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HomeMy WebLinkAbout7803_RobesonCoMSW_Nov2015_2ndSemiAnnual_DIN28080_20151220 Robeson County Landfill Water Quality Monitoring Report November 2015 Semi-Annual Event Prepared on Behalf of: Robeson County Landfill 246 Landfill Rd Lumberton, North Carolina 28360 Facility Permit No. 78-03 Dated: December 20, 2015 Prepared by: 3430 Capuano St. Lumberton NC, 28358 TRANSMITTAL LETTER December 20, 2015 Mrs. Elizabeth Werner Hydrogeologist North Carolina Department of Environment and Natural Resources Division of Waste Management - Solid Waste Section 217 W Jones St, Raleigh, North Carolina 27603 Subject: Robeson County Landfill Water Quality Monitoring Report November 2015 Semi-Annual Event Robeson County Landfill St. Pauls, Robeson County, North Carolina To: Mrs. Werner Hunt Environmental Associates, PLLC has prepared this November 2015 Semi-Annual Water Quality Monitoring Report for the Robeson County Landfill. This report summarizes the findings of sampling data gathered at the site. The scope of work at the site was executed in order to fulfill the NCDENR Solid Waste Section reporting requirements for environmental monitoring We appreciate your consideration and review following the submission of this report. If you have- any questions concerning this report, please don’t hesitate to contact us at (910) 674-5925. Respectfully Submitted, ______________________ Michael Cody Hunt, P.G., M.S. Project Geologist Table of Contents 1.0 INTRODUCTION ............................................................................................................... 1 2.0 SITE BACKGROUND AND MONITORING NETWORK .............................................. 1 3.0 SITE HYDROGEOLOGY................................................................................................... 1 4.0 FIELD ACTIVITIES ........................................................................................................... 2 5.0 ANALYTICAL RESULTS ................................................................................................. 2 5.1 Groundwater ..................................................................................................................... 2 5.2 Surface Water ................................................................................................................... 4 5.3 Leachate ........................................................................................................................... 5 6.0 STATISTICAL PROCEDURES ......................................................................................... 5 6.1 STATISTICAL RESULTS SUMMARY ........................................................................ 6 7.0 CONCLUSIONS AND RECOMMENDATIONS .............................................................. 6 Figures Figure 1: Groundwater Potentiometric Map Tables Table 1: Groundwater Monitoring Program Table 2: Ground Water Elevations & Flow Velocities Table 3: Analytical Results Table 4: Statistical Analysis Summary Appendices Appendix A: Laboratory Analytical Results Appendix B: Time Series Graphs Appendix C: Non-Parametric Prediction Interval Inter-Well Comparisons 1 | P a g e 1.0 INTRODUCTION The Robeson County Landfill, operating under North Carolina Department of Environment and Natural Resources (NCDENR) Solid Waste Permit #78-03, is required to submit semi-annual groundwater monitoring reports for detection monitoring of the Phase 2, Phase 3, and Phase 4 lined landfills and assessment monitoring of the Phase 1 unlined landfill. This report presents the results of the second semi-annual monitoring event for 2015, conducted on November 17 and 18, 2015. Also included in this report are the results of the surface water and leachate monitoring that was performed in conjunction with the groundwater monitoring event. The Robeson County Landfill is currently accepting construction and demolition debris (C&D) waste over the closed Phase 1 Municipal Solid Waste (MSW) unlined landfill. Currently, all MSW is being disposed in the Phase 4 lined landfill. The Phase 1 unlined landfill has been closed per NCDENR Solid Waste Regulations, and the C&D disposal will bring the landfill to final closure contours. 2.0 SITE BACKGROUND AND MONITORING NETWORK Currently twenty-nine groundwater monitoring wells are located around the perimeter of the Phase 1, Phase 2, Phase 3, Phase 4 and C&D landfill cells (Figure 1). Table 1 lists the currently monitored wells associated with each Phase of the landfill. Twenty-two groundwater monitoring wells were monitored during this sampling event. Seven monitoring wells have been damaged and were approved for closure by NCDENR Solid Waste Section correspondence from Ms. Werner on November 22 of 2011, three wells were approved for closure and replacement on January 3, 2013 and therefore, none of them were sampled for this event. Two surface water samples (SW-1 & SW-2) were collected as shown in Figure 1. Leachate samples were also collected during this monitoring event for Phases 2, 3, and 4. Phase 2 and 3 leachate samples were collected from the respective line valves linked to the generator. The Phase 4 leachate sample was collected from the line pump station. This report includes summaries of the field procedures, and field, laboratory, and statistical results from the November 2015 semi-annual groundwater sampling event. Field and laboratory results of the surface water and leachate sampling are also presented. Summary tables of the monitoring network, groundwater characteristics, field measurements, laboratory and statistical analysis results, as well as graphs of groundwater analytical data over time are included at the end of the report. 3.0 SITE HYDROGEOLOGY The site is located in the Coastal Plain Physiographic province within the Cretaceous-age Black Creek Formation. In general, the lithology of the site is composed of sandy soils with clay. As a result, the direction of groundwater flow should be largely controlled by site topography. 2 | P a g e Figure 1 provides potentiometric surface maps and groundwater flow calculations for the shallow aquifer utilizing groundwater level data from the Second Semi-Annual 2015 event. Groundwater flow direction for the Second Semi-Annual 2015 event was to the southeast towards the Big Marsh Swamp, consistent with past events. Groundwater velocity for the Second Semi-Annual 2015 event was calculated utilizing Darcy’s law: V = Ki/n, where K = hydraulic conductivity, i = groundwater gradient, n = porosity. Based on the fall dataset, groundwater velocities are estimated to range from 0.18 feet/year (MW-24) to 91.39 feet/year (MW-9a). 4.0 FIELD ACTIVITIES Groundwater, surface water, and leachate samples from the Robeson County Landfill were collected on November 17 and 18, 2015. Twenty two (22) groundwater samples were collected by use of a disposable, laboratory decontaminated polyethylene bailer. Sampling locations are presented on Figure 1. Groundwater elevations were measured at each well prior to sampling and are presented in Table 2. These groundwater elevations were used to construct the potentiometric contours for this sampling event as shown on Figure 1. The groundwater elevations and potentiometric contours were used to estimate groundwater velocities at each well presented in Table 2. After depth to groundwater was measured, water was purged from each well to provide fresh formation water within the well water column prior to sampling. All samples were collected in clean laboratory prepared containers for the specified analytical methods. Groundwater samples were properly preserved, placed on ice, and transported to the laboratory via overnight delivery. The samples were transported to ESC Lab Sciences Inc., a North Carolina certified laboratory (NC DW #21704). Laboratory analyses consisted of those noted in Table 1 and were reported according to the laboratory’s Method Detection Limits (MDLs). The laboratory analytical reports are included in Appendix A. Trip and equipment blanks were used for quality assurance/quality control (QA/QC). Trip blanks were prepared by the laboratory and accompanied the coolers during the sampling event. One equipment blank was prepared by pouring distilled water over a bailer and collecting the water in containers provided by the laboratory. Sampling methods followed the protocol outlined in NCDENR’s Guidelines for Groundwater, Soil, and Surface Water Sampling (NCDENR 2008) and in accordance with the approved Sampling and Analysis Plan (Water Quality Monitoring Plan, David Garrett and Associates, Raleigh, NC, 2009). 5.0 ANALYTICAL RESULTS 5.1 Groundwater ESC Lab Sciences, Inc. located in Lebanon, Tennesse analyzed samples for the North Carolina Appendix I volatile organic compounds (VOCs) and metals. In accordance with SWS guidelines the analytical results were reported to the laboratory specific method detection limit (MDL) and are quantifiable at or below Solid Waste Section Limits (SWSLs). The following list indicates which analytes were detected above the SWSL at each sampling location. Underlined analytes exceeded the North Carolina 2L Standard (NC 2L), the Groundwater Protection Standard, or the North Carolina Surface Water Standards for Class C Waters. A complete summary of all detected 3 | P a g e and estimated concentrations for this sampling event is presented in Table 3. Copies of the laboratory analytical data reports are provided in Appendix A. MW-3R Volatile Organic Compounds: None Detected Metals: Arsenic, Lead, Selenium MW-5 Volatile Organic Compounds: Chlorobenzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, Cis-1,2-Dichloroethene, Vinyl Chloride Metals: Arsenic MW-6 Volatile Organic Compounds: None Detected Metals: Lead MW-8 Volatile Organic Compounds: 1,1-Dichloroethane Metals: Arsenic, Lead, MW-9A Volatile Organic Compounds: Chlorobenzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, Cis-1,2-Dichloroethene Metals: None Detected MW-10 Volatile Organic Compounds: None Detected Metals: Arsenic, Copper, Lead MW-11 Volatile Organic Compounds: None Detected Metals: Arsenic, Cadmium, Copper, Lead, Zinc MW-12 Volatile Organic Compounds: None Detected Metals: Lead MW-13R Volatile Organic Compounds: Benzene, 1,4-Dichlorobenzene Metals: Lead MW-14 Volatile Organic Compounds: 1,4-Dichlorobenzene Metals: Lead 4 | P a g e MW-15 Volatile Organic Compounds: Benzene, Chlorobenzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane Metals: None Detected MW-16 Volatile Organic Compounds: None Detected Metals: Arsenic MW-17R Volatile Organic Compounds: None Detected Metals: Arsenic, Copper, Lead MW-18 Volatile Organic Compounds: None Detected Metals: Lead MW-19 Volatile Organic Compounds: None Detected Metals: Arsenic, Copper, Lead, Zinc MW-20 Volatile Organic Compounds: None Detected Metals: Lead MW-21R Volatile Organic Compounds: Acetone Metals: Arsenic, Copper, Lead MW-24R Volatile Organic Compounds: None Detected Metals: Lead MW-25R Volatile Organic Compounds: None Detected Metals: Barium, Chromium, Vanadium, Arsenic, Copper, Lead MW-26 Volatile Organic Compounds: Acetone Metals: Barium, Chromium, Nickle, Vanadium, Copper, Lead 5.2 Surface Water HEA personnel sampled two surface water bodies in the vicinity of the Phase 1, 2, 3 and Phase 4 landfills (Figure 1). Surface water sampling point SW-1 is located below the outflow from the existing sediment basin southwest of the Phase 1 cell. Surface water sampling point SW-2 is located in a drainage ditch, southeast of the Phase 2 cell. The following list indicates which 5 | P a g e analytes were detected above the SWSL at each sampling location. Underlined analytes exceeded the North Carolina 2L Standard (NC 2L), the Groundwater Protection Standard, or the North Carolina Surface Water Standards for Class C Waters. SW-1 Volatile Organic Compounds: Acetone, 2-Butanone (Mek) Metals: Barium, Chromium, Cobalt, Nickle, Vanadium, Antimony, Arsenic, Copper, Selenium, Zinc SW-2 Volatile Organic Compounds: None Detected Metals: Barium, Chromium, Vanadium, Arsenic 5.3 Leachate HEA personnel sampled three leachate drainage lines in the vicinity of the Phase 2, 3 and 4 landfill cells. Two leachate sampling locations are east of the Phase 2 and 3 cells; one is located east of the Phase 4 cell. Analytical results are presented in Table 3. 6.0 STATISTICAL PROCEDURES The laboratory data from the sampling event were reviewed and analyzed by HEA in order to evaluate trends and changes in the results and to identify statistically significant differences between compliance and background wells. Data entry and analysis were performed using the Chemstat statistical software package developed by Starpoint Software, Cincinnati, OH. Chemstat follows the EPA document, Statistical Analysis of Ground-Water Monitoring Data at RCRA Facilities – Unified Guidance (March 2009), as well as NCDENR guidelines. The data were reviewed to evaluate the most appropriate analysis methods. Initial analysis consisted of a basic review of the data and of the time vs. concentration graphs (included in Appendix B) to determine any major changes or trends in the data. Individual compliance well historical means were compared to the pooled background historical means for MW-6 and MW- 12 to determine if detected constituents were statistically significantly different from general background groundwater quality. The statistical analysis results are summarized in Table 4 and provided in Appendix C. 6 | P a g e 6.1 STATISTICAL RESULTS SUMMARY For the Second Semi-Annual 2015 event, statistically significant differences from background concentrations and above SWSLs, shown in Table 4, were found for VOCs and Metals as detailed below: VOCs  1,4-Dichlorobenzene – MW-5, MW-9A, MW-15. Metals  Arsenic – MW-11 and MW-16.  Chromium – MW-25R and MW-26. 7.0 CONCLUSIONS AND RECOMMENDATIONS For the Second Semi-Annual 2015 groundwater monitoring event, concentrations that were detected above an NC SWSL and NC GWPS/NC 2L were also determined to statistically exceed the background concentrations. Based on the statistical evaluations: The following groundwater detections were identified as statistically significant increases for the Second Semi-Annual 2015 event:  Chromium The following groundwater detections were identified appearing to decrease sitewide:  1,4-Dichlorobenzene  Acetone  Benzene The following groundwater detections were identified appearing to remain relatively constant sitewide:  Arsenic  Cadmium  Chlorobenzene  Copper  Selenium Chromium was detected in MW-25R and MW-26; no statistical data exists for prior events, therefore trends will be evaluated moving forward. 7 | P a g e During the Second Semi-Annual 2015 event, two Appendix I VOCs and two Appendix I inorganic constituents were detected in surface water samples at quantified concentrations above their respective NC SWSLs at SW-1: acetone, 2-Butanone (Mek), Barium and Zinc. Acetone, 2- Butanone (Mek), Barium, and Zinc do not have a NC 2B Surface Water Standard established for swamp waters (status of discharge locations). The Second Semi-Annual 2015 concentrations of acetone (0.12 mg/L), 2-Butanone (0.31 mg/L), Barium (0.24 mg/L), and Zinc (0.063 mg/L) at surface water location SW-1 are all below the NC 2L Groundwater Standard 6 mg/L, 4 mg/L, 0.7 mg/L, and 1 mg/L respectively. The site will continue monitoring in accordance with the requirements for Detection Monitoring as outlined in Title 15A NCAC 13B .1633. The next semi-annual event is tentatively scheduled for April 2015. FIGURES TABLES Location Phase Gradient Current Use Zone Monitored Laboratory Analysis MW-1 Phase 1 Up Background Shallow N/A MW-2 Phase 1 Down Compliance Shallow N/A MW-3r Phase 1 Down Compliance Shallow Appendix I + MW-4a Phase 1 Up Background Shallow N/A MW-5 Phase 1 Down Compliance Shallow Appendix I + MW-5a Phase 1 Down Compliance Deep N/A MW-6 Phase 1 Up Background Shallow Appendix I + MW-7 Phase 1 Cross Compliance Shallow N/A MW-8 Phase 1 Down Compliance Shallow Appendix I + MW-9 Phase 1 Down Compliance Shallow N/A MW-9a Phase 1 Down Compliance Shallow Appendix I + MW-9b Phase 1 Down Compliance Deep N/A MW-10 Phase 1 Down Compliance Shallow Appendix I MW-11 Phase 1 Down Compliance Shallow Appendix I MW-12 Phase 2 Up Background Shallow Appendix I MW-13r Phase 2 Down Compliance Shallow Appendix I MW-14 Phase 2 Down Compliance Shallow Appendix I MW-15 Phase 2 Down Compliance Shallow Appendix I MW-16 Phase 2 Down Compliance Shallow Appendix I MW-17r Phase 2 Down Compliance Shallow Appendix I MW-18 Phase 2 Down Compliance Shallow Appendix I MW-19 C & D Down Not used Shallow Metals & VOC MW-20 C & D Down Not used Shallow Metals & VOC MW-21 Phase 3 Down Compliance Shallow Appendix I MW-22 Phase 3 Down Compliance Shallow Appendix I MW-23 Phase 3 Cross Compliance Shallow Appendix I MW-24 Phase 4 Cross Compliance Shallow Appendix I MW-25 Phase 4 Down Compliance Shallow Appendix I MW-26 Phase 4 Up Compliance Shallow Appendix I Notes: Appendix 1 = Appendix I constituents were analyzed. N/A = Not Analyzed Table 1 Groundwater Monitoring Program Monitoring wells MW-1, MW-2, MW-4a, MW-5a, MW-7, MW-9, and MW-9b were not analyzed per GNRA's request approved by NCDENR on July 14, 2000. Appendix 1 + = Appendix I plus previously detected Appendix II constituents were analyzed. Well TOC Elevation (ft) DTW (ft) WTE (ft) Hyd Cond* (ft/day) Porosity** (%) Gradient*** (ft/ft) Velocity**** (ft/day)(ft/year) MW-1 151.14 nm NA 0.877 0.18 0.005 NA NA MW-2 136.53 nm NA 0.822 0.16 0.005 NA NAMW-3r 137.38 8.62 128.76 0.142 0.20 0.005 0.0033 1.22MW-4a 153.02 nm NA 0.959 0.18 0.005 NA NA MW-5 130.50 3.13 127.37 0.036 0.18 0.005 0.0009 0.34MW-6 150.73 10.30 140.43 2.000 0.15 0.005 0.063 22.87 MW-7 155.89 nm NA 0.493 0.16 0.005 NA NAMW-8 131.01 4.70 126.31 5.479 0.20 0.005 0.129 47.00MW-9 131.18 nm NA 0.466 0.20 0.005 NA NA MW-9a 131.60 4.39 127.21 9.589 0.18 0.005 0.250 91.39MW-10 133.33 5.32 128.01 0.603 0.18 0.005 0.016 5.75 MW-11 135.30 5.30 130.00 0.874 0.16 0.005 0.026 9.37MW-12 157.79 17.50 140.29 2.041 0.18 0.005 0.053 19.45MW-13r 154.98 19.58 135.40 0.237 0.18 0.005 0.006 2.26 MW-14 156.11 19.55 136.56 0.271 0.18 0.005 0.007 2.58MW-15a 151.91 16.95 134.96 0.183 0.16 0.005 0.005 1.96 MW-16 149.64 15.35 134.29 8.506 0.18 0.005 0.222 81.07MW-17r 150.31 13.51 136.80 0.257 0.15 0.005 0.008 2.94MW-18 151.17 14.31 136.86 0.246 0.18 0.005 0.006 2.34 MW-19 146.95 14.98 131.97 0.020 0.18 0.005 0.001 0.19MW-20 139.88 8.70 131.18 7.140 0.18 0.005 0.186 68.05 MW-21 150.88 14.80 136.08 0.065 0.18 0.005 0.002 0.62MW-22 152.28 16.51 135.77 0.057 0.18 0.005 0.001 0.54MW-23 151.75 13.00 138.75 0.028 0.18 0.005 0.001 0.27 MW-24 154.58 13.85 140.73 0.019 0.18 0.005 0.00049 0.18MW-25R 154.25 16.40 137.85 0.025 0.18 0.005 0.00065 0.24 MW-26 154.59 13.60 140.99 0.05 0.18 0.005 0.00131 0.48 Notes TOC = Top of casing elevation NA = not available DTW = Depth to Water from TOC nm = not measured WTE = Water Table Elevation ft = feet Hyd Cond = Hydraulic Conductivity % = percent * Hydraulic Conductivity values from previous slug tests ** Effective Porosity from Groundwater & Wells (Driscoll, 1986) ***Average gradient for the October 2011 sampling event ****Velocity calculated by HEA using V=KI/n where V = Ground water velocity K = Hydraulic conductivity I = Ground water gradient n = Effective porosity Table 2 Ground Water Elevations & Flow Velocities M W - 3 R M W - 5 M W - 6 M W - 8 M W - 9 A M W - 1 0 M W - 1 1 M W - 1 2 M W - 1 3 R M W - 1 4 M W - 1 5 M W - 1 6 M W - 1 7 R M W - 1 8 M W - 1 9 M W - 2 0 M W - 2 1 R M W - 2 2 M W - 2 3 M W - 2 4 R M W - 2 5 R M W - 2 6 S W - 1 S W - 2 T R I P B L A N K E Q U I P M E N T B L A N K L E A C H A T E P H A S E 2 L E A C H A T E P H A S E 3 L E A C H A T E P H A S E 4 Analyte Solid Waste Selection Limits Alkalinity Dissolved Solids 164 58 Phosphorus,Total 3.08 0.53 0.28 Cod 1300 427 3920 Bod 9 26 2310 Barium 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.042 0.098 0.24 0.089 BDL BDL 0.178 0.268 0.238 Chromium 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.012 0.025 0.0085 0.0019 BDL BDL BDL 0.020 0.018 Cobalt 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0079 BDL BDL BDL 0.044 BDL BDL Nickel 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0063 0.0214 BDL BDL BDL BDL 0.044 0.083 Silver 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Vanadium 0.025 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0191 0.046 0.0122 0.0045 BDL BDL 0.033 0.059 0.048 Antimony 0.006 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0038 BDL BDL BDL 0.071 BDL BDL Arsenic 0.01 0.0034 0.0026 BDL 0.0055 BDL 0.0044 0.012 BDL BDL BDL BDL 0.014 0.0037 BDL 0.0062 BDL 0.0053 BDL BDL BDL 0.0047 BDL 0.0081 0.0026 BDL BDL 0.21 0.027 0.07 Beryllium 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Cadmium 0.001 BDL BDL BDL BDL BDL BDL 0.0044 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Copper 0.01 BDL BDL BDL BDL BDL 0.0065 0.044 BDL BDL BDL BDL BDL 0.010 BDL 0.010 BDL 0.0059 BDL BDL BDL 0.0086 0.0076 BDL BDL BDL BDL 0.31 0.055 BDL Lead 0.01 0.0098 BDL 0.0022 0.032 BDL 0.017 0.035 0.0056 0.0068 0.0020 BDL BDL 0.017 0.0072 0.031 0.0024 0.0031 BDL BDL 0.0088 0.0039 0.009 BDL BDL BDL BDL 0.16 BDL BDL Selenium 0.01 0.015 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Thallium 0.0055 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Zinc 0.01 BDL BDL BDL BDL BDL BDL 0.221 BDL BDL BDL BDL BDL BDL BDL 0.039 BDL BDL BDL BDL BDL BDL BDL 0.063 BDL BDL BDL BDL BDL BDL Acetone 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.059 BDL BDL BDL BDL BDL 0.12 BDL BDL BDL 0.11 0.1 2.6 Acrylonitrile 0.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Benzene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL 0.0022 BDL 0.0016 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0044 0.0059 BDL Bromochloromethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Bromodichloromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Bromoform 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Bromomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Carbon Disulfide 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Carbon Tetrachloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Chlorobenzene 0.003 BDL 0.0015 BDL BDL 0.0015 BDL BDL BDL BDL BDL 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0015 0.0021 BDL Chlorodibromomethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Chloroethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Chloroform 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Chloromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Dibromomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,2-Dichlorobenzene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,4-Dichlorobenzene 0.001 BDL 0.0050 BDL BDL 0.0074 BDL BDL BDL 0.0014 0.0024 0.0084 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0059 0.012 BDL Trans-1,4-Dichloro-2-Butene 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,1-Dichloroethane 0.005 BDL 0.0038 BDL 0.0031 0.0082 BDL BDL BDL BDL BDL 0.0044 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Project Sample ID Table 3 Analytical Results 1,2-Dichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,1-Dichloroethene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Cis-1,2-Dichloroethene 0.005 BDL 0.0016 BDL BDL 0.0012 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Trans-1,2-Dichloroethene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,2-Dichloropropane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Cis-1,3-Dichloropropene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Trans-1,3-Dichloropropene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Ethylbenzene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0079 0.023 0.012 2-Hexanone 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Iodomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 2-Butanone (Mek)0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.31 BDL BDL BDL 0.083 0.12 3.05 Methylene Chloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 4-Methyl-2-Pentanone (Mibk)0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Styrene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,1,1,2-Tetrachloroethane 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,1,2,2-Tetrachloroethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Tetrachloroethene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Toluene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0072 BDL 1,1,1-Trichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,1,2-Trichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Trichloroethene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Trichlorofluoromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,2,3-Trichloropropane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Vinyl Acetate 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Vinyl Chloride 0.001 BDL 0.0011 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0012 BDL Xylenes, Total 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.026 0.081 BDL Chloride BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.72 8.34 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Nitrate 10 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.33 0.42 BDL Sulfate 250 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 5.45 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 736 51 99 Notes:BDL = Below Detection Limit * All units mg/L Location Parameter Detected Concentration Detection Limit Units %ND Test Statistically Significant? Above 2L/MCL MW-3R Selenium 0.015 <0.0020 mg/L 58.4759 NPPL N N MW-5 1,4-Dichlorobenzene 0.005 <0.0010 mg/L 61.5863 NPPL Y N MW-8 Lead 0.032 <0.0020 mg/L 47.9688 NPPL N Y MW-9A 1,4-Dichlorobenzene 0.0074 <0.0010 mg/L 61.5863 NPPL Y Y MW-10 Lead 0.017 <0.0020 mg/L 47.9688 NPPL N Y MW-11 Arsenic 0.012 <0.0020 mg/L 55.296 NPPL Y Y MW-11 Cadmium 0.0044 <0.0010 mg/L 51.7941 NPPL N Y MW-11 Copper 0.044 <0.0050 mg/L 53.7291 NPPL N N MW-11 Lead 0.035 <0.0020 mg/L 47.9688 NPPL N Y MW-11 Zinc 0.221 <0.025 mg/L 43.5508 NPPL N N MW-13R Benzene 0.0022 <0.0010 mg/L 63.5938 NPPL N Y MW-13R 1,4-Dichlorobenzene 0.0014 <0.0010 mg/L 61.5863 NPPL N N MW-14 1,4-Dichlorobenzene 0.0024 <0.0010 mg/L 61.5863 NPPL N N MW-15 Benzene 0.0016 <0.0010 mg/L 63.5938 NPPL N Y MW-15 Chlorobenzene 0.003 <0.0010 mg/L 65.1969 NPPL N N MW-15 1,4-Dichlorobenzene 0.0084 <0.0010 mg/L 61.5863 NPPL Y Y MW-16 Arsenic 0.014 <0.0020 mg/L 55.296 NPPL Y Y MW-17R Copper 0.01 <0.0050 mg/L 53.7291 NPPL N N MW-17R Lead 0.017 <0.0020 mg/L 47.9688 NPPL N Y MW-19 Copper 0.01 <0.0050 mg/L 53.7291 NPPL N N MW-19 Lead 0.031 <0.0020 mg/L 47.9688 NPPL N Y MW-19 Zinc 0.039 <0.025 mg/L 43.5508 NPPL N N MW-25R Chromium 0.012 <0.010 mg/L 0 NPPL Y Y MW-26 Chromium 0.025 <0.010 mg/L 0 NPPL Y Y MW-26 Vanadium 0.046 <0.020 mg/L 50.234 NPPL N Y Notes: MW-1 (historical data only), MW-6 and MW-12 were used as background wells. Wells not listed did not have any detected constituents. % ND = percent non-detect NPPL = Non-Parametric Prediction Limit (Inter-Well) mg/L = milligrams per Liter NA = Not available Table 4 Statistical Analysis Summary APPENDIX A: LABORATORY ANALYTICAL RESULTS ANALYTICAL REPORT December 01, 2015 Hunt Environmental Associates Sample Delivery Group:L801958 Samples Received:11/19/2015 Project Number:14-011550 Description:Robeson Co Solid Waste Semi-Annual Env Monitoring Report To:Cody Hunt 3430 Capuano Street Lumberton, NC 28358 Entire Report Reviewed By: December 01, 2015 [Preliminary Report] Jimmy Hunt Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com December 02, 2015 Jimmy Hunt Technical Service Representative ONE LAB. NATIONWIDE.TABLE OF CONTENTS ¹Cp: Cover Page 1 ²Tc: Table of Contents 2 ³Ss: Sample Summary 4 ⁴Cn: Case Narrative 9 ⁵Sr: Sample Results 10 MW-3R 15FT L801958-01 10 MW-5 15FT L801958-02 12 MW-6 15FT L801958-03 14 MW-8 15FT L801958-04 16 MW-9A 15FT L801958-05 18 MW-10 15FT L801958-06 20 MW-11 15FT L801958-07 22 MW-12 15FT L801958-08 24 MW-13R 15FT L801958-09 26 MW-14 15FT L801958-10 28 MW-15 15FT L801958-11 30 MW-16 15FT L801958-12 32 MW-17R 15FT L801958-13 34 MW-18 15FT L801958-14 36 MW-19 15FT L801958-15 38 MW-20 15FT L801958-16 40 MW-21R 15FT L801958-17 42 MW-22 15FT L801958-18 44 MW-23 15FT L801958-19 46 MW-24R 15FT L801958-20 48 MW-25R 15FT L801958-21 50 MW-26 15FT L801958-22 52 SW-1 L801958-23 54 SW-2 L801958-24 56 TRIP BLANK L801958-25 58 TRIP BLANK L801958-26 59 LEACHATE PHASE 2 L801958-27 60 LEACHATE PHASE 3 L801958-28 62 LEACHATE PHASE 4 L801958-29 64 ⁶Qc: Quality Control Summary 66 Gravimetric Analysis by Method 2540 C-2011 66 Wet Chemistry by Method 2320 B-2011 67 Wet Chemistry by Method 365.4 68 Wet Chemistry by Method 410.4 69 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 2 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 2 of 101 ONE LAB. NATIONWIDE.TABLE OF CONTENTS Wet Chemistry by Method 5210 B-2011 70 Wet Chemistry by Method 9056MOD 72 Metals (ICPMS) by Method 6020 78 Volatile Organic Compounds (GC/MS) by Method 8260B 82 ⁷Gl: Glossary of Terms 97 ⁸Al: Accreditations & Locations 98 ⁹Sc: Chain of Custody 99 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 3 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 3 of 101 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-3R 15FT L801958-01 GW 11/17/15 15:05 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 19:50 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/20/15 21:58 11/20/15 21:58 ACG Collected by Collected date/time Received date/time MW-5 15FT L801958-02 GW 11/18/15 16:15 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 19:52 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/20/15 22:16 11/20/15 22:16 ACG Collected by Collected date/time Received date/time MW-6 15FT L801958-03 GW 11/17/15 09:15 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 19:55 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/20/15 22:34 11/20/15 22:34 ACG Collected by Collected date/time Received date/time MW-8 15FT L801958-04 GW 11/17/15 15:25 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 19:57 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/20/15 22:53 11/20/15 22:53 ACG Collected by Collected date/time Received date/time MW-9A 15FT L801958-05 GW 11/18/15 16:35 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 18:51 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/20/15 23:11 11/20/15 23:11 ACG Collected by Collected date/time Received date/time MW-10 15FT L801958-06 GW 11/17/15 15:45 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 19:59 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/20/15 23:29 11/20/15 23:29 ACG Collected by Collected date/time Received date/time MW-11 15FT L801958-07 GW 11/17/15 15:40 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:02 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/20/15 23:48 11/20/15 23:48 ACG 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 4 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 4 of 101 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-12 15FT L801958-08 GW 11/17/15 10:10 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:04 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/20/15 21:03 11/20/15 21:03 ACG Collected by Collected date/time Received date/time MW-13R 15FT L801958-09 GW 11/17/15 11:50 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:06 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/21/15 00:06 11/21/15 00:06 ACG Collected by Collected date/time Received date/time MW-14 15FT L801958-10 GW 11/17/15 12:10 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:09 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/21/15 00:24 11/21/15 00:24 ACG Collected by Collected date/time Received date/time MW-15 15FT L801958-11 GW 11/17/15 12:20 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:11 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/21/15 00:43 11/21/15 00:43 ACG Collected by Collected date/time Received date/time MW-16 15FT L801958-12 GW 11/17/15 14:15 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:27 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/21/15 01:01 11/21/15 01:01 ACG Collected by Collected date/time Received date/time MW-17R 15FT L801958-13 GW 11/17/15 14:45 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:30 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/21/15 01:19 11/21/15 01:19 ACG Collected by Collected date/time Received date/time MW-18 15FT L801958-14 GW 11/17/15 14:30 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:32 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830452 1 11/21/15 01:38 11/21/15 01:38 ACG 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 5 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 5 of 101 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-19 15FT L801958-15 GW 11/18/15 16:55 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG830703 1 11/23/15 17:24 11/23/15 18:04 MF Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:34 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 07:15 11/21/15 07:15 BMB Wet Chemistry by Method 2320 B-2011 WG830995 1 11/24/15 17:02 11/24/15 17:02 MCG Wet Chemistry by Method 9056MOD WG830629 1 11/21/15 17:08 11/21/15 17:08 NJM Collected by Collected date/time Received date/time MW-20 15FT L801958-16 GW 11/18/15 16:45 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG830703 1 11/23/15 17:24 11/23/15 18:04 MF Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:36 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 07:33 11/21/15 07:33 BMB Wet Chemistry by Method 2320 B-2011 WG830995 1 11/24/15 17:02 11/24/15 17:02 MCG Wet Chemistry by Method 9056MOD WG830629 1 11/21/15 17:24 11/21/15 17:24 NJM Collected by Collected date/time Received date/time MW-21R 15FT L801958-17 GW 11/17/15 11:10 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:39 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 07:51 11/21/15 07:51 BMB Collected by Collected date/time Received date/time MW-22 15FT L801958-18 GW 11/17/15 11:30 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:41 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 08:09 11/21/15 08:09 BMB Collected by Collected date/time Received date/time MW-23 15FT L801958-19 GW 11/17/15 10:50 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:43 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 08:27 11/21/15 08:27 BMB Collected by Collected date/time Received date/time MW-24R 15FT L801958-20 GW 11/17/15 10:25 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830588 1 11/24/15 23:20 11/27/15 20:46 ST Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 08:45 11/21/15 08:45 BMB 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 6 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 6 of 101 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-25R 15FT L801958-21 GW 11/17/15 08:30 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830587 1 11/21/15 13:16 11/23/15 12:50 JDG Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 09:03 11/21/15 09:03 BMB Collected by Collected date/time Received date/time MW-26 15FT L801958-22 GW 11/17/15 09:55 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830587 1 11/21/15 13:16 11/23/15 12:59 JDG Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 09:21 11/21/15 09:21 BMB Collected by Collected date/time Received date/time SW-1 L801958-23 GW 11/17/15 07:45 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830587 1 11/21/15 13:16 11/23/15 13:02 JDG Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 09:39 11/21/15 09:39 BMB Collected by Collected date/time Received date/time SW-2 L801958-24 GW 11/17/15 08:05 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830587 1 11/21/15 13:16 11/23/15 13:04 JDG Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 09:57 11/21/15 09:57 BMB Collected by Collected date/time Received date/time TRIP BLANK L801958-25 GW 11/17/15 00:00 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 06:38 11/21/15 06:38 BMB Collected by Collected date/time Received date/time TRIP BLANK L801958-26 GW 11/17/15 00:00 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 06:56 11/21/15 06:56 BMB Collected by Collected date/time Received date/time LEACHATE PHASE 2 L801958-27 GW 11/18/15 15:10 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830587 9 11/21/15 13:16 11/23/15 13:28 JDG Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 10:15 11/21/15 10:15 BMB Wet Chemistry by Method 365.4 WG830333 1 11/20/15 11:26 11/27/15 15:29 DR Wet Chemistry by Method 410.4 WG830753 10 11/23/15 09:46 11/23/15 13:45 JER Wet Chemistry by Method 5210 B-2011 WG830211 1 11/19/15 15:45 11/24/15 10:53 RTB Wet Chemistry by Method 9056MOD WG830498 1 11/20/15 13:17 11/20/15 13:17 CM Wet Chemistry by Method 9056MOD WG830779 100 11/24/15 10:35 11/24/15 10:35 DJD 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 7 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 7 of 101 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time LEACHATE PHASE 3 L801958-28 GW 11/18/15 15:15 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830587 9 11/21/15 13:16 11/23/15 13:31 JDG Volatile Organic Compounds (GC/MS) by Method 8260B WG830461 1 11/21/15 10:33 11/21/15 10:33 BMB Wet Chemistry by Method 365.4 WG830333 1 11/20/15 11:26 11/27/15 15:30 DR Wet Chemistry by Method 410.4 WG830753 10 11/23/15 09:46 11/23/15 13:45 JER Wet Chemistry by Method 5210 B-2011 WG830211 1 11/19/15 15:49 11/24/15 10:56 RTB Wet Chemistry by Method 9056MOD WG830498 1 11/20/15 13:32 11/20/15 13:32 CM Collected by Collected date/time Received date/time LEACHATE PHASE 4 L801958-29 GW 11/18/15 15:50 11/19/15 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Metals (ICPMS) by Method 6020 WG830587 9 11/21/15 13:16 11/23/15 13:33 JDG Volatile Organic Compounds (GC/MS) by Method 8260B WG832427 10 12/01/15 10:02 12/01/15 10:02 BMB Wet Chemistry by Method 365.4 WG830333 1 11/20/15 11:26 11/27/15 15:31 DR Wet Chemistry by Method 410.4 WG830753 10 11/23/15 09:46 11/23/15 13:45 JER Wet Chemistry by Method 5210 B-2011 WG830211 10 11/19/15 15:55 11/24/15 11:01 RTB Wet Chemistry by Method 9056MOD WG830498 1 11/20/15 13:48 11/20/15 13:48 CM 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 8 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 8 of 101 ONE LAB. NATIONWIDE.CASE NARRATIVE All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] Jimmy Hunt Technical Service Representative Sample Handling and Receiving The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample. ESC Sample ID Project Sample ID Method L801958-27 LEACHATE PHASE 2 6020 L801958-28 LEACHATE PHASE 3 6020 L801958-29 LEACHATE PHASE 4 6020 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 9 of 101 Jimmy Hunt Technical Service Representative ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 9 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L801958 MW-3R 15FT Collected date/time: 11/17/15 15:05 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 19:50 WG830588 Arsenic 0.00337 0.00200 1 11/27/2015 19:50 WG830588 Barium 0.0555 0.00500 1 11/27/2015 19:50 WG830588 Beryllium ND 0.00200 1 11/27/2015 19:50 WG830588 Cadmium ND 0.00100 1 11/27/2015 19:50 WG830588 Chromium 0.0125 0.00200 1 11/27/2015 19:50 WG830588 Copper ND 0.00500 1 11/27/2015 19:50 WG830588 Cobalt ND 0.00200 1 11/27/2015 19:50 WG830588 Lead 0.00976 0.00200 1 11/27/2015 19:50 WG830588 Nickel ND 0.00200 1 11/27/2015 19:50 WG830588 Selenium 0.0152 0.00200 1 11/27/2015 19:50 WG830588 Silver ND 0.00200 1 11/27/2015 19:50 WG830588 Thallium ND 0.00200 1 11/27/2015 19:50 WG830588 Vanadium 0.0302 0.00500 1 11/27/2015 19:50 WG830588 Zinc ND 0.0250 1 11/27/2015 19:50 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/20/2015 21:58 WG830452 Acrylonitrile ND 0.0100 1 11/20/2015 21:58 WG830452 Benzene ND 0.00100 1 11/20/2015 21:58 WG830452 Bromochloromethane ND 0.00100 1 11/20/2015 21:58 WG830452 Bromodichloromethane ND 0.00100 1 11/20/2015 21:58 WG830452 Bromoform ND 0.00100 1 11/20/2015 21:58 WG830452 Bromomethane ND 0.00500 1 11/20/2015 21:58 WG830452 Carbon disulfide ND 0.00100 1 11/20/2015 21:58 WG830452 Carbon tetrachloride ND 0.00100 1 11/20/2015 21:58 WG830452 Chlorobenzene ND 0.00100 1 11/20/2015 21:58 WG830452 Chlorodibromomethane ND 0.00100 1 11/20/2015 21:58 WG830452 Chloroethane ND 0.00500 1 11/20/2015 21:58 WG830452 Chloroform ND 0.00500 1 11/20/2015 21:58 WG830452 Chloromethane ND 0.00250 1 11/20/2015 21:58 WG830452 Dibromomethane ND 0.00100 1 11/20/2015 21:58 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/20/2015 21:58 WG830452 1,4-Dichlorobenzene ND 0.00100 1 11/20/2015 21:58 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/20/2015 21:58 WG830452 1,1-Dichloroethane ND 0.00100 1 11/20/2015 21:58 WG830452 1,2-Dichloroethane ND 0.00100 1 11/20/2015 21:58 WG830452 1,1-Dichloroethene ND 0.00100 1 11/20/2015 21:58 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/20/2015 21:58 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/20/2015 21:58 WG830452 1,2-Dichloropropane ND 0.00100 1 11/20/2015 21:58 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/20/2015 21:58 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/20/2015 21:58 WG830452 Ethylbenzene ND 0.00100 1 11/20/2015 21:58 WG830452 2-Hexanone ND 0.0100 1 11/20/2015 21:58 WG830452 Iodomethane ND 0.0100 1 11/20/2015 21:58 WG830452 2-Butanone (MEK)ND 0.0100 1 11/20/2015 21:58 WG830452 Methylene Chloride ND 0.00500 1 11/20/2015 21:58 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/20/2015 21:58 WG830452 Styrene ND 0.00100 1 11/20/2015 21:58 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/20/2015 21:58 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/20/2015 21:58 WG830452 Tetrachloroethene ND 0.00100 1 11/20/2015 21:58 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 10 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 10 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L801958 MW-3R 15FT Collected date/time: 11/17/15 15:05 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/20/2015 21:58 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/20/2015 21:58 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/20/2015 21:58 WG830452 Trichloroethene ND 0.00100 1 11/20/2015 21:58 WG830452 Trichlorofluoromethane ND 0.00500 1 11/20/2015 21:58 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/20/2015 21:58 WG830452 Vinyl acetate ND 0.0100 1 11/20/2015 21:58 WG830452 Vinyl chloride ND 0.00100 1 11/20/2015 21:58 WG830452 Xylenes, Total ND 0.00300 1 11/20/2015 21:58 WG830452 (S) Toluene-d8 108 90.0-115 11/20/2015 21:58 WG830452 (S) Dibromofluoromethane 98.3 79.0-121 11/20/2015 21:58 WG830452 (S) a,a,a-Trifluorotoluene 110 90.4-116 11/20/2015 21:58 WG830452 (S) 4-Bromofluorobenzene 103 80.1-120 11/20/2015 21:58 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 11 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 11 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L801958 MW-5 15FT Collected date/time: 11/18/15 16:15 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 19:52 WG830588 Arsenic 0.00264 0.00200 1 11/27/2015 19:52 WG830588 Barium 0.0172 0.00500 1 11/27/2015 19:52 WG830588 Beryllium ND 0.00200 1 11/27/2015 19:52 WG830588 Cadmium ND 0.00100 1 11/27/2015 19:52 WG830588 Chromium ND 0.00200 1 11/27/2015 19:52 WG830588 Copper ND 0.00500 1 11/27/2015 19:52 WG830588 Cobalt ND 0.00200 1 11/27/2015 19:52 WG830588 Lead ND 0.00200 1 11/27/2015 19:52 WG830588 Nickel ND 0.00200 1 11/27/2015 19:52 WG830588 Selenium ND 0.00200 1 11/27/2015 19:52 WG830588 Silver ND 0.00200 1 11/27/2015 19:52 WG830588 Thallium ND 0.00200 1 11/27/2015 19:52 WG830588 Vanadium ND 0.00500 1 11/27/2015 19:52 WG830588 Zinc ND 0.0250 1 11/27/2015 19:52 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/20/2015 22:16 WG830452 Acrylonitrile ND 0.0100 1 11/20/2015 22:16 WG830452 Benzene ND 0.00100 1 11/20/2015 22:16 WG830452 Bromochloromethane ND 0.00100 1 11/20/2015 22:16 WG830452 Bromodichloromethane ND 0.00100 1 11/20/2015 22:16 WG830452 Bromoform ND 0.00100 1 11/20/2015 22:16 WG830452 Bromomethane ND 0.00500 1 11/20/2015 22:16 WG830452 Carbon disulfide ND 0.00100 1 11/20/2015 22:16 WG830452 Carbon tetrachloride ND 0.00100 1 11/20/2015 22:16 WG830452 Chlorobenzene 0.00153 0.00100 1 11/20/2015 22:16 WG830452 Chlorodibromomethane ND 0.00100 1 11/20/2015 22:16 WG830452 Chloroethane ND 0.00500 1 11/20/2015 22:16 WG830452 Chloroform ND 0.00500 1 11/20/2015 22:16 WG830452 Chloromethane ND 0.00250 1 11/20/2015 22:16 WG830452 Dibromomethane ND 0.00100 1 11/20/2015 22:16 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/20/2015 22:16 WG830452 1,4-Dichlorobenzene 0.00501 0.00100 1 11/20/2015 22:16 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/20/2015 22:16 WG830452 1,1-Dichloroethane 0.00381 0.00100 1 11/20/2015 22:16 WG830452 1,2-Dichloroethane ND 0.00100 1 11/20/2015 22:16 WG830452 1,1-Dichloroethene ND 0.00100 1 11/20/2015 22:16 WG830452 cis-1,2-Dichloroethene 0.00157 0.00100 1 11/20/2015 22:16 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/20/2015 22:16 WG830452 1,2-Dichloropropane ND 0.00100 1 11/20/2015 22:16 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/20/2015 22:16 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/20/2015 22:16 WG830452 Ethylbenzene ND 0.00100 1 11/20/2015 22:16 WG830452 2-Hexanone ND 0.0100 1 11/20/2015 22:16 WG830452 Iodomethane ND 0.0100 1 11/20/2015 22:16 WG830452 2-Butanone (MEK)ND 0.0100 1 11/20/2015 22:16 WG830452 Methylene Chloride ND 0.00500 1 11/20/2015 22:16 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/20/2015 22:16 WG830452 Styrene ND 0.00100 1 11/20/2015 22:16 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/20/2015 22:16 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/20/2015 22:16 WG830452 Tetrachloroethene ND 0.00100 1 11/20/2015 22:16 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 12 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 12 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L801958 MW-5 15FT Collected date/time: 11/18/15 16:15 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/20/2015 22:16 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/20/2015 22:16 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/20/2015 22:16 WG830452 Trichloroethene ND 0.00100 1 11/20/2015 22:16 WG830452 Trichlorofluoromethane ND 0.00500 1 11/20/2015 22:16 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/20/2015 22:16 WG830452 Vinyl acetate ND 0.0100 1 11/20/2015 22:16 WG830452 Vinyl chloride 0.00105 0.00100 1 11/20/2015 22:16 WG830452 Xylenes, Total ND 0.00300 1 11/20/2015 22:16 WG830452 (S) Toluene-d8 104 90.0-115 11/20/2015 22:16 WG830452 (S) Dibromofluoromethane 98.0 79.0-121 11/20/2015 22:16 WG830452 (S) a,a,a-Trifluorotoluene 106 90.4-116 11/20/2015 22:16 WG830452 (S) 4-Bromofluorobenzene 107 80.1-120 11/20/2015 22:16 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 13 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 13 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03 L801958 MW-6 15FT Collected date/time: 11/17/15 09:15 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 19:55 WG830588 Arsenic ND 0.00200 1 11/27/2015 19:55 WG830588 Barium 0.0111 0.00500 1 11/27/2015 19:55 WG830588 Beryllium ND 0.00200 1 11/27/2015 19:55 WG830588 Cadmium ND 0.00100 1 11/27/2015 19:55 WG830588 Chromium ND 0.00200 1 11/27/2015 19:55 WG830588 Copper ND 0.00500 1 11/27/2015 19:55 WG830588 Cobalt ND 0.00200 1 11/27/2015 19:55 WG830588 Lead 0.00221 0.00200 1 11/27/2015 19:55 WG830588 Nickel ND 0.00200 1 11/27/2015 19:55 WG830588 Selenium ND 0.00200 1 11/27/2015 19:55 WG830588 Silver ND 0.00200 1 11/27/2015 19:55 WG830588 Thallium ND 0.00200 1 11/27/2015 19:55 WG830588 Vanadium ND 0.00500 1 11/27/2015 19:55 WG830588 Zinc ND 0.0250 1 11/27/2015 19:55 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/20/2015 22:34 WG830452 Acrylonitrile ND 0.0100 1 11/20/2015 22:34 WG830452 Benzene ND 0.00100 1 11/20/2015 22:34 WG830452 Bromochloromethane ND 0.00100 1 11/20/2015 22:34 WG830452 Bromodichloromethane ND 0.00100 1 11/20/2015 22:34 WG830452 Bromoform ND 0.00100 1 11/20/2015 22:34 WG830452 Bromomethane ND 0.00500 1 11/20/2015 22:34 WG830452 Carbon disulfide ND 0.00100 1 11/20/2015 22:34 WG830452 Carbon tetrachloride ND 0.00100 1 11/20/2015 22:34 WG830452 Chlorobenzene ND 0.00100 1 11/20/2015 22:34 WG830452 Chlorodibromomethane ND 0.00100 1 11/20/2015 22:34 WG830452 Chloroethane ND 0.00500 1 11/20/2015 22:34 WG830452 Chloroform ND 0.00500 1 11/20/2015 22:34 WG830452 Chloromethane ND 0.00250 1 11/20/2015 22:34 WG830452 Dibromomethane ND 0.00100 1 11/20/2015 22:34 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/20/2015 22:34 WG830452 1,4-Dichlorobenzene ND 0.00100 1 11/20/2015 22:34 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/20/2015 22:34 WG830452 1,1-Dichloroethane ND 0.00100 1 11/20/2015 22:34 WG830452 1,2-Dichloroethane ND 0.00100 1 11/20/2015 22:34 WG830452 1,1-Dichloroethene ND 0.00100 1 11/20/2015 22:34 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/20/2015 22:34 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/20/2015 22:34 WG830452 1,2-Dichloropropane ND 0.00100 1 11/20/2015 22:34 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/20/2015 22:34 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/20/2015 22:34 WG830452 Ethylbenzene ND 0.00100 1 11/20/2015 22:34 WG830452 2-Hexanone ND 0.0100 1 11/20/2015 22:34 WG830452 Iodomethane ND 0.0100 1 11/20/2015 22:34 WG830452 2-Butanone (MEK)ND 0.0100 1 11/20/2015 22:34 WG830452 Methylene Chloride ND 0.00500 1 11/20/2015 22:34 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/20/2015 22:34 WG830452 Styrene ND 0.00100 1 11/20/2015 22:34 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/20/2015 22:34 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/20/2015 22:34 WG830452 Tetrachloroethene ND 0.00100 1 11/20/2015 22:34 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 14 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 14 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03 L801958 MW-6 15FT Collected date/time: 11/17/15 09:15 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/20/2015 22:34 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/20/2015 22:34 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/20/2015 22:34 WG830452 Trichloroethene ND 0.00100 1 11/20/2015 22:34 WG830452 Trichlorofluoromethane ND 0.00500 1 11/20/2015 22:34 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/20/2015 22:34 WG830452 Vinyl acetate ND 0.0100 1 11/20/2015 22:34 WG830452 Vinyl chloride ND 0.00100 1 11/20/2015 22:34 WG830452 Xylenes, Total ND 0.00300 1 11/20/2015 22:34 WG830452 (S) Toluene-d8 105 90.0-115 11/20/2015 22:34 WG830452 (S) Dibromofluoromethane 95.6 79.0-121 11/20/2015 22:34 WG830452 (S) a,a,a-Trifluorotoluene 108 90.4-116 11/20/2015 22:34 WG830452 (S) 4-Bromofluorobenzene 106 80.1-120 11/20/2015 22:34 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 15 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 15 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04 L801958 MW-8 15FT Collected date/time: 11/17/15 15:25 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 19:57 WG830588 Arsenic 0.00551 0.00200 1 11/27/2015 19:57 WG830588 Barium 0.0633 0.00500 1 11/27/2015 19:57 WG830588 Beryllium ND 0.00200 1 11/27/2015 19:57 WG830588 Cadmium ND 0.00100 1 11/27/2015 19:57 WG830588 Chromium 0.00203 0.00200 1 11/27/2015 19:57 WG830588 Copper ND 0.00500 1 11/27/2015 19:57 WG830588 Cobalt ND 0.00200 1 11/27/2015 19:57 WG830588 Lead 0.0321 0.00200 1 11/27/2015 19:57 WG830588 Nickel ND 0.00200 1 11/27/2015 19:57 WG830588 Selenium ND 0.00200 1 11/27/2015 19:57 WG830588 Silver ND 0.00200 1 11/27/2015 19:57 WG830588 Thallium ND 0.00200 1 11/27/2015 19:57 WG830588 Vanadium 0.00757 0.00500 1 11/27/2015 19:57 WG830588 Zinc ND 0.0250 1 11/27/2015 19:57 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/20/2015 22:53 WG830452 Acrylonitrile ND 0.0100 1 11/20/2015 22:53 WG830452 Benzene ND 0.00100 1 11/20/2015 22:53 WG830452 Bromochloromethane ND 0.00100 1 11/20/2015 22:53 WG830452 Bromodichloromethane ND 0.00100 1 11/20/2015 22:53 WG830452 Bromoform ND 0.00100 1 11/20/2015 22:53 WG830452 Bromomethane ND 0.00500 1 11/20/2015 22:53 WG830452 Carbon disulfide ND 0.00100 1 11/20/2015 22:53 WG830452 Carbon tetrachloride ND 0.00100 1 11/20/2015 22:53 WG830452 Chlorobenzene ND 0.00100 1 11/20/2015 22:53 WG830452 Chlorodibromomethane ND 0.00100 1 11/20/2015 22:53 WG830452 Chloroethane ND 0.00500 1 11/20/2015 22:53 WG830452 Chloroform ND 0.00500 1 11/20/2015 22:53 WG830452 Chloromethane ND 0.00250 1 11/20/2015 22:53 WG830452 Dibromomethane ND 0.00100 1 11/20/2015 22:53 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/20/2015 22:53 WG830452 1,4-Dichlorobenzene ND 0.00100 1 11/20/2015 22:53 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/20/2015 22:53 WG830452 1,1-Dichloroethane 0.00310 0.00100 1 11/20/2015 22:53 WG830452 1,2-Dichloroethane ND 0.00100 1 11/20/2015 22:53 WG830452 1,1-Dichloroethene ND 0.00100 1 11/20/2015 22:53 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/20/2015 22:53 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/20/2015 22:53 WG830452 1,2-Dichloropropane ND 0.00100 1 11/20/2015 22:53 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/20/2015 22:53 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/20/2015 22:53 WG830452 Ethylbenzene ND 0.00100 1 11/20/2015 22:53 WG830452 2-Hexanone ND 0.0100 1 11/20/2015 22:53 WG830452 Iodomethane ND 0.0100 1 11/20/2015 22:53 WG830452 2-Butanone (MEK)ND 0.0100 1 11/20/2015 22:53 WG830452 Methylene Chloride ND 0.00500 1 11/20/2015 22:53 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/20/2015 22:53 WG830452 Styrene ND 0.00100 1 11/20/2015 22:53 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/20/2015 22:53 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/20/2015 22:53 WG830452 Tetrachloroethene ND 0.00100 1 11/20/2015 22:53 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 16 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 16 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04 L801958 MW-8 15FT Collected date/time: 11/17/15 15:25 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/20/2015 22:53 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/20/2015 22:53 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/20/2015 22:53 WG830452 Trichloroethene ND 0.00100 1 11/20/2015 22:53 WG830452 Trichlorofluoromethane ND 0.00500 1 11/20/2015 22:53 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/20/2015 22:53 WG830452 Vinyl acetate ND 0.0100 1 11/20/2015 22:53 WG830452 Vinyl chloride ND 0.00100 1 11/20/2015 22:53 WG830452 Xylenes, Total ND 0.00300 1 11/20/2015 22:53 WG830452 (S) Toluene-d8 106 90.0-115 11/20/2015 22:53 WG830452 (S) Dibromofluoromethane 99.3 79.0-121 11/20/2015 22:53 WG830452 (S) a,a,a-Trifluorotoluene 112 90.4-116 11/20/2015 22:53 WG830452 (S) 4-Bromofluorobenzene 108 80.1-120 11/20/2015 22:53 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 17 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 17 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05 L801958 MW-9A 15FT Collected date/time: 11/18/15 16:35 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 18:51 WG830588 Arsenic ND 0.00200 1 11/27/2015 18:51 WG830588 Barium 0.0624 0.00500 1 11/27/2015 18:51 WG830588 Beryllium ND 0.00200 1 11/27/2015 18:51 WG830588 Cadmium ND 0.00100 1 11/27/2015 18:51 WG830588 Chromium ND 0.00200 1 11/27/2015 18:51 WG830588 Copper ND 0.00500 1 11/27/2015 18:51 WG830588 Cobalt ND 0.00200 1 11/27/2015 18:51 WG830588 Lead ND 0.00200 1 11/27/2015 18:51 WG830588 Nickel ND 0.00200 1 11/27/2015 18:51 WG830588 Selenium ND 0.00200 1 11/27/2015 18:51 WG830588 Silver ND 0.00200 1 11/27/2015 18:51 WG830588 Thallium ND 0.00200 1 11/27/2015 18:51 WG830588 Vanadium ND 0.00500 1 11/27/2015 18:51 WG830588 Zinc ND 0.0250 1 11/27/2015 18:51 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/20/2015 23:11 WG830452 Acrylonitrile ND 0.0100 1 11/20/2015 23:11 WG830452 Benzene ND 0.00100 1 11/20/2015 23:11 WG830452 Bromochloromethane ND 0.00100 1 11/20/2015 23:11 WG830452 Bromodichloromethane ND 0.00100 1 11/20/2015 23:11 WG830452 Bromoform ND 0.00100 1 11/20/2015 23:11 WG830452 Bromomethane ND 0.00500 1 11/20/2015 23:11 WG830452 Carbon disulfide ND 0.00100 1 11/20/2015 23:11 WG830452 Carbon tetrachloride ND 0.00100 1 11/20/2015 23:11 WG830452 Chlorobenzene 0.00147 0.00100 1 11/20/2015 23:11 WG830452 Chlorodibromomethane ND 0.00100 1 11/20/2015 23:11 WG830452 Chloroethane ND 0.00500 1 11/20/2015 23:11 WG830452 Chloroform ND 0.00500 1 11/20/2015 23:11 WG830452 Chloromethane ND 0.00250 1 11/20/2015 23:11 WG830452 Dibromomethane ND 0.00100 1 11/20/2015 23:11 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/20/2015 23:11 WG830452 1,4-Dichlorobenzene 0.00743 0.00100 1 11/20/2015 23:11 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/20/2015 23:11 WG830452 1,1-Dichloroethane 0.00816 0.00100 1 11/20/2015 23:11 WG830452 1,2-Dichloroethane ND 0.00100 1 11/20/2015 23:11 WG830452 1,1-Dichloroethene ND 0.00100 1 11/20/2015 23:11 WG830452 cis-1,2-Dichloroethene 0.00115 0.00100 1 11/20/2015 23:11 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/20/2015 23:11 WG830452 1,2-Dichloropropane ND 0.00100 1 11/20/2015 23:11 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/20/2015 23:11 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/20/2015 23:11 WG830452 Ethylbenzene ND 0.00100 1 11/20/2015 23:11 WG830452 2-Hexanone ND 0.0100 1 11/20/2015 23:11 WG830452 Iodomethane ND 0.0100 1 11/20/2015 23:11 WG830452 2-Butanone (MEK)ND 0.0100 1 11/20/2015 23:11 WG830452 Methylene Chloride ND 0.00500 1 11/20/2015 23:11 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/20/2015 23:11 WG830452 Styrene ND 0.00100 1 11/20/2015 23:11 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/20/2015 23:11 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/20/2015 23:11 WG830452 Tetrachloroethene ND 0.00100 1 11/20/2015 23:11 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 18 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 18 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05 L801958 MW-9A 15FT Collected date/time: 11/18/15 16:35 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/20/2015 23:11 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/20/2015 23:11 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/20/2015 23:11 WG830452 Trichloroethene ND 0.00100 1 11/20/2015 23:11 WG830452 Trichlorofluoromethane ND 0.00500 1 11/20/2015 23:11 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/20/2015 23:11 WG830452 Vinyl acetate ND 0.0100 1 11/20/2015 23:11 WG830452 Vinyl chloride ND 0.00100 1 11/20/2015 23:11 WG830452 Xylenes, Total ND 0.00300 1 11/20/2015 23:11 WG830452 (S) Toluene-d8 102 90.0-115 11/20/2015 23:11 WG830452 (S) Dibromofluoromethane 94.5 79.0-121 11/20/2015 23:11 WG830452 (S) a,a,a-Trifluorotoluene 105 90.4-116 11/20/2015 23:11 WG830452 (S) 4-Bromofluorobenzene 102 80.1-120 11/20/2015 23:11 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 19 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 19 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06 L801958 MW-10 15FT Collected date/time: 11/17/15 15:45 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 19:59 WG830588 Arsenic 0.00436 0.00200 1 11/27/2015 19:59 WG830588 Barium 0.0655 0.00500 1 11/27/2015 19:59 WG830588 Beryllium ND 0.00200 1 11/27/2015 19:59 WG830588 Cadmium ND 0.00100 1 11/27/2015 19:59 WG830588 Chromium 0.0181 0.00200 1 11/27/2015 19:59 WG830588 Copper 0.00651 0.00500 1 11/27/2015 19:59 WG830588 Cobalt ND 0.00200 1 11/27/2015 19:59 WG830588 Lead 0.0167 0.00200 1 11/27/2015 19:59 WG830588 Nickel 0.00470 0.00200 1 11/27/2015 19:59 WG830588 Selenium ND 0.00200 1 11/27/2015 19:59 WG830588 Silver ND 0.00200 1 11/27/2015 19:59 WG830588 Thallium ND 0.00200 1 11/27/2015 19:59 WG830588 Vanadium 0.0348 0.00500 1 11/27/2015 19:59 WG830588 Zinc ND 0.0250 1 11/27/2015 19:59 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/20/2015 23:29 WG830452 Acrylonitrile ND 0.0100 1 11/20/2015 23:29 WG830452 Benzene ND 0.00100 1 11/20/2015 23:29 WG830452 Bromochloromethane ND 0.00100 1 11/20/2015 23:29 WG830452 Bromodichloromethane ND 0.00100 1 11/20/2015 23:29 WG830452 Bromoform ND 0.00100 1 11/20/2015 23:29 WG830452 Bromomethane ND 0.00500 1 11/20/2015 23:29 WG830452 Carbon disulfide ND 0.00100 1 11/20/2015 23:29 WG830452 Carbon tetrachloride ND 0.00100 1 11/20/2015 23:29 WG830452 Chlorobenzene ND 0.00100 1 11/20/2015 23:29 WG830452 Chlorodibromomethane ND 0.00100 1 11/20/2015 23:29 WG830452 Chloroethane ND 0.00500 1 11/20/2015 23:29 WG830452 Chloroform ND 0.00500 1 11/20/2015 23:29 WG830452 Chloromethane ND 0.00250 1 11/20/2015 23:29 WG830452 Dibromomethane ND 0.00100 1 11/20/2015 23:29 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/20/2015 23:29 WG830452 1,4-Dichlorobenzene ND 0.00100 1 11/20/2015 23:29 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/20/2015 23:29 WG830452 1,1-Dichloroethane ND 0.00100 1 11/20/2015 23:29 WG830452 1,2-Dichloroethane ND 0.00100 1 11/20/2015 23:29 WG830452 1,1-Dichloroethene ND 0.00100 1 11/20/2015 23:29 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/20/2015 23:29 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/20/2015 23:29 WG830452 1,2-Dichloropropane ND 0.00100 1 11/20/2015 23:29 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/20/2015 23:29 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/20/2015 23:29 WG830452 Ethylbenzene ND 0.00100 1 11/20/2015 23:29 WG830452 2-Hexanone ND 0.0100 1 11/20/2015 23:29 WG830452 Iodomethane ND 0.0100 1 11/20/2015 23:29 WG830452 2-Butanone (MEK)ND 0.0100 1 11/20/2015 23:29 WG830452 Methylene Chloride ND 0.00500 1 11/20/2015 23:29 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/20/2015 23:29 WG830452 Styrene ND 0.00100 1 11/20/2015 23:29 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/20/2015 23:29 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/20/2015 23:29 WG830452 Tetrachloroethene ND 0.00100 1 11/20/2015 23:29 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 20 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 20 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06 L801958 MW-10 15FT Collected date/time: 11/17/15 15:45 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/20/2015 23:29 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/20/2015 23:29 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/20/2015 23:29 WG830452 Trichloroethene ND 0.00100 1 11/20/2015 23:29 WG830452 Trichlorofluoromethane ND 0.00500 1 11/20/2015 23:29 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/20/2015 23:29 WG830452 Vinyl acetate ND 0.0100 1 11/20/2015 23:29 WG830452 Vinyl chloride ND 0.00100 1 11/20/2015 23:29 WG830452 Xylenes, Total ND 0.00300 1 11/20/2015 23:29 WG830452 (S) Toluene-d8 103 90.0-115 11/20/2015 23:29 WG830452 (S) Dibromofluoromethane 100 79.0-121 11/20/2015 23:29 WG830452 (S) a,a,a-Trifluorotoluene 106 90.4-116 11/20/2015 23:29 WG830452 (S) 4-Bromofluorobenzene 104 80.1-120 11/20/2015 23:29 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 21 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 21 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07 L801958 MW-11 15FT Collected date/time: 11/17/15 15:40 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:02 WG830588 Arsenic 0.0115 0.00200 1 11/27/2015 20:02 WG830588 Barium 0.0889 0.00500 1 11/27/2015 20:02 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:02 WG830588 Cadmium 0.00443 0.00100 1 11/27/2015 20:02 WG830588 Chromium 0.0338 0.00200 1 11/27/2015 20:02 WG830588 Copper 0.0443 0.00500 1 11/27/2015 20:02 WG830588 Cobalt 0.00646 0.00200 1 11/27/2015 20:02 WG830588 Lead 0.0352 0.00200 1 11/27/2015 20:02 WG830588 Nickel 0.0197 0.00200 1 11/27/2015 20:02 WG830588 Selenium ND 0.00200 1 11/27/2015 20:02 WG830588 Silver ND 0.00200 1 11/27/2015 20:02 WG830588 Thallium ND 0.00200 1 11/27/2015 20:02 WG830588 Vanadium 0.0667 0.00500 1 11/27/2015 20:02 WG830588 Zinc 0.221 0.0250 1 11/27/2015 20:02 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/20/2015 23:48 WG830452 Acrylonitrile ND 0.0100 1 11/20/2015 23:48 WG830452 Benzene ND 0.00100 1 11/20/2015 23:48 WG830452 Bromochloromethane ND 0.00100 1 11/20/2015 23:48 WG830452 Bromodichloromethane ND 0.00100 1 11/20/2015 23:48 WG830452 Bromoform ND 0.00100 1 11/20/2015 23:48 WG830452 Bromomethane ND 0.00500 1 11/20/2015 23:48 WG830452 Carbon disulfide ND 0.00100 1 11/20/2015 23:48 WG830452 Carbon tetrachloride ND 0.00100 1 11/20/2015 23:48 WG830452 Chlorobenzene ND 0.00100 1 11/20/2015 23:48 WG830452 Chlorodibromomethane ND 0.00100 1 11/20/2015 23:48 WG830452 Chloroethane ND 0.00500 1 11/20/2015 23:48 WG830452 Chloroform ND 0.00500 1 11/20/2015 23:48 WG830452 Chloromethane ND 0.00250 1 11/20/2015 23:48 WG830452 Dibromomethane ND 0.00100 1 11/20/2015 23:48 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/20/2015 23:48 WG830452 1,4-Dichlorobenzene ND 0.00100 1 11/20/2015 23:48 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/20/2015 23:48 WG830452 1,1-Dichloroethane ND 0.00100 1 11/20/2015 23:48 WG830452 1,2-Dichloroethane ND 0.00100 1 11/20/2015 23:48 WG830452 1,1-Dichloroethene ND 0.00100 1 11/20/2015 23:48 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/20/2015 23:48 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/20/2015 23:48 WG830452 1,2-Dichloropropane ND 0.00100 1 11/20/2015 23:48 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/20/2015 23:48 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/20/2015 23:48 WG830452 Ethylbenzene ND 0.00100 1 11/20/2015 23:48 WG830452 2-Hexanone ND 0.0100 1 11/20/2015 23:48 WG830452 Iodomethane ND 0.0100 1 11/20/2015 23:48 WG830452 2-Butanone (MEK)ND 0.0100 1 11/20/2015 23:48 WG830452 Methylene Chloride ND 0.00500 1 11/20/2015 23:48 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/20/2015 23:48 WG830452 Styrene ND 0.00100 1 11/20/2015 23:48 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/20/2015 23:48 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/20/2015 23:48 WG830452 Tetrachloroethene ND 0.00100 1 11/20/2015 23:48 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 22 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 22 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07 L801958 MW-11 15FT Collected date/time: 11/17/15 15:40 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/20/2015 23:48 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/20/2015 23:48 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/20/2015 23:48 WG830452 Trichloroethene ND 0.00100 1 11/20/2015 23:48 WG830452 Trichlorofluoromethane ND 0.00500 1 11/20/2015 23:48 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/20/2015 23:48 WG830452 Vinyl acetate ND 0.0100 1 11/20/2015 23:48 WG830452 Vinyl chloride ND 0.00100 1 11/20/2015 23:48 WG830452 Xylenes, Total ND 0.00300 1 11/20/2015 23:48 WG830452 (S) Toluene-d8 102 90.0-115 11/20/2015 23:48 WG830452 (S) Dibromofluoromethane 102 79.0-121 11/20/2015 23:48 WG830452 (S) a,a,a-Trifluorotoluene 111 90.4-116 11/20/2015 23:48 WG830452 (S) 4-Bromofluorobenzene 104 80.1-120 11/20/2015 23:48 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 23 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 23 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08 L801958 MW-12 15FT Collected date/time: 11/17/15 10:10 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:04 WG830588 Arsenic ND 0.00200 1 11/27/2015 20:04 WG830588 Barium 0.102 0.00500 1 11/27/2015 20:04 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:04 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:04 WG830588 Chromium 0.00835 0.00200 1 11/27/2015 20:04 WG830588 Copper ND 0.00500 1 11/27/2015 20:04 WG830588 Cobalt ND 0.00200 1 11/27/2015 20:04 WG830588 Lead 0.00559 0.00200 1 11/27/2015 20:04 WG830588 Nickel 0.00235 0.00200 1 11/27/2015 20:04 WG830588 Selenium ND 0.00200 1 11/27/2015 20:04 WG830588 Silver ND 0.00200 1 11/27/2015 20:04 WG830588 Thallium ND 0.00200 1 11/27/2015 20:04 WG830588 Vanadium 0.0150 0.00500 1 11/27/2015 20:04 WG830588 Zinc ND 0.0250 1 11/27/2015 20:04 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/20/2015 21:03 WG830452 Acrylonitrile ND 0.0100 1 11/20/2015 21:03 WG830452 Benzene ND 0.00100 1 11/20/2015 21:03 WG830452 Bromochloromethane ND 0.00100 1 11/20/2015 21:03 WG830452 Bromodichloromethane ND 0.00100 1 11/20/2015 21:03 WG830452 Bromoform ND 0.00100 1 11/20/2015 21:03 WG830452 Bromomethane ND 0.00500 1 11/20/2015 21:03 WG830452 Carbon disulfide ND 0.00100 1 11/20/2015 21:03 WG830452 Carbon tetrachloride ND 0.00100 1 11/20/2015 21:03 WG830452 Chlorobenzene ND 0.00100 1 11/20/2015 21:03 WG830452 Chlorodibromomethane ND 0.00100 1 11/20/2015 21:03 WG830452 Chloroethane ND 0.00500 1 11/20/2015 21:03 WG830452 Chloroform ND 0.00500 1 11/20/2015 21:03 WG830452 Chloromethane ND 0.00250 1 11/20/2015 21:03 WG830452 Dibromomethane ND 0.00100 1 11/20/2015 21:03 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/20/2015 21:03 WG830452 1,4-Dichlorobenzene ND 0.00100 1 11/20/2015 21:03 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/20/2015 21:03 WG830452 1,1-Dichloroethane ND 0.00100 1 11/20/2015 21:03 WG830452 1,2-Dichloroethane ND 0.00100 1 11/20/2015 21:03 WG830452 1,1-Dichloroethene ND 0.00100 1 11/20/2015 21:03 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/20/2015 21:03 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/20/2015 21:03 WG830452 1,2-Dichloropropane ND 0.00100 1 11/20/2015 21:03 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/20/2015 21:03 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/20/2015 21:03 WG830452 Ethylbenzene ND 0.00100 1 11/20/2015 21:03 WG830452 2-Hexanone ND 0.0100 1 11/20/2015 21:03 WG830452 Iodomethane ND 0.0100 1 11/20/2015 21:03 WG830452 2-Butanone (MEK)ND 0.0100 1 11/20/2015 21:03 WG830452 Methylene Chloride ND 0.00500 1 11/20/2015 21:03 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/20/2015 21:03 WG830452 Styrene ND 0.00100 1 11/20/2015 21:03 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/20/2015 21:03 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/20/2015 21:03 WG830452 Tetrachloroethene ND 0.00100 1 11/20/2015 21:03 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 24 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 24 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08 L801958 MW-12 15FT Collected date/time: 11/17/15 10:10 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/20/2015 21:03 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/20/2015 21:03 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/20/2015 21:03 WG830452 Trichloroethene ND 0.00100 1 11/20/2015 21:03 WG830452 Trichlorofluoromethane ND 0.00500 1 11/20/2015 21:03 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/20/2015 21:03 WG830452 Vinyl acetate ND 0.0100 1 11/20/2015 21:03 WG830452 Vinyl chloride ND 0.00100 1 11/20/2015 21:03 WG830452 Xylenes, Total ND 0.00300 1 11/20/2015 21:03 WG830452 (S) Toluene-d8 102 90.0-115 11/20/2015 21:03 WG830452 (S) Dibromofluoromethane 96.9 79.0-121 11/20/2015 21:03 WG830452 (S) a,a,a-Trifluorotoluene 109 90.4-116 11/20/2015 21:03 WG830452 (S) 4-Bromofluorobenzene 110 80.1-120 11/20/2015 21:03 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 25 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 25 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09 L801958 MW-13R 15FT Collected date/time: 11/17/15 11:50 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:06 WG830588 Arsenic ND 0.00200 1 11/27/2015 20:06 WG830588 Barium 0.204 0.00500 1 11/27/2015 20:06 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:06 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:06 WG830588 Chromium 0.00224 0.00200 1 11/27/2015 20:06 WG830588 Copper ND 0.00500 1 11/27/2015 20:06 WG830588 Cobalt 0.00429 0.00200 1 11/27/2015 20:06 WG830588 Lead 0.00679 0.00200 1 11/27/2015 20:06 WG830588 Nickel 0.00264 0.00200 1 11/27/2015 20:06 WG830588 Selenium ND 0.00200 1 11/27/2015 20:06 WG830588 Silver ND 0.00200 1 11/27/2015 20:06 WG830588 Thallium ND 0.00200 1 11/27/2015 20:06 WG830588 Vanadium ND 0.00500 1 11/27/2015 20:06 WG830588 Zinc ND 0.0250 1 11/27/2015 20:06 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 00:06 WG830452 Acrylonitrile ND 0.0100 1 11/21/2015 00:06 WG830452 Benzene 0.00217 0.00100 1 11/21/2015 00:06 WG830452 Bromochloromethane ND 0.00100 1 11/21/2015 00:06 WG830452 Bromodichloromethane ND 0.00100 1 11/21/2015 00:06 WG830452 Bromoform ND 0.00100 1 11/21/2015 00:06 WG830452 Bromomethane ND 0.00500 1 11/21/2015 00:06 WG830452 Carbon disulfide ND 0.00100 1 11/21/2015 00:06 WG830452 Carbon tetrachloride ND 0.00100 1 11/21/2015 00:06 WG830452 Chlorobenzene ND 0.00100 1 11/21/2015 00:06 WG830452 Chlorodibromomethane ND 0.00100 1 11/21/2015 00:06 WG830452 Chloroethane ND 0.00500 1 11/21/2015 00:06 WG830452 Chloroform ND 0.00500 1 11/21/2015 00:06 WG830452 Chloromethane ND 0.00250 1 11/21/2015 00:06 WG830452 Dibromomethane ND 0.00100 1 11/21/2015 00:06 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 00:06 WG830452 1,4-Dichlorobenzene 0.00135 0.00100 1 11/21/2015 00:06 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 00:06 WG830452 1,1-Dichloroethane ND 0.00100 1 11/21/2015 00:06 WG830452 1,2-Dichloroethane ND 0.00100 1 11/21/2015 00:06 WG830452 1,1-Dichloroethene ND 0.00100 1 11/21/2015 00:06 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 00:06 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 00:06 WG830452 1,2-Dichloropropane ND 0.00100 1 11/21/2015 00:06 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 00:06 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 00:06 WG830452 Ethylbenzene ND 0.00100 1 11/21/2015 00:06 WG830452 2-Hexanone ND 0.0100 1 11/21/2015 00:06 WG830452 Iodomethane ND 0.0100 1 11/21/2015 00:06 WG830452 2-Butanone (MEK)ND 0.0100 1 11/21/2015 00:06 WG830452 Methylene Chloride ND 0.00500 1 11/21/2015 00:06 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 00:06 WG830452 Styrene ND 0.00100 1 11/21/2015 00:06 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 00:06 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 00:06 WG830452 Tetrachloroethene ND 0.00100 1 11/21/2015 00:06 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 26 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 26 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09 L801958 MW-13R 15FT Collected date/time: 11/17/15 11:50 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 00:06 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 00:06 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 00:06 WG830452 Trichloroethene ND 0.00100 1 11/21/2015 00:06 WG830452 Trichlorofluoromethane ND 0.00500 1 11/21/2015 00:06 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 00:06 WG830452 Vinyl acetate ND 0.0100 1 11/21/2015 00:06 WG830452 Vinyl chloride ND 0.00100 1 11/21/2015 00:06 WG830452 Xylenes, Total ND 0.00300 1 11/21/2015 00:06 WG830452 (S) Toluene-d8 102 90.0-115 11/21/2015 00:06 WG830452 (S) Dibromofluoromethane 95.8 79.0-121 11/21/2015 00:06 WG830452 (S) a,a,a-Trifluorotoluene 111 90.4-116 11/21/2015 00:06 WG830452 (S) 4-Bromofluorobenzene 110 80.1-120 11/21/2015 00:06 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 27 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 27 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10 L801958 MW-14 15FT Collected date/time: 11/17/15 12:10 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:09 WG830588 Arsenic ND 0.00200 1 11/27/2015 20:09 WG830588 Barium 0.211 0.00500 1 11/27/2015 20:09 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:09 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:09 WG830588 Chromium ND 0.00200 1 11/27/2015 20:09 WG830588 Copper ND 0.00500 1 11/27/2015 20:09 WG830588 Cobalt 0.00302 0.00200 1 11/27/2015 20:09 WG830588 Lead 0.00202 0.00200 1 11/27/2015 20:09 WG830588 Nickel 0.00336 0.00200 1 11/27/2015 20:09 WG830588 Selenium ND 0.00200 1 11/27/2015 20:09 WG830588 Silver ND 0.00200 1 11/27/2015 20:09 WG830588 Thallium ND 0.00200 1 11/27/2015 20:09 WG830588 Vanadium ND 0.00500 1 11/27/2015 20:09 WG830588 Zinc ND 0.0250 1 11/27/2015 20:09 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 00:24 WG830452 Acrylonitrile ND 0.0100 1 11/21/2015 00:24 WG830452 Benzene ND 0.00100 1 11/21/2015 00:24 WG830452 Bromochloromethane ND 0.00100 1 11/21/2015 00:24 WG830452 Bromodichloromethane ND 0.00100 1 11/21/2015 00:24 WG830452 Bromoform ND 0.00100 1 11/21/2015 00:24 WG830452 Bromomethane ND 0.00500 1 11/21/2015 00:24 WG830452 Carbon disulfide ND 0.00100 1 11/21/2015 00:24 WG830452 Carbon tetrachloride ND 0.00100 1 11/21/2015 00:24 WG830452 Chlorobenzene ND 0.00100 1 11/21/2015 00:24 WG830452 Chlorodibromomethane ND 0.00100 1 11/21/2015 00:24 WG830452 Chloroethane ND 0.00500 1 11/21/2015 00:24 WG830452 Chloroform ND 0.00500 1 11/21/2015 00:24 WG830452 Chloromethane ND 0.00250 1 11/21/2015 00:24 WG830452 Dibromomethane ND 0.00100 1 11/21/2015 00:24 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 00:24 WG830452 1,4-Dichlorobenzene 0.00235 0.00100 1 11/21/2015 00:24 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 00:24 WG830452 1,1-Dichloroethane ND 0.00100 1 11/21/2015 00:24 WG830452 1,2-Dichloroethane ND 0.00100 1 11/21/2015 00:24 WG830452 1,1-Dichloroethene ND 0.00100 1 11/21/2015 00:24 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 00:24 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 00:24 WG830452 1,2-Dichloropropane ND 0.00100 1 11/21/2015 00:24 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 00:24 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 00:24 WG830452 Ethylbenzene ND 0.00100 1 11/21/2015 00:24 WG830452 2-Hexanone ND 0.0100 1 11/21/2015 00:24 WG830452 Iodomethane ND 0.0100 1 11/21/2015 00:24 WG830452 2-Butanone (MEK)ND 0.0100 1 11/21/2015 00:24 WG830452 Methylene Chloride ND 0.00500 1 11/21/2015 00:24 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 00:24 WG830452 Styrene ND 0.00100 1 11/21/2015 00:24 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 00:24 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 00:24 WG830452 Tetrachloroethene ND 0.00100 1 11/21/2015 00:24 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 28 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 28 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10 L801958 MW-14 15FT Collected date/time: 11/17/15 12:10 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 00:24 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 00:24 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 00:24 WG830452 Trichloroethene ND 0.00100 1 11/21/2015 00:24 WG830452 Trichlorofluoromethane ND 0.00500 1 11/21/2015 00:24 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 00:24 WG830452 Vinyl acetate ND 0.0100 1 11/21/2015 00:24 WG830452 Vinyl chloride ND 0.00100 1 11/21/2015 00:24 WG830452 Xylenes, Total ND 0.00300 1 11/21/2015 00:24 WG830452 (S) Toluene-d8 100 90.0-115 11/21/2015 00:24 WG830452 (S) Dibromofluoromethane 99.6 79.0-121 11/21/2015 00:24 WG830452 (S) a,a,a-Trifluorotoluene 108 90.4-116 11/21/2015 00:24 WG830452 (S) 4-Bromofluorobenzene 104 80.1-120 11/21/2015 00:24 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 29 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 29 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11 L801958 MW-15 15FT Collected date/time: 11/17/15 12:20 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:11 WG830588 Arsenic ND 0.00200 1 11/27/2015 20:11 WG830588 Barium 0.0909 0.00500 1 11/27/2015 20:11 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:11 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:11 WG830588 Chromium ND 0.00200 1 11/27/2015 20:11 WG830588 Copper ND 0.00500 1 11/27/2015 20:11 WG830588 Cobalt 0.00334 0.00200 1 11/27/2015 20:11 WG830588 Lead ND 0.00200 1 11/27/2015 20:11 WG830588 Nickel ND 0.00200 1 11/27/2015 20:11 WG830588 Selenium ND 0.00200 1 11/27/2015 20:11 WG830588 Silver ND 0.00200 1 11/27/2015 20:11 WG830588 Thallium ND 0.00200 1 11/27/2015 20:11 WG830588 Vanadium ND 0.00500 1 11/27/2015 20:11 WG830588 Zinc ND 0.0250 1 11/27/2015 20:11 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 00:43 WG830452 Acrylonitrile ND 0.0100 1 11/21/2015 00:43 WG830452 Benzene 0.00156 0.00100 1 11/21/2015 00:43 WG830452 Bromochloromethane ND 0.00100 1 11/21/2015 00:43 WG830452 Bromodichloromethane ND 0.00100 1 11/21/2015 00:43 WG830452 Bromoform ND 0.00100 1 11/21/2015 00:43 WG830452 Bromomethane ND 0.00500 1 11/21/2015 00:43 WG830452 Carbon disulfide ND 0.00100 1 11/21/2015 00:43 WG830452 Carbon tetrachloride ND 0.00100 1 11/21/2015 00:43 WG830452 Chlorobenzene 0.00302 0.00100 1 11/21/2015 00:43 WG830452 Chlorodibromomethane ND 0.00100 1 11/21/2015 00:43 WG830452 Chloroethane ND 0.00500 1 11/21/2015 00:43 WG830452 Chloroform ND 0.00500 1 11/21/2015 00:43 WG830452 Chloromethane ND 0.00250 1 11/21/2015 00:43 WG830452 Dibromomethane ND 0.00100 1 11/21/2015 00:43 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 00:43 WG830452 1,4-Dichlorobenzene 0.00843 0.00100 1 11/21/2015 00:43 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 00:43 WG830452 1,1-Dichloroethane 0.00442 0.00100 1 11/21/2015 00:43 WG830452 1,2-Dichloroethane ND 0.00100 1 11/21/2015 00:43 WG830452 1,1-Dichloroethene ND 0.00100 1 11/21/2015 00:43 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 00:43 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 00:43 WG830452 1,2-Dichloropropane ND 0.00100 1 11/21/2015 00:43 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 00:43 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 00:43 WG830452 Ethylbenzene ND 0.00100 1 11/21/2015 00:43 WG830452 2-Hexanone ND 0.0100 1 11/21/2015 00:43 WG830452 Iodomethane ND 0.0100 1 11/21/2015 00:43 WG830452 2-Butanone (MEK)ND 0.0100 1 11/21/2015 00:43 WG830452 Methylene Chloride ND 0.00500 1 11/21/2015 00:43 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 00:43 WG830452 Styrene ND 0.00100 1 11/21/2015 00:43 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 00:43 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 00:43 WG830452 Tetrachloroethene ND 0.00100 1 11/21/2015 00:43 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 30 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 30 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11 L801958 MW-15 15FT Collected date/time: 11/17/15 12:20 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 00:43 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 00:43 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 00:43 WG830452 Trichloroethene ND 0.00100 1 11/21/2015 00:43 WG830452 Trichlorofluoromethane ND 0.00500 1 11/21/2015 00:43 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 00:43 WG830452 Vinyl acetate ND 0.0100 1 11/21/2015 00:43 WG830452 Vinyl chloride ND 0.00100 1 11/21/2015 00:43 WG830452 Xylenes, Total ND 0.00300 1 11/21/2015 00:43 WG830452 (S) Toluene-d8 103 90.0-115 11/21/2015 00:43 WG830452 (S) Dibromofluoromethane 102 79.0-121 11/21/2015 00:43 WG830452 (S) a,a,a-Trifluorotoluene 111 90.4-116 11/21/2015 00:43 WG830452 (S) 4-Bromofluorobenzene 101 80.1-120 11/21/2015 00:43 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 31 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 31 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12 L801958 MW-16 15FT Collected date/time: 11/17/15 14:15 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:27 WG830588 Arsenic 0.0137 0.00200 1 11/27/2015 20:27 WG830588 Barium 0.224 0.00500 1 11/27/2015 20:27 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:27 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:27 WG830588 Chromium 0.00228 0.00200 1 11/27/2015 20:27 WG830588 Copper ND 0.00500 1 11/27/2015 20:27 WG830588 Cobalt 0.00662 0.00200 1 11/27/2015 20:27 WG830588 Lead ND 0.00200 1 11/27/2015 20:27 WG830588 Nickel ND 0.00200 1 11/27/2015 20:27 WG830588 Selenium ND 0.00200 1 11/27/2015 20:27 WG830588 Silver ND 0.00200 1 11/27/2015 20:27 WG830588 Thallium ND 0.00200 1 11/27/2015 20:27 WG830588 Vanadium ND 0.00500 1 11/27/2015 20:27 WG830588 Zinc ND 0.0250 1 11/27/2015 20:27 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 01:01 WG830452 Acrylonitrile ND 0.0100 1 11/21/2015 01:01 WG830452 Benzene ND 0.00100 1 11/21/2015 01:01 WG830452 Bromochloromethane ND 0.00100 1 11/21/2015 01:01 WG830452 Bromodichloromethane ND 0.00100 1 11/21/2015 01:01 WG830452 Bromoform ND 0.00100 1 11/21/2015 01:01 WG830452 Bromomethane ND 0.00500 1 11/21/2015 01:01 WG830452 Carbon disulfide ND 0.00100 1 11/21/2015 01:01 WG830452 Carbon tetrachloride ND 0.00100 1 11/21/2015 01:01 WG830452 Chlorobenzene ND 0.00100 1 11/21/2015 01:01 WG830452 Chlorodibromomethane ND 0.00100 1 11/21/2015 01:01 WG830452 Chloroethane ND 0.00500 1 11/21/2015 01:01 WG830452 Chloroform ND 0.00500 1 11/21/2015 01:01 WG830452 Chloromethane ND 0.00250 1 11/21/2015 01:01 WG830452 Dibromomethane ND 0.00100 1 11/21/2015 01:01 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 01:01 WG830452 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 01:01 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 01:01 WG830452 1,1-Dichloroethane ND 0.00100 1 11/21/2015 01:01 WG830452 1,2-Dichloroethane ND 0.00100 1 11/21/2015 01:01 WG830452 1,1-Dichloroethene ND 0.00100 1 11/21/2015 01:01 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 01:01 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 01:01 WG830452 1,2-Dichloropropane ND 0.00100 1 11/21/2015 01:01 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 01:01 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 01:01 WG830452 Ethylbenzene ND 0.00100 1 11/21/2015 01:01 WG830452 2-Hexanone ND 0.0100 1 11/21/2015 01:01 WG830452 Iodomethane ND 0.0100 1 11/21/2015 01:01 WG830452 2-Butanone (MEK)ND 0.0100 1 11/21/2015 01:01 WG830452 Methylene Chloride ND 0.00500 1 11/21/2015 01:01 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 01:01 WG830452 Styrene ND 0.00100 1 11/21/2015 01:01 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 01:01 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 01:01 WG830452 Tetrachloroethene ND 0.00100 1 11/21/2015 01:01 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 32 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 32 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12 L801958 MW-16 15FT Collected date/time: 11/17/15 14:15 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 01:01 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 01:01 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 01:01 WG830452 Trichloroethene ND 0.00100 1 11/21/2015 01:01 WG830452 Trichlorofluoromethane ND 0.00500 1 11/21/2015 01:01 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 01:01 WG830452 Vinyl acetate ND 0.0100 1 11/21/2015 01:01 WG830452 Vinyl chloride ND 0.00100 1 11/21/2015 01:01 WG830452 Xylenes, Total ND 0.00300 1 11/21/2015 01:01 WG830452 (S) Toluene-d8 97.6 90.0-115 11/21/2015 01:01 WG830452 (S) Dibromofluoromethane 102 79.0-121 11/21/2015 01:01 WG830452 (S) a,a,a-Trifluorotoluene 106 90.4-116 11/21/2015 01:01 WG830452 (S) 4-Bromofluorobenzene 105 80.1-120 11/21/2015 01:01 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 33 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 33 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13 L801958 MW-17R 15FT Collected date/time: 11/17/15 14:45 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:30 WG830588 Arsenic 0.00367 0.00200 1 11/27/2015 20:30 WG830588 Barium 0.145 0.00500 1 11/27/2015 20:30 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:30 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:30 WG830588 Chromium 0.0162 0.00200 1 11/27/2015 20:30 WG830588 Copper 0.0103 0.00500 1 11/27/2015 20:30 WG830588 Cobalt 0.00736 0.00200 1 11/27/2015 20:30 WG830588 Lead 0.0167 0.00200 1 11/27/2015 20:30 WG830588 Nickel 0.00581 0.00200 1 11/27/2015 20:30 WG830588 Selenium ND 0.00200 1 11/27/2015 20:30 WG830588 Silver ND 0.00200 1 11/27/2015 20:30 WG830588 Thallium ND 0.00200 1 11/27/2015 20:30 WG830588 Vanadium 0.0396 0.00500 1 11/27/2015 20:30 WG830588 Zinc ND 0.0250 1 11/27/2015 20:30 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 01:19 WG830452 Acrylonitrile ND 0.0100 1 11/21/2015 01:19 WG830452 Benzene ND 0.00100 1 11/21/2015 01:19 WG830452 Bromochloromethane ND 0.00100 1 11/21/2015 01:19 WG830452 Bromodichloromethane ND 0.00100 1 11/21/2015 01:19 WG830452 Bromoform ND 0.00100 1 11/21/2015 01:19 WG830452 Bromomethane ND 0.00500 1 11/21/2015 01:19 WG830452 Carbon disulfide ND 0.00100 1 11/21/2015 01:19 WG830452 Carbon tetrachloride ND 0.00100 1 11/21/2015 01:19 WG830452 Chlorobenzene ND 0.00100 1 11/21/2015 01:19 WG830452 Chlorodibromomethane ND 0.00100 1 11/21/2015 01:19 WG830452 Chloroethane ND 0.00500 1 11/21/2015 01:19 WG830452 Chloroform ND 0.00500 1 11/21/2015 01:19 WG830452 Chloromethane ND 0.00250 1 11/21/2015 01:19 WG830452 Dibromomethane ND 0.00100 1 11/21/2015 01:19 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 01:19 WG830452 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 01:19 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 01:19 WG830452 1,1-Dichloroethane ND 0.00100 1 11/21/2015 01:19 WG830452 1,2-Dichloroethane ND 0.00100 1 11/21/2015 01:19 WG830452 1,1-Dichloroethene ND 0.00100 1 11/21/2015 01:19 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 01:19 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 01:19 WG830452 1,2-Dichloropropane ND 0.00100 1 11/21/2015 01:19 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 01:19 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 01:19 WG830452 Ethylbenzene ND 0.00100 1 11/21/2015 01:19 WG830452 2-Hexanone ND 0.0100 1 11/21/2015 01:19 WG830452 Iodomethane ND 0.0100 1 11/21/2015 01:19 WG830452 2-Butanone (MEK)ND 0.0100 1 11/21/2015 01:19 WG830452 Methylene Chloride ND 0.00500 1 11/21/2015 01:19 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 01:19 WG830452 Styrene ND 0.00100 1 11/21/2015 01:19 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 01:19 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 01:19 WG830452 Tetrachloroethene ND 0.00100 1 11/21/2015 01:19 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 34 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 34 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13 L801958 MW-17R 15FT Collected date/time: 11/17/15 14:45 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 01:19 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 01:19 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 01:19 WG830452 Trichloroethene ND 0.00100 1 11/21/2015 01:19 WG830452 Trichlorofluoromethane ND 0.00500 1 11/21/2015 01:19 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 01:19 WG830452 Vinyl acetate ND 0.0100 1 11/21/2015 01:19 WG830452 Vinyl chloride ND 0.00100 1 11/21/2015 01:19 WG830452 Xylenes, Total ND 0.00300 1 11/21/2015 01:19 WG830452 (S) Toluene-d8 103 90.0-115 11/21/2015 01:19 WG830452 (S) Dibromofluoromethane 99.7 79.0-121 11/21/2015 01:19 WG830452 (S) a,a,a-Trifluorotoluene 106 90.4-116 11/21/2015 01:19 WG830452 (S) 4-Bromofluorobenzene 103 80.1-120 11/21/2015 01:19 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 35 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 35 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14 L801958 MW-18 15FT Collected date/time: 11/17/15 14:30 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:32 WG830588 Arsenic ND 0.00200 1 11/27/2015 20:32 WG830588 Barium 0.121 0.00500 1 11/27/2015 20:32 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:32 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:32 WG830588 Chromium 0.00648 0.00200 1 11/27/2015 20:32 WG830588 Copper ND 0.00500 1 11/27/2015 20:32 WG830588 Cobalt 0.00236 0.00200 1 11/27/2015 20:32 WG830588 Lead 0.00724 0.00200 1 11/27/2015 20:32 WG830588 Nickel 0.00311 0.00200 1 11/27/2015 20:32 WG830588 Selenium ND 0.00200 1 11/27/2015 20:32 WG830588 Silver ND 0.00200 1 11/27/2015 20:32 WG830588 Thallium ND 0.00200 1 11/27/2015 20:32 WG830588 Vanadium 0.0138 0.00500 1 11/27/2015 20:32 WG830588 Zinc ND 0.0250 1 11/27/2015 20:32 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 01:38 WG830452 Acrylonitrile ND 0.0100 1 11/21/2015 01:38 WG830452 Benzene ND 0.00100 1 11/21/2015 01:38 WG830452 Bromochloromethane ND 0.00100 1 11/21/2015 01:38 WG830452 Bromodichloromethane ND 0.00100 1 11/21/2015 01:38 WG830452 Bromoform ND 0.00100 1 11/21/2015 01:38 WG830452 Bromomethane ND 0.00500 1 11/21/2015 01:38 WG830452 Carbon disulfide ND 0.00100 1 11/21/2015 01:38 WG830452 Carbon tetrachloride ND 0.00100 1 11/21/2015 01:38 WG830452 Chlorobenzene ND 0.00100 1 11/21/2015 01:38 WG830452 Chlorodibromomethane ND 0.00100 1 11/21/2015 01:38 WG830452 Chloroethane ND 0.00500 1 11/21/2015 01:38 WG830452 Chloroform ND 0.00500 1 11/21/2015 01:38 WG830452 Chloromethane ND 0.00250 1 11/21/2015 01:38 WG830452 Dibromomethane ND 0.00100 1 11/21/2015 01:38 WG830452 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 01:38 WG830452 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 01:38 WG830452 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 01:38 WG830452 1,1-Dichloroethane ND 0.00100 1 11/21/2015 01:38 WG830452 1,2-Dichloroethane ND 0.00100 1 11/21/2015 01:38 WG830452 1,1-Dichloroethene ND 0.00100 1 11/21/2015 01:38 WG830452 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 01:38 WG830452 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 01:38 WG830452 1,2-Dichloropropane ND 0.00100 1 11/21/2015 01:38 WG830452 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 01:38 WG830452 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 01:38 WG830452 Ethylbenzene ND 0.00100 1 11/21/2015 01:38 WG830452 2-Hexanone ND 0.0100 1 11/21/2015 01:38 WG830452 Iodomethane ND 0.0100 1 11/21/2015 01:38 WG830452 2-Butanone (MEK)ND 0.0100 1 11/21/2015 01:38 WG830452 Methylene Chloride ND 0.00500 1 11/21/2015 01:38 WG830452 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 01:38 WG830452 Styrene ND 0.00100 1 11/21/2015 01:38 WG830452 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 01:38 WG830452 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 01:38 WG830452 Tetrachloroethene ND 0.00100 1 11/21/2015 01:38 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 36 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 36 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14 L801958 MW-18 15FT Collected date/time: 11/17/15 14:30 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 01:38 WG830452 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 01:38 WG830452 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 01:38 WG830452 Trichloroethene ND 0.00100 1 11/21/2015 01:38 WG830452 Trichlorofluoromethane ND 0.00500 1 11/21/2015 01:38 WG830452 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 01:38 WG830452 Vinyl acetate ND 0.0100 1 11/21/2015 01:38 WG830452 Vinyl chloride ND 0.00100 1 11/21/2015 01:38 WG830452 Xylenes, Total ND 0.00300 1 11/21/2015 01:38 WG830452 (S) Toluene-d8 102 90.0-115 11/21/2015 01:38 WG830452 (S) Dibromofluoromethane 101 79.0-121 11/21/2015 01:38 WG830452 (S) a,a,a-Trifluorotoluene 108 90.4-116 11/21/2015 01:38 WG830452 (S) 4-Bromofluorobenzene 107 80.1-120 11/21/2015 01:38 WG830452 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 37 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 37 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15 L801958 MW-19 15FT Collected date/time: 11/18/15 16:55 Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Dissolved Solids 164 10.0 1 11/23/2015 18:04 WG830703 Wet Chemistry by Method 2320 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Alkalinity ND 20.0 1 11/24/2015 17:02 WG830995 Wet Chemistry by Method 9056MOD Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Chloride 1.72 1.00 1 11/21/2015 17:08 WG830629 Sulfate 5.45 5.00 1 11/21/2015 17:08 WG830629 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:34 WG830588 Arsenic 0.00620 0.00200 1 11/27/2015 20:34 WG830588 Barium 0.138 0.00500 1 11/27/2015 20:34 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:34 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:34 WG830588 Chromium 0.0195 0.00200 1 11/27/2015 20:34 WG830588 Copper 0.0102 0.00500 1 11/27/2015 20:34 WG830588 Cobalt 0.00298 0.00200 1 11/27/2015 20:34 WG830588 Lead 0.0310 0.00200 1 11/27/2015 20:34 WG830588 Nickel 0.00915 0.00200 1 11/27/2015 20:34 WG830588 Selenium ND 0.00200 1 11/27/2015 20:34 WG830588 Silver ND 0.00200 1 11/27/2015 20:34 WG830588 Thallium ND 0.00200 1 11/27/2015 20:34 WG830588 Vanadium 0.0345 0.00500 1 11/27/2015 20:34 WG830588 Zinc 0.0388 0.0250 1 11/27/2015 20:34 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND J3 0.0500 1 11/21/2015 07:15 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 07:15 WG830461 Benzene ND 0.00100 1 11/21/2015 07:15 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 07:15 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 07:15 WG830461 Bromoform ND 0.00100 1 11/21/2015 07:15 WG830461 Bromomethane ND 0.00500 1 11/21/2015 07:15 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 07:15 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 07:15 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 07:15 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 07:15 WG830461 Chloroethane ND 0.00500 1 11/21/2015 07:15 WG830461 Chloroform ND 0.00500 1 11/21/2015 07:15 WG830461 Chloromethane ND 0.00250 1 11/21/2015 07:15 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 07:15 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 07:15 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 07:15 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 07:15 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 07:15 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 38 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 38 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15 L801958 MW-19 15FT Collected date/time: 11/18/15 16:55 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time 1,2-Dichloroethane ND 0.00100 1 11/21/2015 07:15 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 07:15 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 07:15 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 07:15 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 07:15 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 07:15 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 07:15 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 07:15 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 07:15 WG830461 Iodomethane ND 0.0100 1 11/21/2015 07:15 WG830461 2-Butanone (MEK)ND J6 0.0100 1 11/21/2015 07:15 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 07:15 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 07:15 WG830461 Styrene ND 0.00100 1 11/21/2015 07:15 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 07:15 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 07:15 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 07:15 WG830461 Toluene ND 0.00500 1 11/21/2015 07:15 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 07:15 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 07:15 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 07:15 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 07:15 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 07:15 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 07:15 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 07:15 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 07:15 WG830461 (S) Toluene-d8 99.9 90.0-115 11/21/2015 07:15 WG830461 (S) Dibromofluoromethane 97.3 79.0-121 11/21/2015 07:15 WG830461 (S) a,a,a-Trifluorotoluene 112 90.4-116 11/21/2015 07:15 WG830461 (S) 4-Bromofluorobenzene 102 80.1-120 11/21/2015 07:15 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 39 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 39 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16 L801958 MW-20 15FT Collected date/time: 11/18/15 16:45 Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Dissolved Solids 58.0 10.0 1 11/23/2015 18:04 WG830703 Wet Chemistry by Method 2320 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Alkalinity ND 20.0 1 11/24/2015 17:02 WG830995 Wet Chemistry by Method 9056MOD Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Chloride 8.34 1.00 1 11/21/2015 17:24 WG830629 Sulfate ND 5.00 1 11/21/2015 17:24 WG830629 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:36 WG830588 Arsenic ND 0.00200 1 11/27/2015 20:36 WG830588 Barium 0.0231 0.00500 1 11/27/2015 20:36 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:36 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:36 WG830588 Chromium 0.00357 0.00200 1 11/27/2015 20:36 WG830588 Copper ND 0.00500 1 11/27/2015 20:36 WG830588 Cobalt ND 0.00200 1 11/27/2015 20:36 WG830588 Lead 0.00238 0.00200 1 11/27/2015 20:36 WG830588 Nickel ND 0.00200 1 11/27/2015 20:36 WG830588 Selenium ND 0.00200 1 11/27/2015 20:36 WG830588 Silver ND 0.00200 1 11/27/2015 20:36 WG830588 Thallium ND 0.00200 1 11/27/2015 20:36 WG830588 Vanadium ND 0.00500 1 11/27/2015 20:36 WG830588 Zinc ND 0.0250 1 11/27/2015 20:36 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 07:33 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 07:33 WG830461 Benzene ND 0.00100 1 11/21/2015 07:33 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 07:33 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 07:33 WG830461 Bromoform ND 0.00100 1 11/21/2015 07:33 WG830461 Bromomethane ND 0.00500 1 11/21/2015 07:33 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 07:33 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 07:33 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 07:33 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 07:33 WG830461 Chloroethane ND 0.00500 1 11/21/2015 07:33 WG830461 Chloroform ND 0.00500 1 11/21/2015 07:33 WG830461 Chloromethane ND 0.00250 1 11/21/2015 07:33 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 07:33 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 07:33 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 07:33 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 07:33 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 07:33 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 40 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 40 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16 L801958 MW-20 15FT Collected date/time: 11/18/15 16:45 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time 1,2-Dichloroethane ND 0.00100 1 11/21/2015 07:33 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 07:33 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 07:33 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 07:33 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 07:33 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 07:33 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 07:33 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 07:33 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 07:33 WG830461 Iodomethane ND 0.0100 1 11/21/2015 07:33 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 07:33 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 07:33 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 07:33 WG830461 Styrene ND 0.00100 1 11/21/2015 07:33 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 07:33 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 07:33 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 07:33 WG830461 Toluene ND 0.00500 1 11/21/2015 07:33 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 07:33 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 07:33 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 07:33 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 07:33 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 07:33 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 07:33 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 07:33 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 07:33 WG830461 (S) Toluene-d8 100 90.0-115 11/21/2015 07:33 WG830461 (S) Dibromofluoromethane 99.6 79.0-121 11/21/2015 07:33 WG830461 (S) a,a,a-Trifluorotoluene 109 90.4-116 11/21/2015 07:33 WG830461 (S) 4-Bromofluorobenzene 104 80.1-120 11/21/2015 07:33 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 41 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 41 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17 L801958 MW-21R 15FT Collected date/time: 11/17/15 11:10 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:39 WG830588 Arsenic 0.00528 0.00200 1 11/27/2015 20:39 WG830588 Barium 0.0302 0.00500 1 11/27/2015 20:39 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:39 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:39 WG830588 Chromium 0.00357 0.00200 1 11/27/2015 20:39 WG830588 Copper 0.00588 0.00500 1 11/27/2015 20:39 WG830588 Cobalt 0.0178 0.00200 1 11/27/2015 20:39 WG830588 Lead 0.00314 0.00200 1 11/27/2015 20:39 WG830588 Nickel ND 0.00200 1 11/27/2015 20:39 WG830588 Selenium ND 0.00200 1 11/27/2015 20:39 WG830588 Silver ND 0.00200 1 11/27/2015 20:39 WG830588 Thallium ND 0.00200 1 11/27/2015 20:39 WG830588 Vanadium ND 0.00500 1 11/27/2015 20:39 WG830588 Zinc ND 0.0250 1 11/27/2015 20:39 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone 0.0586 0.0500 1 11/21/2015 07:51 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 07:51 WG830461 Benzene ND 0.00100 1 11/21/2015 07:51 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 07:51 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 07:51 WG830461 Bromoform ND 0.00100 1 11/21/2015 07:51 WG830461 Bromomethane ND 0.00500 1 11/21/2015 07:51 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 07:51 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 07:51 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 07:51 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 07:51 WG830461 Chloroethane ND 0.00500 1 11/21/2015 07:51 WG830461 Chloroform ND 0.00500 1 11/21/2015 07:51 WG830461 Chloromethane ND 0.00250 1 11/21/2015 07:51 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 07:51 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 07:51 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 07:51 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 07:51 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 07:51 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 07:51 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 07:51 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 07:51 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 07:51 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 07:51 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 07:51 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 07:51 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 07:51 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 07:51 WG830461 Iodomethane ND 0.0100 1 11/21/2015 07:51 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 07:51 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 07:51 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 07:51 WG830461 Styrene ND 0.00100 1 11/21/2015 07:51 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 07:51 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 07:51 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 07:51 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 42 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 42 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17 L801958 MW-21R 15FT Collected date/time: 11/17/15 11:10 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 07:51 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 07:51 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 07:51 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 07:51 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 07:51 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 07:51 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 07:51 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 07:51 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 07:51 WG830461 (S) Toluene-d8 101 90.0-115 11/21/2015 07:51 WG830461 (S) Dibromofluoromethane 103 79.0-121 11/21/2015 07:51 WG830461 (S) a,a,a-Trifluorotoluene 108 90.4-116 11/21/2015 07:51 WG830461 (S) 4-Bromofluorobenzene 103 80.1-120 11/21/2015 07:51 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 43 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 43 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18 L801958 MW-22 15FT Collected date/time: 11/17/15 11:30 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:41 WG830588 Arsenic ND 0.00200 1 11/27/2015 20:41 WG830588 Barium 0.0258 0.00500 1 11/27/2015 20:41 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:41 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:41 WG830588 Chromium ND 0.00200 1 11/27/2015 20:41 WG830588 Copper ND 0.00500 1 11/27/2015 20:41 WG830588 Cobalt ND 0.00200 1 11/27/2015 20:41 WG830588 Lead ND 0.00200 1 11/27/2015 20:41 WG830588 Nickel ND 0.00200 1 11/27/2015 20:41 WG830588 Selenium ND 0.00200 1 11/27/2015 20:41 WG830588 Silver ND 0.00200 1 11/27/2015 20:41 WG830588 Thallium ND 0.00200 1 11/27/2015 20:41 WG830588 Vanadium ND 0.00500 1 11/27/2015 20:41 WG830588 Zinc ND 0.0250 1 11/27/2015 20:41 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 08:09 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 08:09 WG830461 Benzene ND 0.00100 1 11/21/2015 08:09 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 08:09 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 08:09 WG830461 Bromoform ND 0.00100 1 11/21/2015 08:09 WG830461 Bromomethane ND 0.00500 1 11/21/2015 08:09 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 08:09 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 08:09 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 08:09 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 08:09 WG830461 Chloroethane ND 0.00500 1 11/21/2015 08:09 WG830461 Chloroform ND 0.00500 1 11/21/2015 08:09 WG830461 Chloromethane ND 0.00250 1 11/21/2015 08:09 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 08:09 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 08:09 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 08:09 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 08:09 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 08:09 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 08:09 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 08:09 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 08:09 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 08:09 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 08:09 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 08:09 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 08:09 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 08:09 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 08:09 WG830461 Iodomethane ND 0.0100 1 11/21/2015 08:09 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 08:09 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 08:09 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 08:09 WG830461 Styrene ND 0.00100 1 11/21/2015 08:09 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 08:09 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 08:09 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 08:09 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 44 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 44 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18 L801958 MW-22 15FT Collected date/time: 11/17/15 11:30 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 08:09 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 08:09 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 08:09 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 08:09 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 08:09 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 08:09 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 08:09 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 08:09 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 08:09 WG830461 (S) Toluene-d8 95.1 90.0-115 11/21/2015 08:09 WG830461 (S) Dibromofluoromethane 102 79.0-121 11/21/2015 08:09 WG830461 (S) a,a,a-Trifluorotoluene 104 90.4-116 11/21/2015 08:09 WG830461 (S) 4-Bromofluorobenzene 99.2 80.1-120 11/21/2015 08:09 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 45 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 45 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19 L801958 MW-23 15FT Collected date/time: 11/17/15 10:50 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:43 WG830588 Arsenic ND 0.00200 1 11/27/2015 20:43 WG830588 Barium 0.00623 0.00500 1 11/27/2015 20:43 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:43 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:43 WG830588 Chromium ND 0.00200 1 11/27/2015 20:43 WG830588 Copper ND 0.00500 1 11/27/2015 20:43 WG830588 Cobalt ND 0.00200 1 11/27/2015 20:43 WG830588 Lead ND 0.00200 1 11/27/2015 20:43 WG830588 Nickel ND 0.00200 1 11/27/2015 20:43 WG830588 Selenium ND 0.00200 1 11/27/2015 20:43 WG830588 Silver ND 0.00200 1 11/27/2015 20:43 WG830588 Thallium ND 0.00200 1 11/27/2015 20:43 WG830588 Vanadium ND 0.00500 1 11/27/2015 20:43 WG830588 Zinc ND 0.0250 1 11/27/2015 20:43 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 08:27 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 08:27 WG830461 Benzene ND 0.00100 1 11/21/2015 08:27 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 08:27 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 08:27 WG830461 Bromoform ND 0.00100 1 11/21/2015 08:27 WG830461 Bromomethane ND 0.00500 1 11/21/2015 08:27 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 08:27 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 08:27 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 08:27 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 08:27 WG830461 Chloroethane ND 0.00500 1 11/21/2015 08:27 WG830461 Chloroform ND 0.00500 1 11/21/2015 08:27 WG830461 Chloromethane ND 0.00250 1 11/21/2015 08:27 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 08:27 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 08:27 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 08:27 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 08:27 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 08:27 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 08:27 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 08:27 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 08:27 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 08:27 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 08:27 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 08:27 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 08:27 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 08:27 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 08:27 WG830461 Iodomethane ND 0.0100 1 11/21/2015 08:27 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 08:27 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 08:27 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 08:27 WG830461 Styrene ND 0.00100 1 11/21/2015 08:27 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 08:27 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 08:27 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 08:27 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 46 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 46 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19 L801958 MW-23 15FT Collected date/time: 11/17/15 10:50 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 08:27 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 08:27 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 08:27 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 08:27 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 08:27 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 08:27 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 08:27 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 08:27 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 08:27 WG830461 (S) Toluene-d8 101 90.0-115 11/21/2015 08:27 WG830461 (S) Dibromofluoromethane 97.7 79.0-121 11/21/2015 08:27 WG830461 (S) a,a,a-Trifluorotoluene 110 90.4-116 11/21/2015 08:27 WG830461 (S) 4-Bromofluorobenzene 105 80.1-120 11/21/2015 08:27 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 47 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 47 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20 L801958 MW-24R 15FT Collected date/time: 11/17/15 10:25 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/27/2015 20:46 WG830588 Arsenic ND 0.00200 1 11/27/2015 20:46 WG830588 Barium 0.0374 0.00500 1 11/27/2015 20:46 WG830588 Beryllium ND 0.00200 1 11/27/2015 20:46 WG830588 Cadmium ND 0.00100 1 11/27/2015 20:46 WG830588 Chromium 0.00845 0.00200 1 11/27/2015 20:46 WG830588 Copper ND 0.00500 1 11/27/2015 20:46 WG830588 Cobalt ND 0.00200 1 11/27/2015 20:46 WG830588 Lead 0.00881 0.00200 1 11/27/2015 20:46 WG830588 Nickel 0.00293 0.00200 1 11/27/2015 20:46 WG830588 Selenium ND 0.00200 1 11/27/2015 20:46 WG830588 Silver ND 0.00200 1 11/27/2015 20:46 WG830588 Thallium ND 0.00200 1 11/27/2015 20:46 WG830588 Vanadium 0.0142 0.00500 1 11/27/2015 20:46 WG830588 Zinc ND 0.0250 1 11/27/2015 20:46 WG830588 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 08:45 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 08:45 WG830461 Benzene ND 0.00100 1 11/21/2015 08:45 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 08:45 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 08:45 WG830461 Bromoform ND 0.00100 1 11/21/2015 08:45 WG830461 Bromomethane ND 0.00500 1 11/21/2015 08:45 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 08:45 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 08:45 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 08:45 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 08:45 WG830461 Chloroethane ND 0.00500 1 11/21/2015 08:45 WG830461 Chloroform ND 0.00500 1 11/21/2015 08:45 WG830461 Chloromethane ND 0.00250 1 11/21/2015 08:45 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 08:45 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 08:45 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 08:45 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 08:45 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 08:45 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 08:45 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 08:45 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 08:45 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 08:45 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 08:45 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 08:45 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 08:45 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 08:45 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 08:45 WG830461 Iodomethane ND 0.0100 1 11/21/2015 08:45 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 08:45 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 08:45 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 08:45 WG830461 Styrene ND 0.00100 1 11/21/2015 08:45 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 08:45 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 08:45 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 08:45 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 48 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 48 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20 L801958 MW-24R 15FT Collected date/time: 11/17/15 10:25 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Toluene ND 0.00500 1 11/21/2015 08:45 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 08:45 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 08:45 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 08:45 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 08:45 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 08:45 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 08:45 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 08:45 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 08:45 WG830461 (S) Toluene-d8 105 90.0-115 11/21/2015 08:45 WG830461 (S) Dibromofluoromethane 97.2 79.0-121 11/21/2015 08:45 WG830461 (S) a,a,a-Trifluorotoluene 112 90.4-116 11/21/2015 08:45 WG830461 (S) 4-Bromofluorobenzene 111 80.1-120 11/21/2015 08:45 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 49 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 49 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21 L801958 MW-25R 15FT Collected date/time: 11/17/15 08:30 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/23/2015 12:50 WG830587 Arsenic 0.00469 0.00200 1 11/23/2015 12:50 WG830587 Beryllium ND 0.00200 1 11/23/2015 12:50 WG830587 Cadmium ND 0.00100 1 11/23/2015 12:50 WG830587 Copper 0.00857 0.00500 1 11/23/2015 12:50 WG830587 Lead 0.00392 0.00200 1 11/23/2015 12:50 WG830587 Selenium ND 0.00200 1 11/23/2015 12:50 WG830587 Thallium ND 0.00200 1 11/23/2015 12:50 WG830587 Zinc ND J3 J5 0.0250 1 11/23/2015 12:50 WG830587 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 09:03 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 09:03 WG830461 Benzene ND 0.00100 1 11/21/2015 09:03 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 09:03 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 09:03 WG830461 Bromoform ND 0.00100 1 11/21/2015 09:03 WG830461 Bromomethane ND 0.00500 1 11/21/2015 09:03 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 09:03 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 09:03 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 09:03 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 09:03 WG830461 Chloroethane ND 0.00500 1 11/21/2015 09:03 WG830461 Chloroform ND 0.00500 1 11/21/2015 09:03 WG830461 Chloromethane ND 0.00250 1 11/21/2015 09:03 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 09:03 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 09:03 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 09:03 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 09:03 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 09:03 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 09:03 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 09:03 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 09:03 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 09:03 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 09:03 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 09:03 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 09:03 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 09:03 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 09:03 WG830461 Iodomethane ND 0.0100 1 11/21/2015 09:03 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 09:03 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 09:03 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 09:03 WG830461 Styrene ND 0.00100 1 11/21/2015 09:03 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 09:03 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 09:03 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 09:03 WG830461 Toluene ND 0.00500 1 11/21/2015 09:03 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 09:03 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 09:03 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 09:03 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 09:03 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 09:03 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 50 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 50 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21 L801958 MW-25R 15FT Collected date/time: 11/17/15 08:30 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Vinyl acetate ND 0.0100 1 11/21/2015 09:03 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 09:03 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 09:03 WG830461 (S) Toluene-d8 100 90.0-115 11/21/2015 09:03 WG830461 (S) Dibromofluoromethane 96.5 79.0-121 11/21/2015 09:03 WG830461 (S) a,a,a-Trifluorotoluene 108 90.4-116 11/21/2015 09:03 WG830461 (S) 4-Bromofluorobenzene 106 80.1-120 11/21/2015 09:03 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 51 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 51 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22 L801958 MW-26 15FT Collected date/time: 11/17/15 09:55 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/23/2015 12:59 WG830587 Arsenic ND 0.00200 1 11/23/2015 12:59 WG830587 Beryllium ND 0.00200 1 11/23/2015 12:59 WG830587 Cadmium ND 0.00100 1 11/23/2015 12:59 WG830587 Copper 0.00764 0.00500 1 11/23/2015 12:59 WG830587 Lead 0.00896 0.00200 1 11/23/2015 12:59 WG830587 Selenium ND 0.00200 1 11/23/2015 12:59 WG830587 Thallium ND 0.00200 1 11/23/2015 12:59 WG830587 Zinc ND 0.0250 1 11/23/2015 12:59 WG830587 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 09:21 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 09:21 WG830461 Benzene ND 0.00100 1 11/21/2015 09:21 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 09:21 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 09:21 WG830461 Bromoform ND 0.00100 1 11/21/2015 09:21 WG830461 Bromomethane ND 0.00500 1 11/21/2015 09:21 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 09:21 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 09:21 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 09:21 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 09:21 WG830461 Chloroethane ND 0.00500 1 11/21/2015 09:21 WG830461 Chloroform ND 0.00500 1 11/21/2015 09:21 WG830461 Chloromethane ND 0.00250 1 11/21/2015 09:21 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 09:21 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 09:21 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 09:21 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 09:21 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 09:21 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 09:21 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 09:21 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 09:21 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 09:21 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 09:21 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 09:21 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 09:21 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 09:21 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 09:21 WG830461 Iodomethane ND 0.0100 1 11/21/2015 09:21 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 09:21 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 09:21 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 09:21 WG830461 Styrene ND 0.00100 1 11/21/2015 09:21 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 09:21 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 09:21 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 09:21 WG830461 Toluene ND 0.00500 1 11/21/2015 09:21 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 09:21 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 09:21 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 09:21 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 09:21 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 09:21 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 52 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 52 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22 L801958 MW-26 15FT Collected date/time: 11/17/15 09:55 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Vinyl acetate ND 0.0100 1 11/21/2015 09:21 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 09:21 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 09:21 WG830461 (S) Toluene-d8 103 90.0-115 11/21/2015 09:21 WG830461 (S) Dibromofluoromethane 97.1 79.0-121 11/21/2015 09:21 WG830461 (S) a,a,a-Trifluorotoluene 110 90.4-116 11/21/2015 09:21 WG830461 (S) 4-Bromofluorobenzene 110 80.1-120 11/21/2015 09:21 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 53 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 53 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23 L801958 SW-1 Collected date/time: 11/17/15 07:45 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony 0.00384 0.00200 1 11/23/2015 13:02 WG830587 Arsenic 0.00814 0.00200 1 11/23/2015 13:02 WG830587 Beryllium ND 0.00200 1 11/23/2015 13:02 WG830587 Cadmium ND 0.00100 1 11/23/2015 13:02 WG830587 Copper ND 0.00500 1 11/23/2015 13:02 WG830587 Lead ND 0.00200 1 11/23/2015 13:02 WG830587 Selenium ND 0.00200 1 11/23/2015 13:02 WG830587 Thallium ND 0.00200 1 11/23/2015 13:02 WG830587 Zinc 0.0631 0.0250 1 11/23/2015 13:02 WG830587 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone 0.118 0.0500 1 11/21/2015 09:39 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 09:39 WG830461 Benzene ND 0.00100 1 11/21/2015 09:39 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 09:39 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 09:39 WG830461 Bromoform ND 0.00100 1 11/21/2015 09:39 WG830461 Bromomethane ND 0.00500 1 11/21/2015 09:39 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 09:39 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 09:39 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 09:39 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 09:39 WG830461 Chloroethane ND 0.00500 1 11/21/2015 09:39 WG830461 Chloroform ND 0.00500 1 11/21/2015 09:39 WG830461 Chloromethane ND 0.00250 1 11/21/2015 09:39 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 09:39 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 09:39 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 09:39 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 09:39 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 09:39 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 09:39 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 09:39 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 09:39 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 09:39 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 09:39 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 09:39 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 09:39 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 09:39 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 09:39 WG830461 Iodomethane ND 0.0100 1 11/21/2015 09:39 WG830461 2-Butanone (MEK)0.307 0.0100 1 11/21/2015 09:39 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 09:39 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 09:39 WG830461 Styrene ND 0.00100 1 11/21/2015 09:39 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 09:39 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 09:39 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 09:39 WG830461 Toluene ND 0.00500 1 11/21/2015 09:39 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 09:39 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 09:39 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 09:39 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 09:39 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 09:39 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 54 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 54 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23 L801958 SW-1 Collected date/time: 11/17/15 07:45 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Vinyl acetate ND 0.0100 1 11/21/2015 09:39 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 09:39 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 09:39 WG830461 (S) Toluene-d8 110 90.0-115 11/21/2015 09:39 WG830461 (S) Dibromofluoromethane 98.1 79.0-121 11/21/2015 09:39 WG830461 (S) a,a,a-Trifluorotoluene 112 90.4-116 11/21/2015 09:39 WG830461 (S) 4-Bromofluorobenzene 107 80.1-120 11/21/2015 09:39 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 55 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 55 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 24 L801958 SW-2 Collected date/time: 11/17/15 08:05 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.00200 1 11/23/2015 13:04 WG830587 Arsenic 0.00264 0.00200 1 11/23/2015 13:04 WG830587 Beryllium ND 0.00200 1 11/23/2015 13:04 WG830587 Cadmium ND 0.00100 1 11/23/2015 13:04 WG830587 Copper ND 0.00500 1 11/23/2015 13:04 WG830587 Lead ND 0.00200 1 11/23/2015 13:04 WG830587 Selenium ND 0.00200 1 11/23/2015 13:04 WG830587 Thallium ND 0.00200 1 11/23/2015 13:04 WG830587 Zinc ND 0.0250 1 11/23/2015 13:04 WG830587 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 09:57 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 09:57 WG830461 Benzene ND 0.00100 1 11/21/2015 09:57 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 09:57 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 09:57 WG830461 Bromoform ND 0.00100 1 11/21/2015 09:57 WG830461 Bromomethane ND 0.00500 1 11/21/2015 09:57 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 09:57 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 09:57 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 09:57 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 09:57 WG830461 Chloroethane ND 0.00500 1 11/21/2015 09:57 WG830461 Chloroform ND 0.00500 1 11/21/2015 09:57 WG830461 Chloromethane ND 0.00250 1 11/21/2015 09:57 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 09:57 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 09:57 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 09:57 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 09:57 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 09:57 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 09:57 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 09:57 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 09:57 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 09:57 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 09:57 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 09:57 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 09:57 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 09:57 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 09:57 WG830461 Iodomethane ND 0.0100 1 11/21/2015 09:57 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 09:57 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 09:57 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 09:57 WG830461 Styrene ND 0.00100 1 11/21/2015 09:57 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 09:57 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 09:57 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 09:57 WG830461 Toluene ND 0.00500 1 11/21/2015 09:57 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 09:57 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 09:57 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 09:57 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 09:57 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 09:57 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 56 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 56 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 24 L801958 SW-2 Collected date/time: 11/17/15 08:05 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Vinyl acetate ND 0.0100 1 11/21/2015 09:57 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 09:57 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 09:57 WG830461 (S) Toluene-d8 101 90.0-115 11/21/2015 09:57 WG830461 (S) Dibromofluoromethane 98.7 79.0-121 11/21/2015 09:57 WG830461 (S) a,a,a-Trifluorotoluene 110 90.4-116 11/21/2015 09:57 WG830461 (S) 4-Bromofluorobenzene 106 80.1-120 11/21/2015 09:57 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 57 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 57 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 25 L801958 TRIP BLANK Collected date/time: 11/17/15 00:00 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 06:38 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 06:38 WG830461 Benzene ND 0.00100 1 11/21/2015 06:38 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 06:38 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 06:38 WG830461 Bromoform ND 0.00100 1 11/21/2015 06:38 WG830461 Bromomethane ND 0.00500 1 11/21/2015 06:38 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 06:38 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 06:38 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 06:38 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 06:38 WG830461 Chloroethane ND 0.00500 1 11/21/2015 06:38 WG830461 Chloroform ND 0.00500 1 11/21/2015 06:38 WG830461 Chloromethane ND 0.00250 1 11/21/2015 06:38 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 06:38 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 06:38 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 06:38 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 06:38 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 06:38 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 06:38 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 06:38 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 06:38 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 06:38 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 06:38 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 06:38 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 06:38 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 06:38 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 06:38 WG830461 Iodomethane ND 0.0100 1 11/21/2015 06:38 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 06:38 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 06:38 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 06:38 WG830461 Styrene ND 0.00100 1 11/21/2015 06:38 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 06:38 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 06:38 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 06:38 WG830461 Toluene ND 0.00500 1 11/21/2015 06:38 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 06:38 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 06:38 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 06:38 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 06:38 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 06:38 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 06:38 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 06:38 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 06:38 WG830461 (S) Toluene-d8 99.1 90.0-115 11/21/2015 06:38 WG830461 (S) Dibromofluoromethane 97.6 79.0-121 11/21/2015 06:38 WG830461 (S) a,a,a-Trifluorotoluene 107 90.4-116 11/21/2015 06:38 WG830461 (S) 4-Bromofluorobenzene 104 80.1-120 11/21/2015 06:38 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 58 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 58 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 26 L801958 TRIP BLANK Collected date/time: 11/17/15 00:00 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 0.0500 1 11/21/2015 06:56 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 06:56 WG830461 Benzene ND 0.00100 1 11/21/2015 06:56 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 06:56 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 06:56 WG830461 Bromoform ND 0.00100 1 11/21/2015 06:56 WG830461 Bromomethane ND 0.00500 1 11/21/2015 06:56 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 06:56 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 06:56 WG830461 Chlorobenzene ND 0.00100 1 11/21/2015 06:56 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 06:56 WG830461 Chloroethane ND 0.00500 1 11/21/2015 06:56 WG830461 Chloroform ND 0.00500 1 11/21/2015 06:56 WG830461 Chloromethane ND 0.00250 1 11/21/2015 06:56 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 06:56 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 06:56 WG830461 1,4-Dichlorobenzene ND 0.00100 1 11/21/2015 06:56 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 06:56 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 06:56 WG830461 1,2-Dichloroethane ND 0.00100 1 11/21/2015 06:56 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 06:56 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 06:56 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 06:56 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 06:56 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 06:56 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 06:56 WG830461 Ethylbenzene ND 0.00100 1 11/21/2015 06:56 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 06:56 WG830461 Iodomethane ND 0.0100 1 11/21/2015 06:56 WG830461 2-Butanone (MEK)ND 0.0100 1 11/21/2015 06:56 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 06:56 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 06:56 WG830461 Styrene ND 0.00100 1 11/21/2015 06:56 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 06:56 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 06:56 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 06:56 WG830461 Toluene ND 0.00500 1 11/21/2015 06:56 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 06:56 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 06:56 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 06:56 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 06:56 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 06:56 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 06:56 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 06:56 WG830461 Xylenes, Total ND 0.00300 1 11/21/2015 06:56 WG830461 (S) Toluene-d8 107 90.0-115 11/21/2015 06:56 WG830461 (S) Dibromofluoromethane 98.3 79.0-121 11/21/2015 06:56 WG830461 (S) a,a,a-Trifluorotoluene 113 90.4-116 11/21/2015 06:56 WG830461 (S) 4-Bromofluorobenzene 101 80.1-120 11/21/2015 06:56 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 59 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 59 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 27 L801958 LEACHATE PHASE 2 Collected date/time: 11/18/15 15:10 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Phosphorus,Total 3.08 0.100 1 11/27/2015 15:29 WG830333 Wet Chemistry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time COD 1300 100 10 11/23/2015 13:45 WG830753 Wet Chemistry by Method 5210 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time BOD 8.90 3.33 1 11/24/2015 10:53 WG830211 Wet Chemistry by Method 9056MOD Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Nitrate 1.33 0.100 1 11/20/2015 13:17 WG830498 Sulfate 736 500 100 11/24/2015 10:35 WG830779 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony 0.0708 0.0180 9 11/23/2015 13:28 WG830587 Arsenic 0.213 0.0180 9 11/23/2015 13:28 WG830587 Beryllium ND 0.0180 9 11/23/2015 13:28 WG830587 Cadmium ND 0.00900 9 11/23/2015 13:28 WG830587 Copper 0.311 0.0450 9 11/23/2015 13:28 WG830587 Lead 0.162 0.0180 9 11/23/2015 13:28 WG830587 Selenium ND 0.0180 9 11/23/2015 13:28 WG830587 Thallium ND 0.0180 9 11/23/2015 13:28 WG830587 Zinc ND 0.225 9 11/23/2015 13:28 WG830587 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone 0.110 0.0500 1 11/21/2015 10:15 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 10:15 WG830461 Benzene 0.00436 0.00100 1 11/21/2015 10:15 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 10:15 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 10:15 WG830461 Bromoform ND 0.00100 1 11/21/2015 10:15 WG830461 Bromomethane ND 0.00500 1 11/21/2015 10:15 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 10:15 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 10:15 WG830461 Chlorobenzene 0.00152 0.00100 1 11/21/2015 10:15 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 10:15 WG830461 Chloroethane ND 0.00500 1 11/21/2015 10:15 WG830461 Chloroform ND 0.00500 1 11/21/2015 10:15 WG830461 Chloromethane ND 0.00250 1 11/21/2015 10:15 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 10:15 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 10:15 WG830461 1,4-Dichlorobenzene 0.00585 0.00100 1 11/21/2015 10:15 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 10:15 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 10:15 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 60 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 60 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 27 L801958 LEACHATE PHASE 2 Collected date/time: 11/18/15 15:10 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time 1,2-Dichloroethane ND 0.00100 1 11/21/2015 10:15 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 10:15 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 10:15 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 10:15 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 10:15 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 10:15 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 10:15 WG830461 Ethylbenzene 0.00790 0.00100 1 11/21/2015 10:15 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 10:15 WG830461 Iodomethane ND 0.0100 1 11/21/2015 10:15 WG830461 2-Butanone (MEK)0.0828 0.0100 1 11/21/2015 10:15 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 10:15 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 10:15 WG830461 Styrene ND 0.00100 1 11/21/2015 10:15 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 10:15 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 10:15 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 10:15 WG830461 Toluene ND 0.00500 1 11/21/2015 10:15 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 10:15 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 10:15 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 10:15 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 10:15 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 10:15 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 10:15 WG830461 Vinyl chloride ND 0.00100 1 11/21/2015 10:15 WG830461 Xylenes, Total 0.0262 0.00300 1 11/21/2015 10:15 WG830461 (S) Toluene-d8 107 90.0-115 11/21/2015 10:15 WG830461 (S) Dibromofluoromethane 26.5 J2 79.0-121 11/21/2015 10:15 WG830461 (S) a,a,a-Trifluorotoluene 114 90.4-116 11/21/2015 10:15 WG830461 (S) 4-Bromofluorobenzene 106 80.1-120 11/21/2015 10:15 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 61 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 61 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 28 L801958 LEACHATE PHASE 3 Collected date/time: 11/18/15 15:15 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Phosphorus,Total 0.534 0.100 1 11/27/2015 15:30 WG830333 Wet Chemistry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time COD 427 100 10 11/23/2015 13:45 WG830753 Wet Chemistry by Method 5210 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time BOD 26.4 10.0 1 11/24/2015 10:56 WG830211 Wet Chemistry by Method 9056MOD Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Nitrate 0.415 0.100 1 11/20/2015 13:32 WG830498 Sulfate 50.9 5.00 1 11/20/2015 13:32 WG830498 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.0180 9 11/23/2015 13:31 WG830587 Arsenic 0.0269 0.0180 9 11/23/2015 13:31 WG830587 Beryllium ND 0.0180 9 11/23/2015 13:31 WG830587 Cadmium ND 0.00900 9 11/23/2015 13:31 WG830587 Copper 0.0547 0.0450 9 11/23/2015 13:31 WG830587 Lead ND 0.0180 9 11/23/2015 13:31 WG830587 Selenium ND 0.0180 9 11/23/2015 13:31 WG830587 Thallium ND 0.0180 9 11/23/2015 13:31 WG830587 Zinc ND 0.225 9 11/23/2015 13:31 WG830587 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone 0.0998 0.0500 1 11/21/2015 10:33 WG830461 Acrylonitrile ND J4 0.0100 1 11/21/2015 10:33 WG830461 Benzene 0.00589 0.00100 1 11/21/2015 10:33 WG830461 Bromochloromethane ND 0.00100 1 11/21/2015 10:33 WG830461 Bromodichloromethane ND 0.00100 1 11/21/2015 10:33 WG830461 Bromoform ND 0.00100 1 11/21/2015 10:33 WG830461 Bromomethane ND 0.00500 1 11/21/2015 10:33 WG830461 Carbon disulfide ND 0.00100 1 11/21/2015 10:33 WG830461 Carbon tetrachloride ND 0.00100 1 11/21/2015 10:33 WG830461 Chlorobenzene 0.00208 0.00100 1 11/21/2015 10:33 WG830461 Chlorodibromomethane ND 0.00100 1 11/21/2015 10:33 WG830461 Chloroethane ND 0.00500 1 11/21/2015 10:33 WG830461 Chloroform ND 0.00500 1 11/21/2015 10:33 WG830461 Chloromethane ND 0.00250 1 11/21/2015 10:33 WG830461 Dibromomethane ND 0.00100 1 11/21/2015 10:33 WG830461 1,2-Dichlorobenzene ND 0.00100 1 11/21/2015 10:33 WG830461 1,4-Dichlorobenzene 0.0121 0.00100 1 11/21/2015 10:33 WG830461 trans-1,4-Dichloro-2-butene ND 0.00250 1 11/21/2015 10:33 WG830461 1,1-Dichloroethane ND 0.00100 1 11/21/2015 10:33 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 62 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 62 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 28 L801958 LEACHATE PHASE 3 Collected date/time: 11/18/15 15:15 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time 1,2-Dichloroethane ND 0.00100 1 11/21/2015 10:33 WG830461 1,1-Dichloroethene ND 0.00100 1 11/21/2015 10:33 WG830461 cis-1,2-Dichloroethene ND 0.00100 1 11/21/2015 10:33 WG830461 trans-1,2-Dichloroethene ND 0.00100 1 11/21/2015 10:33 WG830461 1,2-Dichloropropane ND 0.00100 1 11/21/2015 10:33 WG830461 cis-1,3-Dichloropropene ND 0.00100 1 11/21/2015 10:33 WG830461 trans-1,3-Dichloropropene ND 0.00100 1 11/21/2015 10:33 WG830461 Ethylbenzene 0.0232 0.00100 1 11/21/2015 10:33 WG830461 2-Hexanone ND 0.0100 1 11/21/2015 10:33 WG830461 Iodomethane ND 0.0100 1 11/21/2015 10:33 WG830461 2-Butanone (MEK)0.124 0.0100 1 11/21/2015 10:33 WG830461 Methylene Chloride ND 0.00500 1 11/21/2015 10:33 WG830461 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 11/21/2015 10:33 WG830461 Styrene ND 0.00100 1 11/21/2015 10:33 WG830461 1,1,1,2-Tetrachloroethane ND 0.00100 1 11/21/2015 10:33 WG830461 1,1,2,2-Tetrachloroethane ND 0.00100 1 11/21/2015 10:33 WG830461 Tetrachloroethene ND 0.00100 1 11/21/2015 10:33 WG830461 Toluene 0.00723 0.00500 1 11/21/2015 10:33 WG830461 1,1,1-Trichloroethane ND 0.00100 1 11/21/2015 10:33 WG830461 1,1,2-Trichloroethane ND 0.00100 1 11/21/2015 10:33 WG830461 Trichloroethene ND 0.00100 1 11/21/2015 10:33 WG830461 Trichlorofluoromethane ND 0.00500 1 11/21/2015 10:33 WG830461 1,2,3-Trichloropropane ND 0.00250 1 11/21/2015 10:33 WG830461 Vinyl acetate ND 0.0100 1 11/21/2015 10:33 WG830461 Vinyl chloride 0.00120 0.00100 1 11/21/2015 10:33 WG830461 Xylenes, Total 0.0806 0.00300 1 11/21/2015 10:33 WG830461 (S) Toluene-d8 105 90.0-115 11/21/2015 10:33 WG830461 (S) Dibromofluoromethane 90.7 79.0-121 11/21/2015 10:33 WG830461 (S) a,a,a-Trifluorotoluene 113 90.4-116 11/21/2015 10:33 WG830461 (S) 4-Bromofluorobenzene 108 80.1-120 11/21/2015 10:33 WG830461 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 63 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 63 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 29 L801958 LEACHATE PHASE 4 Collected date/time: 11/18/15 15:50 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Phosphorus,Total 0.279 0.100 1 11/27/2015 15:31 WG830333 Wet Chemistry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time COD 3920 100 10 11/23/2015 13:45 WG830753 Wet Chemistry by Method 5210 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time BOD 2310 1000 10 11/24/2015 11:01 WG830211 Wet Chemistry by Method 9056MOD Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Nitrate ND 0.100 1 11/20/2015 13:48 WG830498 Sulfate 99.1 5.00 1 11/20/2015 13:48 WG830498 Metals (ICPMS) by Method 6020 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Antimony ND 0.0180 9 11/23/2015 13:33 WG830587 Arsenic 0.0704 0.0180 9 11/23/2015 13:33 WG830587 Beryllium ND 0.0180 9 11/23/2015 13:33 WG830587 Cadmium ND 0.00900 9 11/23/2015 13:33 WG830587 Copper ND 0.0450 9 11/23/2015 13:33 WG830587 Lead ND 0.0180 9 11/23/2015 13:33 WG830587 Selenium ND 0.0180 9 11/23/2015 13:33 WG830587 Thallium ND 0.0180 9 11/23/2015 13:33 WG830587 Zinc ND 0.225 9 11/23/2015 13:33 WG830587 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone 2.61 0.500 10 12/01/2015 10:02 WG832427 Acrylonitrile ND 0.100 10 12/01/2015 10:02 WG832427 Benzene ND 0.0100 10 12/01/2015 10:02 WG832427 Bromochloromethane ND 0.0100 10 12/01/2015 10:02 WG832427 Bromodichloromethane ND 0.0100 10 12/01/2015 10:02 WG832427 Bromoform ND 0.0100 10 12/01/2015 10:02 WG832427 Bromomethane ND 0.0500 10 12/01/2015 10:02 WG832427 Carbon disulfide ND 0.0100 10 12/01/2015 10:02 WG832427 Carbon tetrachloride ND 0.0100 10 12/01/2015 10:02 WG832427 Chlorobenzene ND 0.0100 10 12/01/2015 10:02 WG832427 Chlorodibromomethane ND 0.0100 10 12/01/2015 10:02 WG832427 Chloroethane ND 0.0500 10 12/01/2015 10:02 WG832427 Chloroform ND 0.0500 10 12/01/2015 10:02 WG832427 Chloromethane ND 0.0250 10 12/01/2015 10:02 WG832427 Dibromomethane ND 0.0100 10 12/01/2015 10:02 WG832427 1,2-Dichlorobenzene ND 0.0100 10 12/01/2015 10:02 WG832427 1,4-Dichlorobenzene ND 0.0100 10 12/01/2015 10:02 WG832427 trans-1,4-Dichloro-2-butene ND 0.0250 10 12/01/2015 10:02 WG832427 1,1-Dichloroethane ND 0.0100 10 12/01/2015 10:02 WG832427 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 64 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 64 of 101 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 29 L801958 LEACHATE PHASE 4 Collected date/time: 11/18/15 15:50 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time 1,2-Dichloroethane ND 0.0100 10 12/01/2015 10:02 WG832427 1,1-Dichloroethene ND 0.0100 10 12/01/2015 10:02 WG832427 cis-1,2-Dichloroethene ND 0.0100 10 12/01/2015 10:02 WG832427 trans-1,2-Dichloroethene ND 0.0100 10 12/01/2015 10:02 WG832427 1,2-Dichloropropane ND 0.0100 10 12/01/2015 10:02 WG832427 cis-1,3-Dichloropropene ND 0.0100 10 12/01/2015 10:02 WG832427 trans-1,3-Dichloropropene ND 0.0100 10 12/01/2015 10:02 WG832427 Ethylbenzene 0.0116 0.0100 10 12/01/2015 10:02 WG832427 2-Hexanone ND 0.100 10 12/01/2015 10:02 WG832427 Iodomethane ND 0.100 10 12/01/2015 10:02 WG832427 2-Butanone (MEK)3.05 0.100 10 12/01/2015 10:02 WG832427 Methylene Chloride ND 0.0500 10 12/01/2015 10:02 WG832427 4-Methyl-2-pentanone (MIBK)ND 0.100 10 12/01/2015 10:02 WG832427 Styrene ND 0.0100 10 12/01/2015 10:02 WG832427 1,1,1,2-Tetrachloroethane ND 0.0100 10 12/01/2015 10:02 WG832427 1,1,2,2-Tetrachloroethane ND 0.0100 10 12/01/2015 10:02 WG832427 Tetrachloroethene ND 0.0100 10 12/01/2015 10:02 WG832427 Toluene ND 0.0500 10 12/01/2015 10:02 WG832427 1,1,1-Trichloroethane ND 0.0100 10 12/01/2015 10:02 WG832427 1,1,2-Trichloroethane ND 0.0100 10 12/01/2015 10:02 WG832427 Trichloroethene ND 0.0100 10 12/01/2015 10:02 WG832427 Trichlorofluoromethane ND 0.0500 10 12/01/2015 10:02 WG832427 1,2,3-Trichloropropane ND 0.0250 10 12/01/2015 10:02 WG832427 Vinyl acetate ND 0.100 10 12/01/2015 10:02 WG832427 Vinyl chloride ND 0.0100 10 12/01/2015 10:02 WG832427 Xylenes, Total ND 0.0300 10 12/01/2015 10:02 WG832427 (S) Toluene-d8 102 90.0-115 12/01/2015 10:02 WG832427 (S) Dibromofluoromethane 102 79.0-121 12/01/2015 10:02 WG832427 (S) a,a,a-Trifluorotoluene 106 90.4-116 12/01/2015 10:02 WG832427 (S) 4-Bromofluorobenzene 105 80.1-120 12/01/2015 10:02 WG832427 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 65 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 65 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830703 Gravimetric Analysis by Method 2540 C-2011 L801958-15,16 Method Blank (MB) (MB) 11/23/15 18:04 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Dissolved Solids ND 10.0 L801846-01 Original Sample (OS) • Duplicate (DUP) (OS) 11/23/15 18:04 • (DUP) 11/23/15 18:04 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Dissolved Solids 71.0 71.0 1 0.000 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/23/15 18:04 • (LCSD) 11/23/15 18:04 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Dissolved Solids 8800 8690 8720 98.8 99.1 85.0-115 0.345 5 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 66 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 66 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830995 Wet Chemistry by Method 2320 B-2011 L801958-15,16 Method Blank (MB) (MB) 11/24/15 17:02 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Alkalinity ND 20.0 L802287-02 Original Sample (OS) • Duplicate (DUP) (OS) 11/24/15 17:02 • (DUP) 11/24/15 17:02 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Alkalinity 36.8 33.1 1 10.6 20 L802314-09 Original Sample (OS) • Duplicate (DUP) (OS) 11/24/15 17:02 • (DUP) 11/24/15 17:02 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Alkalinity 629 599 10 4.89 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/24/15 17:02 • (LCSD) 11/24/15 17:02 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Alkalinity 100 110 106 110 106 85.0-115 3.70 20 L802287-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/24/15 17:02 • (MS) 11/24/15 17:02 • (MSD) 11/24/15 17:02 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Alkalinity 100 147 238 240 91.0 93.0 1 80.0-120 0.837 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 67 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 67 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830333 Wet Chemistry by Method 365.4 L801958-27,28,29 Method Blank (MB) (MB) 11/27/15 15:00 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Phosphorus,Total ND 0.100 L801873-01 Original Sample (OS) • Duplicate (DUP) (OS) 11/27/15 15:07 • (DUP) 11/27/15 15:08 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Phosphorus,Total 0.102 ND 1 22.0 P1 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/27/15 15:03 • (LCSD) 11/27/15 15:04 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Phosphorus,Total 1.00 1.00 0.986 100 99.0 90.0-110 1.00 20 L801941-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/27/15 15:25 • (MS) 11/27/15 15:26 • (MSD) 11/27/15 15:27 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Phosphorus,Total 2.50 2.55 4.18 3.90 65.0 54.0 1 90.0-110 J6 J6 7.00 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 68 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 68 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830753 Wet Chemistry by Method 410.4 L801958-27,28,29 Method Blank (MB) (MB) 11/23/15 13:42 MB Result MB Qualifier MB RDL Analyte mg/l mg/l COD ND 10.0 L801976-01 Original Sample (OS) • Duplicate (DUP) (OS) 11/23/15 13:45 • (DUP) 11/23/15 13:46 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % COD 23.7 23.8 1 0.421 5 L801918-01 Original Sample (OS) • Duplicate (DUP) (OS) 11/23/15 13:43 • (DUP) 11/23/15 13:44 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % COD 56.9 56.5 1 0.705 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/23/15 13:43 • (LCSD) 11/23/15 13:43 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% COD 242 252 251 104 104 90.0-110 0.398 5 L801976-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/23/15 13:46 • (MS) 11/23/15 13:46 • (MSD) 11/23/15 13:46 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% COD 400 25.7 495 494 117 117 1 90.0-110 J5 J5 0.202 5 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 69 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 69 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830211 Wet Chemistry by Method 5210 B-2011 L801958-27,28,29 Method Blank (MB) (MB) 11/24/15 11:56 MB Result MB Qualifier MB RDL Analyte mg/l mg/l BOD ND 1.00 L801749-02 Original Sample (OS) • Duplicate (DUP) (OS) 11/24/15 09:28 • (DUP) 11/24/15 09:29 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % BOD ND 0.000 1 0 30 L801915-01 Original Sample (OS) • Duplicate (DUP) (OS) 11/24/15 09:51 • (DUP) 11/24/15 09:52 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % BOD 2.00 2.90 1 0 30 L801984-01 Original Sample (OS) • Duplicate (DUP) (OS) 11/24/15 11:08 • (DUP) 11/24/15 11:11 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % BOD 30.4 30.3 1 0 30 L801991-01 Original Sample (OS) • Duplicate (DUP) (OS) 11/24/15 11:19 • (DUP) 11/24/15 11:23 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % BOD 17.2 15.5 1 11 30 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 70 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 70 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830211 Wet Chemistry by Method 5210 B-2011 L801958-27,28,29 Laboratory Control Sample (LCS) (LCS) 11/24/15 08:55 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% BOD 198 198 100 84.6-115 Laboratory Control Sample (LCS) (LCS) 11/24/15 10:34 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% BOD 198 195 98.3 84.6-115 Laboratory Control Sample (LCS) (LCS) 11/24/15 11:35 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% BOD 198 182 91.9 84.6-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 71 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 71 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830498 Wet Chemistry by Method 9056MOD L801958-27,28,29 Method Blank (MB) (MB) 11/20/15 06:31 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Nitrate ND 0.100 Sulfate ND 5.00 L801988-05 Original Sample (OS) • Duplicate (DUP) (OS) 11/20/15 10:12 • (DUP) 11/20/15 10:58 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Nitrate 0.132 0.132 1 0 20 Sulfate 48.0 47.9 1 0 20 L802004-03 Original Sample (OS) • Duplicate (DUP) (OS) 11/20/15 12:46 • (DUP) 11/20/15 13:02 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Nitrate ND 0.000 1 0 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/20/15 06:47 • (LCSD) 11/20/15 07:21 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Nitrate 8.00 8.17 8.15 102 102 90-110 0 20 Sulfate 40.0 39.4 39.3 99 98 90-110 0 20 L801988-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/20/15 10:43 • (MS) 11/20/15 11:14 • (MSD) 11/20/15 11:29 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Nitrate 5.00 0.560 5.47 5.43 98 97 1 80-120 1 20 Sulfate 50.0 22.3 70.7 70.6 97 97 1 80-120 0 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 72 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 72 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830498 Wet Chemistry by Method 9056MOD L801958-27,28,29 L802287-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/20/15 14:04 • (MS) 11/20/15 14:47 • (MSD) 11/20/15 15:03 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Nitrate 5.00 1.19 6.07 6.19 98 100 1 80-120 2 20 Sulfate 50.0 5.77 55.3 55.4 99 99 1 80-120 0 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 73 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 73 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830629 Wet Chemistry by Method 9056MOD L801958-15,16 Method Blank (MB) (MB) 11/21/15 12:00 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Chloride ND 1.00 Sulfate ND 5.00 L801908-01 Original Sample (OS) • Duplicate (DUP) (OS) 11/21/15 14:19 • (DUP) 11/21/15 14:34 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Chloride 179 183 20 2 20 Sulfate 1050 1070 20 1 20 L802005-09 Original Sample (OS) • Duplicate (DUP) (OS) 11/21/15 18:56 • (DUP) 11/21/15 19:12 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Chloride 1.19 1.18 1 1 20 Sulfate 0.957 0.963 1 0 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/21/15 12:15 • (LCSD) 11/21/15 12:31 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Chloride 40.0 39.7 39.7 99 99 90-110 0 20 Sulfate 40.0 40.1 40.1 100 100 90-110 0 20 L801908-03 Original Sample (OS) • Matrix Spike (MS) (OS) 11/21/15 14:49 • (MS) 11/21/15 15:05 Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier Analyte mg/l mg/l mg/l %% Chloride 5.00 102 591 98 10 80-120 Sulfate 5.00 319 795 95 10 80-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 74 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 74 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830629 Wet Chemistry by Method 9056MOD L801958-15,16 L802005-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/21/15 19:27 • (MS) 11/21/15 19:42 • (MSD) 11/21/15 19:58 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Chloride 50.0 2.04 51.8 51.9 100 100 1 80-120 0 20 Sulfate 50.0 3.02 52.7 52.7 99 99 1 80-120 0 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 75 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 75 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830779 Wet Chemistry by Method 9056MOD L801958-27 Method Blank (MB) (MB) 11/24/15 07:42 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Sulfate ND 5.00 L801979-01 Original Sample (OS) • Duplicate (DUP) (OS) 11/24/15 10:51 • (DUP) 11/24/15 11:06 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Sulfate 422 422 10 0 20 L802323-07 Original Sample (OS) • Duplicate (DUP) (OS) 11/24/15 14:26 • (DUP) 11/24/15 14:42 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % Sulfate 110 109 10 0 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/24/15 07:58 • (LCSD) 11/24/15 08:13 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Sulfate 40.0 40.1 40.2 100 100 90-110 0 20 L801999-04 Original Sample (OS) • Matrix Spike (MS) (OS) 11/24/15 11:21 • (MS) 11/24/15 11:37 Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier Analyte mg/l mg/l mg/l %% Sulfate 5.00 207 691 97 10 80-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 76 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 76 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830779 Wet Chemistry by Method 9056MOD L801958-27 L802323-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/24/15 13:40 • (MS) 11/24/15 13:55 • (MSD) 11/24/15 14:11 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Sulfate 5.00 539 1030 1030 97 97 10 80-120 0 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 77 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 77 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830587 Metals (ICPMS) by Method 6020 L801958-21,22,23,24,27,28,29 Method Blank (MB) (MB) 11/23/15 12:43 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Antimony ND 0.00200 Arsenic ND 0.00200 Beryllium ND 0.00200 Cadmium ND 0.00100 Copper ND 0.00500 Lead ND 0.00200 Selenium ND 0.00200 Thallium ND 0.00200 Zinc ND 0.0250 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/23/15 12:45 • (LCSD) 11/23/15 12:48 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Antimony 0.0500 0.0534 0.0534 107 107 80-120 0 20 Arsenic 0.0500 0.0515 0.0516 103 103 80-120 0 20 Beryllium 0.0500 0.0546 0.0549 109 110 80-120 1 20 Cadmium 0.0500 0.0538 0.0540 108 108 80-120 0 20 Copper 0.0500 0.0544 0.0524 109 105 80-120 4 20 Lead 0.0500 0.0482 0.0491 96 98 80-120 2 20 Selenium 0.0500 0.0495 0.0486 99 97 80-120 2 20 Thallium 0.0500 0.0495 0.0492 99 98 80-120 1 20 Zinc 0.0500 0.0502 0.0494 100 99 80-120 2 20 L801958-21 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/23/15 12:50 • (MS) 11/23/15 12:55 • (MSD) 11/23/15 12:57 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Antimony 0.0500 0.000429 0.0496 0.0506 98 100 1 75-125 2 20 Arsenic 0.0500 0.00469 0.0515 0.0552 94 101 1 75-125 7 20 Beryllium 0.0500 0.0000791 0.0551 0.0556 110 111 1 75-125 1 20 Cadmium 0.0500 0.0000218 0.0521 0.0551 104 110 1 75-125 5 20 Copper 0.0500 0.00857 0.0617 0.0618 106 106 1 75-125 0 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 78 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 78 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830587 Metals (ICPMS) by Method 6020 L801958-21,22,23,24,27,28,29 L801958-21 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/23/15 12:50 • (MS) 11/23/15 12:55 • (MSD) 11/23/15 12:57 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Lead 0.0500 0.00392 0.0545 0.0536 101 99 1 75-125 2 20 Selenium 0.0500 0.000537 0.0413 0.0429 81 85 1 75-125 4 20 Thallium 0.0500 0.0000847 0.0486 0.0485 97 97 1 75-125 0 20 Zinc 0.0500 0.0120 0.0561 0.0758 88 128 1 75-125 J3 J5 30 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 79 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 79 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830588 Metals (ICPMS) by Method 6020 L801958-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) 11/27/15 18:44 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Antimony ND 0.00200 Arsenic ND 0.00200 Barium ND 0.00500 Beryllium ND 0.00200 Cadmium ND 0.00100 Chromium ND 0.00200 Copper ND 0.00500 Cobalt ND 0.00200 Lead ND 0.00200 Nickel ND 0.00200 Selenium ND 0.00200 Silver ND 0.00200 Thallium ND 0.00200 Vanadium ND 0.00500 Zinc ND 0.0250 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/27/15 18:46 • (LCSD) 11/27/15 18:48 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Antimony 0.0500 0.0521 0.0533 104 107 80-120 2 20 Arsenic 0.0500 0.0491 0.0502 98 100 80-120 2 20 Barium 0.0500 0.0511 0.0502 102 100 80-120 2 20 Beryllium 0.0500 0.0488 0.0487 98 97 80-120 0 20 Cadmium 0.0500 0.0511 0.0527 102 105 80-120 3 20 Chromium 0.0500 0.0488 0.0509 98 102 80-120 4 20 Copper 0.0500 0.0518 0.0530 104 106 80-120 2 20 Cobalt 0.0500 0.0507 0.0514 101 103 80-120 1 20 Lead 0.0500 0.0485 0.0463 97 93 80-120 5 20 Nickel 0.0500 0.0512 0.0515 102 103 80-120 1 20 Selenium 0.0500 0.0497 0.0490 99 98 80-120 1 20 Silver 0.0500 0.0517 0.0522 103 104 80-120 1 20 Thallium 0.0500 0.0488 0.0471 98 94 80-120 3 20 Vanadium 0.0500 0.0474 0.0489 95 98 80-120 3 20 Zinc 0.0500 0.0473 0.0475 95 95 80-120 1 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 80 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 80 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830588 Metals (ICPMS) by Method 6020 L801958-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 L801958-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/27/15 18:51 • (MS) 11/27/15 18:55 • (MSD) 11/27/15 18:58 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Antimony 0.0500 0.000449 0.0525 0.0526 104 104 1 75-125 0 20 Arsenic 0.0500 0.000841 0.0516 0.0516 102 101 1 75-125 0 20 Barium 0.0500 0.0624 0.114 0.113 103 101 1 75-125 1 20 Beryllium 0.0500 0.0000258 0.0490 0.0498 98 100 1 75-125 2 20 Cadmium 0.0500 0.0000470 0.0530 0.0530 106 106 1 75-125 0 20 Chromium 0.0500 0.00114 0.0496 0.0497 97 97 1 75-125 0 20 Copper 0.0500 0.000907 0.0527 0.0523 104 103 1 75-125 1 20 Cobalt 0.0500 0.0000949 0.0496 0.0505 99 101 1 75-125 2 20 Lead 0.0500 0.000101 0.0479 0.0492 96 98 1 75-125 3 20 Nickel 0.0500 0.00101 0.0512 0.0523 100 103 1 75-125 2 20 Selenium 0.0500 0.000698 0.0498 0.0498 98 98 1 75-125 0 20 Silver 0.0500 0.000167 0.0517 0.0519 103 104 1 75-125 0 20 Thallium 0.0500 0.000186 0.0486 0.0504 97 100 1 75-125 4 20 Vanadium 0.0500 0.000180 0.0479 0.0479 95 96 1 75-125 0 20 Zinc 0.0500 0.000887 0.0471 0.0461 92 91 1 75-125 2 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 81 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 81 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830452 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-01,02,03,04,05,06,07,08,09,10,11,12,13,14 Method Blank (MB) (MB) 11/20/15 18:18 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Acetone ND 0.0500 Acrylonitrile ND 0.0100 Benzene ND 0.00100 Bromodichloromethane ND 0.00100 Bromochloromethane ND 0.00100 Bromoform ND 0.00100 Bromomethane ND 0.00500 Carbon disulfide ND 0.00100 Carbon tetrachloride ND 0.00100 Chlorobenzene ND 0.00100 Chlorodibromomethane ND 0.00100 Chloroethane ND 0.00500 Chloroform ND 0.00500 Chloromethane ND 0.00250 Dibromomethane ND 0.00100 1,2-Dichlorobenzene ND 0.00100 1,4-Dichlorobenzene ND 0.00100 trans-1,4-Dichloro-2-butene ND 0.00250 1,1-Dichloroethane ND 0.00100 1,2-Dichloroethane ND 0.00100 1,1-Dichloroethene ND 0.00100 cis-1,2-Dichloroethene ND 0.00100 trans-1,2-Dichloroethene ND 0.00100 1,2-Dichloropropane ND 0.00100 cis-1,3-Dichloropropene ND 0.00100 trans-1,3-Dichloropropene ND 0.00100 Ethylbenzene ND 0.00100 2-Hexanone ND 0.0100 Iodomethane ND 0.0100 2-Butanone (MEK)ND 0.0100 Methylene Chloride ND 0.00500 4-Methyl-2-pentanone (MIBK)ND 0.0100 Styrene ND 0.00100 Toluene ND 0.00500 1,1,1,2-Tetrachloroethane ND 0.00100 1,1,2,2-Tetrachloroethane ND 0.00100 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 82 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 82 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830452 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-01,02,03,04,05,06,07,08,09,10,11,12,13,14 Method Blank (MB) (MB) 11/20/15 18:18 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Tetrachloroethene ND 0.00100 1,1,1-Trichloroethane ND 0.00100 1,1,2-Trichloroethane ND 0.00100 Trichloroethene ND 0.00100 Trichlorofluoromethane ND 0.00500 1,2,3-Trichloropropane ND 0.00250 Xylenes, Total ND 0.00300 Vinyl acetate ND 0.0100 Vinyl chloride ND 0.00100 (S) Toluene-d8 100 90.0-115 (S) Dibromofluoromethane 96.5 79.0-121 (S) a,a,a-Trifluorotoluene 107 90.4-116 (S) 4-Bromofluorobenzene 111 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/20/15 17:05 • (LCSD) 11/20/15 19:15 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Acetone 0.125 0.120 0.115 96.3 91.9 28.7-175 4.68 20.9 Benzene 0.0250 0.0211 0.0211 84.3 84.3 73.0-122 0.0500 20 Acrylonitrile 0.125 0.0826 0.0792 66.1 63.4 58.2-145 4.13 20 Bromodichloromethane 0.0250 0.0277 0.0275 111 110 75.5-121 0.960 20 Bromochloromethane 0.0250 0.0225 0.0224 90.2 89.7 78.9-123 0.450 20 Bromoform 0.0250 0.0267 0.0241 107 96.4 71.5-131 10.2 20 Bromomethane 0.0250 0.0252 0.0228 101 91.1 22.4-187 10.3 20 Carbon disulfide 0.0250 0.0221 0.0205 88.4 82.1 53.0-134 7.30 20 Carbon tetrachloride 0.0250 0.0266 0.0280 107 112 70.9-129 5.16 20 Chlorobenzene 0.0250 0.0251 0.0254 101 102 79.7-122 1.19 20 Chlorodibromomethane 0.0250 0.0276 0.0256 111 102 78.2-124 7.61 20 Chloroethane 0.0250 0.0244 0.0236 97.7 94.5 41.2-153 3.31 20 Chloroform 0.0250 0.0248 0.0251 99.1 101 73.2-125 1.43 20 Chloromethane 0.0250 0.0192 0.0188 76.9 75.1 55.8-134 2.41 20 Dibromomethane 0.0250 0.0240 0.0238 96.1 95.2 79.5-118 0.860 20 1,2-Dichlorobenzene 0.0250 0.0243 0.0241 97.0 96.5 84.7-118 0.490 20 1,4-Dichlorobenzene 0.0250 0.0235 0.0239 93.9 95.7 82.2-114 1.90 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 83 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 83 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830452 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-01,02,03,04,05,06,07,08,09,10,11,12,13,14 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/20/15 17:05 • (LCSD) 11/20/15 19:15 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% trans-1,4-Dichloro-2-butene 0.0250 0.0257 0.0239 103 95.7 58.3-129 7.18 20 1,1-Dichloroethane 0.0250 0.0232 0.0231 92.9 92.6 71.7-127 0.370 20 1,2-Dichloroethane 0.0250 0.0265 0.0270 106 108 65.3-126 1.63 20 1,1-Dichloroethene 0.0250 0.0273 0.0268 109 107 59.9-137 1.84 20 cis-1,2-Dichloroethene 0.0250 0.0224 0.0220 89.4 87.8 77.3-122 1.79 20 trans-1,2-Dichloroethene 0.0250 0.0226 0.0217 90.6 86.8 72.6-125 4.26 20 1,2-Dichloropropane 0.0250 0.0231 0.0230 92.3 92.1 77.4-125 0.190 20 cis-1,3-Dichloropropene 0.0250 0.0250 0.0239 100 95.7 77.7-124 4.52 20 trans-1,3-Dichloropropene 0.0250 0.0252 0.0263 101 105 73.5-127 4.47 20 Ethylbenzene 0.0250 0.0252 0.0262 101 105 80.9-121 3.70 20 2-Hexanone 0.125 0.103 0.0942 82.7 75.3 59.4-151 9.32 20 Iodomethane 0.125 0.105 0.102 83.8 81.6 64.6-137 2.65 20 2-Butanone (MEK)0.125 0.0862 0.0819 68.9 65.5 46.4-155 5.08 20 Methylene Chloride 0.0250 0.0208 0.0215 83.2 86.1 69.5-120 3.44 20 4-Methyl-2-pentanone (MIBK)0.125 0.0902 0.0864 72.2 69.1 63.3-138 4.35 20 Styrene 0.0250 0.0255 0.0241 102 96.6 79.9-124 5.62 20 1,1,1,2-Tetrachloroethane 0.0250 0.0274 0.0275 110 110 78.5-125 0.260 20 1,1,2,2-Tetrachloroethane 0.0250 0.0226 0.0206 90.5 82.4 79.3-123 9.41 20 Tetrachloroethene 0.0250 0.0263 0.0266 105 106 73.5-130 1.18 20 Toluene 0.0250 0.0234 0.0238 93.5 95.1 77.9-116 1.74 20 1,1,1-Trichloroethane 0.0250 0.0272 0.0280 109 112 71.1-129 2.78 20 1,1,2-Trichloroethane 0.0250 0.0233 0.0222 93.2 88.9 81.6-120 4.76 20 Trichloroethene 0.0250 0.0257 0.0258 103 103 79.5-121 0.0600 20 Trichlorofluoromethane 0.0250 0.0293 0.0288 117 115 49.1-157 1.83 20 1,2,3-Trichloropropane 0.0250 0.0250 0.0231 99.9 92.6 74.9-124 7.60 20 Vinyl acetate 0.125 0.0989 0.103 79.1 82.3 41.7-159 3.95 20 Xylenes, Total 0.0750 0.0745 0.0749 99.4 99.8 79.2-122 0.420 20 Vinyl chloride 0.0250 0.0253 0.0236 101 94.5 61.5-134 6.72 20 (S) Toluene-d8 103 106 90.0-115 (S) Dibromofluoromethane 94.4 97.8 79.0-121 (S) a,a,a-Trifluorotoluene 106 107 90.4-116 (S) 4-Bromofluorobenzene 111 107 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 84 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 84 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830452 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-01,02,03,04,05,06,07,08,09,10,11,12,13,14 L801958-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/20/15 21:03 • (MS) 11/20/15 19:50 • (MSD) 11/20/15 20:08 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Acetone 0.125 0.000934 0.0540 0.0521 42.5 41.0 1 25.0-156 3.51 21.5 Benzene 0.0250 ND 0.0189 0.0187 75.5 74.7 1 58.6-133 1.09 20 Acrylonitrile 0.125 ND 0.0807 0.0805 64.6 64.4 1 55.9-161 0.190 20 Bromodichloromethane 0.0250 ND 0.0252 0.0247 101 98.9 1 69.2-127 2.04 20 Bromochloromethane 0.0250 ND 0.0200 0.0206 80.1 82.3 1 74.4-128 2.70 20 Bromoform 0.0250 ND 0.0247 0.0235 98.9 94.2 1 66.3-140 4.86 20 Bromomethane 0.0250 ND 0.0200 0.0209 79.8 83.6 1 16.6-183 4.55 20.5 Carbon disulfide 0.0250 ND 0.0151 0.0158 60.6 63.3 1 34.9-138 4.40 20 Carbon tetrachloride 0.0250 ND 0.0256 0.0258 102 103 1 60.6-139 1.10 20 Chlorobenzene 0.0250 ND 0.0242 0.0226 96.6 90.5 1 70.1-130 6.50 20 Chlorodibromomethane 0.0250 ND 0.0254 0.0243 102 97.4 1 71.6-132 4.16 20 Chloroethane 0.0250 ND 0.0226 0.0227 90.2 90.7 1 33.3-155 0.510 20 Chloroform 0.0250 ND 0.0233 0.0234 93.1 93.6 1 66.1-133 0.600 20 Chloromethane 0.0250 ND 0.0166 0.0167 66.4 66.7 1 40.7-139 0.540 20 Dibromomethane 0.0250 ND 0.0223 0.0230 89.0 92.0 1 72.8-127 3.29 20 1,2-Dichlorobenzene 0.0250 ND 0.0232 0.0225 93.0 90.1 1 77.4-127 3.21 20 1,4-Dichlorobenzene 0.0250 ND 0.0229 0.0230 91.5 91.9 1 74.4-123 0.520 20 trans-1,4-Dichloro-2-butene 0.0250 ND 0.0259 0.0239 104 95.4 1 57.6-136 8.40 20 1,1-Dichloroethane 0.0250 ND 0.0211 0.0213 84.6 85.2 1 64.0-134 0.720 20 1,2-Dichloroethane 0.0250 ND 0.0239 0.0250 95.5 100 1 60.7-132 4.66 20 1,1-Dichloroethene 0.0250 ND 0.0236 0.0240 94.6 96.0 1 48.8-144 1.48 20 cis-1,2-Dichloroethene 0.0250 ND 0.0199 0.0209 79.5 83.6 1 60.6-136 5.01 20 trans-1,2-Dichloroethene 0.0250 ND 0.0192 0.0199 76.7 79.8 1 61.0-132 3.85 20 1,2-Dichloropropane 0.0250 ND 0.0209 0.0219 83.7 87.6 1 69.7-130 4.59 20 cis-1,3-Dichloropropene 0.0250 ND 0.0225 0.0225 89.8 89.9 1 71.1-129 0.110 20 trans-1,3-Dichloropropene 0.0250 ND 0.0246 0.0242 98.3 96.9 1 66.3-136 1.45 20 Ethylbenzene 0.0250 ND 0.0243 0.0228 97.1 91.0 1 62.7-136 6.44 20 2-Hexanone 0.125 ND 0.0792 0.0743 63.4 59.4 1 59.4-154 6.45 20.1 Iodomethane 0.125 0.000971 0.0896 0.0906 70.9 71.7 1 55.2-140 1.09 20 2-Butanone (MEK)0.125 ND 0.0571 0.0574 45.7 45.9 1 45.0-156 0.500 20.8 Methylene Chloride 0.0250 ND 0.0185 0.0188 74.2 75.2 1 61.5-125 1.42 20 4-Methyl-2-pentanone (MIBK)0.125 ND 0.0819 0.0862 65.5 69.0 1 60.7-150 5.12 20 Styrene 0.0250 ND 0.0246 0.0236 98.5 94.2 1 68.2-133 4.36 20 1,1,1,2-Tetrachloroethane 0.0250 ND 0.0261 0.0252 105 101 1 70.5-132 3.46 20 1,1,2,2-Tetrachloroethane 0.0250 ND 0.0212 0.0204 84.7 81.5 1 64.9-145 3.83 20 Tetrachloroethene 0.0250 ND 0.0252 0.0232 101 92.7 1 57.4-141 8.29 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 85 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 85 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830452 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-01,02,03,04,05,06,07,08,09,10,11,12,13,14 L801958-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/20/15 21:03 • (MS) 11/20/15 19:50 • (MSD) 11/20/15 20:08 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Toluene 0.0250 ND 0.0215 0.0217 86.1 86.6 1 67.8-124 0.610 20 1,1,1-Trichloroethane 0.0250 ND 0.0251 0.0260 100 104 1 58.7-134 3.66 20 1,1,2-Trichloroethane 0.0250 ND 0.0226 0.0219 90.6 87.4 1 74.1-130 3.53 20 Trichloroethene 0.0250 ND 0.0236 0.0229 94.2 91.7 1 48.9-148 2.71 20 Trichlorofluoromethane 0.0250 ND 0.0257 0.0257 103 103 1 39.9-165 0.150 20 1,2,3-Trichloropropane 0.0250 ND 0.0230 0.0211 92.0 84.3 1 71.5-134 8.66 20 Vinyl acetate 0.125 ND 0.0958 0.0993 76.7 79.4 1 42.8-181 3.51 20 Xylenes, Total 0.0750 ND 0.0715 0.0699 95.3 93.3 1 65.6-133 2.17 20 Vinyl chloride 0.0250 ND 0.0208 0.0221 83.1 88.5 1 44.3-143 6.28 20 (S) Toluene-d8 105 106 90.0-115 (S) Dibromofluoromethane 94.6 97.1 79.0-121 (S) a,a,a-Trifluorotoluene 107 109 90.4-116 (S) 4-Bromofluorobenzene 108 106 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 86 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 86 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830461 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-15,16,17,18,19,20,21,22,23,24,25,26,27,28 Method Blank (MB) (MB) 11/21/15 05:07 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Acetone ND 0.0500 Acrylonitrile ND 0.0100 Benzene ND 0.00100 Bromodichloromethane ND 0.00100 Bromochloromethane ND 0.00100 Bromoform ND 0.00100 Bromomethane ND 0.00500 Carbon disulfide ND 0.00100 Carbon tetrachloride ND 0.00100 Chlorobenzene ND 0.00100 Chlorodibromomethane ND 0.00100 Chloroethane ND 0.00500 Chloroform ND 0.00500 Chloromethane ND 0.00250 Dibromomethane ND 0.00100 1,2-Dichlorobenzene ND 0.00100 1,4-Dichlorobenzene ND 0.00100 trans-1,4-Dichloro-2-butene ND 0.00250 1,1-Dichloroethane ND 0.00100 1,2-Dichloroethane ND 0.00100 1,1-Dichloroethene ND 0.00100 cis-1,2-Dichloroethene ND 0.00100 trans-1,2-Dichloroethene ND 0.00100 1,2-Dichloropropane ND 0.00100 cis-1,3-Dichloropropene ND 0.00100 trans-1,3-Dichloropropene ND 0.00100 Ethylbenzene ND 0.00100 2-Hexanone ND 0.0100 Iodomethane ND 0.0100 2-Butanone (MEK)ND 0.0100 Methylene Chloride ND 0.00500 4-Methyl-2-pentanone (MIBK)ND 0.0100 Styrene ND 0.00100 1,1,1,2-Tetrachloroethane ND 0.00100 1,1,2,2-Tetrachloroethane ND 0.00100 Tetrachloroethene ND 0.00100 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 87 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 87 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830461 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-15,16,17,18,19,20,21,22,23,24,25,26,27,28 Method Blank (MB) (MB) 11/21/15 05:07 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Toluene ND 0.00500 1,1,1-Trichloroethane ND 0.00100 1,1,2-Trichloroethane ND 0.00100 Trichloroethene ND 0.00100 Trichlorofluoromethane ND 0.00500 1,2,3-Trichloropropane ND 0.00250 Vinyl acetate ND 0.0100 Vinyl chloride ND 0.00100 Xylenes, Total ND 0.00300 (S) Toluene-d8 101 90.0-115 (S) Dibromofluoromethane 102 79.0-121 (S) a,a,a-Trifluorotoluene 106 90.4-116 (S) 4-Bromofluorobenzene 103 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/21/15 03:17 • (LCSD) 11/21/15 03:35 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Acetone 0.125 0.0964 0.0873 77.1 69.8 28.7-175 9.90 20.9 Acrylonitrile 0.125 0.0758 0.0708 60.7 56.6 58.2-145 J4 6.91 20 Benzene 0.0250 0.0195 0.0197 77.8 78.9 73.0-122 1.37 20 Bromodichloromethane 0.0250 0.0270 0.0271 108 109 75.5-121 0.540 20 Bromochloromethane 0.0250 0.0213 0.0213 85.0 85.1 78.9-123 0.130 20 Bromoform 0.0250 0.0262 0.0254 105 102 71.5-131 3.15 20 Bromomethane 0.0250 0.0223 0.0222 89.1 88.6 22.4-187 0.530 20 Carbon disulfide 0.0250 0.0188 0.0192 75.3 76.7 53.0-134 1.86 20 Carbon tetrachloride 0.0250 0.0267 0.0263 107 105 70.9-129 1.53 20 Chlorobenzene 0.0250 0.0230 0.0243 91.8 97.2 79.7-122 5.71 20 Chlorodibromomethane 0.0250 0.0266 0.0267 106 107 78.2-124 0.540 20 Chloroethane 0.0250 0.0235 0.0228 93.9 91.1 41.2-153 3.08 20 Chloroform 0.0250 0.0246 0.0243 98.2 97.2 73.2-125 1.06 20 Chloromethane 0.0250 0.0177 0.0175 70.7 69.9 55.8-134 1.21 20 Dibromomethane 0.0250 0.0246 0.0242 98.4 96.8 79.5-118 1.62 20 1,2-Dichlorobenzene 0.0250 0.0240 0.0236 95.9 94.5 84.7-118 1.47 20 1,4-Dichlorobenzene 0.0250 0.0225 0.0233 90.2 93.3 82.2-114 3.42 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 88 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 88 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830461 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-15,16,17,18,19,20,21,22,23,24,25,26,27,28 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/21/15 03:17 • (LCSD) 11/21/15 03:35 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% trans-1,4-Dichloro-2-butene 0.0250 0.0240 0.0250 96.2 99.9 58.3-129 3.78 20 1,1-Dichloroethane 0.0250 0.0216 0.0214 86.5 85.6 71.7-127 1.08 20 1,2-Dichloroethane 0.0250 0.0265 0.0251 106 101 65.3-126 5.43 20 1,1-Dichloroethene 0.0250 0.0245 0.0242 98.0 96.6 59.9-137 1.42 20 cis-1,2-Dichloroethene 0.0250 0.0211 0.0209 84.5 83.8 77.3-122 0.880 20 trans-1,2-Dichloroethene 0.0250 0.0218 0.0211 87.2 84.4 72.6-125 3.36 20 1,2-Dichloropropane 0.0250 0.0214 0.0218 85.6 87.2 77.4-125 1.96 20 cis-1,3-Dichloropropene 0.0250 0.0236 0.0244 94.4 97.7 77.7-124 3.40 20 trans-1,3-Dichloropropene 0.0250 0.0252 0.0251 101 100 73.5-127 0.420 20 Ethylbenzene 0.0250 0.0227 0.0235 90.8 94.1 80.9-121 3.62 20 2-Hexanone 0.125 0.0955 0.0998 76.4 79.8 59.4-151 4.35 20 Iodomethane 0.125 0.0955 0.0963 76.4 77.0 64.6-137 0.770 20 2-Butanone (MEK)0.125 0.0802 0.0784 64.1 62.7 46.4-155 2.28 20 Methylene Chloride 0.0250 0.0205 0.0205 81.9 82.0 69.5-120 0.100 20 4-Methyl-2-pentanone (MIBK)0.125 0.0921 0.0917 73.7 73.4 63.3-138 0.470 20 Styrene 0.0250 0.0236 0.0239 94.4 95.6 79.9-124 1.26 20 1,1,1,2-Tetrachloroethane 0.0250 0.0262 0.0270 105 108 78.5-125 2.87 20 1,1,2,2-Tetrachloroethane 0.0250 0.0210 0.0212 83.9 84.9 79.3-123 1.26 20 Tetrachloroethene 0.0250 0.0244 0.0268 97.4 107 73.5-130 9.62 20 Toluene 0.0250 0.0221 0.0233 88.4 93.1 77.9-116 5.17 20 1,1,1-Trichloroethane 0.0250 0.0264 0.0265 105 106 71.1-129 0.610 20 1,1,2-Trichloroethane 0.0250 0.0218 0.0227 87.3 91.0 81.6-120 4.19 20 Trichloroethene 0.0250 0.0242 0.0248 96.9 99.4 79.5-121 2.53 20 Trichlorofluoromethane 0.0250 0.0280 0.0258 112 103 49.1-157 8.27 20 1,2,3-Trichloropropane 0.0250 0.0235 0.0247 94.0 98.6 74.9-124 4.84 20 Vinyl acetate 0.125 0.0895 0.0917 71.6 73.3 41.7-159 2.42 20 Vinyl chloride 0.0250 0.0229 0.0222 91.5 88.9 61.5-134 2.90 20 Xylenes, Total 0.0750 0.0687 0.0708 91.6 94.5 79.2-122 3.04 20 (S) Toluene-d8 106 105 90.0-115 (S) Dibromofluoromethane 98.3 96.0 79.0-121 (S) a,a,a-Trifluorotoluene 114 109 90.4-116 (S) 4-Bromofluorobenzene 107 103 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 89 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 89 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830461 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-15,16,17,18,19,20,21,22,23,24,25,26,27,28 L801958-15 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/21/15 07:15 • (MS) 11/21/15 05:43 • (MSD) 11/21/15 06:02 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Acetone 0.125 0.000703 0.0365 0.0478 28.6 37.7 1 25.0-156 J3 26.8 21.5 Acrylonitrile 0.125 ND 0.0804 0.0829 64.3 66.3 1 55.9-161 3.10 20 Benzene 0.0250 ND 0.0197 0.0188 78.6 75.1 1 58.6-133 4.58 20 Bromodichloromethane 0.0250 ND 0.0268 0.0262 107 105 1 69.2-127 2.11 20 Bromochloromethane 0.0250 ND 0.0217 0.0215 86.9 85.9 1 74.4-128 1.13 20 Bromoform 0.0250 ND 0.0264 0.0241 106 96.3 1 66.3-140 9.12 20 Bromomethane 0.0250 ND 0.0206 0.0206 82.3 82.5 1 16.6-183 0.240 20.5 Carbon disulfide 0.0250 ND 0.0178 0.0181 71.1 72.6 1 34.9-138 2.09 20 Carbon tetrachloride 0.0250 ND 0.0261 0.0260 104 104 1 60.6-139 0.130 20 Chlorobenzene 0.0250 ND 0.0239 0.0222 95.4 88.8 1 70.1-130 7.24 20 Chlorodibromomethane 0.0250 ND 0.0263 0.0245 105 98.0 1 71.6-132 7.20 20 Chloroethane 0.0250 ND 0.0205 0.0220 82.2 87.8 1 33.3-155 6.65 20 Chloroform 0.0250 ND 0.0236 0.0233 94.4 93.2 1 66.1-133 1.27 20 Chloromethane 0.0250 ND 0.0168 0.0172 67.1 68.6 1 40.7-139 2.19 20 Dibromomethane 0.0250 ND 0.0247 0.0239 98.6 95.5 1 72.8-127 3.28 20 1,2-Dichlorobenzene 0.0250 ND 0.0239 0.0221 95.8 88.5 1 77.4-127 7.89 20 1,4-Dichlorobenzene 0.0250 ND 0.0228 0.0219 91.2 87.7 1 74.4-123 3.91 20 trans-1,4-Dichloro-2-butene 0.0250 ND 0.0247 0.0251 98.8 100 1 57.6-136 1.47 20 1,1-Dichloroethane 0.0250 ND 0.0215 0.0214 85.9 85.6 1 64.0-134 0.350 20 1,2-Dichloroethane 0.0250 ND 0.0254 0.0253 102 101 1 60.7-132 0.560 20 1,1-Dichloroethene 0.0250 ND 0.0233 0.0239 93.1 95.5 1 48.8-144 2.48 20 cis-1,2-Dichloroethene 0.0250 ND 0.0207 0.0203 82.7 81.1 1 60.6-136 1.95 20 trans-1,2-Dichloroethene 0.0250 ND 0.0215 0.0198 86.0 79.3 1 61.0-132 8.15 20 1,2-Dichloropropane 0.0250 ND 0.0221 0.0213 88.5 85.3 1 69.7-130 3.69 20 cis-1,3-Dichloropropene 0.0250 ND 0.0237 0.0239 94.6 95.5 1 71.1-129 0.930 20 trans-1,3-Dichloropropene 0.0250 ND 0.0258 0.0242 103 96.7 1 66.3-136 6.54 20 Ethylbenzene 0.0250 ND 0.0239 0.0217 95.5 86.8 1 62.7-136 9.53 20 2-Hexanone 0.125 ND 0.0837 0.0805 67.0 64.4 1 59.4-154 3.97 20.1 Iodomethane 0.125 ND 0.0931 0.0942 74.5 75.4 1 55.2-140 1.16 20 2-Butanone (MEK)0.125 ND 0.0553 0.0619 44.2 49.5 1 45.0-156 J6 11.3 20.8 Methylene Chloride 0.0250 0.000436 0.0194 0.0199 76.0 77.9 1 61.5-125 2.37 20 4-Methyl-2-pentanone (MIBK)0.125 ND 0.0929 0.0910 74.3 72.8 1 60.7-150 2.08 20 Styrene 0.0250 ND 0.0235 0.0222 93.8 88.8 1 68.2-133 5.53 20 1,1,1,2-Tetrachloroethane 0.0250 ND 0.0265 0.0239 106 95.6 1 70.5-132 10.3 20 1,1,2,2-Tetrachloroethane 0.0250 ND 0.0220 0.0203 88.2 81.1 1 64.9-145 8.38 20 Tetrachloroethene 0.0250 ND 0.0261 0.0235 104 94.0 1 57.4-141 10.6 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 90 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 90 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG830461 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-15,16,17,18,19,20,21,22,23,24,25,26,27,28 L801958-15 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 11/21/15 07:15 • (MS) 11/21/15 05:43 • (MSD) 11/21/15 06:02 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Toluene 0.0250 ND 0.0226 0.0225 90.3 90.1 1 67.8-124 0.150 20 1,1,1-Trichloroethane 0.0250 ND 0.0256 0.0253 102 101 1 58.7-134 0.840 20 1,1,2-Trichloroethane 0.0250 ND 0.0228 0.0214 91.1 85.7 1 74.1-130 6.15 20 Trichloroethene 0.0250 ND 0.0245 0.0232 97.9 92.7 1 48.9-148 5.46 20 Trichlorofluoromethane 0.0250 ND 0.0262 0.0271 105 108 1 39.9-165 3.52 20 1,2,3-Trichloropropane 0.0250 ND 0.0251 0.0226 100 90.6 1 71.5-134 10.3 20 Vinyl acetate 0.125 ND 0.103 0.105 82.3 83.8 1 42.8-181 1.75 20 Vinyl chloride 0.0250 ND 0.0224 0.0226 89.4 90.2 1 44.3-143 0.860 20 Xylenes, Total 0.0750 ND 0.0678 0.0654 90.4 87.2 1 65.6-133 3.57 20 (S) Toluene-d8 103 107 90.0-115 (S) Dibromofluoromethane 96.0 101 79.0-121 (S) a,a,a-Trifluorotoluene 109 109 90.4-116 (S) 4-Bromofluorobenzene 106 103 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 91 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 91 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG832427 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-29 Method Blank (MB) (MB) 12/01/15 06:38 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Acetone ND 0.0500 Acrylonitrile ND 0.0100 Benzene ND 0.00100 Bromodichloromethane ND 0.00100 Bromochloromethane ND 0.00100 Bromoform ND 0.00100 Bromomethane ND 0.00500 Carbon disulfide ND 0.00100 Carbon tetrachloride ND 0.00100 Chlorobenzene ND 0.00100 Chlorodibromomethane ND 0.00100 Chloroethane ND 0.00500 Chloroform ND 0.00500 Chloromethane ND 0.00250 Dibromomethane ND 0.00100 1,2-Dichlorobenzene ND 0.00100 1,4-Dichlorobenzene ND 0.00100 trans-1,4-Dichloro-2-butene ND 0.00250 1,1-Dichloroethane ND 0.00100 1,2-Dichloroethane ND 0.00100 1,1-Dichloroethene ND 0.00100 cis-1,2-Dichloroethene ND 0.00100 trans-1,2-Dichloroethene ND 0.00100 1,2-Dichloropropane ND 0.00100 cis-1,3-Dichloropropene ND 0.00100 trans-1,3-Dichloropropene ND 0.00100 Ethylbenzene ND 0.00100 2-Hexanone ND 0.0100 Iodomethane ND 0.0100 2-Butanone (MEK)ND 0.0100 Methylene Chloride ND 0.00500 4-Methyl-2-pentanone (MIBK)ND 0.0100 Styrene ND 0.00100 Toluene ND 0.00500 1,1,1,2-Tetrachloroethane ND 0.00100 1,1,2,2-Tetrachloroethane ND 0.00100 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 92 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 92 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG832427 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-29 Method Blank (MB) (MB) 12/01/15 06:38 MB Result MB Qualifier MB RDL Analyte mg/l mg/l Tetrachloroethene ND 0.00100 1,1,1-Trichloroethane ND 0.00100 1,1,2-Trichloroethane ND 0.00100 Trichloroethene ND 0.00100 Trichlorofluoromethane ND 0.00500 1,2,3-Trichloropropane ND 0.00250 Xylenes, Total ND 0.00300 Vinyl acetate ND 0.0100 Vinyl chloride ND 0.00100 (S) Toluene-d8 100 90.0-115 (S) Dibromofluoromethane 98.4 79.0-121 (S) a,a,a-Trifluorotoluene 106 90.4-116 (S) 4-Bromofluorobenzene 109 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 12/01/15 05:21 • (LCSD) 12/01/15 05:40 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Acetone 0.125 0.135 0.140 108 112 28.7-175 3.72 20.9 Benzene 0.0250 0.0230 0.0230 92.0 92.1 73.0-122 0.100 20 Acrylonitrile 0.125 0.107 0.111 85.4 88.8 58.2-145 3.85 20 Bromodichloromethane 0.0250 0.0269 0.0268 108 107 75.5-121 0.340 20 Bromochloromethane 0.0250 0.0267 0.0269 107 108 78.9-123 0.880 20 Bromoform 0.0250 0.0266 0.0275 107 110 71.5-131 3.12 20 Bromomethane 0.0250 0.0404 0.0381 162 153 22.4-187 5.75 20 Carbon disulfide 0.0250 0.0234 0.0232 93.6 92.8 53.0-134 0.820 20 Carbon tetrachloride 0.0250 0.0272 0.0262 109 105 70.9-129 3.67 20 Chlorobenzene 0.0250 0.0259 0.0259 104 104 79.7-122 0.0100 20 Chlorodibromomethane 0.0250 0.0288 0.0285 115 114 78.2-124 1.11 20 Chloroethane 0.0250 0.0364 0.0372 146 149 41.2-153 2.22 20 Chloroform 0.0250 0.0262 0.0260 105 104 73.2-125 0.540 20 Chloromethane 0.0250 0.0215 0.0212 85.9 84.8 55.8-134 1.26 20 Dibromomethane 0.0250 0.0266 0.0265 106 106 79.5-118 0.370 20 1,2-Dichlorobenzene 0.0250 0.0256 0.0253 102 101 84.7-118 0.930 20 1,4-Dichlorobenzene 0.0250 0.0244 0.0244 97.7 97.4 82.2-114 0.230 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 93 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 93 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG832427 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-29 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 12/01/15 05:21 • (LCSD) 12/01/15 05:40 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% trans-1,4-Dichloro-2-butene 0.0250 0.0297 0.0290 119 116 58.3-129 2.35 20 1,1-Dichloroethane 0.0250 0.0241 0.0241 96.3 96.6 71.7-127 0.270 20 1,2-Dichloroethane 0.0250 0.0291 0.0292 116 117 65.3-126 0.170 20 1,1-Dichloroethene 0.0250 0.0263 0.0267 105 107 59.9-137 1.54 20 cis-1,2-Dichloroethene 0.0250 0.0243 0.0249 97.0 99.8 77.3-122 2.78 20 trans-1,2-Dichloroethene 0.0250 0.0245 0.0248 97.8 99.4 72.6-125 1.56 20 1,2-Dichloropropane 0.0250 0.0231 0.0232 92.2 92.9 77.4-125 0.730 20 cis-1,3-Dichloropropene 0.0250 0.0262 0.0262 105 105 77.7-124 0.0700 20 trans-1,3-Dichloropropene 0.0250 0.0271 0.0275 109 110 73.5-127 1.37 20 Ethylbenzene 0.0250 0.0264 0.0258 106 103 80.9-121 2.48 20 2-Hexanone 0.125 0.132 0.136 106 109 59.4-151 2.60 20 Iodomethane 0.125 0.148 0.140 119 112 64.6-137 5.86 20 2-Butanone (MEK)0.125 0.124 0.128 98.9 102 46.4-155 3.35 20 Methylene Chloride 0.0250 0.0226 0.0228 90.4 91.4 69.5-120 1.10 20 4-Methyl-2-pentanone (MIBK)0.125 0.117 0.120 93.7 95.9 63.3-138 2.38 20 Styrene 0.0250 0.0266 0.0264 106 106 79.9-124 0.620 20 1,1,1,2-Tetrachloroethane 0.0250 0.0278 0.0279 111 112 78.5-125 0.570 20 1,1,2,2-Tetrachloroethane 0.0250 0.0256 0.0255 102 102 79.3-123 0.250 20 Tetrachloroethene 0.0250 0.0272 0.0268 109 107 73.5-130 1.53 20 Toluene 0.0250 0.0251 0.0248 100 99.3 77.9-116 1.00 20 1,1,1-Trichloroethane 0.0250 0.0285 0.0282 114 113 71.1-129 1.20 20 1,1,2-Trichloroethane 0.0250 0.0258 0.0264 103 106 81.6-120 2.21 20 Trichloroethene 0.0250 0.0265 0.0265 106 106 79.5-121 0.0400 20 Trichlorofluoromethane 0.0250 0.0316 0.0314 126 126 49.1-157 0.420 20 1,2,3-Trichloropropane 0.0250 0.0264 0.0270 106 108 74.9-124 2.40 20 Vinyl acetate 0.125 0.122 0.126 97.7 101 41.7-159 3.19 20 Xylenes, Total 0.0750 0.0765 0.0758 102 101 79.2-122 0.910 20 Vinyl chloride 0.0250 0.0260 0.0260 104 104 61.5-134 0.120 20 (S) Toluene-d8 100 100 90.0-115 (S) Dibromofluoromethane 101 102 79.0-121 (S) a,a,a-Trifluorotoluene 103 104 90.4-116 (S) 4-Bromofluorobenzene 106 105 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 94 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 94 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG832427 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-29 L803079-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 12/01/15 11:39 • (MS) 12/01/15 09:05 • (MSD) 12/01/15 09:24 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Acetone 0.125 0.000763 0.0664 0.0658 52.5 52.0 1 25.0-156 1.01 21.5 Acrylonitrile 0.125 ND 0.109 0.105 86.8 84.0 1 55.9-161 3.31 20 Benzene 0.0250 ND 0.0221 0.0210 88.2 83.8 1 58.6-133 5.09 20 Bromodichloromethane 0.0250 ND 0.0262 0.0249 105 99.7 1 69.2-127 5.03 20 Bromochloromethane 0.0250 ND 0.0260 0.0247 104 98.7 1 74.4-128 5.09 20 Bromoform 0.0250 ND 0.0273 0.0258 109 103 1 66.3-140 5.35 20 Bromomethane 0.0250 ND 0.0428 0.0361 171 144 1 16.6-183 17.1 20.5 Carbon disulfide 0.0250 ND 0.0219 0.0212 87.8 84.7 1 34.9-138 3.54 20 Carbon tetrachloride 0.0250 ND 0.0258 0.0241 103 96.3 1 60.6-139 6.87 20 Chlorobenzene 0.0250 ND 0.0251 0.0239 100 95.7 1 70.1-130 4.80 20 Chlorodibromomethane 0.0250 ND 0.0279 0.0267 112 107 1 71.6-132 4.58 20 Chloroethane 0.0250 ND 0.0364 0.0340 146 136 1 33.3-155 6.77 20 Chloroform 0.0250 ND 0.0253 0.0242 101 96.8 1 66.1-133 4.56 20 Chloromethane 0.0250 ND 0.0203 0.0194 81.3 77.7 1 40.7-139 4.57 20 Dibromomethane 0.0250 ND 0.0255 0.0249 102 99.6 1 72.8-127 2.26 20 1,2-Dichlorobenzene 0.0250 ND 0.0240 0.0234 96.1 93.4 1 77.4-127 2.81 20 1,4-Dichlorobenzene 0.0250 ND 0.0234 0.0228 93.7 91.2 1 74.4-123 2.70 20 trans-1,4-Dichloro-2-butene 0.0250 ND 0.0297 0.0294 119 117 1 57.6-136 1.01 20 1,1-Dichloroethane 0.0250 ND 0.0235 0.0222 93.8 88.8 1 64.0-134 5.49 20 1,2-Dichloroethane 0.0250 ND 0.0290 0.0272 116 109 1 60.7-132 6.43 20 1,1-Dichloroethene 0.0250 ND 0.0259 0.0244 104 97.5 1 48.8-144 5.99 20 cis-1,2-Dichloroethene 0.0250 ND 0.0241 0.0224 96.5 89.6 1 60.6-136 7.35 20 trans-1,2-Dichloroethene 0.0250 ND 0.0238 0.0224 95.1 89.6 1 61.0-132 5.93 20 1,2-Dichloropropane 0.0250 ND 0.0222 0.0211 88.7 84.6 1 69.7-130 4.77 20 cis-1,3-Dichloropropene 0.0250 ND 0.0253 0.0239 101 95.7 1 71.1-129 5.45 20 trans-1,3-Dichloropropene 0.0250 ND 0.0262 0.0250 105 100 1 66.3-136 4.56 20 Ethylbenzene 0.0250 ND 0.0254 0.0240 101 96.1 1 62.7-136 5.35 20 2-Hexanone 0.125 ND 0.104 0.103 83.1 82.6 1 59.4-154 0.600 20.1 Iodomethane 0.125 ND 0.129 0.126 103 101 1 55.2-140 2.58 20 2-Butanone (MEK)0.125 ND 0.0912 0.0901 73.0 72.1 1 45.0-156 1.26 20.8 Methylene Chloride 0.0250 ND 0.0219 0.0207 87.7 82.6 1 61.5-125 6.00 20 4-Methyl-2-pentanone (MIBK)0.125 ND 0.116 0.112 92.8 89.4 1 60.7-150 3.74 20 Styrene 0.0250 ND 0.0254 0.0244 102 97.8 1 68.2-133 3.94 20 1,1,1,2-Tetrachloroethane 0.0250 ND 0.0276 0.0261 110 104 1 70.5-132 5.54 20 1,1,2,2-Tetrachloroethane 0.0250 ND 0.0259 0.0246 103 98.5 1 64.9-145 4.86 20 Tetrachloroethene 0.0250 ND 0.0265 0.0248 106 99.2 1 57.4-141 6.57 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 95 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 95 of 101 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG832427 Volatile Organic Compounds (GC/MS) by Method 8260B L801958-29 L803079-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 12/01/15 11:39 • (MS) 12/01/15 09:05 • (MSD) 12/01/15 09:24 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Toluene 0.0250 ND 0.0244 0.0227 97.6 91.0 1 67.8-124 7.07 20 1,1,1-Trichloroethane 0.0250 ND 0.0278 0.0258 111 103 1 58.7-134 7.37 20 1,1,2-Trichloroethane 0.0250 ND 0.0257 0.0245 103 98.1 1 74.1-130 4.55 20 Trichloroethene 0.0250 ND 0.0250 0.0239 99.9 95.7 1 48.9-148 4.32 20 Trichlorofluoromethane 0.0250 ND 0.0313 0.0289 125 116 1 39.9-165 7.98 20 1,2,3-Trichloropropane 0.0250 ND 0.0265 0.0253 106 101 1 71.5-134 4.37 20 Vinyl acetate 0.125 ND 0.129 0.123 104 98.2 1 42.8-181 5.27 20 Xylenes, Total 0.0750 ND 0.0744 0.0700 99.3 93.3 1 65.6-133 6.15 20 Vinyl chloride 0.0250 ND 0.0249 0.0237 99.4 94.9 1 44.3-143 4.60 20 (S) Toluene-d8 102 102 90.0-115 (S) Dibromofluoromethane 102 103 79.0-121 (S) a,a,a-Trifluorotoluene 103 102 90.4-116 (S) 4-Bromofluorobenzene 108 108 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 96 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 96 of 101 ONE LAB. NATIONWIDE.GLOSSARY OF TERMS Abbreviations and Definitions SDG Sample Delivery Group. MDL Method Detection Limit. RDL Reported Detection Limit. ND,U Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. (dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. (S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. Rec.Recovery. SDL Sample Detection Limit. MQL Method Quantitation Limit. Unadj. MQL Unadjusted Method Quantitation Limit. Qualifier Description J2 Surrogate recovery limits have been exceeded; values are outside lower control limits. J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 97 of 101 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 97 of 101 ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/01/15 20:38 98 of 101 Our Locations Alabama 40660 Alaska UST-080 Arizona AZ0612 Arkansas 88-0469 California 01157CA Colorado TN00003 Conneticut PH-0197 Florida E87487 Georgia NELAP Georgia 1 923 Idaho TN00003 Illinois 200008 Indiana C-TN-01 Iowa 364 Kansas E-10277 Kentucky 1 90010 Kentucky 2 16 Louisiana AI30792 Maine TN0002 Maryland 324 Massachusetts M-TN003 Michigan 9958 Minnesota 047-999-395 Mississippi TN00003 Missouri 340 Montana CERT0086 Nebraska NE-OS-15-05 Nevada TN-03-2002-34 New Hampshire 2975 New Jersey–NELAP TN002 New Mexico TN00003 New York 11742 North Carolina Env375 North Carolina 1 DW21704 North Carolina 2 41 North Dakota R-140 Ohio–VAP CL0069 Oklahoma 9915 Oregon TN200002 Pennsylvania 68-02979 Rhode Island 221 South Carolina 84004 South Dakota n/a Tennessee 1 4 2006 Texas T 104704245-07-TX Texas 5 LAB0152 Utah 6157585858 Vermont VT2006 Virginia 109 Washington C1915 West Virginia 233 Wisconsin 9980939910 Wyoming A2LA A2LA – ISO 17025 1461.01 Canada 1461.01 EPA–Crypto TN00003 AIHA 100789 DOD 1461.01 USDA S-67674 State Accreditations Third Party & Federal Accreditations ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. 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Mold n/a Accreditation not applicable 1461.02A2LA – ISO 170255 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Hunt Environmental Associates 14-011550 L801958 12/02/15 12:56 98 of 101 APPENDIX B: TIME SERIES GRAPHS Page 1 1,4-Dichlorobenzene Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 5 10 15 20 25 30 MW-9A MW-5 MW-14 MW-13R MW-15 5/ 6 / 1 9 9 4 6/ 2 / 1 9 9 7 6/ 3 0 / 2 0 0 0 7/ 2 9 / 2 0 0 3 8/ 2 5 / 2 0 0 6 9/ 2 2 / 2 0 0 9 10 / 2 0 / 2 0 1 2 11 / 1 8 / 2 0 1 5 Page 1 Arsenic Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 5 10 15 20 25 30 MW-11 MW-16 9/ 2 1 / 1 9 9 4 9/ 2 8 / 1 9 9 7 10 / 6 / 2 0 0 0 10 / 1 5 / 2 0 0 3 10 / 2 3 / 2 0 0 6 10 / 3 1 / 2 0 0 9 11 / 8 / 2 0 1 2 11 / 1 7 / 2 0 1 5 Page 1 Benzene Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 1 2 3 4 5 MW-13R MW-15 1/ 1 5 / 1 9 9 8 8/ 2 / 2 0 0 0 2/ 1 9 / 2 0 0 3 9/ 7 / 2 0 0 5 3/ 2 5 / 2 0 0 8 10 / 1 2 / 2 0 1 0 4/ 3 0 / 2 0 1 3 11 / 1 7 / 2 0 1 5 Page 1 Cadmium Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 5 10 15 20 25 30 MW-11 9/ 2 1 / 1 9 9 4 9/ 2 8 / 1 9 9 7 10 / 6 / 2 0 0 0 10 / 1 5 / 2 0 0 3 10 / 2 3 / 2 0 0 6 10 / 3 1 / 2 0 0 9 11 / 8 / 2 0 1 2 11 / 1 7 / 2 0 1 5 Page 1 Chlorobenzene Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 0.5 1 1.5 2 2.5 3 3.5 4 MW-15 3/ 2 8 / 2 0 1 3 8/ 1 2 / 2 0 1 3 12 / 2 8 / 2 0 1 3 5/ 1 5 / 2 0 1 4 9/ 2 9 / 2 0 1 4 2/ 1 4 / 2 0 1 5 7/ 2 / 2 0 1 5 11 / 1 7 / 2 0 1 5 Page 1 Chromium Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( ) 0 5 10 15 20 25 30 MW-25R MW-26 4/ 8 / 2 0 1 5 5/ 9 / 2 0 1 5 6/ 1 0 / 2 0 1 5 7/ 1 2 / 2 0 1 5 8/ 1 3 / 2 0 1 5 9/ 1 4 / 2 0 1 5 10 / 1 6 / 2 0 1 5 11 / 1 7 / 2 0 1 5 Page 1 Copper Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 50 100 150 200 MW-11 MW-17R 9/ 2 1 / 1 9 9 4 9/ 2 8 / 1 9 9 7 10 / 6 / 2 0 0 0 10 / 1 5 / 2 0 0 3 10 / 2 3 / 2 0 0 6 10 / 3 1 / 2 0 0 9 11 / 8 / 2 0 1 2 11 / 1 7 / 2 0 1 5 Page 1 Lead Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 10 20 30 40 50 60 70 80 90 100 MW-10 MW-8 MW-11 MW-17R 5/ 6 / 1 9 9 4 6/ 2 / 1 9 9 7 6/ 3 0 / 2 0 0 0 7/ 2 8 / 2 0 0 3 8/ 2 5 / 2 0 0 6 9/ 2 1 / 2 0 0 9 10 / 1 9 / 2 0 1 2 11 / 1 7 / 2 0 1 5 Page 1 Selenium Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 10 20 30 40 50 60 70 80 90 100 MW-3R 5/ 2 3 / 2 0 0 2 4/ 2 5 / 2 0 0 4 3/ 3 0 / 2 0 0 6 3/ 3 / 2 0 0 8 2/ 4 / 2 0 1 0 1/ 9 / 2 0 1 2 12 / 1 3 / 2 0 1 3 11 / 1 7 / 2 0 1 5 Page 1 Vanadium Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 10 20 30 40 50 MW-26 11 / 2 0 / 2 0 0 9 9/ 2 8 / 2 0 1 0 8/ 7 / 2 0 1 1 6/ 1 4 / 2 0 1 2 4/ 2 3 / 2 0 1 3 3/ 1 / 2 0 1 4 1/ 8 / 2 0 1 5 11 / 1 7 / 2 0 1 5 Page 1 Zinc Multi-Well Time-Series Graph Sample Date Co n c e n t r a t i o n ( p p b ) 0 100 200 300 400 500 600 MW-11 9/ 2 1 / 1 9 9 4 9/ 2 8 / 1 9 9 7 10 / 6 / 2 0 0 0 10 / 1 5 / 2 0 0 3 10 / 2 3 / 2 0 0 6 10 / 3 1 / 2 0 0 9 11 / 8 / 2 0 1 2 11 / 1 7 / 2 0 1 5 APPENDIX C: NON-PARAMETRIC PREDICTION INTERVAL INTER-WELL COMPARISONS Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: 1,4-Dichlorobenzene Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 61.5863% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 99 Maximum Background Value = 5 Confidence Level = 92.5% False Positive Rate = 7.5% Location Date Count Mean Significant MW-10 11/17/2015 1 0.274 FALSE MW-2 3/24/2000 1 5 FALSE MW-7 3/24/2000 1 5 FALSE MW-8 11/17/2015 1 0.274 FALSE MW-9A 11/18/2015 1 7.43 TRUE MW-11 11/17/2015 1 0.274 FALSE MW-5 11/18/2015 1 5.01 TRUE MW-16 11/17/2015 1 0.274 FALSE MW-18 11/17/2015 1 0.274 FALSE MW-14 11/17/2015 1 2.35 FALSE MW-13R 11/17/2015 1 1.35 FALSE MW-17R 11/17/2015 1 0.274 FALSE MW-5A 10/21/2011 1 0.39 FALSE MW-3R 11/17/2015 1 0.274 FALSE MW-22 11/17/2015 1 0.274 FALSE MW-23 11/17/2015 1 0.274 FALSE MW-24 10/1/2013 1 0.39 FALSE MW-26 11/17/2015 1 0.274 FALSE MW-25R 11/17/2015 1 0.274 FALSE MW-15 11/17/2015 1 8.43 TRUE Page 2 MW-24R 11/17/2015 1 0.274 FALSE MW-21R 11/17/2015 1 0.274 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Arsenic Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 55.296% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 101 Maximum Background Value = 10 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 11/17/2015 1 4.36 FALSE MW-2 3/24/2000 1 35 TRUE MW-7 3/24/2000 1 10 FALSE MW-8 11/17/2015 1 5.51 FALSE MW-9A 11/18/2015 1 0.25 FALSE MW-11 11/17/2015 1 11.5 TRUE MW-5 11/18/2015 1 2.64 FALSE MW-16 11/17/2015 1 13.7 TRUE MW-18 11/17/2015 1 0.25 FALSE MW-14 11/17/2015 1 0.25 FALSE MW-13R 11/17/2015 1 0.25 FALSE MW-17R 11/17/2015 1 3.67 FALSE MW-5A 3/19/2012 1 0 FALSE MW-3R 11/17/2015 1 3.37 FALSE MW-22 11/17/2015 1 0.25 FALSE MW-23 11/17/2015 1 0.25 FALSE MW-24 10/1/2013 1 0.41 FALSE MW-26 11/17/2015 1 0.25 FALSE MW-25R 11/17/2015 1 4.69 FALSE MW-15 11/17/2015 1 0.25 FALSE Page 2 MW-24R 11/17/2015 1 0.25 FALSE MW-21R 11/17/2015 1 5.28 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Benzene Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 63.5938% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 99 Maximum Background Value = 5 Confidence Level = 92.5% False Positive Rate = 7.5% Location Date Count Mean Significant MW-10 11/17/2015 1 0.331 FALSE MW-2 3/24/2000 1 5 FALSE MW-7 3/24/2000 1 5 FALSE MW-8 11/17/2015 1 0.331 FALSE MW-9A 11/18/2015 1 0.331 FALSE MW-11 11/17/2015 1 0.331 FALSE MW-5 11/18/2015 1 0.331 FALSE MW-16 11/17/2015 1 0.331 FALSE MW-18 11/17/2015 1 0.331 FALSE MW-14 11/17/2015 1 0.331 FALSE MW-13R 11/17/2015 1 2.17 FALSE MW-17R 11/17/2015 1 0.331 FALSE MW-5A 10/21/2011 1 0.24 FALSE MW-3R 11/17/2015 1 0.331 FALSE MW-22 11/17/2015 1 0.331 FALSE MW-23 11/17/2015 1 0.331 FALSE MW-24 10/1/2013 1 0.24 FALSE MW-26 11/17/2015 1 0.331 FALSE MW-25R 11/17/2015 1 0.331 FALSE MW-15 11/17/2015 1 1.56 FALSE Page 2 MW-24R 11/17/2015 1 0.331 FALSE MW-21R 11/17/2015 1 0.331 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Cadmium Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 51.7941% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 101 Maximum Background Value = 6 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 11/17/2015 1 0.16 FALSE MW-2 3/24/2000 1 18 TRUE MW-7 3/24/2000 1 1 FALSE MW-8 11/17/2015 1 0.16 FALSE MW-9A 11/18/2015 1 0.16 FALSE MW-11 11/17/2015 1 4.43 FALSE MW-5 11/18/2015 1 0.16 FALSE MW-16 11/17/2015 1 0.16 FALSE MW-18 11/17/2015 1 0.16 FALSE MW-14 11/17/2015 1 0.16 FALSE MW-13R 11/17/2015 1 0.16 FALSE MW-17R 11/17/2015 1 0.16 FALSE MW-5A 3/19/2012 1 0 FALSE MW-3R 11/17/2015 1 0.16 FALSE MW-22 11/17/2015 1 0.16 FALSE MW-23 11/17/2015 1 0.16 FALSE MW-24 10/1/2013 1 0.05 FALSE MW-26 11/17/2015 1 0.16 FALSE MW-25R 11/17/2015 1 0.16 FALSE MW-15 11/17/2015 1 0.16 FALSE Page 2 MW-24R 11/17/2015 1 0.16 FALSE MW-21R 11/17/2015 1 0.16 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Chlorobenzene Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 65.1969% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 99 Maximum Background Value = 5 Confidence Level = 92.5% False Positive Rate = 7.5% Location Date Count Mean Significant MW-10 11/17/2015 1 0.348 FALSE MW-2 3/24/2000 1 6 TRUE MW-7 3/24/2000 1 5 FALSE MW-8 11/17/2015 1 0.348 FALSE MW-9A 11/18/2015 1 1.47 FALSE MW-11 11/17/2015 1 0.348 FALSE MW-5 11/18/2015 1 1.53 FALSE MW-16 11/17/2015 1 0.348 FALSE MW-18 11/17/2015 1 0.348 FALSE MW-14 11/17/2015 1 0.348 FALSE MW-13R 11/17/2015 1 0.348 FALSE MW-17R 11/17/2015 1 0.348 FALSE MW-5A 10/21/2011 1 0.3 FALSE MW-3R 11/17/2015 1 0.348 FALSE MW-22 11/17/2015 1 0.348 FALSE MW-23 11/17/2015 1 0.348 FALSE MW-24 10/1/2013 1 0.3 FALSE MW-26 11/17/2015 1 0.348 FALSE MW-25R 11/17/2015 1 0.348 FALSE MW-15 11/17/2015 1 3.02 FALSE Page 2 MW-24R 11/17/2015 1 0.348 FALSE MW-21R 11/17/2015 1 0.348 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Chromium Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 0% Number of comparisons = 18 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 4 Maximum Background Value = 8.35 Confidence Level = 33.3% False Positive Rate = 66.7% Location Date Count Mean Significant MW-3R 11/17/2015 1 12.5 TRUE MW-5 11/18/2015 1 0.54 FALSE MW-8 11/17/2015 1 2.03 FALSE MW-9A 11/18/2015 1 0.54 FALSE MW-10 11/17/2015 1 18.1 TRUE MW-11 11/17/2015 1 33.8 TRUE MW-13R 11/17/2015 1 2.24 FALSE MW-14 11/17/2015 1 0.54 FALSE MW-15 11/17/2015 1 0.54 FALSE MW-16 11/17/2015 1 2.28 FALSE MW-17R 11/17/2015 1 16.2 TRUE MW-18 11/17/2015 1 6.48 FALSE MW-21R 11/17/2015 1 3.57 FALSE MW-22 11/17/2015 1 0.54 FALSE MW-23 11/17/2015 1 0.54 FALSE MW-24R 11/17/2015 1 8.45 TRUE MW-25R 11/17/2015 1 11.8 TRUE MW-26 11/17/2015 1 25.3 TRUE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Copper Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 53.7291% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 104 Maximum Background Value = 200 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 11/17/2015 1 6.51 FALSE MW-2 3/24/2000 1 200 FALSE MW-7 3/24/2000 1 200 FALSE MW-8 11/17/2015 1 0.52 FALSE MW-9A 11/18/2015 1 0.52 FALSE MW-11 11/17/2015 1 44.3 FALSE MW-5 11/18/2015 1 0.52 FALSE MW-16 11/17/2015 1 0.52 FALSE MW-18 11/17/2015 1 0.52 FALSE MW-14 11/17/2015 1 0.52 FALSE MW-13R 11/17/2015 1 0.52 FALSE MW-17R 11/17/2015 1 10.2 FALSE MW-5A 3/19/2012 1 0 FALSE MW-3R 11/17/2015 1 0.52 FALSE MW-22 11/17/2015 1 0.52 FALSE MW-23 11/17/2015 1 0.52 FALSE MW-24 10/1/2013 1 4.5 FALSE MW-26 11/17/2015 1 7.64 FALSE MW-25R 11/17/2015 1 8.57 FALSE MW-15 11/17/2015 1 0.52 FALSE Page 2 MW-24R 11/17/2015 1 0.52 FALSE MW-21R 11/17/2015 1 5.88 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Lead Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 47.9688% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 101 Maximum Background Value = 41 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 11/17/2015 1 16.7 FALSE MW-2 3/24/2000 1 20 FALSE MW-7 3/24/2000 1 10 FALSE MW-8 11/17/2015 1 32.1 FALSE MW-9A 11/18/2015 1 0.24 FALSE MW-11 11/17/2015 1 35.2 FALSE MW-5 11/18/2015 1 0.24 FALSE MW-16 11/17/2015 1 0.24 FALSE MW-18 11/17/2015 1 7.24 FALSE MW-14 11/17/2015 1 2.02 FALSE MW-13R 11/17/2015 1 6.79 FALSE MW-17R 11/17/2015 1 16.7 FALSE MW-5A 3/19/2012 1 0 FALSE MW-3R 11/17/2015 1 9.76 FALSE MW-22 11/17/2015 1 0.24 FALSE MW-23 11/17/2015 1 0.24 FALSE MW-24 10/1/2013 1 1.1 FALSE MW-26 11/17/2015 1 8.96 FALSE MW-25R 11/17/2015 1 3.92 FALSE MW-15 11/17/2015 1 0.24 FALSE Page 2 MW-24R 11/17/2015 1 8.81 FALSE MW-21R 11/17/2015 1 3.14 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Selenium Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 58.4759% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 101 Maximum Background Value = 20 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 11/17/2015 1 0.38 FALSE MW-2 3/24/2000 1 20 FALSE MW-7 3/24/2000 1 20 FALSE MW-8 11/17/2015 1 0.38 FALSE MW-9A 11/18/2015 1 0.38 FALSE MW-11 11/17/2015 1 0.38 FALSE MW-5 11/18/2015 1 0.38 FALSE MW-16 11/17/2015 1 0.38 FALSE MW-18 11/17/2015 1 0.38 FALSE MW-14 11/17/2015 1 0.38 FALSE MW-13R 11/17/2015 1 0.38 FALSE MW-17R 11/17/2015 1 0.38 FALSE MW-5A 3/19/2012 1 0 FALSE MW-3R 11/17/2015 1 15.2 FALSE MW-22 11/17/2015 1 0.38 FALSE MW-23 11/17/2015 1 0.38 FALSE MW-24 10/1/2013 1 0.18 FALSE MW-26 11/17/2015 1 0.38 FALSE MW-25R 11/17/2015 1 0.38 FALSE MW-15 11/17/2015 1 0.38 FALSE Page 2 MW-24R 11/17/2015 1 0.38 FALSE MW-21R 11/17/2015 1 0.38 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Vanadium Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 50.234% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 101 Maximum Background Value = 210 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 11/17/2015 1 34.8 FALSE MW-2 3/24/2000 1 40 FALSE MW-7 3/24/2000 1 40 FALSE MW-8 11/17/2015 1 7.57 FALSE MW-9A 11/18/2015 1 0.18 FALSE MW-11 11/17/2015 1 66.7 FALSE MW-5 11/18/2015 1 0.18 FALSE MW-16 11/17/2015 1 0.18 FALSE MW-18 11/17/2015 1 13.8 FALSE MW-14 11/17/2015 1 0.18 FALSE MW-13R 11/17/2015 1 0.18 FALSE MW-17R 11/17/2015 1 39.6 FALSE MW-5A 3/19/2012 1 0 FALSE MW-3R 11/17/2015 1 30.2 FALSE MW-22 11/17/2015 1 0.18 FALSE MW-23 11/17/2015 1 0.18 FALSE MW-24 10/1/2013 1 0.91 FALSE MW-26 11/17/2015 1 45.9 FALSE MW-25R 11/17/2015 1 19.1 FALSE MW-15 11/17/2015 1 0.18 FALSE Page 2 MW-24R 11/17/2015 1 14.2 FALSE MW-21R 11/17/2015 1 0.18 FALSE Page 1 Non-Parametric Prediction Interval Inter-Well Comparison Parameter: Zinc Original Data (Not Transformed) Non-Detects Replaced with Detection Limit Total Percent Non-Detects = 43.5508% Number of comparisons = 22 Future Samples (k) = 8 Recent Dates = 1 Background Measurements (n) = 103 Maximum Background Value = 260 Confidence Level = 92.6% False Positive Rate = 7.4% Location Date Count Mean Significant MW-10 11/17/2015 1 2.56 FALSE MW-2 3/24/2000 1 50 FALSE MW-7 3/24/2000 1 50 FALSE MW-8 11/17/2015 1 2.56 FALSE MW-9A 11/18/2015 1 2.56 FALSE MW-11 11/17/2015 1 221 FALSE MW-5 11/18/2015 1 2.56 FALSE MW-16 11/17/2015 1 2.56 FALSE MW-18 11/17/2015 1 2.56 FALSE MW-14 11/17/2015 1 2.56 FALSE MW-13R 11/17/2015 1 2.56 FALSE MW-17R 11/17/2015 1 2.56 FALSE MW-5A 3/19/2012 1 0 FALSE MW-3R 11/17/2015 1 2.56 FALSE MW-22 11/17/2015 1 2.56 FALSE MW-23 11/17/2015 1 2.56 FALSE MW-24 10/1/2013 1 2.4 FALSE MW-26 11/17/2015 1 2.56 FALSE MW-25R 11/17/2015 1 2.56 FALSE MW-15 11/17/2015 1 2.56 FALSE Page 2 MW-24R 11/17/2015 1 2.56 FALSE MW-21R 11/17/2015 1 2.56 FALSE