2602_FortBrag_MSWLF_2ndSemiGWMReport_DIN27211_20151114

FINAL
November 2015 (N=38) GROUNDWATER, SURFACE-WATER, AND
METHANE MONITORING REPORT
FOR
LONGSTREET ROAD MSW LANDFILL
NCDENR LANDFILL PERMIT #26-02

FORT BRAGG, NORTH CAROLINA

Prepared by:

US Army Corps of Engineers
Savannah District
Hazardous, Toxic & Radioactive Waste Section
CESAS-EN-GH 100 W. Oglethorpe Avenue Savannah, GA 31401

January 2016

DRAFT November 2015 (N=38) GROUNDWATER, SURFACE-WATER, AND
METHANE MONITORING REPORT

FOR

LONGSTREET ROAD MSW LANDFILL
NCDENR LANDFILL PERMIT #26-02
FORT BRAGG, NORTH CAROLINA

Prepared by:

US Army Corps of Engineers
Savannah District
Geology/Hydrogeology and HTRW design section
CESAS-EN-GG
100 W. Oglethorpe Avenue
Savannah, GA 31401 January 2016

Prepared by:

28 January 2016

John Markov, P.G.

TABLE OF CONTENTS
SECTION PAGE

1.0 INTRODUCTION .......................................................................................................................... 1
1.1 Project Background ............................................................................................. 1
1.2 Project Scope ...................................................................................................... 2
2.0 PROJECT HISTORY .................................................................................................................... 2
2.1 Site Description ................................................................................................... 2
2.2 General Site Geology and Hydrology ................................................................. 3
2.3 Previous Investigation and Results ..................................................................... 3
3.0 METHODS ..................................................................................................................................... 3
3.1 Methane Monitoring ........................................................................................... 3
3.2 Water-Level Gauging.......................................................................................... 4
3.3 Groundwater and Surface-Water Sampling ....................................................... 4
3.4 Investigation Derived Wastes Handling ............................................................. 5
4.0 ANALYTICAL RESULTS AND STATISTICAL ANALYSIS ................................................. 5
4.1 Analytical Data Summary ................................................................................... 6
4.2 Statistical Analysis Results ................................................................................. 8
4.3 Methane Monitoring Results ............................................................................... 9
5.0 CONCLUSIONS AND RECOMMENATIONS .......................................................................... 9
6.0 REFERENCES ..............................................................................................................................10
In Order
Following Page 10

ii
FIGURES

Figure 1 Site Map – Ft. Bragg, NC
Figure 2 Location Map – Longstreet Road Landfill, Ft. Bragg, NC
Figure 3 Methane Monitoring Results
Figure 4 Potentiometric Map
Figure 5 Groundwater Analytical Results
TABLES
Table 1 Methane Monitoring Results

Table 2 Groundwater Elevation Data
Table 3 Field Parameter Measurements

APPENDICES

Appendix A – Groundwater Sampling Logs
Appendix B – Chains of Custody and Laboratory Analytical Reports
Appendix C – Statistical Reports
Appendix D – Historical Sampling Results

iii
LIST OF ACRONYMS

C&D Construction and Demolition COCs Chemicals of Concern
DPW Directorate of Public Works
IDW Investigation Derived Waste
LCID Land Clearing and Inert Debris
µg/L Micrograms Per Liter
MSWLF Municipal Solid Waste Landfill Facility
NC2L North Carolina Administrative Code, Title 15A, Subchapter 2L
NCDENR North Carolina Department of Environmental and Natural Resources RCRA Resource Conservation and Recovery Act SAP Sampling and Analysis Plan
SSI Statistically Significant Increase
USACE US Army Corps of Engineers
VOCs Volatile Organic Compounds

1
November 2015 (N=38) GROUNDWATER, SURFACE-WATER, AND METHANE MONITORING REPORT FOR
LONGSTREET ROAD MSW LANDFILL
NCDENR LANDFILL PERMIT #26-02 FORT BRAGG, NORTH CAROLINA

1.0 INTRODUCTION
The report for the groundwater, surface-water, and methane monitoring for the
Longstreet Landfill (Figure 1) was performed by the United States Army Corps of
Engineers (USACE), Savannah District in November 2015. The monitoring is required
by the North Carolina Department of Environmental and Natural Resources (NCDENR)
Solid Waste Management Division. This is the thirty-eighth (N=38) monitoring event
for the site. This report summarizes the methods used for the groundwater, surface-
water, and methane monitoring and presents the results of the sampling event.

3.2 Project Background

The Longstreet Road landfill is a closed Municipal Solid Waste Landfill Facility
(MSWLF) located north of Longstreet Road at Fort Bragg in Cumberland County, North
Carolina. The landfill was closed on August 3, 1999. Figure 1 is a map of the site
location. The United States Army Corps of Engineers (USACE), Savannah District has
been contracted by the Fort Bragg Directorate of Public Works (DPW) to conduct water
quality and methane sampling for the Environmental Branch to satisfy the permit and the
Sampling and Analysis Plan (SAP) requirements. Groundwater, surface-water, and
methane monitoring locations are shown on Figure 2. The current SAP, approved by
NCDENR, includes sampling nine groundwater monitoring wells, two surface-water
stations, fifteen methane monitoring wells and four buildings for methane. The
groundwater monitoring wells are SLMW-6, SLMW-7R, SLMW-8R, SLMW-9R,
SLMW-10, SLMW-11R, SLMW-12AR, SLMW-12BR, and SLMW-13R; the surface-
water stations are SW-1 & SW-2; the methane monitoring wells are GP-1R2, GP-2R,
GP-3R, GP-4R, GP-5R, GP-6, GP-7, GP-8R, GP-9R, GP-10R, GP-11R2, GP-12R2, GP-
13R2, GP-14R2, and GP-15R2; and the buildings are O-9388, O-9389, the former scale

2
house, and the wash rack control booth ( O-9382). In May 2015 three groundwater
monitoring wells were installed to the south and east, SLMW-14, SLMW-15 and SLMW-
16. All sampling was conducted according to North Carolina Solid Waste Management
Guidelines.

3.3 Project Scope

The scope for this project included collecting groundwater samples from the nine
wells identified in the SAP as well as the three new wells that were installed in May
2015. Groundwater samples were analyzed for all Appendix I and triggered Appendix II
constituents. The scope also included collecting two surface-water samples for all
Appendix I & II constituents, performing methane monitoring at 15 methane monitoring
wells and four buildings on site, evaluating the analytical results, and reporting the results
of the investigation. The groundwater sampling and data analyses included obtaining
field parameter measurements (i.e. pH, temperature, etc.), measuring water levels at the
monitoring well locations, determining groundwater flow directions, validating
laboratory analytical data, performing statistical analyses for each detected constituent as
required by NC regulations, and determining the concentration changes of chemicals of
concern (COCs) with time.

2.0 PROJECT HISTORY

2.1 Site Description

The MSWLF is located north of Longstreet Road at Fort Bragg in Cumberland
County, North Carolina. Figures 1 and 2 show the site location and layout. The MSWLF
is west of the main post and east of Cooleyconch Mountain. Cooleyconch Mountain is
the prominent terrain feature west of the main post. A vehicle washing facility borders
the site to the east, the Lamont Road LCID and C&D Landfills are approximately 1.5
miles west/northwest of the site (on the west side of Cooleyconch Mountain).

3
2.2 General Site Geology and Hydrology

Lithologic descriptions of soil borings and monitoring well borings from previous
investigations at Fort Bragg indicate that in general Fort Bragg is underlain by alternating
sands, silty sands, clayey sands, sandy clays, and clays, likely belonging to the
Middendorf Formation. The sands and silty sands range in thickness from
approximately 2 to 22 ft and are coarse grained. The clay units range in thickness from
approximately 2 to 7 ft and are typically plastic.

2.3 Previous Investigation and Results

Several sampling events have been conducted at the Landfill. Initially, four
monthly sampling events were conducted in July, August, September, and October 1996
by R, S & H Architect, Engineering, & Planning, Inc. Law & Company, Inc. conducted
two sampling events in March and September, 1999 in conjunction with the installation
of new wells. Then until 2005, sampling events were conducted by BPA Environmental
& Engineering, Inc. The USACE has monitored the site since 2005.

The previous sampling event, held in May 2015 for Longstreet Landfill, was
conducted by the USACE, Savannah District. Low levels of VOCs, SVOCs, pesticides
and Appendix II inorganics were detected, but most detections were below NC2L
standards. Monitoring wells, SLMW-8R, SLMW-9R, SLMW-10, SLMW-14 and
SLMW-16, contained analytes above the NC2L standard. These wells remain in
assessment monitoring.

3.0 METHODS
3.1 Methane Monitoring
Methane monitoring was performed at 15 wells and 4 buildings. The monitoring
included measuring levels of methane, carbon dioxide, hydrogen sulfide and oxygen at
each of the locations. The results of the monitoring are summarized in Table 1 and are

4
also presented on Figure 3.

3.2 Water-Level Gauging
During this sampling event, USACE personnel measured the water levels in 9
monitoring wells. Measured water levels and calculated groundwater elevations are
presented in Table 2. A Potentiometric map was developed based on the groundwater
elevations; the map is presented as Figure 4. The map shows that the general direction of
the groundwater flow at the Longstreet Landfill is towards the east-southeast.
3.3 Groundwater and Surface-Water Sampling
The groundwater sampling was conducted in accordance with the SAP for the
Longstreet Road MSWLF (NCDENR Landfill Permit #26-02, which has been updated to
reflect the most recent SAP). Groundwater samples were collected from nine monitoring
wells and two surface-water stations. Water quality parameters pH, specific conductivity,
temperature, turbidity, dissolved oxygen (DO), and oxidation-reduction potential (ORP)
were measured during the purge cycle of each well and prior to sampling the surface-
water stations. The measurements are summarized in Table 3.

The surface-water sampling was conducted using a peristaltic pump. The water to
be collected for VOC analysis was not allowed to pass through the head of the pump,
instead the tubing was filled and the flow was reversed to fill the bottles. Groundwater
samples were collected using a low-flow purge method with a bladder pump.
Immediately before purging a well, the static water level below the top of the well casing
and the total depth of the well were measured to the nearest 0.01 foot and recorded in the
field notebook. The volume of water in the well was calculated based on the static water
level and the well construction information. Well volume calculations were placed in the
field notebook. The inlet of the sampling pump was placed at the mid-point of the
screened interval. This level was adjusted for wells where the static water level is within
the well screen. The monitoring wells were purged using a variable-flow bladder pump at
a rate of 500 ml/min or less.

5
The wells were purged until the water quality had stabilized or five purge volumes
were removed. The wells were considered stable when the following requirements were
met for three consecutive readings: turbidity values within 10% or lower than 10
Nephelometric Turbidity Units (NTUs), temperature values within a range of 0.5 degrees
Celsius, pH readings within 0.1 Standard Units (SU), ORP values within a range of 10
millivolts (mV), and conductivity values within 3%, and DO values within 10%.

The rate of pumping was determined and noted in the field notebook. The purge
rate was adjusted, as necessary, to avoid purging any well to dryness and to equal the
recharge of the aquifer. All sampling equipment was protected from contaminated soil
surfaces to prevent contamination of the samples (e.g., equipment may be placed on
disposable polyethylene plastic sheeting). Groundwater samples were collected after
purging was complete. The tubing was disconnected from the flow through cell and the
samples were collected from the pump outlet. The samples were labeled and placed into
an ice-filled cooler for preservation.

Groundwater sampling data (including sample number, location, quantity of water
purged, field parameters, site conditions, etc.) were documented in the field notebook.
Water samples for Resource Conservation and Recovery Act (RCRA) metal analyses
were un-filtered. The results of the groundwater sampling are presented in Appendix D
and on Figure 5. The groundwater sampling field data logs are presented in Appendix A.

3.4 Investigation Derived Wastes Handling The investigation derived wastes (IDW), including the waste water from well
purging and decontamination water, were containerized in 55-gallon drums. Those
drums were appropriately labeled, sealed, and staged within designated areas until
analytical results had been received and reviewed. Based on the analytical results of the
groundwater samples, the IDW was classified as non-hazardous. With the concurrence of
the Fort Bragg Installation Restoration Program Manager, the IDW was disposed of at an
appropriate disposal facility.

6
4.0 ANALYTICAL RESULTS AND STATISTICAL ANALYSIS
4.1 Analytical Data Summary Groundwater samples were analyzed for VOCs, SVOCs, Pesticides, PCBs,
Organophosphorus Pesticides, and Appendix II Inorganics. The surface-water samples
were analyzed for all Appendix I and Appendix II constituents. The summary of
detections of the COCs is presented in Appendix D. Figure 5 shows the distribution of
the detections and their concentrations from this sampling event. The laboratory reports
of analytical results are included as Appendix B. For comparison, the analytical results
of previous investigations are also presented in the Statistical Analyses Summary Report
included in Appendix C. For comparison, the analytical results of previous
investigations are presented in Appendix D.

In accordance with North Carolina guidance, analytical results are compared to
North Carolina Groundwater 2L Standards (NC2L standards) or the North Carolina
Surface Water 2B Standards (NC2B standards). The analytical data of the second 2015
sampling event indicate that some VOCs and inorganics were detected at low levels, and
most detections were below NC2L or NC2B standards (Appendix D). Five sampling
locations had detections exceeding the remedial standards: wells SLMW-8R, SLMW-9R,
SLMW-14, SLMW-16 and surface-water sample SW-1. A summary of the analytical
results for each of those wells are as follows:

• Well SLMW-8R
Two compounds were detected above the 2L standard as listed below:
Compound 2L Concentration
Benzene 1 µg/L 2.7 µg/L Vinyl Chloride 0.03 µg/L 9.3 µg/L
No other constituents were above their 2L standards.

7
• Well SLMW-9R
Three compounds were detected above the 2L standard as listed below:
Compound 2L Concentration Benzene 1 µg/L 2.4 µg/L
Vinyl Chloride 0.03 µg/L 2.2 µg/L
Arsenic 10 µg/L 27 µg/L

No other constituents were above their 2L standards.

• Well SLMW-14
One compound was detected above the 2L standard as listed below:
Compound 2L Concentration
Benzene 1 µg/L 1.1 µg/L

No other constituents were above their 2L standard.

• Well SLMW-16
Three compounds were detected above the 2L standard as listed below:
Compound 2L Concentration
Benzene 1 µg/L 1.9 µg/L
Vinyl Chloride 0.03 µg/L 2.1 µg/L
Arsenic 10 µg/L 14 µg/L
No other constituents were above their 2L standard.

• Surface-water SW-1
Two compounds were detected above the 2B standard as listed below:
Compound 2B Concentration
Zinc 36 µg/L 150 µg/L Selenium 5 µg/L 14 µg/L

No other constituents were above their 2B standard.

8
Though samples had constituent detections above method detection limits, all
other detections were below the respective NC2L standard and most detections were
estimated values that were detected above the method detection limits but below the
reporting limit (Appendix D).

4.2 Statistical Analysis Results

A statistical test predicts the average behavior (distribution) of a random variable
by comparing the means (normal distribution) or medians (lognormal and non-parametric
distributions) of the compliance well data to background well data. Different statistical
tests were used as appropriate for the different distributional patterns that occur within
the data. Prior to testing for statistical significance, the distribution of each parameter
was determined to be normal, lognormal, or non-normal.
If the data were non-normally distributed, or the fraction of nondetects exceeded
15% but were less than 90%, then the Kruskal-Wallis Test was applied. However, the
Kruskal-Wallis test is prone to false positives. Therefore, additional statistical analyses
were used to determine the validity of the positive results. If the fraction of non-detects
exceeded 90%, then the Non-Parametric Prediction Limit was applied. Intra-well
comparisons of data from a single well to previous data from the same well were
performed to confirm if a trend of increasing concentration is occurring. The Mann-
Kendall Trend Analysis and the Shewhart-CUSUM Control Chart statistical tests were
selected for these additional analyses.
A detailed discussion of the statistical methods is presented in Appendix C. The
results of the analysis indicated that the samples collected at the Longstreet Road
Municipal Solid Waste Landfill indicated evidence that statistically significant increases
(SSIs) were still present in a few wells and that assessment monitoring should continue.
According to North Carolina Administrative Code Title 15A Chapter 13 Subchapter
B Section 1634 paragraph f [15A NC3AC 13B.1634 (f)], assessment monitoring shall
continue if Appendix II parameters are detected at statistically significant levels above
background. Assessment monitoring will have to continue at the landfill until the
presence of no SSIs is confirmed in two consecutive monitoring events.

9

4.3 Methane Monitoring Results

Methane monitoring was performed at 15 wells and 4 buildings. The monitoring
included measuring levels of methane, carbon dioxide, hydrogen sulfide and oxygen at
each of the locations. The results of the monitoring are summarized in Table 1 and are
also presented on Figure 3. No methane monitoring wells or buildings contained high
levels of methane (> 5% Methane by Volume).

5.0 CONCLUSIONS AND RECOMMENATIONS

The annual monitoring program consists of two sampling events (this was the
second of 2015) conducted six months apart. This was the N=38 sampling event for the
Longstreet Road Landfill. Low levels of VOCs, SVOCs, and Appendix II inorganics
were detected, but most detections were at estimated levels and/or were below remedial
standards. Analytes were detected above the NC2L standards at monitoring wells
SLMW-8R, SLMW-9R, SLMW-14, and SLMW-16 and above the NC2B standards in
surface-water sample SW-1.
According to the Statistical Analysis of groundwater Data (Appendix D), the
results of the analysis indicated that several locations at the Longstreet Road Municipal
Solid Waste Landfill had statistically significant increases (SSIs).
According to North Carolina Administrative Code Title 15A Chapter 13
Subchapter B Section 1634 paragraph f [15A NC3AC 13B.1634 (f)], assessment
monitoring shall continue if Appendix II parameters are detected at statistically
significant levels above background. Assessment monitoring will continue until no SSIs
are confirmed in two consecutive sampling events.
The methane levels were measured at 19 locations at Longstreet. No methane
monitoring wells or buildings contained high levels of methane (> 5% Methane by
Volume).

10
6.0 REFERENCES

North Carolina Administrative Code, Title 15A, Department of Environment, Health, and
Natural Resources, Division of Solid Waste, Management, Subchapter 13B, Solid
Waste Management, Section .1600 (January 4, 1994).

North Carolina Administrative Code, Title 15A, Department of Environment, Health, and
Natural Resources, Division of Solid Waste, Management, SubchapterNC2L,
Classifications and Water Quality Standards Applicable to the Groundwaters of
North Carolina, Sections .0100, .0200, and .0300 (November 8, 1993): from the
Environmental Management Commission, Raleigh, North Carolina.

FIGURES
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Site Map -- Ft. Bragg, NC
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SLMW-07R
SLMW-13R SLMW-11R
SLMW-12BRSLMW-12AR
SLMW-15
SLMW-14
SLMW-16
SW-1
SW-2
DATE: JAN 2016 FIGURE: 2
LONGSTREET ROAD LANDFILL
LOCATION MAP
FORT BRAGG, NC
$0 350 700175'
1 inch = 350 feet
Legend
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GP-11R2
GP-14R2
GP-12R2GP-13R2
GP-09R
DATE: JANUARY 2016 FIGURE: 3
LONGSTREET ROAD LANDFILL
METHANE MONITORING RESULTSNOVEMBER 2015
FORT BRAGG, NC
$0 400 800200'
1 inch = 400 feet
Legend
&§M Methane Well
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Secondary Road
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0.0% Methane
0.0% Methane 0.0% Methane
0.0% Methane
0.0% Methane
0.0% Methane
0.0% Methane
0.0% Methane
0.0% Methane
0.0% Methane
0.0% Methane
0.0% Methane0.0% Methane
Former Scale House0.0% Methane
O-93880.0% Methane
Wash Rack Control Booth0.0% Methane
O-93890.0% Methane
0.0% Methane
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SLMW-12AR(235.8)
SLMW-09R(251.29)
SLMW-13R(286.14)
SLMW-11R(275.22)
SLMW-12BR(234.44)
DATE: JAN 2016 FIGURE: 4
LONGSTREET ROAD LANDFILL
POTENTIOMETRIC SURFACE MAPNOVEMBER 2015
FORT BRAGG, NC
$0 350 700175'
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TABLES
Monitoring Date:Facility Name:Facility Permit #:Monitoring Personnel (Name/Position):
NC Landfill Rule:Monitoring Personnel (Name/Position):County (Location):Equipment Field Calibrated by:
Equipment Type:Manufacturer Cal/Service Date:Equipment Serial #:Date/Time of Field Calibration:
Calibration Gas:Cal Gas Expiration Date:Meter pump rate:
Gas Monitoring Wells
Time Initial %CH4 Initial %LEL Purge Time Stable %CH4 Stable %LEL Stable *H2S Stable %O2 Stable %CO2
1407 0 1406 0 0 10.3 9.7
1329 0 1328 0 0 20 0.7
1326 0 1325 0 0 9.3 6.2
1306 0 1305 0 0 167 3.4
1337 0 1336 0 0 20.3 0.4
1311 0 1310 0 0 13.1 7.2
1317 0 1316 0 0 9.9 12.4
1246 0 1245 0 0 9.1 3
1229 0 1227 0 0 10.5 3.2
1417 0 1416 0 0 18.8 1.1
1422 0 1421 0 0 8.3 1.9
1428 0 1427 0 0 17 2.8
1425 6 1424 0 0 20 0.7
1438 0 1437 0.9 0 16.5 3.2
1451 0 1450 0 0 17.4 1.8
Notes:
H2S recorded in ppm
Gas MW-9R
Periodic Methane Monitoring Report
Monitoring Point ID
Gas MW-7
Gas MW-12R2
Gas MW-1R2
Gas MW-3R
Gas MW-4R
Gas MW-5R
Gas MW-6
Gas MW-8R
Gas MW-2R
Gas MW-14R2
Gas MW-10R
Gas MW-11R2
Gas MW-13R2
Gas MW-15R2
Longstreet Road MSW LandfillJ. Wood/R. Hill Physical Scientists
M. Senktas-ChemistJ. Wood
11/12/2015 0826
#26-02November 14, 2015
0.1600
O2-09/2016 CH4-01/2016CH4-50% CO2-35% O2-4%
GM 12051109GEM 2000
Cumberland
11/12/2015
Facility Structures
Time Initial %CH4 Initial %LEL Purge Time Stable %CH4 Stable %LEL Stable *H2S Stable %O2 Stable %CO2
1342 0 1341 0 0 20.6 0
1234 0 1233 0 0 20.6 0
1242 0 1241 0 0 20.7 0
1241 0 1240 0 0 20.7 0
Drawings identifying location where each building sampled (include north arrow):
Climatic/Physical Conditions at Site
a. Soil Conditions:
b. Weather Conditions:
c. Temperature:
d. Barometric Conditions:Rising Falling Steady Reading:30.24 (mmHg)
e. Relative Humidity within range of 10%-90%? Yes Value:
f. Condition and Access: Are all monitoring points identified in the field (signage) in accordance
with approved monitoring plan; are they secured; has the owner/operator maintained access? Yes
O-9389
O-9389
O-9382
O-9388
24%
If no, explain in space provided below.
61°F
Sunny
Monitoring Point ID
Former Scalehouse
Samples must be collected under normal/average conditions of temperature, pressure, and climate for the season. Barhole punch sampling
should not be performed during or immediately after rain events, or when soils are saturated or frozen. All sampling must be performed after
12:00 pm (subsurface gases have a diurnal cycle and generally are at a maximum during the afternoon), and preferably when barometric
conditions are not rising (subsurface gas pressures will be less than atmospheric pressure under these conditions and gas will therefore not
migrate), or representative samples may not be obtained. Barometric information can be obtained from many locations (i.e.
http://weather.noaa.gov).
O-9388
O-9382Former Scale House
N
N
N
N
X
X
X
X
Additional Comments:
Certification:
SIGNATURE TITLE
g. If stressed vegetation is noted, describe the extent and location in the space provided below.
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. I am
Description of Sampling Techniques: (e.g., wells are vented or not, barhole punch methodology, etc.)
Table 2. Summary of GroundwaterElevations Longstreet Landfill, Fort Bragg, NC
Nov-08 Nov-08 Jun-09 Jun-09 Nov-09 Nov-09 Jun-10 Jun-10 Nov-10 Nov-10 Jun-11 Jun-11 Nov-11 Nov-11 May-12 May-12 Nov-12 Nov-12 May-13 May-13 Nov-13 Nov-13 May-14 May-14 May-15 May-15 Nov-15 Nov-15
SLMW-6 293.55 26.27 267.28 26.11 267.44 28.22 265.33 25.08 268.47 28.02 265.53 30.31 263.24 31.55 262.00 30.84 262.71 30.72 262.83 29.75 263.8 27.4 266.15 25.6 267.95 26.27 267.28 25.73 267.82
SLMW-
7R**289.74 20.76 269.74 20.59 269.91 22.19 268.31 20.43 270.07 22.14 268.36 21.86 268.64 22.06 268.44 21.78 267.96 22.28 267.46 20.89 268.85 21.89 267.85 20.27 269.47 20.61 267.13 21.14 268.6
SLMW-
8R**289.4 22.91 267.43 23.03 267.31 24.21 266.13 22.91 267.43 24.31 266.03 24 266.34 24.3 266.04 24.15 265.25 24.3 265.10 22.95 266.45 23.8 265.6 21.77 267.63 22.47 266.93 22.1 267.3
SLMW-
9R**288.44 38.31 251.23 37.3 252.24 38.72 250.82 36.66 252.88 38.34 251.2 40.2 249.34 41.75 247.79 42.53 245.91 43.51 244.93 42.9 245.54 41.5 246.94 36.68 251.76 38 250.44 37.15 251.29
SLMW-10 305.99 19.42 286.57 19.59 286.4 20.39 285.6 19.7 286.29 20.59 285.4 20.57 285.42 20.87 285.12 20.8 285.19 20.86 285.13 20.14 285.85 19.8 286.19 30.97 275.02 19.21 286.78 17.7 288.29
SLMW-
11R 354.61 78.96 278.84 77.62 280.18 79.2 278.6 74.31 283.49 76.42 281.38 81.12 276.68 82.13 275.67 83.14 271.47 83.92 270.69 84.44 270.17 86.7 267.91 80.02 274.59 78.96 275.65 79.39 275.22
SLMW-
12AR 243.36 8.45 234.91 9.03 234.33 9.53 233.83 8.75 234.61 9.44 233.92 8.65 23.71 9.6 233.76 9.45 233.91 9.92 233.44 8.5 234.86 9.7 233.66 8.02 235.34 8.69 234.67 7.56 235.8
SLMW-12BR 243.42 9.23 234.19 8.09 235.33 9.2 234.22 8.79 234.63 9.19 234.23 9.25 234.17 9.61 233.81 9.52 233.9 10 233.42 9.72 233.7 9.8 233.62 9.23 234.19 9.18 234.24 8.98 234.44
SLMW-
13R**340.42 53.14 286.88 51.9 288.12 53.29 286.73 50.58 289.44 53.05 286.97 55.07 284.95 56.91 283.11 ****60.45 279.97 56.7 283.75 54.85 285.57 53.86 286.56 54.28 286.14
SLMW-14 NA NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI 16.63 NA 15.13 NA
SLMW-15 NA NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI 29.05 NA 29.15 NA
SLMW-16 NA NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI 29.08 NA 28.06 NA
Note:
* - well was dry
** - Elevation is for replacement well but data is for original well up through May 2013
NA-Not Available-New wells were not surveyed at the time of sampling
NI-Not Installed
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)Well ID TOC Elev. (ft. amsl)
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)
Water Level Elev. (ft. amsl)
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)
Water Level Elev. (ft. amsl)
Water Level (ft. BTOC)
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)
Water Level (ft. BTOC)
Water Level Elev. (ft. amsl)
TOC elevation is based on vertical datum NGVD29 (source: USGS RFI, Aug. 1999)
btoc – below top of casing
amsl – above mean sea level
Water Level (ft. BTOC)
Water
Level
Elev. (ft.
amsl)
Water
Level
(ft.
BTOC)
Water
Level
Elev. (ft.
amsl)
D --- Selected Well for Long Term Monitoring
TOC – Top of casing
bgs – Below ground surface,
Water Level (ft. BTOC)
Table 3. Field Parameter Measurements Longstreet Landfill, Fort Bragg, NC

Sample Specific Temperature Turbidity Dissolved
Well Identification pH Conductivity (µs/cm) (°C) (N.T.U.) Oxygen (mg/L) ORP
SLMW-6 SLMW-6-11-15 4.44 0.018 17.56 1.14 0.16 190
SLMW-7R SLMW-7R-11-15 5.96 0.409 18.75 40.3 0.51 -7.9
SLMW-8R SLMW-8R-11-15 5.60 0.278 18.83 * 0.06 -28
SLMW-9R SLMW-9R-11-15 6.45 1.317 18.21 16 0.09 -125.6
SLMW-10 SLMW-10-11-15 6.34 0.906 17.92 4.85 0.10 -87.0
SLMW-11R SLMW-11R-11-15 4.61 0.024 18.13 4.21 0.19 171.0
SLMW-12AR SLMW-12AR-11-15 4.11 0.038 19.36 3.55 4.31 138.8
SLMW-12BR SLMW-12BR-11-15 4.45 0.073 18.19 3.49 0.62 262.5
SLMW-13R SLMW-13R-11-15 4.61 0.017 16.8 20.6 4.44 323
SLMW-14 SLMW-14-11-15 6.01 0.486 18.69 3.78 0.39 -62.9
SLMW-15 SLMW-15-11-15 4.66 0.018 16.14 * 4.18 183.1
SLMW-16 SLMW-16-11-15 6.18 0.708 18.65 25.6 0.10 -59.9
SW-1* SW-1-11-15 -- -- -- -- -- --
SW-2* SW-2-11-15 -- -- -- -- -- --

Note:
N.T.U. --- Nephelometric Turbidity Unit

ORP --- Oxidation Reduction Potential
NS - Not Sampled
* - Not recorded

APPENDIX A
GROUNDWATER SAMPLING LOGS

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-13-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1225
WEATHER CONDITIONS: sunny

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-12AR-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):20 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):7.56 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =2.04 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:8.0 (gallons)
Length of Time Purged:30 (minutes)Purge Time:1155
Amount Purged:N/A (gallons)Pump Depth:18
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1213 1216 1219 1222 1225
Temp. °C 19.50 19.47 19.42 19.37 19.36
Sp. Cond 0.039 0.039 0.038 0.038 0.038
DO 4.03 4.09 4.38 4.32 4.31
pH 4.03 4.09 4.08 4.06 4.11
ORP 131.8 131.5 133.4 138.2 138.8
Turbidity 47.4 23.2 15.0 8.88 3.55
Water Level 9.42 9.45 9.83 9.83 9.83

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-13-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1400
WEATHER CONDITIONS: sunny

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-12BR-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):64.81 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):8.98 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =9.16 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:7.0 (gallons)
Length of Time Purged:130 (minutes)Purge Time:1150
Amount Purged:N/A (gallons)Pump Depth:58
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1345 1348 1351 1354 1357
Temp. °C 18.08 18.09 18.14 18.12 18.19
Sp. Cond 0.073 0.073 0.073 0.073 0.073
DO 0.63 0.70 0.65 0.68 0.62
pH 4.40 4.42 4.42 4.45 4.45
ORP 265.6 264.3 264.1 261.7 262.5
Turbidity 14.4 12.6 6.58 - 3.49
Water Level 11.85 13.00 20.5 22.9 35.5

5. NOTES: WL dropping switched to 40/20 MP10 cycle and water stabilized. During
sampling, WL still dropping and changed to 45/35 MP10 cycle. WL stabilized to 36.9’ and
sampling resumed.

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-15-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 0910
WEATHER CONDITIONS: sunny, 40°

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-15-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):40.51 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):29.15 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.86 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:3.6 (gallons)
Length of Time Purged:31 (minutes)Purge Time:839
Amount Purged:N/A (gallons)Pump Depth:38
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 0854 0857 0900 0903 0906
Temp. °C 16.16 16.15 16.10 16.11 16.14
Sp. Cond 0.018 0.018 0.018 0.018 0.018
DO 4.36 4.31 4.29 4.21 4.18
pH 4.79 4.77 4.74 4.68 4.66
ORP 171.9 173.5 176.0 180.7 183.1
Turbidity 47.7 16.8 7.90 6.15 -
Water Level 29.4 27.8 30.25 30.27 30.27

5. NOTES: Metals and nitrates collected 11-16-2015 @ 0825

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-15-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1105
WEATHER CONDITIONS: sunny, calm

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-10-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):27.8 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):17.7 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.66 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:8.0 (gallons)
Length of Time Purged:59 (minutes)Purge Time:1006
Amount Purged:N/A (gallons)Pump Depth:25.5
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1047 1050 1053 1056 1059
Temp. °C 17.89 17.89 17.86 17.93 17.92
Sp. Cond 0.908 0.905 0.905 0.906 0.906
DO 0.11 0.11 0.11 0.10 0.10
pH 6.34 6.34 6.34 6.34 6.34
ORP -84.3 -85.0 -85.4 -86.3 -87.0
Turbidity 21.1 15.1 9.61 8.26 4.85
Water Level 18.30 18.35 18.49 18.50 18.50

5. NOTES: cap missing from well. Purged 5x well volume. Metals and nitrates collected
11-16-15 @ 0845.

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-15-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1225
WEATHER CONDITIONS: sunny, 60°

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-11R-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):86.73 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):79.39 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.20 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:3.0 (gallons)
Length of Time Purged:30 (minutes)Purge Time:1155
Amount Purged:N/A (gallons)Pump Depth:84
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1209 1212 1215 1218 1220
Temp. °C 18.24 18.12 18.13 18.10 18.13
Sp. Cond 0.024 0.024 0.024 0.024 0.024
DO 0.25 0.23 0.20 0.19 0.19
pH 4.66 4.65 4.60 4.61 4.61
ORP 127.4 139.6 154.8 166.0 171.0
Turbidity 35.2 14.4 10.4 7.81 4.21
Water Level 79.51 79.51 79.51 79.51 79.51

5. NOTES: Metals and nitrates collected 11-16-15 @ 0900

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-15-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1515
WEATHER CONDITIONS: sunny, 65°

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-13R-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):67.05 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):54.28 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =2.09 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:10.0 (gallons)
Length of Time Purged:30 (minutes)Purge Time:1345
Amount Purged:N/A (gallons)Pump Depth:65
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1458 1501 1504 1507 1510
Temp. °C 16.80 16.80 16.80 16.78 16.80
Sp. Cond 0.017 0.017 0.017 0.017 0.017
DO 4.46 4.42 4.30 4.22 4.44
pH 4.56 4.53 4.57 4.57 4.61
ORP 319.3 322.5 322.0 323.7 323.0
Turbidity 320 182 35 21.9 20.6
Water Level 54.30 54.30 54.30 54.30 54.30

5. NOTES: Purged 5x well volume. Metals and nitrates collected 11-16-15 @ 0925.

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-16-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1115
WEATHER CONDITIONS: sunny, 47°

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-16-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):37.28 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):28.06 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.51 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:7.5 (gallons)
Length of Time Purged:73 (minutes)Purge Time:1002
Amount Purged:N/A (gallons)Pump Depth:35
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1059 1102 1105 1108 1111
Temp. °C 18.59 18.55 18.66 18.60 18.65
Sp. Cond 0.697 0.701 0.703 0.705 0.708
DO 0.10 0.09 0.09 0.10 0.10
pH 6.18 6.17 6.17 6.17 6.18
ORP -58.8 -59.3 -59.7 -59.8 -59.9
Turbidity >1000 96.7 32.0 30.1 25.6
Water Level 28.08 28.08 28.08 28.08 28.08

5. NOTES: Purged 5x well volume

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-16-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1245
WEATHER CONDITIONS: sunny

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-14-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):29.07 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):15.13 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =2.29 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:5.5 (gallons)
Length of Time Purged:33 (minutes)Purge Time:1212
Amount Purged:N/A (gallons)Pump Depth:27
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1230 1233 1236 1239 1242
Temp. °C 18.68 18.76 18.79 18.71 18.69
Sp. Cond 0.432 0.449 0.469 0.477 0.486
DO 0.51 0.45 0.43 0.42 0.39
pH 5.96 5.99 6.01 6.02 6.01
ORP -37.4 -47.8 -55.8 -60.0 -62.9
Turbidity 21.7 12.9 - 6.64 3.78
Water Level 16.00 16.00 16.00 16.00 16.00

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-16-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1620
WEATHER CONDITIONS: sunny

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-8R-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):32.8 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):22.1 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.75 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:1.8 (gallons)
Length of Time Purged:47 (minutes)Purge Time:1433
Amount Purged:N/A (gallons)Pump Depth:30
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1600 1605 1610 1615 1620
Temp. °C 19.54 19.41 19.19 18.91 18.83
Sp. Cond 0.530 0.406 0.279 0.278 0.278
DO 0.06 0.05 0.05 0.07 0.06
pH 5.86 5.76 5.60 5.58 5.60
ORP -59.8 -49.9 -33.6 -28.8 -28.0
Turbidity 56.4 37.2 - - -
Water Level 22.3 22.75 INTAKE INTAKE INTAKE

5. NOTES: Unable to stabilize WL, WL dropped below top of pump. 5x well volume
purged and samples collected @ 1620.

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-17-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1055
WEATHER CONDITIONS:

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-7R-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 16
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):32.25 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):21.14 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.82 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:9.0 (gallons)
Length of Time Purged:140 (minutes)Purge Time:835
Amount Purged:N/A (gallons)Pump Depth:30
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1037 1041 1044 1047 1050
Temp. °C 18.70 18.79 18.76 18.75 18.75
Sp. Cond 0.406 0.408 0.409 0.408 0.409
DO 0.94 0.82 0.70 0.60 0.51
pH 5.96 5.96 5.97 5.96 5.96
ORP -3.2 -5.0 -6.2 -6.9 -7.9
Turbidity 39.1 22.2 37.5 62.9 40.3
Water Level 21.66 21.76 21.90 22.16 22.16

5. NOTES: Purged 5x well volume.

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-17-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1330
WEATHER CONDITIONS: 67°, sunny, light wind

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-9R-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 32
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):54.7 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):37.15 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =2.88 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:8.1 (gallons)
Length of Time Purged:75 (minutes)Purge Time:1215
Amount Purged:N/A (gallons)Pump Depth:52.5
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1315 1318 1321 1324 1327
Temp. °C 18.21 18.24 18.23 18.21 18.21
Sp. Cond 1.317 1.318 1.318 1.318 1.317
DO 0.09 0.09 0.10 0.10 0.09
pH 6.44 6.45 6.45 6.45 6.45
ORP -125.0 -125.2 -125.6 -125.5 -125.6
Turbidity >1000 538 122 28.6 16.0
Water Level 37.2 37.2 37.2 37.2 37.2

5. NOTES: DUP-1-11-15 collected.

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: USACE DATE: 11-17-2015
SAMPLED BY: M. Senktas, J. Wood, R. Hill TIME : 1530
WEATHER CONDITIONS: 66°, overcast

Location: Fort Bragg, Longstreet Landfill Sample ID: SLMW-6-11-15

PRESERVATIVE: ice, HNO3, Zn(O2CCH3)2, NaOH, HCl
ANALYSES REQUESTED: 8141, 300, 6020 Appendix II, 8081_8082, 8156, 8270, 9034, 9012, 8260
# OF CONTAINERS: 32
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):37.86 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):25.73 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.99 (gallons)
Flow Rate:N/A (ml/min)Purge Vol:3.0 (gallons)
Length of Time Purged:30 (minutes)Purge Time:1500
Amount Purged:N/A (gallons)Pump Depth:35
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter – YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2–

Time 1516 1519 1522 1525 1528
Temp. °C 17.57 17.56 17.54 17.55 17.56
Sp. Cond 0.018 0.018 0.018 0.018 0.018
DO 0.20 0.18 0.17 0.16 0.16
pH 4.51 4.49 4.45 4.44 4.44
ORP 157.8 169.2 178.9 185.3 190.0
Turbidity 14.3 3.45 1.71 1.51 1.14
Water Level 25.89 25.89 25.89 25.89 25.89

5. NOTES: MS/MSD collected.

APPENDIX B

CHAINS OF CUSTODY & LAB ANALYTICAL REPORTS
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-119203-3
Client Project/Site: Ft.Bragg - Longstreet Landfill
For:
U.S. Army Corps of Engineers
100 W. Oglethorpe Ave.
Savannah, Georgia 31401
Attn: John P. Markov
Authorized for release by:
12/7/2015 2:24:18 PM
Bernard Kirkland, Manager of Project Management
[phone] e.3238
[e-mail]
Designee for
Linda Wolfe, Project Manager II
[phone] e.3005
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
TestAmerica Job ID: 680-119203-3
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .74
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .79
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .82
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .85
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .89
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-119203-3
Project/Site: Ft.Bragg - Longstreet Landfill
Job ID: 680-119203-3
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: U.S. Army Corps of Engineers
Project: Ft.Bragg - Longstreet Landfill
Report Number: 680-119203-3
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 11/19/2015; the samples arrived in good condition, properly preserved and on ice. The temperatures of
the 9 coolers at receipt time were 0.8º C, 1.0º C, 1.0º C, 1.6º C, 1.8º C, 2.2º C, 3.0º C, 3.2º C and 3.6º C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples Trip Blank (680-119203-14) and BLK-1-11-15 (680-119203-15) were analyzed for Volatile Organic Compounds (GC-MS) in
accordance with EPA SW-846 Method 8260B. The samples were analyzed on 12/01/2015.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch
680-412491.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SEMIVOLATILE ORGANIC COMPOUNDS (AQUEOUS)
Samples BLK-1-11-15 (680-119203-15), SLMW-6-11-15 (680-119203-16), SLMW-7R-11-15 (680-119203-17), SLMW-9R-11-15
(680-119203-18), DUP-1-11-15 (680-119203-19), SW-1-11-15 (680-119203-20) and SW-2-11-15 (680-119203-21) were analyzed for
Semivolatile Organic Compounds (Aqueous) in accordance with EPA SW-846 Method 8270D. The samples were prepared on 11/20/2015
and 12/01/2015 and analyzed on 11/27/2015, 11/30/2015 and 12/02/2015.
Surrogate recovery for the following sample was outside control limits: SW-1-11-15 (680-119203-20). Re-extraction and/or re-analysis
was performed outside of holding time with acceptable results.
The following analyte(s) recovered outside control limits for the LCS associated with preparation batch 680-412509 and analytical batch
680-412816: 3,3'-Dichlorobenzidine, and N-Nitrosodiphenylamine. This is not indicative of a systematic control problem because these
were random marginal exceedances. Qualified results have been reported.
Several analytes failed the recovery criteria low for the MS/MSD of sample SLMW-6-11-15 (680-119203-16) in batch 680-412162. Several
analytes exceeded the RPD limit.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated
with prep batch 412509.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PESTICIDES AND PCBS
Samples BLK-1-11-15 (680-119203-15), SLMW-6-11-15 (680-119203-16), SLMW-7R-11-15 (680-119203-17), SLMW-9R-11-15
(680-119203-18), DUP-1-11-15 (680-119203-19), SW-1-11-15 (680-119203-20) and SW-2-11-15 (680-119203-21) were analyzed for
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-119203-3
Project/Site: Ft.Bragg - Longstreet Landfill
Job ID: 680-119203-3 (Continued)
Laboratory: TestAmerica Savannah (Continued)
Pesticides and PCBs in accordance with EPA SW-846 Method 8081B_8082A. The samples were prepared on 11/20/2015 and 11/27/2015
and analyzed on 11/23/2015 and 11/29/2015.
This method incorporates 2nd column confirmation. Corrective action is not taken for surrogate/spike compounds unless results from
both columns are unacceptable. Results outside criteria are qualified.
Surrogate recovery for the following samples was outside control limits: SLMW-7R-11-15 (680-119203-17), SLMW-9R-11-15
(680-119203-18) and DUP-1-11-15 (680-119203-19). Re-extraction and/or re-analysis was performed with concurring results. The
original analysis has been reported.
Surrogate recovery for the following sample was outside control limits: SW-1-11-15 (680-119203-20). Re-extraction and/or re-analysis
was performed outside of holding time with acceptable results. Both sets of data were reported.
Several analytes failed the recovery criteria for the MS/MSD of sample SLMW-6-11-15MS (680-119203-16) in batch 680-411571. Aldrin
and Heptachlor exceeded the RPD limit.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ORGANOPHOSPHORUS PESTICIDES
Samples BLK-1-11-15 (680-119203-15), SLMW-6-11-15 (680-119203-16), SLMW-7R-11-15 (680-119203-17), SLMW-9R-11-15
(680-119203-18), DUP-1-11-15 (680-119203-19), SW-1-11-15 (680-119203-20) and SW-2-11-15 (680-119203-21) were analyzed for
organophosphorus pesticides in accordance with EPA SW-846 Method 8141B. The samples were prepared on 11/20/2015 and analyzed
on 11/25/2015 and 11/26/2015.
This method incorporates 2nd column confirmation. Corrective action is not taken for surrogate/spike compounds unless results from
both columns are unacceptable. Results outside criteria are qualified.
Dimethoate and Fensulfothion were detected in method blank MB 180-161246/1-A at levels that were above the method detection limit but
below the reporting limit. The values should be considered estimates, and have been flagged. If the associated sample reported a result
above the MDL and/or RL, the result has been flagged. Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHLORINATED HERBICIDES
Samples BLK-1-11-15 (680-119203-15), SLMW-6-11-15 (680-119203-16), SLMW-7R-11-15 (680-119203-17), SLMW-9R-11-15
(680-119203-18), DUP-1-11-15 (680-119203-19), SW-1-11-15 (680-119203-20) and SW-2-11-15 (680-119203-21) were analyzed for
chlorinated herbicides in accordance with EPA SW-846 Method 8151A. The samples were prepared on 11/23/2015 and analyzed on
11/27/2015 and 11/28/2015.
This method incorporates 2nd column confirmation. Corrective action is not taken for surrogate/spike compounds unless results from
both columns are unacceptable. Results outside criteria are qualified.
Dinoseb exceeded the RPD limit for the MSD of sample SLMW-6-11-15MSD (680-119203-16) in batch 680-412147.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ANIONS BY ION CHROMATOGRAPHY (48 HOUR)
Sample BLK-1-11-15 (680-119203-15) was analyzed for Anions by Ion Chromatography (48 Hour) in accordance with EPA Method 300.0.
The samples were analyzed on 11/19/2015.
Manual integration was performed on the following sample: (CCV 680-411146/16).
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL CYANIDE
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-119203-3
Project/Site: Ft.Bragg - Longstreet Landfill
Job ID: 680-119203-3 (Continued)
Laboratory: TestAmerica Savannah (Continued)
Sample BLK-1-11-15 (680-119203-15) was analyzed for total cyanide in accordance with EPA SW-846 Method 9012B. The samples were
prepared and analyzed on 11/23/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SULFIDE
Samples BLK-1-11-15 (680-119203-15) and SLMW-6-11-15 (680-119203-16) were analyzed for sulfide in accordance with EPA SW-846
Method 9034. The samples were prepared and analyzed on 11/23/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Sample Summary
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-119203-14 Trip Blank Water 11/18/15 07:00 11/19/15 09:16
680-119203-15 BLK-1-11-15 Water 11/18/15 18:00 11/19/15 09:16
680-119203-16 SLMW-6-11-15 Water 11/17/15 15:30 11/19/15 09:16
680-119203-17 SLMW-7R-11-15 Water 11/17/15 10:55 11/19/15 09:16
680-119203-18 SLMW-9R-11-15 Water 11/17/15 13:30 11/19/15 09:16
680-119203-19 DUP-1-11-15 Water 11/17/15 07:00 11/19/15 09:16
680-119203-20 SW-1-11-15 Water 11/17/15 17:00 11/19/15 09:16
680-119203-21 SW-2-11-15 Water 11/17/15 17:00 11/19/15 09:16
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Method Summary
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL SAV
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL SAV
SW8468081B/8082A Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography TAL SAV
SW8468141BOrganophosphorous Compounds by Gas Chromatography, Capillary Column Technique TAL PIT
SW8468151AHerbicides (GC)TAL SAV
MCAWW300.0 Anions, Ion Chromatography TAL SAV
SW8469012BCyanide, Total andor Amenable TAL SAV
SW8469034Sulfide, Acid Soluble and Insoluble (Titrimetric)TAL SAV
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Definitions/Glossary
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Qualifiers
GC/MS VOA
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
GC/MS Semi VOA
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
Q One or more quality control criteria failed.
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
J Estimated: The analyte was positively identified; the quantitation is an estimation
H Sample was prepped or analyzed beyond the specified holding time
GC Semi VOA
Qualifier Description
M Manual integrated compound.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
U Undetected at the Limit of Detection.
H Sample was prepped or analyzed beyond the specified holding time
HPLC/IC
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
General Chemistry
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Detection Summary
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Client Sample ID: Trip Blank Lab Sample ID: 680-119203-14
No Detections.
Client Sample ID: BLK-1-11-15 Lab Sample ID: 680-119203-15
No Detections.
Client Sample ID: SLMW-6-11-15 Lab Sample ID: 680-119203-16
Bis(2-ethylhexyl) phthalate
RL
9.9 ug/L
MDL
1.6
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J2.7 8270D
Sulfide
RL
10 mg/L
RL
10
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1269034
Client Sample ID: SLMW-7R-11-15 Lab Sample ID: 680-119203-17
Dimethoate
RL
0.94 ug/L
MDL
0.11
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.15 8141B
Fensulfothion 0.94 ug/L0.16 Total/NA10.17 J 8141B
Client Sample ID: SLMW-9R-11-15 Lab Sample ID: 680-119203-18
1,4-Dichlorobenzene
RL
9.6 ug/L
MDL
0.52
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J1.6 8270D
Diethyl phthalate 9.6 ug/L0.84 Total/NA11.1 J 8270D
Client Sample ID: DUP-1-11-15 Lab Sample ID: 680-119203-19
1,4-Dichlorobenzene
RL
9.6 ug/L
MDL
0.52
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J1.6 8270D
Diethyl phthalate 9.6 ug/L0.84 Total/NA11.2 J 8270D
Client Sample ID: SW-1-11-15 Lab Sample ID: 680-119203-20
Diethyl phthalate - RE
RL
9.6 ug/L
MDL
0.84
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J H1.7 8270D
Client Sample ID: SW-2-11-15 Lab Sample ID: 680-119203-21
No Detections.
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-14Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 11/18/15 07:00
Date Received: 11/19/15 09:16
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 7.0 U 10 7.0 ug/L 12/01/15 11:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.43 ug/L 12/01/15 11:14 1Benzene0.43 U
1.0 0.50 ug/L 12/01/15 11:14 1Bromobenzene0.50 U
1.0 0.43 ug/L 12/01/15 11:14 1Bromoform0.43 U
5.0 2.5 ug/L 12/01/15 11:14 1Bromomethane2.5 U
10 3.4 ug/L 12/01/15 11:14 12-Butanone (MEK)3.4 U
1.0 0.33 ug/L 12/01/15 11:14 1Carbon tetrachloride 0.33 U
1.0 0.26 ug/L 12/01/15 11:14 1Chlorobenzene0.26 U
1.0 0.45 ug/L 12/01/15 11:14 1Chlorobromomethane0.45 U
1.0 0.32 ug/L 12/01/15 11:14 1Chlorodibromomethane0.32 U
5.0 2.5 ug/L 12/01/15 11:14 1Chloroethane2.5 U
1.0 0.50 ug/L 12/01/15 11:14 1Chloroform0.50 U
5.0 1.1 ug/L 12/01/15 11:14 11-Chlorohexane 1.1 U
1.0 0.40 ug/L 12/01/15 11:14 1Chloromethane0.40 U
1.0 0.27 ug/L 12/01/15 11:14 12-Chlorotoluene 0.27 U
1.0 0.45 ug/L 12/01/15 11:14 14-Chlorotoluene 0.45 U
1.0 0.41 ug/L 12/01/15 11:14 1cis-1,2-Dichloroethene 0.41 U
1.0 0.40 ug/L 12/01/15 11:14 1cis-1,3-Dichloropropene 0.40 U
5.0 1.1 ug/L 12/01/15 11:14 11,2-Dibromo-3-Chloropropane 1.1 U
1.0 0.37 ug/L 12/01/15 11:14 11,2-Dichlorobenzene 0.37 U
1.0 0.43 ug/L 12/01/15 11:14 11,3-Dichlorobenzene 0.43 U
1.0 0.46 ug/L 12/01/15 11:14 11,4-Dichlorobenzene 0.46 U
1.0 0.44 ug/L 12/01/15 11:14 1Dichlorobromomethane0.44 U
1.0 0.60 ug/L 12/01/15 11:14 1Dichlorodifluoromethane0.60 U
1.0 0.38 ug/L 12/01/15 11:14 11,1-Dichloroethane 0.38 U
1.0 0.50 ug/L 12/01/15 11:14 11,2-Dichloroethane 0.50 U
1.0 0.36 ug/L 12/01/15 11:14 11,1-Dichloroethene 0.36 U
1.0 0.67 ug/L 12/01/15 11:14 11,2-Dichloropropane 0.67 U
1.0 0.34 ug/L 12/01/15 11:14 11,3-Dichloropropane 0.34 U
1.0 0.37 ug/L 12/01/15 11:14 12,2-Dichloropropane 0.37 U
1.0 0.34 ug/L 12/01/15 11:14 11,1-Dichloropropene 0.34 U
1.0 0.33 ug/L 12/01/15 11:14 1Ethylbenzene0.33 U
1.0 0.44 ug/L 12/01/15 11:14 1Ethylene Dibromide 0.44 U
5.0 2.5 ug/L 12/01/15 11:14 1Hexachlorobutadiene2.5 U
1.0 0.35 ug/L 12/01/15 11:14 1Isopropylbenzene0.35 U
10 1.0 ug/L 12/01/15 11:14 1Isopropyl ether 1.0 U
1.0 0.48 ug/L 12/01/15 11:14 14-Isopropyltoluene 0.48 U
5.0 2.5 ug/L 12/01/15 11:14 1Methylene Chloride 2.5 U
10 2.1 ug/L 12/01/15 11:14 14-Methyl-2-pentanone (MIBK)2.1 U
10 0.30 ug/L 12/01/15 11:14 1Methyl tert-butyl ether 0.30 U
5.0 2.5 ug/L 12/01/15 11:14 1Naphthalene2.5 U
1.0 0.47 ug/L 12/01/15 11:14 1n-Butylbenzene 0.47 U
1.0 0.38 ug/L 12/01/15 11:14 1N-Propylbenzene 0.38 U
1.0 0.42 ug/L 12/01/15 11:14 1sec-Butylbenzene 0.42 U
1.0 0.27 ug/L 12/01/15 11:14 1Styrene0.27 U
1.0 0.45 ug/L 12/01/15 11:14 1tert-Butylbenzene 0.45 U
1.0 0.37 ug/L 12/01/15 11:14 11,1,1,2-Tetrachloroethane 0.37 U
1.0 0.62 ug/L 12/01/15 11:14 11,1,2,2-Tetrachloroethane 0.62 U
1.0 0.74 ug/L 12/01/15 11:14 1Tetrachloroethene0.74 U
TestAmerica Savannah
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-14Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 11/18/15 07:00
Date Received: 11/19/15 09:16
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene 0.48 U 1.0 0.48 ug/L 12/01/15 11:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.37 ug/L 12/01/15 11:14 1trans-1,2-Dichloroethene 0.37 U
1.0 0.42 ug/L 12/01/15 11:14 1trans-1,3-Dichloropropene 0.42 U
5.0 2.5 ug/L 12/01/15 11:14 11,2,3-Trichlorobenzene 2.5 U
5.0 2.5 ug/L 12/01/15 11:14 11,2,4-Trichlorobenzene 2.5 U
1.0 0.37 ug/L 12/01/15 11:14 11,1,1-Trichloroethane 0.37 U
1.0 0.33 ug/L 12/01/15 11:14 11,1,2-Trichloroethane 0.33 U
1.0 0.48 ug/L 12/01/15 11:14 1Trichloroethene0.48 U
1.0 0.42 ug/L 12/01/15 11:14 1Trichlorofluoromethane0.42 U
1.0 0.39 ug/L 12/01/15 11:14 11,2,3-Trichloropropane 0.39 U
1.0 0.47 ug/L 12/01/15 11:14 11,2,4-Trimethylbenzene 0.47 U
1.0 0.31 ug/L 12/01/15 11:14 11,3,5-Trimethylbenzene 0.31 U
1.0 0.50 ug/L 12/01/15 11:14 1Vinyl chloride 0.50 U
Toluene-d8 (Surr)107 70-130 12/01/15 11:14 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)101 12/01/15 11:14 170-130
Dibromofluoromethane (Surr)104 12/01/15 11:14 170-130
4-Bromofluorobenzene (Surr)101 12/01/15 11:14 170-130
Lab Sample ID: 680-119203-15Client Sample ID: BLK-1-11-15
Matrix: WaterDate Collected: 11/18/15 18:00
Date Received: 11/19/15 09:16
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 7.0 U 10 7.0 ug/L 12/01/15 12:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.43 ug/L 12/01/15 12:19 1Benzene0.43 U
1.0 0.50 ug/L 12/01/15 12:19 1Bromobenzene0.50 U
1.0 0.43 ug/L 12/01/15 12:19 1Bromoform0.43 U
5.0 2.5 ug/L 12/01/15 12:19 1Bromomethane2.5 U
10 3.4 ug/L 12/01/15 12:19 12-Butanone (MEK)3.4 U
1.0 0.33 ug/L 12/01/15 12:19 1Carbon tetrachloride 0.33 U
1.0 0.26 ug/L 12/01/15 12:19 1Chlorobenzene0.26 U
1.0 0.45 ug/L 12/01/15 12:19 1Chlorobromomethane0.45 U
1.0 0.32 ug/L 12/01/15 12:19 1Chlorodibromomethane0.32 U
5.0 2.5 ug/L 12/01/15 12:19 1Chloroethane2.5 U
1.0 0.50 ug/L 12/01/15 12:19 1Chloroform0.50 U
5.0 1.1 ug/L 12/01/15 12:19 11-Chlorohexane 1.1 U
1.0 0.40 ug/L 12/01/15 12:19 1Chloromethane0.40 U
1.0 0.27 ug/L 12/01/15 12:19 12-Chlorotoluene 0.27 U
1.0 0.45 ug/L 12/01/15 12:19 14-Chlorotoluene 0.45 U
1.0 0.41 ug/L 12/01/15 12:19 1cis-1,2-Dichloroethene 0.41 U
1.0 0.40 ug/L 12/01/15 12:19 1cis-1,3-Dichloropropene 0.40 U
5.0 1.1 ug/L 12/01/15 12:19 11,2-Dibromo-3-Chloropropane 1.1 U
1.0 0.37 ug/L 12/01/15 12:19 11,2-Dichlorobenzene 0.37 U
1.0 0.43 ug/L 12/01/15 12:19 11,3-Dichlorobenzene 0.43 U
1.0 0.46 ug/L 12/01/15 12:19 11,4-Dichlorobenzene 0.46 U
1.0 0.44 ug/L 12/01/15 12:19 1Dichlorobromomethane0.44 U
1.0 0.60 ug/L 12/01/15 12:19 1Dichlorodifluoromethane0.60 U
TestAmerica Savannah
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-15Client Sample ID: BLK-1-11-15
Matrix: WaterDate Collected: 11/18/15 18:00
Date Received: 11/19/15 09:16
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloroethane 0.38 U 1.0 0.38 ug/L 12/01/15 12:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.50 ug/L 12/01/15 12:19 11,2-Dichloroethane 0.50 U
1.0 0.36 ug/L 12/01/15 12:19 11,1-Dichloroethene 0.36 U
1.0 0.67 ug/L 12/01/15 12:19 11,2-Dichloropropane 0.67 U
1.0 0.34 ug/L 12/01/15 12:19 11,3-Dichloropropane 0.34 U
1.0 0.37 ug/L 12/01/15 12:19 12,2-Dichloropropane 0.37 U
1.0 0.34 ug/L 12/01/15 12:19 11,1-Dichloropropene 0.34 U
1.0 0.33 ug/L 12/01/15 12:19 1Ethylbenzene0.33 U
1.0 0.44 ug/L 12/01/15 12:19 1Ethylene Dibromide 0.44 U
5.0 2.5 ug/L 12/01/15 12:19 1Hexachlorobutadiene2.5 U
1.0 0.35 ug/L 12/01/15 12:19 1Isopropylbenzene0.35 U
10 1.0 ug/L 12/01/15 12:19 1Isopropyl ether 1.0 U
1.0 0.48 ug/L 12/01/15 12:19 14-Isopropyltoluene 0.48 U
5.0 2.5 ug/L 12/01/15 12:19 1Methylene Chloride 2.5 U
10 2.1 ug/L 12/01/15 12:19 14-Methyl-2-pentanone (MIBK)2.1 U
10 0.30 ug/L 12/01/15 12:19 1Methyl tert-butyl ether 0.30 U
5.0 2.5 ug/L 12/01/15 12:19 1Naphthalene2.5 U
1.0 0.47 ug/L 12/01/15 12:19 1n-Butylbenzene 0.47 U
1.0 0.38 ug/L 12/01/15 12:19 1N-Propylbenzene 0.38 U
1.0 0.42 ug/L 12/01/15 12:19 1sec-Butylbenzene 0.42 U
1.0 0.27 ug/L 12/01/15 12:19 1Styrene0.27 U
1.0 0.45 ug/L 12/01/15 12:19 1tert-Butylbenzene 0.45 U
1.0 0.37 ug/L 12/01/15 12:19 11,1,1,2-Tetrachloroethane 0.37 U
1.0 0.62 ug/L 12/01/15 12:19 11,1,2,2-Tetrachloroethane 0.62 U
1.0 0.74 ug/L 12/01/15 12:19 1Tetrachloroethene0.74 U
1.0 0.48 ug/L 12/01/15 12:19 1Toluene0.48 U
1.0 0.37 ug/L 12/01/15 12:19 1trans-1,2-Dichloroethene 0.37 U
1.0 0.42 ug/L 12/01/15 12:19 1trans-1,3-Dichloropropene 0.42 U
5.0 2.5 ug/L 12/01/15 12:19 11,2,3-Trichlorobenzene 2.5 U
5.0 2.5 ug/L 12/01/15 12:19 11,2,4-Trichlorobenzene 2.5 U
1.0 0.37 ug/L 12/01/15 12:19 11,1,1-Trichloroethane 0.37 U
1.0 0.33 ug/L 12/01/15 12:19 11,1,2-Trichloroethane 0.33 U
1.0 0.48 ug/L 12/01/15 12:19 1Trichloroethene0.48 U
1.0 0.42 ug/L 12/01/15 12:19 1Trichlorofluoromethane0.42 U
1.0 0.39 ug/L 12/01/15 12:19 11,2,3-Trichloropropane 0.39 U
1.0 0.47 ug/L 12/01/15 12:19 11,2,4-Trimethylbenzene 0.47 U
1.0 0.31 ug/L 12/01/15 12:19 11,3,5-Trimethylbenzene 0.31 U
1.0 0.50 ug/L 12/01/15 12:19 1Vinyl chloride 0.50 U
Toluene-d8 (Surr)107 70-130 12/01/15 12:19 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)104 12/01/15 12:19 170-130
Dibromofluoromethane (Surr)105 12/01/15 12:19 170-130
4-Bromofluorobenzene (Surr)102 12/01/15 12:19 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,2,4-Trichlorobenzene 0.54 U 9.6 0.54 ug/L 11/20/15 15:44 11/30/15 18:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.6 0.51 ug/L 11/20/15 15:44 11/30/15 18:56 11,2-Dichlorobenzene 0.51 U
9.6 0.56 ug/L 11/20/15 15:44 11/30/15 18:56 11,3-Dichlorobenzene 0.56 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-15Client Sample ID: BLK-1-11-15
Matrix: WaterDate Collected: 11/18/15 18:00
Date Received: 11/19/15 09:16
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,4-Dichlorobenzene 0.52 U 9.6 0.52 ug/L 11/20/15 15:44 11/30/15 18:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 18:56 12,4,5-Trichlorophenol 1.1 U
9.6 0.81 ug/L 11/20/15 15:44 11/30/15 18:56 12,4,6-Trichlorophenol 0.81 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 18:56 12,4-Dichlorophenol 1.1 U
9.6 3.8 ug/L 11/20/15 15:44 11/30/15 18:56 12,4-Dimethylphenol 3.8 U
48 9.6 ug/L 11/20/15 15:44 11/30/15 18:56 12,4-Dinitrophenol 9.6 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 18:56 12,4-Dinitrotoluene 1.1 U
9.6 0.83 ug/L 11/20/15 15:44 11/30/15 18:56 12-Chlorophenol 0.83 U
9.6 0.76 ug/L 11/20/15 15:44 11/30/15 18:56 12-Chloronaphthalene 0.76 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 18:56 12-Methylnaphthalene 0.75 U
9.6 0.85 ug/L 11/20/15 15:44 11/30/15 18:56 12-Methylphenol 0.85 U
48 1.2 ug/L 11/20/15 15:44 11/30/15 18:56 12-Nitroaniline 1.2 U
9.6 0.73 ug/L 11/20/15 15:44 11/30/15 18:56 12-Nitrophenol 0.73 U
9.6 1.2 ug/L 11/20/15 15:44 11/30/15 18:56 13 & 4 Methylphenol 1.2 U
57 29 ug/L 11/20/15 15:44 11/30/15 18:56 13,3'-Dichlorobenzidine 29 U
48 4.8 ug/L 11/20/15 15:44 11/30/15 18:56 13-Nitroaniline 4.8 U
48 9.6 ug/L 11/20/15 15:44 11/30/15 18:56 14,6-Dinitro-2-methylphenol 9.6 U
9.6 0.74 ug/L 11/20/15 15:44 11/30/15 18:56 14-Bromophenyl phenyl ether 0.74 U
9.6 0.96 ug/L 11/20/15 15:44 11/30/15 18:56 14-Chloro-3-methylphenol 0.96 U
19 2.1 ug/L 11/20/15 15:44 11/30/15 18:56 14-Chloroaniline 2.1 U
9.6 0.80 ug/L 11/20/15 15:44 11/30/15 18:56 14-Chlorophenyl phenyl ether 0.80 U
48 4.8 ug/L 11/20/15 15:44 11/30/15 18:56 14-Nitroaniline 4.8 U
9.6 0.73 ug/L 11/20/15 15:44 11/30/15 18:56 1Acenaphthene0.73 U
9.6 0.81 ug/L 11/20/15 15:44 11/30/15 18:56 1Acenaphthylene0.81 U
9.6 0.66 ug/L 11/20/15 15:44 11/30/15 18:56 1Anthracene0.66 U
9.6 0.53 ug/L 11/20/15 15:44 11/30/15 18:56 1Benzo[a]anthracene 0.53 U
9.6 0.68 ug/L 11/20/15 15:44 11/30/15 18:56 1Benzo[a]pyrene 0.68 U
9.6 2.5 ug/L 11/20/15 15:44 11/30/15 18:56 1Benzo[b]fluoranthene 2.5 U
9.6 0.83 ug/L 11/20/15 15:44 11/30/15 18:56 1Benzo[g,h,i]perylene 0.83 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 18:56 1Benzo[k]fluoranthene 1.1 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 18:56 1Benzyl alcohol 1.1 U
9.6 0.90 ug/L 11/20/15 15:44 11/30/15 18:56 1Bis(2-chloroethoxy)methane 0.90 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 18:56 1Bis(2-chloroethyl)ether 1.1 U
9.6 1.5 ug/L 11/20/15 15:44 11/30/15 18:56 1Bis(2-ethylhexyl) phthalate 1.5 U
9.6 0.49 ug/L 11/20/15 15:44 11/30/15 18:56 1Chrysene0.49 U
9.6 0.96 ug/L 11/20/15 15:44 11/30/15 18:56 1Dibenz(a,h)anthracene 0.96 U
9.6 0.76 ug/L 11/20/15 15:44 11/30/15 18:56 1Dibenzofuran0.76 U
9.6 0.79 ug/L 11/20/15 15:44 11/30/15 18:56 1Di-n-butyl phthalate 0.79 U
9.6 0.84 ug/L 11/20/15 15:44 11/30/15 18:56 1Diethyl phthalate 0.84 U
9.6 0.95 ug/L 11/20/15 15:44 11/30/15 18:56 1Dimethyl phthalate 0.95 U
9.6 1.3 ug/L 11/20/15 15:44 11/30/15 18:56 1Di-n-octyl phthalate 1.3 U
9.6 0.71 ug/L 11/20/15 15:44 11/30/15 18:56 1Fluoranthene0.71 U
9.6 0.92 ug/L 11/20/15 15:44 11/30/15 18:56 1Fluorene0.92 U
9.6 0.76 ug/L 11/20/15 15:44 11/30/15 18:56 1Hexachlorobenzene0.76 U
9.6 0.59 ug/L 11/20/15 15:44 11/30/15 18:56 1Hexachlorobutadiene0.59 U
9.6 0.73 ug/L 11/20/15 15:44 11/30/15 18:56 1Hexachloroethane0.73 U
9.6 0.96 ug/L 11/20/15 15:44 11/30/15 18:56 1Indeno[1,2,3-cd]pyrene 0.96 U
9.6 0.86 ug/L 11/20/15 15:44 11/30/15 18:56 1Isophorone0.86 U
9.6 0.67 ug/L 11/20/15 15:44 11/30/15 18:56 1Naphthalene0.67 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-15Client Sample ID: BLK-1-11-15
Matrix: WaterDate Collected: 11/18/15 18:00
Date Received: 11/19/15 09:16
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Nitrobenzene 0.70 U 9.6 0.70 ug/L 11/20/15 15:44 11/30/15 18:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.6 0.88 ug/L 11/20/15 15:44 11/30/15 18:56 1N-Nitrosodiphenylamine 0.88 U Q
9.6 0.69 ug/L 11/20/15 15:44 11/30/15 18:56 1N-Nitrosodi-n-propylamine 0.69 U
48 1.9 ug/L 11/20/15 15:44 11/30/15 18:56 1Pentachlorophenol1.9 U
9.6 0.74 ug/L 11/20/15 15:44 11/30/15 18:56 1Phenanthrene0.74 U
9.6 0.79 ug/L 11/20/15 15:44 11/30/15 18:56 1Phenol0.79 U
9.6 0.60 ug/L 11/20/15 15:44 11/30/15 18:56 1Pyrene0.60 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 18:56 1Butyl benzyl phthalate 1.1 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 18:56 1bis(chloroisopropyl) ether 0.75 U
48 4.8 ug/L 11/20/15 15:44 11/30/15 18:56 1Benzoic acid 4.8 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 18:56 12,6-Dinitrotoluene 1.1 U
48 1.8 ug/L 11/20/15 15:44 11/30/15 18:56 14-Nitrophenol 1.8 U
2,4,6-Tribromophenol 55 39-124 11/20/15 15:44 11/30/15 18:56 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 55 11/20/15 15:44 11/30/15 18:56 132-113
2-Fluorophenol 44 11/20/15 15:44 11/30/15 18:56 126-109
Terphenyl-d14 70 11/20/15 15:44 11/30/15 18:56 110-126
Phenol-d5 50 11/20/15 15:44 11/30/15 18:56 127-110
Nitrobenzene-d5 52 11/20/15 15:44 11/30/15 18:56 132-118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography
RL MDL
Toxaphene 0.38 U 4.8 0.38 ug/L 11/20/15 15:44 11/23/15 15:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.048 0.0072 ug/L 11/20/15 15:44 11/23/15 15:59 1delta-BHC 0.0072 U
0.048 0.0036 ug/L 11/20/15 15:44 11/23/15 15:59 1Dieldrin0.0036 U
0.048 0.0034 ug/L 11/20/15 15:44 11/23/15 15:59 1Endosulfan I 0.0034 U
0.048 0.0040 ug/L 11/20/15 15:44 11/23/15 15:59 1Endosulfan II 0.0040 U
0.048 0.0049 ug/L 11/20/15 15:44 11/23/15 15:59 1Endosulfan sulfate 0.0049 U
0.048 0.0051 ug/L 11/20/15 15:44 11/23/15 15:59 1Endrin0.0051 U
0.048 0.0059 ug/L 11/20/15 15:44 11/23/15 15:59 1Endrin aldehyde 0.0059 U
0.048 0.0044 ug/L 11/20/15 15:44 11/23/15 15:59 1Endrin ketone 0.0044 U
0.048 0.0035 ug/L 11/20/15 15:44 11/23/15 15:59 1gamma-BHC (Lindane)0.0035 U
0.048 0.0068 ug/L 11/20/15 15:44 11/23/15 15:59 1Heptachlor0.0068 U
0.048 0.0036 ug/L 11/20/15 15:44 11/23/15 15:59 1Heptachlor epoxide 0.0036 U
0.048 0.0094 ug/L 11/20/15 15:44 11/23/15 15:59 1Methoxychlor0.0094 U
0.96 0.17 ug/L 11/20/15 15:44 11/23/15 15:59 1PCB-1016 0.17 U
0.048 0.0061 ug/L 11/20/15 15:44 11/23/15 15:59 14,4'-DDD 0.0061 U
0.048 0.0049 ug/L 11/20/15 15:44 11/23/15 15:59 14,4'-DDE 0.0049 U
0.048 0.0067 ug/L 11/20/15 15:44 11/23/15 15:59 14,4'-DDT 0.0067 U
0.048 0.0069 ug/L 11/20/15 15:44 11/23/15 15:59 1Aldrin0.0069 U
0.048 0.0033 ug/L 11/20/15 15:44 11/23/15 15:59 1alpha-BHC 0.0033 U
0.048 0.0087 ug/L 11/20/15 15:44 11/23/15 15:59 1beta-BHC 0.0087 U
0.48 0.091 ug/L 11/20/15 15:44 11/23/15 15:59 1Chlordane (technical)0.091 U
0.96 0.18 ug/L 11/20/15 15:44 11/23/15 15:59 1PCB-1221 0.18 U
0.96 0.24 ug/L 11/20/15 15:44 11/23/15 15:59 1PCB-1232 0.24 U
0.96 0.18 ug/L 11/20/15 15:44 11/23/15 15:59 1PCB-1242 0.18 U
0.96 0.20 ug/L 11/20/15 15:44 11/23/15 15:59 1PCB-1248 0.20 U
0.96 0.11 ug/L 11/20/15 15:44 11/23/15 15:59 1PCB-1254 0.11 U
0.96 0.12 ug/L 11/20/15 15:44 11/23/15 15:59 1PCB-1260 0.12 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-15Client Sample ID: BLK-1-11-15
Matrix: WaterDate Collected: 11/18/15 18:00
Date Received: 11/19/15 09:16
Tetrachloro-m-xylene 58 40-130 11/20/15 15:44 11/23/15 15:59 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 22 11/20/15 15:44 11/23/15 15:59 114-130
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique
RL MDL
Azinphos-methyl 0.11 U 0.94 0.11 ug/L 11/20/15 12:40 11/26/15 02:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.94 0.10 ug/L 11/20/15 12:40 11/26/15 02:33 1Bolstar0.10 U
0.94 0.096 ug/L 11/20/15 12:40 11/26/15 02:33 1Chlorpyrifos0.096 U
0.94 0.14 ug/L 11/20/15 12:40 11/26/15 02:33 1Coumaphos0.14 U
1.9 0.16 ug/L 11/20/15 12:40 11/26/15 02:33 1Demeton, Total 0.16 U
0.94 0.089 ug/L 11/20/15 12:40 11/26/15 02:33 1Diazinon0.089 U
0.94 0.080 ug/L 11/20/15 12:40 11/26/15 02:33 1Dichlorvos0.080 U
0.94 0.11 ug/L 11/20/15 12:40 11/26/15 02:33 1Dimethoate0.11 U
0.94 0.095 ug/L 11/20/15 12:40 11/26/15 02:33 1Disulfoton0.095 U
0.94 0.11 ug/L 11/20/15 12:40 11/26/15 02:33 1EPN0.11 U
0.94 0.095 ug/L 11/20/15 12:40 11/26/15 02:33 1Mocap0.095 U
0.94 0.12 ug/L 11/20/15 12:40 11/26/15 02:33 1Famphur0.12 U
0.94 0.16 ug/L 11/20/15 12:40 11/26/15 02:33 1Fensulfothion0.16 U
0.94 0.080 ug/L 11/20/15 12:40 11/26/15 02:33 1Fenthion0.080 U
0.94 0.10 ug/L 11/20/15 12:40 11/26/15 02:33 1Malathion0.10 U
0.94 0.15 ug/L 11/20/15 12:40 11/26/15 02:33 1Parathion0.15 U
0.94 0.10 ug/L 11/20/15 12:40 11/26/15 02:33 1Methyl parathion 0.10 U
0.94 0.092 ug/L 11/20/15 12:40 11/26/15 02:33 1Mevinphos0.092 U
0.94 0.087 ug/L 11/20/15 12:40 11/26/15 02:33 1Phorate0.087 U
0.94 0.097 ug/L 11/20/15 12:40 11/26/15 02:33 1Ronnel0.097 U
0.94 0.090 ug/L 11/20/15 12:40 11/26/15 02:33 1Stirophos0.090 U
0.94 0.089 ug/L 11/20/15 12:40 11/26/15 02:33 1Sulfotepp0.089 U
0.94 0.095 ug/L 11/20/15 12:40 11/26/15 02:33 1Thionazin0.095 U
0.94 0.088 ug/L 11/20/15 12:40 11/26/15 02:33 1Tokuthion0.088 U
0.94 0.094 ug/L 11/20/15 12:40 11/26/15 02:33 1Trichloronate0.094 U
0.94 0.094 ug/L 11/20/15 12:40 11/26/15 02:33 1O,O,O-Triethyl phosphorothioate 0.094 U
Tributyl phosphate 98 49-122 11/20/15 12:40 11/26/15 02:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tributyl phosphate 102 11/20/15 12:40 11/26/15 02:33 149-122
Triphenylphosphate 102 11/20/15 12:40 11/26/15 02:33 145-145
Triphenylphosphate 106 11/20/15 12:40 11/26/15 02:33 145-145
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D 0.035 U 0.48 0.035 ug/L 11/23/15 07:48 11/27/15 22:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.48 0.14 ug/L 11/23/15 07:48 11/27/15 22:51 12,4-DB 0.14 U
0.24 0.059 ug/L 11/23/15 07:48 11/27/15 22:51 12,4,5-T 0.059 U
0.24 0.059 ug/L 11/23/15 07:48 11/27/15 22:51 1Silvex (2,4,5-TP)0.059 U
4.8 0.095 ug/L 11/23/15 07:48 11/27/15 22:51 1Dalapon0.095 U
0.48 0.081 ug/L 11/23/15 07:48 11/27/15 22:51 1Dicamba0.081 U
0.48 0.14 ug/L 11/23/15 07:48 11/27/15 22:51 1Dichlorprop0.14 U
0.95 0.15 ug/L 11/23/15 07:48 11/27/15 22:51 1Dinoseb0.15 U
110 16 ug/L 11/23/15 07:48 11/27/15 22:51 1MCPA16 U
110 18 ug/L 11/23/15 07:48 11/27/15 22:51 1Mecoprop18 U
0.24 0.035 ug/L 11/23/15 07:48 11/27/15 22:51 1Pentachlorophenol0.035 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-15Client Sample ID: BLK-1-11-15
Matrix: WaterDate Collected: 11/18/15 18:00
Date Received: 11/19/15 09:16
DCAA 68 45-130 11/23/15 07:48 11/27/15 22:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.023 U 0.050 0.023 mg/L 11/19/15 20:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Cyanide, Total 0.0025 U 0.010 0.0025 mg/L 11/23/15 07:00 11/23/15 12:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
RL RL
Sulfide 10 U 10 10 mg/L 11/23/15 14:09 11/23/15 14:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Lab Sample ID: 680-119203-16Client Sample ID: SLMW-6-11-15
Matrix: WaterDate Collected: 11/17/15 15:30
Date Received: 11/19/15 09:16
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,2,4-Trichlorobenzene 0.56 U J 9.9 0.56 ug/L 11/20/15 15:44 11/27/15 20:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.9 0.53 ug/L 11/20/15 15:44 11/27/15 20:16 11,2-Dichlorobenzene 0.53 U J
9.9 0.59 ug/L 11/20/15 15:44 11/27/15 20:16 11,3-Dichlorobenzene 0.59 U J
9.9 0.54 ug/L 11/20/15 15:44 11/27/15 20:16 11,4-Dichlorobenzene 0.54 U J
9.9 1.2 ug/L 11/20/15 15:44 11/27/15 20:16 12,4,5-Trichlorophenol 1.2 U
9.9 0.84 ug/L 11/20/15 15:44 11/27/15 20:16 12,4,6-Trichlorophenol 0.84 U
9.9 1.1 ug/L 11/20/15 15:44 11/27/15 20:16 12,4-Dichlorophenol 1.1 U
9.9 4.0 ug/L 11/20/15 15:44 11/27/15 20:16 12,4-Dimethylphenol 4.0 U
50 9.9 ug/L 11/20/15 15:44 11/27/15 20:16 12,4-Dinitrophenol 9.9 U
9.9 1.2 ug/L 11/20/15 15:44 11/27/15 20:16 12,4-Dinitrotoluene 1.2 U
9.9 0.86 ug/L 11/20/15 15:44 11/27/15 20:16 12-Chlorophenol 0.86 U
9.9 0.79 ug/L 11/20/15 15:44 11/27/15 20:16 12-Chloronaphthalene 0.79 U J
9.9 0.77 ug/L 11/20/15 15:44 11/27/15 20:16 12-Methylnaphthalene 0.77 U J
9.9 0.88 ug/L 11/20/15 15:44 11/27/15 20:16 12-Methylphenol 0.88 U
50 1.3 ug/L 11/20/15 15:44 11/27/15 20:16 12-Nitroaniline 1.3 U
9.9 0.75 ug/L 11/20/15 15:44 11/27/15 20:16 12-Nitrophenol 0.75 U
9.9 1.3 ug/L 11/20/15 15:44 11/27/15 20:16 13 & 4 Methylphenol 1.3 U
60 30 ug/L 11/20/15 15:44 11/27/15 20:16 13,3'-Dichlorobenzidine 30 U J
50 5.0 ug/L 11/20/15 15:44 11/27/15 20:16 13-Nitroaniline 5.0 U J
50 9.9 ug/L 11/20/15 15:44 11/27/15 20:16 14,6-Dinitro-2-methylphenol 9.9 U
9.9 0.76 ug/L 11/20/15 15:44 11/27/15 20:16 14-Bromophenyl phenyl ether 0.76 U J
9.9 0.99 ug/L 11/20/15 15:44 11/27/15 20:16 14-Chloro-3-methylphenol 0.99 U
20 2.2 ug/L 11/20/15 15:44 11/27/15 20:16 14-Chloroaniline 2.2 U J
9.9 0.83 ug/L 11/20/15 15:44 11/27/15 20:16 14-Chlorophenyl phenyl ether 0.83 U J
50 5.0 ug/L 11/20/15 15:44 11/27/15 20:16 14-Nitroaniline 5.0 U J
9.9 0.75 ug/L 11/20/15 15:44 11/27/15 20:16 1Acenaphthene0.75 U
9.9 0.84 ug/L 11/20/15 15:44 11/27/15 20:16 1Acenaphthylene0.84 U J
9.9 0.68 ug/L 11/20/15 15:44 11/27/15 20:16 1Anthracene0.68 U
9.9 0.55 ug/L 11/20/15 15:44 11/27/15 20:16 1Benzo[a]anthracene 0.55 U
9.9 0.70 ug/L 11/20/15 15:44 11/27/15 20:16 1Benzo[a]pyrene 0.70 U
9.9 2.6 ug/L 11/20/15 15:44 11/27/15 20:16 1Benzo[b]fluoranthene 2.6 U
9.9 0.86 ug/L 11/20/15 15:44 11/27/15 20:16 1Benzo[g,h,i]perylene 0.86 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-16Client Sample ID: SLMW-6-11-15
Matrix: WaterDate Collected: 11/17/15 15:30
Date Received: 11/19/15 09:16
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Benzo[k]fluoranthene 1.2 U 9.9 1.2 ug/L 11/20/15 15:44 11/27/15 20:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.9 1.1 ug/L 11/20/15 15:44 11/27/15 20:16 1Benzyl alcohol 1.1 U
9.9 0.93 ug/L 11/20/15 15:44 11/27/15 20:16 1Bis(2-chloroethoxy)methane 0.93 U
9.9 1.1 ug/L 11/20/15 15:44 11/27/15 20:16 1Bis(2-chloroethyl)ether 1.1 U
9.9 1.6 ug/L 11/20/15 15:44 11/27/15 20:16 1Bis(2-ethylhexyl) phthalate 2.7 J
9.9 0.51 ug/L 11/20/15 15:44 11/27/15 20:16 1Chrysene0.51 U
9.9 0.99 ug/L 11/20/15 15:44 11/27/15 20:16 1Dibenz(a,h)anthracene 0.99 U
9.9 0.78 ug/L 11/20/15 15:44 11/27/15 20:16 1Dibenzofuran0.78 U J
9.9 0.82 ug/L 11/20/15 15:44 11/27/15 20:16 1Di-n-butyl phthalate 0.82 U
9.9 0.87 ug/L 11/20/15 15:44 11/27/15 20:16 1Diethyl phthalate 0.87 U
9.9 0.98 ug/L 11/20/15 15:44 11/27/15 20:16 1Dimethyl phthalate 0.98 U
9.9 1.4 ug/L 11/20/15 15:44 11/27/15 20:16 1Di-n-octyl phthalate 1.4 U
9.9 0.73 ug/L 11/20/15 15:44 11/27/15 20:16 1Fluoranthene0.73 U
9.9 0.95 ug/L 11/20/15 15:44 11/27/15 20:16 1Fluorene0.95 U J
9.9 0.78 ug/L 11/20/15 15:44 11/27/15 20:16 1Hexachlorobenzene0.78 U
9.9 0.61 ug/L 11/20/15 15:44 11/27/15 20:16 1Hexachlorobutadiene0.61 U J
9.9 0.75 ug/L 11/20/15 15:44 11/27/15 20:16 1Hexachloroethane0.75 U J
9.9 0.99 ug/L 11/20/15 15:44 11/27/15 20:16 1Indeno[1,2,3-cd]pyrene 0.99 U
9.9 0.89 ug/L 11/20/15 15:44 11/27/15 20:16 1Isophorone0.89 U
9.9 0.69 ug/L 11/20/15 15:44 11/27/15 20:16 1Naphthalene0.69 U J
9.9 0.72 ug/L 11/20/15 15:44 11/27/15 20:16 1Nitrobenzene0.72 U
9.9 0.91 ug/L 11/20/15 15:44 11/27/15 20:16 1N-Nitrosodiphenylamine 0.91 U J Q
9.9 0.71 ug/L 11/20/15 15:44 11/27/15 20:16 1N-Nitrosodi-n-propylamine 0.71 U
50 2.0 ug/L 11/20/15 15:44 11/27/15 20:16 1Pentachlorophenol2.0 U
9.9 0.76 ug/L 11/20/15 15:44 11/27/15 20:16 1Phenanthrene0.76 U
9.9 0.82 ug/L 11/20/15 15:44 11/27/15 20:16 1Phenol0.82 U
9.9 0.62 ug/L 11/20/15 15:44 11/27/15 20:16 1Pyrene0.62 U
9.9 1.2 ug/L 11/20/15 15:44 11/27/15 20:16 1Butyl benzyl phthalate 1.2 U
9.9 0.77 ug/L 11/20/15 15:44 11/27/15 20:16 1bis(chloroisopropyl) ether 0.77 U
50 5.0 ug/L 11/20/15 15:44 11/27/15 20:16 1Benzoic acid 5.0 U
9.9 1.1 ug/L 11/20/15 15:44 11/27/15 20:16 12,6-Dinitrotoluene 1.1 U
50 1.9 ug/L 11/20/15 15:44 11/27/15 20:16 14-Nitrophenol 1.9 U
2,4,6-Tribromophenol 75 39-124 11/20/15 15:44 11/27/15 20:16 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 63 11/20/15 15:44 11/27/15 20:16 132-113
2-Fluorophenol 59 11/20/15 15:44 11/27/15 20:16 126-109
Terphenyl-d14 74 11/20/15 15:44 11/27/15 20:16 110-126
Phenol-d5 61 11/20/15 15:44 11/27/15 20:16 127-110
Nitrobenzene-d5 70 11/20/15 15:44 11/27/15 20:16 132-118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography
RL MDL
Toxaphene 0.37 U 4.6 0.37 ug/L 11/20/15 15:44 11/23/15 16:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.046 0.0070 ug/L 11/20/15 15:44 11/23/15 16:14 1delta-BHC 0.0070 U
0.046 0.0035 ug/L 11/20/15 15:44 11/23/15 16:14 1Dieldrin0.0035 U
0.046 0.0032 ug/L 11/20/15 15:44 11/23/15 16:14 1Endosulfan I 0.0032 U
0.046 0.0039 ug/L 11/20/15 15:44 11/23/15 16:14 1Endosulfan II 0.0039 U
0.046 0.0047 ug/L 11/20/15 15:44 11/23/15 16:14 1Endosulfan sulfate 0.0047 U
0.046 0.0049 ug/L 11/20/15 15:44 11/23/15 16:14 1Endrin0.0049 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-16Client Sample ID: SLMW-6-11-15
Matrix: WaterDate Collected: 11/17/15 15:30
Date Received: 11/19/15 09:16
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued)
RL MDL
Endrin aldehyde 0.0057 U 0.046 0.0057 ug/L 11/20/15 15:44 11/23/15 16:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.046 0.0043 ug/L 11/20/15 15:44 11/23/15 16:14 1Endrin ketone 0.0043 U
0.046 0.0033 ug/L 11/20/15 15:44 11/23/15 16:14 1gamma-BHC (Lindane)0.0033 U
0.046 0.0066 ug/L 11/20/15 15:44 11/23/15 16:14 1Heptachlor0.0066 U J
0.046 0.0034 ug/L 11/20/15 15:44 11/23/15 16:14 1Heptachlor epoxide 0.0034 U
0.046 0.0091 ug/L 11/20/15 15:44 11/23/15 16:14 1Methoxychlor0.0091 U
0.93 0.17 ug/L 11/20/15 15:44 11/23/15 16:14 1PCB-1016 0.17 U
0.046 0.0058 ug/L 11/20/15 15:44 11/23/15 16:14 14,4'-DDD 0.0058 U
0.046 0.0047 ug/L 11/20/15 15:44 11/23/15 16:14 14,4'-DDE 0.0047 U J
0.046 0.0065 ug/L 11/20/15 15:44 11/23/15 16:14 14,4'-DDT 0.0065 U
0.046 0.0067 ug/L 11/20/15 15:44 11/23/15 16:14 1Aldrin0.0067 U J
0.046 0.0032 ug/L 11/20/15 15:44 11/23/15 16:14 1alpha-BHC 0.0032 U
0.046 0.0084 ug/L 11/20/15 15:44 11/23/15 16:14 1beta-BHC 0.0084 U
0.46 0.088 ug/L 11/20/15 15:44 11/23/15 16:14 1Chlordane (technical)0.088 U J
0.93 0.18 ug/L 11/20/15 15:44 11/23/15 16:14 1PCB-1221 0.18 U
0.93 0.23 ug/L 11/20/15 15:44 11/23/15 16:14 1PCB-1232 0.23 U
0.93 0.18 ug/L 11/20/15 15:44 11/23/15 16:14 1PCB-1242 0.18 U
0.93 0.19 ug/L 11/20/15 15:44 11/23/15 16:14 1PCB-1248 0.19 U
0.93 0.10 ug/L 11/20/15 15:44 11/23/15 16:14 1PCB-1254 0.10 U
0.93 0.11 ug/L 11/20/15 15:44 11/23/15 16:14 1PCB-1260 0.11 U
Tetrachloro-m-xylene 66 40-130 11/20/15 15:44 11/23/15 16:14 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 63 11/20/15 15:44 11/23/15 16:14 114-130
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique
RL MDL
Azinphos-methyl 0.11 U 0.94 0.11 ug/L 11/20/15 12:40 11/25/15 18:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.94 0.10 ug/L 11/20/15 12:40 11/25/15 18:44 1Bolstar0.10 U
0.94 0.096 ug/L 11/20/15 12:40 11/25/15 18:44 1Chlorpyrifos0.096 U
0.94 0.14 ug/L 11/20/15 12:40 11/25/15 18:44 1Coumaphos0.14 U
1.9 0.16 ug/L 11/20/15 12:40 11/25/15 18:44 1Demeton, Total 0.16 U
0.94 0.089 ug/L 11/20/15 12:40 11/25/15 18:44 1Diazinon0.089 U
0.94 0.080 ug/L 11/20/15 12:40 11/25/15 18:44 1Dichlorvos0.080 U
0.94 0.11 ug/L 11/20/15 12:40 11/25/15 18:44 1Dimethoate0.11 U
0.94 0.095 ug/L 11/20/15 12:40 11/25/15 18:44 1Disulfoton0.095 U
0.94 0.11 ug/L 11/20/15 12:40 11/25/15 18:44 1EPN0.11 U
0.94 0.095 ug/L 11/20/15 12:40 11/25/15 18:44 1Mocap0.095 U
0.94 0.12 ug/L 11/20/15 12:40 11/25/15 18:44 1Famphur0.12 U
0.94 0.16 ug/L 11/20/15 12:40 11/25/15 18:44 1Fensulfothion0.16 U
0.94 0.080 ug/L 11/20/15 12:40 11/25/15 18:44 1Fenthion0.080 U
0.94 0.10 ug/L 11/20/15 12:40 11/25/15 18:44 1Malathion0.10 U
0.94 0.15 ug/L 11/20/15 12:40 11/25/15 18:44 1Parathion0.15 U
0.94 0.10 ug/L 11/20/15 12:40 11/25/15 18:44 1Methyl parathion 0.10 U
0.94 0.092 ug/L 11/20/15 12:40 11/25/15 18:44 1Mevinphos0.092 U
0.94 0.087 ug/L 11/20/15 12:40 11/25/15 18:44 1Phorate0.087 U
0.94 0.097 ug/L 11/20/15 12:40 11/25/15 18:44 1Ronnel0.097 U
0.94 0.090 ug/L 11/20/15 12:40 11/25/15 18:44 1Stirophos0.090 U
0.94 0.089 ug/L 11/20/15 12:40 11/25/15 18:44 1Sulfotepp0.089 U
0.94 0.095 ug/L 11/20/15 12:40 11/25/15 18:44 1Thionazin0.095 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-16Client Sample ID: SLMW-6-11-15
Matrix: WaterDate Collected: 11/17/15 15:30
Date Received: 11/19/15 09:16
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique (Continued)
RL MDL
Tokuthion 0.088 U 0.94 0.088 ug/L 11/20/15 12:40 11/25/15 18:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.94 0.094 ug/L 11/20/15 12:40 11/25/15 18:44 1Trichloronate0.094 U
0.94 0.094 ug/L 11/20/15 12:40 11/25/15 18:44 1O,O,O-Triethyl phosphorothioate 0.094 U
Tributyl phosphate 103 49-122 11/20/15 12:40 11/25/15 18:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tributyl phosphate 106 11/20/15 12:40 11/25/15 18:44 149-122
Triphenylphosphate 106 11/20/15 12:40 11/25/15 18:44 145-145
Triphenylphosphate 111 11/20/15 12:40 11/25/15 18:44 145-145
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D 0.035 U 0.48 0.035 ug/L 11/23/15 07:48 11/27/15 17:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.48 0.14 ug/L 11/23/15 07:48 11/27/15 17:20 12,4-DB 0.14 U
0.24 0.059 ug/L 11/23/15 07:48 11/27/15 17:20 12,4,5-T 0.059 U
0.24 0.059 ug/L 11/23/15 07:48 11/27/15 17:20 1Silvex (2,4,5-TP)0.059 U
4.8 0.095 ug/L 11/23/15 07:48 11/27/15 17:20 1Dalapon0.095 U
0.48 0.081 ug/L 11/23/15 07:48 11/27/15 17:20 1Dicamba0.081 U
0.48 0.14 ug/L 11/23/15 07:48 11/27/15 17:20 1Dichlorprop0.14 U
0.95 0.15 ug/L 11/23/15 07:48 11/27/15 17:20 1Dinoseb0.15 U
110 16 ug/L 11/23/15 07:48 11/27/15 17:20 1MCPA16 U
110 18 ug/L 11/23/15 07:48 11/27/15 17:20 1Mecoprop18 U
0.24 0.035 ug/L 11/23/15 07:48 11/27/15 17:20 1Pentachlorophenol0.035 U
DCAA 106 M 45-130 11/23/15 07:48 11/27/15 17:20 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
General Chemistry
RL RL
Sulfide 26 10 10 mg/L 11/23/15 14:09 11/23/15 14:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Lab Sample ID: 680-119203-17Client Sample ID: SLMW-7R-11-15
Matrix: WaterDate Collected: 11/17/15 10:55
Date Received: 11/19/15 09:16
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,2,4-Trichlorobenzene 0.54 U 9.6 0.54 ug/L 11/20/15 15:44 11/30/15 19:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.6 0.51 ug/L 11/20/15 15:44 11/30/15 19:44 11,2-Dichlorobenzene 0.51 U
9.6 0.56 ug/L 11/20/15 15:44 11/30/15 19:44 11,3-Dichlorobenzene 0.56 U
9.6 0.52 ug/L 11/20/15 15:44 11/30/15 19:44 11,4-Dichlorobenzene 0.52 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 19:44 12,4,5-Trichlorophenol 1.1 U
9.6 0.81 ug/L 11/20/15 15:44 11/30/15 19:44 12,4,6-Trichlorophenol 0.81 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 19:44 12,4-Dichlorophenol 1.1 U
9.6 3.8 ug/L 11/20/15 15:44 11/30/15 19:44 12,4-Dimethylphenol 3.8 U
48 9.6 ug/L 11/20/15 15:44 11/30/15 19:44 12,4-Dinitrophenol 9.6 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 19:44 12,4-Dinitrotoluene 1.1 U
9.6 0.83 ug/L 11/20/15 15:44 11/30/15 19:44 12-Chlorophenol 0.83 U
9.6 0.76 ug/L 11/20/15 15:44 11/30/15 19:44 12-Chloronaphthalene 0.76 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 19:44 12-Methylnaphthalene 0.75 U
9.6 0.85 ug/L 11/20/15 15:44 11/30/15 19:44 12-Methylphenol 0.85 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-17Client Sample ID: SLMW-7R-11-15
Matrix: WaterDate Collected: 11/17/15 10:55
Date Received: 11/19/15 09:16
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitroaniline 1.2 U 48 1.2 ug/L 11/20/15 15:44 11/30/15 19:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.6 0.73 ug/L 11/20/15 15:44 11/30/15 19:44 12-Nitrophenol 0.73 U
9.6 1.2 ug/L 11/20/15 15:44 11/30/15 19:44 13 & 4 Methylphenol 1.2 U
57 29 ug/L 11/20/15 15:44 11/30/15 19:44 13,3'-Dichlorobenzidine 29 U
48 4.8 ug/L 11/20/15 15:44 11/30/15 19:44 13-Nitroaniline 4.8 U
48 9.6 ug/L 11/20/15 15:44 11/30/15 19:44 14,6-Dinitro-2-methylphenol 9.6 U
9.6 0.74 ug/L 11/20/15 15:44 11/30/15 19:44 14-Bromophenyl phenyl ether 0.74 U
9.6 0.96 ug/L 11/20/15 15:44 11/30/15 19:44 14-Chloro-3-methylphenol 0.96 U
19 2.1 ug/L 11/20/15 15:44 11/30/15 19:44 14-Chloroaniline 2.1 U
9.6 0.80 ug/L 11/20/15 15:44 11/30/15 19:44 14-Chlorophenyl phenyl ether 0.80 U
48 4.8 ug/L 11/20/15 15:44 11/30/15 19:44 14-Nitroaniline 4.8 U
9.6 0.73 ug/L 11/20/15 15:44 11/30/15 19:44 1Acenaphthene0.73 U
9.6 0.81 ug/L 11/20/15 15:44 11/30/15 19:44 1Acenaphthylene0.81 U
9.6 0.66 ug/L 11/20/15 15:44 11/30/15 19:44 1Anthracene0.66 U
9.6 0.53 ug/L 11/20/15 15:44 11/30/15 19:44 1Benzo[a]anthracene 0.53 U
9.6 0.68 ug/L 11/20/15 15:44 11/30/15 19:44 1Benzo[a]pyrene 0.68 U
9.6 2.5 ug/L 11/20/15 15:44 11/30/15 19:44 1Benzo[b]fluoranthene 2.5 U
9.6 0.83 ug/L 11/20/15 15:44 11/30/15 19:44 1Benzo[g,h,i]perylene 0.83 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 19:44 1Benzo[k]fluoranthene 1.1 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 19:44 1Benzyl alcohol 1.1 U
9.6 0.90 ug/L 11/20/15 15:44 11/30/15 19:44 1Bis(2-chloroethoxy)methane 0.90 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 19:44 1Bis(2-chloroethyl)ether 1.1 U
9.6 1.5 ug/L 11/20/15 15:44 11/30/15 19:44 1Bis(2-ethylhexyl) phthalate 1.5 U
9.6 0.49 ug/L 11/20/15 15:44 11/30/15 19:44 1Chrysene0.49 U
9.6 0.96 ug/L 11/20/15 15:44 11/30/15 19:44 1Dibenz(a,h)anthracene 0.96 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 19:44 1Dibenzofuran0.75 U
9.6 0.79 ug/L 11/20/15 15:44 11/30/15 19:44 1Di-n-butyl phthalate 0.79 U
9.6 0.84 ug/L 11/20/15 15:44 11/30/15 19:44 1Diethyl phthalate 0.84 U
9.6 0.95 ug/L 11/20/15 15:44 11/30/15 19:44 1Dimethyl phthalate 0.95 U
9.6 1.3 ug/L 11/20/15 15:44 11/30/15 19:44 1Di-n-octyl phthalate 1.3 U
9.6 0.71 ug/L 11/20/15 15:44 11/30/15 19:44 1Fluoranthene0.71 U
9.6 0.92 ug/L 11/20/15 15:44 11/30/15 19:44 1Fluorene0.92 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 19:44 1Hexachlorobenzene0.75 U
9.6 0.59 ug/L 11/20/15 15:44 11/30/15 19:44 1Hexachlorobutadiene0.59 U
9.6 0.73 ug/L 11/20/15 15:44 11/30/15 19:44 1Hexachloroethane0.73 U
9.6 0.96 ug/L 11/20/15 15:44 11/30/15 19:44 1Indeno[1,2,3-cd]pyrene 0.96 U
9.6 0.86 ug/L 11/20/15 15:44 11/30/15 19:44 1Isophorone0.86 U
9.6 0.67 ug/L 11/20/15 15:44 11/30/15 19:44 1Naphthalene0.67 U
9.6 0.70 ug/L 11/20/15 15:44 11/30/15 19:44 1Nitrobenzene0.70 U
9.6 0.88 ug/L 11/20/15 15:44 11/30/15 19:44 1N-Nitrosodiphenylamine 0.88 U Q
9.6 0.69 ug/L 11/20/15 15:44 11/30/15 19:44 1N-Nitrosodi-n-propylamine 0.69 U
48 1.9 ug/L 11/20/15 15:44 11/30/15 19:44 1Pentachlorophenol1.9 U
9.6 0.74 ug/L 11/20/15 15:44 11/30/15 19:44 1Phenanthrene0.74 U
9.6 0.79 ug/L 11/20/15 15:44 11/30/15 19:44 1Phenol0.79 U
9.6 0.60 ug/L 11/20/15 15:44 11/30/15 19:44 1Pyrene0.60 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 19:44 1Butyl benzyl phthalate 1.1 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 19:44 1bis(chloroisopropyl) ether 0.75 U
48 4.8 ug/L 11/20/15 15:44 11/30/15 19:44 1Benzoic acid 4.8 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 19:44 12,6-Dinitrotoluene 1.1 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-17Client Sample ID: SLMW-7R-11-15
Matrix: WaterDate Collected: 11/17/15 10:55
Date Received: 11/19/15 09:16
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
4-Nitrophenol 1.8 U 48 1.8 ug/L 11/20/15 15:44 11/30/15 19:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2,4,6-Tribromophenol 61 39-124 11/20/15 15:44 11/30/15 19:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 47 11/20/15 15:44 11/30/15 19:44 132-113
2-Fluorophenol 43 11/20/15 15:44 11/30/15 19:44 126-109
Terphenyl-d14 11 11/20/15 15:44 11/30/15 19:44 110-126
Phenol-d5 47 11/20/15 15:44 11/30/15 19:44 127-110
Nitrobenzene-d5 53 11/20/15 15:44 11/30/15 19:44 132-118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography
RL MDL
Toxaphene 0.38 U 4.8 0.38 ug/L 11/20/15 15:44 11/23/15 16:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.048 0.0072 ug/L 11/20/15 15:44 11/23/15 16:28 1delta-BHC 0.0072 U
0.048 0.0036 ug/L 11/20/15 15:44 11/23/15 16:28 1Dieldrin0.0036 U
0.048 0.0034 ug/L 11/20/15 15:44 11/23/15 16:28 1Endosulfan I 0.0034 U
0.048 0.0040 ug/L 11/20/15 15:44 11/23/15 16:28 1Endosulfan II 0.0040 U
0.048 0.0049 ug/L 11/20/15 15:44 11/23/15 16:28 1Endosulfan sulfate 0.0049 U
0.048 0.0051 ug/L 11/20/15 15:44 11/23/15 16:28 1Endrin0.0051 U
0.048 0.0058 ug/L 11/20/15 15:44 11/23/15 16:28 1Endrin aldehyde 0.0058 U
0.048 0.0044 ug/L 11/20/15 15:44 11/23/15 16:28 1Endrin ketone 0.0044 U
0.048 0.0034 ug/L 11/20/15 15:44 11/23/15 16:28 1gamma-BHC (Lindane)0.0034 U
0.048 0.0068 ug/L 11/20/15 15:44 11/23/15 16:28 1Heptachlor0.0068 U
0.048 0.0035 ug/L 11/20/15 15:44 11/23/15 16:28 1Heptachlor epoxide 0.0035 U
0.048 0.0094 ug/L 11/20/15 15:44 11/23/15 16:28 1Methoxychlor0.0094 U
0.96 0.17 ug/L 11/20/15 15:44 11/23/15 16:28 1PCB-1016 0.17 U
0.048 0.0060 ug/L 11/20/15 15:44 11/23/15 16:28 14,4'-DDD 0.0060 U
0.048 0.0049 ug/L 11/20/15 15:44 11/23/15 16:28 14,4'-DDE 0.0049 U
0.048 0.0067 ug/L 11/20/15 15:44 11/23/15 16:28 14,4'-DDT 0.0067 U
0.048 0.0069 ug/L 11/20/15 15:44 11/23/15 16:28 1Aldrin0.0069 U
0.048 0.0033 ug/L 11/20/15 15:44 11/23/15 16:28 1alpha-BHC 0.0033 U
0.048 0.0087 ug/L 11/20/15 15:44 11/23/15 16:28 1beta-BHC 0.0087 U
0.48 0.091 ug/L 11/20/15 15:44 11/23/15 16:28 1Chlordane (technical)0.091 U
0.96 0.18 ug/L 11/20/15 15:44 11/23/15 16:28 1PCB-1221 0.18 U
0.96 0.24 ug/L 11/20/15 15:44 11/23/15 16:28 1PCB-1232 0.24 U
0.96 0.18 ug/L 11/20/15 15:44 11/23/15 16:28 1PCB-1242 0.18 U
0.96 0.20 ug/L 11/20/15 15:44 11/23/15 16:28 1PCB-1248 0.20 U
0.96 0.11 ug/L 11/20/15 15:44 11/23/15 16:28 1PCB-1254 0.11 U
0.96 0.11 ug/L 11/20/15 15:44 11/23/15 16:28 1PCB-1260 0.11 U
Tetrachloro-m-xylene 29 J 40-130 11/20/15 15:44 11/23/15 16:28 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 11 J M 11/20/15 15:44 11/23/15 16:28 114-130
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique
RL MDL
Azinphos-methyl 0.11 U 0.94 0.11 ug/L 11/20/15 12:40 11/25/15 21:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.94 0.10 ug/L 11/20/15 12:40 11/25/15 21:31 1Bolstar0.10 U
0.94 0.096 ug/L 11/20/15 12:40 11/25/15 21:31 1Chlorpyrifos0.096 U
0.94 0.14 ug/L 11/20/15 12:40 11/25/15 21:31 1Coumaphos0.14 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-17Client Sample ID: SLMW-7R-11-15
Matrix: WaterDate Collected: 11/17/15 10:55
Date Received: 11/19/15 09:16
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique (Continued)
RL MDL
Demeton, Total 0.16 U 1.9 0.16 ug/L 11/20/15 12:40 11/25/15 21:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.94 0.089 ug/L 11/20/15 12:40 11/25/15 21:31 1Diazinon0.089 U
0.94 0.080 ug/L 11/20/15 12:40 11/25/15 21:31 1Dichlorvos0.080 U
0.94 0.11 ug/L 11/20/15 12:40 11/25/15 21:31 1Dimethoate0.15 J
0.94 0.095 ug/L 11/20/15 12:40 11/25/15 21:31 1Disulfoton0.095 U
0.94 0.11 ug/L 11/20/15 12:40 11/25/15 21:31 1EPN0.11 U
0.94 0.095 ug/L 11/20/15 12:40 11/25/15 21:31 1Mocap0.095 U
0.94 0.12 ug/L 11/20/15 12:40 11/25/15 21:31 1Famphur0.12 U
0.94 0.16 ug/L 11/20/15 12:40 11/25/15 21:31 1Fensulfothion0.17 J
0.94 0.080 ug/L 11/20/15 12:40 11/25/15 21:31 1Fenthion0.080 U
0.94 0.10 ug/L 11/20/15 12:40 11/25/15 21:31 1Malathion0.10 U
0.94 0.15 ug/L 11/20/15 12:40 11/25/15 21:31 1Parathion0.15 U
0.94 0.10 ug/L 11/20/15 12:40 11/25/15 21:31 1Methyl parathion 0.10 U
0.94 0.092 ug/L 11/20/15 12:40 11/25/15 21:31 1Mevinphos0.092 U
0.94 0.087 ug/L 11/20/15 12:40 11/25/15 21:31 1Phorate0.087 U
0.94 0.097 ug/L 11/20/15 12:40 11/25/15 21:31 1Ronnel0.097 U
0.94 0.090 ug/L 11/20/15 12:40 11/25/15 21:31 1Stirophos0.090 U
0.94 0.089 ug/L 11/20/15 12:40 11/25/15 21:31 1Sulfotepp0.089 U
0.94 0.095 ug/L 11/20/15 12:40 11/25/15 21:31 1Thionazin0.095 U
0.94 0.088 ug/L 11/20/15 12:40 11/25/15 21:31 1Tokuthion0.088 U
0.94 0.094 ug/L 11/20/15 12:40 11/25/15 21:31 1Trichloronate0.094 U
0.94 0.094 ug/L 11/20/15 12:40 11/25/15 21:31 1O,O,O-Triethyl phosphorothioate 0.094 U
Tributyl phosphate 102 49-122 11/20/15 12:40 11/25/15 21:31 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tributyl phosphate 102 11/20/15 12:40 11/25/15 21:31 149-122
Triphenylphosphate 105 11/20/15 12:40 11/25/15 21:31 145-145
Triphenylphosphate 110 11/20/15 12:40 11/25/15 21:31 145-145
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D 0.035 U 0.48 0.035 ug/L 11/23/15 07:48 11/27/15 23:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.48 0.14 ug/L 11/23/15 07:48 11/27/15 23:10 12,4-DB 0.14 U
0.24 0.059 ug/L 11/23/15 07:48 11/27/15 23:10 12,4,5-T 0.059 U
0.24 0.059 ug/L 11/23/15 07:48 11/27/15 23:10 1Silvex (2,4,5-TP)0.059 U
4.8 0.096 ug/L 11/23/15 07:48 11/27/15 23:10 1Dalapon0.096 U
0.48 0.081 ug/L 11/23/15 07:48 11/27/15 23:10 1Dicamba0.081 U
0.48 0.14 ug/L 11/23/15 07:48 11/27/15 23:10 1Dichlorprop0.14 U
0.96 0.15 ug/L 11/23/15 07:48 11/27/15 23:10 1Dinoseb0.15 U
110 16 ug/L 11/23/15 07:48 11/27/15 23:10 1MCPA16 U
110 18 ug/L 11/23/15 07:48 11/27/15 23:10 1Mecoprop18 U
0.24 0.035 ug/L 11/23/15 07:48 11/27/15 23:10 1Pentachlorophenol0.035 U
DCAA 97 45-130 11/23/15 07:48 11/27/15 23:10 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-18Client Sample ID: SLMW-9R-11-15
Matrix: WaterDate Collected: 11/17/15 13:30
Date Received: 11/19/15 09:16
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,2,4-Trichlorobenzene 0.54 U 9.6 0.54 ug/L 11/20/15 15:44 11/30/15 20:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.6 0.51 ug/L 11/20/15 15:44 11/30/15 20:08 11,2-Dichlorobenzene 0.51 U
9.6 0.56 ug/L 11/20/15 15:44 11/30/15 20:08 11,3-Dichlorobenzene 0.56 U
9.6 0.52 ug/L 11/20/15 15:44 11/30/15 20:08 11,4-Dichlorobenzene 1.6 J
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 20:08 12,4,5-Trichlorophenol 1.1 U
9.6 0.81 ug/L 11/20/15 15:44 11/30/15 20:08 12,4,6-Trichlorophenol 0.81 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 20:08 12,4-Dichlorophenol 1.1 U
9.6 3.8 ug/L 11/20/15 15:44 11/30/15 20:08 12,4-Dimethylphenol 3.8 U
48 9.6 ug/L 11/20/15 15:44 11/30/15 20:08 12,4-Dinitrophenol 9.6 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 20:08 12,4-Dinitrotoluene 1.1 U
9.6 0.83 ug/L 11/20/15 15:44 11/30/15 20:08 12-Chlorophenol 0.83 U
9.6 0.76 ug/L 11/20/15 15:44 11/30/15 20:08 12-Chloronaphthalene 0.76 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 20:08 12-Methylnaphthalene 0.75 U
9.6 0.85 ug/L 11/20/15 15:44 11/30/15 20:08 12-Methylphenol 0.85 U
48 1.2 ug/L 11/20/15 15:44 11/30/15 20:08 12-Nitroaniline 1.2 U
9.6 0.73 ug/L 11/20/15 15:44 11/30/15 20:08 12-Nitrophenol 0.73 U
9.6 1.2 ug/L 11/20/15 15:44 11/30/15 20:08 13 & 4 Methylphenol 1.2 U
57 29 ug/L 11/20/15 15:44 11/30/15 20:08 13,3'-Dichlorobenzidine 29 U
48 4.8 ug/L 11/20/15 15:44 11/30/15 20:08 13-Nitroaniline 4.8 U
48 9.6 ug/L 11/20/15 15:44 11/30/15 20:08 14,6-Dinitro-2-methylphenol 9.6 U
9.6 0.74 ug/L 11/20/15 15:44 11/30/15 20:08 14-Bromophenyl phenyl ether 0.74 U
9.6 0.96 ug/L 11/20/15 15:44 11/30/15 20:08 14-Chloro-3-methylphenol 0.96 U
19 2.1 ug/L 11/20/15 15:44 11/30/15 20:08 14-Chloroaniline 2.1 U
9.6 0.80 ug/L 11/20/15 15:44 11/30/15 20:08 14-Chlorophenyl phenyl ether 0.80 U
48 4.8 ug/L 11/20/15 15:44 11/30/15 20:08 14-Nitroaniline 4.8 U
9.6 0.73 ug/L 11/20/15 15:44 11/30/15 20:08 1Acenaphthene0.73 U
9.6 0.81 ug/L 11/20/15 15:44 11/30/15 20:08 1Acenaphthylene0.81 U
9.6 0.66 ug/L 11/20/15 15:44 11/30/15 20:08 1Anthracene0.66 U
9.6 0.53 ug/L 11/20/15 15:44 11/30/15 20:08 1Benzo[a]anthracene 0.53 U
9.6 0.68 ug/L 11/20/15 15:44 11/30/15 20:08 1Benzo[a]pyrene 0.68 U
9.6 2.5 ug/L 11/20/15 15:44 11/30/15 20:08 1Benzo[b]fluoranthene 2.5 U
9.6 0.83 ug/L 11/20/15 15:44 11/30/15 20:08 1Benzo[g,h,i]perylene 0.83 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 20:08 1Benzo[k]fluoranthene 1.1 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 20:08 1Benzyl alcohol 1.1 U
9.6 0.90 ug/L 11/20/15 15:44 11/30/15 20:08 1Bis(2-chloroethoxy)methane 0.90 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 20:08 1Bis(2-chloroethyl)ether 1.1 U
9.6 1.5 ug/L 11/20/15 15:44 11/30/15 20:08 1Bis(2-ethylhexyl) phthalate 1.5 U
9.6 0.49 ug/L 11/20/15 15:44 11/30/15 20:08 1Chrysene0.49 U
9.6 0.96 ug/L 11/20/15 15:44 11/30/15 20:08 1Dibenz(a,h)anthracene 0.96 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 20:08 1Dibenzofuran0.75 U
9.6 0.79 ug/L 11/20/15 15:44 11/30/15 20:08 1Di-n-butyl phthalate 0.79 U
9.6 0.84 ug/L 11/20/15 15:44 11/30/15 20:08 1Diethyl phthalate 1.1 J
9.6 0.95 ug/L 11/20/15 15:44 11/30/15 20:08 1Dimethyl phthalate 0.95 U
9.6 1.3 ug/L 11/20/15 15:44 11/30/15 20:08 1Di-n-octyl phthalate 1.3 U
9.6 0.71 ug/L 11/20/15 15:44 11/30/15 20:08 1Fluoranthene0.71 U
9.6 0.92 ug/L 11/20/15 15:44 11/30/15 20:08 1Fluorene0.92 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 20:08 1Hexachlorobenzene0.75 U
9.6 0.59 ug/L 11/20/15 15:44 11/30/15 20:08 1Hexachlorobutadiene0.59 U
9.6 0.73 ug/L 11/20/15 15:44 11/30/15 20:08 1Hexachloroethane0.73 U
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Client Sample Results
TestAmerica Job ID: 680-119203-3Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-119203-18Client Sample ID: SLMW-9R-11-15
Matrix: WaterDate Collected: 11/17/15 13:30
Date Received: 11/19/15 09:16
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Indeno[1,2,3-cd]pyrene 0.96 U 9.6 0.96 ug/L 11/20/15 15:44 11/30/15 20:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.6 0.86 ug/L 11/20/15 15:44 11/30/15 20:08 1Isophorone0.86 U
9.6 0.67 ug/L 11/20/15 15:44 11/30/15 20:08 1Naphthalene0.67 U
9.6 0.70 ug/L 11/20/15 15:44 11/30/15 20:08 1Nitrobenzene0.70 U
9.6 0.88 ug/L 11/20/15 15:44 11/30/15 20:08 1N-Nitrosodiphenylamine 0.88 U Q
9.6 0.69 ug/L 11/20/15 15:44 11/30/15 20:08 1N-Nitrosodi-n-propylamine 0.69 U
48 1.9 ug/L 11/20/15 15:44 11/30/15 20:08 1Pentachlorophenol1.9 U
9.6 0.74 ug/L 11/20/15 15:44 11/30/15 20:08 1Phenanthrene0.74 U
9.6 0.79 ug/L 11/20/15 15:44 11/30/15 20:08 1Phenol0.79 U
9.6 0.60 ug/L 11/20/15 15:44 11/30/15 20:08 1Pyrene0.60 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 20:08 1Butyl benzyl phthalate 1.1 U
9.6 0.75 ug/L 11/20/15 15:44 11/30/15 20:08 1bis(chloroisopropyl) ether 0.75 U
48 4.8 ug/L 11/20/15 15:44 11/30/15 20:08 1Benzoic acid 4.8 U
9.6 1.1 ug/L 11/20/15 15:44 11/30/15 20:08 12,6-Dinitrotoluene 1.1 U
48 1.8 ug/L 11/20/15 15:44 11/30/15 20:08 14-Nitrophenol 1.8 U
2,4,6-Tribromophenol 91 39-124 11/20/15 15:44 11/30/15 20:08 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 67 11/20/15 15:44 11/30/15 20:08 132-113
2-Fluorophenol 47 11/20/15 15:44 11/30/15 20:08 126-109
Terphenyl-d14 55 11/20/15 15:44 11/30/15 20:08 110-126
Phenol-d5 51 11/20/15 15:44 11/30/15 20:08 127-110
Nitrobenzene-d5 62 11/20/15 15:44 11/30/15 20:08 132-118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography
RL MDL
Toxaphene 0.38 U 4.8 0.38 ug/L 11/20/15 15:44 11/23/15 16:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.048 0.0072 ug/L 11/20/15 15:44 11/23/15 16:43 1delta-BHC 0.0072 U
0.048 0.0036 ug/L 11/20/15 15:44 11/23/15 16:43 1Dieldrin0.0036 U
0.048 0.0033 ug/L 11/20/15 15:44 11/23/15 16:43 1Endosulfan I 0.0033 U
0.048 0.0040 ug/L 11/20/15 15:44 11/23/15 16:43 1Endosulfan II 0.0040 U
0.048 0.0049 ug/L 11/20/15 15:44 11/23/15 16:43 1Endosulfan sulfate 0.0049 U
0.048 0.0051 ug/L 11/20/15 15:44 11/23/15 16:43 1Endrin0.0051 U
0.048 0.0058 ug/L 11/20/15 15:44 11/23/15 16:43 1Endrin aldehyde 0.0058 U
0.048 0.0044 ug/L 11/20/15 15:44 11/23/15 16:43 1Endrin ketone 0.0044 U
0.048 0.0034 ug/L 11/20/15 15:44 11/23/15 16:43 1gamma-BHC (Lindane)0.0034 U
0.048 0.0068 ug/L 11/20/15 15:44 11/23/15 16:43 1Heptachlor0.0068 U
0.048 0.0035 ug/L 11/20/15 15:44 11/23/15 16:43 1Heptachlor epoxide 0.0035 U
0.048 0.0094 ug/L 11/20/15 15:44 11/23/15 16:43 1Methoxychlor0.0094 U
0.95 0.17 ug/L 11/20/15 15:44 11/23/15 16:43 1PCB-1016 0.17 U
0.048 0.0060 ug/L 11/20/15 15:44 11/23/15 16:43 14,4'-DDD 0.0060 U
0.048 0.0049 ug/L 11/20/15 15:44 11/23/15 16:43 14,4'-DDE 0.0049 U
0.048 0.0067 ug/L 11/20/15 15:44 11/23/15 16:43 14,4'-DDT 0.0067 U
0.048 0.0069 ug/L 11/20/15 15:44 11/23/15 16:43 1Aldrin0.0069 U
0.048 0.0032 ug/L 11/20/15 15:44 11/23/15 16:43 1alpha-BHC 0.0032 U
0.048 0.0087 ug/L 11/20/15 15:44 11/23/15 16:43 1beta-BHC 0.0087 U
0.48 0.091 ug/L 11/20/15 15:44 11/23/15 16:43 1Chlordane (technical)0.091 U
0.95 0.18 ug/L 11/20/15 15:44 11/23/15 16:43 1PCB-1221 0.18 U
0.95 0.24 ug/L 11/20/15 15:44 11/23/15 16:43 1PCB-1232 0.24 U
0.95 0.18 ug/L 11/20/15 15:44 11/23/15 16:43 1PCB-1242 0.18 U
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