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HomeMy WebLinkAbout8606_SurryCounty_MSWLF_ASDInorganics_DIN27391_20170421Surry County Subtitle D Lined MSWLF Mt. Airy, North Carolina April 21, 2017 Permit Number: 86-06 Alternative Source Demonstration-Metals Prepared for Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina MESCO Project Number: G16025.0 P.O. Box 97 Garner, NC 27529 License No. C-0281 April 21, 2017 Ms. Jaclynne Drummond Solid Waste Section (SWS) Division of Waste Management/ NCDEQ 2090 US Highway 70 Swannanoa, NC 28778 Re: Alternative Source Demonstration-Metals Surry County Landfill Permit No. 86-02 and 86-06 MESCO Project No. G16025.0 Dear Ms. Drummond, Introduction On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Alternative Source Demonstration (ASD) with new groundwater protection standards for metals detected in groundwater samples at the Surry County Landfill located in Mount Airy NC. NC Solid Waste Rule 15A NCAC 13B .1634 (f)(2) provides that an owner/operator may demonstrate that a source other than a MSWLF unit caused the exceedance of the groundwater protection standards, or the exceedance resulted from error in sampling, analysis, or natural variation in groundwater quality. NC Solid Waste Rule 15A NCAC 13B .1634 (g)(5) allows the Division to approve background levels as groundwater protection standards. The NC Solid Waste Section required, through a letter (DIN:26557) dated August 8, 2016, that either an ASD for metal exceedances be approved or assessment monitoring should be implemented. Assessment monitoring has already been initiated at both landfills in response to detections of volatile organic compounds (VOCs). This ASD may potentially aid in future decision making concerning the scope of assessments and/or corrective actions. This ASD provides six lines of evidence supporting that the source of metals below background levels is from natural variation and not from a landfill release. We request that the SWS approve this ASD which establishes background levels as the groundwater protection standard for ten metals and preserve the current 2L/GWP Standards for five metals. The new groundwater Standards will be used for future compliance decisions at the entire Surry County Mount Airy landfill facility. Background The Surry County Mount Airy Landfill is located at 237 Landfill Road, Mount Airy, North Carolina. The facility consists of an unlined closed MSWLF with a Construction and Demolition Landfill upon a portion of a closed MSWLF (Permit 86-02) and an active Subtitle D Landfill (86-06). Groundwater at the unlined closed landfill has been continuously monitored since 1990, began assessment monitoring in 1997 and initiated corrective action in response to volatile organic compounds detected in groundwater in May 2010. Metals have been detected with some above groundwater Standards. Past studies (Assessment of Corrective Measures (Oct 2007), Corrective Action Plan (March 2010), Corrective Action Evaluation Report (May 2013) have never attributed detections of inorganics to an anthropogenic source rather represent natural background levels. Unfortunately true background/baseline results are unavailable at the closed landfill since wells were installed following operations and evidence suggests that the background well may have previously been impacted. Pre- operation baseline samples were collected from the adjacent lined landfill which are discussed in detail below which were used to establish background levels for the entire site. The Surry County Subtitle D lined Landfill Subtitle D Lined MSWLF, permit #86-06,currently consists of two Phases (1&2) that are contiguous thus monitored and reported together. The lined landfill initiated site-wide assessment monitoring in June 2016 in response to detections of VOCs in downgradient wells MW-2, MW-6R and MW-9S. Recent potentiometric maps with monitoring well locations is shown on Sheet 1 and Sheet 2. Water quality at this facility has been monitored at least semi-annually since prior to commencement of operations in 1998 with all historical data reviewed in support of this ASD. Both phases have had a baseline established by four independent events performed within the first six months of operations including at least one prior to opening. Baseline water quality monitoring reports were prepared for both Phases and previously submitted to the SWS (DIN:12909). Formulation of this ASD involved a review of site specific literature which confirms that the site conceptual model developed in support of the site’s water quality monitoring plans remain valid. Comparisons of dissolved metals to total metals were made. Metals in leachate samples were evaluated. A statistical analysis using historical site-wide groundwater data was performed. The evidence reviewed in support of this ASD concluded that metals are naturally inherent in the geochemistry of the fractured rock aquifer system. The site has correctly characterized the hydrogeology over a significant period of time and has an appropriate number of monitoring wells in place to determine site background conditions. The upgradient well accurately reflect the concentrations of metals naturally present in the aquifer on site. At the lined landfill the downgradient results are believed to be a valid reflection of aquifer metal concentrations at all locations, except for potentially the wells impacted by VOCs. Metal concentrations have remained stable over time suggesting that the landfill is likely not affecting the natural geochemistry of the downgradient aquifer. Basically, if the landfill was not there, one would expect to still observe the same metal concentrations. Leachate and LFG is a complex mix of mobile compounds. When there is a release, the more mobile compounds such as VOCs would be detected in the wells before the much less mobile total metals. Therefore, VOCs may serve as a much better indicator of a release than total metals. Metals were originally intended to serve as an indicator parameter before low level VOC testing was readily available. Today quantification of metals is less useful especially downgradient of modern lined landfills. Leachate and landfill gas may change the geochemistry resulting in increased levels of metals but our experience has shown that low level VOCs will be detected before an increase in metals is noticed. Since portions of the aquifer downgradient of the landfill have been impacted by VOCs, the altered geochemistry may solubilize greater quantities of metals. These areas remain under assessment monitoring. If corrective action is implemented, focus should be centered on VOCs based on the premise that the metals are natural but can precipitate in response to the release. Remediation of the leachate and/or LFG has the potential to collaterally reduce metal concentrations. 2 In the spring of 2013 groundwater samples MW-12 and MW-13 and in the fall of 2016 MW-9S were tested for both dissolved metals (lab filtered) and total metals (no filtration). Aqueous phase dissolved metals comprised between 7% and 78% of total metals Table 1. These findings are consistent with other sites across NC and also expected to be consistent at other on site wells. NC Department of Water Resources refers to the 2L Standards as the total concentration “of any constituent in a dissolved, colloidal or particulate form which is mobile in groundwater. This does not apply to sediment or other particulate matter which is preserved in a groundwater sample as a result of well construction or sampling procedures”. However, the NC SWS requires samples to be analyzed for non-filtered total metals which lends itself to higher prevalence of 2L exceedances. Total metal concentrations may also appear elevated due to the reaction of acid preservatives and sediment which may be entrained in the sample containers, as metal solubility is conversely related to pH. Unpreserved samples would likely be more appropriate to use to quantify aqueous phase metal concentrations. Extended hold times are unnecessary; however, preservation of samples is required to conform to laboratory methods. Each inorganic constituent listed in 40 CFR Subpart 258 Appendix I is a naturally occurring metal. All Appendix I metals have historically been detected within samples collected from the facility background well. Chromium, cobalt and vanadium are the most common metals detected above regulatory compliance Standards. Metal detections are largely inconsistent and concentrations are not increasing over time. This ASD presents background concentrations for inorganics which were used to statistically determine new groundwater protection Standards for ten specific metals at the Surry County Mount Airy Landfill. The research performed in support of this report suggests that any detection of inorganics above background levels should be able to differentiate between natural variation and a landfill release. Derivation of the background levels are explained below. Groundwater Protection Standards Derivation Procedure An ASD should not be perpetually and unconditionally valid since metal concentrations may increase over time which actually may originate or be indicative of a MSWLF release. Rather than indiscriminately claim all future metals originate from an alternative source, we propose new groundwater protection standards for ten metals. The background levels were established in accordance with Rule .1631(a)(1) and Rule .1632. The groundwater monitoring data for each of the ten inorganic constituents was evaluated through statistical analysis methods that conform to Rule .1632 (g)(3) and USEPA Statistical Analysis of Grounder Monitoring Data at RCRA Facilities Unified Guidance document 2009 Section 17.2.2. All historical laboratory data was imported into a commercially produced Chempoint statistical database. All historical detections in the upgradient background well MW-1 and the detections observed during the four event baseline data from all other wells are tabulated on Table 2. Chemstat statistical analysis software specifically developed for evaluation of groundwater data at RCRA facilities was used on all historical data to perform descriptive statistics, evaluate data independence, test for data distribution and analyze trends. 3 An upper tolerance limit (UTL) was calculated for each of the ten metals from the maximum value observed from a pool of background data using the non-parametric tolerance interval method (Appendix A). The laboratory results from which the respective metals UTL was calculated are shown in Appendix B. An UTL is the value defined at a particular confidence level for a specified percentage of all future measurements. The background data consisted of all historical data spanning 18 years from upgradient background well MW-1 and the four “baseline” events performed at each well within 6 months of landfill operations for a total of 100 independent events. At a 95% confidence level the large pool of 97 events the average coverage is a robust 98.98%. The UTL, rounded to the nearest whole number, for each of the ten metals will be the new groundwater protection standards at the Surry County landfill as shown in (ug/L) below. The NC 2L/GWP Standard will continue to be the regulatory compliance limit for all other constituents. New Groundwater Protection Standards for Surry County Landfill (Mount Airy) Antimony Arsenic Beryllium Cadmium Chromium Cobalt Lead Nickel Thallium Vanadium 13 19 26 28 300 164 110 159 11 256 Graphs of the highest concentrations of metals observed during the baseline period (intrawell), highest levels ever recorded within the background well (interwell) and the highest ever observed in leachate samples compared to Standards is attached (Figure 1). A summary of data observations is outlined below. Intrawell Baseline Evaluation Of the samples collected during the baseline period every metal except for antimony and selenium were detected at least once and 8 of the 13 detected metals (62%) exceeded their respective current 2L/GWP Standard at least once. The baseline reports and analytical data were evaluated with no censorship and the UTL for each metal was determined. This value is considered as the baseline for each respective well which was pooled to represent the entire site. These baseline levels represent natural conditions as if the landfill was never constructed. Interwell Background Evaluation Samples collected from the upgradient background well (MW-1) over the entire period of record (18 years) contained every Appendix I metal at least once. Ten of the fifteen (67%) metals have exceeded the current 2L/GWP Standard. All historical data from the background well was evaluated with no censorship and the UTL for each metal was determined. The UTL value is considered background and represents conditions hydraulically upgradient of the landfill and is also representative of water quality that will eventually migrate to downgradient wells. 4 Leachate Evaluation Samples of untreated leachate have historically contained ten of the fifteen (67%) Appendix I metals with 40% of the metals eclipsing their respective 2L/GWP Standard at least once. Since leachate quality is highly variable, a conservative approach was used which retained all data. Since a leachate release will attenuate and dilute with groundwater a dilution attenuation factor (DAF) was assigned to the metal concentrations observed in the leachate samples. A DAF of 20:1 was chosen based on the US EPA default value and the dilution factor used in the Synthetic Precipitation Leach Procedure (SPLP; EPA Test Method 1312). After applying the DAF the only metal detected in a leachate sample above a 2L/GWP Standard (0.28 uq/L) was thallium (2.9 uq/L). Most of the historical and all of the most recent inorganic contaminants could not have resulted from the MSWLF given that leachate characteristics are generally lower in concentration compared to groundwater samples. Metal concentrations in the leachate are also generally much lower at this facility compared to published leachate values from other facilities EPA 1. The concentrations of metals in the leachate samples are presented for comparison purposes and not used in the formulation of the UTL. Conclusion In conclusion, the six lines of evidence to support that natural variation, rather than a MSWLF release, is the source of metals at specific levels documented within this ASD, is summarized as: 1. An alternate source of metals exist which is natural variation from erosion of native deposits. Concentrations of total metals may be artificially elevated due to the reaction of solids with acid preservatives in the container which is required by the laboratory method. 2. A hydraulic connection between the metallic minerals associated with the upper regolith and metamorphic bedrock that comprise the uppermost aquifer exists. The background well is hydraulically upgradient and contain species of metals and at comparable or higher concentrations as detected downgradient. 3. Metals are naturally inherent in the upper bedrock aquifer which underlay the facility along all flow paths including downgradient of the landfill. 4. Metal concentrations were elevated during the baseline period established through the four events during the initial first six months operation. Metals would be elevated regardless of the presence of the landfill. Numbers of metal detections and concentrations have generally remained stable or decreased over time. 5. Dissolved phase metal concentrations have been significantly lower compared to total metals. The composite liner system should inhibit particulate metals from migrating downgradient allowing only dissolved phase metals to become mobile. 6. Metals likely did not originate from leachate. The vast majority of metals detected in groundwater samples are higher compared to leachate samples and only a “j-qualified” concentration of thallium would be above the 2L/GWP Standard after applying a conservative dilution attenuation factor. As a contingency, if a metal concentration exceeds a groundwater protection standard, further empirical evidence will be evaluated such as dissolved metal analysis and/or further verification sampling. If further data suggests the metal concentration may be attributed to a release, additional assessment will be initiated to determine the source which may necessitate another ASD. 1 1988 EPA document-Summary of Data on MSWLFLeachate Characteristics – EPA/530-SW-88-038 5 Figures Figure 1 Background Levels 13 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0 2 4 6 8 10 12 14 16 ug / L Background Levels Antimony Antimony SWS GWP Surry LF GWP LEACHATE DILUTED UTL 19 ND ND ND ND ND ND ND ND ND ND 0 4 8 12 16 20 ug / L Background Levels Arsenic Arsenic NC 2L Std Surry LF GWP LEACHATE DILUTED UTL ND ND 26 ND ND ND ND ND 0 5 10 15 20 25 30 ug / L Background Levels Berrylium Beryllium SWS GWP Surry LF GWP LEACHATE DILUTED UTL All Time Max in Background Well MW-1 Max Baseline in Other Wells UTL = Upper Tolerance Limit ND = Not Detected (represented as 1/2 detection limit) Surry County Landfill (Mt. Airy)Page 1 of 4 Figure 1 Background Levels 28 ND ND ND ND ND ND ND ND ND ND 0 5 10 15 20 25 30 ug / L Background Levels Cadmium Cadmium NC 2L Std Surry LF GWP LEACHATE DILUTED UTL 300 ND ND ND 0 50 100 150 200 250 300 350 ug / L Background Levels Chromium Chromium NC 2L Std Surry LF GWP LEACHATE DILUTED UTL ND ND 164 ND 0 20 40 60 80 100 120 140 160 180 ug / L Background Levels Cobalt Cobalt SWS GWP Surry LF GWP LEACHATE DILUTED UTL All Time Max in Background Well MW-1 Max Baseline in Other Wells UTL = Upper Tolerance Limit ND = Not Detected (represented as 1/2 detection limit) Surry County Landfill (Mt. Airy)Page 2 of 4 Figure 1 Background Levels ND ND 110 ND ND ND 0 20 40 60 80 100 120 ug / L Background Levels Lead Lead NC 2L Std Surry LF GWP LEACHATE DILUTED UTL ND ND 159 ND 0 20 40 60 80 100 120 140 160 180 ug / L Background Levels Nickel Nickel NC 2L Std Surry LF GWP LEACHATE DILUTED UTL 11 ND ND ND ND ND ND ND ND ND ND ND ND 0 2 4 6 8 10 12 ug / L Background Levels Thallium Thallium SWS GWP Surry LF GWP LEACHATE DILUTED UTL All Time Max in Background Well MW-1 Max Baseline in Other Wells UTL = Upper Tolerance Limit ND = Not Detected (represented as 1/2 detection limit) Surry County Landfill (Mt. Airy)Page 3 of 4 Figure 1 Background Levels ND ND ND ND 256 0 50 100 150 200 250 300 ug / L Background Levels Vanadium Vanadium SWS GWP Surry LF GWP LEACHATE DILUTED UTL All Time Max in Background Well MW-1 Max Baseline in Other Wells UTL = Upper Tolerance Limit ND = Not Detected (represented as 1/2 detection limit) Surry County Landfill (Mt. Airy)Page 4 of 4 Tables Table 1 Comparison of Total and Dissolved Metals Sample ID Parameter Name Sample Date 2L/GWP Standard Total Undissolved Concentration (ug/L) Dissolved Concentration (ug/L) Concentration Difference (ug/L) Concentration Differential Total to Dissolved (%) Concentration Differential Total to Dissolved Average (%) MW-12 Cadmium 05/31/13 2 5.2 1.4 3.8 37 MW-12 Thallium 05/31/13 0.28 6 <3 ND 3.0 50 MW-12 Barium 05/31/13 700.16.9 9.1 7.8 54 MW-12 Vanadium 05/31/13 3.5 <5 0.85 4.2 7 MW-12 Zinc 05/31/13 1000.<10 2.6 7.4 26 MW-13 Barium 06/01/13 700.36.6 28.6 8.0 78 MW-13 Cadmium 06/01/13 2.<1 ND 0.3 0.7 30 MW-13 Chromium 06/01/13 10.2.2 0.58 1.6 26 MW-13 Cobalt 06/01/13 1.5.6 3.9 1.7 70 MW-13 Nickel 06/01/13 100.<5 ND 2.2 2.8 44 MW-13 Vanadium 06/01/13 3.5 <5 0.96 4.0 19 MW-13 Zinc 06/01/13 1000.<10 ND 4.2 5.8 42 MW-9S Barium 12/01/16 700.117.60 57.0 51 MW-9S Cadmium 12/01/16 2.1.6 1 0.6 62 MW-9S Cobalt 12/01/16 1.107 83.9 23.1 78 MW-9S Zinc 12/01/16 1000.17.8 4 13.8 23 MW-9S Nickel 12/01/16 100.15.7 12.1 3.6 23 MW-9S Vanadium 12/01/16 3.5 3.1 <2.5 ND 0.6 19 MW-9S Lead 12/01/16 15.3.8 <2.5 ND 1.3 34 MW-9S Copper 12/01/16 1000.8.<2.5 ND 5.5 69 MW-9S Chromium 12/01/16 10.5.7 <2.5 ND 3.2 56 < = Not Detected relative to MDL MDL = Method Detection Limit ND = Not Detected ND substituted with MDL for calculations RED :Above 2L/GWP Standard Spring 2013 and Fall 2016 35 44 46 Surry County Landfill (Mount Airy)Page 1 of 1 Table 2 Metal Detections Summary (Represents Background) An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Le a d Ni c k e l Se l e n i u m Si l v e r Th a l l i u m Va n a d i u m Zi n c NEW SITE SPECIFIC GWP STANDARD*12.5 18.6 2000 26 28.4 300 164 1000 110 159 20 20 10.5 256 1000 6 10 100 1 1 10 10 10 10 50 10 10 5.5 25 10 10 700 2 10 1000 15 100 20 20 1000 1.4 4 1 0.28 3.5 SAMPLE ID Screened Lithology Data Period MW-1 (BG Well)Bedrock ALL TIME HIGH12.5 18.6 942 13.7 28.4 300 58.2 456 92.9 90.5 17.8 1.2 10.5 249 806. MW-2 Bedrock Max Baseline <30 <10 <500 <2 <1 <10 <10 <200 <10 <50 <20 <10 <10 <40 <50 MW-3 Bedrock Max Baseline <30 <10 <500 2 <1 <10 <10 <200 <10 <50 <20 <10 <10 <40 <50 MW-4S Bedrock Max Baseline <30 <10 1860 26 9 146 164 <200 110 80.<20 <10 <10 215 615. MW-4D Bedrock Max Baseline <30 <10 <500 <2 13 29 18 <200 <10 159 <20 <10 <10 <40 67. MW-5 Bedrock Max Baseline <30 <10 <500 <2 4 29 15.<200 <10 99.<20 <10 <10 42 107. MW-6/MW-6R Bedrock Max Baseline <30 <10 <500 <2 2.16 18.<200 17 <50 <20 <10 <10 <40 93. MW-8 Bedrock Max Baseline <2.6 15 2000 9.8 <0.5 154 87.5 108 44.5 99.5 <3.8 <0.1 5.4 256 720 MW-9S Bedrock Max Baseline <2.6 4.7 313 1.4 <0.5 39.7 10.4 19.2 <4 21.0 <3.8 0.46 4.4 57.9 105 MW-9D Bedrock Max Baseline <2.6 <2.7 116 0.46 <0.5 21.9 7.3 10.1 <5 27.4 <3.8 0.41 <3 20.3 45.9 MW-10 Bedrock Max Baseline <2.6 <2.7 150 0.97 <0.5 25.2 8.8 18.9 7.3 22.4 <3.8 <0.1 <3 34.6 92.2 MW-11S Bedrock Max Baseline <2.6 5.6 182 2.4 <0.5 27.5 23 26.3 17.6 21.4 <3.8 0.12 <3 40.5 67.7 MW-11D Bedrock Max Baseline <2.6 6.3 119 0.79 <0.5 26.9 14.6 21.9 8 20.8 <3.8 0.24 <3 35.3 69.7 MW-12 Bedrock Max Baseline <2.6 <2.7 155 0.77 2.5 22.4 13.3 25.2 8.2 19.5 <3.8 <0.1 <3 31.2 47.6 MW-13 Bedrock Max Baseline <2.6 4.4 114 3.3 <0.5 16.1 19 20.8 10.5 14.8 <3.8 <0.1 19.2 22.7 59.7 LEACHATE -ALL TIME HIGH10 8.2 847 <2 <1 13.3 137 5.9 6.1 21.7 13.4 4.7 57 21 31.1 LEACHATE Diluted -All Time High D 0.5 0.4 42.4 <0.1 <0.2 0.7 6.9 0.3 0.3 1.1 0.7 0.2 2.85 1.1 1.6 Table contains concentrations of Appendix I total metals * = New Groundwater Protection Standard established for the Surry County Landfill. Derived statistically from observed background concentrations. All Time High = Highest ever recorded at either the upgradient backgound well or untreated leachate sample. Samples consistantly collected on a semi-annual basis. Diluted D = Extrapolated concentration when untreated leachate is mixed with groundwater. Calculated by a 20:1 dilution ratio (dividing by 20). When two wells shown together indicates wells that have been replaced so data used for both wells RED BOLD = (BG Well) = Background Well Located hydraulically upgradient of Waste Unit Concentration Exceeded 2L or GWP Standard UNTREATED LEACHATE (EFFECTIVELY A COMPOSITE OF PHASES 1&2) RESULTS FROM 1998 - 2016 Max Baseline = Maximum concentration detected during the first four events performed within 6 months of commencement of landfill operations including at least 1 before opening. Considered natural intrawell background levels. < = Not Detected with Detection Limit Indicated SWSL = Solid Waste Section Reporting Limit 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard (Current as of 10/6/16) GWP = Groundwater Protection Standard (Current as of 10/6/16) PHASE 2 BASELINE 2009-2010 SWSL 2L STANDARD GWP STANDARD BACKGROUND WELL PHASES 1-2 PHASE 1 BASELINE 1998 Surry County Landfill (Mt. Airy)Page 1 of 6 Table 2 Metal Detections (Represents Background) MW-1 MW-2 MW-3/3R MW-4S MW-4D MW-5 MW-6/MW-6R MW-7 MW-8 MW-9S MW-9D MW-10 MW-11S MW-11D MW-12 MW-13 LAGOON UTL UTL UTL UTL UTL UTL UTL UTL UTL UTL UTL UTL UTL UTL UTL UTL UTL (AT MAX)(BL MAX) (BL MAX) (BL MAX) (BL MAX) (BL MAX) (BL MAX)(BL MAX) (BL MAX) (BL MAX) (BL MAX) (BL MAX) (BL MAX) (BL MAX) (BL MAX) (BL MAX) (AT MAX)Antimony, total 1 13 12.5 12.5 <30 <30 <30 <30 <30 <30 <30 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 10 Arsenic, total 10 19 18.6 18.6 <10 <10 <10 <10 <10 <10 <10 15 4.7 <2.7 <2.7 5.6 6.3 <2.7 4.4 8.2 Barium, total 700 2000 2000 942 <500 <500 1860 <500 <500 <500 <500 2000 313 116 150 182 119 155 114 847Beryllium, total 4 26 26 13.7 <2 <2 26 <2 <2 <2 <2 9.8 1.4 0.46 0.97 2.4 0.79 0.77 3.3 <2 Cadmium, total 2 28 28.4 28.4 <1 <1 9 13 4 2 1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.5 <0.5 <1 Chromium, total 10 300 300 300 <10 <10 146 <10 29 16 <10 154 39.7 21.9 25.2 27.5 26.9 22.4 16.1 13.3 Cobalt, total 1 164 164 58.2 <10 <10 164 <10 15 18 11 87.5 10.4 7.3 8.8 23 14.6 13.3 19 137Copper, total 1000 1000 456 456 <200 <200 <200 <200 <200 <200 <200 108 19.2 10.1 18.9 26.3 21.9 25.2 20.8 5.9 Lead, total 15 110 110 92.9 <10 <10 110 <10 <10 17 <10 44.5 12.2 <4 7.3 17.6 8 8.2 10.5 6.1 Nickel, total 100 159 159 90.5 <50 <50 80 159 99 <50 <50 99.5 21 27.4 22.4 21.4 20.8 19.5 14.8 21.7 Selenium, total 20 20 17.8 17.8 <20 <20 <20 <20 <20 <20 <20 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 13.4 Silver, total 20 20 1.2 1.2 <10 <10 <10 <10 <10 <10 <10 <0.1 0.46 0.41 <0.1 0.12 0.24 <0.1 <0.1 4.7 Thallium, total 0.28 11 10.5 10.5 <10 <10 <10 <10 <10 <10 <10 5.4 4.4 <3 <3 <3 <3 <3 <3 57 Vanadium, total 3.5 256 256 249 <40 <40 215 <40 42 <40 <40 256 57.9 20.3 34.6 40.5 35.3 31.2 22.7 21 Zinc, total 1000 1000 806 806 <50 <50 615 67 107 93 61 720 105 45.9 92.2 67.7 69.7 47.6 59.7 31.1 ALL WELLSParameter Name 2L/GWP Std NEW GW STANDAR D Shaded = Above 2L/GWP Standard < = ND relative to MDL Surry County Landfill (Mt. Airy)Page 2 of 6 Table 2 Metal Detections (Represents Background) UTL (AT MAX)9/17/98 1/21/99 3/5/99 4/12/99 10/21/99 4/11/00 10/26/00 4/23/01 11/9/01 5/23/02 10/23/02 5/16/03 10/22/03 4/27/04 10/11/04 5/5/05 10/18/05 5/2/06 10/18/06 Antimony, total 1 12.5 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <10 <10 Arsenic, total 10 18.6 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Barium, total 700 942 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <20 <20 Beryllium, total 4 13.7 <2 <2 5 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <1 <1 Cadmium, total 2 28.4 <1 2 1.7 <1 <1 <1 <1 <1 <1 <1 4 <1 <1 <1 <1 <1 <1 <1 <1 Chromium, total 10 300 <10 <10 36 <10 36 <10 <10 <10 107 30 <10 15 <10 <10 <10 <10 <10 <10 <10 Cobalt, total 1 58.2 <10 10 20 <10 19 <10 <10 <10 41 21 <10 <10 <10 <10 <10 <10 <10 <10 <10 Copper, total 1000 456 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <10 <10 Lead, total 15 92.9 <10 <10 10 <10 <10 <10 <10 <10 37 16 <10 10 <10 <10 <10 <10 <10 <10 <10 Nickel, total 100 90.5 <50 <50 <50 <50 <50 <50 <50 <50 51 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 Selenium, total 20 17.8 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <10 <10 Silver, total 20 1.2 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Thallium, total 0.28 10.5 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 10 <10 <10 <10 Vanadium, total 3.5 249 <40 <40 <40 <40 <40 <40 <40 <40 124 53 <40 <40 <40 <40 <40 <40 <40 <10 <10 Zinc, total 1000 806 <50 76 75 <50 160 <50 <50 <50 310 99 <50 57 <50 <50 <50 <50 <50 <10 <10 5/8/07 10/23/07 5/7/08 10/28/08 5/11/09 10/19/09 5/17/10 10/18/10 5/23/11 10/11/11 5/29/12 10/25/12 5/31/13 11/1/13 5/26/14 10/21/14 5/29/15 11/23/15 6/15/16 11/30/16 Antimony, total 1 <0.58 <0.68 <0.68 12.5 9.8 <2.6 3.8 2.8 <2.6 <5 <5 <5 <5 <5 <5 <5 <3.8 <3.8 <3.8 <3.8 Arsenic, total 10 <2 <2 <2 5.6 10 3.5 5 7.5 18.6 5.3 <5 <5 <10 <5 <5 <5 <2.5 3.5 <2.5 <2.5 Barium, total 700 53.1 62 228 326 551 184 149 303 942 174 65.1 136 38.1 58.7 80.3 67.5 55.1 107 66.7 52.8 Beryllium, total 4 <0.7 <0.7 1.3 3.3 7.9 3.1 2 4.5 13.7 2.7 <1 1.7 <1 1 <1 <1 0.68 1.2 0.63 0.58 Cadmium, total 2 3.5 <0.5 <0.5 <0.5 15.7 <0.5 <0.5 0.78 28.4 <1 <1 <1 <1 <1 <1 <1 1 0.92 <0.5 1.7 Chromium, total 10 <2 18 54.3 85.8 196 42.2 43.7 92.8 300 53.4 14.3 33.7 7.1 7.5 15.1 11.7 10.6 25.2 13.7 9.6 Cobalt, total 1 18.2 3.2 9.1 <0.6 43.6 16.7 23 58.2 25 9.8 15.8 11.1 19.1 27.7 14.4 11.9 9.2 14.5 12 8.3Copper, total 1000 <0.6 12.2 36.4 90.9 262 95.8 44 94.5 456 63.9 14.6 39 8.7 18 18.4 19.3 20.7 33.8 15.9 17.3 Lead, total 15 <2 3.8 15.9 11.7 48.3 18.6 13.3 28.3 92.9 12.7 <5 8.7 <5 <5 <5 <5 4.6 8.2 <2.5 3.6 Nickel, total 100 19.7 8.8 19.4 30.4 83.2 29 18.4 38.7 90.5 15.5 8.4 30.5 14.1 29.1 26.2 24 17.6 21.2 20.8 16.2 Selenium, total 20 <2 <2 <2 17.8 6.8 <3.8 <3.8 5.9 9.6 <10 <10 <10 <10 <10 <10 <10 <5 <5 <5 <5 Silver, total 20 <2 <2 <2 <0.1 0.41 0.17 0.14 <0.1 1.2 <5 <5 <5 <5 <5 <5 <5 <2.5 <2.5 <2.5 <2.5 Thallium, total 0.28 0.227 0.302 1.07 10.5 6.3 <3 <3 <3 <3 <5.4 <5.4 <5.4 <5.5 <5.4 <5.4 <5.4 <5 <5 <5 <5 Vanadium, total 3.5 <1 11.2 42.5 89.4 147 34 37.1 85.8 249 44.1 15 29.9 6.8 8.6 14.2 11.3 9 22.1 9.8 7.9 Zinc, total 1000 29 49.6 168 240 516 135 115 235 806 127 44.5 117 35.4 54.1 65.4 59.6 36.4 75.3 55.9 45.3 Parameter Name 2L/GWP Std MW-1 Parameter Name 2L/GWP Std MW-1 Shaded = Above 2L/GWP Standard < = ND relative to MDL Surry County Landfill (Mt. Airy)Page 3 of 6 Table 2 Metal Detections (Represents Background) BL MAX 9/17/98 1/21/99 3/5/99 4/12/99 BL MAX 9/17/98 1/21/99 3/5/99 4/12/99 BL MAX 9/17/98 1/21/99 3/5/99 4/12/99 BL MAX 9/17/98 1/21/99 3/5/99 4/12/99 Antimony, total 1 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 Arsenic, total 10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Barium, total 700 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 1860 1860 <500 <500 <500 <500 <500 <500 <500 <500 Beryllium, total 4 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 26 26 2 <2 5 <2 <2 <2 <2 <2 Cadmium, total 2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 9 9 <1 2 <1 13 <1 13 2 <1 Chromium, total 10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 146 146 <10 10 41 <10 <10 <10 <10 <10 Cobalt, total 1 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 164 164 44 14 39 <10 <10 <10 <10 <10 Copper, total 1000 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 Lead, total 15 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 110 110 16 11 <10 <10 <10 <10 <10 <10 Nickel, total 100 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 80 80 <50 <50 <50 159 <50 159 <50 <50 Selenium, total 20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 Silver, total 20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Thallium, total 0.28 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Vanadium, total 3.5 <40 <40 <40 <40 <40 <40 <40 <40 <40 <40 215 215 <40 <40 52 <40 <40 <40 <40 <40 Zinc, total 1000 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 615 615 76 <50 <50 67 58 67 <50 <50 MW-6/6R MW-6R BL MAX 9/17/98 1/21/99 3/5/99 4/12/99 BL MAX 9/17/98 1/21/99 3/5/99 4/12/99 BL MAX 9/17/98 1/21/99 3/5/99 4/12/99 BL MAX 9/8/09 10/27/09 1/28/10 3/8/10 Antimony, total 1 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <2.6 <2.6 <2.6 <13 <5.2 Arsenic, total 10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 15 <2.7 <2.7 15 14.1 Barium, total 700 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 2000 85 162 2000 1340 Beryllium, total 4 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 9.8 0.3 0.33 9.8 6 Cadmium, total 2 4 <1 4 2 <1 2 2 <1 2 <1 1 <1 <1 1 <1 <0.5 <0.5 <0.5 <2.5 <1 Chromium, total 10 29 29 <10 15 <10 16 16 <10 <10 <10 0 <10 <10 <10 <10 154 14.8 2.9 154 65.8 Cobalt, total 1 15 15 <10 <10 <10 18 18 <10 <10 <10 11 11 <10 10 <10 87.5 2.5 3.9 87.5 42.2 Copper, total 1000 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 108 4 3.3 108 51.4 Lead, total 15 <10 <10 <10 <10 <10 17 17 <10 <10 <10 <10 <10 <10 <10 <10 44.5 --<4 44.5 27.4 Nickel, total 100 99 <50 99 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 99.5 4.6 3.9 99.5 43.8 Selenium, total 20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <3.8 <3.8 <3.8 <19 <7.6 Silver, total 20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <0.1 <0.1 <0.1 <0.5 <0.2 Thallium, total 0.28 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 5.4 5.4 <3 <15 <6 Vanadium, total 3.5 42 42 <40 <40 <40 <40 <40 <40 <40 <40 <40 <40 <40 <40 <40 256 6.9 5.6 256 121 Zinc, total 1000 107 <50 107 <50 <50 93 93 <50 <50 <50 61 61 <50 <50 <50 720 14.5 7.8 720 161 MW-4D MW-7Parameter Name 2L/GWP Std MW-8 Parameter Name 2L/GWP Std MW-2 MW-3 MW-4S MW-5 MW-6 Shaded = Above 2L/GWP Standard < = ND relative to MDL Surry County Landfill (Mt. Airy)Page 4 of 6 Table 2 Metal Detections (Represents Background) BL MAX 9/4/09 10/27/09 1/28/10 3/8/10 BL MAX 9/4/09 10/27/09 1/28/10 3/8/10 BL MAX 9/8/09 10/27/09 1/28/10 3/8/10 BL MAX 9/8/09 10/27/09 1/28/10 3/8/10 Antimony, total 1 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 Arsenic, total 10 4.7 <2.7 <2.7 4.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 5.6 <2.7 <2.7 <2.7 5.6 Barium, total 700 313 62.9 96.6 313 53.7 116 78 109 40.7 116 150 150 117 106 87.8 182 98.4 68.7 59.1 182 Beryllium, total 4 1.4 <0.1 0.23 1.4 <0.1 0.46 <0.1 0.26 <0.1 0.46 0.97 0.97 0.58 0.48 0.33 2.4 1.6 1.1 0.46 2.4 Cadmium, total 2 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Chromium, total 10 39.7 3.2 8.4 39.7 6.2 21.9 10.7 21.9 2 10.8 25.2 25.2 19.7 15 10.8 27.5 15.7 12.1 11.2 27.5 Cobalt, total 1 10.4 3.7 5.4 10.4 3 7.3 2.8 5 <0.6 7.3 8.8 8.4 8.8 3.9 6.8 23 13.3 7.6 5.4 23Copper, total 1000 19.2 0.41 2.8 19.2 2.8 10.1 4 10.1 1.1 5 18.9 18.9 12.4 11.9 7 26.3 15.7 12.3 8 26.3 Lead, total 15 12.2 <4 <4 12.2 <4 <4 <4 <4 <4 <4 7.3 5.4 6.2 7.3 <4 17.6 7.1 7.3 4.5 17.6 Nickel, total 100 21 4.4 6.2 21 4.7 27.4 13.9 27.4 4.6 5.9 22.4 22.4 19 10.8 8.8 21.4 17.1 11.6 8.6 21.4 Selenium, total 20 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 Silver, total 20 0.46 0.36 0.22 0.46 <0.1 0.41 0.22 0.41 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0.12 <0.1 <0.1 <0.1 0.12 Thallium, total 0.28 4.4 4.4 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 Vanadium, total 3.5 57.9 4.8 12.4 57.9 7.4 20.3 11.3 20.3 2.5 15.6 34.6 34.6 28.9 22.4 15.6 40.5 23.2 17.8 15 40.5 Zinc, total 1000 105 8.6 25.2 105 13.2 45.9 22.3 45.9 3.5 26.1 92.2 92.2 50.7 31.7 26.7 67.7 41.3 37.3 27.3 67.7 BL MAX 10/27/09 1/28/10 3/8/10 BL MAX 9/8/09 10/27/09 1/28/10 3/8/10 BL MAX 9/8/09 10/27/09 1/28/10 3/8/10 Antimony, total 1 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 Arsenic, total 10 6.3 2.8 4.2 6.3 <2.7 <2.7 <2.7 <2.7 <2.7 4.4 <2.7 <2.7 <2.7 4.4 Barium, total 700 119 90.7 90.9 119 155 131 82.3 60.6 155 114 39.2 40.7 56.1 114 Beryllium, total 4 0.79 0.34 0.14 0.79 0.77 0.38 0.14 <0.1 0.77 3.3 0.4 0.43 0.58 3.3 Cadmium, total 2 <0.5 <0.5 <0.5 <0.5 2.5 <0.5 0.68 <0.5 2.5 <0.5 <0.5 <0.5 <0.5 <0.5 Chromium, total 10 26.9 6.2 18.4 26.9 22.4 16.1 8.4 6 22.4 16.1 2.8 4 6 16.1 Cobalt, total 1 14.6 6.8 7.5 14.6 13.3 7.2 3.4 2.2 13.3 19 2.1 2.6 3.2 19 Copper, total 1000 21.9 7.9 15.9 21.9 25.2 12.3 7.1 6.4 25.2 20.8 2.5 2.8 4.5 20.8 Lead, total 15 8 <4 <4 8 8.2 <4 <4 <4 8.2 10.5 <4 <4 <4 10.5 Nickel, total 100 20.8 17.1 15.7 20.8 19.5 14.7 11.6 7.1 19.5 14.8 3.2 3.5 5 14.8 Selenium, total 20 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 Silver, total 20 0.24 0.24 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 Thallium, total 0.28 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 Vanadium, total 3.5 35.3 9.2 21.1 35.3 31.2 21.1 11.4 8.9 31.2 22.7 4.2 5.3 7.9 22.7 Zinc, total 1000 69.7 48.5 36.3 69.7 47.6 30.9 27.8 13.9 47.6 59.7 19.2 20.6 22.2 59.7 MW-12 MW-13Parameter Name 2L/GWP Std MW-11D MW-11SParameter Name 2L/GWP Std MW-9S MW-9D MW-10 Shaded = Above 2L/GWP Standard < = ND relative to MDL Surry County Landfill (Mt. Airy)Page 5 of 6 Table 2 Metal Detections (Leachate) LAGOON MAX (ALL 11/9/01 10/23/02 5/16/03 10/22/03 10/11/04 5/5/05 10/18/05 5/3/06 10/20/06 5/11/07 10/29/07 5/9/08 10/30/08 5/12/09 10/19/09 5/19/10 10/22/10 5/23/11 10/11/11 Antimony, total 1 10 <30 <30 <30 <30 <30 <30 <30 <10 <10 <0.58 <0.68 <0.68 10 <2.6 <2.6 <2.6 <2.6 <2.6 <5 Arsenic, total 10 8.2 <10 <10 <10 <10 <10 <10 <10 <10 <10 <2 <2 <2 <2.7 3 <2.7 <2.7 8.2 <2.7 <5 Barium, total 700 847 <500 <500 <500 <500 <500 <500 <0.5 <20 <20 17.3 16.8 36.7 209 44.4 34.4 392 847 84.2 133 Beryllium, total 4 <2 <2 <2 <2 <2 <2 <2 <2 <1 <1 <0.7 <0.7 <0.7 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <1 Cadmium, total 2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 Chromium, total 10 13.3 <10 <10 <10 <10 <10 <10 <10 <10 <10 <2 <2 <2 <0.4 0.65 <0.4 1.2 <0.4 3.3 5.6 Cobalt, total 1 137 <10 <10 17 21 <10 36 <10 <10 <10 <2 3.5 11 12.2 13.9 6.7 104 137 16.8 18.4 Copper, total 1000 5.9 <200 <200 <200 <200 <200 <200 <200 <10 <10 <0.6 <0.6 <0.6 <0.3 4.3 <0.3 <0.3 <0.3 3.6 5.9 Lead, total 15 6.1 <10 <10 <10 <10 <10 <10 <10 <10 <10 <2 <2 <2 <4 <4 <4 <4 <4 <4 <5 Nickel, total 100 21.7 <50 <50 <50 <50 <50 <50 <50 <50 <50 <2 5.6 6 8.9 7.2 3.5 11.3 12.5 4.6 9.6 Selenium, total 20 13.4 <20 <20 <20 <20 <20 <20 <20 <10 <10 <2 <2 <2 13.4 <3.8 <3.8 <3.8 <3.8 <3.8 <10 Silver, total 20 4.7 <10 <10 <10 <10 <10 <10 <10 <10 <10 <2 <2 <2 2.4 0.92 0.49 <0.1 <0.1 <0.1 <5 Thallium, total 0.28 57 <10 <10 <10 <10 <10 57 0.016 <10 <10 <0.04 <0.036 <0.03 4.9 <3 <3 7.7 9.2 <3 <5.4 Vanadium, total 3.5 21 <40 <40 <40 <40 <40 <40 <40 <10 <10 <1 <1 <1 <0.2 0.23 0.5 <0.2 <0.2 6.1 9.5 Zinc, total 1000 31.1 <50 <50 <50 <50 <50 <50 <50 <10 <10 <1 <1 1.6 <0.4 6.9 4.3 9.9 <0.4 13.2 31.1 5/29/12 10/25/12 5/30/13 10/31/13 5/27/14 10/23/14 5/28/15 11/24/15 6/15/16 12/1/16 Antimony, total 1 <5 <5 <5 <5 <5 <5 <3.8 4.3 4.8 4.5 Arsenic, total 10 <5 <5 <10 <5 <5 <5 <2.5 <2.5 <2.5 <2.5 Barium, total 700 91.2 64.8 104 106 87.1 83.7 179 108 189 154 Beryllium, total 4 <1 <1 <1 <1 <1 <1 <0.5 <0.5 <0.5 <0.5 Cadmium, total 2 <1 <1 <1 <1 <1 <1 <0.5 <0.5 <0.5 <0.5 Chromium, total 10 <5 <5 <5 <5 <5 <5 3.8 <2.5 13.3 <2.5 Cobalt, total 1 69.8 6.9 53.1 22.6 14.6 10.4 9 13.3 9.9 6.4 Copper, total 1000 <5 <5 <5 <5 <5 <5 <2.5 2.6 <2.5 3.2 Lead, total 15 <5 <5 <5 <5 <5 <5 4.7 4.3 6.1 <2.5 Nickel, total 100 <5 <5 <5 <5 14.4 <5 3.3 11.7 4.9 21.7 Selenium, total 20 <10 <10 11.3 <10 12.8 <10 <5 <5 <5 <5 Silver, total 20 <5 <5 <5 <5 <5 <5 4.7 <2.5 <2.5 <2.5 Thallium, total 0.28 <5.4 <5.4 <5.5 <5.4 <5.4 <5.4 6.9 5.5 8.9 <5 Vanadium, total 3.5 <5 <5 <5 <5 <5 <5 21 <2.5 <2.5 <2.5 Zinc, total 1000 <10 13.1 <10 30.7 <10 <10 6.5 <5 <5 7.4 Parameter Name 2L/GWP Std LAGOON Parameter Name 2L/GWP Std LAGOON Shaded = Above 2L/GWP Standard < = ND relative to MDL Surry County Landfill (Mt. Airy)Page 6 of 6 Sheets P. O . B O X 9 7 G A R N E R , N . C . 2 7 5 2 9 (9 1 9 ) 7 7 2 - 5 3 9 3 (8 2 8 ) 2 6 2 - 1 7 6 7 P. O . B O X 3 4 9 B O O N E , N . C . 2 8 6 0 7 LI C E N S E N U M B E R : C - 0 2 8 1 P. O . B O X 9 7 G A R N E R , N . C . 2 7 5 2 9 (9 1 9 ) 7 7 2 - 5 3 9 3 (8 2 8 ) 2 6 2 - 1 7 6 7 P. O . B O X 3 4 9 B O O N E , N . C . 2 8 6 0 7 LI C E N S E N U M B E R : C - 0 2 8 1 Appendix A Statistical Analyses Results Non-Parametric Upper Tolerance Limit Pooled Background Well (MW-1) All Events & Other Wells Baseline Events Original Data (Not Transformed) Surry County Lined Landfill (Mount Airy) Antimony, total Non-Detects Replaced with 0 Page 1 Non-Parametric Tolerance Interval Parameter: Antimony, total Original Data (Not Transformed) Non-Detects Replaced with 0 Total Percent Non-Detects = 95.8763% Background measurements (n) = 97 Maximum Background Concentration = 12.5 Minimum Coverage = 97% Average Coverage = 98.9796% Location Date Value Significant Original Data (Not Transformed) Surry County Lined Landfill (Mount Airy) Arsenic, total Non-Detects Replaced with 0 Page 2 Non-Parametric Tolerance Interval Parameter: Arsenic, total Original Data (Not Transformed) Non-Detects Replaced with 0 Total Percent Non-Detects = 83.5052% Background measurements (n) = 97 Maximum Background Concentration = 18.6 Minimum Coverage = 97% Average Coverage = 98.9796% Location Date Value Significant Original Data (Not Transformed) Surry County Lined Landfill (Mount Airy) Barium, total Non-Detects Replaced with 0 Page 3 Non-Parametric Tolerance Interval Parameter: Barium, total Original Data (Not Transformed) Non-Detects Replaced with 0 Total Percent Non-Detects = 46.3918% Background measurements (n) = 97 Maximum Background Concentration = 2000 Minimum Coverage = 97% Average Coverage = 98.9796% Location Date Value Significant Original Data (Not Transformed) Surry County Lined Landfill (Mount Airy) Beryllium, total Non-Detects Replaced with 0 Page 4 Non-Parametric Tolerance Interval Parameter: Beryllium, total Original Data (Not Transformed) Non-Detects Replaced with 0 Total Percent Non-Detects = 54.6392% Background measurements (n) = 97 Maximum Background Concentration = 26 Minimum Coverage = 97% Average Coverage = 98.9796% Location Date Value Significant Original Data (Not Transformed) Surry County Lined Landfill (Mount Airy) Chromium, total Non-Detects Replaced with 0 Page 5 Non-Parametric Tolerance Interval Parameter: Chromium, total Original Data (Not Transformed) Non-Detects Replaced with 0 Total Percent Non-Detects = 37.1134% Background measurements (n) = 97 Maximum Background Concentration = 300 Minimum Coverage = 97% Average Coverage = 98.9796% Location Date Value Significant Original Data (Not Transformed) Surry County Lined Landfill (Mount Airy) Cobalt, total Non-Detects Replaced with 0 Page 6 Non-Parametric Tolerance Interval Parameter: Cobalt, total Original Data (Not Transformed) Non-Detects Replaced with 0 Total Percent Non-Detects = 36.0825% Background measurements (n) = 97 Maximum Background Concentration = 164 Minimum Coverage = 97% Average Coverage = 98.9796% Location Date Value Significant Original Data (Not Transformed) Surry County Lined Landfill (Mount Airy) Lead, total Non-Detects Replaced with 0 Page 7 Non-Parametric Tolerance Interval Parameter: Lead, total Original Data (Not Transformed) Non-Detects Replaced with 0 Total Percent Non-Detects = 64.5833% Background measurements (n) = 96 Maximum Background Concentration = 110 Minimum Coverage = 97% Average Coverage = 98.9691% Location Date Value Significant Original Data (Not Transformed) Surry County Lined Landfill (Mount Airy) Thallium, total Non-Detects Replaced with 0 Page 8 Non-Parametric Tolerance Interval Parameter: Thallium, total Original Data (Not Transformed) Non-Detects Replaced with 0 Total Percent Non-Detects = 91.7526% Background measurements (n) = 97 Maximum Background Concentration = 10.5 Minimum Coverage = 97% Average Coverage = 98.9796% Location Date Value Significant Original Data (Not Transformed) Surry County Lined Landfill (Mount Airy) Vanadium, total Non-Detects Replaced with 0 Page 9 Non-Parametric Tolerance Interval Parameter: Vanadium, total Original Data (Not Transformed) Non-Detects Replaced with 0 Total Percent Non-Detects = 43.299% Background measurements (n) = 97 Maximum Background Concentration = 256 Minimum Coverage = 97% Average Coverage = 98.9796% Location Date Value Significant Appendix B Laboratory Analysis Reports September 1998 January 1999 January 2010 October 2010 May 2011 November 10, 2008 LIMS USE: FR - JONATHAN PFOHL LIMS OBJECT ID: 9231169 9231169 Project: Pace Project No.: RE: Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 SURRY CO. SUBTITLE DLF Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on October 30, 2008. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Renee Spencer for Bonnie McKee bonnie.mckee@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Charlotte Certification IDsConnecticut Certification Number: PH-0104Pennsylvania Certification Number: 68-00784 West Virginia Certification Number: 357Virginia Certification Number: 00213Tennessee Certification Number: 04010South Carolina Drinking Water Cert. Number: 990060003South Carolina Certification Number: 990060001 North Carolina Field Services Certification Number: 5342North Carolina Wastewater Certification Number: 12 North Carolina Drinking Water Certification Number: 37706Louisiana/LELAP Certification Number: 04034Kentucky UST Certification Number: 84New Jersey Certification Number: NC012Florida/NELAP Certification Number: E87627 Asheville Certification IDs Connecticut Certification Number: PH-0106 Massachusetts Certification Number: M-NC030West Virginia Certification Number: 356Virginia Certification Number: 00072 Tennessee Certification Number: 2980South Carolina Bioassay Certification Number: 99030002 South Carolina Certification Number: 99030001 Pennsylvania Certification Number: 68-03578 North Carolina Bioassay Certification Number: 9North Carolina Wastewater Certification Number: 40North Carolina Drinking Water Certification Number: 37712 New Jersey Certification Number: NC011Louisiana/LELAP Certification Number: 03095 Florida/NELAP Certification Number: E87648 Eden Certification IDs Virginia Drinking Water Certification Number: 00424 North Carolina Wastewater Certification Number: 633 North Carolina Drinking Water Certification Number: 37738 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Lab ID Sample ID Matrix Date Collected Date Received 9231169001 MW-2 Water 10/27/08 11:30 10/30/08 15:00 9231169002 MW-3R Water 10/27/08 12:00 10/30/08 15:00 9231169003 MW-4D Water 10/27/08 13:00 10/30/08 15:00 9231169004 MW-4S Water 10/27/08 13:35 10/30/08 15:00 9231169005 MW-5 Water 10/27/08 14:05 10/30/08 15:00 9231169006 MW-6R Water 10/27/08 15:00 10/30/08 15:00 9231169007 MW-1 Water 10/28/08 08:30 10/30/08 15:00 9231169008 SWN-2 Water 10/28/08 09:00 10/30/08 15:00 9231169009 SWN-1 Water 10/28/08 09:35 10/30/08 15:00 9231169010 LAGOON Water 10/30/08 07:30 10/30/08 15:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 9231169001 MW-2 EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK 9231169002 MW-3R EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK 9231169003 MW-4D EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK 9231169004 MW-4S EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK 9231169005 MW-5 EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK 9231169006 MW-6R EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK 9231169007 MW-1 EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK 9231169008 SWN-2 EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK 9231169009 SWN-1 EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK 9231169010 LAGOON ASTM D516-90 1 PASI-ALEP EPA 353.2 3 PASI-ADMN EPA 365.1 1 PASI-AJDA EPA 6010 GW North Carolina 15 PASI-AJMW EPA 8260 54 PASI-CMCK EPA 9040 1 PASI-ALEP SM 2540D 1 PASI-ATEE SM 5210B 1 PASI-ALEP SM 5220D 1 PASI-ATEE REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-2 Lab ID:9231169001 Collected:10/27/08 11:30 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony ND ug/L 6.0 1 11/05/08 03:58 7440-36-011/03/08 14:152.6 Arsenic ND ug/L 10.0 1 11/05/08 03:58 7440-38-211/03/08 14:152.7 Barium 32.2J ug/L 100 1 11/05/08 03:58 7440-39-311/03/08 14:150.20 Beryllium ND ug/L 1.0 1 11/05/08 03:58 7440-41-711/03/08 14:150.10 Cadmium ND ug/L 1.0 1 11/05/08 03:58 7440-43-911/03/08 14:150.50 Chromium ND ug/L 10.0 1 11/05/08 03:58 7440-47-311/03/08 14:150.40 Cobalt 2.9J ug/L 10.0 1 11/05/08 03:58 7440-48-4 Z211/03/08 14:150.60 Copper 0.38J ug/L 10.0 1 11/05/08 03:58 7440-50-811/03/08 14:150.30 Lead ND ug/L 10.0 1 11/05/08 03:58 7439-92-111/03/08 14:154.0 Nickel ND ug/L 50.0 1 11/05/08 03:58 7440-02-011/03/08 14:151.7 Selenium ND ug/L 10.0 1 11/05/08 03:58 7782-49-211/03/08 14:153.8 Silver 0.11J ug/L 10.0 1 11/05/08 03:58 7440-22-411/03/08 14:150.10 Thallium 3.5J ug/L 5.5 1 11/05/08 03:58 7440-28-011/03/08 14:153.0 Vanadium 0.78J ug/L 25.0 1 11/05/08 03:58 7440-62-211/03/08 14:150.20 Zinc 2.0J ug/L 10.0 1 11/05/08 03:58 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 100 1 11/05/08 18:06 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/05/08 18:06 107-13-11.9 Benzene ND ug/L 1.0 1 11/05/08 18:06 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/05/08 18:06 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/05/08 18:06 75-27-40.18 Bromoform ND ug/L 3.0 1 11/05/08 18:06 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/05/08 18:06 74-83-90.29 2-Butanone (MEK)ND ug/L 100 1 11/05/08 18:06 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/05/08 18:06 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/05/08 18:06 56-23-50.25 Chlorobenzene ND ug/L 3.0 1 11/05/08 18:06 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/05/08 18:06 75-00-30.54 Chloroform ND ug/L 5.0 1 11/05/08 18:06 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/05/08 18:06 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/05/08 18:06 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/05/08 18:06 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/05/08 18:06 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/05/08 18:06 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/05/08 18:06 95-50-10.30 1,4-Dichlorobenzene ND ug/L 1.0 1 11/05/08 18:06 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/05/08 18:06 110-57-61.0 1,1-Dichloroethane 2.7J ug/L 5.0 1 11/05/08 18:06 75-34-30.32 1,2-Dichloroethane ND ug/L 1.0 1 11/05/08 18:06 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/05/08 18:06 75-35-40.56 cis-1,2-Dichloroethene 0.72J ug/L 5.0 1 11/05/08 18:06 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/05/08 18:06 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/05/08 18:06 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/05/08 18:06 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/05/08 18:06 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 5 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-2 Lab ID:9231169001 Collected:10/27/08 11:30 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/05/08 18:06 10061-02-60.26 Ethylbenzene ND ug/L 1.0 1 11/05/08 18:06 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/05/08 18:06 591-78-60.46 Iodomethane ND ug/L 10.0 1 11/05/08 18:06 74-88-40.32 Methylene Chloride ND ug/L 2.0 1 11/05/08 18:06 75-09-20.97 4-Methyl-2-pentanone (MIBK)ND ug/L 100 1 11/05/08 18:06 108-10-10.33 Styrene ND ug/L 1.0 1 11/05/08 18:06 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/05/08 18:06 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/05/08 18:06 79-34-50.40 Tetrachloroethene 0.93J ug/L 1.0 1 11/05/08 18:06 127-18-40.46 Toluene ND ug/L 1.0 1 11/05/08 18:06 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/05/08 18:06 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/05/08 18:06 79-00-50.29 Trichloroethene ND ug/L 1.0 1 11/05/08 18:06 79-01-60.47 Trichlorofluoromethane 0.68J ug/L 1.0 1 11/05/08 18:06 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/05/08 18:06 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/05/08 18:06 108-05-40.35 Vinyl chloride ND ug/L 1.0 1 11/05/08 18:06 75-01-40.62 Xylene (Total)ND ug/L 5.0 1 11/05/08 18:06 1330-20-70.66 m&p-Xylene ND ug/L 2.0 1 11/05/08 18:06 1330-20-70.66 o-Xylene ND ug/L 1.0 1 11/05/08 18:06 95-47-60.23 4-Bromofluorobenzene (S)99 %87-109 1 11/05/08 18:06 460-00-4 Dibromofluoromethane (S)103 %85-115 1 11/05/08 18:06 1868-53-7 1,2-Dichloroethane-d4 (S)106 %79-120 1 11/05/08 18:06 17060-07-0 Toluene-d8 (S)103 %70-120 1 11/05/08 18:06 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 6 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-3R Lab ID:9231169002 Collected:10/27/08 12:00 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony ND ug/L 6.0 1 11/05/08 04:06 7440-36-011/03/08 14:152.6 Arsenic 3.7J ug/L 10.0 1 11/05/08 04:06 7440-38-211/03/08 14:152.7 Barium 81.5J ug/L 100 1 11/05/08 04:06 7440-39-311/03/08 14:150.20 Beryllium 0.37J ug/L 1.0 1 11/05/08 04:06 7440-41-711/03/08 14:150.10 Cadmium ND ug/L 1.0 1 11/05/08 04:06 7440-43-911/03/08 14:150.50 Chromium 5.6J ug/L 10.0 1 11/05/08 04:06 7440-47-311/03/08 14:150.40 Cobalt 4.9J ug/L 10.0 1 11/05/08 04:06 7440-48-4 Z211/03/08 14:150.60 Copper 5.8J ug/L 10.0 1 11/05/08 04:06 7440-50-811/03/08 14:150.30 Lead ND ug/L 10.0 1 11/05/08 04:06 7439-92-111/03/08 14:154.0 Nickel 5.6J ug/L 50.0 1 11/05/08 04:06 7440-02-011/03/08 14:151.7 Selenium ND ug/L 10.0 1 11/05/08 04:06 7782-49-211/03/08 14:153.8 Silver 0.23J ug/L 10.0 1 11/05/08 04:06 7440-22-411/03/08 14:150.10 Thallium ND ug/L 5.5 1 11/05/08 04:06 7440-28-011/03/08 14:153.0 Vanadium 13.1J ug/L 25.0 1 11/05/08 04:06 7440-62-211/03/08 14:150.20 Zinc 13.2 ug/L 10.0 1 11/05/08 04:06 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 100 1 11/05/08 18:30 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/05/08 18:30 107-13-11.9 Benzene ND ug/L 1.0 1 11/05/08 18:30 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/05/08 18:30 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/05/08 18:30 75-27-40.18 Bromoform ND ug/L 3.0 1 11/05/08 18:30 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/05/08 18:30 74-83-90.29 2-Butanone (MEK)ND ug/L 100 1 11/05/08 18:30 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/05/08 18:30 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/05/08 18:30 56-23-50.25 Chlorobenzene ND ug/L 3.0 1 11/05/08 18:30 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/05/08 18:30 75-00-30.54 Chloroform ND ug/L 5.0 1 11/05/08 18:30 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/05/08 18:30 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/05/08 18:30 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/05/08 18:30 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/05/08 18:30 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/05/08 18:30 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/05/08 18:30 95-50-10.30 1,4-Dichlorobenzene ND ug/L 1.0 1 11/05/08 18:30 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/05/08 18:30 110-57-61.0 1,1-Dichloroethane 2.0J ug/L 5.0 1 11/05/08 18:30 75-34-30.32 1,2-Dichloroethane ND ug/L 1.0 1 11/05/08 18:30 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/05/08 18:30 75-35-40.56 cis-1,2-Dichloroethene 1.1J ug/L 5.0 1 11/05/08 18:30 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/05/08 18:30 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/05/08 18:30 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/05/08 18:30 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/05/08 18:30 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 7 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-3R Lab ID:9231169002 Collected:10/27/08 12:00 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/05/08 18:30 10061-02-60.26 Ethylbenzene ND ug/L 1.0 1 11/05/08 18:30 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/05/08 18:30 591-78-60.46 Iodomethane ND ug/L 10.0 1 11/05/08 18:30 74-88-40.32 Methylene Chloride ND ug/L 2.0 1 11/05/08 18:30 75-09-20.97 4-Methyl-2-pentanone (MIBK)ND ug/L 100 1 11/05/08 18:30 108-10-10.33 Styrene ND ug/L 1.0 1 11/05/08 18:30 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/05/08 18:30 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/05/08 18:30 79-34-50.40 Tetrachloroethene 0.62J ug/L 1.0 1 11/05/08 18:30 127-18-40.46 Toluene 0.41J ug/L 1.0 1 11/05/08 18:30 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/05/08 18:30 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/05/08 18:30 79-00-50.29 Trichloroethene ND ug/L 1.0 1 11/05/08 18:30 79-01-60.47 Trichlorofluoromethane ND ug/L 1.0 1 11/05/08 18:30 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/05/08 18:30 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/05/08 18:30 108-05-40.35 Vinyl chloride ND ug/L 1.0 1 11/05/08 18:30 75-01-40.62 Xylene (Total)ND ug/L 5.0 1 11/05/08 18:30 1330-20-70.66 m&p-Xylene ND ug/L 2.0 1 11/05/08 18:30 1330-20-70.66 o-Xylene ND ug/L 1.0 1 11/05/08 18:30 95-47-60.23 4-Bromofluorobenzene (S)99 %87-109 1 11/05/08 18:30 460-00-4 Dibromofluoromethane (S)103 %85-115 1 11/05/08 18:30 1868-53-7 1,2-Dichloroethane-d4 (S)106 %79-120 1 11/05/08 18:30 17060-07-0 Toluene-d8 (S)102 %70-120 1 11/05/08 18:30 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 8 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-4D Lab ID:9231169003 Collected:10/27/08 13:00 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony ND ug/L 6.0 1 11/05/08 04:13 7440-36-011/03/08 14:152.6 Arsenic ND ug/L 10.0 1 11/05/08 04:13 7440-38-211/03/08 14:152.7 Barium 45.2J ug/L 100 1 11/05/08 04:13 7440-39-311/03/08 14:150.20 Beryllium ND ug/L 1.0 1 11/05/08 04:13 7440-41-711/03/08 14:150.10 Cadmium ND ug/L 1.0 1 11/05/08 04:13 7440-43-911/03/08 14:150.50 Chromium ND ug/L 10.0 1 11/05/08 04:13 7440-47-311/03/08 14:150.40 Cobalt ND ug/L 10.0 1 11/05/08 04:13 7440-48-411/03/08 14:150.60 Copper 4.1J ug/L 10.0 1 11/05/08 04:13 7440-50-811/03/08 14:150.30 Lead ND ug/L 10.0 1 11/05/08 04:13 7439-92-111/03/08 14:154.0 Nickel ND ug/L 50.0 1 11/05/08 04:13 7440-02-011/03/08 14:151.7 Selenium ND ug/L 10.0 1 11/05/08 04:13 7782-49-211/03/08 14:153.8 Silver 0.13J ug/L 10.0 1 11/05/08 04:13 7440-22-411/03/08 14:150.10 Thallium ND ug/L 5.5 1 11/05/08 04:13 7440-28-011/03/08 14:153.0 Vanadium ND ug/L 25.0 1 11/05/08 04:13 7440-62-211/03/08 14:150.20 Zinc 1.9J ug/L 10.0 1 11/05/08 04:13 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 100 1 11/06/08 18:11 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/06/08 18:11 107-13-11.9 Benzene ND ug/L 1.0 1 11/06/08 18:11 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/06/08 18:11 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/06/08 18:11 75-27-40.18 Bromoform ND ug/L 3.0 1 11/06/08 18:11 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/06/08 18:11 74-83-90.29 2-Butanone (MEK)ND ug/L 100 1 11/06/08 18:11 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/06/08 18:11 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/06/08 18:11 56-23-50.25 Chlorobenzene ND ug/L 3.0 1 11/06/08 18:11 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/06/08 18:11 75-00-30.54 Chloroform ND ug/L 5.0 1 11/06/08 18:11 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/06/08 18:11 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/06/08 18:11 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/06/08 18:11 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/06/08 18:11 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/06/08 18:11 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/06/08 18:11 95-50-10.30 1,4-Dichlorobenzene ND ug/L 1.0 1 11/06/08 18:11 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/06/08 18:11 110-57-61.0 1,1-Dichloroethane ND ug/L 5.0 1 11/06/08 18:11 75-34-30.32 1,2-Dichloroethane ND ug/L 1.0 1 11/06/08 18:11 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/06/08 18:11 75-35-40.56 cis-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 18:11 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 18:11 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/06/08 18:11 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/06/08 18:11 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 18:11 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 9 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-4D Lab ID:9231169003 Collected:10/27/08 13:00 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 18:11 10061-02-60.26 Ethylbenzene ND ug/L 1.0 1 11/06/08 18:11 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/06/08 18:11 591-78-60.46 Iodomethane ND ug/L 10.0 1 11/06/08 18:11 74-88-40.32 Methylene Chloride ND ug/L 2.0 1 11/06/08 18:11 75-09-20.97 4-Methyl-2-pentanone (MIBK)ND ug/L 100 1 11/06/08 18:11 108-10-10.33 Styrene ND ug/L 1.0 1 11/06/08 18:11 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/06/08 18:11 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/06/08 18:11 79-34-50.40 Tetrachloroethene ND ug/L 1.0 1 11/06/08 18:11 127-18-40.46 Toluene ND ug/L 1.0 1 11/06/08 18:11 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/06/08 18:11 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/06/08 18:11 79-00-50.29 Trichloroethene ND ug/L 1.0 1 11/06/08 18:11 79-01-60.47 Trichlorofluoromethane ND ug/L 1.0 1 11/06/08 18:11 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/06/08 18:11 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/06/08 18:11 108-05-40.35 Vinyl chloride ND ug/L 1.0 1 11/06/08 18:11 75-01-40.62 Xylene (Total)ND ug/L 5.0 1 11/06/08 18:11 1330-20-70.66 m&p-Xylene ND ug/L 2.0 1 11/06/08 18:11 1330-20-70.66 o-Xylene ND ug/L 1.0 1 11/06/08 18:11 95-47-60.23 4-Bromofluorobenzene (S)101 %87-109 1 11/06/08 18:11 460-00-4 Dibromofluoromethane (S)99 %85-115 1 11/06/08 18:11 1868-53-7 1,2-Dichloroethane-d4 (S)105 %79-120 1 11/06/08 18:11 17060-07-0 Toluene-d8 (S)101 %70-120 1 11/06/08 18:11 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 10 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-4S Lab ID:9231169004 Collected:10/27/08 13:35 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony ND ug/L 6.0 1 11/05/08 04:24 7440-36-011/03/08 14:152.6 Arsenic ND ug/L 10.0 1 11/05/08 04:24 7440-38-211/03/08 14:152.7 Barium 41.0J ug/L 100 1 11/05/08 04:24 7440-39-311/03/08 14:150.20 Beryllium ND ug/L 1.0 1 11/05/08 04:24 7440-41-711/03/08 14:150.10 Cadmium ND ug/L 1.0 1 11/05/08 04:24 7440-43-911/03/08 14:150.50 Chromium 0.77J ug/L 10.0 1 11/05/08 04:24 7440-47-311/03/08 14:150.40 Cobalt 3.3J ug/L 10.0 1 11/05/08 04:24 7440-48-4 Z211/03/08 14:150.60 Copper 0.66J ug/L 10.0 1 11/05/08 04:24 7440-50-811/03/08 14:150.30 Lead ND ug/L 10.0 1 11/05/08 04:24 7439-92-111/03/08 14:154.0 Nickel ND ug/L 50.0 1 11/05/08 04:24 7440-02-011/03/08 14:151.7 Selenium ND ug/L 10.0 1 11/05/08 04:24 7782-49-211/03/08 14:153.8 Silver ND ug/L 10.0 1 11/05/08 04:24 7440-22-411/03/08 14:150.10 Thallium ND ug/L 5.5 1 11/05/08 04:24 7440-28-011/03/08 14:153.0 Vanadium 0.76J ug/L 25.0 1 11/05/08 04:24 7440-62-211/03/08 14:150.20 Zinc 1.7J ug/L 10.0 1 11/05/08 04:24 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 100 1 11/06/08 18:27 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/06/08 18:27 107-13-11.9 Benzene ND ug/L 1.0 1 11/06/08 18:27 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/06/08 18:27 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/06/08 18:27 75-27-40.18 Bromoform ND ug/L 3.0 1 11/06/08 18:27 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/06/08 18:27 74-83-90.29 2-Butanone (MEK)ND ug/L 100 1 11/06/08 18:27 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/06/08 18:27 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/06/08 18:27 56-23-50.25 Chlorobenzene ND ug/L 3.0 1 11/06/08 18:27 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/06/08 18:27 75-00-30.54 Chloroform ND ug/L 5.0 1 11/06/08 18:27 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/06/08 18:27 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/06/08 18:27 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/06/08 18:27 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/06/08 18:27 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/06/08 18:27 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/06/08 18:27 95-50-10.30 1,4-Dichlorobenzene ND ug/L 1.0 1 11/06/08 18:27 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/06/08 18:27 110-57-61.0 1,1-Dichloroethane ND ug/L 5.0 1 11/06/08 18:27 75-34-30.32 1,2-Dichloroethane ND ug/L 1.0 1 11/06/08 18:27 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/06/08 18:27 75-35-40.56 cis-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 18:27 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 18:27 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/06/08 18:27 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/06/08 18:27 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 18:27 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 11 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-4S Lab ID:9231169004 Collected:10/27/08 13:35 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 18:27 10061-02-60.26 Ethylbenzene ND ug/L 1.0 1 11/06/08 18:27 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/06/08 18:27 591-78-60.46 Iodomethane ND ug/L 10.0 1 11/06/08 18:27 74-88-40.32 Methylene Chloride ND ug/L 2.0 1 11/06/08 18:27 75-09-20.97 4-Methyl-2-pentanone (MIBK)ND ug/L 100 1 11/06/08 18:27 108-10-10.33 Styrene ND ug/L 1.0 1 11/06/08 18:27 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/06/08 18:27 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/06/08 18:27 79-34-50.40 Tetrachloroethene ND ug/L 1.0 1 11/06/08 18:27 127-18-40.46 Toluene ND ug/L 1.0 1 11/06/08 18:27 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/06/08 18:27 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/06/08 18:27 79-00-50.29 Trichloroethene ND ug/L 1.0 1 11/06/08 18:27 79-01-60.47 Trichlorofluoromethane ND ug/L 1.0 1 11/06/08 18:27 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/06/08 18:27 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/06/08 18:27 108-05-40.35 Vinyl chloride ND ug/L 1.0 1 11/06/08 18:27 75-01-40.62 Xylene (Total)ND ug/L 5.0 1 11/06/08 18:27 1330-20-70.66 m&p-Xylene ND ug/L 2.0 1 11/06/08 18:27 1330-20-70.66 o-Xylene ND ug/L 1.0 1 11/06/08 18:27 95-47-60.23 4-Bromofluorobenzene (S)102 %87-109 1 11/06/08 18:27 460-00-4 Dibromofluoromethane (S)100 %85-115 1 11/06/08 18:27 1868-53-7 1,2-Dichloroethane-d4 (S)103 %79-120 1 11/06/08 18:27 17060-07-0 Toluene-d8 (S)100 %70-120 1 11/06/08 18:27 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 12 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-5 Lab ID:9231169005 Collected:10/27/08 14:05 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony ND ug/L 6.0 1 11/05/08 04:27 7440-36-011/03/08 14:152.6 Arsenic ND ug/L 10.0 1 11/05/08 04:27 7440-38-211/03/08 14:152.7 Barium 28.7J ug/L 100 1 11/05/08 04:27 7440-39-311/03/08 14:150.20 Beryllium ND ug/L 1.0 1 11/05/08 04:27 7440-41-711/03/08 14:150.10 Cadmium ND ug/L 1.0 1 11/05/08 04:27 7440-43-911/03/08 14:150.50 Chromium ND ug/L 10.0 1 11/05/08 04:27 7440-47-311/03/08 14:150.40 Cobalt 1.0J ug/L 10.0 1 11/05/08 04:27 7440-48-4 Z211/03/08 14:150.60 Copper ND ug/L 10.0 1 11/05/08 04:27 7440-50-811/03/08 14:150.30 Lead ND ug/L 10.0 1 11/05/08 04:27 7439-92-111/03/08 14:154.0 Nickel ND ug/L 50.0 1 11/05/08 04:27 7440-02-011/03/08 14:151.7 Selenium ND ug/L 10.0 1 11/05/08 04:27 7782-49-211/03/08 14:153.8 Silver ND ug/L 10.0 1 11/05/08 04:27 7440-22-411/03/08 14:150.10 Thallium ND ug/L 5.5 1 11/05/08 04:27 7440-28-011/03/08 14:153.0 Vanadium ND ug/L 25.0 1 11/05/08 04:27 7440-62-211/03/08 14:150.20 Zinc ND ug/L 10.0 1 11/05/08 04:27 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 100 1 11/06/08 18:43 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/06/08 18:43 107-13-11.9 Benzene ND ug/L 1.0 1 11/06/08 18:43 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/06/08 18:43 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/06/08 18:43 75-27-40.18 Bromoform ND ug/L 3.0 1 11/06/08 18:43 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/06/08 18:43 74-83-90.29 2-Butanone (MEK)ND ug/L 100 1 11/06/08 18:43 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/06/08 18:43 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/06/08 18:43 56-23-50.25 Chlorobenzene ND ug/L 3.0 1 11/06/08 18:43 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/06/08 18:43 75-00-30.54 Chloroform ND ug/L 5.0 1 11/06/08 18:43 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/06/08 18:43 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/06/08 18:43 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/06/08 18:43 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/06/08 18:43 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/06/08 18:43 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/06/08 18:43 95-50-10.30 1,4-Dichlorobenzene ND ug/L 1.0 1 11/06/08 18:43 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/06/08 18:43 110-57-61.0 1,1-Dichloroethane ND ug/L 5.0 1 11/06/08 18:43 75-34-30.32 1,2-Dichloroethane ND ug/L 1.0 1 11/06/08 18:43 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/06/08 18:43 75-35-40.56 cis-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 18:43 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 18:43 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/06/08 18:43 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/06/08 18:43 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 18:43 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 13 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-5 Lab ID:9231169005 Collected:10/27/08 14:05 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 18:43 10061-02-60.26 Ethylbenzene ND ug/L 1.0 1 11/06/08 18:43 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/06/08 18:43 591-78-60.46 Iodomethane ND ug/L 10.0 1 11/06/08 18:43 74-88-40.32 Methylene Chloride ND ug/L 2.0 1 11/06/08 18:43 75-09-20.97 4-Methyl-2-pentanone (MIBK)ND ug/L 100 1 11/06/08 18:43 108-10-10.33 Styrene ND ug/L 1.0 1 11/06/08 18:43 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/06/08 18:43 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/06/08 18:43 79-34-50.40 Tetrachloroethene ND ug/L 1.0 1 11/06/08 18:43 127-18-40.46 Toluene ND ug/L 1.0 1 11/06/08 18:43 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/06/08 18:43 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/06/08 18:43 79-00-50.29 Trichloroethene ND ug/L 1.0 1 11/06/08 18:43 79-01-60.47 Trichlorofluoromethane ND ug/L 1.0 1 11/06/08 18:43 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/06/08 18:43 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/06/08 18:43 108-05-40.35 Vinyl chloride ND ug/L 1.0 1 11/06/08 18:43 75-01-40.62 Xylene (Total)ND ug/L 5.0 1 11/06/08 18:43 1330-20-70.66 m&p-Xylene ND ug/L 2.0 1 11/06/08 18:43 1330-20-70.66 o-Xylene ND ug/L 1.0 1 11/06/08 18:43 95-47-60.23 4-Bromofluorobenzene (S)102 %87-109 1 11/06/08 18:43 460-00-4 Dibromofluoromethane (S)97 %85-115 1 11/06/08 18:43 1868-53-7 1,2-Dichloroethane-d4 (S)100 %79-120 1 11/06/08 18:43 17060-07-0 Toluene-d8 (S)100 %70-120 1 11/06/08 18:43 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 14 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-6R Lab ID:9231169006 Collected:10/27/08 15:00 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony ND ug/L 6.0 1 11/05/08 04:31 7440-36-011/03/08 14:152.6 Arsenic ND ug/L 10.0 1 11/05/08 04:31 7440-38-211/03/08 14:152.7 Barium 28.5J ug/L 100 1 11/05/08 04:31 7440-39-311/03/08 14:150.20 Beryllium ND ug/L 1.0 1 11/05/08 04:31 7440-41-711/03/08 14:150.10 Cadmium ND ug/L 1.0 1 11/05/08 04:31 7440-43-911/03/08 14:150.50 Chromium 0.81J ug/L 10.0 1 11/05/08 04:31 7440-47-311/03/08 14:150.40 Cobalt ND ug/L 10.0 1 11/05/08 04:31 7440-48-411/03/08 14:150.60 Copper 1.9J ug/L 10.0 1 11/05/08 04:31 7440-50-811/03/08 14:150.30 Lead ND ug/L 10.0 1 11/05/08 04:31 7439-92-111/03/08 14:154.0 Nickel 2.5J ug/L 50.0 1 11/05/08 04:31 7440-02-011/03/08 14:151.7 Selenium ND ug/L 10.0 1 11/05/08 04:31 7782-49-211/03/08 14:153.8 Silver ND ug/L 10.0 1 11/05/08 04:31 7440-22-411/03/08 14:150.10 Thallium ND ug/L 5.5 1 11/05/08 04:31 7440-28-011/03/08 14:153.0 Vanadium 1.7J ug/L 25.0 1 11/05/08 04:31 7440-62-211/03/08 14:150.20 Zinc 2.7J ug/L 10.0 1 11/05/08 04:31 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 100 1 11/06/08 19:00 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/06/08 19:00 107-13-11.9 Benzene ND ug/L 1.0 1 11/06/08 19:00 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/06/08 19:00 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/06/08 19:00 75-27-40.18 Bromoform ND ug/L 3.0 1 11/06/08 19:00 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/06/08 19:00 74-83-90.29 2-Butanone (MEK)ND ug/L 100 1 11/06/08 19:00 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/06/08 19:00 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/06/08 19:00 56-23-50.25 Chlorobenzene ND ug/L 3.0 1 11/06/08 19:00 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/06/08 19:00 75-00-30.54 Chloroform ND ug/L 5.0 1 11/06/08 19:00 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/06/08 19:00 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/06/08 19:00 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/06/08 19:00 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/06/08 19:00 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/06/08 19:00 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/06/08 19:00 95-50-10.30 1,4-Dichlorobenzene ND ug/L 1.0 1 11/06/08 19:00 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/06/08 19:00 110-57-61.0 1,1-Dichloroethane ND ug/L 5.0 1 11/06/08 19:00 75-34-30.32 1,2-Dichloroethane ND ug/L 1.0 1 11/06/08 19:00 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/06/08 19:00 75-35-40.56 cis-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 19:00 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 19:00 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/06/08 19:00 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/06/08 19:00 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 19:00 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 15 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-6R Lab ID:9231169006 Collected:10/27/08 15:00 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 19:00 10061-02-60.26 Ethylbenzene ND ug/L 1.0 1 11/06/08 19:00 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/06/08 19:00 591-78-60.46 Iodomethane ND ug/L 10.0 1 11/06/08 19:00 74-88-40.32 Methylene Chloride ND ug/L 2.0 1 11/06/08 19:00 75-09-20.97 4-Methyl-2-pentanone (MIBK)ND ug/L 100 1 11/06/08 19:00 108-10-10.33 Styrene ND ug/L 1.0 1 11/06/08 19:00 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/06/08 19:00 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/06/08 19:00 79-34-50.40 Tetrachloroethene ND ug/L 1.0 1 11/06/08 19:00 127-18-40.46 Toluene ND ug/L 1.0 1 11/06/08 19:00 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/06/08 19:00 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/06/08 19:00 79-00-50.29 Trichloroethene ND ug/L 1.0 1 11/06/08 19:00 79-01-60.47 Trichlorofluoromethane ND ug/L 1.0 1 11/06/08 19:00 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/06/08 19:00 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/06/08 19:00 108-05-40.35 Vinyl chloride ND ug/L 1.0 1 11/06/08 19:00 75-01-40.62 Xylene (Total)ND ug/L 5.0 1 11/06/08 19:00 1330-20-70.66 m&p-Xylene ND ug/L 2.0 1 11/06/08 19:00 1330-20-70.66 o-Xylene ND ug/L 1.0 1 11/06/08 19:00 95-47-60.23 4-Bromofluorobenzene (S)100 %87-109 1 11/06/08 19:00 460-00-4 Dibromofluoromethane (S)98 %85-115 1 11/06/08 19:00 1868-53-7 1,2-Dichloroethane-d4 (S)103 %79-120 1 11/06/08 19:00 17060-07-0 Toluene-d8 (S)101 %70-120 1 11/06/08 19:00 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 16 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-1 Lab ID:9231169007 Collected:10/28/08 08:30 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony 12.5 ug/L 6.0 1 11/05/08 04:35 7440-36-011/03/08 14:152.6 Arsenic 5.6J ug/L 10.0 1 11/05/08 04:35 7440-38-211/03/08 14:152.7 Barium 326 ug/L 100 1 11/05/08 04:35 7440-39-311/03/08 14:150.20 Beryllium 3.3 ug/L 1.0 1 11/05/08 04:35 7440-41-711/03/08 14:150.10 Cadmium ND ug/L 1.0 1 11/05/08 04:35 7440-43-911/03/08 14:150.50 Chromium 85.8 ug/L 10.0 1 11/05/08 04:35 7440-47-311/03/08 14:150.40 Cobalt ND ug/L 10.0 1 11/05/08 04:35 7440-48-411/03/08 14:150.60 Copper 90.9 ug/L 10.0 1 11/05/08 04:35 7440-50-811/03/08 14:150.30 Lead 11.7 ug/L 10.0 1 11/05/08 04:35 7439-92-111/03/08 14:154.0 Nickel 30.4J ug/L 50.0 1 11/05/08 04:35 7440-02-011/03/08 14:151.7 Selenium 17.8 ug/L 10.0 1 11/05/08 04:35 7782-49-211/03/08 14:153.8 Silver ND ug/L 10.0 1 11/05/08 04:35 7440-22-411/03/08 14:150.10 Thallium 10.5 ug/L 5.5 1 11/05/08 04:35 7440-28-011/03/08 14:153.0 Vanadium 89.4 ug/L 25.0 1 11/05/08 04:35 7440-62-211/03/08 14:150.20 Zinc 240 ug/L 10.0 1 11/05/08 04:35 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 100 1 11/06/08 19:17 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/06/08 19:17 107-13-11.9 Benzene ND ug/L 1.0 1 11/06/08 19:17 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/06/08 19:17 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/06/08 19:17 75-27-40.18 Bromoform ND ug/L 3.0 1 11/06/08 19:17 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/06/08 19:17 74-83-90.29 2-Butanone (MEK)ND ug/L 100 1 11/06/08 19:17 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/06/08 19:17 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/06/08 19:17 56-23-50.25 Chlorobenzene ND ug/L 3.0 1 11/06/08 19:17 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/06/08 19:17 75-00-30.54 Chloroform ND ug/L 5.0 1 11/06/08 19:17 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/06/08 19:17 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/06/08 19:17 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/06/08 19:17 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/06/08 19:17 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/06/08 19:17 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/06/08 19:17 95-50-10.30 1,4-Dichlorobenzene ND ug/L 1.0 1 11/06/08 19:17 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/06/08 19:17 110-57-61.0 1,1-Dichloroethane ND ug/L 5.0 1 11/06/08 19:17 75-34-30.32 1,2-Dichloroethane ND ug/L 1.0 1 11/06/08 19:17 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/06/08 19:17 75-35-40.56 cis-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 19:17 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 19:17 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/06/08 19:17 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/06/08 19:17 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 19:17 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 17 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:MW-1 Lab ID:9231169007 Collected:10/28/08 08:30 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 19:17 10061-02-60.26 Ethylbenzene ND ug/L 1.0 1 11/06/08 19:17 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/06/08 19:17 591-78-60.46 Iodomethane ND ug/L 10.0 1 11/06/08 19:17 74-88-40.32 Methylene Chloride ND ug/L 2.0 1 11/06/08 19:17 75-09-20.97 4-Methyl-2-pentanone (MIBK)ND ug/L 100 1 11/06/08 19:17 108-10-10.33 Styrene ND ug/L 1.0 1 11/06/08 19:17 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/06/08 19:17 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/06/08 19:17 79-34-50.40 Tetrachloroethene ND ug/L 1.0 1 11/06/08 19:17 127-18-40.46 Toluene ND ug/L 1.0 1 11/06/08 19:17 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/06/08 19:17 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/06/08 19:17 79-00-50.29 Trichloroethene ND ug/L 1.0 1 11/06/08 19:17 79-01-60.47 Trichlorofluoromethane ND ug/L 1.0 1 11/06/08 19:17 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/06/08 19:17 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/06/08 19:17 108-05-40.35 Vinyl chloride ND ug/L 1.0 1 11/06/08 19:17 75-01-40.62 Xylene (Total)ND ug/L 5.0 1 11/06/08 19:17 1330-20-70.66 m&p-Xylene ND ug/L 2.0 1 11/06/08 19:17 1330-20-70.66 o-Xylene ND ug/L 1.0 1 11/06/08 19:17 95-47-60.23 4-Bromofluorobenzene (S)101 %87-109 1 11/06/08 19:17 460-00-4 Dibromofluoromethane (S)100 %85-115 1 11/06/08 19:17 1868-53-7 1,2-Dichloroethane-d4 (S)105 %79-120 1 11/06/08 19:17 17060-07-0 Toluene-d8 (S)100 %70-120 1 11/06/08 19:17 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 18 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:SWN-2 Lab ID:9231169008 Collected:10/28/08 09:00 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony ND ug/L 6.0 1 11/05/08 04:40 7440-36-011/03/08 14:152.6 Arsenic ND ug/L 10.0 1 11/05/08 04:40 7440-38-211/03/08 14:152.7 Barium 14.8J ug/L 100 1 11/05/08 04:40 7440-39-311/03/08 14:150.20 Beryllium ND ug/L 1.0 1 11/05/08 04:40 7440-41-711/03/08 14:150.10 Cadmium ND ug/L 1.0 1 11/05/08 04:40 7440-43-911/03/08 14:150.50 Chromium ND ug/L 10.0 1 11/05/08 04:40 7440-47-311/03/08 14:150.40 Cobalt 2.4J ug/L 10.0 1 11/05/08 04:40 7440-48-4 Z211/03/08 14:150.60 Copper 0.96J ug/L 10.0 1 11/05/08 04:40 7440-50-811/03/08 14:150.30 Lead ND ug/L 10.0 1 11/05/08 04:40 7439-92-111/03/08 14:154.0 Nickel ND ug/L 50.0 1 11/05/08 04:40 7440-02-011/03/08 14:151.7 Selenium ND ug/L 10.0 1 11/05/08 04:40 7782-49-211/03/08 14:153.8 Silver ND ug/L 10.0 1 11/05/08 04:40 7440-22-411/03/08 14:150.10 Thallium ND ug/L 5.5 1 11/05/08 04:40 7440-28-011/03/08 14:153.0 Vanadium 0.27J ug/L 25.0 1 11/05/08 04:40 7440-62-211/03/08 14:150.20 Zinc 0.76J ug/L 10.0 1 11/05/08 04:40 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 100 1 11/06/08 19:33 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/06/08 19:33 107-13-11.9 Benzene ND ug/L 1.0 1 11/06/08 19:33 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/06/08 19:33 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/06/08 19:33 75-27-40.18 Bromoform ND ug/L 3.0 1 11/06/08 19:33 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/06/08 19:33 74-83-90.29 2-Butanone (MEK)ND ug/L 100 1 11/06/08 19:33 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/06/08 19:33 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/06/08 19:33 56-23-50.25 Chlorobenzene ND ug/L 3.0 1 11/06/08 19:33 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/06/08 19:33 75-00-30.54 Chloroform ND ug/L 5.0 1 11/06/08 19:33 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/06/08 19:33 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/06/08 19:33 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/06/08 19:33 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/06/08 19:33 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/06/08 19:33 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/06/08 19:33 95-50-10.30 1,4-Dichlorobenzene ND ug/L 1.0 1 11/06/08 19:33 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/06/08 19:33 110-57-61.0 1,1-Dichloroethane ND ug/L 5.0 1 11/06/08 19:33 75-34-30.32 1,2-Dichloroethane ND ug/L 1.0 1 11/06/08 19:33 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/06/08 19:33 75-35-40.56 cis-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 19:33 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/06/08 19:33 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/06/08 19:33 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/06/08 19:33 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 19:33 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 19 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:SWN-2 Lab ID:9231169008 Collected:10/28/08 09:00 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/06/08 19:33 10061-02-60.26 Ethylbenzene ND ug/L 1.0 1 11/06/08 19:33 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/06/08 19:33 591-78-60.46 Iodomethane ND ug/L 10.0 1 11/06/08 19:33 74-88-40.32 Methylene Chloride ND ug/L 2.0 1 11/06/08 19:33 75-09-20.97 4-Methyl-2-pentanone (MIBK)ND ug/L 100 1 11/06/08 19:33 108-10-10.33 Styrene ND ug/L 1.0 1 11/06/08 19:33 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/06/08 19:33 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/06/08 19:33 79-34-50.40 Tetrachloroethene ND ug/L 1.0 1 11/06/08 19:33 127-18-40.46 Toluene ND ug/L 1.0 1 11/06/08 19:33 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/06/08 19:33 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/06/08 19:33 79-00-50.29 Trichloroethene ND ug/L 1.0 1 11/06/08 19:33 79-01-60.47 Trichlorofluoromethane ND ug/L 1.0 1 11/06/08 19:33 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/06/08 19:33 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/06/08 19:33 108-05-40.35 Vinyl chloride ND ug/L 1.0 1 11/06/08 19:33 75-01-40.62 Xylene (Total)ND ug/L 5.0 1 11/06/08 19:33 1330-20-70.66 m&p-Xylene ND ug/L 2.0 1 11/06/08 19:33 1330-20-70.66 o-Xylene ND ug/L 1.0 1 11/06/08 19:33 95-47-60.23 4-Bromofluorobenzene (S)102 %87-109 1 11/06/08 19:33 460-00-4 Dibromofluoromethane (S)101 %85-115 1 11/06/08 19:33 1868-53-7 1,2-Dichloroethane-d4 (S)105 %79-120 1 11/06/08 19:33 17060-07-0 Toluene-d8 (S)100 %70-120 1 11/06/08 19:33 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 20 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:SWN-1 Lab ID:9231169009 Collected:10/28/08 09:35 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony ND ug/L 6.0 1 11/05/08 04:43 7440-36-011/03/08 14:152.6 Arsenic ND ug/L 10.0 1 11/05/08 04:43 7440-38-211/03/08 14:152.7 Barium 15.2J ug/L 100 1 11/05/08 04:43 7440-39-311/03/08 14:150.20 Beryllium ND ug/L 1.0 1 11/05/08 04:43 7440-41-711/03/08 14:150.10 Cadmium 1.1 ug/L 1.0 1 11/05/08 04:43 7440-43-911/03/08 14:150.50 Chromium ND ug/L 10.0 1 11/05/08 04:43 7440-47-311/03/08 14:150.40 Cobalt 2.7J ug/L 10.0 1 11/05/08 04:43 7440-48-4 Z211/03/08 14:150.60 Copper 1.6J ug/L 10.0 1 11/05/08 04:43 7440-50-811/03/08 14:150.30 Lead ND ug/L 10.0 1 11/05/08 04:43 7439-92-111/03/08 14:154.0 Nickel ND ug/L 50.0 1 11/05/08 04:43 7440-02-011/03/08 14:151.7 Selenium ND ug/L 10.0 1 11/05/08 04:43 7782-49-211/03/08 14:153.8 Silver 0.11J ug/L 10.0 1 11/05/08 04:43 7440-22-411/03/08 14:150.10 Thallium ND ug/L 5.5 1 11/05/08 04:43 7440-28-011/03/08 14:153.0 Vanadium 0.34J ug/L 25.0 1 11/05/08 04:43 7440-62-211/03/08 14:150.20 Zinc 8.4J ug/L 10.0 1 11/05/08 04:43 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 100 1 11/07/08 10:51 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/07/08 10:51 107-13-11.9 Benzene ND ug/L 1.0 1 11/07/08 10:51 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/07/08 10:51 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/07/08 10:51 75-27-40.18 Bromoform ND ug/L 3.0 1 11/07/08 10:51 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/07/08 10:51 74-83-90.29 2-Butanone (MEK)ND ug/L 100 1 11/07/08 10:51 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/07/08 10:51 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/07/08 10:51 56-23-50.25 Chlorobenzene ND ug/L 3.0 1 11/07/08 10:51 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/07/08 10:51 75-00-30.54 Chloroform ND ug/L 5.0 1 11/07/08 10:51 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/07/08 10:51 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/07/08 10:51 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/07/08 10:51 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/07/08 10:51 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/07/08 10:51 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/07/08 10:51 95-50-10.30 1,4-Dichlorobenzene ND ug/L 1.0 1 11/07/08 10:51 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/07/08 10:51 110-57-61.0 1,1-Dichloroethane ND ug/L 5.0 1 11/07/08 10:51 75-34-30.32 1,2-Dichloroethane ND ug/L 1.0 1 11/07/08 10:51 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/07/08 10:51 75-35-40.56 cis-1,2-Dichloroethene ND ug/L 5.0 1 11/07/08 10:51 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/07/08 10:51 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/07/08 10:51 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/07/08 10:51 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/07/08 10:51 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 21 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:SWN-1 Lab ID:9231169009 Collected:10/28/08 09:35 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/07/08 10:51 10061-02-60.26 Ethylbenzene ND ug/L 1.0 1 11/07/08 10:51 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/07/08 10:51 591-78-60.46 Iodomethane ND ug/L 10.0 1 11/07/08 10:51 74-88-40.32 Methylene Chloride ND ug/L 2.0 1 11/07/08 10:51 75-09-20.97 4-Methyl-2-pentanone (MIBK)ND ug/L 100 1 11/07/08 10:51 108-10-10.33 Styrene ND ug/L 1.0 1 11/07/08 10:51 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/07/08 10:51 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/07/08 10:51 79-34-50.40 Tetrachloroethene ND ug/L 1.0 1 11/07/08 10:51 127-18-40.46 Toluene ND ug/L 1.0 1 11/07/08 10:51 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/07/08 10:51 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/07/08 10:51 79-00-50.29 Trichloroethene ND ug/L 1.0 1 11/07/08 10:51 79-01-60.47 Trichlorofluoromethane ND ug/L 1.0 1 11/07/08 10:51 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/07/08 10:51 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/07/08 10:51 108-05-40.35 Vinyl chloride ND ug/L 1.0 1 11/07/08 10:51 75-01-40.62 Xylene (Total)ND ug/L 5.0 1 11/07/08 10:51 1330-20-70.66 m&p-Xylene ND ug/L 2.0 1 11/07/08 10:51 1330-20-70.66 o-Xylene ND ug/L 1.0 1 11/07/08 10:51 95-47-60.23 4-Bromofluorobenzene (S)98 %87-109 1 11/07/08 10:51 460-00-4 Dibromofluoromethane (S)100 %85-115 1 11/07/08 10:51 1868-53-7 1,2-Dichloroethane-d4 (S)104 %79-120 1 11/07/08 10:51 17060-07-0 Toluene-d8 (S)99 %70-120 1 11/07/08 10:51 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 22 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:LAGOON Lab ID:9231169010 Collected:10/30/08 07:30 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 GW North Carolina Preparation Method: EPA 3010 Antimony 10 ug/L 6.0 1 11/05/08 04:46 7440-36-011/03/08 14:152.6 Arsenic ND ug/L 10.0 1 11/05/08 04:46 7440-38-211/03/08 14:152.7 Barium 209 ug/L 100 1 11/05/08 04:46 7440-39-311/03/08 14:150.20 Beryllium ND ug/L 1.0 1 11/05/08 04:46 7440-41-711/03/08 14:150.10 Cadmium ND ug/L 1.0 1 11/05/08 04:46 7440-43-911/03/08 14:150.50 Chromium ND ug/L 10.0 1 11/05/08 04:46 7440-47-311/03/08 14:150.40 Cobalt 12.2 ug/L 10.0 1 11/05/08 04:46 7440-48-4 Z211/03/08 14:150.60 Copper ND ug/L 10.0 1 11/05/08 04:46 7440-50-811/03/08 14:150.30 Lead ND ug/L 10.0 1 11/05/08 04:46 7439-92-111/03/08 14:154.0 Nickel 8.9J ug/L 50.0 1 11/05/08 04:46 7440-02-011/03/08 14:151.7 Selenium 13.4 ug/L 10.0 1 11/05/08 04:46 7782-49-211/03/08 14:153.8 Silver 2.4J ug/L 10.0 1 11/05/08 04:46 7440-22-411/03/08 14:150.10 Thallium 4.9J ug/L 5.5 1 11/05/08 04:46 7440-28-011/03/08 14:153.0 Vanadium ND ug/L 25.0 1 11/05/08 04:46 7440-62-211/03/08 14:150.20 Zinc ND ug/L 10.0 1 11/05/08 04:46 7440-66-611/03/08 14:150.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 6.9J ug/L 100 1 11/07/08 11:07 67-64-12.2 Acrylonitrile ND ug/L 200 1 11/07/08 11:07 107-13-11.9 Benzene 0.90J ug/L 1.0 1 11/07/08 11:07 71-43-20.25 Bromochloromethane ND ug/L 3.0 1 11/07/08 11:07 74-97-50.17 Bromodichloromethane ND ug/L 1.0 1 11/07/08 11:07 75-27-40.18 Bromoform ND ug/L 3.0 1 11/07/08 11:07 75-25-20.26 Bromomethane ND ug/L 10.0 1 11/07/08 11:07 74-83-90.29 2-Butanone (MEK)15.1J ug/L 100 1 11/07/08 11:07 78-93-30.96 Carbon disulfide ND ug/L 100 1 11/07/08 11:07 75-15-01.2 Carbon tetrachloride ND ug/L 1.0 1 11/07/08 11:07 56-23-50.25 Chlorobenzene 0.73J ug/L 3.0 1 11/07/08 11:07 108-90-70.23 Chloroethane ND ug/L 10.0 1 11/07/08 11:07 75-00-30.54 Chloroform ND ug/L 5.0 1 11/07/08 11:07 67-66-30.14 Chloromethane ND ug/L 1.0 1 11/07/08 11:07 74-87-30.11 1,2-Dibromo-3-chloropropane ND ug/L 13.0 1 11/07/08 11:07 96-12-82.5 Dibromochloromethane ND ug/L 3.0 1 11/07/08 11:07 124-48-10.21 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 11/07/08 11:07 106-93-40.27 Dibromomethane ND ug/L 10.0 1 11/07/08 11:07 74-95-30.21 1,2-Dichlorobenzene ND ug/L 5.0 1 11/07/08 11:07 95-50-10.30 1,4-Dichlorobenzene 6.5 ug/L 1.0 1 11/07/08 11:07 106-46-70.33 trans-1,4-Dichloro-2-butene ND ug/L 100 1 11/07/08 11:07 110-57-61.0 1,1-Dichloroethane ND ug/L 5.0 1 11/07/08 11:07 75-34-30.32 1,2-Dichloroethane 0.56J ug/L 1.0 1 11/07/08 11:07 107-06-20.12 1,1-Dichloroethene ND ug/L 5.0 1 11/07/08 11:07 75-35-40.56 cis-1,2-Dichloroethene 9.4 ug/L 5.0 1 11/07/08 11:07 156-59-20.19 trans-1,2-Dichloroethene ND ug/L 5.0 1 11/07/08 11:07 156-60-50.49 1,2-Dichloropropane ND ug/L 1.0 1 11/07/08 11:07 78-87-50.27 1,3-Dichloropropane ND ug/L 1.0 1 11/07/08 11:07 142-28-90.28 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/07/08 11:07 10061-01-50.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 23 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:LAGOON Lab ID:9231169010 Collected:10/30/08 07:30 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/07/08 11:07 10061-02-60.26 Ethylbenzene 2.4 ug/L 1.0 1 11/07/08 11:07 100-41-40.30 2-Hexanone ND ug/L 50.0 1 11/07/08 11:07 591-78-60.46 Iodomethane 4.4J ug/L 10.0 1 11/07/08 11:07 74-88-40.32 Methylene Chloride 4.3 ug/L 2.0 1 11/07/08 11:07 75-09-20.97 4-Methyl-2-pentanone (MIBK)2.9J ug/L 100 1 11/07/08 11:07 108-10-10.33 Styrene ND ug/L 1.0 1 11/07/08 11:07 100-42-50.26 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1 11/07/08 11:07 630-20-60.33 1,1,2,2-Tetrachloroethane ND ug/L 3.0 1 11/07/08 11:07 79-34-50.40 Tetrachloroethene ND ug/L 1.0 1 11/07/08 11:07 127-18-40.46 Toluene 3.6 ug/L 1.0 1 11/07/08 11:07 108-88-30.26 1,1,1-Trichloroethane ND ug/L 1.0 1 11/07/08 11:07 71-55-60.48 1,1,2-Trichloroethane ND ug/L 1.0 1 11/07/08 11:07 79-00-50.29 Trichloroethene 0.50J ug/L 1.0 1 11/07/08 11:07 79-01-60.47 Trichlorofluoromethane ND ug/L 1.0 1 11/07/08 11:07 75-69-40.20 1,2,3-Trichloropropane ND ug/L 1.0 1 11/07/08 11:07 96-18-40.41 Vinyl acetate ND ug/L 50.0 1 11/07/08 11:07 108-05-40.35 Vinyl chloride 5.9 ug/L 1.0 1 11/07/08 11:07 75-01-40.62 Xylene (Total)8.3 ug/L 5.0 1 11/07/08 11:07 1330-20-70.66 m&p-Xylene 3.7 ug/L 2.0 1 11/07/08 11:07 1330-20-70.66 o-Xylene 4.6 ug/L 1.0 1 11/07/08 11:07 95-47-60.23 4-Bromofluorobenzene (S)103 %87-109 1 11/07/08 11:07 460-00-4 Dibromofluoromethane (S)98 %85-115 1 11/07/08 11:07 1868-53-7 1,2-Dichloroethane-d4 (S)98 %79-120 1 11/07/08 11:07 17060-07-0 Toluene-d8 (S)100 %70-120 1 11/07/08 11:07 2037-26-5 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 29.6 mg/L 4.0 1 11/03/08 21:41 5210B BOD, Low Level Analytical Method: SM 5210B BOD, 5 day 80400 ug/L 2000 1 11/05/08 15:00 B2,B4, B610/31/08 10:45 9040 pH Analytical Method: EPA 9040 pH 6.3 Std. Units 0.10 1 10/31/08 18:42 H1,H60.10 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 288 ug/L 100 1 10/30/08 23:09100 Nitrogen, Nitrite ND ug/L 100 1 10/30/08 23:09100 Nitrogen, NO2 plus NO3 288 ug/L 100 1 10/30/08 23:09100 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus ND ug/L 100 1 11/04/08 10:55 7723-14-0100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 24 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Sample:LAGOON Lab ID:9231169010 Collected:10/30/08 07:30 Received:10/30/08 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 99000 ug/L 25000 1 11/04/08 15:4525000 ASTM D516-90 Sulfate Water Analytical Method: ASTM D516-90 Sulfate ND ug/L 5000 1 11/03/08 10:54 14808-79-85000 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 25 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/3782 EPA 353.2 EPA 353.2 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples:9231169010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:190907 Associated Lab Samples:9231169010 Matrix:Water Analyzed Nitrogen, Nitrate ug/L ND 100 10/30/08 23:09 Nitrogen, Nitrite ug/L ND 100 10/30/08 23:09 Nitrogen, NO2 plus NO3 ug/L ND 100 10/30/08 23:09 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 190908LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate ug/L 48605000 97 90-110 Nitrogen, Nitrite ug/L 10701000 107 90-110 Nitrogen, NO2 plus NO3 ug/L 48605000 97 90-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 190909MATRIX SPIKE SAMPLE: MSSpike Result 9231126001 Nitrogen, Nitrate ug/L 451005000 91 90-11040.6 mg/L Nitrogen, Nitrite ug/L 16301000 98 90-1100.65 mg/L Nitrogen, NO2 plus NO3 ug/L 45100 M150007890-11041.2 mg/L Parameter Units Dup Result Max RPD QualifiersRPDResult 9231096001 190910SAMPLE DUPLICATE: Nitrogen, Nitrate ug/L 3590 2 203.5 mg/L Nitrogen, Nitrite ug/L ND 20ND Nitrogen, NO2 plus NO3 ug/L 3590 2 203.5 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 26 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WET/6074 SM 5210B SM 5210B 5210B BOD, Low Level Associated Lab Samples:9231169010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:190922 Associated Lab Samples:9231169010 Matrix:Water Analyzed BOD, 5 day ug/L 0.0J 2000 11/05/08 15:00 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 190923LABORATORY CONTROL SAMPLE: LCSSpike BOD, 5 day ug/L 158000 B4,B61980008084-115 Parameter Units Dup Result Max RPD QualifiersRPDResult 9231174001 190924SAMPLE DUPLICATE: BOD, 5 day ug/L 100J B2,B4,B620ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 27 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WET/6089 EPA 9040 EPA 9040 9040 pH Associated Lab Samples:9231169010 Parameter Units Dup Result Max RPD QualifiersRPDResult 9231169010 191524SAMPLE DUPLICATE: pH Std. Units 6.3 H60206.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 28 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/3803 ASTM D516-90 ASTM D516-90 ASTM D516-90 Sulfate Water Associated Lab Samples:9231169010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:191899 Associated Lab Samples:9231169010 Matrix:Water Analyzed Sulfate ug/L ND 5000 11/03/08 10:54 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 191900LABORATORY CONTROL SAMPLE: LCSSpike Sulfate ug/L 1980020000 99 90-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 191902MATRIX SPIKE SAMPLE: MSSpike Result 9231169010 Sulfate ug/L 1940020000 87 75-125ND Parameter Units Dup Result Max RPD QualifiersRPDResult 9231169010 191901SAMPLE DUPLICATE: Sulfate ug/L ND 20ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 29 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/3304 EPA 3010 EPA 6010 GW North Carolina 6010 MET NC Groundwater Associated Lab Samples:9231169001, 9231169002, 9231169003, 9231169004, 9231169005, 9231169006, 9231169007, 9231169008, 9231169009, 9231169010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:191903 Associated Lab Samples:9231169001, 9231169002, 9231169003, 9231169004, 9231169005, 9231169006, 9231169007, 9231169008, 9231169009, 9231169010 Matrix:Water Analyzed Antimony ug/L ND 6.0 11/05/08 03:51 Arsenic ug/L ND 10.0 11/05/08 03:51 Barium ug/L ND 100 11/05/08 03:51 Beryllium ug/L ND 1.0 11/05/08 03:51 Cadmium ug/L ND 1.0 11/05/08 03:51 Chromium ug/L ND 10.0 11/05/08 03:51 Cobalt ug/L 2.3J 10.0 11/05/08 03:51 Copper ug/L ND 10.0 11/05/08 03:51 Lead ug/L ND 10.0 11/05/08 03:51 Nickel ug/L ND 50.0 11/05/08 03:51 Selenium ug/L ND 10.0 11/05/08 03:51 Silver ug/L ND 10.0 11/05/08 03:51 Thallium ug/L ND 5.5 11/05/08 03:51 Vanadium ug/L ND 25.0 11/05/08 03:51 Zinc ug/L ND 10.0 11/05/08 03:51 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 191904LABORATORY CONTROL SAMPLE: LCSSpike Antimony ug/L 512500 102 80-120 Arsenic ug/L 504500 101 80-120 Barium ug/L 500500 100 80-120 Beryllium ug/L 502500 100 80-120 Cadmium ug/L 501500 100 80-120 Chromium ug/L 503500 101 80-120 Cobalt ug/L 499500 100 80-120 Copper ug/L 508500 102 80-120 Lead ug/L 510500 102 80-120 Nickel ug/L 508500 102 80-120 Selenium ug/L 500500 100 80-120 Silver ug/L 248250 99 80-120 Thallium ug/L 486500 97 80-120 Vanadium ug/L 501500 100 80-120 Zinc ug/L 500500 100 80-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 30 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 191905MATRIX SPIKE SAMPLE: MSSpike Result 9231169001 Antimony ug/L 504500 101 75-125ND Arsenic ug/L 499500 100 75-125ND Barium ug/L 520500 98 75-12532.2J Beryllium ug/L 495500 99 75-125ND Cadmium ug/L 490500 98 75-125ND Chromium ug/L 494500 99 75-125ND Cobalt ug/L 491500 98 75-1252.9J Copper ug/L 501500 100 75-1250.38J Lead ug/L 495500 99 75-125ND Nickel ug/L 496500 99 75-125ND Selenium ug/L 489500 97 75-125ND Silver ug/L 243250 97 75-1250.11J Thallium ug/L 476500 94 75-1253.5J Vanadium ug/L 494500 99 75-1250.78J Zinc ug/L 493500 98 75-1252.0J Parameter Units Dup Result Max RPD QualifiersRPDResult 9231169002 191906SAMPLE DUPLICATE: Antimony ug/L ND 25ND Arsenic ug/L 3.5J 253.7J Barium ug/L 81.4J .1 2581.5J Beryllium ug/L 0.31J 250.37J Cadmium ug/L ND 25ND Chromium ug/L 5.3J 5 255.6J Cobalt ug/L 2.3J 254.9J Copper ug/L 5.8J 0 255.8J Lead ug/L ND 25ND Nickel ug/L 5.6J .5 255.6J Selenium ug/L ND 25ND Silver ug/L 0.22J 250.23J Thallium ug/L ND 25ND Vanadium ug/L 13.0J .8 2513.1J Zinc ug/L 12.2 8 2513.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 31 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/3807 SM 5220D SM 5220D 5220D COD Associated Lab Samples:9231169010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:192144 Associated Lab Samples:9231169010 Matrix:Water Analyzed Chemical Oxygen Demand ug/L ND 25000 11/04/08 15:45 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 192145LABORATORY CONTROL SAMPLE: LCSSpike Chemical Oxygen Demand ug/L 741000750000 99 90-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 192146MATRIX SPIKE SAMPLE: MSSpike Result 9230486001 Chemical Oxygen Demand ug/L 138000000 M0120000002875-125103000 mg/L Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 192150MATRIX SPIKE SAMPLE: MSSpike Result 9230526002 Chemical Oxygen Demand ug/L 1000000 M0750000175-125995 mg/L Parameter Units Dup Result Max RPD QualifiersRPDResult 9230663001 192151SAMPLE DUPLICATE: Chemical Oxygen Demand ug/L 127000 4 20122 mg/L Parameter Units Dup Result Max RPD QualifiersRPDResult 9230660001 192153SAMPLE DUPLICATE: Chemical Oxygen Demand ug/L 186000 R12320148 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 32 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WET/6104 SM 2540D SM 2540D 2540D Total Suspended Solids Associated Lab Samples:9231169010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:192154 Associated Lab Samples:9231169010 Matrix:Water Analyzed Total Suspended Solids mg/L 0.0J 1.0 11/03/08 21:34 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 192155LABORATORY CONTROL SAMPLE: LCSSpike Total Suspended Solids mg/L 240250 96 80-120 Parameter Units Dup Result Max RPD QualifiersRPDResult 9230922001 192156SAMPLE DUPLICATE: Total Suspended Solids mg/L 2.5 202.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 33 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/3809 EPA 365.1 EPA 365.1 365.1 Phosphorus, Total Associated Lab Samples:9231169010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:192171 Associated Lab Samples:9231169010 Matrix:Water Analyzed Phosphorus ug/L ND 100 11/04/08 11:14 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 192172LABORATORY CONTROL SAMPLE: LCSSpike Phosphorus ug/L 10501000 105 90-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 192173MATRIX SPIKE SAMPLE: MSSpike Result 9231231001 Phosphorus ug/L 10500 M0100013390-1109.2 mg/L Parameter Units Dup Result Max RPD QualifiersRPDResult 9231231002 192174SAMPLE DUPLICATE: Phosphorus ug/L 275 3 200.28 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 34 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/5140 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:9231169001, 9231169002 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:192872 Associated Lab Samples:9231169001, 9231169002 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 11/05/08 10:40 1,1,1-Trichloroethane ug/L ND 1.0 11/05/08 10:40 1,1,2,2-Tetrachloroethane ug/L ND 3.0 11/05/08 10:40 1,1,2-Trichloroethane ug/L ND 1.0 11/05/08 10:40 1,1-Dichloroethane ug/L ND 5.0 11/05/08 10:40 1,1-Dichloroethene ug/L ND 5.0 11/05/08 10:40 1,2,3-Trichloropropane ug/L ND 1.0 11/05/08 10:40 1,2-Dibromo-3-chloropropane ug/L ND 13.0 11/05/08 10:40 1,2-Dibromoethane (EDB)ug/L ND 1.0 11/05/08 10:40 1,2-Dichlorobenzene ug/L ND 5.0 11/05/08 10:40 1,2-Dichloroethane ug/L ND 1.0 11/05/08 10:40 1,2-Dichloropropane ug/L ND 1.0 11/05/08 10:40 1,3-Dichloropropane ug/L ND 1.0 11/05/08 10:40 1,4-Dichlorobenzene ug/L ND 1.0 11/05/08 10:40 2-Butanone (MEK)ug/L ND 100 11/05/08 10:40 2-Hexanone ug/L ND 50.0 11/05/08 10:40 4-Methyl-2-pentanone (MIBK)ug/L ND 100 11/05/08 10:40 Acetone ug/L ND 100 11/05/08 10:40 Acrylonitrile ug/L ND 200 11/05/08 10:40 Benzene ug/L ND 1.0 11/05/08 10:40 Bromochloromethane ug/L ND 3.0 11/05/08 10:40 Bromodichloromethane ug/L ND 1.0 11/05/08 10:40 Bromoform ug/L ND 3.0 11/05/08 10:40 Bromomethane ug/L ND 10.0 11/05/08 10:40 Carbon disulfide ug/L ND 100 11/05/08 10:40 Carbon tetrachloride ug/L ND 1.0 11/05/08 10:40 Chlorobenzene ug/L ND 3.0 11/05/08 10:40 Chloroethane ug/L ND 10.0 11/05/08 10:40 Chloroform ug/L 0.32J 5.0 11/05/08 10:40 Chloromethane ug/L ND 1.0 11/05/08 10:40 cis-1,2-Dichloroethene ug/L ND 5.0 11/05/08 10:40 cis-1,3-Dichloropropene ug/L ND 1.0 11/05/08 10:40 Dibromochloromethane ug/L ND 3.0 11/05/08 10:40 Dibromomethane ug/L ND 10.0 11/05/08 10:40 Ethylbenzene ug/L ND 1.0 11/05/08 10:40 Iodomethane ug/L ND 10.0 11/05/08 10:40 m&p-Xylene ug/L ND 2.0 11/05/08 10:40 Methylene Chloride ug/L ND 2.0 11/05/08 10:40 o-Xylene ug/L ND 1.0 11/05/08 10:40 Styrene ug/L ND 1.0 11/05/08 10:40 Tetrachloroethene ug/L ND 1.0 11/05/08 10:40 Toluene ug/L ND 1.0 11/05/08 10:40 trans-1,2-Dichloroethene ug/L ND 5.0 11/05/08 10:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 35 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:192872 Associated Lab Samples:9231169001, 9231169002 Matrix:Water Analyzed trans-1,3-Dichloropropene ug/L ND 1.0 11/05/08 10:40 trans-1,4-Dichloro-2-butene ug/L ND 100 11/05/08 10:40 Trichloroethene ug/L ND 1.0 11/05/08 10:40 Trichlorofluoromethane ug/L ND 1.0 11/05/08 10:40 Vinyl acetate ug/L ND 50.0 11/05/08 10:40 Vinyl chloride ug/L ND 1.0 11/05/08 10:40 Xylene (Total)ug/L ND 5.0 11/05/08 10:40 1,2-Dichloroethane-d4 (S)%103 79-120 11/05/08 10:40 4-Bromofluorobenzene (S)%98 87-109 11/05/08 10:40 Dibromofluoromethane (S)%103 85-115 11/05/08 10:40 Toluene-d8 (S)%102 70-120 11/05/08 10:40 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 192873LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 45.050 90 83-125 1,1,1-Trichloroethane ug/L 48.750 97 80-129 1,1,2,2-Tetrachloroethane ug/L 43.550 87 73-127 1,1,2-Trichloroethane ug/L 45.050 90 77-123 1,1-Dichloroethane ug/L 48.750 97 76-129 1,1-Dichloroethene ug/L 50.450 101 78-146 1,2,3-Trichloropropane ug/L 43.750 87 72-125 1,2-Dibromo-3-chloropropane ug/L 41.550 83 65-128 1,2-Dibromoethane (EDB)ug/L 45.150 90 81-125 1,2-Dichlorobenzene ug/L 43.750 87 82-126 1,2-Dichloroethane ug/L 43.550 87 72-126 1,2-Dichloropropane ug/L 46.550 93 80-127 1,3-Dichloropropane ug/L 43.550 87 79-124 1,4-Dichlorobenzene ug/L 48.850 98 79-125 2-Butanone (MEK)ug/L 96.4J100 96 50-134 2-Hexanone ug/L 99.2100 99 58-138 4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-131 Acetone ug/L 93.6J100 94 50-146 Acrylonitrile ug/L 218250 87 66-124 Benzene ug/L 46.850 94 78-128 Bromochloromethane ug/L 43.550 87 73-124 Bromodichloromethane ug/L 44.950 90 81-125 Bromoform ug/L 38.850 78 71-125 Bromomethane ug/L 38.750 77 50-150 Carbon disulfide ug/L 46.8J50 94 54-150 Carbon tetrachloride ug/L 47.250 94 81-137 Chlorobenzene ug/L 43.450 87 82-126 Chloroethane ug/L 46.250 92 69-140 Chloroform ug/L 53.350 107 77-129 Chloromethane ug/L 47.150 94 54-139 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 36 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 192873LABORATORY CONTROL SAMPLE: LCSSpike cis-1,2-Dichloroethene ug/L 51.450 103 76-133 cis-1,3-Dichloropropene ug/L 47.350 95 76-127 Dibromochloromethane ug/L 43.350 87 77-125 Dibromomethane ug/L 47.150 94 77-125 Ethylbenzene ug/L 46.950 94 80-127 Iodomethane ug/L 109100 109 65-172 m&p-Xylene ug/L 98.7100 99 82-127 Methylene Chloride ug/L 51.650 103 67-133 o-Xylene ug/L 45.950 92 83-124 Styrene ug/L 49.450 99 80-130 Tetrachloroethene ug/L 46.450 93 78-128 Toluene ug/L 46.050 92 76-126 trans-1,2-Dichloroethene ug/L 47.950 96 78-134 trans-1,3-Dichloropropene ug/L 47.450 95 75-125 trans-1,4-Dichloro-2-butene ug/L 44.4J50 89 51-140 Trichloroethene ug/L 45.550 91 79-127 Trichlorofluoromethane ug/L 48.850 98 76-148 Vinyl acetate ug/L 117100 117 50-150 Vinyl chloride ug/L 50.350 101 67-143 Xylene (Total)ug/L 145150 96 83-125 1,2-Dichloroethane-d4 (S)%101 79-120 4-Bromofluorobenzene (S)%101 87-109 Dibromofluoromethane (S)%105 85-115 Toluene-d8 (S)%102 70-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 192874MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9230676004 192875 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1-Dichloroethene ug/L R1509160-150127 33 3050ND45.5 63.7 Benzene ug/L R1508674-136125 37 3050ND43.1 62.6 Chlorobenzene ug/L R1508079-135114 36 3050ND39.8 57.0 Toluene ug/L R1508773-131124 36 3050ND43.3 62.1 Trichloroethene ug/L R1508173-131116 36 3050ND40.3 57.9 1,2-Dichloroethane-d4 (S)%102 79-120101 4-Bromofluorobenzene (S)%96 87-10996 Dibromofluoromethane (S)%101 85-11599 Toluene-d8 (S)%102 70-120102 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 37 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/5142 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:9231169003, 9231169004, 9231169005, 9231169006, 9231169007, 9231169008 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:193019 Associated Lab Samples:9231169003, 9231169004, 9231169005, 9231169006, 9231169007, 9231169008 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 11/06/08 14:02 1,1,1-Trichloroethane ug/L ND 1.0 11/06/08 14:02 1,1,2,2-Tetrachloroethane ug/L ND 3.0 11/06/08 14:02 1,1,2-Trichloroethane ug/L ND 1.0 11/06/08 14:02 1,1-Dichloroethane ug/L ND 5.0 11/06/08 14:02 1,1-Dichloroethene ug/L ND 5.0 11/06/08 14:02 1,2,3-Trichloropropane ug/L ND 1.0 11/06/08 14:02 1,2-Dibromo-3-chloropropane ug/L ND 13.0 11/06/08 14:02 1,2-Dibromoethane (EDB)ug/L ND 1.0 11/06/08 14:02 1,2-Dichlorobenzene ug/L ND 5.0 11/06/08 14:02 1,2-Dichloroethane ug/L ND 1.0 11/06/08 14:02 1,2-Dichloropropane ug/L ND 1.0 11/06/08 14:02 1,3-Dichloropropane ug/L ND 1.0 11/06/08 14:02 1,4-Dichlorobenzene ug/L ND 1.0 11/06/08 14:02 2-Butanone (MEK)ug/L ND 100 11/06/08 14:02 2-Hexanone ug/L ND 50.0 11/06/08 14:02 4-Methyl-2-pentanone (MIBK)ug/L ND 100 11/06/08 14:02 Acetone ug/L ND 100 11/06/08 14:02 Acrylonitrile ug/L ND 200 11/06/08 14:02 Benzene ug/L ND 1.0 11/06/08 14:02 Bromochloromethane ug/L ND 3.0 11/06/08 14:02 Bromodichloromethane ug/L ND 1.0 11/06/08 14:02 Bromoform ug/L ND 3.0 11/06/08 14:02 Bromomethane ug/L ND 10.0 11/06/08 14:02 Carbon disulfide ug/L ND 100 11/06/08 14:02 Carbon tetrachloride ug/L ND 1.0 11/06/08 14:02 Chlorobenzene ug/L ND 3.0 11/06/08 14:02 Chloroethane ug/L ND 10.0 11/06/08 14:02 Chloroform ug/L ND 5.0 11/06/08 14:02 Chloromethane ug/L ND 1.0 11/06/08 14:02 cis-1,2-Dichloroethene ug/L ND 5.0 11/06/08 14:02 cis-1,3-Dichloropropene ug/L ND 1.0 11/06/08 14:02 Dibromochloromethane ug/L ND 3.0 11/06/08 14:02 Dibromomethane ug/L ND 10.0 11/06/08 14:02 Ethylbenzene ug/L ND 1.0 11/06/08 14:02 Iodomethane ug/L ND 10.0 11/06/08 14:02 m&p-Xylene ug/L ND 2.0 11/06/08 14:02 Methylene Chloride ug/L ND 2.0 11/06/08 14:02 o-Xylene ug/L ND 1.0 11/06/08 14:02 Styrene ug/L ND 1.0 11/06/08 14:02 Tetrachloroethene ug/L ND 1.0 11/06/08 14:02 Toluene ug/L ND 1.0 11/06/08 14:02 trans-1,2-Dichloroethene ug/L ND 5.0 11/06/08 14:02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 38 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:193019 Associated Lab Samples:9231169003, 9231169004, 9231169005, 9231169006, 9231169007, 9231169008 Matrix:Water Analyzed trans-1,3-Dichloropropene ug/L ND 1.0 11/06/08 14:02 trans-1,4-Dichloro-2-butene ug/L ND 100 11/06/08 14:02 Trichloroethene ug/L ND 1.0 11/06/08 14:02 Trichlorofluoromethane ug/L ND 1.0 11/06/08 14:02 Vinyl acetate ug/L ND 50.0 11/06/08 14:02 Vinyl chloride ug/L ND 1.0 11/06/08 14:02 Xylene (Total)ug/L ND 5.0 11/06/08 14:02 1,2-Dichloroethane-d4 (S)%104 79-120 11/06/08 14:02 4-Bromofluorobenzene (S)%99 87-109 11/06/08 14:02 Dibromofluoromethane (S)%104 85-115 11/06/08 14:02 Toluene-d8 (S)%101 70-120 11/06/08 14:02 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 193020LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 52.250 104 83-125 1,1,1-Trichloroethane ug/L 52.450 105 80-129 1,1,2,2-Tetrachloroethane ug/L 48.850 98 73-127 1,1,2-Trichloroethane ug/L 50.250 100 77-123 1,1-Dichloroethane ug/L 53.550 107 76-129 1,1-Dichloroethene ug/L 53.550 107 78-146 1,2,3-Trichloropropane ug/L 50.850 102 72-125 1,2-Dibromo-3-chloropropane ug/L 57.150 114 65-128 1,2-Dibromoethane (EDB)ug/L 52.950 106 81-125 1,2-Dichlorobenzene ug/L 51.350 103 82-126 1,2-Dichloroethane ug/L 53.050 106 72-126 1,2-Dichloropropane ug/L 51.250 102 80-127 1,3-Dichloropropane ug/L 52.250 104 79-124 1,4-Dichlorobenzene ug/L 51.450 103 79-125 2-Butanone (MEK)ug/L 99.7J100 100 50-134 2-Hexanone ug/L 103100 103 58-138 4-Methyl-2-pentanone (MIBK)ug/L 104100 104 70-131 Acetone ug/L 99.5J100 100 50-146 Acrylonitrile ug/L 264250 106 66-124 Benzene ug/L 50.850 102 78-128 Bromochloromethane ug/L 54.450 109 73-124 Bromodichloromethane ug/L 50.050 100 81-125 Bromoform ug/L 55.850 112 71-125 Bromomethane ug/L 86.4 L35017350-150 Carbon disulfide ug/L 50.6J50 101 54-150 Carbon tetrachloride ug/L 50.450 101 81-137 Chlorobenzene ug/L 51.750 103 82-126 Chloroethane ug/L 55.950 112 69-140 Chloroform ug/L 53.250 106 77-129 Chloromethane ug/L 45.750 91 54-139 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 39 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 193020LABORATORY CONTROL SAMPLE: LCSSpike cis-1,2-Dichloroethene ug/L 54.750 109 76-133 cis-1,3-Dichloropropene ug/L 54.050 108 76-127 Dibromochloromethane ug/L 51.450 103 77-125 Dibromomethane ug/L 52.950 106 77-125 Ethylbenzene ug/L 49.750 99 80-127 Iodomethane ug/L 119100 119 65-172 m&p-Xylene ug/L 102100 102 82-127 Methylene Chloride ug/L 55.350 111 67-133 o-Xylene ug/L 50.450 101 83-124 Styrene ug/L 53.150 106 80-130 Tetrachloroethene ug/L 49.850 100 78-128 Toluene ug/L 49.150 98 76-126 trans-1,2-Dichloroethene ug/L 51.950 104 78-134 trans-1,3-Dichloropropene ug/L 56.450 113 75-125 trans-1,4-Dichloro-2-butene ug/L 58.2J50 116 51-140 Trichloroethene ug/L 50.250 100 79-127 Trichlorofluoromethane ug/L 48.450 97 76-148 Vinyl acetate ug/L 119100 119 50-150 Vinyl chloride ug/L 54.750 109 67-143 Xylene (Total)ug/L 153150 102 83-125 1,2-Dichloroethane-d4 (S)%106 79-120 4-Bromofluorobenzene (S)%101 87-109 Dibromofluoromethane (S)%103 85-115 Toluene-d8 (S)%99 70-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 193021MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9231169006 193022 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1-Dichloroethene ug/L 50 108 60-15089 20 3050ND54.2 44.3 Benzene ug/L 50 113 74-136102 10 3050ND56.6 51.1 Chlorobenzene ug/L 50 109 79-135104 5 3050ND54.5 52.1 Toluene ug/L 50 127 73-131107 16 3050ND63.3 53.7 Trichloroethene ug/L 50 106 73-13194 12 3050ND53.1 47.2 1,2-Dichloroethane-d4 (S)%104 79-12099 4-Bromofluorobenzene (S)%101 87-109100 Dibromofluoromethane (S)%100 85-11595 Toluene-d8 (S)%100 70-12098 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 40 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/5160 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:9231169009, 9231169010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:194322 Associated Lab Samples:9231169009, 9231169010 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 11/07/08 10:34 1,1,1-Trichloroethane ug/L ND 1.0 11/07/08 10:34 1,1,2,2-Tetrachloroethane ug/L ND 3.0 11/07/08 10:34 1,1,2-Trichloroethane ug/L ND 1.0 11/07/08 10:34 1,1-Dichloroethane ug/L ND 5.0 11/07/08 10:34 1,1-Dichloroethene ug/L ND 5.0 11/07/08 10:34 1,2,3-Trichloropropane ug/L ND 1.0 11/07/08 10:34 1,2-Dibromo-3-chloropropane ug/L ND 13.0 11/07/08 10:34 1,2-Dibromoethane (EDB)ug/L ND 1.0 11/07/08 10:34 1,2-Dichlorobenzene ug/L ND 5.0 11/07/08 10:34 1,2-Dichloroethane ug/L ND 1.0 11/07/08 10:34 1,2-Dichloropropane ug/L ND 1.0 11/07/08 10:34 1,3-Dichloropropane ug/L ND 1.0 11/07/08 10:34 1,4-Dichlorobenzene ug/L ND 1.0 11/07/08 10:34 2-Butanone (MEK)ug/L ND 100 11/07/08 10:34 2-Hexanone ug/L ND 50.0 11/07/08 10:34 4-Methyl-2-pentanone (MIBK)ug/L ND 100 11/07/08 10:34 Acetone ug/L ND 100 11/07/08 10:34 Acrylonitrile ug/L ND 200 11/07/08 10:34 Benzene ug/L ND 1.0 11/07/08 10:34 Bromochloromethane ug/L ND 3.0 11/07/08 10:34 Bromodichloromethane ug/L ND 1.0 11/07/08 10:34 Bromoform ug/L ND 3.0 11/07/08 10:34 Bromomethane ug/L ND 10.0 11/07/08 10:34 Carbon disulfide ug/L ND 100 11/07/08 10:34 Carbon tetrachloride ug/L ND 1.0 11/07/08 10:34 Chlorobenzene ug/L ND 3.0 11/07/08 10:34 Chloroethane ug/L ND 10.0 11/07/08 10:34 Chloroform ug/L ND 5.0 11/07/08 10:34 Chloromethane ug/L ND 1.0 11/07/08 10:34 cis-1,2-Dichloroethene ug/L ND 5.0 11/07/08 10:34 cis-1,3-Dichloropropene ug/L ND 1.0 11/07/08 10:34 Dibromochloromethane ug/L ND 3.0 11/07/08 10:34 Dibromomethane ug/L ND 10.0 11/07/08 10:34 Ethylbenzene ug/L ND 1.0 11/07/08 10:34 Iodomethane ug/L ND 10.0 11/07/08 10:34 m&p-Xylene ug/L ND 2.0 11/07/08 10:34 Methylene Chloride ug/L ND 2.0 11/07/08 10:34 o-Xylene ug/L ND 1.0 11/07/08 10:34 Styrene ug/L ND 1.0 11/07/08 10:34 Tetrachloroethene ug/L ND 1.0 11/07/08 10:34 Toluene ug/L ND 1.0 11/07/08 10:34 trans-1,2-Dichloroethene ug/L ND 5.0 11/07/08 10:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 41 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:194322 Associated Lab Samples:9231169009, 9231169010 Matrix:Water Analyzed trans-1,3-Dichloropropene ug/L ND 1.0 11/07/08 10:34 trans-1,4-Dichloro-2-butene ug/L ND 100 11/07/08 10:34 Trichloroethene ug/L ND 1.0 11/07/08 10:34 Trichlorofluoromethane ug/L ND 1.0 11/07/08 10:34 Vinyl acetate ug/L ND 50.0 11/07/08 10:34 Vinyl chloride ug/L ND 1.0 11/07/08 10:34 Xylene (Total)ug/L ND 5.0 11/07/08 10:34 1,2-Dichloroethane-d4 (S)%103 79-120 11/07/08 10:34 4-Bromofluorobenzene (S)%100 87-109 11/07/08 10:34 Dibromofluoromethane (S)%98 85-115 11/07/08 10:34 Toluene-d8 (S)%100 70-120 11/07/08 10:34 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 194323LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 45.550 91 83-125 1,1,1-Trichloroethane ug/L 45.450 91 80-129 1,1,2,2-Tetrachloroethane ug/L 42.450 85 73-127 1,1,2-Trichloroethane ug/L 42.650 85 77-123 1,1-Dichloroethane ug/L 47.450 95 76-129 1,1-Dichloroethene ug/L 46.750 93 78-146 1,2,3-Trichloropropane ug/L 45.950 92 72-125 1,2-Dibromo-3-chloropropane ug/L 51.950 104 65-128 1,2-Dibromoethane (EDB)ug/L 46.150 92 81-125 1,2-Dichlorobenzene ug/L 46.350 93 82-126 1,2-Dichloroethane ug/L 46.050 92 72-126 1,2-Dichloropropane ug/L 45.150 90 80-127 1,3-Dichloropropane ug/L 46.150 92 79-124 1,4-Dichlorobenzene ug/L 46.650 93 79-125 2-Butanone (MEK)ug/L 85.5J100 86 50-134 2-Hexanone ug/L 91.0100 91 58-138 4-Methyl-2-pentanone (MIBK)ug/L 87.7J100 88 70-131 Acetone ug/L 87.5J100 88 50-146 Acrylonitrile ug/L 228250 91 66-124 Benzene ug/L 43.550 87 78-128 Bromochloromethane ug/L 46.450 93 73-124 Bromodichloromethane ug/L 41.850 84 81-125 Bromoform ug/L 46.350 93 71-125 Bromomethane ug/L 64.650 129 50-150 Carbon disulfide ug/L 44.4J50 89 54-150 Carbon tetrachloride ug/L 42.050 84 81-137 Chlorobenzene ug/L 45.950 92 82-126 Chloroethane ug/L 49.650 99 69-140 Chloroform ug/L 46.250 92 77-129 Chloromethane ug/L 43.050 86 54-139 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 42 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 194323LABORATORY CONTROL SAMPLE: LCSSpike cis-1,2-Dichloroethene ug/L 47.950 96 76-133 cis-1,3-Dichloropropene ug/L 44.750 89 76-127 Dibromochloromethane ug/L 44.350 89 77-125 Dibromomethane ug/L 43.250 86 77-125 Ethylbenzene ug/L 44.350 89 80-127 Iodomethane ug/L 87.8100 88 65-172 m&p-Xylene ug/L 90.4100 90 82-127 Methylene Chloride ug/L 48.050 96 67-133 o-Xylene ug/L 44.250 88 83-124 Styrene ug/L 46.950 94 80-130 Tetrachloroethene ug/L 43.550 87 78-128 Toluene ug/L 42.150 84 76-126 trans-1,2-Dichloroethene ug/L 44.950 90 78-134 trans-1,3-Dichloropropene ug/L 46.250 92 75-125 trans-1,4-Dichloro-2-butene ug/L 53.4J50 107 51-140 Trichloroethene ug/L 42.250 84 79-127 Trichlorofluoromethane ug/L 41.050 82 76-148 Vinyl acetate ug/L 114100 114 50-150 Vinyl chloride ug/L 46.750 93 67-143 Xylene (Total)ug/L 135150 90 83-125 1,2-Dichloroethane-d4 (S)%104 79-120 4-Bromofluorobenzene (S)%98 87-109 Dibromofluoromethane (S)%101 85-115 Toluene-d8 (S)%99 70-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 194324MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9231170018 194325 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1-Dichloroethene ug/L 50 105 60-150105 .3 3050ND52.5 52.3 Benzene ug/L 50 108 74-136114 5 3050ND54.1 57.1 Chlorobenzene ug/L 50 101 79-135106 5 3050ND50.6 53.0 Toluene ug/L 50 103 73-131109 5 3050ND51.8 54.5 Trichloroethene ug/L 50 100 73-131106 6 3050ND50.0 52.8 1,2-Dichloroethane-d4 (S)%105 79-120107 4-Bromofluorobenzene (S)%97 87-10996 Dibromofluoromethane (S)%102 85-115101 Toluene-d8 (S)%100 70-120102 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 43 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Pace Project No.: Project: 9231169 SURRY CO. SUBTITLE DLF DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated for the dilution using the most amount of sample.B2 The glucose/glutamic acid standard exceeded the range of 198 plus or minus 30.5 mg/L.B4 The calculated seed correction exceeded the range of 0.6 to 1.0 mg/L.B6 Analysis conducted outside the EPA method holding time.H1 Analysis initiated more than 15 minutes after sample collection.H6 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery was outside laboratory control limits.M0 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 RPD value was outside control limits.R1 Analyte present in the associated method blank above the detection limit.Z2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 11/10/2008 05:27 PM Page 44 of 44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 February 12, 2010 LIMS USE: FR - JONATHAN PFOHL LIMS OBJECT ID: 9262291 9262291 Project: Pace Project No.: RE: Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 SURRY LINED, PH 2 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on January 29, 2010. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Bonnie McKee bonnie.mckee@pacelabs.com Project Manager Enclosures cc:Ms. Maggie German, Municipal Engineering Services REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Charlotte Certification IDs9800 Kincey Ave. - Ste 100 Huntersville, NC 28078West Virginia Certification #: 357 Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana/LELAP Certification #: 04034New Jersey Certification #: NC012 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12 Pennsylvania Certification #: 68-00784South Carolina Certification #: 990060001South Carolina Drinking Water Cert. #: 990060003Tennessee Certification #: 04010Virginia Certification #: 00213 Asheville Certification IDs Florida/NELAP Certification #: E87648Louisiana/LELAP Certification #: 03095New Jersey Certification #: NC011 North Carolina Bioassay Certification #: 9North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002 South Carolina Certification #: 99030001Tennessee Certification #: 2980Virginia Certification #: 00072 West Virginia Certification #: 3562225 Riverside Dr. Asheville, NC 28804 Connecticut Certification #: PH-0106Massachusetts Certification #: M-NC030 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Lab ID Sample ID Matrix Date Collected Date Received 9262291001 MW-8 Water 01/28/10 08:50 01/29/10 14:12 9262291002 MW-9S Water 01/28/10 09:25 01/29/10 14:12 9262291003 MW-9D Water 01/28/10 10:10 01/29/10 14:12 9262291004 MW-10 Water 01/28/10 10:55 01/29/10 14:12 9262291005 MW-11S Water 01/28/10 15:00 01/29/10 14:12 9262291006 MW-11D Water 01/28/10 14:25 01/29/10 14:12 9262291007 MW-12 Water 01/28/10 13:30 01/29/10 14:12 9262291008 MW-13 Water 01/28/10 11:40 01/29/10 14:12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 9262291001 MW-8 EPA 6010 15 PASI-AEWS EPA 8260 52 PASI-CMCK 9262291002 MW-9S EPA 6010 15 PASI-ASAJ EPA 8260 52 PASI-CMCK 9262291003 MW-9D EPA 6010 15 PASI-ASAJ EPA 8260 52 PASI-CMCK 9262291004 MW-10 EPA 6010 15 PASI-ASAJ EPA 8260 52 PASI-CMCK 9262291005 MW-11S EPA 6010 15 PASI-ASAJ EPA 8260 52 PASI-CMCK 9262291006 MW-11D EPA 6010 15 PASI-ASAJ EPA 8260 52 PASI-CMCK 9262291007 MW-12 EPA 6010 15 PASI-ASAJ EPA 8260 52 PASI-CMCK 9262291008 MW-13 EPA 6010 15 PASI-ASAJ EPA 8260 52 PASI-CMCK REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-8 Lab ID:9262291001 Collected:01/28/10 08:50 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 5 02/11/10 13:56 7440-36-002/03/10 16:4330.0 13.0 Arsenic 15.0J ug/L 5 02/11/10 13:56 7440-38-202/03/10 16:4350.0 13.5 Barium 2000 ug/L 5 02/11/10 13:56 7440-39-302/03/10 16:435001.0 Beryllium 9.8 ug/L 5 02/11/10 13:56 7440-41-702/03/10 16:435.0 0.50 Cadmium ND ug/L 5 02/11/10 13:56 7440-43-902/03/10 16:435.0 2.5 Chromium 154 ug/L 5 02/11/10 13:56 7440-47-302/03/10 16:4350.0 2.0 Cobalt 87.5 ug/L 5 02/11/10 13:56 7440-48-402/03/10 16:4350.0 3.0 Copper 108 ug/L 5 02/11/10 13:56 7440-50-802/03/10 16:4350.0 1.5 Lead 44.5J ug/L 5 02/11/10 13:56 7439-92-102/03/10 16:4350.0 20.0 Nickel 99.5J ug/L 5 02/11/10 13:56 7440-02-002/03/10 16:432508.5 Selenium ND ug/L 5 02/11/10 13:56 7782-49-202/03/10 16:4350.0 19.0 Silver ND ug/L 5 02/11/10 13:56 7440-22-402/03/10 16:4350.0 0.50 Thallium ND ug/L 5 02/11/10 13:56 7440-28-002/03/10 16:4327.5 15.0 Vanadium 256 ug/L 5 02/11/10 13:56 7440-62-202/03/10 16:431251.0 Zinc 720 ug/L 5 02/11/10 13:56 7440-66-602/03/10 16:4350.0 2.0 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 02/04/10 21:17 67-64-11002.2 Acrylonitrile ND ug/L 1 02/04/10 21:17 107-13-12001.9 Benzene ND ug/L 1 02/04/10 21:17 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 02/04/10 21:17 74-97-53.0 0.17 Bromodichloromethane 0.24J ug/L 1 02/04/10 21:17 75-27-41.0 0.18 Bromoform ND ug/L 1 02/04/10 21:17 75-25-23.0 0.26 Bromomethane ND ug/L 1 02/04/10 21:17 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 02/04/10 21:17 78-93-31000.96 Carbon disulfide ND ug/L 1 02/04/10 21:17 75-15-01001.2 Carbon tetrachloride ND ug/L 1 02/04/10 21:17 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 02/04/10 21:17 108-90-73.0 0.23 Chloroethane ND ug/L 1 02/04/10 21:17 75-00-310.0 0.54 Chloroform 0.38J ug/L 1 02/04/10 21:17 67-66-35.0 0.14 Chloromethane ND ug/L 1 02/04/10 21:17 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 02/04/10 21:17 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 02/04/10 21:17 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 02/04/10 21:17 106-93-41.0 0.27 Dibromomethane ND ug/L 1 02/04/10 21:17 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 02/04/10 21:17 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 02/04/10 21:17 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 02/04/10 21:17 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 02/04/10 21:17 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 02/04/10 21:17 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 02/04/10 21:17 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 02/04/10 21:17 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 02/04/10 21:17 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 02/04/10 21:17 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 02/04/10 21:17 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 02/04/10 21:17 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 5 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-8 Lab ID:9262291001 Collected:01/28/10 08:50 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 02/04/10 21:17 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 02/04/10 21:17 100-41-41.0 0.30 2-Hexanone ND ug/L 1 02/04/10 21:17 591-78-650.0 0.46 Iodomethane ND ug/L 1 02/04/10 21:17 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 02/04/10 21:17 75-09-22.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 02/04/10 21:17 108-10-11000.33 Styrene ND ug/L 1 02/04/10 21:17 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 02/04/10 21:17 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 02/04/10 21:17 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 02/04/10 21:17 127-18-41.0 0.46 Toluene ND ug/L 1 02/04/10 21:17 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 02/04/10 21:17 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 02/04/10 21:17 79-00-51.0 0.29 Trichloroethene ND ug/L 1 02/04/10 21:17 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 02/04/10 21:17 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 02/04/10 21:17 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 02/04/10 21:17 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 02/04/10 21:17 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 02/04/10 21:17 1330-20-72.0 0.66 4-Bromofluorobenzene (S)101 %1 02/04/10 21:17 460-00-487-109 Dibromofluoromethane (S)107 %1 02/04/10 21:17 1868-53-785-115 1,2-Dichloroethane-d4 (S)114 %1 02/04/10 21:17 17060-07-079-120 Toluene-d8 (S)101 %1 02/04/10 21:17 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 6 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-9S Lab ID:9262291002 Collected:01/28/10 09:25 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 02/10/10 15:13 7440-36-002/03/10 16:436.0 2.6 Arsenic 4.7J ug/L 1 02/10/10 15:13 7440-38-202/03/10 16:4310.0 2.7 Barium 313 ug/L 1 02/10/10 15:13 7440-39-302/03/10 16:431000.20 Beryllium 1.4 ug/L 1 02/10/10 15:13 7440-41-702/03/10 16:431.0 0.10 Cadmium ND ug/L 1 02/10/10 15:13 7440-43-902/03/10 16:431.0 0.50 Chromium 39.7 ug/L 1 02/10/10 15:13 7440-47-302/03/10 16:4310.0 0.40 Cobalt 10.4 ug/L 1 02/10/10 15:13 7440-48-402/03/10 16:4310.0 0.60 Copper 19.2 ug/L 1 02/10/10 15:13 7440-50-802/03/10 16:4310.0 0.30 Lead 12.2 ug/L 1 02/10/10 15:13 7439-92-102/03/10 16:4310.0 4.0 Nickel 21.0J ug/L 1 02/10/10 15:13 7440-02-002/03/10 16:4350.0 1.7 Selenium ND ug/L 1 02/10/10 15:13 7782-49-202/03/10 16:4310.0 3.8 Silver 0.46J ug/L 1 02/10/10 15:13 7440-22-402/03/10 16:4310.0 0.10 Thallium ND ug/L 1 02/10/10 15:13 7440-28-002/03/10 16:435.5 3.0 Vanadium 57.9 ug/L 1 02/10/10 15:13 7440-62-202/03/10 16:4325.0 0.20 Zinc 105 ug/L 1 02/10/10 15:13 7440-66-602/03/10 16:4310.0 0.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 02/04/10 21:41 67-64-11002.2 Acrylonitrile ND ug/L 1 02/04/10 21:41 107-13-12001.9 Benzene ND ug/L 1 02/04/10 21:41 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 02/04/10 21:41 74-97-53.0 0.17 Bromodichloromethane 0.25J ug/L 1 02/04/10 21:41 75-27-41.0 0.18 Bromoform ND ug/L 1 02/04/10 21:41 75-25-23.0 0.26 Bromomethane ND ug/L 1 02/04/10 21:41 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 02/04/10 21:41 78-93-31000.96 Carbon disulfide ND ug/L 1 02/04/10 21:41 75-15-01001.2 Carbon tetrachloride ND ug/L 1 02/04/10 21:41 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 02/04/10 21:41 108-90-73.0 0.23 Chloroethane ND ug/L 1 02/04/10 21:41 75-00-310.0 0.54 Chloroform 0.44J ug/L 1 02/04/10 21:41 67-66-35.0 0.14 Chloromethane ND ug/L 1 02/04/10 21:41 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 02/04/10 21:41 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 02/04/10 21:41 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 02/04/10 21:41 106-93-41.0 0.27 Dibromomethane ND ug/L 1 02/04/10 21:41 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 02/04/10 21:41 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 02/04/10 21:41 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 02/04/10 21:41 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 02/04/10 21:41 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 02/04/10 21:41 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 02/04/10 21:41 75-35-45.0 0.56 cis-1,2-Dichloroethene 1.0J ug/L 1 02/04/10 21:41 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 02/04/10 21:41 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 02/04/10 21:41 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 02/04/10 21:41 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 02/04/10 21:41 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 7 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-9S Lab ID:9262291002 Collected:01/28/10 09:25 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 02/04/10 21:41 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 02/04/10 21:41 100-41-41.0 0.30 2-Hexanone ND ug/L 1 02/04/10 21:41 591-78-650.0 0.46 Iodomethane ND ug/L 1 02/04/10 21:41 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 02/04/10 21:41 75-09-22.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 02/04/10 21:41 108-10-11000.33 Styrene ND ug/L 1 02/04/10 21:41 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 02/04/10 21:41 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 02/04/10 21:41 79-34-53.0 0.40 Tetrachloroethene 0.50J ug/L 1 02/04/10 21:41 127-18-41.0 0.46 Toluene ND ug/L 1 02/04/10 21:41 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 02/04/10 21:41 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 02/04/10 21:41 79-00-51.0 0.29 Trichloroethene 0.48J ug/L 1 02/04/10 21:41 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 02/04/10 21:41 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 02/04/10 21:41 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 02/04/10 21:41 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 02/04/10 21:41 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 02/04/10 21:41 1330-20-72.0 0.66 4-Bromofluorobenzene (S)101 %1 02/04/10 21:41 460-00-487-109 Dibromofluoromethane (S)106 %1 02/04/10 21:41 1868-53-785-115 1,2-Dichloroethane-d4 (S)113 %1 02/04/10 21:41 17060-07-079-120 Toluene-d8 (S)102 %1 02/04/10 21:41 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 8 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-9D Lab ID:9262291003 Collected:01/28/10 10:10 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 02/10/10 15:18 7440-36-002/03/10 16:436.0 2.6 Arsenic ND ug/L 1 02/10/10 15:18 7440-38-202/03/10 16:4310.0 2.7 Barium 40.7J ug/L 1 02/10/10 15:18 7440-39-302/03/10 16:431000.20 Beryllium ND ug/L 1 02/10/10 15:18 7440-41-702/03/10 16:431.0 0.10 Cadmium ND ug/L 1 02/10/10 15:18 7440-43-902/03/10 16:431.0 0.50 Chromium 2.0J ug/L 1 02/10/10 15:18 7440-47-302/03/10 16:4310.0 0.40 Cobalt ND ug/L 1 02/10/10 15:18 7440-48-402/03/10 16:4310.0 0.60 Copper 1.1J ug/L 1 02/10/10 15:18 7440-50-802/03/10 16:4310.0 0.30 Lead ND ug/L 1 02/10/10 15:18 7439-92-102/03/10 16:4310.0 4.0 Nickel 4.6J ug/L 1 02/10/10 15:18 7440-02-002/03/10 16:4350.0 1.7 Selenium ND ug/L 1 02/10/10 15:18 7782-49-202/03/10 16:4310.0 3.8 Silver ND ug/L 1 02/10/10 15:18 7440-22-402/03/10 16:4310.0 0.10 Thallium ND ug/L 1 02/10/10 15:18 7440-28-002/03/10 16:435.5 3.0 Vanadium 2.5J ug/L 1 02/10/10 15:18 7440-62-202/03/10 16:4325.0 0.20 Zinc 3.5J ug/L 1 02/10/10 15:18 7440-66-602/03/10 16:4310.0 0.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 02/04/10 22:05 67-64-11002.2 Acrylonitrile ND ug/L 1 02/04/10 22:05 107-13-12001.9 Benzene ND ug/L 1 02/04/10 22:05 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 02/04/10 22:05 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 02/04/10 22:05 75-27-41.0 0.18 Bromoform ND ug/L 1 02/04/10 22:05 75-25-23.0 0.26 Bromomethane ND ug/L 1 02/04/10 22:05 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 02/04/10 22:05 78-93-31000.96 Carbon disulfide ND ug/L 1 02/04/10 22:05 75-15-01001.2 Carbon tetrachloride ND ug/L 1 02/04/10 22:05 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 02/04/10 22:05 108-90-73.0 0.23 Chloroethane ND ug/L 1 02/04/10 22:05 75-00-310.0 0.54 Chloroform 0.50J ug/L 1 02/04/10 22:05 67-66-35.0 0.14 Chloromethane ND ug/L 1 02/04/10 22:05 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 02/04/10 22:05 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 02/04/10 22:05 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 02/04/10 22:05 106-93-41.0 0.27 Dibromomethane ND ug/L 1 02/04/10 22:05 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 02/04/10 22:05 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 02/04/10 22:05 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 02/04/10 22:05 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 02/04/10 22:05 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 02/04/10 22:05 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 02/04/10 22:05 75-35-45.0 0.56 cis-1,2-Dichloroethene 0.22J ug/L 1 02/04/10 22:05 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 02/04/10 22:05 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 02/04/10 22:05 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 02/04/10 22:05 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 02/04/10 22:05 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 9 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-9D Lab ID:9262291003 Collected:01/28/10 10:10 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 02/04/10 22:05 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 02/04/10 22:05 100-41-41.0 0.30 2-Hexanone ND ug/L 1 02/04/10 22:05 591-78-650.0 0.46 Iodomethane ND ug/L 1 02/04/10 22:05 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 02/04/10 22:05 75-09-22.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 02/04/10 22:05 108-10-11000.33 Styrene ND ug/L 1 02/04/10 22:05 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 02/04/10 22:05 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 02/04/10 22:05 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 02/04/10 22:05 127-18-41.0 0.46 Toluene ND ug/L 1 02/04/10 22:05 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 02/04/10 22:05 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 02/04/10 22:05 79-00-51.0 0.29 Trichloroethene ND ug/L 1 02/04/10 22:05 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 02/04/10 22:05 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 02/04/10 22:05 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 02/04/10 22:05 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 02/04/10 22:05 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 02/04/10 22:05 1330-20-72.0 0.66 4-Bromofluorobenzene (S)101 %1 02/04/10 22:05 460-00-487-109 Dibromofluoromethane (S)106 %1 02/04/10 22:05 1868-53-785-115 1,2-Dichloroethane-d4 (S)113 %1 02/04/10 22:05 17060-07-079-120 Toluene-d8 (S)101 %1 02/04/10 22:05 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 10 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-10 Lab ID:9262291004 Collected:01/28/10 10:55 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 02/10/10 15:22 7440-36-002/03/10 16:436.0 2.6 Arsenic ND ug/L 1 02/10/10 15:22 7440-38-202/03/10 16:4310.0 2.7 Barium 106 ug/L 1 02/10/10 15:22 7440-39-302/03/10 16:431000.20 Beryllium 0.48J ug/L 1 02/10/10 15:22 7440-41-702/03/10 16:431.0 0.10 Cadmium ND ug/L 1 02/10/10 15:22 7440-43-902/03/10 16:431.0 0.50 Chromium 15.0 ug/L 1 02/10/10 15:22 7440-47-302/03/10 16:4310.0 0.40 Cobalt 3.9J ug/L 1 02/10/10 15:22 7440-48-402/03/10 16:4310.0 0.60 Copper 11.9 ug/L 1 02/10/10 15:22 7440-50-802/03/10 16:4310.0 0.30 Lead 7.3J ug/L 1 02/10/10 15:22 7439-92-102/03/10 16:4310.0 4.0 Nickel 10.8J ug/L 1 02/10/10 15:22 7440-02-002/03/10 16:4350.0 1.7 Selenium ND ug/L 1 02/10/10 15:22 7782-49-202/03/10 16:4310.0 3.8 Silver ND ug/L 1 02/10/10 15:22 7440-22-402/03/10 16:4310.0 0.10 Thallium ND ug/L 1 02/10/10 15:22 7440-28-002/03/10 16:435.5 3.0 Vanadium 22.4J ug/L 1 02/10/10 15:22 7440-62-202/03/10 16:4325.0 0.20 Zinc 31.7 ug/L 1 02/10/10 15:22 7440-66-602/03/10 16:4310.0 0.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 02/04/10 22:29 67-64-11002.2 Acrylonitrile ND ug/L 1 02/04/10 22:29 107-13-12001.9 Benzene ND ug/L 1 02/04/10 22:29 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 02/04/10 22:29 74-97-53.0 0.17 Bromodichloromethane 0.23J ug/L 1 02/04/10 22:29 75-27-41.0 0.18 Bromoform ND ug/L 1 02/04/10 22:29 75-25-23.0 0.26 Bromomethane ND ug/L 1 02/04/10 22:29 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 02/04/10 22:29 78-93-31000.96 Carbon disulfide ND ug/L 1 02/04/10 22:29 75-15-01001.2 Carbon tetrachloride ND ug/L 1 02/04/10 22:29 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 02/04/10 22:29 108-90-73.0 0.23 Chloroethane ND ug/L 1 02/04/10 22:29 75-00-310.0 0.54 Chloroform 0.45J ug/L 1 02/04/10 22:29 67-66-35.0 0.14 Chloromethane ND ug/L 1 02/04/10 22:29 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 02/04/10 22:29 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 02/04/10 22:29 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 02/04/10 22:29 106-93-41.0 0.27 Dibromomethane ND ug/L 1 02/04/10 22:29 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 02/04/10 22:29 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 02/04/10 22:29 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 02/04/10 22:29 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 02/04/10 22:29 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 02/04/10 22:29 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 02/04/10 22:29 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 02/04/10 22:29 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 02/04/10 22:29 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 02/04/10 22:29 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 02/04/10 22:29 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 02/04/10 22:29 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 11 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-10 Lab ID:9262291004 Collected:01/28/10 10:55 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 02/04/10 22:29 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 02/04/10 22:29 100-41-41.0 0.30 2-Hexanone ND ug/L 1 02/04/10 22:29 591-78-650.0 0.46 Iodomethane ND ug/L 1 02/04/10 22:29 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 02/04/10 22:29 75-09-22.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 02/04/10 22:29 108-10-11000.33 Styrene ND ug/L 1 02/04/10 22:29 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 02/04/10 22:29 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 02/04/10 22:29 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 02/04/10 22:29 127-18-41.0 0.46 Toluene ND ug/L 1 02/04/10 22:29 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 02/04/10 22:29 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 02/04/10 22:29 79-00-51.0 0.29 Trichloroethene ND ug/L 1 02/04/10 22:29 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 02/04/10 22:29 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 02/04/10 22:29 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 02/04/10 22:29 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 02/04/10 22:29 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 02/04/10 22:29 1330-20-72.0 0.66 4-Bromofluorobenzene (S)101 %1 02/04/10 22:29 460-00-487-109 Dibromofluoromethane (S)108 %1 02/04/10 22:29 1868-53-785-115 1,2-Dichloroethane-d4 (S)115 %1 02/04/10 22:29 17060-07-079-120 Toluene-d8 (S)102 %1 02/04/10 22:29 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 12 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-11S Lab ID:9262291005 Collected:01/28/10 15:00 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 02/10/10 15:26 7440-36-002/03/10 16:436.0 2.6 Arsenic ND ug/L 1 02/10/10 15:26 7440-38-202/03/10 16:4310.0 2.7 Barium 59.1J ug/L 1 02/10/10 15:26 7440-39-302/03/10 16:431000.20 Beryllium 0.46J ug/L 1 02/10/10 15:26 7440-41-702/03/10 16:431.0 0.10 Cadmium ND ug/L 1 02/10/10 15:26 7440-43-902/03/10 16:431.0 0.50 Chromium 11.2 ug/L 1 02/10/10 15:26 7440-47-302/03/10 16:4310.0 0.40 Cobalt 5.4J ug/L 1 02/10/10 15:26 7440-48-402/03/10 16:4310.0 0.60 Copper 8.0J ug/L 1 02/10/10 15:26 7440-50-802/03/10 16:4310.0 0.30 Lead 4.5J ug/L 1 02/10/10 15:26 7439-92-102/03/10 16:4310.0 4.0 Nickel 8.6J ug/L 1 02/10/10 15:26 7440-02-002/03/10 16:4350.0 1.7 Selenium ND ug/L 1 02/10/10 15:26 7782-49-202/03/10 16:4310.0 3.8 Silver ND ug/L 1 02/10/10 15:26 7440-22-402/03/10 16:4310.0 0.10 Thallium ND ug/L 1 02/10/10 15:26 7440-28-002/03/10 16:435.5 3.0 Vanadium 15.0J ug/L 1 02/10/10 15:26 7440-62-202/03/10 16:4325.0 0.20 Zinc 27.3 ug/L 1 02/10/10 15:26 7440-66-602/03/10 16:4310.0 0.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 02/04/10 22:53 67-64-11002.2 Acrylonitrile ND ug/L 1 02/04/10 22:53 107-13-12001.9 Benzene ND ug/L 1 02/04/10 22:53 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 02/04/10 22:53 74-97-53.0 0.17 Bromodichloromethane 0.21J ug/L 1 02/04/10 22:53 75-27-41.0 0.18 Bromoform ND ug/L 1 02/04/10 22:53 75-25-23.0 0.26 Bromomethane ND ug/L 1 02/04/10 22:53 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 02/04/10 22:53 78-93-31000.96 Carbon disulfide ND ug/L 1 02/04/10 22:53 75-15-01001.2 Carbon tetrachloride ND ug/L 1 02/04/10 22:53 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 02/04/10 22:53 108-90-73.0 0.23 Chloroethane ND ug/L 1 02/04/10 22:53 75-00-310.0 0.54 Chloroform 0.47J ug/L 1 02/04/10 22:53 67-66-35.0 0.14 Chloromethane ND ug/L 1 02/04/10 22:53 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 02/04/10 22:53 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 02/04/10 22:53 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 02/04/10 22:53 106-93-41.0 0.27 Dibromomethane ND ug/L 1 02/04/10 22:53 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 02/04/10 22:53 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 02/04/10 22:53 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 02/04/10 22:53 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 02/04/10 22:53 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 02/04/10 22:53 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 02/04/10 22:53 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 02/04/10 22:53 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 02/04/10 22:53 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 02/04/10 22:53 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 02/04/10 22:53 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 02/04/10 22:53 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 13 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-11S Lab ID:9262291005 Collected:01/28/10 15:00 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 02/04/10 22:53 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 02/04/10 22:53 100-41-41.0 0.30 2-Hexanone ND ug/L 1 02/04/10 22:53 591-78-650.0 0.46 Iodomethane ND ug/L 1 02/04/10 22:53 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 02/04/10 22:53 75-09-22.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 02/04/10 22:53 108-10-11000.33 Styrene ND ug/L 1 02/04/10 22:53 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 02/04/10 22:53 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 02/04/10 22:53 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 02/04/10 22:53 127-18-41.0 0.46 Toluene ND ug/L 1 02/04/10 22:53 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 02/04/10 22:53 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 02/04/10 22:53 79-00-51.0 0.29 Trichloroethene ND ug/L 1 02/04/10 22:53 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 02/04/10 22:53 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 02/04/10 22:53 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 02/04/10 22:53 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 02/04/10 22:53 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 02/04/10 22:53 1330-20-72.0 0.66 4-Bromofluorobenzene (S)100 %1 02/04/10 22:53 460-00-487-109 Dibromofluoromethane (S)107 %1 02/04/10 22:53 1868-53-785-115 1,2-Dichloroethane-d4 (S)115 %1 02/04/10 22:53 17060-07-079-120 Toluene-d8 (S)102 %1 02/04/10 22:53 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 14 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-11D Lab ID:9262291006 Collected:01/28/10 14:25 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 02/10/10 15:31 7440-36-002/03/10 16:436.0 2.6 Arsenic 4.2J ug/L 1 02/10/10 15:31 7440-38-202/03/10 16:4310.0 2.7 Barium 90.9J ug/L 1 02/10/10 15:31 7440-39-302/03/10 16:431000.20 Beryllium 0.14J ug/L 1 02/10/10 15:31 7440-41-702/03/10 16:431.0 0.10 Cadmium ND ug/L 1 02/10/10 15:31 7440-43-902/03/10 16:431.0 0.50 Chromium 18.4 ug/L 1 02/10/10 15:31 7440-47-302/03/10 16:4310.0 0.40 Cobalt 7.5J ug/L 1 02/10/10 15:31 7440-48-402/03/10 16:4310.0 0.60 Copper 15.9 ug/L 1 02/10/10 15:31 7440-50-802/03/10 16:4310.0 0.30 Lead ND ug/L 1 02/10/10 15:31 7439-92-102/03/10 16:4310.0 4.0 Nickel 15.7J ug/L 1 02/10/10 15:31 7440-02-002/03/10 16:4350.0 1.7 Selenium ND ug/L 1 02/10/10 15:31 7782-49-202/03/10 16:4310.0 3.8 Silver ND ug/L 1 02/10/10 15:31 7440-22-402/03/10 16:4310.0 0.10 Thallium ND ug/L 1 02/10/10 15:31 7440-28-002/03/10 16:435.5 3.0 Vanadium 21.1J ug/L 1 02/10/10 15:31 7440-62-202/03/10 16:4325.0 0.20 Zinc 36.3 ug/L 1 02/10/10 15:31 7440-66-602/03/10 16:4310.0 0.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 02/04/10 23:17 67-64-11002.2 Acrylonitrile ND ug/L 1 02/04/10 23:17 107-13-12001.9 Benzene ND ug/L 1 02/04/10 23:17 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 02/04/10 23:17 74-97-53.0 0.17 Bromodichloromethane 0.26J ug/L 1 02/04/10 23:17 75-27-41.0 0.18 Bromoform ND ug/L 1 02/04/10 23:17 75-25-23.0 0.26 Bromomethane ND ug/L 1 02/04/10 23:17 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 02/04/10 23:17 78-93-31000.96 Carbon disulfide ND ug/L 1 02/04/10 23:17 75-15-01001.2 Carbon tetrachloride ND ug/L 1 02/04/10 23:17 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 02/04/10 23:17 108-90-73.0 0.23 Chloroethane ND ug/L 1 02/04/10 23:17 75-00-310.0 0.54 Chloroform 0.49J ug/L 1 02/04/10 23:17 67-66-35.0 0.14 Chloromethane ND ug/L 1 02/04/10 23:17 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 02/04/10 23:17 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 02/04/10 23:17 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 02/04/10 23:17 106-93-41.0 0.27 Dibromomethane ND ug/L 1 02/04/10 23:17 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 02/04/10 23:17 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 02/04/10 23:17 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 02/04/10 23:17 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 02/04/10 23:17 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 02/04/10 23:17 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 02/04/10 23:17 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 02/04/10 23:17 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 02/04/10 23:17 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 02/04/10 23:17 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 02/04/10 23:17 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 02/04/10 23:17 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 15 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-11D Lab ID:9262291006 Collected:01/28/10 14:25 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 02/04/10 23:17 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 02/04/10 23:17 100-41-41.0 0.30 2-Hexanone ND ug/L 1 02/04/10 23:17 591-78-650.0 0.46 Iodomethane ND ug/L 1 02/04/10 23:17 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 02/04/10 23:17 75-09-22.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 02/04/10 23:17 108-10-11000.33 Styrene ND ug/L 1 02/04/10 23:17 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 02/04/10 23:17 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 02/04/10 23:17 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 02/04/10 23:17 127-18-41.0 0.46 Toluene ND ug/L 1 02/04/10 23:17 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 02/04/10 23:17 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 02/04/10 23:17 79-00-51.0 0.29 Trichloroethene ND ug/L 1 02/04/10 23:17 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 02/04/10 23:17 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 02/04/10 23:17 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 02/04/10 23:17 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 02/04/10 23:17 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 02/04/10 23:17 1330-20-72.0 0.66 4-Bromofluorobenzene (S)102 %1 02/04/10 23:17 460-00-487-109 Dibromofluoromethane (S)109 %1 02/04/10 23:17 1868-53-785-115 1,2-Dichloroethane-d4 (S)117 %1 02/04/10 23:17 17060-07-079-120 Toluene-d8 (S)103 %1 02/04/10 23:17 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 16 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-12 Lab ID:9262291007 Collected:01/28/10 13:30 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 02/10/10 15:35 7440-36-002/03/10 16:436.0 2.6 Arsenic ND ug/L 1 02/10/10 15:35 7440-38-202/03/10 16:4310.0 2.7 Barium 60.6J ug/L 1 02/10/10 15:35 7440-39-302/03/10 16:431000.20 Beryllium ND ug/L 1 02/10/10 15:35 7440-41-702/03/10 16:431.0 0.10 Cadmium ND ug/L 1 02/10/10 15:35 7440-43-902/03/10 16:431.0 0.50 Chromium 6.0J ug/L 1 02/10/10 15:35 7440-47-302/03/10 16:4310.0 0.40 Cobalt 2.2J ug/L 1 02/10/10 15:35 7440-48-402/03/10 16:4310.0 0.60 Copper 6.4J ug/L 1 02/10/10 15:35 7440-50-802/03/10 16:4310.0 0.30 Lead ND ug/L 1 02/10/10 15:35 7439-92-102/03/10 16:4310.0 4.0 Nickel 7.1J ug/L 1 02/10/10 15:35 7440-02-002/03/10 16:4350.0 1.7 Selenium ND ug/L 1 02/10/10 15:35 7782-49-202/03/10 16:4310.0 3.8 Silver ND ug/L 1 02/10/10 15:35 7440-22-402/03/10 16:4310.0 0.10 Thallium ND ug/L 1 02/10/10 15:35 7440-28-002/03/10 16:435.5 3.0 Vanadium 8.9J ug/L 1 02/10/10 15:35 7440-62-202/03/10 16:4325.0 0.20 Zinc 13.9 ug/L 1 02/10/10 15:35 7440-66-602/03/10 16:4310.0 0.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 02/04/10 23:41 67-64-11002.2 Acrylonitrile ND ug/L 1 02/04/10 23:41 107-13-12001.9 Benzene ND ug/L 1 02/04/10 23:41 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 02/04/10 23:41 74-97-53.0 0.17 Bromodichloromethane 0.20J ug/L 1 02/04/10 23:41 75-27-41.0 0.18 Bromoform ND ug/L 1 02/04/10 23:41 75-25-23.0 0.26 Bromomethane ND ug/L 1 02/04/10 23:41 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 02/04/10 23:41 78-93-31000.96 Carbon disulfide ND ug/L 1 02/04/10 23:41 75-15-01001.2 Carbon tetrachloride ND ug/L 1 02/04/10 23:41 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 02/04/10 23:41 108-90-73.0 0.23 Chloroethane ND ug/L 1 02/04/10 23:41 75-00-310.0 0.54 Chloroform 0.35J ug/L 1 02/04/10 23:41 67-66-35.0 0.14 Chloromethane ND ug/L 1 02/04/10 23:41 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 02/04/10 23:41 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 02/04/10 23:41 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 02/04/10 23:41 106-93-41.0 0.27 Dibromomethane ND ug/L 1 02/04/10 23:41 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 02/04/10 23:41 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 02/04/10 23:41 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 02/04/10 23:41 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 02/04/10 23:41 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 02/04/10 23:41 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 02/04/10 23:41 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 02/04/10 23:41 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 02/04/10 23:41 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 02/04/10 23:41 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 02/04/10 23:41 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 02/04/10 23:41 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 17 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-12 Lab ID:9262291007 Collected:01/28/10 13:30 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 02/04/10 23:41 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 02/04/10 23:41 100-41-41.0 0.30 2-Hexanone ND ug/L 1 02/04/10 23:41 591-78-650.0 0.46 Iodomethane ND ug/L 1 02/04/10 23:41 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 02/04/10 23:41 75-09-22.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 02/04/10 23:41 108-10-11000.33 Styrene ND ug/L 1 02/04/10 23:41 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 02/04/10 23:41 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 02/04/10 23:41 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 02/04/10 23:41 127-18-41.0 0.46 Toluene ND ug/L 1 02/04/10 23:41 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 02/04/10 23:41 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 02/04/10 23:41 79-00-51.0 0.29 Trichloroethene ND ug/L 1 02/04/10 23:41 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 02/04/10 23:41 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 02/04/10 23:41 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 02/04/10 23:41 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 02/04/10 23:41 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 02/04/10 23:41 1330-20-72.0 0.66 4-Bromofluorobenzene (S)102 %1 02/04/10 23:41 460-00-487-109 Dibromofluoromethane (S)108 %1 02/04/10 23:41 1868-53-785-115 1,2-Dichloroethane-d4 (S)115 %1 02/04/10 23:41 17060-07-079-120 Toluene-d8 (S)103 %1 02/04/10 23:41 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 18 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-13 Lab ID:9262291008 Collected:01/28/10 11:40 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 02/10/10 15:39 7440-36-002/03/10 16:436.0 2.6 Arsenic ND ug/L 1 02/10/10 15:39 7440-38-202/03/10 16:4310.0 2.7 Barium 56.1J ug/L 1 02/10/10 15:39 7440-39-302/03/10 16:431000.20 Beryllium 0.58J ug/L 1 02/10/10 15:39 7440-41-702/03/10 16:431.0 0.10 Cadmium ND ug/L 1 02/10/10 15:39 7440-43-902/03/10 16:431.0 0.50 Chromium 6.0J ug/L 1 02/10/10 15:39 7440-47-302/03/10 16:4310.0 0.40 Cobalt 3.2J ug/L 1 02/10/10 15:39 7440-48-402/03/10 16:4310.0 0.60 Copper 4.5J ug/L 1 02/10/10 15:39 7440-50-802/03/10 16:4310.0 0.30 Lead ND ug/L 1 02/10/10 15:39 7439-92-102/03/10 16:4310.0 4.0 Nickel 5.0J ug/L 1 02/10/10 15:39 7440-02-002/03/10 16:4350.0 1.7 Selenium ND ug/L 1 02/10/10 15:39 7782-49-202/03/10 16:4310.0 3.8 Silver ND ug/L 1 02/10/10 15:39 7440-22-402/03/10 16:4310.0 0.10 Thallium ND ug/L 1 02/10/10 15:39 7440-28-002/03/10 16:435.5 3.0 Vanadium 7.9J ug/L 1 02/10/10 15:39 7440-62-202/03/10 16:4325.0 0.20 Zinc 22.2 ug/L 1 02/10/10 15:39 7440-66-602/03/10 16:4310.0 0.40 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 02/05/10 00:05 67-64-11002.2 Acrylonitrile ND ug/L 1 02/05/10 00:05 107-13-12001.9 Benzene ND ug/L 1 02/05/10 00:05 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 02/05/10 00:05 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 02/05/10 00:05 75-27-41.0 0.18 Bromoform ND ug/L 1 02/05/10 00:05 75-25-23.0 0.26 Bromomethane ND ug/L 1 02/05/10 00:05 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 02/05/10 00:05 78-93-31000.96 Carbon disulfide ND ug/L 1 02/05/10 00:05 75-15-01001.2 Carbon tetrachloride ND ug/L 1 02/05/10 00:05 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 02/05/10 00:05 108-90-73.0 0.23 Chloroethane ND ug/L 1 02/05/10 00:05 75-00-310.0 0.54 Chloroform 0.45J ug/L 1 02/05/10 00:05 67-66-35.0 0.14 Chloromethane ND ug/L 1 02/05/10 00:05 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 02/05/10 00:05 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 02/05/10 00:05 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 02/05/10 00:05 106-93-41.0 0.27 Dibromomethane ND ug/L 1 02/05/10 00:05 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 02/05/10 00:05 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 02/05/10 00:05 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 02/05/10 00:05 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 02/05/10 00:05 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 02/05/10 00:05 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 02/05/10 00:05 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 02/05/10 00:05 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 02/05/10 00:05 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 02/05/10 00:05 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 02/05/10 00:05 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 02/05/10 00:05 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 19 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Sample:MW-13 Lab ID:9262291008 Collected:01/28/10 11:40 Received:01/29/10 14:12 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 02/05/10 00:05 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 02/05/10 00:05 100-41-41.0 0.30 2-Hexanone ND ug/L 1 02/05/10 00:05 591-78-650.0 0.46 Iodomethane ND ug/L 1 02/05/10 00:05 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 02/05/10 00:05 75-09-22.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 02/05/10 00:05 108-10-11000.33 Styrene ND ug/L 1 02/05/10 00:05 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 02/05/10 00:05 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 02/05/10 00:05 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 02/05/10 00:05 127-18-41.0 0.46 Toluene ND ug/L 1 02/05/10 00:05 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 02/05/10 00:05 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 02/05/10 00:05 79-00-51.0 0.29 Trichloroethene ND ug/L 1 02/05/10 00:05 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 02/05/10 00:05 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 02/05/10 00:05 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 02/05/10 00:05 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 02/05/10 00:05 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 02/05/10 00:05 1330-20-72.0 0.66 4-Bromofluorobenzene (S)101 %1 02/05/10 00:05 460-00-487-109 Dibromofluoromethane (S)107 %1 02/05/10 00:05 1868-53-785-115 1,2-Dichloroethane-d4 (S)116 %1 02/05/10 00:05 17060-07-079-120 Toluene-d8 (S)102 %1 02/05/10 00:05 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 20 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9262291 SURRY LINED, PH 2 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/5775 EPA 3010 EPA 6010 6010 MET NC Groundwater Associated Lab Samples:9262291001, 9262291002, 9262291003, 9262291004, 9262291005, 9262291006, 9262291007, 9262291008 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:398004 Associated Lab Samples:9262291001, 9262291002, 9262291003, 9262291004, 9262291005, 9262291006, 9262291007, 9262291008 Matrix:Water Analyzed Antimony ug/L ND 6.0 02/10/10 14:16 Arsenic ug/L ND 10.0 02/10/10 14:16 Barium ug/L ND 100 02/10/10 14:16 Beryllium ug/L ND 1.0 02/10/10 14:16 Cadmium ug/L ND 1.0 02/10/10 14:16 Chromium ug/L ND 10.0 02/10/10 14:16 Cobalt ug/L ND 10.0 02/10/10 14:16 Copper ug/L ND 10.0 02/10/10 14:16 Lead ug/L ND 10.0 02/10/10 14:16 Nickel ug/L ND 50.0 02/10/10 14:16 Selenium ug/L ND 10.0 02/10/10 14:16 Silver ug/L ND 10.0 02/10/10 14:16 Thallium ug/L ND 5.5 02/10/10 14:16 Vanadium ug/L ND 25.0 02/10/10 14:16 Zinc ug/L ND 10.0 02/10/10 14:16 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 398005LABORATORY CONTROL SAMPLE: LCSSpike Antimony ug/L 504500 101 80-120 Arsenic ug/L 476500 95 80-120 Barium ug/L 485500 97 80-120 Beryllium ug/L 490500 98 80-120 Cadmium ug/L 479500 96 80-120 Chromium ug/L 493500 99 80-120 Cobalt ug/L 482500 96 80-120 Copper ug/L 487500 97 80-120 Lead ug/L 480500 96 80-120 Nickel ug/L 487500 97 80-120 Selenium ug/L 470500 94 80-120 Silver ug/L 238250 95 80-120 Thallium ug/L 438500 88 80-120 Vanadium ug/L 489500 98 80-120 Zinc ug/L 482500 96 80-120 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 398006MATRIX SPIKE SAMPLE: MSSpike Result 9262217001 Antimony ug/L 488500 97 75-125ND Arsenic ug/L 473500 94 75-125ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 21 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 398006MATRIX SPIKE SAMPLE: MSSpike Result 9262217001 Barium ug/L 894500 94 75-125423 Beryllium ug/L 482500 96 75-125ND Cadmium ug/L 457500 91 75-125ND Chromium ug/L 509500 95 75-12533.0 Cobalt ug/L 472500 92 75-12514.4 Copper ug/L 521500 96 75-12538.8 Lead ug/L 442500 88 75-125ND Nickel ug/L 488500 92 75-12525.5 Selenium ug/L 470500 94 75-125ND Silver ug/L 235250 94 75-125ND Thallium ug/L 409500 81 75-1255.6 Vanadium ug/L 545500 95 75-12567.9 Zinc ug/L 515500 96 75-12537.3 Parameter Units Dup Result Max RPD QualifiersRPDResult 9262217002 398007SAMPLE DUPLICATE: Antimony ug/L ND 25ND Arsenic ug/L 5.4J 25ND Barium ug/L 258 1 25255 Beryllium ug/L 1.7 1 251.6 Cadmium ug/L ND 25ND Chromium ug/L 20.0 2 2520.4 Cobalt ug/L 15.3 1 2515.2 Copper ug/L 39.0 3 2540.3 Lead ug/L 11.2 6 2510.6 Nickel ug/L 31.7J 2 2531.2 Selenium ug/L ND 25ND Silver ug/L 0.27J 25ND Thallium ug/L ND 25ND Vanadium ug/L 48.7 0 2548.6 Zinc ug/L 52.4 1 2551.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 22 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9262291 SURRY LINED, PH 2 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/9845 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:9262291001, 9262291002, 9262291003, 9262291004, 9262291005, 9262291006, 9262291007, 9262291008 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:398487 Associated Lab Samples:9262291001, 9262291002, 9262291003, 9262291004, 9262291005, 9262291006, 9262291007, 9262291008 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/04/10 15:17 1,1,1-Trichloroethane ug/L ND 1.0 02/04/10 15:17 1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/04/10 15:17 1,1,2-Trichloroethane ug/L ND 1.0 02/04/10 15:17 1,1-Dichloroethane ug/L ND 5.0 02/04/10 15:17 1,1-Dichloroethene ug/L ND 5.0 02/04/10 15:17 1,2,3-Trichloropropane ug/L ND 1.0 02/04/10 15:17 1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/04/10 15:17 1,2-Dibromoethane (EDB)ug/L ND 1.0 02/04/10 15:17 1,2-Dichlorobenzene ug/L ND 5.0 02/04/10 15:17 1,2-Dichloroethane ug/L ND 1.0 02/04/10 15:17 1,2-Dichloropropane ug/L ND 1.0 02/04/10 15:17 1,3-Dichloropropane ug/L ND 1.0 02/04/10 15:17 1,4-Dichlorobenzene ug/L ND 1.0 02/04/10 15:17 2-Butanone (MEK)ug/L ND 100 02/04/10 15:17 2-Hexanone ug/L ND 50.0 02/04/10 15:17 4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/04/10 15:17 Acetone ug/L ND 100 02/04/10 15:17 Acrylonitrile ug/L ND 200 02/04/10 15:17 Benzene ug/L ND 1.0 02/04/10 15:17 Bromochloromethane ug/L ND 3.0 02/04/10 15:17 Bromodichloromethane ug/L 0.26J 1.0 02/04/10 15:17 Bromoform ug/L ND 3.0 02/04/10 15:17 Bromomethane ug/L ND 10.0 02/04/10 15:17 Carbon disulfide ug/L ND 100 02/04/10 15:17 Carbon tetrachloride ug/L ND 1.0 02/04/10 15:17 Chlorobenzene ug/L ND 3.0 02/04/10 15:17 Chloroethane ug/L ND 10.0 02/04/10 15:17 Chloroform ug/L 0.47J 5.0 02/04/10 15:17 Chloromethane ug/L ND 1.0 02/04/10 15:17 cis-1,2-Dichloroethene ug/L ND 5.0 02/04/10 15:17 cis-1,3-Dichloropropene ug/L ND 1.0 02/04/10 15:17 Dibromochloromethane ug/L ND 3.0 02/04/10 15:17 Dibromomethane ug/L ND 10.0 02/04/10 15:17 Ethylbenzene ug/L ND 1.0 02/04/10 15:17 Iodomethane ug/L ND 10.0 02/04/10 15:17 Methylene Chloride ug/L 2.2 2.0 C902/04/10 15:17 Styrene ug/L ND 1.0 02/04/10 15:17 Tetrachloroethene ug/L ND 1.0 02/04/10 15:17 Toluene ug/L ND 1.0 02/04/10 15:17 trans-1,2-Dichloroethene ug/L ND 5.0 02/04/10 15:17 trans-1,3-Dichloropropene ug/L ND 1.0 02/04/10 15:17 trans-1,4-Dichloro-2-butene ug/L ND 100 02/04/10 15:17 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 23 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:398487 Associated Lab Samples:9262291001, 9262291002, 9262291003, 9262291004, 9262291005, 9262291006, 9262291007, 9262291008 Matrix:Water Analyzed Trichloroethene ug/L ND 1.0 02/04/10 15:17 Trichlorofluoromethane ug/L ND 1.0 02/04/10 15:17 Vinyl acetate ug/L ND 50.0 02/04/10 15:17 Vinyl chloride ug/L ND 1.0 02/04/10 15:17 Xylene (Total)ug/L ND 2.0 02/04/10 15:17 1,2-Dichloroethane-d4 (S)%109 79-120 02/04/10 15:17 4-Bromofluorobenzene (S)%99 87-109 02/04/10 15:17 Dibromofluoromethane (S)%106 85-115 02/04/10 15:17 Toluene-d8 (S)%103 70-120 02/04/10 15:17 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 398488LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 49.950 100 83-125 1,1,1-Trichloroethane ug/L 54.050 108 80-129 1,1,2,2-Tetrachloroethane ug/L 48.350 97 73-127 1,1,2-Trichloroethane ug/L 53.350 107 77-123 1,1-Dichloroethane ug/L 57.550 115 76-129 1,1-Dichloroethene ug/L 52.850 106 78-146 1,2,3-Trichloropropane ug/L 49.650 99 72-125 1,2-Dibromo-3-chloropropane ug/L 50.150 100 65-128 1,2-Dibromoethane (EDB)ug/L 50.950 102 81-125 1,2-Dichlorobenzene ug/L 52.050 104 82-126 1,2-Dichloroethane ug/L 52.250 104 72-126 1,2-Dichloropropane ug/L 50.950 102 80-127 1,3-Dichloropropane ug/L 50.550 101 79-124 1,4-Dichlorobenzene ug/L 50.850 102 79-125 2-Butanone (MEK)ug/L 101100 101 50-134 2-Hexanone ug/L 112100 112 58-138 4-Methyl-2-pentanone (MIBK)ug/L 112100 112 70-131 Acetone ug/L 83.5J100 83 50-146 Acrylonitrile ug/L 282250 113 66-124 Benzene ug/L 50.250 100 78-128 Bromochloromethane ug/L 55.650 111 73-124 Bromodichloromethane ug/L 50.250 100 81-125 Bromoform ug/L 49.050 98 71-125 Bromomethane ug/L 25.950 52 50-150 Carbon disulfide ug/L 48.3J50 97 54-150 Carbon tetrachloride ug/L 55.050 110 81-137 Chlorobenzene ug/L 51.750 103 82-126 Chloroethane ug/L 46.650 93 69-140 Chloroform ug/L 50.550 101 77-129 Chloromethane ug/L 39.450 79 54-139 cis-1,2-Dichloroethene ug/L 53.350 107 76-133 cis-1,3-Dichloropropene ug/L 53.550 107 76-127 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 24 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9262291 SURRY LINED, PH 2 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 398488LABORATORY CONTROL SAMPLE: LCSSpike Dibromochloromethane ug/L 49.150 98 77-125 Dibromomethane ug/L 55.150 110 77-125 Ethylbenzene ug/L 51.850 104 80-127 Iodomethane ug/L 101100 101 65-172 Methylene Chloride ug/L 50.850 102 67-133 Styrene ug/L 53.050 106 80-130 Tetrachloroethene ug/L 49.750 99 78-128 Toluene ug/L 51.150 102 76-126 trans-1,2-Dichloroethene ug/L 51.750 103 78-134 trans-1,3-Dichloropropene ug/L 54.350 109 75-125 trans-1,4-Dichloro-2-butene ug/L 63.4J50 127 51-140 Trichloroethene ug/L 50.950 102 79-127 Trichlorofluoromethane ug/L 45.850 92 76-148 Vinyl acetate ug/L 124100 124 50-150 Vinyl chloride ug/L 39.850 80 67-143 Xylene (Total)ug/L 154150 103 83-125 1,2-Dichloroethane-d4 (S)%102 79-120 4-Bromofluorobenzene (S)%102 87-109 Dibromofluoromethane (S)%102 85-115 Toluene-d8 (S)%101 70-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 398489MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9262291006 398490 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1-Dichloroethene ug/L 50 129 60-150127 2 3050ND64.7 63.7 Benzene ug/L 50 119 74-136117 2 3050ND59.3 58.4 Chlorobenzene ug/L 50 122 79-135122 0 3050ND61.0 61.2 Toluene ug/L 50 125 73-131123 2 3050ND62.7 61.3 Trichloroethene ug/L 50 121 73-131120 1 3050ND60.5 59.8 1,2-Dichloroethane-d4 (S)%114 79-120114 4-Bromofluorobenzene (S)%101 87-109102 Dibromofluoromethane (S)%106 85-115107 Toluene-d8 (S)%101 70-120101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 25 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Pace Project No.: Project: 9262291 SURRY LINED, PH 2 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. U - Indicates the compound was analyzed for, but not detected. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Common Laboratory Contaminant.C9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 02/12/2010 02:59 PM Page 26 of 26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 June 15, 2011 LIMS USE: FR - JONATHAN PFOHL LIMS OBJECT ID: 9294822 9294822 Project: Pace Project No.: RE: Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 SURRY CO. LINED MSWLF Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory between May 24, 2011 and May 25, 2011. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures cc:Ms. Maggie German, Municipal Engineering Services REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 CERTIFICATIONS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034 New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213 Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030New Jersey Certification #: NC011 North Carolina Bioassay Certification #: 9North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002 South Carolina Certification #: 99030001Virginia Certification #: 00072 West Virginia Certification #: 356 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 SAMPLE SUMMARY Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Lab ID Sample ID Matrix Date Collected Date Received 9294822001 MW-1 Water 05/23/11 10:30 05/24/11 15:45 9294822002 MW-2 Water 05/23/11 11:00 05/24/11 15:45 9294822003 MW-3R Water 05/23/11 11:35 05/24/11 15:45 9294822004 MW-4S Water 05/23/11 12:10 05/24/11 15:45 9294822005 MW-4D Water 05/23/11 13:50 05/24/11 15:45 9294822006 MW-5 Water 05/23/11 14:25 05/24/11 15:45 9294822007 MW-6R Water 05/23/11 15:35 05/24/11 15:45 9294822008 MW-8 Water 05/23/11 15:00 05/24/11 15:45 9294822009 MW-10 Water 05/23/11 17:00 05/24/11 15:45 9294822010 MW-11S Water 05/23/11 16:25 05/24/11 15:45 9294822011 MW-11D Water 05/23/11 15:40 05/24/11 15:45 9294822012 LAGOON Water 05/23/11 17:20 05/24/11 15:45 9294822013 MW-9S Water 05/24/11 00:00 05/25/11 15:35 9294822014 MW-9D Water 05/24/11 00:00 05/25/11 15:35 9294822015 MW-12 Water 05/24/11 00:00 05/25/11 15:35 9294822016 MW-13 Water 05/24/11 00:00 05/25/11 15:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 SAMPLE ANALYTE COUNT Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 9294822001 MW-1 EPA 6010 15 PASI-AJDA, JMW EPA 8260 52 PASI-CMCK 9294822002 MW-2 EPA 6010 15 PASI-AJDA, JMW EPA 8260 52 PASI-CMCK 9294822003 MW-3R EPA 6010 15 PASI-AJDA, JMW EPA 8260 52 PASI-CMCK 9294822004 MW-4S EPA 6010 15 PASI-AJDA, JMW EPA 8260 52 PASI-CMCK 9294822005 MW-4D EPA 6010 15 PASI-AJMW EPA 8260 52 PASI-CMCK 9294822006 MW-5 EPA 6010 15 PASI-AJMW EPA 8260 52 PASI-CMCK 9294822007 MW-6R EPA 6010 15 PASI-AJMW EPA 8260 52 PASI-CMCK 9294822008 MW-8 EPA 6010 15 PASI-AJMW EPA 8260 52 PASI-CMCK 9294822009 MW-10 EPA 6010 15 PASI-AJDA, JMW EPA 8260 52 PASI-CMCK 9294822010 MW-11S EPA 6010 15 PASI-AJDA, JMW EPA 8260 52 PASI-CMCK 9294822011 MW-11D EPA 6010 15 PASI-AJDA, JMW EPA 8260 52 PASI-CMCK 9294822012 LAGOON EPA 6010 15 PASI-AJDA, JMW EPA 8260 52 PASI-CMCK SM 5210B 1 PASI-AGW1 EPA 9040 1 PASI-ASAJ EPA 300.0 1 PASI-AEWS EPA 353.2 1 PASI-ADMN EPA 365.1 1 PASI-ALEP SM 5220D 1 PASI-ASDH 9294822013 MW-9S EPA 6010 15 PASI-AJMW EPA 8260 52 PASI-CMCK 9294822014 MW-9D EPA 6010 15 PASI-AJMW EPA 8260 52 PASI-CMCK 9294822015 MW-12 EPA 6010 15 PASI-AJMW EPA 8260 52 PASI-CMCK 9294822016 MW-13 EPA 6010 15 PASI-AJMW REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 SAMPLE ANALYTE COUNT Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts EPA 8260 52 PASI-CMCK REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-1 Lab ID:9294822001 Collected:05/23/11 10:30 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/27/11 18:14 7440-36-005/26/11 16:006.0 2.6 Arsenic 18.6 ug/L 1 05/28/11 20:49 7440-38-205/26/11 16:0010.0 2.7 Barium 942 ug/L 1 05/27/11 18:14 7440-39-305/26/11 16:001000.20 Beryllium 13.7 ug/L 1 05/27/11 18:14 7440-41-705/26/11 16:001.0 0.10 Cadmium 28.4 ug/L 1 05/27/11 18:14 7440-43-905/26/11 16:001.0 0.50 Chromium 300 ug/L 1 05/27/11 18:14 7440-47-305/26/11 16:0010.0 0.40 Cobalt 25.0 ug/L 1 05/27/11 18:14 7440-48-405/26/11 16:0010.0 0.60 Copper 456 ug/L 1 05/27/11 18:14 7440-50-805/26/11 16:0010.0 0.30 Lead 92.9 ug/L 1 05/27/11 18:14 7439-92-105/26/11 16:0010.0 4.0 Nickel 90.5 ug/L 1 05/27/11 18:14 7440-02-005/26/11 16:0050.0 1.7 Selenium 9.6J ug/L 1 05/27/11 18:14 7782-49-205/26/11 16:0010.0 3.8 Silver 1.2J ug/L 1 05/27/11 18:14 7440-22-405/26/11 16:0010.0 0.10 Thallium ND ug/L 1 05/27/11 18:14 7440-28-005/26/11 16:005.5 3.0 Vanadium 249 ug/L 1 05/27/11 18:14 7440-62-205/26/11 16:0025.0 0.20 Zinc 806 ug/L 1 05/27/11 18:14 7440-66-605/26/11 16:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 3.7J ug/L 1 05/25/11 20:00 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 20:00 107-13-12001.9 Benzene ND ug/L 1 05/25/11 20:00 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 20:00 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 20:00 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 20:00 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 20:00 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 20:00 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 20:00 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 20:00 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 20:00 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 20:00 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 20:00 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 20:00 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 20:00 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 20:00 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 20:00 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 20:00 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 20:00 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 20:00 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 20:00 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/25/11 20:00 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 20:00 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 20:00 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/25/11 20:00 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 20:00 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 20:00 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 20:00 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 20:00 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 6 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-1 Lab ID:9294822001 Collected:05/23/11 10:30 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 20:00 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 20:00 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 20:00 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 20:00 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 20:00 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 20:00 108-10-11000.33 Styrene ND ug/L 1 05/25/11 20:00 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 20:00 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 20:00 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/25/11 20:00 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 20:00 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 20:00 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 20:00 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 20:00 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/25/11 20:00 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 20:00 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 20:00 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 20:00 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 20:00 1330-20-75.0 0.66 4-Bromofluorobenzene (S)97 %1 05/25/11 20:00 460-00-470-130 Dibromofluoromethane (S)105 %1 05/25/11 20:00 1868-53-770-130 1,2-Dichloroethane-d4 (S)104 %1 05/25/11 20:00 17060-07-070-130 Toluene-d8 (S)100 %1 05/25/11 20:00 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 7 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-2 Lab ID:9294822002 Collected:05/23/11 11:00 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/27/11 18:22 7440-36-005/26/11 16:006.0 2.6 Arsenic ND ug/L 1 05/28/11 20:57 7440-38-205/26/11 16:0010.0 2.7 Barium 35.4J ug/L 1 05/27/11 18:22 7440-39-305/26/11 16:001000.20 Beryllium ND ug/L 1 05/27/11 18:22 7440-41-705/26/11 16:001.0 0.10 Cadmium ND ug/L 1 05/27/11 18:22 7440-43-905/26/11 16:001.0 0.50 Chromium 2.4J ug/L 1 05/27/11 18:22 7440-47-305/26/11 16:0010.0 0.40 Cobalt ND ug/L 1 05/27/11 18:22 7440-48-405/26/11 16:0010.0 0.60 Copper ND ug/L 1 05/27/11 18:22 7440-50-805/26/11 16:0010.0 0.30 Lead ND ug/L 1 05/27/11 18:22 7439-92-105/26/11 16:0010.0 4.0 Nickel ND ug/L 1 05/27/11 18:22 7440-02-005/26/11 16:0050.0 1.7 Selenium ND ug/L 1 05/27/11 18:22 7782-49-205/26/11 16:0010.0 3.8 Silver ND ug/L 1 05/27/11 18:22 7440-22-405/26/11 16:0010.0 0.10 Thallium ND ug/L 1 05/27/11 18:22 7440-28-005/26/11 16:005.5 3.0 Vanadium 0.27J ug/L 1 05/27/11 18:22 7440-62-205/26/11 16:0025.0 0.20 Zinc 7.2J ug/L 1 05/27/11 18:22 7440-66-605/26/11 16:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 2.2J ug/L 1 05/25/11 20:26 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 20:26 107-13-12001.9 Benzene ND ug/L 1 05/25/11 20:26 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 20:26 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 20:26 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 20:26 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 20:26 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 20:26 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 20:26 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 20:26 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 20:26 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 20:26 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 20:26 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 20:26 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 20:26 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 20:26 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 20:26 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 20:26 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 20:26 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 20:26 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 20:26 110-57-61001.0 1,1-Dichloroethane 3.2J ug/L 1 05/25/11 20:26 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 20:26 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 20:26 75-35-45.0 0.56 cis-1,2-Dichloroethene 1.0J ug/L 1 05/25/11 20:26 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 20:26 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 20:26 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 20:26 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 20:26 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 8 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-2 Lab ID:9294822002 Collected:05/23/11 11:00 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 20:26 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 20:26 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 20:26 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 20:26 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 20:26 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 20:26 108-10-11000.33 Styrene ND ug/L 1 05/25/11 20:26 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 20:26 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 20:26 79-34-53.0 0.40 Tetrachloroethene 0.92J ug/L 1 05/25/11 20:26 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 20:26 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 20:26 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 20:26 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 20:26 79-01-61.0 0.47 Trichlorofluoromethane 0.46J ug/L 1 05/25/11 20:26 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 20:26 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 20:26 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 20:26 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 20:26 1330-20-75.0 0.66 4-Bromofluorobenzene (S)98 %1 05/25/11 20:26 460-00-470-130 Dibromofluoromethane (S)102 %1 05/25/11 20:26 1868-53-770-130 1,2-Dichloroethane-d4 (S)104 %1 05/25/11 20:26 17060-07-070-130 Toluene-d8 (S)97 %1 05/25/11 20:26 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 9 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-3R Lab ID:9294822003 Collected:05/23/11 11:35 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/27/11 18:25 7440-36-005/26/11 16:006.0 2.6 Arsenic ND ug/L 1 05/28/11 21:00 7440-38-205/26/11 16:0010.0 2.7 Barium 83.8J ug/L 1 05/27/11 18:25 7440-39-305/26/11 16:001000.20 Beryllium ND ug/L 1 05/27/11 18:25 7440-41-705/26/11 16:001.0 0.10 Cadmium 1.9 ug/L 1 05/27/11 18:25 7440-43-905/26/11 16:001.0 0.50 Chromium 1.7J ug/L 1 05/27/11 18:25 7440-47-305/26/11 16:0010.0 0.40 Cobalt ND ug/L 1 05/27/11 18:25 7440-48-405/26/11 16:0010.0 0.60 Copper 1.1J ug/L 1 05/27/11 18:25 7440-50-805/26/11 16:0010.0 0.30 Lead ND ug/L 1 05/27/11 18:25 7439-92-105/26/11 16:0010.0 4.0 Nickel 3.6J ug/L 1 05/27/11 18:25 7440-02-005/26/11 16:0050.0 1.7 Selenium ND ug/L 1 05/27/11 18:25 7782-49-205/26/11 16:0010.0 3.8 Silver ND ug/L 1 05/27/11 18:25 7440-22-405/26/11 16:0010.0 0.10 Thallium ND ug/L 1 05/27/11 18:25 7440-28-005/26/11 16:005.5 3.0 Vanadium ND ug/L 1 05/27/11 18:25 7440-62-205/26/11 16:0025.0 0.20 Zinc 5.4J ug/L 1 05/27/11 18:25 7440-66-605/26/11 16:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 1 05/25/11 20:51 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 20:51 107-13-12001.9 Benzene ND ug/L 1 05/25/11 20:51 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 20:51 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 20:51 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 20:51 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 20:51 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 20:51 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 20:51 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 20:51 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 20:51 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 20:51 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 20:51 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 20:51 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 20:51 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 20:51 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 20:51 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 20:51 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 20:51 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 20:51 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 20:51 110-57-61001.0 1,1-Dichloroethane 2.1J ug/L 1 05/25/11 20:51 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 20:51 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 20:51 75-35-45.0 0.56 cis-1,2-Dichloroethene 1.5J ug/L 1 05/25/11 20:51 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 20:51 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 20:51 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 20:51 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 20:51 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 10 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-3R Lab ID:9294822003 Collected:05/23/11 11:35 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 20:51 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 20:51 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 20:51 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 20:51 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 20:51 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 20:51 108-10-11000.33 Styrene ND ug/L 1 05/25/11 20:51 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 20:51 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 20:51 79-34-53.0 0.40 Tetrachloroethene 0.46J ug/L 1 05/25/11 20:51 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 20:51 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 20:51 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 20:51 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 20:51 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/25/11 20:51 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 20:51 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 20:51 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 20:51 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 20:51 1330-20-75.0 0.66 4-Bromofluorobenzene (S)98 %1 05/25/11 20:51 460-00-470-130 Dibromofluoromethane (S)103 %1 05/25/11 20:51 1868-53-770-130 1,2-Dichloroethane-d4 (S)106 %1 05/25/11 20:51 17060-07-070-130 Toluene-d8 (S)100 %1 05/25/11 20:51 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 11 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-4S Lab ID:9294822004 Collected:05/23/11 12:10 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/27/11 18:29 7440-36-005/26/11 16:006.0 2.6 Arsenic ND ug/L 1 05/28/11 21:04 7440-38-205/26/11 16:0010.0 2.7 Barium 38.8J ug/L 1 05/27/11 18:29 7440-39-305/26/11 16:001000.20 Beryllium 0.10J ug/L 1 05/27/11 18:29 7440-41-705/26/11 16:001.0 0.10 Cadmium 0.57J ug/L 1 05/27/11 18:29 7440-43-905/26/11 16:001.0 0.50 Chromium 2.2J ug/L 1 05/27/11 18:29 7440-47-305/26/11 16:0010.0 0.40 Cobalt 0.77J ug/L 1 05/27/11 18:29 7440-48-405/26/11 16:0010.0 0.60 Copper 0.72J ug/L 1 05/27/11 18:29 7440-50-805/26/11 16:0010.0 0.30 Lead ND ug/L 1 05/27/11 18:29 7439-92-105/26/11 16:0010.0 4.0 Nickel ND ug/L 1 05/27/11 18:29 7440-02-005/26/11 16:0050.0 1.7 Selenium ND ug/L 1 05/27/11 18:29 7782-49-205/26/11 16:0010.0 3.8 Silver ND ug/L 1 05/27/11 18:29 7440-22-405/26/11 16:0010.0 0.10 Thallium ND ug/L 1 05/27/11 18:29 7440-28-005/26/11 16:005.5 3.0 Vanadium 1.1J ug/L 1 05/27/11 18:29 7440-62-205/26/11 16:0025.0 0.20 Zinc 3.7J ug/L 1 05/27/11 18:29 7440-66-605/26/11 16:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 1 05/25/11 21:17 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 21:17 107-13-12001.9 Benzene ND ug/L 1 05/25/11 21:17 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 21:17 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 21:17 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 21:17 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 21:17 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 21:17 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 21:17 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 21:17 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 21:17 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 21:17 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 21:17 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 21:17 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 21:17 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 21:17 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 21:17 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 21:17 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 21:17 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 21:17 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 21:17 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/25/11 21:17 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 21:17 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 21:17 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/25/11 21:17 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 21:17 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 21:17 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 21:17 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 21:17 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 12 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-4S Lab ID:9294822004 Collected:05/23/11 12:10 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 21:17 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 21:17 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 21:17 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 21:17 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 21:17 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 21:17 108-10-11000.33 Styrene ND ug/L 1 05/25/11 21:17 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 21:17 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 21:17 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/25/11 21:17 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 21:17 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 21:17 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 21:17 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 21:17 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/25/11 21:17 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 21:17 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 21:17 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 21:17 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 21:17 1330-20-75.0 0.66 4-Bromofluorobenzene (S)94 %1 05/25/11 21:17 460-00-470-130 Dibromofluoromethane (S)109 %1 05/25/11 21:17 1868-53-770-130 1,2-Dichloroethane-d4 (S)110 %1 05/25/11 21:17 17060-07-070-130 Toluene-d8 (S)100 %1 05/25/11 21:17 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 13 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-4D Lab ID:9294822005 Collected:05/23/11 13:50 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/27/11 18:44 7440-36-005/26/11 16:006.0 2.6 Arsenic ND ug/L 1 05/27/11 18:44 7440-38-205/26/11 16:0010.0 2.7 Barium 30.7J ug/L 1 05/27/11 18:44 7440-39-305/26/11 16:001000.20 Beryllium ND ug/L 1 05/27/11 18:44 7440-41-705/26/11 16:001.0 0.10 Cadmium 5.9 ug/L 1 05/27/11 18:44 7440-43-905/26/11 16:001.0 0.50 Chromium 0.46J ug/L 1 05/27/11 18:44 7440-47-305/26/11 16:0010.0 0.40 Cobalt 1.1J ug/L 1 05/27/11 18:44 7440-48-405/26/11 16:0010.0 0.60 Copper 4.4J ug/L 1 05/27/11 18:44 7440-50-805/26/11 16:0010.0 0.30 Lead ND ug/L 1 05/27/11 18:44 7439-92-105/26/11 16:0010.0 4.0 Nickel ND ug/L 1 05/27/11 18:44 7440-02-005/26/11 16:0050.0 1.7 Selenium ND ug/L 1 05/27/11 18:44 7782-49-205/26/11 16:0010.0 3.8 Silver ND ug/L 1 05/27/11 18:44 7440-22-405/26/11 16:0010.0 0.10 Thallium ND ug/L 1 05/27/11 18:44 7440-28-005/26/11 16:005.5 3.0 Vanadium ND ug/L 1 05/27/11 18:44 7440-62-205/26/11 16:0025.0 0.20 Zinc 26.2 ug/L 1 05/27/11 18:44 7440-66-605/26/11 16:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 3.8J ug/L 1 05/25/11 21:42 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 21:42 107-13-12001.9 Benzene ND ug/L 1 05/25/11 21:42 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 21:42 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 21:42 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 21:42 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 21:42 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 21:42 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 21:42 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 21:42 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 21:42 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 21:42 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 21:42 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 21:42 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 21:42 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 21:42 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 21:42 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 21:42 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 21:42 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 21:42 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 21:42 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/25/11 21:42 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 21:42 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 21:42 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/25/11 21:42 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 21:42 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 21:42 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 21:42 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 21:42 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 14 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-4D Lab ID:9294822005 Collected:05/23/11 13:50 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 21:42 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 21:42 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 21:42 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 21:42 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 21:42 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 21:42 108-10-11000.33 Styrene ND ug/L 1 05/25/11 21:42 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 21:42 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 21:42 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/25/11 21:42 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 21:42 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 21:42 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 21:42 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 21:42 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/25/11 21:42 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 21:42 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 21:42 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 21:42 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 21:42 1330-20-75.0 0.66 4-Bromofluorobenzene (S)94 %1 05/25/11 21:42 460-00-470-130 Dibromofluoromethane (S)109 %1 05/25/11 21:42 1868-53-770-130 1,2-Dichloroethane-d4 (S)107 %1 05/25/11 21:42 17060-07-070-130 Toluene-d8 (S)100 %1 05/25/11 21:42 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 15 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-5 Lab ID:9294822006 Collected:05/23/11 14:25 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/27/11 18:47 7440-36-005/26/11 16:006.0 2.6 Arsenic ND ug/L 1 05/27/11 18:47 7440-38-205/26/11 16:0010.0 2.7 Barium 15.4J ug/L 1 05/27/11 18:47 7440-39-305/26/11 16:001000.20 Beryllium ND ug/L 1 05/27/11 18:47 7440-41-705/26/11 16:001.0 0.10 Cadmium ND ug/L 1 05/27/11 18:47 7440-43-905/26/11 16:001.0 0.50 Chromium 0.65J ug/L 1 05/27/11 18:47 7440-47-305/26/11 16:0010.0 0.40 Cobalt 1.2J ug/L 1 05/27/11 18:47 7440-48-405/26/11 16:0010.0 0.60 Copper 0.80J ug/L 1 05/27/11 18:47 7440-50-805/26/11 16:0010.0 0.30 Lead ND ug/L 1 05/27/11 18:47 7439-92-105/26/11 16:0010.0 4.0 Nickel ND ug/L 1 05/27/11 18:47 7440-02-005/26/11 16:0050.0 1.7 Selenium ND ug/L 1 05/27/11 18:47 7782-49-205/26/11 16:0010.0 3.8 Silver ND ug/L 1 05/27/11 18:47 7440-22-405/26/11 16:0010.0 0.10 Thallium ND ug/L 1 05/27/11 18:47 7440-28-005/26/11 16:005.5 3.0 Vanadium ND ug/L 1 05/27/11 18:47 7440-62-205/26/11 16:0025.0 0.20 Zinc 5.4J ug/L 1 05/27/11 18:47 7440-66-605/26/11 16:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 4.9J ug/L 1 05/25/11 22:07 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 22:07 107-13-12001.9 Benzene ND ug/L 1 05/25/11 22:07 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 22:07 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 22:07 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 22:07 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 22:07 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 22:07 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 22:07 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 22:07 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 22:07 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 22:07 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 22:07 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 22:07 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 22:07 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 22:07 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 22:07 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 22:07 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 22:07 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 22:07 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 22:07 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/25/11 22:07 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 22:07 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 22:07 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/25/11 22:07 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 22:07 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 22:07 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 22:07 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 22:07 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 16 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-5 Lab ID:9294822006 Collected:05/23/11 14:25 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 22:07 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 22:07 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 22:07 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 22:07 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 22:07 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 22:07 108-10-11000.33 Styrene ND ug/L 1 05/25/11 22:07 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 22:07 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 22:07 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/25/11 22:07 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 22:07 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 22:07 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 22:07 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 22:07 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/25/11 22:07 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 22:07 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 22:07 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 22:07 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 22:07 1330-20-75.0 0.66 4-Bromofluorobenzene (S)97 %1 05/25/11 22:07 460-00-470-130 Dibromofluoromethane (S)109 %1 05/25/11 22:07 1868-53-770-130 1,2-Dichloroethane-d4 (S)109 %1 05/25/11 22:07 17060-07-070-130 Toluene-d8 (S)98 %1 05/25/11 22:07 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 17 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-6R Lab ID:9294822007 Collected:05/23/11 15:35 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/27/11 18:50 7440-36-005/26/11 16:006.0 2.6 Arsenic ND ug/L 1 05/27/11 18:50 7440-38-205/26/11 16:0010.0 2.7 Barium 47.5J ug/L 1 05/27/11 18:50 7440-39-305/26/11 16:001000.20 Beryllium 0.28J ug/L 1 05/27/11 18:50 7440-41-705/26/11 16:001.0 0.10 Cadmium ND ug/L 1 05/27/11 18:50 7440-43-905/26/11 16:001.0 0.50 Chromium 4.1J ug/L 1 05/27/11 18:50 7440-47-305/26/11 16:0010.0 0.40 Cobalt 2.6J ug/L 1 05/27/11 18:50 7440-48-405/26/11 16:0010.0 0.60 Copper 6.6J ug/L 1 05/27/11 18:50 7440-50-805/26/11 16:0010.0 0.30 Lead ND ug/L 1 05/27/11 18:50 7439-92-105/26/11 16:0010.0 4.0 Nickel 3.3J ug/L 1 05/27/11 18:50 7440-02-005/26/11 16:0050.0 1.7 Selenium ND ug/L 1 05/27/11 18:50 7782-49-205/26/11 16:0010.0 3.8 Silver ND ug/L 1 05/27/11 18:50 7440-22-405/26/11 16:0010.0 0.10 Thallium ND ug/L 1 05/27/11 18:50 7440-28-005/26/11 16:005.5 3.0 Vanadium 4.1J ug/L 1 05/27/11 18:50 7440-62-205/26/11 16:0025.0 0.20 Zinc 13.9 ug/L 1 05/27/11 18:50 7440-66-605/26/11 16:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 2.8J ug/L 1 05/25/11 22:33 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 22:33 107-13-12001.9 Benzene ND ug/L 1 05/25/11 22:33 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 22:33 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 22:33 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 22:33 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 22:33 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 22:33 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 22:33 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 22:33 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 22:33 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 22:33 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 22:33 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 22:33 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 22:33 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 22:33 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 22:33 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 22:33 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 22:33 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 22:33 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 22:33 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/25/11 22:33 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 22:33 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 22:33 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/25/11 22:33 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 22:33 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 22:33 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 22:33 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 22:33 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 18 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-6R Lab ID:9294822007 Collected:05/23/11 15:35 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 22:33 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 22:33 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 22:33 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 22:33 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 22:33 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 22:33 108-10-11000.33 Styrene ND ug/L 1 05/25/11 22:33 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 22:33 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 22:33 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/25/11 22:33 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 22:33 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 22:33 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 22:33 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 22:33 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/25/11 22:33 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 22:33 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 22:33 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 22:33 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 22:33 1330-20-75.0 0.66 4-Bromofluorobenzene (S)96 %1 05/25/11 22:33 460-00-470-130 Dibromofluoromethane (S)111 %1 05/25/11 22:33 1868-53-770-130 1,2-Dichloroethane-d4 (S)108 %1 05/25/11 22:33 17060-07-070-130 Toluene-d8 (S)100 %1 05/25/11 22:33 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 19 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-8 Lab ID:9294822008 Collected:05/23/11 15:00 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/27/11 18:53 7440-36-005/26/11 16:006.0 2.6 Arsenic ND ug/L 1 05/27/11 18:53 7440-38-205/26/11 16:0010.0 2.7 Barium 57.6J ug/L 1 05/27/11 18:53 7440-39-305/26/11 16:001000.20 Beryllium 0.19J ug/L 1 05/27/11 18:53 7440-41-705/26/11 16:001.0 0.10 Cadmium ND ug/L 1 05/27/11 18:53 7440-43-905/26/11 16:001.0 0.50 Chromium 2.6J ug/L 1 05/27/11 18:53 7440-47-305/26/11 16:0010.0 0.40 Cobalt 1.3J ug/L 1 05/27/11 18:53 7440-48-405/26/11 16:0010.0 0.60 Copper 1.5J ug/L 1 05/27/11 18:53 7440-50-805/26/11 16:0010.0 0.30 Lead ND ug/L 1 05/27/11 18:53 7439-92-105/26/11 16:0010.0 4.0 Nickel ND ug/L 1 05/27/11 18:53 7440-02-005/26/11 16:0050.0 1.7 Selenium ND ug/L 1 05/27/11 18:53 7782-49-205/26/11 16:0010.0 3.8 Silver ND ug/L 1 05/27/11 18:53 7440-22-405/26/11 16:0010.0 0.10 Thallium ND ug/L 1 05/27/11 18:53 7440-28-005/26/11 16:005.5 3.0 Vanadium 3.0J ug/L 1 05/27/11 18:53 7440-62-205/26/11 16:0025.0 0.20 Zinc 6.1J ug/L 1 05/27/11 18:53 7440-66-605/26/11 16:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 2.7J ug/L 1 05/25/11 22:58 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 22:58 107-13-12001.9 Benzene ND ug/L 1 05/25/11 22:58 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 22:58 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 22:58 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 22:58 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 22:58 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 22:58 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 22:58 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 22:58 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 22:58 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 22:58 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 22:58 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 22:58 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 22:58 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 22:58 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 22:58 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 22:58 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 22:58 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 22:58 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 22:58 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/25/11 22:58 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 22:58 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 22:58 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/25/11 22:58 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 22:58 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 22:58 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 22:58 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 22:58 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 20 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-8 Lab ID:9294822008 Collected:05/23/11 15:00 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 22:58 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 22:58 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 22:58 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 22:58 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 22:58 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 22:58 108-10-11000.33 Styrene ND ug/L 1 05/25/11 22:58 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 22:58 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 22:58 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/25/11 22:58 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 22:58 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 22:58 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 22:58 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 22:58 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/25/11 22:58 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 22:58 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 22:58 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 22:58 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 22:58 1330-20-75.0 0.66 4-Bromofluorobenzene (S)96 %1 05/25/11 22:58 460-00-470-130 Dibromofluoromethane (S)108 %1 05/25/11 22:58 1868-53-770-130 1,2-Dichloroethane-d4 (S)108 %1 05/25/11 22:58 17060-07-070-130 Toluene-d8 (S)101 %1 05/25/11 22:58 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 21 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-10 Lab ID:9294822009 Collected:05/23/11 17:00 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/28/11 21:14 7440-36-005/27/11 17:006.0 2.6 Arsenic ND ug/L 1 05/28/11 21:14 7440-38-205/27/11 17:0010.0 2.7 Barium 45.4J ug/L 1 05/28/11 21:14 7440-39-305/27/11 17:001000.20 Beryllium ND ug/L 1 05/28/11 21:14 7440-41-705/27/11 17:001.0 0.10 Cadmium ND ug/L 1 05/28/11 21:14 7440-43-905/27/11 17:001.0 0.50 Chromium 3.0J ug/L 1 05/28/11 21:14 7440-47-305/27/11 17:0010.0 0.40 Cobalt 1.3J ug/L 1 05/28/11 21:14 7440-48-405/27/11 17:0010.0 0.60 Copper 1.2J ug/L 1 05/28/11 21:14 7440-50-805/27/11 17:0010.0 0.30 Lead ND ug/L 1 05/28/11 21:14 7439-92-105/27/11 17:0010.0 4.0 Nickel ND ug/L 1 05/28/11 21:14 7440-02-005/27/11 17:0050.0 1.7 Selenium ND ug/L 1 05/28/11 21:14 7782-49-205/27/11 17:0010.0 3.8 Silver ND ug/L 1 05/28/11 21:14 7440-22-405/27/11 17:0010.0 0.10 Thallium 6.1 ug/L 1 05/31/11 11:27 7440-28-005/27/11 17:005.5 3.0 Vanadium 2.0J ug/L 1 05/28/11 21:14 7440-62-205/27/11 17:0025.0 0.20 Zinc 10.5 ug/L 1 05/28/11 21:14 7440-66-605/27/11 17:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 3.7J ug/L 1 05/25/11 23:24 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 23:24 107-13-12001.9 Benzene ND ug/L 1 05/25/11 23:24 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 23:24 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 23:24 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 23:24 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 23:24 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 23:24 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 23:24 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 23:24 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 23:24 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 23:24 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 23:24 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 23:24 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 23:24 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 23:24 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 23:24 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 23:24 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 23:24 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 23:24 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 23:24 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/25/11 23:24 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 23:24 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 23:24 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/25/11 23:24 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 23:24 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 23:24 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 23:24 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 23:24 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 22 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-10 Lab ID:9294822009 Collected:05/23/11 17:00 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 23:24 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 23:24 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 23:24 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 23:24 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 23:24 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 23:24 108-10-11000.33 Styrene ND ug/L 1 05/25/11 23:24 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 23:24 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 23:24 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/25/11 23:24 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 23:24 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 23:24 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 23:24 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 23:24 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/25/11 23:24 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 23:24 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 23:24 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 23:24 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 23:24 1330-20-75.0 0.66 4-Bromofluorobenzene (S)92 %1 05/25/11 23:24 460-00-470-130 Dibromofluoromethane (S)110 %1 05/25/11 23:24 1868-53-770-130 1,2-Dichloroethane-d4 (S)108 %1 05/25/11 23:24 17060-07-070-130 Toluene-d8 (S)100 %1 05/25/11 23:24 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 23 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-11S Lab ID:9294822010 Collected:05/23/11 16:25 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/28/11 21:30 7440-36-005/27/11 17:006.0 2.6 Arsenic 5.8J ug/L 1 05/28/11 21:30 7440-38-205/27/11 17:0010.0 2.7 Barium 74.2J ug/L 1 05/28/11 21:30 7440-39-305/27/11 17:001000.20 Beryllium 0.21J ug/L 1 05/28/11 21:30 7440-41-705/27/11 17:001.0 0.10 Cadmium ND ug/L 1 05/28/11 21:30 7440-43-905/27/11 17:001.0 0.50 Chromium 8.6J ug/L 1 05/28/11 21:30 7440-47-305/27/11 17:0010.0 0.40 Cobalt 6.5J ug/L 1 05/28/11 21:30 7440-48-405/27/11 17:0010.0 0.60 Copper 11.5 ug/L 1 05/28/11 21:30 7440-50-805/27/11 17:0010.0 0.30 Lead ND ug/L 1 05/28/11 21:30 7439-92-105/27/11 17:0010.0 4.0 Nickel 5.9J ug/L 1 05/28/11 21:30 7440-02-005/27/11 17:0050.0 1.7 Selenium ND ug/L 1 05/28/11 21:30 7782-49-205/27/11 17:0010.0 3.8 Silver 0.41J ug/L 1 05/28/11 21:30 7440-22-405/27/11 17:0010.0 0.10 Thallium ND ug/L 1 05/31/11 11:30 7440-28-005/27/11 17:005.5 3.0 Vanadium 11.9J ug/L 1 05/28/11 21:30 7440-62-205/27/11 17:0025.0 0.20 Zinc 27.1 ug/L 1 05/28/11 21:30 7440-66-605/27/11 17:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 1 05/25/11 23:49 67-64-11002.2 Acrylonitrile ND ug/L 1 05/25/11 23:49 107-13-12001.9 Benzene ND ug/L 1 05/25/11 23:49 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/25/11 23:49 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/25/11 23:49 75-27-41.0 0.18 Bromoform ND ug/L 1 05/25/11 23:49 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/25/11 23:49 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/25/11 23:49 78-93-31000.96 Carbon disulfide ND ug/L 1 05/25/11 23:49 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/25/11 23:49 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/25/11 23:49 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/25/11 23:49 75-00-310.0 0.54 Chloroform ND ug/L 1 05/25/11 23:49 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/25/11 23:49 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/25/11 23:49 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/25/11 23:49 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/25/11 23:49 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/25/11 23:49 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/25/11 23:49 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/25/11 23:49 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/25/11 23:49 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/25/11 23:49 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/25/11 23:49 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/25/11 23:49 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/25/11 23:49 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/25/11 23:49 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/25/11 23:49 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/25/11 23:49 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/25/11 23:49 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 24 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-11S Lab ID:9294822010 Collected:05/23/11 16:25 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/25/11 23:49 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/25/11 23:49 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/25/11 23:49 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/25/11 23:49 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/25/11 23:49 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/25/11 23:49 108-10-11000.33 Styrene ND ug/L 1 05/25/11 23:49 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/25/11 23:49 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/25/11 23:49 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/25/11 23:49 127-18-41.0 0.46 Toluene ND ug/L 1 05/25/11 23:49 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/25/11 23:49 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/25/11 23:49 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/25/11 23:49 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/25/11 23:49 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/25/11 23:49 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/25/11 23:49 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/25/11 23:49 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/25/11 23:49 1330-20-75.0 0.66 4-Bromofluorobenzene (S)96 %1 05/25/11 23:49 460-00-470-130 Dibromofluoromethane (S)108 %1 05/25/11 23:49 1868-53-770-130 1,2-Dichloroethane-d4 (S)109 %1 05/25/11 23:49 17060-07-070-130 Toluene-d8 (S)102 %1 05/25/11 23:49 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 25 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-11D Lab ID:9294822011 Collected:05/23/11 15:40 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/28/11 21:37 7440-36-005/27/11 17:006.0 2.6 Arsenic ND ug/L 1 05/28/11 21:37 7440-38-205/27/11 17:0010.0 2.7 Barium 34.0J ug/L 1 05/28/11 21:37 7440-39-305/27/11 17:001000.20 Beryllium ND ug/L 1 05/28/11 21:37 7440-41-705/27/11 17:001.0 0.10 Cadmium 0.55J ug/L 1 05/28/11 21:37 7440-43-905/27/11 17:001.0 0.50 Chromium 0.91J ug/L 1 05/28/11 21:37 7440-47-305/27/11 17:0010.0 0.40 Cobalt 1.0J ug/L 1 05/28/11 21:37 7440-48-405/27/11 17:0010.0 0.60 Copper 1.2J ug/L 1 05/28/11 21:37 7440-50-805/27/11 17:0010.0 0.30 Lead ND ug/L 1 05/28/11 21:37 7439-92-105/27/11 17:0010.0 4.0 Nickel ND ug/L 1 05/28/11 21:37 7440-02-005/27/11 17:0050.0 1.7 Selenium ND ug/L 1 05/28/11 21:37 7782-49-205/27/11 17:0010.0 3.8 Silver 0.10J ug/L 1 05/28/11 21:37 7440-22-405/27/11 17:0010.0 0.10 Thallium ND ug/L 1 05/29/11 17:21 7440-28-005/27/11 17:005.5 3.0 Vanadium ND ug/L 1 05/28/11 21:37 7440-62-205/27/11 17:0025.0 0.20 Zinc 5.2J ug/L 1 05/28/11 21:37 7440-66-605/27/11 17:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 2.9J ug/L 1 05/26/11 00:15 67-64-11002.2 Acrylonitrile ND ug/L 1 05/26/11 00:15 107-13-12001.9 Benzene ND ug/L 1 05/26/11 00:15 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/26/11 00:15 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/26/11 00:15 75-27-41.0 0.18 Bromoform ND ug/L 1 05/26/11 00:15 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/26/11 00:15 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/26/11 00:15 78-93-31000.96 Carbon disulfide ND ug/L 1 05/26/11 00:15 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/26/11 00:15 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/26/11 00:15 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/26/11 00:15 75-00-310.0 0.54 Chloroform ND ug/L 1 05/26/11 00:15 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/26/11 00:15 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/26/11 00:15 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/26/11 00:15 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/26/11 00:15 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/26/11 00:15 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/26/11 00:15 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/26/11 00:15 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/26/11 00:15 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/26/11 00:15 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/26/11 00:15 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/26/11 00:15 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/26/11 00:15 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/26/11 00:15 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/26/11 00:15 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/26/11 00:15 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/26/11 00:15 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 26 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-11D Lab ID:9294822011 Collected:05/23/11 15:40 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/26/11 00:15 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/26/11 00:15 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/26/11 00:15 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/26/11 00:15 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/26/11 00:15 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/26/11 00:15 108-10-11000.33 Styrene ND ug/L 1 05/26/11 00:15 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/26/11 00:15 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/26/11 00:15 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/26/11 00:15 127-18-41.0 0.46 Toluene ND ug/L 1 05/26/11 00:15 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/26/11 00:15 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/26/11 00:15 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/26/11 00:15 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/26/11 00:15 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/26/11 00:15 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/26/11 00:15 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/26/11 00:15 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/26/11 00:15 1330-20-75.0 0.66 4-Bromofluorobenzene (S)97 %1 05/26/11 00:15 460-00-470-130 Dibromofluoromethane (S)112 %1 05/26/11 00:15 1868-53-770-130 1,2-Dichloroethane-d4 (S)112 %1 05/26/11 00:15 17060-07-070-130 Toluene-d8 (S)99 %1 05/26/11 00:15 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 27 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:LAGOON Lab ID:9294822012 Collected:05/23/11 17:20 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 05/28/11 21:40 7440-36-005/27/11 17:006.0 2.6 Arsenic ND ug/L 1 05/28/11 21:40 7440-38-205/27/11 17:0010.0 2.7 Barium 84.2J ug/L 1 05/28/11 21:40 7440-39-305/27/11 17:001000.20 Beryllium ND ug/L 1 05/28/11 21:40 7440-41-705/27/11 17:001.0 0.10 Cadmium ND ug/L 1 05/28/11 21:40 7440-43-905/27/11 17:001.0 0.50 Chromium 3.3J ug/L 1 05/28/11 21:40 7440-47-305/27/11 17:0010.0 0.40 Cobalt 16.8 ug/L 1 05/28/11 21:40 7440-48-405/27/11 17:0010.0 0.60 Copper 3.6J ug/L 1 05/28/11 21:40 7440-50-805/27/11 17:0010.0 0.30 Lead ND ug/L 1 05/28/11 21:40 7439-92-105/27/11 17:0010.0 4.0 Nickel 4.6J ug/L 1 05/28/11 21:40 7440-02-005/27/11 17:0050.0 1.7 Selenium ND ug/L 1 05/28/11 21:40 7782-49-205/27/11 17:0010.0 3.8 Silver ND ug/L 1 05/28/11 21:40 7440-22-405/27/11 17:0010.0 0.10 Thallium ND ug/L 1 05/29/11 17:25 7440-28-005/27/11 17:005.5 3.0 Vanadium 6.1J ug/L 1 05/28/11 21:40 7440-62-205/27/11 17:0025.0 0.20 Zinc 13.2 ug/L 1 05/28/11 21:40 7440-66-605/27/11 17:0010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 37.4J ug/L 1 05/26/11 00:40 67-64-11002.2 Acrylonitrile ND ug/L 1 05/26/11 00:40 107-13-12001.9 Benzene ND ug/L 1 05/26/11 00:40 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/26/11 00:40 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/26/11 00:40 75-27-41.0 0.18 Bromoform ND ug/L 1 05/26/11 00:40 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/26/11 00:40 74-83-910.0 0.29 2-Butanone (MEK)17.6J ug/L 1 05/26/11 00:40 78-93-31000.96 Carbon disulfide ND ug/L 1 05/26/11 00:40 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/26/11 00:40 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/26/11 00:40 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/26/11 00:40 75-00-310.0 0.54 Chloroform ND ug/L 1 05/26/11 00:40 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/26/11 00:40 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/26/11 00:40 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/26/11 00:40 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/26/11 00:40 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/26/11 00:40 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/26/11 00:40 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/26/11 00:40 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/26/11 00:40 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/26/11 00:40 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/26/11 00:40 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/26/11 00:40 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/26/11 00:40 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/26/11 00:40 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/26/11 00:40 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/26/11 00:40 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/26/11 00:40 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 28 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:LAGOON Lab ID:9294822012 Collected:05/23/11 17:20 Received:05/24/11 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/26/11 00:40 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/26/11 00:40 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/26/11 00:40 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/26/11 00:40 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/26/11 00:40 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/26/11 00:40 108-10-11000.33 Styrene ND ug/L 1 05/26/11 00:40 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/26/11 00:40 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/26/11 00:40 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/26/11 00:40 127-18-41.0 0.46 Toluene 0.38J ug/L 1 05/26/11 00:40 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/26/11 00:40 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/26/11 00:40 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/26/11 00:40 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/26/11 00:40 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/26/11 00:40 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/26/11 00:40 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/26/11 00:40 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/26/11 00:40 1330-20-75.0 0.66 4-Bromofluorobenzene (S)95 %1 05/26/11 00:40 460-00-470-130 Dibromofluoromethane (S)111 %1 05/26/11 00:40 1868-53-770-130 1,2-Dichloroethane-d4 (S)111 %1 05/26/11 00:40 17060-07-070-130 Toluene-d8 (S)99 %1 05/26/11 00:40 2037-26-570-130 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 7980 ug/L 1 05/30/11 11:4505/25/11 15:2520002000 9040 pH Analytical Method: EPA 9040 pH 7.5 Std. Units 1 05/31/11 13:46 H60.10 0.10 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 9670J ug/L 1 06/06/11 18:44 14808-79-82500005000 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 7160J ug/L 1 05/24/11 23:15 M110000100 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 297 ug/L 1 06/09/11 11:10 7723-14-050.0 50.0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 80000 ug/L 1 06/07/11 14:182500025000 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 29 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-9S Lab ID:9294822013 Collected:05/24/11 00:00 Received:05/25/11 15:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 06/03/11 21:29 7440-36-006/02/11 15:306.0 2.6 Arsenic ND ug/L 1 06/03/11 21:29 7440-38-206/02/11 15:3010.0 2.7 Barium 54.5J ug/L 1 06/03/11 21:29 7440-39-306/02/11 15:301000.20 Beryllium ND ug/L 1 06/03/11 21:29 7440-41-706/02/11 15:301.0 0.10 Cadmium ND ug/L 1 06/03/11 21:29 7440-43-906/02/11 15:301.0 0.50 Chromium 3.6J ug/L 1 06/03/11 21:29 7440-47-306/02/11 15:3010.0 0.40 Cobalt 7.0J ug/L 1 06/03/11 21:29 7440-48-406/02/11 15:3010.0 0.60 Copper 1.9J ug/L 1 06/03/11 21:29 7440-50-806/02/11 15:3010.0 0.30 Lead ND ug/L 1 06/03/11 21:29 7439-92-106/02/11 15:3010.0 4.0 Nickel 3.6J ug/L 1 06/03/11 21:29 7440-02-006/02/11 15:3050.0 1.7 Selenium ND ug/L 1 06/03/11 21:29 7782-49-206/02/11 15:3010.0 3.8 Silver ND ug/L 1 06/03/11 21:29 7440-22-406/02/11 15:3010.0 0.10 Thallium ND ug/L 1 06/03/11 21:29 7440-28-006/02/11 15:305.5 3.0 Vanadium 2.5J ug/L 1 06/03/11 21:29 7440-62-206/02/11 15:3025.0 0.20 Zinc 20.5 ug/L 1 06/03/11 21:29 7440-66-606/02/11 15:3010.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 3.1J ug/L 1 05/27/11 20:18 67-64-11002.2 Acrylonitrile ND ug/L 1 05/27/11 20:18 107-13-12001.9 Benzene 0.26J ug/L 1 05/27/11 20:18 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/27/11 20:18 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/27/11 20:18 75-27-41.0 0.18 Bromoform ND ug/L 1 05/27/11 20:18 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/27/11 20:18 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/27/11 20:18 78-93-31000.96 Carbon disulfide ND ug/L 1 05/27/11 20:18 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/27/11 20:18 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/27/11 20:18 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/27/11 20:18 75-00-310.0 0.54 Chloroform ND ug/L 1 05/27/11 20:18 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/27/11 20:18 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/27/11 20:18 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/27/11 20:18 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/27/11 20:18 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/27/11 20:18 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/27/11 20:18 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/27/11 20:18 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/27/11 20:18 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/27/11 20:18 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/27/11 20:18 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/27/11 20:18 75-35-45.0 0.56 cis-1,2-Dichloroethene 2.0J ug/L 1 05/27/11 20:18 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/27/11 20:18 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/27/11 20:18 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/27/11 20:18 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/27/11 20:18 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 30 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-9S Lab ID:9294822013 Collected:05/24/11 00:00 Received:05/25/11 15:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/27/11 20:18 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/27/11 20:18 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/27/11 20:18 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/27/11 20:18 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/27/11 20:18 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/27/11 20:18 108-10-11000.33 Styrene ND ug/L 1 05/27/11 20:18 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/27/11 20:18 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/27/11 20:18 79-34-53.0 0.40 Tetrachloroethene 0.62J ug/L 1 05/27/11 20:18 127-18-41.0 0.46 Toluene ND ug/L 1 05/27/11 20:18 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/27/11 20:18 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/27/11 20:18 79-00-51.0 0.29 Trichloroethene 0.97J ug/L 1 05/27/11 20:18 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/27/11 20:18 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/27/11 20:18 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/27/11 20:18 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/27/11 20:18 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/27/11 20:18 1330-20-75.0 0.66 4-Bromofluorobenzene (S)98 %1 05/27/11 20:18 460-00-470-130 Dibromofluoromethane (S)95 %1 05/27/11 20:18 1868-53-770-130 1,2-Dichloroethane-d4 (S)98 %1 05/27/11 20:18 17060-07-070-130 Toluene-d8 (S)100 %1 05/27/11 20:18 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 31 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-9D Lab ID:9294822014 Collected:05/24/11 00:00 Received:05/25/11 15:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 06/09/11 14:26 7440-36-006/06/11 12:456.0 2.6 Arsenic ND ug/L 1 06/09/11 14:26 7440-38-206/06/11 12:4510.0 2.7 Barium 32.2J ug/L 1 06/09/11 14:26 7440-39-306/06/11 12:451000.20 Beryllium ND ug/L 1 06/09/11 14:26 7440-41-706/06/11 12:451.0 0.10 Cadmium 0.75J ug/L 1 06/09/11 14:26 7440-43-906/06/11 12:451.0 0.50 Chromium ND ug/L 1 06/09/11 14:26 7440-47-306/06/11 12:4510.0 0.40 Cobalt ND ug/L 1 06/09/11 14:26 7440-48-406/06/11 12:4510.0 0.60 Copper 0.52J ug/L 1 06/09/11 14:26 7440-50-806/06/11 12:4510.0 0.30 Lead ND ug/L 1 06/09/11 14:26 7439-92-106/06/11 12:4510.0 4.0 Nickel 3.1J ug/L 1 06/09/11 14:26 7440-02-006/06/11 12:4550.0 1.7 Selenium ND ug/L 1 06/09/11 14:26 7782-49-206/06/11 12:4510.0 3.8 Silver 0.13J ug/L 1 06/09/11 14:26 7440-22-406/06/11 12:4510.0 0.10 Thallium ND ug/L 1 06/09/11 14:26 7440-28-006/06/11 12:455.5 3.0 Vanadium ND ug/L 1 06/09/11 14:26 7440-62-206/06/11 12:4525.0 0.20 Zinc 12.2 ug/L 1 06/09/11 14:26 7440-66-606/06/11 12:4510.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 3.8J ug/L 1 05/27/11 20:42 67-64-11002.2 Acrylonitrile ND ug/L 1 05/27/11 20:42 107-13-12001.9 Benzene ND ug/L 1 05/27/11 20:42 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/27/11 20:42 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/27/11 20:42 75-27-41.0 0.18 Bromoform ND ug/L 1 05/27/11 20:42 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/27/11 20:42 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/27/11 20:42 78-93-31000.96 Carbon disulfide ND ug/L 1 05/27/11 20:42 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/27/11 20:42 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/27/11 20:42 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/27/11 20:42 75-00-310.0 0.54 Chloroform ND ug/L 1 05/27/11 20:42 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/27/11 20:42 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/27/11 20:42 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/27/11 20:42 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/27/11 20:42 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/27/11 20:42 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/27/11 20:42 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/27/11 20:42 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/27/11 20:42 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/27/11 20:42 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/27/11 20:42 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/27/11 20:42 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/27/11 20:42 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/27/11 20:42 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/27/11 20:42 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/27/11 20:42 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/27/11 20:42 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 32 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-9D Lab ID:9294822014 Collected:05/24/11 00:00 Received:05/25/11 15:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/27/11 20:42 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/27/11 20:42 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/27/11 20:42 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/27/11 20:42 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/27/11 20:42 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/27/11 20:42 108-10-11000.33 Styrene ND ug/L 1 05/27/11 20:42 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/27/11 20:42 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/27/11 20:42 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/27/11 20:42 127-18-41.0 0.46 Toluene ND ug/L 1 05/27/11 20:42 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/27/11 20:42 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/27/11 20:42 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/27/11 20:42 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/27/11 20:42 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/27/11 20:42 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/27/11 20:42 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/27/11 20:42 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/27/11 20:42 1330-20-75.0 0.66 4-Bromofluorobenzene (S)98 %1 05/27/11 20:42 460-00-470-130 Dibromofluoromethane (S)95 %1 05/27/11 20:42 1868-53-770-130 1,2-Dichloroethane-d4 (S)98 %1 05/27/11 20:42 17060-07-070-130 Toluene-d8 (S)100 %1 05/27/11 20:42 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 33 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-12 Lab ID:9294822015 Collected:05/24/11 00:00 Received:05/25/11 15:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 06/03/11 16:42 7440-36-005/31/11 12:156.0 2.6 Arsenic ND ug/L 1 06/03/11 16:42 7440-38-205/31/11 12:1510.0 2.7 Barium 14.1J ug/L 1 06/03/11 16:42 7440-39-305/31/11 12:151000.20 Beryllium ND ug/L 1 06/07/11 17:32 7440-41-705/31/11 12:151.0 0.10 Cadmium 0.93J ug/L 1 06/03/11 16:42 7440-43-905/31/11 12:151.0 0.50 Chromium 1.6J ug/L 1 06/03/11 16:42 7440-47-305/31/11 12:1510.0 0.40 Cobalt ND ug/L 1 06/03/11 16:42 7440-48-405/31/11 12:1510.0 0.60 Copper 1.3J ug/L 1 06/03/11 16:42 7440-50-805/31/11 12:1510.0 0.30 Lead ND ug/L 1 06/03/11 16:42 7439-92-105/31/11 12:1510.0 4.0 Nickel ND ug/L 1 06/03/11 16:42 7440-02-005/31/11 12:1550.0 1.7 Selenium ND ug/L 1 06/03/11 16:42 7782-49-205/31/11 12:1510.0 3.8 Silver ND ug/L 1 06/03/11 16:42 7440-22-405/31/11 12:1510.0 0.10 Thallium ND ug/L 1 06/03/11 16:42 7440-28-005/31/11 12:155.5 3.0 Vanadium ND ug/L 1 06/03/11 16:42 7440-62-205/31/11 12:1525.0 0.20 Zinc 6.0J ug/L 1 06/03/11 16:42 7440-66-605/31/11 12:1510.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 3.5J ug/L 1 05/27/11 21:07 67-64-11002.2 Acrylonitrile ND ug/L 1 05/27/11 21:07 107-13-12001.9 Benzene ND ug/L 1 05/27/11 21:07 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/27/11 21:07 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/27/11 21:07 75-27-41.0 0.18 Bromoform ND ug/L 1 05/27/11 21:07 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/27/11 21:07 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/27/11 21:07 78-93-31000.96 Carbon disulfide ND ug/L 1 05/27/11 21:07 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/27/11 21:07 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/27/11 21:07 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/27/11 21:07 75-00-310.0 0.54 Chloroform ND ug/L 1 05/27/11 21:07 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/27/11 21:07 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/27/11 21:07 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/27/11 21:07 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/27/11 21:07 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/27/11 21:07 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/27/11 21:07 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/27/11 21:07 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/27/11 21:07 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/27/11 21:07 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/27/11 21:07 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/27/11 21:07 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/27/11 21:07 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/27/11 21:07 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/27/11 21:07 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/27/11 21:07 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/27/11 21:07 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 34 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-12 Lab ID:9294822015 Collected:05/24/11 00:00 Received:05/25/11 15:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/27/11 21:07 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/27/11 21:07 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/27/11 21:07 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/27/11 21:07 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/27/11 21:07 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/27/11 21:07 108-10-11000.33 Styrene ND ug/L 1 05/27/11 21:07 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/27/11 21:07 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/27/11 21:07 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/27/11 21:07 127-18-41.0 0.46 Toluene ND ug/L 1 05/27/11 21:07 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/27/11 21:07 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/27/11 21:07 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/27/11 21:07 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/27/11 21:07 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/27/11 21:07 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/27/11 21:07 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/27/11 21:07 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/27/11 21:07 1330-20-75.0 0.66 4-Bromofluorobenzene (S)96 %1 05/27/11 21:07 460-00-470-130 Dibromofluoromethane (S)95 %1 05/27/11 21:07 1868-53-770-130 1,2-Dichloroethane-d4 (S)97 %1 05/27/11 21:07 17060-07-070-130 Toluene-d8 (S)99 %1 05/27/11 21:07 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 35 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-13 Lab ID:9294822016 Collected:05/24/11 00:00 Received:05/25/11 15:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 1 06/03/11 16:56 7440-36-005/31/11 12:156.0 2.6 Arsenic ND ug/L 1 06/03/11 16:56 7440-38-205/31/11 12:1510.0 2.7 Barium 29.7J ug/L 1 06/03/11 16:56 7440-39-305/31/11 12:151000.20 Beryllium 0.13J ug/L 1 06/07/11 17:35 7440-41-705/31/11 12:151.0 0.10 Cadmium 1.0 ug/L 1 06/03/11 16:56 7440-43-905/31/11 12:151.0 0.50 Chromium 1.1J ug/L 1 06/03/11 16:56 7440-47-305/31/11 12:1510.0 0.40 Cobalt 2.3J ug/L 1 06/03/11 16:56 7440-48-405/31/11 12:1510.0 0.60 Copper 1.9J ug/L 1 06/03/11 16:56 7440-50-805/31/11 12:1510.0 0.30 Lead ND ug/L 1 06/03/11 16:56 7439-92-105/31/11 12:1510.0 4.0 Nickel 1.8J ug/L 1 06/03/11 16:56 7440-02-005/31/11 12:1550.0 1.7 Selenium ND ug/L 1 06/03/11 16:56 7782-49-205/31/11 12:1510.0 3.8 Silver 0.13J ug/L 1 06/03/11 16:56 7440-22-405/31/11 12:1510.0 0.10 Thallium ND ug/L 1 06/03/11 16:56 7440-28-005/31/11 12:155.5 3.0 Vanadium 0.58J ug/L 1 06/03/11 16:56 7440-62-205/31/11 12:1525.0 0.20 Zinc 8.6J ug/L 1 06/03/11 16:56 7440-66-605/31/11 12:1510.0 0.40 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 2.8J ug/L 1 05/27/11 21:31 67-64-11002.2 Acrylonitrile ND ug/L 1 05/27/11 21:31 107-13-12001.9 Benzene ND ug/L 1 05/27/11 21:31 71-43-21.0 0.25 Bromochloromethane ND ug/L 1 05/27/11 21:31 74-97-53.0 0.17 Bromodichloromethane ND ug/L 1 05/27/11 21:31 75-27-41.0 0.18 Bromoform ND ug/L 1 05/27/11 21:31 75-25-23.0 0.26 Bromomethane ND ug/L 1 05/27/11 21:31 74-83-910.0 0.29 2-Butanone (MEK)ND ug/L 1 05/27/11 21:31 78-93-31000.96 Carbon disulfide ND ug/L 1 05/27/11 21:31 75-15-01001.2 Carbon tetrachloride ND ug/L 1 05/27/11 21:31 56-23-51.0 0.25 Chlorobenzene ND ug/L 1 05/27/11 21:31 108-90-73.0 0.23 Chloroethane ND ug/L 1 05/27/11 21:31 75-00-310.0 0.54 Chloroform ND ug/L 1 05/27/11 21:31 67-66-35.0 0.14 Chloromethane ND ug/L 1 05/27/11 21:31 74-87-31.0 0.11 1,2-Dibromo-3-chloropropane ND ug/L 1 05/27/11 21:31 96-12-813.0 2.5 Dibromochloromethane ND ug/L 1 05/27/11 21:31 124-48-13.0 0.21 1,2-Dibromoethane (EDB)ND ug/L 1 05/27/11 21:31 106-93-41.0 0.27 Dibromomethane ND ug/L 1 05/27/11 21:31 74-95-310.0 0.21 1,2-Dichlorobenzene ND ug/L 1 05/27/11 21:31 95-50-15.0 0.30 1,4-Dichlorobenzene ND ug/L 1 05/27/11 21:31 106-46-71.0 0.33 trans-1,4-Dichloro-2-butene ND ug/L 1 05/27/11 21:31 110-57-61001.0 1,1-Dichloroethane ND ug/L 1 05/27/11 21:31 75-34-35.0 0.32 1,2-Dichloroethane ND ug/L 1 05/27/11 21:31 107-06-21.0 0.12 1,1-Dichloroethene ND ug/L 1 05/27/11 21:31 75-35-45.0 0.56 cis-1,2-Dichloroethene ND ug/L 1 05/27/11 21:31 156-59-25.0 0.19 trans-1,2-Dichloroethene ND ug/L 1 05/27/11 21:31 156-60-55.0 0.49 1,2-Dichloropropane ND ug/L 1 05/27/11 21:31 78-87-51.0 0.27 1,3-Dichloropropane ND ug/L 1 05/27/11 21:31 142-28-91.0 0.28 cis-1,3-Dichloropropene ND ug/L 1 05/27/11 21:31 10061-01-51.0 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 36 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 ANALYTICAL RESULTS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Sample:MW-13 Lab ID:9294822016 Collected:05/24/11 00:00 Received:05/25/11 15:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans-1,3-Dichloropropene ND ug/L 1 05/27/11 21:31 10061-02-61.0 0.26 Ethylbenzene ND ug/L 1 05/27/11 21:31 100-41-41.0 0.30 2-Hexanone ND ug/L 1 05/27/11 21:31 591-78-650.0 0.46 Iodomethane ND ug/L 1 05/27/11 21:31 74-88-410.0 0.32 Methylene Chloride ND ug/L 1 05/27/11 21:31 75-09-21.0 0.97 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/27/11 21:31 108-10-11000.33 Styrene ND ug/L 1 05/27/11 21:31 100-42-51.0 0.26 1,1,1,2-Tetrachloroethane ND ug/L 1 05/27/11 21:31 630-20-65.0 0.33 1,1,2,2-Tetrachloroethane ND ug/L 1 05/27/11 21:31 79-34-53.0 0.40 Tetrachloroethene ND ug/L 1 05/27/11 21:31 127-18-41.0 0.46 Toluene ND ug/L 1 05/27/11 21:31 108-88-31.0 0.26 1,1,1-Trichloroethane ND ug/L 1 05/27/11 21:31 71-55-61.0 0.48 1,1,2-Trichloroethane ND ug/L 1 05/27/11 21:31 79-00-51.0 0.29 Trichloroethene ND ug/L 1 05/27/11 21:31 79-01-61.0 0.47 Trichlorofluoromethane ND ug/L 1 05/27/11 21:31 75-69-41.0 0.20 1,2,3-Trichloropropane ND ug/L 1 05/27/11 21:31 96-18-41.0 0.41 Vinyl acetate ND ug/L 1 05/27/11 21:31 108-05-450.0 0.35 Vinyl chloride ND ug/L 1 05/27/11 21:31 75-01-41.0 0.62 Xylene (Total)ND ug/L 1 05/27/11 21:31 1330-20-75.0 0.66 4-Bromofluorobenzene (S)98 %1 05/27/11 21:31 460-00-470-130 Dibromofluoromethane (S)96 %1 05/27/11 21:31 1868-53-770-130 1,2-Dichloroethane-d4 (S)97 %1 05/27/11 21:31 17060-07-070-130 Toluene-d8 (S)99 %1 05/27/11 21:31 2037-26-570-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 37 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/8437 EPA 3010 EPA 6010 6010 MET NC Groundwater Associated Lab Samples:9294822001, 9294822002, 9294822003, 9294822004, 9294822005, 9294822006, 9294822007, 9294822008 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:610900 Associated Lab Samples:9294822001, 9294822002, 9294822003, 9294822004, 9294822005, 9294822006, 9294822007, 9294822008 Matrix:Water Analyzed Antimony ug/L ND 6.0 05/27/11 16:59 Arsenic ug/L ND 10.0 05/28/11 19:37 Barium ug/L ND 100 05/27/11 16:59 Beryllium ug/L ND 1.0 05/27/11 16:59 Cadmium ug/L ND 1.0 05/27/11 16:59 Chromium ug/L 0.62J 10.0 05/27/11 16:59 Cobalt ug/L ND 10.0 05/27/11 16:59 Copper ug/L ND 10.0 05/27/11 16:59 Lead ug/L ND 10.0 05/27/11 16:59 Nickel ug/L ND 50.0 05/27/11 16:59 Selenium ug/L ND 10.0 05/27/11 16:59 Silver ug/L ND 10.0 05/27/11 16:59 Thallium ug/L ND 5.5 05/27/11 16:59 Vanadium ug/L ND 25.0 05/27/11 16:59 Zinc ug/L 8.0J 10.0 05/28/11 19:37 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 610901LABORATORY CONTROL SAMPLE: LCSSpike Antimony ug/L 486500 97 80-120 Arsenic ug/L 473500 95 80-120 Barium ug/L 495500 99 80-120 Beryllium ug/L 512500 102 80-120 Cadmium ug/L 501500 100 80-120 Chromium ug/L 489500 98 80-120 Cobalt ug/L 500500 100 80-120 Copper ug/L 487500 97 80-120 Lead ug/L 494500 99 80-120 Nickel ug/L 506500 101 80-120 Selenium ug/L 482500 96 80-120 Silver ug/L 245250 98 80-120 Thallium ug/L 497500 99 80-120 Vanadium ug/L 493500 99 80-120 Zinc ug/L 501500 100 80-120 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 610902MATRIX SPIKE SAMPLE: MSSpike Result 9294284003 Antimony ug/L 481500 96 75-125ND Arsenic ug/L 481500 95 75-125ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 38 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 610902MATRIX SPIKE SAMPLE: MSSpike Result 9294284003 Barium ug/L 768500 96 75-125287 Beryllium ug/L 504500 101 75-125ND Cadmium ug/L 488500 98 75-125ND Chromium ug/L 479500 96 75-125ND Cobalt ug/L 488500 97 75-125ND Copper ug/L 478500 96 75-125ND Lead ug/L 475500 95 75-125ND Nickel ug/L 492500 98 75-125ND Selenium ug/L 479500 96 75-125ND Silver ug/L 241250 96 75-125ND Thallium ug/L 482500 96 75-125ND Vanadium ug/L 483500 96 75-125ND Zinc ug/L 502500 98 75-12512.1 Parameter Units Dup Result Max RPD QualifiersRPDResult 9294284004 610903SAMPLE DUPLICATE: Antimony ug/L ND 25ND Arsenic ug/L ND 25ND Barium ug/L 101 2 2599.0 Beryllium ug/L ND 25ND Cadmium ug/L ND 25ND Chromium ug/L 0.70J 25ND Cobalt ug/L 1.1J 25ND Copper ug/L ND 25ND Lead ug/L ND 25ND Nickel ug/L ND 25ND Selenium ug/L ND 25ND Silver ug/L ND 25ND Thallium ug/L ND 25ND Vanadium ug/L ND 25ND Zinc ug/L 10.7 25ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 39 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/8450 EPA 3010 EPA 6010 6010 MET NC Groundwater Associated Lab Samples:9294822009, 9294822010, 9294822011, 9294822012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:612132 Associated Lab Samples:9294822009, 9294822010, 9294822011, 9294822012 Matrix:Water Analyzed Antimony ug/L ND 6.0 05/28/11 21:07 Arsenic ug/L ND 10.0 05/28/11 21:07 Barium ug/L ND 100 05/28/11 21:07 Beryllium ug/L ND 1.0 05/28/11 21:07 Cadmium ug/L ND 1.0 05/28/11 21:07 Chromium ug/L ND 10.0 05/28/11 21:07 Cobalt ug/L ND 10.0 05/28/11 21:07 Copper ug/L ND 10.0 05/28/11 21:07 Lead ug/L ND 10.0 05/28/11 21:07 Nickel ug/L ND 50.0 05/28/11 21:07 Selenium ug/L ND 10.0 05/28/11 21:07 Silver ug/L 0.25J 10.0 05/28/11 21:07 Thallium ug/L ND 5.5 05/28/11 21:07 Vanadium ug/L ND 25.0 05/28/11 21:07 Zinc ug/L 3.3J 10.0 05/28/11 21:07 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 612133LABORATORY CONTROL SAMPLE: LCSSpike Antimony ug/L 412500 82 80-120 Arsenic ug/L 427500 85 80-120 Barium ug/L 422500 84 80-120 Beryllium ug/L 416500 83 80-120 Cadmium ug/L 418500 84 80-120 Chromium ug/L 414500 83 80-120 Cobalt ug/L 420500 84 80-120 Copper ug/L 422500 84 80-120 Lead ug/L 424500 85 80-120 Nickel ug/L 420500 84 80-120 Selenium ug/L 414500 83 80-120 Silver ug/L 209250 84 80-120 Thallium ug/L 406500 81 80-120 Vanadium ug/L 413500 83 80-120 Zinc ug/L 432500 86 80-120 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 612134MATRIX SPIKE SAMPLE: MSSpike Result 9294822009 Antimony ug/L 412500 82 75-125ND Arsenic ug/L 422500 84 75-125ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 40 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 612134MATRIX SPIKE SAMPLE: MSSpike Result 9294822009 Barium ug/L 460500 83 75-12545.4J Beryllium ug/L 413500 83 75-125ND Cadmium ug/L 413500 83 75-125ND Chromium ug/L 412500 82 75-1253.0J Cobalt ug/L 416500 83 75-1251.3J Copper ug/L 423500 84 75-1251.2J Lead ug/L 412500 82 75-125ND Nickel ug/L 416500 83 75-125ND Selenium ug/L 417500 83 75-125ND Silver ug/L 210250 84 75-125ND Thallium ug/L 396500 78 75-1256.1 Vanadium ug/L 414500 82 75-1252.0J Zinc ug/L 432500 84 75-12510.5 Parameter Units Dup Result Max RPD QualifiersRPDResult 9294822010 612135SAMPLE DUPLICATE: Antimony ug/L ND 25ND Arsenic ug/L 4.0J 255.8J Barium ug/L 72.3J 3 2574.2J Beryllium ug/L 0.19J 250.21J Cadmium ug/L ND 25ND Chromium ug/L 8.2J 5 258.6J Cobalt ug/L 6.7J 3 256.5J Copper ug/L 11.6 1 2511.5 Lead ug/L ND 25ND Nickel ug/L 5.9J 1 255.9J Selenium ug/L ND 25ND Silver ug/L ND 250.41J Thallium ug/L ND 25ND Vanadium ug/L 11.8J 1 2511.9J Zinc ug/L 27.5 1 2527.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 41 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/8466 EPA 3010 EPA 6010 6010 MET NC Groundwater Associated Lab Samples:9294822015, 9294822016 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:613173 Associated Lab Samples:9294822015, 9294822016 Matrix:Water Analyzed Antimony ug/L ND 6.0 06/03/11 16:37 Arsenic ug/L ND 10.0 06/03/11 16:37 Barium ug/L ND 100 06/03/11 16:37 Beryllium ug/L ND 1.0 06/03/11 16:37 Cadmium ug/L ND 1.0 06/03/11 16:37 Chromium ug/L ND 10.0 06/03/11 16:37 Cobalt ug/L ND 10.0 06/03/11 16:37 Copper ug/L ND 10.0 06/03/11 16:37 Lead ug/L ND 10.0 06/03/11 16:37 Nickel ug/L ND 50.0 06/03/11 16:37 Selenium ug/L ND 10.0 06/03/11 16:37 Silver ug/L ND 10.0 06/03/11 16:37 Thallium ug/L ND 5.5 06/03/11 16:37 Vanadium ug/L ND 25.0 06/03/11 16:37 Zinc ug/L 7.7J 10.0 06/03/11 16:37 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 613174LABORATORY CONTROL SAMPLE: LCSSpike Antimony ug/L 482500 96 80-120 Arsenic ug/L 499500 100 80-120 Barium ug/L 508500 102 80-120 Beryllium ug/L 488500 98 80-120 Cadmium ug/L 497500 99 80-120 Chromium ug/L 498500 100 80-120 Cobalt ug/L 500500 100 80-120 Copper ug/L 491500 98 80-120 Lead ug/L 499500 100 80-120 Nickel ug/L 501500 100 80-120 Selenium ug/L 497500 99 80-120 Silver ug/L 241250 96 80-120 Thallium ug/L 495500 99 80-120 Vanadium ug/L 486500 97 80-120 Zinc ug/L 514500 103 80-120 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 613260MATRIX SPIKE SAMPLE: MSSpike Result 9294822015 Antimony ug/L 482500 96 75-125ND Arsenic ug/L 497500 99 75-125ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 42 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 613260MATRIX SPIKE SAMPLE: MSSpike Result 9294822015 Barium ug/L 518500 101 75-12514.1J Beryllium ug/L 487500 97 75-125ND Cadmium ug/L 493500 98 75-1250.93J Chromium ug/L 489500 97 75-1251.6J Cobalt ug/L 486500 97 75-125ND Copper ug/L 492500 98 75-1251.3J Lead ug/L 485500 97 75-125ND Nickel ug/L 488500 97 75-125ND Selenium ug/L 497500 99 75-125ND Silver ug/L 241250 96 75-125ND Thallium ug/L 481500 96 75-125ND Vanadium ug/L 484500 97 75-125ND Zinc ug/L 496500 98 75-1256.0J Parameter Units Dup Result Max RPD QualifiersRPDResult 9294822016 613261SAMPLE DUPLICATE: Antimony ug/L ND 25ND Arsenic ug/L ND 25ND Barium ug/L 28.9J 3 2529.7J Beryllium ug/L 0.32J 250.13J Cadmium ug/L 0.68J 251.0 Chromium ug/L 1.4J 251.1J Cobalt ug/L 2.0J 252.3J Copper ug/L 1.4J 251.9J Lead ug/L ND 25ND Nickel ug/L 1.8J 251.8J Selenium ug/L ND 25ND Silver ug/L ND 250.13J Thallium ug/L ND 25ND Vanadium ug/L 0.90J 250.58J Zinc ug/L 7.6J 258.6J REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 43 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/8476 EPA 3010 EPA 6010 6010 MET NC Groundwater Associated Lab Samples:9294822013 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:614257 Associated Lab Samples:9294822013 Matrix:Water Analyzed Antimony ug/L ND 6.0 06/03/11 21:20 Arsenic ug/L ND 10.0 06/03/11 21:20 Barium ug/L ND 100 06/03/11 21:20 Beryllium ug/L ND 1.0 06/03/11 21:20 Cadmium ug/L ND 1.0 06/03/11 21:20 Chromium ug/L ND 10.0 06/03/11 21:20 Cobalt ug/L ND 10.0 06/03/11 21:20 Copper ug/L ND 10.0 06/03/11 21:20 Lead ug/L ND 10.0 06/03/11 21:20 Nickel ug/L ND 50.0 06/03/11 21:20 Selenium ug/L ND 10.0 06/03/11 21:20 Silver ug/L ND 10.0 06/03/11 21:20 Thallium ug/L ND 5.5 06/03/11 21:20 Vanadium ug/L ND 25.0 06/03/11 21:20 Zinc ug/L 6.1J 10.0 06/03/11 21:20 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 614258LABORATORY CONTROL SAMPLE: LCSSpike Antimony ug/L 449500 90 80-120 Arsenic ug/L 471500 94 80-120 Barium ug/L 472500 94 80-120 Beryllium ug/L 468500 94 80-120 Cadmium ug/L 472500 94 80-120 Chromium ug/L 475500 95 80-120 Cobalt ug/L 480500 96 80-120 Copper ug/L 461500 92 80-120 Lead ug/L 471500 94 80-120 Nickel ug/L 475500 95 80-120 Selenium ug/L 457500 91 80-120 Silver ug/L 234250 94 80-120 Thallium ug/L 449500 90 80-120 Vanadium ug/L 477500 95 80-120 Zinc ug/L 469500 94 80-120 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 614279MATRIX SPIKE SAMPLE: MSSpike Result 9294822013 Antimony ug/L 468500 94 75-125ND Arsenic ug/L 499500 100 75-125ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 44 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 614279MATRIX SPIKE SAMPLE: MSSpike Result 9294822013 Barium ug/L 538500 97 75-12554.5J Beryllium ug/L 486500 97 75-125ND Cadmium ug/L 482500 96 75-125ND Chromium ug/L 489500 97 75-1253.6J Cobalt ug/L 498500 98 75-1257.0J Copper ug/L 492500 98 75-1251.9J Lead ug/L 476500 95 75-125ND Nickel ug/L 486500 96 75-1253.6J Selenium ug/L 478500 96 75-125ND Silver ug/L 244250 98 75-125ND Thallium ug/L 453500 90 75-125ND Vanadium ug/L 495500 98 75-1252.5J Zinc ug/L 494500 95 75-12520.5 Parameter Units Dup Result Max RPD QualifiersRPDResult 9294940019 614280SAMPLE DUPLICATE: Antimony ug/L ND 25ND Arsenic ug/L ND 25ND Barium ug/L 32.0J 2 2531.5J Beryllium ug/L 0.11J 25ND Cadmium ug/L ND 25ND Chromium ug/L 2.6J 253.6J Cobalt ug/L 5.0J 254.9J Copper ug/L 0.99J 251.6J Lead ug/L ND 25ND Nickel ug/L ND 25ND Selenium ug/L ND 25ND Silver ug/L ND 25ND Thallium ug/L ND 25ND Vanadium ug/L 2.1J 252.2J Zinc ug/L 15.2 24 2519.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 45 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/8485 EPA 3010 EPA 6010 6010 MET NC Groundwater Associated Lab Samples:9294822014 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:614938 Associated Lab Samples:9294822014 Matrix:Water Analyzed Antimony ug/L ND 6.0 06/09/11 14:19 Arsenic ug/L ND 10.0 06/09/11 14:19 Barium ug/L ND 100 06/09/11 14:19 Beryllium ug/L ND 1.0 06/09/11 14:19 Cadmium ug/L ND 1.0 06/09/11 14:19 Chromium ug/L ND 10.0 06/09/11 14:19 Cobalt ug/L ND 10.0 06/09/11 14:19 Copper ug/L ND 10.0 06/09/11 14:19 Lead ug/L ND 10.0 06/09/11 14:19 Nickel ug/L ND 50.0 06/09/11 14:19 Selenium ug/L ND 10.0 06/09/11 14:19 Silver ug/L 0.17J 10.0 06/09/11 14:19 Thallium ug/L ND 5.5 06/09/11 14:19 Vanadium ug/L ND 25.0 06/09/11 14:19 Zinc ug/L 6.9J 10.0 06/09/11 14:19 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 614939LABORATORY CONTROL SAMPLE: LCSSpike Antimony ug/L 487500 97 80-120 Arsenic ug/L 494500 99 80-120 Barium ug/L 507500 101 80-120 Beryllium ug/L 497500 99 80-120 Cadmium ug/L 495500 99 80-120 Chromium ug/L 485500 97 80-120 Cobalt ug/L 494500 99 80-120 Copper ug/L 507500 101 80-120 Lead ug/L 493500 99 80-120 Nickel ug/L 498500 100 80-120 Selenium ug/L 494500 99 80-120 Silver ug/L 243250 97 80-120 Thallium ug/L 492500 98 80-120 Vanadium ug/L 490500 98 80-120 Zinc ug/L 491500 98 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 614940MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9295374002 614941 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Antimony ug/L 500 97 75-12599 2 25500ND483495 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 46 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Parameter Units MS Result % Rec Limits Qual% RecConc. 614940MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9295374002 614941 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic ug/L 500 98 75-125100 2 25500ND488498 Barium ug/L 500 100 75-125102 2 2550074.4J 573 585 Beryllium ug/L 500 98 75-12599 1 25500ND491497 Cadmium ug/L 500 98 75-125100 2 25500ND489499 Chromium ug/L 500 96 75-12598 2 25500ND482492 Cobalt ug/L 500 98 75-125100 2 2550041.7 533 543 Copper ug/L 500 101 75-125103 2 255004.8J 508 519 Lead ug/L 500 97 75-12599 2 25500ND487495 Nickel ug/L 500 98 75-125100 2 255003.0J 494 503 Selenium ug/L 500 98 75-125101 3 25500ND493507 Silver ug/L 250 96 75-12598 2 252500.29J 241 246 Thallium ug/L 500 97 75-125100 3 25500ND485498 Vanadium ug/L 500 97 75-12599 2 255000.37J 486 497 Zinc ug/L 500 96 75-12597 2 2550020.1 499 507 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 47 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/15415 EPA 8260 EPA 8260 8260 MSV Low Level Landfill Associated Lab Samples:9294822001, 9294822002, 9294822003, 9294822004, 9294822005, 9294822006, 9294822007, 9294822008, 9294822009, 9294822010, 9294822011, 9294822012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:611052 Associated Lab Samples:9294822001, 9294822002, 9294822003, 9294822004, 9294822005, 9294822006, 9294822007, 9294822008, 9294822009, 9294822010, 9294822011, 9294822012 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/25/11 19:35 1,1,1-Trichloroethane ug/L ND 1.0 05/25/11 19:35 1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/25/11 19:35 1,1,2-Trichloroethane ug/L ND 1.0 05/25/11 19:35 1,1-Dichloroethane ug/L ND 5.0 05/25/11 19:35 1,1-Dichloroethene ug/L ND 5.0 05/25/11 19:35 1,2,3-Trichloropropane ug/L ND 1.0 05/25/11 19:35 1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/25/11 19:35 1,2-Dibromoethane (EDB)ug/L ND 1.0 05/25/11 19:35 1,2-Dichlorobenzene ug/L ND 5.0 05/25/11 19:35 1,2-Dichloroethane ug/L ND 1.0 05/25/11 19:35 1,2-Dichloropropane ug/L ND 1.0 05/25/11 19:35 1,3-Dichloropropane ug/L ND 1.0 05/25/11 19:35 1,4-Dichlorobenzene ug/L ND 1.0 05/25/11 19:35 2-Butanone (MEK)ug/L ND 100 05/25/11 19:35 2-Hexanone ug/L ND 50.0 05/25/11 19:35 4-Methyl-2-pentanone (MIBK)ug/L ND 100 05/25/11 19:35 Acetone ug/L ND 100 05/25/11 19:35 Acrylonitrile ug/L ND 200 05/25/11 19:35 Benzene ug/L ND 1.0 05/25/11 19:35 Bromochloromethane ug/L ND 3.0 05/25/11 19:35 Bromodichloromethane ug/L ND 1.0 05/25/11 19:35 Bromoform ug/L ND 3.0 05/25/11 19:35 Bromomethane ug/L ND 10.0 05/25/11 19:35 Carbon disulfide ug/L ND 100 05/25/11 19:35 Carbon tetrachloride ug/L ND 1.0 05/25/11 19:35 Chlorobenzene ug/L ND 3.0 05/25/11 19:35 Chloroethane ug/L ND 10.0 05/25/11 19:35 Chloroform ug/L ND 5.0 05/25/11 19:35 Chloromethane ug/L ND 1.0 05/25/11 19:35 cis-1,2-Dichloroethene ug/L ND 5.0 05/25/11 19:35 cis-1,3-Dichloropropene ug/L ND 1.0 05/25/11 19:35 Dibromochloromethane ug/L ND 3.0 05/25/11 19:35 Dibromomethane ug/L ND 10.0 05/25/11 19:35 Ethylbenzene ug/L ND 1.0 05/25/11 19:35 Iodomethane ug/L ND 10.0 05/25/11 19:35 Methylene Chloride ug/L ND 1.0 05/25/11 19:35 Styrene ug/L ND 1.0 05/25/11 19:35 Tetrachloroethene ug/L ND 1.0 05/25/11 19:35 Toluene ug/L ND 1.0 05/25/11 19:35 trans-1,2-Dichloroethene ug/L ND 5.0 05/25/11 19:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 48 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:611052 Associated Lab Samples:9294822001, 9294822002, 9294822003, 9294822004, 9294822005, 9294822006, 9294822007, 9294822008, 9294822009, 9294822010, 9294822011, 9294822012 Matrix:Water Analyzed trans-1,3-Dichloropropene ug/L ND 1.0 05/25/11 19:35 trans-1,4-Dichloro-2-butene ug/L ND 100 05/25/11 19:35 Trichloroethene ug/L ND 1.0 05/25/11 19:35 Trichlorofluoromethane ug/L ND 1.0 05/25/11 19:35 Vinyl acetate ug/L ND 50.0 05/25/11 19:35 Vinyl chloride ug/L ND 1.0 05/25/11 19:35 Xylene (Total)ug/L ND 5.0 05/25/11 19:35 1,2-Dichloroethane-d4 (S)%103 70-130 05/25/11 19:35 4-Bromofluorobenzene (S)%94 70-130 05/25/11 19:35 Dibromofluoromethane (S)%102 70-130 05/25/11 19:35 Toluene-d8 (S)%97 70-130 05/25/11 19:35 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 611053LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 54.050 108 70-130 1,1,1-Trichloroethane ug/L 56.750 113 70-130 1,1,2,2-Tetrachloroethane ug/L 50.150 100 70-130 1,1,2-Trichloroethane ug/L 51.650 103 70-130 1,1-Dichloroethane ug/L 55.750 111 70-130 1,1-Dichloroethene ug/L 60.350 121 70-132 1,2,3-Trichloropropane ug/L 49.250 98 70-130 1,2-Dibromo-3-chloropropane ug/L 46.150 92 70-130 1,2-Dibromoethane (EDB)ug/L 52.750 105 70-130 1,2-Dichlorobenzene ug/L 49.950 100 70-130 1,2-Dichloroethane ug/L 55.050 110 70-130 1,2-Dichloropropane ug/L 55.250 110 70-130 1,3-Dichloropropane ug/L 52.250 104 70-130 1,4-Dichlorobenzene ug/L 49.050 98 70-130 2-Butanone (MEK)ug/L 109100 109 70-145 2-Hexanone ug/L 93.5100 93 70-144 4-Methyl-2-pentanone (MIBK)ug/L 103100 103 70-140 Acetone ug/L 107100 107 50-175 Acrylonitrile ug/L 272250 109 70-143 Benzene ug/L 55.550 111 70-130 Bromochloromethane ug/L 57.350 115 70-130 Bromodichloromethane ug/L 55.850 112 70-130 Bromoform ug/L 47.050 94 70-130 Bromomethane ug/L 52.050 104 54-130 Carbon disulfide ug/L 60.2J50 120 70-131 Carbon tetrachloride ug/L 57.350 115 70-132 Chlorobenzene ug/L 51.650 103 70-130 Chloroethane ug/L 48.650 97 64-134 Chloroform ug/L 55.850 112 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 49 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 611053LABORATORY CONTROL SAMPLE: LCSSpike Chloromethane ug/L 46.150 92 64-130 cis-1,2-Dichloroethene ug/L 53.450 107 70-131 cis-1,3-Dichloropropene ug/L 59.150 118 70-130 Dibromochloromethane ug/L 53.650 107 70-130 Dibromomethane ug/L 54.550 109 70-131 Ethylbenzene ug/L 51.150 102 70-130 Iodomethane ug/L 121100 121 49-180 Methylene Chloride ug/L 58.250 116 63-130 Styrene ug/L 55.750 111 70-130 Tetrachloroethene ug/L 54.950 110 70-130 Toluene ug/L 54.950 110 70-130 trans-1,2-Dichloroethene ug/L 54.550 109 70-130 trans-1,3-Dichloropropene ug/L 56.650 113 70-132 trans-1,4-Dichloro-2-butene ug/L 45.0J50 90 70-141 Trichloroethene ug/L 56.850 114 70-130 Trichlorofluoromethane ug/L 49.350 99 62-133 Vinyl acetate ug/L 114100 114 66-157 Vinyl chloride ug/L 46.050 92 69-130 Xylene (Total)ug/L 150150 100 70-130 1,2-Dichloroethane-d4 (S)%98 70-130 4-Bromofluorobenzene (S)%101 70-130 Dibromofluoromethane (S)%100 70-130 Toluene-d8 (S)%102 70-130 Parameter Units MS Result % Rec Limits Qual% RecConc. 611054MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9294822011 611055 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1-Dichloroethene ug/L 50 148 70-166147 1 3050ND74.1 73.5 Benzene ug/L 50 129 70-148129 0 3050ND64.5 64.5 Chlorobenzene ug/L 50 119 70-146117 1 3050ND59.4 58.7 Toluene ug/L 50 122 70-155120 1 3050ND61.0 60.2 Trichloroethene ug/L 50 127 69-151126 1 3050ND63.3 62.9 1,2-Dichloroethane-d4 (S)%109 70-130108 4-Bromofluorobenzene (S)%98 70-13099 Dibromofluoromethane (S)%106 70-130107 Toluene-d8 (S)%97 70-13096 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 50 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/15449 EPA 8260 EPA 8260 8260 MSV Low Level Landfill Associated Lab Samples:9294822013, 9294822014, 9294822015, 9294822016 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:612554 Associated Lab Samples:9294822013, 9294822014, 9294822015, 9294822016 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/27/11 19:54 1,1,1-Trichloroethane ug/L ND 1.0 05/27/11 19:54 1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/27/11 19:54 1,1,2-Trichloroethane ug/L ND 1.0 05/27/11 19:54 1,1-Dichloroethane ug/L ND 5.0 05/27/11 19:54 1,1-Dichloroethene ug/L ND 5.0 05/27/11 19:54 1,2,3-Trichloropropane ug/L ND 1.0 05/27/11 19:54 1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/27/11 19:54 1,2-Dibromoethane (EDB)ug/L ND 1.0 05/27/11 19:54 1,2-Dichlorobenzene ug/L ND 5.0 05/27/11 19:54 1,2-Dichloroethane ug/L ND 1.0 05/27/11 19:54 1,2-Dichloropropane ug/L ND 1.0 05/27/11 19:54 1,3-Dichloropropane ug/L ND 1.0 05/27/11 19:54 1,4-Dichlorobenzene ug/L ND 1.0 05/27/11 19:54 2-Butanone (MEK)ug/L ND 100 05/27/11 19:54 2-Hexanone ug/L ND 50.0 05/27/11 19:54 4-Methyl-2-pentanone (MIBK)ug/L ND 100 05/27/11 19:54 Acetone ug/L ND 100 05/27/11 19:54 Acrylonitrile ug/L ND 200 05/27/11 19:54 Benzene ug/L ND 1.0 05/27/11 19:54 Bromochloromethane ug/L ND 3.0 05/27/11 19:54 Bromodichloromethane ug/L ND 1.0 05/27/11 19:54 Bromoform ug/L ND 3.0 05/27/11 19:54 Bromomethane ug/L ND 10.0 05/27/11 19:54 Carbon disulfide ug/L ND 100 05/27/11 19:54 Carbon tetrachloride ug/L ND 1.0 05/27/11 19:54 Chlorobenzene ug/L 0.28J 3.0 05/27/11 19:54 Chloroethane ug/L ND 10.0 05/27/11 19:54 Chloroform ug/L ND 5.0 05/27/11 19:54 Chloromethane ug/L ND 1.0 05/27/11 19:54 cis-1,2-Dichloroethene ug/L ND 5.0 05/27/11 19:54 cis-1,3-Dichloropropene ug/L ND 1.0 05/27/11 19:54 Dibromochloromethane ug/L ND 3.0 05/27/11 19:54 Dibromomethane ug/L ND 10.0 05/27/11 19:54 Ethylbenzene ug/L ND 1.0 05/27/11 19:54 Iodomethane ug/L ND 10.0 05/27/11 19:54 Methylene Chloride ug/L ND 1.0 05/27/11 19:54 Styrene ug/L ND 1.0 05/27/11 19:54 Tetrachloroethene ug/L ND 1.0 05/27/11 19:54 Toluene ug/L ND 1.0 05/27/11 19:54 trans-1,2-Dichloroethene ug/L ND 5.0 05/27/11 19:54 trans-1,3-Dichloropropene ug/L ND 1.0 05/27/11 19:54 trans-1,4-Dichloro-2-butene ug/L ND 100 05/27/11 19:54 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 51 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:612554 Associated Lab Samples:9294822013, 9294822014, 9294822015, 9294822016 Matrix:Water Analyzed Trichloroethene ug/L ND 1.0 05/27/11 19:54 Trichlorofluoromethane ug/L ND 1.0 05/27/11 19:54 Vinyl acetate ug/L ND 50.0 05/27/11 19:54 Vinyl chloride ug/L ND 1.0 05/27/11 19:54 Xylene (Total)ug/L ND 5.0 05/27/11 19:54 1,2-Dichloroethane-d4 (S)%96 70-130 05/27/11 19:54 4-Bromofluorobenzene (S)%99 70-130 05/27/11 19:54 Dibromofluoromethane (S)%96 70-130 05/27/11 19:54 Toluene-d8 (S)%100 70-130 05/27/11 19:54 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 612555LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 54.050 108 70-130 1,1,1-Trichloroethane ug/L 52.250 104 70-130 1,1,2,2-Tetrachloroethane ug/L 52.950 106 70-130 1,1,2-Trichloroethane ug/L 52.550 105 70-130 1,1-Dichloroethane ug/L 51.850 104 70-130 1,1-Dichloroethene ug/L 51.150 102 70-132 1,2,3-Trichloropropane ug/L 50.050 100 70-130 1,2-Dibromo-3-chloropropane ug/L 54.350 109 70-130 1,2-Dibromoethane (EDB)ug/L 51.450 103 70-130 1,2-Dichlorobenzene ug/L 51.650 103 70-130 1,2-Dichloroethane ug/L 52.350 105 70-130 1,2-Dichloropropane ug/L 51.950 104 70-130 1,3-Dichloropropane ug/L 52.650 105 70-130 1,4-Dichlorobenzene ug/L 51.450 103 70-130 2-Butanone (MEK)ug/L 103100 103 70-145 2-Hexanone ug/L 107100 107 70-144 4-Methyl-2-pentanone (MIBK)ug/L 104100 104 70-140 Acetone ug/L 96.1J100 96 50-175 Acrylonitrile ug/L 245250 98 70-143 Benzene ug/L 50.250 100 70-130 Bromochloromethane ug/L 46.250 92 70-130 Bromodichloromethane ug/L 52.850 106 70-130 Bromoform ug/L 54.850 110 70-130 Bromomethane ug/L 48.150 96 54-130 Carbon disulfide ug/L 51.4J50 103 70-131 Carbon tetrachloride ug/L 52.850 106 70-132 Chlorobenzene ug/L 51.850 104 70-130 Chloroethane ug/L 50.550 101 64-134 Chloroform ug/L 53.050 106 70-130 Chloromethane ug/L 47.050 94 64-130 cis-1,2-Dichloroethene ug/L 50.150 100 70-131 cis-1,3-Dichloropropene ug/L 52.950 106 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 52 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 612555LABORATORY CONTROL SAMPLE: LCSSpike Dibromochloromethane ug/L 53.650 107 70-130 Dibromomethane ug/L 52.950 106 70-131 Ethylbenzene ug/L 53.550 107 70-130 Iodomethane ug/L 90.4100 90 49-180 Methylene Chloride ug/L 47.450 95 63-130 Styrene ug/L 55.250 110 70-130 Tetrachloroethene ug/L 54.350 109 70-130 Toluene ug/L 51.250 102 70-130 trans-1,2-Dichloroethene ug/L 50.650 101 70-130 trans-1,3-Dichloropropene ug/L 53.650 107 70-132 trans-1,4-Dichloro-2-butene ug/L 56.0J50 112 70-141 Trichloroethene ug/L 52.850 106 70-130 Trichlorofluoromethane ug/L 54.550 109 62-133 Vinyl acetate ug/L 102100 102 66-157 Vinyl chloride ug/L 50.050 100 69-130 Xylene (Total)ug/L 159150 106 70-130 1,2-Dichloroethane-d4 (S)%98 70-130 4-Bromofluorobenzene (S)%100 70-130 Dibromofluoromethane (S)%98 70-130 Toluene-d8 (S)%99 70-130 Parameter Units MS Result % Rec Limits Qual% RecConc. 612556MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9294940013 612557 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1-Dichloroethene ug/L 50 109 70-166109 0 3050ND54.3 54.4 Benzene ug/L 50 115 70-148114 1 3050ND57.4 56.8 Chlorobenzene ug/L 50 113 70-146116 2 3050ND56.7 58.1 Toluene ug/L 50 114 70-155113 1 3050ND57.2 56.4 Trichloroethene ug/L 50 119 69-151116 3 30501.0 60.5 59.0 1,2-Dichloroethane-d4 (S)%99 70-13097 4-Bromofluorobenzene (S)%97 70-13098 Dibromofluoromethane (S)%95 70-13095 Toluene-d8 (S)%100 70-13097 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 53 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WET/16516 SM 5210B SM 5210B 5210B BOD, 5 day Associated Lab Samples:9294822012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:611058 Associated Lab Samples:9294822012 Matrix:Water Analyzed BOD, 5 day ug/L ND 2000 05/30/11 11:45 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 611059LABORATORY CONTROL SAMPLE: LCSSpike BOD, 5 day ug/L 182000198000 92 84-115 Parameter Units Dup Result Max RPD QualifiersRPDResult 9294785001 611060SAMPLE DUPLICATE: BOD, 5 day ug/L 280000 R19420101 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 54 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WET/16571 EPA 9040 EPA 9040 9040 pH Associated Lab Samples:9294822012 Parameter Units Dup Result Max RPD QualifiersRPDResult 9294488003 613212SAMPLE DUPLICATE: pH Std. Units 6.1 H60206.1 Parameter Units Dup Result Max RPD QualifiersRPDResult 9294563001 613213SAMPLE DUPLICATE: pH Std. Units 6.7 H60206.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 55 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/9803 EPA 300.0 EPA 300.0 300.0 IC Anions Associated Lab Samples:9294822012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:614553 Associated Lab Samples:9294822012 Matrix:Water Analyzed Sulfate ug/L ND 250000 06/06/11 18:17 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 614554LABORATORY CONTROL SAMPLE: LCSSpike Sulfate ug/L 18900J20000 95 90-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 614555MATRIX SPIKE SAMPLE: MSSpike Result 9294822012 Sulfate ug/L 32100J M02000011290-1109670J Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 614557MATRIX SPIKE SAMPLE: MSSpike Result 9294816005 Sulfate ug/L 25000J20000 106 90-110ND Parameter Units Dup Result Max RPD QualifiersRPDResult 9294822012 614556SAMPLE DUPLICATE: Sulfate ug/L 9660J 0 209670J Parameter Units Dup Result Max RPD QualifiersRPDResult 9294816005 614558SAMPLE DUPLICATE: Sulfate ug/L ND 20ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 56 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/9759 EPA 353.2 EPA 353.2 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples:9294822012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:610742 Associated Lab Samples:9294822012 Matrix:Water Analyzed Nitrogen, Nitrate ug/L ND 10000 05/24/11 23:11 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 610743LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate ug/L 5160J5000 103 90-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 610744MATRIX SPIKE SAMPLE: MSSpike Result 9294822012 Nitrogen, Nitrate ug/L 15800J M1500017290-1107160J Parameter Units Dup Result Max RPD QualifiersRPDResult 9294822012 610745SAMPLE DUPLICATE: Nitrogen, Nitrate ug/L 7140J 0 207160J REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 57 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/9844 EPA 365.1 EPA 365.1 365.1 Phosphorus, Total Associated Lab Samples:9294822012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:617647 Associated Lab Samples:9294822012 Matrix:Water Analyzed Phosphorus ug/L ND 50.0 06/09/11 11:08 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 617648LABORATORY CONTROL SAMPLE: LCSSpike Phosphorus ug/L 25202500 101 90-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 617649MATRIX SPIKE SAMPLE: MSSpike Result 9294822012 Phosphorus ug/L 3140 M1250011490-110297 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 617655MATRIX SPIKE SAMPLE: MSSpike Result 9295072001 Phosphorus ug/L 28802500 101 90-1100.36 mg/L Parameter Units Dup Result Max RPD QualifiersRPDResult 9295072002 617656SAMPLE DUPLICATE: Phosphorus ug/L 86.5 6 200.092 mg/L Parameter Units Dup Result Max RPD QualifiersRPDResult 9295072003 617657SAMPLE DUPLICATE: Phosphorus ug/L 228 19 200.19 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 58 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/9834 SM 5220D SM 5220D 5220D COD Associated Lab Samples:9294822012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:616413 Associated Lab Samples:9294822012 Matrix:Water Analyzed Chemical Oxygen Demand ug/L ND 25000 06/07/11 14:18 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 616414LABORATORY CONTROL SAMPLE: LCSSpike Chemical Oxygen Demand ug/L 745000750000 99 90-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 616416MATRIX SPIKE SAMPLE: MSSpike Result 9294815001 Chemical Oxygen Demand ug/L 976000750000 124 75-12546.0 mg/L Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 616418MATRIX SPIKE SAMPLE: MSSpike Result 9294822012 Chemical Oxygen Demand ug/L 911000750000 111 75-12580000 Parameter Units Dup Result Max RPD QualifiersRPDResult 9294815001 616415SAMPLE DUPLICATE: Chemical Oxygen Demand ug/L 55000 18 2046.0 mg/L Parameter Units Dup Result Max RPD QualifiersRPDResult 9294855001 616417SAMPLE DUPLICATE: Chemical Oxygen Demand ug/L 105000 6 20111 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 59 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALIFIERS Pace Project No.: Project: 9294822 SURRY CO. LINED MSWLF DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Analysis initiated more than 15 minutes after sample collection.H6 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/15/2011 04:43 PM Page 60 of 60 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921