 11/26/14 22:32 1Trichlorofluoromethane
0.41 U 0.411.0 ug/L 11/26/14 22:32 11,2,3-Trichloropropane
0.33 U 0.331.0 ug/L 11/26/14 22:32 11,2,4-Trimethylbenzene
0.33 U 0.331.0 ug/L 11/26/14 22:32 11,3,5-Trimethylbenzene
0.18 U 0.181.0 ug/L 11/26/14 22:32 1Vinyl chloride
Toluene-d8 (Surr)99 70-130 11/26/14 22:32 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
80 11/26/14 22:32 11,2-Dichloroethane-d4 (Surr)70-130
90 11/26/14 22:32 1Dibromofluoromethane (Surr)70-130
93 11/26/14 22:32 14-Bromofluorobenzene (Surr)70-130
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