The URL can be used to link to this page

Home My WebLink About6301_MooreCoCDLF_GWMR_DIN27991_20160412Page 120 of 137 Page 121 of 137 Page 122 of 137 Page 123 of 137 Page 124 of 137 Page 125 of 137 Page 126 of 137 Page 127 of 137 Page 128 of 137 Page 129 of 137 Page 130 of 137 Page 131 of 137 Page 132 of 137 Page 133 of 137 Page 134 of 137 Page 135 of 137 Page 136 of 137 Page 137 of 137 GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 1 of 4 Project Name: Moore County Landfill - MNA wells Project Reference Number: 073-9615015.100 Sampling Event Date: April 11-12, 2016 Review Date: August 30, 2016 Initials: TM Report #: CZ05222, CZ04434 Person(s) performing the review are to initial each item on this form as acknowledgement of data acceptance, or as acknowledgement of a review issue. In the case of the latter, a brief explanation should follow the applicable item. Golder Associates Inc. has reviewed the laboratory certificates of analysis, chain-of-custody form, and laboratory provided sample group quality assurance and quality control data for the above referenced sample group to identify potential bias or inaccuracy, in general accordance with the following United States Environmental Protection Agency documents: • Region III Modifications to Functional Guidelines for Organic Data Review Multi-Media, Multi-Concentration, September 1994; • Region III Modifications to the Laboratory Data Validation Functional Guidelines for Evaluating Inorganic Analyses, April 1993; and • Laboratory Data Validation Functional Guidelines for Evaluating Inorganic Analyses, July 1998. COMPLIANCE ANALYTE LIST(S) (check all that apply) NC Closed Facility/C & D List X NC Appendix I NC Appendix I + Detects NC Appendix II NC Subtitle D Leachate List Other: RCRA Metals & MNA parameters 1.0 CHAIN OF CUSTODY (COC) REVIEW TM COC was properly signed by all parties. TM Correct project name and number are on the form. TM Sample receipt condition at laboratory was acceptable. TM Each sample and blank submitted for analysis appears in the report. 2.0 SAMPLE HOLDING TIMES TM Holding times for extraction and/or analysis were met for each analytical Method (see below for reference). Review Criteria GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 2 of 4 Method Analytes Holding Time SW-846 Method 8260 and 8011 VOCs 14 days SW-846 Methods 8270, 8080, 8081, 8082, and 8151 SVOCs, PCBs, pesticides and herbicides 7 days for extraction, 40 days from extraction for analysis SW-846 Methods 6000 and 7000 Series Metals except mercury 6 months (no temperature requirements) SW-846 Method 7470 Mercury 28 days SM18 4500-S2 D Sulfide 7 days SW-846 Method 9010 Cyanide 14 days EPA Method 300 Nitrate/Sulfate 48 hours/28 days EPA Method 405.1 BOD 48 hours EPA Method 410.4 COD 28 days EPA Method 365.4 Phosphorous 28 days 3.0 LABORATORY QUALITY CONTROL REVIEW TM Laboratory analyzed at least one internal blank for each method, where applicable. TM Laboratory blank is interference-free. TM Surrogate recoveries are provided for each analytical method, where applicable. TM Surrogate recoveries for each method are within the acceptable limits (i.e., at least 50% of the surrogates were within range). TM MS/MSD/LCS data results are provided for each analytical method. TM MS/MSD/LCS recoveries for each method are within the acceptable limits (i.e., at least 1 of the 3 were within range). • The spike recoveries of Alkalinity, Nitrate/Nitrite (NOx), Nitrite, Sulfate, Sulfide, and TOC were outside of control limits for the MS and/or MSD samples, and precision between duplicate spikes of Sulfide exceeded acceptance criteria for the MS and MSD samples. The QC batches were approved based on acceptable LCS recovery of these analytes. 4.0 ANALYTE LISTS/METHODS TM The proper number of constituents are present for each analyte list as identified above (including detects where applicable). TM Proper EPA SW-846 analytical methods were used for analysis. 5.0 DATA REPORTING TM All analytical reporting associated with the event was performed by the contracted lab. TM Trip, field and/or equipment, and laboratory blank results have all been reported. All detects for blanks are listed below by constituent. All laboratory method blanks, if any, have been ‘flagged’ with a ‘B’ where detected in other samples as appropriate and a laboratory narrative was provided. If the sample was flagged by the laboratory and is not within 5X of the concentration in the blank (or 10X for commonly detected GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 3 of 4 laboratory contaminants-acetone, methylene chloride and phthalates), list below with explanation if flags should be removed. If flags need to be added for samples, also list below. TM It is clear from the laboratory report that samples have or have not been diluted during analysis, and if the samples have been diluted, the result is reported as a multiple of the dilution (e.g., a sample diluted 10x resulting in an analytical detection of 1.0 should be reported as 10). Those that have been diluted are listed below with the dilution factor. • Alkalinity o MW-9 (10x) o MW-11S (5x) o MW-16S (5x) • Nitrate/Nitrite as N o MW-4 (5x) • Sulfate o MW-15 (4x) o MW-16S (2x) • Methane o MW-4 (5x) o MW-6 (50x) o MW-7 (50x) o MW-9 (21x) o MW-11S (21x) o MW-14 (21x) o MW-15 (21x) o MW-16S (5x) TM The report provides the reporting limit for each constituent. TM The results were reported at or below their proper reporting limits (e.g., NC Solid Waste Section RLs). Those that are not reported correctly are listed below (by constituent) with the proper reporting limit listed beside them. State if the reporting limit error is due to dilutions. TM No inorganic or organic constituents were reported above their respective NC 2L Drinking Water Standards or Groundwater Protection Standards in wells, surface points, or field/equipment/trip blanks. • Arsenic (NC 2L = 10 ug/L) o MW-6 @ 12.6 ug/L o MW-7 @ 27.0 ug/L o MW-9 @ 38.7 ug/L o MW-15 @ 29.6 o MW-16s @ 12.9 • Benzene (NC 2L = 1 ug/L) o MW-6 @ 2.0 ug/L o MW-9 @ 3.8 ug/L o MW-11S @ 1.8 ug/L o MW-14 @ 2.2 o MW-15 @ 2.8 ug/L o MW-16S @ 1.0 ug/L • Vinyl Chloride (NC 2L = 0.03 ug/L) o MW-6 @ 0.72 ug/L (J) o MW-7 @ 0.71 ug/L (J) o MW-9 @ 0.42 ug/L (J) o MW-11S @ 2.8 ug/L o MW-14 @ 3.3 ug/L o MW-16s @ 1.2 ug/L TM No quantifiable inorganic or organic constituents were detected in a well or surface water point at concentrations outside of their historical range (more than 5X previous concentrations or first-time detections). TM Other report issues/Communications with laboratory/etc.: GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 4 of 4 • The Fatty Acids Continuing Calibration Verification sample (CCV) exhibited a high bias for Butyric Acid, Hexanoic Acid, and iso-Hexanoic Acid; however, these analytes were not detected in the associated samples, reducing the impact of the deviation. Page 1 of 18 Page 2 of 18 Page 3 of 18 Page 4 of 18 Page 5 of 18 Page 6 of 18 Page 7 of 18 Page 8 of 18 Page 9 of 18 Page 10 of 18 Page 11 of 18 Page 12 of 18 Page 13 of 18 Page 14 of 18 Page 15 of 18 Page 16 of 18 Page 17 of 18 Page 18 of 18 Date:22 April 2016 Client:Golder Associates, Inc. (GO007) Project:Moore Co LF Lab ID:CZ04432, CZ05223 Overview Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples No Comments Quality Control Remarks No Comments Other Comments All samples received under this project arrived in acceptable conditions. The samples were not checked for residual chlorine, as it is not required. Sample SW-3 was not submitted for analysis, as there was no flow at the time of collection. The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Stephanie Franz Project Manager GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 1 of 3 Project Name: Moore County Landfill Project Reference Number: 073-9615015.100 Sampling Event Date: April 11-12, 2016 Review Date: August 30, 2016 Initials: TM Report #: CZ04432, CZ05223 Person(s) performing the review are to initial each item on this form as acknowledgement of data acceptance, or as acknowledgement of a review issue. In the case of the latter, a brief explanation should follow the applicable item. Golder Associates Inc. has reviewed the laboratory certificates of analysis, chain-of-custody form, and laboratory provided sample group quality assurance and quality control data for the above referenced sample group to identify potential bias or inaccuracy, in general accordance with the following United States Environmental Protection Agency documents: • Region III Modifications to Functional Guidelines for Organic Data Review Multi-Media, Multi-Concentration, September 1994; • Region III Modifications to the Laboratory Data Validation Functional Guidelines for Evaluating Inorganic Analyses, April 1993; and • Laboratory Data Validation Functional Guidelines for Evaluating Inorganic Analyses, July 1998. COMPLIANCE ANALYTE LIST(S) (check all that apply) NC Closed Facility/C & D List X NC Appendix I NC Appendix I + Detects NC Appendix II NC Subtitle D Leachate List Other: 1.0 CHAIN OF CUSTODY (COC) REVIEW TM COC was properly signed by all parties. TM Correct project name and number are on the form. TM Sample receipt condition at laboratory was acceptable. TM Each sample and blank submitted for analysis appears in the report. 2.0 SAMPLE HOLDING TIMES TM Holding times for extraction and/or analysis were met for each analytical Method (see below for reference). GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 2 of 3 Review Criteria Method Analytes Holding Time SW-846 Method 8260 and 8011 VOCs 14 days SW-846 Methods 8270, 8080, 8081, 8082, and 8151 SVOCs, PCBs, pesticides and herbicides 7 days for extraction, 40 days from extraction for analysis SW-846 Methods 6000 and 7000 Series Metals except mercury 6 months (no temperature requirements) SW-846 Method 7470 Mercury 28 days SM18 4500-S2 D Sulfide 7 days SW-846 Method 9010 Cyanide 14 days EPA Method 300 Nitrate/Sulfate 48 hours/28 days EPA Method 405.1 BOD 48 hours EPA Method 410.4 COD 28 days EPA Method 365.4 Phosphorous 28 days 3.0 LABORATORY QUALITY CONTROL REVIEW TM Laboratory analyzed at least one internal blank for each method, where applicable. TM Laboratory blank is interference-free. TM Surrogate recoveries are provided for each analytical method, where applicable. TM Surrogate recoveries for each method are within the acceptable limits (i.e., at least 50% of the surrogates were within range). TM MS/MSD/LCS data results are provided for each analytical method. TM MS/MSD/LCS recoveries for each method are within the acceptable limits (i.e., at least 1 of the 3 were within range). 4.0 ANALYTE LISTS/METHODS TM The proper number of constituents are present for each analyte list as identified above (including detects where applicable). TM Proper EPA SW-846 analytical methods were used for analysis. Notes: 5.0 DATA REPORTING TM All analytical reporting associated with the event was performed by the contracted lab. TM Trip, field and/or equipment, and laboratory blank results have all been reported. All detects for blanks are listed below by constituent. All laboratory method blanks, if any, have been ‘flagged’ with a ‘B’ where detected in other samples as appropriate and a laboratory narrative was provided. If the sample was flagged by the laboratory and is not within 5X of the concentration in the blank (or 10X for commonly detected laboratory contaminants-acetone, methylene chloride and phthalates), list below with explanation if flags should be removed. If flags need to be added for samples, also list below. GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 3 of 3 TM It is clear from the laboratory report that samples have or have not been diluted during analysis, and if the samples have been diluted, the result is reported as a multiple of the dilution (e.g., a sample diluted 10x resulting in an analytical detection of 1.0 should be reported as 10). Those that have been diluted are listed below with the dilution factor. TM The report provides the reporting limit for each constituent. TM The results were reported at or below their proper reporting limits (e.g., NC Solid Waste Section RLs). Those that are not reported correctly are listed below (by constituent) with the proper reporting limit listed beside them. State if the reporting limit error is due to dilutions. TM No inorganic or organic constituents were reported above their respective NC 2L Drinking Water Standards or Groundwater Protection Standards in wells, surface points, or field/equipment/trip blanks. • Arsenic (NC2L = 10 ug/L) o MW-8 @ 11.3 ug/L • Benzene (NC2L = 1 ug/L) o MW-8 @ 3.5 ug/L o MW-11D @ 1.3 ug/L • Vinyl chloride (NC2L = 0.03 ug/L) o MW-8 @ 0.48 ug/L (J) o MW-11D @ 2.5 ug/L o MW-16D @ 0.61 (J) TM No quantifiable inorganic or organic constituents were detected in a well or surface water point at concentrations outside of their historical range (more than 5X previous concentrations or first-time detections). TM Other report issues/Communications with laboratory/etc.: Page 1 of 15 Date:22 April 2016 Client:Golder Associates, Inc. (GO007) Project:Moore Co LF- Blake Residence Lab ID:CZ04433 Overview Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples The spike recoveries of Chlorobenzene and Trichloroethene were outside of control limits for the 8260B MS sample, and precision between duplicate spikes of 1,1-Dichloroethene, Benzene, Chlorobenzene, Toluene, and Trichloroethene exceeded acceptance criteria. The QC batch was approved based on acceptable LCS recovery of these analytes. Quality Control Remarks No Comments Other Comments All samples received under this work order arrived in acceptable conditions. The samples were not checked for residual chlorine, as it is not required. The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Stephanie Franz Project Manager Page 2 of 15 Page 3 of 15 Page 4 of 15 Page 5 of 15 Page 6 of 15 Page 7 of 15 Page 8 of 15 Page 9 of 15 Page 10 of 15 Page 11 of 15 Page 12 of 15 Page 13 of 15 Page 14 of 15 Page 15 of 15 GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 1 of 3 Project Name: Moore County Landfill – Blake Residence Project Reference Number: 073-9615015.100 Sampling Event Date: April 12, 2016 Review Date: August 23, 2016 Initials: WB Report #: CZ04433 Person(s) performing the review are to initial each item on this form as acknowledgement of data acceptance, or as acknowledgement of a review issue. In the case of the latter, a brief explanation should follow the applicable item. Golder Associates Inc. has reviewed the laboratory certificates of analysis, chain-of-custody form, and laboratory provided sample group quality assurance and quality control data for the above referenced sample group to identify potential bias or inaccuracy, in general accordance with the following United States Environmental Protection Agency documents: • Region III Modifications to Functional Guidelines for Organic Data Review Multi-Media, Multi-Concentration, September 1994; • Region III Modifications to the Laboratory Data Validation Functional Guidelines for Evaluating Inorganic Analyses, April 1993; and • Laboratory Data Validation Functional Guidelines for Evaluating Inorganic Analyses, July 1998. COMPLIANCE ANALYTE LIST(S) (check all that apply) NC Closed Facility/C & D List NC Appendix I NC Appendix I + Detects NC Appendix II NC Subtitle D Leachate List Other: Arsenic 1.0 CHAIN OF CUSTODY (COC) REVIEW WB COC was properly signed by all parties. WB Correct project name and number are on the form. WB Sample receipt condition at laboratory was acceptable. WB Each sample and blank submitted for analysis appears in the report. 2.0 SAMPLE HOLDING TIMES WB Holding times for extraction and/or analysis were met for each analytical Method (see below for reference). GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 2 of 3 Review Criteria Method Analytes Holding Time SW-846 Method 8260 and 8011 VOCs 14 days SW-846 Methods 8270, 8080, 8081, 8082, and 8151 SVOCs, PCBs, pesticides and herbicides 7 days for extraction, 40 days from extraction for analysis SW-846 Methods 6000 and 7000 Series Metals except mercury 6 months (no temperature requirements) SW-846 Method 7470 Mercury 28 days SM18 4500-S2 D Sulfide 7 days SW-846 Method 9010 Cyanide 14 days EPA Method 300 Nitrate/Sulfate 48 hours/28 days EPA Method 405.1 BOD 48 hours EPA Method 410.4 COD 28 days EPA Method 365.4 Phosphorous 28 days 3.0 LABORATORY QUALITY CONTROL REVIEW WB Laboratory analyzed at least one internal blank for each method, where applicable. WB Laboratory blank is interference-free. WB Surrogate recoveries are provided for each analytical method, where applicable. WB Surrogate recoveries for each method are within the acceptable limits (i.e., at least 50% of the surrogates were within range). WB MS/MSD/LCS data results are provided for each analytical method. WB MS/MSD/LCS recoveries for each method are within the acceptable limits (i.e., at least 1 of the 3 were within range). • The spike recoveries of Chlorobenzene and Trichloroethene were outside of control limits for the 8260B MS sample, and precision between duplicate spikes of 1,1-Dichloroethene, Benzene, Chlorobenzene, Toluene, and Trichloroethene exceeded acceptance criteria. The QC batch was approved based on acceptable LCS recovery of these analytes. 4.0 ANALYTE LISTS/METHODS WB The proper number of constituents are present for each analyte list as identified above (including detects where applicable). WB Proper EPA SW-846 analytical methods were used for analysis. Notes: 5.0 DATA REPORTING WB All analytical reporting associated with the event was performed by the contracted lab. WB Trip, field and/or equipment, and laboratory blank results have all been reported. All detects for blanks are listed below by constituent. All laboratory method blanks, if any, have been ‘flagged’ with a ‘B’ where detected in other samples as appropriate and a GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 3 of 3 laboratory narrative was provided. If the sample was flagged by the laboratory and is not within 5X of the concentration in the blank (or 10X for commonly detected laboratory contaminants-acetone, methylene chloride and phthalates), list below with explanation if flags should be removed. If flags need to be added for samples, also list below. WB It is clear from the laboratory report that samples have or have not been diluted during analysis, and if the samples have been diluted, the result is reported as a multiple of the dilution (e.g., a sample diluted 10x resulting in an analytical detection of 1.0 should be reported as 10). Those that have been diluted are listed below with the dilution factor. WB The report provides the reporting limit for each constituent. WB The results were reported at or below their proper reporting limits (e.g., NC Solid Waste Section RLs). Those that are not reported correctly are listed below (by constituent) with the proper reporting limit listed beside them. State if the reporting limit error is due to dilutions. • Lead (NC SWSL = 10 ug/L)  Blake Residence @ 21.0 ug/L WB No inorganic or organic constituents were reported above their respective NC 2L Drinking Water Standards or Groundwater Protection Standards in wells, surface points, or field/equipment/trip blanks. • Lead (NC 2L = 15 ug/L)  Blake Residence @ 21.0 ug/L WB No quantifiable inorganic or organic constituents were detected in a well or surface water point at concentrations outside of their historical range (more than 5X previous concentrations or first-time detections). WB Other report issues/Communications with laboratory/etc.: Page 1 of 13 Date:16 August 2016 Client:Golder Associates, Inc. (GO007) Project:Moore County LF Lab ID:CZ11756 Overview Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples No Comments Quality Control Remarks No Comments Other Comments All samples received under this work order arrived in acceptable conditions. The samples were not checked for residual chlorine, as it is not required. No aqueous volatile samples were received, negating the need to check for preservation or headspace. The project as not received on a preprinted chain of custody. The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Stephanie Franz Project Manager Page 2 of 13 Page 3 of 13 Page 4 of 13 Page 5 of 13 Page 6 of 13 Page 7 of 13 Page 8 of 13 Page 9 of 13 Page 10 of 13 Page 11 of 13 Page 12 of 13 Page 13 of 13 GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 1 of 3 Project Name: Moore County Landfill – Resample Project Reference Number: 073-9615015.100 Sampling Event Date: August 5, 2016 Review Date: August 23, 2016 Initials: WB Report #: CZ11756 Person(s) performing the review are to initial each item on this form as acknowledgement of data acceptance, or as acknowledgement of a review issue. In the case of the latter, a brief explanation should follow the applicable item. Golder Associates Inc. has reviewed the laboratory certificates of analysis, chain-of-custody form, and laboratory provided sample group quality assurance and quality control data for the above referenced sample group to identify potential bias or inaccuracy, in general accordance with the following United States Environmental Protection Agency documents: • Region III Modifications to Functional Guidelines for Organic Data Review Multi-Media, Multi-Concentration, September 1994; • Region III Modifications to the Laboratory Data Validation Functional Guidelines for Evaluating Inorganic Analyses, April 1993; and • Laboratory Data Validation Functional Guidelines for Evaluating Inorganic Analyses, July 1998. COMPLIANCE ANALYTE LIST(S) (check all that apply) NC Closed Facility/C & D List NC Appendix I NC Appendix I + Detects NC Appendix II NC Subtitle D Leachate List Other: Arsenic 1.0 CHAIN OF CUSTODY (COC) REVIEW WB COC was properly signed by all parties. WB Correct project name and number are on the form. WB Sample receipt condition at laboratory was acceptable. WB Each sample and blank submitted for analysis appears in the report. 2.0 SAMPLE HOLDING TIMES WB Holding times for extraction and/or analysis were met for each analytical Method (see below for reference). GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 2 of 3 Review Criteria Method Analytes Holding Time SW-846 Method 8260 and 8011 VOCs 14 days SW-846 Methods 8270, 8080, 8081, 8082, and 8151 SVOCs, PCBs, pesticides and herbicides 7 days for extraction, 40 days from extraction for analysis SW-846 Methods 6000 and 7000 Series Metals except mercury 6 months (no temperature requirements) SW-846 Method 7470 Mercury 28 days SM18 4500-S2 D Sulfide 7 days SW-846 Method 9010 Cyanide 14 days EPA Method 300 Nitrate/Sulfate 48 hours/28 days EPA Method 405.1 BOD 48 hours EPA Method 410.4 COD 28 days EPA Method 365.4 Phosphorous 28 days 3.0 LABORATORY QUALITY CONTROL REVIEW WB Laboratory analyzed at least one internal blank for each method, where applicable. WB Laboratory blank is interference-free. WB Surrogate recoveries are provided for each analytical method, where applicable. • Surrogate recoveries are not applicable N/A Surrogate recoveries for each method are within the acceptable limits (i.e., at least 50% of the surrogates were within range). WB MS/MSD/LCS data results are provided for each analytical method. WB MS/MSD/LCS recoveries for each method are within the acceptable limits (i.e., at least 1 of the 3 were within range). 4.0 ANALYTE LISTS/METHODS WB The proper number of constituents are present for each analyte list as identified above (including detects where applicable). WB Proper EPA SW-846 analytical methods were used for analysis. Notes: 5.0 DATA REPORTING WB All analytical reporting associated with the event was performed by the contracted lab. WB Trip, field and/or equipment, and laboratory blank results have all been reported. All detects for blanks are listed below by constituent. All laboratory method blanks, if any, have been ‘flagged’ with a ‘B’ where detected in other samples as appropriate and a laboratory narrative was provided. If the sample was flagged by the laboratory and is not within 5X of the concentration in the blank (or 10X for commonly detected laboratory contaminants-acetone, methylene chloride and phthalates), list below with explanation if flags should be removed. If flags need to be added for samples, also list below. GOLDER ASSOCIATES NC, INC. QUALITY ASSURANCE & QUALITY CONTROL LABORATORY DATA REVIEW Page 3 of 3 WB It is clear from the laboratory report that samples have or have not been diluted during analysis, and if the samples have been diluted, the result is reported as a multiple of the dilution (e.g., a sample diluted 10x resulting in an analytical detection of 1.0 should be reported as 10). Those that have been diluted are listed below with the dilution factor. WB The report provides the reporting limit for each constituent. WB The results were reported at or below their proper reporting limits (e.g., NC Solid Waste Section RLs). Those that are not reported correctly are listed below (by constituent) with the proper reporting limit listed beside them. State if the reporting limit error is due to dilutions. • Arsenic (NC SWSL = 10 ug/L)  MW-9 @ 53.2 ug/L  MW-9 (dissolved) 64.4 @ ug/L  MW-15 30.4 @ ug/L  MW-9 (dissolved) 31.4 @ ug/L WB No inorganic or organic constituents were reported above their respective NC 2L Drinking Water Standards or Groundwater Protection Standards in wells, surface points, or field/equipment/trip blanks. • Arsenic (NC 2L = 10 ug/L)  MW-9 @ 53.2 ug/L  MW-9 (dissolved) 64.4 @ ug/L  MW-15 30.4 @ ug/L  MW-9 (dissolved) 31.4 @ ug/L WB No quantifiable inorganic or organic constituents were detected in a well or surface water point at concentrations outside of their historical range (more than 5X previous concentrations or first-time detections). WB Other report issues/Communications with laboratory/etc.: • No aqueous volatile samples were received, negating the need to check for preservation or headspace. The project as not received on a preprinted chain of custody. APPENDIX C STATISTICAL EVALUATION WORKSHEETS & SUMMARY TABLE Caption Text August 2016 1 of 1 0739-615015 MW-1 MW-2 MW-3 MW-4 MW-6 MW-7 MW-8 MW-9 MW-11S MW-11D MW-13S MW-13D MW-14 MW-15 MW-16S MW-16D Interwell Nonparametric Prediction Interval 10.0Intrawell MW-6 Nonparametric Prediction Interval 29.5Intrawell MW-7 Nonparametric Prediction Interval 33.0Intrawell MW-8 Nonparametric Prediction Interval 22.6Intrawell MW-9 Nonparametric Prediction Interval 38.6Intrawell MW-15 Nonparametric Prediction Interval 28.5Intrawell MW-16S Nonparametric Prediction Interval 13.7 Notes:1. Shaded values represent apparent statistical significant increases (SSIs) over background concentrations.2. Statistical worksheets are provided as Appendix C. 3. ug/L = micrograms per liter4. J = estimated concentration below the Solid Waste Section Limit 5. ND = Not Detected 38.7 NDArsenicug/L ND ND ND ND ND 29.6 Summary of Statistical Analysis Moore County Landfill, Permit No. 63-01 Moore County, North Carolina April 2016 Downgradient Monitoring Wells and Concentrations 12.6 27.0 11.3 12.9 ND Detected Monitoring Constituent Reporting Units Prediction IntervalStatistical Evaluation Method ND ND ND G:\Projects\Moore County\Groundwater\April 2016 Event\Stats\Moore Stats Summary Oct 2015.xls APPENDIX D SOIL AND STREAM SEDIMENT DATA August 2016 Page 1 of 1 Appendix D Summary Table 0739615015 Sample #NURE ID Lab ID Sample Date Type Datum Latitude Longitude As (Max) Concentration (ppm)Method 1 5286932 C-110082 09/21/76 Sediment NAD27 35.2457 -79.3637 5.18 INAA 2 5286911 C-110755 09/17/76 Sediment NAD27 35.2310 -79.3635 1.2 AA 3 5287194 C-110837 10/01/76 Sediment NAD27 35.1510 -79.6394 5.54 INAA 4 5287187 C-116880 09/30/76 Sediment NAD27 35.0285 -79.5447 2.6 AA 5 5286908 C-116889 09/17/76 Sediment NAD27 35.2333 -79.2552 10 ICP40 6 5286962 C-116900 09/22/76 Sediment NAD27 35.2093 -79.6284 47 ICP40 7 5287188 C-143341 09/30/76 Sediment NAD27 35.0214 -79.5284 7.2 AA 8 5286939 C-143589 09/21/76 Sediment NAD27 35.2350 -79.4938 1.1 AA 9 5286967 C-143670 09/22/76 Sediment NAD27 35.2883 -79.5946 12 ICP40 10 5285098 C-143893 08/10/77 Sediment NAD27 34.9908 -79.5188 12.8 AA Average 10.462 G:\Projects\Moore County\Groundwater\April 2016 Event\FINAL\Appendix D\Appendix D Summary Table.xlsx NGS sample #C-110082) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110082[8/31/2016 11:10:53 AM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-110082 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5286932 Lab identification number C-110082 Real field name NCMO035S1 Collection date 19760921 Field name as analyzed NCMO035 Description NURE sample Location count 1 Sample set NURE800 Sample type code 750 Map datum NAD27 Active channel width dry Water depth dry Water color other Flow stage dry Flow rate dry Collector 57 Stream bed sand Relief low Contamination source farm Vegetation deciduous Latitude 35.2457 Longitude -79.3637 1:24k quadrangle 36080SWF3 1:250k quadrangle 36080 1:100,000 quadrangle 36080SW FIPS of county f37125 NGS sample #C-110082) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110082[8/31/2016 11:10:53 AM] Hydrologic unit 3030004 Sample category NURE 1:250k quad name Raleigh Short description of sample type STRM-SED-DRY Sample medium Sediment Sample source Stream Source modifier Dry Upper limit of sieve size 150 Drying procedure <110oC Sample type note Original NURE code was 50, but stream was dry ICP40 job GF34 As job number GF34 Se job number GF34 Hg job number GF34 ICP10 job number GF34 INAA job no. (USGS)WR85 XRF job number WR85 LOI (wt%)5.74 Zip code, 3-digit 283 Congressional district 3706C2 Geographic context:Political divisions (FIPS codes) Moore (county) North Carolina (state) United States (country)North America (continent) Land (continent) USGS map quadrangles Niagara (quadrangle 1:24,000 scale)Southern Pines (quadrangle 1:100,000 scale) Raleigh (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Upper Cape Fear (hydrologic unit)Cape Fear (hydrologic accounting unit) Cape Fear (hydrologic subregion) South Atlantic-Gulf (hydrologic region) Geologic map unit Middendorf Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method NGS sample #C-110082) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110082[8/31/2016 11:10:53 AM] Lithium 11 parts per million by weight ICP40 Beryllium <1 parts per million by weight ICP40 Sodium 0.02 percent by weight ICP40 0.023 percent by weight INAA <0.15 percent by weight XRF Magnesium 0.05 percent by weight ICP40 0.1 percent by weight XRF Aluminum 2.6 percent by weight ICP40 5.19 percent by weight XRF Silicon 84.5 percent by weight XRF Phosphorus 0.04 percent by weight ICP40 0.12 percent by weight XRF Potassium 0.2 percent by weight ICP40 0.24 percent by weight XRF Calcium 0.03 percent by weight ICP40 0.05 percent by weight XRF Scandium 6 parts per million by weight ICP40 5.78 parts per million by weight INAA Titanium 0.69 percent by weight ICP40 1.29 percent by weight XRF Vanadium 49 parts per million by weight ICP40 Chromium 33 parts per million by weight ICP40 40.7 parts per million by weight INAA Manganese 131 parts per million by weight ICP40 0.02 percent by weight XRF Iron 1.1 percent by weight ICP40 1.15 percent by weight INAA 1.65 percent by weight XRF Cobalt <2 parts per million by weight ICP40 1.46 parts per million by weight INAA Nickel 7 parts per million by weight ICP40 23.4 parts per million by weight INAA Copper 8 parts per million by weight ICP40 7 parts per million by weight ICP10 Zinc 27 parts per million by weight ICP40 NGS sample #C-110082) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110082[8/31/2016 11:10:53 AM] 24.6 parts per million by weight ICP10 Gallium 5 parts per million by weight ICP40 Arsenic <10 parts per million by weight ICP40 3.2 parts per million by weight As_AA <1 parts per million by weight ICP10 5.18 parts per million by weight INAA Selenium 0.4 parts per million by weight Se_AA Rubidium 20.7 parts per million by weight INAA Strontium 13 parts per million by weight ICP40 42 parts per million by weight INAA Yttrium 13 parts per million by weight ICP40 Zirconium 1370 parts per million by weight INAA Niobium 18 parts per million by weight ICP40 Molybdenum 3 parts per million by weight ICP40 0.8 parts per million by weight ICP10 Silver <2 parts per million by weight ICP40 <0.08 parts per million by weight ICP10 Cadmium <2 parts per million by weight ICP40 0.08 parts per million by weight ICP10 Tin 49 parts per million by weight ICP40 Antimony <1 parts per million by weight ICP10 0.57 parts per million by weight INAA Cesium 2.34 parts per million by weight INAA Barium 89 parts per million by weight ICP40 100 parts per million by weight INAA Lanthanum 96 parts per million by weight ICP40 106 parts per million by weight INAA Cerium 203 parts per million by weight ICP40 206 parts per million by weight INAA Neodymium 77 parts per million by weight ICP40 92 parts per million by weight INAA Samarium 17.2 parts per million by weight INAA Europium 1 parts per million by weight ICP40 0.877 parts per million by weight INAA Terbium 1.68 parts per million by weight INAA NGS sample #C-110082) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110082[8/31/2016 11:10:53 AM] Holmium <4 parts per million by weight ICP40 Ytterbium <1 parts per million by weight ICP40 5.72 parts per million by weight INAA Lutetium 0.886 parts per million by weight INAA Hafnium 39 parts per million by weight INAA Tantalum <40 parts per million by weight ICP40 3.28 parts per million by weight INAA Tungsten 1.69 parts per million by weight INAA Gold <8 parts per billion by weight ICP40 <0.1 parts per billion by weight ICP10 6.84 parts per billion by weight INAA Mercury 0.05 parts per million by weight Hg_AA Lead 32 parts per million by weight ICP40 24 parts per million by weight ICP10 Bismuth <10 parts per million by weight ICP40 <1 parts per million by weight ICP10 Thorium 41 parts per million by weight ICP40 41.9 parts per million by weight INAA Uranium <100 parts per million by weight ICP40 9.95 parts per million by weight INAA Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-110082 Page Contact Information: Peter Schweitzer NGS sample #C-110755) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110755[8/30/2016 6:41:02 PM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-110755 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5286911 Lab identification number C-110755 Real field name NCMO014S1 Collection date 19760917 Field name as analyzed NCMO014 Description NURE sample Location count 1 Sample set NURE800 Sample type code 50 Map datum NAD27 Active channel width 4-8' Water depth 2-4' Water color clear Flow stage normal Flow rate mod Collector 57 Stream bed sand Relief low Vegetation deciduous Latitude 35.231 Longitude -79.3635 1:24k quadrangle 36080SWF3 1:250k quadrangle 36080 1:100,000 quadrangle 36080SW FIPS of county f37125 Hydrologic unit 3030004 NGS sample #C-110755) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110755[8/30/2016 6:41:02 PM] Sample category NURE 1:250k quad name Raleigh Short description of sample type STRM-SED-WET Sample medium Sediment Sample source Stream Source modifier Wet Upper limit of sieve size 150 Drying procedure <110oC ICP40 job GF58 As job number GF58 Se job number GF58 Hg job number GF58 ICP10 job number GF58 INAA job no. (USGS)WS02 XRF job number WS02 LOI (wt%)1.4 Zip code, 3-digit 283 Congressional district 3706C2 Geographic context:Political divisions (FIPS codes) Moore (county)North Carolina (state) United States (country) North America (continent) Land (continent) USGS map quadrangles Niagara (quadrangle 1:24,000 scale) Southern Pines (quadrangle 1:100,000 scale) Raleigh (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Upper Cape Fear (hydrologic unit) Cape Fear (hydrologic accounting unit) Cape Fear (hydrologic subregion)South Atlantic-Gulf (hydrologic region) Geologic map unit Middendorf Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method Lithium 2 parts per million by weight ICP40 Beryllium <1 parts per million by weight ICP40 NGS sample #C-110755) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110755[8/30/2016 6:41:02 PM] Sodium 0.007 percent by weight ICP40 0.013 percent by weight INAA <0.15 percent by weight XRF Magnesium 0.009 percent by weight ICP40 <0.1 percent by weight XRF Aluminum 0.42 percent by weight ICP40 1.09 percent by weight XRF Silicon 93.5 percent by weight XRF Phosphorus 0.03 percent by weight ICP40 0.19 percent by weight XRF Potassium 0.1 percent by weight ICP40 0.14 percent by weight XRF Calcium 0.01 percent by weight ICP40 0.03 percent by weight XRF Scandium 4 parts per million by weight ICP40 4.02 parts per million by weight INAA Titanium 0.76 percent by weight ICP40 1.5 percent by weight XRF Vanadium 20 parts per million by weight ICP40 Chromium 3 parts per million by weight ICP40 27.2 parts per million by weight INAA Manganese 95 parts per million by weight ICP40 0.01 percent by weight XRF Iron 0.34 percent by weight ICP40 0.377 percent by weight INAA 0.53 percent by weight XRF Cobalt <2 parts per million by weight ICP40 0.87 parts per million by weight INAA Nickel 13 parts per million by weight ICP40 27.9 parts per million by weight INAA Copper 5 parts per million by weight ICP40 4.6 parts per million by weight ICP10 Zinc 18 parts per million by weight ICP40 14.1 parts per million by weight ICP10 57.8 parts per million by weight INAA NGS sample #C-110755) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110755[8/30/2016 6:41:02 PM] Gallium <4 parts per million by weight ICP40 Arsenic <10 parts per million by weight ICP40 1.2 parts per million by weight As_AA <1 parts per million by weight ICP10 1.08 parts per million by weight INAA Selenium <0.2 parts per million by weight Se_AA Rubidium 4.74 parts per million by weight INAA Strontium 6 parts per million by weight ICP40 31 parts per million by weight INAA Yttrium 20 parts per million by weight ICP40 Zirconium 2100 parts per million by weight INAA Niobium 13 parts per million by weight ICP40 Molybdenum <2 parts per million by weight ICP40 0.7 parts per million by weight ICP10 Silver <2 parts per million by weight ICP40 0.1 parts per million by weight ICP10 Cadmium <2 parts per million by weight ICP40 0.1 parts per million by weight ICP10 Tin 80 parts per million by weight ICP40 Antimony <1 parts per million by weight ICP10 0.18 parts per million by weight INAA Cesium 0.18 parts per million by weight INAA Barium 64 parts per million by weight ICP40 <28 parts per million by weight INAA Lanthanum 190 parts per million by weight ICP40 177 parts per million by weight INAA Cerium 371 parts per million by weight ICP40 347 parts per million by weight INAA Neodymium 151 parts per million by weight ICP40 164 parts per million by weight INAA Samarium 30.3 parts per million by weight INAA Europium 1 parts per million by weight ICP40 1.15 parts per million by weight INAA Terbium 2.52 parts per million by weight INAA Holmium <4 parts per million by weight ICP40 NGS sample #C-110755) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110755[8/30/2016 6:41:02 PM] Ytterbium <1 parts per million by weight ICP40 7.14 parts per million by weight INAA Lutetium 1.08 parts per million by weight INAA Hafnium 54.8 parts per million by weight INAA Tantalum <40 parts per million by weight ICP40 7.61 parts per million by weight INAA Tungsten 1.52 parts per million by weight INAA Gold <8 parts per billion by weight ICP40 <0.1 parts per billion by weight ICP10 16.5 parts per billion by weight INAA Mercury 0.07 parts per million by weight Hg_AA Lead 32 parts per million by weight ICP40 12 parts per million by weight ICP10 Bismuth 24 parts per million by weight ICP40 <1 parts per million by weight ICP10 Thorium 94 parts per million by weight ICP40 71.3 parts per million by weight INAA Uranium <100 parts per million by weight ICP40 13.3 parts per million by weight INAA Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-110755 Page Contact Information: Peter Schweitzer NGS sample #C-110837) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110837[8/30/2016 6:34:04 PM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-110837 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5287194 Lab identification number C-110837 Real field name NCRI009S1 Collection date 19761001 Field name as analyzed NCRI009 Description NURE sample Location count 1 Sample set NURE800 Sample type code 750 Map datum NAD27 Active channel width dry Water depth dry Water color other Flow stage dry Flow rate dry Collector 57 Stream bed sand Relief low Contamination source unknown Vegetation deciduous Latitude 35.151 Longitude -79.6394 1:24k quadrangle 36080SWC3 1:250k quadrangle 36080 1:100,000 quadrangle 36080SW FIPS of county f37153 NGS sample #C-110837) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110837[8/30/2016 6:34:04 PM] Hydrologic unit 3040203 Sample category NURE 1:250k quad name Raleigh Short description of sample type STRM-SED-DRY Sample medium Sediment Sample source Stream Source modifier Dry Upper limit of sieve size 150 Drying procedure <110oC Sample type note Original NURE code was 50, but stream was dry ICP40 job GF61 As job number GF61 Se job number GF61 Hg job number GF61 ICP10 job number GF61 INAA job no. (USGS)WS04 XRF job number WS04 LOI (wt%)6.29 Zip code, 3-digit 283 Congressional district 3708C2 Geographic context:Political divisions (FIPS codes) Richmond (county) North Carolina (state) United States (country)North America (continent) Land (continent) USGS map quadrangles Norman (quadrangle 1:24,000 scale)Southern Pines (quadrangle 1:100,000 scale) Raleigh (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Lumber (hydrologic unit)Lower Pee Dee (hydrologic accounting unit) Pee Dee (hydrologic subregion) South Atlantic-Gulf (hydrologic region) Geologic map unit Pinehurst Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method NGS sample #C-110837) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110837[8/30/2016 6:34:04 PM] Lithium 9 parts per million by weight ICP40 Beryllium <1 parts per million by weight ICP40 Sodium 0.02 percent by weight ICP40 0.026 percent by weight INAA <0.15 percent by weight XRF Magnesium 0.07 percent by weight ICP40 0.12 percent by weight XRF Aluminum 2.6 percent by weight ICP40 4.76 percent by weight XRF Silicon 84.2 percent by weight XRF Phosphorus 0.05 percent by weight ICP40 0.22 percent by weight XRF Potassium 0.23 percent by weight ICP40 0.29 percent by weight XRF Calcium 0.04 percent by weight ICP40 0.08 percent by weight XRF Scandium 5 parts per million by weight ICP40 5.76 parts per million by weight INAA Titanium 0.64 percent by weight ICP40 1.18 percent by weight XRF Vanadium 52 parts per million by weight ICP40 Chromium 5 parts per million by weight ICP40 37.6 parts per million by weight INAA Manganese 103 parts per million by weight ICP40 0.02 percent by weight XRF Iron 1.2 percent by weight ICP40 1.16 percent by weight INAA 1.68 percent by weight XRF Cobalt <2 parts per million by weight ICP40 1.81 parts per million by weight INAA Nickel 6 parts per million by weight ICP40 13 parts per million by weight INAA Copper 11 parts per million by weight ICP40 9.6 parts per million by weight ICP10 Zinc 36 parts per million by weight ICP40 NGS sample #C-110837) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110837[8/30/2016 6:34:04 PM] 34.8 parts per million by weight ICP10 90.9 parts per million by weight INAA Gallium <4 parts per million by weight ICP40 Arsenic <10 parts per million by weight ICP40 4.8 parts per million by weight As_AA 1 parts per million by weight ICP10 5.54 parts per million by weight INAA Selenium 0.9 parts per million by weight Se_AA Rubidium 19.2 parts per million by weight INAA Strontium 12 parts per million by weight ICP40 <14 parts per million by weight INAA Yttrium 16 parts per million by weight ICP40 Zirconium 1190 parts per million by weight INAA Niobium 14 parts per million by weight ICP40 Molybdenum <2 parts per million by weight ICP40 0.7 parts per million by weight ICP10 Silver <2 parts per million by weight ICP40 <0.08 parts per million by weight ICP10 Cadmium <2 parts per million by weight ICP40 0.1 parts per million by weight ICP10 Tin 61 parts per million by weight ICP40 Antimony <1 parts per million by weight ICP10 0.486 parts per million by weight INAA Cesium 1.8 parts per million by weight INAA Barium 95 parts per million by weight ICP40 66.7 parts per million by weight INAA Lanthanum 101 parts per million by weight ICP40 107 parts per million by weight INAA Cerium 214 parts per million by weight ICP40 207 parts per million by weight INAA Neodymium 75 parts per million by weight ICP40 99.7 parts per million by weight INAA Samarium 17.3 parts per million by weight INAA Europium 1 parts per million by weight ICP40 0.865 parts per million by weight INAA NGS sample #C-110837) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-110837[8/30/2016 6:34:04 PM] Terbium 1.63 parts per million by weight INAA Holmium <4 parts per million by weight ICP40 Ytterbium <1 parts per million by weight ICP40 5.95 parts per million by weight INAA Lutetium 0.868 parts per million by weight INAA Hafnium 34.1 parts per million by weight INAA Tantalum <40 parts per million by weight ICP40 2.11 parts per million by weight INAA Tungsten 1.44 parts per million by weight INAA Gold <8 parts per billion by weight ICP40 <0.1 parts per billion by weight ICP10 <0.28 parts per billion by weight INAA Mercury 0.07 parts per million by weight Hg_AA Lead 58 parts per million by weight ICP40 43 parts per million by weight ICP10 Bismuth 25 parts per million by weight ICP40 <1 parts per million by weight ICP10 Thorium 53 parts per million by weight ICP40 40.4 parts per million by weight INAA Uranium <100 parts per million by weight ICP40 9.43 parts per million by weight INAA Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-110837 Page Contact Information: Peter Schweitzer NGS sample #C-116880) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116880[8/30/2016 6:28:05 PM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-116880 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5287187 Lab identification number C-116880 Real field name NCRI002S1 Collection date 19760930 Field name as analyzed NCRI002 Description NURE STREAM SEDIMENT Location count 1 Sample set NURE Coastal 98 Sample type code 750 Map datum NAD27 Active channel width dry Water depth dry Water color other Flow stage dry Flow rate dry Collector 57 Stream bed sand Relief gentle Vegetation deciduous Latitude 35.0285 Longitude -79.5447 1:24k quadrangle 36080SWD4 1:250k quadrangle 36080 1:100,000 quadrangle 36080SW FIPS of county f37153 Hydrologic unit 3040203 NGS sample #C-116880) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116880[8/30/2016 6:28:05 PM] Sample category NURE 1:250k quad name Raleigh Short description of sample type STRM-SED-DRY Sample medium Sediment Sample source Stream Source modifier Dry Upper limit of sieve size 150 Drying procedure <110oC Sample type note Original NURE code was 50, but stream was dry ICP40 job MRP-00821 As job number MRP-00827 Se job number MRP-00827 ICP10 job number MRP-00827 INAA job no. (USGS)WS84 Zip code, 3-digit 283 Congressional district 3708C2 Geographic context:Political divisions (FIPS codes) Richmond (county) North Carolina (state) United States (country)North America (continent) Land (continent) USGS map quadrangles Hoffman (quadrangle 1:24,000 scale)Southern Pines (quadrangle 1:100,000 scale) Raleigh (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Lumber (hydrologic unit)Lower Pee Dee (hydrologic accounting unit) Pee Dee (hydrologic subregion) South Atlantic-Gulf (hydrologic region) Geologic map unit Middendorf Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method Lithium 3 parts per million by weight ICP40 Beryllium <1 parts per million by weight ICP40 Sodium 0.007 percent by weight ICP40 0.011 percent by weight INAA NGS sample #C-116880) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116880[8/30/2016 6:28:05 PM] Magnesium 0.013 percent by weight ICP40 Aluminum 1.249 percent by weight ICP40 Phosphorus 0.01 percent by weight ICP40 Potassium 0.08 percent by weight ICP40 Calcium 0.008 percent by weight ICP40 Scandium 5 parts per million by weight ICP40 5.15 parts per million by weight INAA Titanium 0.478 percent by weight ICP40 Vanadium 27 parts per million by weight ICP40 Chromium 2 parts per million by weight ICP40 25.5 parts per million by weight INAA Manganese 49 parts per million by weight ICP40 Iron 0.49 percent by weight ICP40 0.522 percent by weight INAA Cobalt <2 parts per million by weight ICP40 0.668 parts per million by weight INAA Nickel <3 parts per million by weight ICP40 5.62 parts per million by weight INAA Copper 3 parts per million by weight ICP40 1.7 parts per million by weight ICP10 Zinc 30 parts per million by weight ICP40 18.8 parts per million by weight ICP10 Gallium <4 parts per million by weight ICP40 Arsenic <10 parts per million by weight ICP40 2.6 parts per million by weight As_AA <1 parts per million by weight ICP10 2.69 parts per million by weight INAA Selenium <0.2 parts per million by weight Se_AA Rubidium 5.53 parts per million by weight INAA Strontium 3 parts per million by weight ICP40 <10.8 parts per million by weight INAA Yttrium 10 parts per million by weight ICP40 Zirconium 891 parts per million by weight INAA Niobium 6 parts per million by weight ICP40 Molybdenum <2 parts per million by weight ICP40 NGS sample #C-116880) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116880[8/30/2016 6:28:05 PM] 0.6 parts per million by weight ICP10 Silver <2 parts per million by weight ICP40 <0.08 parts per million by weight ICP10 Cadmium <2 parts per million by weight ICP40 <0.05 parts per million by weight ICP10 Tin 34 parts per million by weight ICP40 Antimony <1 parts per million by weight ICP10 0.193 parts per million by weight INAA Cesium 0.34 parts per million by weight INAA Barium 47 parts per million by weight ICP40 <37.1 parts per million by weight INAA Lanthanum 59 parts per million by weight ICP40 58.7 parts per million by weight INAA Cerium 115 parts per million by weight ICP40 123 parts per million by weight INAA Neodymium 45 parts per million by weight ICP40 59 parts per million by weight INAA Samarium 10.1 parts per million by weight INAA Europium 1 parts per million by weight ICP40 0.698 parts per million by weight INAA Terbium 1.1 parts per million by weight INAA Holmium <4 parts per million by weight ICP40 Ytterbium <1 parts per million by weight ICP40 4.68 parts per million by weight INAA Lutetium 0.698 parts per million by weight INAA Hafnium 25.6 parts per million by weight INAA Tantalum <40 parts per million by weight ICP40 1.58 parts per million by weight INAA Tungsten 0.771 parts per million by weight INAA Gold <8 parts per billion by weight ICP40 0.3 parts per billion by weight ICP10 <0.37 parts per billion by weight INAA Lead 21 parts per million by weight ICP40 20 parts per million by weight ICP10 Bismuth 13 parts per million by weight ICP40 NGS sample #C-116880) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116880[8/30/2016 6:28:05 PM] <1 parts per million by weight ICP10 Thorium 29 parts per million by weight ICP40 24.9 parts per million by weight INAA Uranium <100 parts per million by weight ICP40 6.74 parts per million by weight INAA Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-116880 Page Contact Information: Peter Schweitzer NGS sample #C-116889) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116889[8/31/2016 11:11:29 AM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-116889 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5286908 Lab identification number C-116889 Real field name NCMO011S1 Collection date 19760917 Field name as analyzed NCMO011 Description NURE STREAM SEDIMENT Location count 1 Sample set NURE Coastal 98 Sample type code 50 Map datum NAD27 Active channel width 1-2' Water depth <0.5' Water color clear Flow stage low Flow rate slow Collector 57 Stream bed sand Relief low Vegetation swamp Latitude 35.2333 Longitude -79.2552 1:24k quadrangle 36080SWF3 1:250k quadrangle 36080 1:100,000 quadrangle 36080SW FIPS of county f37125 Hydrologic unit 3030004 NGS sample #C-116889) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116889[8/31/2016 11:11:29 AM] Sample category NURE 1:250k quad name Raleigh Short description of sample type STRM-SED-WET Sample medium Sediment Sample source Stream Source modifier Wet Upper limit of sieve size 150 Drying procedure <110oC ICP40 job MRP-00821 As job number MRP-00827 Se job number MRP-00827 ICP10 job number MRP-00827 INAA job no. (USGS)WS84 Zip code, 3-digit 283 Congressional district 3706C2 Geographic context:Political divisions (FIPS codes) Moore (county) North Carolina (state) United States (country) North America (continent)Land (continent) USGS map quadrangles Niagara (quadrangle 1:24,000 scale) Southern Pines (quadrangle 1:100,000 scale)Raleigh (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Upper Cape Fear (hydrologic unit) Cape Fear (hydrologic accounting unit)Cape Fear (hydrologic subregion) South Atlantic-Gulf (hydrologic region) Geologic map unit Cape Fear Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method Lithium 4 parts per million by weight ICP40 Beryllium <1 parts per million by weight ICP40 Sodium 0.011 percent by weight ICP40 0.018 percent by weight INAA Magnesium 0.017 percent by weight ICP40 NGS sample #C-116889) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116889[8/31/2016 11:11:29 AM] Aluminum 0.917 percent by weight ICP40 Phosphorus 0.025 percent by weight ICP40 Potassium 0.28 percent by weight ICP40 Calcium 0.036 percent by weight ICP40 Scandium 3 parts per million by weight ICP40 4.01 parts per million by weight INAA Titanium 0.724 percent by weight ICP40 Vanadium 30 parts per million by weight ICP40 Chromium 17 parts per million by weight ICP40 32.5 parts per million by weight INAA Manganese 90 parts per million by weight ICP40 Iron 0.61 percent by weight ICP40 0.615 percent by weight INAA Cobalt <2 parts per million by weight ICP40 0.775 parts per million by weight INAA Nickel <3 parts per million by weight ICP40 10.2 parts per million by weight INAA Copper 2 parts per million by weight ICP40 0.78 parts per million by weight ICP10 Zinc 28 parts per million by weight ICP40 4.33 parts per million by weight ICP10 Gallium <4 parts per million by weight ICP40 Arsenic 10 parts per million by weight ICP40 2 parts per million by weight As_AA <1 parts per million by weight ICP10 2.04 parts per million by weight INAA Selenium <0.2 parts per million by weight Se_AA Rubidium 7.75 parts per million by weight INAA Strontium 8 parts per million by weight ICP40 <18.7 parts per million by weight INAA Yttrium 10 parts per million by weight ICP40 Zirconium 1410 parts per million by weight INAA Niobium 9 parts per million by weight ICP40 Molybdenum <2 parts per million by weight ICP40 0.2 parts per million by weight ICP10 NGS sample #C-116889) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116889[8/31/2016 11:11:29 AM] Silver <2 parts per million by weight ICP40 <0.08 parts per million by weight ICP10 Cadmium <2 parts per million by weight ICP40 <0.05 parts per million by weight ICP10 Tin 77 parts per million by weight ICP40 Antimony <1 parts per million by weight ICP10 0.25 parts per million by weight INAA Cesium 0.536 parts per million by weight INAA Barium 82 parts per million by weight ICP40 115 parts per million by weight INAA Lanthanum 82 parts per million by weight ICP40 80.5 parts per million by weight INAA Cerium 158 parts per million by weight ICP40 160 parts per million by weight INAA Neodymium 61 parts per million by weight ICP40 82.3 parts per million by weight INAA Samarium 14.3 parts per million by weight INAA Europium 1 parts per million by weight ICP40 0.649 parts per million by weight INAA Terbium 1.49 parts per million by weight INAA Holmium <4 parts per million by weight ICP40 Ytterbium <1 parts per million by weight ICP40 6.02 parts per million by weight INAA Lutetium 0.981 parts per million by weight INAA Hafnium 38.8 parts per million by weight INAA Tantalum <40 parts per million by weight ICP40 2.33 parts per million by weight INAA Tungsten 0.757 parts per million by weight INAA Gold <8 parts per billion by weight ICP40 0.2 parts per billion by weight ICP10 <0.933 parts per billion by weight INAA Lead 26 parts per million by weight ICP40 8 parts per million by weight ICP10 Bismuth 20 parts per million by weight ICP40 <1 parts per million by weight ICP10 NGS sample #C-116889) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116889[8/31/2016 11:11:29 AM] Thorium 41 parts per million by weight ICP40 33.9 parts per million by weight INAA Uranium <100 parts per million by weight ICP40 9.38 parts per million by weight INAA Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-116889 Page Contact Information: Peter Schweitzer NGS sample #C-116900) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116900[8/30/2016 6:35:30 PM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-116900 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5286962 Lab identification number C-116900 Real field name NCMO065S1 Collection date 19760922 Field name as analyzed NCMO065 Description NURE STREAM SEDIMENT Location count 1 Sample set NURE Coastal 98 Sample type code 50 Map datum NAD27 Active channel width 2-4' Water depth 0.5-1.0' Water color clear Flow stage normal Flow rate mod Collector 57 Stream bed sand Relief low Vegetation deciduous Latitude 35.2093 Longitude -79.6284 1:24k quadrangle 36080SWC3 1:250k quadrangle 36080 1:100,000 quadrangle 36080SW FIPS of county f37125 Hydrologic unit 3040203 NGS sample #C-116900) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116900[8/30/2016 6:35:30 PM] Sample category NURE 1:250k quad name Raleigh Short description of sample type STRM-SED-WET Sample medium Sediment Sample source Stream Source modifier Wet Upper limit of sieve size 150 Drying procedure <110oC ICP40 job MRP-00821 As job number MRP-00827 Se job number MRP-00827 ICP10 job number MRP-00827 INAA job no. (USGS)WS84 Zip code, 3-digit 272 Congressional district 3706C2 Geographic context:Political divisions (FIPS codes) Moore (county) North Carolina (state) United States (country) North America (continent)Land (continent) USGS map quadrangles Norman (quadrangle 1:24,000 scale) Southern Pines (quadrangle 1:100,000 scale)Raleigh (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Lumber (hydrologic unit) Lower Pee Dee (hydrologic accounting unit)Pee Dee (hydrologic subregion) South Atlantic-Gulf (hydrologic region) Geologic map unit Middendorf Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method Lithium 3 parts per million by weight ICP40 Beryllium <1 parts per million by weight ICP40 Sodium 0.012 percent by weight ICP40 0.047 percent by weight INAA Magnesium 0.008 percent by weight ICP40 NGS sample #C-116900) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116900[8/30/2016 6:35:30 PM] Aluminum 0.427 percent by weight ICP40 Phosphorus 0.144 percent by weight ICP40 Potassium 0.29 percent by weight ICP40 Calcium 0.017 percent by weight ICP40 Scandium 10 parts per million by weight ICP40 9.88 parts per million by weight INAA Titanium 1.371 percent by weight ICP40 Vanadium 43 parts per million by weight ICP40 Chromium 2 parts per million by weight ICP40 Manganese 172 parts per million by weight ICP40 Iron 0.53 percent by weight ICP40 0.662 percent by weight INAA Cobalt <2 parts per million by weight ICP40 1.48 parts per million by weight INAA Nickel <3 parts per million by weight ICP40 <5.46 parts per million by weight INAA Copper 3 parts per million by weight ICP40 0.96 parts per million by weight ICP10 Zinc 10 parts per million by weight ICP40 5.79 parts per million by weight ICP10 91.3 parts per million by weight INAA Gallium <4 parts per million by weight ICP40 Arsenic 47 parts per million by weight ICP40 3.4 parts per million by weight As_AA <1 parts per million by weight ICP10 Selenium <0.2 parts per million by weight Se_AA Rubidium 7.56 parts per million by weight INAA Strontium 17 parts per million by weight ICP40 57.2 parts per million by weight INAA Yttrium 151 parts per million by weight ICP40 Zirconium 14000 parts per million by weight INAA Niobium 17 parts per million by weight ICP40 Molybdenum <2 parts per million by weight ICP40 0.2 parts per million by weight ICP10 Silver <2 parts per million by weight ICP40 NGS sample #C-116900) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116900[8/30/2016 6:35:30 PM] <0.08 parts per million by weight ICP10 Cadmium <2 parts per million by weight ICP40 <0.05 parts per million by weight ICP10 Tin 203 parts per million by weight ICP40 Antimony <1 parts per million by weight ICP10 0.331 parts per million by weight INAA Cesium 0.24 parts per million by weight INAA Barium 123 parts per million by weight ICP40 <291 parts per million by weight INAA Lanthanum 1410 parts per million by weight ICP40 1540 parts per million by weight INAA Cerium 2810 parts per million by weight ICP40 3390 parts per million by weight INAA Neodymium 1220 parts per million by weight ICP40 1450 parts per million by weight INAA Samarium 280 parts per million by weight INAA Europium 4 parts per million by weight ICP40 8.32 parts per million by weight INAA Terbium 23.8 parts per million by weight INAA Holmium 12 parts per million by weight ICP40 Ytterbium 4 parts per million by weight ICP40 35.3 parts per million by weight INAA Lutetium 5.46 parts per million by weight INAA Hafnium 353 parts per million by weight INAA Tantalum <40 parts per million by weight ICP40 24 parts per million by weight INAA Tungsten <7.18 parts per million by weight INAA Gold <8 parts per billion by weight ICP40 0.1 parts per billion by weight ICP10 <3.34 parts per billion by weight INAA Lead 52 parts per million by weight ICP40 13 parts per million by weight ICP10 Bismuth 48 parts per million by weight ICP40 <1 parts per million by weight ICP10 Thorium 746 parts per million by weight ICP40 NGS sample #C-116900) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-116900[8/30/2016 6:35:30 PM] 697 parts per million by weight INAA Uranium <100 parts per million by weight ICP40 107 parts per million by weight INAA Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-116900 Page Contact Information: Peter Schweitzer NGS sample #C-143341) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143341[8/30/2016 6:23:38 PM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-143341 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5287188 Lab identification number C-143341 Real field name NCRI003S1 Collection date 19760930 Field name as analyzed NCRI003S1 Description NURE sample, AEG014 1-02-318 Location count 1 Sample set NURE2000 Sample type code 750 Map datum NAD27 Active channel width 1-2' Water depth 0.5-1.0' Water color clear Flow stage dry Flow rate slow Collector 57 Stream bed boulders Relief low Vegetation conifers Latitude 35.0214 Longitude -79.5284 1:24k quadrangle 36080SWD4 1:250k quadrangle 36080 1:100,000 quadrangle 36080SW FIPS of county f37153 Hydrologic unit 3040203 NGS sample #C-143341) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143341[8/30/2016 6:23:38 PM] Sample category NURE 1:250k quad name Raleigh Short description of sample type STRM-SED-DRY Sample medium Sediment Sample source Stream Source modifier Dry Upper limit of sieve size 150 Drying procedure <110oC Sample type note Original NURE code was 50, but stream was dry ICP40 job MRP-01959 As job number MRP-01959 Se job number MRP-01959 Hg job number MRP-01959 Zip code, 3-digit 283 Congressional district 3708C2 Geographic context:Political divisions (FIPS codes) Richmond (county) North Carolina (state) United States (country) North America (continent)Land (continent) USGS map quadrangles Hoffman (quadrangle 1:24,000 scale) Southern Pines (quadrangle 1:100,000 scale)Raleigh (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Lumber (hydrologic unit) Lower Pee Dee (hydrologic accounting unit)Pee Dee (hydrologic subregion) South Atlantic-Gulf (hydrologic region) Federal lands Geologic map unit Middendorf Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method Lithium 3 parts per million by weight ICP40 Beryllium <1 parts per million by weight ICP40 Sodium 0.005 percent by weight ICP40 Magnesium 0.015 percent by weight ICP40 NGS sample #C-143341) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143341[8/30/2016 6:23:38 PM] Aluminum 0.72 percent by weight ICP40 Phosphorus 0.06 percent by weight ICP40 Potassium 0.04 percent by weight ICP40 Calcium 0.01 percent by weight ICP40 Scandium 6 parts per million by weight ICP40 Titanium 1.08 percent by weight ICP40 Vanadium 28 parts per million by weight ICP40 Chromium 20 parts per million by weight ICP40 Manganese 116 parts per million by weight ICP40 Iron 0.69 percent by weight ICP40 Cobalt <2 parts per million by weight ICP40 Nickel <3 parts per million by weight ICP40 Copper 7 parts per million by weight ICP40 Zinc 10 parts per million by weight ICP40 Gallium 8 parts per million by weight ICP40 Arsenic <10 parts per million by weight ICP40 7.2 parts per million by weight As_AA Selenium <0.2 parts per million by weight Se_AA Strontium 3 parts per million by weight ICP40 Yttrium 72 parts per million by weight ICP40 Niobium 20 parts per million by weight ICP40 Molybdenum <2 parts per million by weight ICP40 Silver <2 parts per million by weight ICP40 Cadmium <2 parts per million by weight ICP40 Tin <50 parts per million by weight ICP40 Barium 19 parts per million by weight ICP40 Lanthanum 584 parts per million by weight ICP40 Cerium 1120 parts per million by weight ICP40 Neodymium 476 parts per million by weight ICP40 Europium 3 parts per million by weight ICP40 Holmium <4 parts per million by weight ICP40 Ytterbium 2 parts per million by weight ICP40 Tantalum <40 parts per million by weight ICP40 Gold <8 parts per billion by weight ICP40 Mercury 0.04 parts per million by weight Hg_AA NGS sample #C-143341) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143341[8/30/2016 6:23:38 PM] Lead 18 parts per million by weight ICP40 Bismuth <50 parts per million by weight ICP40 Thorium 239 parts per million by weight ICP40 Uranium <100 parts per million by weight ICP40 Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-143341 Page Contact Information: Peter Schweitzer NGS sample #C-143589) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143589[8/31/2016 11:12:16 AM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-143589 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5286939 Lab identification number C-143589 Real field name NCMO042S1 Collection date 19760921 Field name as analyzed NCMO042S1 Description NURE sample, AEG016 1-02-566 Location count 1 Lab grain size Fine Sample set NURE2000 Sample type code 50 Color of reanalyzed powder tan Map datum NAD27 Active channel width 2-4' Water depth 0.5-1.0' Water color clear Flow stage low Flow rate slow Collector 57 Stream bed sand Relief low Vegetation conifers Latitude 35.235 Longitude -79.4938 1:24k quadrangle 36080SWE3 1:250k quadrangle 36080 1:100,000 quadrangle 36080SW NGS sample #C-143589) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143589[8/31/2016 11:12:16 AM] FIPS of county f37125 Hydrologic unit 3030004 Sample category NURE 1:250k quad name Raleigh Short description of sample type STRM-SED-WET Sample medium Sediment Sample source Stream Source modifier Wet Upper limit of sieve size 150 Drying procedure <110oC ICP40 job MRP-01961 As job number MRP-01961 Se job number MRP-01961 Hg job number MRP-01961 Zip code, 3-digit 273 Congressional district 3706C2 Geographic context:Political divisions (FIPS codes) Moore (county) North Carolina (state) United States (country)North America (continent) Land (continent) USGS map quadrangles Southern Pines (quadrangle 1:24,000 scale)Southern Pines (quadrangle 1:100,000 scale) Raleigh (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Upper Cape Fear (hydrologic unit)Cape Fear (hydrologic accounting unit) Cape Fear (hydrologic subregion) South Atlantic-Gulf (hydrologic region) Geologic map unit Middendorf Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method Lithium 3 parts per million by weight ICP40 Beryllium <1 parts per million by weight ICP40 Sodium 0.015 percent by weight ICP40 Magnesium 0.016 percent by weight ICP40 NGS sample #C-143589) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143589[8/31/2016 11:12:16 AM] Aluminum 0.72 percent by weight ICP40 Phosphorus 0.005 percent by weight ICP40 Potassium 0.38 percent by weight ICP40 Calcium 0.017 percent by weight ICP40 Scandium 2 parts per million by weight ICP40 Titanium 0.406 percent by weight ICP40 Vanadium 16 parts per million by weight ICP40 Chromium 24 parts per million by weight ICP40 Manganese 47 parts per million by weight ICP40 Iron 0.41 percent by weight ICP40 Cobalt <2 parts per million by weight ICP40 Nickel <3 parts per million by weight ICP40 Copper 3 parts per million by weight ICP40 Zinc 4 parts per million by weight ICP40 Gallium <4 parts per million by weight ICP40 Arsenic <10 parts per million by weight ICP40 1.1 parts per million by weight As_AA Selenium <0.2 parts per million by weight Se_AA Strontium 20 parts per million by weight ICP40 Yttrium 6 parts per million by weight ICP40 Niobium 8 parts per million by weight ICP40 Molybdenum <2 parts per million by weight ICP40 Silver <2 parts per million by weight ICP40 Cadmium <2 parts per million by weight ICP40 Tin <50 parts per million by weight ICP40 Barium 147 parts per million by weight ICP40 Lanthanum 31 parts per million by weight ICP40 Cerium 60 parts per million by weight ICP40 Neodymium 25 parts per million by weight ICP40 Europium 1 parts per million by weight ICP40 Holmium <4 parts per million by weight ICP40 Ytterbium <1 parts per million by weight ICP40 Tantalum <40 parts per million by weight ICP40 Gold <8 parts per billion by weight ICP40 parts per million by weight Hg_AA NGS sample #C-143589) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143589[8/31/2016 11:12:16 AM] Mercury 0.08 Lead 9 parts per million by weight ICP40 Bismuth <50 parts per million by weight ICP40 Thorium 14 parts per million by weight ICP40 Uranium <100 parts per million by weight ICP40 Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-143589 Page Contact Information: Peter Schweitzer NGS sample #C-143670) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143670[8/30/2016 6:37:41 PM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-143670 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5286967 Lab identification number C-143670 Real field name NCMO070S1 Collection date 19760922 Field name as analyzed NCMO070S1 Description NURE sample, AEG017 1-02-647 Location count 1 Lab grain size Coarse Sample set NURE2000 Sample type code 50 Color of reanalyzed powder tan Map datum NAD27 Active channel width 2-4' Water depth 0.5-1.0' Water color clear Flow stage normal Flow rate mod Collector 57 Stream bed sand Relief low Vegetation deciduous Latitude 35.2883 Longitude -79.5946 1:24k quadrangle 36080SWD2 1:250k quadrangle 36080 1:100,000 quadrangle 36080SW NGS sample #C-143670) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143670[8/30/2016 6:37:41 PM] FIPS of county f37125 Hydrologic unit 3030003 Sample category NURE 1:250k quad name Raleigh Short description of sample type STRM-SED-WET Sample medium Sediment Sample source Stream Source modifier Wet Upper limit of sieve size 150 Drying procedure <110oC ICP40 job MRP-01962 As job number MRP-01962 Se job number MRP-01962 Hg job number MRP-01962 Zip code, 3-digit 272 Congressional district 3706C2 Geographic context:Political divisions (FIPS codes) Moore (county) North Carolina (state) United States (country)North America (continent) Land (continent) USGS map quadrangles Zion Grove (quadrangle 1:24,000 scale)Southern Pines (quadrangle 1:100,000 scale) Raleigh (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Deep (hydrologic unit)Cape Fear (hydrologic accounting unit) Cape Fear (hydrologic subregion) South Atlantic-Gulf (hydrologic region) Geologic map unit Newark Supergroup, Chatham Group; Pekin Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method Lithium 15 parts per million by weight ICP40 Beryllium 1 parts per million by weight ICP40 Sodium 0.305 percent by weight ICP40 Magnesium 0.361 percent by weight ICP40 NGS sample #C-143670) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143670[8/30/2016 6:37:41 PM] Aluminum 3.802 percent by weight ICP40 Phosphorus 0.064 percent by weight ICP40 Potassium 0.91 percent by weight ICP40 Calcium 0.082 percent by weight ICP40 Scandium 12 parts per million by weight ICP40 Titanium 1.011 percent by weight ICP40 Vanadium 73 parts per million by weight ICP40 Chromium 43 parts per million by weight ICP40 Manganese 416 parts per million by weight ICP40 Iron 2.63 percent by weight ICP40 Cobalt 13 parts per million by weight ICP40 Nickel 18 parts per million by weight ICP40 Copper 23 parts per million by weight ICP40 Zinc 42 parts per million by weight ICP40 Gallium 9 parts per million by weight ICP40 Arsenic 12 parts per million by weight ICP40 4.7 parts per million by weight As_AA Selenium <0.2 parts per million by weight Se_AA Strontium 43 parts per million by weight ICP40 Yttrium 77 parts per million by weight ICP40 Niobium 33 parts per million by weight ICP40 Molybdenum <2 parts per million by weight ICP40 Silver <2 parts per million by weight ICP40 Cadmium <2 parts per million by weight ICP40 Tin <50 parts per million by weight ICP40 Barium 312 parts per million by weight ICP40 Lanthanum 505 parts per million by weight ICP40 Cerium 953 parts per million by weight ICP40 Neodymium 469 parts per million by weight ICP40 Europium 3 parts per million by weight ICP40 Holmium <4 parts per million by weight ICP40 Ytterbium 3 parts per million by weight ICP40 Tantalum <40 parts per million by weight ICP40 Gold <8 parts per billion by weight ICP40 parts per million by weight Hg_AA NGS sample #C-143670) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143670[8/30/2016 6:37:41 PM] Mercury 0.06 Lead 29 parts per million by weight ICP40 Bismuth <50 parts per million by weight ICP40 Thorium 258 parts per million by weight ICP40 Uranium <100 parts per million by weight ICP40 Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-143670 Page Contact Information: Peter Schweitzer NGS sample #C-143893) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143893[8/31/2016 11:13:40 AM] USGS Home Contact USGS Search USGS Mineral Resources On-Line Spatial Data Mineral Resources > Online Spatial Data > National Geochemical Survey NGS sample C-143893 View location using [Google Earth] or [Google Maps] Field Value NURE record ID 5285098 Lab identification number C-143893 Real field name NCSC019S1 Collection date 19770810 Field name as analyzed NCSC019S1 Description NURE sample, AEG019 1-02-870 Location count 1 Lab grain size Fine Sample set NURE2000 Sample type code 50 Color of reanalyzed powder tan Map datum NAD27 Active channel width 4-8' Water depth 1-2' Water color brown/clear Flow stage normal Flow rate mod Collector 123 Stream bed sand Relief low Vegetation swamp Latitude 34.9908 Longitude -79.5188 1:24k quadrangle 35080NWD1 1:250k quadrangle 35080 1:100,000 quadrangle 35080NW NGS sample #C-143893) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143893[8/31/2016 11:13:40 AM] FIPS of county f37165 Hydrologic unit 3040203 Sample category NURE 1:250k quad name Florence Short description of sample type STRM-SED-WET Sample medium Sediment Sample source Stream Source modifier Wet Upper limit of sieve size 150 Drying procedure <110oC ICP40 job MRP-01964 As job number MRP-01964 Se job number MRP-01964 Hg job number MRP-01964 Zip code, 3-digit 283 Congressional district 3708C2 Geographic context:Political divisions (FIPS codes) Scotland (county) North Carolina (state) United States (country)North America (continent) Land (continent) USGS map quadrangles Marston (quadrangle 1:24,000 scale)Laurinburg (quadrangle 1:100,000 scale) Florence (quadrangle 1:250,000 scale) Hydrologic units (watersheds) Lumber (hydrologic unit)Lower Pee Dee (hydrologic accounting unit) Pee Dee (hydrologic subregion) South Atlantic-Gulf (hydrologic region) Geologic map unit Middendorf Formation Nearby scientific data Find additional scientific data near this location Chemical analyses Element Measured value Units of measure Analytical method Lithium 3 parts per million by weight ICP40 Beryllium <1 parts per million by weight ICP40 Sodium 0.009 percent by weight ICP40 Magnesium 0.015 percent by weight ICP40 NGS sample #C-143893) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143893[8/31/2016 11:13:40 AM] Aluminum 0.757 percent by weight ICP40 Phosphorus 0.015 percent by weight ICP40 Potassium 0.08 percent by weight ICP40 Calcium 0.011 percent by weight ICP40 Scandium 11 parts per million by weight ICP40 Titanium 0.56 percent by weight ICP40 Vanadium 14 parts per million by weight ICP40 Chromium 28 parts per million by weight ICP40 Manganese 100 parts per million by weight ICP40 Iron 0.71 percent by weight ICP40 Cobalt <2 parts per million by weight ICP40 Nickel <3 parts per million by weight ICP40 Copper 7 parts per million by weight ICP40 Zinc 7 parts per million by weight ICP40 Gallium 7 parts per million by weight ICP40 Arsenic <10 parts per million by weight ICP40 12.8 parts per million by weight As_AA Selenium 1.2 parts per million by weight Se_AA Strontium 3 parts per million by weight ICP40 Yttrium 52 parts per million by weight ICP40 Niobium 7 parts per million by weight ICP40 Molybdenum <2 parts per million by weight ICP40 Silver <2 parts per million by weight ICP40 Cadmium <2 parts per million by weight ICP40 Tin <50 parts per million by weight ICP40 Barium 51 parts per million by weight ICP40 Lanthanum 363 parts per million by weight ICP40 Cerium 710 parts per million by weight ICP40 Neodymium 331 parts per million by weight ICP40 Europium 1 parts per million by weight ICP40 Holmium <4 parts per million by weight ICP40 Ytterbium 2 parts per million by weight ICP40 Tantalum <40 parts per million by weight ICP40 Gold <8 parts per billion by weight ICP40 parts per million by weight Hg_AA NGS sample #C-143893) http://mrdata.usgs.gov/ngs/show-ngs.php?labno=C-143893[8/31/2016 11:13:40 AM] Mercury 0.03 Lead 23 parts per million by weight ICP40 Bismuth <50 parts per million by weight ICP40 Thorium 148 parts per million by weight ICP40 Uranium <100 parts per million by weight ICP40 Show this information as [XML] - [GeoJSON] - [RDF] Accessibility FOIA Privacy Policies and Notices U.S. Department of the Interior | U.S. Geological Survey URL: http://mrdata.usgs.gov/geochem/show-ngs-xml.php?lab_id=C-143893 Page Contact Information: Peter Schweitzer APPENDIX E EPA NATURAL ATTENUATION SCREENING PROTOCOL FORMS AND PLOTS, MNA EVALUATION TABLE, AND BIOCHLOR MNA ANALYSIS FOR APRIL 2016 SAMPLING EVENT Reviewed By: DYR Prepared By: BSD Project #:0739615015 DATE: 08/31/16 Figure No. 1 Title: MW-6 MNA SCREENING Moore County Landfill, Permit No. 63-01 Reviewed By: DYR Prepared By: BSD Project #:0739615015 DATE: 08/31/16 Figure No. 2 Title: MW-11S MNA SCREENING Moore County Landfill, Permit No. 63-01 Reviewed By: DYR Prepared By: BSD Project #: 0739615015 DATE: 08/31/16 Figure No. 3 Title: MW-4 MNA SCREENING Moore County Landfill, Permit No. 63-01 Reviewed By: DYR Prepared By: BSD Project #: 0739615015 DATE: 08/31/16 Figure No. 4 Title: MW-15 MNA SCREENING Moore County Landfill, Permit No. 63-01 Reviewed By: DYR Prepared By: BSD Project #: 0739615015 DATE: 08/31/16 Figure No. 5 Title: BIOCHLOR SUMMARY Moore County Landfill, Permit # 61-03 Moore County, North Carolina Biochlor Model: Results and Predictions 2014