1303_USTire_April2017_1stSemiAnnual_DIN27785_20170508

11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]

Explanatory Text for Notification Table
US Tire Monofill Landfill
Concord, Cabarrus, NC
Permit # 13-03
April 6, 2017 Water Quality Monitoring

The results of the April 2017 groundwater and surface water quality monitoring conducted at the
US Tire Monofill Landfill are generally consistent with the results of previous monitoring
conducted at the site. Acetone was detected in trace concentrations in the samples collected
from surface water sampling locations SW-1, SW-4, and SW-5. The concentrations of acetone
detected are all well below the 15A NCAC 2B surface water quality standard for fresh water
aquatic life. Moreover, SW-1 is an upstream sampling location on Coddle Creek at the
northeast corner of the site that provides an indication of surface water quality upstream of the
site. Acetone is a common laboratory contaminant introduced to samples during preparation for
analysis. Given that acetone was detected in the surface water sample collected from upstream
sampling location SW-1 at a similar concentration to those reported at sampling locations SW-4
and SW-5, it is possible that acetone detected in the samples is an artifact of sample
preparation in the laboratory. In addition, benzene, methyl ethyl ketone (MEK), and methyl
isobutyl ketone (MIBK) were detected in the surface water sample collected from sampling
location SW-5 at trace concentrations well below the applicable 15A NCAC 2B surface water
quality standards for fresh water aquatic life. Various RCRA metals were reported in all of the
surface water samples. The estimated concentration of silver reported in the sample collected
from surface water sampling location SW-2 slightly exceed the 15A NCAC 2B surface water
quality standards for fresh water aquatic life (0.71 µg/L vs. 0.60 µg/L). It is noted, however, that
surface water sampling location SW-2 is located on the landfill property, and no exceedances of
surface water quality standards for any analytes were observed at sampling location SW-4,
which is a downstream sampling location on Coddle Creek at the southeast corner of the site.
No other reported concentrations of RCRA metals exceed the applicable 15A NCAC 2B surface
water quality standards for fresh water aquatic life.

Various RCRA metals were detected in all of the groundwater samples collected from the site
monitoring wells on April 6, 2017. Cadmium was reported at a concentration of 3.5 µg/L in the
groundwater sample collected from monitoring well MW-7, which slightly exceeds the
corresponding 15A NCAC 2L groundwater quality standards of 2.0 µg/L. None of the other
RCRA metals were detected in any of the groundwater samples at concentrations exceeding the
corresponding 15A NCAC 2L groundwater quality standards. Acetone was detected at a trace
concentration well below the 15A NCAC 2L groundwater quality standard in the groundwater
– 2 – May 8, 2017
sample collected from monitoring well MW-5A. In addition, chloroform was detected at a trace
concentration well below the 15A NCAC 2L groundwater quality standard in the groundwater
sample collected from background monitoring well MW-1. Further, bromodichloromethane was
detected at a concentration of 0.97 µg/L in the groundwater sample collected from up gradient
background monitoring well MW-1, which slightly exceeds the 15A NCAC 2L groundwater
quality standard of 0.60 µg/L. No other Appendix I VOCs were detected in any of the
groundwater samples collected in April 2017.

11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]

May 5, 2017

Ms. Elizabeth S. Werner, Hydrogeologist
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
1646 Mail Service Center
Raleigh, NC 27699-1646

RE: Report of Results
Semi-Annual Groundwater and Surface Water Monitoring: April 2017
US Tire Monofill Landfill
Concord, Cabarrus County, NC
Permit # 13-03

Dear Ms. Werner:

This report presents the results of semi-annual groundwater and surface water quality
monitoring conducted at the landfill site referenced above (Figure 1) in April 2017. The scope
of work performed included sampling and laboratory analysis of groundwater samples from 8
on-site monitoring wells and surface water samples from five on-site locations. It is noted that
monitoring well MW-4 was abandoned on January 31, 2011 due to landfill expansion. It is
further noted that no groundwater sample was collected from monitoring well MW-2A in April
2017 due to flooding conditions at the time of sampling that encompassed the area of the well.
The groundwater and surface water samples were collected in accordance with the NCDEQ,
Division of Waste Management (DWM), Solid Waste Section (SWS), Groundwater Monitoring
Guidance Document and the facility Water Quality Monitoring Plan. The sampling and data
collection methods, as well as the current and historical results of field and laboratory testing of
the water samples, are presented in the following sections.

1.0 POTENTIOMETRIC PATTERN AND GROUNDWATER FLOW

Groundwater levels were gauged in the site groundwater monitoring wells on April 6, 2017 as
part of the site monitoring. Depths to groundwater were measured using an electronic water
level probe that was thoroughly decontaminated between wells with a non-phosphate soap and
water wash followed in order by multiple rinses with distilled water, an isopropyl alcohol rinse,
and multiple distilled water rinses. Depth-to-water measurements were made after the wells
were opened for a sufficient period of time to allow water levels to equilibrate with atmospheric
– 2 – May 5, 2017
11112 Branding Iron Place, Wendell, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
pressure. The locations of the site monitoring wells are depicted in Figure 2. Groundwater
elevation data collected at the monitoring wells in April 2017 are presented in Table 1. The
depth to groundwater across the site, as measured in the Type II groundwater-monitoring wells,
ranged from approximately 2.54 (MW-10) to 39 (MW-1) feet below the tops of the PVC well
casings, which is consistent with the surface topography.

A water-table elevation contour map that was developed based on the April 6, 2017
groundwater-gauging data for the Type II monitoring wells is presented as Figure 3. The
pattern of the water-table contours indicates that the horizontal component of shallow
groundwater flow at the site is generally to the northeast toward Coddle Creek, which is
consistent with the surface topography and drainage features at the site. The hydraulic gradient
of the water table, based on the data depicted in Figure 3, is approximately 0.041 ft./ft. over the
west-southwest area of the site and transitions to approximately 0.018 ft./ft. in the east-
northeast part of the site near Coddle Creek.

2.0 RESULTS OF GROUNDWATER AND SURFACE WATER SAMPLING AND ANALYSIS

Groundwater samples were collected from the site monitoring wells (except MW-2A, as
discussed above) and surface water samples were collected from three on-site locations, as
well as two locations on Coddle Creek, on April 6, 2017 for laboratory analysis to monitor the
quality of groundwater and surface water at the site. The groundwater and surface water
samples were collected and handled in accordance with the sampling protocols included in the
site Water Quality Monitoring Plan as well as the SWS Groundwater Monitoring Guidance
Document. All reusable sampling equipment was properly decontaminated between sampling
locations with a non-phosphate soap and water wash, followed by multiple rinses with distilled
water. Disposable sampling equipment/material was discarded after each use.

The locations of the groundwater monitoring wells at the site are depicted in Figure 2. Prior to
groundwater sampling, all monitoring wells, with the exception of MW-1, were purged using
Teflon-lined disposable polyethylene tubing connected to a peristaltic pump under low flow
conditions. Monitoring well MW-1 was purged and sampled using a 12-volt submersible pump
under low-flow conditions. During purging, measurements were made in the field of the pH,
temperature, specific conductance and turbidity of the groundwater collected from the
monitoring wells, in accordance with SWS requirements. The results of the field analyses of
these parameters are presented in Table 1. Copies of Groundwater Sampling Forms containing
pertinent information recorded in the field during purging and sampling at each groundwater
monitoring well are presented in Appendix A. The results of the field-measured water-quality
parameters indicate that the values measured in groundwater collected from the site monitoring
wells were generally within the applicable stabilization criteria (see Groundwater Sampling
Forms). Groundwater at the site is slightly acidic to neutral based on the pH values measured
in the field (5.55 to 6.86). Specific conductance values ranged from 62 (MW-8) to 598 (MW-5A)
– 3 – May 5, 2017
11112 Branding Iron Place, Wendell, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
µS/cm, and turbidity values ranged from 0.6 (MW-1) to 123 (MW-8) nephelometric turbidity units
(NTUs).

Surface water samples were collected from five locations at the site (SW-1 through SW-5). The
sampling locations are depicted in Figure 2. SW-1 is an upstream sampling location on Coddle
Creek at the northeast corner of the site; SW-2, SW-3 and SW-5 are sampling locations along
site streams that discharge to Coddle Creek; SW-4 is a downstream sampling location on
Coddle Creek at the southeast corner of the site. Coddle Creek is classified as a Class C
surface water by the NCDEQ Division of Water Quality. All surface water samples were
collected in accordance with the protocol presented in the SWS Groundwater Monitoring
Guidance Document.

All groundwater and surface water samples were analyzed at a North Carolina-certified
laboratory for Appendix I volatile organic compounds (VOCs) by SW 846 Method 8260 and the
8 RCRA metals by EPA 6000/7000 series methods. Summarized results of laboratory analyses
for groundwater and surface water samples collected from the site on April 6, 2017 are
presented in Table 2. Summarized historical groundwater and surface water quality data for the
site are presented in Table 3. Copies of the original laboratory reports are included in
Appendix B.

The laboratory analytical results for the surface water samples collected from the site on April 6.
2017 indicate that acetone was detected in trace concentrations in the samples collected from
surface water sampling locations SW-1, SW-4, and SW-5. The concentrations of acetone
detected are all well below the 15A NCAC 2B surface water quality standard for fresh water
aquatic life. Moreover, SW-1 is an upstream sampling location on Coddle Creek at the
northeast corner of the site that provides an indication of surface water quality upstream of the
site. In addition, benzene, methyl ethyl ketone (MEK), and methyl isobutyl ketone (MIBK) were
detected in the surface water sample collected from sampling location SW-5 at trace
concentrations well below the applicable 15A NCAC 2B surface water quality standards for fresh
water aquatic life. Various RCRA metals were reported in all of the surface water samples. The
estimated concentration of silver reported in the sample collected from surface water sampling
location SW-2 slightly exceed the 15A NCAC 2B surface water quality standards for fresh water
aquatic life (0.71 µg/L vs. 0.60 µg/L). It is noted, however, that surface water sampling location
SW-2 is located on the landfill property, and no exceedances of surface water quality standards
for any analytes were observed at sampling location SW-4, which is a downstream sampling
location on Coddle Creek at the southeast corner of the site. No other reported concentrations
of RCRA metals exceed the applicable 15A NCAC 2B surface water quality standards for fresh
water aquatic life.

– 4 – May 5, 2017
11112 Branding Iron Place, Wendell, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
The laboratory analytical results for the groundwater samples collected from the site monitoring
wells on April 6, 2017 indicate that low levels of various RCRA metals were detected in all of the
samples. Cadmium was reported at a concentration of 3.5 µg/L in the groundwater sample
collected from monitoring well MW-7, which slightly exceeds the corresponding 15A NCAC 2L
groundwater quality standards of 2.0 µg/L. None of the other RCRA metals were detected in
any of the groundwater samples at concentrations exceeding the corresponding 15A NCAC 2L
groundwater quality standards. Acetone was detected at a trace concentration well below the
15A NCAC 2L groundwater quality standard in the groundwater sample collected from
monitoring well MW-5A. In addition, chloroform was detected at a trace concentration well
below the 15A NCAC 2L groundwater quality standard in the groundwater sample collected from
background monitoring well MW-1. Further, bromodichloromethane was detected at a
concentration of 0.97 µg/L in the groundwater sample collected from background monitoring
well MW-1, which slightly exceeds the 15A NCAC 2L groundwater quality standard of 0.60 µg/L.
No other Appendix I VOCs were detected in any of the groundwater samples collected in April
2017.

CONCLUSIONS AND RECOMMENDATIONS

The results of the April 2017 groundwater and surface water quality monitoring conducted at the
US Tire Monofill Landfill are generally consistent with the results of previous monitoring
conducted at the site. Acetone was detected in trace concentrations in the samples collected
from surface water sampling locations SW-1, SW-4, and SW-5. The concentrations of acetone
detected are all well below the 15A NCAC 2B surface water quality standard for fresh water
aquatic life. Moreover, SW-1 is an upstream sampling location on Coddle Creek at the
northeast corner of the site that provides an indication of surface water quality upstream of the
site. Acetone is a common laboratory contaminant introduced to samples during preparation for
analysis. Given that acetone was detected in the surface water sample collected from upstream
sampling location SW-1 at a similar concentration to those reported at sampling locations SW-4
and SW-5, it is possible that acetone detected in the samples is an artifact of sample
preparation in the laboratory. In addition, benzene, methyl ethyl ketone (MEK), and methyl
isobutyl ketone (MIBK) were detected in the surface water sample collected from sampling
location SW-5 at trace concentrations well below the applicable 15A NCAC 2B surface water
quality standards for fresh water aquatic life. Various RCRA metals were reported in all of the
surface water samples. The estimated concentration of silver reported in the sample collected
from surface water sampling location SW-2 slightly exceed the 15A NCAC 2B surface water
quality standards for fresh water aquatic life (0.71 µg/L vs. 0.60 µg/L). It is noted, however, that
surface water sampling location SW-2 is located on the landfill property, and no exceedances of
surface water quality standards for any analytes were observed at sampling location SW-4,
which is a downstream sampling location on Coddle Creek at the southeast corner of the site.
No other reported concentrations of RCRA metals exceed the applicable 15A NCAC 2B surface
water quality standards for fresh water aquatic life.
– 5 – May 5, 2017
11112 Branding Iron Place, Wendell, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]

Various RCRA metals were detected in all of the groundwater samples collected from the site
monitoring wells on April 6, 2017. Cadmium was reported at a concentration of 3.5 µg/L in the
groundwater sample collected from monitoring well MW-7, which slightly exceeds the
corresponding 15A NCAC 2L groundwater quality standards of 2.0 µg/L. None of the other
RCRA metals were detected in any of the groundwater samples at concentrations exceeding the
corresponding 15A NCAC 2L groundwater quality standards. Acetone was detected at a trace
concentration well below the 15A NCAC 2L groundwater quality standard in the groundwater
sample collected from monitoring well MW-5A. In addition, chloroform was detected at a trace
concentration well below the 15A NCAC 2L groundwater quality standard in the groundwater
sample collected from background monitoring well MW-1. Further, bromodichloromethane was
detected at a concentration of 0.97 µg/L in the groundwater sample collected from up gradient
background monitoring well MW-1, which slightly exceeds the 15A NCAC 2L groundwater
quality standard of 0.60 µg/L. No other Appendix I VOCs were detected in any of the
groundwater samples collected in April 2017. Based on the results of the April 2017 water
quality monitoring event, no changes in the semiannual monitoring program are recommended.

If you have any questions or require further assistance regarding this report, please call me at
919-995-0363. The next water quality monitoring event for the US Tire Monofill Landfill is
scheduled for October 2017.

Sincerely,
Brian S. Boutin, P.G.
Consulting Geologist

Cc: Gene Helton, General Manager, US Tire Recycling
Vance Moore, Garrett and Moore, Inc.
Craig Fortner, Garrett and Moore, Inc.
Garrett and Moore, Inc.
Engineering Consulting Services
1428 Aversboro Rd., Suite D, Garner, NC 27529
Tel: [phone] Fax: [phone]
Drawn by:Reviewed by:Drawing #:
Drawing Date:1
SITE LOCATION MAP
US Tire Monofill Landfill
6322 Poplar Tent Rd.
Concord, Cabarrus County, North Carolina
Source: USGS 7.5’ Topographic Quadrangle Series
Kannapolis, North Carolina 1996
Figure No.Project #:
Scale:USGS USGS
1:24,000 6/11/07
UST0607-1
N
SCALE
020001000 1000 2000
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Wendell, NC 27591
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Cell: [phone]
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MW-1 66.7 4.0 696.50 39.17 657.33 16.9 5.55 131 0.6
MW-2A 18.8 2.0 651.78 NG ----NS NS NS NS
MW-3 31.6 4.0 614.43 11.68 602.75 17.4 6.51 528 6.9
MW-4
MW-5A 20.0 2.0 605.96 6.54 599.42 15.3 6.53 598 3.02
MW-6 17.6 2.0 603.36 10.34 593.02 14.8 5.98 243 19.1
MW-7 19.9 2.0 602.07 8.93 593.14 15.9 6.59 327 4.64
MW-8 17.8 2.0 601.08 10.32 590.76 14.5 5.65 62 123
MW-9 51.6 2.0 614.38 20.36 594.02 18.0 6.86 330 0.74
MW-10 25.1 2.0 599.17 2.51 596.66 15.8 5.92 364 8.1
Notes:BTOC = Below Top of Casing NG - Not Gauged; area around well flooded at time of site monitoring.
GW = Groundwater NS- Not Sampled; area around well flooded at time of site monitoring
S.C. = Specific Conductance
ntu = Nephelometric Turbidity Units
Depth to GW
BTOC (Feet)
Well Diameter
(Inches)
Field Parameters
Turbidity
(ntu)
Top of Casing
Elevation
(Feet)
Groundwater
Elevation
(Feet)
Monitoring Well and Groundwater Data
Table 1
April 2017 Sampling Event
US Tire Monofill Landfill
Cabarras County, North Carolina
Well
Identity Temp. Co
Well Depth
BTOC (Feet)
April 6, 2017
pH S.C.
umhos/cm
Abandoned due to landfill expansion
ORGANIC CONSTITUENTS GWP Std NCAC 2L STD
(ug/L)(ug/L)(ug/L)
Acetone 5.5 ND ND 5.5 7 ND NS ND 5.1 ND ND ND ND ND NE 6000
Acrylonitrile ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE NE
Benzene ND ND ND ND 3.2 ND NS ND ND ND ND ND ND ND NE 1
Bromochloromethane ND ND ND ND ND ND NS ND ND ND ND ND ND ND 0.6 NE
Bromodichloromethane ND ND ND ND ND 0.97 NS ND ND ND ND ND ND ND NE 0.6
Bromoform (Tribromomethane)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 4
Bromomethane (Methyl Bromide)ND ND ND ND ND ND NS ND ND ND ND ND ND ND 10 10
2-Butanone (MEK), (Methyl Ethyl Ketone)ND ND ND ND 6.8 ND NS ND ND ND ND ND ND ND NE 4000
Carbon Disulfide ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 700
Carbon Tetrachloride ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 0.3
Chlorobenzene ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 50
Chloroethane (Ethyl Chloride)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 3000
Chloroform (Trichloromethane)ND ND ND ND ND 0.63 NS ND ND ND ND ND ND ND NE 70
1,2-Dibromo-3-Chloropropane (DBCP)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 0.04
Dibromochloromethane (Chlorodibromomethane)ND ND ND ND ND ND NS ND ND ND ND ND ND ND 0.41 0.4
1,2,-Dibromoethane (Ethylene Dibromide)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 0.02
Dibromomethane (Methylene Bromide)ND ND ND ND ND ND NS ND ND ND ND ND ND ND 5.5 70
1,2-Dichlorobenzene (O-Dichlorobenzene)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 20
1,3-Dichlorobenzene (M-Dichlorobenzene)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 200
1,4-Dichlorobenzene (P-Dichlorobenzene)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 6
Trans-1,4-Dichloro-2-butene ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE NE
1,1-Dichloroethane ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 6
1,2-Dichloroethane (Ethylene Dichloride)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 0.4
1,1-Dichloroethene (Vinylidene Chloride)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 7
1,2-Dichloroethene (cis and trans isomers))ND ND ND ND ND ND NS ND ND ND ND ND ND ND 60 60
1,2-Dichloropropane (Propylene Dichloride)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 0.6
1,1-Dichloropropene ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE NE
1,3-Dichloropropene (cis and trans isomers)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 0.4
Ethylbenzene ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 600
Iodomethane (Methyl Iodide)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE NE
2-Hexanone (Methyl Butyl Ketone)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 280
Methyl Chloride (Chloromethane)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 3
Methylene Chloride (Dichloromethane)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 5
4-Methyl-2-Pentanone (Methyl Isobutyl Ketone)ND ND ND ND 4.1 J ND NS ND ND ND ND ND ND ND 560 NE
Styrene ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 70
1,1,1,2-Tetrachloroethane ND ND ND ND ND ND NS ND ND ND ND ND ND ND 1 1
1,1,2,2-Tetrachloroethane ND ND ND ND ND ND NS ND ND ND ND ND ND ND 0.18 0.2
Tetrachloroethene (Tetrachloroethylene), (PCE)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 0.7
Tetrahydrofuran ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE NE
Toluene ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 600
1,1,1-Trichloroethane (Methylchloroform)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 200
1,1,2-Trichloroethane ND ND ND ND ND ND NS ND ND ND ND ND ND ND 0.6 0.6
Trichloroethene (Trichloroethylene), (TCE)ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 3
Trichlorofluoromethane (CFC-11) ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 2000
1,2,3-Trichloropropane ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 0.005
Vinyl Acetate ND ND ND ND ND ND NS ND ND ND ND ND ND ND 88 88
Vinyl Chloride ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 0.03
Total Xylenes ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 500
INORGANIC CONSTITUENTS GWP Std NCAC 2L STD
(in ug/L)(ug/L)(ug/L)
Arsenic ND ND ND ND 1.0 ND NS ND ND ND ND 1.20 ND ND NE 10
Barium 45 75 67 48 180 21 NS 130 160 120 140 59 110 180 NE 700
Cadmium ND ND ND ND 0.082 J ND NS 0.082 J 0.11 J ND 3.5 0.11 J 0.059 J 0.065 J NE 2
Chromium 2.7 0.57 J ND 2.40 4.3 0.35 J NS ND 0.32 J ND ND 10 ND 0.47 J NE 10
Lead 0.89 J 0.67 J 0.10 J 0.84 J 9.4 0.21 J NS 0.47 J 0.12 J 0.15 J 0.25 J 2.8 0.096 J 0.082 J NE 15
Mercury ND ND ND ND ND ND NS ND ND ND ND ND ND ND NE 1
Selenium 1.2 J ND ND 0.64 J 1.8 J 0.78 J NS ND ND 0.54 J ND 3.9 J ND ND NE 20
Silver ND 0.071 J ND ND ND ND NS 0.070 J ND 0.39 J 0.16 J 0.088 J 0.12 J 0.12 J NE 20
Notes:
Values in boldface exceed the corresponding 15A NCAC 2L .0202 groundwater quality standard for Class GA groundwater or 15A NCAC 2B surface water quality standard for freshwater aquatic life.
NCAC 2L STD = North Carolina Groundwater Standard established in Title 15A of North Carolina Administrative Code Subchapter 2L
GWP Std = Solid Waste Section Groundwater Protection Standard NE = No standard established
ND = None detected above laboratory method detection limit.B = Analyte found in associated field and/or laboratory blank.
J = Estimated value above laboratory method detection limit and below SWSL or reporting limit. NS = Not Sampled, No sample exists for this sampling period
Table 2
SW-1 MW-10MW-1SW-2 SW-5 MW-9MW-5A MW-6
US Tire Monofil Landfill, Concord, NC
MW-7 MW-8SW-3
April 6, 2017
April 2017 Sampling Event
Laboratory Results for Surface Water and Groundwater Samples
Permit # 13-03
MW-2A MW-3SW-4
Page 1 of 4
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-1
Arsenic 10 ND ND ND ND ND ND ND 0.30 J ND ND 1.3 J 0.53 J 0.53 J ND ND ND 20 ND ND ND
Barium 700 21.6 JB 31.4 JB 28.0 JB 35.0 JB 12.3 J 24.0 17 J 18.0 17.0 20.0 20.0 19.0 18.0 18 18 19 0.14 J 20.00 21 21
Cadmium 2 ND ND ND ND ND ND ND ND ND ND 0.34 J 0.041 J 0.67 J,B 0.070 J 0.095 J ND 0.96 J 0.13 J 0.089 J ND
Chromium 10 ND 3.22 JB 3.68 JB 2.17 JB ND ND ND 3.4 B 3.30 ND 1.5 B ND ND 0.68 JB 1.30 ND 0.14 J 1.8 JB 0.91 J 0.35 J
Lead 15 ND 8.09 JB 7.86 JB ND ND 0.58 ND 0.33 J 0.31 J 0.19 J 0.51 J ND 0.40 J 0.15 J 0.28 J ND ND 0.58 J 0.25 J 0.21 J
Mercury 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.37 J ND ND ND
Selenium 20 8.15 JB ND ND ND ND ND ND ND 0.84 J 1.0 JB ND 0.59 J ND ND ND ND 0.045 J ND ND 0.78 J
Silver 20 2.11 JB 3.42 JB 7.38 JB 2.62 JB 2.83 JB ND ND ND 0.17 J 0.063 JB 0.37 J 0.026 J 0.047 J ND ND ND ND 0.020 J ND ND
Acetone 6000 ND ND ND ND 2.81 J ND ND ND ND ND ND ND ND ND ND ND ND ND 7.80 ND
Bromodichloromethane 0.6 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.97
Chloroform 70 0.13 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.63
Toluene 600 ND ND 0.180 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-2A
Arsenic 10 ND ND ND ND ND ND ND 0.56 J 0.12 J 0.36 JB 0.16 J ND ND 0.76 J ND ND ND ND ND NS
Barium 700 159 B 124 B 104 B 137 B 101 110 55 66 91 80 70 58 70 79 70 68 68 69 65 NS
Cadmium 2 ND ND ND ND ND ND 0.37 J ND ND 0.35 J ND 0.10 J 1.8 B ND ND ND 0.10 J 0.15 J 0.031 J NS
Chromium 10 4.37 JB 5.91 JB 4.1 JB 8.03 JB ND 14 1.4 J 4.0 B 5.2 ND 1.0 B ND 0.24 J 2.9 1.9 0.97 J 1.5 2.7 JB ND NS
Lead 15 ND 12.7 B 10.1 JB ND ND 3.3 J ND 0.83 J 0.56 J 0.99 J 0.16 J 0.61 J 0.77 J 0.92 J 0.74 J 0.48 J 0.37 J 0.78 J 0.18 J NS
Mercury 1 ND ND ND ND ND ND ND ND ND 0.011 J ND ND ND ND ND ND ND ND ND NS
Selenium 20 ND ND ND ND ND 0.7 J ND ND 0.60 J ND ND 0.67 J ND ND ND ND 0.52 J ND ND NS
Silver 20 2.23 JB 3.39 JB 7.36 JB 2.34 JB ND ND ND ND ND ND ND 0.056 J ND ND ND ND 0.033 J 0.016 J ND NS
Acetone 6000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9.3 NS
Methylene Chloride 5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NS
Toluene 600 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.63 NS
Total Xylenes 500 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.55 J NS
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-3
Arsenic 10 ND ND ND ND ND ND 1.1 J 3.2 2.9 2.1 JB 3.5 1.2 1 1.1 1.1 3.40 0.93 J ND 1.20 ND
Barium 700 217 JB 277 B 215 B 241 B 162 170 140 120 180 150 170 110 170 150 180 150.00 190 150 180 130
Cadmium 2 ND ND ND ND ND ND ND ND 0.33 J 0.28 J 0.22 J 0.048 J 0.093 J 0.042 J 0.17 J ND 0.24 J 0.15 J 0.14 J 0.082 J
Chromium 10 2.82 JB 7.7 JB 4.21 JB 1.91 JB ND ND ND 3.0 B 2.8 ND 1.6 B ND ND 0.32 JB ND ND ND 1.9 JB ND ND
Lead 15 3.58 9.15 JB 7.18 JB 4.84 JB ND ND ND 0.88 J 0.8 J 0.36 J 0.51 J 0.22 J 0.97 J 0.31 J 0.72 J 0.21 J 0.51 J 0.64 J 0.58 J 0.47 J
Mercury 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Selenium 20 7.58 JB ND ND ND ND ND 8.5 10 11 6.7 B 12 B 8.6 3.5 5.9 4.2 15.00 4.8 1.3 4.2 ND
Silver 20 2.10 JB 3.24 JB 7.59 JB 2.39 JB ND ND ND 0.15 J 0.13 J 0.24 JB ND ND ND ND ND ND 0.012 J 0.013 J ND 0.070 J
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-4
Arsenic 10 ND ND ND ND ND ND 1.2 J
Barium 700 330 JB 260 B 188 B 158 B 110.0 120.0 110.0
Cadmium 2 ND ND ND 0.15 J ND ND ND
Chromium 10 4.12 JB 6.2 JB 3.89 JB 2.85 JB ND ND ND
Lead 15 8.16 J 13.7 B 13.6 B 8.20 JB ND ND ND
Mercury 1 ND ND ND ND ND ND ND
Selenium 20 8.73 JB 14.90 ND ND 3.58 JB ND 4.7 J
Silver 20 2.08 JB 3.48 JB 7.32 JB 3.19 JB ND ND ND
Acetone 6000 ND ND ND ND 7.47 J ND 10.00
Chloroethane 3000 ND ND ND ND ND ND ND
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-5A
Arsenic 10 ND 3.32 JB ND ND ND ND 2.1 J 4.60 3.90 1.1 JB 2.70 2.90 0.69 J 0.71 J 1.10 2.70 1.20 ND 0.59 J ND
Barium 700 154 B 197 B 151 B 168 B 70 J 93.0 93.0 110.0 110.0 110.0 110.0 110.0 97.0 100 160 160 170 95 100 160
Cadmium 2 ND ND ND ND 1.96 ND ND 0.59 J 0.43 J 0.35 J 0.28 J 0.56 J 0.18 J 0.23 J 0.21 J 0.27 J 0.52 J 0.26 J 0.27 J 0.11 J
Chromium 10 1.68 JB 6.36 JB 4.21 JB 3.89 JB 3.89 JB ND ND 2.8 B 3.60 ND 0.69 JB ND ND 0.43 JB ND ND ND 1.9 JB ND 0.32 J
Lead 15 4.41 J 16.9 B 8.92 JB 6.43 JB 6.43 JB ND ND 1.8 0.5 J 0.22 J ND 0.20 J 0.40 J 0.063 J ND ND 0.26 J 0.42 J 0.070 J 0.12 J
Mercury 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Selenium 20 ND 10.00 ND ND ND 4.90 9.60 20.00 16.00 4.5 JB 11 B 13.00 2.60 5.1 3.6 11.0 6.3 ND 3.8 ND
Silver 20 2.17 JB 3.08 JB 6.73 JB 2.10 JB 2.10 JB ND ND ND 0.16 J ND ND 0.043 J ND ND ND ND 0.023 J 0.020 J ND ND
Acetone 6000 1.20 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5.10
Benzene 1 ND ND ND ND ND ND ND ND ND ND ND 1.50 ND 24 7.4 1.4 ND ND ND ND
Tetrahydrofuran NE NA NA NA NA NA NA NA NA ND 4.8 J 3.7 J 3.0 JB ND 6.1 J ND ND ND ND ND ND
ND ND
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Concord, Cabarrus County, North Carolina, Permit # 13-03
70 NDND ND NDND NDNDND
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Table 3
US Tire Monofill LandfillHistorical Summary of Constituent Detections
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Page 2 of 4
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-6
Arsenic 10 67.0 B 4.97 JB 3.63 J ND ND ND 0.72 J 0.71 J 0.37 J 1.2 JB 1.3 J ND 0.91 J ND ND ND 1.10 ND 0.60 J ND
Barium 700 2460 B 185 B 177 B 107 B 106 95 86 38 47 75 72 39 87 59 98 71 160 88 160 120
Cadmium 2 ND ND ND ND ND ND ND ND ND ND 0.33 J 0.15 J ND 0.14 J 0.12 J 0.11 J 0.15 J 0.13 J 0.15 J ND
Chromium 10 145 B 9.95 JB 8.5 JB 3.29 JB 1.54 J 3.3 J ND 3.1 B 3.30 ND 1.7 B ND 0.17 J 0.60 JB ND ND 0.77 J 2.2 JB ND ND
Lead 15 131 18.3 B 16.8 B 7.63 JB ND 3.6 J ND 0.22 J 0.64 J 0.19 J 0.96 J 0.39 J 2 0.28 J ND ND 0.48 J 0.70 J 0.19 J 0.15 J
Mercury 1 0.59 0.053 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Selenium 20 ND ND ND ND 6.65 J 3.30 ND ND 0.97 J ND 0.57 JB ND ND ND ND ND 0.64 J ND 1.30 0.54 J
Silver 20 ND 3.14 JB 6.94 JB 2.52 JB ND ND ND ND ND ND ND 0.027 J ND ND ND ND 0.015 J 0.019 J 0.019 J 0.39 J
Acetone 6000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3.7 J ND 6.00 ND
2-hexanone 280 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9.0 ND ND ND
Methylene Chloride 5 0.370 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Toluene 600 ND ND ND ND 0.30 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-7
Arsenic 10 ND 2.54 JB ND ND ND ND ND ND 0.91 J 1.8 JB 2.90 1.50 ND 0.92 J 1.10 3.50 2.00 ND 0.87 J ND
Barium 700 130 JB 216 B 126 B 128 B 85.1 J 90.0 110.0 120.0 120.0 130.0 140.0 160.0 130 130 130 200 150 150 150 140
Cadmium 2 ND ND 0.16 J 0.6 J ND 0.27 3.60 0.55 J 0.36 J 0.32 J 0.40 J 2.5 2.5 B 0.28 J 0.58 J 4.7 4.5 0.47 J 0.88 J 3.5
Chromium 10 5.67 JB 9.95 JB 4.62 JB 3.80 JB ND 0.79 1.2 J 2.8 B 3.30 ND 1.5 B ND ND 0.50 JB ND ND ND 1.6 JB ND ND
Lead 15 4.70 J 19.6 B 11.7 B 4.91 B ND ND ND 0.39 J 0.34 J ND 0.57 J 1.00 ND ND 1.50 0.23 J 0.30 J 0.44 J 0.22 J 0.25 J
Mercury 1 0.041 J 0.063 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Selenium 20 ND 9.21 J ND ND 2.85 J ND 2.7 J 2.9 J 3.80 3.3 JB 7.9 B 7.60 ND 6.70 4.80 15.00 8.30 1.8 4.2 ND
Silver 20 2.29 JB 3.06 JB 7.6 JB 2.86 JB ND ND ND ND ND ND ND 0.072 J ND ND ND ND 0.023 J 0.043 J 0.061 J 0.16 J
Acetone 6000 ND 2.19 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Toluene 600 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.50 ND ND ND ND ND
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-8
Arsenic 10 ND 4.83 JB ND ND ND ND 1.2 J 0.99 J 0.61 J 1.0 JB 0.94 J 0.45 J 1.60 ND 2.40 ND 1.20 ND 8.20 1.20
Barium 700 221 JB 460 JB 191 B 230 B 165.0 220.0 250.0 200.0 98.0 320.0 220.0 230.0 130.0 110.0 180.0 120.0 79.0 69 410 59
Cadmium 2 3.46 J 1.33 ND ND ND ND ND ND ND 0.75 J ND 0.064 J 0.12 J 0.29 J 0.13 J 0.11 J 0.16 J 0.45 J 1.50 0.11 J
Chromium 10 4.53 JB 18.9 B 4.83 JB 4.49 JB ND ND 1.3 J 3.1 B 3.40 ND 1.9 B ND 1.10 2.70 15.00 1.60 9.80 5.4 B 32 10
Lead 15 10.5 38.4 B 11.1 B 7.43 JB ND ND 6.0 0.71 J 1.0 2.3 0.52 J 0.30 J 1.8 1.2 7.5 1.3 3.9 1.4 37 3
Mercury 1 ND 0.038 J ND ND ND ND ND ND ND 0.017 J ND ND ND ND ND ND ND 1.5 ND ND
Selenium 20 ND 47.00 ND 7.94 J 11 B 11 J ND 0.79 J ND 1.0 JB 1.4 B 1.80 ND 0.17 J ND 1.40 0.43 J ND 2.1 3.9 J
Silver 20 2.62 JB 3.52 JB 7.20 JB 3.20 JB ND ND ND ND ND 0.067 JB ND 0.036 J ND ND 0.084 J 0.042 J 0.050 J 0.096 J 0.66 J 0.088 J
Acetone 6000 ND 16.0 J ND ND ND ND 3.8 J ND ND 40.0 ND ND ND ND ND ND ND ND ND ND
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-9
Arsenic 10 3.83 JB 5.85 JB ND ND ND ND ND ND 1.60 0.67 JB 1.2 J 1.00 0.57 J ND ND 1.30 0.83 J ND 0.72 J ND
Barium 700 351 JB 194 JB 157 B 156 B 130.0 110.0 150.0 140.0 120.0 130.0 130.0 110.0 120.0 110.0 100.0 110 120 110 13 110
Cadmium 2 ND ND ND ND ND 0.4 J 1.30 0.24 J ND ND ND 0.20 J 1.9 B 0.046 J 0.08 J 0.075 J 0.13 J 0.19 J 0.034 J 0.059 J
Chromium 10 9.66 JB 5.16 JB 3.16 JB 2.08 JB ND ND ND 2.6 B 3.20 ND 1.1 B ND ND 0.36 JB ND ND ND 1.7 JB 1.20 ND
Lead 15 12.5 10.3 B 7.34 JB ND ND ND ND 0.24 J 0.49 J ND 0.13 J ND 1.4 ND ND ND 0.24 J 0.49 J 0.35 J 0.096 J
Mercury 1 0.567 0.083 J ND 0.033 J 0.077 J 0.12 J 6.600 0.11 J 0.400 0.0079 J ND ND ND ND ND ND ND ND ND ND
Selenium 20 ND ND ND ND 3.08 JB ND 3.4 J 3.1 J 0.35 0.61 JB 4.6 B 4.60 0.87 J 1.90 1.10 5.50 4.20 ND ND ND
Silver 20 0.91 JB 3.26 JB 7.47 JB 3.11 JB ND ND 1.1 J ND 0.13 J 0.062 JB ND 0.025 J ND ND ND ND 0.016 J ND ND 0.12 J
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:MW-10
Arsenic 10 ND 2.97 JB ND ND ND ND ND 1.40 0.64 J 2.6 JB 0.53 J 0.59 J 0.55 J 0.50 J ND ND ND ND ND ND
Barium 700 142 JB 169 JB 167 B 175 B 156.0 150.0 150.0 170.0 160.0 190.0 190.0 170.0 350.0 350.0 230.0 210 200 150 170 180
Cadmium 2 ND ND ND ND ND 0.76 J ND ND ND 0.58 J ND 0.16 J 0.91 J,B 0.047 J 0.15 J 1.00 0.11 J 0.12 J 0.084 J 0.065 J
Chromium 10 ND 4.26 JB 2.53 JB 1.56 JB ND ND ND 3.0 B 2.90 ND 2.6 B ND 2.50 1.50 2.10 ND ND 2.0 JB ND 0.47 J
Lead 15 3.58 14.1 B 6.08 JB 5.59 JB ND ND ND 0.48 J 0.29 J 0.31 J ND 0.27 J 0.23 J ND ND ND 0.036 J 0.41 J 0.13 J 0.082 J
Mercury 1 ND ND ND ND ND ND ND ND 0.041 J ND ND ND ND ND ND ND ND ND ND ND
Selenium 20 ND 13.40 ND ND ND ND ND 1.0 J 2.00 0.99 JB 2.2 B 1.70 ND 0.72 J ND 1.90 0.78 J ND 0.57 J ND
Silver 20 2.24 JB 3.72 JB 6.95 JB 2.96 JB ND ND ND ND ND 0.27 JB ND 0.10 J 0.051 J 0.059 J ND ND 0.027 J 0.015 J ND 0.12 J
Acetone 6000 ND ND ND ND ND ND ND ND ND ND ND 6.40 ND ND ND ND ND ND ND ND
Bromoform 4 ND ND ND ND 0.32 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Dibromochloromethane 0.4 ND ND ND ND 0.13 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Tetrachloroethene 0.7 0.41 J 0.35 J 0.33 J 0.32 J ND ND ND ND ND 0.97 ND ND ND ND ND ND ND ND ND ND
Concord, Cabarrus County, North Carolina, Permit # 13-03
US Tire Monofill Landfill
Table 3 (Continued)
Historical Summary of Constituent Detections
Page 3 of 4
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:SW-1
Arsenic 10 ND ND ND ND ND ND ND 0.96 J 2.00 0.99 JB 0.73 J 1.0 J 0.63 J ND ND ND 0.42 J ND 0.47 J ND
Barium 700 34.5 JB 59.9 JB 49.8 JB 49.9 JB 35.0 J 31.00 22.00 34.00 560.00 43.00 47.00 37.00 35.00 41.00 35.00 41 30 32 45 45
Cadmium 2 ND ND ND ND ND ND ND ND 2.40 ND ND ND 0.34 J 0.041 J ND ND 0.064 J 0.15 J 0.074 J ND
Chromium 10 ND 6.05 JB 3.79 JB 2.52 JB ND 0.76 ND 3.0 B 5.70 ND 1.2 B ND ND 0.86 JB ND 1.20 ND 1.6 JB ND 2.7
Lead 15 ND 6.92 JB 7.58 JB ND ND ND ND 0.42 J 4.80 0.24 J 0.28 J 0.29 J 0.25 J 0.38 J ND ND 0.19 J 0.67 J 0.33 J 0.89 J
Mercury 1 ND ND ND ND ND ND ND ND ND 0.0081 J ND ND ND ND ND ND ND ND ND ND
Selenium 20 ND ND ND ND ND ND ND ND 2.30 ND ND 0.32 J ND 0.18 J ND ND 0.87 J ND 0.54 J 1.2 J
Silver 20 2.44 JB 3.99 JB 7.06 JB 2.58 JB 0.72 J ND ND ND 2.20 ND 0.062 J ND ND ND ND ND 0.011 J 0.21 J 0.013 J ND
Acetone 6000 2.25 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5.50
Chloroform 70 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.53 ND ND ND ND
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:SW-2
Arsenic 10 NS 2.01 JB ND ND ND ND 1.7 J 0.82 J 1.6 1.1 JB 2.2 1.2 1.1 0.91 J 0.92 J 2.1 1.4 ND 0.89 J ND
Barium 700 NS 99.1 JB 75.5 JB 84.8 JB 69.1 J 70 92 62 72 53 75 73 70 97 74 69 98 76 76 75
Cadmium 2 NS ND ND ND ND ND ND ND ND ND ND ND 1.4 ND 0.086 J ND 0.13 J 0.11 J 0.047 J ND
Chromium 10 NS 4.57 JB 3.57 JB 3.11 JB ND ND ND 3.0 B 30 ND 1.1 B ND 0.78 J 0.76 JB ND ND 1.1 1.6 JB ND 0.57 J
Lead 15 NS 7.46 JB 6.95 JB 5.38 JB ND ND ND 0.52 J 0.28 J 0.27 J 0.18 J ND 0.90 J 0.16 J ND ND 0.51 J 0.48 J 0.25 J 0.67 J
Mercury 1 NS ND ND ND ND ND ND ND ND 0.012 J ND ND ND ND ND ND ND ND ND ND
Selenium 20 NS ND ND ND 2.87 JB ND 3.3 J 4.0 J 4.4 2.2 JB 6.7 B 6.6 2 3.4 2 7.9 4.7 1.2 2.6 ND
Silver 20 NS 3.22 JB 7.51 JB 2.78 JB ND ND ND ND ND 0.14 JB ND ND ND ND ND ND 0.021 J 0.043 J 0.38 J 0.071 J
Acetone 6000 ND ND ND 2.96 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND 4.8 J ND
2-butanone 4000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.5 J ND ND ND
4-Methyl-2-Pentanone 560*ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.0 J ND ND ND
Tetrahydrofuran NE NA NA NA NA NA NA NA NA ND ND ND ND ND 4.9 J ND ND 2.1 J ND ND ND
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:SW-3
Arsenic 10 NS 3.68 JB ND ND ND ND NS 0.35 J 1 0.37 JB 6.2 2.4 DRY 0.81 J ND ND ND ND ND ND
Barium 700 NS 185 B 232 B 184 B 162 41 NS 150 170 290 1100 140 180 39 44 29 35 51 67
Cadmium 2 NS ND ND ND ND ND NS ND ND 0.25 J ND ND ND 0.42 J ND 0.064 J 0.15 J 0.059J ND
Chromium 10 NS 5.30 JB 5.35 JB 4.06 JB 1.53 J 0.63 NS 2.9 B 3.3 ND 4.8 B ND 0.54 JB ND 1 ND .0 JB 1.4 ND
Lead 15 NS 12.0 B 10.1 B ND ND ND NS 0.99 J 0.29 J 0.42 J 5.5 ND 0.31 J ND ND 0.23 J 0.51 J 0.51 J 0.10 J
Mercury 1 NS ND ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND
Selenium 20 NS ND 7.91 J ND 10.3 B ND NS 3.0 J 3.9 ND 4.9 B 9.7 3.1 ND ND 0.40 J ND ND ND
Silver 20 NS 4.07 JB 8.52 JB 3.23 JB ND ND NS ND ND ND 0.062 J ND ND ND ND 0.016 J 0.025 J 0.072 J ND
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:SW-4
Arsenic 10 ND 5.31 JB ND ND ND ND 1.1 J 1.50 0.32 J ND ND 1.30 ND 0.41 J ND ND ND ND ND ND
Barium 700 36.9 JB 74.7 JB 53.5 JB 50.7 JB 36.6 J 34.00 23.00 35.00 46.00 45.00 50.00 36.00 34.00 39.00 35.00 43 32 36 31 48
Cadmium 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.38 J 0.068 J 0.091 J 0.065 J ND
Chromium 10 ND 5.16 JB 4.0 JB 3.03 JB ND ND ND 3.5 B 3.00 ND 1.9 B ND ND 0.94 JB ND 0.82 J ND 2.2 JB ND 2.40
Lead 15 ND 6.35 JB 6.12 JB 5.32 JB ND ND ND 0.3 J 0.59 J 0.32 J ND 0.27 J 0.30 J 1.70 ND 0.33 J 0.49 J 0.52 J 0.27 J 0.84 J
Mercury 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Selenium 20 ND ND ND ND ND ND ND ND ND ND ND 0.51 J ND 0.55 J ND ND 0.40 J ND ND 0.64 J
Silver 20 2.81 JB 3.64 JB 7.40 JB 2.45 JB ND ND ND ND ND ND ND ND ND ND ND ND 0.014 J 0.012 J 0.051 J ND
Acetone 6000 2.57 JB 2.07 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5.60 5.50
Historical Summary of Constituent Detections
Table 3 (Continued)
US Tire Monofill Landfill
Concord, Cabarrus County, North Carolina, Permit # 13-03
Page 4 of 4
Sampling Date:2L Standard 10/9/07 5/1/08 10/13/08 4/17/09 10/15/09 4/15/10 10/18/10 4/6/11 10/13/11 4/10/12 10/9/12 4/10/13 10/16/13 4/2/14 10/2/14 4/9/15 10/20/15 4/6/16 10/4/16 4/6/17
Well No:SW-5
Arsenic 10 8.45 JB ND NS 3.32 JB ND ND ND ND 3.80 DRY 10.00 6.10 1.30 0.80 J 0.97 J 2 1 ND 3.3 1.0
Barium 700 823 JB 161 B NS 321 B 308 180 130 170 240 190 300 180 260 200 370 230 220 290 180
Cadmium 2 ND ND NS 0.290 J 0.57 J ND ND ND ND ND 0.21 J ND 0.13 J 0.079 J 0.41 J 0.10 J 0.15 J 0.083 J 0.082 J
Chromium 10 6.99 JB 5.6 JB NS 16.8 B 13.30 ND ND 3.7 B 3.60 5.0 B 3.90 ND 1.40 6.60 22.00 1.00 2.1 JB 9.2 4.3
Lead 15 177 7.6 JB NS 34.8 B 29 ND ND 3 5 26 30 1.6 2.6 1.6 51.0 2.0 0.61 J 8.1 9.4
Mercury 1 0.060 J ND NS NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Selenium 20 10 JB ND NS 14.60 22.9 B ND ND 2.2 J 13.00 37 B 23 0.68 J 2 2 7 5 ND 12.0 1.8 J
Silver 20 2.82 JB 4.34 JB NS 4.34 JB 2.83 J ND ND ND ND ND 0.046 J ND ND ND 0.045 J 0.013 J 0.01 J 0.070 J ND
Acetone 6000 95.5 B 2.97 JB NS 34.9 J 14.5 J ND ND ND 50.00 21 18 ND ND ND ND 32 ND 96 7
Benzene 1 ND ND ND 0.980 J 0.10 J 2.80 ND ND 2.20 6.70 250 1.5 4.8 8.0 2.1 21 ND 46 3.2
2-butanone 4000 14.4 J ND NS 11.1 J ND ND ND ND 7.10 ND 5.40 ND ND ND ND 1.8 J ND 6.80 6.80
1,1 Dichloroethane 6 ND 0.36 J NS ND 0.20 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Ethylbenzene 600 ND ND NS ND ND 2.40 ND ND ND ND 34 ND ND ND ND ND ND ND ND
2-Hexanone 280 ND ND NS ND ND ND ND ND ND ND 0.63 J ND ND 3.3 J ND ND ND ND ND
4-Methyl-2-Pentanone 560*62.6 ND NS 104 9.96 J ND ND 2.9 J 98 28 46 ND 1.8 J 3.3 J ND 16 ND 88 4.1 J
Styrene 70 ND ND NS ND ND ND ND ND ND ND 20 ND ND ND ND ND ND ND ND
Tetrahydrofuran ---NA NA NA NA NA NA NA ND 12 ND 160 B ND 6.4 J 3.8 J ND 24 ND 14 ND
Toluene 600 0.120 JB ND NS 0.150 JB ND 0.65 J ND ND ND ND 150 ND 0.5 1.5 ND 1.9 ND 1.2 ND
Total Xylenes 500 ND ND NS ND ND 5.80 ND ND ND ND 66 ND ND ND ND 3.3 ND 4.5 ND
Notes:
Results in parts per billion (ppb)
ND - Not Detected above the laboratory method detection limit or practical qualtitation limit (results prior to April 2007).
NE = No standard established
NA - Not analyzed for or not available
NS - Not sampled; no sample exists for this sampling period.
Values in boldface exceed the corresponding 15A NCAC 2L .0202 groundwater quality standard for Class GA groundwater or 15A NCAC 2B surface water quality standard for freshwater aquatic life.
Results for sampling conducted prior to April 2007 as presented in previous GW reports prepared by Withers & Ravenel.
J = Estimated value above laboratory method detection limit and below SWSL or reporting limit.
B = Analyte found in associated field and/or laboratory blank.
* - Solid Waste Section Groundwater Protection Standard
Concord, Cabarrus County, North Carolina, Permit # 13-03
Historical Summary of Constituent Detections
Table 3 (Continued)
US Tire Monofill Landfill

11112 Branding Iron Place, Wendell, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
APPENDIX A

Groundwater Sampling Forms

11112 Branding Iron Place, Wendell, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
APPENDIX B

Laboratory Reports
And
Chain-of-Custody Records

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
04/21/2017
Nautilus Geologic Consulting, PLLC
Brian S. Boutin
11112 Branding Iron Place
Wendell, NC 27591
Project: US Tire Monofill Landfill
Project No.: 13-03
Lab Submittal Date: 04/06/2017
Prism Work Order: 7040140
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 41
Sample Receipt Summary
04/21/2017
Prism Work Order: 7040140
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7040140-01 04/06/171303-Trip Blank 04/06/17Water
7040140-02 04/06/171303-EB01 04/06/17Water
7040140-03 04/06/171303-SW1 04/06/17Water
7040140-04 04/06/171303-SW2 04/06/17Water
7040140-05 04/06/171303-SW3 04/06/17Water
7040140-06 04/06/171303-SW4 04/06/17Water
7040140-07 04/06/171303-SW5 04/06/17Water
7040140-08 04/06/171303-MW1 04/06/17Water
7040140-09 04/06/171303-MW5 04/06/17Water
7040140-10 04/06/171303-MW6 04/06/17Water
7040140-11 04/06/171303-MW10 04/06/17Water
7040140-12 04/06/171303-MW8 04/06/17Water
7040140-13 04/06/171303-MW9 04/06/17Water
7040140-14 04/06/171303-MW7 04/06/17Water
7040140-15 04/06/171303-MW3 04/06/17Water
Samples were received in good condition at 4.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 41
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040140
04/21/2017
Summary of Detections
0.69 J ug/L7040140-02 1303-EB01 Barium 6020B
0.14 J ug/L7040140-02 1303-EB01 Lead 6020B
0.076 J ug/L7040140-02 1303-EB01 Silver 6020B
45 ug/L7040140-03 1303-SW1 Barium 6020B
2.7 ug/L7040140-03 1303-SW1 Chromium 6020B
0.89 J ug/L7040140-03 1303-SW1 Lead 6020B
1.2 J ug/L7040140-03 1303-SW1 Selenium 6020B
5.5 ug/L7040140-03 1303-SW1 Acetone 8260B
75 ug/L7040140-04 1303-SW2 Barium 6020B
0.57 J ug/L7040140-04 1303-SW2 Chromium 6020B
0.67 J ug/L7040140-04 1303-SW2 Lead 6020B
0.071 J ug/L7040140-04 1303-SW2 Silver 6020B
67 ug/L7040140-05 1303-SW3 Barium 6020B
0.10 J ug/L7040140-05 1303-SW3 Lead 6020B
48 ug/L7040140-06 1303-SW4 Barium 6020B
2.4 ug/L7040140-06 1303-SW4 Chromium 6020B
0.84 J ug/L7040140-06 1303-SW4 Lead 6020B
0.64 J ug/L7040140-06 1303-SW4 Selenium 6020B
5.5 ug/L7040140-06 1303-SW4 Acetone 8260B
0.96 J ug/L7040140-07 1303-SW5 Arsenic 6020B
180 ug/L7040140-07 1303-SW5 Barium 6020B
0.082 J ug/L7040140-07 1303-SW5 Cadmium 6020B
4.3 ug/L7040140-07 1303-SW5 Chromium 6020B
9.4 ug/L7040140-07 1303-SW5 Lead 6020B
1.8 J ug/L7040140-07 1303-SW5 Selenium 6020B
7.0 ug/L7040140-07 1303-SW5 Acetone 8260B
3.2 ug/L7040140-07 1303-SW5 Benzene 8260B
4.1 J ug/L7040140-07 1303-SW5 Methyl Isobutyl Ketone 8260B
21 ug/L7040140-08 1303-MW1 Barium 6020B
0.35 J ug/L7040140-08 1303-MW1 Chromium 6020B
0.21 J ug/L7040140-08 1303-MW1 Lead 6020B
0.78 J ug/L7040140-08 1303-MW1 Selenium 6020B
0.97 ug/L7040140-08 1303-MW1 Bromodichloromethane 8260B
0.63 ug/L7040140-08 1303-MW1 Chloroform 8260B
160 ug/L7040140-09 1303-MW5 Barium 6020B
0.11 J ug/L7040140-09 1303-MW5 Cadmium 6020B
0.32 J ug/L7040140-09 1303-MW5 Chromium 6020B
0.12 J ug/L7040140-09 1303-MW5 Lead 6020B
5.1 ug/L7040140-09 1303-MW5 Acetone 8260B
120 ug/L7040140-10 1303-MW6 Barium 6020B
0.15 J ug/L7040140-10 1303-MW6 Lead 6020B
0.54 J ug/L7040140-10 1303-MW6 Selenium 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 41
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040140
04/21/2017
Summary of Detections
0.39 J ug/L7040140-10 1303-MW6 Silver 6020B
180 ug/L7040140-11 1303-MW10 Barium 6020B
0.065 J ug/L7040140-11 1303-MW10 Cadmium 6020B
0.47 J ug/L7040140-11 1303-MW10 Chromium 6020B
0.082 J ug/L7040140-11 1303-MW10 Lead 6020B
0.12 J ug/L7040140-11 1303-MW10 Silver 6020B
1.2 ug/L7040140-12 1303-MW8 Arsenic 6020B
59 ug/L7040140-12 1303-MW8 Barium 6020B
0.11 J ug/L7040140-12 1303-MW8 Cadmium 6020B
10 ug/L7040140-12 1303-MW8 Chromium 6020B
2.8 ug/L7040140-12 1303-MW8 Lead 6020B
3.9 J ug/L7040140-12 1303-MW8 Selenium 6020B
0.088 J ug/L7040140-12 1303-MW8 Silver 6020B
110 ug/L7040140-13 1303-MW9 Barium 6020B
0.059 J ug/L7040140-13 1303-MW9 Cadmium 6020B
0.096 J ug/L7040140-13 1303-MW9 Lead 6020B
0.12 J ug/L7040140-13 1303-MW9 Silver 6020B
140 ug/L7040140-14 1303-MW7 Barium 6020B
3.5 ug/L7040140-14 1303-MW7 Cadmium 6020B
0.25 J ug/L7040140-14 1303-MW7 Lead 6020B
0.16 J ug/L7040140-14 1303-MW7 Silver 6020B
130 ug/L7040140-15 1303-MW3 Barium 6020B
0.082 J ug/L7040140-15 1303-MW3 Cadmium 6020B
0.47 J ug/L7040140-15 1303-MW3 Lead 6020B
0.070 J ug/L7040140-15 1303-MW3 Silver 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-01
Prism Work Order: 7040140
Time Collected: 04/06/17 00:00
Time Submitted: 04/06/17 16:00
1303-Trip Blank
13-03
SWSL
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 14:52 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 14:52 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 14:52 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 14:52 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 14:52 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 14:52 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 14:52 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 14:52 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 14:52 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 14:52 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 14:52 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 14:52 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-01
Prism Work Order: 7040140
Time Collected: 04/06/17 00:00
Time Submitted: 04/06/17 16:00
1303-Trip Blank
13-03
SWSL
8260B P7D022011.0 4/18/17 14:52 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 14:52 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 14:52 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 14:52 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 14:52 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 14:52 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124109 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-02
Prism Work Order: 7040140
Time Collected: 04/06/17 08:45
Time Submitted: 04/06/17 16:00
1303-EB01
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:10 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 20:37 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 20:37 7800Jug/L 0.12Barium1000.69
6020B P7D013811.0 4/11/17 20:37 7800ug/L 0.053Cadmium1<0.053
6020B P7D013811.0 4/11/17 20:37 7800ug/L 0.32Chromium10<0.32
6020B P7D013811.0 4/11/17 20:37 7800Jug/L 0.061Lead100.14
6020B P7D013815.0 4/11/17 20:37 7800ug/L 0.45Selenium10<0.45
6020B P7D013815.0 4/11/17 20:37 7800Jug/L 0.067Silver100.076
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 16:36 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 16:36 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 16:36 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 16:36 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 16:36 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 16:36 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 16:36 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-02
Prism Work Order: 7040140
Time Collected: 04/06/17 08:45
Time Submitted: 04/06/17 16:00
1303-EB01
13-03
SWSL
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 16:36 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 16:36 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 16:36 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 16:36 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 16:36 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 16:36 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 16:36 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 16:36 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 16:36 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 16:36 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 16:36 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124112 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-03
Prism Work Order: 7040140
Time Collected: 04/06/17 11:38
Time Submitted: 04/06/17 16:00
1303-SW1
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:14 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 20:50 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 20:50 7800ug/L 0.12Barium10045
6020B P7D013811.0 4/11/17 20:50 7800ug/L 0.053Cadmium1<0.053
6020B P7D013811.0 4/11/17 20:50 7800ug/L 0.32Chromium102.7
6020B P7D013811.0 4/11/17 20:50 7800Jug/L 0.061Lead100.89
6020B P7D013815.0 4/11/17 20:50 7800Jug/L 0.45Selenium101.2
6020B P7D013815.0 4/11/17 20:50 7800ug/L 0.067Silver10<0.067
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 17:02 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 17:02 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 17:02 KDMug/L 0.31Acetone1005.5
8260B P7D02201204/18/17 17:02 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 17:02 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 17:02 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 17:02 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-03
Prism Work Order: 7040140
Time Collected: 04/06/17 11:38
Time Submitted: 04/06/17 16:00
1303-SW1
13-03
SWSL
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 17:02 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 17:02 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 17:02 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 17:02 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 17:02 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 17:02 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 17:02 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 17:02 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 17:02 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 17:02 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 17:02 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124113 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-04
Prism Work Order: 7040140
Time Collected: 04/06/17 11:47
Time Submitted: 04/06/17 16:00
1303-SW2
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:18 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 20:54 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 20:54 7800ug/L 0.12Barium10075
6020B P7D013811.0 4/11/17 20:54 7800ug/L 0.053Cadmium1<0.053
6020B P7D013811.0 4/11/17 20:54 7800Jug/L 0.32Chromium100.57
6020B P7D013811.0 4/11/17 20:54 7800Jug/L 0.061Lead100.67
6020B P7D013815.0 4/11/17 20:54 7800ug/L 0.45Selenium10<0.45
6020B P7D013815.0 4/11/17 20:54 7800Jug/L 0.067Silver100.071
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 17:28 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 17:28 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 17:28 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 17:28 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 17:28 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 17:28 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 17:28 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-04
Prism Work Order: 7040140
Time Collected: 04/06/17 11:47
Time Submitted: 04/06/17 16:00
1303-SW2
13-03
SWSL
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 17:28 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 17:28 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 17:28 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 17:28 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 17:28 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 17:28 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 17:28 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 17:28 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 17:28 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 17:28 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 17:28 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124111 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-05
Prism Work Order: 7040140
Time Collected: 04/06/17 11:56
Time Submitted: 04/06/17 16:00
1303-SW3
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:21 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 20:59 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 20:59 7800ug/L 0.12Barium10067
6020B P7D013811.0 4/11/17 20:59 7800ug/L 0.053Cadmium1<0.053
6020B P7D013811.0 4/11/17 20:59 7800ug/L 0.32Chromium10<0.32
6020B P7D013811.0 4/11/17 20:59 7800Jug/L 0.061Lead100.10
6020B P7D013815.0 4/11/17 20:59 7800ug/L 0.45Selenium10<0.45
6020B P7D013815.0 4/11/17 20:59 7800ug/L 0.067Silver10<0.067
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 17:54 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 17:54 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 17:54 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 17:54 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 17:54 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 17:54 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 17:54 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-05
Prism Work Order: 7040140
Time Collected: 04/06/17 11:56
Time Submitted: 04/06/17 16:00
1303-SW3
13-03
SWSL
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 17:54 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 17:54 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 17:54 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 17:54 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 17:54 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 17:54 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 17:54 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 17:54 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 17:54 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 17:54 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 17:54 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124111 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-06
Prism Work Order: 7040140
Time Collected: 04/06/17 12:20
Time Submitted: 04/06/17 16:00
1303-SW4
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:25 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:03 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 21:03 7800ug/L 0.12Barium10048
6020B P7D013811.0 4/11/17 21:03 7800ug/L 0.053Cadmium1<0.053
6020B P7D013811.0 4/11/17 21:03 7800ug/L 0.32Chromium102.4
6020B P7D013811.0 4/11/17 21:03 7800Jug/L 0.061Lead100.84
6020B P7D013815.0 4/11/17 21:03 7800Jug/L 0.45Selenium100.64
6020B P7D013815.0 4/11/17 21:03 7800ug/L 0.067Silver10<0.067
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 18:20 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 18:20 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 18:20 KDMug/L 0.31Acetone1005.5
8260B P7D02201204/18/17 18:20 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 18:20 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 18:20 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 18:20 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-06
Prism Work Order: 7040140
Time Collected: 04/06/17 12:20
Time Submitted: 04/06/17 16:00
1303-SW4
13-03
SWSL
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 18:20 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 18:20 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 18:20 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 18:20 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 18:20 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 18:20 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 18:20 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 18:20 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 18:20 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 18:20 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 18:20 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124111 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-12399 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-07
Prism Work Order: 7040140
Time Collected: 04/06/17 12:30
Time Submitted: 04/06/17 16:00
1303-SW5
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:29 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:07 7800Jug/L 0.45Arsenic100.96
6020B P7D013815.0 4/11/17 21:07 7800ug/L 0.12Barium100180
6020B P7D013811.0 4/11/17 21:07 7800Jug/L 0.053Cadmium10.082
6020B P7D013811.0 4/11/17 21:07 7800ug/L 0.32Chromium104.3
6020B P7D013811.0 4/11/17 21:07 7800ug/L 0.061Lead109.4
6020B P7D013815.0 4/11/17 21:07 7800Jug/L 0.45Selenium101.8
6020B P7D013815.0 4/11/17 21:07 7800ug/L 0.067Silver10<0.067
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 18:46 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 18:46 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 18:46 KDMug/L 0.31Acetone1007.0
8260B P7D02201204/18/17 18:46 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.048Benzene13.2
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 18:46 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 18:46 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 18:46 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-07
Prism Work Order: 7040140
Time Collected: 04/06/17 12:30
Time Submitted: 04/06/17 16:00
1303-SW5
13-03
SWSL
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 18:46 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 18:46 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 18:46 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 18:46 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 18:46 KDMJug/L 0.078Methyl Isobutyl Ketone 1004.1
8260B P7D022011.0 4/18/17 18:46 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 18:46 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 18:46 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 18:46 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 18:46 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 18:46 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124109 %4-Bromofluorobenzene
75-129100 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-08
Prism Work Order: 7040140
Time Collected: 04/06/17 09:30
Time Submitted: 04/06/17 16:00
1303-MW1
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:33 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:12 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 21:12 7800ug/L 0.12Barium10021
6020B P7D013811.0 4/11/17 21:12 7800ug/L 0.053Cadmium1<0.053
6020B P7D013811.0 4/11/17 21:12 7800Jug/L 0.32Chromium100.35
6020B P7D013811.0 4/11/17 21:12 7800Jug/L 0.061Lead100.21
6020B P7D013815.0 4/11/17 21:12 7800Jug/L 0.45Selenium100.78
6020B P7D013815.0 4/11/17 21:12 7800ug/L 0.067Silver10<0.067
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 19:12 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 19:12 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 19:12 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 19:12 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.062Bromodichloromethane10.97
8260B P7D022011.0 4/18/17 19:12 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 19:12 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 19:12 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.076Chloroform50.63
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-08
Prism Work Order: 7040140
Time Collected: 04/06/17 09:30
Time Submitted: 04/06/17 16:00
1303-MW1
13-03
SWSL
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 19:12 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 19:12 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 19:12 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 19:12 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 19:12 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 19:12 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 19:12 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 19:12 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 19:12 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 19:12 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 19:12 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124114 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-09
Prism Work Order: 7040140
Time Collected: 04/06/17 09:35
Time Submitted: 04/06/17 16:00
1303-MW5
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:36 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:16 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 21:16 7800ug/L 0.12Barium100160
6020B P7D013811.0 4/11/17 21:16 7800Jug/L 0.053Cadmium10.11
6020B P7D013811.0 4/11/17 21:16 7800Jug/L 0.32Chromium100.32
6020B P7D013811.0 4/11/17 21:16 7800Jug/L 0.061Lead100.12
6020B P7D013815.0 4/11/17 21:16 7800ug/L 0.45Selenium10<0.45
6020B P7D013815.0 4/11/17 21:16 7800ug/L 0.067Silver10<0.067
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 19:38 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 19:38 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 19:38 KDMug/L 0.31Acetone1005.1
8260B P7D02201204/18/17 19:38 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 19:38 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 19:38 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 19:38 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-09
Prism Work Order: 7040140
Time Collected: 04/06/17 09:35
Time Submitted: 04/06/17 16:00
1303-MW5
13-03
SWSL
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 19:38 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 19:38 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 19:38 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 19:38 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 19:38 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 19:38 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 19:38 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 19:38 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 19:38 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 19:38 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 19:38 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124113 %4-Bromofluorobenzene
75-129104 %Dibromofluoromethane
77-123102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-10
Prism Work Order: 7040140
Time Collected: 04/06/17 10:30
Time Submitted: 04/06/17 16:00
1303-MW6
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:40 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:29 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 21:29 7800ug/L 0.12Barium100120
6020B P7D013811.0 4/11/17 21:29 7800ug/L 0.053Cadmium1<0.053
6020B P7D013811.0 4/11/17 21:29 7800ug/L 0.32Chromium10<0.32
6020B P7D013811.0 4/11/17 21:29 7800Jug/L 0.061Lead100.15
6020B P7D013815.0 4/11/17 21:29 7800Jug/L 0.45Selenium100.54
6020B P7D013815.0 4/11/17 21:29 7800Jug/L 0.067Silver100.39
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 20:04 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 20:04 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 20:04 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 20:04 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 20:04 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 20:04 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 20:04 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-10
Prism Work Order: 7040140
Time Collected: 04/06/17 10:30
Time Submitted: 04/06/17 16:00
1303-MW6
13-03
SWSL
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 20:04 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 20:04 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 20:04 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 20:04 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 20:04 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 20:04 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 20:04 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 20:04 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 20:04 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 20:04 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 20:04 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124113 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-11
Prism Work Order: 7040140
Time Collected: 04/06/17 10:35
Time Submitted: 04/06/17 16:00
1303-MW10
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:52 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:33 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 21:33 7800ug/L 0.12Barium100180
6020B P7D013811.0 4/11/17 21:33 7800Jug/L 0.053Cadmium10.065
6020B P7D013811.0 4/11/17 21:33 7800Jug/L 0.32Chromium100.47
6020B P7D013811.0 4/11/17 21:33 7800Jug/L 0.061Lead100.082
6020B P7D013815.0 4/11/17 21:33 7800ug/L 0.45Selenium10<0.45
6020B P7D013815.0 4/11/17 21:33 7800Jug/L 0.067Silver100.12
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 20:30 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 20:30 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 20:30 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 20:30 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 20:30 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 20:30 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 20:30 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-11
Prism Work Order: 7040140
Time Collected: 04/06/17 10:35
Time Submitted: 04/06/17 16:00
1303-MW10
13-03
SWSL
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 20:30 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 20:30 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 20:30 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 20:30 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 20:30 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 20:30 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 20:30 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 20:30 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 20:30 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 20:30 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 20:30 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124111 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-12
Prism Work Order: 7040140
Time Collected: 04/06/17 11:20
Time Submitted: 04/06/17 16:00
1303-MW8
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:55 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:38 7800ug/L 0.45Arsenic101.2
6020B P7D013815.0 4/11/17 21:38 7800ug/L 0.12Barium10059
6020B P7D013811.0 4/11/17 21:38 7800Jug/L 0.053Cadmium10.11
6020B P7D013811.0 4/11/17 21:38 7800ug/L 0.32Chromium1010
6020B P7D013811.0 4/11/17 21:38 7800ug/L 0.061Lead102.8
6020B P7D013815.0 4/11/17 21:38 7800Jug/L 0.45Selenium103.9
6020B P7D013815.0 4/11/17 21:38 7800Jug/L 0.067Silver100.088
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 20:56 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 20:56 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 20:56 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 20:56 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 20:56 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 20:56 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 20:56 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-12
Prism Work Order: 7040140
Time Collected: 04/06/17 11:20
Time Submitted: 04/06/17 16:00
1303-MW8
13-03
SWSL
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 20:56 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 20:56 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 20:56 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 20:56 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 20:56 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 20:56 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 20:56 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 20:56 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 20:56 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 20:56 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 20:56 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124113 %4-Bromofluorobenzene
75-129104 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-13
Prism Work Order: 7040140
Time Collected: 04/06/17 11:40
Time Submitted: 04/06/17 16:00
1303-MW9
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 14:59 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:42 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 21:42 7800ug/L 0.12Barium100110
6020B P7D013811.0 4/11/17 21:42 7800Jug/L 0.053Cadmium10.059
6020B P7D013811.0 4/11/17 21:42 7800ug/L 0.32Chromium10<0.32
6020B P7D013811.0 4/11/17 21:42 7800Jug/L 0.061Lead100.096
6020B P7D013815.0 4/11/17 21:42 7800ug/L 0.45Selenium10<0.45
6020B P7D013815.0 4/11/17 21:42 7800Jug/L 0.067Silver100.12
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 21:21 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 21:21 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 21:21 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 21:21 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 21:21 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 21:21 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 21:21 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-13
Prism Work Order: 7040140
Time Collected: 04/06/17 11:40
Time Submitted: 04/06/17 16:00
1303-MW9
13-03
SWSL
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 21:21 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 21:21 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 21:21 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 21:21 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 21:21 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 21:21 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 21:21 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 21:21 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 21:21 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 21:21 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 21:21 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124111 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-14
Prism Work Order: 7040140
Time Collected: 04/06/17 12:40
Time Submitted: 04/06/17 16:00
1303-MW7
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 15:03 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:46 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 21:46 7800ug/L 0.12Barium100140
6020B P7D013811.0 4/11/17 21:46 7800ug/L 0.053Cadmium13.5
6020B P7D013811.0 4/11/17 21:46 7800ug/L 0.32Chromium10<0.32
6020B P7D013811.0 4/11/17 21:46 7800Jug/L 0.061Lead100.25
6020B P7D013815.0 4/11/17 21:46 7800ug/L 0.45Selenium10<0.45
6020B P7D013815.0 4/11/17 21:46 7800Jug/L 0.067Silver100.16
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 21:47 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 21:47 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 21:47 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 21:47 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 21:47 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 21:47 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 21:47 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-14
Prism Work Order: 7040140
Time Collected: 04/06/17 12:40
Time Submitted: 04/06/17 16:00
1303-MW7
13-03
SWSL
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 21:47 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 21:47 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 21:47 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 21:47 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 21:47 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 21:47 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 21:47 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 21:47 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 21:47 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 21:47 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 21:47 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124112 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-12399 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-15
Prism Work Order: 7040140
Time Collected: 04/06/17 13:15
Time Submitted: 04/06/17 16:00
1303-MW3
13-03
SWSL
Total Metals
7470A P7D028910.20 4/19/17 15:07 JABug/L 0.030Mercury0.2<0.030
6020B P7D013811.0 4/11/17 21:51 7800ug/L 0.45Arsenic10<0.45
6020B P7D013815.0 4/11/17 21:51 7800ug/L 0.12Barium100130
6020B P7D013811.0 4/11/17 21:51 7800Jug/L 0.053Cadmium10.082
6020B P7D013811.0 4/11/17 21:51 7800ug/L 0.32Chromium10<0.32
6020B P7D013811.0 4/11/17 21:51 7800Jug/L 0.061Lead100.47
6020B P7D013815.0 4/11/17 21:51 7800ug/L 0.45Selenium10<0.45
6020B P7D013815.0 4/11/17 21:51 7800Jug/L 0.067Silver100.070
Volatile Organic Compounds by GC/MS
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D022011.0 4/18/17 22:13 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D022012.0 4/18/17 22:13 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D022015.0 4/18/17 22:13 KDMug/L 0.31Acetone100<0.31
8260B P7D02201204/18/17 22:13 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.048Benzene1<0.048
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D022011.0 4/18/17 22:13 KDMug/L 0.040Bromoform3<0.040
8260B P7D022011.0 4/18/17 22:13 KDMug/L 0.18Bromomethane10<0.18
8260B P7D022015.0 4/18/17 22:13 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.22Chloroethane10<0.22
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.076Chloroform5<0.076
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.079Chloromethane1<0.079
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 41
Laboratory Report
04/21/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7040140-15
Prism Work Order: 7040140
Time Collected: 04/06/17 13:15
Time Submitted: 04/06/17 16:00
1303-MW3
13-03
SWSL
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D022011.0 4/18/17 22:13 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D022015.0 4/18/17 22:13 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D022015.0 4/18/17 22:13 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D022015.0 4/18/17 22:13 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D022015.0 4/18/17 22:13 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D022011.0 4/18/17 22:13 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.047Styrene1<0.047
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D02201104/18/17 22:13 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.044Toluene1<0.044
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D02201104/18/17 22:13 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D022012.0 4/18/17 22:13 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D022010.50 4/18/17 22:13 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D022011.5 4/18/17 22:13 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124111 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 41
4/21/17
Level II QC Report
11112 Branding Iron Place Project No: 13-03
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 7040140
Time Submitted: 4/6/2017 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0220 - 5030B
Blank (P7D0220-BLK1)Prepared & Analyzed: 04/18/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 41
4/21/17
Level II QC Report
11112 Branding Iron Place Project No: 13-03
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 7040140
Time Submitted: 4/6/2017 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0220 - 5030B
Blank (P7D0220-BLK1)Prepared & Analyzed: 04/18/17
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 11155.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10251.2
ug/L 50.00 77-123Surrogate: Toluene-d8 10250.8
LCS (P7D0220-BS1)Prepared & Analyzed: 04/18/17
1,1-Dichloroethylene ug/L19.6 0.50 20.00 70-15498
Benzene ug/L21.4 0.50 20.00 77-128107
Chlorobenzene ug/L20.7 0.50 20.00 78-119104
Toluene ug/L21.0 0.50 20.00 76-131105
Trichloroethylene ug/L20.6 0.50 20.00 77-133103
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 11255.8
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10250.8
ug/L 50.00 77-123Surrogate: Toluene-d8 10351.4
LCS Dup (P7D0220-BSD1)Prepared & Analyzed: 04/18/17
1,1-Dichloroethylene ug/L18.8 0.50 20.00 2070-15494 4
Benzene ug/L20.4 0.50 20.00 2077-128102 4
Chlorobenzene ug/L19.9 0.50 20.00 2078-119100 4
Toluene ug/L20.3 0.50 20.00 2076-131101 4
Trichloroethylene ug/L19.6 0.50 20.00 2077-13398 5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10954.5
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10050.2
ug/L 50.00 77-123Surrogate: Toluene-d8 10050.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 41
4/21/17
Level II QC Report
11112 Branding Iron Place Project No: 13-03
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 7040140
Time Submitted: 4/6/2017 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0138 - 3005A
Blank (P7D0138-BLK1)Prepared & Analyzed: 04/11/17
Arsenic ug/LBRL1.0
Barium ug/L0.142 5.0 J
Cadmium ug/LBRL1.0
Chromium ug/LBRL1.0
Lead ug/L0.115 1.0 J
Selenium ug/LBRL5.0
Silver ug/L0.242 5.0 J
LCS (P7D0138-BS1)Prepared & Analyzed: 04/11/17
Arsenic ug/L1031.0 100.0 80-120103
Barium ug/L99.2 5.0 100.0 80-12099
Cadmium ug/L1051.0 100.0 80-120105
Chromium ug/L96.7 1.0 100.0 80-12097
Lead ug/L1071.0 100.0 80-120107
Selenium ug/L97.9 5.0 100.0 80-12098
Silver ug/L1155.0 100.0 80-120115
Matrix Spike (P7D0138-MS1)Prepared & Analyzed: 04/11/17 Source: 7040140-02
Arsenic ug/L99.9 1.0 100.0 BRL 75-125100
Barium ug/L97.7 5.0 100.0 0.692 75-12597
Cadmium ug/L1031.0 100.0 BRL 75-125103
Chromium ug/L94.5 1.0 100.0 BRL 75-12594
Lead ug/L1051.0 100.0 0.137 75-125105
Selenium ug/L99.7 5.0 100.0 BRL 75-125100
Silver ug/L1155.0 100.0 0.0760 75-125115
Matrix Spike Dup (P7D0138-MSD1)Prepared & Analyzed: 04/11/17 Source: 7040140-02
Arsenic ug/L1001.0 100.0 BRL 2075-125100 0.05
Barium ug/L99.9 5.0 100.0 0.692 2075-12599 2
Cadmium ug/L1041.0 100.0 BRL 2075-125104 1
Chromium ug/L95.0 1.0 100.0 BRL 2075-12595 0.5
Lead ug/L1051.0 100.0 0.137 2075-125105 0.5
Selenium ug/L1025.0 100.0 BRL 2075-125102 2
Silver ug/L1155.0 100.0 0.0760 2075-125115 0.04
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 41
4/21/17
Level II QC Report
11112 Branding Iron Place Project No: 13-03
Project: US Tire Monofill LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 7040140
Time Submitted: 4/6/2017 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0138 - 3005A
Post Spike (P7D0138-PS1)Prepared & Analyzed: 04/11/17 Source: 7040140-02
Arsenic ug/L98.2 100.0 0.0490 80-12098
Barium ug/L99.3 100.0 0.692 80-12099
Cadmium ug/L103 100.0 0.0140 80-120103
Chromium ug/L94.6 100.0 0.123 80-12094
Lead ug/L105 100.0 0.137 80-120105
Selenium ug/L100 100.0 0.0610 80-120100
Silver ug/L110 100.0 0.0760 80-120110
Batch P7D0289 - 7470A
Blank (P7D0289-BLK1)Prepared & Analyzed: 04/19/17
Mercury ug/LBRL0.20
LCS (P7D0289-BS1)Prepared & Analyzed: 04/19/17
Mercury ug/L9.10 0.20 9.375 80-12097
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 41
Sample Extraction Data
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7D01387040140-02 04/11/17 7:505050mLmL
P7D01387040140-03 04/11/17 7:505050mLmL
P7D01387040140-04 04/11/17 7:505050mLmL
P7D01387040140-05 04/11/17 7:505050mLmL
P7D01387040140-06 04/11/17 7:505050mLmL
P7D01387040140-07 04/11/17 7:505050mLmL
P7D01387040140-08 04/11/17 7:505050mLmL
P7D01387040140-09 04/11/17 7:505050mLmL
P7D01387040140-10 04/11/17 7:505050mLmL
P7D01387040140-11 04/11/17 7:505050mLmL
P7D01387040140-12 04/11/17 7:505050mLmL
P7D01387040140-13 04/11/17 7:505050mLmL
P7D01387040140-14 04/11/17 7:505050mLmL
P7D01387040140-15 04/11/17 7:505050mLmL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P7D02897040140-02 04/19/17 8:302030mLmL
P7D02897040140-03 04/19/17 8:302030mLmL
P7D02897040140-04 04/19/17 8:302030mLmL
P7D02897040140-05 04/19/17 8:302030mLmL
P7D02897040140-06 04/19/17 8:302030mLmL
P7D02897040140-07 04/19/17 8:302030mLmL
P7D02897040140-08 04/19/17 8:302030mLmL
P7D02897040140-09 04/19/17 8:302030mLmL
P7D02897040140-10 04/19/17 8:302030mLmL
P7D02897040140-11 04/19/17 8:302030mLmL
P7D02897040140-12 04/19/17 8:302030mLmL
P7D02897040140-13 04/19/17 8:302030mLmL
P7D02897040140-14 04/19/17 8:302030mLmL
P7D02897040140-15 04/19/17 8:302030mLmL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7D02207040140-01 04/18/17 9:191010mLmL
P7D02207040140-02 04/18/17 9:191010mLmL
P7D02207040140-03 04/18/17 9:191010mLmL
P7D02207040140-04 04/18/17 9:191010mLmL
P7D02207040140-05 04/18/17 9:191010mLmL
P7D02207040140-06 04/18/17 9:191010mLmL
P7D02207040140-07 04/18/17 9:191010mLmL
P7D02207040140-08 04/18/17 9:191010mLmL
P7D02207040140-09 04/18/17 9:191010mLmL
P7D02207040140-10 04/18/17 9:191010mLmL
P7D02207040140-11 04/18/17 9:191010mLmL
P7D02207040140-12 04/18/17 9:191010mLmL
P7D02207040140-13 04/18/17 9:191010mLmL
P7D02207040140-14 04/18/17 9:191010mLmL
P7D02207040140-15 04/18/17 9:191010mLmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 41
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