SW_F_7502-CDLF-2002_07-01-2015_RM_GW.pdf

Prepared for
Polk County, North Carolina
Project Number 2036.13

Prepared by
Altamont Environmental, Inc.
231 Haywood Street
Asheville, NC 28801
828.281.3350

Spring 2015 Semiannual
Water Quality Monitoring Report
Polk County
Construction and Demolition Debris Landfill
and Municipal Solid Waste Landfill
Permit 75-02
Route 9, Polk County, North Carolina

July 1, 2015

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Table of Contents
1.0 Introduction .................................................................................................................... 1
2.0 C&D Landfill.................................................................................................................... 2
2.1 Sampling and Analysis Methods....................................................................................2
2.2 Analytical Results ..........................................................................................................3
2.2.1 Groundwater Samples ......................................................................................4
2.2.2 Surface Water Samples ....................................................................................4
3.0 MSW Landfill .................................................................................................................. 5
3.1 Sampling and Analysis Methods....................................................................................5
3.2 Analytical Results ..........................................................................................................5
3.2.1 Groundwater Samples ......................................................................................5
4.0 Background Monitoring Well .......................................................................................... 6
4.1 Statistical Analysis Methodology ...................................................................................6
4.2 Results of Statistical Analysis ........................................................................................6
5.0 Summary ........................................................................................................................ 7
5.1 Future Activities .............................................................................................................7

Figures
1. Site Location Map
2. Site Layout Map
3. Groundwater Elevation Map
Tables
1. Summary of Groundwater Elevation Data—March 2015
2. Summary of Laboratory Analyses Performed on Samples
3. Summary of Detected Constituents
4. Solid Waste Section Limits Exceedances Notification
5. Water Quality Standards Exceedances Notification
6. VOCs Background Well Comparison
7. Metals Background Well Comparison

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Appendices
A. Sampling Logs and Equipment Documentation and Instrument Calibration Data Sheets
B. Report of Laboratory Analysis and Chain-of-Custody Documentation
C. Environmental Monitoring Reporting Form and Electronic Submittal of Environmental Monitoring
Data 7502Mar2015 (Electronic Format Only)
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1.0 Introduction
The Polk County Solid Waste Department (County) maintains two landfills at the Polk County Route 9 Landfill
Facility (site), located on the west side of North Carolina Route 9, approximately 1.5 miles northwest of the
community of Mill Spring (Figure 1).
The northernmost landfill area is an inactive permitted Construction and Demolition Debris (C&D) Landfill
(Figure 2). The 3.5-acre C&D Landfill (formerly known as the “Operating Landfill”) was capped during the
summer of 2006, and a Closure Plan was submitted to Mr. James Coffey at the North Carolina Department
of Environment and Natural Resources (DENR) on August 21, 2006.
The second landfill is a Municipal Solid Waste (MSW) Landfill composed of two discrete areas in the west-
central and southern parts of the site (Figure 2). The MSW Landfill (formerly known as the “Closed Landfill”)
is inactive, closed, and maintained by the County. It was officially closed on April 9, 1994.
Both landfills are regulated by the DENR, Division of Waste Management (DWM), under Permit No.75-02
(Polk County C&D Landfill and MSW Landfill) as well as DENR Solid Waste Management Rules Title 15A,
North Carolina Administrative Code (NCAC) Subchapter 13B, Section .0500 Rule (C&D Landfill) and Title 15A
NCAC 13B.1600 Rule (MSW Landfill). The permit requires semiannual monitoring of groundwater and
surface water quality. This report is being submitted in accordance with the monitoring and reporting
requirements stated in the permit as well as the rules, and it provides an evaluation of surface water and
groundwater quality for the C&D Landfill and an evaluation of the groundwater quality for the closed MSW
Landfill.
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2.0 C&D Landfill
2.1 Sampling and Analysis Methods
Three monitoring wells (MW-01CD, MW-02CD, and MW-03CD) and three surface water locations (SS-1, SS-2,
and SP-1) are monitored in association with the C&D Landfill. All monitoring points were sampled by
Altamont Environmental, Inc. (Altamont) on March 18 and 19, 2015. The approximate locations of the
groundwater monitoring wells and surface water sampling points are shown on Figure 2. Field sampling logs
are included in Appendix A.
Monitoring wells MW-01CD, MW-02CD, and MW-03CD sampled during the spring 2015 sampling event are
constructed of 2-inch-diameter Schedule 40 polyvinyl chloride (PVC) well material. Well construction logs for
these wells are not available. Prior to sampling, water level measurements were obtained. Table 1 and
Figure 3 present the groundwater elevation data relative to an assumed benchmark elevation.
Monitoring wells MW-01CD and MW-03CD were purged and sampled using low-flow techniques in
accordance with the procedures described in “Low-Flow (Minimal Drawdown) Ground-Water Sampling
Procedures”, U.S. Environmental Protection Agency (EPA), Groundwater Issues (April 1996). During purging,
the pH, specific conductivity, dissolved oxygen (DO), oxidation-reduction potential (ORP), turbidity, and
temperature were measured and recorded approximately every 3 minutes. Well purging continued until
these parameters stabilized, as determined by three successive readings in which each parameter was
within a range of values, as follows:
 pH +/- 0.1 unit
 Specific conductivity +/- 3 percent
 Temperature +/- 10 percent
 DO +/- 10 percent
 Turbidity +/- 10 percent
 ORP +/- 10 millivolts
Once all these parameters stabilized, a groundwater sample was collected in laboratory-supplied sample
containers by a technician wearing a new pair of nitrile gloves.
Since MW-02CD was last sampled in September 2012, the water level has been insufficient to allow purging
and sampling of the well. However, on March 18, 2015, Altamont technicians measured a sufficient volume
of water in MW-02CD to allow the monitoring well to be purged with a disposable bailer. Monitoring well MW-
02CD was purged dry after removing approximately 2 gallons of water and allowed to recharge overnight.
Technicians returned to MW-02CD on March 19, 2015 to collect a sample in laboratory-supplied sample
containers, wearing a new pair of nitrile gloves.
The surface water sample collected at the SS-1 location is representative of surface water quality upstream
of the landfill. The surface water sample collected at the SS-2 location is representative of surface water
quality downstream of the landfill. The surface water sample collected from the SP-1 location is
representative of surface water quality at a nearby spring that is situated at an elevation lower than the
landfill in an apparent downgradient direction (Figure 2). At each of these surface water sampling locations,
pH, specific conductivity, DO, ORP, turbidity, and temperature were measured and a grab sample was
collected by a technician wearing a new pair of nitrile gloves.
Collected groundwater and surface water samples were immediately placed on ice in sample coolers for
transport to the laboratory. Proper chain-of-custody documentation was maintained during the collection and
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transport of each sample. A trip blank was also transported in the sample cooler and analyzed for Appendix I
volatile organic compounds (VOCs).
The groundwater and surface water samples were analyzed by TestAmerica Laboratories, Inc. (TestAmerica),
a laboratory certified in North Carolina, for Appendix I VOCs by EPA Method 8260 and for Appendix I metals
by EPA Methods 6010, 6020, and 7470 (Table 2). The report of laboratory analysis and chain-of-custody
forms are included in Appendix B. Additional observations and descriptions pertaining to individual wells are
provided on the sampling logs that are included in Appendix A. Additionally, water level measurements and
field parameters are summarized in the Electronic Data Deliverable (EDD) format included in Appendix C.
2.2 Analytical Results
The laboratory analytical results for groundwater, surface water, and trip blank samples collected at the C&D
Landfill are provided in the report of laboratory analysis issued by TestAmerica and included in Appendix B.
In addition, all the laboratory analytical results are summarized in the EDD format specified by the Solid
Waste Section (SWS) on May 5, 2010.
As stipulated in the DWM document referenced above, all laboratory analytical results were reported and
appropriately qualified. Non-detections (non-detects), which are values reported by the laboratory as below
method detection limits (MDLs), are tabulated in Table 3 and the EDD at MDL levels, and are qualified with
the “U” qualifier. The MDL is the minimum concentration of a substance that can be measured and reported
by a laboratory with 99 percent confidence that the analyte concentration is greater than zero. All detections
(values above the MDL) were compared to analyte-specific Solid Waste Section Limits (SWSLs) established
by the SWS. The SWSL is the lowest concentration of an analyte in a sample that can be quantitatively
determined with suitable precision and accuracy. If the reported concentration is above the laboratory MDL
and below the method reporting limit (MRL), the analytical result is qualified by the laboratory as estimated,
and is flagged with a “J” qualifier (J-flag). The MRL is the minimum concentration of a target analyte that can
be accurately determined by the referenced method. If the reported concentration is above the laboratory
MRL and below the SWSL, the analytical result is qualified as estimated, and is flagged with an italicized “J”
qualifier (italicized J-flag) by Altamont per DENR requirements. The MRL is listed in the “Report Limit” (RL)
column in the report of laboratory analysis (Appendix B). Concentrations below the respective SWSLs are not
discussed in the text of this report unless they exceed their contaminant-specific water quality standards.
Detected concentrations of analytes in groundwater samples were compared to current groundwater quality
standards specified in 15A NCAC 2L.0202, which are referred to as “2L standards”. Detected concentrations
of analytes in groundwater with no established 2L standards were compared either to the interim maximum
allowable concentrations (IMACs) for Class GA and GSA groundwater (in accordance with 15A NCAC 02L
.0202 [c]) or Groundwater Protection (GWP) Standards, pursuant to 15A NCAC 13B.1634. Detections of
analytes in surface-water samples were compared to 15A NCAC 2B surface-water quality standards (2B
standards).
Table 3 presents the summary of laboratory analytical results for detected constituents only. Table 4
presents all analytical results that were above the applicable SWSLs. Table 5 presents only the
concentrations of analytes detected in groundwater and/or surface-water samples that exceeded their
respective 2L standards (including IMACs, if applicable), GWP Standards, or 2B standards.
In the EDD (Appendix C), the identification of a well (“WELL ID” on the table) consists of the name of the well
prefaced by the un-hyphenated permit number for the facility. For example, the groundwater sample from
monitoring well MW-01CD is identified on the tables as 7502-MW01CD. However, in the tables and figures
of this report, the identification of a well consists of the name of the well without the permit number
associated with the facility.

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2.2.1 Groundwater Samples
Eight metals (barium, beryllium, chromium, copper, lead, thallium, vanadium, and zinc) were detected in one
or more of the groundwater samples collected from the monitoring wells at the C&D landfill. Two of the
detected metals (barium and zinc) were detected at concentrations above their respective SWSLs in one or
more groundwater samples collected from the monitoring wells (Table 4). In addition, thallium and vanadium
exceeded their respective IMAC in one or more groundwater samples collected at the C&D landfill (Table 5).
Four VOCs were detected in one or more of the groundwater samples collected at the C&D landfill (1,2-
dichlorobenzene, 1,4-dichlorobenzene, tetrahydrofuran, and trichlorofluoromethane). No VOCs were
detected at concentrations above their respective SWSLs (Table 3) or water quality standards.
Groundwater pH readings were obtained from all monitoring wells sampled. The measured groundwater pH
value in MW-01CD and MW-03CD were outside the 2L standard pH range of 6.5 to 8.5 Standard Units (SU)
(Tables 3 and 5).
Turbidity values at the time of sampling monitoring wells MW-01CD, MW-02CD, and MW-03CD ranged from
29.06 nephelometric turbidity units (NTUs) to 177.1 NTUs (Table 3).
2.2.2 Surface Water Samples
Two metals (barium and lead) were detected in one or more surface water samples collected at designated
sampling locations (Table 3). Barium was detected at sample location SP-1 above its respective SWSL, but
below the 2B surface water standard.
No VOCs were detected in any of the collected surface water samples (Table 3).
The pH readings obtained from all sampled locations were within the 2B standard range of 6.00 to 9.00 SU
(Table 3).
Turbidity values measured in the surface water samples ranged from 21.14 NTUs (SS-2) to 75.01 NTUs (SP-
1) (Table 3). Turbidity measure at SP-1 exceeded the 2B turbidity standard of 25 NTUs.

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3.0 MSW Landfill
3.1 Sampling and Analysis Methods
Three monitoring wells, MW-1R, MW-2R, and MW-3R, are monitored in association with the MSW Landfill.
During the spring 2015 sampling event, all monitoring points were sampled by Altamont on March 18 and
19, 2015. The approximate locations of the groundwater monitoring wells are shown on Figure 2. Field
sampling logs are included in Appendix A.
The wells MW-1R and MW-2R are constructed of 2-inch-diameter Schedule 40 PVC well material. Well
construction logs for these wells are not available. The well construction record for the newly installed
monitoring well MW-3R is available and was included in Appendix D of the Fall 2012 Semiannual Water
Quality Monitoring Report.
Prior to sampling the wells, field parameters and water level measurements were obtained. Table 1 and
Figure 3 present the groundwater elevation data relative to an assumed benchmark elevation. Field
parameters are presented in the sampling logs (Appendix A) and in the EDD (Appendix C).
Groundwater samples from monitoring wells MW-1R and MW-2R were collected using the same low-flow
protocol described in Section 2.1. Monitoring well MW-3R was pumped dry using a Grundfos Redi Flow 2
pump on March 17, 2015 and the groundwater sample was collected following recharge the next day, March
18, 2015. A duplicate sample was taken at MW-2R to ensure consistency with laboratory practices, and is
listed as MW-2RDUP.
Proper chain-of-custody documentation procedures were followed during collection and transport of the
samples. Analysis of the groundwater samples was performed by TestAmerica using the same methods
described in Section 2.1 (Table 2). Additional observations and descriptions pertaining to individual wells are
provided on the sampling logs included in Appendix A.
3.2 Analytical Results
3.2.1 Groundwater Samples
Nine metals (barium, beryllium, cadmium, chromium, copper, lead, thallium, vanadium, and zinc) were
detected in one or more of the groundwater samples collected from the monitoring wells. Of the detected
metals, four (barium, cadmium, copper, and zinc) were present at concentrations above their respective
SWSLs in one or more groundwater samples collected from the monitoring wells (Table 4). In addition, two
metals (thallium and vanadium) exceeded their respective IMAC concentrations in monitoring well MW-1R.
Four VOCs were detected in the groundwater sample and the duplicate sample collected from MW-2R (Table
3). Cis-1,2-dichloroethene and trichloroethene were detected above the SWSL, but below the 2L
groundwater standards (Table 4) in the sample collected from MW-2R. None of the VOCs were present at
concentrations above established 2L groundwater quality standards.
The measured pH was below the acceptable range established as the 2L standard in MW-1R and MW-2R.
Refer to Tables 3 and 5 for sample results.
Turbidity values at the time of sampling monitoring wells MW-1R, MW-2R, and MW-3R ranged from 1.50
NTUs to 24.32 NTUs (Table 3).

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4.0 Background Monitoring Well
4.1 Statistical Analysis Methodology
In 2012, background monitoring well, MW-3R, was installed upgradient of the other two MSW monitoring
wells and three C&D monitoring wells. MW-3R was installed to establish background concentrations of
Appendix I VOCs and metals upgradient of the MSW Landfill and C&D Landfill. MW-3R, consistent with the
other five monitoring wells, is sampled on a semiannual basis. MW-3R has been sampled six times from
October 2012 to March 2015.
A brief statistical analysis presented herein compares background concentrations in MW-3R to downgradient
monitoring wells, and applicable groundwater standards. Historical data was summarized for MW-01CD,
MW-02CD, MW03CD, MW-1R, and MW-2R from the six sampling events occurring from September 2012 to
March 2015. Data from MW-3R was summarized from the six sampling events occurring from October 2012
to March 2015. Tables 6 and 7 list the constituents detected in each well for the subject monitoring period,
minimum concentration, maximum concentration, and average concentration of each detected constituent,
as well as the frequency of detection in each well. Results below the MDL were assumed to equal half of the
MDL.
4.2 Results of Statistical Analysis
A comparison of VOCs is presented in Table 6. No VOCs were detected in the background well (MW-3R)
during the subject statistical analysis period. Eleven VOCs (1,1-dichloroethane, 1,2-dichlorobenzene, 1,4-
dichlorobenzene, cis-1,2-dichloroethene, acetone, tetrachloroethene, tetrahydrofuran, trichloroethene,
trichlorofluoromethane, vinyl chloride, and total xylenes) were detected in one or more of the downgradient
monitoring wells. However, all detections were at concentrations below the respective 2L standards. A
comparison of the average concentrations of VOCs in downgradient wells with the average concentrations of
VOCs in the background well shows that the majority of average concentrations in downgradient wells
exceed those of the background well.
A comparison of metals is presented in Table 7. Barium, cadmium, and chromium were detected in MW-3R
at concentrations below groundwater quality standards. Thirteen metals (arsenic, barium, beryllium,
cadmium, chromium, cobalt, copper, lead, nickel, silver, thallium, vanadium, and zinc) were detected in one
or more of the downgradient monitoring wells. Four of the average concentrations of these metals (cobalt,
chromium, thallium, and vanadium) exceeded groundwater quality standards in one or more downgradient
monitoring wells. Additionally, average concentrations for the majority of metals in downgradient monitoring
wells exceeded the average concentrations of those metals in the background well.

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5.0 Summary
Altamont completed the first semiannual water quality monitoring event of 2015 at the Polk County Landfills
on March 17, 18, and 19, 2015.
Tables 3, 4, and 5 of this report, the TestAmerica report of laboratory analysis in Appendix B, and the EDD in
Appendix C provide detailed analytical results and field data demonstrating the groundwater and surface
water quality at the Polk County Landfills.
5.1 Future Activities
Altamont recommends that Polk County continue to monitor VOCs and metals concentrations in groundwater
and surface water at the closed C&D and MSW landfills.
Based on the data trends and evaluation presented in this report, Altamont has discussed with Polk County
options for addressing the water quality impacts identified at the site. Based on these discussions, Altamont
understands that Polk County is considering options for addressing identified water quality impacts.
Altamont will continue to monitor the groundwater and surface water on a semiannual basis at the Polk
County C&D and MSW Landfills. The next sampling event is scheduled for September 2015.

FIGURES

Copyright:© 2013 National Geographic Society, i-cubed
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Inactive ClosedMSW Landfill cell
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TABLES

Table 1
Summary of Groundwater Elevation Data---March 2015
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Top Of Casing (TOC)
Elevation (From
Assumed Datum)
Depth To Water Groundwater
Elevation
(feet) (feet TOC)(feet)
C&D Landfill
MW-01CD 2,955.50 110.66 2,844.84
MW-02CD 2,951.90 119.20 2,832.70
MW-03CD 2,969.60 120.12 2,849.48
MSW Landfill
MW-1R 2,867.70 28.41 2,839.29
MW-2R 2,837.20 33.52 2,803.68
MW-3R 2,962.00 77.53 2,884.47
Notes:
1. All elevations were based on an assumed datum of 3,000 feet.
2. Monitoring well MW-3R was surveyed on November 8, 2012 by Wes Cole Land Surveying, PA.
3. Monitoring wells MW-1R and MW-2R were surveyed on November 13, 2010 by Wes Cole
Land Surveying, PA.
4. Remaining wells were surveyed on December 9, 2006 by Wes Cole Land Surveying, PA.
5. Depth to water for all monitoring wells was measured on March 17, 18, and 19, 2015.
Well ID
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Spring\Tables\7502March2015 T1 GW Elevation Data Page 1 of 1
Table 2
Summary of Laboratory Analyses Performed on Samples
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
GROUNDWATER SAMPLES
VOCs
EPA 8260 EPA 6010 EPA 6020 EPA 7470
C&D Landfill
75-02 MW-01CD 3/19/2015 X X X X
75-02 MW-02CD 3/19/2015 X X X X
75-02 MW-03CD 3/18/2015 X X X X
MSW Landfill
75-02 MW-1R 3/19/2015 X X X X
75-02 MW-2R 3/19/2015 X X X X
75-02 MW-2RDUP 3/19/2015 X X X X
75-02 MW-3R 3/18/2015 X X X X
SURFACE WATER SAMPLES
VOCs
EPA 8260 EPA 6010 EPA 6020 EPA 7470
C&D Landfill
75-02 SP-1 3/18/2015 X X X X
75-02 SS-1 3/18/2015 X X X X
75-02 SS-2 3/18/2015 X X X X
QUALITY CONTROL SAMPLES
VOCs
EPA 8260
75-02 TRIP BLANK 3/18/2015 X
Notes:
1. VOCs = volatile organic compounds
2. VOCs and metals analyses include Appendix I constituents per 40 CFR Part 258.
Facility
Permit Sample ID Collect Date
Facility
Permit Sample ID Collect Date
Metals
Metals
Facility
Permit Well ID Collect Date
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Spring\Tables\7502Mar2015 T2,T3,T4,T5 Page 1 of 1
Table 3
Summary of Detected Constituents
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Metals (Appendix I)VOCs (Appendix I)Field Parameters
Laboratory Certification 387 387
Laboratory Methods EPA 6010, EPA 7470 EPA 8260 5445 (pH only)
Parameter Barium Beryllium Cadmium Chromium Copper Lead Thallium Vanadium Zinc
1,1-
Dichloro-
ethane
1,2-
Dichloro-
benzene
1,4-
Dichloro-
benzene
cis-1,2-
Dichloro-
ethene
Tetrachloro-
ethene
Tetrahydro-
furan
Trichloro-
ethene
Trichloro-
fluoromethane pH Turbidity
CAS Number 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-50-8 7439-92-1 7440-28-0 7440-62-2 7440-66-6 75-34-3 95-50-1 106-46-7 156-59-2 127-18-4 109-99-9 79-01-6 75-69-4 SW320 SW330
SWS ID 15 23 34 51 54 131 194 209 213 75 69 71 78 192 458 201 203 320 330
Units µg/L ug/L ug/L ug/L ug/L ug/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L SU NTU
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
MW-01CD 3/19/2015 104 0.597 J 0.500 U 3.00 U 8.30 J 7.60 J 0.521 J 10.0 U 14.7 J 0.240 U 0.190 U 0.170 U 0.210 U 0.140 U 0.820 U 0.200 U 0.568 J 6.42 177.1
MW-02CD 3/19/2015 41.0 J 0.500 U 0.500 U 3.00 U 5.00 U 2.00 U 0.200 U 10.0 U 10.0 U 0.240 U 0.190 U 0.170 U 0.210 U 0.140 U 0.820 U 0.200 U 0.210 U 6.93 29.06
MW-03CD 3/18/2015 370 0.570 J 0.500 U 4.30 J 5.90 J 7.20 J 0.644 J 13.2 J 86.8 0.240 U 0.194 J 0.350 J 0.210 U 0.140 U 2.53 J 0.200 U 0.407 J 5.98 127.2
MW-1R 3/19/2015 185 0.605 J 1.90 3.60 J 13.0 6.40 J 0.272 J 14.4 J 24.2 J 0.240 U 0.190 U 0.170 U 0.210 U 0.140 U 0.820 U 0.200 U 0.210 U 5.02 24.32
MW-2R 3/19/2015 180 0.500 U 0.500 U 3.00 U 5.00 U 2.00 U 0.200 U 10.0 U 10.0 U 0.756 J 0.190 U 0.170 U 11.5 0.151 J 0.820 U 1.03 0.210 U 6.02 1.50
MW-2RDUP 3/19/2015 189 0.500 U 0.500 U 3.00 U 5.00 U 2.00 U 0.200 U 10.0 U 10.0 U 0.668 J 0.190 U 0.170 U 10.3 0.183 J 0.820 U 0.982 J 0.210 U 6.02 1.50
MW-3R 3/18/2015 7.50 J 0.500 U 0.500 U 3.00 U 5.00 U 2.00 U 0.200 U 10.0 U 10.0 U 0.240 U 0.190 U 0.170 U 0.210 U 0.140 U 0.820 U 0.200 U 0.210 U 6.69 17.59
SP-1 3/18/2015 106 0.500 U 0.500 U 3.00 U 5.00 U 2.00 J 0.200 U 10.0 U 10.0 U 0.240 U 0.190 U 0.170 U 0.210 U 0.140 U 0.820 U 0.200 U 0.210 U 6.82 75.01
SS-1 3/18/2015 36.2 J 0.500 U 0.500 U 3.00 U 5.00 U 2.00 U 0.200 U 10.0 U 10.0 U 0.240 U 0.190 U 0.170 U 0.210 U 0.140 U 0.820 U 0.200 U 0.210 U 6.92 24.71
SS-2 3/18/2015 36.6 J 0.500 U 0.500 U 3.00 U 5.00 U 2.80 J 0.200 U 10.0 U 10.0 U 0.240 U 0.190 U 0.170 U 0.210 U 0.140 U 0.820 U 0.200 U 0.210 U 7.12 21.14
TRIP BLANK 3/18/2015 NA NA NA NA NA NA NA NA NA 0.240 U 0.190 U 0.170 U 0.210 U 0.140 U 0.820 U 0.200 U 0.210 U NA NA
MDL 5.0 0.500 0.500 3.00 5.00 2.00 0.200 10.0 10.0 0.240 0.190 0.170 0.210 0.140 0.820 0.200 0.210 NA NA
MRL 10.0 2.00 1.00 5.00 10.0 5.00 2.00 20.0 25.0 1.00 1.00 1.00 1.00 1.00 10.0 1.00 1.00 NA NA
SWSL 100 1 1 10 10 10 5.5 25 10 5 5 1 5 1 NE 1 1 NE NE
2L 700 NE 2 10 1,000 15 NE NE 1,000 6 20 6 70 0.7 NE 3 2,000 6.5-8.5 NE
IMAC NE 4 NE NE NE NE 0.2 0.3 NE NE NE NE NE NE NE NE NE NE NE
GWP NE 4 NE NE NE NE 0.28 0.3 NE NE NE NE NE NE NE NE NE NE NE
2B 200,000 6.5 2 50 7 25 0.47 NE 50 100 470 100 720 3.3 NE 30 67,000 6.0-9.0 25
Notes:
1.Only detected constituents are listed on this table. Please refer to TestAmerica Report of Laboratory Analysis (Appendix B) for further details.
2."Lab Method" is the analytical method used to analyze the constituents.
3."CAS Number" is a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
4."SWS ID" is the Solid Waste Section Identification Number.
5."Units" are micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH, and nephelometric turbidity units (NTU) for turbidity.
6."Collect Date" is the date on which the sample was collected in the field.
7."Result" is analytical data reported by the laboratory or field data collected by Altamont.
8."MDL" is the method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
9."MRL" is the method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
10."SWSL" is the Solid Waste Section Limit. This limit (identified by DENR) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
11."U" is a laboratory data qualifier used for parameters not detected at concentrations above MDL.
12."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
An italicized "J" qualifier is assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
13."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources,
Subchapter 2L - Groundwater Classifications and Standards," DENR (Amended April 1, 2013). The IMAC concentrations listed in Appendix #1 of the 2L.
14."GWP" is the Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DENR. Current standards were obtained from http://portal.ncdenr.org/web/sw/envmonitoringlist (last updated June 13, 2011).
GWP standard is used only if 2L or IMAC standards are not established for specific constituent.
15."2B" indicates surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2B - Surface Water and Wetland Standards,"
(last amended on May 1, 2007) or standard obtained from National Criteria per EPA table (current as of May 15, 2013).
16."NE" means Not Established. "NA" means Not Applicable.
17.Bold numbers indicate a detection. Grayed cells indicate result in exceedance of the 2L, IMAC, GWP, or 2B standard.
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Table 4
Solid Waste Section Limits Exceedances Notification
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
FACILITY
PERMIT SAMPLE ID CAS
NUMBER SWS ID PARAMETER RESULT UNITS METHOD MDL MRL SWSL COLLECT DATE
GROUNDWATER SAMPLES
75-02 MW-01CD 7440-39-3 15 Barium 104 µg/L EPA 6010 5.00 10.0 100 3/19/2015
75-02 MW-01CD 7440-66-6 213 Zinc 14.7 J µg/L EPA 6020 10.0 25.0 10 3/19/2015
75-02 MW-03CD 7440-39-3 15 Barium 370 µg/L EPA 6010 5.00 10.0 100 3/18/2015
75-02 MW-03CD 7440-66-6 213 Zinc 86.8 µg/L EPA 6020 10.0 25.0 10 3/18/2015
75-02 MW-1R 7440-39-3 15 Barium 185 µg/L EPA 6010 5.00 10.0 100 3/19/2015
75-02 MW-1R 7440-43-9 34 Cadmium 1.90 µg/L EPA 6010 0.500 1.00 1 3/19/2015
75-02 MW-1R 7440-50-8 54 Copper 13.0 µg/L EPA 6010 5.00 10.0 10 3/19/2015
75-02 MW-1R 7440-66-6 213 Zinc 24.2 J µg/L EPA 6020 10.0 25.0 10 3/19/2015
75-02 MW-2R 7440-39-3 15 Barium 180 µg/L EPA 6010 5.00 10.0 100 3/19/2015
75-02 MW-2R 156-59-2 78 cis-1,2-Dichloroethene 11.5 µg/L EPA 8260 0.210 1.00 5 3/19/2015
75-02 MW-2R 79-01-6 201 Trichloroethene 1.03 µg/L EPA 8260 0.200 1.00 1 3/19/2015
75-02 MW-2RDUP 7440-39-3 15 Barium 189 µg/L EPA 6010 5.00 10.0 100 3/19/2015
75-02 MW-2RDUP 156-59-2 78 cis-1,2-Dichloro-ethene 10.3 µg/L EPA 8260 0.210 1.00 5 3/19/2015
75-02 SP-1 7440-39-3 15 Barium 106 µg/L EPA 6010 5.00 10.0 100 3/18/2015
Notes:
1."CAS NUMBER" is a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
2."SWS ID" is the Solid Waste Section Identification Number.
3."RESULT" is the analytical data reported by the laboratory.
4."µg/L" indicates unit of micrograms per liter for analytical results.
5."METHOD" is the analytical method used to analyze the constituents.
6."MDL" is the method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence
that the analyte concentration is greater than zero.
7."MRL" is the method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
8."SWSL" is the Solid Waste Section Limit. This limit (identified by DENR) is the lowest amount of analyte in a sample that can be quantitatively
determined with suitable precision and accuracy.
9."COLLECT DATE" is the date on which the sample was collected in the field.
10.Grayed cells indicate result in exceedance of the applicable water quality standards ("2L", "IMAC", or "GWP").
11."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code,
Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater Classifications and Standards," DENR
(Amended April 1, 2013). The IMAC concentrations are listed in Appendix #1 of the 2L rule.
12."GWP" is the Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DENR. Current standards were obtained from
http://portal.ncdenr.org/web/sw/envmonitoringlist (last updated June 13, 2011). GWP standard is used only if 2L or IMAC standards are not
established for specific constituent.
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Spring\Tables\7502Mar2015 T2,T3,T4,T5 Page 1 of 1
Table 5
Water Quality Standards Exceedances Notification
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
FACILITY
PERMIT WELL ID CAS
NUMBER
SWS
ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
WATER
QUALITY
STANDARD
COLLECT
DATE CAUSE AND SIGNIFICANCE
GROUNDWATER SAMPLES - 2L STANDARD, IMAC OR GROUNDWATER PROTECTION STANDARD (GWP; ug/L or SU)
75-02 MW-01CD 7440-28-0 194 Thallium 0.521 µg/L J EPA 6020 0.200 2.00 5.5 0.2 3/19/2015 Likely due to high turbidity.
75-02 MW-01CD SW320 320 pH 6.42 SU 5445 NA NA NE 6.5 - 8.5 3/19/2015 Consistent with historic readings.
75-02 MW-03CD 7440-28-0 194 Thallium 0.644 µg/L J EPA 6020 0.200 2.00 5.5 0.2 3/18/2015 Likely due to high turbidity.
75-02 MW-03CD 7440-62-2 209 Vanadium 13.2 µg/L J EPA 6010 10.0 20.0 25 0.3 3/18/2015 Consistent with historic readings.
75-02 MW-03CD SW320 320 pH 5.98 SU 5445 NA NA NE 6.5 - 8.5 3/18/2015 Consistent with historic readings.
75-02 MW-1R 7440-28-0 194 Thallium 0.272 µg/L J EPA 6020 0.200 2.00 5.5 0.2 3/19/2015 Likely due to high turbidity.
75-02 MW-1R 7440-62-2 209 Vanadium 14.4 µg/L J EPA 6010 10.0 20.0 25 0.3 3/19/2015 Consistent with historic readings.
75-02 MW-1R SW320 320 pH 5.02 SU 5445 NA NA NE 6.5 - 8.5 3/19/2015 Consistent with historic readings.
75-02 MW-2R SW320 320 pH 6.02 SU 5445 NA NA NE 6.5 - 8.5 3/19/2015 Consistent with historic readings.
75-02 MW-2RDUP SW320 320 pH 6.02 SU 5445 NA NA NE 6.5 - 8.5 3/19/2015 Consistent with historic readings.
75-02 SP-1 SW330 330 Turbidity 75.01 NTU NA NA NA NE 25 3/18/2015
Notes:
1."CAS NUMBER" is a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
2."SWS ID" is the Solid Waste Section Identification Number.
3."RESULT" is analytical data reported by the laboratory or field data collected by Altamont.
4."UNITS" are micrograms per liter (µg/L) for analytical results and Standard Units (SU) for pH.
5."QUALIFIER" is a data qualifier or "flag". A blank cell indicates that there is no qualifier associated with the reported result.
6."METHOD" is the analytical method used to analyze the constituents.
7."MDL" is the method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration
is greater than zero.
8."MRL" is the method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
9."SWSL" is the Solid Waste Section Limit. This limit (identified by DENR) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
10."WATER QUALITY STANDARD" refers to the 2L Standard, Interim Maximum Allowable Concentration (IMAC), or Groundwater Protection Standard (GWP) for groundwater,
2B Standard for surface water.
11."COLLECT DATE" is the date on which the sample was collected in the field.
12.2L standard and IMAC are from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2L -
Groundwater Classifications and Standards," DENR (Amended April 1, 2013). The IMAC concentrations are listed in Appendix #1 of the 2L rule.
13."NE" means not established.
14.Blank cell indicates that there is no relevant information associated with this cell.
15.2B standard is from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2B - Surface Water
and Wetland Standards," (last amended on May 1, 2007) or National Criteria per EPA obtained from table current as of May 15, 2013.
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Spring\Tables\7502Mar2015 T2,T3,T4,T5 Page 1 of 1
Table 6
VOCs Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
MW-01CD 6/6 Trichlorofluoromethane 0.28 J 0.65 J 0.418 2,000
1/2 Acetone 2.53 J 2.66 U 1.93 6,000
1/2 Trichlorofluoromethane 0.210 U 0.42 J 0.26 2,000
1/2 Xylene (Total)0.38 U 0.47 J 0.33 500
1/6 1,2-Dichlorobenzene 0.12 U 0.30 U 0.14 20
1/6 1,4-Dichlorobenzene 0.33 U 0.463 U 0.21 6
1/6 Acetone 0.598 U 4.59 J 4.32 6,000
1/5 Tetrahydrafuran 2.53 J 3.1 U 1.75 NE
6/6 Trichlorofluoromethane 0.34 J 0.52 J 0.4 2,000
1/6 Xylene (Total)0.38 U 0.55 J 0.34 500
1/6 1,4-Dichlorobenzene 0.17 J 0.33 U 0.15 6
1/6 cis-1,2-Dichloroethene 0.19 U 1.85 J 0.39 70
9/11 1,1-Dichloroethane 0.32 U 1.06 J 0.81 6
10/11 cis-1,2-Dichloroethene 5.2 13.9 10.17 70
3/11 Tetrachloroethene 0.151 U 0.25 J 0.21 0.7
10/11 Trichloroethene 0.200 U 1.56 0.86 3
1/11 Vinyl chloride 0.1 J 0.62 U 0.23 0.03
0/6 1,1-Dichloroethane 0.215 U 0.32 U 0.14 6
0/6 1,2-Dichlorobenzene 0.19 0.3 0.35 20
0/6 1,4-Dichlorobenzene 0.33 U 0.463 U 0.16 6
0/6 cis-1,2-Dichloroethene 0.19 U 0.19 U 0.11 70
0/6 Acetone 0.598 U 10 U 3.67 6,000
0/6 Tetrachloroethene 0.264 U 0.46 U 0.19 0.7
0/6 Trichloroethene 0.227 U 0.47 U 0.19 3
0/6 Trichlorofluoromethane 0.137 U 0.21 U 0.096 2,000
0/6 Vinyl chloride 0.189 U 0.62 U 0.24 0.03
0/6 Xylene (Total)0.20 U 0.66 U 0.28 500
Notes:
1."µg/L" = micrograms per liter
2."Min." = minimum concentration (µg/L)
3."Max." = maximum concentration (µg/L)
4."Avg." = average concentration (µg/L)
5."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code,
Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater Classifications and Standards,"
DENR (Amended April 1, 2013). The IMAC concentrations listed in Appendix #1 of the 2L.
6."U" is a laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit (MDL).
7."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method reporting limit (MRL).
8."NA" = not applicable
9."# Detections" = number of times the constituent was detected during the sample collection period. MW-2R had duplicate samples collected
during 5 of the 6 sampling events, thus there are 11 total samples representing MW-2R.
10.Grayed cells indicate results above 2L Standard or IMAC.
11.Average concentrations were calculated by summing the contiuent detections and dividing by the number of samples. When the sample was
below the MDL, half of the MDL value was used as the result. Some results are estimated (J flagged) and the average concentration is thus estimated.
12.MW-02CD was only sampled in September 2012 and March 2015 due to a lack of well recharge during other sampling events.
13.The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September 2012.
MW-2R (and
MW-2RDUP)
MW-3R
MW-1R
MW-03CD
MW-02CD
September 2012 - March 2015
Well # Detections Detected Constituents Concentration (µg/L)2L Standard or
IMAC
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Spring\Statistics_Background 2015 0416 Page 1 of 1
Table 7
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
6/6 Barium 2.5/3.69/5.0 12.5 J 104 40.75 700
1/6 Beryllium 0.0594/0.65/0.50/1.0 0.5 U 0.65 U 0.45 700
1/6 Cadmium 0.0278/0.155/0.50/1.0 0.3 J 1.0 U 0.44 2
1/6 Chromium 1.47/2.5/5.0 3.28 J 5.0 U 2.26 10
2/6 Copper 0.672/2.5/5.0 2.5 U 8.30 J 4.05 1,000
2/6 Lead 2.5/5.0/5.41 2.5 U 7.72 J 4.01 15
1/6 Silver 1.05/2.5/5.0 2.5 U 5.02 J 2.50 20
2/6 Thallium 0.019/0.025/0.641 0.019 U 0.641 U 0.15 0.2
1/6 Vanadium 0.0661/2.5/5.0 1.8 J 10 U 2.60 0.3
4/6 Zinc 2.26/5.0/10.0 10.0 U 105 25.50 1,000
2/2 Barium 2.5/3.69/5.0 41.0 J 79.6 J 60.3 700
1/2 Cadmium 0.0278/0.155/0.50/1.0 0.3 J 0.5 U 0.275 2
1/2 Chromium 1.47/5.0 3.0 U 3.66 J 2.58 10
1/2 Copper 0.672/5.0 5.0 U 5.52 J 4.01 1,000
1/2 Lead 5.0/5.41 2.0 U 10.9 5.95 15
1/2 Silver 1.05/5.0 2.5 U 4.99 J 3.12 20
1/2 Vanadium 0.0661/2.5/5.0 1.6 J 10 U 3.3 0.3
1/2 Zinc 2.26/5.0/10.0 10 U 15.6 10.3 1,000
6/6 Barium 2.5/3.69/5.0 184 768 370 700
2/6 Beryllium 0.65/1.0 0.570 J 1.7 0.68 NA
4/6 Chromium 1.47/2.5/5.0 4.30 J 20.3 7.78 10
2/6 Cobalt 2.5/3.39/5.0 3.39 U 10.1 4.2 1
4/6 Copper 0.672/2.5/5.0 5.0 U 21.8 9.85 1,000
3/6 Lead 1.05/2.5/5.0 5.0 U 8.15 J 6.91 15
3/6 Nickel 1.05/2.5/5.0 3.0 U 18.6 6.58 100
1/6 Silver 1.05/2.5/5.0 2.5 U 5.97 J 2.66 20
5/6 Thallium 0.019/0.025/0.641 0.026 J 0.644 J 0.25 0.2
6/6 Vanadium 0.0661/2.5/5.0 4 J 54 17.9 0.3
6/6 Zinc 2.26/5.0/10.0 21.8 223 75.9 1,000
1/6 Arsenic 2.5/3.69/5.0/ 10.0 2.5 U 25.6 6.22 10
6/6 Barium 2.5/3.69/5.0 41.4 J 2,270 463.8 700
3/6 Beryllium 0.0594/0.65/0.50/1.0 0.50 U 13.3 2.68 4
3/6 Cadmium 0.0278/0.155/0.50/1.0 0.3 J 5.8 1.54 2
3/6 Chromium 1.47/2.5/5.0 3.60 J 51.5 10.92 10
3/6 Copper 0.672/2.5/5.0 2.5 U 122 25.49 1,000
3/6 Lead 2.5/5 2.5 U 64.7 13.84 15
2/6 Nickel 2.5/3.06/5.0 2.5 U 29.1 J 7.12 100
1/6 Silver 1.05/2.5/5.0 2.5 U 5.0 U 2.49 20
3/6 Thallium 0.019/0.025/0.641 0.025 U 1.2 J 0.31 0.2
3/6 Vanadium 0.0661/2.5/5.0 2.5 U 407 74.9 0.3
6/6 Zinc 2.26/5.0/10.0 11.9 428 87.13 1,000
11/11 Barium 2.5/3.69/5.0 63.3 J 189 149.30 700
1/11 Cadmium 0.0278/0.155/0.50/1.0 0.155 U 1.0 U 0.37 2
2/11 Chromium 1.47/2.5/5.0 2.5 U 5.0 U 2.28 10
2/11 Copper 0.672/2.5/5.0 2.5 U 7.01 J 3.08 1,000
1/11 Nickel 2.5/3.06/5.0 2.5 U 5.0 U 2.35 100
2/11 Silver 1.05/2.5/5.0 2.5 U 5.88 J 2.60 20
1/11 Thallium 0.019/0.025/0.641 0.019 U 0.641 U 0.085 0.2
6/11 Zinc 2.26/5.0/10.0 10.0 U 19.5 11.14 1,000
MW-03CD
MW-1R
MW-2R (and
MW-2RDUP)
MW-02CD
Well
MW-01CD
September 2012 - March 2015
# Detections MDL (ug/L)
Concentration (µg/L)
Constituents Detected 2L Standard
or IMAC
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Spring\Statistics_Background 2015 0416 Page 1 of 2
Table 7
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
Well
MW-01CD
September 2012 - March 2015
# Detections MDL (ug/L)
Concentration (µg/L)
Constituents Detected 2L Standard
or IMAC
0/6 Arsenic 3.69/5.0/ 10.0 3.69 U 10.0 U 2.78 10
6/6 Barium 2.5/3.69/5.0 3.25 J 12.3 J 6.11 700
0/6 Beryllium 0.13/0.5/1.0 0.13 U 1.0 U 0.34 4
1/6 Cadmium 0.0278/0.155/0.50/1.0 0.04 J 1.0 U 0.34 2
1/6 Chromium 1.47/2.5/5.0 2.02 J 5.0 U 2.05 10
0/6 Cobalt 2.5/3.39/5.0 3.39 U 5.0 U 2.16 1
0/6 Copper 0.672/5.0 0.672 U 5.0 U 1.76 1,000
0/6 Lead 2.0/2.5/5.0/5.41 2.0 U 5.41 U 2.08 15
0/6 Nickel 3.06/5.0 2.5 U 5.0 U 1.96 100
0/6 Silver 1.05/2.5/5.0 1.05 U 5.0 U 1.75 20
0/6 Thallium 0.019/0.025/0.641 0.019U 0.641 U 0.078 0.2
0/6 Vanadium 0.903/5.0 0.903 U 5.0 U 1.55 0.3
0/6 Zinc 2.26/5.0/10.0 2.26 U 10.0 U 3.94 1,000
Notes:
1."µg/L" = micrograms per liter
2."Min." = minimum concentration (µg/L)
3."Max." = maximum concentration (ug/L)
4."Avg." = average concentration (µg/L)
5."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code,
Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater Classifications and Standards,"
DENR (Amended April 1, 2013). The IMAC concentrations listed in Appendix #1 of the 2L.
6."U" is a laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit (MDL).
7."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method reporting limit (MRL).
8."NA" = not applicable
9."# Detections" = number of times the constituent was detected during the sample collection period. MW-2R had duplicate samples collected
during 5 of the 6 sampling events, thus there are 11 total samples representing MW-2R.
10.Grayed cells indicate results above 2L Standard or IMAC.
11.Average concentrations were calculated by summing the constituent detections and dividing by the number of samples. When the sample was
below the MDL, half of the MDL value was used as the result. Some results are estimated (J flagged) and the average concentration is thus estimated.
12.MW-02CD was only sampled in September 2012 and March 2015 due to a lack of well recharge during subsequent sampling events.
13.The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September 2012.
MW-3R
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Spring\Statistics_Background 2015 0416 Page 2 of 2

APPENDICES

APPENDIX A

Sampling Logs and
Equipment Documentation and
Instrument Calibration Data Sheets

APPENDIX B

Report of Laboratory Analysis
and
Chain-of-Custody Documentation

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-74829-1
Client Project/Site: Polk County Route 9 Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
4/1/2015 10:43:58 AM
Heather Baker, Project Manager I
[phone]
[e-mail]
Designee for
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
TestAmerica Job ID: 490-74829-1
Page 2 of 55 TestAmerica Nashville4/1/2015
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .45
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .48
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55
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Sample Summary
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-74829-1 MW-01CD Water 03/19/15 12:01 03/20/15 08:40
490-74829-2 MW-03CD Water 03/18/15 11:20 03/20/15 08:40
490-74829-3 MW-1R Water 03/19/15 10:20 03/20/15 08:40
490-74829-4 MW-2R Water 03/19/15 13:45 03/20/15 08:40
490-74829-5 MW-2RDUP Water 03/19/15 13:45 03/20/15 08:40
490-74829-6 MW-3R Water 03/18/15 12:37 03/20/15 08:40
490-74829-7 SP-1 Water 03/18/15 13:30 03/20/15 08:40
490-74829-8 SS-1 Water 03/18/15 12:53 03/20/15 08:40
490-74829-9 SS-2 Water 03/18/15 13:08 03/20/15 08:40
490-74829-10 MW-02CD Water 03/19/15 12:26 03/20/15 08:40
490-74829-11 Trip Blank Water 03/18/15 01:00 03/20/15 08:40
TestAmerica Nashville
Page 3 of 55 4/1/2015
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Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-74829-1
Project/Site: Polk County Route 9 Landfill
Job ID: 490-74829-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-74829-1
Comments
No additional comments.
Receipt
The samples were received on 3/20/2015 8:40 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 0.4º C.
GC/MS VOA
Method(s) 8260B: The continuing calibration verification (CCV) associated with batch 237281 recovered above the upper control limit for
Vinyl acetate.The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
The following samples are impacted: (CCVIS 490-237281/2).
Method(s) 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for batch 237281 recovered
outside control limits for the following analyte: Vinyl acetate.This analyte was biased high in the LCS and was not detected in the
associated samples; therefore, the data have been reported.
Method(s) 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for batch 237488 recovered
outside control limits for the following analytes: Vinyl acetate and Tetrahydrofuran. These analytes were biased high in the LCS and were
not detected in the associated samples; therefore, the data have been reported.
Method(s) 8260B: The continuing calibration verification (CCV) associated with batch 237488 recovered above the upper control limit for
Vinyl acetate. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
The following samples are impacted: (CCVIS 490-237488/2).
Method(s) 8260B: The method blank for batch 237488 contained Methylene Chloride above the method detection limit. This target analyte
concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica NashvillePage 4 of 55 4/1/2015
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Definitions/Glossary
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
*LCS or LCSD exceeds the control limits
F1 MS and/or MSD Recovery exceeds the control limits
F2 MS/MSD RPD exceeds control limits
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 03/19/15 12:01
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 00:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 00:01 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 00:01 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 00:01 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 00:01 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 00:01 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 00:01 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 00:01 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 00:01 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 00:01 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 00:01 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 00:01 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 00:01 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 00:01 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 00:01 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/29/15 00:01 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 00:01 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 00:01 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 00:01 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 00:01 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 00:01 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/29/15 00:01 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/29/15 00:01 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/29/15 00:01 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 00:01 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 00:01 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 00:01 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 00:01 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 00:01 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 00:01 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 00:01 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 00:01 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 00:01 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 00:01 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 00:01 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/29/15 00:01 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/29/15 00:01 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 00:01 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 00:01 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 00:01 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 00:01 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 00:01 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 00:01 1Trichloroethene<0.200
1.00 0.210 ug/L 03/29/15 00:01 1Trichlorofluoromethane0.568 J
1.00 0.230 ug/L 03/29/15 00:01 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 00:01 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 00:01 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 00:01 1Xylenes, Total <0.380
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 03/19/15 12:01
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)105 70-130 03/29/15 00:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)99 03/29/15 00:01 170-130
1,2-Dichloroethane-d4 (Surr)94 03/29/15 00:01 170-130
Toluene-d8 (Surr)101 03/29/15 00:01 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 20:28 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:28 1Barium0.104
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 20:28 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 20:28 1Chromium<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:28 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:28 1Copper0.00830 J
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 20:28 1Lead0.00760
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 20:28 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:28 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 20:28 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 20:28 1Vanadium<0.0100
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium 0.000597 J 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 15:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 15:48 1Thallium0.000521 J
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 15:48 1Zinc0.0147 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/23/15 18:56 03/24/15 18:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-2Client Sample ID: MW-03CD
Matrix: WaterDate Collected: 03/18/15 11:20
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 00:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 00:28 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 00:28 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 00:28 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 00:28 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 00:28 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 00:28 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 00:28 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 00:28 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 00:28 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 00:28 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 00:28 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 00:28 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 00:28 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 00:28 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/29/15 00:28 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 00:28 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 00:28 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 00:28 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 00:28 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 00:28 11,2-Dichlorobenzene 0.194 J
1.00 0.170 ug/L 03/29/15 00:28 11,4-Dichlorobenzene 0.350 J
1.00 0.240 ug/L 03/29/15 00:28 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/29/15 00:28 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 00:28 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 00:28 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 00:28 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 00:28 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 00:28 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 00:28 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 00:28 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 00:28 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 00:28 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 00:28 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 00:28 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/29/15 00:28 1Tetrahydrofuran2.53 J
1.00 0.170 ug/L 03/29/15 00:28 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 00:28 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 00:28 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 00:28 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 00:28 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 00:28 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 00:28 1Trichloroethene<0.200
1.00 0.210 ug/L 03/29/15 00:28 1Trichlorofluoromethane0.407 J
1.00 0.230 ug/L 03/29/15 00:28 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 00:28 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 00:28 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 00:28 1Xylenes, Total <0.380
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-2Client Sample ID: MW-03CD
Matrix: WaterDate Collected: 03/18/15 11:20
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)102 70-130 03/29/15 00:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 03/29/15 00:28 170-130
1,2-Dichloroethane-d4 (Surr)92 03/29/15 00:28 170-130
Toluene-d8 (Surr)104 03/29/15 00:28 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 20:46 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:46 1Barium0.370
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 20:46 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 20:46 1Chromium0.00430 J
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:46 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:46 1Copper0.00590 J
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 20:46 1Lead0.00720
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 20:46 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:46 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 20:46 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 20:46 1Vanadium0.0132 J
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium 0.000570 J 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 16:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 16:13 1Thallium0.000644 J
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 16:13 1Zinc0.0868
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/23/15 18:56 03/24/15 18:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-3Client Sample ID: MW-1R
Matrix: WaterDate Collected: 03/19/15 10:20
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 00:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 00:56 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 00:56 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 00:56 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 00:56 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 00:56 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 00:56 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 00:56 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 00:56 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 00:56 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 00:56 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 00:56 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 00:56 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 00:56 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 00:56 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/29/15 00:56 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 00:56 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 00:56 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 00:56 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 00:56 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 00:56 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/29/15 00:56 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/29/15 00:56 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/29/15 00:56 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 00:56 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 00:56 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 00:56 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 00:56 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 00:56 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 00:56 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 00:56 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 00:56 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 00:56 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 00:56 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 00:56 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/29/15 00:56 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/29/15 00:56 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 00:56 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 00:56 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 00:56 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 00:56 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 00:56 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 00:56 1Trichloroethene<0.200
1.00 0.210 ug/L 03/29/15 00:56 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/29/15 00:56 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 00:56 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 00:56 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 00:56 1Xylenes, Total <0.380
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-3Client Sample ID: MW-1R
Matrix: WaterDate Collected: 03/19/15 10:20
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)102 70-130 03/29/15 00:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 03/29/15 00:56 170-130
1,2-Dichloroethane-d4 (Surr)91 03/29/15 00:56 170-130
Toluene-d8 (Surr)102 03/29/15 00:56 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 20:59 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:59 1Barium0.185
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 20:59 1Cadmium0.00190
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 20:59 1Chromium0.00360 J
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:59 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:59 1Copper0.0130
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 20:59 1Lead0.00640
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 20:59 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:59 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 20:59 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 20:59 1Vanadium0.0144 J
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium 0.000605 J 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 16:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 16:19 1Thallium0.000272 J
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 16:19 1Zinc0.0242 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/23/15 18:56 03/24/15 18:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 03/19/15 13:45
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 01:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 01:24 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 01:24 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 01:24 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 01:24 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 01:24 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 01:24 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 01:24 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 01:24 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 01:24 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 01:24 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 01:24 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 01:24 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 01:24 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 01:24 1cis-1,2-Dichloroethene 11.5
1.00 0.170 ug/L 03/29/15 01:24 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 01:24 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 01:24 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 01:24 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 01:24 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 01:24 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/29/15 01:24 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/29/15 01:24 11,1-Dichloroethane 0.756 J
1.00 0.200 ug/L 03/29/15 01:24 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 01:24 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 01:24 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 01:24 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 01:24 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 01:24 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 01:24 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 01:24 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 01:24 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 01:24 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 01:24 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 01:24 1Tetrachloroethene0.151 J
10.0 0.820 ug/L 03/29/15 01:24 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/29/15 01:24 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 01:24 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 01:24 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 01:24 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 01:24 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 01:24 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 01:24 1Trichloroethene1.03
1.00 0.210 ug/L 03/29/15 01:24 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/29/15 01:24 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 01:24 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 01:24 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 01:24 1Xylenes, Total <0.380
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 03/19/15 13:45
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)102 70-130 03/29/15 01:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)105 03/29/15 01:24 170-130
1,2-Dichloroethane-d4 (Surr)94 03/29/15 01:24 170-130
Toluene-d8 (Surr)103 03/29/15 01:24 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 21:03 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:03 1Barium0.180
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 21:03 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 21:03 1Chromium<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:03 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:03 1Copper<0.00500
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 21:03 1Lead<0.00200
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 21:03 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:03 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 21:03 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 21:03 1Vanadium<0.0100
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium <0.000500 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 16:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 16:24 1Thallium<0.000200
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 16:24 1Zinc<0.0100
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/23/15 18:56 03/24/15 18:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 03/19/15 13:45
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 01:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 01:52 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 01:52 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 01:52 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 01:52 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 01:52 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 01:52 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 01:52 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 01:52 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 01:52 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 01:52 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 01:52 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 01:52 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 01:52 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 01:52 1cis-1,2-Dichloroethene 10.3
1.00 0.170 ug/L 03/29/15 01:52 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 01:52 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 01:52 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 01:52 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 01:52 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 01:52 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/29/15 01:52 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/29/15 01:52 11,1-Dichloroethane 0.668 J
1.00 0.200 ug/L 03/29/15 01:52 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 01:52 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 01:52 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 01:52 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 01:52 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 01:52 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 01:52 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 01:52 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 01:52 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 01:52 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 01:52 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 01:52 1Tetrachloroethene0.183 J
10.0 0.820 ug/L 03/29/15 01:52 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/29/15 01:52 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 01:52 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 01:52 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 01:52 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 01:52 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 01:52 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 01:52 1Trichloroethene0.982 J
1.00 0.210 ug/L 03/29/15 01:52 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/29/15 01:52 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 01:52 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 01:52 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 01:52 1Xylenes, Total <0.380
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 03/19/15 13:45
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)99 70-130 03/29/15 01:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)98 03/29/15 01:52 170-130
1,2-Dichloroethane-d4 (Surr)94 03/29/15 01:52 170-130
Toluene-d8 (Surr)103 03/29/15 01:52 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 21:08 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:08 1Barium0.189
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 21:08 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 21:08 1Chromium<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:08 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:08 1Copper<0.00500
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 21:08 1Lead<0.00200
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 21:08 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:08 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 21:08 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 21:08 1Vanadium<0.0100
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium <0.000500 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 16:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 16:39 1Thallium<0.000200
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 16:39 1Zinc<0.0100
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/23/15 18:56 03/24/15 18:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 03/18/15 12:37
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 02:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 02:20 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 02:20 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 02:20 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 02:20 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 02:20 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 02:20 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 02:20 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 02:20 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 02:20 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 02:20 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 02:20 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 02:20 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 02:20 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 02:20 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/29/15 02:20 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 02:20 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 02:20 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 02:20 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 02:20 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 02:20 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/29/15 02:20 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/29/15 02:20 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/29/15 02:20 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 02:20 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 02:20 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 02:20 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 02:20 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 02:20 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 02:20 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 02:20 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 02:20 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 02:20 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 02:20 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 02:20 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/29/15 02:20 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/29/15 02:20 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 02:20 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 02:20 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 02:20 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 02:20 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 02:20 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 02:20 1Trichloroethene<0.200
1.00 0.210 ug/L 03/29/15 02:20 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/29/15 02:20 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 02:20 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 02:20 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 02:20 1Xylenes, Total <0.380
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 03/18/15 12:37
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)103 70-130 03/29/15 02:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 03/29/15 02:20 170-130
1,2-Dichloroethane-d4 (Surr)92 03/29/15 02:20 170-130
Toluene-d8 (Surr)103 03/29/15 02:20 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 21:12 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:12 1Barium0.00750 J
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 21:12 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 21:12 1Chromium<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:12 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:12 1Copper<0.00500
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 21:12 1Lead<0.00200
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 21:12 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:12 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 21:12 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 21:12 1Vanadium<0.0100
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium <0.000500 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 16:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 16:44 1Thallium<0.000200
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 16:44 1Zinc<0.0100
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/24/15 12:23 03/24/15 20:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-7Client Sample ID: SP-1
Matrix: WaterDate Collected: 03/18/15 13:30
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 02:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 02:48 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 02:48 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 02:48 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 02:48 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 02:48 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 02:48 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 02:48 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 02:48 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 02:48 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 02:48 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 02:48 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 02:48 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 02:48 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 02:48 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/29/15 02:48 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 02:48 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 02:48 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 02:48 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 02:48 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 02:48 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/29/15 02:48 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/29/15 02:48 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/29/15 02:48 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 02:48 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 02:48 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 02:48 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 02:48 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 02:48 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 02:48 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 02:48 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 02:48 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 02:48 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 02:48 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 02:48 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/29/15 02:48 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/29/15 02:48 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 02:48 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 02:48 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 02:48 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 02:48 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 02:48 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 02:48 1Trichloroethene<0.200
1.00 0.210 ug/L 03/29/15 02:48 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/29/15 02:48 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 02:48 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 02:48 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 02:48 1Xylenes, Total <0.380
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-7Client Sample ID: SP-1
Matrix: WaterDate Collected: 03/18/15 13:30
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)102 70-130 03/29/15 02:48 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 03/29/15 02:48 170-130
1,2-Dichloroethane-d4 (Surr)88 03/29/15 02:48 170-130
Toluene-d8 (Surr)101 03/29/15 02:48 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 21:17 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:17 1Barium0.106
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 21:17 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 21:17 1Chromium<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:17 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:17 1Copper<0.00500
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 21:17 1Lead0.00200 J
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 21:17 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:17 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 21:17 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 21:17 1Vanadium<0.0100
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium <0.000500 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 16:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 16:49 1Thallium<0.000200
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 16:49 1Zinc<0.0100
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/24/15 12:23 03/24/15 20:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-8Client Sample ID: SS-1
Matrix: WaterDate Collected: 03/18/15 12:53
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 03:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 03:16 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 03:16 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 03:16 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 03:16 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 03:16 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 03:16 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 03:16 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 03:16 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 03:16 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 03:16 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 03:16 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 03:16 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 03:16 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 03:16 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/29/15 03:16 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 03:16 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 03:16 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 03:16 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 03:16 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 03:16 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/29/15 03:16 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/29/15 03:16 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/29/15 03:16 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 03:16 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 03:16 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 03:16 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 03:16 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 03:16 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 03:16 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 03:16 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 03:16 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 03:16 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 03:16 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 03:16 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/29/15 03:16 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/29/15 03:16 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 03:16 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 03:16 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 03:16 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 03:16 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 03:16 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 03:16 1Trichloroethene<0.200
1.00 0.210 ug/L 03/29/15 03:16 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/29/15 03:16 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 03:16 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 03:16 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 03:16 1Xylenes, Total <0.380
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-8Client Sample ID: SS-1
Matrix: WaterDate Collected: 03/18/15 12:53
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)101 70-130 03/29/15 03:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 03/29/15 03:16 170-130
1,2-Dichloroethane-d4 (Surr)89 03/29/15 03:16 170-130
Toluene-d8 (Surr)103 03/29/15 03:16 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 21:21 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:21 1Barium0.0362
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 21:21 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 21:21 1Chromium<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:21 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:21 1Copper<0.00500
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 21:21 1Lead<0.00200
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 21:21 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:21 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 21:21 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 21:21 1Vanadium<0.0100
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium <0.000500 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 16:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 16:54 1Thallium<0.000200
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 16:54 1Zinc<0.0100
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/24/15 12:23 03/24/15 20:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-9Client Sample ID: SS-2
Matrix: WaterDate Collected: 03/18/15 13:08
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 03:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 03:44 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 03:44 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 03:44 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 03:44 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 03:44 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 03:44 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 03:44 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 03:44 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 03:44 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 03:44 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 03:44 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 03:44 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 03:44 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 03:44 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/29/15 03:44 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 03:44 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 03:44 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 03:44 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 03:44 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 03:44 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/29/15 03:44 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/29/15 03:44 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/29/15 03:44 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 03:44 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 03:44 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 03:44 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 03:44 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 03:44 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 03:44 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 03:44 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 03:44 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 03:44 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 03:44 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 03:44 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/29/15 03:44 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/29/15 03:44 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 03:44 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 03:44 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 03:44 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 03:44 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 03:44 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 03:44 1Trichloroethene<0.200
1.00 0.210 ug/L 03/29/15 03:44 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/29/15 03:44 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 03:44 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 03:44 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 03:44 1Xylenes, Total <0.380
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-9Client Sample ID: SS-2
Matrix: WaterDate Collected: 03/18/15 13:08
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)104 70-130 03/29/15 03:44 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)104 03/29/15 03:44 170-130
1,2-Dichloroethane-d4 (Surr)93 03/29/15 03:44 170-130
Toluene-d8 (Surr)105 03/29/15 03:44 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 21:26 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:26 1Barium0.0366
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 21:26 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 21:26 1Chromium<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:26 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:26 1Copper<0.00500
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 21:26 1Lead0.00280 J
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 21:26 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:26 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 21:26 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 21:26 1Vanadium<0.0100
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium <0.000500 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 17:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 17:00 1Thallium<0.000200
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 17:00 1Zinc<0.0100
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/24/15 12:23 03/24/15 20:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-10Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 03/19/15 12:26
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/29/15 04:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/29/15 04:11 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/29/15 04:11 1Benzene<0.200
1.00 0.150 ug/L 03/29/15 04:11 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/29/15 04:11 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/29/15 04:11 1Bromoform<0.290
1.00 0.350 ug/L 03/29/15 04:11 1Bromomethane<0.350
50.0 2.64 ug/L 03/29/15 04:11 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/29/15 04:11 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/29/15 04:11 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/29/15 04:11 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/29/15 04:11 1Chloroethane<0.360
1.00 0.230 ug/L 03/29/15 04:11 1Chloroform<0.230
1.00 0.360 ug/L 03/29/15 04:11 1Chloromethane<0.360
1.00 0.210 ug/L 03/29/15 04:11 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/29/15 04:11 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/29/15 04:11 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/29/15 04:11 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/29/15 04:11 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/29/15 04:11 1Dibromomethane<0.450
1.00 0.190 ug/L 03/29/15 04:11 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/29/15 04:11 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/29/15 04:11 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/29/15 04:11 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/29/15 04:11 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/29/15 04:11 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/29/15 04:11 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/29/15 04:11 12-Hexanone <1.28
10.0 1.50 ug/L 03/29/15 04:11 1Iodomethane<1.50
5.00 0.220 ug/L 03/29/15 04:11 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/29/15 04:11 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/29/15 04:11 1Styrene<0.280
1.00 0.150 ug/L 03/29/15 04:11 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/29/15 04:11 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/29/15 04:11 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/29/15 04:11 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/29/15 04:11 1Toluene<0.170
5.00 0.460 ug/L 03/29/15 04:11 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/29/15 04:11 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/29/15 04:11 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/29/15 04:11 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/29/15 04:11 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/29/15 04:11 1Trichloroethene<0.200
1.00 0.210 ug/L 03/29/15 04:11 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/29/15 04:11 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/29/15 04:11 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/29/15 04:11 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/29/15 04:11 1Xylenes, Total <0.380
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-10Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 03/19/15 12:26
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)100 70-130 03/29/15 04:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 03/29/15 04:11 170-130
1,2-Dichloroethane-d4 (Surr)91 03/29/15 04:11 170-130
Toluene-d8 (Surr)102 03/29/15 04:11 170-130
Method: 6010C - Metals (ICP)
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00720 mg/L 03/25/15 09:14 03/26/15 21:30 1Arsenic<0.00720
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:30 1Barium0.0410
0.00100 0.000500 mg/L 03/25/15 09:14 03/26/15 21:30 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/25/15 09:14 03/26/15 21:30 1Chromium<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:30 1Cobalt<0.00500
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:30 1Copper<0.00500
0.00500 0.00200 mg/L 03/25/15 09:14 03/26/15 21:30 1Lead<0.00200
0.0100 0.00300 mg/L 03/25/15 09:14 03/26/15 21:30 1Nickel<0.00300
0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 21:30 1Selenium<0.00500
0.00500 0.00250 mg/L 03/25/15 09:14 03/26/15 21:30 1Silver<0.00250
0.0200 0.0100 mg/L 03/25/15 09:14 03/26/15 21:30 1Vanadium<0.0100
Method: 6020A - Metals (ICP/MS)
RL MDL
Beryllium <0.000500 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000200 mg/L 03/25/15 09:14 03/26/15 17:05 1Thallium<0.000200
0.0250 0.0100 mg/L 03/25/15 09:14 03/26/15 17:05 1Zinc<0.0100
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/24/15 12:23 03/24/15 20:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-11Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 03/18/15 01:00
Date Received: 03/20/15 08:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/30/15 15:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/30/15 15:00 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/30/15 15:00 1Benzene<0.200
1.00 0.150 ug/L 03/30/15 15:00 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/30/15 15:00 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/30/15 15:00 1Bromoform<0.290
1.00 0.350 ug/L 03/30/15 15:00 1Bromomethane<0.350
50.0 2.64 ug/L 03/30/15 15:00 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/30/15 15:00 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/30/15 15:00 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/30/15 15:00 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/30/15 15:00 1Chloroethane<0.360
1.00 0.230 ug/L 03/30/15 15:00 1Chloroform<0.230
1.00 0.360 ug/L 03/30/15 15:00 1Chloromethane<0.360
1.00 0.210 ug/L 03/30/15 15:00 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/30/15 15:00 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/30/15 15:00 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/30/15 15:00 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/30/15 15:00 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/30/15 15:00 1Dibromomethane<0.450
1.00 0.190 ug/L 03/30/15 15:00 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/30/15 15:00 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/30/15 15:00 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/30/15 15:00 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/30/15 15:00 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/30/15 15:00 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/30/15 15:00 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/30/15 15:00 12-Hexanone <1.28
10.0 1.50 ug/L 03/30/15 15:00 1Iodomethane<1.50
5.00 0.220 ug/L 03/30/15 15:00 1Methylene Chloride <0.220
10.0 0.810 ug/L 03/30/15 15:00 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/30/15 15:00 1Styrene<0.280
1.00 0.150 ug/L 03/30/15 15:00 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/30/15 15:00 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/30/15 15:00 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/30/15 15:00 1Tetrahydrofuran<0.820 *
1.00 0.170 ug/L 03/30/15 15:00 1Toluene<0.170
5.00 0.460 ug/L 03/30/15 15:00 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/30/15 15:00 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/30/15 15:00 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/30/15 15:00 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/30/15 15:00 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/30/15 15:00 1Trichloroethene<0.200
1.00 0.210 ug/L 03/30/15 15:00 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/30/15 15:00 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/30/15 15:00 1Vinyl acetate <1.71 *
1.00 0.180 ug/L 03/30/15 15:00 1Vinyl chloride <0.180
2.00 0.380 ug/L 03/30/15 15:00 1Xylenes, Total <0.380
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Client Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-74829-11Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 03/18/15 01:00
Date Received: 03/20/15 08:40
4-Bromofluorobenzene (Surr)100 70-130 03/30/15 15:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 03/30/15 15:00 170-130
1,2-Dichloroethane-d4 (Surr)96 03/30/15 15:00 170-130
Toluene-d8 (Surr)102 03/30/15 15:00 170-130
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-237281/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/28/15 19:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 03/28/15 19:22 1Acrylonitrile
<0.200 0.2001.00 ug/L 03/28/15 19:22 1Benzene
<0.150 0.1501.00 ug/L 03/28/15 19:22 1Bromochloromethane
<0.170 0.1701.00 ug/L 03/28/15 19:22 1Bromodichloromethane
<0.290 0.2901.00 ug/L 03/28/15 19:22 1Bromoform
<0.350 0.3501.00 ug/L 03/28/15 19:22 1Bromomethane
<2.64 2.6450.0 ug/L 03/28/15 19:22 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 03/28/15 19:22 1Carbon disulfide
<0.180 0.1801.00 ug/L 03/28/15 19:22 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 03/28/15 19:22 1Chlorobenzene
<0.360 0.3601.00 ug/L 03/28/15 19:22 1Chloroethane
<0.230 0.2301.00 ug/L 03/28/15 19:22 1Chloroform
<0.360 0.3601.00 ug/L 03/28/15 19:22 1Chloromethane
<0.210 0.2101.00 ug/L 03/28/15 19:22 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/28/15 19:22 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 03/28/15 19:22 1Dibromochloromethane
<0.940 0.94010.0 ug/L 03/28/15 19:22 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 03/28/15 19:22 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 03/28/15 19:22 1Dibromomethane
<0.190 0.1901.00 ug/L 03/28/15 19:22 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 03/28/15 19:22 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 03/28/15 19:22 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 03/28/15 19:22 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 03/28/15 19:22 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 03/28/15 19:22 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 03/28/15 19:22 1Ethylbenzene
<1.28 1.2810.0 ug/L 03/28/15 19:22 12-Hexanone
<1.50 1.5010.0 ug/L 03/28/15 19:22 1Iodomethane
<0.220 0.2205.00 ug/L 03/28/15 19:22 1Methylene Chloride
<0.810 0.81010.0 ug/L 03/28/15 19:22 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 03/28/15 19:22 1Styrene
<0.150 0.1501.00 ug/L 03/28/15 19:22 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 03/28/15 19:22 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 03/28/15 19:22 1Tetrachloroethene
<0.820 0.82010.0 ug/L 03/28/15 19:22 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 03/28/15 19:22 1Toluene
<0.460 0.4605.00 ug/L 03/28/15 19:22 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 03/28/15 19:22 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/28/15 19:22 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 03/28/15 19:22 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 03/28/15 19:22 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 03/28/15 19:22 1Trichloroethene
<0.210 0.2101.00 ug/L 03/28/15 19:22 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 03/28/15 19:22 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 03/28/15 19:22 1Vinyl acetate
<0.180 0.1801.00 ug/L 03/28/15 19:22 1Vinyl chloride
<0.380 0.3802.00 ug/L 03/28/15 19:22 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-237281/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
4-Bromofluorobenzene (Surr)101 70-130 03/28/15 19:22 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
100 03/28/15 19:22 1Dibromofluoromethane (Surr)70-130
95 03/28/15 19:22 11,2-Dichloroethane-d4 (Surr)70-130
100 03/28/15 19:22 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-237281/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
Acetone 250 250.7 ug/L 100 54 -145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 467.8 ug/L 94 61 -140
Benzene 50.0 49.15 ug/L 98 80 -121
Bromochloromethane 50.0 48.74 ug/L 97 78 -129
Bromodichloromethane 50.0 50.93 ug/L 102 75 -129
Bromoform 50.0 46.01 ug/L 92 46 -145
Bromomethane 50.0 50.76 ug/L 102 41 -150
2-Butanone (MEK)250 237.4 ug/L 95 62 -133
Carbon disulfide 50.0 52.07 ug/L 104 77 -126
Carbon tetrachloride 50.0 55.31 ug/L 111 64 -147
Chlorobenzene 50.0 47.85 ug/L 96 80 -120
Chloroethane 50.0 51.37 ug/L 103 72 -120
Chloroform 50.0 55.84 ug/L 112 73 -129
Chloromethane 50.0 50.43 ug/L 101 12 -150
cis-1,2-Dichloroethene 50.0 55.14 ug/L 110 76 -125
cis-1,3-Dichloropropene 50.0 52.16 ug/L 104 74 -140
Dibromochloromethane 50.0 52.27 ug/L 105 69 -133
1,2-Dibromo-3-Chloropropane 50.0 50.74 ug/L 101 54 -125
1,2-Dibromoethane (EDB)50.0 48.56 ug/L 97 80 -129
Dibromomethane 50.0 49.82 ug/L 100 71 -125
1,2-Dichlorobenzene 50.0 48.24 ug/L 96 80 -121
1,4-Dichlorobenzene 50.0 46.68 ug/L 93 80 -120
1,1-Dichloroethane 50.0 54.34 ug/L 109 78 -125
1,2-Dichloroethane 50.0 56.09 ug/L 112 77 -121
1,1-Dichloroethene 50.0 49.42 ug/L 99 79 -124
1,2-Dichloropropane 50.0 51.14 ug/L 102 75 -120
Ethylbenzene 50.0 49.20 ug/L 98 80 -130
2-Hexanone 250 239.3 ug/L 96 60 -142
Iodomethane 50.0 55.87 ug/L 112 40 -150
Methylene Chloride 50.0 48.98 ug/L 98 79 -123
4-Methyl-2-pentanone (MIBK)250 231.6 ug/L 93 60 -137
Styrene 50.0 50.04 ug/L 100 80 -127
1,1,1,2-Tetrachloroethane 50.0 50.63 ug/L 101 74 -135
1,1,2,2-Tetrachloroethane 50.0 42.61 ug/L 85 69 -131
Tetrachloroethene 50.0 51.56 ug/L 103 80 -126
Tetrahydrofuran 100 101.5 ug/L 101 51 -124
Toluene 50.0 47.94 ug/L 96 80 -126
trans-1,4-Dichloro-2-butene 50.0 50.63 ug/L 101 41 -147
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-237281/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
trans-1,2-Dichloroethene 50.0 55.88 ug/L 112 79 -126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
trans-1,3-Dichloropropene 50.0 55.22 ug/L 110 63 -134
1,1,1-Trichloroethane 50.0 51.61 ug/L 103 78 -135
1,1,2-Trichloroethane 50.0 47.95 ug/L 96 80 -124
Trichloroethene 50.0 50.42 ug/L 101 80 -123
Trichlorofluoromethane 50.0 51.61 ug/L 103 65 -124
1,2,3-Trichloropropane 50.0 42.61 ug/L 85 70 -131
Vinyl acetate 100 207.7 *ug/L 208 54 -139
Vinyl chloride 50.0 51.87 ug/L 104 68 -120
Xylenes, Total 100 100.2 ug/L 100 80 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-237281/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
Acetone 250 250.0 ug/L 100 54 -145 0 21
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 500 471.1 ug/L 94 61 -140 1 18
Benzene 50.0 50.25 ug/L 100 80 -121 2 17
Bromochloromethane 50.0 49.72 ug/L 99 78 -129 2 17
Bromodichloromethane 50.0 51.50 ug/L 103 75 -129 1 18
Bromoform 50.0 47.10 ug/L 94 46 -145 2 16
Bromomethane 50.0 52.60 ug/L 105 41 -150 4 50
2-Butanone (MEK)250 232.3 ug/L 93 62 -133 2 19
Carbon disulfide 50.0 51.65 ug/L 103 77 -126 1 21
Carbon tetrachloride 50.0 56.37 ug/L 113 64 -147 2 19
Chlorobenzene 50.0 48.96 ug/L 98 80 -120 2 14
Chloroethane 50.0 51.78 ug/L 104 72 -120 1 20
Chloroform 50.0 56.95 ug/L 114 73 -129 2 18
Chloromethane 50.0 53.22 ug/L 106 12 -150 5 31
cis-1,2-Dichloroethene 50.0 55.82 ug/L 112 76 -125 1 17
cis-1,3-Dichloropropene 50.0 52.79 ug/L 106 74 -140 1 15
Dibromochloromethane 50.0 51.40 ug/L 103 69 -133 2 15
1,2-Dibromo-3-Chloropropane 50.0 51.72 ug/L 103 54 -125 2 24
1,2-Dibromoethane (EDB)50.0 49.32 ug/L 99 80 -129 2 15
Dibromomethane 50.0 50.54 ug/L 101 71 -125 1 16
1,2-Dichlorobenzene 50.0 48.55 ug/L 97 80 -121 1 15
1,4-Dichlorobenzene 50.0 47.28 ug/L 95 80 -120 1 15
1,1-Dichloroethane 50.0 55.25 ug/L 110 78 -125 2 17
1,2-Dichloroethane 50.0 57.56 ug/L 115 77 -121 3 17
1,1-Dichloroethene 50.0 50.12 ug/L 100 79 -124 1 17
1,2-Dichloropropane 50.0 50.42 ug/L 101 75 -120 1 17
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-237281/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
Ethylbenzene 50.0 49.79 ug/L 100 80 -130 1 15
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2-Hexanone 250 248.2 ug/L 99 60 -142 4 15
Iodomethane 50.0 57.56 ug/L 115 40 -150 3 23
Methylene Chloride 50.0 52.09 ug/L 104 79 -123 6 17
4-Methyl-2-pentanone (MIBK)250 233.9 ug/L 94 60 -137 1 17
Styrene 50.0 50.01 ug/L 100 80 -127 0 24
1,1,1,2-Tetrachloroethane 50.0 50.92 ug/L 102 74 -135 1 16
1,1,2,2-Tetrachloroethane 50.0 43.46 ug/L 87 69 -131 2 20
Tetrachloroethene 50.0 51.34 ug/L 103 80 -126 0 16
Tetrahydrofuran 100 100.3 ug/L 100 51 -124 1 18
Toluene 50.0 48.15 ug/L 96 80 -126 0 15
trans-1,4-Dichloro-2-butene 50.0 52.52 ug/L 105 41 -147 4 26
trans-1,2-Dichloroethene 50.0 56.57 ug/L 113 79 -126 1 16
trans-1,3-Dichloropropene 50.0 55.82 ug/L 112 63 -134 1 14
1,1,1-Trichloroethane 50.0 52.73 ug/L 105 78 -135 2 17
1,1,2-Trichloroethane 50.0 47.02 ug/L 94 80 -124 2 15
Trichloroethene 50.0 48.41 ug/L 97 80 -123 4 17
Trichlorofluoromethane 50.0 52.36 ug/L 105 65 -124 1 18
1,2,3-Trichloropropane 50.0 44.83 ug/L 90 70 -131 5 19
Vinyl acetate 100 207.9 *ug/L 208 54 -139 0 21
Vinyl chloride 50.0 51.94 ug/L 104 68 -120 0 17
Xylenes, Total 100 100.1 ug/L 100 80 -132 0 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
LCSD LCSD
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
951,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-74984-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
Acetone <2.66 250 193.6 ug/L 77 45 -141
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 407.4 ug/L 81 50 -148
Benzene <0.200 50.0 46.18 ug/L 92 75 -133
Bromochloromethane <0.150 50.0 44.18 ug/L 88 67 -139
Bromodichloromethane <0.170 50.0 47.33 ug/L 95 70 -140
Bromoform <0.290 50.0 41.93 ug/L 84 42 -147
Bromomethane <0.350 50.0 44.57 ug/L 89 16 -163
2-Butanone (MEK)<2.64 250 197.5 ug/L 79 50 -138
Carbon disulfide <0.220 50.0 40.30 ug/L 81 48 -152
Carbon tetrachloride <0.180 50.0 50.50 ug/L 101 62 -164
Chlorobenzene 0.841 J 50.0 45.26 ug/L 89 80 -129
Chloroethane <0.360 50.0 50.71 ug/L 101 58 -137
Chloroform <0.230 50.0 52.92 ug/L 106 66 -138
Chloromethane <0.360 50.0 53.54 ug/L 107 10 -169
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-74984-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
cis-1,2-Dichloroethene 3.13 50.0 55.43 ug/L 105 68 -138
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
cis-1,3-Dichloropropene <0.170 50.0 46.82 ug/L 94 71 -141
Dibromochloromethane <0.250 50.0 45.37 ug/L 91 66 -140
1,2-Dibromo-3-Chloropropane <0.940 50.0 44.53 ug/L 89 52 -126
1,2-Dibromoethane (EDB)<0.210 50.0 42.53 ug/L 85 75 -137
Dibromomethane <0.450 50.0 45.78 ug/L 92 58 -140
1,2-Dichlorobenzene 0.246 J 50.0 44.02 ug/L 88 79 -128
1,4-Dichlorobenzene 3.40 50.0 45.28 ug/L 84 78 -126
1,1-Dichloroethane 1.50 50.0 53.05 ug/L 103 71 -139
1,2-Dichloroethane <0.200 50.0 52.30 ug/L 105 64 -136
1,1-Dichloroethene <0.250 50.0 45.98 ug/L 92 70 -142
1,2-Dichloropropane <0.250 50.0 47.89 ug/L 96 67 -131
Ethylbenzene <0.190 50.0 45.63 ug/L 91 79 -139
2-Hexanone <1.28 F2 250 202.1 ug/L 81 50 -150
Iodomethane <1.50 50.0 45.31 ug/L 91 34 -191
Methylene Chloride <0.220 50.0 45.04 ug/L 90 64 -139
4-Methyl-2-pentanone (MIBK)<0.810 F2 250 192.9 ug/L 77 50 -147
Styrene <0.280 50.0 46.63 ug/L 93 61 -148
1,1,1,2-Tetrachloroethane <0.150 50.0 46.07 ug/L 92 73 -141
1,1,2,2-Tetrachloroethane <0.190 50.0 37.23 ug/L 74 56 -143
Tetrachloroethene <0.140 50.0 47.17 ug/L 94 72 -145
Tetrahydrofuran <0.820 F2 100 89.22 ug/L 89 34 -133
Toluene <0.170 50.0 43.42 ug/L 87 75 -136
trans-1,4-Dichloro-2-butene <0.460 50.0 43.53 ug/L 87 29 -156
trans-1,2-Dichloroethene <0.230 50.0 50.19 ug/L 100 66 -143
trans-1,3-Dichloropropene <0.170 50.0 49.89 ug/L 100 59 -135
1,1,1-Trichloroethane <0.190 50.0 50.45 ug/L 101 76 -149
1,1,2-Trichloroethane <0.190 50.0 41.88 ug/L 84 74 -134
Trichloroethene 0.309 J 50.0 47.16 ug/L 94 73 -144
Trichlorofluoromethane <0.210 50.0 55.69 ug/L 111 58 -139
1,2,3-Trichloropropane <0.230 F2 50.0 37.18 ug/L 74 53 -144
Vinyl acetate <1.71 * F1 100 187.5 F1 ug/L 188 37 -154
Vinyl chloride <0.180 50.0 52.51 ug/L 105 56 -129
Xylenes, Total <0.380 100 94.67 ug/L 95 74 -141
4-Bromofluorobenzene (Surr)70 -130
Surrogate
104
MS MS
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
921,2-Dichloroethane-d4 (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-74984-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
Acetone <2.66 250 236.3 ug/L 95 45 -141 20 21
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 480.0 ug/L 96 50 -148 16 18
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-74984-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
Benzene <0.200 50.0 48.69 ug/L 97 75 -133 5 17
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromochloromethane <0.150 50.0 49.41 ug/L 99 67 -139 11 17
Bromodichloromethane <0.170 50.0 51.92 ug/L 104 70 -140 9 18
Bromoform <0.290 50.0 46.67 ug/L 93 42 -147 11 16
Bromomethane <0.350 50.0 52.03 ug/L 104 16 -163 15 50
2-Butanone (MEK)<2.64 250 236.1 ug/L 94 50 -138 18 19
Carbon disulfide <0.220 50.0 42.12 ug/L 84 48 -152 4 21
Carbon tetrachloride <0.180 50.0 54.19 ug/L 108 62 -164 7 19
Chlorobenzene 0.841 J 50.0 49.04 ug/L 96 80 -129 8 14
Chloroethane <0.360 50.0 53.89 ug/L 108 58 -137 6 20
Chloroform <0.230 50.0 57.04 ug/L 114 66 -138 7 18
Chloromethane <0.360 50.0 57.15 ug/L 114 10 -169 7 31
cis-1,2-Dichloroethene 3.13 50.0 58.91 ug/L 112 68 -138 6 17
cis-1,3-Dichloropropene <0.170 50.0 52.77 ug/L 106 71 -141 12 15
Dibromochloromethane <0.250 50.0 51.60 ug/L 103 66 -140 13 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 51.65 ug/L 103 52 -126 15 24
1,2-Dibromoethane (EDB)<0.210 50.0 49.35 ug/L 99 75 -137 15 15
Dibromomethane <0.450 50.0 50.22 ug/L 100 58 -140 9 16
1,2-Dichlorobenzene 0.246 J 50.0 47.64 ug/L 95 79 -128 8 15
1,4-Dichlorobenzene 3.40 50.0 48.98 ug/L 91 78 -126 8 15
1,1-Dichloroethane 1.50 50.0 56.70 ug/L 110 71 -139 7 17
1,2-Dichloroethane <0.200 50.0 57.08 ug/L 114 64 -136 9 17
1,1-Dichloroethene <0.250 50.0 47.65 ug/L 95 70 -142 4 17
1,2-Dichloropropane <0.250 50.0 48.98 ug/L 98 67 -131 2 17
Ethylbenzene <0.190 50.0 48.53 ug/L 97 79 -139 6 15
2-Hexanone <1.28 F2 250 242.5 F2 ug/L 97 50 -150 18 15
Iodomethane <1.50 50.0 52.02 ug/L 104 34 -191 14 23
Methylene Chloride <0.220 50.0 48.41 ug/L 97 64 -139 7 17
4-Methyl-2-pentanone (MIBK)<0.810 F2 250 241.0 F2 ug/L 96 50 -147 22 17
Styrene <0.280 50.0 49.07 ug/L 98 61 -148 5 24
1,1,1,2-Tetrachloroethane <0.150 50.0 50.85 ug/L 102 73 -141 10 16
1,1,2,2-Tetrachloroethane <0.190 50.0 44.27 ug/L 89 56 -143 17 20
Tetrachloroethene <0.140 50.0 49.34 ug/L 99 72 -145 4 16
Tetrahydrofuran <0.820 F2 100 111.8 F2 ug/L 112 34 -133 22 18
Toluene <0.170 50.0 46.02 ug/L 92 75 -136 6 15
trans-1,4-Dichloro-2-butene <0.460 50.0 53.41 ug/L 107 29 -156 20 26
trans-1,2-Dichloroethene <0.230 50.0 53.41 ug/L 107 66 -143 6 16
trans-1,3-Dichloropropene <0.170 50.0 55.49 ug/L 111 59 -135 11 14
1,1,1-Trichloroethane <0.190 50.0 52.67 ug/L 105 76 -149 4 17
1,1,2-Trichloroethane <0.190 50.0 46.78 ug/L 94 74 -134 11 15
Trichloroethene 0.309 J 50.0 48.06 ug/L 96 73 -144 2 17
Trichlorofluoromethane <0.210 50.0 59.80 ug/L 120 58 -139 7 18
1,2,3-Trichloropropane <0.230 F2 50.0 46.96 F2 ug/L 94 53 -144 23 19
Vinyl acetate <1.71 * F1 100 212.4 F1 ug/L 212 37 -154 12 21
Vinyl chloride <0.180 50.0 54.00 ug/L 108 56 -129 3 17
Xylenes, Total <0.380 100 97.08 ug/L 97 74 -141 3 15
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-74984-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237281
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
MSD MSD
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
961,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 490-237488/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/30/15 14:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 03/30/15 14:32 1Acrylonitrile
<0.200 0.2001.00 ug/L 03/30/15 14:32 1Benzene
<0.150 0.1501.00 ug/L 03/30/15 14:32 1Bromochloromethane
<0.170 0.1701.00 ug/L 03/30/15 14:32 1Bromodichloromethane
<0.290 0.2901.00 ug/L 03/30/15 14:32 1Bromoform
<0.350 0.3501.00 ug/L 03/30/15 14:32 1Bromomethane
<2.64 2.6450.0 ug/L 03/30/15 14:32 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 03/30/15 14:32 1Carbon disulfide
<0.180 0.1801.00 ug/L 03/30/15 14:32 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 03/30/15 14:32 1Chlorobenzene
<0.360 0.3601.00 ug/L 03/30/15 14:32 1Chloroethane
<0.230 0.2301.00 ug/L 03/30/15 14:32 1Chloroform
<0.360 0.3601.00 ug/L 03/30/15 14:32 1Chloromethane
<0.210 0.2101.00 ug/L 03/30/15 14:32 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/30/15 14:32 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 03/30/15 14:32 1Dibromochloromethane
<0.940 0.94010.0 ug/L 03/30/15 14:32 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 03/30/15 14:32 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 03/30/15 14:32 1Dibromomethane
<0.190 0.1901.00 ug/L 03/30/15 14:32 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 03/30/15 14:32 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 03/30/15 14:32 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 03/30/15 14:32 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 03/30/15 14:32 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 03/30/15 14:32 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 03/30/15 14:32 1Ethylbenzene
<1.28 1.2810.0 ug/L 03/30/15 14:32 12-Hexanone
<1.50 1.5010.0 ug/L 03/30/15 14:32 1Iodomethane
0.2233 J 0.2205.00 ug/L 03/30/15 14:32 1Methylene Chloride
<0.810 0.81010.0 ug/L 03/30/15 14:32 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 03/30/15 14:32 1Styrene
<0.150 0.1501.00 ug/L 03/30/15 14:32 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 03/30/15 14:32 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 03/30/15 14:32 1Tetrachloroethene
<0.820 0.82010.0 ug/L 03/30/15 14:32 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 03/30/15 14:32 1Toluene
<0.460 0.4605.00 ug/L 03/30/15 14:32 1trans-1,4-Dichloro-2-butene
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-237488/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
RL MDL
trans-1,2-Dichloroethene <0.230 1.00 0.230 ug/L 03/30/15 14:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.170 0.1701.00 ug/L 03/30/15 14:32 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 03/30/15 14:32 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 03/30/15 14:32 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 03/30/15 14:32 1Trichloroethene
<0.210 0.2101.00 ug/L 03/30/15 14:32 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 03/30/15 14:32 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 03/30/15 14:32 1Vinyl acetate
<0.180 0.1801.00 ug/L 03/30/15 14:32 1Vinyl chloride
<0.380 0.3802.00 ug/L 03/30/15 14:32 1Xylenes, Total
4-Bromofluorobenzene (Surr)99 70-130 03/30/15 14:32 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
103 03/30/15 14:32 1Dibromofluoromethane (Surr)70-130
96 03/30/15 14:32 11,2-Dichloroethane-d4 (Surr)70-130
100 03/30/15 14:32 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-237488/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
Acetone 250 275.2 ug/L 110 54 -145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 517.3 ug/L 103 61 -140
Benzene 50.0 51.52 ug/L 103 80 -121
Bromochloromethane 50.0 52.82 ug/L 106 78 -129
Bromodichloromethane 50.0 52.32 ug/L 105 75 -129
Bromoform 50.0 51.25 ug/L 102 46 -145
Bromomethane 50.0 54.49 ug/L 109 41 -150
2-Butanone (MEK)250 253.5 ug/L 101 62 -133
Carbon disulfide 50.0 52.30 ug/L 105 77 -126
Carbon tetrachloride 50.0 56.80 ug/L 114 64 -147
Chlorobenzene 50.0 49.12 ug/L 98 80 -120
Chloroethane 50.0 55.51 ug/L 111 72 -120
Chloroform 50.0 58.68 ug/L 117 73 -129
Chloromethane 50.0 61.17 ug/L 122 12 -150
cis-1,2-Dichloroethene 50.0 58.28 ug/L 117 76 -125
cis-1,3-Dichloropropene 50.0 54.80 ug/L 110 74 -140
Dibromochloromethane 50.0 54.63 ug/L 109 69 -133
1,2-Dibromo-3-Chloropropane 50.0 58.40 ug/L 117 54 -125
1,2-Dibromoethane (EDB)50.0 51.59 ug/L 103 80 -129
Dibromomethane 50.0 53.11 ug/L 106 71 -125
1,2-Dichlorobenzene 50.0 50.53 ug/L 101 80 -121
1,4-Dichlorobenzene 50.0 48.12 ug/L 96 80 -120
1,1-Dichloroethane 50.0 57.32 ug/L 115 78 -125
1,2-Dichloroethane 50.0 60.16 ug/L 120 77 -121
1,1-Dichloroethene 50.0 49.54 ug/L 99 79 -124
1,2-Dichloropropane 50.0 51.54 ug/L 103 75 -120
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-237488/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
Ethylbenzene 50.0 49.49 ug/L 99 80 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
2-Hexanone 250 269.3 ug/L 108 60 -142
Iodomethane 50.0 58.58 ug/L 117 40 -150
Methylene Chloride 50.0 53.27 ug/L 107 79 -123
4-Methyl-2-pentanone (MIBK)250 254.4 ug/L 102 60 -137
Styrene 50.0 50.89 ug/L 102 80 -127
1,1,1,2-Tetrachloroethane 50.0 52.96 ug/L 106 74 -135
1,1,2,2-Tetrachloroethane 50.0 48.39 ug/L 97 69 -131
Tetrachloroethene 50.0 51.24 ug/L 102 80 -126
Tetrahydrofuran 100 126.4 *ug/L 126 51 -124
Toluene 50.0 47.78 ug/L 96 80 -126
trans-1,4-Dichloro-2-butene 50.0 57.75 ug/L 116 41 -147
trans-1,2-Dichloroethene 50.0 56.79 ug/L 114 79 -126
trans-1,3-Dichloropropene 50.0 59.33 ug/L 119 63 -134
1,1,1-Trichloroethane 50.0 54.09 ug/L 108 78 -135
1,1,2-Trichloroethane 50.0 50.06 ug/L 100 80 -124
Trichloroethene 50.0 50.21 ug/L 100 80 -123
Trichlorofluoromethane 50.0 55.40 ug/L 111 65 -124
1,2,3-Trichloropropane 50.0 47.82 ug/L 96 70 -131
Vinyl acetate 100 228.2 *ug/L 228 54 -139
Vinyl chloride 50.0 55.08 ug/L 110 68 -120
Xylenes, Total 100 100.2 ug/L 100 80 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
1001,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-237488/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
Acetone 250 268.6 ug/L 107 54 -145 2 21
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 500 487.6 ug/L 98 61 -140 6 18
Benzene 50.0 47.46 ug/L 95 80 -121 8 17
Bromochloromethane 50.0 48.86 ug/L 98 78 -129 8 17
Bromodichloromethane 50.0 50.46 ug/L 101 75 -129 4 18
Bromoform 50.0 48.05 ug/L 96 46 -145 6 16
Bromomethane 50.0 51.25 ug/L 102 41 -150 6 50
2-Butanone (MEK)250 238.0 ug/L 95 62 -133 6 19
Carbon disulfide 50.0 47.87 ug/L 96 77 -126 9 21
Carbon tetrachloride 50.0 50.92 ug/L 102 64 -147 11 19
Chlorobenzene 50.0 46.86 ug/L 94 80 -120 5 14
Chloroethane 50.0 48.99 ug/L 98 72 -120 12 20
Chloroform 50.0 54.40 ug/L 109 73 -129 8 18
Chloromethane 50.0 54.31 ug/L 109 12 -150 12 31
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-237488/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
cis-1,2-Dichloroethene 50.0 53.81 ug/L 108 76 -125 8 17
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
cis-1,3-Dichloropropene 50.0 52.31 ug/L 105 74 -140 5 15
Dibromochloromethane 50.0 52.55 ug/L 105 69 -133 4 15
1,2-Dibromo-3-Chloropropane 50.0 54.05 ug/L 108 54 -125 8 24
1,2-Dibromoethane (EDB)50.0 50.12 ug/L 100 80 -129 3 15
Dibromomethane 50.0 49.98 ug/L 100 71 -125 6 16
1,2-Dichlorobenzene 50.0 47.06 ug/L 94 80 -121 7 15
1,4-Dichlorobenzene 50.0 45.21 ug/L 90 80 -120 6 15
1,1-Dichloroethane 50.0 52.33 ug/L 105 78 -125 9 17
1,2-Dichloroethane 50.0 55.85 ug/L 112 77 -121 7 17
1,1-Dichloroethene 50.0 45.90 ug/L 92 79 -124 8 17
1,2-Dichloropropane 50.0 49.86 ug/L 100 75 -120 3 17
Ethylbenzene 50.0 47.78 ug/L 96 80 -130 4 15
2-Hexanone 250 259.1 ug/L 104 60 -142 4 15
Iodomethane 50.0 54.53 ug/L 109 40 -150 7 23
Methylene Chloride 50.0 49.49 ug/L 99 79 -123 7 17
4-Methyl-2-pentanone (MIBK)250 244.8 ug/L 98 60 -137 4 17
Styrene 50.0 49.74 ug/L 99 80 -127 2 24
1,1,1,2-Tetrachloroethane 50.0 50.78 ug/L 102 74 -135 4 16
1,1,2,2-Tetrachloroethane 50.0 43.78 ug/L 88 69 -131 10 20
Tetrachloroethene 50.0 49.36 ug/L 99 80 -126 4 16
Tetrahydrofuran 100 115.4 ug/L 115 51 -124 9 18
Toluene 50.0 46.18 ug/L 92 80 -126 3 15
trans-1,4-Dichloro-2-butene 50.0 52.44 ug/L 105 41 -147 10 26
trans-1,2-Dichloroethene 50.0 53.06 ug/L 106 79 -126 7 16
trans-1,3-Dichloropropene 50.0 57.12 ug/L 114 63 -134 4 14
1,1,1-Trichloroethane 50.0 49.97 ug/L 100 78 -135 8 17
1,1,2-Trichloroethane 50.0 47.39 ug/L 95 80 -124 5 15
Trichloroethene 50.0 47.16 ug/L 94 80 -123 6 17
Trichlorofluoromethane 50.0 51.95 ug/L 104 65 -124 6 18
1,2,3-Trichloropropane 50.0 44.21 ug/L 88 70 -131 8 19
Vinyl acetate 100 211.4 *ug/L 211 54 -139 8 21
Vinyl chloride 50.0 50.80 ug/L 102 68 -120 8 17
Xylenes, Total 100 97.64 ug/L 98 80 -132 3 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
99Dibromofluoromethane (Surr)70 -130
941,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-74865-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
Acetone 16.8 J 250 218.6 ug/L 81 45 -141
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 425.2 ug/L 85 50 -148
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-74865-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
Benzene 1.07 50.0 50.59 ug/L 99 75 -133
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Bromochloromethane <0.150 50.0 46.35 ug/L 93 67 -139
Bromodichloromethane <0.170 50.0 47.98 ug/L 96 70 -140
Bromoform <0.290 50.0 44.54 ug/L 89 42 -147
Bromomethane <0.350 50.0 44.01 ug/L 88 16 -163
2-Butanone (MEK)<2.64 250 207.9 ug/L 83 50 -138
Carbon disulfide 0.224 J 50.0 49.05 ug/L 98 48 -152
Carbon tetrachloride <0.180 50.0 55.69 ug/L 111 62 -164
Chlorobenzene <0.180 50.0 46.97 ug/L 94 80 -129
Chloroethane <0.360 50.0 49.58 ug/L 99 58 -137
Chloroform <0.230 50.0 55.54 ug/L 111 66 -138
Chloromethane <0.360 50.0 51.10 ug/L 102 10 -169
cis-1,2-Dichloroethene <0.210 50.0 53.09 ug/L 106 68 -138
cis-1,3-Dichloropropene <0.170 50.0 50.33 ug/L 101 71 -141
Dibromochloromethane <0.250 50.0 50.27 ug/L 101 66 -140
1,2-Dibromo-3-Chloropropane <0.940 50.0 53.37 ug/L 107 52 -126
1,2-Dibromoethane (EDB)<0.210 50.0 46.58 ug/L 93 75 -137
Dibromomethane <0.450 50.0 44.45 ug/L 89 58 -140
1,2-Dichlorobenzene 1.30 50.0 44.45 ug/L 86 79 -128
1,4-Dichlorobenzene <0.170 50.0 43.11 ug/L 86 78 -126
1,1-Dichloroethane <0.240 50.0 52.37 ug/L 105 71 -139
1,2-Dichloroethane <0.200 50.0 53.72 ug/L 107 64 -136
1,1-Dichloroethene <0.250 50.0 48.57 ug/L 97 70 -142
1,2-Dichloropropane <0.250 50.0 48.77 ug/L 98 67 -131
Ethylbenzene 13.8 50.0 60.71 ug/L 94 79 -139
2-Hexanone <1.28 250 292.7 ug/L 117 50 -150
Iodomethane <1.50 50.0 38.94 ug/L 78 34 -191
Methylene Chloride <0.220 50.0 47.62 ug/L 95 64 -139
4-Methyl-2-pentanone (MIBK)<0.810 250 275.2 ug/L 110 50 -147
Styrene <0.280 50.0 49.83 ug/L 100 61 -148
1,1,1,2-Tetrachloroethane <0.150 50.0 49.47 ug/L 99 73 -141
1,1,2,2-Tetrachloroethane <0.190 50.0 41.59 ug/L 83 56 -143
Tetrachloroethene <0.140 50.0 49.16 ug/L 98 72 -145
Tetrahydrofuran <0.820 F2 *100 86.55 ug/L 87 34 -133
Toluene 1.61 50.0 48.00 ug/L 93 75 -136
trans-1,4-Dichloro-2-butene <0.460 50.0 46.72 ug/L 93 29 -156
trans-1,2-Dichloroethene <0.230 50.0 53.21 ug/L 106 66 -143
trans-1,3-Dichloropropene <0.170 50.0 52.99 ug/L 106 59 -135
1,1,1-Trichloroethane <0.190 50.0 52.76 ug/L 106 76 -149
1,1,2-Trichloroethane <0.190 50.0 48.63 ug/L 97 74 -134
Trichloroethene <0.200 50.0 48.14 ug/L 96 73 -144
Trichlorofluoromethane <0.210 50.0 54.06 ug/L 108 58 -139
1,2,3-Trichloropropane <0.230 50.0 42.32 ug/L 85 53 -144
Vinyl acetate <1.71 * F1 100 196.2 F1 ug/L 196 37 -154
Vinyl chloride <0.180 50.0 50.46 ug/L 101 56 -129
Xylenes, Total 202 F1 100 282.4 ug/L 81 74 -141
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-74865-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
MS MS
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-74865-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
Acetone 16.8 J 250 247.6 ug/L 92 45 -141 12 21
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 477.2 ug/L 95 50 -148 12 18
Benzene 1.07 50.0 48.57 ug/L 95 75 -133 4 17
Bromochloromethane <0.150 50.0 47.27 ug/L 95 67 -139 2 17
Bromodichloromethane <0.170 50.0 48.32 ug/L 97 70 -140 1 18
Bromoform <0.290 50.0 46.37 ug/L 93 42 -147 4 16
Bromomethane <0.350 50.0 46.26 ug/L 93 16 -163 5 50
2-Butanone (MEK)<2.64 250 239.2 ug/L 96 50 -138 14 19
Carbon disulfide 0.224 J 50.0 49.24 ug/L 98 48 -152 0 21
Carbon tetrachloride <0.180 50.0 56.49 ug/L 113 62 -164 1 19
Chlorobenzene <0.180 50.0 44.26 ug/L 89 80 -129 6 14
Chloroethane <0.360 50.0 49.80 ug/L 100 58 -137 0 20
Chloroform <0.230 50.0 54.58 ug/L 109 66 -138 2 18
Chloromethane <0.360 50.0 51.38 ug/L 103 10 -169 1 31
cis-1,2-Dichloroethene <0.210 50.0 53.87 ug/L 108 68 -138 1 17
cis-1,3-Dichloropropene <0.170 50.0 47.19 ug/L 94 71 -141 6 15
Dibromochloromethane <0.250 50.0 49.58 ug/L 99 66 -140 1 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 54.44 ug/L 109 52 -126 2 24
1,2-Dibromoethane (EDB)<0.210 50.0 46.98 ug/L 94 75 -137 1 15
Dibromomethane <0.450 50.0 46.87 ug/L 94 58 -140 5 16
1,2-Dichlorobenzene 1.30 50.0 42.51 ug/L 82 79 -128 4 15
1,4-Dichlorobenzene <0.170 50.0 40.29 ug/L 81 78 -126 7 15
1,1-Dichloroethane <0.240 50.0 53.36 ug/L 107 71 -139 2 17
1,2-Dichloroethane <0.200 50.0 56.74 ug/L 113 64 -136 5 17
1,1-Dichloroethene <0.250 50.0 49.53 ug/L 99 70 -142 2 17
1,2-Dichloropropane <0.250 50.0 47.39 ug/L 95 67 -131 3 17
Ethylbenzene 13.8 50.0 56.99 ug/L 86 79 -139 6 15
2-Hexanone <1.28 250 305.9 ug/L 122 50 -150 4 15
Iodomethane <1.50 50.0 41.23 ug/L 82 34 -191 6 23
Methylene Chloride <0.220 50.0 48.51 ug/L 97 64 -139 2 17
4-Methyl-2-pentanone (MIBK)<0.810 250 283.9 ug/L 114 50 -147 3 17
Styrene <0.280 50.0 47.21 ug/L 94 61 -148 5 24
1,1,1,2-Tetrachloroethane <0.150 50.0 47.57 ug/L 95 73 -141 4 16
1,1,2,2-Tetrachloroethane <0.190 50.0 42.24 ug/L 84 56 -143 2 20
Tetrachloroethene <0.140 50.0 46.78 ug/L 94 72 -145 5 16
Tetrahydrofuran <0.820 F2 *100 116.8 F2 ug/L 117 34 -133 30 18
Toluene 1.61 50.0 44.48 ug/L 86 75 -136 8 15
trans-1,4-Dichloro-2-butene <0.460 50.0 50.86 ug/L 102 29 -156 8 26
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-74865-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 237488
trans-1,2-Dichloroethene <0.230 50.0 53.32 ug/L 107 66 -143 0 16
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
trans-1,3-Dichloropropene <0.170 50.0 53.26 ug/L 107 59 -135 1 14
1,1,1-Trichloroethane <0.190 50.0 51.08 ug/L 102 76 -149 3 17
1,1,2-Trichloroethane <0.190 50.0 49.18 ug/L 98 74 -134 1 15
Trichloroethene <0.200 50.0 46.76 ug/L 94 73 -144 3 17
Trichlorofluoromethane <0.210 50.0 49.50 ug/L 99 58 -139 9 18
1,2,3-Trichloropropane <0.230 50.0 43.89 ug/L 88 53 -144 4 19
Vinyl acetate <1.71 * F1 100 214.9 F1 ug/L 215 37 -154 9 21
Vinyl chloride <0.180 50.0 50.72 ug/L 101 56 -129 1 17
Xylenes, Total 202 F1 100 270.2 F1 ug/L 69 74 -141 4 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
MSD MSD
Qualifier Limits%Recovery
110Dibromofluoromethane (Surr)70 -130
1051,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Method: 6010C - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-236173/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236833 Prep Batch: 236173
RL MDL
Antimony <0.00500 0.0100 0.00500 mg/L 03/25/15 09:14 03/26/15 20:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00720 0.007200.0100 mg/L 03/25/15 09:14 03/26/15 20:15 1Arsenic
<0.00500 0.005000.0100 mg/L 03/25/15 09:14 03/26/15 20:15 1Barium
<0.000500 0.0005000.00100 mg/L 03/25/15 09:14 03/26/15 20:15 1Cadmium
<0.00300 0.003000.00500 mg/L 03/25/15 09:14 03/26/15 20:15 1Chromium
<0.00500 0.005000.0100 mg/L 03/25/15 09:14 03/26/15 20:15 1Cobalt
<0.00500 0.005000.0100 mg/L 03/25/15 09:14 03/26/15 20:15 1Copper
<0.00200 0.002000.00500 mg/L 03/25/15 09:14 03/26/15 20:15 1Lead
<0.00300 0.003000.0100 mg/L 03/25/15 09:14 03/26/15 20:15 1Nickel
<0.00500 0.005000.0100 mg/L 03/25/15 09:14 03/26/15 20:15 1Selenium
<0.00250 0.002500.00500 mg/L 03/25/15 09:14 03/26/15 20:15 1Silver
<0.0100 0.01000.0200 mg/L 03/25/15 09:14 03/26/15 20:15 1Vanadium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-236173/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236833 Prep Batch: 236173
Antimony 0.100 0.09620 mg/L 96 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 0.0500 0.04740 mg/L 95 80 -120
Barium 2.00 2.018 mg/L 101 80 -120
Cadmium 0.0500 0.04930 mg/L 99 80 -120
Chromium 0.200 0.2042 mg/L 102 80 -120
Cobalt 0.500 0.5038 mg/L 101 80 -120
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 6010C - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-236173/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236833 Prep Batch: 236173
Copper 0.250 0.2510 mg/L 100 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Lead 0.0500 0.05020 mg/L 100 80 -120
Nickel 0.500 0.5015 mg/L 100 80 -120
Selenium 0.0500 0.04680 mg/L 94 80 -120
Silver 0.0500 0.04140 mg/L 83 80 -120
Vanadium 0.500 0.4960 mg/L 99 80 -120
Client Sample ID: MW-01CDLab Sample ID: 490-74829-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236833 Prep Batch: 236173
Antimony <0.00500 0.100 0.09260 mg/L 93 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic <0.00720 0.0500 0.04680 mg/L 94 75 -125
Barium 0.104 2.00 2.417 mg/L 116 75 -125
Cadmium <0.000500 0.0500 0.04960 mg/L 99 75 -125
Chromium <0.00300 0.200 0.2092 mg/L 105 75 -125
Cobalt <0.00500 0.500 0.5094 mg/L 102 75 -125
Copper 0.00830 J 0.250 0.2607 mg/L 101 75 -125
Lead 0.00760 0.0500 0.05950 mg/L 104 75 -125
Nickel <0.00300 0.500 0.5064 mg/L 101 75 -125
Selenium <0.00500 0.0500 0.04670 mg/L 93 75 -125
Silver <0.00250 0.0500 0.04060 mg/L 81 75 -125
Vanadium <0.0100 0.500 0.5164 mg/L 103 75 -125
Client Sample ID: MW-01CDLab Sample ID: 490-74829-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236833 Prep Batch: 236173
Antimony <0.00500 0.100 0.09520 mg/L 95 75 -125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic <0.00720 0.0500 0.04620 mg/L 92 75 -125 1 20
Barium 0.104 2.00 2.443 mg/L 117 75 -125 1 20
Cadmium <0.000500 0.0500 0.05010 mg/L 100 75 -125 1 20
Chromium <0.00300 0.200 0.2124 mg/L 106 75 -125 2 20
Cobalt <0.00500 0.500 0.5146 mg/L 103 75 -125 1 20
Copper 0.00830 J 0.250 0.2626 mg/L 102 75 -125 1 20
Lead 0.00760 0.0500 0.05970 mg/L 104 75 -125 0 20
Nickel <0.00300 0.500 0.5116 mg/L 102 75 -125 1 20
Selenium <0.00500 0.0500 0.04700 mg/L 94 75 -125 1 20
Silver <0.00250 0.0500 0.04190 mg/L 84 75 -125 3 20
Vanadium <0.0100 0.500 0.5219 mg/L 104 75 -125 1 20
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 6020A - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-236178/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236845 Prep Batch: 236178
RL MDL
Beryllium <0.000500 0.00200 0.000500 mg/L 03/25/15 09:14 03/26/15 15:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000200 0.0002000.00200 mg/L 03/25/15 09:14 03/26/15 15:38 1Thallium
<0.0100 0.01000.0250 mg/L 03/25/15 09:14 03/26/15 15:38 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-236178/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236845 Prep Batch: 236178
Beryllium 0.100 0.1166 mg/L 117 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Thallium 0.100 0.1022 mg/L 102 80 -120
Zinc 0.100 0.09909 mg/L 99 80 -120
Client Sample ID: MW-01CDLab Sample ID: 490-74829-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236845 Prep Batch: 236178
Beryllium 0.000597 J 0.100 0.1115 mg/L 111 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Thallium 0.000521 J 0.100 0.09835 mg/L 98 75 -125
Zinc 0.0147 J 0.100 0.1054 mg/L 91 75 -125
Client Sample ID: MW-01CDLab Sample ID: 490-74829-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236845 Prep Batch: 236178
Beryllium 0.000597 J 0.100 0.1098 mg/L 109 75 -125 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Thallium 0.000521 J 0.100 0.09725 mg/L 97 75 -125 1 20
Zinc 0.0147 J 0.100 0.1031 mg/L 88 75 -125 2 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-235776/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236233 Prep Batch: 235776
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/23/15 18:56 03/24/15 18:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-235776/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236230 Prep Batch: 235776
Mercury 1.00 1.043 ug/L 104 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-235776/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236230 Prep Batch: 235776
Mercury 1.00 1.006 ug/L 101 80 -120 4 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-74547-E-12-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236230 Prep Batch: 235776
Mercury <0.150 1.00 1.010 ug/L 101 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-74547-E-12-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236230 Prep Batch: 235776
Mercury <0.150 1.00 1.042 ug/L 104 75 -125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 490-235941/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236233 Prep Batch: 235941
RL MDL
Mercury <0.150 0.200 0.150 ug/L 03/24/15 12:23 03/24/15 19:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-235941/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236233 Prep Batch: 235941
Mercury 1.00 1.080 ug/L 108 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-235941/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236233 Prep Batch: 235941
Mercury 1.00 1.036 ug/L 104 80 -120 4 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-74795-A-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236233 Prep Batch: 235941
Mercury <0.150 1.00 1.087 ug/L 109 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-74795-A-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 236233 Prep Batch: 235941
Mercury <0.150 1.00 1.043 ug/L 104 75 -125 4 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
TestAmerica Nashville
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QC Association Summary
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
GC/MS VOA
Analysis Batch: 237281
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-74829-1 MW-01CD Total/NA
Water 8260B490-74829-2 MW-03CD Total/NA
Water 8260B490-74829-3 MW-1R Total/NA
Water 8260B490-74829-4 MW-2R Total/NA
Water 8260B490-74829-5 MW-2RDUP Total/NA
Water 8260B490-74829-6 MW-3R Total/NA
Water 8260B490-74829-7 SP-1 Total/NA
Water 8260B490-74829-8 SS-1 Total/NA
Water 8260B490-74829-9 SS-2 Total/NA
Water 8260B490-74829-10 MW-02CD Total/NA
Water 8260B490-74984-B-1 MS Matrix Spike Total/NA
Water 8260B490-74984-C-1 MSD Matrix Spike Duplicate Total/NA
Water 8260BLCS 490-237281/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-237281/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-237281/7 Method Blank Total/NA
Analysis Batch: 237488
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-74829-11 Trip Blank Total/NA
Water 8260B490-74865-B-1 MS Matrix Spike Total/NA
Water 8260B490-74865-C-1 MSD Matrix Spike Duplicate Total/NA
Water 8260BLCS 490-237488/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-237488/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-237488/7 Method Blank Total/NA
Metals
Prep Batch: 235776
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-74547-E-12-C MS Matrix Spike Total/NA
Water 7470A490-74547-E-12-D MSD Matrix Spike Duplicate Total/NA
Water 7470A490-74829-1 MW-01CD Total/NA
Water 7470A490-74829-2 MW-03CD Total/NA
Water 7470A490-74829-3 MW-1R Total/NA
Water 7470A490-74829-4 MW-2R Total/NA
Water 7470A490-74829-5 MW-2RDUP Total/NA
Water 7470ALCS 490-235776/2-A Lab Control Sample Total/NA
Water 7470ALCSD 490-235776/3-A Lab Control Sample Dup Total/NA
Water 7470AMB 490-235776/1-A Method Blank Total/NA
Prep Batch: 235941
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-74795-A-1-B MS Matrix Spike Total/NA
Water 7470A490-74795-A-1-C MSD Matrix Spike Duplicate Total/NA
Water 7470A490-74829-6 MW-3R Total/NA
Water 7470A490-74829-7 SP-1 Total/NA
Water 7470A490-74829-8 SS-1 Total/NA
Water 7470A490-74829-9 SS-2 Total/NA
Water 7470A490-74829-10 MW-02CD Total/NA
Water 7470ALCS 490-235941/2-A Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Prep Batch: 235941 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470ALCSD 490-235941/3-A Lab Control Sample Dup Total/NA
Water 7470AMB 490-235941/1-A Method Blank Total/NA
Prep Batch: 236173
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-74829-1 MW-01CD Total/NA
Water 3010A490-74829-1 MS MW-01CD Total/NA
Water 3010A490-74829-1 MSD MW-01CD Total/NA
Water 3010A490-74829-2 MW-03CD Total/NA
Water 3010A490-74829-3 MW-1R Total/NA
Water 3010A490-74829-4 MW-2R Total/NA
Water 3010A490-74829-5 MW-2RDUP Total/NA
Water 3010A490-74829-6 MW-3R Total/NA
Water 3010A490-74829-7 SP-1 Total/NA
Water 3010A490-74829-8 SS-1 Total/NA
Water 3010A490-74829-9 SS-2 Total/NA
Water 3010A490-74829-10 MW-02CD Total/NA
Water 3010ALCS 490-236173/2-A Lab Control Sample Total/NA
Water 3010AMB 490-236173/1-A Method Blank Total/NA
Prep Batch: 236178
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-74829-1 MW-01CD Total/NA
Water 3010A490-74829-1 MS MW-01CD Total/NA
Water 3010A490-74829-1 MSD MW-01CD Total/NA
Water 3010A490-74829-2 MW-03CD Total/NA
Water 3010A490-74829-3 MW-1R Total/NA
Water 3010A490-74829-4 MW-2R Total/NA
Water 3010A490-74829-5 MW-2RDUP Total/NA
Water 3010A490-74829-6 MW-3R Total/NA
Water 3010A490-74829-7 SP-1 Total/NA
Water 3010A490-74829-8 SS-1 Total/NA
Water 3010A490-74829-9 SS-2 Total/NA
Water 3010A490-74829-10 MW-02CD Total/NA
Water 3010ALCS 490-236178/2-A Lab Control Sample Total/NA
Water 3010AMB 490-236178/1-A Method Blank Total/NA
Analysis Batch: 236230
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 235776490-74547-E-12-C MS Matrix Spike Total/NA
Water 7470A 235776490-74547-E-12-D MSD Matrix Spike Duplicate Total/NA
Water 7470A 235776LCS 490-235776/2-A Lab Control Sample Total/NA
Water 7470A 235776LCSD 490-235776/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 236233
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 235941490-74795-A-1-B MS Matrix Spike Total/NA
Water 7470A 235941490-74795-A-1-C MSD Matrix Spike Duplicate Total/NA
Water 7470A 235776490-74829-1 MW-01CD Total/NA
Water 7470A 235776490-74829-2 MW-03CD Total/NA
Water 7470A 235776490-74829-3 MW-1R Total/NA
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QC Association Summary
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Analysis Batch: 236233 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 235776490-74829-4 MW-2R Total/NA
Water 7470A 235776490-74829-5 MW-2RDUP Total/NA
Water 7470A 235941490-74829-6 MW-3R Total/NA
Water 7470A 235941490-74829-7 SP-1 Total/NA
Water 7470A 235941490-74829-8 SS-1 Total/NA
Water 7470A 235941490-74829-9 SS-2 Total/NA
Water 7470A 235941490-74829-10 MW-02CD Total/NA
Water 7470A 235941LCS 490-235941/2-A Lab Control Sample Total/NA
Water 7470A 235941LCSD 490-235941/3-A Lab Control Sample Dup Total/NA
Water 7470A 235776MB 490-235776/1-A Method Blank Total/NA
Water 7470A 235941MB 490-235941/1-A Method Blank Total/NA
Analysis Batch: 236833
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010C 236173490-74829-1 MW-01CD Total/NA
Water 6010C 236173490-74829-1 MS MW-01CD Total/NA
Water 6010C 236173490-74829-1 MSD MW-01CD Total/NA
Water 6010C 236173490-74829-2 MW-03CD Total/NA
Water 6010C 236173490-74829-3 MW-1R Total/NA
Water 6010C 236173490-74829-4 MW-2R Total/NA
Water 6010C 236173490-74829-5 MW-2RDUP Total/NA
Water 6010C 236173490-74829-6 MW-3R Total/NA
Water 6010C 236173490-74829-7 SP-1 Total/NA
Water 6010C 236173490-74829-8 SS-1 Total/NA
Water 6010C 236173490-74829-9 SS-2 Total/NA
Water 6010C 236173490-74829-10 MW-02CD Total/NA
Water 6010C 236173LCS 490-236173/2-A Lab Control Sample Total/NA
Water 6010C 236173MB 490-236173/1-A Method Blank Total/NA
Analysis Batch: 236845
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 236178490-74829-1 MW-01CD Total/NA
Water 6020A 236178490-74829-1 MS MW-01CD Total/NA
Water 6020A 236178490-74829-1 MSD MW-01CD Total/NA
Water 6020A 236178490-74829-2 MW-03CD Total/NA
Water 6020A 236178490-74829-3 MW-1R Total/NA
Water 6020A 236178490-74829-4 MW-2R Total/NA
Water 6020A 236178490-74829-5 MW-2RDUP Total/NA
Water 6020A 236178490-74829-6 MW-3R Total/NA
Water 6020A 236178490-74829-7 SP-1 Total/NA
Water 6020A 236178490-74829-8 SS-1 Total/NA
Water 6020A 236178490-74829-9 SS-2 Total/NA
Water 6020A 236178490-74829-10 MW-02CD Total/NA
Water 6020A 236178LCS 490-236178/2-A Lab Control Sample Total/NA
Water 6020A 236178MB 490-236178/1-A Method Blank Total/NA
TestAmerica Nashville
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-74829-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-01CD Lab Sample ID: 490-74829-1
Matrix: WaterDate Collected: 03/19/15 12:01
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 00:011 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 20:28 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 236178 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 15:48 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235776 03/23/15 18:56 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 18:26 TDP TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-03CD Lab Sample ID: 490-74829-2
Matrix: WaterDate Collected: 03/18/15 11:20
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 00:281 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 20:46 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 236178 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 16:13 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235776 03/23/15 18:56 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 18:28 TDP TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-1R Lab Sample ID: 490-74829-3
Matrix: WaterDate Collected: 03/19/15 10:20
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 00:561 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 20:59 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 236178 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 16:19 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235776 03/23/15 18:56 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 18:31 TDP TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-2R Lab Sample ID: 490-74829-4
Matrix: WaterDate Collected: 03/19/15 13:45
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 01:241 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 21:03 ADN TAL NSHTotal/NA 50 mL 50 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-74829-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-2R Lab Sample ID: 490-74829-4
Matrix: WaterDate Collected: 03/19/15 13:45
Date Received: 03/20/15 08:40
Prep 3010A AJD03/25/15 09:14 TAL NSH236178
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 16:24 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235776 03/23/15 18:56 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 18:34 TDP TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-2RDUP Lab Sample ID: 490-74829-5
Matrix: WaterDate Collected: 03/19/15 13:45
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 01:521 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 21:08 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 236178 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 16:39 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235776 03/23/15 18:56 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 18:37 TDP TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-3R Lab Sample ID: 490-74829-6
Matrix: WaterDate Collected: 03/18/15 12:37
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 02:201 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 21:12 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 236178 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 16:44 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235941 03/24/15 12:23 TDP TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 20:38 TDP TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: SP-1 Lab Sample ID: 490-74829-7
Matrix: WaterDate Collected: 03/18/15 13:30
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 02:481 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 21:17 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 236178 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 16:49 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235941 03/24/15 12:23 TDP TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 20:41 TDP TAL NSHTotal/NA 30 mL 30 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-74829-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: SS-1 Lab Sample ID: 490-74829-8
Matrix: WaterDate Collected: 03/18/15 12:53
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 03:161 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 21:21 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 236178 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 16:54 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235941 03/24/15 12:23 TDP TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 20:44 TDP TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: SS-2 Lab Sample ID: 490-74829-9
Matrix: WaterDate Collected: 03/18/15 13:08
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 03:441 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 21:26 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 236178 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 17:00 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235941 03/24/15 12:23 TDP TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 20:46 TDP TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-02CD Lab Sample ID: 490-74829-10
Matrix: WaterDate Collected: 03/19/15 12:26
Date Received: 03/20/15 08:40
Analysis 8260B PS03/29/15 04:111 TAL NSH237281
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 236173 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 236833 03/26/15 21:30 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 236178 03/25/15 09:14 AJD TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 236845 03/26/15 17:05 JBD TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 235941 03/24/15 12:23 TDP TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 236233 03/24/15 20:49 TDP TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: Trip Blank Lab Sample ID: 490-74829-11
Matrix: WaterDate Collected: 03/18/15 01:00
Date Received: 03/20/15 08:40
Analysis 8260B KS03/30/15 15:001 TAL NSH237488
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-74829-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010CMetals (ICP)TAL NSH
SW8466020AMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-74829-1
Project/Site: Polk County Route 9 Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-15
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-74829-1
Login Number: 74829
Question Answer Comment
Creator: McBride, Mike
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a
survey meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.0.4
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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APPENDIX C

Environmental Monitoring Reporting Form
and Electronic Submittal of
Environmental Monitoring Data
7502Mar2015
(Electronic Format Only)