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HomeMy WebLinkAbout7803_RobesonCoMSW_Nov2016_2ndSemiAnnual_DIN28078_20170131 Robeson County Landfill Water Quality Monitoring Report November 2016 Semi-Annual Event Prepared on Behalf of: Robeson County Landfill 246 Landfill Rd Lumberton, North Carolina 28360 Facility Permit No. 78-03 Dated: January 31, 2017 Prepared by: 1730 Rennert Rd. Lumberton NC, 28360 TRANSMITTAL LETTER January 26, 2017 Mrs. Elizabeth Werner Hydrogeologist North Carolina Department of Environment and Natural Resources Division of Waste Management - Solid Waste Section 217 W Jones St, Raleigh, North Carolina 27603 Subject: Robeson County Landfill Water Quality Monitoring Report November 2016 Semi-Annual Event Robeson County Landfill St. Pauls, Robeson County, North Carolina To: Mrs. Werner Hunt Environmental Associates, PLLC has prepared this November 2016 Semi-Annual Water Quality Monitoring Report for the Robeson County Landfill. This report summarizes the findings of sampling data gathered at the site. The scope of work at the site was executed in order to fulfill the NCDENR Solid Waste Section reporting requirements for environmental monitoring We appreciate your consideration and review following the submission of this report. If you have- any questions concerning this report, please don’t hesitate to contact us at (910) 674-5925. Respectfully Submitted, ______________________ Michael Cody Hunt, P.G., M.S. Project Geologist Table of Contents 1.0 INTRODUCTION ............................................................................................................... 1 2.0 SITE BACKGROUND AND MONITORING NETWORK .............................................. 1 3.0 SITE HYDROGEOLOGY ................................................................................................... 1 4.0 FIELD ACTIVITIES ........................................................................................................... 2 5.0 ANALYTICAL RESULTS ................................................................................................. 2 5.1 Groundwater ..................................................................................................................... 2 5.2 Surface Water ................................................................................................................... 5 5.3 Leachate ........................................................................................................................... 5 6.0 STATISTICAL PROCEDURES ......................................................................................... 5 6.1 STATISTICAL RESULTS SUMMARY......................................................................... 6 7.0 CONCLUSIONS AND RECOMMENDATIONS .............................................................. 6 Figures Figure 1: Groundwater Potentiometric Map Tables Table 1: Groundwater Monitoring Program Table 2: Ground Water Elevations & Flow Velocities Table 3: Analytical Results Table 4: Statistical Analysis Summary Appendices Appendix A: Laboratory Analytical Results Appendix B: Time Series Graphs Appendix C: Non-Parametric Prediction Interval Inter-Well Comparisons 1 | P a g e 1.0 INTRODUCTION The Robeson County Landfill, operating under North Carolina Department of Environment and Natural Resources (NCDENR) Solid Waste Permit #78-03, is required to submit semi-annual groundwater monitoring reports for detection monitoring of the Phase 2, Phase 3, and Phase 4 lined landfills and assessment monitoring of the Phase 1 unlined landfill. This report presents the results of the first semi-annual monitoring event for 2016, conducted in March of 2016. Also included in this report are the results of the surface water and leachate monitoring that was performed in conjunction with the groundwater monitoring event. The Robeson County Landfill is currently accepting construction and demolition debris (C&D) waste over the closed Phase 1 Municipal Solid Waste (MSW) unlined landfill. Currently, all MSW is being disposed in the Phase 4 lined landfill. The Phase 1 unlined landfill has been closed per NCDENR Solid Waste Regulations, and the C&D disposal will bring the landfill to final closure contours. 2.0 SITE BACKGROUND AND MONITORING NETWORK Currently twenty-nine groundwater monitoring wells are located around the perimeter of the Phase 1, Phase 2, Phase 3, Phase 4 and C&D landfill cells (Figure 1). Table 1 lists the currently monitored wells associated with each Phase of the landfill. Twenty-two groundwater monitoring wells were monitored during this sampling event. Seven monitoring wells have been damaged and were approved for closure by NCDENR Solid Waste Section correspondence from Ms. Werner on March 22 of 2011, three wells were approved for closure and replacement on January 3, 2013 and therefore, none of them were sampled for this event. Two surface water samples (SW-1 & SW-2) were collected as shown in Figure 1. Leachate samples were also collected during this monitoring event for Phases 2, 3, and 4. Phase 2 and 3 leachate samples were collected from the respective line valves linked to the generator. The Phase 4 leachate sample was collected from the line pump station. This report includes summaries of the field procedures, and field, laboratory, and statistical results from the November 2016 semi-annual groundwater sampling event. Field and laboratory results of the surface water and leachate sampling are also presented. Summary tables of the monitoring network, groundwater characteristics, field measurements, laboratory and statistical analysis results, as well as graphs of groundwater analytical data over time are included at the end of the report. 3.0 SITE HYDROGEOLOGY The site is located in the Coastal Plain Physiographic province within the Cretaceous-age Black Creek Formation. In general, the lithology of the site is composed of sandy soils with clay. As a result, the direction of groundwater flow should be largely controlled by site topography. 2 | P a g e Figure 1 provides potentiometric surface maps and groundwater flow calculations for the shallow aquifer utilizing groundwater level data from the Second Semi-Annual 2016 event. Groundwater flow direction for the Second Semi-Annual 2016 event was to the southeast towards the Big Marsh Swamp, consistent with past events. Groundwater velocity for the Second Semi-Annual 2016 event was calculated utilizing Darcy’s law: V = Ki/n, where K = hydraulic conductivity, i = groundwater gradient, n = porosity. Based on the fall dataset, groundwater velocities are estimated to range from 0.18 feet/year (MW-24) to 91.39 feet/year (MW-9a). 4.0 FIELD ACTIVITIES Groundwater, surface water, and leachate samples from the Robeson County Landfill were collected on November 30 and December 1, 2016. Twenty two (22) groundwater samples were collected by use of a disposable, laboratory decontaminated polyethylene bailer. Sampling locations are presented on Figure 1. Groundwater elevations were measured at each well prior to sampling and are presented in Table 2. These groundwater elevations were used to construct the potentiometric contours for this sampling event as shown on Figure 1. The groundwater elevations and potentiometric contours were used to estimate groundwater velocities at each well presented in Table 2. After depth to groundwater was measured, water was purged from each well to provide fresh formation water within the well water column prior to sampling. All samples were collected in clean laboratory prepared containers for the specified analytical methods. Groundwater samples were properly preserved, placed on ice, and transported to the laboratory via overnight delivery. The samples were transported to ESC Lab Sciences Inc., a North Carolina certified laboratory (NC DW #21704). Laboratory analyses consisted of those noted in Table 1 and were reported according to the laboratory’s Method Detection Limits (MDLs). The laboratory analytical reports are included in Appendix A. Trip and equipment blanks were used for quality assurance/quality control (QA/QC). Trip blanks were prepared by the laboratory and accompanied the coolers during the sampling event. One equipment blank was prepared by pouring distilled water over a bailer and collecting the water in containers provided by the laboratory. Sampling methods followed the protocol outlined in NCDENR’s Guidelines for Groundwater, Soil, and Surface Water Sampling (NCDENR 2008) and in accordance with the approved Sampling and Analysis Plan (Water Quality Monitoring Plan, David Garrett and Associates, Raleigh, NC, 2009). 5.0 ANALYTICAL RESULTS 5.1 Groundwater ESC Lab Sciences, Inc. located in Lebanon, Tennessee analyzed samples for the North Carolina Appendix I volatile organic compounds (VOCs) and metals. In accordance with SWS guidelines the analytical results were reported to the laboratory specific method detection limit (MDL) and are quantifiable at or below Solid Waste Section Limits (SWSLs). The following list indicates which analytes were detected above the SWSL at each sampling location. Underlined analytes exceeded the North Carolina 2L Standard (NC 2L), the Groundwater Protection Standard, or the North Carolina Surface Water Standards for Class C Waters. A complete summary of all 3 | P a g e detected and estimated concentrations for this sampling event is presented in Table 3. Copies of the laboratory analytical data reports are provided in Appendix A. MW-3R Volatile Organic Compounds: None Detected Metals: Chromium, Vanadium, Selenium MW-5 Volatile Organic Compounds: 1,4-Dichlorobenzene Metals: None Detected MW-6 Volatile Organic Compounds: None Detected Metals: None Detected MW-8 Volatile Organic Compounds: 1,4-Dichlorobenzene, Metals: None Detected MW-9A Volatile Organic Compounds: 1,4-Dichlorobenzene, 1,1-Dichloroethane, Benzene Metals: None Detected MW-10 Volatile Organic Compounds: None Detected Metals: Chromium, Zinc MW-11 Volatile Organic Compounds: None Detected Metals: Zinc MW-12 Volatile Organic Compounds: None Detected Metals: None Detected MW-13R Volatile Organic Compounds: Benzene, 1,4-Dichlorobenzene Metals: Barium MW-14 Volatile Organic Compounds: None Detected Metals: Barium MW-15 Volatile Organic Compounds: Acetone, Benzene, 1,4-Dichlorobenzene, Metals: None Detected 4 | P a g e MW-16 Volatile Organic Compounds: Benzene, Chloroethane, 1,4-Dichlorobenzene Metals: Barium, Arsenic MW-17R Volatile Organic Compounds: Tetrachloroethene, Trichloroethene Metals: Barium, Chromium, Cobalt MW-18 Volatile Organic Compounds: None Detected Metals: Barium MW-19 Volatile Organic Compounds: None Detected Metals: Barium, Chromium, Vanadium, Copper, Lead, Zinc, Arsenic MW-20 Volatile Organic Compounds: None Detected Metals: Barium, Lead MW-21R Volatile Organic Compounds: None Detected Metals: Cobalt MW-22 Volatile Organic Compounds: None Detected Metals: None Detected MW-23 Volatile Organic Compounds: None Detected Metals: None Detected MW-24R Volatile Organic Compounds: None Detected Metals: None Detected MW-25R Volatile Organic Compounds: None Detected Metals: None Detected MW-26 Volatile Organic Compounds: None Detected Metals: None Detected 5 | P a g e 5.2 Surface Water HEA personnel sampled two surface water bodies in the vicinity of the Phase 1, 2, 3 and Phase 4 landfills (Figure 1). Surface water sampling point SW-1 is located below the outflow from the existing sediment basin southwest of the Phase 1 cell. Surface water sampling point SW-2 is located in a drainage ditch, southeast of the Phase 2 cell. The following list indicates which analytes were detected above the SWSL at each sampling location. Underlined analytes exceeded the North Carolina 2L Standard (NC 2L), the Groundwater Protection Standard, or the North Carolina Surface Water Standards for Class C Waters. SW-1 Volatile Organic Compounds: None Detected Metals: Barium SW-2 During the Second Semi-Annual sampling event this pond was dry therefore we did not conduct a sampling. 5.3 Leachate HEA personnel sampled three leachate drainage lines in the vicinity of the Phase 2, 3 and 4 landfill cells. Two leachate sampling locations are east of the Phase 2 and 3 cells; one is located east of the Phase 4 cell. Analytical results are presented in Table 3. 6.0 STATISTICAL PROCEDURES The laboratory data from the sampling event were reviewed and analyzed by HEA in order to evaluate trends and changes in the results and to identify statistically significant differences between compliance and background wells. Data entry and analysis were performed using the Chemstat statistical software package developed by Starpoint Software, Cincinnati, OH. Chemstat follows the EPA document, Statistical Analysis of Ground-Water Monitoring Data at RCRA Facilities – Unified Guidance (March 2009), as well as NCDENR guidelines. The data were reviewed to evaluate the most appropriate analysis methods. Initial analysis consisted of a basic review of the data and of the time vs. concentration graphs (included in Appendix B) to determine any major changes or trends in the data. Individual compliance well historical means were compared to the pooled background historical means for MW-6 and MW- 12 to determine if detected constituents were statistically significantly different from general background groundwater quality. The statistical analysis results are summarized in Table 4 and provided in Appendix C. 6 | P a g e 6.1 STATISTICAL RESULTS SUMMARY For the Second Semi-Annual 2016 event, statistically significant differences from background concentrations and above SWSLs, shown in Table 4, were found for VOCs and Metals as detailed below: VOCs  1,4-Dichlorobenzene – MW-9A, MW-15  1,1-Dichloroethane – MW-9A  Acetone – MW-15  Chloroethane – MW-16 Metals  Arsenic – MW-16  Chromium – MW-3R MW-10, MW -17R  Cobalt – MW-17R, MW-21R  Selenium – MW-3R, 7.0 CONCLUSIONS AND RECOMMENDATIONS For the Second Semi-Annual 2016 groundwater monitoring event, concentrations that were detected above an NC SWSL and NC GWPS/NC 2L were also determined to statistically exceed the background concentrations. Based on the statistical evaluations: No groundwater detections were identified as statistically significant increases for the Second Semi-Annual 2016 event. The following groundwater detections were identified appearing to decrease site wide:  Acetone  Cadmium The following groundwater detections were identified appearing to remain relatively constant site wide:  1,4-Dichlorobenzene  1,1-Dichloroethane  Arsenic  Chromium  Zinc  Cobalt  Selenium  Benzene 7 | P a g e During the Second Semi-Annual 2016 event, one Appendix I VOCs and two Appendix I inorganic constituents were detected in surface water samples at quantified concentrations above their respective NC SWSLs at SW-2: Acetone, Barium, and Zinc. These constituents do not have a NC 2B Surface Water Standard established for swamp waters (status of discharge locations). The site will continue monitoring in accordance with the requirements for Detection Monitoring as outlined in Title 15A NCAC 13B .1633. The next semi-annual event is tentatively scheduled for 2017. 8 | P a g e FIGURES 9 | P a g e TABLES Location Phase Gradient Current Use Zone Monitored Laboratory Analysis MW-1 Phase 1 Up Background Shallow N/A MW-2 Phase 1 Down Compliance Shallow N/A MW-3r Phase 1 Down Compliance Shallow Appendix I + MW-4a Phase 1 Up Background Shallow N/A MW-5 Phase 1 Down Compliance Shallow Appendix I + MW-5a Phase 1 Down Compliance Deep N/A MW-6 Phase 1 Up Background Shallow Appendix I + MW-7 Phase 1 Cross Compliance Shallow N/A MW-8 Phase 1 Down Compliance Shallow Appendix I + MW-9 Phase 1 Down Compliance Shallow N/A MW-9a Phase 1 Down Compliance Shallow Appendix I + MW-9b Phase 1 Down Compliance Deep N/A MW-10 Phase 1 Down Compliance Shallow Appendix I MW-11 Phase 1 Down Compliance Shallow Appendix I MW-12 Phase 2 Up Background Shallow Appendix I MW-13r Phase 2 Down Compliance Shallow Appendix I MW-14 Phase 2 Down Compliance Shallow Appendix I MW-15 Phase 2 Down Compliance Shallow Appendix I MW-16 Phase 2 Down Compliance Shallow Appendix I MW-17r Phase 2 Down Compliance Shallow Appendix I MW-18 Phase 2 Down Compliance Shallow Appendix I MW-19 C & D Down Not used Shallow Metals & VOC MW-20 C & D Down Not used Shallow Metals & VOC MW-21 Phase 3 Down Compliance Shallow Appendix I MW-22 Phase 3 Down Compliance Shallow Appendix I MW-23 Phase 3 Cross Compliance Shallow Appendix I MW-24R Phase 4 Cross Compliance Shallow Appendix I MW-25R Phase 4 Down Compliance Shallow Appendix I MW-26 Phase 4 Up Compliance Shallow Appendix I Notes: Appendix 1 = Appendix I constituents were analyzed. N/A = Not Analyzed Table 1 Groundwater Monitoring Program Monitoring wells MW-1, MW-2, MW-4a, MW-5a, MW-7, MW-9, and MW-9b were not analyzed per GNRA's request approved by NCDENR on July 14, 2000. Appendix 1 + = Appendix I plus previously detected Appendix II constituents were analyzed. Well TOC Elevation (ft) DTW (ft) WTE (ft) Hyd Cond* Porosity** (%) Gradient** * (ft/ft) Velocity**** (ft/day)(ft/year) MW-1 151.14 nm NA 0.877 0.18 0.005 NA NA MW-2 136.53 nm NA 0.822 0.16 0.005 NA NA MW-4a 153.02 nm NA 0.959 0.18 0.005 NA NA MW-7 155.89 nm NA 0.493 0.16 0.005 NA NA MW-9 131.18 nm NA 0.466 0.20 0.005 NA NA MW-9a 131.60 4.31 127.29 9.589 0.18 0.005 0.250 91.39 MW-16 149.64 15.80 133.84 8.506 0.18 0.005 0.222 81.07 MW-20 139.88 8.37 131.51 7.140 0.18 0.005 0.186 68.05 MW-8 131.01 4.81 126.20 5.479 0.20 0.005 0.129 47.00 MW-6 150.73 9.15 141.58 2.000 0.15 0.005 0.063 22.87 MW-12 157.79 16.45 141.34 2.041 0.18 0.005 0.053 19.45 MW-11 135.30 6.55 128.75 0.874 0.16 0.005 0.026 9.37 MW-10 133.33 5.25 128.08 0.603 0.18 0.005 0.016 5.75 MW-17r 150.31 12.35 137.96 0.257 0.15 0.005 0.008 2.94 MW-14 156.11 19.16 136.95 0.271 0.18 0.005 0.007 2.58 MW-18 151.17 13.55 137.62 0.246 0.18 0.005 0.006 2.34 MW-13r 154.98 18.74 136.24 0.237 0.18 0.005 0.006 2.26 MW-15a 151.91 16.00 135.91 0.183 0.16 0.005 0.005 1.96 MW-3r 137.38 9.85 127.53 0.142 0.20 0.005 0.0033 1.22 MW-21 150.88 14.00 136.88 0.065 0.18 0.005 0.002 0.62 MW-22 152.28 15.62 136.66 0.057 0.18 0.005 0.001 0.54 MW-26 154.59 13.61 140.98 0.05 0.18 0.005 0.00131 0.48 MW-5 130.50 3.48 127.02 0.036 0.18 0.005 0.0009 0.34 MW-23 151.75 12.31 139.44 0.028 0.18 0.005 0.001 0.27 MW- 154.25 15.85 138.40 0.025 0.18 0.005 0.00065 0.24 MW-19 146.95 14.88 132.07 0.020 0.18 0.005 0.001 0.19 MW-24 154.58 13.58 141.00 0.019 0.18 0.005 0.00049 0.18 Notes TOC = Top of casing elevation NA = not available DTW = Depth to Water from TOC nm = not measured WTE = Water Table Elevation ft = feet Hyd Cond = Hydraulic Conductivity % = percent * Hydraulic Conductivity values from previous slug tests ** Effective Porosity from Groundwater & Wells (Driscoll, 1986) ***Average gradient for the October 2011 sampling event ****Velocity calculated by HEA using V=KI/n where V = Ground water velocity K = Hydraulic conductivity I = Ground water gradient n = Effective porosity Table 2 Ground Water Elevations & Flow Velocities M W - 3 R M W - 5 M W - 6 M W - 8 M W - 9 A M W - 1 0 M W - 1 1 M W - 1 2 M W - 1 3 R M W - 1 4 M W - 1 5 M W - 1 6 M W - 1 7 R M W - 1 8 M W - 1 9 M W - 2 0 M W - 2 1 R M W - 2 2 M W - 2 3 M W - 2 4 R M W - 2 5 R M W - 2 6 S W - 1 S W - 2 L E A C H A T E P H A S E 2 L E A C H A T E P H A S E 3 L E A C H A T E P H A S E 4 Analyte Solid Waste Selection Limits Alkalinity BDL BDL NM Dissolved Solids 570 61 NM Phosphorus,Total NM 0.332 0.824 1.3 Cod NM 418 634 1420 Bod NM 15 17.9 69 Barium 0.1 0.0849 0.015 0.012 0.0621 0.0868 0.0532 0.0439 0.0927 0.159 0.181 0.0669 0.144 0.137 0.122 0.512 0.105 0.029 0.0612 0.0115 0.0362 0.0219 0.0401 0.109 NM 0.32 0.218 0.147 Chromium 0.01 0.0101 BDL BDL BDL BDL 0.0122 BDL BDL BDL BDL BDL BDL 0.0116 BDL 0.0962 BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0149 0.0194 BDL Cobalt 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.017 BDL BDL BDL 0.0112 BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Nickel 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0262 BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0187 0.0574 0.132 Silver 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Vanadium 0.025 0.0253 BDL BDL BDL BDL 0.0215 BDL 0.0228 BDL BDL BDL BDL 0.0237 BDL 0.154 BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0233 0.0401 BDL Antimony 0.006 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Arsenic 0.01 0.0021 BDL BDL 0.0028 BDL BDL 0.0024 BDL BDL BDL 0.0025 0.0141 BDL BDL 0.0138 BDL 0.0034 BDL BDL BDL 0.0026 BDL 0.0027 NM 0.0196 0.0366 0.125 Beryllium 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Cadmium 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Copper 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0261 BDL 0.0065 BDL BDL BDL BDL BDL BDL NM 0.0597 1.49 BDL Lead 0.01 0.0046 BDL BDL 0.0085 BDL 0.0076 0.0029 0.004 0.0034 BDL BDL BDL 0.0086 0.0034 0.0878 0.0102 0.0025 BDL BDL BDL BDL BDL BDL NM 0.0061 0.212 BDL Selenium 0.01 0.0463 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0073 BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Thallium 0.0055 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Zinc 0.01 BDL BDL BDL BDL BDL 0.0274 0.0347 BDL BDL BDL BDL BDL BDL BDL 0.114 BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0401 0.369 BDL Acetone 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.104 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Acrylonitrile 0.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Benzene 0.001 BDL BDL BDL BDL 0.0014 BDL BDL BDL 0.0019 BDL 0.0017 0.00145 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0069 0.0051 0.0096 Bromochloromethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Bromodichloromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Bromoform 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Bromomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Carbon Disulfide 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Carbon Tetrachloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Chlorobenzene 0.003 BDL 0.0018 BDL BDL 0.002 BDL BDL BDL BDL BDL 0.0029 0.00162 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0023 0.0027 BDL Chlorodibromomethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Chloroethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0105 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Chloroform 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Chloromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Dibromomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,2-Dichlorobenzene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,4-Dichlorobenzene 0.001 BDL 0.0050 BDL 0.0029 0.0095 BDL BDL BDL 0.0025 BDL 0.0081 0.002 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM 0.016 0.0101 0.0038 Trans-1,4-Dichloro-2-Butene 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Project Sample ID Table 3 Analytical Results 1,1-Dichloroethane 0.005 0.0022 0.0036 BDL 0.0042 0.0104 BDL BDL BDL BDL BDL 0.003 0.00115 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,2-Dichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,1-Dichloroethene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Cis-1,2-Dichloroethene 0.005 BDL 0.0017 BDL BDL 0.0016 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Trans-1,2-Dichloroethene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,2-Dichloropropane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Cis-1,3-Dichloropropene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Trans-1,3-Dichloropropene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Ethylbenzene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL 0.0061 0.009 2-Hexanone 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Iodomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 2-Butanone (Mek)0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Methylene Chloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 4-Methyl-2-Pentanone (Mibk)0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Styrene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,1,1,2-Tetrachloroethane 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,1,2,2-Tetrachloroethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Tetrachloroethene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0012 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Toluene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,1,1-Trichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,1,2-Trichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Trichloroethene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Trichlorofluoromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL 1,2,3-Trichloropropane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Vinyl Acetate 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Vinyl Chloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL Xylenes, Total 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM 0.02 0.0381 0.0217 Chloride 9.61 5.23 NM Nitrate 10 NM BDL 0.151 BDL Sulfate 250 BDL 7.35 NM BDL 62.1 16.4 Notes:BDL = Below Detection Limit * All units mg/L NM - Not Measured / Well Dry at Time of Sampling Location Parameter Detected Concentration Detection Limit Units %ND Test Statistically Significant? Above 2L/MCL MW-3R Chromium 0.010 <0.0100 mg/L 0%NPPL Y Y MW-3R Vanadium 0.025 <0.0200 mg/L 49.09%NPPL N Y MW-3R Selenium 0.046 <0.00200 mg/L 56.20%NPPL Y Y MW-5 1,4-Dichlorobenzene 0.0050 <0.00100 mg/L 58.86%NPPL N N MW-8 1,4-Dichlorobenzene 0.003 <0.00100 mg/L 58.86%NPPL N N MW-9A Benzene 0.001 <0.00100 mg/L 61.43%NPPL N Y MW-9A 1,4-Dichlorobenzene 0.0095 <0.00100 mg/L 58.86%NPPL Y Y MW-9A 1,1-Dichloroethane 0.010 <0.00100 mg/L 40.10%NPPL Y Y MW-10 Chromium 0.012 <0.0100 mg/L 0%NPPL Y Y MW-10 Zinc 0.027 <0.0250 mg/L 42.86%NPPL N N MW-11 Zinc 0.035 <0.0250 mg/L 42.86%NPPL N N MW-12 Barium 0.11 <0.00500 mg/L 49.61%NPPL N N MW-13R Barium 0.159 <0.00500 mg/L 49.61%NPPL N N MW-13R Benzene 0.00189 <0.00100 mg/L 61.43%NPPL N Y MW-13R 1,4-Dichlorobenzene 0.002 <0.00100 mg/L 58.86%NPPL N N MW-14 Barium 0.181 <0.00500 mg/L 49.61%NPPL N N MW-15 Benzene 0.002 <0.00100 mg/L 61.43%NPPL N Y MW-15 Acetone 0.104 <0.05 mg/L 67.02%NPPL Y N MW-15 1,4-Dichlorobenzene 0.008 <0.00100 mg/L 58.86%NPPL Y Y MW-16 Barium 0.144 <0.00500 mg/L 49.61%NPPL N N MW-16 Benzene 0.001 <0.0100 mg/L 61.43%NPPL N Y MW-16 Arsenic 0.014 <0.002 mg/L 52.26%NPPL Y Y MW-16 Chloroethane 0.011 <0.005 mg/L 54.07%NPPL Y N MW-16 1,4-Dichlorobenzene 0.002 <0.00100 mg/L 58.86%NPPL N N MW-17R Barium 0.137 <0.00500 mg/L 49.61%NPPL N N MW-17R Chromium 0.012 <0.0100 mg/L 0%NPPL Y Y MW-17R Cobalt 0.017 <0.0100 mg/L 52.84%NPPL Y Y MW-17R Tetrachloroethene 0.001 <0.00100 mg/L 43.13%NPPL N N MW-17R Trichloroethene 0.001 <0.00100 mg/L 66.08%NPPL N N MW-18 Barium 0.122 <0.00500 mg/L 49.61%NPPL N N MW-19 Barium 0.512 <0.00500 mg/L 49.61%NPPL N N MW-19 Chromium 0.096 <0.0100 mg/L 0%NPPL N Y MW-19 Vanadium 0.154 <0.0200 mg/L 49.09%NPPL N Y MW-19 Arsenic 0.014 <0.002 mg/L 52.26%NPPL N Y MW-19 Copper 0.026 <0.005 mg/L 52.34%NPPL N N MW-19 Lead 0.088 <0.00200 mg/L 46.04%NPPL N Y MW-19 Zinc 0.114 <0.0250 mg/L 42.86%NPPL N N MW-20 Barium 0.105 <0.00500 mg/L 49.61%NPPL N N MW-20 Lead 0.010 <0.00200 mg/L 46.04%NPPL N N MW-21R Cobalt 0.011 <0.0100 mg/L 52.84%NPPL Y Y Notes: MW-1 (historical data only), MW-6 and MW-12 were used as background wells. Wells not listed did not have any detected constituents. % ND = percent non-detect NPPL = Non-Parametric Prediction Limit (Inter-Well) mg/L = milligrams per Liter NA = Not available Table 4 Statistical Analysis Summary APPENDIX A: LABORATORY ANALYTIC RESULTS ANALYTICAL REPORT December 09, 2016 Hunt Environmental Associates Sample Delivery Group:L875822 Samples Received:12/02/2016 Project Number:14-011550 Description:Robeson Co Solid Waste Semi-Annual Env Monitoring Report To:Cody Hunt 1730 Rennert Road Lumberton, NC 28360 Entire Report Reviewed By: December 09, 2016 [Preliminary Report] Jimmy Hunt Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com December 12, 2016 Jimmy Hunt Technical Service Representative ONE LAB. NATIONWIDE.TABLE OF CONTENTS ¹Cp: Cover Page 1 ²Tc: Table of Contents 2 ³Ss: Sample Summary 4 ⁴Cn: Case Narrative 10 ⁵Sr: Sample Results 11 MW-3R L875822-01 11 MW-5 L875822-02 13 MW-8 L875822-03 15 MW-9A L875822-04 17 MW-12 L875822-05 19 MW-13R L875822-06 21 MW-14 L875822-07 23 MW-15 L875822-08 25 MW-16 L875822-09 27 MW-17R L875822-10 29 MW-18 L875822-11 31 MW-19 L875822-12 33 MW-21R L875822-13 35 MW-22 L875822-14 37 MW-23 L875822-15 39 MW-24R L875822-16 41 MW-25R L875822-17 43 SW-1 L875822-18 45 TRIP BLANK L875822-19 47 LEACHATE PHASE 2 L875822-20 48 LEACHATE PHASE 3 L875822-21 50 LEACHATE PHASE 4 L875822-22 52 MW-10 L875822-23 54 MW-11 L875822-24 56 MW-20 L875822-25 58 MW-26 L875822-26 60 TRIP BLANK L875822-27 62 MW-6 L875822-28 63 ⁶Qc: Quality Control Summary 65 Gravimetric Analysis by Method 2540 C-2011 65 Wet Chemistry by Method 2320 B-2011 67 Wet Chemistry by Method 365.4 69 Wet Chemistry by Method 410.4 70 Wet Chemistry by Method 5210 B-2011 71 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 2 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 2 of 110 ONE LAB. NATIONWIDE.TABLE OF CONTENTS Wet Chemistry by Method 9056A 73 Metals (ICP) by Method 6010C 78 Metals (ICPMS) by Method 6020 81 Volatile Organic Compounds (GC/MS) by Method 8260B 86 ⁷Gl: Glossary of Terms 102 ⁸Al: Accreditations & Locations 103 ⁹Sc: Chain of Custody 104 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 3 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 3 of 110 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-3R L875822-01 GW 12/01/16 09:56 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 06:57 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:24 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 18:21 12/04/16 18:21 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:04 12/07/16 23:04 LRL Collected by Collected date/time Received date/time MW-5 L875822-02 GW 12/01/16 15:40 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:00 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:28 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 18:44 12/04/16 18:44 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:17 12/07/16 23:17 LRL Collected by Collected date/time Received date/time MW-8 L875822-03 GW 12/01/16 11:38 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:03 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:31 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 19:07 12/04/16 19:07 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:29 12/07/16 23:29 LRL Collected by Collected date/time Received date/time MW-9A L875822-04 GW 12/01/16 10:38 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 06:47 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:43 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:02 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 19:30 12/04/16 19:30 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:42 12/07/16 23:42 LRL Collected by Collected date/time Received date/time MW-12 L875822-05 GW 11/30/16 11:53 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:11 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:47 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:18 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 19:53 12/04/16 19:53 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:55 12/07/16 23:55 LRL Collected by Collected date/time Received date/time MW-13R L875822-06 GW 11/30/16 15:50 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:13 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:10 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 20:16 12/04/16 20:16 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:07 12/08/16 00:07 LRL 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 4 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 4 of 110 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-14 L875822-07 GW 11/30/16 16:44 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:16 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:50 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:05 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 20:39 12/04/16 20:39 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:20 12/08/16 00:20 LRL Collected by Collected date/time Received date/time MW-15 L875822-08 GW 11/30/16 17:09 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:19 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:54 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:25 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 21:02 12/04/16 21:02 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:32 12/08/16 00:32 LRL Collected by Collected date/time Received date/time MW-16 L875822-09 GW 12/01/16 08:27 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:22 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:57 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:09 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 21:25 12/04/16 21:25 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:45 12/08/16 00:45 LRL Collected by Collected date/time Received date/time MW-17R L875822-10 GW 12/01/16 08:52 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:24 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:01 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:32 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 21:48 12/04/16 21:48 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:58 12/08/16 00:58 LRL Collected by Collected date/time Received date/time MW-18 L875822-11 GW 12/01/16 09:24 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:27 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:04 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:12 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 22:11 12/04/16 22:11 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 01:10 12/08/16 01:10 LRL 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 5 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 5 of 110 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-19 L875822-12 GW 11/30/16 14:00 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG931570 1 12/02/16 21:42 12/03/16 01:42 JM Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:30 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:08 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:43 LAT Metals (ICPMS) by Method 6020 WG931509 5 12/03/16 20:55 12/05/16 15:50 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 22:35 12/04/16 22:35 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 01:22 12/08/16 01:22 LRL Wet Chemistry by Method 2320 B-2011 WG931590 1 12/05/16 08:08 12/05/16 08:08 AMC Wet Chemistry by Method 9056A WG931818 1 12/05/16 14:07 12/05/16 14:07 SAM Collected by Collected date/time Received date/time MW-21R L875822-13 GW 11/30/16 13:55 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:33 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:11 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:47 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 22:58 12/04/16 22:58 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 01:35 12/08/16 01:35 LRL Collected by Collected date/time Received date/time MW-22 L875822-14 GW 11/30/16 15:22 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:35 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:15 LAT Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:50 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 23:21 12/04/16 23:21 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 01:47 12/08/16 01:47 LRL Collected by Collected date/time Received date/time MW-23 L875822-15 GW 11/30/16 13:20 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:44 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:16 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 23:44 12/04/16 23:44 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:00 12/08/16 02:00 LRL Collected by Collected date/time Received date/time MW-24R L875822-16 GW 11/30/16 11:06 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:46 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:19 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/05/16 00:07 12/05/16 00:07 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:12 12/08/16 02:12 LRL 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 6 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 6 of 110 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-25R L875822-17 GW 11/30/16 10:30 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:49 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:23 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/05/16 00:30 12/05/16 00:30 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:25 12/08/16 02:25 LRL Collected by Collected date/time Received date/time SW-1 L875822-18 GW 12/01/16 13:17 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:52 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:26 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/05/16 00:53 12/05/16 00:53 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:37 12/08/16 02:37 LRL Collected by Collected date/time Received date/time TRIP BLANK L875822-19 GW 12/01/16 00:00 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 17:58 12/04/16 17:58 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 22:39 12/07/16 22:39 LRL Collected by Collected date/time Received date/time LEACHATE PHASE 2 L875822-20 GW 12/01/16 14:30 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:55 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:30 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/05/16 01:16 12/05/16 01:16 BMB Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:49 12/08/16 02:49 LRL Wet Chemistry by Method 365.4 WG932178 1 12/06/16 11:35 12/07/16 14:25 JER Wet Chemistry by Method 410.4 WG931630 1 12/02/16 17:59 12/02/16 20:28 MZ Wet Chemistry by Method 5210 B-2011 WG931445 1 12/02/16 15:20 12/07/16 10:31 ARM Wet Chemistry by Method 9056A WG931491 1 12/03/16 01:35 12/03/16 01:35 SAM Collected by Collected date/time Received date/time LEACHATE PHASE 3 L875822-21 GW 12/01/16 14:40 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:57 LTB Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:33 LAT Metals (ICPMS) by Method 6020 WG931509 5 12/03/16 20:55 12/05/16 15:54 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG931684 1 12/04/16 17:48 12/04/16 17:48 JAH Wet Chemistry by Method 365.4 WG932178 1 12/06/16 11:35 12/07/16 14:26 JER Wet Chemistry by Method 410.4 WG931630 1 12/02/16 17:59 12/02/16 20:28 MZ Wet Chemistry by Method 5210 B-2011 WG931445 1 12/02/16 15:24 12/07/16 10:34 ARM Wet Chemistry by Method 9056A WG931491 1 12/03/16 01:50 12/03/16 01:50 SAM 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 7 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 7 of 110 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time LEACHATE PHASE 4 L875822-22 GW 12/01/16 14:52 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG931720 9 12/03/16 08:33 12/05/16 08:56 LTB Metals (ICPMS) by Method 6020 WG931723 9 12/05/16 17:50 12/06/16 11:05 LAT Metals (ICPMS) by Method 6020 WG932463 9 12/06/16 13:39 12/06/16 19:59 VSS Volatile Organic Compounds (GC/MS) by Method 8260B WG931684 1 12/04/16 19:13 12/04/16 19:13 JAH Wet Chemistry by Method 365.4 WG932178 1 12/06/16 11:35 12/07/16 14:28 JER Wet Chemistry by Method 410.4 WG931630 25 12/02/16 17:59 12/02/16 20:29 MZ Wet Chemistry by Method 5210 B-2011 WG931445 10 12/02/16 15:28 12/07/16 10:37 ARM Wet Chemistry by Method 9056A WG931491 1 12/03/16 02:04 12/03/16 02:04 SAM Collected by Collected date/time Received date/time MW-10 L875822-23 GW 12/02/16 09:46 12/03/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 16:09 CCE Metals (ICPMS) by Method 6020 WG932285 1 12/06/16 09:07 12/07/16 01:42 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/08/16 01:54 12/08/16 01:54 DAH Collected by Collected date/time Received date/time MW-11 L875822-24 GW 12/02/16 09:20 12/03/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 16:16 CCE Metals (ICPMS) by Method 6020 WG932285 1 12/06/16 09:07 12/07/16 01:46 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/08/16 02:25 12/08/16 02:25 DAH Collected by Collected date/time Received date/time MW-20 L875822-25 GW 12/02/16 08:45 12/03/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG932797 1 12/08/16 09:45 12/08/16 10:32 MMF Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 16:19 CCE Metals (ICPMS) by Method 6020 WG932285 1 12/06/16 09:07 12/07/16 01:49 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/09/16 17:32 12/09/16 17:32 DN Wet Chemistry by Method 2320 B-2011 WG932588 1 12/07/16 11:57 12/07/16 11:57 AMC Wet Chemistry by Method 9056A WG932605 1 12/07/16 10:38 12/07/16 10:38 SAM Collected by Collected date/time Received date/time MW-26 L875822-26 GW 12/02/16 08:15 12/03/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 15:22 CCE Metals (ICPMS) by Method 6020 WG932285 1 12/06/16 09:07 12/07/16 01:53 LAT Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/08/16 02:57 12/08/16 02:57 ACG Collected by Collected date/time Received date/time TRIP BLANK L875822-27 GW 12/01/16 00:00 12/02/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/08/16 13:39 12/08/16 13:39 DAH 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 8 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 8 of 110 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-6 L875822-28 GW 12/05/16 14:21 12/06/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 16:22 CCE Metals (ICPMS) by Method 6020 WG932780 1 12/07/16 15:39 12/07/16 18:25 VSS Volatile Organic Compounds (GC/MS) by Method 8260B WG933189 1 12/09/16 13:28 12/09/16 13:28 DWR Volatile Organic Compounds (GC/MS) by Method 8260B WG933189 1 12/09/16 16:09 12/09/16 16:09 DWR 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 9 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 9 of 110 ONE LAB. NATIONWIDE.CASE NARRATIVE All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] Jimmy Hunt Technical Service Representative Sample Handling and Receiving The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample. ESC Sample ID Project Sample ID Method L875822-22 LEACHATE PHASE 4 6010C, 6020 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 10 of 110 Jimmy Hunt Technical Service Representative ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 10 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L875822 MW-3R Collected date/time: 12/01/16 09:56 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0849 0.00500 1 12/06/2016 06:57 WG931506 Chromium 0.0101 0.0100 1 12/06/2016 06:57 WG931506 Cobalt ND 0.0100 1 12/06/2016 06:57 WG931506 Nickel ND 0.0100 1 12/06/2016 06:57 WG931506 Silver ND 0.00500 1 12/06/2016 06:57 WG931506 Vanadium 0.0253 0.0200 1 12/06/2016 06:57 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 11:24 WG931509 Arsenic 0.00214 0.00200 1 12/05/2016 11:24 WG931509 Beryllium ND 0.00200 1 12/05/2016 11:24 WG931509 Cadmium ND 0.00100 1 12/05/2016 11:24 WG931509 Copper ND 0.00500 1 12/05/2016 11:24 WG931509 Lead 0.00459 0.00200 1 12/05/2016 11:24 WG931509 Selenium 0.0463 0.00200 1 12/05/2016 11:24 WG931509 Thallium ND 0.00200 1 12/05/2016 11:24 WG931509 Zinc ND 0.0250 1 12/05/2016 11:24 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 18:21 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 18:21 WG931552 Benzene ND 0.00100 1 12/04/2016 18:21 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 18:21 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 18:21 WG931552 Bromoform ND 0.00100 1 12/04/2016 18:21 WG931552 Bromomethane ND 0.00500 1 12/04/2016 18:21 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 18:21 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 18:21 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 18:21 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 18:21 WG931552 Chloroethane ND 0.00500 1 12/04/2016 18:21 WG931552 Chloroform ND 0.00500 1 12/04/2016 18:21 WG931552 Chloromethane ND 0.00250 1 12/04/2016 18:21 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 18:21 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 18:21 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 18:21 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 18:21 WG931552 1,1-Dichloroethane 0.00217 0.00100 1 12/04/2016 18:21 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 18:21 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 18:21 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 18:21 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 18:21 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 18:21 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 18:21 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 18:21 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 18:21 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 18:21 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 18:21 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 18:21 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 18:21 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 18:21 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 11 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 11 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L875822 MW-3R Collected date/time: 12/01/16 09:56 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 18:21 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 18:21 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 18:21 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 18:21 WG931552 Toluene ND 0.00500 1 12/04/2016 18:21 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 18:21 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 18:21 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 18:21 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 18:21 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 18:21 WG931552 Vinyl acetate ND 0.0100 1 12/07/2016 23:04 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 18:21 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 18:21 WG931552 (S) Toluene-d8 103 90.0-115 12/04/2016 18:21 WG931552 (S) Toluene-d8 100 90.0-115 12/07/2016 23:04 WG931552 (S) Dibromofluoromethane 87.5 79.0-121 12/07/2016 23:04 WG931552 (S) Dibromofluoromethane 100 79.0-121 12/04/2016 18:21 WG931552 (S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 18:21 WG931552 (S) a,a,a-Trifluorotoluene 101 90.4-116 12/07/2016 23:04 WG931552 (S) 4-Bromofluorobenzene 99.7 80.1-120 12/07/2016 23:04 WG931552 (S) 4-Bromofluorobenzene 103 80.1-120 12/04/2016 18:21 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 12 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 12 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L875822 MW-5 Collected date/time: 12/01/16 15:40 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0154 0.00500 1 12/06/2016 07:00 WG931506 Chromium ND 0.0100 1 12/06/2016 07:00 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:00 WG931506 Nickel ND 0.0100 1 12/06/2016 07:00 WG931506 Silver ND 0.00500 1 12/06/2016 07:00 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:00 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 11:28 WG931509 Arsenic ND 0.00200 1 12/05/2016 11:28 WG931509 Beryllium ND 0.00200 1 12/05/2016 11:28 WG931509 Cadmium ND 0.00100 1 12/05/2016 11:28 WG931509 Copper ND 0.00500 1 12/05/2016 11:28 WG931509 Lead ND 0.00200 1 12/05/2016 11:28 WG931509 Selenium ND 0.00200 1 12/05/2016 11:28 WG931509 Thallium ND 0.00200 1 12/05/2016 11:28 WG931509 Zinc ND 0.0250 1 12/05/2016 11:28 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 18:44 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 18:44 WG931552 Benzene ND 0.00100 1 12/04/2016 18:44 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 18:44 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 18:44 WG931552 Bromoform ND 0.00100 1 12/04/2016 18:44 WG931552 Bromomethane ND 0.00500 1 12/04/2016 18:44 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 18:44 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 18:44 WG931552 Chlorobenzene 0.00184 0.00100 1 12/04/2016 18:44 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 18:44 WG931552 Chloroethane ND 0.00500 1 12/04/2016 18:44 WG931552 Chloroform ND 0.00500 1 12/04/2016 18:44 WG931552 Chloromethane ND 0.00250 1 12/04/2016 18:44 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 18:44 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 18:44 WG931552 1,4-Dichlorobenzene 0.00499 0.00100 1 12/04/2016 18:44 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 18:44 WG931552 1,1-Dichloroethane 0.00359 0.00100 1 12/04/2016 18:44 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 18:44 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 18:44 WG931552 cis-1,2-Dichloroethene 0.00174 0.00100 1 12/04/2016 18:44 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 18:44 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 18:44 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 18:44 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 18:44 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 18:44 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 18:44 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 18:44 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 18:44 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 18:44 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 18:44 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 13 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 13 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L875822 MW-5 Collected date/time: 12/01/16 15:40 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 18:44 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 18:44 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 18:44 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 18:44 WG931552 Toluene ND 0.00500 1 12/04/2016 18:44 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 18:44 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 18:44 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 18:44 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 18:44 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 18:44 WG931552 Vinyl acetate ND 0.0100 1 12/07/2016 23:17 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 18:44 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 18:44 WG931552 (S) Toluene-d8 102 90.0-115 12/04/2016 18:44 WG931552 (S) Toluene-d8 100 90.0-115 12/07/2016 23:17 WG931552 (S) Dibromofluoromethane 88.5 79.0-121 12/07/2016 23:17 WG931552 (S) Dibromofluoromethane 99.8 79.0-121 12/04/2016 18:44 WG931552 (S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 18:44 WG931552 (S) a,a,a-Trifluorotoluene 102 90.4-116 12/07/2016 23:17 WG931552 (S) 4-Bromofluorobenzene 99.7 80.1-120 12/07/2016 23:17 WG931552 (S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 18:44 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 14 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 14 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03 L875822 MW-8 Collected date/time: 12/01/16 11:38 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0621 0.00500 1 12/06/2016 07:03 WG931506 Chromium ND 0.0100 1 12/06/2016 07:03 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:03 WG931506 Nickel ND 0.0100 1 12/06/2016 07:03 WG931506 Silver ND 0.00500 1 12/06/2016 07:03 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:03 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 11:31 WG931509 Arsenic 0.00278 0.00200 1 12/05/2016 11:31 WG931509 Beryllium ND 0.00200 1 12/05/2016 11:31 WG931509 Cadmium ND 0.00100 1 12/05/2016 11:31 WG931509 Copper ND 0.00500 1 12/05/2016 11:31 WG931509 Lead 0.00846 0.00200 1 12/05/2016 11:31 WG931509 Selenium ND 0.00200 1 12/05/2016 11:31 WG931509 Thallium ND 0.00200 1 12/05/2016 11:31 WG931509 Zinc ND 0.0250 1 12/05/2016 11:31 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 19:07 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 19:07 WG931552 Benzene ND 0.00100 1 12/04/2016 19:07 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 19:07 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 19:07 WG931552 Bromoform ND 0.00100 1 12/04/2016 19:07 WG931552 Bromomethane ND 0.00500 1 12/04/2016 19:07 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 19:07 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 19:07 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 19:07 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 19:07 WG931552 Chloroethane ND 0.00500 1 12/04/2016 19:07 WG931552 Chloroform ND 0.00500 1 12/04/2016 19:07 WG931552 Chloromethane ND 0.00250 1 12/04/2016 19:07 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 19:07 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 19:07 WG931552 1,4-Dichlorobenzene 0.00291 0.00100 1 12/04/2016 19:07 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 19:07 WG931552 1,1-Dichloroethane 0.00417 0.00100 1 12/04/2016 19:07 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 19:07 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 19:07 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:07 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:07 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 19:07 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:07 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:07 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 19:07 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 19:07 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 19:07 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 19:07 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 19:07 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 19:07 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 15 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 15 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03 L875822 MW-8 Collected date/time: 12/01/16 11:38 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 19:07 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:07 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:07 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 19:07 WG931552 Toluene ND 0.00500 1 12/04/2016 19:07 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 19:07 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 19:07 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 19:07 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 19:07 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 19:07 WG931552 Vinyl acetate ND 0.0100 1 12/07/2016 23:29 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 19:07 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 19:07 WG931552 (S) Toluene-d8 103 90.0-115 12/04/2016 19:07 WG931552 (S) Toluene-d8 99.3 90.0-115 12/07/2016 23:29 WG931552 (S) Dibromofluoromethane 84.4 79.0-121 12/07/2016 23:29 WG931552 (S) Dibromofluoromethane 97.9 79.0-121 12/04/2016 19:07 WG931552 (S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 19:07 WG931552 (S) a,a,a-Trifluorotoluene 99.0 90.4-116 12/07/2016 23:29 WG931552 (S) 4-Bromofluorobenzene 99.2 80.1-120 12/07/2016 23:29 WG931552 (S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 19:07 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 16 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 16 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04 L875822 MW-9A Collected date/time: 12/01/16 10:38 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0868 0.00500 1 12/06/2016 06:47 WG931506 Chromium ND 0.0100 1 12/06/2016 06:47 WG931506 Cobalt ND 0.0100 1 12/06/2016 06:47 WG931506 Nickel ND 0.0100 1 12/06/2016 06:47 WG931506 Silver ND 0.00500 1 12/06/2016 06:47 WG931506 Vanadium ND 0.0200 1 12/06/2016 06:47 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 11:43 WG931509 Arsenic ND 0.00200 1 12/05/2016 11:43 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:02 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:02 WG931509 Copper ND 0.00500 1 12/05/2016 11:43 WG931509 Lead ND 0.00200 1 12/05/2016 11:43 WG931509 Selenium ND 0.00200 1 12/05/2016 11:43 WG931509 Thallium ND 0.00200 1 12/05/2016 11:43 WG931509 Zinc ND 0.0250 1 12/05/2016 11:43 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 19:30 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 19:30 WG931552 Benzene 0.00144 0.00100 1 12/04/2016 19:30 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 19:30 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 19:30 WG931552 Bromoform ND 0.00100 1 12/04/2016 19:30 WG931552 Bromomethane ND 0.00500 1 12/04/2016 19:30 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 19:30 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 19:30 WG931552 Chlorobenzene 0.00199 0.00100 1 12/04/2016 19:30 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 19:30 WG931552 Chloroethane ND 0.00500 1 12/04/2016 19:30 WG931552 Chloroform ND 0.00500 1 12/04/2016 19:30 WG931552 Chloromethane ND 0.00250 1 12/04/2016 19:30 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 19:30 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 19:30 WG931552 1,4-Dichlorobenzene 0.00951 0.00100 1 12/04/2016 19:30 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 19:30 WG931552 1,1-Dichloroethane 0.0104 0.00100 1 12/04/2016 19:30 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 19:30 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 19:30 WG931552 cis-1,2-Dichloroethene 0.00155 0.00100 1 12/04/2016 19:30 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:30 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 19:30 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:30 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:30 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 19:30 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 19:30 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 19:30 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 19:30 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 19:30 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 19:30 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 17 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 17 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04 L875822 MW-9A Collected date/time: 12/01/16 10:38 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 19:30 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:30 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:30 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 19:30 WG931552 Toluene ND 0.00500 1 12/04/2016 19:30 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 19:30 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 19:30 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 19:30 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 19:30 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 19:30 WG931552 Vinyl acetate ND 0.0100 1 12/07/2016 23:42 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 19:30 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 19:30 WG931552 (S) Toluene-d8 102 90.0-115 12/04/2016 19:30 WG931552 (S) Toluene-d8 101 90.0-115 12/07/2016 23:42 WG931552 (S) Dibromofluoromethane 87.8 79.0-121 12/07/2016 23:42 WG931552 (S) Dibromofluoromethane 99.2 79.0-121 12/04/2016 19:30 WG931552 (S) a,a,a-Trifluorotoluene 103 90.4-116 12/04/2016 19:30 WG931552 (S) a,a,a-Trifluorotoluene 102 90.4-116 12/07/2016 23:42 WG931552 (S) 4-Bromofluorobenzene 99.7 80.1-120 12/07/2016 23:42 WG931552 (S) 4-Bromofluorobenzene 106 80.1-120 12/04/2016 19:30 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 18 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 18 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05 L875822 MW-12 Collected date/time: 11/30/16 11:53 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0927 0.00500 1 12/06/2016 07:11 WG931506 Chromium ND 0.0100 1 12/06/2016 07:11 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:11 WG931506 Nickel ND 0.0100 1 12/06/2016 07:11 WG931506 Silver ND 0.00500 1 12/06/2016 07:11 WG931506 Vanadium 0.0228 0.0200 1 12/06/2016 07:11 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 11:47 WG931509 Arsenic ND 0.00200 1 12/05/2016 11:47 WG931509 Beryllium ND 0.00200 1 12/05/2016 14:18 WG931509 Cadmium ND 0.00100 1 12/05/2016 14:18 WG931509 Copper ND 0.00500 1 12/05/2016 11:47 WG931509 Lead 0.00399 0.00200 1 12/05/2016 11:47 WG931509 Selenium ND 0.00200 1 12/05/2016 11:47 WG931509 Thallium ND 0.00200 1 12/05/2016 11:47 WG931509 Zinc ND 0.0250 1 12/05/2016 11:47 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 19:53 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 19:53 WG931552 Benzene ND 0.00100 1 12/04/2016 19:53 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 19:53 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 19:53 WG931552 Bromoform ND 0.00100 1 12/04/2016 19:53 WG931552 Bromomethane ND 0.00500 1 12/04/2016 19:53 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 19:53 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 19:53 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 19:53 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 19:53 WG931552 Chloroethane ND 0.00500 1 12/04/2016 19:53 WG931552 Chloroform ND 0.00500 1 12/04/2016 19:53 WG931552 Chloromethane ND 0.00250 1 12/04/2016 19:53 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 19:53 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 19:53 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 19:53 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 19:53 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 19:53 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 19:53 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 19:53 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:53 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:53 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 19:53 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:53 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:53 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 19:53 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 19:53 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 19:53 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 19:53 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 19:53 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 19:53 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 19 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 19 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05 L875822 MW-12 Collected date/time: 11/30/16 11:53 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 19:53 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:53 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:53 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 19:53 WG931552 Toluene ND 0.00500 1 12/04/2016 19:53 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 19:53 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 19:53 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 19:53 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 19:53 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 19:53 WG931552 Vinyl acetate ND 0.0100 1 12/07/2016 23:55 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 19:53 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 19:53 WG931552 (S) Toluene-d8 102 90.0-115 12/04/2016 19:53 WG931552 (S) Toluene-d8 101 90.0-115 12/07/2016 23:55 WG931552 (S) Dibromofluoromethane 88.7 79.0-121 12/07/2016 23:55 WG931552 (S) Dibromofluoromethane 98.9 79.0-121 12/04/2016 19:53 WG931552 (S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 19:53 WG931552 (S) a,a,a-Trifluorotoluene 102 90.4-116 12/07/2016 23:55 WG931552 (S) 4-Bromofluorobenzene 101 80.1-120 12/07/2016 23:55 WG931552 (S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 19:53 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 20 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 20 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06 L875822 MW-13R Collected date/time: 11/30/16 15:50 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.159 0.00500 1 12/06/2016 07:13 WG931506 Chromium ND 0.0100 1 12/06/2016 07:13 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:13 WG931506 Nickel ND 0.0100 1 12/06/2016 07:13 WG931506 Silver ND 0.00500 1 12/06/2016 07:13 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:13 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 11:10 WG931509 Arsenic ND 0.00200 1 12/05/2016 11:10 WG931509 Beryllium ND 0.00200 1 12/05/2016 11:10 WG931509 Cadmium ND 0.00100 1 12/05/2016 11:10 WG931509 Copper ND 0.00500 1 12/05/2016 11:10 WG931509 Lead 0.00335 0.00200 1 12/05/2016 11:10 WG931509 Selenium ND 0.00200 1 12/05/2016 11:10 WG931509 Thallium ND 0.00200 1 12/05/2016 11:10 WG931509 Zinc ND 0.0250 1 12/05/2016 11:10 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 20:16 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 20:16 WG931552 Benzene 0.00189 0.00100 1 12/04/2016 20:16 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 20:16 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 20:16 WG931552 Bromoform ND 0.00100 1 12/04/2016 20:16 WG931552 Bromomethane ND 0.00500 1 12/04/2016 20:16 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 20:16 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 20:16 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 20:16 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 20:16 WG931552 Chloroethane ND 0.00500 1 12/04/2016 20:16 WG931552 Chloroform ND 0.00500 1 12/04/2016 20:16 WG931552 Chloromethane ND 0.00250 1 12/04/2016 20:16 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 20:16 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 20:16 WG931552 1,4-Dichlorobenzene 0.00249 0.00100 1 12/04/2016 20:16 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 20:16 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 20:16 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 20:16 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 20:16 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 20:16 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 20:16 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 20:16 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 20:16 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 20:16 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 20:16 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 20:16 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 20:16 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 20:16 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 20:16 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 20:16 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 21 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 21 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06 L875822 MW-13R Collected date/time: 11/30/16 15:50 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 20:16 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 20:16 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 20:16 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 20:16 WG931552 Toluene ND 0.00500 1 12/04/2016 20:16 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 20:16 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 20:16 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 20:16 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 20:16 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 20:16 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 00:07 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 20:16 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 20:16 WG931552 (S) Toluene-d8 102 90.0-115 12/04/2016 20:16 WG931552 (S) Toluene-d8 102 90.0-115 12/08/2016 00:07 WG931552 (S) Dibromofluoromethane 88.8 79.0-121 12/08/2016 00:07 WG931552 (S) Dibromofluoromethane 101 79.0-121 12/04/2016 20:16 WG931552 (S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 20:16 WG931552 (S) a,a,a-Trifluorotoluene 103 90.4-116 12/08/2016 00:07 WG931552 (S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 00:07 WG931552 (S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 20:16 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 22 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 22 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07 L875822 MW-14 Collected date/time: 11/30/16 16:44 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.181 0.00500 1 12/06/2016 07:16 WG931506 Chromium ND 0.0100 1 12/06/2016 07:16 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:16 WG931506 Nickel ND 0.0100 1 12/06/2016 07:16 WG931506 Silver ND 0.00500 1 12/06/2016 07:16 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:16 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 11:50 WG931509 Arsenic ND 0.00200 1 12/05/2016 11:50 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:05 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:05 WG931509 Copper ND 0.00500 1 12/05/2016 11:50 WG931509 Lead ND 0.00200 1 12/05/2016 11:50 WG931509 Selenium ND 0.00200 1 12/05/2016 11:50 WG931509 Thallium ND 0.00200 1 12/05/2016 11:50 WG931509 Zinc ND 0.0250 1 12/05/2016 11:50 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 20:39 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 20:39 WG931552 Benzene ND 0.00100 1 12/04/2016 20:39 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 20:39 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 20:39 WG931552 Bromoform ND 0.00100 1 12/04/2016 20:39 WG931552 Bromomethane ND 0.00500 1 12/04/2016 20:39 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 20:39 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 20:39 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 20:39 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 20:39 WG931552 Chloroethane ND 0.00500 1 12/04/2016 20:39 WG931552 Chloroform ND 0.00500 1 12/04/2016 20:39 WG931552 Chloromethane ND 0.00250 1 12/04/2016 20:39 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 20:39 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 20:39 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 20:39 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 20:39 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 20:39 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 20:39 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 20:39 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 20:39 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 20:39 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 20:39 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 20:39 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 20:39 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 20:39 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 20:39 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 20:39 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 20:39 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 20:39 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 20:39 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 23 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 23 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07 L875822 MW-14 Collected date/time: 11/30/16 16:44 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 20:39 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 20:39 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 20:39 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 20:39 WG931552 Toluene ND 0.00500 1 12/04/2016 20:39 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 20:39 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 20:39 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 20:39 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 20:39 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 20:39 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 00:20 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 20:39 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 20:39 WG931552 (S) Toluene-d8 103 90.0-115 12/04/2016 20:39 WG931552 (S) Toluene-d8 101 90.0-115 12/08/2016 00:20 WG931552 (S) Dibromofluoromethane 89.9 79.0-121 12/08/2016 00:20 WG931552 (S) Dibromofluoromethane 100 79.0-121 12/04/2016 20:39 WG931552 (S) a,a,a-Trifluorotoluene 106 90.4-116 12/04/2016 20:39 WG931552 (S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 00:20 WG931552 (S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 00:20 WG931552 (S) 4-Bromofluorobenzene 103 80.1-120 12/04/2016 20:39 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 24 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 24 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08 L875822 MW-15 Collected date/time: 11/30/16 17:09 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0669 0.00500 1 12/06/2016 07:19 WG931506 Chromium ND 0.0100 1 12/06/2016 07:19 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:19 WG931506 Nickel ND 0.0100 1 12/06/2016 07:19 WG931506 Silver ND 0.00500 1 12/06/2016 07:19 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:19 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 11:54 WG931509 Arsenic 0.00251 0.00200 1 12/05/2016 11:54 WG931509 Beryllium ND 0.00200 1 12/05/2016 14:25 WG931509 Cadmium ND 0.00100 1 12/05/2016 14:25 WG931509 Copper ND 0.00500 1 12/05/2016 11:54 WG931509 Lead ND 0.00200 1 12/05/2016 11:54 WG931509 Selenium ND 0.00200 1 12/05/2016 11:54 WG931509 Thallium ND 0.00200 1 12/05/2016 11:54 WG931509 Zinc ND 0.0250 1 12/05/2016 11:54 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone 0.104 0.0500 1 12/04/2016 21:02 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 21:02 WG931552 Benzene 0.00174 0.00100 1 12/04/2016 21:02 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 21:02 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 21:02 WG931552 Bromoform ND 0.00100 1 12/04/2016 21:02 WG931552 Bromomethane ND 0.00500 1 12/04/2016 21:02 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 21:02 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 21:02 WG931552 Chlorobenzene 0.00286 0.00100 1 12/04/2016 21:02 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 21:02 WG931552 Chloroethane ND 0.00500 1 12/04/2016 21:02 WG931552 Chloroform ND 0.00500 1 12/04/2016 21:02 WG931552 Chloromethane ND 0.00250 1 12/04/2016 21:02 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 21:02 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 21:02 WG931552 1,4-Dichlorobenzene 0.00813 0.00100 1 12/04/2016 21:02 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 21:02 WG931552 1,1-Dichloroethane 0.00303 0.00100 1 12/04/2016 21:02 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 21:02 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 21:02 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:02 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:02 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 21:02 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:02 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:02 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 21:02 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 21:02 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 21:02 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 21:02 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 21:02 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 21:02 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 25 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 25 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08 L875822 MW-15 Collected date/time: 11/30/16 17:09 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 21:02 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:02 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:02 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 21:02 WG931552 Toluene ND 0.00500 1 12/04/2016 21:02 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 21:02 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 21:02 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 21:02 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 21:02 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 21:02 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 00:32 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 21:02 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 21:02 WG931552 (S) Toluene-d8 102 90.0-115 12/04/2016 21:02 WG931552 (S) Toluene-d8 101 90.0-115 12/08/2016 00:32 WG931552 (S) Dibromofluoromethane 87.9 79.0-121 12/08/2016 00:32 WG931552 (S) Dibromofluoromethane 99.0 79.0-121 12/04/2016 21:02 WG931552 (S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 21:02 WG931552 (S) a,a,a-Trifluorotoluene 102 90.4-116 12/08/2016 00:32 WG931552 (S) 4-Bromofluorobenzene 99.3 80.1-120 12/08/2016 00:32 WG931552 (S) 4-Bromofluorobenzene 103 80.1-120 12/04/2016 21:02 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 26 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 26 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09 L875822 MW-16 Collected date/time: 12/01/16 08:27 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.144 0.00500 1 12/06/2016 07:22 WG931506 Chromium ND 0.0100 1 12/06/2016 07:22 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:22 WG931506 Nickel ND 0.0100 1 12/06/2016 07:22 WG931506 Silver ND 0.00500 1 12/06/2016 07:22 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:22 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 11:57 WG931509 Arsenic 0.0141 0.00200 1 12/05/2016 11:57 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:09 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:09 WG931509 Copper ND 0.00500 1 12/05/2016 11:57 WG931509 Lead ND 0.00200 1 12/05/2016 11:57 WG931509 Selenium ND 0.00200 1 12/05/2016 11:57 WG931509 Thallium ND 0.00200 1 12/05/2016 11:57 WG931509 Zinc ND 0.0250 1 12/05/2016 11:57 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 21:25 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 21:25 WG931552 Benzene 0.00145 0.00100 1 12/04/2016 21:25 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 21:25 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 21:25 WG931552 Bromoform ND 0.00100 1 12/04/2016 21:25 WG931552 Bromomethane ND 0.00500 1 12/04/2016 21:25 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 21:25 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 21:25 WG931552 Chlorobenzene 0.00162 0.00100 1 12/04/2016 21:25 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 21:25 WG931552 Chloroethane 0.0105 0.00500 1 12/04/2016 21:25 WG931552 Chloroform ND 0.00500 1 12/04/2016 21:25 WG931552 Chloromethane ND 0.00250 1 12/04/2016 21:25 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 21:25 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 21:25 WG931552 1,4-Dichlorobenzene 0.00200 0.00100 1 12/04/2016 21:25 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 21:25 WG931552 1,1-Dichloroethane 0.00115 0.00100 1 12/04/2016 21:25 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 21:25 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 21:25 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:25 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:25 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 21:25 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:25 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:25 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 21:25 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 21:25 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 21:25 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 21:25 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 21:25 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 21:25 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 27 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 27 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09 L875822 MW-16 Collected date/time: 12/01/16 08:27 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 21:25 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:25 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:25 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 21:25 WG931552 Toluene ND 0.00500 1 12/04/2016 21:25 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 21:25 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 21:25 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 21:25 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 21:25 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 21:25 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 00:45 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 21:25 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 21:25 WG931552 (S) Toluene-d8 103 90.0-115 12/04/2016 21:25 WG931552 (S) Toluene-d8 100 90.0-115 12/08/2016 00:45 WG931552 (S) Dibromofluoromethane 88.7 79.0-121 12/08/2016 00:45 WG931552 (S) Dibromofluoromethane 99.8 79.0-121 12/04/2016 21:25 WG931552 (S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 21:25 WG931552 (S) a,a,a-Trifluorotoluene 102 90.4-116 12/08/2016 00:45 WG931552 (S) 4-Bromofluorobenzene 101 80.1-120 12/08/2016 00:45 WG931552 (S) 4-Bromofluorobenzene 102 80.1-120 12/04/2016 21:25 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 28 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 28 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10 L875822 MW-17R Collected date/time: 12/01/16 08:52 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.137 0.00500 1 12/06/2016 07:24 WG931506 Chromium 0.0116 0.0100 1 12/06/2016 07:24 WG931506 Cobalt 0.0170 0.0100 1 12/06/2016 07:24 WG931506 Nickel ND 0.0100 1 12/06/2016 07:24 WG931506 Silver ND 0.00500 1 12/06/2016 07:24 WG931506 Vanadium 0.0237 0.0200 1 12/06/2016 07:24 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 12:01 WG931509 Arsenic ND 0.00200 1 12/05/2016 12:01 WG931509 Beryllium ND 0.00200 1 12/05/2016 14:32 WG931509 Cadmium ND 0.00100 1 12/05/2016 14:32 WG931509 Copper ND 0.00500 1 12/05/2016 12:01 WG931509 Lead 0.00858 0.00200 1 12/05/2016 12:01 WG931509 Selenium ND 0.00200 1 12/05/2016 12:01 WG931509 Thallium ND 0.00200 1 12/05/2016 12:01 WG931509 Zinc ND 0.0250 1 12/05/2016 12:01 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 21:48 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 21:48 WG931552 Benzene ND 0.00100 1 12/04/2016 21:48 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 21:48 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 21:48 WG931552 Bromoform ND 0.00100 1 12/04/2016 21:48 WG931552 Bromomethane ND 0.00500 1 12/04/2016 21:48 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 21:48 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 21:48 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 21:48 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 21:48 WG931552 Chloroethane ND 0.00500 1 12/04/2016 21:48 WG931552 Chloroform ND 0.00500 1 12/04/2016 21:48 WG931552 Chloromethane ND 0.00250 1 12/04/2016 21:48 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 21:48 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 21:48 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 21:48 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 21:48 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 21:48 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 21:48 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 21:48 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:48 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:48 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 21:48 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:48 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:48 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 21:48 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 21:48 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 21:48 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 21:48 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 21:48 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 21:48 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 29 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 29 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10 L875822 MW-17R Collected date/time: 12/01/16 08:52 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 21:48 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:48 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:48 WG931552 Tetrachloroethene 0.00121 0.00100 1 12/04/2016 21:48 WG931552 Toluene ND 0.00500 1 12/04/2016 21:48 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 21:48 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 21:48 WG931552 Trichloroethene 0.00102 0.00100 1 12/04/2016 21:48 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 21:48 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 21:48 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 00:58 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 21:48 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 21:48 WG931552 (S) Toluene-d8 103 90.0-115 12/04/2016 21:48 WG931552 (S) Toluene-d8 99.4 90.0-115 12/08/2016 00:58 WG931552 (S) Dibromofluoromethane 87.7 79.0-121 12/08/2016 00:58 WG931552 (S) Dibromofluoromethane 99.8 79.0-121 12/04/2016 21:48 WG931552 (S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 21:48 WG931552 (S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 00:58 WG931552 (S) 4-Bromofluorobenzene 99.7 80.1-120 12/08/2016 00:58 WG931552 (S) 4-Bromofluorobenzene 104 80.1-120 12/04/2016 21:48 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 30 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 30 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11 L875822 MW-18 Collected date/time: 12/01/16 09:24 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.122 0.00500 1 12/06/2016 07:27 WG931506 Chromium ND 0.0100 1 12/06/2016 07:27 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:27 WG931506 Nickel ND 0.0100 1 12/06/2016 07:27 WG931506 Silver ND 0.00500 1 12/06/2016 07:27 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:27 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 12:04 WG931509 Arsenic ND 0.00200 1 12/05/2016 12:04 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:12 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:12 WG931509 Copper ND 0.00500 1 12/05/2016 12:04 WG931509 Lead 0.00338 0.00200 1 12/05/2016 12:04 WG931509 Selenium ND 0.00200 1 12/05/2016 12:04 WG931509 Thallium ND 0.00200 1 12/05/2016 12:04 WG931509 Zinc ND 0.0250 1 12/05/2016 12:04 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 22:11 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 22:11 WG931552 Benzene ND 0.00100 1 12/04/2016 22:11 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 22:11 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 22:11 WG931552 Bromoform ND 0.00100 1 12/04/2016 22:11 WG931552 Bromomethane ND 0.00500 1 12/04/2016 22:11 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 22:11 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 22:11 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 22:11 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 22:11 WG931552 Chloroethane ND 0.00500 1 12/04/2016 22:11 WG931552 Chloroform ND 0.00500 1 12/04/2016 22:11 WG931552 Chloromethane ND 0.00250 1 12/04/2016 22:11 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 22:11 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 22:11 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 22:11 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 22:11 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 22:11 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 22:11 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 22:11 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:11 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:11 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 22:11 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:11 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:11 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 22:11 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 22:11 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 22:11 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 22:11 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 22:11 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 22:11 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 31 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 31 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11 L875822 MW-18 Collected date/time: 12/01/16 09:24 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 22:11 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:11 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:11 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 22:11 WG931552 Toluene ND 0.00500 1 12/04/2016 22:11 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 22:11 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 22:11 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 22:11 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 22:11 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 22:11 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 01:10 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 22:11 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 22:11 WG931552 (S) Toluene-d8 102 90.0-115 12/04/2016 22:11 WG931552 (S) Toluene-d8 99.9 90.0-115 12/08/2016 01:10 WG931552 (S) Dibromofluoromethane 87.4 79.0-121 12/08/2016 01:10 WG931552 (S) Dibromofluoromethane 98.1 79.0-121 12/04/2016 22:11 WG931552 (S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 22:11 WG931552 (S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 01:10 WG931552 (S) 4-Bromofluorobenzene 99.9 80.1-120 12/08/2016 01:10 WG931552 (S) 4-Bromofluorobenzene 103 80.1-120 12/04/2016 22:11 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 32 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 32 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12 L875822 MW-19 Collected date/time: 11/30/16 14:00 Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Dissolved Solids 570 10.0 1 12/03/2016 01:42 WG931570 Wet Chemistry by Method 2320 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Alkalinity ND 20.0 1 12/05/2016 08:08 WG931590 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Chloride 9.61 1.00 1 12/05/2016 14:07 WG931818 Sulfate ND 5.00 1 12/05/2016 14:07 WG931818 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.512 0.00500 1 12/06/2016 07:30 WG931506 Chromium 0.0962 0.0100 1 12/06/2016 07:30 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:30 WG931506 Nickel 0.0262 0.0100 1 12/06/2016 07:30 WG931506 Silver ND 0.00500 1 12/06/2016 07:30 WG931506 Vanadium 0.154 0.0200 1 12/06/2016 07:30 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 12:08 WG931509 Arsenic 0.0138 0.00200 1 12/05/2016 12:08 WG931509 Beryllium ND 0.0100 5 12/05/2016 15:50 WG931509 Cadmium ND 0.00100 1 12/05/2016 14:43 WG931509 Copper 0.0261 0.00500 1 12/05/2016 12:08 WG931509 Lead 0.0878 0.00200 1 12/05/2016 12:08 WG931509 Selenium 0.00726 0.00200 1 12/05/2016 12:08 WG931509 Thallium ND 0.00200 1 12/05/2016 12:08 WG931509 Zinc 0.114 0.0250 1 12/05/2016 12:08 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 22:35 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 22:35 WG931552 Benzene ND 0.00100 1 12/04/2016 22:35 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 22:35 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 22:35 WG931552 Bromoform ND 0.00100 1 12/04/2016 22:35 WG931552 Bromomethane ND 0.00500 1 12/04/2016 22:35 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 22:35 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 22:35 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 22:35 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 22:35 WG931552 Chloroethane ND 0.00500 1 12/04/2016 22:35 WG931552 Chloroform ND 0.00500 1 12/04/2016 22:35 WG931552 Chloromethane ND 0.00250 1 12/04/2016 22:35 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 33 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 33 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12 L875822 MW-19 Collected date/time: 11/30/16 14:00 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Dibromomethane ND 0.00100 1 12/04/2016 22:35 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 22:35 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 22:35 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 22:35 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 22:35 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 22:35 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 22:35 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:35 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:35 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 22:35 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:35 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:35 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 22:35 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 22:35 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 22:35 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 22:35 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 22:35 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 22:35 WG931552 Styrene ND 0.00100 1 12/04/2016 22:35 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:35 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:35 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 22:35 WG931552 Toluene ND 0.00500 1 12/04/2016 22:35 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 22:35 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 22:35 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 22:35 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 22:35 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 22:35 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 01:22 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 22:35 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 22:35 WG931552 (S) Toluene-d8 103 90.0-115 12/04/2016 22:35 WG931552 (S) Toluene-d8 99.5 90.0-115 12/08/2016 01:22 WG931552 (S) Dibromofluoromethane 86.7 79.0-121 12/08/2016 01:22 WG931552 (S) Dibromofluoromethane 100 79.0-121 12/04/2016 22:35 WG931552 (S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 22:35 WG931552 (S) a,a,a-Trifluorotoluene 99.9 90.4-116 12/08/2016 01:22 WG931552 (S) 4-Bromofluorobenzene 98.5 80.1-120 12/08/2016 01:22 WG931552 (S) 4-Bromofluorobenzene 102 80.1-120 12/04/2016 22:35 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 34 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 34 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13 L875822 MW-21R Collected date/time: 11/30/16 13:55 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0290 0.00500 1 12/06/2016 07:33 WG931506 Chromium ND 0.0100 1 12/06/2016 07:33 WG931506 Cobalt 0.0112 0.0100 1 12/06/2016 07:33 WG931506 Nickel ND 0.0100 1 12/06/2016 07:33 WG931506 Silver ND 0.00500 1 12/06/2016 07:33 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:33 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 12:11 WG931509 Arsenic 0.00339 0.00200 1 12/05/2016 12:11 WG931509 Beryllium ND 0.00200 1 12/05/2016 14:47 WG931509 Cadmium ND 0.00100 1 12/05/2016 14:47 WG931509 Copper 0.00648 0.00500 1 12/05/2016 12:11 WG931509 Lead 0.00249 0.00200 1 12/05/2016 12:11 WG931509 Selenium ND 0.00200 1 12/05/2016 12:11 WG931509 Thallium ND 0.00200 1 12/05/2016 12:11 WG931509 Zinc ND 0.0250 1 12/05/2016 12:11 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 22:58 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 22:58 WG931552 Benzene ND 0.00100 1 12/04/2016 22:58 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 22:58 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 22:58 WG931552 Bromoform ND 0.00100 1 12/04/2016 22:58 WG931552 Bromomethane ND 0.00500 1 12/04/2016 22:58 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 22:58 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 22:58 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 22:58 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 22:58 WG931552 Chloroethane ND 0.00500 1 12/04/2016 22:58 WG931552 Chloroform ND 0.00500 1 12/04/2016 22:58 WG931552 Chloromethane ND 0.00250 1 12/04/2016 22:58 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 22:58 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 22:58 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 22:58 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 22:58 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 22:58 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 22:58 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 22:58 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:58 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:58 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 22:58 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:58 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:58 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 22:58 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 22:58 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 22:58 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 22:58 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 22:58 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 22:58 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 35 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 35 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13 L875822 MW-21R Collected date/time: 11/30/16 13:55 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 22:58 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:58 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:58 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 22:58 WG931552 Toluene ND 0.00500 1 12/04/2016 22:58 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 22:58 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 22:58 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 22:58 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 22:58 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 22:58 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 01:35 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 22:58 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 22:58 WG931552 (S) Toluene-d8 103 90.0-115 12/04/2016 22:58 WG931552 (S) Toluene-d8 101 90.0-115 12/08/2016 01:35 WG931552 (S) Dibromofluoromethane 88.1 79.0-121 12/08/2016 01:35 WG931552 (S) Dibromofluoromethane 98.9 79.0-121 12/04/2016 22:58 WG931552 (S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 22:58 WG931552 (S) a,a,a-Trifluorotoluene 102 90.4-116 12/08/2016 01:35 WG931552 (S) 4-Bromofluorobenzene 99.6 80.1-120 12/08/2016 01:35 WG931552 (S) 4-Bromofluorobenzene 104 80.1-120 12/04/2016 22:58 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 36 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 36 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14 L875822 MW-22 Collected date/time: 11/30/16 15:22 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0612 0.00500 1 12/06/2016 07:35 WG931506 Chromium ND 0.0100 1 12/06/2016 07:35 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:35 WG931506 Nickel ND 0.0100 1 12/06/2016 07:35 WG931506 Silver ND 0.00500 1 12/06/2016 07:35 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:35 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 12:15 WG931509 Arsenic ND 0.00200 1 12/05/2016 12:15 WG931509 Beryllium ND 0.00200 1 12/05/2016 14:50 WG931509 Cadmium ND 0.00100 1 12/05/2016 14:50 WG931509 Copper ND 0.00500 1 12/05/2016 12:15 WG931509 Lead ND 0.00200 1 12/05/2016 12:15 WG931509 Selenium ND 0.00200 1 12/05/2016 12:15 WG931509 Thallium ND 0.00200 1 12/05/2016 12:15 WG931509 Zinc ND 0.0250 1 12/05/2016 12:15 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 23:21 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 23:21 WG931552 Benzene ND 0.00100 1 12/04/2016 23:21 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 23:21 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 23:21 WG931552 Bromoform ND 0.00100 1 12/04/2016 23:21 WG931552 Bromomethane ND 0.00500 1 12/04/2016 23:21 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 23:21 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 23:21 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 23:21 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 23:21 WG931552 Chloroethane ND 0.00500 1 12/04/2016 23:21 WG931552 Chloroform ND 0.00500 1 12/04/2016 23:21 WG931552 Chloromethane ND 0.00250 1 12/04/2016 23:21 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 23:21 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 23:21 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 23:21 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 23:21 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 23:21 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 23:21 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 23:21 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 23:21 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 23:21 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 23:21 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 23:21 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 23:21 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 23:21 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 23:21 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 23:21 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 23:21 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 23:21 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 23:21 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 37 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 37 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14 L875822 MW-22 Collected date/time: 11/30/16 15:22 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 23:21 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 23:21 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 23:21 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 23:21 WG931552 Toluene ND 0.00500 1 12/04/2016 23:21 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 23:21 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 23:21 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 23:21 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 23:21 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 23:21 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 01:47 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 23:21 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 23:21 WG931552 (S) Toluene-d8 103 90.0-115 12/04/2016 23:21 WG931552 (S) Toluene-d8 101 90.0-115 12/08/2016 01:47 WG931552 (S) Dibromofluoromethane 89.4 79.0-121 12/08/2016 01:47 WG931552 (S) Dibromofluoromethane 99.9 79.0-121 12/04/2016 23:21 WG931552 (S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 23:21 WG931552 (S) a,a,a-Trifluorotoluene 104 90.4-116 12/08/2016 01:47 WG931552 (S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 01:47 WG931552 (S) 4-Bromofluorobenzene 104 80.1-120 12/04/2016 23:21 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 38 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 38 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15 L875822 MW-23 Collected date/time: 11/30/16 13:20 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0115 0.00500 1 12/06/2016 07:44 WG931506 Chromium ND 0.0100 1 12/06/2016 07:44 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:44 WG931506 Nickel ND 0.0100 1 12/06/2016 07:44 WG931506 Silver ND 0.00500 1 12/06/2016 07:44 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:44 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 15:16 WG931509 Arsenic ND 0.00200 1 12/05/2016 15:16 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:16 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:16 WG931509 Copper ND 0.00500 1 12/05/2016 15:16 WG931509 Lead ND 0.00200 1 12/05/2016 15:16 WG931509 Selenium ND 0.00200 1 12/05/2016 15:16 WG931509 Thallium ND 0.00200 1 12/05/2016 15:16 WG931509 Zinc ND 0.0250 1 12/05/2016 15:16 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 23:44 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 23:44 WG931552 Benzene ND 0.00100 1 12/04/2016 23:44 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 23:44 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 23:44 WG931552 Bromoform ND 0.00100 1 12/04/2016 23:44 WG931552 Bromomethane ND 0.00500 1 12/04/2016 23:44 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 23:44 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 23:44 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 23:44 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 23:44 WG931552 Chloroethane ND 0.00500 1 12/04/2016 23:44 WG931552 Chloroform ND 0.00500 1 12/04/2016 23:44 WG931552 Chloromethane ND 0.00250 1 12/04/2016 23:44 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 23:44 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 23:44 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 23:44 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 23:44 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 23:44 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 23:44 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 23:44 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 23:44 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 23:44 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 23:44 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 23:44 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 23:44 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 23:44 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 23:44 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 23:44 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 23:44 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 23:44 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 23:44 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 39 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 39 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15 L875822 MW-23 Collected date/time: 11/30/16 13:20 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/04/2016 23:44 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 23:44 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 23:44 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 23:44 WG931552 Toluene ND 0.00500 1 12/04/2016 23:44 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 23:44 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 23:44 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 23:44 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 23:44 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 23:44 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 02:00 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 23:44 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 23:44 WG931552 (S) Toluene-d8 103 90.0-115 12/04/2016 23:44 WG931552 (S) Toluene-d8 99.5 90.0-115 12/08/2016 02:00 WG931552 (S) Dibromofluoromethane 86.5 79.0-121 12/08/2016 02:00 WG931552 (S) Dibromofluoromethane 97.9 79.0-121 12/04/2016 23:44 WG931552 (S) a,a,a-Trifluorotoluene 106 90.4-116 12/04/2016 23:44 WG931552 (S) a,a,a-Trifluorotoluene 99.7 90.4-116 12/08/2016 02:00 WG931552 (S) 4-Bromofluorobenzene 98.0 80.1-120 12/08/2016 02:00 WG931552 (S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 23:44 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 40 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 40 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16 L875822 MW-24R Collected date/time: 11/30/16 11:06 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0362 0.00500 1 12/06/2016 07:46 WG931506 Chromium ND 0.0100 1 12/06/2016 07:46 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:46 WG931506 Nickel ND 0.0100 1 12/06/2016 07:46 WG931506 Silver ND 0.00500 1 12/06/2016 07:46 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:46 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 15:19 WG931509 Arsenic ND 0.00200 1 12/05/2016 15:19 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:19 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:19 WG931509 Copper ND 0.00500 1 12/05/2016 15:19 WG931509 Lead ND 0.00200 1 12/05/2016 15:19 WG931509 Selenium ND 0.00200 1 12/05/2016 15:19 WG931509 Thallium ND 0.00200 1 12/05/2016 15:19 WG931509 Zinc ND 0.0250 1 12/05/2016 15:19 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/05/2016 00:07 WG931552 Acrylonitrile ND 0.0100 1 12/05/2016 00:07 WG931552 Benzene ND 0.00100 1 12/05/2016 00:07 WG931552 Bromochloromethane ND 0.00100 1 12/05/2016 00:07 WG931552 Bromodichloromethane ND 0.00100 1 12/05/2016 00:07 WG931552 Bromoform ND 0.00100 1 12/05/2016 00:07 WG931552 Bromomethane ND 0.00500 1 12/05/2016 00:07 WG931552 Carbon disulfide ND 0.00100 1 12/05/2016 00:07 WG931552 Carbon tetrachloride ND 0.00100 1 12/05/2016 00:07 WG931552 Chlorobenzene ND 0.00100 1 12/05/2016 00:07 WG931552 Chlorodibromomethane ND 0.00100 1 12/05/2016 00:07 WG931552 Chloroethane ND 0.00500 1 12/05/2016 00:07 WG931552 Chloroform ND 0.00500 1 12/05/2016 00:07 WG931552 Chloromethane ND 0.00250 1 12/05/2016 00:07 WG931552 Dibromomethane ND 0.00100 1 12/05/2016 00:07 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/05/2016 00:07 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/05/2016 00:07 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/05/2016 00:07 WG931552 1,1-Dichloroethane ND 0.00100 1 12/05/2016 00:07 WG931552 1,2-Dichloroethane ND 0.00100 1 12/05/2016 00:07 WG931552 1,1-Dichloroethene ND 0.00100 1 12/05/2016 00:07 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:07 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:07 WG931552 1,2-Dichloropropane ND 0.00100 1 12/05/2016 00:07 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:07 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:07 WG931552 Ethylbenzene ND 0.00100 1 12/05/2016 00:07 WG931552 2-Hexanone ND 0.0100 1 12/05/2016 00:07 WG931552 Iodomethane ND J4 0.0100 1 12/05/2016 00:07 WG931552 2-Butanone (MEK)ND 0.0100 1 12/05/2016 00:07 WG931552 Methylene Chloride ND 0.00500 1 12/05/2016 00:07 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/05/2016 00:07 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 41 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 41 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16 L875822 MW-24R Collected date/time: 11/30/16 11:06 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/05/2016 00:07 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:07 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:07 WG931552 Tetrachloroethene ND 0.00100 1 12/05/2016 00:07 WG931552 Toluene ND 0.00500 1 12/05/2016 00:07 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/05/2016 00:07 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/05/2016 00:07 WG931552 Trichloroethene ND 0.00100 1 12/05/2016 00:07 WG931552 Trichlorofluoromethane ND 0.00500 1 12/05/2016 00:07 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/05/2016 00:07 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 02:12 WG931552 Vinyl chloride ND 0.00100 1 12/05/2016 00:07 WG931552 Xylenes, Total ND 0.00300 1 12/05/2016 00:07 WG931552 (S) Toluene-d8 103 90.0-115 12/05/2016 00:07 WG931552 (S) Toluene-d8 100 90.0-115 12/08/2016 02:12 WG931552 (S) Dibromofluoromethane 89.1 79.0-121 12/08/2016 02:12 WG931552 (S) Dibromofluoromethane 98.7 79.0-121 12/05/2016 00:07 WG931552 (S) a,a,a-Trifluorotoluene 105 90.4-116 12/05/2016 00:07 WG931552 (S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 02:12 WG931552 (S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 02:12 WG931552 (S) 4-Bromofluorobenzene 103 80.1-120 12/05/2016 00:07 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 42 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 42 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17 L875822 MW-25R Collected date/time: 11/30/16 10:30 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0219 0.00500 1 12/06/2016 07:49 WG931506 Chromium ND 0.0100 1 12/06/2016 07:49 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:49 WG931506 Nickel ND 0.0100 1 12/06/2016 07:49 WG931506 Silver ND 0.00500 1 12/06/2016 07:49 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:49 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 15:23 WG931509 Arsenic 0.00264 0.00200 1 12/05/2016 15:23 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:23 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:23 WG931509 Copper ND 0.00500 1 12/05/2016 15:23 WG931509 Lead ND 0.00200 1 12/05/2016 15:23 WG931509 Selenium ND 0.00200 1 12/05/2016 15:23 WG931509 Thallium ND 0.00200 1 12/05/2016 15:23 WG931509 Zinc ND 0.0250 1 12/05/2016 15:23 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/05/2016 00:30 WG931552 Acrylonitrile ND 0.0100 1 12/05/2016 00:30 WG931552 Benzene ND 0.00100 1 12/05/2016 00:30 WG931552 Bromochloromethane ND 0.00100 1 12/05/2016 00:30 WG931552 Bromodichloromethane ND 0.00100 1 12/05/2016 00:30 WG931552 Bromoform ND 0.00100 1 12/05/2016 00:30 WG931552 Bromomethane ND 0.00500 1 12/05/2016 00:30 WG931552 Carbon disulfide ND 0.00100 1 12/05/2016 00:30 WG931552 Carbon tetrachloride ND 0.00100 1 12/05/2016 00:30 WG931552 Chlorobenzene ND 0.00100 1 12/05/2016 00:30 WG931552 Chlorodibromomethane ND 0.00100 1 12/05/2016 00:30 WG931552 Chloroethane ND 0.00500 1 12/05/2016 00:30 WG931552 Chloroform ND 0.00500 1 12/05/2016 00:30 WG931552 Chloromethane ND 0.00250 1 12/05/2016 00:30 WG931552 Dibromomethane ND 0.00100 1 12/05/2016 00:30 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/05/2016 00:30 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/05/2016 00:30 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/05/2016 00:30 WG931552 1,1-Dichloroethane ND 0.00100 1 12/05/2016 00:30 WG931552 1,2-Dichloroethane ND 0.00100 1 12/05/2016 00:30 WG931552 1,1-Dichloroethene ND 0.00100 1 12/05/2016 00:30 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:30 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:30 WG931552 1,2-Dichloropropane ND 0.00100 1 12/05/2016 00:30 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:30 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:30 WG931552 Ethylbenzene ND 0.00100 1 12/05/2016 00:30 WG931552 2-Hexanone ND 0.0100 1 12/05/2016 00:30 WG931552 Iodomethane ND J4 0.0100 1 12/05/2016 00:30 WG931552 2-Butanone (MEK)ND 0.0100 1 12/05/2016 00:30 WG931552 Methylene Chloride ND 0.00500 1 12/05/2016 00:30 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/05/2016 00:30 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 43 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 43 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17 L875822 MW-25R Collected date/time: 11/30/16 10:30 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/05/2016 00:30 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:30 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:30 WG931552 Tetrachloroethene ND 0.00100 1 12/05/2016 00:30 WG931552 Toluene ND 0.00500 1 12/05/2016 00:30 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/05/2016 00:30 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/05/2016 00:30 WG931552 Trichloroethene ND 0.00100 1 12/05/2016 00:30 WG931552 Trichlorofluoromethane ND 0.00500 1 12/05/2016 00:30 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/05/2016 00:30 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 02:25 WG931552 Vinyl chloride ND 0.00100 1 12/05/2016 00:30 WG931552 Xylenes, Total ND 0.00300 1 12/05/2016 00:30 WG931552 (S) Toluene-d8 103 90.0-115 12/05/2016 00:30 WG931552 (S) Toluene-d8 100 90.0-115 12/08/2016 02:25 WG931552 (S) Dibromofluoromethane 88.2 79.0-121 12/08/2016 02:25 WG931552 (S) Dibromofluoromethane 99.0 79.0-121 12/05/2016 00:30 WG931552 (S) a,a,a-Trifluorotoluene 105 90.4-116 12/05/2016 00:30 WG931552 (S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 02:25 WG931552 (S) 4-Bromofluorobenzene 99.0 80.1-120 12/08/2016 02:25 WG931552 (S) 4-Bromofluorobenzene 104 80.1-120 12/05/2016 00:30 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 44 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 44 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18 L875822 SW-1 Collected date/time: 12/01/16 13:17 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.109 0.00500 1 12/06/2016 07:52 WG931506 Chromium ND 0.0100 1 12/06/2016 07:52 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:52 WG931506 Nickel ND 0.0100 1 12/06/2016 07:52 WG931506 Silver ND 0.00500 1 12/06/2016 07:52 WG931506 Vanadium ND 0.0200 1 12/06/2016 07:52 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 15:26 WG931509 Arsenic 0.00267 0.00200 1 12/05/2016 15:26 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:26 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:26 WG931509 Copper ND 0.00500 1 12/05/2016 15:26 WG931509 Lead ND 0.00200 1 12/05/2016 15:26 WG931509 Selenium ND 0.00200 1 12/05/2016 15:26 WG931509 Thallium ND 0.00200 1 12/05/2016 15:26 WG931509 Zinc ND 0.0250 1 12/05/2016 15:26 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/05/2016 00:53 WG931552 Acrylonitrile ND 0.0100 1 12/05/2016 00:53 WG931552 Benzene ND 0.00100 1 12/05/2016 00:53 WG931552 Bromochloromethane ND 0.00100 1 12/05/2016 00:53 WG931552 Bromodichloromethane ND 0.00100 1 12/05/2016 00:53 WG931552 Bromoform ND 0.00100 1 12/05/2016 00:53 WG931552 Bromomethane ND 0.00500 1 12/05/2016 00:53 WG931552 Carbon disulfide ND 0.00100 1 12/05/2016 00:53 WG931552 Carbon tetrachloride ND 0.00100 1 12/05/2016 00:53 WG931552 Chlorobenzene ND 0.00100 1 12/05/2016 00:53 WG931552 Chlorodibromomethane ND 0.00100 1 12/05/2016 00:53 WG931552 Chloroethane ND 0.00500 1 12/05/2016 00:53 WG931552 Chloroform ND 0.00500 1 12/05/2016 00:53 WG931552 Chloromethane ND 0.00250 1 12/05/2016 00:53 WG931552 Dibromomethane ND 0.00100 1 12/05/2016 00:53 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/05/2016 00:53 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/05/2016 00:53 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/05/2016 00:53 WG931552 1,1-Dichloroethane ND 0.00100 1 12/05/2016 00:53 WG931552 1,2-Dichloroethane ND 0.00100 1 12/05/2016 00:53 WG931552 1,1-Dichloroethene ND 0.00100 1 12/05/2016 00:53 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:53 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:53 WG931552 1,2-Dichloropropane ND 0.00100 1 12/05/2016 00:53 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:53 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:53 WG931552 Ethylbenzene ND 0.00100 1 12/05/2016 00:53 WG931552 2-Hexanone ND 0.0100 1 12/05/2016 00:53 WG931552 Iodomethane ND J4 0.0100 1 12/05/2016 00:53 WG931552 2-Butanone (MEK)ND 0.0100 1 12/05/2016 00:53 WG931552 Methylene Chloride ND 0.00500 1 12/05/2016 00:53 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/05/2016 00:53 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 45 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 45 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18 L875822 SW-1 Collected date/time: 12/01/16 13:17 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/05/2016 00:53 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:53 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:53 WG931552 Tetrachloroethene ND 0.00100 1 12/05/2016 00:53 WG931552 Toluene ND 0.00500 1 12/05/2016 00:53 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/05/2016 00:53 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/05/2016 00:53 WG931552 Trichloroethene ND 0.00100 1 12/05/2016 00:53 WG931552 Trichlorofluoromethane ND 0.00500 1 12/05/2016 00:53 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/05/2016 00:53 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 02:37 WG931552 Vinyl chloride ND 0.00100 1 12/05/2016 00:53 WG931552 Xylenes, Total ND 0.00300 1 12/05/2016 00:53 WG931552 (S) Toluene-d8 102 90.0-115 12/05/2016 00:53 WG931552 (S) Toluene-d8 100 90.0-115 12/08/2016 02:37 WG931552 (S) Dibromofluoromethane 86.8 79.0-121 12/08/2016 02:37 WG931552 (S) Dibromofluoromethane 99.2 79.0-121 12/05/2016 00:53 WG931552 (S) a,a,a-Trifluorotoluene 105 90.4-116 12/05/2016 00:53 WG931552 (S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 02:37 WG931552 (S) 4-Bromofluorobenzene 97.5 80.1-120 12/08/2016 02:37 WG931552 (S) 4-Bromofluorobenzene 104 80.1-120 12/05/2016 00:53 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 46 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 46 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19 L875822 TRIP BLANK Collected date/time: 12/01/16 00:00 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 17:58 WG931552 Acrylonitrile ND 0.0100 1 12/04/2016 17:58 WG931552 Benzene ND 0.00100 1 12/04/2016 17:58 WG931552 Bromochloromethane ND 0.00100 1 12/04/2016 17:58 WG931552 Bromodichloromethane ND 0.00100 1 12/04/2016 17:58 WG931552 Bromoform ND 0.00100 1 12/04/2016 17:58 WG931552 Bromomethane ND 0.00500 1 12/04/2016 17:58 WG931552 Carbon disulfide ND 0.00100 1 12/04/2016 17:58 WG931552 Carbon tetrachloride ND 0.00100 1 12/04/2016 17:58 WG931552 Chlorobenzene ND 0.00100 1 12/04/2016 17:58 WG931552 Chlorodibromomethane ND 0.00100 1 12/04/2016 17:58 WG931552 Chloroethane ND 0.00500 1 12/04/2016 17:58 WG931552 Chloroform ND 0.00500 1 12/04/2016 17:58 WG931552 Chloromethane ND 0.00250 1 12/04/2016 17:58 WG931552 Dibromomethane ND 0.00100 1 12/04/2016 17:58 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 17:58 WG931552 1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 17:58 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 17:58 WG931552 1,1-Dichloroethane ND 0.00100 1 12/04/2016 17:58 WG931552 1,2-Dichloroethane ND 0.00100 1 12/04/2016 17:58 WG931552 1,1-Dichloroethene ND 0.00100 1 12/04/2016 17:58 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 17:58 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 17:58 WG931552 1,2-Dichloropropane ND 0.00100 1 12/04/2016 17:58 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 17:58 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 17:58 WG931552 Ethylbenzene ND 0.00100 1 12/04/2016 17:58 WG931552 2-Hexanone ND 0.0100 1 12/04/2016 17:58 WG931552 Iodomethane ND J4 0.0100 1 12/04/2016 17:58 WG931552 2-Butanone (MEK)ND 0.0100 1 12/04/2016 17:58 WG931552 Methylene Chloride ND 0.00500 1 12/04/2016 17:58 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 17:58 WG931552 Styrene ND 0.00100 1 12/04/2016 17:58 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 17:58 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 17:58 WG931552 Tetrachloroethene ND 0.00100 1 12/04/2016 17:58 WG931552 Toluene ND 0.00500 1 12/04/2016 17:58 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 17:58 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 17:58 WG931552 Trichloroethene ND 0.00100 1 12/04/2016 17:58 WG931552 Trichlorofluoromethane ND 0.00500 1 12/04/2016 17:58 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 17:58 WG931552 Vinyl acetate ND 0.0100 1 12/07/2016 22:39 WG931552 Vinyl chloride ND 0.00100 1 12/04/2016 17:58 WG931552 Xylenes, Total ND 0.00300 1 12/04/2016 17:58 WG931552 (S) Toluene-d8 104 90.0-115 12/04/2016 17:58 WG931552 (S) Toluene-d8 99.3 90.0-115 12/07/2016 22:39 WG931552 (S) Dibromofluoromethane 85.8 79.0-121 12/07/2016 22:39 WG931552 (S) Dibromofluoromethane 98.3 79.0-121 12/04/2016 17:58 WG931552 (S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 17:58 WG931552 (S) a,a,a-Trifluorotoluene 99.7 90.4-116 12/07/2016 22:39 WG931552 (S) 4-Bromofluorobenzene 100 80.1-120 12/07/2016 22:39 WG931552 (S) 4-Bromofluorobenzene 104 80.1-120 12/04/2016 17:58 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 47 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 47 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20 L875822 LEACHATE PHASE 2 Collected date/time: 12/01/16 14:30 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Phosphorus,Total 0.332 B 0.100 1 12/07/2016 14:25 WG932178 Wet Chemistry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time COD 418 10.0 1 12/02/2016 20:28 WG931630 Wet Chemistry by Method 5210 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time BOD 15.0 10.0 1 12/07/2016 10:31 WG931445 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Nitrate as (N)ND 0.100 1 12/03/2016 01:35 WG931491 Sulfate ND 5.00 1 12/03/2016 01:35 WG931491 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.320 0.00500 1 12/06/2016 07:55 WG931506 Chromium 0.0149 0.0100 1 12/06/2016 07:55 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:55 WG931506 Nickel 0.0187 0.0100 1 12/06/2016 07:55 WG931506 Silver ND 0.00500 1 12/06/2016 07:55 WG931506 Vanadium 0.0233 0.0200 1 12/06/2016 07:55 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/05/2016 15:30 WG931509 Arsenic 0.0196 0.00200 1 12/05/2016 15:30 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:30 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:30 WG931509 Copper 0.0597 0.00500 1 12/05/2016 15:30 WG931509 Lead 0.00614 0.00200 1 12/05/2016 15:30 WG931509 Selenium ND 0.00200 1 12/05/2016 15:30 WG931509 Thallium ND 0.00200 1 12/05/2016 15:30 WG931509 Zinc 0.0401 0.0250 1 12/05/2016 15:30 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/05/2016 01:16 WG931552 Acrylonitrile ND 0.0100 1 12/05/2016 01:16 WG931552 Benzene 0.00694 0.00100 1 12/05/2016 01:16 WG931552 Bromochloromethane ND 0.00100 1 12/05/2016 01:16 WG931552 Bromodichloromethane ND 0.00100 1 12/05/2016 01:16 WG931552 Bromoform ND 0.00100 1 12/05/2016 01:16 WG931552 Bromomethane ND 0.00500 1 12/05/2016 01:16 WG931552 Carbon disulfide ND 0.00100 1 12/05/2016 01:16 WG931552 Carbon tetrachloride ND 0.00100 1 12/05/2016 01:16 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 48 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 48 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20 L875822 LEACHATE PHASE 2 Collected date/time: 12/01/16 14:30 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Chlorobenzene 0.00233 0.00100 1 12/05/2016 01:16 WG931552 Chlorodibromomethane ND 0.00100 1 12/05/2016 01:16 WG931552 Chloroethane ND 0.00500 1 12/05/2016 01:16 WG931552 Chloroform ND 0.00500 1 12/05/2016 01:16 WG931552 Chloromethane ND 0.00250 1 12/05/2016 01:16 WG931552 Dibromomethane ND 0.00100 1 12/05/2016 01:16 WG931552 1,2-Dichlorobenzene ND 0.00100 1 12/05/2016 01:16 WG931552 1,4-Dichlorobenzene 0.0160 0.00100 1 12/05/2016 01:16 WG931552 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/05/2016 01:16 WG931552 1,1-Dichloroethane ND 0.00100 1 12/05/2016 01:16 WG931552 1,2-Dichloroethane ND 0.00100 1 12/05/2016 01:16 WG931552 1,1-Dichloroethene ND 0.00100 1 12/05/2016 01:16 WG931552 cis-1,2-Dichloroethene ND 0.00100 1 12/05/2016 01:16 WG931552 trans-1,2-Dichloroethene ND 0.00100 1 12/05/2016 01:16 WG931552 1,2-Dichloropropane ND 0.00100 1 12/05/2016 01:16 WG931552 cis-1,3-Dichloropropene ND 0.00100 1 12/05/2016 01:16 WG931552 trans-1,3-Dichloropropene ND 0.00100 1 12/05/2016 01:16 WG931552 Ethylbenzene ND 0.00100 1 12/05/2016 01:16 WG931552 2-Hexanone ND 0.0100 1 12/05/2016 01:16 WG931552 Iodomethane ND J4 0.0100 1 12/05/2016 01:16 WG931552 2-Butanone (MEK)ND 0.0100 1 12/05/2016 01:16 WG931552 Methylene Chloride ND 0.00500 1 12/05/2016 01:16 WG931552 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/05/2016 01:16 WG931552 Styrene ND 0.00100 1 12/05/2016 01:16 WG931552 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/05/2016 01:16 WG931552 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/05/2016 01:16 WG931552 Tetrachloroethene ND 0.00100 1 12/05/2016 01:16 WG931552 Toluene ND 0.00500 1 12/05/2016 01:16 WG931552 1,1,1-Trichloroethane ND 0.00100 1 12/05/2016 01:16 WG931552 1,1,2-Trichloroethane ND 0.00100 1 12/05/2016 01:16 WG931552 Trichloroethene ND 0.00100 1 12/05/2016 01:16 WG931552 Trichlorofluoromethane ND 0.00500 1 12/05/2016 01:16 WG931552 1,2,3-Trichloropropane ND 0.00250 1 12/05/2016 01:16 WG931552 Vinyl acetate ND 0.0100 1 12/08/2016 02:49 WG931552 Vinyl chloride ND 0.00100 1 12/05/2016 01:16 WG931552 Xylenes, Total 0.0200 0.00300 1 12/05/2016 01:16 WG931552 (S) Toluene-d8 102 90.0-115 12/05/2016 01:16 WG931552 (S) Toluene-d8 101 90.0-115 12/08/2016 02:49 WG931552 (S) Dibromofluoromethane 86.1 79.0-121 12/08/2016 02:49 WG931552 (S) Dibromofluoromethane 99.1 79.0-121 12/05/2016 01:16 WG931552 (S) a,a,a-Trifluorotoluene 104 90.4-116 12/05/2016 01:16 WG931552 (S) a,a,a-Trifluorotoluene 103 90.4-116 12/08/2016 02:49 WG931552 (S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 02:49 WG931552 (S) 4-Bromofluorobenzene 105 80.1-120 12/05/2016 01:16 WG931552 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 49 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 49 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21 L875822 LEACHATE PHASE 3 Collected date/time: 12/01/16 14:40 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Phosphorus,Total 0.824 0.100 1 12/07/2016 14:26 WG932178 Wet Chemistry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time COD 634 10.0 1 12/02/2016 20:28 WG931630 Wet Chemistry by Method 5210 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time BOD 17.9 10.0 1 12/07/2016 10:34 WG931445 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Nitrate as (N)0.151 0.100 1 12/03/2016 01:50 WG931491 Sulfate 62.1 5.00 1 12/03/2016 01:50 WG931491 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.218 0.00500 1 12/06/2016 07:57 WG931506 Chromium 0.0194 0.0100 1 12/06/2016 07:57 WG931506 Cobalt ND 0.0100 1 12/06/2016 07:57 WG931506 Nickel 0.0574 0.0100 1 12/06/2016 07:57 WG931506 Silver ND 0.00500 1 12/06/2016 07:57 WG931506 Vanadium 0.0401 0.0200 1 12/06/2016 07:57 WG931506 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.0100 5 12/05/2016 15:54 WG931509 Arsenic 0.0366 0.0100 5 12/05/2016 15:54 WG931509 Beryllium ND 0.00200 1 12/05/2016 15:33 WG931509 Cadmium ND 0.00100 1 12/05/2016 15:33 WG931509 Copper 1.49 0.0250 5 12/05/2016 15:54 WG931509 Lead 0.212 0.00200 1 12/05/2016 15:33 WG931509 Selenium ND 0.00200 1 12/05/2016 15:33 WG931509 Thallium ND 0.00200 1 12/05/2016 15:33 WG931509 Zinc 0.369 0.125 5 12/05/2016 15:54 WG931509 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 17:48 WG931684 Acrylonitrile ND 0.0100 1 12/04/2016 17:48 WG931684 Benzene 0.00507 0.00100 1 12/04/2016 17:48 WG931684 Bromochloromethane ND 0.00100 1 12/04/2016 17:48 WG931684 Bromodichloromethane ND 0.00100 1 12/04/2016 17:48 WG931684 Bromoform ND 0.00100 1 12/04/2016 17:48 WG931684 Bromomethane ND 0.00500 1 12/04/2016 17:48 WG931684 Carbon disulfide ND 0.00100 1 12/04/2016 17:48 WG931684 Carbon tetrachloride ND 0.00100 1 12/04/2016 17:48 WG931684 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 50 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 50 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21 L875822 LEACHATE PHASE 3 Collected date/time: 12/01/16 14:40 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Chlorobenzene 0.00271 0.00100 1 12/04/2016 17:48 WG931684 Chlorodibromomethane ND 0.00100 1 12/04/2016 17:48 WG931684 Chloroethane ND 0.00500 1 12/04/2016 17:48 WG931684 Chloroform ND 0.00500 1 12/04/2016 17:48 WG931684 Chloromethane ND 0.00250 1 12/04/2016 17:48 WG931684 Dibromomethane ND 0.00100 1 12/04/2016 17:48 WG931684 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 17:48 WG931684 1,4-Dichlorobenzene 0.0101 0.00100 1 12/04/2016 17:48 WG931684 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 17:48 WG931684 1,1-Dichloroethane ND 0.00100 1 12/04/2016 17:48 WG931684 1,2-Dichloroethane ND 0.00100 1 12/04/2016 17:48 WG931684 1,1-Dichloroethene ND 0.00100 1 12/04/2016 17:48 WG931684 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 17:48 WG931684 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 17:48 WG931684 1,2-Dichloropropane ND 0.00100 1 12/04/2016 17:48 WG931684 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 17:48 WG931684 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 17:48 WG931684 Ethylbenzene 0.00611 0.00100 1 12/04/2016 17:48 WG931684 2-Hexanone ND 0.0100 1 12/04/2016 17:48 WG931684 Iodomethane ND 0.0100 1 12/04/2016 17:48 WG931684 2-Butanone (MEK)ND 0.0100 1 12/04/2016 17:48 WG931684 Methylene Chloride ND 0.00500 1 12/04/2016 17:48 WG931684 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 17:48 WG931684 Styrene ND 0.00100 1 12/04/2016 17:48 WG931684 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 17:48 WG931684 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 17:48 WG931684 Tetrachloroethene ND 0.00100 1 12/04/2016 17:48 WG931684 Toluene ND 0.00500 1 12/04/2016 17:48 WG931684 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 17:48 WG931684 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 17:48 WG931684 Trichloroethene ND 0.00100 1 12/04/2016 17:48 WG931684 Trichlorofluoromethane ND 0.00500 1 12/04/2016 17:48 WG931684 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 17:48 WG931684 Vinyl acetate ND 0.0100 1 12/04/2016 17:48 WG931684 Vinyl chloride ND 0.00100 1 12/04/2016 17:48 WG931684 Xylenes, Total 0.0381 0.00300 1 12/04/2016 17:48 WG931684 (S) Toluene-d8 105 90.0-115 12/04/2016 17:48 WG931684 (S) Dibromofluoromethane 97.2 79.0-121 12/04/2016 17:48 WG931684 (S) a,a,a-Trifluorotoluene 107 90.4-116 12/04/2016 17:48 WG931684 (S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 17:48 WG931684 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 51 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 51 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22 L875822 LEACHATE PHASE 4 Collected date/time: 12/01/16 14:52 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Phosphorus,Total 1.30 0.100 1 12/07/2016 14:28 WG932178 Wet Chemistry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time COD 1420 250 25 12/02/2016 20:29 WG931630 Wet Chemistry by Method 5210 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time BOD 69.0 33.3 10 12/07/2016 10:37 WG931445 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Nitrate as (N)ND 0.100 1 12/03/2016 02:04 WG931491 Sulfate 16.4 5.00 1 12/03/2016 02:04 WG931491 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.147 0.0450 9 12/05/2016 08:56 WG931720 Chromium ND 0.0900 9 12/05/2016 08:56 WG931720 Cobalt ND 0.0900 9 12/05/2016 08:56 WG931720 Nickel 0.132 0.0900 9 12/05/2016 08:56 WG931720 Silver ND 0.0450 9 12/05/2016 08:56 WG931720 Vanadium ND 0.180 9 12/05/2016 08:56 WG931720 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.0180 9 12/06/2016 11:05 WG931723 Arsenic 0.125 0.0180 9 12/06/2016 11:05 WG931723 Beryllium ND 0.0180 9 12/06/2016 11:05 WG931723 Cadmium ND 0.00900 9 12/06/2016 11:05 WG931723 Copper ND 0.0450 9 12/06/2016 19:59 WG932463 Lead ND 0.0180 9 12/06/2016 11:05 WG931723 Selenium ND 0.0180 9 12/06/2016 11:05 WG931723 Thallium ND 0.0180 9 12/06/2016 11:05 WG931723 Zinc ND 0.225 9 12/06/2016 11:05 WG931723 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/04/2016 19:13 WG931684 Acrylonitrile ND 0.0100 1 12/04/2016 19:13 WG931684 Benzene 0.00959 0.00100 1 12/04/2016 19:13 WG931684 Bromochloromethane ND 0.00100 1 12/04/2016 19:13 WG931684 Bromodichloromethane ND 0.00100 1 12/04/2016 19:13 WG931684 Bromoform ND 0.00100 1 12/04/2016 19:13 WG931684 Bromomethane ND 0.00500 1 12/04/2016 19:13 WG931684 Carbon disulfide ND 0.00100 1 12/04/2016 19:13 WG931684 Carbon tetrachloride ND 0.00100 1 12/04/2016 19:13 WG931684 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 52 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 52 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22 L875822 LEACHATE PHASE 4 Collected date/time: 12/01/16 14:52 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Chlorobenzene ND 0.00100 1 12/04/2016 19:13 WG931684 Chlorodibromomethane ND 0.00100 1 12/04/2016 19:13 WG931684 Chloroethane ND 0.00500 1 12/04/2016 19:13 WG931684 Chloroform ND 0.00500 1 12/04/2016 19:13 WG931684 Chloromethane ND 0.00250 1 12/04/2016 19:13 WG931684 Dibromomethane ND 0.00100 1 12/04/2016 19:13 WG931684 1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 19:13 WG931684 1,4-Dichlorobenzene 0.00379 0.00100 1 12/04/2016 19:13 WG931684 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 19:13 WG931684 1,1-Dichloroethane ND 0.00100 1 12/04/2016 19:13 WG931684 1,2-Dichloroethane ND 0.00100 1 12/04/2016 19:13 WG931684 1,1-Dichloroethene ND 0.00100 1 12/04/2016 19:13 WG931684 cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:13 WG931684 trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:13 WG931684 1,2-Dichloropropane ND 0.00100 1 12/04/2016 19:13 WG931684 cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:13 WG931684 trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:13 WG931684 Ethylbenzene 0.00899 0.00100 1 12/04/2016 19:13 WG931684 2-Hexanone ND 0.0100 1 12/04/2016 19:13 WG931684 Iodomethane ND 0.0100 1 12/04/2016 19:13 WG931684 2-Butanone (MEK)ND 0.0100 1 12/04/2016 19:13 WG931684 Methylene Chloride ND 0.00500 1 12/04/2016 19:13 WG931684 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 19:13 WG931684 Styrene ND 0.00100 1 12/04/2016 19:13 WG931684 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:13 WG931684 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:13 WG931684 Tetrachloroethene ND 0.00100 1 12/04/2016 19:13 WG931684 Toluene ND 0.00500 1 12/04/2016 19:13 WG931684 1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 19:13 WG931684 1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 19:13 WG931684 Trichloroethene ND 0.00100 1 12/04/2016 19:13 WG931684 Trichlorofluoromethane ND 0.00500 1 12/04/2016 19:13 WG931684 1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 19:13 WG931684 Vinyl acetate ND 0.0100 1 12/04/2016 19:13 WG931684 Vinyl chloride ND 0.00100 1 12/04/2016 19:13 WG931684 Xylenes, Total 0.0217 0.00300 1 12/04/2016 19:13 WG931684 (S) Toluene-d8 105 90.0-115 12/04/2016 19:13 WG931684 (S) Dibromofluoromethane 91.9 79.0-121 12/04/2016 19:13 WG931684 (S) a,a,a-Trifluorotoluene 111 90.4-116 12/04/2016 19:13 WG931684 (S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 19:13 WG931684 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 53 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 53 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23 L875822 MW-10 Collected date/time: 12/02/16 09:46 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0532 0.00500 1 12/07/2016 16:09 WG932146 Chromium 0.0122 B 0.0100 1 12/07/2016 16:09 WG932146 Cobalt ND 0.0100 1 12/07/2016 16:09 WG932146 Nickel ND 0.0100 1 12/07/2016 16:09 WG932146 Silver ND 0.00500 1 12/07/2016 16:09 WG932146 Vanadium 0.0215 0.0200 1 12/07/2016 16:09 WG932146 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/07/2016 01:42 WG932285 Arsenic ND 0.00200 1 12/07/2016 01:42 WG932285 Beryllium ND 0.00200 1 12/07/2016 01:42 WG932285 Cadmium ND 0.00100 1 12/07/2016 01:42 WG932285 Copper ND 0.00500 1 12/07/2016 01:42 WG932285 Lead 0.00760 0.00200 1 12/07/2016 01:42 WG932285 Selenium ND 0.00200 1 12/07/2016 01:42 WG932285 Thallium ND 0.00200 1 12/07/2016 01:42 WG932285 Zinc 0.0274 B 0.0250 1 12/07/2016 01:42 WG932285 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND J3 J4 0.0500 1 12/08/2016 01:54 WG932369 Acrylonitrile ND 0.0100 1 12/08/2016 01:54 WG932369 Benzene ND 0.00100 1 12/08/2016 01:54 WG932369 Bromochloromethane ND 0.00100 1 12/08/2016 01:54 WG932369 Bromodichloromethane ND 0.00100 1 12/08/2016 01:54 WG932369 Bromoform ND 0.00100 1 12/08/2016 01:54 WG932369 Bromomethane ND 0.00500 1 12/08/2016 01:54 WG932369 Carbon disulfide ND J3 0.00100 1 12/08/2016 01:54 WG932369 Carbon tetrachloride ND 0.00100 1 12/08/2016 01:54 WG932369 Chlorobenzene ND 0.00100 1 12/08/2016 01:54 WG932369 Chlorodibromomethane ND 0.00100 1 12/08/2016 01:54 WG932369 Chloroethane ND 0.00500 1 12/08/2016 01:54 WG932369 Chloroform ND 0.00500 1 12/08/2016 01:54 WG932369 Chloromethane ND 0.00250 1 12/08/2016 01:54 WG932369 Dibromomethane ND 0.00100 1 12/08/2016 01:54 WG932369 1,2-Dichlorobenzene ND 0.00100 1 12/08/2016 01:54 WG932369 1,4-Dichlorobenzene ND 0.00100 1 12/08/2016 01:54 WG932369 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/08/2016 01:54 WG932369 1,1-Dichloroethane ND 0.00100 1 12/08/2016 01:54 WG932369 1,2-Dichloroethane ND 0.00100 1 12/08/2016 01:54 WG932369 1,1-Dichloroethene ND J3 0.00100 1 12/08/2016 01:54 WG932369 cis-1,2-Dichloroethene ND 0.00100 1 12/08/2016 01:54 WG932369 trans-1,2-Dichloroethene ND J3 0.00100 1 12/08/2016 01:54 WG932369 1,2-Dichloropropane ND 0.00100 1 12/08/2016 01:54 WG932369 cis-1,3-Dichloropropene ND 0.00100 1 12/08/2016 01:54 WG932369 trans-1,3-Dichloropropene ND 0.00100 1 12/08/2016 01:54 WG932369 Ethylbenzene ND 0.00100 1 12/08/2016 01:54 WG932369 2-Hexanone ND 0.0100 1 12/08/2016 01:54 WG932369 Iodomethane ND 0.0100 1 12/08/2016 01:54 WG932369 2-Butanone (MEK)ND 0.0100 1 12/08/2016 01:54 WG932369 Methylene Chloride ND 0.00500 1 12/08/2016 01:54 WG932369 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/08/2016 01:54 WG932369 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 54 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 54 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23 L875822 MW-10 Collected date/time: 12/02/16 09:46 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/08/2016 01:54 WG932369 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/08/2016 01:54 WG932369 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/08/2016 01:54 WG932369 Tetrachloroethene ND J3 0.00100 1 12/08/2016 01:54 WG932369 Toluene ND 0.00500 1 12/08/2016 01:54 WG932369 1,1,1-Trichloroethane ND J3 0.00100 1 12/08/2016 01:54 WG932369 1,1,2-Trichloroethane ND 0.00100 1 12/08/2016 01:54 WG932369 Trichloroethene ND 0.00100 1 12/08/2016 01:54 WG932369 Trichlorofluoromethane ND J3 0.00500 1 12/08/2016 01:54 WG932369 1,2,3-Trichloropropane ND 0.00250 1 12/08/2016 01:54 WG932369 Vinyl acetate ND 0.0100 1 12/08/2016 01:54 WG932369 Vinyl chloride ND J3 0.00100 1 12/08/2016 01:54 WG932369 Xylenes, Total ND J3 0.00300 1 12/08/2016 01:54 WG932369 (S) Toluene-d8 100 90.0-115 12/08/2016 01:54 WG932369 (S) Dibromofluoromethane 104 79.0-121 12/08/2016 01:54 WG932369 (S) a,a,a-Trifluorotoluene 100 90.4-116 12/08/2016 01:54 WG932369 (S) 4-Bromofluorobenzene 96.5 80.1-120 12/08/2016 01:54 WG932369 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 55 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 55 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 24 L875822 MW-11 Collected date/time: 12/02/16 09:20 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0439 0.00500 1 12/07/2016 16:16 WG932146 Chromium ND 0.0100 1 12/07/2016 16:16 WG932146 Cobalt ND 0.0100 1 12/07/2016 16:16 WG932146 Nickel ND 0.0100 1 12/07/2016 16:16 WG932146 Silver ND 0.00500 1 12/07/2016 16:16 WG932146 Vanadium ND 0.0200 1 12/07/2016 16:16 WG932146 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/07/2016 01:46 WG932285 Arsenic 0.00242 0.00200 1 12/07/2016 01:46 WG932285 Beryllium ND 0.00200 1 12/07/2016 01:46 WG932285 Cadmium ND 0.00100 1 12/07/2016 01:46 WG932285 Copper ND 0.00500 1 12/07/2016 01:46 WG932285 Lead 0.00293 0.00200 1 12/07/2016 01:46 WG932285 Selenium ND 0.00200 1 12/07/2016 01:46 WG932285 Thallium ND 0.00200 1 12/07/2016 01:46 WG932285 Zinc 0.0347 B 0.0250 1 12/07/2016 01:46 WG932285 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND J3 J4 0.0500 1 12/08/2016 02:25 WG932369 Acrylonitrile ND 0.0100 1 12/08/2016 02:25 WG932369 Benzene ND 0.00100 1 12/08/2016 02:25 WG932369 Bromochloromethane ND 0.00100 1 12/08/2016 02:25 WG932369 Bromodichloromethane ND 0.00100 1 12/08/2016 02:25 WG932369 Bromoform ND 0.00100 1 12/08/2016 02:25 WG932369 Bromomethane ND 0.00500 1 12/08/2016 02:25 WG932369 Carbon disulfide ND J3 0.00100 1 12/08/2016 02:25 WG932369 Carbon tetrachloride ND 0.00100 1 12/08/2016 02:25 WG932369 Chlorobenzene ND 0.00100 1 12/08/2016 02:25 WG932369 Chlorodibromomethane ND 0.00100 1 12/08/2016 02:25 WG932369 Chloroethane ND 0.00500 1 12/08/2016 02:25 WG932369 Chloroform ND 0.00500 1 12/08/2016 02:25 WG932369 Chloromethane ND 0.00250 1 12/08/2016 02:25 WG932369 Dibromomethane ND 0.00100 1 12/08/2016 02:25 WG932369 1,2-Dichlorobenzene ND 0.00100 1 12/08/2016 02:25 WG932369 1,4-Dichlorobenzene ND 0.00100 1 12/08/2016 02:25 WG932369 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/08/2016 02:25 WG932369 1,1-Dichloroethane ND 0.00100 1 12/08/2016 02:25 WG932369 1,2-Dichloroethane ND 0.00100 1 12/08/2016 02:25 WG932369 1,1-Dichloroethene ND J3 0.00100 1 12/08/2016 02:25 WG932369 cis-1,2-Dichloroethene ND 0.00100 1 12/08/2016 02:25 WG932369 trans-1,2-Dichloroethene ND J3 0.00100 1 12/08/2016 02:25 WG932369 1,2-Dichloropropane ND 0.00100 1 12/08/2016 02:25 WG932369 cis-1,3-Dichloropropene ND 0.00100 1 12/08/2016 02:25 WG932369 trans-1,3-Dichloropropene ND 0.00100 1 12/08/2016 02:25 WG932369 Ethylbenzene ND 0.00100 1 12/08/2016 02:25 WG932369 2-Hexanone ND 0.0100 1 12/08/2016 02:25 WG932369 Iodomethane ND 0.0100 1 12/08/2016 02:25 WG932369 2-Butanone (MEK)ND 0.0100 1 12/08/2016 02:25 WG932369 Methylene Chloride ND 0.00500 1 12/08/2016 02:25 WG932369 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/08/2016 02:25 WG932369 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 56 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 56 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 24 L875822 MW-11 Collected date/time: 12/02/16 09:20 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/08/2016 02:25 WG932369 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/08/2016 02:25 WG932369 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/08/2016 02:25 WG932369 Tetrachloroethene ND J3 0.00100 1 12/08/2016 02:25 WG932369 Toluene ND 0.00500 1 12/08/2016 02:25 WG932369 1,1,1-Trichloroethane ND J3 0.00100 1 12/08/2016 02:25 WG932369 1,1,2-Trichloroethane ND 0.00100 1 12/08/2016 02:25 WG932369 Trichloroethene ND 0.00100 1 12/08/2016 02:25 WG932369 Trichlorofluoromethane ND J3 0.00500 1 12/08/2016 02:25 WG932369 1,2,3-Trichloropropane ND 0.00250 1 12/08/2016 02:25 WG932369 Vinyl acetate ND 0.0100 1 12/08/2016 02:25 WG932369 Vinyl chloride ND J3 0.00100 1 12/08/2016 02:25 WG932369 Xylenes, Total ND J3 0.00300 1 12/08/2016 02:25 WG932369 (S) Toluene-d8 101 90.0-115 12/08/2016 02:25 WG932369 (S) Dibromofluoromethane 106 79.0-121 12/08/2016 02:25 WG932369 (S) a,a,a-Trifluorotoluene 99.6 90.4-116 12/08/2016 02:25 WG932369 (S) 4-Bromofluorobenzene 93.1 80.1-120 12/08/2016 02:25 WG932369 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 57 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 57 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 25 L875822 MW-20 Collected date/time: 12/02/16 08:45 Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Dissolved Solids 61.0 10.0 1 12/08/2016 10:32 WG932797 Wet Chemistry by Method 2320 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Alkalinity ND 20.0 1 12/07/2016 11:57 WG932588 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Chloride 5.23 1.00 1 12/07/2016 10:38 WG932605 Sulfate 7.35 5.00 1 12/07/2016 10:38 WG932605 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.105 0.00500 1 12/07/2016 16:19 WG932146 Chromium ND 0.0100 1 12/07/2016 16:19 WG932146 Cobalt ND 0.0100 1 12/07/2016 16:19 WG932146 Nickel ND 0.0100 1 12/07/2016 16:19 WG932146 Silver ND 0.00500 1 12/07/2016 16:19 WG932146 Vanadium ND 0.0200 1 12/07/2016 16:19 WG932146 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/07/2016 01:49 WG932285 Arsenic ND 0.00200 1 12/07/2016 01:49 WG932285 Beryllium ND 0.00200 1 12/07/2016 01:49 WG932285 Cadmium ND 0.00100 1 12/07/2016 01:49 WG932285 Copper ND 0.00500 1 12/07/2016 01:49 WG932285 Lead 0.0102 0.00200 1 12/07/2016 01:49 WG932285 Selenium ND 0.00200 1 12/07/2016 01:49 WG932285 Thallium ND 0.00200 1 12/07/2016 01:49 WG932285 Zinc ND 0.0250 1 12/07/2016 01:49 WG932285 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND J3 J4 0.0500 1 12/09/2016 17:32 WG932369 Acrylonitrile ND 0.0100 1 12/09/2016 17:32 WG932369 Benzene ND 0.00100 1 12/09/2016 17:32 WG932369 Bromochloromethane ND 0.00100 1 12/09/2016 17:32 WG932369 Bromodichloromethane ND 0.00100 1 12/09/2016 17:32 WG932369 Bromoform ND 0.00100 1 12/09/2016 17:32 WG932369 Bromomethane ND 0.00500 1 12/09/2016 17:32 WG932369 Carbon disulfide ND J3 0.00100 1 12/09/2016 17:32 WG932369 Carbon tetrachloride ND 0.00100 1 12/09/2016 17:32 WG932369 Chlorobenzene ND 0.00100 1 12/09/2016 17:32 WG932369 Chlorodibromomethane ND 0.00100 1 12/09/2016 17:32 WG932369 Chloroethane ND 0.00500 1 12/09/2016 17:32 WG932369 Chloroform ND 0.00500 1 12/09/2016 17:32 WG932369 Chloromethane ND 0.00250 1 12/09/2016 17:32 WG932369 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 58 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 58 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 25 L875822 MW-20 Collected date/time: 12/02/16 08:45 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Dibromomethane ND 0.00100 1 12/09/2016 17:32 WG932369 1,2-Dichlorobenzene ND 0.00100 1 12/09/2016 17:32 WG932369 1,4-Dichlorobenzene ND 0.00100 1 12/09/2016 17:32 WG932369 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/09/2016 17:32 WG932369 1,1-Dichloroethane ND 0.00100 1 12/09/2016 17:32 WG932369 1,2-Dichloroethane ND 0.00100 1 12/09/2016 17:32 WG932369 1,1-Dichloroethene ND J3 0.00100 1 12/09/2016 17:32 WG932369 cis-1,2-Dichloroethene ND 0.00100 1 12/09/2016 17:32 WG932369 trans-1,2-Dichloroethene ND J3 0.00100 1 12/09/2016 17:32 WG932369 1,2-Dichloropropane ND 0.00100 1 12/09/2016 17:32 WG932369 cis-1,3-Dichloropropene ND 0.00100 1 12/09/2016 17:32 WG932369 trans-1,3-Dichloropropene ND 0.00100 1 12/09/2016 17:32 WG932369 Ethylbenzene ND 0.00100 1 12/09/2016 17:32 WG932369 2-Hexanone ND 0.0100 1 12/09/2016 17:32 WG932369 Iodomethane ND 0.0100 1 12/09/2016 17:32 WG932369 2-Butanone (MEK)ND 0.0100 1 12/09/2016 17:32 WG932369 Methylene Chloride ND 0.00500 1 12/09/2016 17:32 WG932369 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/09/2016 17:32 WG932369 Styrene ND 0.00100 1 12/09/2016 17:32 WG932369 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/09/2016 17:32 WG932369 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/09/2016 17:32 WG932369 Tetrachloroethene ND J3 0.00100 1 12/09/2016 17:32 WG932369 Toluene ND 0.00500 1 12/09/2016 17:32 WG932369 1,1,1-Trichloroethane ND J3 0.00100 1 12/09/2016 17:32 WG932369 1,1,2-Trichloroethane ND 0.00100 1 12/09/2016 17:32 WG932369 Trichloroethene ND 0.00100 1 12/09/2016 17:32 WG932369 Trichlorofluoromethane ND J3 0.00500 1 12/09/2016 17:32 WG932369 1,2,3-Trichloropropane ND 0.00250 1 12/09/2016 17:32 WG932369 Vinyl acetate ND 0.0100 1 12/09/2016 17:32 WG932369 Vinyl chloride ND J3 0.00100 1 12/09/2016 17:32 WG932369 Xylenes, Total ND J3 0.00300 1 12/09/2016 17:32 WG932369 (S) Toluene-d8 106 90.0-115 12/09/2016 17:32 WG932369 (S) Dibromofluoromethane 104 79.0-121 12/09/2016 17:32 WG932369 (S) a,a,a-Trifluorotoluene 103 90.4-116 12/09/2016 17:32 WG932369 (S) 4-Bromofluorobenzene 96.7 80.1-120 12/09/2016 17:32 WG932369 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 59 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 59 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 26 L875822 MW-26 Collected date/time: 12/02/16 08:15 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0401 0.00500 1 12/07/2016 15:22 WG932146 Chromium ND 0.0100 1 12/07/2016 15:22 WG932146 Cobalt ND 0.0100 1 12/07/2016 15:22 WG932146 Nickel ND 0.0100 1 12/07/2016 15:22 WG932146 Silver ND 0.00500 1 12/07/2016 15:22 WG932146 Vanadium ND 0.0200 1 12/07/2016 15:22 WG932146 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/07/2016 01:53 WG932285 Arsenic ND 0.00200 1 12/07/2016 01:53 WG932285 Beryllium ND 0.00200 1 12/07/2016 01:53 WG932285 Cadmium ND 0.00100 1 12/07/2016 01:53 WG932285 Copper ND 0.00500 1 12/07/2016 01:53 WG932285 Lead ND 0.00200 1 12/07/2016 01:53 WG932285 Selenium ND 0.00200 1 12/07/2016 01:53 WG932285 Thallium ND 0.00200 1 12/07/2016 01:53 WG932285 Zinc ND 0.0250 1 12/07/2016 01:53 WG932285 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND J3 J4 0.0500 1 12/08/2016 02:57 WG932369 Acrylonitrile ND 0.0100 1 12/08/2016 02:57 WG932369 Benzene ND 0.00100 1 12/08/2016 02:57 WG932369 Bromochloromethane ND 0.00100 1 12/08/2016 02:57 WG932369 Bromodichloromethane ND 0.00100 1 12/08/2016 02:57 WG932369 Bromoform ND 0.00100 1 12/08/2016 02:57 WG932369 Bromomethane ND 0.00500 1 12/08/2016 02:57 WG932369 Carbon disulfide ND J3 0.00100 1 12/08/2016 02:57 WG932369 Carbon tetrachloride ND 0.00100 1 12/08/2016 02:57 WG932369 Chlorobenzene ND 0.00100 1 12/08/2016 02:57 WG932369 Chlorodibromomethane ND 0.00100 1 12/08/2016 02:57 WG932369 Chloroethane ND 0.00500 1 12/08/2016 02:57 WG932369 Chloroform ND 0.00500 1 12/08/2016 02:57 WG932369 Chloromethane ND 0.00250 1 12/08/2016 02:57 WG932369 Dibromomethane ND 0.00100 1 12/08/2016 02:57 WG932369 1,2-Dichlorobenzene ND 0.00100 1 12/08/2016 02:57 WG932369 1,4-Dichlorobenzene ND 0.00100 1 12/08/2016 02:57 WG932369 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/08/2016 02:57 WG932369 1,1-Dichloroethane ND 0.00100 1 12/08/2016 02:57 WG932369 1,2-Dichloroethane ND 0.00100 1 12/08/2016 02:57 WG932369 1,1-Dichloroethene ND J3 0.00100 1 12/08/2016 02:57 WG932369 cis-1,2-Dichloroethene ND 0.00100 1 12/08/2016 02:57 WG932369 trans-1,2-Dichloroethene ND J3 0.00100 1 12/08/2016 02:57 WG932369 1,2-Dichloropropane ND 0.00100 1 12/08/2016 02:57 WG932369 cis-1,3-Dichloropropene ND 0.00100 1 12/08/2016 02:57 WG932369 trans-1,3-Dichloropropene ND 0.00100 1 12/08/2016 02:57 WG932369 Ethylbenzene ND 0.00100 1 12/08/2016 02:57 WG932369 2-Hexanone ND 0.0100 1 12/08/2016 02:57 WG932369 Iodomethane ND 0.0100 1 12/08/2016 02:57 WG932369 2-Butanone (MEK)ND 0.0100 1 12/08/2016 02:57 WG932369 Methylene Chloride ND 0.00500 1 12/08/2016 02:57 WG932369 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/08/2016 02:57 WG932369 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 60 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 60 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 26 L875822 MW-26 Collected date/time: 12/02/16 08:15 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/08/2016 02:57 WG932369 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/08/2016 02:57 WG932369 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/08/2016 02:57 WG932369 Tetrachloroethene ND J3 0.00100 1 12/08/2016 02:57 WG932369 Toluene ND 0.00500 1 12/08/2016 02:57 WG932369 1,1,1-Trichloroethane ND J3 0.00100 1 12/08/2016 02:57 WG932369 1,1,2-Trichloroethane ND 0.00100 1 12/08/2016 02:57 WG932369 Trichloroethene ND 0.00100 1 12/08/2016 02:57 WG932369 Trichlorofluoromethane ND J3 0.00500 1 12/08/2016 02:57 WG932369 1,2,3-Trichloropropane ND 0.00250 1 12/08/2016 02:57 WG932369 Vinyl acetate ND 0.0100 1 12/08/2016 02:57 WG932369 Vinyl chloride ND J3 0.00100 1 12/08/2016 02:57 WG932369 Xylenes, Total ND J3 0.00300 1 12/08/2016 02:57 WG932369 (S) Toluene-d8 99.9 90.0-115 12/08/2016 02:57 WG932369 (S) Dibromofluoromethane 106 79.0-121 12/08/2016 02:57 WG932369 (S) a,a,a-Trifluorotoluene 99.7 90.4-116 12/08/2016 02:57 WG932369 (S) 4-Bromofluorobenzene 94.5 80.1-120 12/08/2016 02:57 WG932369 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 61 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 61 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 27 L875822 TRIP BLANK Collected date/time: 12/01/16 00:00 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND J3 J4 0.0500 1 12/08/2016 13:39 WG932369 Acrylonitrile ND 0.0100 1 12/08/2016 13:39 WG932369 Benzene ND 0.00100 1 12/08/2016 13:39 WG932369 Bromochloromethane ND 0.00100 1 12/08/2016 13:39 WG932369 Bromodichloromethane ND 0.00100 1 12/08/2016 13:39 WG932369 Bromoform ND 0.00100 1 12/08/2016 13:39 WG932369 Bromomethane ND 0.00500 1 12/08/2016 13:39 WG932369 Carbon disulfide ND J3 0.00100 1 12/08/2016 13:39 WG932369 Carbon tetrachloride ND 0.00100 1 12/08/2016 13:39 WG932369 Chlorobenzene ND 0.00100 1 12/08/2016 13:39 WG932369 Chlorodibromomethane ND 0.00100 1 12/08/2016 13:39 WG932369 Chloroethane ND 0.00500 1 12/08/2016 13:39 WG932369 Chloroform ND 0.00500 1 12/08/2016 13:39 WG932369 Chloromethane ND 0.00250 1 12/08/2016 13:39 WG932369 Dibromomethane ND 0.00100 1 12/08/2016 13:39 WG932369 1,2-Dichlorobenzene ND 0.00100 1 12/08/2016 13:39 WG932369 1,4-Dichlorobenzene ND 0.00100 1 12/08/2016 13:39 WG932369 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/08/2016 13:39 WG932369 1,1-Dichloroethane ND 0.00100 1 12/08/2016 13:39 WG932369 1,2-Dichloroethane ND 0.00100 1 12/08/2016 13:39 WG932369 1,1-Dichloroethene ND J3 0.00100 1 12/08/2016 13:39 WG932369 cis-1,2-Dichloroethene ND 0.00100 1 12/08/2016 13:39 WG932369 trans-1,2-Dichloroethene ND J3 0.00100 1 12/08/2016 13:39 WG932369 1,2-Dichloropropane ND 0.00100 1 12/08/2016 13:39 WG932369 cis-1,3-Dichloropropene ND 0.00100 1 12/08/2016 13:39 WG932369 trans-1,3-Dichloropropene ND 0.00100 1 12/08/2016 13:39 WG932369 Ethylbenzene ND 0.00100 1 12/08/2016 13:39 WG932369 2-Hexanone ND 0.0100 1 12/08/2016 13:39 WG932369 Iodomethane ND 0.0100 1 12/08/2016 13:39 WG932369 2-Butanone (MEK)ND 0.0100 1 12/08/2016 13:39 WG932369 Methylene Chloride ND 0.00500 1 12/08/2016 13:39 WG932369 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/08/2016 13:39 WG932369 Styrene ND 0.00100 1 12/08/2016 13:39 WG932369 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/08/2016 13:39 WG932369 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/08/2016 13:39 WG932369 Tetrachloroethene ND J3 0.00100 1 12/08/2016 13:39 WG932369 Toluene ND 0.00500 1 12/08/2016 13:39 WG932369 1,1,1-Trichloroethane ND J3 0.00100 1 12/08/2016 13:39 WG932369 1,1,2-Trichloroethane ND 0.00100 1 12/08/2016 13:39 WG932369 Trichloroethene ND 0.00100 1 12/08/2016 13:39 WG932369 Trichlorofluoromethane ND J3 0.00500 1 12/08/2016 13:39 WG932369 1,2,3-Trichloropropane ND 0.00250 1 12/08/2016 13:39 WG932369 Vinyl acetate ND 0.0100 1 12/08/2016 13:39 WG932369 Vinyl chloride ND J3 0.00100 1 12/08/2016 13:39 WG932369 Xylenes, Total ND J3 0.00300 1 12/08/2016 13:39 WG932369 (S) Toluene-d8 100 90.0-115 12/08/2016 13:39 WG932369 (S) Dibromofluoromethane 108 79.0-121 12/08/2016 13:39 WG932369 (S) a,a,a-Trifluorotoluene 98.6 90.4-116 12/08/2016 13:39 WG932369 (S) 4-Bromofluorobenzene 91.9 80.1-120 12/08/2016 13:39 WG932369 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 62 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 62 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 28 L875822 MW-6 Collected date/time: 12/05/16 14:21 Metals (ICP) by Method 6010C Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Barium 0.0120 0.00500 1 12/07/2016 16:22 WG932146 Chromium ND 0.0100 1 12/07/2016 16:22 WG932146 Cobalt ND 0.0100 1 12/07/2016 16:22 WG932146 Nickel ND 0.0100 1 12/07/2016 16:22 WG932146 Silver ND 0.00500 1 12/07/2016 16:22 WG932146 Vanadium ND 0.0200 1 12/07/2016 16:22 WG932146 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 12/07/2016 18:25 WG932780 Arsenic ND 0.00200 1 12/07/2016 18:25 WG932780 Beryllium ND 0.00200 1 12/07/2016 18:25 WG932780 Cadmium ND 0.00100 1 12/07/2016 18:25 WG932780 Copper ND 0.00500 1 12/07/2016 18:25 WG932780 Lead ND 0.00200 1 12/07/2016 18:25 WG932780 Selenium ND 0.00200 1 12/07/2016 18:25 WG932780 Thallium ND 0.00200 1 12/07/2016 18:25 WG932780 Zinc ND 0.0250 1 12/07/2016 18:25 WG932780 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 12/09/2016 16:09 WG933189 Acrylonitrile ND 0.0100 1 12/09/2016 16:09 WG933189 Benzene ND 0.00100 1 12/09/2016 16:09 WG933189 Bromochloromethane ND 0.00100 1 12/09/2016 16:09 WG933189 Bromodichloromethane ND 0.00100 1 12/09/2016 16:09 WG933189 Bromoform ND 0.00100 1 12/09/2016 16:09 WG933189 Bromomethane ND J3 0.00500 1 12/09/2016 13:28 WG933189 Carbon disulfide ND 0.00100 1 12/09/2016 16:09 WG933189 Carbon tetrachloride ND 0.00100 1 12/09/2016 16:09 WG933189 Chlorobenzene ND 0.00100 1 12/09/2016 16:09 WG933189 Chlorodibromomethane ND 0.00100 1 12/09/2016 16:09 WG933189 Chloroethane ND 0.00500 1 12/09/2016 16:09 WG933189 Chloroform ND 0.00500 1 12/09/2016 16:09 WG933189 Chloromethane ND 0.00250 1 12/09/2016 16:09 WG933189 Dibromomethane ND 0.00100 1 12/09/2016 16:09 WG933189 1,2-Dichlorobenzene ND 0.00100 1 12/09/2016 16:09 WG933189 1,4-Dichlorobenzene ND 0.00100 1 12/09/2016 16:09 WG933189 trans-1,4-Dichloro-2-butene ND 0.00250 1 12/09/2016 16:09 WG933189 1,1-Dichloroethane ND 0.00100 1 12/09/2016 16:09 WG933189 1,2-Dichloroethane ND 0.00100 1 12/09/2016 16:09 WG933189 1,1-Dichloroethene ND 0.00100 1 12/09/2016 16:09 WG933189 cis-1,2-Dichloroethene ND 0.00100 1 12/09/2016 16:09 WG933189 trans-1,2-Dichloroethene ND 0.00100 1 12/09/2016 16:09 WG933189 1,2-Dichloropropane ND 0.00100 1 12/09/2016 16:09 WG933189 cis-1,3-Dichloropropene ND 0.00100 1 12/09/2016 16:09 WG933189 trans-1,3-Dichloropropene ND 0.00100 1 12/09/2016 16:09 WG933189 Ethylbenzene ND 0.00100 1 12/09/2016 16:09 WG933189 2-Hexanone ND 0.0100 1 12/09/2016 16:09 WG933189 Iodomethane ND J4 0.0100 1 12/09/2016 16:09 WG933189 2-Butanone (MEK)ND 0.0100 1 12/09/2016 16:09 WG933189 Methylene Chloride ND 0.00500 1 12/09/2016 16:09 WG933189 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/09/2016 16:09 WG933189 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 63 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 63 of 110 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 28 L875822 MW-6 Collected date/time: 12/05/16 14:21 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Styrene ND 0.00100 1 12/09/2016 16:09 WG933189 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/09/2016 16:09 WG933189 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/09/2016 16:09 WG933189 Tetrachloroethene ND 0.00100 1 12/09/2016 16:09 WG933189 Toluene ND 0.00500 1 12/09/2016 16:09 WG933189 1,1,1-Trichloroethane ND 0.00100 1 12/09/2016 16:09 WG933189 1,1,2-Trichloroethane ND 0.00100 1 12/09/2016 16:09 WG933189 Trichloroethene ND 0.00100 1 12/09/2016 16:09 WG933189 Trichlorofluoromethane ND 0.00500 1 12/09/2016 16:09 WG933189 1,2,3-Trichloropropane ND 0.00250 1 12/09/2016 16:09 WG933189 Vinyl acetate ND 0.0100 1 12/09/2016 16:09 WG933189 Vinyl chloride ND 0.00100 1 12/09/2016 16:09 WG933189 Xylenes, Total ND 0.00300 1 12/09/2016 16:09 WG933189 (S) Toluene-d8 104 90.0-115 12/09/2016 16:09 WG933189 (S) Toluene-d8 107 90.0-115 12/09/2016 13:28 WG933189 (S) Dibromofluoromethane 108 79.0-121 12/09/2016 13:28 WG933189 (S) Dibromofluoromethane 104 79.0-121 12/09/2016 16:09 WG933189 (S) a,a,a-Trifluorotoluene 102 90.4-116 12/09/2016 16:09 WG933189 (S) a,a,a-Trifluorotoluene 102 90.4-116 12/09/2016 13:28 WG933189 (S) 4-Bromofluorobenzene 102 80.1-120 12/09/2016 13:28 WG933189 (S) 4-Bromofluorobenzene 101 80.1-120 12/09/2016 16:09 WG933189 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 64 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 64 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931570 Gravimetric Analysis by Method 2540 C-2011 L875822-12 Method Blank (MB) (MB) R3182284-1 12/03/16 01:42 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Dissolved Solids U 2.82 10.0 L875591-03 Original Sample (OS) • Duplicate (DUP) (OS) L875591-03 12/03/16 01:42 • (DUP) R3182284-4 12/03/16 01:42 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Dissolved Solids 743 711 1 4.40 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182284-2 12/03/16 01:42 • (LCSD) R3182284-3 12/03/16 01:42 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Dissolved Solids 8800 8420 8640 95.7 98.2 85.0-115 2.58 5 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 65 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 65 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932797 Gravimetric Analysis by Method 2540 C-2011 L875822-25 Method Blank (MB) (MB) R3183725-1 12/08/16 10:32 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Dissolved Solids U 2.82 10.0 L876439-02 Original Sample (OS) • Duplicate (DUP) (OS) L876439-02 12/08/16 10:32 • (DUP) R3183725-4 12/08/16 10:32 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Dissolved Solids 5560 5480 1 1.45 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183725-2 12/08/16 10:32 • (LCSD) R3183725-3 12/08/16 10:32 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Dissolved Solids 8800 8550 8790 97.2 99.9 85.0-115 2.77 5 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 66 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 66 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931590 Wet Chemistry by Method 2320 B-2011 L875822-12 Method Blank (MB) (MB) R3182429-1 12/05/16 07:25 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Alkalinity U 2.71 20.0 L876120-01 Original Sample (OS) • Duplicate (DUP) (OS) L876120-01 12/05/16 07:34 • (DUP) R3182429-3 12/05/16 07:44 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Alkalinity 63.2 64.3 1 2.00 20 L875837-18 Original Sample (OS) • Duplicate (DUP) (OS) L875837-18 12/05/16 10:31 • (DUP) R3182429-8 12/05/16 10:39 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Alkalinity 671 654 1 3.00 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182429-4 12/05/16 08:37 • (LCSD) R3182429-5 12/05/16 10:19 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Alkalinity 100 92.8 96.2 93.0 96.0 85.0-115 4.00 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 67 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 67 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932588 Wet Chemistry by Method 2320 B-2011 L875822-25 Method Blank (MB) (MB) R3183099-1 12/07/16 11:29 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Alkalinity 4.19 J 2.71 20.0 L876441-01 Original Sample (OS) • Duplicate (DUP) (OS) L876441-01 12/07/16 11:42 • (DUP) R3183099-3 12/07/16 11:50 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Alkalinity 132 134 1 2.00 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183099-4 12/07/16 12:40 • (LCSD) R3183099-8 12/07/16 16:06 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Alkalinity 100 99.5 85.8 99.0 86.0 85.0-115 15.0 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 68 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 68 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932178 Wet Chemistry by Method 365.4 L875822-20,21,22 Method Blank (MB) (MB) R3183300-1 12/07/16 14:16 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Phosphorus,Total 0.0398 J 0.0350 0.100 L875763-01 Original Sample (OS) • Duplicate (DUP) (OS) L875763-01 12/07/16 14:21 • (DUP) R3183300-4 12/07/16 14:22 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Phosphorus,Total 1.21 1.27 1 5.00 20 L876134-01 Original Sample (OS) • Duplicate (DUP) (OS) L876134-01 12/07/16 14:36 • (DUP) R3183300-5 12/07/16 14:38 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Phosphorus,Total 0.427 0.420 1 2.00 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183300-2 12/07/16 14:17 • (LCSD) R3183300-3 12/07/16 14:19 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Phosphorus,Total 1.00 1.03 0.999 103 100 90.0-110 3.00 20 L876151-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L876151-01 12/07/16 14:45 • (MS) R3183300-6 12/07/16 14:47 • (MSD) R3183300-7 12/07/16 14:48 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Phosphorus,Total 2.50 ND 2.37 2.29 91.0 88.0 1 90.0-110 J6 3.00 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 69 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 69 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931630 Wet Chemistry by Method 410.4 L875822-20,21,22 Method Blank (MB) (MB) R3182204-1 12/02/16 20:26 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l COD U 3.00 10.0 L875790-01 Original Sample (OS) • Duplicate (DUP) (OS) L875790-01 12/02/16 20:27 • (DUP) R3182204-4 12/02/16 20:27 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% COD 22.8 22.5 1 1.00 20 L875836-09 Original Sample (OS) • Duplicate (DUP) (OS) L875836-09 12/02/16 20:30 • (DUP) R3182204-7 12/02/16 20:32 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% COD 10.4 ND 1 12.0 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182204-2 12/02/16 20:26 • (LCSD) R3182204-3 12/02/16 20:26 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% COD 242 244 241 101 99.0 90.0-110 1.00 20 L875836-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L875836-03 12/02/16 20:29 • (MS) R3182204-5 12/02/16 20:29 • (MSD) R3182204-6 12/02/16 20:29 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% COD 400 21.7 435 424 103 101 1 80.0-120 3.00 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 70 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 70 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931445 Wet Chemistry by Method 5210 B-2011 L875822-20,21,22 Method Blank (MB) (MB) R3182990-1 12/07/16 11:27 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l BOD U 1 1.00 L875804-02 Original Sample (OS) • Duplicate (DUP) (OS) L875804-02 12/07/16 09:59 • (DUP) R3182990-5 12/07/16 10:02 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% BOD ND 0.000 1 0 30 L875836-09 Original Sample (OS) • Duplicate (DUP) (OS) L875836-09 12/07/16 10:25 • (DUP) R3182990-6 12/07/16 10:27 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% BOD ND 0.000 1 0 30 L875834-01 Original Sample (OS) • Duplicate (DUP) (OS) L875834-01 12/07/16 10:47 • (DUP) R3182990-7 12/07/16 10:48 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% BOD 7.20 8.50 1 17 30 Laboratory Control Sample (LCS) (LCS) R3182990-2 12/07/16 09:44 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% BOD 198 197 99.7 84.6-115 Laboratory Control Sample (LCS) (LCS) R3182990-3 12/07/16 10:38 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% BOD 198 201 102 84.6-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 71 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 71 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931445 Wet Chemistry by Method 5210 B-2011 L875822-20,21,22 Laboratory Control Sample (LCS) (LCS) R3182990-4 12/07/16 11:26 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% BOD 198 176 88.7 84.6-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 72 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 72 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931491 Wet Chemistry by Method 9056A L875822-20,21,22 Method Blank (MB) (MB) R3182241-1 12/02/16 19:52 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Nitrate U 0.0227 0.100 Sulfate U 0.0774 5.00 L875818-07 Original Sample (OS) • Duplicate (DUP) (OS) L875818-07 12/02/16 23:35 • (DUP) R3182241-5 12/02/16 23:50 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Nitrate ND 0.000 1 0 15 Sulfate 5.18 11.5 1 76 P1 15 L875837-15 Original Sample (OS) • Duplicate (DUP) (OS) L875837-15 12/03/16 02:19 • (DUP) R3182241-6 12/03/16 02:34 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Nitrate U 0.000 1 0 15 Sulfate 3.17 3.19 1 1 J 15 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182241-2 12/02/16 20:06 • (LCSD) R3182241-3 12/02/16 20:21 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Nitrate 8.00 7.90 7.92 99 99 80-120 0 15 Sulfate 40.0 39.1 39.1 98 98 80-120 0 15 L875837-17 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L875837-17 12/03/16 03:04 • (MS) R3182241-7 12/03/16 03:19 • (MSD) R3182241-8 12/03/16 03:34 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Nitrate 5.00 U 4.85 4.81 97 96 1 80-120 1 15 Sulfate 50.0 26.2 74.7 74.8 97 97 1 80-120 0 15 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 73 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 73 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931491 Wet Chemistry by Method 9056A L875822-20,21,22 L875809-04 Original Sample (OS) • Matrix Spike (MS) (OS) L875809-04 12/02/16 22:06 • (MS) R3182241-4 12/02/16 23:05 Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier Analyte mg/l mg/l mg/l %% Sulfate 50.0 31.3 75.3 88 1 80-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 74 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 74 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931818 Wet Chemistry by Method 9056A L875822-12 Method Blank (MB) (MB) R3182594-1 12/05/16 10:04 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Chloride 0.125 J 0.0519 1.00 Sulfate 0.118 J 0.0774 5.00 L875818-01 Original Sample (OS) • Duplicate (DUP) (OS) L875818-01 12/05/16 11:24 • (DUP) R3182594-4 12/05/16 11:38 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Chloride 209 208 10 0 15 Sulfate 591 588 10 1 15 L875829-31 Original Sample (OS) • Duplicate (DUP) (OS) L875829-31 12/05/16 14:52 • (DUP) R3182594-6 12/05/16 15:07 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Chloride 28.0 30.1 1 7 15 Sulfate U 0.000 1 0 15 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182594-2 12/05/16 10:19 • (LCSD) R3182594-3 12/05/16 10:34 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Chloride 40.0 40.0 39.5 100 99 80-120 1 15 Sulfate 40.0 39.9 39.7 100 99 80-120 0 15 L875818-02 Original Sample (OS) • Matrix Spike (MS) (OS) L875818-02 12/05/16 11:53 • (MS) R3182594-5 12/05/16 12:08 Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier Analyte mg/l mg/l mg/l %% Sulfate 50.0 14.0 64.4 101 1 80-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 75 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 75 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932605 Wet Chemistry by Method 9056A L875822-25 Method Blank (MB) (MB) R3183265-1 12/07/16 07:00 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Chloride U 0.0519 1.00 Sulfate U 0.0774 5.00 L875924-01 Original Sample (OS) • Duplicate (DUP) (OS) L875924-01 12/07/16 11:08 • (DUP) R3183265-5 12/07/16 11:23 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Chloride 19.3 19.3 1 0 15 Sulfate 65.5 65.5 1 0 15 L876290-01 Original Sample (OS) • Duplicate (DUP) (OS) L876290-01 12/07/16 15:06 • (DUP) R3183265-6 12/07/16 15:21 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l %% Sulfate 8.58 8.61 1 0 15 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183265-2 12/07/16 07:15 • (LCSD) R3183265-3 12/07/16 07:30 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Chloride 40.0 38.7 38.8 97 97 80-120 0 15 Sulfate 40.0 39.4 39.4 98 99 80-120 0 15 L875822-25 Original Sample (OS) • Matrix Spike (MS) (OS) L875822-25 12/07/16 10:38 • (MS) R3183265-4 12/07/16 10:53 Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier Analyte mg/l mg/l mg/l %% Chloride 50.0 5.23 54.8 99 1 80-120 Sulfate 50.0 7.35 57.9 101 1 80-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 76 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 76 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932605 Wet Chemistry by Method 9056A L875822-25 L876290-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L876290-02 12/07/16 15:36 • (MS) R3183265-7 12/07/16 15:51 • (MSD) R3183265-8 12/07/16 16:06 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Sulfate 50.0 ND 49.5 49.5 99 99 1 80-120 0 15 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 77 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 77 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931506 Metals (ICP) by Method 6010C L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21 Method Blank (MB) (MB) R3182600-1 12/06/16 06:39 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Barium U 0.0017 0.00500 Chromium U 0.0014 0.0100 Cobalt U 0.0023 0.0100 Nickel U 0.0049 0.0100 Silver U 0.0028 0.00500 Vanadium U 0.0024 0.0200 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182600-2 12/06/16 06:42 • (LCSD) R3182600-3 12/06/16 06:44 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Barium 1.00 1.03 1.04 103 104 80-120 1 20 Chromium 1.00 0.973 0.977 97 98 80-120 0 20 Cobalt 1.00 1.00 1.01 100 101 80-120 1 20 Nickel 1.00 0.955 0.958 95 96 80-120 0 20 Silver 0.200 0.173 0.173 86 87 80-120 0 20 Vanadium 1.00 0.954 0.961 95 96 80-120 1 20 L875822-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L875822-04 12/06/16 06:47 • (MS) R3182600-5 12/06/16 06:52 • (MSD) R3182600-6 12/06/16 06:55 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Barium 1.00 0.0868 1.12 1.12 103 103 1 75-125 0 20 Chromium 1.00 ND 0.952 0.954 95 95 1 75-125 0 20 Cobalt 1.00 ND 1.01 1.00 101 100 1 75-125 0 20 Nickel 1.00 ND 0.954 0.949 95 95 1 75-125 1 20 Silver 0.200 ND 0.172 0.172 86 86 1 75-125 0 20 Vanadium 1.00 ND 0.956 0.957 96 96 1 75-125 0 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 78 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 78 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931720 Metals (ICP) by Method 6010C L875822-22 Method Blank (MB) (MB) R3182402-1 12/05/16 08:18 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Barium U 0.0017 0.00500 Chromium U 0.0014 0.0100 Cobalt U 0.0023 0.0100 Nickel U 0.0049 0.0100 Silver U 0.0028 0.00500 Vanadium U 0.0024 0.0200 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182402-2 12/05/16 08:20 • (LCSD) R3182402-3 12/05/16 08:23 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Barium 1.00 1.01 1.03 101 103 80-120 2 20 Chromium 1.00 0.961 0.977 96 98 80-120 2 20 Cobalt 1.00 0.984 1.00 98 100 80-120 2 20 Nickel 1.00 0.978 0.996 98 100 80-120 2 20 Silver 0.200 0.177 0.181 89 90 80-120 2 20 Vanadium 1.00 0.994 1.03 99 103 80-120 4 20 L876003-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L876003-05 12/05/16 08:25 • (MS) R3182402-5 12/05/16 08:31 • (MSD) R3182402-6 12/05/16 08:33 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Barium 1.00 ND 1.03 1.02 103 102 1 75-125 0 20 Chromium 1.00 ND 0.967 0.975 97 98 1 75-125 1 20 Cobalt 1.00 ND 1.00 1.00 100 100 1 75-125 0 20 Nickel 1.00 ND 0.989 0.991 99 99 1 75-125 0 20 Silver 0.200 ND 0.177 0.177 89 88 1 75-125 0 20 Vanadium 1.00 ND 1.00 0.989 100 99 1 75-125 1 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 79 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 79 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932146 Metals (ICP) by Method 6010C L875822-23,24,25,26,28 Method Blank (MB) (MB) R3183085-1 12/07/16 15:14 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Barium U 0.0017 0.00500 Chromium 0.00189 J 0.0014 0.0100 Cobalt U 0.0023 0.0100 Nickel U 0.0049 0.0100 Silver U 0.0028 0.00500 Vanadium U 0.0024 0.0200 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183085-2 12/07/16 15:17 • (LCSD) R3183085-3 12/07/16 15:19 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Barium 1.00 1.04 1.04 104 104 80-120 1 20 Chromium 1.00 0.941 0.950 94 95 80-120 1 20 Cobalt 1.00 1.01 1.02 101 102 80-120 1 20 Nickel 1.00 0.999 1.01 100 101 80-120 1 20 Silver 0.200 0.182 0.183 91 91 80-120 1 20 Vanadium 1.00 0.985 0.987 99 99 80-120 0 20 L875822-26 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L875822-26 12/07/16 15:22 • (MS) R3183085-5 12/07/16 15:33 • (MSD) R3183085-6 12/07/16 15:36 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Barium 1.00 0.0401 1.07 1.07 103 103 1 75-125 0 20 Chromium 1.00 ND 0.947 0.943 95 94 1 75-125 0 20 Cobalt 1.00 ND 1.01 1.01 101 101 1 75-125 1 20 Nickel 1.00 ND 1.00 0.998 100 100 1 75-125 0 20 Silver 0.200 ND 0.182 0.181 91 91 1 75-125 0 20 Vanadium 1.00 ND 0.984 0.980 98 98 1 75-125 0 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 80 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 80 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931509 Metals (ICPMS) by Method 6020 L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21 Method Blank (MB) (MB) R3182477-1 12/05/16 11:00 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Antimony U 0.000754 0.00200 Arsenic U 0.00025 0.00200 Beryllium U 0.00012 0.00200 Cadmium U 0.00016 0.00100 Copper U 0.00052 0.00500 Lead U 0.00024 0.00200 Selenium U 0.00038 0.00200 Thallium U 0.00019 0.00200 Zinc U 0.00256 0.0250 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182477-2 12/05/16 11:03 • (LCSD) R3182477-3 12/05/16 11:07 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Antimony 0.0579 0.0489 0.0486 84 84 80-120 1 20 Arsenic 0.0500 0.0481 0.0477 96 95 80-120 1 20 Beryllium 0.0500 0.0442 0.0428 88 86 80-120 3 20 Cadmium 0.0500 0.0507 0.0519 101 104 80-120 2 20 Copper 0.0500 0.0550 0.0541 110 108 80-120 2 20 Lead 0.0500 0.0494 0.0490 99 98 80-120 1 20 Selenium 0.0500 0.0541 0.0519 108 104 80-120 4 20 Thallium 0.0500 0.0468 0.0459 94 92 80-120 2 20 Zinc 0.0500 0.0511 0.0498 102 100 80-120 3 20 L875822-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L875822-06 12/05/16 11:10 • (MS) R3182477-5 12/05/16 11:17 • (MSD) R3182477-6 12/05/16 11:21 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Antimony 0.0579 ND 0.0498 0.0502 86 87 1 75-125 1 20 Arsenic 0.0500 ND 0.0472 0.0478 93 94 1 75-125 1 20 Beryllium 0.0500 ND 0.0424 0.0425 84 85 1 75-125 0 20 Cadmium 0.0500 ND 0.0525 0.0526 105 105 1 75-125 0 20 Copper 0.0500 ND 0.0553 0.0551 108 107 1 75-125 0 20 Lead 0.0500 0.00335 0.0534 0.0541 100 101 1 75-125 1 20 Selenium 0.0500 ND 0.0540 0.0547 106 107 1 75-125 1 20 Thallium 0.0500 ND 0.0470 0.0477 94 95 1 75-125 2 20 Zinc 0.0500 ND 0.0628 0.0603 102 97 1 75-125 4 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 81 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 81 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931723 Metals (ICPMS) by Method 6020 L875822-22 Method Blank (MB) (MB) R3182667-1 12/06/16 10:37 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Antimony U 0.000754 0.00200 Arsenic U 0.00025 0.00200 Beryllium U 0.00012 0.00200 Cadmium U 0.00016 0.00100 Lead U 0.00024 0.00200 Selenium U 0.00038 0.00200 Thallium U 0.00019 0.00200 Zinc U 0.00256 0.0250 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182667-2 12/06/16 10:40 • (LCSD) R3182667-3 12/06/16 10:44 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Antimony 0.0579 0.0504 0.0503 87 87 80-120 0 20 Arsenic 0.0500 0.0482 0.0480 96 96 80-120 1 20 Beryllium 0.0500 0.0455 0.0458 91 92 80-120 1 20 Cadmium 0.0500 0.0520 0.0520 104 104 80-120 0 20 Lead 0.0500 0.0480 0.0482 96 96 80-120 0 20 Selenium 0.0500 0.0543 0.0526 109 105 80-120 3 20 Thallium 0.0500 0.0480 0.0481 96 96 80-120 0 20 Zinc 0.0500 0.0494 0.0480 99 96 80-120 3 20 L875797-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L875797-02 12/06/16 10:47 • (MS) R3182667-5 12/06/16 10:55 • (MSD) R3182667-6 12/06/16 10:58 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Antimony 0.0579 U 0.0517 0.0517 89 89 1 75-125 0 20 Arsenic 0.0500 0.000331 0.0464 0.0469 92 93 1 75-125 1 20 Beryllium 0.0500 U 0.0452 0.0449 90 90 1 75-125 1 20 Cadmium 0.0500 U 0.0504 0.0507 101 101 1 75-125 1 20 Lead 0.0500 U 0.0480 0.0482 96 96 1 75-125 0 20 Selenium 0.0500 0.00872 0.0598 0.0609 102 104 1 75-125 2 20 Thallium 0.0500 U 0.0476 0.0480 95 96 1 75-125 1 20 Zinc 0.0500 0.00315 0.0461 0.0637 86 121 1 75-125 J3 32 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 82 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 82 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932285 Metals (ICPMS) by Method 6020 L875822-23,24,25,26 Method Blank (MB) (MB) R3182868-1 12/07/16 01:11 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Antimony U 0.000754 0.00200 Arsenic U 0.00025 0.00200 Beryllium U 0.00012 0.00200 Cadmium U 0.00016 0.00100 Copper U 0.00052 0.00500 Lead U 0.00024 0.00200 Selenium U 0.00038 0.00200 Thallium U 0.00019 0.00200 Zinc 0.00363 J 0.00256 0.0250 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182868-2 12/07/16 01:14 • (LCSD) R3182868-3 12/07/16 01:18 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Antimony 0.0579 0.0539 0.0514 93 89 80-120 5 20 Arsenic 0.0500 0.0489 0.0478 98 96 80-120 2 20 Beryllium 0.0500 0.0469 0.0455 94 91 80-120 3 20 Cadmium 0.0500 0.0488 0.0472 98 94 80-120 3 20 Copper 0.0500 0.0528 0.0499 106 100 80-120 6 20 Lead 0.0500 0.0470 0.0460 94 92 80-120 2 20 Selenium 0.0500 0.0502 0.0479 100 96 80-120 5 20 Thallium 0.0500 0.0469 0.0456 94 91 80-120 3 20 Zinc 0.0500 0.0550 0.0505 110 101 80-120 8 20 L876291-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L876291-13 12/07/16 01:21 • (MS) R3182868-5 12/07/16 01:28 • (MSD) R3182868-6 12/07/16 01:32 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Antimony 0.0579 U 0.0532 0.0537 92 93 1 75-125 1 20 Arsenic 0.0500 0.0739 0.120 0.120 93 92 1 75-125 0 20 Beryllium 0.0500 U 0.0449 0.0451 90 90 1 75-125 0 20 Cadmium 0.0500 U 0.0472 0.0495 94 99 1 75-125 5 20 Copper 0.0500 0.000946 0.0465 0.0479 91 94 1 75-125 3 20 Lead 0.0500 U 0.0461 0.0463 92 93 1 75-125 1 20 Selenium 0.0500 U 0.0504 0.0484 101 97 1 75-125 4 20 Thallium 0.0500 U 0.0461 0.0465 92 93 1 75-125 1 20 Zinc 0.0500 0.00626 0.0498 0.0507 87 89 1 75-125 2 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 83 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 83 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932463 Metals (ICPMS) by Method 6020 L875822-22 Method Blank (MB) (MB) R3182825-1 12/06/16 19:10 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Copper U 0.00052 0.00500 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3182825-2 12/06/16 19:13 • (LCSD) R3182825-3 12/06/16 19:17 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Copper 0.0500 0.0475 0.0499 95 100 80-120 5 20 L876441-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L876441-05 12/06/16 19:20 • (MS) R3182825-5 12/06/16 19:28 • (MSD) R3182825-6 12/06/16 19:31 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Copper 0.0500 U 0.0434 0.0441 87 88 1 75-125 2 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 84 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 84 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932780 Metals (ICPMS) by Method 6020 L875822-28 Method Blank (MB) (MB) R3183132-1 12/07/16 17:31 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Antimony U 0.000754 0.00200 Arsenic U 0.00025 0.00200 Beryllium U 0.00012 0.00200 Cadmium U 0.00016 0.00100 Copper U 0.00052 0.00500 Lead U 0.00024 0.00200 Selenium U 0.00038 0.00200 Thallium U 0.00019 0.00200 Zinc U 0.00256 0.0250 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183132-2 12/07/16 17:35 • (LCSD) R3183132-3 12/07/16 17:38 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Antimony 0.0579 0.0520 0.0514 90 89 80-120 1 20 Arsenic 0.0500 0.0472 0.0459 94 92 80-120 3 20 Beryllium 0.0500 0.0444 0.0438 89 88 80-120 1 20 Cadmium 0.0500 0.0519 0.0507 104 101 80-120 2 20 Copper 0.0500 0.0509 0.0496 102 99 80-120 3 20 Lead 0.0500 0.0478 0.0470 96 94 80-120 2 20 Selenium 0.0500 0.0502 0.0480 100 96 80-120 4 20 Thallium 0.0500 0.0473 0.0470 95 94 80-120 1 20 Zinc 0.0500 0.0471 0.0450 94 90 80-120 5 20 L876653-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L876653-08 12/07/16 17:42 • (MS) R3183132-5 12/07/16 17:49 • (MSD) R3183132-6 12/07/16 17:52 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Antimony 0.0579 ND 0.0502 0.0504 87 87 1 75-125 0 20 Arsenic 0.0500 ND 0.0481 0.0461 96 92 1 75-125 4 20 Beryllium 0.0500 ND 0.0440 0.0434 88 87 1 75-125 1 20 Cadmium 0.0500 ND 0.0529 0.0523 106 105 1 75-125 1 20 Copper 0.0500 ND 0.0530 0.0517 103 100 1 75-125 2 20 Lead 0.0500 ND 0.0477 0.0477 95 95 1 75-125 0 20 Selenium 0.0500 ND 0.0489 0.0468 98 94 1 75-125 4 20 Thallium 0.0500 ND 0.0472 0.0473 94 95 1 75-125 0 20 Zinc 0.0500 ND 0.0488 0.0469 98 94 1 75-125 4 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 85 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 85 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931552 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3183096-3 12/04/16 17:07 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Acetone U 0.0100 0.0500 Acrylonitrile U 0.00187 0.0100 Benzene U 0.000331 0.00100 Bromodichloromethane U 0.000380 0.00100 Bromochloromethane U 0.000520 0.00100 Bromoform U 0.000469 0.00100 Bromomethane U 0.000866 0.00500 Carbon disulfide U 0.000275 0.00100 Carbon tetrachloride U 0.000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0.000453 0.00500 Chloroform U 0.000324 0.00500 Chloromethane U 0.000276 0.00250 Dibromomethane U 0.000346 0.00100 1,2-Dichlorobenzene U 0.000349 0.00100 1,4-Dichlorobenzene U 0.000274 0.00100 trans-1,4-Dichloro-2-butene U 0.000866 0.00250 1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 1,1-Dichloroethene U 0.000398 0.00100 cis-1,2-Dichloroethene U 0.000260 0.00100 trans-1,2-Dichloroethene U 0.000396 0.00100 1,2-Dichloropropane U 0.000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0.000419 0.00100 Ethylbenzene U 0.000384 0.00100 2-Hexanone U 0.00382 0.0100 Iodomethane U 0.00171 0.0100 2-Butanone (MEK)U 0.00393 0.0100 Methylene Chloride U 0.00100 0.00500 4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100 Styrene U 0.000307 0.00100 1,1,1,2-Tetrachloroethane U 0.000385 0.00100 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000780 0.00500 1,1,1-Trichloroethane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 86 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 86 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931552 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3183096-3 12/04/16 17:07 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Trichlorofluoromethane U 0.00120 0.00500 1,2,3-Trichloropropane U 0.000807 0.00250 Vinyl chloride U 0.000259 0.00100 Xylenes, Total U 0.00106 0.00300 (S) Toluene-d8 102 90.0-115 (S) Dibromofluoromethane 98.6 79.0-121 (S) a,a,a-Trifluorotoluene 105 90.4-116 (S) 4-Bromofluorobenzene 104 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183096-1 12/04/16 15:58 • (LCSD) R3183096-2 12/04/16 16:21 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Acetone 0.125 0.112 0.114 89.3 91.4 28.7-175 2.31 20.9 Acrylonitrile 0.125 0.134 0.127 107 102 58.2-145 5.40 20 Benzene 0.0250 0.0262 0.0258 105 103 73.0-122 1.45 20 Bromodichloromethane 0.0250 0.0277 0.0277 111 111 75.5-121 0.200 20 Bromochloromethane 0.0250 0.0299 0.0285 120 114 78.9-123 4.63 20 Bromoform 0.0250 0.0276 0.0269 110 108 71.5-131 2.49 20 Bromomethane 0.0250 0.0189 0.0198 75.5 79.1 22.4-187 4.74 20 Carbon disulfide 0.0250 0.0233 0.0230 93.2 92.1 53.0-134 1.12 20 Carbon tetrachloride 0.0250 0.0261 0.0264 104 106 70.9-129 1.37 20 Chlorobenzene 0.0250 0.0286 0.0286 114 115 79.7-122 0.200 20 Chlorodibromomethane 0.0250 0.0284 0.0286 114 114 78.2-124 0.850 20 Chloroethane 0.0250 0.0285 0.0294 114 117 41.2-153 2.87 20 Chloroform 0.0250 0.0283 0.0277 113 111 73.2-125 1.96 20 Chloromethane 0.0250 0.0173 0.0180 69.4 71.9 55.8-134 3.57 20 Dibromomethane 0.0250 0.0266 0.0266 106 107 79.5-118 0.230 20 1,2-Dichlorobenzene 0.0250 0.0286 0.0286 115 114 84.7-118 0.150 20 1,4-Dichlorobenzene 0.0250 0.0263 0.0268 105 107 82.2-114 2.02 20 trans-1,4-Dichloro-2-butene 0.0250 0.0273 0.0272 109 109 58.3-129 0.510 20 1,1-Dichloroethane 0.0250 0.0273 0.0273 109 109 71.7-127 0.210 20 1,2-Dichloroethane 0.0250 0.0263 0.0263 105 105 65.3-126 0.190 20 1,1-Dichloroethene 0.0250 0.0256 0.0253 102 101 59.9-137 0.960 20 cis-1,2-Dichloroethene 0.0250 0.0284 0.0282 113 113 77.3-122 0.460 20 trans-1,2-Dichloroethene 0.0250 0.0278 0.0278 111 111 72.6-125 0.110 20 1,2-Dichloropropane 0.0250 0.0277 0.0280 111 112 77.4-125 0.990 20 cis-1,3-Dichloropropene 0.0250 0.0289 0.0289 115 115 77.7-124 0.0400 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 87 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 87 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931552 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183096-1 12/04/16 15:58 • (LCSD) R3183096-2 12/04/16 16:21 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% trans-1,3-Dichloropropene 0.0250 0.0300 0.0300 120 120 73.5-127 0.100 20 Ethylbenzene 0.0250 0.0278 0.0281 111 112 80.9-121 1.00 20 2-Hexanone 0.125 0.138 0.134 111 107 59.4-151 2.85 20 Iodomethane 0.125 0.0734 0.0777 58.7 62.2 64.6-137 J4 J4 5.69 20 2-Butanone (MEK)0.125 0.130 0.124 104 99.2 46.4-155 4.66 20 Methylene Chloride 0.0250 0.0249 0.0245 99.7 97.9 69.5-120 1.85 20 4-Methyl-2-pentanone (MIBK)0.125 0.127 0.127 102 101 63.3-138 0.620 20 Styrene 0.0250 0.0283 0.0294 113 118 79.9-124 3.67 20 1,1,1,2-Tetrachloroethane 0.0250 0.0276 0.0281 111 112 78.5-125 1.66 20 1,1,2,2-Tetrachloroethane 0.0250 0.0258 0.0260 103 104 79.3-123 0.990 20 Tetrachloroethene 0.0250 0.0274 0.0279 110 112 73.5-130 2.01 20 Toluene 0.0250 0.0277 0.0280 111 112 77.9-116 1.34 20 1,1,1-Trichloroethane 0.0250 0.0271 0.0276 109 110 71.1-129 1.56 20 1,1,2-Trichloroethane 0.0250 0.0269 0.0266 107 106 81.6-120 1.07 20 Trichloroethene 0.0250 0.0276 0.0283 110 113 79.5-121 2.54 20 Trichlorofluoromethane 0.0250 0.0284 0.0282 113 113 49.1-157 0.690 20 1,2,3-Trichloropropane 0.0250 0.0275 0.0274 110 110 74.9-124 0.300 20 Vinyl chloride 0.0250 0.0276 0.0272 110 109 61.5-134 1.57 20 Xylenes, Total 0.0750 0.0832 0.0835 111 111 79.2-122 0.430 20 (S) Toluene-d8 104 103 90.0-115 (S) Dibromofluoromethane 102 98.4 79.0-121 (S) a,a,a-Trifluorotoluene 104 105 90.4-116 (S) 4-Bromofluorobenzene 102 102 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183281-4 12/07/16 22:01 • (LCSD) R3183281-6 12/08/16 03:02 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Vinyl acetate 0.125 0.111 0.107 89.0 85.6 41.7-159 3.91 20 (S) Toluene-d8 100 101 90.0-115 (S) Dibromofluoromethane 88.2 89.6 79.0-121 (S) a,a,a-Trifluorotoluene 100 101 90.4-116 (S) 4-Bromofluorobenzene 97.5 96.5 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 88 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 88 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22 Method Blank (MB) (MB) R3183112-4 12/04/16 14:27 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Acetone U 0.0100 0.0500 Acrylonitrile U 0.00187 0.0100 Benzene U 0.000331 0.00100 Bromodichloromethane U 0.000380 0.00100 Bromochloromethane U 0.000520 0.00100 Bromoform U 0.000469 0.00100 Bromomethane U 0.000866 0.00500 Carbon disulfide U 0.000275 0.00100 Carbon tetrachloride U 0.000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0.000453 0.00500 Chloroform U 0.000324 0.00500 Chloromethane U 0.000276 0.00250 Dibromomethane U 0.000346 0.00100 1,2-Dichlorobenzene U 0.000349 0.00100 1,4-Dichlorobenzene U 0.000274 0.00100 trans-1,4-Dichloro-2-butene U 0.000866 0.00250 1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 1,1-Dichloroethene U 0.000398 0.00100 cis-1,2-Dichloroethene U 0.000260 0.00100 trans-1,2-Dichloroethene U 0.000396 0.00100 1,2-Dichloropropane U 0.000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0.000419 0.00100 Ethylbenzene U 0.000384 0.00100 2-Hexanone U 0.00382 0.0100 Iodomethane U 0.00171 0.0100 2-Butanone (MEK)U 0.00393 0.0100 Methylene Chloride U 0.00100 0.00500 4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100 Styrene U 0.000307 0.00100 1,1,1,2-Tetrachloroethane U 0.000385 0.00100 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000780 0.00500 1,1,1-Trichloroethane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 89 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 89 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22 Method Blank (MB) (MB) R3183112-4 12/04/16 14:27 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Trichlorofluoromethane U 0.00120 0.00500 1,2,3-Trichloropropane U 0.000807 0.00250 Vinyl acetate U 0.00163 0.0100 Vinyl chloride U 0.000259 0.00100 Xylenes, Total U 0.00106 0.00300 (S) Toluene-d8 105 90.0-115 (S) Dibromofluoromethane 104 79.0-121 (S) a,a,a-Trifluorotoluene 107 90.4-116 (S) 4-Bromofluorobenzene 104 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183112-1 12/04/16 11:08 • (LCSD) R3183112-2 12/04/16 11:28 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Acetone 0.125 0.174 0.170 139 136 28.7-175 2.29 20.9 Acrylonitrile 0.125 0.141 0.143 113 115 58.2-145 1.51 20 Benzene 0.0250 0.0250 0.0247 100 98.8 73.0-122 1.37 20 Bromodichloromethane 0.0250 0.0237 0.0232 94.9 92.7 75.5-121 2.33 20 Bromochloromethane 0.0250 0.0256 0.0255 102 102 78.9-123 0.260 20 Bromoform 0.0250 0.0255 0.0256 102 103 71.5-131 0.670 20 Bromomethane 0.0250 0.0258 0.0233 103 93.4 22.4-187 10.0 20 Carbon disulfide 0.0250 0.0216 0.0212 86.5 84.7 53.0-134 2.01 20 Carbon tetrachloride 0.0250 0.0240 0.0236 96.2 94.5 70.9-129 1.72 20 Chlorobenzene 0.0250 0.0261 0.0255 104 102 79.7-122 2.20 20 Chlorodibromomethane 0.0250 0.0259 0.0257 104 103 78.2-124 0.760 20 Chloroethane 0.0250 0.0253 0.0245 101 98.2 41.2-153 3.07 20 Chloroform 0.0250 0.0248 0.0243 99.3 97.1 73.2-125 2.26 20 Chloromethane 0.0250 0.0246 0.0236 98.4 94.3 55.8-134 4.19 20 Dibromomethane 0.0250 0.0246 0.0245 98.5 98.1 79.5-118 0.320 20 1,2-Dichlorobenzene 0.0250 0.0265 0.0262 106 105 84.7-118 1.09 20 1,4-Dichlorobenzene 0.0250 0.0249 0.0249 99.5 99.4 82.2-114 0.0300 20 trans-1,4-Dichloro-2-butene 0.0250 0.0257 0.0255 103 102 58.3-129 0.480 20 1,1-Dichloroethane 0.0250 0.0258 0.0257 103 103 71.7-127 0.150 20 1,2-Dichloroethane 0.0250 0.0234 0.0230 93.6 92.1 65.3-126 1.56 20 1,1-Dichloroethene 0.0250 0.0216 0.0212 86.2 84.9 59.9-137 1.56 20 cis-1,2-Dichloroethene 0.0250 0.0256 0.0255 102 102 77.3-122 0.280 20 trans-1,2-Dichloroethene 0.0250 0.0259 0.0253 103 101 72.6-125 2.00 20 1,2-Dichloropropane 0.0250 0.0252 0.0248 101 99.1 77.4-125 1.54 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 90 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 90 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183112-1 12/04/16 11:08 • (LCSD) R3183112-2 12/04/16 11:28 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% cis-1,3-Dichloropropene 0.0250 0.0262 0.0262 105 105 77.7-124 0.0400 20 trans-1,3-Dichloropropene 0.0250 0.0247 0.0248 98.6 99.1 73.5-127 0.510 20 Ethylbenzene 0.0250 0.0260 0.0254 104 102 80.9-121 2.40 20 2-Hexanone 0.125 0.128 0.127 102 102 59.4-151 0.190 20 Iodomethane 0.125 0.114 0.113 91.2 90.1 64.6-137 1.22 20 2-Butanone (MEK)0.125 0.131 0.133 105 107 46.4-155 1.79 20 Methylene Chloride 0.0250 0.0233 0.0229 93.2 91.4 69.5-120 1.90 20 4-Methyl-2-pentanone (MIBK)0.125 0.126 0.125 100 99.8 63.3-138 0.670 20 Styrene 0.0250 0.0263 0.0256 105 102 79.9-124 2.62 20 1,1,1,2-Tetrachloroethane 0.0250 0.0266 0.0255 106 102 78.5-125 4.37 20 1,1,2,2-Tetrachloroethane 0.0250 0.0246 0.0245 98.5 98.2 79.3-123 0.310 20 Tetrachloroethene 0.0250 0.0264 0.0255 106 102 73.5-130 3.33 20 Toluene 0.0250 0.0243 0.0238 97.2 95.3 77.9-116 2.01 20 1,1,1-Trichloroethane 0.0250 0.0250 0.0240 100 96.0 71.1-129 4.21 20 1,1,2-Trichloroethane 0.0250 0.0247 0.0247 98.8 98.7 81.6-120 0.140 20 Trichloroethene 0.0250 0.0256 0.0252 102 101 79.5-121 1.65 20 Trichlorofluoromethane 0.0250 0.0220 0.0219 88.0 87.7 49.1-157 0.410 20 1,2,3-Trichloropropane 0.0250 0.0254 0.0251 102 100 74.9-124 1.32 20 Vinyl acetate 0.125 0.128 0.127 103 102 41.7-159 0.720 20 Vinyl chloride 0.0250 0.0271 0.0263 108 105 61.5-134 2.84 20 Xylenes, Total 0.0750 0.0779 0.0765 104 102 79.2-122 1.77 20 (S) Toluene-d8 105 104 90.0-115 (S) Dibromofluoromethane 107 107 79.0-121 (S) a,a,a-Trifluorotoluene 105 105 90.4-116 (S) 4-Bromofluorobenzene 103 101 80.1-120 L875828-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L875828-05 12/04/16 20:56 • (MS) R3183112-5 12/04/16 21:16 • (MSD) R3183112-6 12/04/16 21:36 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Acetone 0.125 31.2 87.8 85.3 90.6 86.6 500 25.0-156 2.88 21.5 Acrylonitrile 0.125 ND 76.3 71.0 122 114 500 55.9-161 7.19 20 Benzene 0.0250 0.409 13.1 12.6 101 97.6 500 58.6-133 3.80 20 Bromodichloromethane 0.0250 ND 12.5 12.1 100 96.6 500 69.2-127 3.53 20 Bromochloromethane 0.0250 ND 13.3 12.7 106 102 500 74.4-128 4.25 20 Bromoform 0.0250 ND 14.1 14.0 113 112 500 66.3-140 1.26 20 Bromomethane 0.0250 ND 11.9 11.1 94.9 88.9 500 16.6-183 6.51 20.5 Carbon disulfide 0.0250 ND 10.2 10.2 81.3 81.2 500 34.9-138 0.0700 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 91 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 91 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22 L875828-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L875828-05 12/04/16 20:56 • (MS) R3183112-5 12/04/16 21:16 • (MSD) R3183112-6 12/04/16 21:36 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Carbon tetrachloride 0.0250 ND 12.2 11.9 97.8 95.5 500 60.6-139 2.36 20 Chlorobenzene 0.0250 ND 13.9 13.4 111 107 500 70.1-130 3.21 20 Chlorodibromomethane 0.0250 ND 14.1 14.0 113 112 500 71.6-132 0.690 20 Chloroethane 0.0250 ND 12.2 11.9 97.6 95.5 500 33.3-155 2.22 20 Chloroform 0.0250 0.467 13.1 12.4 101 95.6 500 66.1-133 5.07 20 Chloromethane 0.0250 ND 10.9 10.4 87.0 83.2 500 40.7-139 4.48 20 Dibromomethane 0.0250 ND 12.9 12.5 103 99.8 500 72.8-127 3.31 20 1,2-Dichlorobenzene 0.0250 ND 13.7 13.5 109 108 500 77.4-127 1.03 20 1,4-Dichlorobenzene 0.0250 ND 12.9 12.6 103 101 500 74.4-123 2.34 20 trans-1,4-Dichloro-2-butene 0.0250 ND 12.7 12.5 102 100 500 57.6-136 1.77 20 1,1-Dichloroethane 0.0250 ND 13.5 12.8 108 102 500 64.0-134 5.23 20 1,2-Dichloroethane 0.0250 ND 12.3 11.9 98.0 94.8 500 60.7-132 3.30 20 1,1-Dichloroethene 0.0250 ND 11.6 10.9 92.8 87.5 500 48.8-144 5.96 20 cis-1,2-Dichloroethene 0.0250 ND 13.3 12.4 106 99.1 500 60.6-136 7.05 20 trans-1,2-Dichloroethene 0.0250 ND 12.8 12.1 103 96.5 500 61.0-132 6.09 20 1,2-Dichloropropane 0.0250 ND 13.1 12.7 105 102 500 69.7-130 3.42 20 cis-1,3-Dichloropropene 0.0250 ND 13.6 13.2 108 106 500 71.1-129 2.59 20 trans-1,3-Dichloropropene 0.0250 ND 12.8 12.5 102 99.9 500 66.3-136 2.47 20 Ethylbenzene 0.0250 1.66 15.2 14.8 108 105 500 62.7-136 2.98 20 2-Hexanone 0.125 ND 66.1 64.9 106 104 500 59.4-154 1.92 20.1 Iodomethane 0.125 ND 61.8 59.4 98.9 95.0 500 55.2-140 3.95 20 2-Butanone (MEK)0.125 26.6 76.9 72.6 80.5 73.6 500 45.0-156 5.74 20.8 Methylene Chloride 0.0250 ND 12.3 11.9 98.4 95.1 500 61.5-125 3.37 20 4-Methyl-2-pentanone (MIBK)0.125 47.9 117 113 110 104 500 60.7-150 3.36 20 Styrene 0.0250 ND 13.9 13.6 112 108 500 68.2-133 2.87 20 1,1,1,2-Tetrachloroethane 0.0250 ND 14.3 13.9 114 111 500 70.5-132 2.74 20 1,1,2,2-Tetrachloroethane 0.0250 ND 13.4 13.2 107 106 500 64.9-145 1.51 20 Tetrachloroethene 0.0250 ND 13.4 13.2 107 105 500 57.4-141 1.78 20 Toluene 0.0250 89.4 100 99.5 88.0 80.4 500 67.8-124 0.950 20 1,1,1-Trichloroethane 0.0250 ND 13.0 12.5 104 99.7 500 58.7-134 4.23 20 1,1,2-Trichloroethane 0.0250 ND 13.6 13.3 109 107 500 74.1-130 2.18 20 Trichloroethene 0.0250 ND 13.1 12.7 105 102 500 48.9-148 3.24 20 Trichlorofluoromethane 0.0250 ND 11.3 10.9 90.3 87.5 500 39.9-165 3.20 20 1,2,3-Trichloropropane 0.0250 ND 14.2 13.6 113 109 500 71.5-134 4.22 20 Vinyl acetate 0.125 ND 70.9 68.0 113 109 500 42.8-181 4.23 20 Vinyl chloride 0.0250 ND 12.6 11.9 101 95.5 500 44.3-143 5.26 20 Xylenes, Total 0.0750 8.64 49.7 48.3 109 106 500 65.6-133 2.72 20 (S) Toluene-d8 104 104 90.0-115 (S) Dibromofluoromethane 105 103 79.0-121 (S) a,a,a-Trifluorotoluene 106 107 90.4-116 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 92 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 92 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22 L875828-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L875828-05 12/04/16 20:56 • (MS) R3183112-5 12/04/16 21:16 • (MSD) R3183112-6 12/04/16 21:36 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% (S) 4-Bromofluorobenzene 104 103 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 93 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 93 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27 Method Blank (MB) (MB) R3183408-3 12/07/16 22:59 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Acetone 0.0254 J 0.0100 0.0500 Acrylonitrile U 0.00187 0.0100 Benzene U 0.000331 0.00100 Bromochloromethane U 0.000520 0.00100 Bromodichloromethane U 0.000380 0.00100 Bromoform U 0.000469 0.00100 Bromomethane U 0.000866 0.00500 Carbon disulfide U 0.000275 0.00100 Carbon tetrachloride U 0.000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0.000453 0.00500 Chloroform U 0.000324 0.00500 Chloromethane U 0.000276 0.00250 Dibromomethane U 0.000346 0.00100 1,2-Dichlorobenzene U 0.000349 0.00100 1,4-Dichlorobenzene U 0.000274 0.00100 trans-1,4-Dichloro-2-butene U 0.000866 0.00250 1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 1,1-Dichloroethene U 0.000398 0.00100 cis-1,2-Dichloroethene U 0.000260 0.00100 trans-1,2-Dichloroethene U 0.000396 0.00100 1,2-Dichloropropane U 0.000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0.000419 0.00100 Ethylbenzene U 0.000384 0.00100 2-Hexanone U 0.00382 0.0100 Iodomethane U 0.00171 0.0100 2-Butanone (MEK)U 0.00393 0.0100 Methylene Chloride U 0.00100 0.00500 4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100 Styrene U 0.000307 0.00100 1,1,1,2-Tetrachloroethane U 0.000385 0.00100 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000780 0.00500 1,1,1-Trichloroethane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 94 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 94 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27 Method Blank (MB) (MB) R3183408-3 12/07/16 22:59 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Trichlorofluoromethane U 0.00120 0.00500 1,2,3-Trichloropropane U 0.000807 0.00250 Vinyl acetate U 0.00163 0.0100 Vinyl chloride U 0.000259 0.00100 Xylenes, Total U 0.00106 0.00300 (S) a,a,a-Trifluorotoluene 101 90.4-116 (S) Toluene-d8 101 89.0-112 (S) Dibromofluoromethane 105 80.0-119 (S) 4-Bromofluorobenzene 94.8 85.0-114 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183408-1 12/07/16 21:00 • (LCSD) R3183408-2 12/07/16 21:28 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Bromochloromethane 0.0250 0.0292 0.0248 117 99.2 78.9-123 16.3 20 Acetone 0.125 0.226 0.170 181 136 28.7-175 J4 J3 28.3 20.9 Acrylonitrile 0.125 0.170 0.140 136 112 58.2-145 19.4 20 Benzene 0.0250 0.0283 0.0234 113 93.6 73.0-122 19.2 20 Carbon disulfide 0.0250 0.0302 0.0244 121 97.6 53.0-134 J3 21.2 20 Bromodichloromethane 0.0250 0.0261 0.0219 104 87.8 75.5-121 17.2 20 Bromoform 0.0250 0.0272 0.0231 109 92.4 71.5-131 16.5 20 Bromomethane 0.0250 0.0308 0.0261 123 104 22.4-187 16.5 20 Carbon tetrachloride 0.0250 0.0262 0.0215 105 85.9 70.9-129 19.9 20 Chlorobenzene 0.0250 0.0267 0.0221 107 88.3 79.7-122 18.8 20 Chlorodibromomethane 0.0250 0.0278 0.0233 111 93.1 78.2-124 17.7 20 Chloroethane 0.0250 0.0288 0.0239 115 95.5 41.2-153 18.6 20 Chloroform 0.0250 0.0277 0.0231 111 92.4 73.2-125 18.0 20 Chloromethane 0.0250 0.0283 0.0232 113 92.9 55.8-134 19.7 20 trans-1,4-Dichloro-2-butene 0.0250 0.0183 0.0156 73.3 62.4 58.3-129 16.0 20 Dibromomethane 0.0250 0.0284 0.0240 114 96.0 79.5-118 16.9 20 1,2-Dichlorobenzene 0.0250 0.0276 0.0233 110 93.4 84.7-118 16.6 20 1,4-Dichlorobenzene 0.0250 0.0259 0.0219 104 87.7 82.2-114 16.6 20 1,1-Dichloroethane 0.0250 0.0304 0.0249 122 99.7 71.7-127 19.8 20 1,2-Dichloroethane 0.0250 0.0285 0.0242 114 96.7 65.3-126 16.5 20 1,1-Dichloroethene 0.0250 0.0296 0.0237 118 94.6 59.9-137 J3 22.3 20 cis-1,2-Dichloroethene 0.0250 0.0287 0.0237 115 94.9 77.3-122 19.0 20 trans-1,2-Dichloroethene 0.0250 0.0291 0.0234 116 93.7 72.6-125 J3 21.5 20 1,2-Dichloropropane 0.0250 0.0293 0.0247 117 98.8 77.4-125 17.2 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 95 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 95 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183408-1 12/07/16 21:00 • (LCSD) R3183408-2 12/07/16 21:28 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% cis-1,3-Dichloropropene 0.0250 0.0289 0.0243 115 97.0 77.7-124 17.3 20 2-Hexanone 0.125 0.130 0.112 104 90.0 59.4-151 14.9 20 trans-1,3-Dichloropropene 0.0250 0.0277 0.0234 111 93.7 73.5-127 16.9 20 Iodomethane 0.125 0.153 0.127 122 102 64.6-137 18.5 20 Ethylbenzene 0.0250 0.0256 0.0209 102 83.7 80.9-121 20.0 20 2-Butanone (MEK)0.125 0.149 0.125 119 100 46.4-155 16.9 20 Methylene Chloride 0.0250 0.0281 0.0233 112 93.2 69.5-120 18.7 20 4-Methyl-2-pentanone (MIBK)0.125 0.158 0.137 126 110 63.3-138 14.2 20 Styrene 0.0250 0.0261 0.0217 105 86.7 79.9-124 18.7 20 1,1,1,2-Tetrachloroethane 0.0250 0.0273 0.0225 109 89.9 78.5-125 19.4 20 1,1,2,2-Tetrachloroethane 0.0250 0.0280 0.0233 112 93.2 79.3-123 18.2 20 Tetrachloroethene 0.0250 0.0254 0.0205 102 81.9 73.5-130 J3 21.6 20 Toluene 0.0250 0.0263 0.0216 105 86.5 77.9-116 19.5 20 1,1,1-Trichloroethane 0.0250 0.0262 0.0214 105 85.6 71.1-129 J3 20.1 20 1,1,2-Trichloroethane 0.0250 0.0266 0.0224 107 89.7 81.6-120 17.2 20 Vinyl acetate 0.125 0.170 0.141 136 113 41.7-159 18.9 20 Trichloroethene 0.0250 0.0272 0.0225 109 90.0 79.5-121 18.9 20 Trichlorofluoromethane 0.0250 0.0320 0.0252 128 101 49.1-157 J3 23.7 20 1,2,3-Trichloropropane 0.0250 0.0262 0.0221 105 88.2 74.9-124 17.1 20 Vinyl chloride 0.0250 0.0300 0.0240 120 96.1 61.5-134 J3 22.0 20 Xylenes, Total 0.0750 0.0771 0.0627 103 83.6 79.2-122 J3 20.6 20 (S) a,a,a-Trifluorotoluene 100 99.4 90.4-116 (S) Toluene-d8 100 100 89.0-112 (S) Dibromofluoromethane 106 107 80.0-119 (S) 4-Bromofluorobenzene 94.5 93.6 85.0-114 L876258-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L876258-01 12/08/16 06:01 • (MS) R3183408-4 12/08/16 00:31 • (MSD) R3183408-5 12/08/16 01:00 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Bromochloromethane 0.0250 ND 0.244 0.244 97.5 97.4 10 74.4-128 0.0900 20 Acetone 0.125 ND 1.85 1.78 137 131 10 25.0-156 4.21 21.5 Acrylonitrile 0.125 ND 1.42 1.36 113 109 10 55.9-161 3.69 20 Benzene 0.0250 0.417 0.603 0.606 74.6 75.8 10 58.6-133 0.510 20 Carbon disulfide 0.0250 ND 0.205 0.199 82.0 79.6 10 34.9-138 2.95 20 Bromodichloromethane 0.0250 ND 0.229 0.223 91.5 89.1 10 69.2-127 2.68 20 Bromoform 0.0250 ND 0.238 0.235 95.1 93.9 10 66.3-140 1.31 20 Bromomethane 0.0250 ND 0.258 0.252 103 101 10 16.6-183 2.33 20.5 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 96 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 96 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27 L876258-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L876258-01 12/08/16 06:01 • (MS) R3183408-4 12/08/16 00:31 • (MSD) R3183408-5 12/08/16 01:00 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Carbon tetrachloride 0.0250 ND 0.230 0.226 92.1 90.3 10 60.6-139 1.89 20 Chlorobenzene 0.0250 ND 0.234 0.227 93.8 90.8 10 70.1-130 3.20 20 Chlorodibromomethane 0.0250 ND 0.241 0.234 96.6 93.6 10 71.6-132 3.10 20 Chloroethane 0.0250 ND 0.247 0.241 99.0 96.5 10 33.3-155 2.56 20 Chloroform 0.0250 ND 0.242 0.239 96.8 95.4 10 66.1-133 1.43 20 Chloromethane 0.0250 ND 0.236 0.229 94.5 91.6 10 40.7-139 3.15 20 trans-1,4-Dichloro-2-butene 0.0250 ND 0.175 0.171 69.8 68.3 10 57.6-136 2.25 20 Dibromomethane 0.0250 ND 0.240 0.236 95.9 94.4 10 72.8-127 1.52 20 1,2-Dichlorobenzene 0.0250 ND 0.244 0.239 97.7 95.6 10 77.4-127 2.21 20 1,4-Dichlorobenzene 0.0250 ND 0.232 0.223 92.8 89.3 10 74.4-123 3.87 20 1,1-Dichloroethane 0.0250 ND 0.258 0.257 103 103 10 64.0-134 0.490 20 1,2-Dichloroethane 0.0250 ND 0.243 0.240 97.1 95.9 10 60.7-132 1.31 20 1,1-Dichloroethene 0.0250 ND 0.244 0.233 97.6 93.3 10 48.8-144 4.43 20 cis-1,2-Dichloroethene 0.0250 ND 0.247 0.243 97.7 96.0 10 60.6-136 1.83 20 trans-1,2-Dichloroethene 0.0250 ND 0.241 0.236 96.4 94.6 10 61.0-132 1.95 20 1,2-Dichloropropane 0.0250 0.0119 0.255 0.251 97.3 95.8 10 69.7-130 1.58 20 cis-1,3-Dichloropropene 0.0250 ND 0.248 0.242 99.3 96.9 10 71.1-129 2.44 20 2-Hexanone 0.125 ND 1.16 1.13 92.6 90.2 10 59.4-154 2.59 20.1 trans-1,3-Dichloropropene 0.0250 ND 0.239 0.232 93.3 90.6 10 66.3-136 2.88 20 Iodomethane 0.125 ND 1.16 1.13 92.5 90.7 10 55.2-140 1.94 20 Ethylbenzene 0.0250 0.200 0.408 0.405 83.1 81.9 10 62.7-136 0.740 20 2-Butanone (MEK)0.125 0.109 1.23 1.20 89.7 86.9 10 45.0-156 2.89 20.8 Methylene Chloride 0.0250 ND 0.233 0.229 93.3 91.5 10 61.5-125 1.89 20 4-Methyl-2-pentanone (MIBK)0.125 ND 1.32 1.29 105 103 10 60.7-150 1.99 20 Styrene 0.0250 ND 0.234 0.229 91.7 89.7 10 68.2-133 2.12 20 1,1,1,2-Tetrachloroethane 0.0250 ND 0.240 0.227 96.0 90.9 10 70.5-132 5.44 20 1,1,2,2-Tetrachloroethane 0.0250 ND 0.241 0.235 96.6 94.0 10 64.9-145 2.66 20 Tetrachloroethene 0.0250 ND 0.221 0.218 88.5 87.4 10 57.4-141 1.28 20 Toluene 0.0250 0.321 0.518 0.513 78.8 76.9 10 67.8-124 0.930 20 1,1,1-Trichloroethane 0.0250 ND 0.228 0.225 91.1 89.8 10 58.7-134 1.43 20 1,1,2-Trichloroethane 0.0250 ND 0.232 0.225 92.8 90.0 10 74.1-130 3.11 20 Vinyl acetate 0.125 ND 1.45 1.42 116 113 10 42.8-181 2.19 20 Trichloroethene 0.0250 ND 0.241 0.232 96.3 92.9 10 48.9-148 3.57 20 Trichlorofluoromethane 0.0250 ND 0.295 0.286 118 114 10 39.9-165 3.23 20 1,2,3-Trichloropropane 0.0250 ND 0.226 0.220 90.6 87.8 10 71.5-134 3.12 20 Vinyl chloride 0.0250 ND 0.261 0.253 104 101 10 44.3-143 2.99 20 Xylenes, Total 0.0750 0.466 1.10 1.08 84.5 81.8 10 65.6-133 1.87 20 (S) a,a,a-Trifluorotoluene 100 97.8 90.4-116 (S) Toluene-d8 102 101 89.0-112 (S) Dibromofluoromethane 105 106 80.0-119 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 97 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 97 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27 L876258-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L876258-01 12/08/16 06:01 • (MS) R3183408-4 12/08/16 00:31 • (MSD) R3183408-5 12/08/16 01:00 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% (S) 4-Bromofluorobenzene 96.0 94.7 85.0-114 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 98 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 98 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG933189 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-28 Method Blank (MB) (MB) R3183710-1 12/09/16 09:33 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Acetone 0.0329 J 0.0100 0.0500 Acrylonitrile U 0.00187 0.0100 Benzene U 0.000331 0.00100 Bromodichloromethane U 0.000380 0.00100 Bromochloromethane U 0.000520 0.00100 Bromoform U 0.000469 0.00100 Carbon disulfide U 0.000275 0.00100 Carbon tetrachloride U 0.000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0.000453 0.00500 Chloroform U 0.000324 0.00500 Chloromethane 0.000853 J 0.000276 0.00250 Dibromomethane U 0.000346 0.00100 1,2-Dichlorobenzene U 0.000349 0.00100 1,4-Dichlorobenzene U 0.000274 0.00100 trans-1,4-Dichloro-2-butene U 0.000866 0.00250 1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 1,1-Dichloroethene U 0.000398 0.00100 cis-1,2-Dichloroethene U 0.000260 0.00100 trans-1,2-Dichloroethene U 0.000396 0.00100 1,2-Dichloropropane U 0.000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0.000419 0.00100 Ethylbenzene U 0.000384 0.00100 2-Hexanone U 0.00382 0.0100 Iodomethane U 0.00171 0.0100 2-Butanone (MEK)U 0.00393 0.0100 Methylene Chloride U 0.00100 0.00500 4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100 Styrene U 0.000307 0.00100 1,1,1,2-Tetrachloroethane U 0.000385 0.00100 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000780 0.00500 1,1,1-Trichloroethane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 Trichlorofluoromethane U 0.00120 0.00500 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 99 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 99 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG933189 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-28 Method Blank (MB) (MB) R3183710-1 12/09/16 09:33 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l 1,2,3-Trichloropropane U 0.000807 0.00250 Vinyl acetate U 0.00163 0.0100 Vinyl chloride U 0.000259 0.00100 Xylenes, Total U 0.00106 0.00300 (S) Toluene-d8 105 90.0-115 (S) Dibromofluoromethane 101 79.0-121 (S) a,a,a-Trifluorotoluene 101 90.4-116 (S) 4-Bromofluorobenzene 102 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183710-2 12/09/16 11:11 • (LCSD) R3183710-3 12/09/16 11:32 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Acetone 0.125 0.137 0.146 109 117 28.7-175 6.40 20.9 Acrylonitrile 0.125 0.0950 0.108 76.0 86.5 58.2-145 12.9 20 Benzene 0.0250 0.0211 0.0227 84.3 90.9 73.0-122 7.58 20 Bromodichloromethane 0.0250 0.0223 0.0237 89.4 94.8 75.5-121 5.87 20 Bromochloromethane 0.0250 0.0219 0.0231 87.5 92.4 78.9-123 5.43 20 Bromoform 0.0250 0.0211 0.0233 84.4 93.3 71.5-131 10.0 20 Bromomethane 0.0250 0.0218 0.0176 87.3 70.4 22.4-187 J3 21.5 20 Carbon disulfide 0.0250 0.0197 0.0205 78.8 82.0 53.0-134 3.95 20 Carbon tetrachloride 0.0250 0.0220 0.0203 87.9 81.2 70.9-129 7.91 20 Chlorobenzene 0.0250 0.0236 0.0251 94.4 100 79.7-122 6.01 20 Chlorodibromomethane 0.0250 0.0240 0.0256 96.0 103 78.2-124 6.62 20 Chloroethane 0.0250 0.0262 0.0279 105 112 41.2-153 6.32 20 Chloroform 0.0250 0.0225 0.0240 90.2 96.1 73.2-125 6.36 20 Chloromethane 0.0250 0.0284 0.0306 114 122 55.8-134 7.41 20 Dibromomethane 0.0250 0.0234 0.0255 93.5 102 79.5-118 8.58 20 1,2-Dichlorobenzene 0.0250 0.0221 0.0240 88.4 96.0 84.7-118 8.24 20 1,4-Dichlorobenzene 0.0250 0.0218 0.0239 87.2 95.7 82.2-114 9.30 20 trans-1,4-Dichloro-2-butene 0.0250 0.0187 0.0200 74.8 80.1 58.3-129 6.85 20 1,1-Dichloroethane 0.0250 0.0210 0.0225 84.2 90.1 71.7-127 6.79 20 1,2-Dichloroethane 0.0250 0.0231 0.0248 92.5 99.4 65.3-126 7.09 20 1,1-Dichloroethene 0.0250 0.0214 0.0230 85.5 92.0 59.9-137 7.35 20 cis-1,2-Dichloroethene 0.0250 0.0209 0.0231 83.5 92.5 77.3-122 10.2 20 trans-1,2-Dichloroethene 0.0250 0.0216 0.0230 86.4 92.0 72.6-125 6.29 20 1,2-Dichloropropane 0.0250 0.0217 0.0234 86.8 93.6 77.4-125 7.48 20 cis-1,3-Dichloropropene 0.0250 0.0225 0.0247 90.2 98.7 77.7-124 9.00 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 100 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 100 of 110 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG933189 Volatile Organic Compounds (GC/MS) by Method 8260B L875822-28 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3183710-2 12/09/16 11:11 • (LCSD) R3183710-3 12/09/16 11:32 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% trans-1,3-Dichloropropene 0.0250 0.0221 0.0244 88.5 97.6 73.5-127 9.84 20 Ethylbenzene 0.0250 0.0233 0.0251 93.2 100 80.9-121 7.52 20 2-Hexanone 0.125 0.104 0.115 82.9 92.3 59.4-151 10.8 20 Iodomethane 0.125 0.0682 0.0787 54.6 62.9 64.6-137 J4 J4 14.3 20 2-Butanone (MEK)0.125 0.0797 0.0899 63.8 72.0 46.4-155 12.1 20 Methylene Chloride 0.0250 0.0208 0.0213 83.3 85.4 69.5-120 2.42 20 4-Methyl-2-pentanone (MIBK)0.125 0.0998 0.115 79.8 92.1 63.3-138 14.3 20 Styrene 0.0250 0.0235 0.0252 94.0 101 79.9-124 7.17 20 1,1,1,2-Tetrachloroethane 0.0250 0.0224 0.0244 89.4 97.6 78.5-125 8.80 20 1,1,2,2-Tetrachloroethane 0.0250 0.0203 0.0226 81.1 90.4 79.3-123 10.9 20 Tetrachloroethene 0.0250 0.0241 0.0247 96.4 98.7 73.5-130 2.38 20 Toluene 0.0250 0.0221 0.0237 88.6 94.9 77.9-116 6.90 20 1,1,1-Trichloroethane 0.0250 0.0225 0.0244 90.1 97.7 71.1-129 8.06 20 1,1,2-Trichloroethane 0.0250 0.0228 0.0242 91.1 96.7 81.6-120 5.98 20 Trichloroethene 0.0250 0.0228 0.0257 91.0 103 79.5-121 12.3 20 Trichlorofluoromethane 0.0250 0.0223 0.0240 89.1 96.2 49.1-157 7.62 20 1,2,3-Trichloropropane 0.0250 0.0216 0.0244 86.5 97.6 74.9-124 12.1 20 Vinyl acetate 0.125 0.106 0.116 84.5 93.1 41.7-159 9.71 20 Vinyl chloride 0.0250 0.0178 0.0191 71.0 76.4 61.5-134 7.31 20 Xylenes, Total 0.0750 0.0700 0.0753 93.3 100 79.2-122 7.31 20 (S) Toluene-d8 105 105 90.0-115 (S) Dibromofluoromethane 103 100 79.0-121 (S) a,a,a-Trifluorotoluene 104 103 90.4-116 (S) 4-Bromofluorobenzene 103 101 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 101 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 101 of 110 ONE LAB. NATIONWIDE.GLOSSARY OF TERMS Abbreviations and Definitions SDG Sample Delivery Group. MDL Method Detection Limit. RDL Reported Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). U Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. (S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. Rec.Recovery. Qualifier Description B The same analyte is found in the associated blank. J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 102 of 110 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 102 of 110 ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 103 of 110 Our Locations Alabama 40660 Alaska UST-080 Arizona AZ0612 Arkansas 88-0469 California 01157CA Colorado TN00003 Conneticut PH-0197 Florida E87487 Georgia NELAP Georgia 1 923 Idaho TN00003 Illinois 200008 Indiana C-TN-01 Iowa 364 Kansas E-10277 Kentucky 1 90010 Kentucky 2 16 Louisiana AI30792 Maine TN0002 Maryland 324 Massachusetts M-TN003 Michigan 9958 Minnesota 047-999-395 Mississippi TN00003 Missouri 340 Montana CERT0086 Nebraska NE-OS-15-05 Nevada TN-03-2002-34 New Hampshire 2975 New Jersey–NELAP TN002 New Mexico TN00003 New York 11742 North Carolina Env375 North Carolina 1 DW21704 North Carolina 2 41 North Dakota R-140 Ohio–VAP CL0069 Oklahoma 9915 Oregon TN200002 Pennsylvania 68-02979 Rhode Island 221 South Carolina 84004 South Dakota n/a Tennessee 1 4 2006 Texas T 104704245-07-TX Texas 5 LAB0152 Utah 6157585858 Vermont VT2006 Virginia 109 Washington C1915 West Virginia 233 Wisconsin 9980939910 Wyoming A2LA A2LA – ISO 17025 1461.01 Canada 1461.01 EPA–Crypto TN00003 AIHA 100789 DOD 1461.01 USDA S-67674 State Accreditations Third Party & Federal Accreditations ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. 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Chemical/Microbiological 5. Mold n/a Accreditation not applicable 1461.02A2LA – ISO 170255 * Not all certifications held by the laboratory are applicable to the results reported in the attached report. ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 103 of 110 10 | P a g e APPENDIX B: TIME SERIES GRAPHS Pa g e 1 1, 1 - D i c h l o r o e t h e n e Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 0246810 MW - 9 A 5 / 6 / 1 9 9 4 7 / 2 6 / 1 9 9 7 1 0 / 1 6 / 2 0 0 0 1 / 7 / 2 0 0 4 3 / 3 0 / 2 0 0 7 6 / 2 0 / 2 0 1 0 9/10/2013 12/1/2016 Pa g e 1 1, 4 - D i c h l o r o b e n z e n e Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 05101520 MW - 8 MW - 9 A MW - 5 MW - 1 6 MW - 1 3 R MW - 1 5 5 / 6 / 1 9 9 4 7 / 2 6 / 1 9 9 7 1 0 / 1 6 / 2 0 0 0 1 / 7 / 2 0 0 4 3 / 3 0 / 2 0 0 7 6 / 2 0 / 2 0 1 0 9/10/2013 12/1/2016 Pa g e 1 Ac e t o n e Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 050 10 0 15 0 20 0 25 0 30 0 35 0 40 0 MW - 1 5 3 / 2 8 / 2 0 1 3 1 0 / 5 / 2 0 1 3 4 / 1 5 / 2 0 1 4 1 0 / 2 4 / 2 0 1 4 5 / 4 / 2 0 1 5 1 1 / 1 2 / 2 0 1 5 5/22/2016 11/30/2016 Pa g e 1 Ar s e n i c Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 051015202530 MW - 1 6 6 / 1 2 / 1 9 9 7 3 / 2 4 / 2 0 0 0 1 / 4 / 2 0 0 3 1 0 / 1 6 / 2 0 0 5 7 / 2 8 / 2 0 0 8 5 / 1 0 / 2 0 1 1 2/19/2014 12/1/2016 Pa g e 1 Ba r i u m Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 0 10 0 20 0 30 0 40 0 50 0 MW - 1 2 MW - 1 6 MW - 1 8 MW - 1 4 MW - 1 3 R MW - 1 7 R 6 / 1 2 / 1 9 9 7 3 / 2 4 / 2 0 0 0 1 / 4 / 2 0 0 3 1 0 / 1 6 / 2 0 0 5 7 / 2 8 / 2 0 0 8 5 / 1 0 / 2 0 1 1 2/19/2014 12/1/2016 Pa g e 1 Be n z e n e Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 012345 MW - 1 6 MW - 1 3 R MW - 1 5 6 / 1 2 / 1 9 9 7 3 / 2 4 / 2 0 0 0 1 / 4 / 2 0 0 3 1 0 / 1 6 / 2 0 0 5 7 / 2 8 / 2 0 0 8 5 / 1 0 / 2 0 1 1 2/19/2014 12/1/2016 Pa g e 1 Ch l o r o e t h a n e Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 0102030405060 MW - 1 6 6 / 1 2 / 1 9 9 7 3 / 2 4 / 2 0 0 0 1 / 4 / 2 0 0 3 1 0 / 1 6 / 2 0 0 5 7 / 2 8 / 2 0 0 8 5 / 1 0 / 2 0 1 1 2/19/2014 12/1/2016 Pa g e 1 Ch r o m i u m Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( ) 0510152025303540 MW - 1 0 MW - 1 7 R MW - 3 R 4 / 8 / 2 0 1 5 7 / 3 / 2 0 1 5 9 / 2 7 / 2 0 1 5 1 2 / 2 2 / 2 0 1 5 3 / 1 8 / 2 0 1 6 6 / 1 2 / 2 0 1 6 9/6/2016 12/2/2016 Pa g e 1 Co b a l t Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 05101520 MW - 1 7 R 1 / 1 5 / 1 9 9 8 9 / 2 6 / 2 0 0 0 6 / 8 / 2 0 0 3 2 / 1 7 / 2 0 0 6 1 0 / 2 9 / 2 0 0 8 7 / 1 1 / 2 0 1 1 3/22/2014 12/1/2016 Pa g e 1 Se l e n i u m Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 01020304050 MW - 3 R 12/1/2016 Pa g e 1 Te t r a c h l o r o e t h e n e Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 012345 MW - 1 7 R 1 1 / 1 4 / 2 0 0 6 4 / 2 1 / 2 0 0 8 9 / 2 7 / 2 0 0 9 3 / 5 / 2 0 1 1 8 / 1 1 / 2 0 1 2 1 / 1 7 / 2 0 1 4 6/25/2015 12/1/2016 Pa g e 1 Tr i c h l o r o e t h e n e Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 012345 MW - 1 7 R 1 / 1 5 / 1 9 9 8 9 / 2 6 / 2 0 0 0 6 / 8 / 2 0 0 3 2 / 1 7 / 2 0 0 6 1 0 / 2 9 / 2 0 0 8 7 / 1 1 / 2 0 1 1 3/22/2014 12/1/2016 Pa g e 1 Va n a d i u m Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 051015202530 MW - 3 R 12/1/2016 Pa g e 1 Zi n c Mu l t i - W e l l T i m e - S e r i e s G r a p h Sa m p l e D a t e C o n c e n t r a t i o n ( p p b ) 0 10 0 20 0 30 0 40 0 50 0 60 0 MW - 1 0 MW - 1 1 5 / 6 / 1 9 9 4 7 / 2 7 / 1 9 9 7 1 0 / 1 7 / 2 0 0 0 1 / 8 / 2 0 0 4 3 / 3 1 / 2 0 0 7 6 / 2 1 / 2 0 1 0 9/11/2013 12/2/2016 11 | P a g e APPENDIX C: NON-PARAMETRIC PREDICTION INTERVAL INTER-WELL COMPARISONS Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: 1,1-Dichloroethane Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 40.1042% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 103 Maximum Background Value = 5 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 0.259 FALSE MW-2 3/24/2000 1 7 TRUE MW-3 9/11/2001 1 5 FALSE MW-7 3/24/2000 1 5 FALSE MW-8 12/1/2016 1 4.17 FALSE MW-9 9/11/2001 1 5 FALSE MW-9A 12/1/2016 1 10.4 TRUE MW-11 12/2/2016 1 0.259 FALSE MW-5 12/1/2016 1 3.59 FALSE MW-15A 10/2/2013 1 4.6 FALSE MW-16 12/1/2016 1 1.15 FALSE MW-17 6/12/1997 1 5 FALSE MW-18 12/1/2016 1 0.259 FALSE MW-14 11/30/2016 1 0.259 FALSE MW-13R 11/30/2016 1 0.259 FALSE MW-17R 12/1/2016 1 0.259 FALSE MW-5A 10/21/2011 1 0.2 FALSE MW-9B 3/24/2000 1 5 FALSE MW-9R 3/16/2016 1 0.259 FALSE MW-21 10/2/2013 1 0.3 FALSE Page 2 MW-22 11/30/2016 1 0.259 FALSE MW-23 11/30/2016 1 0.259 FALSE MW-24 10/1/2013 1 0.2 FALSE MW-25 3/10/2010 1 0 FALSE MW-26 12/2/2016 1 0.259 FALSE MW-25R 11/30/2016 1 0.259 FALSE MW-15 11/30/2016 1 3.03 FALSE MW-24R 11/30/2016 1 0.259 FALSE MW-21R 11/30/2016 1 0.259 FALSE MW-3R 12/1/2016 1 2.17 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: 1,4-Dichlorobenzene Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 58.8616% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 103 Maximum Background Value = 5 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 0.274 FALSE MW-2 3/24/2000 1 5 FALSE MW-3 9/11/2001 1 5 FALSE MW-7 3/24/2000 1 5 FALSE MW-8 12/1/2016 1 2.91 FALSE MW-9 9/11/2001 1 5 FALSE MW-9A 12/1/2016 1 9.51 TRUE MW-11 12/2/2016 1 0.274 FALSE MW-5 12/1/2016 1 4.99 FALSE MW-15A 10/2/2013 1 8.9 TRUE MW-16 12/1/2016 1 2 FALSE MW-17 6/12/1997 1 5 FALSE MW-18 12/1/2016 1 0.274 FALSE MW-14 11/30/2016 1 0.274 FALSE MW-13R 11/30/2016 1 2.49 FALSE MW-17R 12/1/2016 1 0.274 FALSE MW-5A 10/21/2011 1 0.39 FALSE MW-9B 3/24/2000 1 5 FALSE MW-9R 3/16/2016 1 0.274 FALSE MW-21 10/2/2013 1 0.6 FALSE Page 2 MW-22 11/30/2016 1 0.274 FALSE MW-23 11/30/2016 1 0.274 FALSE MW-24 10/1/2013 1 0.39 FALSE MW-25 3/10/2010 1 0 FALSE MW-26 12/2/2016 1 0.274 FALSE MW-25R 11/30/2016 1 0.274 FALSE MW-15 11/30/2016 1 8.13 TRUE MW-24R 11/30/2016 1 0.274 FALSE MW-21R 11/30/2016 1 0.274 FALSE MW-3R 12/1/2016 1 0.274 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Acetone Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 67.0157% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 103 Maximum Background Value = 100 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 10 FALSE MW-2 3/24/2000 1 100 FALSE MW-3 9/11/2001 1 100 FALSE MW-7 3/24/2000 1 100 FALSE MW-8 12/1/2016 1 10 FALSE MW-9 9/11/2001 1 100 FALSE MW-9A 12/1/2016 1 10 FALSE MW-11 12/2/2016 1 10 FALSE MW-5 12/1/2016 1 10 FALSE MW-15A 10/2/2013 1 52.7 FALSE MW-16 12/1/2016 1 10 FALSE MW-17 6/12/1997 1 100 FALSE MW-18 12/1/2016 1 10 FALSE MW-14 11/30/2016 1 10 FALSE MW-13R 11/30/2016 1 10 FALSE MW-17R 12/1/2016 1 10 FALSE MW-5A 10/21/2011 1 9.06 FALSE MW-9B 3/24/2000 1 100 FALSE MW-9R 3/16/2016 1 10 FALSE MW-21 10/2/2013 1 821 TRUE Page 2 MW-22 11/30/2016 1 10 FALSE MW-23 11/30/2016 1 10 FALSE MW-24 10/1/2013 1 9.06 FALSE MW-25 3/10/2010 1 65.1 FALSE MW-26 12/2/2016 1 10 FALSE MW-25R 11/30/2016 1 10 FALSE MW-15 11/30/2016 1 104 TRUE MW-24R 11/30/2016 1 10 FALSE MW-21R 11/30/2016 1 10 FALSE MW-3R 12/1/2016 1 10 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Arsenic Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 52.2639% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 105 Maximum Background Value = 10 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 0.25 FALSE MW-2 3/24/2000 1 35 TRUE MW-3 9/11/2001 1 10 FALSE MW-7 3/24/2000 1 10 FALSE MW-8 12/1/2016 1 2.78 FALSE MW-9 9/11/2001 1 10 FALSE MW-9A 12/1/2016 1 0.25 FALSE MW-11 12/2/2016 1 2.42 FALSE MW-5 12/1/2016 1 0.25 FALSE MW-15A 10/2/2013 1 6.2 FALSE MW-16 12/1/2016 1 14.1 TRUE MW-17 6/12/1997 1 10 FALSE MW-18 12/1/2016 1 0.25 FALSE MW-14 11/30/2016 1 0.25 FALSE MW-13R 11/30/2016 1 0.25 FALSE MW-17R 12/1/2016 1 0.25 FALSE MW-5A 3/19/2012 1 0 FALSE MW-9B 3/19/2012 1 0 FALSE MW-9R 3/16/2016 1 0.25 FALSE MW-21 10/2/2013 1 2.4 FALSE Page 2 MW-22 11/30/2016 1 0.25 FALSE MW-23 11/30/2016 1 0.25 FALSE MW-24 10/1/2013 1 0.41 FALSE MW-25 3/10/2010 1 3.3 FALSE MW-26 12/2/2016 1 0.25 FALSE MW-25R 11/30/2016 1 2.64 FALSE MW-15 11/30/2016 1 2.51 FALSE MW-24R 11/30/2016 1 0.25 FALSE MW-21R 11/30/2016 1 3.39 FALSE MW-3R 12/1/2016 1 2.14 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Barium Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 49.6134% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 105 Maximum Background Value = 500 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 53.2 FALSE MW-2 3/24/2000 1 500 FALSE MW-3 9/11/2001 1 500 FALSE MW-7 3/24/2000 1 500 FALSE MW-8 12/1/2016 1 62.1 FALSE MW-9 9/11/2001 1 500 FALSE MW-9A 12/1/2016 1 86.8 FALSE MW-11 12/2/2016 1 43.9 FALSE MW-5 12/1/2016 1 15.4 FALSE MW-15A 10/2/2013 1 58.6 FALSE MW-16 12/1/2016 1 144 FALSE MW-17 6/12/1997 1 500 FALSE MW-18 12/1/2016 1 122 FALSE MW-14 11/30/2016 1 181 FALSE MW-13R 11/30/2016 1 159 FALSE MW-17R 12/1/2016 1 137 FALSE MW-5A 3/19/2012 1 0 FALSE MW-9B 3/19/2012 1 0 FALSE MW-9R 3/16/2016 1 66.6 FALSE MW-21 10/2/2013 1 32.1 FALSE Page 2 MW-22 11/30/2016 1 61.2 FALSE MW-23 11/30/2016 1 11.5 FALSE MW-24 10/1/2013 1 38.2 FALSE MW-25 3/10/2010 1 13.7 FALSE MW-26 12/2/2016 1 40.1 FALSE MW-25R 11/30/2016 1 21.9 FALSE MW-15 11/30/2016 1 66.9 FALSE MW-24R 11/30/2016 1 36.2 FALSE MW-21R 11/30/2016 1 29 FALSE MW-3R 12/1/2016 1 84.9 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Benzene Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 61.4286% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 103 Maximum Background Value = 5 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 0.331 FALSE MW-2 3/24/2000 1 5 FALSE MW-3 9/11/2001 1 5 FALSE MW-7 3/24/2000 1 5 FALSE MW-8 12/1/2016 1 0.331 FALSE MW-9 9/11/2001 1 5 FALSE MW-9A 12/1/2016 1 1.44 FALSE MW-11 12/2/2016 1 0.331 FALSE MW-5 12/1/2016 1 0.331 FALSE MW-15A 10/2/2013 1 1.8 FALSE MW-16 12/1/2016 1 1.45 FALSE MW-17 6/12/1997 1 5 FALSE MW-18 12/1/2016 1 0.331 FALSE MW-14 11/30/2016 1 0.331 FALSE MW-13R 11/30/2016 1 1.89 FALSE MW-17R 12/1/2016 1 0.331 FALSE MW-5A 10/21/2011 1 0.24 FALSE MW-9B 3/24/2000 1 5 FALSE MW-9R 3/16/2016 1 0.331 FALSE MW-21 10/2/2013 1 0.9 FALSE Page 2 MW-22 11/30/2016 1 0.331 FALSE MW-23 11/30/2016 1 0.331 FALSE MW-24 10/1/2013 1 0.24 FALSE MW-25 3/10/2010 1 0 FALSE MW-26 12/2/2016 1 0.331 FALSE MW-25R 11/30/2016 1 0.331 FALSE MW-15 11/30/2016 1 1.74 FALSE MW-24R 11/30/2016 1 0.331 FALSE MW-21R 11/30/2016 1 0.331 FALSE MW-3R 12/1/2016 1 0.331 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Chloroethane Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 54.0682% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 103 Maximum Background Value = 10 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 0.453 FALSE MW-2 3/24/2000 1 14 TRUE MW-3 9/11/2001 1 10 FALSE MW-7 3/24/2000 1 10 FALSE MW-8 12/1/2016 1 0.453 FALSE MW-9 9/11/2001 1 43 TRUE MW-9A 12/1/2016 1 0.453 FALSE MW-11 12/2/2016 1 0.453 FALSE MW-5 12/1/2016 1 0.453 FALSE MW-15A 10/2/2013 1 2.6 FALSE MW-16 12/1/2016 1 10.5 TRUE MW-17 6/12/1997 1 10 FALSE MW-18 12/1/2016 1 0.453 FALSE MW-14 11/30/2016 1 0.453 FALSE MW-13R 11/30/2016 1 0.453 FALSE MW-17R 12/1/2016 1 0.453 FALSE MW-5A 10/21/2011 1 0.48 FALSE MW-9B 3/24/2000 1 10 FALSE MW-9R 3/16/2016 1 0.453 FALSE MW-21 10/2/2013 1 0.48 FALSE Page 2 MW-22 11/30/2016 1 0.453 FALSE MW-23 11/30/2016 1 0.453 FALSE MW-24 10/1/2013 1 0.48 FALSE MW-25 3/10/2010 1 0 FALSE MW-26 12/2/2016 1 0.453 FALSE MW-25R 11/30/2016 1 0.453 FALSE MW-15 11/30/2016 1 0.453 FALSE MW-24R 11/30/2016 1 0.453 FALSE MW-21R 11/30/2016 1 0.453 FALSE MW-3R 12/1/2016 1 0.453 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Chromium Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 0% Number of comparisons = 19 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 8 Maximum Background Value = 8.35 Confidence Level = 50% False Positive Rate = 50% Location Date Count Mean Significant MW-9R 3/16/2016 1 12.1 TRUE MW-5 12/1/2016 1 1.4 FALSE MW-8 12/1/2016 1 1.4 FALSE MW-9A 12/1/2016 1 1.4 FALSE MW-10 12/2/2016 1 12.2 TRUE MW-11 12/2/2016 1 1.4 FALSE MW-13R 11/30/2016 1 1.4 FALSE MW-14 11/30/2016 1 1.4 FALSE MW-15 11/30/2016 1 1.4 FALSE MW-16 12/1/2016 1 1.4 FALSE MW-17R 12/1/2016 1 11.6 TRUE MW-18 12/1/2016 1 1.4 FALSE MW-21R 11/30/2016 1 1.4 FALSE MW-22 11/30/2016 1 1.4 FALSE MW-23 11/30/2016 1 1.4 FALSE MW-24R 11/30/2016 1 1.4 FALSE MW-25R 11/30/2016 1 1.4 FALSE MW-26 12/2/2016 1 1.4 FALSE MW-3R 12/1/2016 1 10.1 TRUE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Cobalt Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 52.8424% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 105 Maximum Background Value = 10 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 2.3 FALSE MW-2 3/24/2000 1 10 FALSE MW-3 9/11/2001 1 10 FALSE MW-7 3/24/2000 1 10 FALSE MW-8 12/1/2016 1 2.3 FALSE MW-9 9/11/2001 1 10 FALSE MW-9A 12/1/2016 1 2.3 FALSE MW-11 12/2/2016 1 2.3 FALSE MW-5 12/1/2016 1 2.3 FALSE MW-15A 10/2/2013 1 3.3 FALSE MW-16 12/1/2016 1 2.3 FALSE MW-17 6/12/1997 1 11 TRUE MW-18 12/1/2016 1 2.3 FALSE MW-14 11/30/2016 1 2.3 FALSE MW-13R 11/30/2016 1 2.3 FALSE MW-17R 12/1/2016 1 17 TRUE MW-5A 3/19/2012 1 0 FALSE MW-9B 3/19/2012 1 0 FALSE MW-9R 3/16/2016 1 2.3 FALSE MW-21 10/2/2013 1 19 TRUE Page 2 MW-22 11/30/2016 1 2.3 FALSE MW-23 11/30/2016 1 2.3 FALSE MW-24 10/1/2013 1 1.3 FALSE MW-25 3/10/2010 1 1.6 FALSE MW-26 12/2/2016 1 2.3 FALSE MW-25R 11/30/2016 1 2.3 FALSE MW-15 11/30/2016 1 2.3 FALSE MW-24R 11/30/2016 1 2.3 FALSE MW-21R 11/30/2016 1 11.2 TRUE MW-3R 12/1/2016 1 2.3 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Copper Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 52.3447% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 108 Maximum Background Value = 200 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 0.52 FALSE MW-2 3/24/2000 1 200 FALSE MW-3 9/11/2001 1 200 FALSE MW-7 3/24/2000 1 200 FALSE MW-8 12/1/2016 1 0.52 FALSE MW-9 9/11/2001 1 200 FALSE MW-9A 12/1/2016 1 0.52 FALSE MW-11 12/2/2016 1 0.52 FALSE MW-5 12/1/2016 1 0.52 FALSE MW-15A 10/2/2013 1 8.8 FALSE MW-16 12/1/2016 1 0.52 FALSE MW-17 6/12/1997 1 200 FALSE MW-18 12/1/2016 1 0.52 FALSE MW-14 11/30/2016 1 0.52 FALSE MW-13R 11/30/2016 1 0.52 FALSE MW-17R 12/1/2016 1 0.52 FALSE MW-5A 3/19/2012 1 0 FALSE MW-9B 3/19/2012 1 0 FALSE MW-9R 3/16/2016 1 0.52 FALSE MW-21 10/2/2013 1 4.4 FALSE Page 2 MW-22 11/30/2016 1 0.52 FALSE MW-23 11/30/2016 1 0.52 FALSE MW-24 10/1/2013 1 4.5 FALSE MW-25 3/10/2010 1 4.2 FALSE MW-26 12/2/2016 1 0.52 FALSE MW-25R 11/30/2016 1 0.52 FALSE MW-15 11/30/2016 1 0.52 FALSE MW-24R 11/30/2016 1 0.52 FALSE MW-21R 11/30/2016 1 6.48 FALSE MW-3R 12/1/2016 1 0.52 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Lead Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 46.0441% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 105 Maximum Background Value = 41 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 7.6 FALSE MW-2 3/24/2000 1 20 FALSE MW-3 9/11/2001 1 20 FALSE MW-7 3/24/2000 1 10 FALSE MW-8 12/1/2016 1 8.46 FALSE MW-9 9/11/2001 1 18 FALSE MW-9A 12/1/2016 1 0.24 FALSE MW-11 12/2/2016 1 2.93 FALSE MW-5 12/1/2016 1 0.24 FALSE MW-15A 10/2/2013 1 0.74 FALSE MW-16 12/1/2016 1 0.24 FALSE MW-17 6/12/1997 1 10 FALSE MW-18 12/1/2016 1 3.38 FALSE MW-14 11/30/2016 1 0.24 FALSE MW-13R 11/30/2016 1 3.35 FALSE MW-17R 12/1/2016 1 8.58 FALSE MW-5A 3/19/2012 1 0 FALSE MW-9B 3/19/2012 1 0 FALSE MW-9R 3/16/2016 1 4.26 FALSE MW-21 10/2/2013 1 0.3 FALSE Page 2 MW-22 11/30/2016 1 0.24 FALSE MW-23 11/30/2016 1 0.24 FALSE MW-24 10/1/2013 1 1.1 FALSE MW-25 3/10/2010 1 6.7 FALSE MW-26 12/2/2016 1 0.24 FALSE MW-25R 11/30/2016 1 0.24 FALSE MW-15 11/30/2016 1 0.24 FALSE MW-24R 11/30/2016 1 0.24 FALSE MW-21R 11/30/2016 1 2.49 FALSE MW-3R 12/1/2016 1 4.59 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Selenium Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 56.2016% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 105 Maximum Background Value = 20 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 0.38 FALSE MW-2 3/24/2000 1 20 FALSE MW-3 9/11/2001 1 39 TRUE MW-7 3/24/2000 1 20 FALSE MW-8 12/1/2016 1 0.38 FALSE MW-9 9/11/2001 1 20 FALSE MW-9A 12/1/2016 1 0.38 FALSE MW-11 12/2/2016 1 0.38 FALSE MW-5 12/1/2016 1 0.38 FALSE MW-15A 10/2/2013 1 2.1 FALSE MW-16 12/1/2016 1 0.38 FALSE MW-17 6/12/1997 1 20 FALSE MW-18 12/1/2016 1 0.38 FALSE MW-14 11/30/2016 1 0.38 FALSE MW-13R 11/30/2016 1 0.38 FALSE MW-17R 12/1/2016 1 0.38 FALSE MW-5A 3/19/2012 1 0 FALSE MW-9B 3/19/2012 1 0 FALSE MW-9R 3/16/2016 1 22.6 TRUE MW-21 10/2/2013 1 1.2 FALSE Page 2 MW-22 11/30/2016 1 0.38 FALSE MW-23 11/30/2016 1 0.38 FALSE MW-24 10/1/2013 1 0.18 FALSE MW-25 3/10/2010 1 0.4 FALSE MW-26 12/2/2016 1 0.38 FALSE MW-25R 11/30/2016 1 0.38 FALSE MW-15 11/30/2016 1 0.38 FALSE MW-24R 11/30/2016 1 0.38 FALSE MW-21R 11/30/2016 1 0.38 FALSE MW-3R 12/1/2016 1 46.3 TRUE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Tetrachloroethene Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 43.1267% Number of comparisons = 24 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 37 Maximum Background Value = 5 Confidence Level = 82.2% False Positive Rate = 17.8% Location Date Count Mean Significant MW-10 12/2/2016 1 0.372 FALSE MW-11 12/2/2016 1 0.372 FALSE MW-13R 11/30/2016 1 0.372 FALSE MW-14 11/30/2016 1 0.372 FALSE MW-15A 10/2/2013 1 0.17 FALSE MW-16 12/1/2016 1 0.372 FALSE MW-17R 12/1/2016 1 1.21 FALSE MW-18 12/1/2016 1 0.372 FALSE MW-21 10/2/2013 1 0.17 FALSE MW-22 11/30/2016 1 0.372 FALSE MW-23 11/30/2016 1 0.372 FALSE MW-9R 3/16/2016 1 0.372 FALSE MW-5 12/1/2016 1 0.372 FALSE MW-8 12/1/2016 1 0.372 FALSE MW-9A 12/1/2016 1 0.372 FALSE MW-24 10/1/2013 1 0.17 FALSE MW-25 3/10/2010 1 0 FALSE MW-26 12/2/2016 1 0.372 FALSE MW-25R 11/30/2016 1 0.372 FALSE MW-5A 10/21/2011 1 0.17 FALSE Page 2 MW-15 11/30/2016 1 0.372 FALSE MW-24R 11/30/2016 1 0.372 FALSE MW-21R 11/30/2016 1 0.372 FALSE MW-3R 12/1/2016 1 0.372 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Trichloroethene Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 66.0782% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 107 Maximum Background Value = 7 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 0.398 FALSE MW-2 3/24/2000 1 5 FALSE MW-3 9/11/2001 1 5 FALSE MW-7 3/24/2000 1 5 FALSE MW-8 12/1/2016 1 0.398 FALSE MW-9 9/11/2001 1 5 FALSE MW-9A 12/1/2016 1 0.398 FALSE MW-11 12/2/2016 1 0.398 FALSE MW-5 12/1/2016 1 0.398 FALSE MW-15A 10/2/2013 1 0.23 FALSE MW-16 12/1/2016 1 0.398 FALSE MW-17 6/12/1997 1 5 FALSE MW-18 12/1/2016 1 0.398 FALSE MW-14 11/30/2016 1 0.398 FALSE MW-13R 11/30/2016 1 0.398 FALSE MW-17R 12/1/2016 1 1.02 FALSE MW-5A 10/21/2011 1 0.23 FALSE MW-9B 3/24/2000 1 5 FALSE MW-9R 3/16/2016 1 0.398 FALSE MW-21 10/2/2013 1 0.23 FALSE Page 2 MW-22 11/30/2016 1 0.398 FALSE MW-23 11/30/2016 1 0.398 FALSE MW-24 10/1/2013 1 0.23 FALSE MW-25 3/10/2010 1 0 FALSE MW-26 12/2/2016 1 0.398 FALSE MW-25R 11/30/2016 1 0.398 FALSE MW-15 11/30/2016 1 0.398 FALSE MW-24R 11/30/2016 1 0.398 FALSE MW-21R 11/30/2016 1 0.398 FALSE MW-3R 12/1/2016 1 0.398 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Vanadium Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 49.0933% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 105 Maximum Background Value = 210 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 21.5 FALSE MW-2 3/24/2000 1 40 FALSE MW-3 9/11/2001 1 40 FALSE MW-7 3/24/2000 1 40 FALSE MW-8 12/1/2016 1 2.4 FALSE MW-9 9/11/2001 1 40 FALSE MW-9A 12/1/2016 1 2.4 FALSE MW-11 12/2/2016 1 2.4 FALSE MW-5 12/1/2016 1 2.4 FALSE MW-15A 10/2/2013 1 0.07 FALSE MW-16 12/1/2016 1 2.4 FALSE MW-17 6/12/1997 1 40 FALSE MW-18 12/1/2016 1 2.4 FALSE MW-14 11/30/2016 1 2.4 FALSE MW-13R 11/30/2016 1 2.4 FALSE MW-17R 12/1/2016 1 23.7 FALSE MW-5A 3/19/2012 1 0 FALSE MW-9B 3/19/2012 1 0 FALSE MW-9R 3/16/2016 1 26.2 FALSE MW-21 10/2/2013 1 0.07 FALSE Page 2 MW-22 11/30/2016 1 2.4 FALSE MW-23 11/30/2016 1 2.4 FALSE MW-24 10/1/2013 1 0.91 FALSE MW-25 3/10/2010 1 10.6 FALSE MW-26 12/2/2016 1 2.4 FALSE MW-25R 11/30/2016 1 2.4 FALSE MW-15 11/30/2016 1 2.4 FALSE MW-24R 11/30/2016 1 2.4 FALSE MW-21R 11/30/2016 1 2.4 FALSE MW-3R 12/1/2016 1 25.3 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Zinc Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 42.8571% Number of comparisons = 30 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 107 Maximum Background Value = 260 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 12/2/2016 1 27.4 FALSE MW-2 3/24/2000 1 50 FALSE MW-3 9/11/2001 1 50 FALSE MW-7 3/24/2000 1 50 FALSE MW-8 12/1/2016 1 2.56 FALSE MW-9 9/11/2001 1 50 FALSE MW-9A 12/1/2016 1 2.56 FALSE MW-11 12/2/2016 1 34.7 FALSE MW-5 12/1/2016 1 2.56 FALSE MW-15A 10/2/2013 1 5.4 FALSE MW-16 12/1/2016 1 2.56 FALSE MW-17 6/12/1997 1 50 FALSE MW-18 12/1/2016 1 2.56 FALSE MW-14 11/30/2016 1 2.56 FALSE MW-13R 11/30/2016 1 2.56 FALSE MW-17R 12/1/2016 1 2.56 FALSE MW-5A 3/19/2012 1 0 FALSE MW-9B 3/19/2012 1 0 FALSE MW-9R 3/16/2016 1 2.56 FALSE MW-21 10/2/2013 1 8.4 FALSE Page 2 MW-22 11/30/2016 1 2.56 FALSE MW-23 11/30/2016 1 2.56 FALSE MW-24 10/1/2013 1 2.4 FALSE MW-25 3/10/2010 1 26 FALSE MW-26 12/2/2016 1 2.56 FALSE MW-25R 11/30/2016 1 2.56 FALSE MW-15 11/30/2016 1 2.56 FALSE MW-24R 11/30/2016 1 2.56 FALSE MW-21R 11/30/2016 1 2.56 FALSE MW-3R 12/1/2016 1 2.56 FALSE