9209_NorthWakeSubtitleD_GWMR_DIN28105_20160831

North Wake Subtitle D Landfill
Facility Permit No. 9209-MSWLF-1996
Semi-Annual Sampling Report
(September 2016 Sampling Event)
Wake County
Report
Prepared December 2016

5400 Glenwood Avenue, Suite 400
Raleigh, North Carolina 27612
tel: [phone]
fax: [phone]

December 16, 2016

Ms. Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
2090 U.S. 70 Highway
Swannanoa, North Carolina 28778

Subject: September 2016 Semi-Annual Monitoring Sampling Report
North Wake Subtitle D Landfill
Facility Permit No. 9209-MSWLF-1996

Dear Ms. Drummond:
CDM Smith Inc., on behalf of Wake County (County), is submitting an electronic copy of the
September 2016 semi-annual sampling event report for the North Wake Subtitle D Landfill (site). This
letter report presents the results of the most recent semi-annual sampling event and constitutes the
second semi-annual sampling event for 2016. The approved groundwater monitoring network consists
of two background wells (i.e. MW-11 and -11D), 16 downgradient compliance wells (i.e. MW-12, -12D,
-13, -14, -15, -15d, -16, -17, -17D, -18, -19, -20, -21, -25, -25d, and -26), and three surface water
sample locations (i.e. SW-4, -5, and -6). Field activities and sampling results are discussed below.
Field Activities
Groundwater samples from the North Wake Subtitle D Landfill were collected August 31 and
September 1, 2016. All samples were collected by use of disposable, laboratory decontaminated
bailers. Monitoring well and surface water sampling locations are presented on Figure 1. Well
construction details are provided in Table 1.
Groundwater elevations were measured at each well prior to sampling and are presented in Table 2.
These groundwater elevations were used to construct potentiometric contours for this sampling event
and are presented on Figure 1. The groundwater elevations and potentiometric contours were used to
estimate the groundwater velocity at each well. Groundwater velocity values are provided in Table 3.
After depth to groundwater was determined, three well volumes of water were removed from each
well prior to sampling to provide fresh formation water within the well water column. Each well
volume was measured in the field for pH, conductivity, temperature, turbidity, dissolved oxygen, and
oxidation-reduction potential using a YSI-556 multi-parameter water quality meter and a HANNA HI
98703 turbidity meter. Wells that had elevated turbidity were allowed to stabilize prior to sample
collection. The water quality parameters at the time of sampling are presented in Table 2.

Ms. Jaclynne Drummond
December 16, 2016
Page 2
Sampling Results
Shealy Environmental Services, Inc. located in West Columbia, South Carolina, analyzed the
groundwater and surface water samples for the North Carolina Appendix I volatile organic compounds
and metals. In accordance with Solid Waste Section (SWS) guidelines the analytical results were
reported to the laboratory specific method detection limit (MDL) and are quantifiable at or below
SWS Limits (SWSLs). All monitoring wells and surface water sample locations for the Subtitle D Landfill
had detections of analytes above the MDL with a majority of the detections below SWSLs. These
detections were qualified as estimated or “J” flags.
The following list indicates the analytes detected above the MDL at each sampling location. No “J” flag
detections are provided. Underlined analytes exceeded the 15A NCAC 02L .0202 (NC 2L) Groundwater
Standard, Groundwater Protection Standard, or the 15A NCAC 02B Surface Water Quality Standard for
Class C Waters. A complete summary of all detected and estimated concentrations for the September
2016 and previous sampling events is provided in Table 4. Laboratory analytical data reports are
provided in Appendix A.
MW-11 (Background)
Metals: Zinc
Volatile Organic Compounds: None Detected
MW-11D (Background, Deep)
Metals: None Detected
Volatile Organic Compounds: None Detected
MW-12
Metals: Barium, Beryllium, Cobalt, Copper, Lead, Vanadium, Zinc
Volatile Organic Compounds: None Detected
MW-12D
Metals: None Detected
Volatile Organic Compounds: None Detected
MW-13
Metals: Barium, Chromium, Cobalt, Vanadium, Zinc
Volatile Organic Compounds: None Detected
MW-14
Metals: Copper, Zinc
Volatile Organic Compounds: None Detected

Ms. Jaclynne Drummond
December 16, 2016
Page 3
MW-15
Metals: Copper, Zinc
Volatile Organic Compounds: None Detected
MW-15D
Metals: None Detected
Volatile Organic Compounds: None Detected
MW-16
Metals: Zinc
Volatile Organic Compounds: None Detected
MW-17
Metals: None Detected
Volatile Organic Compounds: None Detected
MW-17D
Metals: None Detected
Volatile Organic Compounds: None Detected
MW-18
Metals: Chromium, Copper, Zinc
Volatile Organic Compounds: None Detected
MW-19
Metals: None Detected
Volatile Organic Compounds: None Detected
MW-20
Metals: Barium, Chromium, Cobalt, Copper, Vanadium, Zinc
Volatile Organic Compounds: None Detected
MW-21
Metals: Barium, Cobalt, Copper, Vanadium, Zinc
Volatile Organic Compounds: None Detected
MW-25
Metals: Zinc
Volatile Organic Compounds: None Detected

Ms. Jaclynne Drummond
December 16, 2016
Page 4
MW-25D
Metals: Copper
Volatile Organic Compounds: None Detected
MW-26
Metals: Cobalt, Copper, Zinc
Volatile Organic Compounds: None Detected
SW-4
Metals: None Detected
Volatile Organic Compounds: None Detected
SW-5
Metals: None Detected
Volatile Organic Compounds: None Detected
SW-6
Metals: None Detected
Volatile Organic Compounds: None Detected
“J” flags were not included in the previous list, but several locations had “J” flag detections that
exceeded the standards. The “J” flag constituents above the standards along with their locations are
listed below.
Cobalt: MW-11, -14, -15, -16, -18, -25, -25D, and SW-6
Lead: SW-6
Thallium: MW-12, -13, and -21
Vanadium: MW-11, -11D, -12D, -14, -15, -15D, -16, -17, -17D, -18, -19, -25, -25D, and -26

Equipment and trip blanks were analyzed for quality control. A duplicate sample was also collected for
quality control. Copper, zinc, acetone, and 2-butanone were detected in the equipment blank below
their respective NC 2L Standard. No analytes were detected in the trip blank above the MDL. The
duplicate sample, identified as Dup, was collected from MW-17D and had similar analyte
concentrations as those detected in MW-17D. Table 5 presents a summary of all parameters detected
during the September 2016 sampling event that exceeded the NC 2L or Groundwater Protection
Standards.
CDM Smith, on behalf of the County, submitted the results of an Alternative Source Demonstration
(ASD) for the site on November 7, 2016. The ASD was prepared in accordance with Solid Waste rule
.1633(c)(3), to demonstrate that select metals exceeding the NC 2L Groundwater Standards detected
in monitoring wells at the site are naturally occurring and not related to a release from the landfill. As
part of the ASD, in order to determine if turbidity was a contributing factor to total reported metals,

Ms. Jaclynne Drummond
December 16, 2016
Page 5
filtered samples were collected during the September 2016 sampling event and analyzed for dissolved
metals. Dissolved metal sample results are provided in Table 4. Based on qualitative and quantitative
evaluation of current and historic groundwater sampling data, the NC 2L metal exceedances were
determined to be indicative of naturally occurring background concentrations as opposed to a release
from the landfill.
The County will continue with the semi-annual groundwater monitoring program. The next sampling
event will take place during the spring of 2017. If you have any questions or require further
explanation, do not hesitate to call me at [phone].
Very truly yours,

Mathew F. Colone, P.G.
CDM Smith Inc.

cc: John Roberson, WCSWM
Elliott Cornell, WCSWM

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December 2016
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1
December 2016
Table 3
Summary of Calculated Groundwater Flow Velocities
September 2016 Semi-Annual Sampling Event
North Wake Lined Landfill - Permit Number 9209-MSWLF-1996
Monitoring Well
Code
Hydraulic
Conductivity feet/day
(cm/s)
Gradient Effective
Porosity
Average Linear Velocity
(feet/day)
MW-11 5.66 (2.00E-03)0.0257 0.13 1.12E+00
MW-11D 0.509 (1.80E-04)0.0257 0.05 2.62E-01
MW-12 0.486 (1.71E-04)0.0281 0.13 1.05E-01
MW-12D 5.24 (1.85E-03)0.0288 0.05 3.02E+00
MW-13 1.02 (3.60E-04)0.0262 0.13 2.06E-01
MW-14 2.05 (7.23E-04)0.0305 0.13 4.82E-01
MW-15 2.54 (8.96E-04)0.0280 0.25 2.84E-01
MW-15D 1.33 (4.69E-04)0.0282 0.05 7.51E-01
MW-16 0.00967 (3.41E-06)0.0256 0.05 4.96E-03
MW-17 1.18 (4.16E-04)0.0260 0.18 1.71E-01
MW-17D 0.367 (1.29E-04)0.0261 0.05 1.92E-01
MW-18 6.86 (2.42E-03)0.0211 0.13 1.11E+00
MW-19 1.40 (4.92E-04)0.0305 0.08 5.33E-01
MW-20 0.58 (2.06E-04)0.0254 0.13 1.13E-01
MW-21 1.34 (4.73E-04)0.0226 0.13 2.33E-01
MW-25 1.40 (4.96E-04)0.0210 0.15 1.96E-01
MW-25D 0.02 (8.04E-06)0.0196 0.15 2.62E-03
MW-26 0.72 (2.54E-04)0.0229 0.13 1.27E-01
Notes:
1. cm/s - centimeters per second
2. Hydraulic conductivity and effective porosity values are estimated from previously performed
slug tests and grain size analyses.
3. The gradient and linear velocity values shown for MW-11 are based on the average of the
regolith monitoring wells.
4. The gradient and linear velocity values shown for MW-11d are based on the average of the
bedrock monitoring wells.
Page 1 of 1 December 2016
Ta
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4
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B

-

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c
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l
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7.

D
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m
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s
a
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A
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n
.
Pa
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7

o
f

1
3
December 2016
Table 4B
Detected Groundwater Constituents - Volatile Organic Compounds
September 2016 Semi-Annual Sampling Event
North Wake Lined Landfill - Permit Number 9209-MSWLF-1996
Mo
n
i
t
o
r
i
n
g

W
e
l
l

C
o
d
e
Sa
m
p
l
e

D
a
t
e
Ac
e
t
o
n
e
Br
o
m
o
m
e
t
h
a
n
e
Ch
l
o
r
o
m
e
t
h
a
n
e
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
m,
p
-
X
y
l
e
n
e
s
o-
X
y
l
e
n
e
6,000 10*3 5 0.7 500 500
100 10 1 1 1 5 5
MW-11 17-Mar-11
MW-11 1-Nov-11
MW-11 25-Apr-12
MW-11 23-Oct-12
MW-11 17-Apr-13
MW-11 16-Oct-13
MW-11 17-Apr-14
MW-11 13-Nov-14
MW-11 30-Apr-15 0.54J
MW-11 15-Oct-15 0.28JB
MW-11 21-Apr-16
MW-11 1-Sep-16
MW-11D 18-Mar-11
MW-11D 2-Nov-11
MW-11D 26-Apr-12
MW-11D 24-Oct-12
MW-11D 18-Apr-13
MW-11D 17-Apr-14
MW-11D 13-Nov-14
MW-11D 29-Apr-15
MW-11D 15-Oct-15 0.24JB
MW-11D 21-Apr-16 1.3J 0.71J
MW-11D 1-Sep-16
MW-12 15-Mar-11 6.0J
MW-12 20-Oct-11
MW-12 11-Apr-12
MW-12 26-Oct-12
MW-12 11-Apr-13 16J
MW-12 2-Oct-13
MW-12 4-Apr-14 6.0J
MW-12 12-Nov-14
MW-12 8-Apr-15 9.6J
MW-12 7-Oct-15
MW-12 25-Mar-16
MW-12 1-Sep-16
MW-12D 15-Mar-11
MW-12D 20-Oct-11
MW-12D 11-Apr-12
MW-12D 26-Oct-12
MW-12D 11-Apr-13
MW-12D (dup)11-Apr-13
MW-12D 2-Oct-13
MW-12D 4-Apr-14
MW-12D 13-Nov-14
MW-12D 8-Apr-15 1.2
MW-12D 13-May-15
MW-12D 7-Oct-15
MW-12D 25-Mar-16
MW-12D 1-Sep-16
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
Page 8 of 13 December 2016
Table 4B
Detected Groundwater Constituents - Volatile Organic Compounds
September 2016 Semi-Annual Sampling Event
North Wake Lined Landfill - Permit Number 9209-MSWLF-1996
Mo
n
i
t
o
r
i
n
g

W
e
l
l

C
o
d
e
Sa
m
p
l
e

D
a
t
e
Ac
e
t
o
n
e
Br
o
m
o
m
e
t
h
a
n
e
Ch
l
o
r
o
m
e
t
h
a
n
e
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
m,
p
-
X
y
l
e
n
e
s
o-
X
y
l
e
n
e
6,000 10*3 5 0.7 500 500
100 10 1 1 1 5 5
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-13 15-Mar-11
MW-13 20-Oct-11
MW-13 11-Apr-12
MW-13 26-Oct-12
MW-13 11-Apr-13
MW-13 2-Oct-13
MW-13 4-Apr-14
MW-13 12-Nov-14
MW-13 8-Apr-15
MW-13 7-Oct-15
MW-13 25-Mar-16
MW-13 1-Sep-16
MW-14 15-Mar-11
MW-14 20-Oct-11
MW-14 11-Apr-12
MW-14 26-Oct-12
MW-14 11-Apr-13
MW-14 2-Oct-13
MW-14 4-Apr-14
MW-14 13-Nov-14
MW-14 8-Apr-15
MW-14 8-Oct-15 0.75J
MW-14 25-Mar-16
MW-14 1-Sep-16
MW-15 14-Mar-11
MW-15 20-Oct-11 4.7J
MW-15 11-Apr-12
MW-15 26-Oct-12
MW-15 11-Apr-13
MW-15 2-Oct-13
MW-15 4-Apr-14
MW-15 13-Nov-14
MW-15 9-Apr-15
MW-15 8-Oct-15
MW-15 25-Mar-16
MW-15 (dup)25-Mar-16
MW-15 1-Sep-16
MW-15D 14-Mar-11
MW-15D 19-Oct-11
MW-15D 10-Apr-12
MW-15D 25-Oct-12
MW-15D 10-Apr-13
MW-15D 2-Oct-13
MW-15D 4-Apr-14
MW-15D 13-Nov-14
MW-15D (dup)13-Nov-14
MW-15D 9-Apr-15 1
MW-15D 14-May-15
MW-15D 8-Oct-15 0.78J
MW-15D 25-Mar-16
MW-15D 1-Sep-16
Page 9 of 13 December 2016
Table 4B
Detected Groundwater Constituents - Volatile Organic Compounds
September 2016 Semi-Annual Sampling Event
North Wake Lined Landfill - Permit Number 9209-MSWLF-1996
Mo
n
i
t
o
r
i
n
g

W
e
l
l

C
o
d
e
Sa
m
p
l
e

D
a
t
e
Ac
e
t
o
n
e
Br
o
m
o
m
e
t
h
a
n
e
Ch
l
o
r
o
m
e
t
h
a
n
e
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
m,
p
-
X
y
l
e
n
e
s
o-
X
y
l
e
n
e
6,000 10*3 5 0.7 500 500
100 10 1 1 1 5 5
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-16 15-Mar-11
MW-16 20-Oct-11
MW-16 11-Apr-12
MW-16 26-Oct-12
MW-16 11-Apr-13
MW-16 2-Oct-13
MW-16 4-Apr-14
MW-16 13-Nov-14
MW-16 9-Apr-15
MW-16 8-Oct-15
MW-16 25-Mar-16
MW-16 1-Sep-16
MW-17 15-Mar-11
MW-17 20-Oct-11
MW-17 11-Apr-12
MW-17 26-Oct-12
MW-17 11-Apr-13
MW-17 2-Oct-13
MW-17 4-Apr-14
MW-17 13-Nov-14
MW-17 9-Apr-15
MW-17 8-Oct-15
MW-17 25-Mar-16
MW-17 1-Sep-16
MW-17D 14-Mar-11
MW-17D 19-Oct-11
MW-17D (dup)19-Oct-11
MW-17D 10-Apr-12
MW-17D 25-Oct-12
MW-17D 10-Apr-13
MW-17D 2-Oct-13
MW-17D 4-Apr-14
MW-17D 13-Nov-14
MW-17D 9-Apr-15 0.84J
MW-17D 14-May-15 0.37J
MW-17D 8-Oct-15 0.69J
MW-17D (dup)8-Oct-15 0.34J 0.20J
MW-17D 25-Mar-16
MW-17D 1-Sep-16
MW-17D (dup)1-Sep-16
MW-18 15-Mar-11
MW-18 20-Oct-11
MW-18 11-Apr-12
MW-18 26-Oct-12
MW-18 11-Apr-13
MW-18 2-Oct-13
MW-18 4-Apr-14
MW-18 13-Nov-14
MW-18 9-Apr-15
MW-18 8-Oct-15 5.7J
MW-18 25-Mar-16
MW-18 1-Sep-16
Page 10 of 13 December 2016
Table 4B
Detected Groundwater Constituents - Volatile Organic Compounds
September 2016 Semi-Annual Sampling Event
North Wake Lined Landfill - Permit Number 9209-MSWLF-1996
Mo
n
i
t
o
r
i
n
g

W
e
l
l

C
o
d
e
Sa
m
p
l
e

D
a
t
e
Ac
e
t
o
n
e
Br
o
m
o
m
e
t
h
a
n
e
Ch
l
o
r
o
m
e
t
h
a
n
e
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
m,
p
-
X
y
l
e
n
e
s
o-
X
y
l
e
n
e
6,000 10*3 5 0.7 500 500
100 10 1 1 1 5 5
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-19 15-Mar-11
MW-19 (dup)15-Mar-11
MW-19 20-Oct-11
MW-19 10-Apr-12
MW-19 26-Oct-12
MW-19 11-Apr-13
MW-19 2-Oct-13
MW-19 4-Apr-14
MW-19 13-Nov-14
MW-19 8-Apr-15
MW-19 7-Oct-15
MW-19 25-Mar-16
MW-19 1-Sep-16
MW-20 15-Mar-11
MW-20 20-Oct-11
MW-20 11-Apr-12 0.42J
MW-20 (dup)11-Apr-12 0.45J
MW-20 26-Oct-12 4.3J
MW-20 11-Apr-13 0.35J
MW-20 2-Oct-13 0.30J
MW-20 4-Apr-14 0.35J
MW-20 12-Nov-14
MW-20 8-Apr-15 0.32J
MW-20 (dup)8-Apr-15 0.28J
MW-20 8-Oct-15
MW-20 25-Mar-16
MW-20 1-Sep-16
MW-21 15-Mar-11
MW-21 20-Oct-11
MW-21 10-Apr-12
MW-21 26-Oct-12
MW-21 11-Apr-13
MW-21 2-Oct-13
MW-21 (dup)2-Oct-13
MW-21 4-Apr-14
MW-21 12-Nov-14
MW-21 8-Apr-15
MW-21 8-Oct-15 7.1J
MW-21 25-Mar-16
MW-21 1-Sep-16
MW-25 14-Mar-11
MW-25 19-Oct-11
MW-25 11-Apr-12
MW-25 26-Oct-12
MW-25 10-Apr-13
MW-25 2-Oct-13
MW-25 4-Apr-14
MW-25 12-Nov-14
MW-25 9-Apr-15 20J
MW-25 7-Oct-15
MW-25 25-Mar-16 0.26J
MW-25 1-Sep-16
Page 11 of 13 December 2016
Table 4B
Detected Groundwater Constituents - Volatile Organic Compounds
September 2016 Semi-Annual Sampling Event
North Wake Lined Landfill - Permit Number 9209-MSWLF-1996
Mo
n
i
t
o
r
i
n
g

W
e
l
l

C
o
d
e
Sa
m
p
l
e

D
a
t
e
Ac
e
t
o
n
e
Br
o
m
o
m
e
t
h
a
n
e
Ch
l
o
r
o
m
e
t
h
a
n
e
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
m,
p
-
X
y
l
e
n
e
s
o-
X
y
l
e
n
e
6,000 10*3 5 0.7 500 500
100 10 1 1 1 5 5
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-25D 14-Mar-11
MW-25D 19-Oct-11
MW-25D 11-Apr-12
MW-25D 26-Oct-12
MW-25D 11-Apr-13
MW-25D 2-Oct-13
MW-25D 4-Apr-14
MW-25D 12-Nov-14
MW-25D 9-Apr-15 0.52J
MW-25D 14-May-15 5.7J
MW-25D 8-Oct-15
MW-25D 24-Mar-16
MW-25D 31-Aug-16
MW-26 15-Mar-11
MW-26 20-Oct-11
MW-26 11-Apr-12
MW-26 25-Oct-12
MW-26 (dup)25-Oct-12
MW-26 11-Apr-13
MW-26 2-Oct-13
MW-26 4-Apr-14
MW-26 12-Nov-14
MW-26 8-Apr-15 10J
MW-26 8-Oct-15 0.21JB
MW-26 25-Mar-16 0.26J
MW-26 1-Sep-16
Notes:
1. All units are in micrograms per liter (parts per billion).
2. dup - Duplicate Sample
4. J - Indicates the analytical result is an estimated concentration between the method detection limit and
the Solid Waste Section Reporting Limit.
5. B - The analyte concentration detected in the method blank was greater than the method detection limit.
6. Additional samples were collected from MW-12D, -15D, -17D, and -25D in May 2015 to confirm the
April 2015 detections of tetrachloroethene.
- Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard.
- Indicates the result is below the detection limit.
3. * - Groundwater Protection Standard
Page 12 of 13 December 2016
Ta
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0
8
J
0.0
0
1
6
7
J
0.
0
0
0
2
4
5
J
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0
1
6
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0.00645J
SW
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5
19
-
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1
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0
3
3
3
J
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0
0
1
2
5
J
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6
7
J
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0
1
9
8
J
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0
0
5
0
7
J
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SW
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5
11
-
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-
1
2
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0
3
6
3
J
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0
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6
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J
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SW
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5
25
-
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J
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0
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4
J
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5
11
-
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3
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3
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J
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0
0
0
5
J
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0
0
4
J
B
0.0
0
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J
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0
0
0
9
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0.003J
SW
-
5
1-
O
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-
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3
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4
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J
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0
0
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9
J
B
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J
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-
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4-
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-
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4
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3
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1
J
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0
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2
J
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0
0
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7
J
0.
0
0
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J
0.005JB
SW
-
5
13
-
N
o
v
-
1
4
0.0
4
0
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0.0
0
0
6
J
0.0
0
0
5
J
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0
0
0
7
J
0.
0
0
0
6
J
0.003J
SW
-
5
9-
A
p
r
-
1
5
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3
0
J
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0
0
2
J
0.0
0
0
8
J
0.0
0
3
J
0.
0
0
0
8
J
0.0
0
1
J
0.
0
0
4
J
0.010JB 16J
SW
-
5
8-
O
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t
-
1
5
0.0
4
0
J
0.0
0
0
8
J
0.0
0
0
4
J
0.0
0
1
J
0.0
0
0
3
J
0.
0
0
0
5
J
0.0
0
1
J
B
0.003J
SW
-
5
25
-
M
a
r
-
1
6
0.0
3
5
J
0.
0
0
0
0
9
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0.0
0
1
9
J
0.0
0
1
3
J
0.
0
0
3
7
J
0.
0
0
1
5
4
J
0.
0
0
1
3
J
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0.0
0
0
1
J
0.
0
0
8
J
0.0098J
SW
-
5
1-
S
e
p
-
1
6

0.0
2
9
J

0.0
0
0
5
5
J

0.0
0
2
6
J
0.0031J
SW
-
6
15
-
M
a
r
-
1
1
0.
0
3
9
1
J
0.
0
0
1
8
8
J
0.00447J
SW
-
6
19
-
O
c
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-
1
1
0.0
0
4
4
1
J
0.
0
2
3
1
J
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0
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1
6
7
J
0.0
0
3
7
8
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0
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5
8
9
J
0.00798J
SW
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6
11
-
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p
r
-
1
2
0.
0
4
0
4
J
SW
-
6
25
-
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2
0.0
0
4
7
4
J
0.
0
4
2
5
J
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0
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2
5
3
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0.
0
0
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4
4
J
0.00508J
SW
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6
11
-
A
p
r
-
1
3
0.
0
4
J
0.
0
0
0
4
J
B
0.0
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0
4
J
B
0.
0
0
0
5
J
0.002J
SW
-
6
2-
O
c
t
-
1
3
0.0
5
0
J
0.
0
0
0
0
9
J
B
0.0
0
1
J
B
0.0
0
2
J
0.0
0
2
J
0.0
0
0
4
J
0.0
0
1
J
0.
0
0
6
J
0.004JB
SW
-
6
4-
A
p
r
-
1
4
0.0
3
0
J
0.0
0
0
3
J
0.0
0
0
4
J
0.0
0
1
J
0.
0
0
3
J
0.006JB
SW
-
6
13
-
N
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v
-
1
4
0.0
5
0
J
0.0
0
0
8
J
0.0
0
3
J
0.0
0
1
J
0.
0
0
0
8
J
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SW
-
6
8-
A
p
r
-
1
5
0.0
3
0
J
0.0
0
0
4
J
0.0
0
0
3
J
0.0
0
2
J
0.
0
0
0
5
J
0.003J 0.37JB
SW
-
6
8-
O
c
t
-
1
5
0.0
4
0
J
0.0
0
0
6
J
0.0
0
0
4
J
0.
0
0
0
5
J
0.003J 0.30JB
SW
-
6
25
-
M
a
r
-
1
6
0.0
3
1
J
0.0
0
0
2
J
0.0
0
0
7
J
0.
0
0
1
6
J
0.0
0
0
1
2
J
0.
0
0
0
8
J
B
0.
0
0
1
J
0.0032J
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-
6
1-
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6

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4
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0.
0
0
0
5
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J
0.0
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9
7
J

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0
9
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J
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December 2016
Table 5
Constituents Detected Above the Standards
September 2016 Semi-Annual Sampling Event
North Wake Lined Landfill - Permit Number 9209-MSWLF-1996
SEPTEMBER 2016 CONSTITUENTS EXCEEDING THE
NORTH CAROLINA 2L or GROUNDWATER PROTECTION STANDARDS
MW-11 (background well)Cobalt*, Vanadium*
MW-11D (background well)Vanadium*
MW-12 Cobalt*, Thallium*, Vanadium*
MW-12D Vanadium*
MW-13 Cobalt*, Thallium*, Vanadium*
MW-14 Cobalt*, Vanadium*
MW-15 Cobalt*, Vanadium*
MW-15D Vanadium*
MW-16 Cobalt*, Vanadium*
MW-17 Vanadium*
MW-17D Vanadium*
MW-18 Chromium, Cobalt*, Vanadium*
MW-19 Vanadium*
MW-20 Chromium, Cobalt*, Vanadium*
MW-21 Cobalt*, Thallium*, Vanadium*
MW-25 Cobalt*, Vanadium*
MW-25D Cobalt*, Vanadium*
MW-26 Cobalt*, Vanadium*
Notes:
1. * - Groundwater Protection Standard
MONITORING WELL CODE
2. Bold - Indicates a "J" flag detection in which the analytical result is an estimated concentration between the laboratory
method detection limit and the Solid Waste Section Limit.
Page 1 of 1 December 2016
Figure 1: Potentiometric Surface Map
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GW Elev.244.51GW Elev.228.73GW Elev.221.91 GW Elev.220.51 GW Elev.233.12 GW Elev.243.07 GW Elev. 242.19 GW Elev.263.94 LEGEND Groundwater Monitoring Well Potentiometric Contour (dashed where inferred)
No
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s site investigations.Surface Water Sample Location
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3
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2 9 5
29 0
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285
2 8 0
275
270
265
260
2 55
25 0
2 4 5
2 4 0
2 3 5230225220 2 2 0 2 2 5 2 3 0 2 3 5 2 4 0 2 4 5 2 5 025 5 2 6 0 2 6 5 2 7 0
2 7 5
2 8 0
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2 7 0 Contour Interval - 5 Feet
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Appendix A
Analytical Data
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
CDM Smith
5400 Glenwood Avenue
Suite 400
Raleigh, NC 27612
Attention: Mathew Colone
RI02010Lot Number:
North Wake Lined LandfillProject Name:
09/13/2016Date Completed:
Catherine S. Dover
Project Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
CDM Smith
Lot Number: RI02010
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: North Wake Lined Landfill
Project Number:
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Metals 6020A
Sample RI02010-001 (MW-12) was diluted due to matrix and resulted in non-detect results and an elevated PQL.
VOC 8260B
For TRIP BLANK2 (RI02010-023) & TRIP BLANK3 (RI02010-024), the original calibration did not pass for trans-1,4-Dichloro-2-butene so the analyst
recalibrated and re-analyzed this trip blank for this one compound. The re-analysis for these two trip blank samples was done a few hours outside
the 7 day holding time, but all of the other compounds were reported from the analysis that was analyzed within the 7 day holding time.
Page: 2 of 119
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Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
CDM Smith
Lot Number: RI02010

Project Name: North Wake Lined Landfill
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 09/01/2016 1130MW-12 Aqueous 09/02/2016
002 09/01/2016 1155MW-12d Aqueous 09/02/2016
003 09/01/2016 1055MW-13 Aqueous 09/02/2016
004 09/01/2016 1040MW-14 Aqueous 09/02/2016
005 09/01/2016 0950MW-15 Aqueous 09/02/2016
006 09/01/2016 0930MW-15d Aqueous 09/02/2016
007 09/01/2016 0900MW-16 Aqueous 09/02/2016
008 09/01/2016 0815MW-17 Aqueous 09/02/2016
009 09/01/2016 0830MW-17d Aqueous 09/02/2016
010 09/01/2016 0755MW-18 Aqueous 09/02/2016
011 09/01/2016 1210MW-19 Aqueous 09/02/2016
012 09/01/2016 1220MW-20 Aqueous 09/02/2016
013 09/01/2016 1255MW-21 Aqueous 09/02/2016
014 09/01/2016 1310MW-25 Aqueous 09/02/2016
015 08/31/2016 1105MW-25d Aqueous 09/02/2016
016 09/01/2016 1230MW-26 Aqueous 09/02/2016
017 09/01/2016 1405EQ BLANK Aqueous 09/02/2016
018 09/01/2016 0800DUPAqueous 09/02/2016
019 09/01/2016TRIP BLANK 1 Aqueous 09/02/2016
020 09/01/2016 1110SW-4 Aqueous 09/02/2016
021 09/01/2016 0850SW-5 Aqueous 09/02/2016
022 09/01/2016 1245SW-6 Aqueous 09/02/2016
023 09/01/2016TRIP BLANK 2 Aqueous 09/02/2016
024 09/01/2016TRIP BLANK 3 Aqueous 09/02/2016
(24 samples)
Page: 3 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
RI02010-001
09/01/2016 1130
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1254 TML 21348
2 5030B 8260B 1 09/07/2016 1153 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 4 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
RI02010-001
09/01/2016 1130
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1254 TML 21348
2 5030B 8260B 1 09/07/2016 1153 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 100 70-130 97 70-130
1,2-Dichloroethane-d4 102 70-130 87 70-130
Toluene-d8 105 70-130 96 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 5 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
RI02010-001
09/01/2016 1130
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2206 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 0.24 J 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 30 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 0.068 J 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 4.2 J 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.62 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 17 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 1.0 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 5.0 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 6 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
RI02010-001
09/01/2016 1130
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2138 BNW 09/06/2016 1606 21343
2 3005A 6020A 5 09/08/2016 1128 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.25 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 50 U 2ug/L1.350
Barium 7440-39-3 6020A 520 1ug/L0.53100
Beryllium 7440-41-7 6020A 2.1 1ug/L0.121.0
Cadmium 7440-43-9 6020A 5.0 U 2ug/L0.225.0
Chromium 7440-47-3 6020A 22 JD 2ug/L3.250
Cobalt 7440-48-4 6020A 18 JD 2ug/L1.350
Copper 7440-50-8 6020A 84 B 1ug/L0.1510
Lead 7439-92-1 6020A 12 1ug/L0.1510
Nickel 7440-02-0 6020A 12 JD 2ug/L3.1250
Selenium 7782-49-2 6020A 1.5 J 1ug/L0.9510
Silver 7440-22-4 6020A 0.18 J 1ug/L0.1710
Thallium 7440-28-0 6020A 0.62 J 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 100 JD 2ug/L5.1130
Zinc 7440-66-6 6020A 100 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 7 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12d
RI02010-002
09/01/2016 1155
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1318 TML 21348
2 5030B 8260B 1 09/07/2016 1216 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 8 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12d
RI02010-002
09/01/2016 1155
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1318 TML 21348
2 5030B 8260B 1 09/07/2016 1216 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 96 70-130 100 70-130
1,2-Dichloroethane-d4 103 70-130 87 70-130
Toluene-d8 100 70-130 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 9 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12d
RI02010-002
09/01/2016 1155
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2217 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 26 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 0.070 J 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 1.0 J 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.81 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 0.94 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 2.5 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 3.2 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 10 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12d
RI02010-002
09/01/2016 1155
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2211 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 25 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.054 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Cobalt 7440-48-4 6020A 0.52 J 1ug/L0.2610
Copper 7440-50-8 6020A 8.2 BJ 1ug/L0.1510
Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Nickel 7440-02-0 6020A 50 U 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 2.3 J 1ug/L1.025
Zinc 7440-66-6 6020A 3.5 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 11 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
RI02010-003
09/01/2016 1055
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1342 TML 21348
2 5030B 8260B 1 09/07/2016 1239 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 12 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
RI02010-003
09/01/2016 1055
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1342 TML 21348
2 5030B 8260B 1 09/07/2016 1239 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 98 70-130 98 70-130
1,2-Dichloroethane-d4 101 70-130 86 70-130
Toluene-d8 102 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 13 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
RI02010-003
09/01/2016 1055
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2240 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 23 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 1.1 J 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.30 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 0.80 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 4.2 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 3.4 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 14 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
RI02010-003
09/01/2016 1055
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2234 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.20 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 170 1ug/L0.53100
Beryllium 7440-41-7 6020A 0.66 J 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.059 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 32 1ug/L0.6310
Cobalt 7440-48-4 6020A 10 1ug/L0.2610
Copper 7440-50-8 6020A 2.9 BJ 1ug/L0.1510
Lead 7439-92-1 6020A 4.1 J 1ug/L0.1510
Nickel 7440-02-0 6020A 15 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 0.17 J 1ug/L0.1710
Thallium 7440-28-0 6020A 0.28 J 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 42 1ug/L1.025
Zinc 7440-66-6 6020A 54 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 15 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
RI02010-004
09/01/2016 1040
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1405 TML 21348
2 5030B 8260B 1 09/07/2016 1302 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 16 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
RI02010-004
09/01/2016 1040
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1405 TML 21348
2 5030B 8260B 1 09/07/2016 1302 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 100 70-130
1,2-Dichloroethane-d4 102 70-130 87 70-130
Toluene-d8 102 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 17 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
RI02010-004
09/01/2016 1040
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2251 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 16 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 1.3 J 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.30 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 0.91 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 5.0 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 3.1 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 18 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
RI02010-004
09/01/2016 1040
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2245 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 60 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 0.28 J 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.045 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 6.9 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 4.8 J 1ug/L0.2610
Copper 7440-50-8 6020A 11 B 1ug/L0.1510
Lead 7439-92-1 6020A 2.5 J 1ug/L0.1510
Nickel 7440-02-0 6020A 6.4 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 0.21 J 1ug/L0.1710
Thallium 7440-28-0 6020A 0.075 J 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 18 J 1ug/L1.025
Zinc 7440-66-6 6020A 17 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 19 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15
RI02010-005
09/01/2016 0950
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1428 TML 21348
2 5030B 8260B 1 09/07/2016 1324 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 20 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15
RI02010-005
09/01/2016 0950
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1428 TML 21348
2 5030B 8260B 1 09/07/2016 1324 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 96 70-130 97 70-130
1,2-Dichloroethane-d4 101 70-130 84 70-130
Toluene-d8 101 70-130 95 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 21 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15
RI02010-005
09/01/2016 0950
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2302 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 41 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 1.5 J 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.44 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 5.9 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 25 U 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 8.8 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 22 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15
RI02010-005
09/01/2016 0950
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2256 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 77 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.11 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 6.9 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 3.8 J 1ug/L0.2610
Copper 7440-50-8 6020A 12 B 1ug/L0.1510
Lead 7439-92-1 6020A 0.89 J 1ug/L0.1510
Nickel 7440-02-0 6020A 4.2 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 19 J 1ug/L1.025
Zinc 7440-66-6 6020A 13 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 23 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15d
RI02010-006
09/01/2016 0930
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1452 TML 21348
2 5030B 8260B 1 09/07/2016 1347 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 24 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15d
RI02010-006
09/01/2016 0930
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1452 TML 21348
2 5030B 8260B 1 09/07/2016 1347 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 96 70-130 97 70-130
1,2-Dichloroethane-d4 102 70-130 85 70-130
Toluene-d8 102 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 25 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15d
RI02010-006
09/01/2016 0930
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2313 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 72 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 1.0 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 1.9 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 3.9 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 10 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 26 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15d
RI02010-006
09/01/2016 0930
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2308 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.27 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 66 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.061 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Copper 7440-50-8 6020A 1.2 BJ 1ug/L0.1510
Lead 7439-92-1 6020A 0.16 J 1ug/L0.1510
Nickel 7440-02-0 6020A 1.1 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 3.6 J 1ug/L1.025
Zinc 7440-66-6 6020A 5.9 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 27 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-16
RI02010-007
09/01/2016 0900
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1515 TML 21348
2 5030B 8260B 1 09/07/2016 1410 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 28 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-16
RI02010-007
09/01/2016 0900
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1515 TML 21348
2 5030B 8260B 1 09/07/2016 1410 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 98 70-130 98 70-130
1,2-Dichloroethane-d4 102 70-130 86 70-130
Toluene-d8 101 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 29 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-16
RI02010-007
09/01/2016 0900
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2325 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 0.18 J 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 93 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 0.063 J 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 2.5 J 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 1.8 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 3.3 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 1.3 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 29 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 30 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-16
RI02010-007
09/01/2016 0900
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2319 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.20 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 0.28 J 1ug/L0.2610
Barium 7440-39-3 6020A 99 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.13 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 1.5 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 3.3 J 1ug/L0.2610
Copper 7440-50-8 6020A 7.1 BJ 1ug/L0.1510
Lead 7439-92-1 6020A 1.0 J 1ug/L0.1510
Nickel 7440-02-0 6020A 3.7 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 0.082 J 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 4.9 J 1ug/L1.025
Zinc 7440-66-6 6020A 23 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 31 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17
RI02010-008
09/01/2016 0815
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1538 TML 21348
2 5030B 8260B 1 09/07/2016 1433 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 32 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17
RI02010-008
09/01/2016 0815
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1538 TML 21348
2 5030B 8260B 1 09/07/2016 1433 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 99 70-130 95 70-130
1,2-Dichloroethane-d4 101 70-130 84 70-130
Toluene-d8 103 70-130 96 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 33 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17
RI02010-008
09/01/2016 0815
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2347 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 17 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 0.067 J 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.53 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 1.2 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 1.4 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 4.1 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 34 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17
RI02010-008
09/01/2016 0815
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2342 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.18 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 18 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 0.18 J 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.11 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 1.5 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 0.34 J 1ug/L0.2610
Copper 7440-50-8 6020A 0.83 BJ 1ug/L0.1510
Lead 7439-92-1 6020A 0.47 J 1ug/L0.1510
Nickel 7440-02-0 6020A 0.73 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 3.3 J 1ug/L1.025
Zinc 7440-66-6 6020A 3.5 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 35 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17d
RI02010-009
09/01/2016 0830
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1601 TML 21348
2 5030B 8260B 1 09/07/2016 1456 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 36 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17d
RI02010-009
09/01/2016 0830
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1601 TML 21348
2 5030B 8260B 1 09/07/2016 1456 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 96 70-130 94 70-130
1,2-Dichloroethane-d4 102 70-130 86 70-130
Toluene-d8 102 70-130 94 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 37 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17d
RI02010-009
09/01/2016 0830
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2358 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 0.47 J 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 15 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 0.15 J 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 0.85 J 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 1.7 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 1.4 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 3.6 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 12 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 38 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17d
RI02010-009
09/01/2016 0830
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/07/2016 2353 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.39 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 34 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.084 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 1.5 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Copper 7440-50-8 6020A 1.9 BJ 1ug/L0.1510
Lead 7439-92-1 6020A 0.31 J 1ug/L0.1510
Nickel 7440-02-0 6020A 1.1 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 4.2 J 1ug/L1.025
Zinc 7440-66-6 6020A 7.9 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 39 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-18
RI02010-010
09/01/2016 0755
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1624 TML 21348
2 5030B 8260B 1 09/07/2016 1519 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 40 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-18
RI02010-010
09/01/2016 0755
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1624 TML 21348
2 5030B 8260B 1 09/07/2016 1519 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 98 70-130
1,2-Dichloroethane-d4 103 70-130 86 70-130
Toluene-d8 100 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 41 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-18
RI02010-010
09/01/2016 0755
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 0010 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 14 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.24 BJ 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 0.83 J 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 0.96 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 2.2 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 2.5 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 42 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-18
RI02010-010
09/01/2016 0755
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 0004 BNW 09/06/2016 1606 21343
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 39 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 0.13 J 1ug/L0.121.0
Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Chromium 7440-47-3 6020A 10 1ug/L0.6310
Cobalt 7440-48-4 6020A 3.6 J 1ug/L0.2610
Copper 7440-50-8 6020A 11 B 1ug/L0.1510
Lead 7439-92-1 6020A 0.64 J 1ug/L0.1510
Nickel 7440-02-0 6020A 5.1 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 10 J 1ug/L1.025
Zinc 7440-66-6 6020A 13 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 43 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
RI02010-011
09/01/2016 1210
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1648 TML 21348
2 5030B 8260B 1 09/07/2016 1541 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 44 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
RI02010-011
09/01/2016 1210
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1648 TML 21348
2 5030B 8260B 1 09/07/2016 1541 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 96 70-130 102 70-130
1,2-Dichloroethane-d4 103 70-130 88 70-130
Toluene-d8 101 70-130 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 45 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
RI02010-011
09/01/2016 1210
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 0930 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 0.18 J 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 13 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 0.11 J 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 2.7 J 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.47 J 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 1.6 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 2.8 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 4.9 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 46 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
RI02010-011
09/01/2016 1210
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 0925 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.37 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 13 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.14 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 2.9 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Copper 7440-50-8 6020A 1.1 J 1ug/L0.1510
Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Nickel 7440-02-0 6020A 1.3 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 3.0 J 1ug/L1.025
Zinc 7440-66-6 6020A 5.8 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 47 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-20
RI02010-012
09/01/2016 1220
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1711 TML 21348
2 5030B 8260B 1 09/07/2016 1604 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 48 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-20
RI02010-012
09/01/2016 1220
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1711 TML 21348
2 5030B 8260B 1 09/07/2016 1604 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 100 70-130 96 70-130
1,2-Dichloroethane-d4 107 70-130 85 70-130
Toluene-d8 105 70-130 96 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 49 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-20
RI02010-012
09/01/2016 1220
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 0953 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 0.26 J 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 15 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 0.061 J 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 1.7 J 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.58 J 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 1.1 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 7.3 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 3.2 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 50 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-20
RI02010-012
09/01/2016 1220
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 0936 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.18 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 130 1ug/L0.53100
Beryllium 7440-41-7 6020A 0.33 J 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.078 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 14 1ug/L0.6310
Cobalt 7440-48-4 6020A 18 1ug/L0.2610
Copper 7440-50-8 6020A 130 1ug/L0.1510
Lead 7439-92-1 6020A 9.7 J 1ug/L0.1510
Nickel 7440-02-0 6020A 20 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 0.16 J 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 41 1ug/L1.025
Zinc 7440-66-6 6020A 68 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 51 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-21
RI02010-013
09/01/2016 1255
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1734 TML 21348
2 5030B 8260B 1 09/07/2016 1627 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 52 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-21
RI02010-013
09/01/2016 1255
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1734 TML 21348
2 5030B 8260B 1 09/07/2016 1627 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 99 70-130
1,2-Dichloroethane-d4 103 70-130 87 70-130
Toluene-d8 101 70-130 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 53 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-21
RI02010-013
09/01/2016 1255
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1004 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 34 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 1.2 J 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.28 J 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 2.4 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 3.5 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 4.6 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 54 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-21
RI02010-013
09/01/2016 1255
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 0958 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.20 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 310 1ug/L0.53100
Beryllium 7440-41-7 6020A 0.60 J 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.11 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 7.2 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 12 1ug/L0.2610
Copper 7440-50-8 6020A 68 1ug/L0.1510
Lead 7439-92-1 6020A 3.8 J 1ug/L0.1510
Nickel 7440-02-0 6020A 4.7 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 0.22 J 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 45 1ug/L1.025
Zinc 7440-66-6 6020A 58 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 55 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25
RI02010-014
09/01/2016 1310
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1757 TML 21348
2 5030B 8260B 1 09/07/2016 1651 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 56 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25
RI02010-014
09/01/2016 1310
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1757 TML 21348
2 5030B 8260B 1 09/07/2016 1651 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 97 70-130
1,2-Dichloroethane-d4 105 70-130 86 70-130
Toluene-d8 102 70-130 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 57 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25
RI02010-014
09/01/2016 1310
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1015 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 57 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 0.69 J 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.31 J 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 2.8 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 1.0 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 4.3 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 58 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25
RI02010-014
09/01/2016 1310
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1010 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 0.32 J 1ug/L0.2610
Barium 7440-39-3 6020A 87 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 0.16 J 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.089 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 5.1 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 3.4 J 1ug/L0.2610
Copper 7440-50-8 6020A 2.3 J 1ug/L0.1510
Lead 7439-92-1 6020A 0.64 J 1ug/L0.1510
Nickel 7440-02-0 6020A 3.2 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 5.4 J 1ug/L1.025
Zinc 7440-66-6 6020A 11 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 59 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25d
RI02010-015
08/31/2016 1105
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1821 TML 21348
2 5030B 8260B 1 09/07/2016 1043 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 60 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25d
RI02010-015
08/31/2016 1105
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1821 TML 21348
2 5030B 8260B 1 09/07/2016 1043 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 98 70-130 99 70-130
1,2-Dichloroethane-d4 104 70-130 87 70-130
Toluene-d8 103 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 61 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25d
RI02010-015
08/31/2016 1105
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1026 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 31 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 1.7 J 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 2.1 J 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 1.5 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 3.8 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 9.3 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 62 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25d
RI02010-015
08/31/2016 1105
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1021 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.22 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 45 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 0.13 J 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.098 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 3.9 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 1.9 J 1ug/L0.2610
Copper 7440-50-8 6020A 10 1ug/L0.1510
Lead 7439-92-1 6020A 0.37 J 1ug/L0.1510
Nickel 7440-02-0 6020A 3.5 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 7.6 J 1ug/L1.025
Zinc 7440-66-6 6020A 9.7 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 63 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-26
RI02010-016
09/01/2016 1230
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1844 TML 21348
2 5030B 8260B 1 09/07/2016 1714 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 64 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-26
RI02010-016
09/01/2016 1230
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1844 TML 21348
2 5030B 8260B 1 09/07/2016 1714 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 97 70-130
1,2-Dichloroethane-d4 103 70-130 86 70-130
Toluene-d8 102 70-130 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 65 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-26
RI02010-016
09/01/2016 1230
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1038 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 31 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 7.8 J 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 0.50 J 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 3.8 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 25 U 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 6.3 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 66 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-26
RI02010-016
09/01/2016 1230
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1032 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 74 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 0.18 J 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.21 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 6.0 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 14 1ug/L0.2610
Copper 7440-50-8 6020A 51 1ug/L0.1510
Lead 7439-92-1 6020A 0.95 J 1ug/L0.1510
Nickel 7440-02-0 6020A 13 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 18 J 1ug/L1.025
Zinc 7440-66-6 6020A 18 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 67 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
RI02010-017
09/01/2016 1405
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1143 TML 21348
2 5030B 8260B 1 09/07/2016 1107 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 5.0 J 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 6.4 J 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 68 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
RI02010-017
09/01/2016 1405
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 1143 TML 21348
2 5030B 8260B 1 09/07/2016 1107 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 96 70-130 103 70-130
1,2-Dichloroethane-d4 98 70-130 88 70-130
Toluene-d8 101 70-130 101 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 69 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
RI02010-017
09/01/2016 1405
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1043 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 100 U 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Copper 7440-50-8 6020A 0.22 J 1ug/L0.1510
Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Nickel 7440-02-0 6020A 50 U 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 25 U 1ug/L1.025
Zinc 7440-66-6 6020A 2.2 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 70 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
RI02010-018
09/01/2016 0800
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 2243 ECP 21411
2 5030B 8260B 1 09/07/2016 1737 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 71 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
RI02010-018
09/01/2016 0800
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 2243 ECP 21411
2 5030B 8260B 1 09/07/2016 1737 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 97 70-130
1,2-Dichloroethane-d4 103 70-130 84 70-130
Toluene-d8 104 70-130 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 72 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
RI02010-018
09/01/2016 0800
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1106 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 0.52 J 1ug/L0.176.0
Dissolved Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Dissolved Barium 7440-39-3 6020A 14 J 1ug/L0.53100
Dissolved Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Dissolved Cadmium 7440-43-9 6020A 0.15 J 1ug/L0.0441.0
Dissolved Chromium 7440-47-3 6020A 1.0 J 1ug/L0.6310
Dissolved Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Dissolved Copper 7440-50-8 6020A 1.7 J 1ug/L0.1510
Dissolved Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Dissolved Nickel 7440-02-0 6020A 0.91 J 1ug/L0.6350
Dissolved Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Dissolved Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Dissolved Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Dissolved Vanadium 7440-62-2 6020A 3.8 J 1ug/L1.025
Dissolved Zinc 7440-66-6 6020A 7.1 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 73 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
RI02010-018
09/01/2016 0800
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1100 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.46 J 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 36 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 0.056 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 1.8 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Copper 7440-50-8 6020A 1.7 J 1ug/L0.1510
Lead 7439-92-1 6020A 0.37 J 1ug/L0.1510
Nickel 7440-02-0 6020A 0.93 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 4.3 J 1ug/L1.025
Zinc 7440-66-6 6020A 7.7 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 74 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK 1
RI02010-019
09/01/2016
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0017 ECP 21411
2 5030B 8260B 1 09/07/2016 1130 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 75 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK 1
RI02010-019
09/01/2016
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0017 ECP 21411
2 5030B 8260B 1 09/07/2016 1130 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 96 70-130 101 70-130
1,2-Dichloroethane-d4 102 70-130 88 70-130
Toluene-d8 101 70-130 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 76 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-4
RI02010-020
09/01/2016 1110
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 2306 ECP 21411
2 5030B 8260B 1 09/07/2016 1800 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 77 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-4
RI02010-020
09/01/2016 1110
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 2306 ECP 21411
2 5030B 8260B 1 09/07/2016 1800 TML 21441
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 94 70-130 100 70-130
1,2-Dichloroethane-d4 105 70-130 88 70-130
Toluene-d8 103 70-130 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 78 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-4
RI02010-020
09/01/2016 1110
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1111 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 41 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Cobalt 7440-48-4 6020A 1.3 J 1ug/L0.2610
Copper 7440-50-8 6020A 1.0 J 1ug/L0.1510
Lead 7439-92-1 6020A 0.26 J 1ug/L0.1510
Nickel 7440-02-0 6020A 50 U 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 2.8 J 1ug/L1.025
Zinc 7440-66-6 6020A 4.1 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 79 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-5
RI02010-021
09/01/2016 0850
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 2330 ECP 21411
2 5030B 8260B 1 09/08/2016 0110 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 80 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-5
RI02010-021
09/01/2016 0850
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 2330 ECP 21411
2 5030B 8260B 1 09/08/2016 0110 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 95 70-130 97 70-130
1,2-Dichloroethane-d4 104 70-130 86 70-130
Toluene-d8 101 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 81 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-5
RI02010-021
09/01/2016 0850
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1117 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 29 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Cobalt 7440-48-4 6020A 10 U 1ug/L0.2610
Copper 7440-50-8 6020A 0.55 J 1ug/L0.1510
Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Nickel 7440-02-0 6020A 50 U 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 2.6 J 1ug/L1.025
Zinc 7440-66-6 6020A 3.1 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 82 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-6
RI02010-022
09/01/2016 1245
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 2353 ECP 21411
2 5030B 8260B 1 09/08/2016 0132 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 83 of 119
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-6
RI02010-022
09/01/2016 1245
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/06/2016 2353 ECP 21411
2 5030B 8260B 1 09/08/2016 0132 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 96 70-130
1,2-Dichloroethane-d4 105 70-130 86 70-130
Toluene-d8 101 70-130 96 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 84 of 119
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ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-6
RI02010-022
09/01/2016 1245
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1122 BNW 09/06/2016 1606 21370
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 6.0 U 1ug/L0.176.0
Arsenic 7440-38-2 6020A 0.37 J 1ug/L0.2610
Barium 7440-39-3 6020A 48 J 1ug/L0.53100
Beryllium 7440-41-7 6020A 1.0 U 1ug/L0.121.0
Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Chromium 7440-47-3 6020A 1.4 J 1ug/L0.6310
Cobalt 7440-48-4 6020A 4.4 J 1ug/L0.2610
Copper 7440-50-8 6020A 1.7 J 1ug/L0.1510
Lead 7439-92-1 6020A 0.54 J 1ug/L0.1510
Nickel 7440-02-0 6020A 0.97 J 1ug/L0.6350
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
Thallium 7440-28-0 6020A 5.5 U 1ug/L0.0755.5
Vanadium 7440-62-2 6020A 9.5 J 1ug/L1.025
Zinc 7440-66-6 6020A 9.7 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 85 of 119
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK 2
RI02010-023
09/01/2016
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0041 ECP 21411
2 5030B 8260B 1 09/08/2016 0154 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 UH 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 86 of 119
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK 2
RI02010-023
09/01/2016
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0041 ECP 21411
2 5030B 8260B 1 09/08/2016 0154 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 95 70-130 H 98 70-130
1,2-Dichloroethane-d4 100 70-130 H 87 70-130
Toluene-d8 99 70-130 H 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 87 of 119
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK 3
RI02010-024
09/01/2016
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0105 ECP 21411
2 5030B 8260B 1 09/08/2016 0217 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 UH 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 88 of 119
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK 3
RI02010-024
09/01/2016
09/02/2016
Aqueous
Project Name: North Wake Lined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0105 ECP 21411
2 5030B 8260B 1 09/08/2016 0217 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 H 101 70-130
1,2-Dichloroethane-d4 105 70-130 H 90 70-130
Toluene-d8 102 70-130 H 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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QC Summary
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21348-001
21348 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 10 09/06/2016 1043U102.0 ug/L1
Acrylonitrile 5.0 09/06/2016 1043U5.0 0.80 ug/L1
Benzene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Bromochloromethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Bromodichloromethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Bromoform 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Bromomethane (Methyl bromide)0.50 09/06/2016 1043U0.50 0.40 ug/L1
2-Butanone (MEK)10 09/06/2016 1043U102.0 ug/L1
Carbon disulfide 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Carbon tetrachloride 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Chlorobenzene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Chloroethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Chloroform 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Chloromethane (Methyl chloride)0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)0.50 09/06/2016 1043U0.50 0.40 ug/L1
Dibromochloromethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,2-Dibromoethane (EDB)0.50 09/06/2016 1043U0.50 0.40 ug/L1
Dibromomethane (Methylene bromide)0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,4-Dichlorobenzene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,2-Dichlorobenzene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,2-Dichloroethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,1-Dichloroethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
cis-1,2-Dichloroethene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,1-Dichloroethene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
trans-1,2-Dichloroethene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,2-Dichloropropane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
cis-1,3-Dichloropropene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
trans-1,3-Dichloropropene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Ethylbenzene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
2-Hexanone 10 09/06/2016 1043U102.0 ug/L1
Methyl iodide (Iodomethane)5.0 09/06/2016 1043U5.0 0.40 ug/L1
4-Methyl-2-pentanone 10 09/06/2016 1043U102.0 ug/L1
Methylene chloride 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Styrene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,1,1,2-Tetrachloroethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Tetrachloroethene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Toluene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,1,2-Trichloroethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,1,1-Trichloroethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Trichloroethene 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Trichlorofluoromethane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
1,2,3-Trichloropropane 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Vinyl acetate 5.0 09/06/2016 1043U5.0 1.2 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 91 of 119
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21348-001
21348 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Vinyl chloride 0.50 09/06/2016 1043U0.50 0.40 ug/L1
Xylenes (total)1.0 09/06/2016 1043U1.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21348-002
21348 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 92 09/06/2016 09429210060-1401
Acrylonitrile 89 09/06/2016 09428910060-1401
Benzene 45 09/06/2016 0942905070-1301
Bromochloromethane 47 09/06/2016 0942935070-1301
Bromodichloromethane 48 09/06/2016 0942975070-1301
Bromoform 46 09/06/2016 0942925070-1301
Bromomethane (Methyl bromide)51 09/06/2016 09421035060-1401
2-Butanone (MEK)92 09/06/2016 09429210060-1401
Carbon disulfide 50 09/06/2016 09421005060-1401
Carbon tetrachloride 48 09/06/2016 0942965070-1301
Chlorobenzene 45 09/06/2016 0942905070-1301
Chloroethane 51 09/06/2016 09421025060-1401
Chloroform 44 09/06/2016 0942885070-1301
Chloromethane (Methyl chloride)46 09/06/2016 0942925050-1301
1,2-Dibromo-3-chloropropane (DBCP)46 09/06/2016 0942915070-1301
Dibromochloromethane 46 09/06/2016 0942935070-1301
1,2-Dibromoethane (EDB)45 09/06/2016 0942905070-1301
Dibromomethane (Methylene bromide)46 09/06/2016 0942925070-1301
1,4-Dichlorobenzene 44 09/06/2016 0942885070-1301
1,2-Dichlorobenzene 46 09/06/2016 0942925070-1301
1,2-Dichloroethane 45 09/06/2016 0942915070-1301
1,1-Dichloroethane 46 09/06/2016 0942935070-1301
cis-1,2-Dichloroethene 47 09/06/2016 0942935070-1301
1,1-Dichloroethene 48 09/06/2016 0942965070-1301
trans-1,2-Dichloroethene 48 09/06/2016 0942965070-1301
1,2-Dichloropropane 46 09/06/2016 0942935070-1301
cis-1,3-Dichloropropene 47 09/06/2016 0942945070-1301
trans-1,3-Dichloropropene 45 09/06/2016 0942915070-1301
Ethylbenzene 47 09/06/2016 0942935070-1301
2-Hexanone 91 09/06/2016 09429110060-1401
Methyl iodide (Iodomethane)48 09/06/2016 0942965070-1301
4-Methyl-2-pentanone 94 09/06/2016 09429410060-1401
Methylene chloride 44 09/06/2016 0942875070-1301
Styrene 48 09/06/2016 0942965070-1301
1,1,2,2-Tetrachloroethane 46 09/06/2016 0942915070-1301
1,1,1,2-Tetrachloroethane 47 09/06/2016 0942945070-1301
Tetrachloroethene 47 09/06/2016 0942935070-1301
Toluene 45 09/06/2016 0942905070-1301
1,1,2-Trichloroethane 46 09/06/2016 0942935070-1301
1,1,1-Trichloroethane 46 09/06/2016 0942925070-1301
Trichloroethene 47 09/06/2016 0942945070-1301
Trichlorofluoromethane 57 09/06/2016 09421145060-1401
1,2,3-Trichloropropane 45 09/06/2016 0942905070-1301
Vinyl acetate 51 09/06/2016 09421035060-1401
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 93 of 119
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21348-002
21348 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Vinyl chloride 47 09/06/2016 0942935060-1401
Xylenes (total)96 09/06/2016 09429610070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 94 of 119
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21411-001
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 10 09/06/2016 2159U102.0 ug/L1
Acrylonitrile 5.0 09/06/2016 2159U5.0 0.80 ug/L1
Benzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromochloromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromodichloromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromoform 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromomethane (Methyl bromide)0.50 09/06/2016 2159U0.50 0.40 ug/L1
2-Butanone (MEK)10 09/06/2016 2159U102.0 ug/L1
Carbon disulfide 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Carbon tetrachloride 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chlorobenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chloroform 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chloromethane (Methyl chloride)0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)0.50 09/06/2016 2159U0.50 0.40 ug/L1
Dibromochloromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dibromoethane (EDB)0.50 09/06/2016 2159U0.50 0.40 ug/L1
Dibromomethane (Methylene bromide)0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,4-Dichlorobenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dichlorobenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1-Dichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
cis-1,2-Dichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1-Dichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
trans-1,2-Dichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dichloropropane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
cis-1,3-Dichloropropene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
trans-1,3-Dichloropropene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Ethylbenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
2-Hexanone 10 09/06/2016 2159U102.0 ug/L1
Methyl iodide (Iodomethane)5.0 09/06/2016 2159U5.0 0.40 ug/L1
4-Methyl-2-pentanone 10 09/06/2016 2159U102.0 ug/L1
Methylene chloride 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Styrene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,1,2-Tetrachloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Tetrachloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Toluene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,2-Trichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,1-Trichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Trichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Trichlorofluoromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2,3-Trichloropropane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Vinyl acetate 5.0 09/06/2016 2159U5.0 1.2 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 95 of 119
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21411-001
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Vinyl chloride 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Xylenes (total)1.0 09/06/2016 2159U1.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 96 of 119
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21411-002
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 95 09/06/2016 20579510060-1401
Acrylonitrile 93 09/06/2016 20579310060-1401
Benzene 47 09/06/2016 2057935070-1301
Bromochloromethane 50 09/06/2016 20571005070-1301
Bromodichloromethane 49 09/06/2016 2057985070-1301
Bromoform 46 09/06/2016 2057925070-1301
Bromomethane (Methyl bromide)55 09/06/2016 20571115060-1401
2-Butanone (MEK)95 09/06/2016 20579510060-1401
Carbon disulfide 50 09/06/2016 20571005060-1401
Carbon tetrachloride 51 09/06/2016 20571025070-1301
Chlorobenzene 46 09/06/2016 2057925070-1301
Chloroethane 56 09/06/2016 20571135060-1401
Chloroform 47 09/06/2016 2057935070-1301
Chloromethane (Methyl chloride)51 09/06/2016 20571025050-1301
1,2-Dibromo-3-chloropropane (DBCP)46 09/06/2016 2057915070-1301
Dibromochloromethane 47 09/06/2016 2057945070-1301
1,2-Dibromoethane (EDB)45 09/06/2016 2057905070-1301
Dibromomethane (Methylene bromide)47 09/06/2016 2057945070-1301
1,4-Dichlorobenzene 44 09/06/2016 2057885070-1301
1,2-Dichlorobenzene 46 09/06/2016 2057925070-1301
1,2-Dichloroethane 47 09/06/2016 2057945070-1301
1,1-Dichloroethane 49 09/06/2016 2057985070-1301
cis-1,2-Dichloroethene 48 09/06/2016 2057975070-1301
1,1-Dichloroethene 50 09/06/2016 2057995070-1301
trans-1,2-Dichloroethene 51 09/06/2016 20571025070-1301
1,2-Dichloropropane 49 09/06/2016 2057975070-1301
cis-1,3-Dichloropropene 47 09/06/2016 2057945070-1301
trans-1,3-Dichloropropene 45 09/06/2016 2057895070-1301
Ethylbenzene 48 09/06/2016 2057965070-1301
2-Hexanone 96 09/06/2016 20579610060-1401
Methyl iodide (Iodomethane)49 09/06/2016 2057975070-1301
4-Methyl-2-pentanone 98 09/06/2016 20579810060-1401
Methylene chloride 45 09/06/2016 2057905070-1301
Styrene 49 09/06/2016 2057995070-1301
1,1,2,2-Tetrachloroethane 45 09/06/2016 2057915070-1301
1,1,1,2-Tetrachloroethane 48 09/06/2016 2057965070-1301
Tetrachloroethene 48 09/06/2016 2057965070-1301
Toluene 46 09/06/2016 2057925070-1301
1,1,2-Trichloroethane 46 09/06/2016 2057935070-1301
1,1,1-Trichloroethane 48 09/06/2016 2057965070-1301
Trichloroethene 49 09/06/2016 2057985070-1301
Trichlorofluoromethane 60 09/06/2016 20571195060-1401
1,2,3-Trichloropropane 46 09/06/2016 2057935070-1301
Vinyl acetate 51 09/06/2016 20571025060-1401
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 97 of 119
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21411-002
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Vinyl chloride 50 09/06/2016 20571015060-1401
Xylenes (total)97 09/06/2016 20579710070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 99 70-130
Toluene-d8 101 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 98 of 119
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Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:RQ21411-003
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Acetone 99 09/07/2016 06359910060-1404.5 201
Acrylonitrile 95 09/07/2016 06359510060-1402.0 401
Benzene 47 09/07/2016 0635945070-1301.3 201
Bromochloromethane 51 09/07/2016 06351025070-1301.8 201
Bromodichloromethane 50 09/07/2016 06351005070-1302.3 201
Bromoform 45 09/07/2016 0635905070-1302.3 201
Bromomethane (Methyl bromide)56 09/07/2016 06351135060-1402.0 201
2-Butanone (MEK)98 09/07/2016 06359810060-1403.5 201
Carbon disulfide 52 09/07/2016 06351045060-1404.3 201
Carbon tetrachloride 52 09/07/2016 06351045070-1302.5 201
Chlorobenzene 47 09/07/2016 0635945070-1302.3 201
Chloroethane 57 09/07/2016 06351145060-1401.3 201
Chloroform 48 09/07/2016 0635965070-1302.6 201
Chloromethane (Methyl chloride)55 09/07/2016 06351115050-1308.1 201
1,2-Dibromo-3-chloropropane (DBCP)43 09/07/2016 0635875070-1304.9 201
Dibromochloromethane 47 09/07/2016 0635945070-1300.26 201
1,2-Dibromoethane (EDB)46 09/07/2016 0635925070-1301.9 201
Dibromomethane (Methylene bromide)49 09/07/2016 0635985070-1304.3 201
1,4-Dichlorobenzene 43 09/07/2016 0635875070-1301.7 201
1,2-Dichlorobenzene 46 09/07/2016 0635935070-1300.62 201
1,2-Dichloroethane 49 09/07/2016 0635985070-1304.8 201
1,1-Dichloroethane 51 09/07/2016 06351015070-1302.8 201
cis-1,2-Dichloroethene 50 09/07/2016 0635995070-1302.4 201
1,1-Dichloroethene 51 09/07/2016 06351015070-1302.4 201
trans-1,2-Dichloroethene 52 09/07/2016 06351045070-1302.2 201
1,2-Dichloropropane 49 09/07/2016 0635985070-1300.69 201
cis-1,3-Dichloropropene 46 09/07/2016 0635925070-1302.2 201
trans-1,3-Dichloropropene 44 09/07/2016 0635875070-1302.0 201
Ethylbenzene 48 09/07/2016 0635975070-1301.1 201
2-Hexanone 97 09/07/2016 06359710060-1400.77 201
Methyl iodide (Iodomethane)51 09/07/2016 06351015070-1304.2 201
4-Methyl-2-pentanone 100 09/07/2016 063510210060-1403.8 201
Methylene chloride 48 09/07/2016 0635965070-1305.6 201
Styrene 50 09/07/2016 06351005070-1301.3 201
1,1,2,2-Tetrachloroethane 45 09/07/2016 0635905070-1300.50 201
1,1,1,2-Tetrachloroethane 49 09/07/2016 0635985070-1302.7 201
Tetrachloroethene 47 09/07/2016 0635945070-1302.0 201
Toluene 46 09/07/2016 0635915070-1300.54 201
1,1,2-Trichloroethane 47 09/07/2016 0635955070-1302.3 201
1,1,1-Trichloroethane 50 09/07/2016 0635995070-1303.1 201
Trichloroethene 50 09/07/2016 06351005070-1302.1 201
Trichlorofluoromethane 61 09/07/2016 06351225060-1402.0 201
1,2,3-Trichloropropane 46 09/07/2016 0635935070-1300.18 201
Vinyl acetate 48 09/07/2016 0635975060-1405.1 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 99 of 119
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Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:RQ21411-003
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Vinyl chloride 52 09/07/2016 06351055060-1404.1 201
Xylenes (total)98 09/07/2016 06359810070-1300.82 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 101 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 100 of 119
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21441-001
21441 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
trans-1,4-Dichloro-2-butene 2.0 09/07/2016 1015U2.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 88 70-130
Toluene-d8 99 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 101 of 119
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21441-002
21441 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
trans-1,4-Dichloro-2-butene 40 09/07/2016 0922805034-1421
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 85 70-130
Toluene-d8 99 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 102 of 119
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Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:RQ21441-003
21441 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
trans-1,4-Dichloro-2-butene 35 09/07/2016 1823705034-14213 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 83 70-130
Toluene-d8 97 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 103 of 119
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21511-001
21511 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
trans-1,4-Dichloro-2-butene 2.0 09/07/2016 2222U2.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 83 70-130
Toluene-d8 98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 104 of 119
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21511-002
21511 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
trans-1,4-Dichloro-2-butene 47 09/07/2016 2131955034-1421
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 82 70-130
Toluene-d8 98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 105 of 119
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ICP-MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:RQ21343-001
21343 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Antimony 6.0 09/07/2016 2126U6.0 0.17 ug/L1
Arsenic 10 09/07/2016 2126U100.26 ug/L1
Barium 100 09/07/2016 2126U1000.53 ug/L1
Beryllium 1.0 09/07/2016 2126U1.0 0.12 ug/L1
Cadmium 1.0 09/07/2016 2126U1.0 0.044 ug/L1
Chromium 10 09/07/2016 2126U100.63 ug/L1
Cobalt 10 09/07/2016 2126U100.26 ug/L1
Copper 0.17 09/07/2016 2126J100.15 ug/L1
Lead 10 09/07/2016 2126U100.15 ug/L1
Nickel 50 09/07/2016 2126U500.63 ug/L1
Selenium 10 09/07/2016 2126U100.95 ug/L1
Silver 10 09/07/2016 2126U100.17 ug/L1
Thallium 5.5 09/07/2016 2126U5.5 0.075 ug/L1
Vanadium 25 09/07/2016 2126U251.0 ug/L1
Zinc 10 09/07/2016 2126U101.6 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 106 of 119
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ICP-MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:RQ21343-002
21343 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Antimony 94 09/07/2016 21329410080-1201
Arsenic 91 09/07/2016 21329110080-1201
Barium 94 09/07/2016 21329410080-1201
Beryllium 94 09/07/2016 21329410080-1201
Cadmium 91 09/07/2016 21329110080-1201
Chromium 95 09/07/2016 21329510080-1201
Cobalt 100 09/07/2016 213210110080-1201
Copper 94 09/07/2016 21329410080-1201
Lead 100 09/07/2016 213210110080-1201
Nickel 98 09/07/2016 21329810080-1201
Selenium 93 09/07/2016 21329310080-1201
Silver 100 09/07/2016 213210210080-1201
Thallium 96 09/07/2016 21329610080-1201
Vanadium 95 09/07/2016 21329510080-1201
Zinc 90 09/07/2016 21329010080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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ICP-MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:RI02010-001MS
21343 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Antimony 72 09/07/2016 2143N7210075-1250.25 1
Arsenic 82 09/08/2016 11348210075-1300.0 5
Barium 570 09/07/2016 2143N5310075-1255201
Beryllium 100 09/07/2016 214310010075-1252.1 1
Cadmium 100 09/08/2016 113410110075-1250.0 5
Chromium 120 09/08/2016 113410110075-125225
Cobalt 120 09/08/2016 11349710075-125185
Copper 180 09/07/2016 21439910075-125841
Lead 110 09/07/2016 21439710075-125121
Nickel 110 09/08/2016 11349510075-125125
Selenium 77 09/07/2016 21437610075-1251.5 1
Silver 93 09/07/2016 21439310075-1250.18 1
Thallium 94 09/07/2016 21439310075-1250.62 1
Vanadium 210 09/08/2016 113410310075-1251005
Zinc 190 09/07/2016 21438810075-1251001
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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ICP-MS - MSD
Batch:Prep Method:
Prep Date:
Sample ID:RI02010-001MD
21343 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Antimony 73 09/07/2016 2149N7310075-1251.6 200.25 1
Arsenic 83 09/08/2016 11398310075-1301.2 200.0 5
Barium 610 09/07/2016 21498910075-1256.2 205201
Beryllium 100 09/07/2016 214910210075-1252.3 202.1 1
Cadmium 110 09/08/2016 113910910075-1257.0 200.0 5
Chromium 130 09/08/2016 113910910075-1256.5 20225
Cobalt 120 09/08/2016 113910410075-1256.1 20185
Copper 180 09/07/2016 21499810075-1250.44 20841
Lead 110 09/07/2016 214910210075-1254.8 20121
Nickel 110 09/08/2016 113910110075-1254.6 20125
Selenium 77 09/07/2016 21497510075-1250.30 201.5 1
Silver 96 09/07/2016 21499610075-1253.4 200.18 1
Thallium 97 09/07/2016 21499710075-1253.8 200.62 1
Vanadium 220 09/08/2016 113911610075-1255.9 201005
Zinc 200 09/07/2016 21499510075-1253.7 201001
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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ICP-MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:RQ21343-001
21343 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Dissolved Antimony 6.0 09/07/2016 2126U6.0 0.17 ug/L1
Dissolved Arsenic 10 09/07/2016 2126U100.26 ug/L1
Dissolved Barium 100 09/07/2016 2126U1000.53 ug/L1
Dissolved Beryllium 1.0 09/07/2016 2126U1.0 0.12 ug/L1
Dissolved Cadmium 1.0 09/07/2016 2126U1.0 0.044 ug/L1
Dissolved Chromium 10 09/07/2016 2126U100.63 ug/L1
Dissolved Cobalt 10 09/07/2016 2126U100.26 ug/L1
Dissolved Copper 0.17 09/07/2016 2126J100.15 ug/L1
Dissolved Lead 10 09/07/2016 2126U100.15 ug/L1
Dissolved Nickel 50 09/07/2016 2126U500.63 ug/L1
Dissolved Selenium 10 09/07/2016 2126U100.95 ug/L1
Dissolved Silver 10 09/07/2016 2126U100.17 ug/L1
Dissolved Thallium 5.5 09/07/2016 2126U5.5 0.075 ug/L1
Dissolved Vanadium 25 09/07/2016 2126U251.0 ug/L1
Dissolved Zinc 10 09/07/2016 2126U101.6 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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ICP-MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:RQ21343-002
21343 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Dissolved Antimony 94 09/07/2016 21329410080-1201
Dissolved Arsenic 91 09/07/2016 21329110080-1201
Dissolved Barium 94 09/07/2016 21329410080-1201
Dissolved Beryllium 94 09/07/2016 21329410080-1201
Dissolved Cadmium 91 09/07/2016 21329110080-1201
Dissolved Chromium 95 09/07/2016 21329510080-1201
Dissolved Cobalt 100 09/07/2016 213210110080-1201
Dissolved Copper 94 09/07/2016 21329410080-1201
Dissolved Lead 100 09/07/2016 213210110080-1201
Dissolved Nickel 98 09/07/2016 21329810080-1201
Dissolved Selenium 93 09/07/2016 21329310080-1201
Dissolved Silver 100 09/07/2016 213210210080-1201
Dissolved Thallium 96 09/07/2016 21329610080-1201
Dissolved Vanadium 95 09/07/2016 21329510080-1201
Dissolved Zinc 90 09/07/2016 21329010080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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ICP-MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:RQ21370-001
21370 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Antimony 6.0 09/08/2016 0846U6.0 0.17 ug/L1
Arsenic 10 09/08/2016 0846U100.26 ug/L1
Barium 100 09/08/2016 0846U1000.53 ug/L1
Beryllium 1.0 09/08/2016 0846U1.0 0.12 ug/L1
Cadmium 1.0 09/08/2016 0846U1.0 0.044 ug/L1
Chromium 10 09/08/2016 0846U100.63 ug/L1
Cobalt 10 09/08/2016 0846U100.26 ug/L1
Copper 10 09/08/2016 0846U100.15 ug/L1
Lead 10 09/08/2016 0846U100.15 ug/L1
Nickel 50 09/08/2016 0846U500.63 ug/L1
Selenium 10 09/08/2016 0846U100.95 ug/L1
Silver 10 09/08/2016 0846U100.17 ug/L1
Thallium 5.5 09/08/2016 0846U5.5 0.075 ug/L1
Vanadium 25 09/08/2016 0846U251.0 ug/L1
Zinc 10 09/08/2016 0846U101.6 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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ICP-MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:RQ21370-002
21370 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Antimony 100 09/08/2016 085110010080-1201
Arsenic 99 09/08/2016 08519910080-1201
Barium 100 09/08/2016 085110010080-1201
Beryllium 100 09/08/2016 085110410080-1201
Cadmium 98 09/08/2016 08519810080-1201
Chromium 100 09/08/2016 085110210080-1201
Cobalt 100 09/08/2016 085110510080-1201
Copper 100 09/08/2016 085110410080-1201
Lead 110 09/08/2016 085110910080-1201
Nickel 99 09/08/2016 08519910080-1201
Selenium 98 09/08/2016 08519810080-1201
Silver 110 09/08/2016 085111010080-1201
Thallium 100 09/08/2016 085110310080-1201
Vanadium 100 09/08/2016 085110310080-1201
Zinc 100 09/08/2016 085110210080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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ICP-MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:RQ21370-001
21370 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Dissolved Antimony 6.0 09/08/2016 0846U6.0 0.17 ug/L1
Dissolved Arsenic 10 09/08/2016 0846U100.26 ug/L1
Dissolved Barium 100 09/08/2016 0846U1000.53 ug/L1
Dissolved Beryllium 1.0 09/08/2016 0846U1.0 0.12 ug/L1
Dissolved Cadmium 1.0 09/08/2016 0846U1.0 0.044 ug/L1
Dissolved Chromium 10 09/08/2016 0846U100.63 ug/L1
Dissolved Cobalt 10 09/08/2016 0846U100.26 ug/L1
Dissolved Copper 10 09/08/2016 0846U100.15 ug/L1
Dissolved Lead 10 09/08/2016 0846U100.15 ug/L1
Dissolved Nickel 50 09/08/2016 0846U500.63 ug/L1
Dissolved Selenium 10 09/08/2016 0846U100.95 ug/L1
Dissolved Silver 10 09/08/2016 0846U100.17 ug/L1
Dissolved Thallium 5.5 09/08/2016 0846U5.5 0.075 ug/L1
Dissolved Vanadium 25 09/08/2016 0846U251.0 ug/L1
Dissolved Zinc 10 09/08/2016 0846U101.6 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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ICP-MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:RQ21370-002
21370 3005A
09/06/2016 1606Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Dissolved Antimony 100 09/08/2016 085110010080-1201
Dissolved Arsenic 99 09/08/2016 08519910080-1201
Dissolved Barium 100 09/08/2016 085110010080-1201
Dissolved Beryllium 100 09/08/2016 085110410080-1201
Dissolved Cadmium 98 09/08/2016 08519810080-1201
Dissolved Chromium 100 09/08/2016 085110210080-1201
Dissolved Cobalt 100 09/08/2016 085110510080-1201
Dissolved Copper 100 09/08/2016 085110410080-1201
Dissolved Lead 110 09/08/2016 085110910080-1201
Dissolved Nickel 99 09/08/2016 08519910080-1201
Dissolved Selenium 98 09/08/2016 08519810080-1201
Dissolved Silver 110 09/08/2016 085111010080-1201
Dissolved Thallium 100 09/08/2016 085110310080-1201
Dissolved Vanadium 100 09/08/2016 085110310080-1201
Dissolved Zinc 100 09/08/2016 085110210080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Chain of Custody
and
Miscellaneous Documents
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SHEALY ENVIRONMENTAL SERVICES, INC.

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SHEALY ENVIRONMENTAL SERVICES, INC.

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SHEALY ENVIRONMENTAL SERVICES, INC.

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SHEALY ENVIRONMENTAL SERVICES, INC.

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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
CDM Smith
5400 Glenwood Avenue
Suite 400
Raleigh, NC 27612
Attention: Mathew Colone
RI02011Lot Number:
North Wake Unlined LandfillProject Name:
09/09/2016Date Completed:
Catherine S. Dover
Project Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
CDM Smith
Lot Number: RI02011
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: North Wake Unlined Landfill
Project Number:
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
CDM Smith
Lot Number: RI02011

Project Name: North Wake Unlined Landfill
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 09/01/2016 0720MW-11 Aqueous 09/02/2016
002 09/01/2016 0740MW-11D Aqueous 09/02/2016
(2 samples)
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Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11
RI02011-001
09/01/2016 0720
09/02/2016
Aqueous
Project Name: North Wake Unlined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/07/2016 1407 HKB 21479
1 (BOD, 5 day) SM 5210B-2011 1 09/07/2016 1052 DMA 09/02/2016 1431 10829
1 (Chloride) 300.0 1 09/02/2016 1920 SLU 21372
1 (COD) SM 5220D-2011 1 09/07/2016 1628 AMM1 09/07/2016 1203
1 (Nitrate - N) 300.0 1 09/02/2016 1920 SLU 21373
1 (Sulfate) 300.0 1 09/02/2016 1920 SLU 21374
1 (Sulfide) SM 4500-S2 F-2011 1 09/07/2016 1450 BWS 21571
1 (TOC) SM 5310C-2011 1 09/07/2016 0221 MJI 21285
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 42 1mg/L2.010
BOD, 5 day SM 5210B-20 15 1mg/L0.182.0
Chloride 300.0 5.1 1mg/L0.201.0
COD SM 5220D-20 10 U 1mg/L5.710
Nitrate - N 300.0 0.81 1mg/L0.00500.020
Sulfate 300.0 1.0 U 1mg/L0.201.0
Sulfide 18496-25-8 SM 4500-S2 1.0 U 1mg/L0.621.0
TOC SM 5310C-20 1.0 U 1mg/L0.401.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11
RI02011-001
09/01/2016 0720
09/02/2016
Aqueous
Project Name: North Wake Unlined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0239 ECP 21411
2 5030B 8260B 1 09/08/2016 0239 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 5 of 49
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11
RI02011-001
09/01/2016 0720
09/02/2016
Aqueous
Project Name: North Wake Unlined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0239 ECP 21411
2 5030B 8260B 1 09/08/2016 0239 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 94 70-130 94 70-130
1,2-Dichloroethane-d4 105 70-130 85 70-130
Toluene-d8 99 70-130 96 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 6 of 49
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Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11
RI02011-001
09/01/2016 0720
09/02/2016
Aqueous
Project Name: North Wake Unlined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1337 BNW 09/07/2016 1253 21415
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 1.0 U 1ug/L0.171.0
Dissolved Arsenic 7440-38-2 6020A 1.0 U 1ug/L0.261.0
Dissolved Barium 7440-39-3 6020A 48 1ug/L0.535.0
Dissolved Beryllium 7440-41-7 6020A 0.40 U 1ug/L0.120.40
Dissolved Cadmium 7440-43-9 6020A 0.10 U 1ug/L0.0440.10
Dissolved Chromium 7440-47-3 6020A 1.1 J 1ug/L0.635.0
Dissolved Cobalt 7440-48-4 6020A 5.0 U 1ug/L0.265.0
Dissolved Copper 7440-50-8 6020A 0.28 BJ 1ug/L0.151.0
Dissolved Lead 7439-92-1 6020A 1.0 U 1ug/L0.151.0
Dissolved Nickel 7440-02-0 6020A 5.0 U 1ug/L0.635.0
Dissolved Selenium 7782-49-2 6020A 1.0 U 1ug/L0.951.0
Dissolved Silver 7440-22-4 6020A 1.0 U 1ug/L0.171.0
Dissolved Thallium 7440-28-0 6020A 0.50 U 1ug/L0.0750.50
Dissolved Vanadium 7440-62-2 6020A 2.0 J 1ug/L1.05.0
Dissolved Zinc 7440-66-6 6020A 6.9 BJ 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 7 of 49
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Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11
RI02011-001
09/01/2016 0720
09/02/2016
Aqueous
Project Name: North Wake Unlined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1343 BNW 09/07/2016 1253 21415
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 1.0 U 1ug/L0.171.0
Arsenic 7440-38-2 6020A 1.0 U 1ug/L0.261.0
Barium 7440-39-3 6020A 90 1ug/L0.535.0
Beryllium 7440-41-7 6020A 0.28 J 1ug/L0.120.40
Cadmium 7440-43-9 6020A 0.054 J 1ug/L0.0440.10
Chromium 7440-47-3 6020A 2.4 J 1ug/L0.635.0
Cobalt 7440-48-4 6020A 2.6 J 1ug/L0.265.0
Copper 7440-50-8 6020A 8.3 B 1ug/L0.151.0
Lead 7439-92-1 6020A 1.3 1ug/L0.151.0
Nickel 7440-02-0 6020A 1.6 J 1ug/L0.635.0
Selenium 7782-49-2 6020A 1.0 U 1ug/L0.951.0
Silver 7440-22-4 6020A 1.0 U 1ug/L0.171.0
Thallium 7440-28-0 6020A 0.50 U 1ug/L0.0750.50
Vanadium 7440-62-2 6020A 11 1ug/L1.05.0
Zinc 7440-66-6 6020A 20 B 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 8 of 49
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11D
RI02011-002
09/01/2016 0740
09/02/2016
Aqueous
Project Name: North Wake Unlined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0302 ECP 21411
2 5030B 8260B 1 09/08/2016 0303 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 9 of 49
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11D
RI02011-002
09/01/2016 0740
09/02/2016
Aqueous
Project Name: North Wake Unlined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0302 ECP 21411
2 5030B 8260B 1 09/08/2016 0303 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 96 70-130
1,2-Dichloroethane-d4 107 70-130 87 70-130
Toluene-d8 102 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 10 of 49
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Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11D
RI02011-002
09/01/2016 0740
09/02/2016
Aqueous
Project Name: North Wake Unlined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1348 BNW 09/07/2016 1253 21415
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Dissolved Antimony 7440-36-0 6020A 1.0 U 1ug/L0.171.0
Dissolved Arsenic 7440-38-2 6020A 1.0 U 1ug/L0.261.0
Dissolved Barium 7440-39-3 6020A 41 1ug/L0.535.0
Dissolved Beryllium 7440-41-7 6020A 0.40 U 1ug/L0.120.40
Dissolved Cadmium 7440-43-9 6020A 0.045 J 1ug/L0.0440.10
Dissolved Chromium 7440-47-3 6020A 0.70 J 1ug/L0.635.0
Dissolved Cobalt 7440-48-4 6020A 5.0 U 1ug/L0.265.0
Dissolved Copper 7440-50-8 6020A 0.73 BJ 1ug/L0.151.0
Dissolved Lead 7439-92-1 6020A 1.0 U 1ug/L0.151.0
Dissolved Nickel 7440-02-0 6020A 0.72 J 1ug/L0.635.0
Dissolved Selenium 7782-49-2 6020A 1.0 U 1ug/L0.951.0
Dissolved Silver 7440-22-4 6020A 1.0 U 1ug/L0.171.0
Dissolved Thallium 7440-28-0 6020A 0.50 U 1ug/L0.0750.50
Dissolved Vanadium 7440-62-2 6020A 1.7 J 1ug/L1.05.0
Dissolved Zinc 7440-66-6 6020A 6.2 BJ 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 11 of 49
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Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11D
RI02011-002
09/01/2016 0740
09/02/2016
Aqueous
Project Name: North Wake Unlined Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1354 BNW 09/07/2016 1253 21415
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.43 BJ 1ug/L0.171.0
Arsenic 7440-38-2 6020A 1.0 U 1ug/L0.261.0
Barium 7440-39-3 6020A 45 1ug/L0.535.0
Beryllium 7440-41-7 6020A 0.40 U 1ug/L0.120.40
Cadmium 7440-43-9 6020A 0.076 J 1ug/L0.0440.10
Chromium 7440-47-3 6020A 1.2 J 1ug/L0.635.0
Cobalt 7440-48-4 6020A 5.0 U 1ug/L0.265.0
Copper 7440-50-8 6020A 2.1 B 1ug/L0.151.0
Lead 7439-92-1 6020A 0.25 J 1ug/L0.151.0
Nickel 7440-02-0 6020A 0.75 J 1ug/L0.635.0
Selenium 7782-49-2 6020A 1.0 U 1ug/L0.951.0
Silver 7440-22-4 6020A 1.0 U 1ug/L0.171.0
Thallium 7440-28-0 6020A 0.50 U 1ug/L0.0750.50
Vanadium 7440-62-2 6020A 2.7 J 1ug/L1.05.0
Zinc 7440-66-6 6020A 9.2 BJ 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 12 of 49
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QC Summary
Page: 13 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MB
Batch:
Sample ID:RQ21285-001
21285
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
TOC 1.0 09/06/2016 1927U1.0 0.40 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 14 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - LCS
Batch:
Sample ID:RQ21285-002
21285
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
TOC 19 09/06/2016 1946952090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 15 of 49
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Inorganic non-metals - MS
Batch:
Sample ID:RI02011-001MS
21285
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
TOC 18 09/07/2016 0240882070-1300.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 16 of 49
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Inorganic non-metals - MSD
Batch:
Sample ID:RI02011-001MD
21285
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
TOC 17 09/07/2016 0259872070-1300.84 200.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 17 of 49
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Inorganic non-metals - MB
Batch:
Sample ID:RQ21372-001
21372
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Chloride 1.0 09/02/2016 1832U1.0 0.20 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 18 of 49
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Inorganic non-metals - LCS
Batch:
Sample ID:RQ21372-002
21372
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Chloride 20 09/02/2016 1856982090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 19 of 49
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Inorganic non-metals - MS
Batch:
Sample ID:RI02011-001MS
21372
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Chloride 25 09/02/2016 1944992090-1105.1 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 20 of 49
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Inorganic non-metals - MSD
Batch:
Sample ID:RI02011-001MD
21372
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Chloride 25 09/02/2016 2008982090-1100.24 205.1 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 21 of 49
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Inorganic non-metals - MB
Batch:
Sample ID:RQ21373-001
21373
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Nitrate - N 0.020 09/02/2016 1832U0.020 0.0050 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 22 of 49
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Inorganic non-metals - LCS
Batch:
Sample ID:RQ21373-002
21373
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Nitrate - N 0.79 09/02/2016 1856990.80 90-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 23 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MS
Batch:
Sample ID:RI02011-001MS
21373
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Nitrate - N 1.6 09/02/2016 1944950.80 90-1100.81 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 24 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MSD
Batch:
Sample ID:RI02011-001MD
21373
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Nitrate - N 1.6 09/02/2016 2008950.80 90-1100.096 200.81 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 25 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MB
Batch:
Sample ID:RQ21374-001
21374
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Sulfate 1.0 09/02/2016 1832U1.0 0.20 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 26 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - LCS
Batch:
Sample ID:RQ21374-002
21374
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Sulfate 19 09/02/2016 1856942090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 27 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MS
Batch:
Sample ID:RI02011-001MS
21374
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfate 19 09/02/2016 1944932090-1100.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 28 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MSD
Batch:
Sample ID:RI02011-001MD
21374
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfate 18 09/02/2016 2008922090-1101.2 200.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 29 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MB
Batch:
Sample ID:RQ21479-001
21479
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Alkalinity 10 09/07/2016 1346U102.0 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 30 of 49
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Inorganic non-metals - LCS
Batch:
Sample ID:RQ21479-002
21479
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 99 09/07/2016 13529910090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 31 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MB
Batch:
Sample ID:RQ21571-001
21571
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Sulfide 1.0 09/07/2016 1450U1.0 0.62 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 32 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - LCS
Batch:
Sample ID:RQ21571-002
21571
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Sulfide 9.8 09/07/2016 1450981080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 33 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MS
Batch:
Sample ID:RI02011-001MS
21571
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfide 8.8 09/07/2016 1450881070-1300.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 34 of 49
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Shealy Environmental Services, Inc.

Inorganic non-metals - MSD
Batch:
Sample ID:RI02011-001MD
21571
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfide 9.0 09/07/2016 1450901070-1302.2 200.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 35 of 49
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21411-001
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 10 09/06/2016 2159U102.0 ug/L1
Acrylonitrile 5.0 09/06/2016 2159U5.0 0.80 ug/L1
Benzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromochloromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromodichloromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromoform 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromomethane (Methyl bromide)0.50 09/06/2016 2159U0.50 0.40 ug/L1
2-Butanone (MEK)10 09/06/2016 2159U102.0 ug/L1
Carbon disulfide 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Carbon tetrachloride 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chlorobenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chloroform 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chloromethane (Methyl chloride)0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)0.50 09/06/2016 2159U0.50 0.40 ug/L1
Dibromochloromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dibromoethane (EDB)0.50 09/06/2016 2159U0.50 0.40 ug/L1
Dibromomethane (Methylene bromide)0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,4-Dichlorobenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dichlorobenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Dichlorodifluoromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1-Dichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
cis-1,2-Dichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1-Dichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
trans-1,2-Dichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dichloropropane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
cis-1,3-Dichloropropene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
trans-1,3-Dichloropropene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Ethylbenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
2-Hexanone 10 09/06/2016 2159U102.0 ug/L1
Methyl iodide (Iodomethane)5.0 09/06/2016 2159U5.0 0.40 ug/L1
4-Methyl-2-pentanone 10 09/06/2016 2159U102.0 ug/L1
Methylene chloride 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Styrene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,1,2-Tetrachloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Tetrachloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Toluene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,2-Trichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,1-Trichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Trichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Trichlorofluoromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2,3-Trichloropropane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 36 of 49
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21411-001
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Vinyl acetate 5.0 09/06/2016 2159U5.0 1.2 ug/L1
Vinyl chloride 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Xylenes (total)1.0 09/06/2016 2159U1.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 37 of 49
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21411-002
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 95 09/06/2016 20579510060-1401
Acrylonitrile 93 09/06/2016 20579310060-1401
Benzene 47 09/06/2016 2057935070-1301
Bromochloromethane 50 09/06/2016 20571005070-1301
Bromodichloromethane 49 09/06/2016 2057985070-1301
Bromoform 46 09/06/2016 2057925070-1301
Bromomethane (Methyl bromide)55 09/06/2016 20571115060-1401
2-Butanone (MEK)95 09/06/2016 20579510060-1401
Carbon disulfide 50 09/06/2016 20571005060-1401
Carbon tetrachloride 51 09/06/2016 20571025070-1301
Chlorobenzene 46 09/06/2016 2057925070-1301
Chloroethane 56 09/06/2016 20571135060-1401
Chloroform 47 09/06/2016 2057935070-1301
Chloromethane (Methyl chloride)51 09/06/2016 20571025050-1301
1,2-Dibromo-3-chloropropane (DBCP)46 09/06/2016 2057915070-1301
Dibromochloromethane 47 09/06/2016 2057945070-1301
1,2-Dibromoethane (EDB)45 09/06/2016 2057905070-1301
Dibromomethane (Methylene bromide)47 09/06/2016 2057945070-1301
1,4-Dichlorobenzene 44 09/06/2016 2057885070-1301
1,2-Dichlorobenzene 46 09/06/2016 2057925070-1301
Dichlorodifluoromethane 56 09/06/2016 20571115060-1401
1,2-Dichloroethane 47 09/06/2016 2057945070-1301
1,1-Dichloroethane 49 09/06/2016 2057985070-1301
cis-1,2-Dichloroethene 48 09/06/2016 2057975070-1301
1,1-Dichloroethene 50 09/06/2016 2057995070-1301
trans-1,2-Dichloroethene 51 09/06/2016 20571025070-1301
1,2-Dichloropropane 49 09/06/2016 2057975070-1301
cis-1,3-Dichloropropene 47 09/06/2016 2057945070-1301
trans-1,3-Dichloropropene 45 09/06/2016 2057895070-1301
Ethylbenzene 48 09/06/2016 2057965070-1301
2-Hexanone 96 09/06/2016 20579610060-1401
Methyl iodide (Iodomethane)49 09/06/2016 2057975070-1301
4-Methyl-2-pentanone 98 09/06/2016 20579810060-1401
Methylene chloride 45 09/06/2016 2057905070-1301
Styrene 49 09/06/2016 2057995070-1301
1,1,2,2-Tetrachloroethane 45 09/06/2016 2057915070-1301
1,1,1,2-Tetrachloroethane 48 09/06/2016 2057965070-1301
Tetrachloroethene 48 09/06/2016 2057965070-1301
Toluene 46 09/06/2016 2057925070-1301
1,1,2-Trichloroethane 46 09/06/2016 2057935070-1301
1,1,1-Trichloroethane 48 09/06/2016 2057965070-1301
Trichloroethene 49 09/06/2016 2057985070-1301
Trichlorofluoromethane 60 09/06/2016 20571195060-1401
1,2,3-Trichloropropane 46 09/06/2016 2057935070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 38 of 49
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21411-002
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Vinyl acetate 51 09/06/2016 20571025060-1401
Vinyl chloride 50 09/06/2016 20571015060-1401
Xylenes (total)97 09/06/2016 20579710070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 99 70-130
Toluene-d8 101 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 39 of 49
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Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:RQ21411-003
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Acetone 99 09/07/2016 06359910060-1404.5 201
Acrylonitrile 95 09/07/2016 06359510060-1402.0 401
Benzene 47 09/07/2016 0635945070-1301.3 201
Bromochloromethane 51 09/07/2016 06351025070-1301.8 201
Bromodichloromethane 50 09/07/2016 06351005070-1302.3 201
Bromoform 45 09/07/2016 0635905070-1302.3 201
Bromomethane (Methyl bromide)56 09/07/2016 06351135060-1402.0 201
2-Butanone (MEK)98 09/07/2016 06359810060-1403.5 201
Carbon disulfide 52 09/07/2016 06351045060-1404.3 201
Carbon tetrachloride 52 09/07/2016 06351045070-1302.5 201
Chlorobenzene 47 09/07/2016 0635945070-1302.3 201
Chloroethane 57 09/07/2016 06351145060-1401.3 201
Chloroform 48 09/07/2016 0635965070-1302.6 201
Chloromethane (Methyl chloride)55 09/07/2016 06351115050-1308.1 201
1,2-Dibromo-3-chloropropane (DBCP)43 09/07/2016 0635875070-1304.9 201
Dibromochloromethane 47 09/07/2016 0635945070-1300.26 201
1,2-Dibromoethane (EDB)46 09/07/2016 0635925070-1301.9 201
Dibromomethane (Methylene bromide)49 09/07/2016 0635985070-1304.3 201
1,4-Dichlorobenzene 43 09/07/2016 0635875070-1301.7 201
1,2-Dichlorobenzene 46 09/07/2016 0635935070-1300.62 201
Dichlorodifluoromethane 58 09/07/2016 06351155060-1403.6 201
1,2-Dichloroethane 49 09/07/2016 0635985070-1304.8 201
1,1-Dichloroethane 51 09/07/2016 06351015070-1302.8 201
cis-1,2-Dichloroethene 50 09/07/2016 0635995070-1302.4 201
1,1-Dichloroethene 51 09/07/2016 06351015070-1302.4 201
trans-1,2-Dichloroethene 52 09/07/2016 06351045070-1302.2 201
1,2-Dichloropropane 49 09/07/2016 0635985070-1300.69 201
cis-1,3-Dichloropropene 46 09/07/2016 0635925070-1302.2 201
trans-1,3-Dichloropropene 44 09/07/2016 0635875070-1302.0 201
Ethylbenzene 48 09/07/2016 0635975070-1301.1 201
2-Hexanone 97 09/07/2016 06359710060-1400.77 201
Methyl iodide (Iodomethane)51 09/07/2016 06351015070-1304.2 201
4-Methyl-2-pentanone 100 09/07/2016 063510210060-1403.8 201
Methylene chloride 48 09/07/2016 0635965070-1305.6 201
Styrene 50 09/07/2016 06351005070-1301.3 201
1,1,2,2-Tetrachloroethane 45 09/07/2016 0635905070-1300.50 201
1,1,1,2-Tetrachloroethane 49 09/07/2016 0635985070-1302.7 201
Tetrachloroethene 47 09/07/2016 0635945070-1302.0 201
Toluene 46 09/07/2016 0635915070-1300.54 201
1,1,2-Trichloroethane 47 09/07/2016 0635955070-1302.3 201
1,1,1-Trichloroethane 50 09/07/2016 0635995070-1303.1 201
Trichloroethene 50 09/07/2016 06351005070-1302.1 201
Trichlorofluoromethane 61 09/07/2016 06351225060-1402.0 201
1,2,3-Trichloropropane 46 09/07/2016 0635935070-1300.18 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 40 of 49
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Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:RQ21411-003
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Vinyl acetate 48 09/07/2016 0635975060-1405.1 201
Vinyl chloride 52 09/07/2016 06351055060-1404.1 201
Xylenes (total)98 09/07/2016 06359810070-1300.82 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 101 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 41 of 49
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21511-001
21511 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
trans-1,4-Dichloro-2-butene 2.0 09/07/2016 2222U2.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 83 70-130
Toluene-d8 98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 42 of 49
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21511-002
21511 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
trans-1,4-Dichloro-2-butene 47 09/07/2016 2131955034-1421
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 82 70-130
Toluene-d8 98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 43 of 49
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Shealy Environmental Services, Inc.

ICP-MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:RQ21415-001
21415 3005A
09/07/2016 1253Analytical Method:6020A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Dissolved Antimony 0.19 09/08/2016 1218J1.0 0.17 ug/L1
Dissolved Arsenic 1.0 09/08/2016 1218U1.0 0.26 ug/L1
Dissolved Barium 5.0 09/08/2016 1218U5.0 0.53 ug/L1
Dissolved Beryllium 0.40 09/08/2016 1218U0.40 0.12 ug/L1
Dissolved Cadmium 0.10 09/08/2016 1218U0.10 0.044 ug/L1
Dissolved Chromium 5.0 09/08/2016 1218U5.0 0.63 ug/L1
Dissolved Cobalt 5.0 09/08/2016 1218U5.0 0.26 ug/L1
Dissolved Copper 0.19 09/08/2016 1218J1.0 0.15 ug/L1
Dissolved Lead 1.0 09/08/2016 1218U1.0 0.15 ug/L1
Dissolved Nickel 5.0 09/08/2016 1218U5.0 0.63 ug/L1
Dissolved Selenium 1.0 09/08/2016 1218U1.0 0.95 ug/L1
Dissolved Silver 1.0 09/08/2016 1218U1.0 0.17 ug/L1
Dissolved Thallium 0.50 09/08/2016 1218U0.50 0.075 ug/L1
Dissolved Vanadium 5.0 09/08/2016 1218U5.0 1.0 ug/L1
Dissolved Zinc 1.8 09/08/2016 1218J101.6 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 44 of 49
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Shealy Environmental Services, Inc.

ICP-MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:RQ21415-002
21415 3005A
09/07/2016 1253Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Dissolved Antimony 96 09/08/2016 12249610080-1201
Dissolved Arsenic 94 09/08/2016 12249410080-1201
Dissolved Barium 95 09/08/2016 12249510080-1201
Dissolved Beryllium 120 09/08/2016 122411810080-1201
Dissolved Cadmium 94 09/08/2016 12249410080-1201
Dissolved Chromium 100 09/08/2016 122410110080-1201
Dissolved Cobalt 100 09/08/2016 122410310080-1201
Dissolved Copper 96 09/08/2016 12249610080-1201
Dissolved Lead 100 09/08/2016 122410310080-1201
Dissolved Nickel 97 09/08/2016 12249710080-1201
Dissolved Selenium 95 09/08/2016 12249510080-1201
Dissolved Silver 100 09/08/2016 122410410080-1201
Dissolved Thallium 97 09/08/2016 12249710080-1201
Dissolved Vanadium 100 09/08/2016 122410110080-1201
Dissolved Zinc 98 09/08/2016 12249810080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 45 of 49
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Shealy Environmental Services, Inc.

ICP-MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:RQ21415-001
21415 3005A
09/07/2016 1253Analytical Method:6020A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Antimony 0.19 09/08/2016 1218J1.0 0.17 ug/L1
Arsenic 1.0 09/08/2016 1218U1.0 0.26 ug/L1
Barium 5.0 09/08/2016 1218U5.0 0.53 ug/L1
Beryllium 0.40 09/08/2016 1218U0.40 0.12 ug/L1
Cadmium 0.10 09/08/2016 1218U0.10 0.044 ug/L1
Chromium 5.0 09/08/2016 1218U5.0 0.63 ug/L1
Cobalt 5.0 09/08/2016 1218U5.0 0.26 ug/L1
Copper 0.19 09/08/2016 1218J1.0 0.15 ug/L1
Lead 1.0 09/08/2016 1218U1.0 0.15 ug/L1
Nickel 5.0 09/08/2016 1218U5.0 0.63 ug/L1
Selenium 1.0 09/08/2016 1218U1.0 0.95 ug/L1
Silver 1.0 09/08/2016 1218U1.0 0.17 ug/L1
Thallium 0.50 09/08/2016 1218U0.50 0.075 ug/L1
Vanadium 5.0 09/08/2016 1218U5.0 1.0 ug/L1
Zinc 1.8 09/08/2016 1218J101.6 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 46 of 49
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:RQ21415-002
21415 3005A
09/07/2016 1253Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Antimony 96 09/08/2016 12249610080-1201
Arsenic 94 09/08/2016 12249410080-1201
Barium 95 09/08/2016 12249510080-1201
Beryllium 120 09/08/2016 122411810080-1201
Cadmium 94 09/08/2016 12249410080-1201
Chromium 100 09/08/2016 122410110080-1201
Cobalt 100 09/08/2016 122410310080-1201
Copper 96 09/08/2016 12249610080-1201
Lead 100 09/08/2016 122410310080-1201
Nickel 97 09/08/2016 12249710080-1201
Selenium 95 09/08/2016 12249510080-1201
Silver 100 09/08/2016 122410410080-1201
Thallium 97 09/08/2016 12249710080-1201
Vanadium 100 09/08/2016 122410110080-1201
Zinc 98 09/08/2016 12249810080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.

Chain of Custody
and
Miscellaneous Documents
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SHEALY ENVIRONMENTAL SERVICES, INC.

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SHEALY ENVIRONMENTAL SERVICES, INC.

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