SW_F_2608-CDLF-1998_09-01-2013_RM_GW.pdf

FINAL
May 2013 (N=26) GROUNDWATER AND
METHANE MONITORING REPORT
FOR
THE LAMONT ROAD LCID (CLOSED) AND C&D LANDFILLS
NCDENR LANDFILL PERMIT #26-08

FORT BRAGG, NORTH CAROLINA

Prepared by: US Army Corps of Engineers
Savannah District
Hazardous, Toxic & Radioactive Waste Section
CESAS-EN-GH
100 W. Oglethorpe Avenue
Savannah, GA 31401

September 2013

FINAL May 2013 (N=26) GROUNDWATER AND METHANE MONITORING REPORT

FOR

THE LAMONT ROAD LCID (CLOSED) AND C&D LANDFILLS
NCDENR LANDFILL PERMIT #26-08

FORT BRAGG, NORTH CAROLINA

Prepared by:

US Army Corps of Engineers
Savannah District
Hazardous, Toxic & Radioactive Waste Section
CESAS-EN-GH
100 W. Oglethorpe Avenue Savannah, GA 31401
September 2013

Prepared by: Date:
__________________________ ______________
Kevin Haborak, P.G.

TABLE OF CONTENTS
SECTION PAGE
1.0 INTRODUCTION .......................................................................................................................... 1
1.1 Project Background ............................................................................................. 1
1.2 Project Scope ...................................................................................................... 2
2.0 PROJECT HISTORY .................................................................................................................... 3
2.1 Site Description and History ............................................................................... 3
2.2 General Site Geology and Hydrology ................................................................. 3
2.3 Previous Investigation and Results ..................................................................... 4
3.0 METHODS ..................................................................................................................................... 5
3.1 Methane Monitoring ........................................................................................... 5
3.2 Water-Level Gauging.......................................................................................... 5
3.3 Groundwater Sampling ....................................................................................... 5
3.4 Investigation Derived Wastes Handling ............................................................. 6
4.0 ANALYTICAL RESULTS AND STATISTICAL ANALYSIS ................................................. 8
4.1 Analytical Data Summary ................................................................................... 8
4.2 Statistical Analysis Results ................................................................................. 8
4.3 Methane Monitoring Results ............................................................................... 9
CONCLUSIONS AND RECOMMENATIONS .......................................................................................10
5.0 REFERENCES ..............................................................................................................................11
In Order
Following Page 11

ii
FIGURES

Figure 1 Site Map – Ft. Bragg, NC
Figure 2 Location Map – Lamont Road Landfill, Ft. Bragg, NC
Figure 3 Methane Monitoring Results
Figure 4 Potentiometric Map
Figure 5 Groundwater Analytical Results
TABLES
Table 1 Methane Monitoring Results

Table 2 Groundwater Elevation Data
Table 3 Field Parameter Measurements Table 4 Summary of Groundwater Detections

APPENDICES

Appendix A – Groundwater Sampling Logs
Appendix B – Data-Validation Reports – Electronic Only
Appendix C – Chains of Custody and Laboratory Analytical Reports – Electronic Only
Appendix D – Statistical Reports – Electronic Only

iii
LIST OF ACRONYMS

C&D Construction and Demolition COCs Chemicals of Concern
DPW Directorate of Public Works
IDW Investigation Derived Waste
LCID Land Clearing and Inert Debris
µg/L Micrograms Per Liter
MSWLF Municipal Solid Waste Landfill Facility
NC2L North Carolina Administrative Code, Title 15A, Subchapter 2L
NCDENR North Carolina Department of Environmental and Natural Resources RCRA Resource Conservation and Recovery Act SAP Sampling and Analysis Plan
SSI Statistically Significant Increase
USACE US Army Corps of Engineers
VOCs Volatile Organic Compounds

1
FINAL May 2013 (N=26) GROUNDWATER AND
METHANE MONITORING REPORT FOR
THE LAMONT ROAD LCID (CLOSED) AND C&D LANDFILLS NCDENR LANDFILL PERMIT #26-08 FORT BRAGG, NORTH CAROLINA

1.0 INTRODUCTION
This is the Report for the May 2013 groundwater and methane monitoring at the
Lamont Road Landfills (Figure 1) performed by the United States Army Corps of
Engineers (USACE), Savannah District in May 2013. The monitoring is required by the
North Carolina Department of Environmental and Natural Resources (NCDENR) Solid
Waste Management Division. This was the twenty-sixth (N=26) event performed for the
Site. This report summarizes the methods used for the groundwater and methane
monitoring and presents the results of the sampling event.

1.1 Project Background The USACE was contracted by the Directorate of Public Works (DPW), Fort
Bragg, North Carolina to perform groundwater sampling and methane monitoring. The
original groundwater monitoring well network for the land clearing and inert debris
(LCID) and construction and demolition (C&D) landfills consisted of 12 wells. Four of
the original eleven monitoring wells have been permanently abandoned and replaced with
new wells at different locations. An additional two wells have also been installed. The
current Sampling and Analysis Plan (SAP), approved by NCDENR, includes sampling
these 13 monitoring wells. The monitoring wells are LMW-3, LMW-3s, LMW-4, LMW-
6, LMW-7, LMW-8, LMW-9, LMW-9s, LMW-9d, LMW-10, LMW-14R, LMW-15R,
and LMW-16. Groundwater monitoring locations are shown on Figure 2. LMW-8 was
not sampled during this event because the path to the well was blocked by a fallen tree.
All sampling was conducted according to North Carolina Solid Waste Management
Guidelines.

2
1.2 Project Scope
The scope for this project included collecting groundwater samples from 12
monitoring wells at the Lamont Road LCID and C&D Landfill for analyses of Appendix
I constituents, sampling for methane at 13 selected methane monitoring wells and at three
additional buildings, evaluating the analytical results, and reporting the results of the
investigation. The groundwater sampling and data analyses included obtaining field
parameter measurements (i.e. pH, temperature, etc.), measuring water levels at the
monitoring well locations, determining groundwater flow directions, validating
laboratory analytical data, performing statistical analysis for each detected constituent as
required by NC regulations, and determining the concentration changes of chemicals of
concern (COCs) with time.
.

3
2.0 PROJECT HISTORY
2.1 Site Description and History

The Lamont Road LCID and C&D Landfills are on the west side of Cooleyconch
Mountain (Figure 2). The site was previously utilized as a maneuver training area
(conducted continuously for 50 years), a borrow pit for sands and clays, and a repository
for unclassified debris from land clearing and construction demolition. The LCID
Landfill started as an uncontrolled dump site which was associated with reclaiming
borrow excavation. Its initial operation pre-dated Federal and State regulations
governing waste disposal. The LCID Landfill has been operated as a controlled
repository for C&D debris as well as for land clearing and inert debris since its permitting
under NCDENR Permit No. 26C on August 28, 1987. From February 1993 to date of
closure, C&D debris was diverted to the Longstreet Road Sanitary Landfill, and only
LCID has been accepted at the LCID Landfill site. It is presumed that asbestos materials
are disposed of in this landfill.

Cooleyconch Mountain is the prominent terrain feature west of the main post.
The LCID Landfill site is 1.5 miles west of the Longstreet Road municipal solid waste
landfill (MSWLF) (closed January 1, 1998) and 200 yards northwest of the Lamont Road
C&D Landfill. The area adjacent and east of the LCID Landfill has been excavated to be
used as a borrow pit for sandy fill material. To the south of the LCID Landfill, in the
C&D Landfill site, petroleum contaminated soils have been spread, dried, and stored for
subsequent removal. To the east of the LCID Landfill, petroleum contaminated sludge
has been stored in earthen impoundments for subsequent removal. The LCID Landfill
drains north to Cypress Creek, which intersects the Little River a mile upstream of the
Fort Bragg Water Plant intake.

2.2 General Site Geology and Hydrology

Lithologic descriptions of soil borings and monitoring well borings from previous
investigations at Fort Bragg indicate that in general Fort Bragg is underlain by alternating
sands, silty sands, clayey sands, sandy clays, and clays, likely belonging to the

4
Middendorf Formation. The sands and silty sands range in thickness from
approximately 2 to 22 ft and are coarse grained. The clay units range in thickness from
approximately 2 to 7 ft and are typically plastic.

2.3 Previous Investigation and Results

Several sampling events have been conducted at the landfills. Initially, four
monthly sampling events were conducted in July, August, September, and October 1996
by R,S & H Architect, Engineering, & Planning, Inc. Law & Company, Inc. conducted
two sampling events in March and September, 1999 in conjunction with the installation
of new wells. Then until 2005, sampling events were conducted by BPA Environmental
& Engineering, Inc. The USACE has monitored the site since 2005.

The previous sampling event, held in November of 2012 for Lamont Landfill, was
conducted by the USACE, Savannah District. Low levels of Appendix I VOCs and
metals were detected. All of the detections were below their respective NC2L standards
and according to the statistical analysis there was no evidence that showed an increasing
contaminant concentration trend.

5
METHODS

2.4 Methane Monitoring

Methane monitoring was performed at 13 wells and at three additional buildings.
The monitoring included measuring levels of methane, carbon dioxide, and oxygen at
each location. The results of the monitoring are summarized in Table 1 and are also
presented on Figure 3.

2.5 Water-Level Gauging During this sampling event, USACE personnel measured the water levels in 12
monitoring wells. Observed water levels and calculated groundwater elevations are
presented in Table 2. A potentiometric map was developed based on the groundwater
elevations; the map is presented as Figure 4. The map shows that the general direction of
the groundwater flow at the Lamont Landfill is towards the west-northwest.

2.6 Groundwater Sampling
The groundwater sampling was conducted in accordance with the SAP for the
Lamont Road LCID and C&D Landfills (NCDENR Landfill Permits # 26G and #26-08
dated April 2005, which have been updated to reflect the most recent SAP).
Groundwater samples were collected from 12 wells. Water quality parameters pH,
specific conductivity, temperature, turbidity, dissolved oxygen (DO), and oxidation-
reduction potential (ORP) were measured during the purge cycle of each well. The
measurements are summarized in Table 3.

Groundwater samples were collected using a low-flow purge method with either a
bladder pump or a peristaltic pump. Immediately before purging a well, the static water
level below the top of the well casing and the total depth of the well were measured to the
nearest 0.01 foot and recorded in the field notebook. The volume of water in the well
was calculated based on the static water level and the well construction information.
Well volume calculations were placed in the field notebook. The inlet of the sampling

6
pump was placed at the mid-point of the screened interval. This level was adjusted for
wells where the static water level is within the well screen. The monitoring wells were
purged using a variable-flow bladder pump or peristaltic pump at a rate of 500 ml/min or
less.

The wells were purged until the water quality had stabilized or five purge volumes
were removed. The wells were considered stable when the following requirements were
met for three consecutive readings: turbidity values within 10% or lower than 10
Nephelometric Turbidity Units (NTUs), temperature values within a range of 0.5 degrees
Celcius, pH readings within 0.1 Standard Units (SU), ORP values within a range of 10
milivolts (mV), and conductivity values within 3%, and DO values within 10%.

The rate of pumping was determined and noted in the field notebook. The purge
rate was adjusted, as necessary, to avoid purging any well to dryness and to equal the
recharge of the aquifer. All sampling equipment was protected from contaminated soil
surfaces to prevent contamination of the samples (e.g., equipment may be placed on
disposable polyethylene plastic sheeting). Groundwater samples were collected after
purging was complete. The tubing was disconnected from the flow through cell, and the
samples were collected from the pump outlet. The samples were labeled and placed into
an ice-filled cooler for preservation.

Groundwater sampling data (including sample number, location, quantity of water
purged, field parameters, site conditions, etc.) were documented in the field notebook.
Water samples for Resource Conservation and Recovery Act (RCRA) metal analyses
were un-filtered. The results of the groundwater sampling are presented in Table 4 and
on Figure 5. The groundwater sampling field data logs are presented in Appendix A.

2.7 Investigation Derived Wastes Handling

The investigation derived wastes (IDW), including the waste water from well
purging and decontamination water, were containerized in 55-gallon drums. Those
drums were appropriately labeled, sealed, and staged within designated areas until

7
analytical results had been received and reviewed. Based on the analytical results of the
groundwater samples, the IDW was classified as non-hazardous. With the concurrence of
the Fort Bragg Installation Restoration Program Manager, the IDW was disposed of at an
appropriate disposal facility.

8
3.0 ANALYTICAL RESULTS AND STATISTICAL ANALYSIS
3.1 Analytical Data Summary Groundwater samples collected in May 2013 were analyzed for Appendix I VOCs
and metals. The summary of detections of the COCs is presented in Table 4. Figure 5
shows the distribution of the detections and their concentrations from this sampling
event. The reports of chemical data quality assessment prepared by the Project Chemist
are included as Appendix B. The laboratory reports of analytical results are included as
Appendix C. For comparison, the analytical results of previous investigations are also
presented in the Statistical Analyses Summary Report included in Appendix D.

In accordance with North Carolina guidance, analytical results are compared to
North Carolina Groundwater 2L Standards (NC2L standards). The analytical data of the
first 2013 sampling event indicated that some VOCs and inorganics were detected at low
levels, and all detections were below NC2L standards (Table 4).

3.2 Statistical Analysis Results
A statistical test predicts the average behavior (distribution) of a random variable
by comparing the means (normal distribution) or medians (lognormal and non-parametric
distributions) of the compliance well data to background well data. Different statistical
tests were used as appropriate for the different distributional patterns that occur within
the data. Prior to testing for statistical significance, the distribution of each parameter
was determined to be normal, lognormal, or non-normal.

If the data were non-normally distributed, or the fraction of nondetects exceeded
15% but were less than 90%, then the Kruskal-Wallis Test was applied. If the fraction of
non-detects exceeded 90%, then the Non-Parametric Prediction Limit was applied. For
these tests to be sufficiently sensitive, the sample size for any group must be at least 4. A
Kruskal-Wallis Test can be used in any situation that the parametric analysis of variance
can be used. This test computes the H-statistic, adjusts it for ties, and compares it to the

9
appropriate chi-square critical value. If the H-statistic is less than the critical value, the
null-hypothesis is accepted, and it is concluded that there are no differences between
median background and compliance well concentrations. If the H-statistic is greater than
the critical value, it is concluded that at least one pair of well groups is statistically
different. However, the Kruskal-Wallis test is prone to false positives. Therefore,
additional statistical analyses were used to determine the validity of the positive results.
Intra-well comparisons of data from a single well to previous data from the same well
were performed to determine if a trend of increasing concentration is occurring. The
Mann-Kendall Trend Analysis and the Shewhart-CUSUM Control Chart statistical tests
were selected for these additional analyses.
A detailed discussion of the statistical methods is presented in Appendix D. The
results of the statistical analysis indicate that there are no SSIs in the concentrations of
the detected constituents.

3.3 Methane Monitoring Results

The methane levels were measured at 16 locations at Lamont Landfill. The
results of the monitoring are summarized in Table 1 and are also presented on Figure 3.
No methane monitoring wells contained a high level of methane (> 5% Methane by
Volume).

10
4.0 CONCLUSIONS AND RECOMMENATIONS
The annual monitoring program consists of two sampling events conducted six
months apart. This was the May 2013 sampling event for groundwater and methane
monitoring performed by the USACE, Savannah District. It was the N=26 sampling
event for the Lamont Road Landfills. Low levels of Appendix I VOCs and metals were
detected, but all of the detections were at estimated levels and/or were below NC2L
standards.
According to the Statistical Analysis of groundwater Data (Appendix D), there is
no evidence of an upward trend in constituent concentrations. The statistical findings at
the Lamont Road Landfill demonstrated that any statistical abnormalities were due to
natural variation in the results. Long-term monitoring should continue at the Lamont
Road Landfill because it is still an active site and NC Solid Waste Regulations require it.
The methane levels were measured at 16 locations around Lamont landfill. No
methane monitoring wells contained a high level of methane (> 5% Methane by Volume).

11
REFERENCES

North Carolina Administrative Code, Title 15A, Department of Environment, Health, and
Natural Resources, Division of Solid Waste, Management, Subchapter 13B, Solid
Waste Management, Section .1600 (January 4, 1994).

North Carolina Administrative Code, Title 15A, Department of Environment, Health, and
Natural Resources, Division of Solid Waste, Management, SubchapterNC2L,
Classifications and Water Quality Standards Applicable to the Ground Waters of
North Carolina, Sections .0100, .0200, and .0300 (November 8, 1993): from the
Environmental Management Commission, Raleigh, North Carolina.

FIGURES

West Virginia
Virginia
Kentucky
Tennessee
Georgia South Carolina
North Carolina
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50 0 50 100 15025Miles
C a p e F e a r R i v e r
Rockfish Creek
Figure 1
Site Map -- Ft. Bragg, NC
U.S. ARMY ENGINEER DISTRICTCORPS OF ENGINEERSSAVANNAH, GEORGIA
Lamont Street Landfill
Longstreet Road
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DATE: SEPT 2013 FIGURE: 2
LAMONT STREET LANDFILL
LOCATION MAP
FORT BRAGG, NC
$0 250 500125'
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DATE: SEPT 2013 FIGURE: 3
LAMONT STREET LANDFILL
METHANE MONITORING RESULTSMAY 2013
FORT BRAGG, NC
$0 250 500125'
1 inch = 250 feet
Legend
&§M METHANE SAMPLE
U.S. ARMY CORPS OF ENGINEERSSAVANNAH DISTRICTSAVANNAH, GEORGIA
0.0% Methane18.0% Oxygen
0.0% Methane19.4% Oxygen
0.0% Methane18.6% Oxygen
0.0% Methane17.9% Oxygen
0.0% Methane17.8% Oxygen
0.0% Methane12.2% Oxygen
0.0% Methane19.3% Oxygen
0.1% Methane4.7% Oxygen
0.0% Methane12.5% Oxygen
2.5% Methane4.4% Oxygen
0.0% Methane15.4% Oxygen
0.0% Methane15.8% Oxygen
% Methane %OxygenScale house 0.0% 20.1%Office 0.0% 20.1%O-3533 0.0% 20.1%
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DATE: SEPT 2013 FIGURE: 4
LAMONT STREET LANDFILL
POTENTIOMETRIC SURFACE MAPMAY 2013FORT BRAGG, NC
$0 250 500125'
1 inch = 250 feet
U.S. ARMY CORPS OF ENGINEERSSAVANNAH DISTRICTSAVANNAH, GEORGIA
Note: Monitoring wells used forpotentiometric surface are displayedwith elevations in feet above MSL inparenthesis below the label.
Arrows point in direction of groundwater flow.
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1 inch = 400 feetLegend@AMONITORING WELL U.S. ARMY CORPS OF ENGINEERS SAVANNAH DISTRICT SAVANNAH, GEORGIANOTE: Only detected analytes shown. NA - Not Available U - Target analytes were not detected above the reporting limits J - Analyte was present but concentration is an estimated value. Bold - Concentrations exceed NC 2L standards. *IMAC - Interim maximum allowable concentration **PRG based on carcinogenic factor.LAMONT STREET LANDFILL GROUNDWATER ANALYTICAL RESULTS MAY 2013
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a
l
s
(µ
g/
L
)
Ba
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i
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1
0
Be
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l
l
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m

0
.
2
Co
b
a
l
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0
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7
Ch
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m
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0
.
2
0

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Co
p
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2
.
8
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0
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6

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5
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3
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7

J
LM
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9
-
0
5
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1
3
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l
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(µ
g/
L
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Ar
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1
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1
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4
6
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0
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2
5

J
LM
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9
S
-
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3
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(µ
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5
6
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l
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1
2

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Va
n
d
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m

3
.
4

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5
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4

J
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A
n
a
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(m
g/
L
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a
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-

N
O
3

0
.
4
1

J
LM
W
-
9
D
-
0
5
-
1
3
VOCS (µg/L)Chloroform

0
.
1
5

J
Dichlorodifluoromethane

3
.
9
Methylene Chloride 1.2 J Trichloroethene

0
.
6
3

J
Trichlorofluoromethane

7
.
9
Metals (µg/L)Barium

2
5
Cobalt

0
.
2
1
Chromium

0
.
4
4

J
Copper

0
.
2
4

J
Nickel

0
.
4
2

J
Selenium

3
.
9
Other Analyses (m g/L)Nitrate - NO3

1
.
1
LMW-10-05-13
Me
t
a
l
s
(µ
g/
L
)
Ba
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1
1
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0
.
5
0

J
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b
a
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0
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1
2

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0
.
7
0

J
Le
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d

0
.
1
2

J
Ni
c
k
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0
.
4
4

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LM
W
-
1
4
R
-
0
5
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1
3
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t
a
l
s
(µ
g/
L
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0
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1
5

J
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0
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1
8

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0
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5
2

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0
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5
8

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0
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0
8
7

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2
.
2
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0
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1
4

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A
n
a
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(m
g/
L
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t
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a
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e
-
N
O
3

6
.
8
LM
W
-
1
5
R
-
0
5
-
1
3
Metals (µg/L)Arsenic

2
.
1
Barium

8
Cobalt

0
.
1
8

J
Chromium

1
.
8
Copper

0
.
7
8

J
Nickel

0
.
7
0

J
LMW-16-05-13

TABLES

Table 1. Methane Monitoring Results
Lamont Landfills, Fort Bragg, NC

Well ID

Date Sampled
Time Sampled

%Methane by Volume

%Oxygen %CO2
Gas-GP-1 05 May 2013 13:19 0.1% 4.7% 14.4% Gas- GP -2 05 May 2013 12:59 0.0 % 12.5% 8.5%
Gas- GP -3 05 May 2013 13:06 0.0% 18.0% 1.7% Gas- GP -4 05 May 2013 12:19 0.0% 19.4% 0.7%
Gas- GP -5 05 May 2013 12:23 0.0 % 18.6% 1.2% Gas- GP -6 05 May 2013 12:27 0.0% 17.9% 7.0%
Gas- GP -7 05 May 2013 12:31 0.0% 17.8% 1.6% Gas- GP -8 05 May 2013 12:36 0.0% 15.8% 3.1%
Gas- GP -9 05 May 2013 12:43 0.0% 12.2% 8.0% Gas- GP -10R 05 May 2013 12:47 4.0% 5.1% 15.8%
Gas- GP -11 05 May 2013 13:32 0.0% 19.3% 0.9% Gas- GP -12 05 May 2013 13:28 2.5% 4.4% 13.0
Gas- GP -13R 05 May 2013 12:08 0.0% 15.4% 2.6% Office 05 May 2013 13:02 0.0% 20.1% 0.0%
Scale House 05 May 2013 13:09 0.0% 20.1% 0.0% O-3533 05 May 2013 13:12 0.0% 20.1% 0.0%

Note: TOC – Top of casing, btoc – Below top of casing, NA – Not Available
bgs – Below ground surface, amsl – Above mean sea level
∆ --- Selected Well for Long Term Monitoring TOC elevation is based on vertical datum NGVD29 (source: USGS RFI, Aug. 1999)
* Erroneous reading not reported in table. **No well cover
Table 2
Groundwater Elevation Data
Lamont Street Landfill, Fort Bragg NC
November-08 November-08 June-09 June-09 November-09 November-09 June-10 June-10 November-10 November-10 June-11 June-11 November-11 November-11 May-12 May-12 November-12 November-12
LMW-3 408.32 102.18 306.14 103.2 305.12 102.21 306.11 87.27 321.05 102.13 306.19 102.79 305.56 104 304.32 106.22 302.1 105.72 302.6
LMW-3s *59.19 NA 60.4 NA 59.12 NA 59.61 NA 58.91 NA 59.64 NA 61.26 NA 62.8 NA 63.17 NA
LMW-4 441.79 75.42 366.37 74.65 367.14 74.74 367.05 75.39 366.4 74.83 366.96 75.33 366.46 75.81 365.98 75.71 366.08 80.34 361.45
LMW-6 431.45 80.3 351.15 81.65 349.8 80.15 351.3 80.75 350.7 80.04 351.41 80.93 350.52 82.7 348.75 84.38 347.07 84.81 346.64
LMW-7 436.62 125.87 310.75 125.63 310.99 124.78 311.84 128.8 307.82 124.54 312.08 124.78 311.84 125 311.62 125.2 311.42 125.11 311.51
LMW-8 354.07 48.68 305.39 76.66 277.41 46.85 307.22 304.86 49.21 46.86 307.21 48.95 305.12 51.02 303.05 50.84 303.23 49.97 304.1
LMW-9 364.79 82.16 282.63 80 284.79 80.71 284.08 87.27 277.52 80.73 284.06 82.43 282.36 85 279.79 86.64 278.15 87.43 277.36
LMW-9S *52.46 NA 49.01 NA 51.01 NA 53.35 NA 51 NA 52.89 NA 55.05 NA 54.83 NA 53.95 NA
LMW-9D *76.95 NA 76.66 NA 75.41 NA 77.03 NA 75.48 NA 77.29 NA 79.73 NA 81.11 NA 82.07 NA
LMW-10 428.68 76.81 351.87 76.48 352.2 76.38 352.3 72.11 356.57 NA NA 76.89 NA 78.84 349.84 79.87 348.81 79.87 348.81
LMW-14R *50.07 NA 49 NA 48.97 NA 50.06 NA 48.99 NA 50.25 NA 51.53 NA 52.02 NA 51.67 NA
LMW-15R *40.89 NA 37 NA 37.55 NA 40.31 NA 38.19 NA 40.28 NA 41.68 NA 40.81 NA 40.35 NA
LMW-16 *86.02 NA 36.48 NA 37.5 NA 37.28 NA 36.61 NA 36 NA 36.8 NA 37.36 NA 37.22 NA
Note:
TOC – Top of casing,btoc – Below top of casing,NA – Not Available
bgs – Below ground surface,amsl – Above mean sea level NS – Not Surveyed
∆ --- Selected Well for Long Term M*Well & ground-water elevations unavailable at this time.
TOC elevation is based on vertical datum NGVD29 (source: USGS RFI, Aug. 1999)
Water Level
(ft. BTOC)
Water Level
Elev. (ft. amsl)
Water Level
Elev. (ft. amsl)
Water Level
(ft. BTOC)
Water Level
Elev. (ft. amsl)
Water Level
(ft. BTOC)
Water Level
Elev. (ft. amsl)
Water Level
(ft. BTOC)
Water Level
Elev. (ft. amsl)
Water Level
(ft. BTOC)
Water Level
Elev. (ft. amsl)
Water Level
(ft. BTOC)
Water Level
Elev. (ft. amsl)
Water Level
(ft. BTOC)
Water Level
(ft. BTOC)Well ID
Water Level
Elev. (ft. amsl)
Water Level
(ft. BTOC)
Water Level
Elev. (ft. amsl)TOC Elev.
(ft. amsl)
Table 3. Field Parameter Measurements Lamont Landfills, Fort Bragg, NC

Well ID Sample Identification pH
Specific
Conductivity
(µs/cm)
Temperature
(°C)
Turbidity (N.T.U.)
Dissolved Oxygen
(mg/L)
ORP
LMW-3 GW-LMW-3-5-13 4.95 0.021 16.88 0.58 5.42 151.8
LMW-3S GW-LMW-3S-5-13 4.80 0.032 16.74 1.15 4.20 160.4
LMW-4 GW-LMW-4-5-13 4.84 0.027 16.64 12.9 4.21 159.6
LMW-6 GW-LMW-6-5-13 5.11 0.177 17.19 1.86 1.14 180.6
LMW-7 GW-LMW-7-5-13 5.69 0.017 16.75 5.48 8.14 161.5
LMW-8 GW-LMW-8-5-13 NS NS NS NS NS NS
LMW-9 GW-LMW-9-5-13 4.78 0.062 19.23 39.9 3.56 222.1
LMW-9S GW-LMW-9S-5-13 5.86 0.343 18.19 -- 0.57 53.7
LMW-9D GW-LMW-9D-5-13 6.39 0.055 16.12 106 6.03 119.5
LMW-10 GW-LMW-10-5-13 5.00 0.057 19.18 6.04 5.31 98.2
LMW-14R GW-LMW-14R-5-13 4.94 0.019 17.50 5.99 6.67 156.5
LMW-15R GW-LMW-15R-5-13 4.60 0.044 17.53 3.33 6.98 174.5
LMW-16 GW-LMW-16-5-13 6.51 0.359 19.14 4.87 0.54 68.0

Note: N.T.U. --- Nephelometric Turbidity Unit ORP --- Oxidation Reduction Potential
* - Not reported NS – Not Sampled
Table 4. Summary of Groundwater DetectionsLamont Landfills, Fort Bragg, NC Page 1
LM
W
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04
/
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LM
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LM
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-
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11
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GW
-
L
M
W
-
3 0
6
/
0
7
GW
-
L
M
W
-
3 1
1
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GW
-
L
M
W
-
3 0
5
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8
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0
8
LM
W
-
3
06
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0
9
LM
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-
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11
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9
LM
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3
06
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1
0
LM
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11
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1
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10
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10
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D
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LM
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11
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6
GW
-
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M
W
-
4 0
6
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0
7
GW
-
L
M
W
-
4 1
1
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0
7
GW
-
L
M
W
-
4 0
5
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8
GW
-
L
M
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-
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LM
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-
4
06
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9
LM
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11
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9
LM
W
-
4
06
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0
LM
W
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11
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1
0
LM
W
-
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6/
1
1
LM
W
-
4
11
/
1
1
LM
W
-
4

5/
1
2
LM
W
-
4

11
/
1
2
LM
W
-
4

05
/
1
3
LM
W
-
6

04
/
0
5
LM
W
-
6

10
/
0
5
LM
W
-
6

6/
0
6
LM
W
-
6

11
/
0
6
LM
W
-
6

Du
p

1
1
/
0
6
GW
-
L
M
W
-
6 0
6
/
0
7
GW
-
L
M
W
-
6
D
u
p

0
6
/
0
7
GW
-
L
M
W
-
6 1
1
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0
7
GW
-
L
M
W
-
6 0
5
/
0
8
GW
-
L
M
W
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6 1
1
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8
GW
-
L
M
W
-
6
GW
-
L
M
W
-
6
LM
W
-
6
06
/
1
0
LM
W
-
6
11
/
1
0
LM
W
-
6
6/
1
1
LM
W
-
6
11
/
1
1
LM
W
-
6

5/
1
2
LM
W
-
6

11
/
1
2
LM
W
-
6

05
/
1
3
LM
W
-
7

04
/
0
5
LM
W
-
7

10
/
0
5
LM
W
-
7

6/
0
6
LM
W
-
7

6/0
6

VOCs (EPA 8260B)
1,1,2,2-tetrachloroethane 0.17 NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1,1-dichloroethane 700 810*BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1,2,3-trichloropropane 0.005 NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1,2,4-trichlorobenzene 70 70 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1,2,4-trimethylbenzene 350 15 *BRL BRL BRL BRL BRL BRL BRL 0.24 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.21 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1,2-dibromo-3-chloropropane 0.025 0.2 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1,2-dibromoethane 0.0004 0.05 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1,2-dichloroethane 0.38 5 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
1,2-dichloropropane 0.56 5 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1,4-dichlorobenzene 75 75 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
2-butanone NA NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL4-Isopropyltoluene NA NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.95 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
4-Methyl-2-pentanone (MIBK)NA NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLacetone700NANABRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNABRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL5.7 J 6.9 J BRL BRL BRL NA BRL BRL BRL BRL BRL BRL BRL 4.69 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NA BRL BRL BRLacroleinNANABRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLbenzene15BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLcarbon disulfide 700 NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLchlorobenzene50100BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLchloroethane28004.6*BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLchloroform7080BRLBRLBRLBRLBRLBRL0.27 J 0.27 J 0.33 J 0.5 J 0.31 J 0.42 J 0.4 J 0.44 J 0.41 J 0.52 J 0.33 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLchloromethane (methyl chloride)2.6 NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLcis-1,2-dichloroethene 70 70 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLdibromochloromethane0.41 80 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLdichlorodifluoromethane1400390*BRL BRL BRL BRL BRL BRL 0.45 J 0.43 J BRL 0.41 J BRL BRL BRL BRL 0.31 J 0.51 J BRL BRL BRL BRL 0.57J 0.92J BRL BRL 0.71 J 0.95 J BRL 1.1 BRL 0.81 J BRL 1 0.66 J 0.60 J 0.42 J BRL BRL 0.93J 2.67 2.80 BRL BRL BRL 0.83 J 0.82 J BRL BRL BRL BRL BRL BRL 0.69 J 0.47 J BRL BRL BRL BRL BRLdiisopropyl ether 70 NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
isopropylbenzene 70 660*BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLm&p xylene 530#10000#BRL BRL BRL BRL BRL BRL BRL 0.44 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.25J BRL BRL 0.23J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
methylene chloride (dichloromethane)4.6 5 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 3.1 J B BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 3.7 J B BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLMTBE20013*BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
o-xylene 530#10000#BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLsec-butylbenzene 70 NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
tetrachloroethene 0.7 5 BRL BRL BRL BRL BRL .025 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.22 J BRL BRL 0.16 J BRL BRL BRL BRL BRL BRLtoluene10001000BRLBRLBRLBRLBRLBRLBRL0.3 J BRL BRL BRL BRL 0.38 J BRL BRL BRL BRL 0.33 J BRL BRL BRL 0.47J BRL BRL BRL 0.25 J < 2 BRL BRL BRL 1.2 BRL BRL 0.42 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.30 J BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.07 J BRL BRL BRL
trans-1,2-dichloroethene 70 100 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLtrichloroethene2.8 5 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.16 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
trichlorofluoromethane 2100 1300*0.25 J 0.34J 0.52J BRL BRL BRL 0.74 J 0.63 J 0.84 J 0.68 J 0.58 J 0.52 J 0.51 J 0.89 J 0.71 J 1.1 0.91 J 2.37 0.68J 0.47J 2.53 2.37 BRL BRL 3.79 2.66 0.82 J 2.4 2 1.7 0.31 J 1.2 1.3 1 0.66 J 0.63 J 1.54J 1.13J BRL 0.860J BRL BRL BRL 1.22 J 0.72 J 0.95 J 1.1 0.72 J 0.48 J 0.70 J 0.35 J 0.67 J 0.41 J 0.64 J BRL BRL BRL BRLTotal Xylenes 530 0.01 BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.32 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.24 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
vinyl chloride 0.015 2 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
Metals (EPA 6010B/6020A)
Arsenic 10 10 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.44 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.13 J BRL BRL BRL 0.51 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.1 J BRL BRL BRL BRL BRL BRL 0.46 J 0.52 J BRL BRL BRL BRL BRL BRL BRL BRL BRLBarium20002000BRL7.2J 5.0J 7.4 5.33 BRL 5.47 5.8 BRL 6.4 5 13 3.5 12 4.6 4.5 3.3 14.2 12.5 11.8 10 13.6 24.7 1.14J 11.20 14.7 15 13 15 14 14 16 15 13 14 9.5 J 12.3 20 33.9 33.7 52.4 46.4 42 49.2 73.7 92 74 77 79 55 44 J 36 33 30 31.7 30 20 10BerylliumNA4NANANANANANANANANANANANABRLBRLBRLBRLBRLNANANANANANANANANANA0.071 J NA NA BRL BRL BRL BRL 0.078 J NA NA NA NA NA NA NA NA NA NA 0.15 J 0.15 J 0.13 J 0.16 J 0.085 J BRL 0.075 J BRL 0.092 J NA NA NA NACadmium55BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.701J 0.57J BRLCobaltNANABRLBRLBRLBRLBRLBRLBRLBRL0.16 J 0.16 J 0.17 J 0.51 BRL 0.43 0.18 J 0.18 J 0.16 J BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.24 0.24 0.27 0.29 J 0.27 0.25 0.26 0.26 0.5 BRL BRL BRL 0.734J 0.733J BRL BRL BRL 0.93 J BRL 1.4 1.2 1.2 1.1 0.72 0.52 0.46 0.41 0.37 BRL BRL BRL BRLChromium50100BRLBRLBRLBRLBRLBRLBRLBRLBRL1.1 B 0.76 J 0.94 J BRL BRL BRL 0.61 J BRL 10.8 J BRL BRL BRL BRL 21.7 BRL BRL BRL 0.84 J 1 B 0.72 J 1 1.7 BRL 0.23 J 0.24 J 0.19 J BRL BRL BRL BRL BRL 4.74 J 3.75 J BRL 7.82 BRL BRL BRL 0.57 J 0.24 J 0.18 J BRL BRL BRL BRL 19.0 J 23.2 BRL BRLCopper10001000BRLBRLBRLBRLBRLBRLBRLBRLBRL1.1 BRL 1.6 1 0.84 J 0.78 J 0.40 J 0.64 J BRL BRL BRL BRL BRL 8.06 J 5.45 J 8.80 BRL BRL 0.78 J 1.3 0.87 J 1.1 0.79 J 0.87 J 0.23 J 1.3 BRL BRL BRL BRL BRL 7.78 J BRL BRL 2.70 J BRL BRL 1.2 3 2.2 1.1 BRL 0.49 J 0.78 J 0.76 J 10.8 J 11.1 10J BRLIron300NABRLBRLBRLBRLBRLBRLBRLBRLBRLBRL53BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL130BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL52BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLLead1515BRLBRLBRLBRLBRLBRLBRLBRLBRL0.37 0.17 J 0.51 0.12 J BRL BRL BRL BRL BRL BRL 0.534J BRL 0.644J 3.52 BRL 0.644J BRL 0.13 J 0.3 J 0.19 J 0.16 J 0.26 J 0.13 J 0.3 BRL 0.13 J BRL BRL BRL BRL BRL 0.839 J0.873 J BRL BRL BRL 0.084 J BRL 0.14 J 0.17 J 0.099 J BRL BRL 0.11 J BRL 3.11 3.07 3.37 2.31Manganese50NABRLBRLBRLBRLBRLBRLBRLBRLBRLBRL1.1 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 5.6 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLNickel100730*BRL BRL BRL BRL BRL BRL 1.12 J BRL BRL 1.1 1.3 J 3 0.85 J 3 0.51 J 1 0.45 J BRL BRL BRL BRL 1.6J 6.98 3.46 5.38 BRL < 50 1.2 0.76 J 1.1 1.2 1.1 0.62 J 1.1 0.77 J BRL BRL BRL 1.13J 1.12J 5.53 J BRL BRL 2.06 BRL 2.2 1.8 J 1.9 1.9 1.1 0.99 J 0.64 J 0.85 J 0.60J 18.9 J BRL BRL BRLSelenium5050BRLBRLBRLBRLBRLBRLBRLBRL0.54 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.8J 2.12 2.83 2.91 2.93 2.46 4.3 2.99 J BRL 3.2 2.6 3.2 6 5.6 3 3.2 3.3 1.8 BRL BRL BRL BRLSilver17.5 180 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLThalliumNA2BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.15 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.18 J BRL BRL BRL BRL 0.17 J BRL BRL BRL BRLTinNANABRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLVanadiumNA260*BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.8 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 15.8 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 3.7 J 4.21 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 12.6 J 18.5J 8.0J BRLZinc21005000BRLBRLBRL6.46J BRL BRL 12 BRL BRL 32 B 8.5 J 11 7.6 J 14 4.0 J 3.0 J BRL BRL BRL BRL BRL 11.1 47.0 BRL 15.30 BRL 6.7 J 16 B 6.9 J 7.3 20 11 6.0 J 11 5.9 J BRL BRL 20J 7.63J 7.85J 17.3 J 15.2 J 27 J 10.1 BRL BRL 41 11 8.6 J 8.7 J 4.9 J 2.9 J 3.4 J 2.6 J 27.5 J 31.4J 40J 20J
Other Analyses
Mercury 1.05 NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA
Nitrate-NO3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 660 J 730 J 640 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL BRL BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 5500 5600 5,800 NA NA NA NA
Nitrate/Nitrite as N (SM 4500)1,000 1,000 NA BRL NA 0.333 209 139 510 5220 N/A 870 J 780 J 190 J 730 200 J NA NA NA NA BRL BRL NA 0.050 643,000 107 370 44 N/A 40 840 J BRL <75 <75 NA NA NA NA BRL NA 1.15 1.14 1,220 1,290 950 1410 908 NA 5000 8,800 1,400 1,700 1,200 NA NA NA NA BRL NA NA
**Used values for Chlordane; <> -- Data not recieved from laboratory; ^value changed based on Data Validation.
COMPOUNDS (µg/L)Groundwater NC 2L
Standard (ug/l)
EPA Drinking water MCL (ug/l)
Note: BRL -- Below Reporting Limit; NA -- Not Available; NS -- Not Sampled; U -- Target analytes were not detected above the reporting limits; J -- Analyte was present but concentration is an estimated value; Bold--Concentration exceeds NC 2L Std; * No MCL, used PRG; #Used total values;
Lamont
Table 4. Summary of Groundwater DetectionsLamont Landfills, Fort Bragg, NC Page 2
VOCs (EPA 8260B)
1,1,2,2-tetrachloroethane 0.17 NA1,1-dichloroethane 700 810*1,2,3-trichloropropane 0.005 NA1,2,4-trichlorobenzene 70 701,2,4-trimethylbenzene 350 15 *1,2-dibromo-3-chloropropane 0.025 0.21,2-dibromoethane 0.0004 0.051,2-dichloroethane 0.38 5
1,2-dichloropropane 0.56 51,4-dichlorobenzene 75 75
2-butanone NA NA4-Isopropyltoluene NA NA
4-Methyl-2-pentanone (MIBK)NA NAacetone700NAacroleinNANAbenzene15carbon disulfide 700 NAchlorobenzene50100chloroethane28004.6*chloroform 70 80chloromethane (methyl chloride)2.6 NAcis-1,2-dichloroethene 70 70dibromochloromethane0.41 80dichlorodifluoromethane1400390*diisopropyl ether 70 NA
isopropylbenzene 70 660*m&p xylene 530#10000#
methylene chloride (dichloromethane)4.6 5MTBE20013*
o-xylene 530#10000#sec-butylbenzene 70 NA
tetrachloroethene 0.7 5toluene10001000
trans-1,2-dichloroethene 70 100trichloroethene2.8 5
trichlorofluoromethane 2100 1300*Total Xylenes 530 0.01
vinyl chloride 0.015 2
Metals (EPA 6010B/6020A)
Arsenic 10 10Barium20002000BerylliumNA4Cadmium55CobaltNANAChromium50100Copper10001000Iron300NALead1515Manganese50NANickel100730*Selenium 50 50Silver17.5 180ThalliumNA2TinNANAVanadiumNA260*Zinc 2100 5000
Other Analyses
Mercury 1.05 NA
Nitrate-NO3 NA NA
Nitrate/Nitrite as N (SM 4500)1,000 1,000
COMPOUNDS (µg/L)Groundwater NC 2L
Standard (ug/l)
EPA Drinking water MCL (ug/l)LM
W
-
7

11
/
0
6
GW
-
L
M
W
-
7 0
6
/
0
7
GW
-
L
M
W
-
7 1
1
/
0
7
GW
-
L
M
W
-
7 0
5
/
0
8
GW
-
L
M
W
-
7 1
1
/
0
8
GW
-
L
M
W
-
7
GW
-
L
M
W
-
7
LM
W
-
7
06
/
1
0
LM
W
-
7
11
/
1
0
LM
W
-
7
6/
1
1
LM
W
-
7
11
/
1
1
LM
W
-
7

5/
1
2
LM
W
-
7

11
/
1
2
LM
W
-
7

05
/
1
3
LM
W
-
8

04
/
0
5
LM
W
-
8

10
/
0
5
LM
W
-
8
b

6/
0
6
LM
W
-
8

11
/
0
6
GW
-
L
M
W
-
8 0
6
/
0
7
GW
-
L
M
W
-
8 1
1
/
0
7
GW
-
L
M
W
-
8 0
5
/
0
8
GW
-
L
M
W
-
8 1
1
/
0
8
GW
-
L
M
W
-
8
GW
-
L
M
W
-
8
LM
W
-
8
06
/
1
0
LM
W
-
8
11
/
1
0
LM
W
-
8
6/
1
1
LM
W
-
8
11
/
1
1
LM
W
-
8

5/
1
2
LM
W
-
8

11
/
1
2
LM
W
-
8

05
/
1
3
LM
W
-
9

04
/
0
5
MW
-
D
U
P
2

04
/
0
5
LM
W
-
9

10
/
0
5
LM
W
-
9

6/
0
6
LM
W
-
9

11
/
0
6
GW
-
L
M
W
-
9 0
6
/
0
7
GW
-
L
M
W
-
9 1
1
/
0
7
GW
-
L
M
W
-
9 0
5
/
0
8
GW
-
L
M
W
-
9 1
1
/
0
8
LM
W
-
9
06
/
0
9
LM
W
-
9
11
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0
9
LM
W
-
9
06
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1
0
LM
W

-
9
11
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1
0
LM
W

-
9
6/
1
1
LM
W

-
9
11
/
1
1
LM
W

-
9

5/
1
2
LM
W

-
9

11
/
1
2
LM
W

-
9

05
/
1
3
LM
W
-
1
0

04
/
0
5
LM
W
-
1
0

10
/
0
5
LM
W
-
1
0

6/
0
6
LM
W
-
1
0

11
/
0
6
GW
-
L
M
W
-
10

0
6
/
0
7
GW
-
B
L
K

11
/
0
6
GW
-
L
M
W
-
10

1
1
/
0
7
GW
-
L
M
W
-
10

0
5
/
0
8
GW
-
L
M
W
-
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1
1
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8
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.43J BRL BRL BRL
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRL0.25 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRL0.21 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRL2824.22 J BRL NS NS 7.5 J BRL 11 J BRL BRL BRL NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 5.6 J BRL NS NA NA BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NA BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.5 J BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRL0.27J 0.43J 0.300J BRL 0.35 J 0.35 J BRL 2.4 BRL 1.1 BRL 1.5 1.7 3.2 2.7 NS BRL 0.44 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLvBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.71 J BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 2.02 9.35 2.5 BRL 3.4 4.66 2.42BRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL0.230J BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL 0.41 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL BRL BRL BRL BRL BRL NS NS BRL 3.0 J B BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.69 J 0.63 J 0.49 JBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL 0.22 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL 0.6J BRL 0.370J BRL 0.22 J 0.22 J 0.22 J 0.31 J 0.26 J 0.25 J 0.19 J BRL BRL BRL BRL NS BRL 1.87 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 4.940.850J BRL BRL BRL BRL 0.5 J NS NS BRL 1.3 BRL BRL 0.94 J 0.39 J BRL BRL BRL BRL BRL BRL BRL 0.39 J BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL 0.52 J BRL 0.41 J BRL BRL 0.39 J BRL BRL BRL BRL 0.26 J BRL BRL BRL BRL 0.57J BRL BRL 0.24 J
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRL0.22 J 0.22 J BRL 0.24J 0.23J BRL BRL BRL BRL BRL 0.41 J 0.19 J 0.29 J 0.14 J BRL 0.23 J 0.23 J 0.19 J NS BRL 0.83 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.16 J 0.14 J BRL BRL BRL 0.39 J 0.56J 0.91J 0.440J BRL BRL 0.48 J BRL 0.58 J
BRL 2.5 4.79 BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.26J 2.07 7.01 3.3 BRL 7.73 10.6 BRLBRLBRLBRLBRLBRLBRLNSNSBRL0.22 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL BRL BRL BRL BRL BRL NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL 1.05 J BRL BRL 10.8 BRL NS NS BRL 1.8 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.49 J 0.53 J 0.43 J 0.48 J 0.81 J 1.2 1.3 1.7 NS 1.04 J BRL BRL 1.52J BRL 1.12 J BRL BRL 8.7 1.1 J BRL 0.58 J 1.6 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.15 J BRL BRL BRL BRL11.6 27.4 6.28 5.48 J 7 12 NS NS 5.2 13 8.5 7.6 6.9 4.3 48.5 38.1 40 32.0 34.0 41.0 34.9 29 40 40 30 44 32 45 39 38 NS BRL BRL BRL 10 3.84 6.29 3 J 2.71 4 3.1 2.9 2.8 4 3.3 3.4 13 21 10 13.5 BRL 20 11.9 21.3 BRL 16.7 12 12.7NANANANANA0.15 J NS NS NA 0.34 BRL 0.094 J 0.092 J BRL NA NA NA NA NA NA NA NA NA NA NA NA BRL BRL BRL BRL NS NA NA NA NA NA NA NA NA NA 0.089 J NA NS 0.12 J BRL BRL 0.27 0.38 0.2 NA NA NA NA NA NA NA NA NABRLBRLBRLBRLBRL1.2 NS NS 0.6 4.9 0.68 0.24 J 0.25 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.94J BRL BRL BRL BRL BRL BRL1.03 BRL BRL BRL BRL 0.63 NS NS 0.19 J 2.7 0.44 0.29 0.41 0.11 J BRL BRL BRL BRL BRL BRL 0.83 J BRL 0.47 0.71 0.78 0.71 1.5 1.4 1.2 0.98 NS BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.15 J 0.13 J 0.13 J 0.16 J 0.13 J 0.11 J 1.3 1.8 0.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL5.28 24.7 BRL 7.18 BRL 5.8 NS NS 0.25 J 12 0.27 J 0.37 J 1.6 0.24 J BRL BRL BRL BRL BRL BRL BRL BRL 0.28 J 0.69 J 0.35 J 0.16 J 0.18 J BRL BRL BRL NS BRL BRL BRL 10J BRL 7.14 BRL BRL BRL 1.2 0.62 J 0.44 J 2.1 0.56 J BRL 0.32 J 0.44 J 0.20 J BRL BRL BRL BRL 2.72 J BRL BRL BRL BRL6.64 6.05 J 7.53 J BRL BRL 4 NS NS 3.8 13 3.5 2.1 1.5 1.1 BRL BRL BRL BRL BRL 6 J BRL BRL 0.75 J 0.65 J 1.3 0.75 J 0.48 J 2.1 0.46 J BRL NS BRL BRL BRL 10J BRL 5.28 J 7 J BRL BRL 0.88 J 0.59 J 2.4 1.7 0.65 J 0.78 J 4.2 5 2.8 BRL BRL BRL BRL BRL BRL 5.41 J 2.79 J BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL9400BRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL200BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL1.81 3.51 BRL BRL 0.533 J 0.88 NS NS 0.86 2.5 0.36 0.4 0.26 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 0.525 J BRL BRL 0.87J 0.989J 1.40 BRL 1.41 BRL 0.17 J BRL 0.16 J 0.57 BRL BRL 0.097 J 0.094 J 0.096 J BRL BRL 0.78J BRL 4.15 BRL BRL BRL 0.524 JBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL150BRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL1.4 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL4.23 7.73 4.71 J 2.42 3 J 5.5 NS NS 1.7 7.5 1.5 4.2 2.1 BRL BRL BRL BRL 1.72J BRL BRL 1.76 J BRL 0.61 0.64 0.69 J 0.65 J 0.95 J 1.3 0.55 J 0.64 J NS BRL BRL BRL BRL BRL 3.26 J BRL 1.49 J 9 0.33 J 0.46 J BRL 0.63 J 0.96 J 0.55 J 2.4 3.5 1.5 BRL BRL BRL BRL BRL BRL 3.24 J 1.53 J BRLBRLBRLBRLBRLBRLBRLNSNSBRL0.30 J 0.86 BRL BRL BRL 3.28 1.67J 1.87J 1.67J 1.04 J 3.73 J BRL BRL 0.64 0.59 0.33 J 0.66 BRL 0.22 J BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.28 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.11 J BRL 0.11 J BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.13 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLNSNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL3.56J 14.8 BRL BRL BRL 2.9 J NS NS BRL 7 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 8.4 J 8.4 J BRL 30 BRL 7.06 BRL 2.78 J BRL 2.6 J BRL BRL 5 BRL BRL BRL BRL BRL BRL BRL 8.0J BRL 3.12 J BRL BRL BRL BRL21.6 51.0 BRL 10.9 BRL BRL NS NS 9.5 J 59 15 11 6.4 J BRL BRL BRL BRL BRL BRL BRL 5.20 J BRL 8.2 J 19 4.5 J 3.2 11J 24 BRL BRL NS BRL BRL BRL 20J BRL 17.1 J BRL 7.93 J BRL BRL 7 J 4.4 J 4.5 J 3.7 J 6.6 J BRL 12 J 3.7 J BRL BRL BRL BRL BRL BRL BRL 40.8 BRL
NA NA NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA 360 J 790 J BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL BRL NS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL BRL BRL NA NA NA NA NA NA NA NA NA
0.119 295 528 130 113 NA NS NS 560 J 86 J 120 J NA NA NA NA BRL NA 0.216 398 527 570 466 NA 740 J 0.45 J 610 260 BRL NA NA NA NA NA BRL NA 0.10 17,200 222 460 236 NA 450 J 450 J 94 J 110 J 98 J NA NA NA NA BRL NA 0.551 1,020 BRL 964 410 513Note: BRL -- Below Rep
**Used values for Chlordane; <> -- Data not recieved from laboratory; ^value changed based on Data Validation.
Note: BRL -- Below Reporting Limit; NA -- Not Available; NS -- Not Sampled; U -- Target analytes were not detected above the reporting limits; J -- Analyte was present but concentration is an estimated value; Bold--Concentration exceeds NC 2L Std; * No MCL, used PRG; #Used total values;
Lamont
Table 4. Summary of Groundwater DetectionsLamont Landfills, Fort Bragg, NC Page 3
VOCs (EPA 8260B)
1,1,2,2-tetrachloroethane 0.17 NA1,1-dichloroethane 700 810*1,2,3-trichloropropane 0.005 NA1,2,4-trichlorobenzene 70 701,2,4-trimethylbenzene 350 15 *1,2-dibromo-3-chloropropane 0.025 0.21,2-dibromoethane 0.0004 0.051,2-dichloroethane 0.38 5
1,2-dichloropropane 0.56 51,4-dichlorobenzene 75 75
2-butanone NA NA4-Isopropyltoluene NA NA
4-Methyl-2-pentanone (MIBK)NA NAacetone700NAacroleinNANAbenzene15carbon disulfide 700 NAchlorobenzene50100chloroethane28004.6*chloroform 70 80chloromethane (methyl chloride)2.6 NAcis-1,2-dichloroethene 70 70dibromochloromethane0.41 80dichlorodifluoromethane1400390*diisopropyl ether 70 NA
isopropylbenzene 70 660*m&p xylene 530#10000#
methylene chloride (dichloromethane)4.6 5MTBE20013*
o-xylene 530#10000#sec-butylbenzene 70 NA
tetrachloroethene 0.7 5toluene10001000
trans-1,2-dichloroethene 70 100trichloroethene2.8 5
trichlorofluoromethane 2100 1300*Total Xylenes 530 0.01
vinyl chloride 0.015 2
Metals (EPA 6010B/6020A)
Arsenic 10 10Barium20002000BerylliumNA4Cadmium55CobaltNANAChromium50100Copper10001000Iron300NALead1515Manganese50NANickel100730*Selenium 50 50Silver17.5 180ThalliumNA2TinNANAVanadiumNA260*Zinc 2100 5000
Other Analyses
Mercury 1.05 NA
Nitrate-NO3 NA NA
Nitrate/Nitrite as N (SM 4500)1,000 1,000
COMPOUNDS (µg/L)Groundwater NC 2L
Standard (ug/l)
EPA Drinking water MCL (ug/l)
LM
W
-
1
0
06
/
0
9
LM
W
-
1
0
11
/
0
9
LM
W
-
1
0
06
/
1
0
LM
W
-
1
0
11
/
1
0
LM
W
-
1
0
6/
1
1
LM
W
-
1
0
11
/
1
1
LM
W
-
1
0

5/
1
2
LM
W
-
1
0

11
/
1
2
LM
W
-
1
0

05
/
1
3
LM
W
-
1

11
/
0
6
LM
W
-
3
S

11
/
0
6
GW
-
L
M
W
-
3S

0
6
/
0
7
GW
-
L
M
W
-
3S

1
1
/
0
7
GW
-
L
M
W
-
3S

0
5
/
0
8
GW
-
L
M
W
-
3S

1
1
/
0
8
LM
W
-
3
S
06
/
0
9
LM
W
-
3
S
11
/
0
9
LM
W
-
3
S
06
/
1
0
LM
W
-
3
S
11
/
1
0
LM
W
-
3
S
6/1
1
LM
W
-
3
S
11
/
1
1
LM
W
-
3
S

5/1
2
LM
W
-
3
S

11
/
1
2
LM
W
-
3
S

05
/
1
3
LM
W
-
9
D

11
/
0
6
GW
-
L
M
W
-
9D

0
6
/
0
7
GW
-
L
M
W
-
9D

1
1
/
0
7
GW
-
L
M
W
-
9D

0
5
/
0
8
GW
-
L
M
W
-
9D

1
1
/
0
8
LM
W
-
9
D
06
/
0
9
LM
W
-
9
D
11
/
0
9
LM
W
-
9
D
06
/
1
0
LM
W
-
9
D

11
/
1
0
LM
W
-
9
D

6/1
1
LM
W
-
9
D

11
/
1
1
LM
W
-
9
D

5/1
2
LM
W
-
9
D

11
/
1
2
LM
W
-
9
D

05
/
1
3
LM
W
-
9
S

11
/
0
6
GW
-
L
M
W
-
9S

0
6
/
0
7
GW
-
L
M
W
-
9S

1
1
/
0
7
GW
-
L
M
W
-
9S

0
5
/
0
8
GW
-
L
M
W
-
9S

1
1
/
0
8
LM
W
-
9
S
06
/
0
9
LM
W
-
9
S
11
/
0
9
LM
W
-
9
S
06
/
1
0
LM
W
-
9
S
11
/
1
0
LM
W
-
9
S
6/1
1
LM
W
-
9
S
11
/
1
1
LM
W
-
9
S

5/1
2
LM
W
-
9
S

11
/
1
2
LM
W
-
9
S

05
/
1
3
LM
W
-
1
5

11
/
0
6
LM
W
-
1
6

11
/
0
6
GW
-
L
M
W
-
16

0
6
/
0
7
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.66 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.76 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.82 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.43 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.24 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRL0.22 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.44 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRL5.8 J BRL BRL BRL 1.60J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL1.3 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.20 J 0.14 J 0.23 J BRL 0.25 J 0.15 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL2.08 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.20 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL 4.9 BRL BRL BRL 10 6.7 6.2 3.9 BRL 12.6 BRL BRL 0.62 J 2.76 BRL BRL 4 2.3 0.76 J BRL 2.1 3.2 1.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL 2.4 J 2.2 J 1.8 J 1.9 J 1.2 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 3.2 J B BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 3.4 J B BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.33 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL 0.24 J BRL 0.27 J BRL 0.35 J 0.28 J 0.29 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRL0.38 J BRL BRL BRL BRL BRL BRL 1.4 1.4 BRL 0.22 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.30 J BRL BRL BRL BRL 0.43 J BRL BRL BRL BRL BRL BRL BRL BRL 0.20 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.240J BRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL0.88 J 1.7 1.1 0.97 J 1.4 1.9 1.4 1.6 0.63 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.13 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
6.6 13 5.8 7.3 3.7 14 14 13 7.9 BRL 0.330J BRL 1.03 J 0.52 J 1.05 J 1.1 0.97 J 1.4 1.1 0.36 J 0.80 J 1.2 1.7 0.97 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1 0.84 J BRL BRL BRL BRL 7.67 7.66 BRL 3.84 3.39 2.1 2 1.8 2 3.2 2.5 2.6 5.3 BRL BRL 1.68 J 4.54 BRL BRL 2.1 0.47 J 0.57 J 1.2 0.46 J 0.47 J 0.54 J 1.2 1.1 BRL BRL 2.13131212142123232525BRL5.95 18.7 13 8.86 13.8 12 10 12 16 14 5.4 13 14 12 13.9 5.57 120 10.1 3 3.1 2.9 2.1 2.8 3.8 2.8 2.5 1.9 10 77.3 80.9 2 75.3 61 3.1 48 38 53 59 66 39 68 46 37.4 23.1 41.3NANANANABRLBRLBRLBRLBRLNANANANANANA0.076 J NA NA 0.12 J 0.10 J BRL BRL BRL 0.073 J NA NA NA NA NA NA NA NA NA BRL BRL BRL BRL 0.2 NA NA NA NA NA NA NA NA 0.071 J BRL BRL BRL BRL BRL NA NA NABRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL BRL BRL BRL BRL BRL BRL BRL BRL BRL0.13 J 0.15 J 0.2 0.16 J 0.23 0.19 J 0.25 0.23 0.21 BRL BRL BRL BRL 0.53 J BRL 0.42 0.42 0.57 0.53 0.45 0.2 0.52 0.61 0.5 BRL BRL 3 BRL BRL BRL BRL BRL 0.081 J 0.13 J BRL BRL BRL 0.7 1.27 1.04 J BRL 1.13 BRL BRL 0.25 0.16 J 0.26 0.87 1.1 1 0.89 1 BRL BRL BRL0.36 J 0.26 J 0.36 J 0.30 J 0.61 J 0.33 J 0.44 J 0.55 J 0.44 J BRL BRL 11.6 BRL BRL BRL 1.7 J 0.54 J 0.37 J 4.1 3.3 BRL BRL BRL BRL 6.51 BRL BRL 3.32 J BRL 1 1.1 0.5 J 0.58 J 3.1 BRL 0.35 J 0.98 J 0.20 J BRL 5.73 BRL BRL BRL BRL 0.44 J 0.58 J 4.4 BRL 0.27 J BRL BRL BRL BRL BRL 20.70.51 J BRL 1.9 0.39 J 0.35 J 0.57 J BRL BRL 0.24 J 8.51 2.54J BRL 6 BRL BRL BRL 0.82 J BRL 1.7 1.3 1.1 0.81 J 0.99 J 0.81 J 6.37 BRL 9 2.63 J BRL 0.69 J 0.75 J 0.9 J 0.53 J BRL 0.94 J 0.63 J 0.66 J 2.8 BRL BRL 7 BRL BRL 0.69 J 1.7 1.7 1.6 0.49 J 0.88 J 0.23 J BRL 0.25 J 3.66J BRL 7.37 JBRLBRL41 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 41 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 150 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 360 BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRL0.11 J BRL BRL BRL 0.25 J BRL BRL BRL BRL 3.71 1.47 BRL BRL 0.58 BRL 0.093 J 1.7 1.7 BRL BRL BRL BRL 3.60 3.97 0.68 3.94 BRL 0.71 0.31 0.23 J 0.44 0.46 0.12 J 0.49 0.29 J 0.096 J BRL 2.16 1.19 BRL 0.761 0.71 0.21 J 0.11 J 0.55 BRL BRL BRL BRL BRL 0.559J 0.643J 5.28BRLBRL1.1 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 23 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.5 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 13 BRL BRL BRL BRL BRL BRL BRL BRL BRL0.38 J 0.5 J BRL BRL 0.70 J 0.89 J BRL 0.71 J 0.42 J BRL 2.41 4.92 J 5 3.72 3.7 J 2.6 2.8 4.1 3.1 3.1 0.95 J 2.8 3 2.7 2.16 BRL BRL 1.45 J BRL 0.55 J 0.69 0.53 J 0.60 J 2.5 0.75 J BRL 0.73 J 1.5 1.15J BRL BRL 1.51 J BRL 0.55 J 0.97 J BRL 0.44 J 0.67 J 0.85 J BRL 0.71 J BRL 1.80J 1.03J BRLBRLBRLBRLBRL2.8 3.1 4.3 5 3.9 1.15J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 4.95 J BRL BRL BRL BRL BRL BRL 0.49 J BRL BRL BRL BRL 4.56 4.53 BRL BRL BRL BRL BRL BRL 0.26 J 0.38 J 0.22 J BRL 0.25 J BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL33BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL2BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.13 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRL0.63 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.67 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL9.91 BRL BRL BRL 2.1 J BRL BRL 4.6 J 3.2 J BRL BRL BRL BRL 10.0 5.73 BRL 5.5 5 2.5 J 2.3 J 1.8 J 2.3 J 2.6 J 2.0 J 2.4 J 3.9 J BRL BRL 5.99 BRL BRL BRL 2.5 J BRL BRL 6.2 BRL BRL BRL BRL BRL BRL BRL 41.9BRL213.6 J 5.3 J 4.2 J 5.5 J BRL BRL BRL BRL 10.1 16.6 J 48 15.2 BRL BRL 13 BRL 11 7.6 J 5.5 J 11 12 8.8 J 7.91 BRL BRL 18 BRL 3.5 J 25 5.6 5.1 J 13 14 2.7 J 5.3 J 3.7 J BRL BRL BRL 32.2 BRL 3.5 J 15 B 3.5 J 3.6 J BRL 8.2 J BRL BRL BRL 14.0 BRL 16.5 J
NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA NA 0.42 NA NA NA NA NA NA
NA NA NA NA NA NA 1300 1300 1,100 NA NA NA NA NA NA NA NA NA NA NA NA 820 J 770 J 920 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
NA 2,400 3,700 520 580 510 NA NA NA BRL 0.321 196 228 550 343 NA 710 J BRL 88 J 150 J 240 J NA NA NA 0.107 461 39 BRL 130 NA 430 J 580 J 97 J 130 J 330 85 J NA NA 0.19 1,000 147 BRL 132 NA 770 J 600 J 210 J BRL50 BRL50 BRL NA NA 4.78 0.0520 166
Lamont
porting Limit; NA -- Not Available; NS -- Not Sampled; U -- Target analytes were not detected above the reporting limits; J -- Analyte was present but concentration is an estimated value; Bold--Concentration exceeds NC 2L Std; * No MCL, used PRG; Note: BRL -- Below Reporting Limit; NA -- N
#Used total values; **Used values for Chlordane; <> -- Data not recieved from laboratory; ^value changed based on Data Validation.
Table 4. Summary of Groundwater DetectionsLamont Landfills, Fort Bragg, NC Page 4
VOCs (EPA 8260B)
1,1,2,2-tetrachloroethane 0.17 NA1,1-dichloroethane 700 810*1,2,3-trichloropropane 0.005 NA1,2,4-trichlorobenzene 70 701,2,4-trimethylbenzene 350 15 *1,2-dibromo-3-chloropropane 0.025 0.21,2-dibromoethane 0.0004 0.051,2-dichloroethane 0.38 5
1,2-dichloropropane 0.56 51,4-dichlorobenzene 75 75
2-butanone NA NA4-Isopropyltoluene NA NA
4-Methyl-2-pentanone (MIBK)NA NAacetone700NAacroleinNANAbenzene15carbon disulfide 700 NAchlorobenzene50100chloroethane28004.6*chloroform 70 80chloromethane (methyl chloride)2.6 NAcis-1,2-dichloroethene 70 70dibromochloromethane0.41 80dichlorodifluoromethane1400390*diisopropyl ether 70 NA
isopropylbenzene 70 660*m&p xylene 530#10000#
methylene chloride (dichloromethane)4.6 5MTBE20013*
o-xylene 530#10000#sec-butylbenzene 70 NA
tetrachloroethene 0.7 5toluene10001000
trans-1,2-dichloroethene 70 100trichloroethene2.8 5
trichlorofluoromethane 2100 1300*Total Xylenes 530 0.01
vinyl chloride 0.015 2
Metals (EPA 6010B/6020A)
Arsenic 10 10Barium20002000BerylliumNA4Cadmium55CobaltNANAChromium50100Copper10001000Iron300NALead1515Manganese50NANickel100730*Selenium 50 50Silver17.5 180ThalliumNA2TinNANAVanadiumNA260*Zinc 2100 5000
Other Analyses
Mercury 1.05 NA
Nitrate-NO3 NA NA
Nitrate/Nitrite as N (SM 4500)1,000 1,000
COMPOUNDS (µg/L)Groundwater NC 2L
Standard (ug/l)
EPA Drinking water MCL (ug/l)
GW
-
L
M
W
-
16

1
1
/
0
7
GM
-
L
M
W
-
16

0
5
/
0
8
GW
-
L
M
W
-
16

1
1
/
0
8
LM
W
-
1
6
06
/
0
9
LM
W
-
1
6
11
/
0
9
LM
W
-
1
6
06
/
1
0
LM
W
-
1
6
11
/
1
0
LM
W
-
1
6
6/
1
1
LM
W
-
1
6
11
/
1
1
LM
W
-
1
6

5/
1
2
LM
W
-
1
6

11
/
1
2
LM
W
-
1
6

05
/
1
3
GW
-
L
M
W
-
16
-
D
U
P

GW
-
L
M
W
-
16
-
D
U
P

GW
-
L
M
W
-
14
R

0
6
/
0
7
GW
-
L
M
W
-
14
R

1
1
/
0
7
GW
-
L
M
W
-
14
R

0
5
/
0
8
GW
-
L
M
W
-
14
R

1
1
/
0
8
LM
W
-
1
4
R

06
/
0
9
LM
W
-
1
4
R

11
/
0
9
LM
W
-
1
4
R
06
/
1
0
LM
W
-
1
4
R
11
/
1
0
LM
W
-
1
4
R
6/
1
1
LM
W
-
1
4
R
-
11
/
1
1
LM
W
-
1
4
R

5/
1
2
LM
W
-
1
4
R

11
/
1
2
LM
W
-
1
4
R

05
/
1
3
GW
-
L
M
W
-
14
R

D
U
P

GW
-
L
M
W
-
15
R

0
6
/
0
7
GW
-
L
M
W
-
15
R

1
1
/
0
7
GW
-
L
M
W
-
15
R

0
5
/
0
8
GW
-
L
M
W
-
15
R

1
1
/
0
8
LM
W
-
1
5
R
06
/
0
9
LM
W
-
1
5
R
11
/
0
9
LM
W
-
1
5
R
06
/
1
0
LM
W
-
1
5
R
11
/
1
0
LM
W
-
1
5
R
6/
1
1
LM
W
-
1
5
R
11
/
1
1
LM
W
-
1
5
R

5/
1
2
LM
W
-
1
5
R

11
/
1
2
LM
W
-
1
5
R

05
/
1
3
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.3 J BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.0 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRL8.8 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL1.8 BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.47 J BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL 3.1 J B BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 3.1 J B BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.24 J BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRL0.61 J BRL BRL BRL BRL BRL BRL BRL BRL 0.29 J BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
BRL BRL 9.27 0.56 J 0.59 J 0.5 J 0.54 J 1 0.54 J 1.8 1.1 2.1 BRL 11 1.11 J BRL BRL 9.08 0.41 J BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL 12.7 2.5 BRL BRL BRL BRL BRL BRL BRL BRL3522.9 23 14 13 8.8 10 11 8.8 9.2 9.2 8 29 4 J 14.6 12 9.72 133 13 12 13 12 11 14 13 13 11 NS 38.5 27 24.3 37.6 42 14 36 30 25 32 32 30 29NANANANANANANABRLBRLBRLBRLBRLNANANANANANANANANANA1.8 BRL BRL BRL BRL NA NA NA NA NA 0.29 NA 0.17 J 0.13 J 0.13 J BRL 0.15 J 0.15 J 0.15 JBRLBRL0.002 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRLBRLBRLBRL0.08 J 0.098 J 0.078 J 0.13 J BRL 0.14 J 0.11 J 0.18 J BRL BRL BRL BRL 0.51 J BRL 0.24 0.3 0.17 J 0.21 0.2 0.18 J 0.15 J 0.19 J 0.12 J NS BRL BRL 0.65 J BRL 0.83 0.26 0.7 0.58 0.75 0.6 0.58 0.57 0.52 JBRLBRLBRL0.83 J 0.53 J 0.56 J 0.70 J BRL BRL 0.94 J 1.8 BRL BRL BRL BRL BRL BRL 1.6 0.53 J 0.49 J 0.60 J 1.2 0.18 J 0.35 J 0.37 J 0.50 J NS BRL BRL BRL BRL 5.5 0.16 J 0.51 J 0.24 J 0.20 J BRL BRL 0.16 J 0.18 J6BRL5 J 0.36 J 0.59 J BRL 0.46 J 0.67 J 0.95 J 0.27 J 0.30 J 0.78 J 6 BRL BRL BRL BRL BRL 0.81 J 0.92 J BRL 0.96 J 2 0.72 J 0.41 J BRL 0.70 J NS 5.33 J 5 J BRL 5.2 J 3.7 0.57 J BRL 2.3 0.59 J 0.74 J 0.51 J BRL 0.58 JBRLBRLBRLBRLBRL150BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL43 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 110 BRL BRL BRL BRL BRL BRL2.62 BRL BRL BRL 0.099 J 0.26 J BRL <0.16 J BRL BRL BRL BRL 4.21 BRL 4.42 BRL BRL BRL 0.22 J 0.14 J 0.10 J 0.11 J 0.3 BRL 0.12 J BRL 0.12 J NS BRL BRL BRL 1.08 0.89 BRL 0.08 J 0.16 J 0.48 BRL 0.15 J BRL 0.087 JBRLBRLBRLBRLBRL1.1 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.3J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.6 J BRL BRL BRL BRL BRL BRLBRLBRLBRL0.72 0.66 0.97 J BRL 0.65 J 0.90 J 0.55 J 0.95 J 0.70 J BRL BRL BRL BRL 2.39 3.2 J 2.2 1.6 J 0.84 J 1.9 1.8 1.6 0.65 J 1.1 0.44 J NS BRL BRL 1.12 J BRL 3 0.8 J 1 0.98 J 0.93 J 0.90 J 0.60 J 0.78 J 2.22.20 J BRL BRL BRL BRL BRL 0.31 J BRL 0.25 J BRL 0.21 J BRL 2.50 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL 0.24 J BRL BRL BRL 0.32 J BRL 0.24 J BRL BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.17 J BRL BRL BRL BRL 0.11 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.14 JBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL69BRLBRLBRLBRLBRLBRL2.7 J BRL BRL 1.5 J BRL 26 BRL 2.30 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS BRL BRL BRL BRL 7.5 BRL BRL BRL BRL BRL BRL BRL BRLBRL15.8 BRL BRL 9.3 J 7.9 J 5.4 J 5.1 J 12 3.8 J BRL BRL BRL BRL 15.4 J BRL 18.2 BRL 6.3 J 26 B 4.9 J 4.5 J 10 10 6.7 J BRL BRL NS BRL BRL 39.3 BRL 6.5 J 9.1 J 6.6 J 8.3 J 8.6 J 8.5 J BRL BRL BRL
NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA BRL NA NA NA NA NA NA NA NA NA NA NA NA NA BRL NA NA NA
NA NA NA NA NA NA NA NA NA BRL BRL BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 7400 6,800
1020 380 33 J NA BRL < 40 72 180 J 240 J NA NA NA 1010 < 40 326 143 370 960 NA BRL BRL 72 350 120 J 360 NA NA 2260 1,400 1620 BRL 1460 NA 7,300 H 21000 1600 68,000 J 1,800 1,600.0 NA NA
Lamont
Not Available; NS -- Not Sampled; U -- Target analytes were not detected above the reporting limits; J -- Analyte was present but concentration is an estimated value; Bold--Concentration exceeds NC 2L Std; * No MCL, used PRG; #Used total values; **Used values for Chlordane; <> -- Data not recieved from laboratory; ^value changed based on Data Validation.

APPENDIX A
GROUNDWATER SAMPLING LOGS

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 5/01/13
SAMPLED BY: R. Hill & C. Poston TIME : 1455
WEATHER CONDITIONS: Cloudy 61⁰

Location: Lamont street Landfill Sample ID: LMW-14R-5-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA

4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1515 1529 1540
pH 5.02 5.00 4.94
Sp. Cond 0.020 0.019 0.019
Temp. °C 17.38 17.5 17.50
Turbidity 15.0 13.2 5.99
DO 6.85 6.72 6.67
ORP 164.5 157.6 156.5
Water Level 52.54 52.50 52.50

5. NOTES: MS/MSD taken 1545

Well Depth (wd):56.9 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):52.28 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =0.76 (gallons)
Flow Rate:189 (ml/min)Purge Vol:2.3 (gallons)
Length of Time Purged:45 (minutes)Sample Time:1540
Amount Purged:3.0 (gallons)Pump Depth:55

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05/02/13
SAMPLED BY: R. Hill & C. Poston TIME : 0832
WEATHER CONDITIONS: Cloudy 60⁰

Location: Lamont street Landfill Sample ID: LMW-15R-5-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):46.4 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):40.82 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =0.92 (gallons)
Flow Rate:237 (ml/min)Purge Vol:1.8 (gallons)
Length of Time Purged:30 (minutes)Sample Time:832
Amount Purged:1.9 (gallons)Pump Depth:44.5
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 0820 0827 0832
pH 4.54 4.58 4.60
Sp. Cond 0.043 0.044 0.044
Temp. °C 17.58 17.57 17.53
Turbidity 8.67 5.11 3.33
DO 7.14 7.00 6.98
ORP 169.3 174.5 174.5
Water Level 41.57 41.60 41.61

5. NOTES: Dup taken at 1230/ DUP1-5-13

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05/03/12
SAMPLED BY: R. Hill & C. Poston TIME : 0950
WEATHER CONDITIONS: Partly Cloudy 64°

Location: Lamont street Landfill Sample ID: LMW-9S-5-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):61.34 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):55.43 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =0.97 (gallons)
Flow Rate:350 (ml/min)Purge Vol:2.5 (gallons)
Length of Time Purged:27 (minutes)Sample Time:950
Amount Purged:2.6 (gallons)Pump Depth:59
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 0935 0940 0945 0950
pH 5.85 5.86 5.86 5.86
Sp. Cond 0.338 0.343 0.344 0.343
Temp. °C 18.06 18.09 18.16 18.19
Turbidity 4.02 2.06 1.13 1.12
DO 0.55 0.57 0.59 0.57
ORP 64.1 58.5 56.1 53.7
Water Level 55.45 55.45 55.45 55.45

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05/03/13
SAMPLED BY: R. Hill & C. Poston TIME : 0850
WEATHER CONDITIONS: Partly Cloudy 60°

Location: Lamont street Landfill Sample ID: LMW-9D-05-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):86.98 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):82.61 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =0.72 (gallons)
Flow Rate:189 (ml/min)Purge Vol:1.5 (gallons)
Length of Time Purged:30 (minutes)Sample Time:846
Amount Purged:1.5 (gallons)Pump Depth:85.5
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 0835 0846
pH 6.33 6.39
Sp. Cond 0.052 0.055
Temp. °C 16.93 16.12
Turbidity 35.4 106
DO 6.89 6.03
ORP 118 119.5
Water Level 84.56 84.62

5. NOTES: Turbidity increase therefore sample was taken @ 850

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05/02/13
SAMPLED BY: R. Hill & C. Poston TIME : 1450
WEATHER CONDITIONS: Cloudy 63°

Location: Lamont street Landfill Sample ID: LMW-10-05-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):83.11 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):80.25 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =0.47 (gallons)
Flow Rate:54 (ml/min)Purge Vol:1.0 (gallons)
Length of Time Purged:70 (minutes)Purge Time:1445
Amount Purged:1.0 (gallons)Pump Depth:82
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1415 1425 1435 1445
pH 5.05 5.03 5.01 5.00
Sp. Cond 0.056 0.056 0.056 0.057
Temp. °C 21.38 21.67 19.26 19.18
Turbidity 40.2 25.2 18.5 6.04
DO 5.91 6.57 5.40 5.31
ORP 100.7 80.2 93.2 98.2
Water Level 80.35 80.35 80.35 80.35

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05-02-13
SAMPLED BY: R. Hill & C. Poston TIME : 1255
WEATHER CONDITIONS: Cloudy 61°

Location: Lamont street Landfill Sample ID: LMW-7-05-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):132 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):125.41 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.08 (gallons)
Flow Rate:2 (ml/min)Purge Vol:< 1 (gallons)
Length of Time Purged:111 (minutes)Sample Time:1255
Amount Purged:< 1 (gallons)Pump Depth:~~
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1121
pH 5.69
Sp. Cond 0.017
Temp. °C 16.75
Turbidity 5.48
DO 8.14
ORP 161.5
Water Level 127.05

5. NOTES: Stopped purging at 1121 because no flow. SHG let well recharge.

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05-02-13
SAMPLED BY: R. Hill & C. Poston TIME : 1031
WEATHER CONDITIONS: Cloudy 60°

Location: Lamont street Landfill Sample ID: LMW-4-05-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):87.11 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):79.85 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.19 (gallons)
Flow Rate:229 (ml/min)Purge Vol:2.0 (gallons)
Length of Time Purged:33 (minutes)Sample Time:1030
Amount Purged:2.0 (gallons)Pump Depth:85
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1005 1015 1025
pH 4.84 4.89 4.84
Sp. Cond 0.027 0.027 0.027
Temp. °C 16.63 16.63 16.63
Turbidity 5.48 6.94 12.9
DO 4.59 4.06 4.21
ORP 157.6 158.8 159.6
Water Level 82.48 82.50 82.55

5. NOTES: Turbidity increasing samples.

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05-01-13
SAMPLED BY: R. Hill & C. Poston TIME : 1140
WEATHER CONDITIONS: Cloudy 62°

Location: Lamont street Landfill Sample ID: LMW-3S-05-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):69.81 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):63.57 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.02 (gallons)
Flow Rate:177 (ml/min)Purge Vol:3.0 (gallons)
Length of Time Purged:64 (minutes)Sample Time:1140
Amount Purged:3.0 (gallons)Pump Depth:68
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1100 1105 1111 1122 1130 1135
pH 4.73 4.75 4.77 4.79 4.80 4.80
Sp. Cond 0.035 0.035 0.034 0.033 0.032 0.032
Temp. °C 16.80 16.92 16.96 16.77 16.71 16.74
Turbidity 12.1 7.21 3.89 2.47 1.73 1.15
DO 2.18 2.53 3.20 3.96 4.00 4.20
ORP 156.4 157.9 158.8 161.3 161.0 160.4
Water Level 65.4 65.4 65.4 65.4 65.4 65.4

5. NOTES: Fecal Coliform sample taken after ½ x vol purged at 5-6-13 @ 1510

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05-1-13
SAMPLED BY: R. Hill & C. Poston TIME : 1415
WEATHER CONDITIONS: Cloudy 61°

Location: Lamont street Landfill Sample ID: LMW-3-05-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):122.99 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):106.27 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =2.74 (gallons)
Flow Rate:118 (ml/min)Purge Vol:2.0 (gallons)
Length of Time Purged:64 (minutes)Sample Time:1415
Amount Purged:2.00 (gallons)Pump Depth:121 (ft)
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1350 1400 1405
pH 4.96 4.95 4.95
Sp. Cond 0.021 0.021 0.021
Temp. °C 16.90 16.76 16.88
Turbidity 1.03 0.70 0.58
DO 5.40 5.44 5.42
ORP 150.7 151.5 151.8
Water Level 108.95 108.93 108.95

5. NOTES:
Fecal coliform sample taken after 1x vol purged. 5-6-13 @ 1535

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05-01-13
SAMPLED BY: R. Hill & C. Poston TIME : 956
WEATHER CONDITIONS: Cloudy 60°

Location: Lamont street Landfill Sample ID: LMW-6-05-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):94.65 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):85.05 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.57 (gallons)
Flow Rate:516 (ml/min)Purge Vol:3.0 (gallons)
Length of Time Purged:22 (minutes)Sample Time:956
Amount Purged:3.0 (gallons)Pump Depth:93
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 0945 0951 0955
pH 5.03 5.04 5.11
Sp. Cond 0.181 0.179 0.177
Temp. °C 17.12 17.17 17.19
Turbidity 3.7 1.92 1.86
DO 0.85 1.02 1.14
ORP 180.2 180.5 180.6
Water Level 85.82 85.80 85.80

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05-02-13
SAMPLED BY: R. Hill & C. Poston TIME : 1630
WEATHER CONDITIONS: Cloudy 67°

Location: Lamont street Landfill Sample ID: LMW-16-05-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):42 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):36.91 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =0.83 (gallons)
Flow Rate:143 (ml/min)Purge Vol:2.5 (gallons)
Length of Time Purged:66 (minutes)Sample Time:1630
Amount Purged:3.0 (gallons)Pump Depth:41
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1531 1541 1551 1601 1611 1621
pH 6.46 6.46 6.48 6.49 6.51 6.51
Sp. Cond 0.352 0.355 0.357 0.358 0.359 0.359
Temp. °C 19.99 19.21 19.45 19.32 19.16 19.14
Turbidity 87.1 86.1 32 15.0 7.0 4.87
DO 2.60 1.51 1.09 0.85 0.66 0.54
ORP 122.1 109.4 98.4 90.2 78.3 68
Water Level 37.91 38.05 38.05 38.05 38.05 38.05

5. NOTES:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 05-03-13
SAMPLED BY: R. Hill & C. Poston TIME : 1350
WEATHER CONDITIONS: Partly Cloudy 67°

Location: Lamont street Landfill Sample ID: LMW-9-05-13

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):135.69 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):87.95 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =7.83 (gallons)
Flow Rate:246 (ml/min)Purge Vol:6.5 (gallons)
Length of Time Purged:100 (minutes)Sample Time:1350
Amount Purged:6.50 (gallons)Pump Depth:132
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2– Hach Digital Titrator

Time 1220 1230 1240 1250 1300 1315 1330 1345
pH 4.63 4.63 4.65 4.67 4.69 4.75 4.77 4.78
Sp. Cond 0.128 0.102 0.093 0.092 0.081 0.072 0.066 0.062
Temp. °C 19.45 19.53 19.43 20.14 19.60 20.17 19.67 19.23
Turbidity 36.1 41.8 45.0 43.3 44.5 37.7 34.8 39.9
DO 1.24 2.46 2.85 3.30 3.55 3.38 3.60 3.56
ORP 203.8 218.6 221.8 224.8 225.6 224.2 223.6 222.1
Water Level 87.99 87.99 87.99 87.99 87.99 87.99 87.99 87.99

5. NOTES: Blank collected at 1515. LMW-8-5-13 unaccessable due to washed out
road and knocked down tree.

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg Lamont St Landfill DATE: 11/28/12
SAMPLED BY: R. Hill & C. Poston TIME : NA
WEATHER CONDITIONS: Sunny 55°

Location: Lamont street Landfill Sample ID: LMW-8-

PRESERVATIVE: Ice, HNO3
ANALYSES REQUESTED: EPA 8260B, 300, 6020A
# OF CONTAINERS: 3
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):88.05 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):49.97 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =6.25 (gallons)
Flow Rate:168.24 (ml/min)Purge Vol:2.0 (gallons)
Length of Time Purged:45 (minutes)Sample Time:NS
Amount Purged:2 (gallons)Pump Depth:60
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556XL
Conductivity Meter – YSI 556XL
Temperature – YSI 556XL
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556XL
ORP Meter – YSI 556XL
CO2 – Hach Digital Titrator

Time
pH
Sp. Cond
Temp. °C
Turbidity
DO
ORP
Water Level

5. NOTES: In-accessable

APPENDIX B
DATA VALIDATION REPORTS
ELECTRONIC ONLY

APPENDIX C
CHAINS OF CUSTODY & LAB ANALYTICAL REPORTS
ELECTRONIC ONLY

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-90002-1
Client Project/Site: Ft.Bragg - Lamont Landfill
For:
U.S. Army Corps of Engineers
PO BOX 889
Savannah, Georgia 31402-0889
Attn: Mr. Kevin Haborak
Authorized for release by:
5/15/2013 3:35:45 PM
Linda Wolfe, Project Manager I
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
TestAmerica Job ID: 680-90002-1
Page 2 of 58 TestAmerica Savannah5/15/2013
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .57
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .58
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-90002-1
Project/Site: Ft.Bragg - Lamont Landfill
Job ID: 680-90002-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: U.S. Army Corps of Engineers
Project: Ft.Bragg - Lamont Landfill
Report Number: 680-90002-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 05/04/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the
cooler at receipt was 2.8 C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples LMW-6-5-13 (680-90002-1), LMW-3-5-13 (680-90002-2), LMW-3S-5-13 (680-90002-3), LMW-14R-5-13 (680-90002-4),
LMW-15R-5-13 (680-90002-5), LMW-4-5-13 (680-90002-6), DUP-1-5-13 (680-90002-7), LMW-7-5-13 (680-90002-8), LMW-10-5-13
(680-90002-9), LMW-16-5-13 (680-90002-10), TRIP BLANK (LOT # 040913) (680-90002-11), LMW-9D-5-13 (680-90002-12), LMW-9S-5-13
(680-90002-13), LMW-9-5-13 (680-90002-14) and BLANK-1-5-13 (680-90002-15) were analyzed for Volatile Organic Compounds (GC-MS)
in accordance with EPA SW-846 Method 8260B. The samples were analyzed on 05/06/2013 and 05/10/2013.
Bromomethane exceeded the rpd limit for the LCS and LCSD in batch 680-275661. Bromomethane and Chloroethane exceeded the rpd
limit for the LCS and LCSD in batch 680-276334/5.
No other difficulties were encountered during the volatiles analyses.
All other quality control parameters were within the acceptance limits.
METALS (ICPMS)
Samples LMW-9D-5-13 (680-90002-12), LMW-9S-5-13 (680-90002-13), LMW-9-5-13 (680-90002-14) and BLANK-1-5-13 (680-90002-15)
were analyzed for Metals (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 05/06/2013 and
analyzed on 05/07/2013.
No difficulties were encountered during the metals analyses.
All quality control parameters were within the acceptance limits.
ANIONS (NITRATE/NITRITE)
Samples LMW-9D-5-13 (680-90002-12), LMW-9S-5-13 (680-90002-13), LMW-9-5-13 (680-90002-14) and BLANK-1-5-13 (680-90002-15)
were analyzed for Anions (Nitrate/Nitrite) in accordance with EPA Method 300.0. The samples were analyzed on 05/04/2013.
Samples LMW-9D-5-13 (680-90002-12)[5X], LMW-9S-5-13 (680-90002-13)[5X], LMW-9-5-13 (680-90002-14)[5X] and BLANK-1-5-13
(680-90002-15)[5X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.
TestAmerica SavannahPage 3 of 58 5/15/2013
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-90002-1
Project/Site: Ft.Bragg - Lamont Landfill
Job ID: 680-90002-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
No difficulties were encountered during the Anions analyses.
All quality control parameters were within the acceptance limits.
TestAmerica SavannahPage 4 of 58 5/15/2013
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Sample Summary
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-90002-1 LMW-6-5-13 Water 05/01/13 09:56 05/04/13 09:40
680-90002-2 LMW-3-5-13 Water 05/01/13 14:15 05/04/13 09:40
680-90002-3 LMW-3S-5-13 Water 05/01/13 11:40 05/04/13 09:40
680-90002-4 LMW-14R-5-13 Water 05/01/13 15:45 05/04/13 09:40
680-90002-5 LMW-15R-5-13 Water 05/02/13 08:35 05/04/13 09:40
680-90002-6 LMW-4-5-13 Water 05/02/13 10:30 05/04/13 09:40
680-90002-7 DUP-1-5-13 Water 05/02/13 12:30 05/04/13 09:40
680-90002-8 LMW-7-5-13 Water 05/02/13 12:55 05/04/13 09:40
680-90002-9 LMW-10-5-13 Water 05/02/13 14:50 05/04/13 09:40
680-90002-10 LMW-16-5-13 Water 05/02/13 16:30 05/04/13 09:40
680-90002-11 TRIP BLANK (LOT # 040913)Water 05/01/13 09:00 05/04/13 09:40
680-90002-12 LMW-9D-5-13 Water 05/03/13 08:50 05/04/13 09:40
680-90002-13 LMW-9S-5-13 Water 05/03/13 09:55 05/04/13 09:40
680-90002-14 LMW-9-5-13 Water 05/03/13 13:50 05/04/13 09:40
680-90002-15 BLANK-1-5-13 Water 05/03/13 15:15 05/04/13 09:40
TestAmerica Savannah
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Method Summary
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL SAV
SW8466020AMetals (ICP/MS)TAL SAV
MCAWW300.0 Anions, Ion Chromatography TAL SAV
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Definitions/Glossary
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Qualifiers
GC/MS VOA
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
Q One or more quality control criteria failed.
J Estimated: The analyte was positively identified; the quantitation is an estimation
Metals
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
General Chemistry
Qualifier Description
J Estimated: The analyte was positively identified; the quantitation is an estimation
Qualifier
U Undetected at the Limit of Detection.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
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Detection Summary
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-6-5-13 Lab Sample ID: 680-90002-1
Trichlorofluoromethane
RL
1.0 ug/L
MDL
0.25
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.64 8260B
Client Sample ID: LMW-3-5-13 Lab Sample ID: 680-90002-2
Chloroform
RL
1.0 ug/L
MDL
0.14
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.33 8260B
Trichlorofluoromethane 1.0 ug/L0.25 Total/NA10.91 J 8260B
Client Sample ID: LMW-3S-5-13 Lab Sample ID: 680-90002-3
Dichlorodifluoromethane
RL
1.0 ug/L
MDL
0.25
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.7 8260B
Trichlorofluoromethane 1.0 ug/L0.25 Total/NA10.97 J 8260B
Client Sample ID: LMW-14R-5-13 Lab Sample ID: 680-90002-4
No Detections.
Client Sample ID: LMW-15R-5-13 Lab Sample ID: 680-90002-5
No Detections.
Client Sample ID: LMW-4-5-13 Lab Sample ID: 680-90002-6
Dichlorodifluoromethane
RL
1.0 ug/L
MDL
0.25
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.42 8260B
Trichlorofluoromethane 1.0 ug/L0.25 Total/NA10.66 J 8260B
Client Sample ID: DUP-1-5-13 Lab Sample ID: 680-90002-7
No Detections.
Client Sample ID: LMW-7-5-13 Lab Sample ID: 680-90002-8
Toluene
RL
1.0 ug/L
MDL
0.33
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.39 8260B
Client Sample ID: LMW-10-5-13 Lab Sample ID: 680-90002-9
Chloroform
RL
1.0 ug/L
MDL
0.14
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.15 8260B
Dichlorodifluoromethane 1.0 ug/L0.25 Total/NA13.9 8260B
Methylene Chloride 5.0 ug/L1.0 Total/NA11.2 J 8260B
Trichloroethene 1.0 ug/L0.13 Total/NA10.63 J 8260B
Trichlorofluoromethane 1.0 ug/L0.25 Total/NA17.9 8260B
Client Sample ID: LMW-16-5-13 Lab Sample ID: 680-90002-10
No Detections.
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: TRIP BLANK (LOT # 040913)Lab Sample ID: 680-90002-11
No Detections.
Client Sample ID: LMW-9D-5-13 Lab Sample ID: 680-90002-12
Arsenic
RL
1.0 ug/L
MDL
0.40
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA14.7 6020A
Barium 1.0 ug/L0.15 Total/NA18.1 6020A
Chromium 1.0 ug/L0.16 Total/NA10.52 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.13 J 6020A
Copper 1.0 ug/L0.21 Total/NA11.4 6020A
Lead 0.30 ug/L0.080 Total/NA10.56 6020A
Nickel 1.0 ug/L0.40 Total/NA11.1 6020A
Thallium 0.20 ug/L0.10 Total/NA10.12 J 6020A
Vanadium 5.0 ug/L1.4 Total/NA13.4 J 6020A
Zinc 10 ug/L2.6 Total/NA15.4 J 6020A
Nitrate-NO3 1.1 mg/L0.36 Total/NA50.41 J 300.0
Client Sample ID: LMW-9S-5-13 Lab Sample ID: 680-90002-13
Arsenic
RL
1.0 ug/L
MDL
0.40
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.1 6020A
Barium 1.0 ug/L0.15 Total/NA1466020A
Cobalt 0.20 ug/L0.078 Total/NA11.0 6020A
Copper 1.0 ug/L0.21 Total/NA10.25 J 6020A
Client Sample ID: LMW-9-5-13 Lab Sample ID: 680-90002-14
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1106020A
Beryllium 0.20 ug/L0.070 Total/NA10.20 6020A
Chromium 1.0 ug/L0.16 Total/NA10.20 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.70 6020A
Copper 1.0 ug/L0.21 Total/NA12.8 6020A
Lead 0.30 ug/L0.080 Total/NA10.096 J 6020A
Nickel 1.0 ug/L0.40 Total/NA11.5 6020A
Zinc 10 ug/L2.6 Total/NA13.7 J 6020A
Client Sample ID: BLANK-1-5-13 Lab Sample ID: 680-90002-15
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.51 6020A
Copper 1.0 ug/L0.21 Total/NA10.32 J 6020A
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-1Client Sample ID: LMW-6-5-13
Matrix: WaterDate Collected: 05/01/13 09:56
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 14:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 14:38 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 14:38 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 14:38 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 14:38 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 14:38 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 14:38 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 14:38 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 14:38 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 14:38 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 14:38 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 14:38 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 14:38 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 14:38 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 14:38 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 14:38 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 14:38 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 14:38 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 14:38 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 14:38 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 14:38 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 14:38 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 14:38 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 14:38 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 14:38 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/06/13 14:38 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 14:38 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 14:38 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 14:38 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 14:38 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 14:38 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 14:38 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 14:38 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 14:38 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 14:38 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 14:38 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 14:38 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 14:38 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 14:38 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 14:38 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 14:38 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 14:38 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 14:38 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 14:38 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 14:38 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 14:38 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 14:38 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 14:38 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 14:38 1Tetrachloroethene0.15 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-1Client Sample ID: LMW-6-5-13
Matrix: WaterDate Collected: 05/01/13 09:56
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene 0.33 U 1.0 0.33 ug/L 05/06/13 14:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.35 ug/L 05/06/13 14:38 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 14:38 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 14:38 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 14:38 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 14:38 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 14:38 1Trichlorofluoromethane0.64 J
1.0 0.41 ug/L 05/06/13 14:38 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 14:38 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 14:38 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 14:38 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 14:38 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 14:38 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 89 70-130 05/06/13 14:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 85 05/06/13 14:38 170-130
Toluene-d8 (Surr)100 05/06/13 14:38 170-130
Lab Sample ID: 680-90002-2Client Sample ID: LMW-3-5-13
Matrix: WaterDate Collected: 05/01/13 14:15
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 15:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 15:08 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 15:08 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 15:08 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 15:08 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 15:08 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 15:08 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 15:08 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 15:08 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 15:08 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 15:08 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 15:08 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 15:08 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 15:08 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 15:08 1Chloroform0.33 J
1.0 0.33 ug/L 05/06/13 15:08 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 15:08 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 15:08 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 15:08 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 15:08 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 15:08 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 15:08 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 15:08 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 15:08 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 15:08 1Dichlorodifluoromethane0.25 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-2Client Sample ID: LMW-3-5-13
Matrix: WaterDate Collected: 05/01/13 14:15
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloroethane 0.25 U 1.0 0.25 ug/L 05/06/13 15:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.10 ug/L 05/06/13 15:08 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 15:08 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 15:08 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 15:08 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 15:08 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 15:08 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 15:08 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 15:08 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 15:08 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 15:08 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 15:08 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 15:08 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 15:08 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 15:08 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 15:08 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 15:08 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 15:08 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 15:08 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 15:08 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 15:08 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 15:08 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 15:08 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 15:08 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 15:08 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 15:08 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 15:08 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 15:08 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 15:08 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 15:08 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 15:08 1Trichlorofluoromethane0.91 J
1.0 0.41 ug/L 05/06/13 15:08 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 15:08 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 15:08 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 15:08 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 15:08 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 15:08 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 87 70-130 05/06/13 15:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 85 05/06/13 15:08 170-130
Toluene-d8 (Surr)99 05/06/13 15:08 170-130
Lab Sample ID: 680-90002-3Client Sample ID: LMW-3S-5-13
Matrix: WaterDate Collected: 05/01/13 11:40
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 15:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-3Client Sample ID: LMW-3S-5-13
Matrix: WaterDate Collected: 05/01/13 11:40
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Benzene 0.25 U 1.0 0.25 ug/L 05/06/13 15:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.16 ug/L 05/06/13 15:38 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 15:38 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 15:38 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 15:38 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 15:38 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 15:38 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 15:38 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 15:38 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 15:38 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 15:38 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 15:38 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 15:38 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 15:38 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 15:38 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 15:38 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 15:38 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 15:38 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 15:38 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 15:38 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 15:38 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 15:38 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 15:38 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 15:38 1Dichlorodifluoromethane1.7
1.0 0.25 ug/L 05/06/13 15:38 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 15:38 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 15:38 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 15:38 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 15:38 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 15:38 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 15:38 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 15:38 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 15:38 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 15:38 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 15:38 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 15:38 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 15:38 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 15:38 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 15:38 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 15:38 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 15:38 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 15:38 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 15:38 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 15:38 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 15:38 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 15:38 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 15:38 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 15:38 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 15:38 1Toluene0.33 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-3Client Sample ID: LMW-3S-5-13
Matrix: WaterDate Collected: 05/01/13 11:40
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2,3-Trichlorobenzene 0.35 U 1.0 0.35 ug/L 05/06/13 15:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 15:38 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 15:38 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 15:38 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 15:38 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 15:38 1Trichlorofluoromethane0.97 J
1.0 0.41 ug/L 05/06/13 15:38 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 15:38 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 15:38 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 15:38 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 15:38 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 15:38 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 89 70-130 05/06/13 15:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 85 05/06/13 15:38 170-130
Toluene-d8 (Surr)97 05/06/13 15:38 170-130
Lab Sample ID: 680-90002-4Client Sample ID: LMW-14R-5-13
Matrix: WaterDate Collected: 05/01/13 15:45
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 16:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 16:08 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 16:08 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 16:08 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 16:08 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 16:08 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 16:08 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 16:08 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 16:08 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 16:08 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 16:08 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 16:08 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 16:08 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 16:08 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 16:08 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 16:08 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 16:08 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 16:08 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 16:08 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 16:08 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 16:08 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 16:08 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 16:08 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 16:08 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 16:08 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/06/13 16:08 11,1-Dichloroethane 0.25 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-4Client Sample ID: LMW-14R-5-13
Matrix: WaterDate Collected: 05/01/13 15:45
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichloroethane 0.10 U 1.0 0.10 ug/L 05/06/13 16:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 05/06/13 16:08 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 16:08 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 16:08 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 16:08 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 16:08 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 16:08 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 16:08 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 16:08 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 16:08 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 16:08 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 16:08 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 16:08 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 16:08 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 16:08 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 16:08 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 16:08 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 16:08 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 16:08 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 16:08 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 16:08 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 16:08 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 16:08 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 16:08 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 16:08 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 16:08 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 16:08 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 16:08 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 16:08 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 16:08 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/06/13 16:08 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 16:08 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 16:08 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 16:08 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 16:08 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 16:08 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 87 70-130 05/06/13 16:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 83 05/06/13 16:08 170-130
Toluene-d8 (Surr)98 05/06/13 16:08 170-130
Lab Sample ID: 680-90002-5Client Sample ID: LMW-15R-5-13
Matrix: WaterDate Collected: 05/02/13 08:35
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 16:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 16:38 1Benzene0.25 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-5Client Sample ID: LMW-15R-5-13
Matrix: WaterDate Collected: 05/02/13 08:35
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Bromobenzene 0.16 U 1.0 0.16 ug/L 05/06/13 16:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.14 ug/L 05/06/13 16:38 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 16:38 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 16:38 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 16:38 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 16:38 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 16:38 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 16:38 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 16:38 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 16:38 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 16:38 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 16:38 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 16:38 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 16:38 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 16:38 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 16:38 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 16:38 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 16:38 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 16:38 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 16:38 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 16:38 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 16:38 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 16:38 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/06/13 16:38 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 16:38 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 16:38 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 16:38 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 16:38 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 16:38 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 16:38 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 16:38 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 16:38 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 16:38 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 16:38 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 16:38 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 16:38 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 16:38 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 16:38 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 16:38 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 16:38 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 16:38 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 16:38 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 16:38 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 16:38 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 16:38 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 16:38 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 16:38 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 16:38 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 16:38 11,2,3-Trichlorobenzene 0.35 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-5Client Sample ID: LMW-15R-5-13
Matrix: WaterDate Collected: 05/02/13 08:35
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2,4-Trichlorobenzene 0.25 U 1.0 0.25 ug/L 05/06/13 16:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.50 ug/L 05/06/13 16:38 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 16:38 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 16:38 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 16:38 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/06/13 16:38 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 16:38 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 16:38 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 16:38 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 16:38 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 16:38 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 88 70-130 05/06/13 16:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 84 05/06/13 16:38 170-130
Toluene-d8 (Surr)97 05/06/13 16:38 170-130
Lab Sample ID: 680-90002-6Client Sample ID: LMW-4-5-13
Matrix: WaterDate Collected: 05/02/13 10:30
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 17:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 17:08 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 17:08 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 17:08 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 17:08 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 17:08 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 17:08 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 17:08 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 17:08 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 17:08 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 17:08 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 17:08 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 17:08 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 17:08 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 17:08 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 17:08 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 17:08 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 17:08 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 17:08 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 17:08 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 17:08 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 17:08 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 17:08 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 17:08 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 17:08 1Dichlorodifluoromethane0.42 J
1.0 0.25 ug/L 05/06/13 17:08 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 17:08 11,2-Dichloroethane 0.10 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-6Client Sample ID: LMW-4-5-13
Matrix: WaterDate Collected: 05/02/13 10:30
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
cis-1,2-Dichloroethene 0.15 U 1.0 0.15 ug/L 05/06/13 17:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.20 ug/L 05/06/13 17:08 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 17:08 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 17:08 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 17:08 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 17:08 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 17:08 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 17:08 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 17:08 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 17:08 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 17:08 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 17:08 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 17:08 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 17:08 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 17:08 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 17:08 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 17:08 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 17:08 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 17:08 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 17:08 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 17:08 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 17:08 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 17:08 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 17:08 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 17:08 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 17:08 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 17:08 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 17:08 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 17:08 1Trichlorofluoromethane0.66 J
1.0 0.41 ug/L 05/06/13 17:08 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 17:08 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 17:08 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 17:08 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 17:08 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 17:08 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 89 70-130 05/06/13 17:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 83 05/06/13 17:08 170-130
Toluene-d8 (Surr)99 05/06/13 17:08 170-130
Lab Sample ID: 680-90002-7Client Sample ID: DUP-1-5-13
Matrix: WaterDate Collected: 05/02/13 12:30
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 17:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 17:38 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 17:38 1Bromobenzene0.16 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-7Client Sample ID: DUP-1-5-13
Matrix: WaterDate Collected: 05/02/13 12:30
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Chlorobromomethane 0.14 U 1.0 0.14 ug/L 05/06/13 17:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 17:38 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 17:38 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 17:38 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 17:38 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 17:38 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 17:38 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 17:38 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 17:38 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 17:38 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 17:38 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 17:38 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 17:38 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 17:38 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 17:38 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 17:38 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 17:38 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 17:38 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 17:38 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 17:38 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 17:38 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 17:38 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/06/13 17:38 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 17:38 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 17:38 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 17:38 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 17:38 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 17:38 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 17:38 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 17:38 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 17:38 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 17:38 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 17:38 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 17:38 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 17:38 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 17:38 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 17:38 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 17:38 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 17:38 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 17:38 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 17:38 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 17:38 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 17:38 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 17:38 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 17:38 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 17:38 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 17:38 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 17:38 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 17:38 11,2,4-Trichlorobenzene 0.25 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-7Client Sample ID: DUP-1-5-13
Matrix: WaterDate Collected: 05/02/13 12:30
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1-Trichloroethane 0.50 U 1.0 0.50 ug/L 05/06/13 17:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.13 ug/L 05/06/13 17:38 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 17:38 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 17:38 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/06/13 17:38 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 17:38 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 17:38 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 17:38 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 17:38 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 17:38 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 88 70-130 05/06/13 17:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 85 05/06/13 17:38 170-130
Toluene-d8 (Surr)99 05/06/13 17:38 170-130
Lab Sample ID: 680-90002-8Client Sample ID: LMW-7-5-13
Matrix: WaterDate Collected: 05/02/13 12:55
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 18:08 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 18:08 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 18:08 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 18:08 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 18:08 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 18:08 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 18:08 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 18:08 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 18:08 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 18:08 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 18:08 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 18:08 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 18:08 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 18:08 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 18:08 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 18:08 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 18:08 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 18:08 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 18:08 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 18:08 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 18:08 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 18:08 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 18:08 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 18:08 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/06/13 18:08 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 18:08 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 18:08 1cis-1,2-Dichloroethene 0.15 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-8Client Sample ID: LMW-7-5-13
Matrix: WaterDate Collected: 05/02/13 12:55
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
trans-1,2-Dichloroethene 0.20 U 1.0 0.20 ug/L 05/06/13 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.11 ug/L 05/06/13 18:08 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 18:08 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 18:08 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 18:08 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 18:08 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 18:08 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 18:08 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 18:08 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 18:08 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 18:08 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 18:08 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 18:08 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 18:08 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 18:08 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 18:08 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 18:08 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 18:08 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 18:08 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 18:08 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 18:08 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 18:08 1Toluene0.39 J
1.0 0.35 ug/L 05/06/13 18:08 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 18:08 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 18:08 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 18:08 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 18:08 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 18:08 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/06/13 18:08 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 18:08 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 18:08 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 18:08 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 18:08 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 18:08 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 89 70-130 05/06/13 18:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 85 05/06/13 18:08 170-130
Toluene-d8 (Surr)99 05/06/13 18:08 170-130
Lab Sample ID: 680-90002-9Client Sample ID: LMW-10-5-13
Matrix: WaterDate Collected: 05/02/13 14:50
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 18:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 18:38 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 18:38 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 18:38 1Chlorobromomethane0.14 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-9Client Sample ID: LMW-10-5-13
Matrix: WaterDate Collected: 05/02/13 14:50
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dichlorobromomethane 0.25 U 1.0 0.25 ug/L 05/06/13 18:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.50 ug/L 05/06/13 18:38 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 18:38 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 18:38 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 18:38 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 18:38 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 18:38 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 18:38 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 18:38 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 18:38 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 18:38 1Chloroform0.15 J
1.0 0.33 ug/L 05/06/13 18:38 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 18:38 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 18:38 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 18:38 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 18:38 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 18:38 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 18:38 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 18:38 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 18:38 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 18:38 1Dichlorodifluoromethane3.9
1.0 0.25 ug/L 05/06/13 18:38 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 18:38 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 18:38 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 18:38 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 18:38 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 18:38 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 18:38 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 18:38 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 18:38 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 18:38 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 18:38 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 18:38 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 18:38 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 18:38 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 18:38 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 18:38 1Methylene Chloride 1.2 J
10 1.0 ug/L 05/06/13 18:38 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 18:38 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 18:38 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 18:38 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 18:38 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 18:38 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 18:38 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 18:38 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 18:38 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 18:38 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 18:38 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 18:38 11,1,1-Trichloroethane 0.50 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-9Client Sample ID: LMW-10-5-13
Matrix: WaterDate Collected: 05/02/13 14:50
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2-Trichloroethane 0.13 U 1.0 0.13 ug/L 05/06/13 18:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.13 ug/L 05/06/13 18:38 1Trichloroethene0.63 J
1.0 0.25 ug/L 05/06/13 18:38 1Trichlorofluoromethane7.9
1.0 0.41 ug/L 05/06/13 18:38 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 18:38 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 18:38 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 18:38 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 18:38 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 18:38 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 88 70-130 05/06/13 18:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 84 05/06/13 18:38 170-130
Toluene-d8 (Surr)98 05/06/13 18:38 170-130
Lab Sample ID: 680-90002-10Client Sample ID: LMW-16-5-13
Matrix: WaterDate Collected: 05/02/13 16:30
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 19:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 19:08 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 19:08 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 19:08 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 19:08 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 19:08 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 19:08 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 19:08 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 19:08 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 19:08 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 19:08 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 19:08 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 19:08 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 19:08 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 19:08 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 19:08 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 19:08 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 19:08 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 19:08 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 19:08 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 19:08 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 19:08 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 19:08 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 19:08 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 19:08 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/06/13 19:08 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 19:08 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 19:08 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 19:08 1trans-1,2-Dichloroethene 0.20 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-10Client Sample ID: LMW-16-5-13
Matrix: WaterDate Collected: 05/02/13 16:30
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloroethene 0.11 U 1.0 0.11 ug/L 05/06/13 19:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.13 ug/L 05/06/13 19:08 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 19:08 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 19:08 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 19:08 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 19:08 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 19:08 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 19:08 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 19:08 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 19:08 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 19:08 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 19:08 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 19:08 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 19:08 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 19:08 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 19:08 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 19:08 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 19:08 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 19:08 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 19:08 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 19:08 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 19:08 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 19:08 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 19:08 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 19:08 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 19:08 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 19:08 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/06/13 19:08 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 19:08 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 19:08 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 19:08 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 19:08 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 19:08 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 87 70-130 05/06/13 19:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 84 05/06/13 19:08 170-130
Toluene-d8 (Surr)96 05/06/13 19:08 170-130
Lab Sample ID: 680-90002-11Client Sample ID: TRIP BLANK (LOT # 040913)
Matrix: WaterDate Collected: 05/01/13 09:00
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 13:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 13:38 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 13:38 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 13:38 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 13:38 1Dichlorobromomethane0.25 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-11Client Sample ID: TRIP BLANK (LOT # 040913)
Matrix: WaterDate Collected: 05/01/13 09:00
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Bromoform 0.50 U 1.0 0.50 ug/L 05/06/13 13:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 2.0 ug/L 05/06/13 13:38 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 13:38 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 13:38 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 13:38 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 13:38 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 13:38 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 13:38 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 13:38 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 13:38 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 13:38 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 13:38 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 13:38 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 13:38 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 13:38 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 13:38 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 13:38 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 13:38 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 13:38 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 13:38 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/06/13 13:38 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 13:38 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 13:38 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 13:38 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 13:38 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 13:38 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 13:38 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 13:38 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 13:38 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 13:38 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 13:38 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 13:38 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 13:38 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 13:38 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 13:38 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 13:38 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 13:38 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 13:38 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 13:38 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 13:38 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 13:38 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 13:38 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 13:38 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 13:38 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 13:38 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 13:38 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 13:38 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 13:38 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 13:38 11,1,2-Trichloroethane 0.13 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-11Client Sample ID: TRIP BLANK (LOT # 040913)
Matrix: WaterDate Collected: 05/01/13 09:00
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Trichloroethene 0.13 U 1.0 0.13 ug/L 05/06/13 13:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 13:38 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/06/13 13:38 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 13:38 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 13:38 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 13:38 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 13:38 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 13:38 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 88 70-130 05/06/13 13:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 86 05/06/13 13:38 170-130
Toluene-d8 (Surr)97 05/06/13 13:38 170-130
Lab Sample ID: 680-90002-12Client Sample ID: LMW-9D-5-13
Matrix: WaterDate Collected: 05/03/13 08:50
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 19:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 19:38 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 19:38 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 19:38 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 19:38 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 19:38 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 19:38 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 19:38 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 19:38 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 19:38 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 19:38 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 19:38 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 19:38 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 19:38 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 19:38 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 19:38 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 19:38 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 19:38 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 19:38 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 19:38 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 19:38 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 19:38 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 19:38 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 19:38 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 19:38 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/06/13 19:38 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 19:38 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 19:38 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 19:38 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 19:38 11,1-Dichloroethene 0.11 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-12Client Sample ID: LMW-9D-5-13
Matrix: WaterDate Collected: 05/03/13 08:50
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichloropropane 0.13 U 1.0 0.13 ug/L 05/06/13 19:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.13 ug/L 05/06/13 19:38 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 19:38 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 19:38 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 19:38 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 19:38 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 19:38 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 19:38 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 19:38 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 19:38 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 19:38 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 19:38 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/06/13 19:38 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/06/13 19:38 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 19:38 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 19:38 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 19:38 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 19:38 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 19:38 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 19:38 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 19:38 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 19:38 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 19:38 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 19:38 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 19:38 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 19:38 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/06/13 19:38 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 19:38 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 19:38 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 19:38 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 19:38 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 19:38 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 86 70-130 05/06/13 19:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 84 05/06/13 19:38 170-130
Toluene-d8 (Surr)98 05/06/13 19:38 170-130
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/06/13 08:38 05/07/13 11:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/06/13 08:38 05/07/13 11:56 1Arsenic4.7
1.0 0.15 ug/L 05/06/13 08:38 05/07/13 11:56 1Barium8.1
0.20 0.070 ug/L 05/06/13 08:38 05/07/13 11:56 1Beryllium0.070 U
0.50 0.20 ug/L 05/06/13 08:38 05/07/13 11:56 1Cadmium0.20 U
1.0 0.16 ug/L 05/06/13 08:38 05/07/13 11:56 1Chromium0.52 J
0.20 0.078 ug/L 05/06/13 08:38 05/07/13 11:56 1Cobalt0.13 J
1.0 0.21 ug/L 05/06/13 08:38 05/07/13 11:56 1Copper1.4
0.30 0.080 ug/L 05/06/13 08:38 05/07/13 11:56 1Lead0.56
1.0 0.40 ug/L 05/06/13 08:38 05/07/13 11:56 1Nickel1.1
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-12Client Sample ID: LMW-9D-5-13
Matrix: WaterDate Collected: 05/03/13 08:50
Date Received: 05/04/13 09:40
Method: 6020A - Metals (ICP/MS) (Continued)
RL MDL
Selenium 0.21 U 0.50 0.21 ug/L 05/06/13 08:38 05/07/13 11:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.20 0.10 ug/L 05/06/13 08:38 05/07/13 11:56 1Silver0.10 U
0.20 0.10 ug/L 05/06/13 08:38 05/07/13 11:56 1Thallium0.12 J
5.0 1.4 ug/L 05/06/13 08:38 05/07/13 11:56 1Vanadium3.4 J
10 2.6 ug/L 05/06/13 08:38 05/07/13 11:56 1Zinc5.4 J
General Chemistry
RL MDL
Nitrate-NO3 0.41 J 1.1 0.36 mg/L 05/04/13 13:19 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-90002-13Client Sample ID: LMW-9S-5-13
Matrix: WaterDate Collected: 05/03/13 09:55
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/10/13 14:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/10/13 14:23 1Benzene0.25 U
1.0 0.16 ug/L 05/10/13 14:23 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/10/13 14:23 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/10/13 14:23 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/10/13 14:23 1Bromoform0.50 U
5.0 2.0 ug/L 05/10/13 14:23 1Bromomethane2.0 U Q
10 1.0 ug/L 05/10/13 14:23 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/10/13 14:23 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/10/13 14:23 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/10/13 14:23 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/10/13 14:23 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/10/13 14:23 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/10/13 14:23 1Chloroethane2.0 U Q
1.0 0.14 ug/L 05/10/13 14:23 1Chloroform0.14 U
1.0 0.33 ug/L 05/10/13 14:23 1Chloromethane0.33 U
1.0 0.17 ug/L 05/10/13 14:23 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/10/13 14:23 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/10/13 14:23 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/10/13 14:23 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/10/13 14:23 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/10/13 14:23 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/10/13 14:23 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/10/13 14:23 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/10/13 14:23 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/10/13 14:23 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/10/13 14:23 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/10/13 14:23 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/10/13 14:23 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/10/13 14:23 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/10/13 14:23 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/10/13 14:23 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/10/13 14:23 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/10/13 14:23 11,1-Dichloropropene 0.25 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-13Client Sample ID: LMW-9S-5-13
Matrix: WaterDate Collected: 05/03/13 09:55
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
cis-1,3-Dichloropropene 0.11 U 1.0 0.11 ug/L 05/10/13 14:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.21 ug/L 05/10/13 14:23 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/10/13 14:23 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/10/13 14:23 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/10/13 14:23 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/10/13 14:23 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/10/13 14:23 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/10/13 14:23 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/10/13 14:23 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/10/13 14:23 1Naphthalene1.0 U
1.0 0.15 ug/L 05/10/13 14:23 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/10/13 14:23 1Styrene0.11 U
1.0 0.33 ug/L 05/10/13 14:23 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/10/13 14:23 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/10/13 14:23 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/10/13 14:23 1Toluene0.33 U
1.0 0.35 ug/L 05/10/13 14:23 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/10/13 14:23 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/10/13 14:23 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/10/13 14:23 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/10/13 14:23 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/10/13 14:23 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/10/13 14:23 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/10/13 14:23 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/10/13 14:23 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/10/13 14:23 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/10/13 14:23 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/10/13 14:23 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 97 70-130 05/10/13 14:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 103 05/10/13 14:23 170-130
Toluene-d8 (Surr)100 05/10/13 14:23 170-130
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/06/13 08:38 05/07/13 12:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/06/13 08:38 05/07/13 12:03 1Arsenic1.1
1.0 0.15 ug/L 05/06/13 08:38 05/07/13 12:03 1Barium46
0.20 0.070 ug/L 05/06/13 08:38 05/07/13 12:03 1Beryllium0.070 U
0.50 0.20 ug/L 05/06/13 08:38 05/07/13 12:03 1Cadmium0.20 U
1.0 0.16 ug/L 05/06/13 08:38 05/07/13 12:03 1Chromium0.16 U
0.20 0.078 ug/L 05/06/13 08:38 05/07/13 12:03 1Cobalt1.0
1.0 0.21 ug/L 05/06/13 08:38 05/07/13 12:03 1Copper0.25 J
0.30 0.080 ug/L 05/06/13 08:38 05/07/13 12:03 1Lead0.080 U
1.0 0.40 ug/L 05/06/13 08:38 05/07/13 12:03 1Nickel0.40 U
0.50 0.21 ug/L 05/06/13 08:38 05/07/13 12:03 1Selenium0.21 U
0.20 0.10 ug/L 05/06/13 08:38 05/07/13 12:03 1Silver0.10 U
0.20 0.10 ug/L 05/06/13 08:38 05/07/13 12:03 1Thallium0.10 U
5.0 1.4 ug/L 05/06/13 08:38 05/07/13 12:03 1Vanadium1.4 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-13Client Sample ID: LMW-9S-5-13
Matrix: WaterDate Collected: 05/03/13 09:55
Date Received: 05/04/13 09:40
Method: 6020A - Metals (ICP/MS) (Continued)
RL MDL
Zinc 2.6 U 10 2.6 ug/L 05/06/13 08:38 05/07/13 12:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/04/13 14:06 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-90002-14Client Sample ID: LMW-9-5-13
Matrix: WaterDate Collected: 05/03/13 13:50
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/10/13 14:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/10/13 14:53 1Benzene0.25 U
1.0 0.16 ug/L 05/10/13 14:53 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/10/13 14:53 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/10/13 14:53 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/10/13 14:53 1Bromoform0.50 U
5.0 2.0 ug/L 05/10/13 14:53 1Bromomethane2.0 U Q
10 1.0 ug/L 05/10/13 14:53 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/10/13 14:53 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/10/13 14:53 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/10/13 14:53 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/10/13 14:53 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/10/13 14:53 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/10/13 14:53 1Chloroethane2.0 U Q
1.0 0.14 ug/L 05/10/13 14:53 1Chloroform0.14 U
1.0 0.33 ug/L 05/10/13 14:53 1Chloromethane0.33 U
1.0 0.17 ug/L 05/10/13 14:53 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/10/13 14:53 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/10/13 14:53 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/10/13 14:53 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/10/13 14:53 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/10/13 14:53 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/10/13 14:53 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/10/13 14:53 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/10/13 14:53 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/10/13 14:53 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/10/13 14:53 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/10/13 14:53 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/10/13 14:53 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/10/13 14:53 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/10/13 14:53 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/10/13 14:53 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/10/13 14:53 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/10/13 14:53 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/10/13 14:53 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/10/13 14:53 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/10/13 14:53 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/10/13 14:53 1Hexachlorobutadiene0.40 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-14Client Sample ID: LMW-9-5-13
Matrix: WaterDate Collected: 05/03/13 13:50
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Isopropylbenzene 0.10 U 1.0 0.10 ug/L 05/10/13 14:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.13 ug/L 05/10/13 14:53 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/10/13 14:53 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/10/13 14:53 14-Methyl-2-pentanone (MIBK)1.0 U
10 0.20 ug/L 05/10/13 14:53 1Methyl tert-butyl ether 0.20 U
5.0 1.0 ug/L 05/10/13 14:53 1Naphthalene1.0 U
1.0 0.15 ug/L 05/10/13 14:53 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/10/13 14:53 1Styrene0.11 U
1.0 0.33 ug/L 05/10/13 14:53 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/10/13 14:53 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/10/13 14:53 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/10/13 14:53 1Toluene0.33 U
1.0 0.35 ug/L 05/10/13 14:53 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/10/13 14:53 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/10/13 14:53 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/10/13 14:53 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/10/13 14:53 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/10/13 14:53 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/10/13 14:53 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/10/13 14:53 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/10/13 14:53 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/10/13 14:53 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/10/13 14:53 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/10/13 14:53 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 98 70-130 05/10/13 14:53 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 104 05/10/13 14:53 170-130
Toluene-d8 (Surr)99 05/10/13 14:53 170-130
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/06/13 08:38 05/07/13 12:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/06/13 08:38 05/07/13 12:10 1Arsenic0.40 U
1.0 0.15 ug/L 05/06/13 08:38 05/07/13 12:10 1Barium10
0.20 0.070 ug/L 05/06/13 08:38 05/07/13 12:10 1Beryllium0.20
0.50 0.20 ug/L 05/06/13 08:38 05/07/13 12:10 1Cadmium0.20 U
1.0 0.16 ug/L 05/06/13 08:38 05/07/13 12:10 1Chromium0.20 J
0.20 0.078 ug/L 05/06/13 08:38 05/07/13 12:10 1Cobalt0.70
1.0 0.21 ug/L 05/06/13 08:38 05/07/13 12:10 1Copper2.8
0.30 0.080 ug/L 05/06/13 08:38 05/07/13 12:10 1Lead0.096 J
1.0 0.40 ug/L 05/06/13 08:38 05/07/13 12:10 1Nickel1.5
0.50 0.21 ug/L 05/06/13 08:38 05/07/13 12:10 1Selenium0.21 U
0.20 0.10 ug/L 05/06/13 08:38 05/07/13 12:10 1Silver0.10 U
0.20 0.10 ug/L 05/06/13 08:38 05/07/13 12:10 1Thallium0.10 U
5.0 1.4 ug/L 05/06/13 08:38 05/07/13 12:10 1Vanadium1.4 U
10 2.6 ug/L 05/06/13 08:38 05/07/13 12:10 1Zinc3.7 J
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-14Client Sample ID: LMW-9-5-13
Matrix: WaterDate Collected: 05/03/13 13:50
Date Received: 05/04/13 09:40
General Chemistry
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/04/13 14:21 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-90002-15Client Sample ID: BLANK-1-5-13
Matrix: WaterDate Collected: 05/03/13 15:15
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 14:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.25 ug/L 05/06/13 14:08 1Benzene0.25 U
1.0 0.16 ug/L 05/06/13 14:08 1Bromobenzene0.16 U
1.0 0.14 ug/L 05/06/13 14:08 1Chlorobromomethane0.14 U
1.0 0.25 ug/L 05/06/13 14:08 1Dichlorobromomethane0.25 U
1.0 0.50 ug/L 05/06/13 14:08 1Bromoform0.50 U
5.0 2.0 ug/L 05/06/13 14:08 1Bromomethane2.0 U Q
10 1.0 ug/L 05/06/13 14:08 12-Butanone (MEK)1.0 U
1.0 0.10 ug/L 05/06/13 14:08 1n-Butylbenzene 0.10 U
1.0 0.16 ug/L 05/06/13 14:08 1sec-Butylbenzene 0.16 U
1.0 0.12 ug/L 05/06/13 14:08 1tert-Butylbenzene 0.12 U
1.0 0.50 ug/L 05/06/13 14:08 1Carbon tetrachloride 0.50 U
1.0 0.25 ug/L 05/06/13 14:08 1Chlorobenzene0.25 U
5.0 2.0 ug/L 05/06/13 14:08 1Chloroethane2.0 U
1.0 0.14 ug/L 05/06/13 14:08 1Chloroform0.14 U
1.0 0.33 ug/L 05/06/13 14:08 1Chloromethane0.33 U
1.0 0.17 ug/L 05/06/13 14:08 12-Chlorotoluene 0.17 U
1.0 0.27 ug/L 05/06/13 14:08 14-Chlorotoluene 0.27 U
1.0 0.10 ug/L 05/06/13 14:08 1Chlorodibromomethane0.10 U
1.0 0.44 ug/L 05/06/13 14:08 11,2-Dibromo-3-Chloropropane 0.44 U
1.0 0.25 ug/L 05/06/13 14:08 1Ethylene Dibromide 0.25 U
1.0 0.21 ug/L 05/06/13 14:08 11,2-Dichlorobenzene 0.21 U
1.0 0.25 ug/L 05/06/13 14:08 11,3-Dichlorobenzene 0.25 U
1.0 0.28 ug/L 05/06/13 14:08 11,4-Dichlorobenzene 0.28 U
1.0 0.25 ug/L 05/06/13 14:08 1Dichlorodifluoromethane0.25 U
1.0 0.25 ug/L 05/06/13 14:08 11,1-Dichloroethane 0.25 U
1.0 0.10 ug/L 05/06/13 14:08 11,2-Dichloroethane 0.10 U
1.0 0.15 ug/L 05/06/13 14:08 1cis-1,2-Dichloroethene 0.15 U
1.0 0.20 ug/L 05/06/13 14:08 1trans-1,2-Dichloroethene 0.20 U
1.0 0.11 ug/L 05/06/13 14:08 11,1-Dichloroethene 0.11 U
1.0 0.13 ug/L 05/06/13 14:08 11,2-Dichloropropane 0.13 U
1.0 0.13 ug/L 05/06/13 14:08 11,3-Dichloropropane 0.13 U
1.0 0.12 ug/L 05/06/13 14:08 12,2-Dichloropropane 0.12 U
1.0 0.25 ug/L 05/06/13 14:08 11,1-Dichloropropene 0.25 U
1.0 0.11 ug/L 05/06/13 14:08 1cis-1,3-Dichloropropene 0.11 U
1.0 0.21 ug/L 05/06/13 14:08 1trans-1,3-Dichloropropene 0.21 U
1.0 0.11 ug/L 05/06/13 14:08 1Ethylbenzene0.11 U
1.0 0.40 ug/L 05/06/13 14:08 1Hexachlorobutadiene0.40 U
1.0 0.10 ug/L 05/06/13 14:08 1Isopropylbenzene0.10 U
1.0 0.13 ug/L 05/06/13 14:08 14-Isopropyltoluene 0.13 U
5.0 1.0 ug/L 05/06/13 14:08 1Methylene Chloride 1.0 U
10 1.0 ug/L 05/06/13 14:08 14-Methyl-2-pentanone (MIBK)1.0 U
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Client Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-90002-15Client Sample ID: BLANK-1-5-13
Matrix: WaterDate Collected: 05/03/13 15:15
Date Received: 05/04/13 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl tert-butyl ether 0.20 U 10 0.20 ug/L 05/06/13 14:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.0 ug/L 05/06/13 14:08 1Naphthalene1.0 U
1.0 0.15 ug/L 05/06/13 14:08 1N-Propylbenzene 0.15 U
1.0 0.11 ug/L 05/06/13 14:08 1Styrene0.11 U
1.0 0.33 ug/L 05/06/13 14:08 11,1,1,2-Tetrachloroethane 0.33 U
1.0 0.18 ug/L 05/06/13 14:08 11,1,2,2-Tetrachloroethane 0.18 U
1.0 0.15 ug/L 05/06/13 14:08 1Tetrachloroethene0.15 U
1.0 0.33 ug/L 05/06/13 14:08 1Toluene0.33 U
1.0 0.35 ug/L 05/06/13 14:08 11,2,3-Trichlorobenzene 0.35 U
1.0 0.25 ug/L 05/06/13 14:08 11,2,4-Trichlorobenzene 0.25 U
1.0 0.50 ug/L 05/06/13 14:08 11,1,1-Trichloroethane 0.50 U
1.0 0.13 ug/L 05/06/13 14:08 11,1,2-Trichloroethane 0.13 U
1.0 0.13 ug/L 05/06/13 14:08 1Trichloroethene0.13 U
1.0 0.25 ug/L 05/06/13 14:08 1Trichlorofluoromethane0.25 U
1.0 0.41 ug/L 05/06/13 14:08 11,2,3-Trichloropropane 0.41 U
1.0 0.33 ug/L 05/06/13 14:08 11,2,4-Trimethylbenzene 0.33 U
1.0 0.33 ug/L 05/06/13 14:08 11,3,5-Trimethylbenzene 0.33 U
1.0 0.18 ug/L 05/06/13 14:08 1Vinyl chloride 0.18 U
1.0 0.27 ug/L 05/06/13 14:08 11-Chlorohexane 0.27 U
10 0.24 ug/L 05/06/13 14:08 1Isopropyl ether 0.24 U
4-Bromofluorobenzene 90 70-130 05/06/13 14:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 86 05/06/13 14:08 170-130
Toluene-d8 (Surr)98 05/06/13 14:08 170-130
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/06/13 08:38 05/07/13 12:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/06/13 08:38 05/07/13 12:16 1Arsenic0.40 U
1.0 0.15 ug/L 05/06/13 08:38 05/07/13 12:16 1Barium0.51 J
0.20 0.070 ug/L 05/06/13 08:38 05/07/13 12:16 1Beryllium0.070 U
0.50 0.20 ug/L 05/06/13 08:38 05/07/13 12:16 1Cadmium0.20 U
1.0 0.16 ug/L 05/06/13 08:38 05/07/13 12:16 1Chromium0.16 U
0.20 0.078 ug/L 05/06/13 08:38 05/07/13 12:16 1Cobalt0.078 U J
1.0 0.21 ug/L 05/06/13 08:38 05/07/13 12:16 1Copper0.32 J
0.30 0.080 ug/L 05/06/13 08:38 05/07/13 12:16 1Lead0.080 U
1.0 0.40 ug/L 05/06/13 08:38 05/07/13 12:16 1Nickel0.40 U
0.50 0.21 ug/L 05/06/13 08:38 05/07/13 12:16 1Selenium0.21 U
0.20 0.10 ug/L 05/06/13 08:38 05/07/13 12:16 1Silver0.10 U
0.20 0.10 ug/L 05/06/13 08:38 05/07/13 12:16 1Thallium0.10 U
5.0 1.4 ug/L 05/06/13 08:38 05/07/13 12:16 1Vanadium1.4 U
10 2.6 ug/L 05/06/13 08:38 05/07/13 12:16 1Zinc2.6 U
General Chemistry
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/04/13 14:37 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Surrogate Summary
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-130)(70-130)(70-130)
BFB DBFM TOL
89 85 100680-90002-1
Percent Surrogate Recovery (Acceptance Limits)
LMW-6-5-13
87 85 99680-90002-2 LMW-3-5-13
89 85 97680-90002-3 LMW-3S-5-13
87 83 98680-90002-4 LMW-14R-5-13
89 87 97680-90002-4 MS LMW-14R-5-13
101 97 107680-90002-4 MSD LMW-14R-5-13
88 84 97680-90002-5 LMW-15R-5-13
89 83 99680-90002-6 LMW-4-5-13
88 85 99680-90002-7 DUP-1-5-13
89 85 99680-90002-8 LMW-7-5-13
88 84 98680-90002-9 LMW-10-5-13
87 84 96680-90002-10 LMW-16-5-13
88 86 97680-90002-11 TRIP BLANK (LOT # 040913)
86 84 98680-90002-12 LMW-9D-5-13
97 103 100680-90002-13 LMW-9S-5-13
98 104 99680-90002-14 LMW-9-5-13
90 86 98680-90002-15 BLANK-1-5-13
96 88 98LCS 680-275661/4 Lab Control Sample
98 94 96LCS 680-276334/4 Lab Control Sample
89 83 91LCSD 680-275661/5 Lab Control Sample Dup
105 103 104LCSD 680-276334/5 Lab Control Sample Dup
88 85 97MB 680-275661/7 Method Blank
97 105 98MB 680-276334/7 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-275661/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/06/13 13:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.25 U 0.251.0 ug/L 05/06/13 13:08 1Benzene
0.16 U 0.161.0 ug/L 05/06/13 13:08 1Bromobenzene
0.14 U 0.141.0 ug/L 05/06/13 13:08 1Chlorobromomethane
0.25 U 0.251.0 ug/L 05/06/13 13:08 1Dichlorobromomethane
0.50 U 0.501.0 ug/L 05/06/13 13:08 1Bromoform
2.0 U 2.05.0 ug/L 05/06/13 13:08 1Bromomethane
1.0 U 1.010 ug/L 05/06/13 13:08 12-Butanone (MEK)
0.10 U 0.101.0 ug/L 05/06/13 13:08 1n-Butylbenzene
0.16 U 0.161.0 ug/L 05/06/13 13:08 1sec-Butylbenzene
0.12 U 0.121.0 ug/L 05/06/13 13:08 1tert-Butylbenzene
0.50 U 0.501.0 ug/L 05/06/13 13:08 1Carbon tetrachloride
0.25 U 0.251.0 ug/L 05/06/13 13:08 1Chlorobenzene
2.0 U 2.05.0 ug/L 05/06/13 13:08 1Chloroethane
0.14 U 0.141.0 ug/L 05/06/13 13:08 1Chloroform
0.33 U 0.331.0 ug/L 05/06/13 13:08 1Chloromethane
0.17 U 0.171.0 ug/L 05/06/13 13:08 12-Chlorotoluene
0.27 U 0.271.0 ug/L 05/06/13 13:08 14-Chlorotoluene
0.10 U 0.101.0 ug/L 05/06/13 13:08 1Chlorodibromomethane
0.44 U 0.441.0 ug/L 05/06/13 13:08 11,2-Dibromo-3-Chloropropane
0.25 U 0.251.0 ug/L 05/06/13 13:08 1Ethylene Dibromide
0.21 U 0.211.0 ug/L 05/06/13 13:08 11,2-Dichlorobenzene
0.25 U 0.251.0 ug/L 05/06/13 13:08 11,3-Dichlorobenzene
0.28 U 0.281.0 ug/L 05/06/13 13:08 11,4-Dichlorobenzene
0.25 U 0.251.0 ug/L 05/06/13 13:08 1Dichlorodifluoromethane
0.25 U 0.251.0 ug/L 05/06/13 13:08 11,1-Dichloroethane
0.10 U 0.101.0 ug/L 05/06/13 13:08 11,2-Dichloroethane
0.15 U 0.151.0 ug/L 05/06/13 13:08 1cis-1,2-Dichloroethene
0.20 U 0.201.0 ug/L 05/06/13 13:08 1trans-1,2-Dichloroethene
0.11 U 0.111.0 ug/L 05/06/13 13:08 11,1-Dichloroethene
0.13 U 0.131.0 ug/L 05/06/13 13:08 11,2-Dichloropropane
0.13 U 0.131.0 ug/L 05/06/13 13:08 11,3-Dichloropropane
0.12 U 0.121.0 ug/L 05/06/13 13:08 12,2-Dichloropropane
0.25 U 0.251.0 ug/L 05/06/13 13:08 11,1-Dichloropropene
0.11 U 0.111.0 ug/L 05/06/13 13:08 1cis-1,3-Dichloropropene
0.21 U 0.211.0 ug/L 05/06/13 13:08 1trans-1,3-Dichloropropene
0.11 U 0.111.0 ug/L 05/06/13 13:08 1Ethylbenzene
0.40 U 0.401.0 ug/L 05/06/13 13:08 1Hexachlorobutadiene
0.10 U 0.101.0 ug/L 05/06/13 13:08 1Isopropylbenzene
0.13 U 0.131.0 ug/L 05/06/13 13:08 14-Isopropyltoluene
1.0 U 1.05.0 ug/L 05/06/13 13:08 1Methylene Chloride
1.0 U 1.010 ug/L 05/06/13 13:08 14-Methyl-2-pentanone (MIBK)
0.20 U 0.2010 ug/L 05/06/13 13:08 1Methyl tert-butyl ether
1.0 U 1.05.0 ug/L 05/06/13 13:08 1Naphthalene
0.15 U 0.151.0 ug/L 05/06/13 13:08 1N-Propylbenzene
0.11 U 0.111.0 ug/L 05/06/13 13:08 1Styrene
0.33 U 0.331.0 ug/L 05/06/13 13:08 11,1,1,2-Tetrachloroethane
0.18 U 0.181.0 ug/L 05/06/13 13:08 11,1,2,2-Tetrachloroethane
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-275661/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
RL MDL
Tetrachloroethene 0.15 U 1.0 0.15 ug/L 05/06/13 13:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.33 U 0.331.0 ug/L 05/06/13 13:08 1Toluene
0.35 U 0.351.0 ug/L 05/06/13 13:08 11,2,3-Trichlorobenzene
0.25 U 0.251.0 ug/L 05/06/13 13:08 11,2,4-Trichlorobenzene
0.50 U 0.501.0 ug/L 05/06/13 13:08 11,1,1-Trichloroethane
0.13 U 0.131.0 ug/L 05/06/13 13:08 11,1,2-Trichloroethane
0.13 U 0.131.0 ug/L 05/06/13 13:08 1Trichloroethene
0.25 U 0.251.0 ug/L 05/06/13 13:08 1Trichlorofluoromethane
0.41 U 0.411.0 ug/L 05/06/13 13:08 11,2,3-Trichloropropane
0.33 U 0.331.0 ug/L 05/06/13 13:08 11,2,4-Trimethylbenzene
0.33 U 0.331.0 ug/L 05/06/13 13:08 11,3,5-Trimethylbenzene
0.18 U 0.181.0 ug/L 05/06/13 13:08 1Vinyl chloride
0.27 U 0.271.0 ug/L 05/06/13 13:08 11-Chlorohexane
0.24 U 0.2410 ug/L 05/06/13 13:08 1Isopropyl ether
4-Bromofluorobenzene 88 70-130 05/06/13 13:08 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
85 05/06/13 13:08 1Dibromofluoromethane70-130
97 05/06/13 13:08 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-275661/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
Acetone 100 115 ug/L 115 39 -162
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 50.7 ug/L 101 74 -123
Bromobenzene 50.0 46.3 ug/L 93 79 -125
Chlorobromomethane 50.0 42.1 ug/L 84 60 -136
Dichlorobromomethane 50.0 54.7 ug/L 109 72 -129
Bromoform 50.0 44.3 ug/L 89 60 -134
Bromomethane 50.0 38.6 ug/L 77 10 -171
2-Butanone (MEK)100 107 ug/L 107 55 -142
n-Butylbenzene 50.0 50.2 ug/L 100 72 -128
sec-Butylbenzene 50.0 48.2 ug/L 96 71 -130
tert-Butylbenzene 50.0 47.9 ug/L 96 72 -130
Carbon tetrachloride 50.0 51.5 ug/L 103 70 -131
Chlorobenzene 50.0 46.3 ug/L 93 79 -120
Chloroethane 50.0 38.2 ug/L 76 47 -148
Chloroform 50.0 45.7 ug/L 91 76 -128
Chloromethane 50.0 48.7 ug/L 97 47 -151
2-Chlorotoluene 50.0 47.0 ug/L 94 78 -126
4-Chlorotoluene 50.0 46.0 ug/L 92 79 -124
Chlorodibromomethane 50.0 50.6 ug/L 101 63 -134
1,2-Dibromo-3-Chloropropane 50.0 40.5 ug/L 81 57 -126
Ethylene Dibromide 50.0 49.1 ug/L 98 75 -127
1,2-Dichlorobenzene 50.0 45.9 ug/L 92 77 -124
1,3-Dichlorobenzene 50.0 47.3 ug/L 95 79 -123
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-275661/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
1,4-Dichlorobenzene 50.0 46.1 ug/L 92 76 -124
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Dichlorodifluoromethane 50.0 45.4 ug/L 91 41 -165
1,1-Dichloroethane 50.0 47.9 ug/L 96 69 -132
1,2-Dichloroethane 50.0 57.9 ug/L 116 75 -120
cis-1,2-Dichloroethene 50.0 44.0 ug/L 88 78 -127
trans-1,2-Dichloroethene 50.0 42.8 ug/L 86 78 -130
1,1-Dichloroethene 50.0 38.8 ug/L 78 73 -134
1,2-Dichloropropane 50.0 58.9 ug/L 118 71 -126
1,3-Dichloropropane 50.0 58.2 ug/L 116 73 -125
2,2-Dichloropropane 50.0 48.8 ug/L 98 72 -147
1,1-Dichloropropene 50.0 60.2 ug/L 120 74 -130
cis-1,3-Dichloropropene 50.0 59.5 ug/L 119 73 -128
trans-1,3-Dichloropropene 50.0 60.6 ug/L 121 72 -127
Ethylbenzene 50.0 48.8 ug/L 98 78 -125
Hexachlorobutadiene 50.0 42.4 ug/L 85 62 -145
Isopropylbenzene 50.0 44.8 ug/L 90 72 -129
4-Isopropyltoluene 50.0 48.0 ug/L 96 69 -129
Methylene Chloride 50.0 42.3 ug/L 85 79 -124
4-Methyl-2-pentanone (MIBK)100 104 ug/L 104 51 -143
Methyl tert-butyl ether 100 90.2 ug/L 90 76 -126
Naphthalene 50.0 46.0 ug/L 92 56 -136
N-Propylbenzene 50.0 47.8 ug/L 96 74 -130
Styrene 50.0 48.4 ug/L 97 75 -129
1,1,1,2-Tetrachloroethane 50.0 50.5 ug/L 101 68 -132
1,1,2,2-Tetrachloroethane 50.0 46.2 ug/L 92 71 -127
Tetrachloroethene 50.0 45.9 ug/L 92 77 -128
Toluene 50.0 49.8 ug/L 100 77 -125
1,2,3-Trichlorobenzene 50.0 43.6 ug/L 87 63 -136
1,2,4-Trichlorobenzene 50.0 42.7 ug/L 85 67 -134
1,1,1-Trichloroethane 50.0 55.2 ug/L 110 76 -126
1,1,2-Trichloroethane 50.0 48.5 ug/L 97 69 -127
Trichloroethene 50.0 50.1 ug/L 100 80 -120
Trichlorofluoromethane 50.0 46.7 ug/L 93 66 -144
1,2,3-Trichloropropane 50.0 54.3 ug/L 109 74 -126
1,2,4-Trimethylbenzene 50.0 49.7 ug/L 99 72 -129
1,3,5-Trimethylbenzene 50.0 49.9 ug/L 100 72 -130
Vinyl chloride 50.0 44.9 ug/L 90 58 -141
Isopropyl ether 50.0 50.9 ug/L 102 54 -153
4-Bromofluorobenzene 70 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
88Dibromofluoromethane 70 -130
98Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-275661/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
Acetone 100 118 ug/L 118 39 -162 3 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 50.0 46.5 ug/L 93 74 -123 9 30
Bromobenzene 50.0 42.9 ug/L 86 79 -125 8 30
Chlorobromomethane 50.0 46.3 ug/L 93 60 -136 9 30
Dichlorobromomethane 50.0 51.0 ug/L 102 72 -129 7 30
Bromoform 50.0 41.1 ug/L 82 60 -134 7 30
Bromomethane 50.0 22.2 Q ug/L 44 10 -171 54 50
2-Butanone (MEK)100 101 ug/L 101 55 -142 6 30
n-Butylbenzene 50.0 47.0 ug/L 94 72 -128 7 30
sec-Butylbenzene 50.0 44.8 ug/L 90 71 -130 7 30
tert-Butylbenzene 50.0 45.0 ug/L 90 72 -130 6 30
Carbon tetrachloride 50.0 47.4 ug/L 95 70 -131 8 30
Chlorobenzene 50.0 43.1 ug/L 86 79 -120 7 30
Chloroethane 50.0 40.0 ug/L 80 47 -148 5 40
Chloroform 50.0 43.3 ug/L 87 76 -128 5 30
Chloromethane 50.0 49.0 ug/L 98 47 -151 1 30
2-Chlorotoluene 50.0 43.1 ug/L 86 78 -126 8 30
4-Chlorotoluene 50.0 42.3 ug/L 85 79 -124 8 30
Chlorodibromomethane 50.0 46.9 ug/L 94 63 -134 8 50
1,2-Dibromo-3-Chloropropane 50.0 37.1 ug/L 74 57 -126 9 50
Ethylene Dibromide 50.0 45.1 ug/L 90 75 -127 8 30
1,2-Dichlorobenzene 50.0 41.8 ug/L 84 77 -124 9 30
1,3-Dichlorobenzene 50.0 43.5 ug/L 87 79 -123 8 30
1,4-Dichlorobenzene 50.0 42.7 ug/L 85 76 -124 8 30
Dichlorodifluoromethane 50.0 43.0 ug/L 86 41 -165 5 50
1,1-Dichloroethane 50.0 45.7 ug/L 91 69 -132 5 30
1,2-Dichloroethane 50.0 52.7 ug/L 105 75 -120 9 30
cis-1,2-Dichloroethene 50.0 42.0 ug/L 84 78 -127 5 30
trans-1,2-Dichloroethene 50.0 40.8 ug/L 82 78 -130 5 30
1,1-Dichloroethene 50.0 41.0 ug/L 82 73 -134 6 30
1,2-Dichloropropane 50.0 54.9 ug/L 110 71 -126 7 30
1,3-Dichloropropane 50.0 54.0 ug/L 108 73 -125 7 30
2,2-Dichloropropane 50.0 45.8 ug/L 92 72 -147 6 30
1,1-Dichloropropene 50.0 55.5 ug/L 111 74 -130 8 30
cis-1,3-Dichloropropene 50.0 55.3 ug/L 111 73 -128 7 30
trans-1,3-Dichloropropene 50.0 55.4 ug/L 111 72 -127 9 50
Ethylbenzene 50.0 45.8 ug/L 92 78 -125 6 30
Hexachlorobutadiene 50.0 43.1 ug/L 86 62 -145 1 30
Isopropylbenzene 50.0 41.2 ug/L 82 72 -129 8 30
4-Isopropyltoluene 50.0 45.1 ug/L 90 69 -129 6 50
Methylene Chloride 50.0 40.5 ug/L 81 79 -124 4 30
4-Methyl-2-pentanone (MIBK)100 97.2 ug/L 97 51 -143 7 30
Methyl tert-butyl ether 100 84.7 ug/L 85 76 -126 6 30
Naphthalene 50.0 43.0 ug/L 86 56 -136 7 30
N-Propylbenzene 50.0 44.6 ug/L 89 74 -130 7 30
Styrene 50.0 45.0 ug/L 90 75 -129 7 30
1,1,1,2-Tetrachloroethane 50.0 47.0 ug/L 94 68 -132 7 30
1,1,2,2-Tetrachloroethane 50.0 43.8 ug/L 88 71 -127 5 30
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-275661/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
Tetrachloroethene 50.0 43.2 ug/L 86 77 -128 6 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Toluene 50.0 45.3 ug/L 91 77 -125 10 30
1,2,3-Trichlorobenzene 50.0 40.7 ug/L 81 63 -136 7 30
1,2,4-Trichlorobenzene 50.0 40.5 ug/L 81 67 -134 5 30
1,1,1-Trichloroethane 50.0 50.2 ug/L 100 76 -126 9 30
1,1,2-Trichloroethane 50.0 45.2 ug/L 90 69 -127 7 30
Trichloroethene 50.0 46.4 ug/L 93 80 -120 8 30
Trichlorofluoromethane 50.0 49.5 ug/L 99 66 -144 6 30
1,2,3-Trichloropropane 50.0 50.6 ug/L 101 74 -126 7 30
1,2,4-Trimethylbenzene 50.0 46.1 ug/L 92 72 -129 7 50
1,3,5-Trimethylbenzene 50.0 46.3 ug/L 93 72 -130 8 50
Vinyl chloride 50.0 43.9 ug/L 88 58 -141 2 30
Isopropyl ether 50.0 51.8 ug/L 104 54 -153 2 50
4-Bromofluorobenzene 70 -130
Surrogate
89
LCSD LCSD
Qualifier Limits%Recovery
83Dibromofluoromethane 70 -130
91Toluene-d8 (Surr)70 -130
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-90002-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
Acetone 5.0 U 100 75.8 ug/L 76 39 -162
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Benzene 0.25 U 50.0 47.9 ug/L 96 74 -123
Bromobenzene 0.16 U 50.0 43.6 ug/L 87 79 -125
Chlorobromomethane 0.14 U 50.0 52.4 ug/L 105 60 -136
Dichlorobromomethane 0.25 U 50.0 50.4 ug/L 101 72 -129
Bromoform 0.50 U 50.0 42.4 ug/L 85 60 -134
Bromomethane 2.0 U Q 50.0 18.5 ug/L 37 10 -171
2-Butanone (MEK)1.0 U 100 83.8 ug/L 84 55 -142
n-Butylbenzene 0.10 U 50.0 45.3 ug/L 91 72 -128
sec-Butylbenzene 0.16 U 50.0 46.0 ug/L 92 71 -130
tert-Butylbenzene 0.12 U 50.0 46.3 ug/L 93 72 -130
Carbon tetrachloride 0.50 U 50.0 54.7 ug/L 109 70 -131
Chlorobenzene 0.25 U 50.0 44.6 ug/L 89 79 -120
Chloroethane 2.0 U 50.0 43.7 ug/L 87 47 -148
Chloroform 0.14 U 50.0 44.8 ug/L 90 76 -128
Chloromethane 0.33 U 50.0 52.7 ug/L 105 47 -151
2-Chlorotoluene 0.17 U 50.0 45.6 ug/L 91 78 -126
4-Chlorotoluene 0.27 U 50.0 44.4 ug/L 89 79 -124
Chlorodibromomethane 0.10 U 50.0 45.7 ug/L 91 63 -134
1,2-Dibromo-3-Chloropropane 0.44 U 50.0 39.9 ug/L 80 57 -126
Ethylene Dibromide 0.25 U 50.0 46.8 ug/L 94 75 -127
1,2-Dichlorobenzene 0.21 U 50.0 43.3 ug/L 87 77 -124
1,3-Dichlorobenzene 0.25 U 50.0 44.8 ug/L 90 79 -123
1,4-Dichlorobenzene 0.28 U 50.0 43.6 ug/L 87 76 -124
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-90002-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
Dichlorodifluoromethane 0.25 U 50.0 51.2 ug/L 102 41 -165
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,1-Dichloroethane 0.25 U 50.0 45.9 ug/L 92 69 -132
1,2-Dichloroethane 0.10 U 50.0 51.3 ug/L 103 75 -120
cis-1,2-Dichloroethene 0.15 U 50.0 41.2 ug/L 82 78 -127
trans-1,2-Dichloroethene 0.20 U 50.0 42.0 ug/L 84 78 -130
1,1-Dichloroethene 0.11 U 50.0 39.2 ug/L 78 73 -134
1,2-Dichloropropane 0.13 U 50.0 48.2 ug/L 96 71 -126
1,3-Dichloropropane 0.13 U 50.0 47.7 ug/L 95 73 -125
2,2-Dichloropropane 0.12 U 50.0 42.7 ug/L 85 72 -147
1,1-Dichloropropene 0.25 U 50.0 49.6 ug/L 99 74 -130
cis-1,3-Dichloropropene 0.11 U 50.0 47.0 ug/L 94 73 -128
trans-1,3-Dichloropropene 0.21 U 50.0 47.9 ug/L 96 72 -127
Ethylbenzene 0.11 U 50.0 46.9 ug/L 94 78 -125
Hexachlorobutadiene 0.40 U 50.0 40.2 ug/L 80 62 -145
Isopropylbenzene 0.10 U 50.0 46.4 ug/L 93 72 -129
4-Isopropyltoluene 0.13 U 50.0 46.2 ug/L 92 69 -129
Methylene Chloride 1.0 U 50.0 47.0 ug/L 94 79 -124
4-Methyl-2-pentanone (MIBK)1.0 U 100 96.6 ug/L 97 51 -143
Methyl tert-butyl ether 0.20 U 100 78.2 ug/L 78 76 -126
Naphthalene 1.0 U 50.0 39.6 ug/L 79 56 -136
N-Propylbenzene 0.15 U 50.0 46.1 ug/L 92 74 -130
Styrene 0.11 U 50.0 45.9 ug/L 92 75 -129
1,1,1,2-Tetrachloroethane 0.33 U 50.0 46.3 ug/L 93 68 -132
1,1,2,2-Tetrachloroethane 0.18 U 50.0 44.3 ug/L 89 71 -127
Tetrachloroethene 0.15 U 50.0 44.1 ug/L 88 77 -128
Toluene 0.33 U 50.0 48.2 ug/L 96 77 -125
1,2,3-Trichlorobenzene 0.35 U 50.0 38.3 ug/L 77 63 -136
1,2,4-Trichlorobenzene 0.25 U 50.0 38.0 ug/L 76 67 -134
1,1,1-Trichloroethane 0.50 U 50.0 53.2 ug/L 106 76 -126
1,1,2-Trichloroethane 0.13 U 50.0 46.7 ug/L 93 69 -127
Trichloroethene 0.13 U 50.0 46.0 ug/L 92 80 -120
Trichlorofluoromethane 0.25 U 50.0 59.5 ug/L 119 66 -144
1,2,3-Trichloropropane 0.41 U 50.0 45.4 ug/L 91 74 -126
1,2,4-Trimethylbenzene 0.33 U 50.0 47.2 ug/L 94 72 -129
1,3,5-Trimethylbenzene 0.33 U 50.0 46.7 ug/L 93 72 -130
Vinyl chloride 0.18 U 50.0 47.9 ug/L 96 58 -141
4-Bromofluorobenzene 70 -130
Surrogate
89
MS MS
Qualifier Limits%Recovery
87Dibromofluoromethane 70 -130
97Toluene-d8 (Surr)70 -130
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-90002-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
Acetone 5.0 U 100 98.8 ug/L 99 39 -162 26 50
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-90002-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
Benzene 0.25 U 50.0 52.7 ug/L 105 74 -123 10 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromobenzene 0.16 U 50.0 49.7 ug/L 99 79 -125 13 30
Chlorobromomethane 0.14 U 50.0 56.9 ug/L 114 60 -136 8 30
Dichlorobromomethane 0.25 U 50.0 55.2 ug/L 110 72 -129 9 30
Bromoform 0.50 U 50.0 47.5 ug/L 95 60 -134 12 30
Bromomethane 2.0 U Q 50.0 21.6 ug/L 43 10 -171 16 50
2-Butanone (MEK)1.0 U 100 91.0 ug/L 91 55 -142 8 30
n-Butylbenzene 0.10 U 50.0 53.9 ug/L 108 72 -128 17 30
sec-Butylbenzene 0.16 U 50.0 53.9 ug/L 108 71 -130 16 30
tert-Butylbenzene 0.12 U 50.0 53.4 ug/L 107 72 -130 14 30
Carbon tetrachloride 0.50 U 50.0 60.2 ug/L 120 70 -131 10 30
Chlorobenzene 0.25 U 50.0 49.7 ug/L 99 79 -120 11 30
Chloroethane 2.0 U 50.0 49.3 ug/L 99 47 -148 12 40
Chloroform 0.14 U 50.0 48.5 ug/L 97 76 -128 8 30
Chloromethane 0.33 U 50.0 59.9 ug/L 120 47 -151 13 30
2-Chlorotoluene 0.17 U 50.0 51.2 ug/L 102 78 -126 12 30
4-Chlorotoluene 0.27 U 50.0 52.1 ug/L 104 79 -124 16 30
Chlorodibromomethane 0.10 U 50.0 51.1 ug/L 102 63 -134 11 50
1,2-Dibromo-3-Chloropropane 0.44 U 50.0 44.7 ug/L 89 57 -126 11 50
Ethylene Dibromide 0.25 U 50.0 50.8 ug/L 102 75 -127 8 30
1,2-Dichlorobenzene 0.21 U 50.0 49.7 ug/L 99 77 -124 14 30
1,3-Dichlorobenzene 0.25 U 50.0 51.4 ug/L 103 79 -123 14 30
1,4-Dichlorobenzene 0.28 U 50.0 50.1 ug/L 100 76 -124 14 30
Dichlorodifluoromethane 0.25 U 50.0 57.6 ug/L 115 41 -165 12 50
1,1-Dichloroethane 0.25 U 50.0 50.2 ug/L 100 69 -132 9 30
1,2-Dichloroethane 0.10 U 50.0 56.0 ug/L 112 75 -120 9 30
cis-1,2-Dichloroethene 0.15 U 50.0 46.5 ug/L 93 78 -127 12 30
trans-1,2-Dichloroethene 0.20 U 50.0 46.3 ug/L 93 78 -130 10 30
1,1-Dichloroethene 0.11 U 50.0 50.5 ug/L 101 73 -134 25 30
1,2-Dichloropropane 0.13 U 50.0 52.4 ug/L 105 71 -126 8 30
1,3-Dichloropropane 0.13 U 50.0 52.9 ug/L 106 73 -125 10 30
2,2-Dichloropropane 0.12 U 50.0 46.8 ug/L 94 72 -147 9 30
1,1-Dichloropropene 0.25 U 50.0 55.8 ug/L 112 74 -130 12 30
cis-1,3-Dichloropropene 0.11 U 50.0 52.2 ug/L 104 73 -128 10 30
trans-1,3-Dichloropropene 0.21 U 50.0 52.9 ug/L 106 72 -127 10 50
Ethylbenzene 0.11 U 50.0 52.7 ug/L 105 78 -125 12 30
Hexachlorobutadiene 0.40 U 50.0 48.1 ug/L 96 62 -145 18 30
Isopropylbenzene 0.10 U 50.0 53.3 ug/L 107 72 -129 14 30
4-Isopropyltoluene 0.13 U 50.0 53.3 ug/L 107 69 -129 14 50
Methylene Chloride 1.0 U 50.0 51.8 ug/L 104 79 -124 10 30
4-Methyl-2-pentanone (MIBK)1.0 U 100 104 ug/L 104 51 -143 8 30
Methyl tert-butyl ether 0.20 U 100 86.7 ug/L 87 76 -126 10 30
Naphthalene 1.0 U 50.0 47.1 ug/L 94 56 -136 17 30
N-Propylbenzene 0.15 U 50.0 53.2 ug/L 106 74 -130 14 30
Styrene 0.11 U 50.0 51.5 ug/L 103 75 -129 11 30
1,1,1,2-Tetrachloroethane 0.33 U 50.0 51.3 ug/L 103 68 -132 10 30
1,1,2,2-Tetrachloroethane 0.18 U 50.0 48.8 ug/L 98 71 -127 10 30
Tetrachloroethene 0.15 U 50.0 50.2 ug/L 100 77 -128 13 30
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-90002-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275661
Toluene 0.33 U 50.0 53.5 ug/L 107 77 -125 11 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2,3-Trichlorobenzene 0.35 U 50.0 46.3 ug/L 93 63 -136 19 30
1,2,4-Trichlorobenzene 0.25 U 50.0 45.9 ug/L 92 67 -134 19 30
1,1,1-Trichloroethane 0.50 U 50.0 58.8 ug/L 118 76 -126 10 30
1,1,2-Trichloroethane 0.13 U 50.0 51.7 ug/L 103 69 -127 10 30
Trichloroethene 0.13 U 50.0 50.7 ug/L 101 80 -120 10 30
Trichlorofluoromethane 0.25 U 50.0 67.9 ug/L 136 66 -144 13 30
1,2,3-Trichloropropane 0.41 U 50.0 50.4 ug/L 101 74 -126 10 30
1,2,4-Trimethylbenzene 0.33 U 50.0 54.1 ug/L 108 72 -129 13 50
1,3,5-Trimethylbenzene 0.33 U 50.0 54.1 ug/L 108 72 -130 15 50
Vinyl chloride 0.18 U 50.0 54.8 ug/L 110 58 -141 13 30
4-Bromofluorobenzene 70 -130
Surrogate
101
MSD MSD
Qualifier Limits%Recovery
97Dibromofluoromethane 70 -130
107Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-276334/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 276334
RL MDL
Acetone 5.0 U 25 5.0 ug/L 05/10/13 11:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.25 U 0.251.0 ug/L 05/10/13 11:52 1Benzene
0.16 U 0.161.0 ug/L 05/10/13 11:52 1Bromobenzene
0.14 U 0.141.0 ug/L 05/10/13 11:52 1Chlorobromomethane
0.25 U 0.251.0 ug/L 05/10/13 11:52 1Dichlorobromomethane
0.50 U 0.501.0 ug/L 05/10/13 11:52 1Bromoform
2.0 U 2.05.0 ug/L 05/10/13 11:52 1Bromomethane
1.0 U 1.010 ug/L 05/10/13 11:52 12-Butanone (MEK)
0.10 U 0.101.0 ug/L 05/10/13 11:52 1n-Butylbenzene
0.16 U 0.161.0 ug/L 05/10/13 11:52 1sec-Butylbenzene
0.12 U 0.121.0 ug/L 05/10/13 11:52 1tert-Butylbenzene
0.50 U 0.501.0 ug/L 05/10/13 11:52 1Carbon tetrachloride
0.25 U 0.251.0 ug/L 05/10/13 11:52 1Chlorobenzene
2.0 U 2.05.0 ug/L 05/10/13 11:52 1Chloroethane
0.14 U 0.141.0 ug/L 05/10/13 11:52 1Chloroform
0.33 U 0.331.0 ug/L 05/10/13 11:52 1Chloromethane
0.17 U 0.171.0 ug/L 05/10/13 11:52 12-Chlorotoluene
0.27 U 0.271.0 ug/L 05/10/13 11:52 14-Chlorotoluene
0.10 U 0.101.0 ug/L 05/10/13 11:52 1Chlorodibromomethane
0.44 U 0.441.0 ug/L 05/10/13 11:52 11,2-Dibromo-3-Chloropropane
0.25 U 0.251.0 ug/L 05/10/13 11:52 1Ethylene Dibromide
0.21 U 0.211.0 ug/L 05/10/13 11:52 11,2-Dichlorobenzene
0.25 U 0.251.0 ug/L 05/10/13 11:52 11,3-Dichlorobenzene
0.28 U 0.281.0 ug/L 05/10/13 11:52 11,4-Dichlorobenzene
0.25 U 0.251.0 ug/L 05/10/13 11:52 1Dichlorodifluoromethane
0.25 U 0.251.0 ug/L 05/10/13 11:52 11,1-Dichloroethane
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-276334/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 276334
RL MDL
1,2-Dichloroethane 0.10 U 1.0 0.10 ug/L 05/10/13 11:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.15 U 0.151.0 ug/L 05/10/13 11:52 1cis-1,2-Dichloroethene
0.20 U 0.201.0 ug/L 05/10/13 11:52 1trans-1,2-Dichloroethene
0.11 U 0.111.0 ug/L 05/10/13 11:52 11,1-Dichloroethene
0.13 U 0.131.0 ug/L 05/10/13 11:52 11,2-Dichloropropane
0.13 U 0.131.0 ug/L 05/10/13 11:52 11,3-Dichloropropane
0.12 U 0.121.0 ug/L 05/10/13 11:52 12,2-Dichloropropane
0.25 U 0.251.0 ug/L 05/10/13 11:52 11,1-Dichloropropene
0.11 U 0.111.0 ug/L 05/10/13 11:52 1cis-1,3-Dichloropropene
0.21 U 0.211.0 ug/L 05/10/13 11:52 1trans-1,3-Dichloropropene
0.11 U 0.111.0 ug/L 05/10/13 11:52 1Ethylbenzene
0.40 U 0.401.0 ug/L 05/10/13 11:52 1Hexachlorobutadiene
0.10 U 0.101.0 ug/L 05/10/13 11:52 1Isopropylbenzene
0.13 U 0.131.0 ug/L 05/10/13 11:52 14-Isopropyltoluene
1.0 U 1.05.0 ug/L 05/10/13 11:52 1Methylene Chloride
1.0 U 1.010 ug/L 05/10/13 11:52 14-Methyl-2-pentanone (MIBK)
0.20 U 0.2010 ug/L 05/10/13 11:52 1Methyl tert-butyl ether
1.0 U 1.05.0 ug/L 05/10/13 11:52 1Naphthalene
0.15 U 0.151.0 ug/L 05/10/13 11:52 1N-Propylbenzene
0.11 U 0.111.0 ug/L 05/10/13 11:52 1Styrene
0.33 U 0.331.0 ug/L 05/10/13 11:52 11,1,1,2-Tetrachloroethane
0.18 U 0.181.0 ug/L 05/10/13 11:52 11,1,2,2-Tetrachloroethane
0.15 U 0.151.0 ug/L 05/10/13 11:52 1Tetrachloroethene
0.33 U 0.331.0 ug/L 05/10/13 11:52 1Toluene
0.35 U 0.351.0 ug/L 05/10/13 11:52 11,2,3-Trichlorobenzene
0.25 U 0.251.0 ug/L 05/10/13 11:52 11,2,4-Trichlorobenzene
0.50 U 0.501.0 ug/L 05/10/13 11:52 11,1,1-Trichloroethane
0.13 U 0.131.0 ug/L 05/10/13 11:52 11,1,2-Trichloroethane
0.13 U 0.131.0 ug/L 05/10/13 11:52 1Trichloroethene
0.25 U 0.251.0 ug/L 05/10/13 11:52 1Trichlorofluoromethane
0.41 U 0.411.0 ug/L 05/10/13 11:52 11,2,3-Trichloropropane
0.33 U 0.331.0 ug/L 05/10/13 11:52 11,2,4-Trimethylbenzene
0.33 U 0.331.0 ug/L 05/10/13 11:52 11,3,5-Trimethylbenzene
0.18 U 0.181.0 ug/L 05/10/13 11:52 1Vinyl chloride
0.27 U 0.271.0 ug/L 05/10/13 11:52 11-Chlorohexane
0.24 U 0.2410 ug/L 05/10/13 11:52 1Isopropyl ether
4-Bromofluorobenzene 97 70-130 05/10/13 11:52 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
105 05/10/13 11:52 1Dibromofluoromethane70-130
98 05/10/13 11:52 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-276334/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 276334
Acetone 100 101 ug/L 101 39 -162
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-276334/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 276334
Benzene 50.0 46.5 ug/L 93 74 -123
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Bromobenzene 50.0 50.1 ug/L 100 79 -125
Chlorobromomethane 50.0 46.4 ug/L 93 60 -136
Dichlorobromomethane 50.0 52.6 ug/L 105 72 -129
Bromoform 50.0 47.6 ug/L 95 60 -134
Bromomethane 50.0 22.3 ug/L 45 10 -171
2-Butanone (MEK)100 95.6 ug/L 96 55 -142
n-Butylbenzene 50.0 51.3 ug/L 103 72 -128
sec-Butylbenzene 50.0 49.9 ug/L 100 71 -130
tert-Butylbenzene 50.0 49.4 ug/L 99 72 -130
Carbon tetrachloride 50.0 52.0 ug/L 104 70 -131
Chlorobenzene 50.0 47.8 ug/L 96 79 -120
Chloroethane 50.0 36.2 ug/L 72 47 -148
Chloroform 50.0 46.2 ug/L 92 76 -128
Chloromethane 50.0 44.1 ug/L 88 47 -151
2-Chlorotoluene 50.0 49.6 ug/L 99 78 -126
4-Chlorotoluene 50.0 49.8 ug/L 100 79 -124
Chlorodibromomethane 50.0 53.9 ug/L 108 63 -134
1,2-Dibromo-3-Chloropropane 50.0 59.5 ug/L 119 57 -126
Ethylene Dibromide 50.0 51.7 ug/L 103 75 -127
1,2-Dichlorobenzene 50.0 49.6 ug/L 99 77 -124
1,3-Dichlorobenzene 50.0 49.5 ug/L 99 79 -123
1,4-Dichlorobenzene 50.0 49.8 ug/L 100 76 -124
Dichlorodifluoromethane 50.0 52.4 ug/L 105 41 -165
1,1-Dichloroethane 50.0 45.1 ug/L 90 69 -132
1,2-Dichloroethane 50.0 50.0 ug/L 100 75 -120
cis-1,2-Dichloroethene 50.0 44.8 ug/L 90 78 -127
trans-1,2-Dichloroethene 50.0 45.2 ug/L 90 78 -130
1,1-Dichloroethene 50.0 46.9 ug/L 94 73 -134
1,2-Dichloropropane 50.0 47.6 ug/L 95 71 -126
1,3-Dichloropropane 50.0 50.4 ug/L 101 73 -125
2,2-Dichloropropane 50.0 50.7 ug/L 101 72 -147
1,1-Dichloropropene 50.0 48.3 ug/L 97 74 -130
cis-1,3-Dichloropropene 50.0 51.5 ug/L 103 73 -128
trans-1,3-Dichloropropene 50.0 53.7 ug/L 107 72 -127
Ethylbenzene 50.0 47.4 ug/L 95 78 -125
Hexachlorobutadiene 50.0 53.1 ug/L 106 62 -145
Isopropylbenzene 50.0 48.7 ug/L 97 72 -129
4-Isopropyltoluene 50.0 51.0 ug/L 102 69 -129
Methylene Chloride 50.0 46.3 ug/L 93 79 -124
4-Methyl-2-pentanone (MIBK)100 103 ug/L 103 51 -143
Methyl tert-butyl ether 100 98.3 ug/L 98 76 -126
Naphthalene 50.0 59.5 ug/L 119 56 -136
N-Propylbenzene 50.0 49.5 ug/L 99 74 -130
Styrene 50.0 49.8 ug/L 100 75 -129
1,1,1,2-Tetrachloroethane 50.0 51.0 ug/L 102 68 -132
1,1,2,2-Tetrachloroethane 50.0 50.9 ug/L 102 71 -127
Tetrachloroethene 50.0 47.8 ug/L 96 77 -128
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-276334/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 276334
Toluene 50.0 46.6 ug/L 93 77 -125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2,3-Trichlorobenzene 50.0 54.5 ug/L 109 63 -136
1,2,4-Trichlorobenzene 50.0 53.6 ug/L 107 67 -134
1,1,1-Trichloroethane 50.0 50.6 ug/L 101 76 -126
1,1,2-Trichloroethane 50.0 49.0 ug/L 98 69 -127
Trichloroethene 50.0 48.3 ug/L 97 80 -120
Trichlorofluoromethane 50.0 42.1 ug/L 84 66 -144
1,2,3-Trichloropropane 50.0 51.6 ug/L 103 74 -126
1,2,4-Trimethylbenzene 50.0 49.7 ug/L 99 72 -129
1,3,5-Trimethylbenzene 50.0 50.3 ug/L 101 72 -130
Vinyl chloride 50.0 41.8 ug/L 84 58 -141
Isopropyl ether 50.0 44.6 ug/L 89 54 -153
4-Bromofluorobenzene 70 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
94Dibromofluoromethane 70 -130
96Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-276334/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 276334
Acetone 100 106 ug/L 106 39 -162 5 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 50.0 50.9 ug/L 102 74 -123 9 30
Bromobenzene 50.0 53.2 ug/L 106 79 -125 6 30
Chlorobromomethane 50.0 50.9 ug/L 102 60 -136 9 30
Dichlorobromomethane 50.0 54.8 ug/L 110 72 -129 4 30
Bromoform 50.0 45.8 ug/L 92 60 -134 4 30
Bromomethane 50.0 51.8 Q ug/L 104 10 -171 80 50
2-Butanone (MEK)100 101 ug/L 101 55 -142 5 30
n-Butylbenzene 50.0 53.7 ug/L 107 72 -128 5 30
sec-Butylbenzene 50.0 52.3 ug/L 105 71 -130 5 30
tert-Butylbenzene 50.0 52.3 ug/L 105 72 -130 6 30
Carbon tetrachloride 50.0 54.3 ug/L 109 70 -131 4 30
Chlorobenzene 50.0 51.8 ug/L 104 79 -120 8 30
Chloroethane 50.0 63.0 Q ug/L 126 47 -148 54 40
Chloroform 50.0 51.1 ug/L 102 76 -128 10 30
Chloromethane 50.0 49.1 ug/L 98 47 -151 11 30
2-Chlorotoluene 50.0 52.0 ug/L 104 78 -126 5 30
4-Chlorotoluene 50.0 53.6 ug/L 107 79 -124 7 30
Chlorodibromomethane 50.0 54.0 ug/L 108 63 -134 0 50
1,2-Dibromo-3-Chloropropane 50.0 56.8 ug/L 114 57 -126 5 50
Ethylene Dibromide 50.0 54.2 ug/L 108 75 -127 5 30
1,2-Dichlorobenzene 50.0 52.8 ug/L 106 77 -124 6 30
1,3-Dichlorobenzene 50.0 52.8 ug/L 106 79 -123 6 30
1,4-Dichlorobenzene 50.0 53.0 ug/L 106 76 -124 6 30
Dichlorodifluoromethane 50.0 55.7 ug/L 111 41 -165 6 50
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-276334/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 276334
1,1-Dichloroethane 50.0 50.7 ug/L 101 69 -132 12 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,2-Dichloroethane 50.0 54.1 ug/L 108 75 -120 8 30
cis-1,2-Dichloroethene 50.0 50.3 ug/L 101 78 -127 12 30
trans-1,2-Dichloroethene 50.0 50.4 ug/L 101 78 -130 11 30
1,1-Dichloroethene 50.0 51.1 ug/L 102 73 -134 9 30
1,2-Dichloropropane 50.0 52.3 ug/L 105 71 -126 10 30
1,3-Dichloropropane 50.0 53.8 ug/L 108 73 -125 7 30
2,2-Dichloropropane 50.0 53.5 ug/L 107 72 -147 5 30
1,1-Dichloropropene 50.0 52.5 ug/L 105 74 -130 8 30
cis-1,3-Dichloropropene 50.0 54.4 ug/L 109 73 -128 6 30
trans-1,3-Dichloropropene 50.0 54.6 ug/L 109 72 -127 2 50
Ethylbenzene 50.0 50.9 ug/L 102 78 -125 7 30
Hexachlorobutadiene 50.0 58.8 ug/L 118 62 -145 10 30
Isopropylbenzene 50.0 51.7 ug/L 103 72 -129 6 30
4-Isopropyltoluene 50.0 53.8 ug/L 108 69 -129 5 50
Methylene Chloride 50.0 50.6 ug/L 101 79 -124 9 30
4-Methyl-2-pentanone (MIBK)100 108 ug/L 108 51 -143 4 30
Methyl tert-butyl ether 100 106 ug/L 106 76 -126 7 30
Naphthalene 50.0 61.0 ug/L 122 56 -136 3 30
N-Propylbenzene 50.0 53.0 ug/L 106 74 -130 7 30
Styrene 50.0 52.6 ug/L 105 75 -129 5 30
1,1,1,2-Tetrachloroethane 50.0 54.3 ug/L 109 68 -132 6 30
1,1,2,2-Tetrachloroethane 50.0 53.1 ug/L 106 71 -127 4 30
Tetrachloroethene 50.0 51.6 ug/L 103 77 -128 8 30
Toluene 50.0 49.8 ug/L 100 77 -125 7 30
1,2,3-Trichlorobenzene 50.0 56.4 ug/L 113 63 -136 3 30
1,2,4-Trichlorobenzene 50.0 55.7 ug/L 111 67 -134 4 30
1,1,1-Trichloroethane 50.0 53.4 ug/L 107 76 -126 6 30
1,1,2-Trichloroethane 50.0 52.7 ug/L 105 69 -127 7 30
Trichloroethene 50.0 52.7 ug/L 105 80 -120 9 30
Trichlorofluoromethane 50.0 49.8 ug/L 100 66 -144 17 30
1,2,3-Trichloropropane 50.0 54.2 ug/L 108 74 -126 5 30
1,2,4-Trimethylbenzene 50.0 52.3 ug/L 105 72 -129 5 50
1,3,5-Trimethylbenzene 50.0 53.1 ug/L 106 72 -130 6 50
Vinyl chloride 50.0 46.9 ug/L 94 58 -141 11 30
Isopropyl ether 50.0 47.0 ug/L 94 54 -153 5 50
4-Bromofluorobenzene 70 -130
Surrogate
105
LCSD LCSD
Qualifier Limits%Recovery
103Dibromofluoromethane 70 -130
104Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 6020A - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-275574/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275778 Prep Batch: 275574
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/06/13 08:38 05/07/13 11:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.40 U 0.401.0 ug/L 05/06/13 08:38 05/07/13 11:43 1Arsenic
0.15 U 0.151.0 ug/L 05/06/13 08:38 05/07/13 11:43 1Barium
0.070 U 0.0700.20 ug/L 05/06/13 08:38 05/07/13 11:43 1Beryllium
0.20 U 0.200.50 ug/L 05/06/13 08:38 05/07/13 11:43 1Cadmium
0.16 U 0.161.0 ug/L 05/06/13 08:38 05/07/13 11:43 1Chromium
0.078 U 0.0780.20 ug/L 05/06/13 08:38 05/07/13 11:43 1Cobalt
0.21 U 0.211.0 ug/L 05/06/13 08:38 05/07/13 11:43 1Copper
0.080 U 0.0800.30 ug/L 05/06/13 08:38 05/07/13 11:43 1Lead
0.40 U 0.401.0 ug/L 05/06/13 08:38 05/07/13 11:43 1Nickel
0.21 U 0.210.50 ug/L 05/06/13 08:38 05/07/13 11:43 1Selenium
0.10 U 0.100.20 ug/L 05/06/13 08:38 05/07/13 11:43 1Silver
0.10 U 0.100.20 ug/L 05/06/13 08:38 05/07/13 11:43 1Thallium
1.4 U 1.45.0 ug/L 05/06/13 08:38 05/07/13 11:43 1Vanadium
2.6 U 2.610 ug/L 05/06/13 08:38 05/07/13 11:43 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-275574/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275778 Prep Batch: 275574
Antimony 20.0 22.3 ug/L 111 75 -125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 40.0 40.9 ug/L 102 75 -125
Barium 40.0 40.7 ug/L 102 75 -125
Beryllium 20.0 22.4 ug/L 112 75 -125
Cadmium 20.0 21.3 ug/L 106 75 -125
Chromium 40.0 35.1 ug/L 88 75 -125
Cobalt 20.0 16.0 ug/L 80 75 -125
Copper 40.0 35.7 ug/L 89 75 -125
Lead 20.0 19.9 ug/L 100 75 -125
Nickel 40.0 35.2 ug/L 88 75 -125
Selenium 40.0 46.3 ug/L 116 75 -125
Silver 20.0 20.5 ug/L 103 75 -125
Thallium 16.0 15.8 ug/L 99 75 -125
Vanadium 40.0 34.6 ug/L 86 75 -125
Zinc 40.0 43.3 ug/L 108 75 -125
Client Sample ID: BLANK-1-5-13Lab Sample ID: 680-90002-15 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275778 Prep Batch: 275574
Antimony 0.99 U 20.0 22.3 ug/L 111 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 0.40 U 40.0 40.7 ug/L 102 75 -125
Barium 0.51 J 40.0 41.4 ug/L 102 75 -125
Beryllium 0.070 U 20.0 22.8 ug/L 114 75 -125
Cadmium 0.20 U 20.0 21.2 ug/L 106 75 -125
Chromium 0.16 U 40.0 35.8 ug/L 89 75 -125
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: BLANK-1-5-13Lab Sample ID: 680-90002-15 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275778 Prep Batch: 275574
Cobalt 0.078 U J 20.0 16.3 ug/L 81 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Copper 0.32 J 40.0 36.1 ug/L 90 75 -125
Lead 0.080 U 20.0 19.8 ug/L 99 75 -125
Nickel 0.40 U 40.0 36.0 ug/L 90 75 -125
Selenium 0.21 U 40.0 45.7 ug/L 114 75 -125
Silver 0.10 U 20.0 20.5 ug/L 102 75 -125
Thallium 0.10 U 16.0 16.1 ug/L 100 75 -125
Vanadium 1.4 U 40.0 35.3 ug/L 88 75 -125
Zinc 2.6 U 40.0 42.7 ug/L 107 75 -125
Client Sample ID: BLANK-1-5-13Lab Sample ID: 680-90002-15 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275778 Prep Batch: 275574
Antimony 0.99 U 20.0 21.6 ug/L 108 75 -125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 0.40 U 40.0 36.2 ug/L 91 75 -125 12 20
Barium 0.51 J 40.0 40.2 ug/L 99 75 -125 3 20
Beryllium 0.070 U 20.0 21.9 ug/L 110 75 -125 4 20
Cadmium 0.20 U 20.0 20.7 ug/L 103 75 -125 3 20
Chromium 0.16 U 40.0 31.9 ug/L 80 75 -125 11 20
Cobalt 0.078 U J 20.0 14.4 J ug/L 72 75 -125 12 20
Copper 0.32 J 40.0 32.1 ug/L 80 75 -125 12 20
Lead 0.080 U 20.0 18.9 ug/L 95 75 -125 4 20
Nickel 0.40 U 40.0 31.8 ug/L 80 75 -125 12 20
Selenium 0.21 U 40.0 40.7 ug/L 102 75 -125 12 20
Silver 0.10 U 20.0 20.2 ug/L 101 75 -125 1 20
Thallium 0.10 U 16.0 15.6 ug/L 97 75 -125 3 20
Vanadium 1.4 U 40.0 31.6 ug/L 79 75 -125 11 20
Zinc 2.6 U 40.0 37.8 ug/L 94 75 -125 12 20
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 680-275630/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275630
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/04/13 12:33 5
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-275630/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275630
Nitrate-NO3 22.1 21.0 mg/L 95 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
TestAmerica Savannah
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QC Sample Results
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 300.0 - Anions, Ion Chromatography (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-275630/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275630
Nitrate-NO3 22.1 21.0 mg/L 95 90 -110 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: LMW-9D-5-13Lab Sample ID: 680-90002-12 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275630
Nitrate-NO3 0.41 J 22.1 21.8 mg/L 97 90 -110
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: LMW-9D-5-13Lab Sample ID: 680-90002-12 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275630
Nitrate-NO3 0.41 J 22.1 21.0 mg/L 93 90 -110 4 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Savannah
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QC Association Summary
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
GC/MS VOA
Analysis Batch: 275661
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B680-90002-1 LMW-6-5-13 Total/NA
Water 8260B680-90002-2 LMW-3-5-13 Total/NA
Water 8260B680-90002-3 LMW-3S-5-13 Total/NA
Water 8260B680-90002-4 LMW-14R-5-13 Total/NA
Water 8260B680-90002-4 MS LMW-14R-5-13 Total/NA
Water 8260B680-90002-4 MSD LMW-14R-5-13 Total/NA
Water 8260B680-90002-5 LMW-15R-5-13 Total/NA
Water 8260B680-90002-6 LMW-4-5-13 Total/NA
Water 8260B680-90002-7 DUP-1-5-13 Total/NA
Water 8260B680-90002-8 LMW-7-5-13 Total/NA
Water 8260B680-90002-9 LMW-10-5-13 Total/NA
Water 8260B680-90002-10 LMW-16-5-13 Total/NA
Water 8260B680-90002-11 TRIP BLANK (LOT # 040913)Total/NA
Water 8260B680-90002-12 LMW-9D-5-13 Total/NA
Water 8260B680-90002-15 BLANK-1-5-13 Total/NA
Water 8260BLCS 680-275661/4 Lab Control Sample Total/NA
Water 8260BLCSD 680-275661/5 Lab Control Sample Dup Total/NA
Water 8260BMB 680-275661/7 Method Blank Total/NA
Analysis Batch: 276334
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B680-90002-13 LMW-9S-5-13 Total/NA
Water 8260B680-90002-14 LMW-9-5-13 Total/NA
Water 8260BLCS 680-276334/4 Lab Control Sample Total/NA
Water 8260BLCSD 680-276334/5 Lab Control Sample Dup Total/NA
Water 8260BMB 680-276334/7 Method Blank Total/NA
Metals
Prep Batch: 275574
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3030C680-90002-12 LMW-9D-5-13 Total/NA
Water 3030C680-90002-13 LMW-9S-5-13 Total/NA
Water 3030C680-90002-14 LMW-9-5-13 Total/NA
Water 3030C680-90002-15 BLANK-1-5-13 Total/NA
Water 3030C680-90002-15 MS BLANK-1-5-13 Total/NA
Water 3030C680-90002-15 MSD BLANK-1-5-13 Total/NA
Water 3030CLCS 680-275574/2-A Lab Control Sample Total/NA
Water 3030CMB 680-275574/1-A Method Blank Total/NA
Analysis Batch: 275778
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 275574680-90002-12 LMW-9D-5-13 Total/NA
Water 6020A 275574680-90002-13 LMW-9S-5-13 Total/NA
Water 6020A 275574680-90002-14 LMW-9-5-13 Total/NA
Water 6020A 275574680-90002-15 BLANK-1-5-13 Total/NA
Water 6020A 275574680-90002-15 MS BLANK-1-5-13 Total/NA
Water 6020A 275574680-90002-15 MSD BLANK-1-5-13 Total/NA
Water 6020A 275574LCS 680-275574/2-A Lab Control Sample Total/NA
Water 6020A 275574MB 680-275574/1-A Method Blank Total/NA
TestAmerica Savannah
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QC Association Summary
TestAmerica Job ID: 680-90002-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
General Chemistry
Analysis Batch: 275630
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0680-90002-12 LMW-9D-5-13 Total/NA
Water 300.0680-90002-12 MS LMW-9D-5-13 Total/NA
Water 300.0680-90002-12 MSD LMW-9D-5-13 Total/NA
Water 300.0680-90002-13 LMW-9S-5-13 Total/NA
Water 300.0680-90002-14 LMW-9-5-13 Total/NA
Water 300.0680-90002-15 BLANK-1-5-13 Total/NA
Water 300.0LCS 680-275630/3 Lab Control Sample Total/NA
Water 300.0LCSD 680-275630/4 Lab Control Sample Dup Total/NA
Water 300.0MB 680-275630/2 Method Blank Total/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-90002-1
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-6-5-13 Lab Sample ID: 680-90002-1
Matrix: WaterDate Collected: 05/01/13 09:56
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 14:38 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-3-5-13 Lab Sample ID: 680-90002-2
Matrix: WaterDate Collected: 05/01/13 14:15
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 15:08 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-3S-5-13 Lab Sample ID: 680-90002-3
Matrix: WaterDate Collected: 05/01/13 11:40
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 15:38 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-14R-5-13 Lab Sample ID: 680-90002-4
Matrix: WaterDate Collected: 05/01/13 15:45
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 16:08 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-15R-5-13 Lab Sample ID: 680-90002-5
Matrix: WaterDate Collected: 05/02/13 08:35
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 16:38 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-4-5-13 Lab Sample ID: 680-90002-6
Matrix: WaterDate Collected: 05/02/13 10:30
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 17:08 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-90002-1
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: DUP-1-5-13 Lab Sample ID: 680-90002-7
Matrix: WaterDate Collected: 05/02/13 12:30
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 17:38 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-7-5-13 Lab Sample ID: 680-90002-8
Matrix: WaterDate Collected: 05/02/13 12:55
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 18:08 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-10-5-13 Lab Sample ID: 680-90002-9
Matrix: WaterDate Collected: 05/02/13 14:50
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 18:38 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-16-5-13 Lab Sample ID: 680-90002-10
Matrix: WaterDate Collected: 05/02/13 16:30
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 19:08 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: TRIP BLANK (LOT # 040913)Lab Sample ID: 680-90002-11
Matrix: WaterDate Collected: 05/01/13 09:00
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 13:38 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: LMW-9D-5-13 Lab Sample ID: 680-90002-12
Matrix: WaterDate Collected: 05/03/13 08:50
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 19:38 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 275574 05/06/13 08:38 BB TAL SAVTotal/NA
Analysis 6020A 1 275778 05/07/13 11:56 BR TAL SAVTotal/NA
Analysis 300.0 5 275630 05/04/13 13:19 PAT TAL SAVTotal/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-90002-1
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-9S-5-13 Lab Sample ID: 680-90002-13
Matrix: WaterDate Collected: 05/03/13 09:55
Date Received: 05/04/13 09:40
Analysis 8260B 05/10/13 14:23 AJMC1276334 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 275574 05/06/13 08:38 BB TAL SAVTotal/NA
Analysis 6020A 1 275778 05/07/13 12:03 BR TAL SAVTotal/NA
Analysis 300.0 5 275630 05/04/13 14:06 PAT TAL SAVTotal/NA
Client Sample ID: LMW-9-5-13 Lab Sample ID: 680-90002-14
Matrix: WaterDate Collected: 05/03/13 13:50
Date Received: 05/04/13 09:40
Analysis 8260B 05/10/13 14:53 AJMC1276334 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 275574 05/06/13 08:38 BB TAL SAVTotal/NA
Analysis 6020A 1 275778 05/07/13 12:10 BR TAL SAVTotal/NA
Analysis 300.0 5 275630 05/04/13 14:21 PAT TAL SAVTotal/NA
Client Sample ID: BLANK-1-5-13 Lab Sample ID: 680-90002-15
Matrix: WaterDate Collected: 05/03/13 15:15
Date Received: 05/04/13 09:40
Analysis 8260B 05/06/13 14:08 AJMC1275661 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3030C 275574 05/06/13 08:38 BB TAL SAVTotal/NA
Analysis 6020A 1 275778 05/07/13 12:16 BR TAL SAVTotal/NA
Analysis 300.0 5 275630 05/04/13 14:37 PAT TAL SAVTotal/NA
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Login Sample Receipt Checklist
Client: U.S. Army Corps of Engineers Job Number: 680-90002-1
Login Number: 90002
Question Answer Comment
Creator: Conner, Keaton
List Source: TestAmerica Savannah
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a
survey meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Savannah Page 57 of 58 5/15/2013
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Certification Summary
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-90002-1
Project/Site: Ft.Bragg - Lamont Landfill
Laboratory: TestAmerica Savannah
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
A2LA 0399-01DoD ELAP 05-31-13
Alabama State Program 4 41450 06-30-13
Alaska (UST)State Program 10 UST-104 06-19-13
Arkansas DEQ State Program 6 88-0692 02-01-13 *
California NELAP 9 3217CA 07-31-13
Colorado State Program 8 N/A 12-31-13
Florida NELAP 4 E87052 06-30-13
GA Dept. of Agriculture State Program 4 N/A 12-31-13
Georgia State Program 4 N/A 06-30-13
Georgia State Program 4 803 06-30-13
Hawaii State Program 9 N/A 06-30-13
Illinois NELAP 5 200022 11-30-13
Indiana State Program 5 N/A 06-30-13
Iowa State Program 7 353 07-01-13 *
Kentucky State Program 4 90084 12-31-12 *
Kentucky (UST)State Program 4 18 03-31-13 *
Louisiana NELAP 6 30690 06-30-13
Louisiana NELAP 6 LA100015 12-31-13
Maine State Program 1 GA00006 08-16-14
Maryland State Program 3 250 12-31-13
Massachusetts State Program 1 M-GA006 06-30-13
Michigan State Program 5 9925 06-30-13
Mississippi State Program 4 N/A 06-30-13
Montana State Program 8 CERT0081 01-01-14
Nebraska State Program 7 TestAmerica-Savannah 06-30-13 *
New Jersey NELAP 2 GA769 06-30-13
New Mexico State Program 6 N/A 06-30-13
New York NELAP 2 10842 04-01-14
North Carolina DENR State Program 4 269 12-31-13
North Carolina DHHS State Program 4 13701 07-31-13
Oklahoma State Program 6 9984 08-31-13
Pennsylvania NELAP 3 68-00474 06-30-13 *
Puerto Rico State Program 2 GA00006 01-01-14
South Carolina State Program 4 98001 06-30-13
Tennessee State Program 4 TN02961 06-30-13
Texas NELAP 6 T104704185-08-TX 11-30-13
USDA Federal SAV 3-04 04-07-14
Virginia NELAP 3 460161 06-14-13 *
Washington State Program 10 C1794 06-10-13
West Virginia State Program 3 9950C 12-31-13
West Virginia DEP State Program 3 94 06-30-13
Wisconsin State Program 5 999819810 08-31-13
Wyoming State Program 8 8TMS-Q 06-30-13
TestAmerica Savannah
* Expired certification is currently pending renewal and is considered valid.
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-89949-1
Client Project/Site: Ft.Bragg - Lamont Landfill
For:
U.S. Army Corps of Engineers
PO BOX 889
Savannah, Georgia 31402-0889
Attn: Mr. Kevin Haborak
Authorized for release by:
5/8/2013 5:09:08 PM
Linda Wolfe, Project Manager I
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
TestAmerica Job ID: 680-89949-1
Page 2 of 20 TestAmerica Savannah5/8/2013
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-89949-1
Project/Site: Ft.Bragg - Lamont Landfill
Job ID: 680-89949-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: U.S. Army Corps of Engineers
Project: Ft.Bragg - Lamont Landfill
Report Number: 680-89949-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 05/03/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the
cooler at receipt was 0.2 C.
METALS (ICPMS)
Samples LMW-15R-5-13 (680-89949-1), LMW-4-5-13 (680-89949-2), DUP-1-5-13 (680-89949-3), LMW-7-5-13 (680-89949-4),
LMW-10-5-13 (680-89949-5) and LMW-16-5-13 (680-89949-6) were analyzed for Metals (ICPMS) in accordance with EPA SW-846 Method
6020A. The samples were prepared on 05/03/2013 and analyzed on 05/07/2013.
No difficulties were encountered during the metals analyses.
All quality control parameters were within the acceptance limits.
ANIONS (NITRATE/NITRITE)
Samples LMW-15R-5-13 (680-89949-1), LMW-4-5-13 (680-89949-2), DUP-1-5-13 (680-89949-3), LMW-7-5-13 (680-89949-4),
LMW-10-5-13 (680-89949-5) and LMW-16-5-13 (680-89949-6) were analyzed for Anions (Nitrate/Nitrite) in accordance with EPA Method
300.0. The samples were analyzed on 05/03/2013.
Samples LMW-15R-5-13 (680-89949-1)[5X], LMW-4-5-13 (680-89949-2)[5X], DUP-1-5-13 (680-89949-3)[5X], LMW-7-5-13 (680-89949-4)
[5X], LMW-10-5-13 (680-89949-5)[5X] and LMW-16-5-13 (680-89949-6)[5X] required dilution prior to analysis. The reporting limits have
been adjusted accordingly.
No difficulties were encountered during the Anions analyses.
All quality control parameters were within the acceptance limits.
TestAmerica SavannahPage 3 of 20 5/8/2013
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Sample Summary
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-89949-1 LMW-15R-5-13 Water 05/02/13 08:35 05/03/13 09:44
680-89949-2 LMW-4-5-13 Water 05/02/13 10:30 05/03/13 09:44
680-89949-3 DUP-1-5-13 Water 05/02/13 12:30 05/03/13 09:44
680-89949-4 LMW-7-5-13 Water 05/02/13 12:55 05/03/13 09:44
680-89949-5 LMW-10-5-13 Water 05/02/13 14:50 05/03/13 09:44
680-89949-6 LMW-16-5-13 Water 05/02/13 16:30 05/03/13 09:44
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Method Summary
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method Method Description LaboratoryProtocol
SW8466020AMetals (ICP/MS)TAL SAV
MCAWW300.0 Anions, Ion Chromatography TAL SAV
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Definitions/Glossary
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Qualifiers
Metals
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
General Chemistry
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
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Detection Summary
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-15R-5-13 Lab Sample ID: 680-89949-1
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1296020A
Beryllium 0.20 ug/L0.070 Total/NA10.15 J 6020A
Chromium 1.0 ug/L0.16 Total/NA10.18 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.52 J 6020A
Copper 1.0 ug/L0.21 Total/NA10.58 J 6020A
Lead 0.30 ug/L0.080 Total/NA10.087 J 6020A
Nickel 1.0 ug/L0.40 Total/NA12.2 6020A
Thallium 0.20 ug/L0.10 Total/NA10.14 J 6020A
Nitrate-NO3 1.1 mg/L0.36 Total/NA56.8 300.0
Client Sample ID: LMW-4-5-13 Lab Sample ID: 680-89949-2
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1146020A
Beryllium 0.20 ug/L0.070 Total/NA10.078 J 6020A
Chromium 1.0 ug/L0.16 Total/NA10.19 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.22 6020A
Copper 1.0 ug/L0.21 Total/NA11.3 6020A
Lead 0.30 ug/L0.080 Total/NA10.13 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.77 J 6020A
Thallium 0.20 ug/L0.10 Total/NA10.15 J 6020A
Zinc 10 ug/L2.6 Total/NA15.9 J 6020A
Client Sample ID: DUP-1-5-13 Lab Sample ID: 680-89949-3
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1296020A
Beryllium 0.20 ug/L0.070 Total/NA10.13 J 6020A
Chromium 1.0 ug/L0.16 Total/NA10.17 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.50 6020A
Copper 1.0 ug/L0.21 Total/NA10.55 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.98 J 6020A
Nitrate-NO3 1.1 mg/L0.36 Total/NA56.7 300.0
Client Sample ID: LMW-7-5-13 Lab Sample ID: 680-89949-4
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA14.3 6020A
Chromium 1.0 ug/L0.16 Total/NA10.24 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.11 J 6020A
Copper 1.0 ug/L0.21 Total/NA11.1 6020A
Client Sample ID: LMW-10-5-13 Lab Sample ID: 680-89949-5
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1256020A
Chromium 1.0 ug/L0.16 Total/NA10.44 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.21 6020A
Copper 1.0 ug/L0.21 Total/NA10.24 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.42 J 6020A
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-10-5-13 (Continued)Lab Sample ID: 680-89949-5
Selenium
RL
0.50 ug/L
MDL
0.21
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.9 6020A
Nitrate-NO3 1.1 mg/L0.36 Total/NA51.1 300.0
Client Sample ID: LMW-16-5-13 Lab Sample ID: 680-89949-6
Arsenic
RL
1.0 ug/L
MDL
0.40
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA12.1 6020A
Barium 1.0 ug/L0.15 Total/NA18.0 6020A
Chromium 1.0 ug/L0.16 Total/NA11.8 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.18 J 6020A
Copper 1.0 ug/L0.21 Total/NA10.78 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.70 J 6020A
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Client Sample Results
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-89949-1Client Sample ID: LMW-15R-5-13
Matrix: WaterDate Collected: 05/02/13 08:35
Date Received: 05/03/13 09:44
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/03/13 16:49 05/07/13 13:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 13:30 1Arsenic0.40 U
1.0 0.15 ug/L 05/03/13 16:49 05/07/13 13:30 1Barium29
0.20 0.070 ug/L 05/03/13 16:49 05/07/13 13:30 1Beryllium0.15 J
0.50 0.20 ug/L 05/03/13 16:49 05/07/13 13:30 1Cadmium0.20 U
1.0 0.16 ug/L 05/03/13 16:49 05/07/13 13:30 1Chromium0.18 J
0.20 0.078 ug/L 05/03/13 16:49 05/07/13 13:30 1Cobalt0.52 J
1.0 0.21 ug/L 05/03/13 16:49 05/07/13 13:30 1Copper0.58 J
0.30 0.080 ug/L 05/03/13 16:49 05/07/13 13:30 1Lead0.087 J
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 13:30 1Nickel2.2
0.50 0.21 ug/L 05/03/13 16:49 05/07/13 13:30 1Selenium0.21 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 13:30 1Silver0.10 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 13:30 1Thallium0.14 J
5.0 1.4 ug/L 05/03/13 16:49 05/07/13 13:30 1Vanadium1.4 U
10 2.6 ug/L 05/03/13 16:49 05/07/13 13:30 1Zinc2.6 U
General Chemistry
RL MDL
Nitrate-NO3 6.8 1.1 0.36 mg/L 05/03/13 17:20 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-89949-2Client Sample ID: LMW-4-5-13
Matrix: WaterDate Collected: 05/02/13 10:30
Date Received: 05/03/13 09:44
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/03/13 16:49 05/07/13 14:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:03 1Arsenic0.40 U
1.0 0.15 ug/L 05/03/13 16:49 05/07/13 14:03 1Barium14
0.20 0.070 ug/L 05/03/13 16:49 05/07/13 14:03 1Beryllium0.078 J
0.50 0.20 ug/L 05/03/13 16:49 05/07/13 14:03 1Cadmium0.20 U
1.0 0.16 ug/L 05/03/13 16:49 05/07/13 14:03 1Chromium0.19 J
0.20 0.078 ug/L 05/03/13 16:49 05/07/13 14:03 1Cobalt0.22
1.0 0.21 ug/L 05/03/13 16:49 05/07/13 14:03 1Copper1.3
0.30 0.080 ug/L 05/03/13 16:49 05/07/13 14:03 1Lead0.13 J
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:03 1Nickel0.77 J
0.50 0.21 ug/L 05/03/13 16:49 05/07/13 14:03 1Selenium0.21 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:03 1Silver0.10 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:03 1Thallium0.15 J
5.0 1.4 ug/L 05/03/13 16:49 05/07/13 14:03 1Vanadium1.4 U
10 2.6 ug/L 05/03/13 16:49 05/07/13 14:03 1Zinc5.9 J
General Chemistry
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/03/13 18:06 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-89949-3Client Sample ID: DUP-1-5-13
Matrix: WaterDate Collected: 05/02/13 12:30
Date Received: 05/03/13 09:44
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/03/13 16:49 05/07/13 14:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:10 1Arsenic0.40 U
1.0 0.15 ug/L 05/03/13 16:49 05/07/13 14:10 1Barium29
0.20 0.070 ug/L 05/03/13 16:49 05/07/13 14:10 1Beryllium0.13 J
0.50 0.20 ug/L 05/03/13 16:49 05/07/13 14:10 1Cadmium0.20 U
1.0 0.16 ug/L 05/03/13 16:49 05/07/13 14:10 1Chromium0.17 J
0.20 0.078 ug/L 05/03/13 16:49 05/07/13 14:10 1Cobalt0.50
1.0 0.21 ug/L 05/03/13 16:49 05/07/13 14:10 1Copper0.55 J
0.30 0.080 ug/L 05/03/13 16:49 05/07/13 14:10 1Lead0.080 U
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:10 1Nickel0.98 J
0.50 0.21 ug/L 05/03/13 16:49 05/07/13 14:10 1Selenium0.21 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:10 1Silver0.10 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:10 1Thallium0.10 U
5.0 1.4 ug/L 05/03/13 16:49 05/07/13 14:10 1Vanadium1.4 U
10 2.6 ug/L 05/03/13 16:49 05/07/13 14:10 1Zinc2.6 U
General Chemistry
RL MDL
Nitrate-NO3 6.7 1.1 0.36 mg/L 05/03/13 18:21 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-89949-4Client Sample ID: LMW-7-5-13
Matrix: WaterDate Collected: 05/02/13 12:55
Date Received: 05/03/13 09:44
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/03/13 16:49 05/07/13 14:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:16 1Arsenic0.40 U
1.0 0.15 ug/L 05/03/13 16:49 05/07/13 14:16 1Barium4.3
0.20 0.070 ug/L 05/03/13 16:49 05/07/13 14:16 1Beryllium0.070 U
0.50 0.20 ug/L 05/03/13 16:49 05/07/13 14:16 1Cadmium0.20 U
1.0 0.16 ug/L 05/03/13 16:49 05/07/13 14:16 1Chromium0.24 J
0.20 0.078 ug/L 05/03/13 16:49 05/07/13 14:16 1Cobalt0.11 J
1.0 0.21 ug/L 05/03/13 16:49 05/07/13 14:16 1Copper1.1
0.30 0.080 ug/L 05/03/13 16:49 05/07/13 14:16 1Lead0.080 U
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:16 1Nickel0.40 U
0.50 0.21 ug/L 05/03/13 16:49 05/07/13 14:16 1Selenium0.21 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:16 1Silver0.10 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:16 1Thallium0.10 U
5.0 1.4 ug/L 05/03/13 16:49 05/07/13 14:16 1Vanadium1.4 U
10 2.6 ug/L 05/03/13 16:49 05/07/13 14:16 1Zinc2.6 U
General Chemistry
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/03/13 18:37 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-89949-5Client Sample ID: LMW-10-5-13
Matrix: WaterDate Collected: 05/02/13 14:50
Date Received: 05/03/13 09:44
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/03/13 16:49 05/07/13 14:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:36 1Arsenic0.40 U
1.0 0.15 ug/L 05/03/13 16:49 05/07/13 14:36 1Barium25
0.20 0.070 ug/L 05/03/13 16:49 05/07/13 14:36 1Beryllium0.070 U
0.50 0.20 ug/L 05/03/13 16:49 05/07/13 14:36 1Cadmium0.20 U
1.0 0.16 ug/L 05/03/13 16:49 05/07/13 14:36 1Chromium0.44 J
0.20 0.078 ug/L 05/03/13 16:49 05/07/13 14:36 1Cobalt0.21
1.0 0.21 ug/L 05/03/13 16:49 05/07/13 14:36 1Copper0.24 J
0.30 0.080 ug/L 05/03/13 16:49 05/07/13 14:36 1Lead0.080 U
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:36 1Nickel0.42 J
0.50 0.21 ug/L 05/03/13 16:49 05/07/13 14:36 1Selenium3.9
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:36 1Silver0.10 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:36 1Thallium0.10 U
5.0 1.4 ug/L 05/03/13 16:49 05/07/13 14:36 1Vanadium1.4 U
10 2.6 ug/L 05/03/13 16:49 05/07/13 14:36 1Zinc2.6 U
General Chemistry
RL MDL
Nitrate-NO3 1.1 1.1 0.36 mg/L 05/03/13 18:52 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-89949-6Client Sample ID: LMW-16-5-13
Matrix: WaterDate Collected: 05/02/13 16:30
Date Received: 05/03/13 09:44
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/03/13 16:49 05/07/13 14:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:43 1Arsenic2.1
1.0 0.15 ug/L 05/03/13 16:49 05/07/13 14:43 1Barium8.0
0.20 0.070 ug/L 05/03/13 16:49 05/07/13 14:43 1Beryllium0.070 U
0.50 0.20 ug/L 05/03/13 16:49 05/07/13 14:43 1Cadmium0.20 U
1.0 0.16 ug/L 05/03/13 16:49 05/07/13 14:43 1Chromium1.8
0.20 0.078 ug/L 05/03/13 16:49 05/07/13 14:43 1Cobalt0.18 J
1.0 0.21 ug/L 05/03/13 16:49 05/07/13 14:43 1Copper0.78 J
0.30 0.080 ug/L 05/03/13 16:49 05/07/13 14:43 1Lead0.080 U
1.0 0.40 ug/L 05/03/13 16:49 05/07/13 14:43 1Nickel0.70 J
0.50 0.21 ug/L 05/03/13 16:49 05/07/13 14:43 1Selenium0.21 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:43 1Silver0.10 U
0.20 0.10 ug/L 05/03/13 16:49 05/07/13 14:43 1Thallium0.10 U
5.0 1.4 ug/L 05/03/13 16:49 05/07/13 14:43 1Vanadium1.4 U
10 2.6 ug/L 05/03/13 16:49 05/07/13 14:43 1Zinc2.6 U
General Chemistry
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/03/13 19:07 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 6020A - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-275474/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275967 Prep Batch: 275474
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/03/13 16:49 05/07/13 13:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.40 U 0.401.0 ug/L 05/03/13 16:49 05/07/13 13:16 1Arsenic
0.15 U 0.151.0 ug/L 05/03/13 16:49 05/07/13 13:16 1Barium
0.070 U 0.0700.20 ug/L 05/03/13 16:49 05/07/13 13:16 1Beryllium
0.20 U 0.200.50 ug/L 05/03/13 16:49 05/07/13 13:16 1Cadmium
0.16 U 0.161.0 ug/L 05/03/13 16:49 05/07/13 13:16 1Chromium
0.078 U 0.0780.20 ug/L 05/03/13 16:49 05/07/13 13:16 1Cobalt
0.21 U 0.211.0 ug/L 05/03/13 16:49 05/07/13 13:16 1Copper
0.080 U 0.0800.30 ug/L 05/03/13 16:49 05/07/13 13:16 1Lead
0.40 U 0.401.0 ug/L 05/03/13 16:49 05/07/13 13:16 1Nickel
0.21 U 0.210.50 ug/L 05/03/13 16:49 05/07/13 13:16 1Selenium
0.10 U 0.100.20 ug/L 05/03/13 16:49 05/07/13 13:16 1Silver
0.10 U 0.100.20 ug/L 05/03/13 16:49 05/07/13 13:16 1Thallium
1.4 U 1.45.0 ug/L 05/03/13 16:49 05/07/13 13:16 1Vanadium
2.6 U 2.610 ug/L 05/03/13 16:49 05/07/13 13:16 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-275474/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275967 Prep Batch: 275474
Antimony 20.0 22.0 ug/L 110 75 -125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 40.0 39.4 ug/L 99 75 -125
Barium 40.0 40.0 ug/L 100 75 -125
Beryllium 20.0 22.8 ug/L 114 75 -125
Cadmium 20.0 21.0 ug/L 105 75 -125
Chromium 40.0 34.7 ug/L 87 75 -125
Cobalt 20.0 15.6 ug/L 78 75 -125
Copper 40.0 34.8 ug/L 87 75 -125
Lead 20.0 19.2 ug/L 96 75 -125
Nickel 40.0 34.7 ug/L 87 75 -125
Selenium 40.0 45.8 ug/L 114 75 -125
Silver 20.0 20.0 ug/L 100 75 -125
Thallium 16.0 15.6 ug/L 98 75 -125
Vanadium 40.0 34.2 ug/L 85 75 -125
Zinc 40.0 41.8 ug/L 104 75 -125
Client Sample ID: LMW-15R-5-13Lab Sample ID: 680-89949-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275967 Prep Batch: 275474
Antimony 0.99 U 20.0 21.5 ug/L 107 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 0.40 U 40.0 40.1 ug/L 100 75 -125
Barium 29 40.0 68.4 ug/L 97 75 -125
Beryllium 0.15 J 20.0 22.2 ug/L 110 75 -125
Cadmium 0.20 U 20.0 20.4 ug/L 102 75 -125
Chromium 0.18 J 40.0 34.9 ug/L 87 75 -125
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QC Sample Results
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: LMW-15R-5-13Lab Sample ID: 680-89949-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275967 Prep Batch: 275474
Cobalt 0.52 J 20.0 16.5 ug/L 80 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Copper 0.58 J 40.0 35.7 ug/L 88 75 -125
Lead 0.087 J 20.0 19.0 ug/L 95 75 -125
Nickel 2.2 40.0 36.8 ug/L 87 75 -125
Selenium 0.21 U 40.0 43.9 ug/L 110 75 -125
Silver 0.10 U 20.0 19.5 ug/L 98 75 -125
Thallium 0.14 J 16.0 15.5 ug/L 96 75 -125
Vanadium 1.4 U 40.0 34.5 ug/L 86 75 -125
Zinc 2.6 U 40.0 43.2 ug/L 108 75 -125
Client Sample ID: LMW-15R-5-13Lab Sample ID: 680-89949-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275967 Prep Batch: 275474
Antimony 0.99 U 20.0 21.2 ug/L 106 75 -125 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 0.40 U 40.0 37.2 ug/L 93 75 -125 7 20
Barium 29 40.0 67.6 ug/L 95 75 -125 1 20
Beryllium 0.15 J 20.0 22.0 ug/L 109 75 -125 1 20
Cadmium 0.20 U 20.0 20.2 ug/L 101 75 -125 1 20
Chromium 0.18 J 40.0 32.3 ug/L 80 75 -125 7 20
Cobalt 0.52 J 20.0 15.2 J ug/L 73 75 -125 9 20
Copper 0.58 J 40.0 32.8 ug/L 81 75 -125 8 20
Lead 0.087 J 20.0 18.8 ug/L 94 75 -125 1 20
Nickel 2.2 40.0 34.4 ug/L 80 75 -125 7 20
Selenium 0.21 U 40.0 41.1 ug/L 103 75 -125 7 20
Silver 0.10 U 20.0 19.1 ug/L 95 75 -125 2 20
Thallium 0.14 J 16.0 15.5 ug/L 96 75 -125 0 20
Vanadium 1.4 U 40.0 31.9 ug/L 80 75 -125 8 20
Zinc 2.6 U 40.0 39.3 ug/L 98 75 -125 9 20
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 680-275527/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275527
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/03/13 16:33 5
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-275527/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275527
Nitrate-NO3 22.1 20.7 mg/L 94 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
TestAmerica Savannah
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QC Sample Results
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 300.0 - Anions, Ion Chromatography (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-275527/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275527
Nitrate-NO3 22.1 20.7 mg/L 94 90 -110 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: LMW-15R-5-13Lab Sample ID: 680-89949-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275527
Nitrate-NO3 6.8 22.1 29.5 mg/L 103 90 -110
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: LMW-15R-5-13Lab Sample ID: 680-89949-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275527
Nitrate-NO3 6.8 22.1 29.4 mg/L 102 90 -110 0 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Savannah
Page 14 of 20 5/8/2013
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QC Association Summary
TestAmerica Job ID: 680-89949-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Metals
Prep Batch: 275474
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3030C680-89949-1 LMW-15R-5-13 Total/NA
Water 3030C680-89949-1 MS LMW-15R-5-13 Total/NA
Water 3030C680-89949-1 MSD LMW-15R-5-13 Total/NA
Water 3030C680-89949-2 LMW-4-5-13 Total/NA
Water 3030C680-89949-3 DUP-1-5-13 Total/NA
Water 3030C680-89949-4 LMW-7-5-13 Total/NA
Water 3030C680-89949-5 LMW-10-5-13 Total/NA
Water 3030C680-89949-6 LMW-16-5-13 Total/NA
Water 3030CLCS 680-275474/2-A Lab Control Sample Total/NA
Water 3030CMB 680-275474/1-A Method Blank Total/NA
Analysis Batch: 275967
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 275474680-89949-1 LMW-15R-5-13 Total/NA
Water 6020A 275474680-89949-1 MS LMW-15R-5-13 Total/NA
Water 6020A 275474680-89949-1 MSD LMW-15R-5-13 Total/NA
Water 6020A 275474680-89949-2 LMW-4-5-13 Total/NA
Water 6020A 275474680-89949-3 DUP-1-5-13 Total/NA
Water 6020A 275474680-89949-4 LMW-7-5-13 Total/NA
Water 6020A 275474680-89949-5 LMW-10-5-13 Total/NA
Water 6020A 275474680-89949-6 LMW-16-5-13 Total/NA
Water 6020A 275474LCS 680-275474/2-A Lab Control Sample Total/NA
Water 6020A 275474MB 680-275474/1-A Method Blank Total/NA
General Chemistry
Analysis Batch: 275527
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0680-89949-1 LMW-15R-5-13 Total/NA
Water 300.0680-89949-1 MS LMW-15R-5-13 Total/NA
Water 300.0680-89949-1 MSD LMW-15R-5-13 Total/NA
Water 300.0680-89949-2 LMW-4-5-13 Total/NA
Water 300.0680-89949-3 DUP-1-5-13 Total/NA
Water 300.0680-89949-4 LMW-7-5-13 Total/NA
Water 300.0680-89949-5 LMW-10-5-13 Total/NA
Water 300.0680-89949-6 LMW-16-5-13 Total/NA
Water 300.0LCS 680-275527/3 Lab Control Sample Total/NA
Water 300.0LCSD 680-275527/4 Lab Control Sample Dup Total/NA
Water 300.0MB 680-275527/2 Method Blank Total/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-89949-1
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-15R-5-13 Lab Sample ID: 680-89949-1
Matrix: WaterDate Collected: 05/02/13 08:35
Date Received: 05/03/13 09:44
Prep 3030C 05/03/13 16:49 BB275474 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275967 05/07/13 13:30 BR TAL SAVTotal/NA
Analysis 300.0 5 275527 05/03/13 17:20 PAT TAL SAVTotal/NA
Client Sample ID: LMW-4-5-13 Lab Sample ID: 680-89949-2
Matrix: WaterDate Collected: 05/02/13 10:30
Date Received: 05/03/13 09:44
Prep 3030C 05/03/13 16:49 BB275474 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275967 05/07/13 14:03 BR TAL SAVTotal/NA
Analysis 300.0 5 275527 05/03/13 18:06 PAT TAL SAVTotal/NA
Client Sample ID: DUP-1-5-13 Lab Sample ID: 680-89949-3
Matrix: WaterDate Collected: 05/02/13 12:30
Date Received: 05/03/13 09:44
Prep 3030C 05/03/13 16:49 BB275474 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275967 05/07/13 14:10 BR TAL SAVTotal/NA
Analysis 300.0 5 275527 05/03/13 18:21 PAT TAL SAVTotal/NA
Client Sample ID: LMW-7-5-13 Lab Sample ID: 680-89949-4
Matrix: WaterDate Collected: 05/02/13 12:55
Date Received: 05/03/13 09:44
Prep 3030C 05/03/13 16:49 BB275474 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275967 05/07/13 14:16 BR TAL SAVTotal/NA
Analysis 300.0 5 275527 05/03/13 18:37 PAT TAL SAVTotal/NA
Client Sample ID: LMW-10-5-13 Lab Sample ID: 680-89949-5
Matrix: WaterDate Collected: 05/02/13 14:50
Date Received: 05/03/13 09:44
Prep 3030C 05/03/13 16:49 BB275474 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275967 05/07/13 14:36 BR TAL SAVTotal/NA
Analysis 300.0 5 275527 05/03/13 18:52 PAT TAL SAVTotal/NA
TestAmerica Savannah
Page 16 of 20 5/8/2013
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-89949-1
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-16-5-13 Lab Sample ID: 680-89949-6
Matrix: WaterDate Collected: 05/02/13 16:30
Date Received: 05/03/13 09:44
Prep 3030C 05/03/13 16:49 BB275474 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275967 05/07/13 14:43 BR TAL SAVTotal/NA
Analysis 300.0 5 275527 05/03/13 19:07 PAT TAL SAVTotal/NA
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 17 of 20 5/8/2013
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Login Sample Receipt Checklist
Client: U.S. Army Corps of Engineers Job Number: 680-89949-1
Login Number: 89949
Question Answer Comment
Creator: Conner, Keaton
List Source: TestAmerica Savannah
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a
survey meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Savannah Page 19 of 20 5/8/2013
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Certification Summary
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-89949-1
Project/Site: Ft.Bragg - Lamont Landfill
Laboratory: TestAmerica Savannah
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
A2LA 0399-01DoD ELAP 05-31-13
Alabama State Program 4 41450 06-30-13
Alaska (UST)State Program 10 UST-104 06-19-13
Arkansas DEQ State Program 6 88-0692 02-01-13 *
California NELAP 9 3217CA 07-31-13
Colorado State Program 8 N/A 12-31-13
Florida NELAP 4 E87052 06-30-13
GA Dept. of Agriculture State Program 4 N/A 12-31-13
Georgia State Program 4 N/A 06-30-13
Georgia State Program 4 803 06-30-13
Hawaii State Program 9 N/A 06-30-13
Illinois NELAP 5 200022 11-30-13
Indiana State Program 5 N/A 06-30-13
Iowa State Program 7 353 07-01-13 *
Kentucky State Program 4 90084 12-31-12 *
Kentucky (UST)State Program 4 18 03-31-13 *
Louisiana NELAP 6 30690 06-30-13
Louisiana NELAP 6 LA100015 12-31-13
Maine State Program 1 GA00006 08-16-14
Maryland State Program 3 250 12-31-13
Massachusetts State Program 1 M-GA006 06-30-13
Michigan State Program 5 9925 06-30-13
Mississippi State Program 4 N/A 06-30-13
Montana State Program 8 CERT0081 01-01-14
Nebraska State Program 7 TestAmerica-Savannah 06-30-13 *
New Jersey NELAP 2 GA769 06-30-13
New Mexico State Program 6 N/A 06-30-13
New York NELAP 2 10842 04-01-14
North Carolina DENR State Program 4 269 12-31-13
North Carolina DHHS State Program 4 13701 07-31-13
Oklahoma State Program 6 9984 08-31-13
Pennsylvania NELAP 3 68-00474 06-30-13 *
Puerto Rico State Program 2 GA00006 01-01-14
South Carolina State Program 4 98001 06-30-13
Tennessee State Program 4 TN02961 06-30-13
Texas NELAP 6 T104704185-08-TX 11-30-13
USDA Federal SAV 3-04 04-07-14
Virginia NELAP 3 460161 06-14-13 *
Washington State Program 10 C1794 06-10-13
West Virginia State Program 3 9950C 12-31-13
West Virginia DEP State Program 3 94 06-30-13
Wisconsin State Program 5 999819810 08-31-13
Wyoming State Program 8 8TMS-Q 06-30-13
TestAmerica Savannah
* Expired certification is currently pending renewal and is considered valid.
Page 20 of 20 5/8/2013
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-89881-1
Client Project/Site: Ft.Bragg - Lamont Landfill
For:
U.S. Army Corps of Engineers
PO BOX 889
Savannah, Georgia 31402-0889
Attn: Mr. Kevin Haborak
Authorized for release by:
5/8/2013 11:44:38 AM
Linda Wolfe, Project Manager I
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
TestAmerica Job ID: 680-89881-1
Page 2 of 17 TestAmerica Savannah5/8/2013
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-89881-1
Project/Site: Ft.Bragg - Lamont Landfill
Job ID: 680-89881-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: U.S. Army Corps of Engineers
Project: Ft.Bragg - Lamont Landfill
Report Number: 680-89881-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 05/02/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the
cooler at receipt was 2.8 C.
METALS (ICPMS)
Samples LMW-6-5-13 (680-89881-1), LMW-3-5-13 (680-89881-2), LMW-3S-5-13 (680-89881-3) and LMW-14R-5-13 (680-89881-4) were
analyzed for Metals (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 05/02/2013 and analyzed on
05/03/2013.
No difficulties were encountered during the metals analyses.
All quality control parameters were within the acceptance limits.
ANIONS (NITRATE/NITRITE)
Samples LMW-6-5-13 (680-89881-1), LMW-3-5-13 (680-89881-2), LMW-3S-5-13 (680-89881-3) and LMW-14R-5-13 (680-89881-4) were
analyzed for Anions (Nitrate/Nitrite) in accordance with EPA Method 300.0. The samples were analyzed on 05/03/2013.
Samples LMW-6-5-13 (680-89881-1)[5X], LMW-3-5-13 (680-89881-2)[5X], LMW-3S-5-13 (680-89881-3)[5X] and LMW-14R-5-13
(680-89881-4)[5X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No difficulties were encountered during the Anions analyses.
All quality control parameters were within the acceptance limits.
TestAmerica SavannahPage 3 of 17 5/8/2013
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Sample Summary
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-89881-1 LMW-6-5-13 Water 05/01/13 09:56 05/02/13 09:49
680-89881-2 LMW-3-5-13 Water 05/01/13 14:15 05/02/13 09:49
680-89881-3 LMW-3S-5-13 Water 05/01/13 11:40 05/02/13 09:49
680-89881-4 LMW-14R-5-13 Water 05/01/13 15:45 05/02/13 09:49
TestAmerica Savannah
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Method Summary
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method Method Description LaboratoryProtocol
SW8466020AMetals (ICP/MS)TAL SAV
MCAWW300.0 Anions, Ion Chromatography TAL SAV
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Definitions/Glossary
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Qualifiers
Metals
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
General Chemistry
Qualifier Description
J Estimated: The analyte was positively identified; the quantitation is an estimation
Qualifier
U Undetected at the Limit of Detection.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
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Detection Summary
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-6-5-13 Lab Sample ID: 680-89881-1
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1306020A
Beryllium 0.20 ug/L0.070 Total/NA10.092 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.37 6020A
Copper 1.0 ug/L0.21 Total/NA10.76 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.60 J 6020A
Selenium 0.50 ug/L0.21 Total/NA11.8 6020A
Thallium 0.20 ug/L0.10 Total/NA10.17 J 6020A
Zinc 10 ug/L2.6 Total/NA12.6 J 6020A
Nitrate-NO3 1.1 mg/L0.36 Total/NA55.8 300.0
Client Sample ID: LMW-3-5-13 Lab Sample ID: 680-89881-2
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.3 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.16 J 6020A
Copper 1.0 ug/L0.21 Total/NA10.64 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.45 J 6020A
Nitrate-NO3 1.1 mg/L0.36 Total/NA50.64 J 300.0
Client Sample ID: LMW-3S-5-13 Lab Sample ID: 680-89881-3
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1126020A
Beryllium 0.20 ug/L0.070 Total/NA10.073 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.50 6020A
Copper 1.0 ug/L0.21 Total/NA10.81 J 6020A
Nickel 1.0 ug/L0.40 Total/NA12.7 6020A
Zinc 10 ug/L2.6 Total/NA18.8 J 6020A
Nitrate-NO3 1.1 mg/L0.36 Total/NA50.92 J 300.0
Client Sample ID: LMW-14R-5-13 Lab Sample ID: 680-89881-4
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1116020A
Chromium 1.0 ug/L0.16 Total/NA10.50 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.12 J 6020A
Copper 1.0 ug/L0.21 Total/NA10.70 J 6020A
Lead 0.30 ug/L0.080 Total/NA10.12 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.44 J 6020A
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Client Sample Results
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-89881-1Client Sample ID: LMW-6-5-13
Matrix: WaterDate Collected: 05/01/13 09:56
Date Received: 05/02/13 09:49
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/02/13 14:05 05/03/13 12:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/02/13 14:05 05/03/13 12:08 1Arsenic0.40 U
1.0 0.15 ug/L 05/02/13 14:05 05/03/13 12:08 1Barium30
0.20 0.070 ug/L 05/02/13 14:05 05/03/13 12:08 1Beryllium0.092 J
0.50 0.20 ug/L 05/02/13 14:05 05/03/13 12:08 1Cadmium0.20 U
1.0 0.16 ug/L 05/02/13 14:05 05/03/13 12:08 1Chromium0.16 U
0.20 0.078 ug/L 05/02/13 14:05 05/03/13 12:08 1Cobalt0.37
1.0 0.21 ug/L 05/02/13 14:05 05/03/13 12:08 1Copper0.76 J
0.30 0.080 ug/L 05/02/13 14:05 05/03/13 12:08 1Lead0.080 U
1.0 0.40 ug/L 05/02/13 14:05 05/03/13 12:08 1Nickel0.60 J
0.50 0.21 ug/L 05/02/13 14:05 05/03/13 12:08 1Selenium1.8
0.20 0.10 ug/L 05/02/13 14:05 05/03/13 12:08 1Silver0.10 U
0.20 0.10 ug/L 05/02/13 14:05 05/03/13 12:08 1Thallium0.17 J
5.0 1.4 ug/L 05/02/13 14:05 05/03/13 12:08 1Vanadium1.4 U
10 2.6 ug/L 05/02/13 14:05 05/03/13 12:08 1Zinc2.6 J
General Chemistry
RL MDL
Nitrate-NO3 5.8 1.1 0.36 mg/L 05/03/13 03:33 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-89881-2Client Sample ID: LMW-3-5-13
Matrix: WaterDate Collected: 05/01/13 14:15
Date Received: 05/02/13 09:49
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/02/13 14:05 05/03/13 12:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/02/13 14:05 05/03/13 12:15 1Arsenic0.40 U
1.0 0.15 ug/L 05/02/13 14:05 05/03/13 12:15 1Barium3.3
0.20 0.070 ug/L 05/02/13 14:05 05/03/13 12:15 1Beryllium0.070 U
0.50 0.20 ug/L 05/02/13 14:05 05/03/13 12:15 1Cadmium0.20 U
1.0 0.16 ug/L 05/02/13 14:05 05/03/13 12:15 1Chromium0.16 U
0.20 0.078 ug/L 05/02/13 14:05 05/03/13 12:15 1Cobalt0.16 J
1.0 0.21 ug/L 05/02/13 14:05 05/03/13 12:15 1Copper0.64 J
0.30 0.080 ug/L 05/02/13 14:05 05/03/13 12:15 1Lead0.080 U
1.0 0.40 ug/L 05/02/13 14:05 05/03/13 12:15 1Nickel0.45 J
0.50 0.21 ug/L 05/02/13 14:05 05/03/13 12:15 1Selenium0.21 U
0.20 0.10 ug/L 05/02/13 14:05 05/03/13 12:15 1Silver0.10 U
0.20 0.10 ug/L 05/02/13 14:05 05/03/13 12:15 1Thallium0.10 U
5.0 1.4 ug/L 05/02/13 14:05 05/03/13 12:15 1Vanadium1.4 U
10 2.6 ug/L 05/02/13 14:05 05/03/13 12:15 1Zinc2.6 U
General Chemistry
RL MDL
Nitrate-NO3 0.64 J 1.1 0.36 mg/L 05/03/13 03:48 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Savannah
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Client Sample Results
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Lab Sample ID: 680-89881-3Client Sample ID: LMW-3S-5-13
Matrix: WaterDate Collected: 05/01/13 11:40
Date Received: 05/02/13 09:49
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/02/13 14:05 05/03/13 12:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/02/13 14:05 05/03/13 12:21 1Arsenic0.40 U
1.0 0.15 ug/L 05/02/13 14:05 05/03/13 12:21 1Barium12
0.20 0.070 ug/L 05/02/13 14:05 05/03/13 12:21 1Beryllium0.073 J
0.50 0.20 ug/L 05/02/13 14:05 05/03/13 12:21 1Cadmium0.20 U
1.0 0.16 ug/L 05/02/13 14:05 05/03/13 12:21 1Chromium0.16 U
0.20 0.078 ug/L 05/02/13 14:05 05/03/13 12:21 1Cobalt0.50
1.0 0.21 ug/L 05/02/13 14:05 05/03/13 12:21 1Copper0.81 J
0.30 0.080 ug/L 05/02/13 14:05 05/03/13 12:21 1Lead0.080 U
1.0 0.40 ug/L 05/02/13 14:05 05/03/13 12:21 1Nickel2.7
0.50 0.21 ug/L 05/02/13 14:05 05/03/13 12:21 1Selenium0.21 U
0.20 0.10 ug/L 05/02/13 14:05 05/03/13 12:21 1Silver0.10 U
0.20 0.10 ug/L 05/02/13 14:05 05/03/13 12:21 1Thallium0.10 U
5.0 1.4 ug/L 05/02/13 14:05 05/03/13 12:21 1Vanadium1.4 U
10 2.6 ug/L 05/02/13 14:05 05/03/13 12:21 1Zinc8.8 J
General Chemistry
RL MDL
Nitrate-NO3 0.92 J 1.1 0.36 mg/L 05/03/13 04:04 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-89881-4Client Sample ID: LMW-14R-5-13
Matrix: WaterDate Collected: 05/01/13 15:45
Date Received: 05/02/13 09:49
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/02/13 14:05 05/03/13 12:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.40 ug/L 05/02/13 14:05 05/03/13 12:28 1Arsenic0.40 U
1.0 0.15 ug/L 05/02/13 14:05 05/03/13 12:28 1Barium11
0.20 0.070 ug/L 05/02/13 14:05 05/03/13 12:28 1Beryllium0.070 U
0.50 0.20 ug/L 05/02/13 14:05 05/03/13 12:28 1Cadmium0.20 U
1.0 0.16 ug/L 05/02/13 14:05 05/03/13 12:28 1Chromium0.50 J
0.20 0.078 ug/L 05/02/13 14:05 05/03/13 12:28 1Cobalt0.12 J
1.0 0.21 ug/L 05/02/13 14:05 05/03/13 12:28 1Copper0.70 J
0.30 0.080 ug/L 05/02/13 14:05 05/03/13 12:28 1Lead0.12 J
1.0 0.40 ug/L 05/02/13 14:05 05/03/13 12:28 1Nickel0.44 J
0.50 0.21 ug/L 05/02/13 14:05 05/03/13 12:28 1Selenium0.21 U
0.20 0.10 ug/L 05/02/13 14:05 05/03/13 12:28 1Silver0.10 U
0.20 0.10 ug/L 05/02/13 14:05 05/03/13 12:28 1Thallium0.10 U
5.0 1.4 ug/L 05/02/13 14:05 05/03/13 12:28 1Vanadium1.4 U
10 2.6 ug/L 05/02/13 14:05 05/03/13 12:28 1Zinc2.6 U
General Chemistry
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/03/13 04:19 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Savannah
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QC Sample Results
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 6020A - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-275267/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275522 Prep Batch: 275267
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/02/13 14:05 05/03/13 11:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.40 U 0.401.0 ug/L 05/02/13 14:05 05/03/13 11:55 1Arsenic
0.15 U 0.151.0 ug/L 05/02/13 14:05 05/03/13 11:55 1Barium
0.070 U 0.0700.20 ug/L 05/02/13 14:05 05/03/13 11:55 1Beryllium
0.20 U 0.200.50 ug/L 05/02/13 14:05 05/03/13 11:55 1Cadmium
0.16 U 0.161.0 ug/L 05/02/13 14:05 05/03/13 11:55 1Chromium
0.078 U 0.0780.20 ug/L 05/02/13 14:05 05/03/13 11:55 1Cobalt
0.21 U 0.211.0 ug/L 05/02/13 14:05 05/03/13 11:55 1Copper
0.080 U 0.0800.30 ug/L 05/02/13 14:05 05/03/13 11:55 1Lead
0.40 U 0.401.0 ug/L 05/02/13 14:05 05/03/13 11:55 1Nickel
0.21 U 0.210.50 ug/L 05/02/13 14:05 05/03/13 11:55 1Selenium
0.10 U 0.100.20 ug/L 05/02/13 14:05 05/03/13 11:55 1Silver
0.10 U 0.100.20 ug/L 05/02/13 14:05 05/03/13 11:55 1Thallium
1.4 U 1.45.0 ug/L 05/02/13 14:05 05/03/13 11:55 1Vanadium
2.6 U 2.610 ug/L 05/02/13 14:05 05/03/13 11:55 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-275267/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275522 Prep Batch: 275267
Antimony 50.0 51.9 ug/L 104 75 -125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 100 104 ug/L 104 75 -125
Barium 100 101 ug/L 101 75 -125
Beryllium 50.0 50.8 ug/L 102 75 -125
Cadmium 50.0 49.7 ug/L 99 75 -125
Chromium 100 95.1 ug/L 95 75 -125
Cobalt 50.0 47.6 ug/L 95 75 -125
Copper 100 97.0 ug/L 97 75 -125
Lead 50.0 47.5 ug/L 95 75 -125
Nickel 100 95.9 ug/L 96 75 -125
Selenium 100 103 ug/L 103 75 -125
Silver 50.0 49.5 ug/L 99 75 -125
Thallium 40.0 38.1 ug/L 95 75 -125
Vanadium 100 95.5 ug/L 96 75 -125
Zinc 100 102 ug/L 102 75 -125
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-89881-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275522 Prep Batch: 275267
Antimony 0.99 U 50.0 50.9 ug/L 102 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 0.40 U 100 105 ug/L 105 75 -125
Barium 11 100 110 ug/L 100 75 -125
Beryllium 0.070 U 50.0 49.9 ug/L 100 75 -125
Cadmium 0.20 U 50.0 48.7 ug/L 97 75 -125
Chromium 0.50 J 100 94.6 ug/L 94 75 -125
TestAmerica Savannah
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QC Sample Results
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-89881-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275522 Prep Batch: 275267
Cobalt 0.12 J 50.0 47.3 ug/L 94 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Copper 0.70 J 100 95.6 ug/L 95 75 -125
Lead 0.12 J 50.0 47.1 ug/L 94 75 -125
Nickel 0.44 J 100 97.7 ug/L 97 75 -125
Selenium 0.21 U 100 101 ug/L 101 75 -125
Silver 0.10 U 50.0 48.3 ug/L 97 75 -125
Thallium 0.10 U 40.0 37.7 ug/L 94 75 -125
Vanadium 1.4 U 100 94.8 ug/L 95 75 -125
Zinc 2.6 U 100 101 ug/L 101 75 -125
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-89881-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275522 Prep Batch: 275267
Antimony 0.99 U 50.0 51.9 ug/L 104 75 -125 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 0.40 U 100 109 ug/L 109 75 -125 4 20
Barium 11 100 113 ug/L 103 75 -125 3 20
Beryllium 0.070 U 50.0 50.6 ug/L 101 75 -125 1 20
Cadmium 0.20 U 50.0 49.2 ug/L 98 75 -125 1 20
Chromium 0.50 J 100 100 ug/L 100 75 -125 6 20
Cobalt 0.12 J 50.0 47.6 ug/L 95 75 -125 1 20
Copper 0.70 J 100 101 ug/L 100 75 -125 5 20
Lead 0.12 J 50.0 47.8 ug/L 95 75 -125 1 20
Nickel 0.44 J 100 100 ug/L 100 75 -125 3 20
Selenium 0.21 U 100 105 ug/L 105 75 -125 4 20
Silver 0.10 U 50.0 49.2 ug/L 98 75 -125 2 20
Thallium 0.10 U 40.0 38.6 ug/L 97 75 -125 2 20
Vanadium 1.4 U 100 101 ug/L 101 75 -125 6 20
Zinc 2.6 U 100 100 ug/L 100 75 -125 1 20
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 680-275389/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275389
RL MDL
Nitrate-NO3 0.36 U 1.1 0.36 mg/L 05/03/13 02:47 5
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-275389/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275389
Nitrate-NO3 22.1 20.6 mg/L 93 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
TestAmerica Savannah
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QC Sample Results
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Method: 300.0 - Anions, Ion Chromatography (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-275389/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275389
Nitrate-NO3 22.1 20.6 mg/L 93 90 -110 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-89881-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275389
Nitrate-NO3 0.36 U 22.1 20.8 mg/L 94 90 -110
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: LMW-14R-5-13Lab Sample ID: 680-89881-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 275389
Nitrate-NO3 0.36 U 22.1 20.9 mg/L 94 90 -110 0 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Savannah
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QC Association Summary
TestAmerica Job ID: 680-89881-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Lamont Landfill
Metals
Prep Batch: 275267
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3030C680-89881-1 LMW-6-5-13 Total/NA
Water 3030C680-89881-2 LMW-3-5-13 Total/NA
Water 3030C680-89881-3 LMW-3S-5-13 Total/NA
Water 3030C680-89881-4 LMW-14R-5-13 Total/NA
Water 3030C680-89881-4 MS LMW-14R-5-13 Total/NA
Water 3030C680-89881-4 MSD LMW-14R-5-13 Total/NA
Water 3030CLCS 680-275267/2-A Lab Control Sample Total/NA
Water 3030CMB 680-275267/1-A Method Blank Total/NA
Analysis Batch: 275522
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 275267680-89881-1 LMW-6-5-13 Total/NA
Water 6020A 275267680-89881-2 LMW-3-5-13 Total/NA
Water 6020A 275267680-89881-3 LMW-3S-5-13 Total/NA
Water 6020A 275267680-89881-4 LMW-14R-5-13 Total/NA
Water 6020A 275267680-89881-4 MS LMW-14R-5-13 Total/NA
Water 6020A 275267680-89881-4 MSD LMW-14R-5-13 Total/NA
Water 6020A 275267LCS 680-275267/2-A Lab Control Sample Total/NA
Water 6020A 275267MB 680-275267/1-A Method Blank Total/NA
General Chemistry
Analysis Batch: 275389
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0680-89881-1 LMW-6-5-13 Total/NA
Water 300.0680-89881-2 LMW-3-5-13 Total/NA
Water 300.0680-89881-3 LMW-3S-5-13 Total/NA
Water 300.0680-89881-4 LMW-14R-5-13 Total/NA
Water 300.0680-89881-4 MS LMW-14R-5-13 Total/NA
Water 300.0680-89881-4 MSD LMW-14R-5-13 Total/NA
Water 300.0LCS 680-275389/3 Lab Control Sample Total/NA
Water 300.0LCSD 680-275389/4 Lab Control Sample Dup Total/NA
Water 300.0MB 680-275389/2 Method Blank Total/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-89881-1
Project/Site: Ft.Bragg - Lamont Landfill
Client Sample ID: LMW-6-5-13 Lab Sample ID: 680-89881-1
Matrix: WaterDate Collected: 05/01/13 09:56
Date Received: 05/02/13 09:49
Prep 3030C 05/02/13 14:05 BB275267 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275522 05/03/13 12:08 BR TAL SAVTotal/NA
Analysis 300.0 5 275389 05/03/13 03:33 PAT TAL SAVTotal/NA
Client Sample ID: LMW-3-5-13 Lab Sample ID: 680-89881-2
Matrix: WaterDate Collected: 05/01/13 14:15
Date Received: 05/02/13 09:49
Prep 3030C 05/02/13 14:05 BB275267 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275522 05/03/13 12:15 BR TAL SAVTotal/NA
Analysis 300.0 5 275389 05/03/13 03:48 PAT TAL SAVTotal/NA
Client Sample ID: LMW-3S-5-13 Lab Sample ID: 680-89881-3
Matrix: WaterDate Collected: 05/01/13 11:40
Date Received: 05/02/13 09:49
Prep 3030C 05/02/13 14:05 BB275267 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275522 05/03/13 12:21 BR TAL SAVTotal/NA
Analysis 300.0 5 275389 05/03/13 04:04 PAT TAL SAVTotal/NA
Client Sample ID: LMW-14R-5-13 Lab Sample ID: 680-89881-4
Matrix: WaterDate Collected: 05/01/13 15:45
Date Received: 05/02/13 09:49
Prep 3030C 05/02/13 14:05 BB275267 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6020A 1 275522 05/03/13 12:28 BR TAL SAVTotal/NA
Analysis 300.0 5 275389 05/03/13 04:19 PAT TAL SAVTotal/NA
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Login Sample Receipt Checklist
Client: U.S. Army Corps of Engineers Job Number: 680-89881-1
Login Number: 89881
Question Answer Comment
Creator: Conner, Keaton
List Source: TestAmerica Savannah
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Savannah
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Certification Summary
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-89881-1
Project/Site: Ft.Bragg - Lamont Landfill
Laboratory: TestAmerica Savannah
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
A2LA 0399-01DoD ELAP 05-31-13
Alabama State Program 4 41450 06-30-13
Alaska (UST)State Program 10 UST-104 06-19-13
Arkansas DEQ State Program 6 88-0692 02-01-13 *
California NELAP 9 3217CA 07-31-13
Colorado State Program 8 N/A 12-31-13
Florida NELAP 4 E87052 06-30-13
GA Dept. of Agriculture State Program 4 N/A 12-31-13
Georgia State Program 4 N/A 06-30-13
Georgia State Program 4 803 06-30-13
Hawaii State Program 9 N/A 06-30-13
Illinois NELAP 5 200022 11-30-13
Indiana State Program 5 N/A 06-30-13
Iowa State Program 7 353 07-01-13 *
Kentucky State Program 4 90084 12-31-12 *
Kentucky (UST)State Program 4 18 03-31-13 *
Louisiana NELAP 6 30690 06-30-13
Louisiana NELAP 6 LA100015 12-31-13
Maine State Program 1 GA00006 08-16-14
Maryland State Program 3 250 12-31-13
Massachusetts State Program 1 M-GA006 06-30-13
Michigan State Program 5 9925 06-30-13
Mississippi State Program 4 N/A 06-30-13
Montana State Program 8 CERT0081 01-01-14
Nebraska State Program 7 TestAmerica-Savannah 06-30-13 *
New Jersey NELAP 2 GA769 06-30-13
New Mexico State Program 6 N/A 06-30-13
New York NELAP 2 10842 04-01-14
North Carolina DENR State Program 4 269 12-31-13
North Carolina DHHS State Program 4 13701 07-31-13
Oklahoma State Program 6 9984 08-31-13
Pennsylvania NELAP 3 68-00474 06-30-13 *
Puerto Rico State Program 2 GA00006 01-01-14
South Carolina State Program 4 98001 06-30-13
Tennessee State Program 4 TN02961 06-30-13
Texas NELAP 6 T104704185-08-TX 11-30-13
USDA Federal SAV 3-04 04-07-14
Virginia NELAP 3 460161 06-14-13 *
Washington State Program 10 C1794 06-10-13
West Virginia State Program 3 9950C 12-31-13
West Virginia DEP State Program 3 94 06-30-13
Wisconsin State Program 5 999819810 08-31-13
Wyoming State Program 8 8TMS-Q 06-30-13
TestAmerica Savannah
* Expired certification is currently pending renewal and is considered valid.
Page 17 of 17 5/8/2013
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APPENDIX D
STATISTICAL REPORTS
ELECTRONIC ONLY

Concentrations (ppb)
Parameter: 1,2,4-Trichlorobenzene
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements: 77
Total Non-Detect: 76
Percent Non-Detects: 98.7013%
Total Background Measurements: 6
There is 1 background location

Loc. Meas. ND Date Conc. Original

LMW-4 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U 11/17/2010 ND<0.25 U ND<0.25 U
7/6/2011 ND<0.25 U ND<0.25 U 11/22/2011 ND<0.25 U ND<0.25 U 5/16/2012 ND<0.25 U ND<0.25 U
11/16/2012 ND<0.25 U ND<0.25 U

There are 12 compliance locations

Loc. Meas. ND Date Conc. Original

LMW-10 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U 11/17/2010 ND<0.25 U ND<0.25 U 7/6/2011 ND<0.25 U ND<0.25 U
11/22/2011 ND<0.25 U ND<0.25 U 5/16/2012 ND<0.25 U ND<0.25 U 11/16/2012 ND<0.25 U ND<0.25 U

LMW-14R 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U
11/17/2010 ND<0.25 U ND<0.25 U 7/6/2011 ND<0.25 U ND<0.25 U 11/22/2011 ND<0.25 U ND<0.25 U
5/16/2012 ND<0.25 U ND<0.25 U 11/16/2012 ND<0.25 U ND<0.25 U

LMW-15R 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U 11/17/2010 ND<0.25 U ND<0.25 U
7/6/2011 ND<0.25 U ND<0.25 U 11/22/2011 ND<0.25 U ND<0.25 U 5/16/2012 ND<0.25 U ND<0.25 U
11/16/2012 ND<0.25 U ND<0.25 U

LMW-16 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U 11/17/2010 ND<0.25 U ND<0.25 U 7/6/2011 ND<0.25 U ND<0.25 U
11/22/2011 ND<0.25 U ND<0.25 U 5/16/2012 ND<0.25 U ND<0.25 U 11/16/2012 ND<0.25 U ND<0.25 U

LMW-3 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U
11/17/2010 ND<0.25 U ND<0.25 U 7/6/2011 ND<0.25 U ND<0.25 U 11/22/2011 ND<0.25 U ND<0.25 U
5/16/2012 ND<0.25 U ND<0.25 U 11/16/2012 ND<0.25 U ND<0.25 U

LMW-3S 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U 11/17/2010 ND<0.25 U ND<0.25 U
7/6/2011 ND<0.25 U ND<0.25 U 11/22/2011 ND<0.25 U ND<0.25 U 5/16/2012 ND<0.25 U ND<0.25 U
11/16/2012 ND<0.25 U ND<0.25 U

LMW-6 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U
11/17/2010 ND<0.25 U ND<0.25 U 7/6/2011 ND<0.25 U ND<0.25 U
11/22/2011 ND<0.25 U ND<0.25 U 5/16/2012 ND<0.25 U ND<0.25 U 11/16/2012 ND<0.25 U ND<0.25 U

LMW-7 5 4 (80%) 11/17/2010 ND<0.25 U ND<0.25 U 7/6/2011 ND<0.25 U ND<0.25 U
11/22/2011 ND<0.25 U ND<0.25 U 5/16/2012 ND<0.25 U ND<0.25 U
11/16/2012 0.25 J 0.25 J

LMW-8 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U
11/17/2010 ND<0.25 U ND<0.25 U 7/6/2011 ND<0.25 U ND<0.25 U 11/22/2011 ND<0.25 U ND<0.25 U
5/16/2012 ND<0.25 U ND<0.25 U 11/16/2012 ND<0.25 U ND<0.25 U

LMW-9 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U 11/17/2010 ND<0.25 U ND<0.25 U
7/6/2011 ND<0.25 U ND<0.25 U 11/22/2011 ND<0.25 U ND<0.25 U 5/16/2012 ND<0.25 U ND<0.25 U
11/16/2012 ND<0.25 U ND<0.25 U

LMW-9D 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U 11/17/2010 ND<0.25 U ND<0.25 U 7/6/2011 ND<0.25 U ND<0.25 U
11/22/2011 ND<0.25 U ND<0.25 U 5/16/2012 ND<0.25 U ND<0.25 U 11/16/2012 ND<0.25 U ND<0.25 U

LMW-9S 6 6 (100%) 6/30/2010 ND<0.25 U ND<0.25 U
11/17/2010 ND<0.25 U ND<0.25 U 7/6/2011 ND<0.25 U ND<0.25 U 11/22/2011 ND<0.25 U ND<0.25 U
5/16/2012 ND<0.25 U ND<0.25 U 11/16/2012 ND<0.25 U ND<0.25 U

There are 0 unused locations

Loc. Meas. ND Date Conc. Original

Shapiro-Francia Test of Normality
Parameter: 1,2,4-Trichlorobenzene
All Locations
Normality Test of Parameter Concentrations
Original Data (Not Transformed)
Non-Detects Replaced with 1/2 DL
Total Number of Measurements = 77

i x(i) m(i) sum(m^2) sum(mx)
1 0.125 -2.25713 5.09463 -0.282141
2 0.125 -1.95996 8.93608 -0.527136
3 0.125 -1.77438 12.0845 -0.748934
4 0.125 -1.63524 14.7585 -0.953338
5 0.125 -1.52203 17.0751 -1.14359
6 0.125 -1.4325 19.1272 -1.32266
7 0.125 -1.34694 20.9414 -1.49102
8 0.125 -1.27024 22.5549 -1.6498
9 0.125 -1.20036 23.9958 -1.79985
10 0.125 -1.1359 25.286 -1.94183
11 0.125 -1.07584 26.4434 -2.07631
12 0.125 -1.02365 27.4913 -2.20427
13 0.125 -0.970094 28.4324 -2.32553
14 0.125 -0.919183 29.2773 -2.44043
15 0.125 -0.87055 30.0351 -2.54925
16 0.125 -0.823893 30.7139 -2.65224
17 0.125 -0.782366 31.326 -2.75003
18 0.125 -0.738846 31.8719 -2.84239
19 0.125 -0.696684 32.3573 -2.92947
20 0.125 -0.655726 32.7873 -3.01144
21 0.125 -0.615839 33.1665 -3.08842
22 0.125 -0.576911 33.4994 -3.16053
23 0.125 -0.541736 33.7928 -3.22825
24 0.125 -0.504372 34.0472 -3.2913
25 0.125 -0.467699 34.266 -3.34976
26 0.125 -0.431644 34.4523 -3.40371
27 0.125 -0.396142 34.6092 -3.45323
28 0.125 -0.363809 34.7416 -3.49871
29 0.125 -0.329206 34.85 -3.53986
30 0.125 -0.294992 34.937 -3.57673
31 0.125 -0.26112 35.0052 -3.60937
32 0.125 -0.227545 35.0569 -3.63782
33 0.125 -0.194225 35.0947 -3.66209
34 0.125 -0.163659 35.1214 -3.68255
35 0.125 -0.130716 35.1385 -3.69889
36 0.125 -0.0979139 35.1481 -3.71113
37 0.125 -0.0652187 35.1524 -3.71928
38 0.125 -0.0325917 35.1534 -3.72336
39 0.125 0 35.1534 -3.72336
40 0.125 0.0325917 35.1545 -3.71928
41 0.125 0.0652187 35.1587 -3.71113
42 0.125 0.0979139 35.1683 -3.69889
43 0.125 0.130716 35.1854 -3.68255
44 0.125 0.163659 35.2122 -3.66209
45 0.125 0.194225 35.2499 -3.63782
46 0.125 0.227545 35.3017 -3.60937
47 0.125 0.26112 35.3699 -3.57673
48 0.125 0.294992 35.4569 -3.53986
49 0.125 0.329206 35.5653 -3.49871
50 0.125 0.363809 35.6976 -3.45323
51 0.125 0.396142 35.8546 -3.40371
52 0.125 0.431644 36.0409 -3.34976
53 0.125 0.467699 36.2596 -3.2913
54 0.125 0.504372 36.514 -3.22825
55 0.125 0.541736 36.8075 -3.16053
56 0.125 0.576911 37.1403 -3.08842
57 0.125 0.615839 37.5196 -3.01144
58 0.125 0.655726 37.9496 -2.92947
59 0.125 0.696684 38.4349 -2.84239
60 0.125 0.738846 38.9808 -2.75003
61 0.125 0.782366 39.5929 -2.65224
62 0.125 0.823893 40.2717 -2.54925
63 0.125 0.87055 41.0296 -2.44043
64 0.125 0.919183 41.8745 -2.32553
65 0.125 0.970094 42.8156 -2.20427
66 0.125 1.02365 43.8634 -2.07631
67 0.125 1.07584 45.0208 -1.94183
68 0.125 1.1359 46.3111 -1.79985
69 0.125 1.20036 47.752 -1.6498
70 0.125 1.27024 49.3655 -1.49102
71 0.125 1.34694 51.1797 -1.32266
72 0.125 1.4325 53.2318 -1.14359
73 0.125 1.52203 55.5484 -0.953338
74 0.125 1.63524 58.2224 -0.748934
75 0.125 1.77438 61.3708 -0.527136
76 0.125 1.95996 65.2122 -0.282141
77 0.25 2.25713 70.3069 0.282141

Data Set Standard Deviation = 0.0142451
Numerator = 0.0796036
Denominator = 1.08428
W Statistic = 0.0734163 = 0.0796036 / 1.08428

5% Critical value of 0.969 exceeds 0.0734163
Evidence of non-normality at 95% level of significance

1% Critical value of 0.957 exceeds 0.0734163
Evidence of non-normality at 99% level of significance

Probability Plot
Parameter: 1,2,4-Trichlorobenzene
Original Data (Not Transformed)
Non-Detects Replaced with 1/2 DL

Probability Plot
Correlation Coefficient = 0.281856
0.281856 < 0.985 -- Normality test fails at 95% level

Plotted Data Points

Datum Value Prob. Quantile. x y
1 0.125 0.0128205 -2.25713 261.917 324.723
2 0.125 0.025641 -1.95996 261.917 310.211
3 0.125 0.0384615 -1.77438 261.917 301.149
4 0.125 0.0512821 -1.63524 261.917 294.354
5 0.125 0.0641026 -1.52203 261.917 288.826
6 0.125 0.0769231 -1.4325 261.917 284.454
7 0.125 0.0897436 -1.34694 261.917 280.276
8 0.125 0.102564 -1.27024 261.917 276.53
9 0.125 0.115385 -1.20036 261.917 273.118
10 0.125 0.128205 -1.1359 261.917 269.97
11 0.125 0.141026 -1.07584 261.917 267.037
12 0.125 0.153846 -1.02365 261.917 264.488
13 0.125 0.166667 -0.970094 261.917 261.873
14 0.125 0.179487 -0.919183 261.917 259.387
15 0.125 0.192308 -0.87055 261.917 257.012
16 0.125 0.205128 -0.823893 261.917 254.733
17 0.125 0.217949 -0.782366 261.917 252.706
18 0.125 0.230769 -0.738846 261.917 250.58
19 0.125 0.24359 -0.696684 261.917 248.521
20 0.125 0.25641 -0.655726 261.917 246.521
21 0.125 0.269231 -0.615839 261.917 244.573
22 0.125 0.282051 -0.576911 261.917 242.672
23 0.125 0.294872 -0.541736 261.917 240.955
24 0.125 0.307692 -0.504372 261.917 239.13
25 0.125 0.320513 -0.467699 261.917 237.339
26 0.125 0.333333 -0.431644 261.917 235.579
27 0.125 0.346154 -0.396142 261.917 233.845
28 0.125 0.358974 -0.363809 261.917 232.266
29 0.125 0.371795 -0.329206 261.917 230.576
30 0.125 0.384615 -0.294992 261.917 228.905
31 0.125 0.397436 -0.26112 261.917 227.251
32 0.125 0.410256 -0.227545 261.917 225.612
33 0.125 0.423077 -0.194225 261.917 223.985
34 0.125 0.435897 -0.163659 261.917 222.492
35 0.125 0.448718 -0.130716 261.917 220.883
36 0.125 0.461538 -0.0979139 261.917 219.281
37 0.125 0.474359 -0.0652187 261.917 217.685
38 0.125 0.487179 -0.0325917 261.917 216.092
39 0.125 0.5 0 261.917 214.5
40 0.125 0.512821 0.0325917 261.917 212.908
41 0.125 0.525641 0.0652187 261.917 211.315
42 0.125 0.538462 0.0979139 261.917 209.719
43 0.125 0.551282 0.130716 261.917 208.117
44 0.125 0.564103 0.163659 261.917 206.508
45 0.125 0.576923 0.194225 261.917 205.015
46 0.125 0.589744 0.227545 261.917 203.388
47 0.125 0.602564 0.26112 261.917 201.749
48 0.125 0.615385 0.294992 261.917 200.095
49 0.125 0.628205 0.329206 261.917 198.424
50 0.125 0.641026 0.363809 261.917 196.734
51 0.125 0.653846 0.396142 261.917 195.155
52 0.125 0.666667 0.431644 261.917 193.421
53 0.125 0.679487 0.467699 261.917 191.661
54 0.125 0.692308 0.504372 261.917 189.87
55 0.125 0.705128 0.541736 261.917 188.045
56 0.125 0.717949 0.576911 261.917 186.328
57 0.125 0.730769 0.615839 261.917 184.427
58 0.125 0.74359 0.655726 261.917 182.479
59 0.125 0.75641 0.696684 261.917 180.479
60 0.125 0.769231 0.738846 261.917 178.42
61 0.125 0.782051 0.782366 261.917 176.294
62 0.125 0.794872 0.823893 261.917 174.267
63 0.125 0.807692 0.87055 261.917 171.988
64 0.125 0.820513 0.919183 261.917 169.613
65 0.125 0.833333 0.970094 261.917 167.127
66 0.125 0.846154 1.02365 261.917 164.512
67 0.125 0.858974 1.07584 261.917 161.963
68 0.125 0.871795 1.1359 261.917 159.03
69 0.125 0.884615 1.20036 261.917 155.882
70 0.125 0.897436 1.27024 261.917 152.47
71 0.125 0.910256 1.34694 261.917 148.724
72 0.125 0.923077 1.4325 261.917 144.546
73 0.125 0.935897 1.52203 261.917 140.174
74 0.125 0.948718 1.63524 261.917 134.646
75 0.125 0.961538 1.77438 261.917 127.851
76 0.125 0.974359 1.95996 261.917 118.789
77 0.25 0.987179 2.25713 484.833 104.277

Shapiro-Francia Test of Normality
Parameter: 1,2,4-Trichlorobenzene
All Locations
Normality Test of Parameter Concentrations
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL
Total Number of Measurements = 77

i x(i) m(i) sum(m^2) sum(mx)
1 -2.07944 -2.25713 5.09463 4.69357
2 -2.07944 -1.95996 8.93608 8.76919
3 -2.07944 -1.77438 12.0845 12.4589
4 -2.07944 -1.63524 14.7585 15.8593
5 -2.07944 -1.52203 17.0751 19.0243
6 -2.07944 -1.4325 19.1272 22.0031
7 -2.07944 -1.34694 20.9414 24.804
8 -2.07944 -1.27024 22.5549 27.4453
9 -2.07944 -1.20036 23.9958 29.9414
10 -2.07944 -1.1359 25.286 32.3034
11 -2.07944 -1.07584 26.4434 34.5406
12 -2.07944 -1.02365 27.4913 36.6692
13 -2.07944 -0.970094 28.4324 38.6865
14 -2.07944 -0.919183 29.2773 40.5979
15 -2.07944 -0.87055 30.0351 42.4081
16 -2.07944 -0.823893 30.7139 44.1213
17 -2.07944 -0.782366 31.326 45.7482
18 -2.07944 -0.738846 31.8719 47.2846
19 -2.07944 -0.696684 32.3573 48.7333
20 -2.07944 -0.655726 32.7873 50.0969
21 -2.07944 -0.615839 33.1665 51.3775
22 -2.07944 -0.576911 33.4994 52.5771
23 -2.07944 -0.541736 33.7928 53.7036
24 -2.07944 -0.504372 34.0472 54.7525
25 -2.07944 -0.467699 34.266 55.725
26 -2.07944 -0.431644 34.4523 56.6226
27 -2.07944 -0.396142 34.6092 57.4463
28 -2.07944 -0.363809 34.7416 58.2029
29 -2.07944 -0.329206 34.85 58.8874
30 -2.07944 -0.294992 34.937 59.5008
31 -2.07944 -0.26112 35.0052 60.0438
32 -2.07944 -0.227545 35.0569 60.517
33 -2.07944 -0.194225 35.0947 60.9209
34 -2.07944 -0.163659 35.1214 61.2612
35 -2.07944 -0.130716 35.1385 61.533
36 -2.07944 -0.0979139 35.1481 61.7366
37 -2.07944 -0.0652187 35.1524 61.8722
38 -2.07944 -0.0325917 35.1534 61.94
39 -2.07944 0 35.1534 61.94
40 -2.07944 0.0325917 35.1545 61.8722
41 -2.07944 0.0652187 35.1587 61.7366
42 -2.07944 0.0979139 35.1683 61.533
43 -2.07944 0.130716 35.1854 61.2612
44 -2.07944 0.163659 35.2122 60.9209
45 -2.07944 0.194225 35.2499 60.517
46 -2.07944 0.227545 35.3017 60.0438
47 -2.07944 0.26112 35.3699 59.5008
48 -2.07944 0.294992 35.4569 58.8874
49 -2.07944 0.329206 35.5653 58.2029
50 -2.07944 0.363809 35.6976 57.4463
51 -2.07944 0.396142 35.8546 56.6226
52 -2.07944 0.431644 36.0409 55.725
53 -2.07944 0.467699 36.2596 54.7525
54 -2.07944 0.504372 36.514 53.7036
55 -2.07944 0.541736 36.8075 52.5771
56 -2.07944 0.576911 37.1403 51.3775
57 -2.07944 0.615839 37.5196 50.0969
58 -2.07944 0.655726 37.9496 48.7333
59 -2.07944 0.696684 38.4349 47.2846
60 -2.07944 0.738846 38.9808 45.7482
61 -2.07944 0.782366 39.5929 44.1213
62 -2.07944 0.823893 40.2717 42.4081
63 -2.07944 0.87055 41.0296 40.5979
64 -2.07944 0.919183 41.8745 38.6865
65 -2.07944 0.970094 42.8156 36.6692
66 -2.07944 1.02365 43.8634 34.5406
67 -2.07944 1.07584 45.0208 32.3034
68 -2.07944 1.1359 46.3111 29.9414
69 -2.07944 1.20036 47.752 27.4453
70 -2.07944 1.27024 49.3655 24.804
71 -2.07944 1.34694 51.1797 22.0031
72 -2.07944 1.4325 53.2318 19.0243
73 -2.07944 1.52203 55.5484 15.8593
74 -2.07944 1.63524 58.2224 12.4589
75 -2.07944 1.77438 61.3708 8.76919
76 -2.07944 1.95996 65.2122 4.69357
77 -1.38629 2.25713 70.3069 1.56452

Data Set Standard Deviation = 0.0789915
Numerator = 2.44773
Denominator = 33.3405
W Statistic = 0.0734163 = 2.44773 / 33.3405

5% Critical value of 0.969 exceeds 0.0734163
Evidence of non-normality at 95% level of significance

1% Critical value of 0.957 exceeds 0.0734163
Evidence of non-normality at 99% level of significance

Probability Plot
Parameter: 1,2,4-Trichlorobenzene
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Probability Plot
Correlation Coefficient = 0.281856
0.281856 < 0.985 -- Normality test fails at 95% level

Plotted Data Points

Datum Value Prob. Quantile. x y
1 -2.07944 0.0128205 -2.25713 203.166 324.723
2 -2.07944 0.025641 -1.95996 203.166 310.211
3 -2.07944 0.0384615 -1.77438 203.166 301.149
4 -2.07944 0.0512821 -1.63524 203.166 294.354
5 -2.07944 0.0641026 -1.52203 203.166 288.826
6 -2.07944 0.0769231 -1.4325 203.166 284.454
7 -2.07944 0.0897436 -1.34694 203.166 280.276
8 -2.07944 0.102564 -1.27024 203.166 276.53
9 -2.07944 0.115385 -1.20036 203.166 273.118
10 -2.07944 0.128205 -1.1359 203.166 269.97
11 -2.07944 0.141026 -1.07584 203.166 267.037
12 -2.07944 0.153846 -1.02365 203.166 264.488
13 -2.07944 0.166667 -0.970094 203.166 261.873
14 -2.07944 0.179487 -0.919183 203.166 259.387
15 -2.07944 0.192308 -0.87055 203.166 257.012
16 -2.07944 0.205128 -0.823893 203.166 254.733
17 -2.07944 0.217949 -0.782366 203.166 252.706
18 -2.07944 0.230769 -0.738846 203.166 250.58
19 -2.07944 0.24359 -0.696684 203.166 248.521
20 -2.07944 0.25641 -0.655726 203.166 246.521
21 -2.07944 0.269231 -0.615839 203.166 244.573
22 -2.07944 0.282051 -0.576911 203.166 242.672
23 -2.07944 0.294872 -0.541736 203.166 240.955
24 -2.07944 0.307692 -0.504372 203.166 239.13
25 -2.07944 0.320513 -0.467699 203.166 237.339
26 -2.07944 0.333333 -0.431644 203.166 235.579
27 -2.07944 0.346154 -0.396142 203.166 233.845
28 -2.07944 0.358974 -0.363809 203.166 232.266
29 -2.07944 0.371795 -0.329206 203.166 230.576
30 -2.07944 0.384615 -0.294992 203.166 228.905
31 -2.07944 0.397436 -0.26112 203.166 227.251
32 -2.07944 0.410256 -0.227545 203.166 225.612
33 -2.07944 0.423077 -0.194225 203.166 223.985
34 -2.07944 0.435897 -0.163659 203.166 222.492
35 -2.07944 0.448718 -0.130716 203.166 220.883
36 -2.07944 0.461538 -0.0979139 203.166 219.281
37 -2.07944 0.474359 -0.0652187 203.166 217.685
38 -2.07944 0.487179 -0.0325917 203.166 216.092
39 -2.07944 0.5 0 203.166 214.5
40 -2.07944 0.512821 0.0325917 203.166 212.908
41 -2.07944 0.525641 0.0652187 203.166 211.315
42 -2.07944 0.538462 0.0979139 203.166 209.719
43 -2.07944 0.551282 0.130716 203.166 208.117
44 -2.07944 0.564103 0.163659 203.166 206.508
45 -2.07944 0.576923 0.194225 203.166 205.015
46 -2.07944 0.589744 0.227545 203.166 203.388
47 -2.07944 0.602564 0.26112 203.166 201.749
48 -2.07944 0.615385 0.294992 203.166 200.095
49 -2.07944 0.628205 0.329206 203.166 198.424
50 -2.07944 0.641026 0.363809 203.166 196.734
51 -2.07944 0.653846 0.396142 203.166 195.155
52 -2.07944 0.666667 0.431644 203.166 193.421
53 -2.07944 0.679487 0.467699 203.166 191.661
54 -2.07944 0.692308 0.504372 203.166 189.87
55 -2.07944 0.705128 0.541736 203.166 188.045
56 -2.07944 0.717949 0.576911 203.166 186.328
57 -2.07944 0.730769 0.615839 203.166 184.427
58 -2.07944 0.74359 0.655726 203.166 182.479
59 -2.07944 0.75641 0.696684 203.166 180.479
60 -2.07944 0.769231 0.738846 203.166 178.42
61 -2.07944 0.782051 0.782366 203.166 176.294
62 -2.07944 0.794872 0.823893 203.166 174.267
63 -2.07944 0.807692 0.87055 203.166 171.988
64 -2.07944 0.820513 0.919183 203.166 169.613
65 -2.07944 0.833333 0.970094 203.166 167.127
66 -2.07944 0.846154 1.02365 203.166 164.512
67 -2.07944 0.858974 1.07584 203.166 161.963
68 -2.07944 0.871795 1.1359 203.166 159.03
69 -2.07944 0.884615 1.20036 203.166 155.882
70 -2.07944 0.897436 1.27024 203.166 152.47
71 -2.07944 0.910256 1.34694 203.166 148.724
72 -2.07944 0.923077 1.4325 203.166 144.546
73 -2.07944 0.935897 1.52203 203.166 140.174
74 -2.07944 0.948718 1.63524 203.166 134.646
75 -2.07944 0.961538 1.77438 203.166 127.851
76 -2.07944 0.974359 1.95996 203.166 118.789
77 -1.38629 0.987179 2.25713 326.778 104.277

Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: 1,2,4-Trichlorobenzene
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Total Percent Non-Detects = 98.7013%
Number of comparisons = 12
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 6
Maximum Background Value = 0
Confidence Level = 42.9%
False Positive Rate = 57.1%

Location Date Count Mean Significant
LMW-10 11/16/2012 1 -2.07944 FALSE

LMW-14R 11/16/2012 1 -2.07944 FALSE

LMW-15R 11/16/2012 1 -2.07944 FALSE

LMW-16 11/16/2012 1 -2.07944 FALSE

LMW-3 11/16/2012 1 -2.07944 FALSE

LMW-3S 11/16/2012 1 -2.07944 FALSE

LMW-6 11/16/2012 1 -2.07944 FALSE

LMW-7 11/16/2012 1 -1.38629 FALSE

LMW-8 11/16/2012 1 -2.07944 FALSE

LMW-9 11/16/2012 1 -2.07944 FALSE

LMW-9D11/16/2012 1 -2.07944 FALSE

LMW-9S 11/16/2012 1 -2.07944 FALSE

Concentrations (ppb)
Parameter: 1,2-cis-Dichloroethylene
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements: 272
Total Non-Detect: 265
Percent Non-Detects: 97.4265%
Total Background Measurements: 22
There is 1 background location

Loc. Meas. ND Date Conc. Original

LMW-4 22 22 (100%) 1/16/1998 ND<1 ND<1 3/16/1999 ND<1 ND<1 9/23/1999 ND<1 ND<1 3/14/2000 ND<1 ND<1
9/23/2003 ND<1 ND<1 3/10/2004 ND<1 ND<1
10/12/2004 ND<1 ND<1 4/1/2005 ND<1 ND<1 10/26/2005 ND<1 ND<1
6/19/2006 ND<1 ND<1 11/18/2006 ND<1 ND<1 6/2/2007 ND<1 ND<1
11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1
6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U 11/17/2010 ND<0.15 U ND<0.15 U
7/6/2011 ND<0.15 U ND<0.15 U 11/22/2011 ND<0.15 U ND<0.15 U
5/16/2012 ND<0.15 U ND<0.15 U 11/16/2012 ND<0.15 U ND<0.15 U

There are 16 compliance locations

Loc. Meas. ND Date Conc. Original

LMW-10 19 19 (100%) 3/14/2000 ND<1 ND<1 9/23/2003 ND<1 ND<1
3/10/2004 ND<1 ND<1 10/12/2004 ND<1 ND<1 4/1/2005 ND<1 ND<1
10/26/2005 ND<1 ND<1 6/19/2006 ND<1 ND<1 11/18/2006 ND<1 ND<1
6/2/2007 ND<1 ND<1 11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1
11/20/2008 ND<1 ND<1 6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U
11/17/2010 ND<0.15 U ND<0.15 U 7/6/2011 ND<0.15 U ND<0.15 U
11/22/2011 ND<0.15 U ND<0.15 U 5/16/2012 ND<0.15 U ND<0.15 U 11/16/2012 ND<0.15 U ND<0.15 U

LMW-11 11 11 (100%) 3/14/2000 ND<1 ND<1
9/23/2003 ND<1 ND<1 3/10/2004 ND<1 ND<1
10/12/2004 ND<1 ND<1 4/1/2005 ND<1 ND<1 10/26/2005 ND<1 ND<1
6/19/2006 ND<1 ND<1 6/2/2007 ND<1 ND<1 11/15/2007 ND<1 ND<1
5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1

LMW-12 11 11 (100%) 3/14/2000 ND<1 ND<1 9/23/2003 ND<1 ND<1
3/10/2004 ND<1 ND<1 10/12/2004 ND<1 ND<1 4/1/2005 ND<1 ND<1
10/26/2005 ND<1 ND<1 6/19/2006 ND<1 ND<1 6/2/2007 ND<1 ND<1
11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1

LMW-13 11 11 (100%) 3/14/2000 ND<1 ND<1
9/23/2003 ND<1 ND<1 3/10/2004 ND<1 ND<1 10/12/2004 ND<1 ND<1
4/1/2005 ND<1 ND<1 10/26/2005 ND<1 ND<1 6/19/2006 ND<1 ND<1
6/2/2007 ND<1 ND<1 11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1
11/20/2008 ND<1 ND<1

LMW-14R 11 11 (100%) 6/2/2007 ND<1 ND<1 11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1
11/20/2008 ND<1 ND<1 6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U
11/17/2010 ND<0.15 U ND<0.15 U 7/6/2011 ND<0.15 U ND<0.15 U 11/22/2011 ND<0.15 U ND<0.15 U
5/16/2012 ND<0.15 U ND<0.15 U 11/16/2012 ND<0.15 U ND<0.15 U

LMW-15R 15 15 (100%) 11/18/2006 ND<1 ND<1 6/2/2007 ND<1 ND<1
11/15/2007 ND<1 ND<1 11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1
5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1
6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U 11/17/2010 ND<0.15 U ND<0.15 U
7/6/2011 ND<0.15 U ND<0.15 U 11/22/2011 ND<0.15 U ND<0.15 U
5/16/2012 ND<0.15 U ND<0.15 U 11/16/2012 ND<0.15 U ND<0.15 U

LMW-16 12 12 (100%) 11/18/2006 ND<1 ND<1
6/2/2007 ND<1 ND<1 11/15/2007 ND<1 ND<1
5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1 6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U
11/17/2010 ND<0.15 U ND<0.15 U 7/6/2011 ND<0.15 U ND<0.15 U
11/22/2011 ND<0.15 U ND<0.15 U 5/16/2012 ND<0.15 U ND<0.15 U 11/16/2012 ND<0.15 U ND<0.15 U

LMW-3 24 24 (100%) 11/19/1996 ND<1 ND<1 3/24/1997 ND<1 ND<1
1/16/1998 ND<1 ND<1 3/16/1999 ND<1 ND<1
9/23/1999 ND<1 ND<1 3/14/2000 ND<1 ND<1 9/23/2003 ND<1 ND<1
3/10/2004 ND<1 ND<1 10/12/2004 ND<1 ND<1 4/1/2005 ND<1 ND<1
10/26/2005 ND<1 ND<1 6/19/2006 ND<1 ND<1 11/18/2006 ND<1 ND<1
6/2/2007 ND<1 ND<1 11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1
11/20/2008 ND<1 ND<1 6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U
11/17/2010 ND<0.15 U ND<0.15 U 7/6/2011 ND<0.15 U ND<0.15 U
11/22/2011 ND<0.15 U ND<0.15 U 5/16/2012 ND<0.15 U ND<0.15 U 11/16/2012 ND<0.15 U ND<0.15 U

LMW-3S 12 12 (100%) 11/18/2006 ND<1 ND<1 6/2/2007 ND<1 ND<1
11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1
6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U 11/17/2010 ND<0.15 U ND<0.15 U
7/6/2011 ND<0.15 U ND<0.15 U 11/22/2011 ND<0.15 U ND<0.15 U
5/16/2012 ND<0.15 U ND<0.15 U 11/16/2012 ND<0.15 U ND<0.15 U

LMW-6 22 22 (100%) 1/16/1998 ND<1 ND<1 3/16/1999 ND<1 ND<1 9/23/1999 ND<1 ND<1
3/14/2000 ND<1 ND<1 9/23/2003 ND<1 ND<1 3/10/2004 ND<1 ND<1
10/12/2004 ND<1 ND<1 4/1/2005 ND<1 ND<1
10/26/2005 ND<1 ND<1 6/19/2006 ND<1 ND<1
11/18/2006 ND<1 ND<1 6/2/2007 ND<1 ND<1
11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1
6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U 11/17/2010 ND<0.15 U ND<0.15 U
7/6/2011 ND<0.15 U ND<0.15 U 11/22/2011 ND<0.15 U ND<0.15 U 5/16/2012 ND<0.15 U ND<0.15 U
11/16/2012 ND<0.15 U ND<0.15 U

LMW-7 21 21 (100%) 1/16/1998 ND<1 ND<1 3/16/1999 ND<1 ND<1 9/23/1999 ND<1 ND<1
3/14/2000 ND<1 ND<1 9/23/2003 ND<1 ND<1 3/10/2004 ND<1 ND<1
10/12/2004 ND<1 ND<1 4/1/2005 ND<1 ND<1 10/26/2005 ND<1 ND<1
6/19/2006 ND<1 ND<1 11/18/2006 ND<1 ND<1 6/2/2007 ND<1 ND<1
11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1 6/11/2009 ND<0.15 U ND<0.15 U 11/17/2010 ND<0.15 U ND<0.15 U
7/6/2011 ND<0.15 U ND<0.15 U 11/22/2011 ND<0.15 U ND<0.15 U 5/16/2012 ND<0.15 U ND<0.15 U
11/16/2012 ND<0.15 U ND<0.15 U

LMW-8 22 15 (68.1818%) 1/16/1998 ND<1 ND<1 3/16/1999 ND<1 ND<1 9/23/1999 ND<1 ND<1 3/14/2000 ND<1 ND<1
9/23/2003 ND<1 ND<1 3/10/2004 ND<1 ND<1
10/12/2004 ND<1 ND<1 4/1/2005 ND<1 ND<1 10/26/2005 ND<0 J ND<0 J
6/19/2006 ND<0 J ND<0 J 11/18/2006 ND<0 J ND<0 J 6/2/2007 ND<1 ND<1
11/15/2007 ND<0 J ND<0 J 5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1
6/11/2009 2.4 2.4 6/30/2010 1.1 1.1 11/17/2010 0.67 J 0.67 J
7/6/2011 1.5 1.5 11/22/2011 1.7 1.7
5/16/2012 3.2 3.2 11/16/2012 2.7 2.7

LMW-9 22 22 (100%) 1/16/1998 ND<1 ND<1 3/16/1999 ND<1 ND<1 9/23/1999 ND<1 ND<1
3/14/2000 ND<1 ND<1
9/23/2003 ND<1 ND<1 3/10/2004 ND<1 ND<1
10/12/2004 ND<1 ND<1 4/1/2005 ND<1 ND<1 10/26/2005 ND<1 ND<1
6/19/2006 ND<1 ND<1 11/18/2006 ND<1 ND<1 6/2/2007 ND<1 ND<1
11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1
6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U 11/17/2010 ND<0.15 U ND<0.15 U
7/6/2011 ND<0.15 U ND<0.15 U 11/22/2011 ND<0.15 U ND<0.15 U
5/16/2012 ND<0.15 U ND<0.15 U 11/16/2012 ND<0.15 U ND<0.15 U

LMW-9D 12 12 (100%) 11/18/2006 ND<1 ND<1 6/2/2007 ND<1 ND<1 11/15/2007 ND<1 ND<1
5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1 6/11/2009 ND<0.15 U ND<0.15 U
6/30/2010 ND<0.15 U ND<0.15 U 11/17/2010 ND<0.15 U ND<0.15 U 7/6/2011 ND<0.15 U ND<0.15 U 11/22/2011 ND<0.15 U ND<0.15 U 5/16/2012 ND<0.15 U ND<0.15 U
11/16/2012 ND<0.15 U ND<0.15 U

LMW-9S 12 12 (100%) 11/18/2006 ND<1 ND<1
6/2/2007 ND<1 ND<1 11/15/2007 ND<1 ND<1
5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1 6/11/2009 ND<0.15 U ND<0.15 U 6/30/2010 ND<0.15 U ND<0.15 U
11/17/2010 ND<0.15 U ND<0.15 U 7/6/2011 ND<0.15 U ND<0.15 U
11/22/2011 ND<0.15 U ND<0.15 U 5/16/2012 ND<0.15 U ND<0.15 U 11/16/2012 ND<0.15 U ND<0.15 U

MW-5 13 13 (100%) 1/16/1998 ND<1 ND<1 3/16/1999 ND<1 ND<1
9/23/1999 ND<1 ND<1 3/14/2000 ND<1 ND<1
9/23/2003 ND<1 ND<1 3/10/2004 ND<1 ND<1 10/12/2004 ND<1 ND<1
4/1/2005 ND<1 ND<1 10/26/2005 ND<1 ND<1 6/19/2006 ND<1 ND<1
11/15/2007 ND<1 ND<1 5/20/2008 ND<1 ND<1 11/20/2008 ND<1 ND<1

There are 0 unused locations

Loc. Meas. ND Date Conc. Original

Shapiro-Francia Test of Normality
Parameter: 1,2-cis-Dichloroethylene
All Locations
Normality Test of Parameter Concentrations
Original Data (Not Transformed)
Non-Detects Replaced with 1/2 DL
Total Number of Measurements = 272

i x(i) m(i) sum(m^2) sum(mx)
1 0 -2.74777 7.55021 0
2 0 -2.45727 13.5884 0
3 0 -2.32634 19.0003 0
4 0 -2.19728 23.8283 0
5 0.075 -2.09693 28.2255 -0.15727
6 0.075 -2.03352 32.3607 -0.309784
7 0.075 -1.95996 36.2021 -0.456781
8 0.075 -1.8957 39.7958 -0.598958
9 0.075 -1.85218 43.2263 -0.737871
10 0.075 -1.79912 46.4632 -0.872805
11 0.075 -1.75069 49.5281 -1.00411
12 0.075 -1.71688 52.4757 -1.13287
13 0.075 -1.67466 55.2802 -1.25847
14 0.075 -1.63524 57.9542 -1.38112
15 0.075 -1.60725 60.5375 -1.50166
16 0.075 -1.57179 63.008 -1.61954
17 0.075 -1.5382 65.3741 -1.73491
18 0.075 -1.5141 67.6666 -1.84847
19 0.075 -1.48328 69.8667 -1.95971
20 0.075 -1.4538 71.9802 -2.06875
21 0.075 -1.4325 74.0323 -2.17619
22 0.075 -1.40507 76.0066 -2.28157
23 0.075 -1.37866 77.9072 -2.38497
24 0.075 -1.35946 79.7554 -2.48692
25 0.075 -1.33462 81.5366 -2.58702
26 0.075 -1.31058 83.2542 -2.68532
27 0.075 -1.29303 84.9262 -2.78229
28 0.075 -1.27024 86.5397 -2.87756
29 0.075 -1.24809 88.0974 -2.97117
30 0.075 -1.23187 89.6149 -3.06356
31 0.075 -1.21073 91.0807 -3.15436
32 0.075 -1.19012 92.4971 -3.24362
33 0.075 -1.17499 93.8777 -3.33174
34 0.075 -1.15522 95.2123 -3.41839
35 0.075 -1.1359 96.5025 -3.50358
36 0.075 -1.12168 97.7607 -3.5877
37 0.075 -1.10306 98.9774 -3.67043
38 0.075 -1.08482 100.154 -3.7518
39 0.075 -1.07138 101.302 -3.83215
40 0.075 -1.05375 102.412 -3.91118
41 0.075 -1.03643 103.487 -3.98891
42 0.075 -1.02365 104.535 -4.06569
43 0.075 -1.00687 105.548 -4.1412
44 0.075 -0.990356 106.529 -4.21548
45 0.075 -0.97815 107.486 -4.28884
46 0.075 -0.9621 108.412 -4.361
47 0.075 -0.946291 109.307 -4.43197
48 0.075 -0.93459 110.18 -4.50206
49 0.075 -0.919183 111.025 -4.571
50 0.075 -0.903992 111.843 -4.6388
51 0.075 -0.892733 112.64 -4.70576
52 0.075 -0.877897 113.41 -4.7716
53 0.075 -0.863249 114.155 -4.83634
54 0.075 -0.852385 114.882 -4.90027
55 0.075 -0.838054 115.584 -4.96312
56 0.075 -0.823893 116.263 -5.02492
57 0.075 -0.813379 116.925 -5.08592
58 0.075 -0.7995 117.564 -5.14588
59 0.075 -0.785774 118.181 -5.20482
60 0.075 -0.775574 118.783 -5.26298
61 0.075 -0.7621 119.364 -5.32014
62 0.075 -0.748762 119.924 -5.3763
63 0.075 -0.738846 120.47 -5.43171
64 0.075 -0.725736 120.997 -5.48614
65 0.075 -0.712751 121.505 -5.5396
66 0.075 -0.703089 121.999 -5.59233
67 0.075 -0.690309 122.476 -5.6441
68 0.075 -0.677639 122.935 -5.69493
69 0.075 -0.668209 123.381 -5.74504
70 0.075 -0.655726 123.811 -5.79422
71 0.075 -0.643345 124.225 -5.84247
72 0.075 -0.634124 124.627 -5.89003
73 0.075 -0.621911 125.014 -5.93667
74 0.075 -0.609791 125.386 -5.98241
75 0.075 -0.60076 125.747 -6.02747
76 0.075 -0.588793 126.094 -6.07163
77 0.075 -0.576911 126.426 -6.11489
78 0.075 -0.568052 126.749 -6.1575
79 0.075 -0.556308 127.059 -6.19922
80 0.075 -0.544642 127.355 -6.24007
81 0.075 -0.53594 127.643 -6.28026
82 0.075 -0.524401 127.918 -6.31959
83 0.075 -0.51293 128.181 -6.35806
84 0.075 -0.504372 128.435 -6.39589
85 0.075 -0.493018 128.678 -6.43287
86 0.075 -0.481728 128.91 -6.469
87 0.075 -0.473299 129.134 -6.5045
88 0.5 -0.462114 129.348 -6.73555
89 0.5 -0.450985 129.551 -6.96105
90 0.5 -0.442676 129.747 -7.18238
91 0.5 -0.431644 129.933 -7.39821
92 0.5 -0.423405 130.113 -7.60991
93 0.5 -0.412463 130.283 -7.81614
94 0.5 -0.401571 130.444 -8.01692
95 0.5 -0.393433 130.599 -8.21364
96 0.5 -0.382622 130.745 -8.40495
97 0.5 -0.371856 130.883 -8.59088
98 0.5 -0.363809 131.016 -8.77278
99 0.5 -0.353118 131.141 -8.94934
100 0.5 -0.342466 131.258 -9.12058
101 0.5 -0.334503 131.37 -9.28783
102 0.5 -0.323919 131.475 -9.44979
103 0.5 -0.31337 131.573 -9.60647
104 0.5 -0.305481 131.666 -9.75921
105 0.5 -0.294992 131.753 -9.90671
106 0.5 -0.284535 131.834 -10.049
107 0.5 -0.276714 131.911 -10.1873
108 0.5 -0.266311 131.982 -10.3205
109 0.5 -0.255936 132.047 -10.4485
110 0.5 -0.248174 132.109 -10.5725
111 0.5 -0.237847 132.165 -10.6915
112 0.5 -0.227545 132.217 -10.8052
113 0.5 -0.219834 132.265 -10.9152
114 0.5 -0.209575 132.309 -11.0199
115 0.5 -0.199336 132.349 -11.1196
116 0.5 -0.191671 132.386 -11.2154
117 0.5 -0.181468 132.419 -11.3062
118 0.5 -0.171285 132.448 -11.3918
119 0.5 -0.163659 132.475 -11.4737
120 0.5 -0.153505 132.498 -11.5504
121 0.5 -0.143367 132.519 -11.6221
122 0.5 -0.135774 132.537 -11.69
123 0.5 -0.125661 132.553 -11.7528
124 0.5 -0.115562 132.567 -11.8106
125 0.5 -0.107995 132.578 -11.8646
126 0.5 -0.0979139 132.588 -11.9135
127 0.5 -0.0878447 132.596 -11.9575
128 0.5 -0.0802981 132.602 -11.9976
129 0.5 -0.0702426 132.607 -12.0327
130 0.5 -0.0601949 132.611 -12.0628
131 0.5 -0.0526632 132.613 -12.0892
132 0.5 -0.0426257 132.615 -12.1105
133 0.5 -0.0325917 132.616 -12.1268
134 0.5 -0.0250691 132.617 -12.1393
135 0.5 -0.0150408 132.617 -12.1468
136 0.5 -0.00501359 132.617 -12.1493
137 0.5 0.00501359 132.617 -12.1468
138 0.5 0.0150408 132.617 -12.1393
139 0.5 0.0250691 132.618 -12.1268
140 0.5 0.0325917 132.619 -12.1105
141 0.5 0.0426257 132.621 -12.0892
142 0.5 0.0526632 132.624 -12.0628
143 0.5 0.0601949 132.627 -12.0327
144 0.5 0.0702426 132.632 -11.9976
145 0.5 0.0802981 132.639 -11.9575
146 0.5 0.0878447 132.646 -11.9135
147 0.5 0.0979139 132.656 -11.8646
148 0.5 0.107995 132.668 -11.8106
149 0.5 0.115562 132.681 -11.7528
150 0.5 0.125661 132.697 -11.69
151 0.5 0.135774 132.715 -11.6221
152 0.5 0.143367 132.736 -11.5504
153 0.5 0.153505 132.759 -11.4737
154 0.5 0.163659 132.786 -11.3918
155 0.5 0.171285 132.815 -11.3062
156 0.5 0.181468 132.848 -11.2154
157 0.5 0.191671 132.885 -11.1196
158 0.5 0.199336 132.925 -11.0199
159 0.5 0.209575 132.969 -10.9152
160 0.5 0.219834 133.017 -10.8052
161 0.5 0.227545 133.069 -10.6915
162 0.5 0.237847 133.125 -10.5725
163 0.5 0.248174 133.187 -10.4485
164 0.5 0.255936 133.252 -10.3205
165 0.5 0.266311 133.323 -10.1873
166 0.5 0.276714 133.4 -10.049
167 0.5 0.284535 133.481 -9.90671
168 0.5 0.294992 133.568 -9.75921
169 0.5 0.305481 133.661 -9.60647
170 0.5 0.31337 133.759 -9.44979
171 0.5 0.323919 133.864 -9.28783
172 0.5 0.334503 133.976 -9.12058
173 0.5 0.342466 134.094 -8.94934
174 0.5 0.353118 134.218 -8.77278
175 0.5 0.363809 134.351 -8.59088
176 0.5 0.371856 134.489 -8.40495
177 0.5 0.382622 134.635 -8.21364
178 0.5 0.393433 134.79 -8.01692
179 0.5 0.401571 134.951 -7.81614
180 0.5 0.412463 135.121 -7.60991
181 0.5 0.423405 135.301 -7.39821
182 0.5 0.431644 135.487 -7.18238
183 0.5 0.442676 135.683 -6.96105
184 0.5 0.450985 135.886 -6.73555
185 0.5 0.462114 136.1 -6.5045
186 0.5 0.473299 136.324 -6.26785
187 0.5 0.481728 136.556 -6.02698
188 0.5 0.493018 136.799 -5.78047
189 0.5 0.504372 137.053 -5.52829
190 0.5 0.51293 137.317 -5.27182
191 0.5 0.524401 137.592 -5.00962
192 0.5 0.53594 137.879 -4.74165
193 0.5 0.544642 138.175 -4.46933
194 0.5 0.556308 138.485 -4.19118
195 0.5 0.568052 138.808 -3.90715
196 0.5 0.576911 139.14 -3.6187
197 0.5 0.588793 139.487 -3.3243
198 0.5 0.60076 139.848 -3.02392
199 0.5 0.609791 140.22 -2.71902
200 0.5 0.621911 140.607 -2.40807
201 0.5 0.634124 141.009 -2.09101
202 0.5 0.643345 141.423 -1.76933
203 0.5 0.655726 141.853 -1.44147
204 0.5 0.668209 142.299 -1.10737
205 0.5 0.677639 142.758 -0.768546
206 0.5 0.690309 143.235 -0.423391
207 0.5 0.703089 143.729 -0.0718467
208 0.5 0.712751 144.237 0.284529
209 0.5 0.725736 144.764 0.647396
210 0.5 0.738846 145.31 1.01682
211 0.5 0.748762 145.87 1.3912
212 0.5 0.7621 146.451 1.77225
213 0.5 0.775574 147.053 2.16004
214 0.5 0.785774 147.67 2.55292
215 0.5 0.7995 148.309 2.95267
216 0.5 0.813379 148.971 3.35936
217 0.5 0.823893 149.65 3.77131
218 0.5 0.838054 150.352 4.19034
219 0.5 0.852385 151.079 4.61653
220 0.5 0.863249 151.824 5.04815
221 0.5 0.877897 152.595 5.4871
222 0.5 0.892733 153.392 5.93347
223 0.5 0.903992 154.209 6.38547
224 0.5 0.919183 155.054 6.84506
225 0.5 0.93459 155.927 7.31235
226 0.5 0.946291 156.823 7.7855
227 0.5 0.9621 157.748 8.26655
228 0.5 0.97815 158.705 8.75562
229 0.5 0.990356 159.686 9.2508
230 0.5 1.00687 160.7 9.75423
231 0.5 1.02365 161.747 10.2661
232 0.5 1.03643 162.822 10.7843
233 0.5 1.05375 163.932 11.3111
234 0.5 1.07138 165.08 11.8468
235 0.5 1.08482 166.257 12.3892
236 0.5 1.10306 167.473 12.9408
237 0.5 1.12168 168.732 13.5016
238 0.5 1.1359 170.022 14.0696
239 0.5 1.15522 171.356 14.6472
240 0.5 1.17499 172.737 15.2347
241 0.5 1.19012 174.153 15.8297
242 0.5 1.21073 175.619 16.4351
243 0.5 1.23187 177.137 17.051
244 0.5 1.24809 178.694 17.6751
245 0.5 1.27024 180.308 18.3102
246 0.5 1.29303 181.98 18.9567
247 0.5 1.31058 183.697 19.612
248 0.5 1.33462 185.479 20.2793
249 0.5 1.35946 187.327 20.959
250 0.5 1.37866 189.228 21.6484
251 0.5 1.40507 191.202 22.3509
252 0.5 1.4325 193.254 23.0672
253 0.5 1.4538 195.367 23.7941
254 0.5 1.48328 197.568 24.5357
255 0.5 1.5141 199.86 25.2928
256 0.5 1.5382 202.226 26.0619
257 0.5 1.57179 204.697 26.8477
258 0.5 1.60725 207.28 27.6514
259 0.5 1.63524 209.954 28.469
260 0.5 1.67466 212.758 29.3063
261 0.5 1.71688 215.706 30.1648
262 0.5 1.75069 218.771 31.0401
263 0.5 1.79912 222.008 31.9397
264 0.5 1.85218 225.438 32.8658
265 0.5 1.8957 229.032 33.8136
266 0.67 1.95996 232.873 35.1268
267 1.1 2.03352 237.009 37.3636
268 1.5 2.09693 241.406 40.509
269 1.7 2.19728 246.234 44.2444
270 2.4 2.32634 251.646 49.8276
271 2.7 2.45727 257.684 56.4623
272 3.2 2.74777 265.234 65.2551

Data Set Standard Deviation = 0.342443
Numerator = 4258.23
Denominator = 8428.99
W Statistic = 0.505189 = 4258.23 / 8428.99

5% Critical value of 0.976 exceeds 0.505189
Evidence of non-normality at 95% level of significance

1% Critical value of 0.967 exceeds 0.505189
Evidence of non-normality at 99% level of significance

Probability Plot
Parameter: 1,2-cis-Dichloroethylene
Original Data (Not Transformed)
Non-Detects Replaced with 1/2 DL

Probability Plot
Correlation Coefficient = 0.714199
0.714199 < 0.987 -- Normality test fails at 95% level

Plotted Data Points

Datum Value Prob. Quantile. x y
1 0 0.003663 -2.74777 39 348.683
2 0 0.00732601 -2.45727 39 334.497
3 0 0.010989 -2.32634 39 328.103
4 0 0.014652 -2.19728 39 321.801
5 0.075 0.018315 -2.09693 49.0313 316.9
6 0.075 0.021978 -2.03352 49.0313 313.804
7 0.075 0.025641 -1.95996 49.0313 310.211
8 0.075 0.029304 -1.8957 49.0313 307.073
9 0.075 0.032967 -1.85218 49.0313 304.948
10 0.075 0.03663 -1.79912 49.0313 302.357
11 0.075 0.040293 -1.75069 49.0313 299.992
12 0.075 0.043956 -1.71688 49.0313 298.341
13 0.075 0.047619 -1.67466 49.0313 296.279
14 0.075 0.0512821 -1.63524 49.0313 294.354
15 0.075 0.0549451 -1.60725 49.0313 292.987
16 0.075 0.0586081 -1.57179 49.0313 291.256
17 0.075 0.0622711 -1.5382 49.0313 289.615
18 0.075 0.0659341 -1.5141 49.0313 288.439
19 0.075 0.0695971 -1.48328 49.0313 286.934
20 0.075 0.0732601 -1.4538 49.0313 285.494
21 0.075 0.0769231 -1.4325 49.0313 284.454
22 0.075 0.0805861 -1.40507 49.0313 283.114
23 0.075 0.0842491 -1.37866 49.0313 281.824
24 0.075 0.0879121 -1.35946 49.0313 280.887
25 0.075 0.0915751 -1.33462 49.0313 279.674
26 0.075 0.0952381 -1.31058 49.0313 278.5
27 0.075 0.0989011 -1.29303 49.0313 277.643
28 0.075 0.102564 -1.27024 49.0313 276.53
29 0.075 0.106227 -1.24809 49.0313 275.448
30 0.075 0.10989 -1.23187 49.0313 274.656
31 0.075 0.113553 -1.21073 49.0313 273.624
32 0.075 0.117216 -1.19012 49.0313 272.617
33 0.075 0.120879 -1.17499 49.0313 271.879
34 0.075 0.124542 -1.15522 49.0313 270.913
35 0.075 0.128205 -1.1359 49.0313 269.97
36 0.075 0.131868 -1.12168 49.0313 269.275
37 0.075 0.135531 -1.10306 49.0313 268.366
38 0.075 0.139194 -1.08482 49.0313 267.476
39 0.075 0.142857 -1.07138 49.0313 266.819
40 0.075 0.14652 -1.05375 49.0313 265.958
41 0.075 0.150183 -1.03643 49.0313 265.112
42 0.075 0.153846 -1.02365 49.0313 264.488
43 0.075 0.157509 -1.00687 49.0313 263.669
44 0.075 0.161172 -0.990356 49.0313 262.862
45 0.075 0.164835 -0.97815 49.0313 262.266
46 0.075 0.168498 -0.9621 49.0313 261.483
47 0.075 0.172161 -0.946291 49.0313 260.711
48 0.075 0.175824 -0.93459 49.0313 260.139
49 0.075 0.179487 -0.919183 49.0313 259.387
50 0.075 0.18315 -0.903992 49.0313 258.645
51 0.075 0.186813 -0.892733 49.0313 258.095
52 0.075 0.190476 -0.877897 49.0313 257.371
53 0.075 0.194139 -0.863249 49.0313 256.655
54 0.075 0.197802 -0.852385 49.0313 256.125
55 0.075 0.201465 -0.838054 49.0313 255.425
56 0.075 0.205128 -0.823893 49.0313 254.733
57 0.075 0.208791 -0.813379 49.0313 254.22
58 0.075 0.212454 -0.7995 49.0313 253.542
59 0.075 0.216117 -0.785774 49.0313 252.872
60 0.075 0.21978 -0.775574 49.0313 252.374
61 0.075 0.223443 -0.7621 49.0313 251.716
62 0.075 0.227106 -0.748762 49.0313 251.065
63 0.075 0.230769 -0.738846 49.0313 250.58
64 0.075 0.234432 -0.725736 49.0313 249.94
65 0.075 0.238095 -0.712751 49.0313 249.306
66 0.075 0.241758 -0.703089 49.0313 248.834
67 0.075 0.245421 -0.690309 49.0313 248.21
68 0.075 0.249084 -0.677639 49.0313 247.591
69 0.075 0.252747 -0.668209 49.0313 247.131
70 0.075 0.25641 -0.655726 49.0313 246.521
71 0.075 0.260073 -0.643345 49.0313 245.917
72 0.075 0.263736 -0.634124 49.0313 245.466
73 0.075 0.267399 -0.621911 49.0313 244.87
74 0.075 0.271062 -0.609791 49.0313 244.278
75 0.075 0.274725 -0.60076 49.0313 243.837
76 0.075 0.278388 -0.588793 49.0313 243.253
77 0.075 0.282051 -0.576911 49.0313 242.672
78 0.075 0.285714 -0.568052 49.0313 242.24
79 0.075 0.289377 -0.556308 49.0313 241.666
80 0.075 0.29304 -0.544642 49.0313 241.097
81 0.075 0.296703 -0.53594 49.0313 240.672
82 0.075 0.300366 -0.524401 49.0313 240.108
83 0.075 0.304029 -0.51293 49.0313 239.548
84 0.075 0.307692 -0.504372 49.0313 239.13
85 0.075 0.311355 -0.493018 49.0313 238.576
86 0.075 0.315018 -0.481728 49.0313 238.024
87 0.075 0.318681 -0.473299 49.0313 237.613
88 0.5 0.322344 -0.462114 105.875 237.067
89 0.5 0.326007 -0.450985 105.875 236.523
90 0.5 0.32967 -0.442676 105.875 236.117
91 0.5 0.333333 -0.431644 105.875 235.579
92 0.5 0.336996 -0.423405 105.875 235.176
93 0.5 0.340659 -0.412463 105.875 234.642
94 0.5 0.344322 -0.401571 105.875 234.11
95 0.5 0.347985 -0.393433 105.875 233.713
96 0.5 0.351648 -0.382622 105.875 233.185
97 0.5 0.355311 -0.371856 105.875 232.659
98 0.5 0.358974 -0.363809 105.875 232.266
99 0.5 0.362637 -0.353118 105.875 231.744
100 0.5 0.3663 -0.342466 105.875 231.224
101 0.5 0.369963 -0.334503 105.875 230.835
102 0.5 0.373626 -0.323919 105.875 230.318
103 0.5 0.377289 -0.31337 105.875 229.803
104 0.5 0.380952 -0.305481 105.875 229.418
105 0.5 0.384615 -0.294992 105.875 228.905
106 0.5 0.388278 -0.284535 105.875 228.395
107 0.5 0.391941 -0.276714 105.875 228.013
108 0.5 0.395604 -0.266311 105.875 227.505
109 0.5 0.399267 -0.255936 105.875 226.998
110 0.5 0.40293 -0.248174 105.875 226.619
111 0.5 0.406593 -0.237847 105.875 226.115
112 0.5 0.410256 -0.227545 105.875 225.612
113 0.5 0.413919 -0.219834 105.875 225.235
114 0.5 0.417582 -0.209575 105.875 224.734
115 0.5 0.421245 -0.199336 105.875 224.234
116 0.5 0.424908 -0.191671 105.875 223.86
117 0.5 0.428571 -0.181468 105.875 223.362
118 0.5 0.432234 -0.171285 105.875 222.864
119 0.5 0.435897 -0.163659 105.875 222.492
120 0.5 0.43956 -0.153505 105.875 221.996
121 0.5 0.443223 -0.143367 105.875 221.501
122 0.5 0.446886 -0.135774 105.875 221.13
123 0.5 0.450549 -0.125661 105.875 220.636
124 0.5 0.454212 -0.115562 105.875 220.143
125 0.5 0.457875 -0.107995 105.875 219.774
126 0.5 0.461538 -0.0979139 105.875 219.281
127 0.5 0.465201 -0.0878447 105.875 218.79
128 0.5 0.468864 -0.0802981 105.875 218.421
129 0.5 0.472527 -0.0702426 105.875 217.93
130 0.5 0.47619 -0.0601949 105.875 217.44
131 0.5 0.479853 -0.0526632 105.875 217.072
132 0.5 0.483516 -0.0426257 105.875 216.582
133 0.5 0.487179 -0.0325917 105.875 216.092
134 0.5 0.490842 -0.0250691 105.875 215.724
135 0.5 0.494505 -0.0150408 105.875 215.234
136 0.5 0.498168 -0.00501359 105.875 214.745
137 0.5 0.501832 0.00501359 105.875 214.255
138 0.5 0.505495 0.0150408 105.875 213.766
139 0.5 0.509158 0.0250691 105.875 213.276
140 0.5 0.512821 0.0325917 105.875 212.908
141 0.5 0.516484 0.0426257 105.875 212.418
142 0.5 0.520147 0.0526632 105.875 211.928
143 0.5 0.52381 0.0601949 105.875 211.56
144 0.5 0.527473 0.0702426 105.875 211.07
145 0.5 0.531136 0.0802981 105.875 210.579
146 0.5 0.534799 0.0878447 105.875 210.21
147 0.5 0.538462 0.0979139 105.875 209.719
148 0.5 0.542125 0.107995 105.875 209.226
149 0.5 0.545788 0.115562 105.875 208.857
150 0.5 0.549451 0.125661 105.875 208.364
151 0.5 0.553114 0.135774 105.875 207.87
152 0.5 0.556777 0.143367 105.875 207.499
153 0.5 0.56044 0.153505 105.875 207.004
154 0.5 0.564103 0.163659 105.875 206.508
155 0.5 0.567766 0.171285 105.875 206.136
156 0.5 0.571429 0.181468 105.875 205.638
157 0.5 0.575092 0.191671 105.875 205.14
158 0.5 0.578755 0.199336 105.875 204.766
159 0.5 0.582418 0.209575 105.875 204.266
160 0.5 0.586081 0.219834 105.875 203.765
161 0.5 0.589744 0.227545 105.875 203.388
162 0.5 0.593407 0.237847 105.875 202.885
163 0.5 0.59707 0.248174 105.875 202.381
164 0.5 0.600733 0.255936 105.875 202.002
165 0.5 0.604396 0.266311 105.875 201.495
166 0.5 0.608059 0.276714 105.875 200.987
167 0.5 0.611722 0.284535 105.875 200.605
168 0.5 0.615385 0.294992 105.875 200.095
169 0.5 0.619048 0.305481 105.875 199.582
170 0.5 0.622711 0.31337 105.875 199.197
171 0.5 0.626374 0.323919 105.875 198.682
172 0.5 0.630037 0.334503 105.875 198.165
173 0.5 0.6337 0.342466 105.875 197.776
174 0.5 0.637363 0.353118 105.875 197.256
175 0.5 0.641026 0.363809 105.875 196.734
176 0.5 0.644689 0.371856 105.875 196.341
177 0.5 0.648352 0.382622 105.875 195.815
178 0.5 0.652015 0.393433 105.875 195.287
179 0.5 0.655678 0.401571 105.875 194.89
180 0.5 0.659341 0.412463 105.875 194.358
181 0.5 0.663004 0.423405 105.875 193.824
182 0.5 0.666667 0.431644 105.875 193.421
183 0.5 0.67033 0.442676 105.875 192.883
184 0.5 0.673993 0.450985 105.875 192.477
185 0.5 0.677656 0.462114 105.875 191.933
186 0.5 0.681319 0.473299 105.875 191.387
187 0.5 0.684982 0.481728 105.875 190.976
188 0.5 0.688645 0.493018 105.875 190.424
189 0.5 0.692308 0.504372 105.875 189.87
190 0.5 0.695971 0.51293 105.875 189.452
191 0.5 0.699634 0.524401 105.875 188.892
192 0.5 0.703297 0.53594 105.875 188.328
193 0.5 0.70696 0.544642 105.875 187.903
194 0.5 0.710623 0.556308 105.875 187.334
195 0.5 0.714286 0.568052 105.875 186.76
196 0.5 0.717949 0.576911 105.875 186.328
197 0.5 0.721612 0.588793 105.875 185.747
198 0.5 0.725275 0.60076 105.875 185.163
199 0.5 0.728938 0.609791 105.875 184.722
200 0.5 0.732601 0.621911 105.875 184.13
201 0.5 0.736264 0.634124 105.875 183.534
202 0.5 0.739927 0.643345 105.875 183.083
203 0.5 0.74359 0.655726 105.875 182.479
204 0.5 0.747253 0.668209 105.875 181.869
205 0.5 0.750916 0.677639 105.875 181.409
206 0.5 0.754579 0.690309 105.875 180.79
207 0.5 0.758242 0.703089 105.875 180.166
208 0.5 0.761905 0.712751 105.875 179.694
209 0.5 0.765568 0.725736 105.875 179.06
210 0.5 0.769231 0.738846 105.875 178.42
211 0.5 0.772894 0.748762 105.875 177.935
212 0.5 0.776557 0.7621 105.875 177.284
213 0.5 0.78022 0.775574 105.875 176.626
214 0.5 0.783883 0.785774 105.875 176.128
215 0.5 0.787546 0.7995 105.875 175.458
216 0.5 0.791209 0.813379 105.875 174.78
217 0.5 0.794872 0.823893 105.875 174.267
218 0.5 0.798535 0.838054 105.875 173.575
219 0.5 0.802198 0.852385 105.875 172.875
220 0.5 0.805861 0.863249 105.875 172.345
221 0.5 0.809524 0.877897 105.875 171.629
222 0.5 0.813187 0.892733 105.875 170.905
223 0.5 0.81685 0.903992 105.875 170.355
224 0.5 0.820513 0.919183 105.875 169.613
225 0.5 0.824176 0.93459 105.875 168.861
226 0.5 0.827839 0.946291 105.875 168.289
227 0.5 0.831502 0.9621 105.875 167.517
228 0.5 0.835165 0.97815 105.875 166.734
229 0.5 0.838828 0.990356 105.875 166.138
230 0.5 0.842491 1.00687 105.875 165.331
231 0.5 0.846154 1.02365 105.875 164.512
232 0.5 0.849817 1.03643 105.875 163.888
233 0.5 0.85348 1.05375 105.875 163.042
234 0.5 0.857143 1.07138 105.875 162.181
235 0.5 0.860806 1.08482 105.875 161.524
236 0.5 0.864469 1.10306 105.875 160.634
237 0.5 0.868132 1.12168 105.875 159.725
238 0.5 0.871795 1.1359 105.875 159.03
239 0.5 0.875458 1.15522 105.875 158.087
240 0.5 0.879121 1.17499 105.875 157.121
241 0.5 0.882784 1.19012 105.875 156.383
242 0.5 0.886447 1.21073 105.875 155.376
243 0.5 0.89011 1.23187 105.875 154.344
244 0.5 0.893773 1.24809 105.875 153.552
245 0.5 0.897436 1.27024 105.875 152.47
246 0.5 0.901099 1.29303 105.875 151.357
247 0.5 0.904762 1.31058 105.875 150.5
248 0.5 0.908425 1.33462 105.875 149.326
249 0.5 0.912088 1.35946 105.875 148.113
250 0.5 0.915751 1.37866 105.875 147.176
251 0.5 0.919414 1.40507 105.875 145.886
252 0.5 0.923077 1.4325 105.875 144.546
253 0.5 0.92674 1.4538 105.875 143.506
254 0.5 0.930403 1.48328 105.875 142.066
255 0.5 0.934066 1.5141 105.875 140.561
256 0.5 0.937729 1.5382 105.875 139.385
257 0.5 0.941392 1.57179 105.875 137.744
258 0.5 0.945055 1.60725 105.875 136.013
259 0.5 0.948718 1.63524 105.875 134.646
260 0.5 0.952381 1.67466 105.875 132.721
261 0.5 0.956044 1.71688 105.875 130.659
262 0.5 0.959707 1.75069 105.875 129.008
263 0.5 0.96337 1.79912 105.875 126.643
264 0.5 0.967033 1.85218 105.875 124.052
265 0.5 0.970696 1.8957 105.875 121.927
266 0.67 0.974359 1.95996 128.613 118.789
267 1.1 0.978022 2.03352 186.125 115.196
268 1.5 0.981685 2.09693 239.625 112.1
269 1.7 0.985348 2.19728 266.375 107.199
270 2.4 0.989011 2.32634 360 100.897
271 2.7 0.992674 2.45727 400.125 94.5032
272 3.2 0.996337 2.74777 467 80.3175

Shapiro-Francia Test of Normality
Parameter: 1,2-cis-Dichloroethylene
All Locations
Normality Test of Parameter Concentrations
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL
Total Number of Measurements = 272

i x(i) m(i) sum(m^2) sum(mx)
1 -2.59027 -2.74777 7.55021 7.11745
2 -2.59027 -2.45727 13.5884 13.4824
3 -2.59027 -2.32634 19.0003 19.5083
4 -2.59027 -2.19728 23.8283 25.1998
5 -2.59027 -2.09693 28.2255 30.6315
6 -2.59027 -2.03352 32.3607 35.8988
7 -2.59027 -1.95996 36.2021 40.9756
8 -2.59027 -1.8957 39.7958 45.886
9 -2.59027 -1.85218 43.2263 50.6836
10 -2.59027 -1.79912 46.4632 55.3438
11 -2.59027 -1.75069 49.5281 59.8786
12 -2.59027 -1.71688 52.4757 64.3258
13 -2.59027 -1.67466 55.2802 68.6636
14 -2.59027 -1.63524 57.9542 72.8993
15 -2.59027 -1.60725 60.5375 77.0625
16 -2.59027 -1.57179 63.008 81.1338
17 -2.59027 -1.5382 65.3741 85.1182
18 -2.59027 -1.5141 67.6666 89.0401
19 -2.59027 -1.48328 69.8667 92.8822
20 -2.59027 -1.4538 71.9802 96.648
21 -2.59027 -1.4325 74.0323 100.359
22 -2.59027 -1.40507 76.0066 103.998
23 -2.59027 -1.37866 77.9072 107.569
24 -2.59027 -1.35946 79.7554 111.091
25 -2.59027 -1.33462 81.5366 114.548
26 -2.59027 -1.31058 83.2542 117.942
27 -2.59027 -1.29303 84.9262 121.292
28 -2.59027 -1.27024 86.5397 124.582
29 -2.59027 -1.24809 88.0974 127.815
30 -2.59027 -1.23187 89.6149 131.006
31 -2.59027 -1.21073 91.0807 134.142
32 -2.59027 -1.19012 92.4971 137.224
33 -2.59027 -1.17499 93.8777 140.268
34 -2.59027 -1.15522 95.2123 143.26
35 -2.59027 -1.1359 96.5025 146.203
36 -2.59027 -1.12168 97.7607 149.108
37 -2.59027 -1.10306 98.9774 151.965
38 -2.59027 -1.08482 100.154 154.775
39 -2.59027 -1.07138 101.302 157.55
40 -2.59027 -1.05375 102.412 160.28
41 -2.59027 -1.03643 103.487 162.964
42 -2.59027 -1.02365 104.535 165.616
43 -2.59027 -1.00687 105.548 168.224
44 -2.59027 -0.990356 106.529 170.789
45 -2.59027 -0.97815 107.486 173.323
46 -2.59027 -0.9621 108.412 175.815
47 -2.59027 -0.946291 109.307 178.266
48 -2.59027 -0.93459 110.18 180.687
49 -2.59027 -0.919183 111.025 183.068
50 -2.59027 -0.903992 111.843 185.41
51 -2.59027 -0.892733 112.64 187.722
52 -2.59027 -0.877897 113.41 189.996
53 -2.59027 -0.863249 114.155 192.232
54 -2.59027 -0.852385 114.882 194.44
55 -2.59027 -0.838054 115.584 196.611
56 -2.59027 -0.823893 116.263 198.745
57 -2.59027 -0.813379 116.925 200.852
58 -2.59027 -0.7995 117.564 202.923
59 -2.59027 -0.785774 118.181 204.958
60 -2.59027 -0.775574 118.783 206.967
61 -2.59027 -0.7621 119.364 208.941
62 -2.59027 -0.748762 119.924 210.88
63 -2.59027 -0.738846 120.47 212.794
64 -2.59027 -0.725736 120.997 214.674
65 -2.59027 -0.712751 121.505 216.52
66 -2.59027 -0.703089 121.999 218.342
67 -2.59027 -0.690309 122.476 220.13
68 -2.59027 -0.677639 122.935 221.885
69 -2.59027 -0.668209 123.381 223.616
70 -2.59027 -0.655726 123.811 225.314
71 -2.59027 -0.643345 124.225 226.981
72 -2.59027 -0.634124 124.627 228.623
73 -2.59027 -0.621911 125.014 230.234
74 -2.59027 -0.609791 125.386 231.814
75 -2.59027 -0.60076 125.747 233.37
76 -2.59027 -0.588793 126.094 234.895
77 -2.59027 -0.576911 126.426 236.389
78 -2.59027 -0.568052 126.749 237.861
79 -2.59027 -0.556308 127.059 239.302
80 -2.59027 -0.544642 127.355 240.712
81 -2.59027 -0.53594 127.643 242.101
82 -2.59027 -0.524401 127.918 243.459
83 -2.59027 -0.51293 128.181 244.788
84 -0.693147 -0.504372 128.435 245.137
85 -0.693147 -0.493018 128.678 245.479
86 -0.693147 -0.481728 128.91 245.813
87 -0.693147 -0.473299 129.134 246.141
88 -0.693147 -0.462114 129.348 246.461
89 -0.693147 -0.450985 129.551 246.774
90 -0.693147 -0.442676 129.747 247.081
91 -0.693147 -0.431644 129.933 247.38
92 -0.693147 -0.423405 130.113 247.673
93 -0.693147 -0.412463 130.283 247.959
94 -0.693147 -0.401571 130.444 248.238
95 -0.693147 -0.393433 130.599 248.51
96 -0.693147 -0.382622 130.745 248.776
97 -0.693147 -0.371856 130.883 249.033
98 -0.693147 -0.363809 131.016 249.285
99 -0.693147 -0.353118 131.141 249.53
100 -0.693147 -0.342466 131.258 249.768
101 -0.693147 -0.334503 131.37 249.999
102 -0.693147 -0.323919 131.475 250.224
103 -0.693147 -0.31337 131.573 250.441
104 -0.693147 -0.305481 131.666 250.653
105 -0.693147 -0.294992 131.753 250.857
106 -0.693147 -0.284535 131.834 251.055
107 -0.693147 -0.276714 131.911 251.246
108 -0.693147 -0.266311 131.982 251.431
109 -0.693147 -0.255936 132.047 251.608
110 -0.693147 -0.248174 132.109 251.78
111 -0.693147 -0.237847 132.165 251.945
112 -0.693147 -0.227545 132.217 252.103
113 -0.693147 -0.219834 132.265 252.255
114 -0.693147 -0.209575 132.309 252.401
115 -0.693147 -0.199336 132.349 252.539
116 -0.693147 -0.191671 132.386 252.672
117 -0.693147 -0.181468 132.419 252.797
118 -0.693147 -0.171285 132.448 252.916
119 -0.693147 -0.163659 132.475 253.03
120 -0.693147 -0.153505 132.498 253.136
121 -0.693147 -0.143367 132.519 253.235
122 -0.693147 -0.135774 132.537 253.33
123 -0.693147 -0.125661 132.553 253.417
124 -0.693147 -0.115562 132.567 253.497
125 -0.693147 -0.107995 132.578 253.572
126 -0.693147 -0.0979139 132.588 253.639
127 -0.693147 -0.0878447 132.596 253.7
128 -0.693147 -0.0802981 132.602 253.756
129 -0.693147 -0.0702426 132.607 253.805
130 -0.693147 -0.0601949 132.611 253.846
131 -0.693147 -0.0526632 132.613 253.883
132 -0.693147 -0.0426257 132.615 253.912
133 -0.693147 -0.0325917 132.616 253.935
134 -0.693147 -0.0250691 132.617 253.952
135 -0.693147 -0.0150408 132.617 253.963
136 -0.693147 -0.00501359 132.617 253.966
137 -0.693147 0.00501359 132.617 253.963
138 -0.693147 0.0150408 132.617 253.952
139 -0.693147 0.0250691 132.618 253.935
140 -0.693147 0.0325917 132.619 253.912
141 -0.693147 0.0426257 132.621 253.883
142 -0.693147 0.0526632 132.624 253.846
143 -0.693147 0.0601949 132.627 253.805
144 -0.693147 0.0702426 132.632 253.756
145 -0.693147 0.0802981 132.639 253.7
146 -0.693147 0.0878447 132.646 253.639
147 -0.693147 0.0979139 132.656 253.572
148 -0.693147 0.107995 132.668 253.497
149 -0.693147 0.115562 132.681 253.417
150 -0.693147 0.125661 132.697 253.33
151 -0.693147 0.135774 132.715 253.235
152 -0.693147 0.143367 132.736 253.136
153 -0.693147 0.153505 132.759 253.03
154 -0.693147 0.163659 132.786 252.916
155 -0.693147 0.171285 132.815 252.797
156 -0.693147 0.181468 132.848 252.672
157 -0.693147 0.191671 132.885 252.539
158 -0.693147 0.199336 132.925 252.401
159 -0.693147 0.209575 132.969 252.255
160 -0.693147 0.219834 133.017 252.103
161 -0.693147 0.227545 133.069 251.945
162 -0.693147 0.237847 133.125 251.78
163 -0.693147 0.248174 133.187 251.608
164 -0.693147 0.255936 133.252 251.431
165 -0.693147 0.266311 133.323 251.246
166 -0.693147 0.276714 133.4 251.055
167 -0.693147 0.284535 133.481 250.857
168 -0.693147 0.294992 133.568 250.653
169 -0.693147 0.305481 133.661 250.441
170 -0.693147 0.31337 133.759 250.224
171 -0.693147 0.323919 133.864 249.999
172 -0.693147 0.334503 133.976 249.768
173 -0.693147 0.342466 134.094 249.53
174 -0.693147 0.353118 134.218 249.285
175 -0.693147 0.363809 134.351 249.033
176 -0.693147 0.371856 134.489 248.776
177 -0.693147 0.382622 134.635 248.51
178 -0.693147 0.393433 134.79 248.238
179 -0.693147 0.401571 134.951 247.959
180 -0.693147 0.412463 135.121 247.673
181 -0.693147 0.423405 135.301 247.38
182 -0.693147 0.431644 135.487 247.081
183 -0.693147 0.442676 135.683 246.774
184 -0.693147 0.450985 135.886 246.461
185 -0.693147 0.462114 136.1 246.141
186 -0.693147 0.473299 136.324 245.813
187 -0.693147 0.481728 136.556 245.479
188 -0.693147 0.493018 136.799 245.137
189 -0.693147 0.504372 137.053 244.788
190 -0.693147 0.51293 137.317 244.432
191 -0.693147 0.524401 137.592 244.069
192 -0.693147 0.53594 137.879 243.697
193 -0.693147 0.544642 138.175 243.32
194 -0.693147 0.556308 138.485 242.934
195 -0.693147 0.568052 138.808 242.54
196 -0.693147 0.576911 139.14 242.14
197 -0.693147 0.588793 139.487 241.732
198 -0.693147 0.60076 139.848 241.316
199 -0.693147 0.609791 140.22 240.893
200 -0.693147 0.621911 140.607 240.462
201 -0.693147 0.634124 141.009 240.023
202 -0.693147 0.643345 141.423 239.577
203 -0.693147 0.655726 141.853 239.122
204 -0.693147 0.668209 142.299 238.659
205 -0.693147 0.677639 142.758 238.189
206 -0.693147 0.690309 143.235 237.711
207 -0.693147 0.703089 143.729 237.223
208 -0.693147 0.712751 144.237 236.729
209 -0.693147 0.725736 144.764 236.226
210 -0.693147 0.738846 145.31 235.714
211 -0.693147 0.748762 145.87 235.195
212 -0.693147 0.7621 146.451 234.667
213 -0.693147 0.775574 147.053 234.129
214 -0.693147 0.785774 147.67 233.585
215 -0.693147 0.7995 148.309 233.031
216 -0.693147 0.813379 148.971 232.467
217 -0.693147 0.823893 149.65 231.896
218 -0.693147 0.838054 150.352 231.315
219 -0.693147 0.852385 151.079 230.724
220 -0.693147 0.863249 151.824 230.126
221 -0.693147 0.877897 152.595 229.517
222 -0.693147 0.892733 153.392 228.898
223 -0.693147 0.903992 154.209 228.272
224 -0.693147 0.919183 155.054 227.635
225 -0.693147 0.93459 155.927 226.987
226 -0.693147 0.946291 156.823 226.331
227 -0.693147 0.9621 157.748 225.664
228 -0.693147 0.97815 158.705 224.986
229 -0.693147 0.990356 159.686 224.299
230 -0.693147 1.00687 160.7 223.602
231 -0.693147 1.02365 161.747 222.892
232 -0.693147 1.03643 162.822 222.174
233 -0.693147 1.05375 163.932 221.443
234 -0.693147 1.07138 165.08 220.701
235 -0.693147 1.08482 166.257 219.949
236 -0.693147 1.10306 167.473 219.184
237 -0.693147 1.12168 168.732 218.407
238 -0.693147 1.1359 170.022 217.619
239 -0.693147 1.15522 171.356 216.819
240 -0.693147 1.17499 172.737 216.004
241 -0.693147 1.19012 174.153 215.179
242 -0.693147 1.21073 175.619 214.34
243 -0.693147 1.23187 177.137 213.486
244 -0.693147 1.24809 178.694 212.621
245 -0.693147 1.27024 180.308 211.74
246 -0.693147 1.29303 181.98 210.844
247 -0.693147 1.31058 183.697 209.936
248 -0.693147 1.33462 185.479 209.011
249 -0.693147 1.35946 187.327 208.068
250 -0.693147 1.37866 189.228 207.113
251 -0.693147 1.40507 191.202 206.139
252 -0.693147 1.4325 193.254 205.146
253 -0.693147 1.4538 195.367 204.138
254 -0.693147 1.48328 197.568 203.11
255 -0.693147 1.5141 199.86 202.061
256 -0.693147 1.5382 202.226 200.994
257 -0.693147 1.57179 204.697 199.905
258 -0.693147 1.60725 207.28 198.791
259 -0.693147 1.63524 209.954 197.657
260 -0.693147 1.67466 212.758 196.497
261 -0.693147 1.71688 215.706 195.307
262 -0.400478 1.75069 218.771 194.605
263 0 1.79912 222.008 194.605
264 0 1.85218 225.438 194.605
265 0 1.8957 229.032 194.605
266 0 1.95996 232.873 194.605
267 0.0953102 2.03352 237.009 194.799
268 0.405465 2.09693 241.406 195.649
269 0.530628 2.19728 246.234 196.815
270 0.875469 2.32634 251.646 198.852
271 0.993252 2.45727 257.684 201.293
272 1.16315 2.74777 265.234 204.489

Data Set Standard Deviation = 0.929731
Numerator = 41815.7
Denominator = 62131.7
W Statistic = 0.673017 = 41815.7 / 62131.7

5% Critical value of 0.976 exceeds 0.673017
Evidence of non-normality at 95% level of significance

1% Critical value of 0.967 exceeds 0.673017
Evidence of non-normality at 99% level of significance

Probability Plot
Parameter: 1,2-cis-Dichloroethylene
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Probability Plot
Correlation Coefficient = 0.819855
0.819855 < 0.987 -- Normality test fails at 95% level

Plotted Data Points

Datum Value Prob. Quantile. x y
1 -2.59027 0.003663 -2.74777 82.8414 348.683
2 -2.59027 0.00732601 -2.45727 82.8414 334.497
3 -2.59027 0.010989 -2.32634 82.8414 328.103
4 -2.59027 0.014652 -2.19728 82.8414 321.801
5 -2.59027 0.018315 -2.09693 82.8414 316.9
6 -2.59027 0.021978 -2.03352 82.8414 313.804
7 -2.59027 0.025641 -1.95996 82.8414 310.211
8 -2.59027 0.029304 -1.8957 82.8414 307.073
9 -2.59027 0.032967 -1.85218 82.8414 304.948
10 -2.59027 0.03663 -1.79912 82.8414 302.357
11 -2.59027 0.040293 -1.75069 82.8414 299.992
12 -2.59027 0.043956 -1.71688 82.8414 298.341
13 -2.59027 0.047619 -1.67466 82.8414 296.279
14 -2.59027 0.0512821 -1.63524 82.8414 294.354
15 -2.59027 0.0549451 -1.60725 82.8414 292.987
16 -2.59027 0.0586081 -1.57179 82.8414 291.256
17 -2.59027 0.0622711 -1.5382 82.8414 289.615
18 -2.59027 0.0659341 -1.5141 82.8414 288.439
19 -2.59027 0.0695971 -1.48328 82.8414 286.934
20 -2.59027 0.0732601 -1.4538 82.8414 285.494
21 -2.59027 0.0769231 -1.4325 82.8414 284.454
22 -2.59027 0.0805861 -1.40507 82.8414 283.114
23 -2.59027 0.0842491 -1.37866 82.8414 281.824
24 -2.59027 0.0879121 -1.35946 82.8414 280.887
25 -2.59027 0.0915751 -1.33462 82.8414 279.674
26 -2.59027 0.0952381 -1.31058 82.8414 278.5
27 -2.59027 0.0989011 -1.29303 82.8414 277.643
28 -2.59027 0.102564 -1.27024 82.8414 276.53
29 -2.59027 0.106227 -1.24809 82.8414 275.448
30 -2.59027 0.10989 -1.23187 82.8414 274.656
31 -2.59027 0.113553 -1.21073 82.8414 273.624
32 -2.59027 0.117216 -1.19012 82.8414 272.617
33 -2.59027 0.120879 -1.17499 82.8414 271.879
34 -2.59027 0.124542 -1.15522 82.8414 270.913
35 -2.59027 0.128205 -1.1359 82.8414 269.97
36 -2.59027 0.131868 -1.12168 82.8414 269.275
37 -2.59027 0.135531 -1.10306 82.8414 268.366
38 -2.59027 0.139194 -1.08482 82.8414 267.476
39 -2.59027 0.142857 -1.07138 82.8414 266.819
40 -2.59027 0.14652 -1.05375 82.8414 265.958
41 -2.59027 0.150183 -1.03643 82.8414 265.112
42 -2.59027 0.153846 -1.02365 82.8414 264.488
43 -2.59027 0.157509 -1.00687 82.8414 263.669
44 -2.59027 0.161172 -0.990356 82.8414 262.862
45 -2.59027 0.164835 -0.97815 82.8414 262.266
46 -2.59027 0.168498 -0.9621 82.8414 261.483
47 -2.59027 0.172161 -0.946291 82.8414 260.711
48 -2.59027 0.175824 -0.93459 82.8414 260.139
49 -2.59027 0.179487 -0.919183 82.8414 259.387
50 -2.59027 0.18315 -0.903992 82.8414 258.645
51 -2.59027 0.186813 -0.892733 82.8414 258.095
52 -2.59027 0.190476 -0.877897 82.8414 257.371
53 -2.59027 0.194139 -0.863249 82.8414 256.655
54 -2.59027 0.197802 -0.852385 82.8414 256.125
55 -2.59027 0.201465 -0.838054 82.8414 255.425
56 -2.59027 0.205128 -0.823893 82.8414 254.733
57 -2.59027 0.208791 -0.813379 82.8414 254.22
58 -2.59027 0.212454 -0.7995 82.8414 253.542
59 -2.59027 0.216117 -0.785774 82.8414 252.872
60 -2.59027 0.21978 -0.775574 82.8414 252.374
61 -2.59027 0.223443 -0.7621 82.8414 251.716
62 -2.59027 0.227106 -0.748762 82.8414 251.065
63 -2.59027 0.230769 -0.738846 82.8414 250.58
64 -2.59027 0.234432 -0.725736 82.8414 249.94
65 -2.59027 0.238095 -0.712751 82.8414 249.306
66 -2.59027 0.241758 -0.703089 82.8414 248.834
67 -2.59027 0.245421 -0.690309 82.8414 248.21
68 -2.59027 0.249084 -0.677639 82.8414 247.591
69 -2.59027 0.252747 -0.668209 82.8414 247.131
70 -2.59027 0.25641 -0.655726 82.8414 246.521
71 -2.59027 0.260073 -0.643345 82.8414 245.917
72 -2.59027 0.263736 -0.634124 82.8414 245.466
73 -2.59027 0.267399 -0.621911 82.8414 244.87
74 -2.59027 0.271062 -0.609791 82.8414 244.278
75 -2.59027 0.274725 -0.60076 82.8414 243.837
76 -2.59027 0.278388 -0.588793 82.8414 243.253
77 -2.59027 0.282051 -0.576911 82.8414 242.672
78 -2.59027 0.285714 -0.568052 82.8414 242.24
79 -2.59027 0.289377 -0.556308 82.8414 241.666
80 -2.59027 0.29304 -0.544642 82.8414 241.097
81 -2.59027 0.296703 -0.53594 82.8414 240.672
82 -2.59027 0.300366 -0.524401 82.8414 240.108
83 -2.59027 0.304029 -0.51293 82.8414 239.548
84 -0.693147 0.307692 -0.504372 285.833 239.13
85 -0.693147 0.311355 -0.493018 285.833 238.576
86 -0.693147 0.315018 -0.481728 285.833 238.024
87 -0.693147 0.318681 -0.473299 285.833 237.613
88 -0.693147 0.322344 -0.462114 285.833 237.067
89 -0.693147 0.326007 -0.450985 285.833 236.523
90 -0.693147 0.32967 -0.442676 285.833 236.117
91 -0.693147 0.333333 -0.431644 285.833 235.579
92 -0.693147 0.336996 -0.423405 285.833 235.176
93 -0.693147 0.340659 -0.412463 285.833 234.642
94 -0.693147 0.344322 -0.401571 285.833 234.11
95 -0.693147 0.347985 -0.393433 285.833 233.713
96 -0.693147 0.351648 -0.382622 285.833 233.185
97 -0.693147 0.355311 -0.371856 285.833 232.659
98 -0.693147 0.358974 -0.363809 285.833 232.266
99 -0.693147 0.362637 -0.353118 285.833 231.744
100 -0.693147 0.3663 -0.342466 285.833 231.224
101 -0.693147 0.369963 -0.334503 285.833 230.835
102 -0.693147 0.373626 -0.323919 285.833 230.318
103 -0.693147 0.377289 -0.31337 285.833 229.803
104 -0.693147 0.380952 -0.305481 285.833 229.418
105 -0.693147 0.384615 -0.294992 285.833 228.905
106 -0.693147 0.388278 -0.284535 285.833 228.395
107 -0.693147 0.391941 -0.276714 285.833 228.013
108 -0.693147 0.395604 -0.266311 285.833 227.505
109 -0.693147 0.399267 -0.255936 285.833 226.998
110 -0.693147 0.40293 -0.248174 285.833 226.619
111 -0.693147 0.406593 -0.237847 285.833 226.115
112 -0.693147 0.410256 -0.227545 285.833 225.612
113 -0.693147 0.413919 -0.219834 285.833 225.235
114 -0.693147 0.417582 -0.209575 285.833 224.734
115 -0.693147 0.421245 -0.199336 285.833 224.234
116 -0.693147 0.424908 -0.191671 285.833 223.86
117 -0.693147 0.428571 -0.181468 285.833 223.362
118 -0.693147 0.432234 -0.171285 285.833 222.864
119 -0.693147 0.435897 -0.163659 285.833 222.492
120 -0.693147 0.43956 -0.153505 285.833 221.996
121 -0.693147 0.443223 -0.143367 285.833 221.501
122 -0.693147 0.446886 -0.135774 285.833 221.13
123 -0.693147 0.450549 -0.125661 285.833 220.636
124 -0.693147 0.454212 -0.115562 285.833 220.143
125 -0.693147 0.457875 -0.107995 285.833 219.774
126 -0.693147 0.461538 -0.0979139 285.833 219.281
127 -0.693147 0.465201 -0.0878447 285.833 218.79
128 -0.693147 0.468864 -0.0802981 285.833 218.421
129 -0.693147 0.472527 -0.0702426 285.833 217.93
130 -0.693147 0.47619 -0.0601949 285.833 217.44
131 -0.693147 0.479853 -0.0526632 285.833 217.072
132 -0.693147 0.483516 -0.0426257 285.833 216.582
133 -0.693147 0.487179 -0.0325917 285.833 216.092
134 -0.693147 0.490842 -0.0250691 285.833 215.724
135 -0.693147 0.494505 -0.0150408 285.833 215.234
136 -0.693147 0.498168 -0.00501359 285.833 214.745
137 -0.693147 0.501832 0.00501359 285.833 214.255
138 -0.693147 0.505495 0.0150408 285.833 213.766
139 -0.693147 0.509158 0.0250691 285.833 213.276
140 -0.693147 0.512821 0.0325917 285.833 212.908
141 -0.693147 0.516484 0.0426257 285.833 212.418
142 -0.693147 0.520147 0.0526632 285.833 211.928
143 -0.693147 0.52381 0.0601949 285.833 211.56
144 -0.693147 0.527473 0.0702426 285.833 211.07
145 -0.693147 0.531136 0.0802981 285.833 210.579
146 -0.693147 0.534799 0.0878447 285.833 210.21
147 -0.693147 0.538462 0.0979139 285.833 209.719
148 -0.693147 0.542125 0.107995 285.833 209.226
149 -0.693147 0.545788 0.115562 285.833 208.857
150 -0.693147 0.549451 0.125661 285.833 208.364
151 -0.693147 0.553114 0.135774 285.833 207.87
152 -0.693147 0.556777 0.143367 285.833 207.499
153 -0.693147 0.56044 0.153505 285.833 207.004
154 -0.693147 0.564103 0.163659 285.833 206.508
155 -0.693147 0.567766 0.171285 285.833 206.136
156 -0.693147 0.571429 0.181468 285.833 205.638
157 -0.693147 0.575092 0.191671 285.833 205.14
158 -0.693147 0.578755 0.199336 285.833 204.766
159 -0.693147 0.582418 0.209575 285.833 204.266
160 -0.693147 0.586081 0.219834 285.833 203.765
161 -0.693147 0.589744 0.227545 285.833 203.388
162 -0.693147 0.593407 0.237847 285.833 202.885
163 -0.693147 0.59707 0.248174 285.833 202.381
164 -0.693147 0.600733 0.255936 285.833 202.002
165 -0.693147 0.604396 0.266311 285.833 201.495
166 -0.693147 0.608059 0.276714 285.833 200.987
167 -0.693147 0.611722 0.284535 285.833 200.605
168 -0.693147 0.615385 0.294992 285.833 200.095
169 -0.693147 0.619048 0.305481 285.833 199.582
170 -0.693147 0.622711 0.31337 285.833 199.197
171 -0.693147 0.626374 0.323919 285.833 198.682
172 -0.693147 0.630037 0.334503 285.833 198.165
173 -0.693147 0.6337 0.342466 285.833 197.776
174 -0.693147 0.637363 0.353118 285.833 197.256
175 -0.693147 0.641026 0.363809 285.833 196.734
176 -0.693147 0.644689 0.371856 285.833 196.341
177 -0.693147 0.648352 0.382622 285.833 195.815
178 -0.693147 0.652015 0.393433 285.833 195.287
179 -0.693147 0.655678 0.401571 285.833 194.89
180 -0.693147 0.659341 0.412463 285.833 194.358
181 -0.693147 0.663004 0.423405 285.833 193.824
182 -0.693147 0.666667 0.431644 285.833 193.421
183 -0.693147 0.67033 0.442676 285.833 192.883
184 -0.693147 0.673993 0.450985 285.833 192.477
185 -0.693147 0.677656 0.462114 285.833 191.933
186 -0.693147 0.681319 0.473299 285.833 191.387
187 -0.693147 0.684982 0.481728 285.833 190.976
188 -0.693147 0.688645 0.493018 285.833 190.424
189 -0.693147 0.692308 0.504372 285.833 189.87
190 -0.693147 0.695971 0.51293 285.833 189.452
191 -0.693147 0.699634 0.524401 285.833 188.892
192 -0.693147 0.703297 0.53594 285.833 188.328
193 -0.693147 0.70696 0.544642 285.833 187.903
194 -0.693147 0.710623 0.556308 285.833 187.334
195 -0.693147 0.714286 0.568052 285.833 186.76
196 -0.693147 0.717949 0.576911 285.833 186.328
197 -0.693147 0.721612 0.588793 285.833 185.747
198 -0.693147 0.725275 0.60076 285.833 185.163
199 -0.693147 0.728938 0.609791 285.833 184.722
200 -0.693147 0.732601 0.621911 285.833 184.13
201 -0.693147 0.736264 0.634124 285.833 183.534
202 -0.693147 0.739927 0.643345 285.833 183.083
203 -0.693147 0.74359 0.655726 285.833 182.479
204 -0.693147 0.747253 0.668209 285.833 181.869
205 -0.693147 0.750916 0.677639 285.833 181.409
206 -0.693147 0.754579 0.690309 285.833 180.79
207 -0.693147 0.758242 0.703089 285.833 180.166
208 -0.693147 0.761905 0.712751 285.833 179.694
209 -0.693147 0.765568 0.725736 285.833 179.06
210 -0.693147 0.769231 0.738846 285.833 178.42
211 -0.693147 0.772894 0.748762 285.833 177.935
212 -0.693147 0.776557 0.7621 285.833 177.284
213 -0.693147 0.78022 0.775574 285.833 176.626
214 -0.693147 0.783883 0.785774 285.833 176.128
215 -0.693147 0.787546 0.7995 285.833 175.458
216 -0.693147 0.791209 0.813379 285.833 174.78
217 -0.693147 0.794872 0.823893 285.833 174.267
218 -0.693147 0.798535 0.838054 285.833 173.575
219 -0.693147 0.802198 0.852385 285.833 172.875
220 -0.693147 0.805861 0.863249 285.833 172.345
221 -0.693147 0.809524 0.877897 285.833 171.629
222 -0.693147 0.813187 0.892733 285.833 170.905
223 -0.693147 0.81685 0.903992 285.833 170.355
224 -0.693147 0.820513 0.919183 285.833 169.613
225 -0.693147 0.824176 0.93459 285.833 168.861
226 -0.693147 0.827839 0.946291 285.833 168.289
227 -0.693147 0.831502 0.9621 285.833 167.517
228 -0.693147 0.835165 0.97815 285.833 166.734
229 -0.693147 0.838828 0.990356 285.833 166.138
230 -0.693147 0.842491 1.00687 285.833 165.331
231 -0.693147 0.846154 1.02365 285.833 164.512
232 -0.693147 0.849817 1.03643 285.833 163.888
233 -0.693147 0.85348 1.05375 285.833 163.042
234 -0.693147 0.857143 1.07138 285.833 162.181
235 -0.693147 0.860806 1.08482 285.833 161.524
236 -0.693147 0.864469 1.10306 285.833 160.634
237 -0.693147 0.868132 1.12168 285.833 159.725
238 -0.693147 0.871795 1.1359 285.833 159.03
239 -0.693147 0.875458 1.15522 285.833 158.087
240 -0.693147 0.879121 1.17499 285.833 157.121
241 -0.693147 0.882784 1.19012 285.833 156.383
242 -0.693147 0.886447 1.21073 285.833 155.376
243 -0.693147 0.89011 1.23187 285.833 154.344
244 -0.693147 0.893773 1.24809 285.833 153.552
245 -0.693147 0.897436 1.27024 285.833 152.47
246 -0.693147 0.901099 1.29303 285.833 151.357
247 -0.693147 0.904762 1.31058 285.833 150.5
248 -0.693147 0.908425 1.33462 285.833 149.326
249 -0.693147 0.912088 1.35946 285.833 148.113
250 -0.693147 0.915751 1.37866 285.833 147.176
251 -0.693147 0.919414 1.40507 285.833 145.886
252 -0.693147 0.923077 1.4325 285.833 144.546
253 -0.693147 0.92674 1.4538 285.833 143.506
254 -0.693147 0.930403 1.48328 285.833 142.066
255 -0.693147 0.934066 1.5141 285.833 140.561
256 -0.693147 0.937729 1.5382 285.833 139.385
257 -0.693147 0.941392 1.57179 285.833 137.744
258 -0.693147 0.945055 1.60725 285.833 136.013
259 -0.693147 0.948718 1.63524 285.833 134.646
260 -0.693147 0.952381 1.67466 285.833 132.721
261 -0.693147 0.956044 1.71688 285.833 130.659
262 -0.400478 0.959707 1.75069 317.149 129.008
263 0 0.96337 1.79912 360 126.643
264 0 0.967033 1.85218 360 124.052
265 0 0.970696 1.8957 360 121.927
266 0 0.974359 1.95996 360 118.789
267 0.0953102 0.978022 2.03352 370.198 115.196
268 0.405465 0.981685 2.09693 403.385 112.1
269 0.530628 0.985348 2.19728 416.777 107.199
270 0.875469 0.989011 2.32634 453.675 100.897
271 0.993252 0.992674 2.45727 466.278 94.5032
272 1.16315 0.996337 2.74777 484.457 80.3175

Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: 1,2-cis-Dichloroethylene
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Total Percent Non-Detects = 97.4265%
Number of comparisons = 16
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 22
Maximum Background Value = 0
Confidence Level = 73.3%
False Positive Rate = 26.7%

Location Date Count Mean Significant
LMW-10 11/16/2012 1 -2.59027 FALSE

LMW-11 11/20/2008 1 -0.693147 FALSE

LMW-12 11/20/2008 1 -0.693147 FALSE

LMW-13 11/20/2008 1 -0.693147 FALSE

LMW-14R 11/16/2012 1 -2.59027 FALSE

LMW-15R 11/16/2012 1 -2.59027 FALSE

LMW-16 11/16/2012 1 -2.59027 FALSE

LMW-3 11/16/2012 1 -2.59027 FALSE

LMW-3S 11/16/2012 1 -2.59027 FALSE

LMW-6 11/16/2012 1 -2.59027 FALSE

LMW-7 11/16/2012 1 -2.59027 FALSE

LMW-8 11/16/2012 1 0.993252 TRUE

LMW-9 11/16/2012 1 -2.59027 FALSE

LMW-9D11/16/2012 1 -2.59027 FALSE

LMW-9S 11/16/2012 1 -2.59027 FALSE

MW-5 11/20/2008 1 -0.693147 FALSE

Mann-Kendall Trend Analysis
Parameter: 1,2-cis-Dichloroethylene
Location: LMW-8
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

95% Confidence Level

Xj Xk Xj - Xk Positives Negatives
ND<-0.693147 ND<-0.693147 0 0 0
ND<-0.693147 ND<-0.693147 0 0 0
ND<-0.693147 ND<-0.693147 0 0 0
ND<-0.693147 ND<-0.693147 0 0 0
ND<-0.693147 ND<-0.693147 0 0 0
ND<-0.693147 ND<-0.693147 0 0 0
ND<-0.693147 ND<-0.693147 0 0 0
ND<0 J ND<-0.693147 0.693147 1 0
ND<0 J ND<-0.693147 0.693147 2 0
ND<0 J ND<-0.693147 0.693147 3 0
ND<-0.693147 ND<-0.693147 0 3 0
ND<0 J ND<-0.693147 0.693147 4 0
ND<-0.693147 ND<-0.693147 0 4 0
ND<-0.693147 ND<-0.693147 0 4 0
0.875469 ND<-0.693147 1.56862 5 0
0.0953102 ND<-0.693147 0.788457 6 0
-0.400478 J ND<-0.693147 0.29267 7 0
0.405465 ND<-0.693147 1.09861 8 0
0.530628 ND<-0.693147 1.22378 9 0
1.16315 ND<-0.693147 1.8563 10 0
0.993252 ND<-0.693147 1.6864 11 0

ND<-0.693147 ND<-0.693147 0 11 0
ND<-0.693147 ND<-0.693147 0 11 0
ND<-0.693147 ND<-0.693147 0 11 0
ND<-0.693147 ND<-0.693147 0 11 0
ND<-0.693147 ND<-0.693147 0 11 0
ND<-0.693147 ND<-0.693147 0 11 0
ND<0 J ND<-0.693147 0.693147 12 0
ND<0 J ND<-0.693147 0.693147 13 0
ND<0 J ND<-0.693147 0.693147 14 0
ND<-0.693147 ND<-0.693147 0 14 0
ND<0 J ND<-0.693147 0.693147 15 0
ND<-0.693147 ND<-0.693147 0 15 0
ND<-0.693147 ND<-0.693147 0 15 0
0.875469 ND<-0.693147 1.56862 16 0
0.0953102 ND<-0.693147 0.788457 17 0
-0.400478 J ND<-0.693147 0.29267 18 0
0.405465 ND<-0.693147 1.09861 19 0
0.530628 ND<-0.693147 1.22378 20 0
1.16315 ND<-0.693147 1.8563 21 0
0.993252 ND<-0.693147 1.6864 22 0

ND<-0.693147 ND<-0.693147 0 22 0
ND<-0.693147 ND<-0.693147 0 22 0
ND<-0.693147 ND<-0.693147 0 22 0
ND<-0.693147 ND<-0.693147 0 22 0
ND<-0.693147 ND<-0.693147 0 22 0
ND<0 J ND<-0.693147 0.693147 23 0
ND<0 J ND<-0.693147 0.693147 24 0
ND<0 J ND<-0.693147 0.693147 25 0
ND<-0.693147 ND<-0.693147 0 25 0
ND<0 J ND<-0.693147 0.693147 26 0
ND<-0.693147 ND<-0.693147 0 26 0
ND<-0.693147 ND<-0.693147 0 26 0
0.875469 ND<-0.693147 1.56862 27 0
0.0953102 ND<-0.693147 0.788457 28 0
-0.400478 J ND<-0.693147 0.29267 29 0
0.405465 ND<-0.693147 1.09861 30 0
0.530628 ND<-0.693147 1.22378 31 0
1.16315 ND<-0.693147 1.8563 32 0
0.993252 ND<-0.693147 1.6864 33 0

ND<-0.693147 ND<-0.693147 0 33 0
ND<-0.693147 ND<-0.693147 0 33 0
ND<-0.693147 ND<-0.693147 0 33 0
ND<-0.693147 ND<-0.693147 0 33 0
ND<0 J ND<-0.693147 0.693147 34 0
ND<0 J ND<-0.693147 0.693147 35 0
ND<0 J ND<-0.693147 0.693147 36 0
ND<-0.693147 ND<-0.693147 0 36 0
ND<0 J ND<-0.693147 0.693147 37 0
ND<-0.693147 ND<-0.693147 0 37 0
ND<-0.693147 ND<-0.693147 0 37 0
0.875469 ND<-0.693147 1.56862 38 0
0.0953102 ND<-0.693147 0.788457 39 0
-0.400478 J ND<-0.693147 0.29267 40 0
0.405465 ND<-0.693147 1.09861 41 0
0.530628 ND<-0.693147 1.22378 42 0
1.16315 ND<-0.693147 1.8563 43 0
0.993252 ND<-0.693147 1.6864 44 0

ND<-0.693147 ND<-0.693147 0 44 0
ND<-0.693147 ND<-0.693147 0 44 0
ND<-0.693147 ND<-0.693147 0 44 0
ND<0 J ND<-0.693147 0.693147 45 0
ND<0 J ND<-0.693147 0.693147 46 0
ND<0 J ND<-0.693147 0.693147 47 0
ND<-0.693147 ND<-0.693147 0 47 0
ND<0 J ND<-0.693147 0.693147 48 0
ND<-0.693147 ND<-0.693147 0 48 0
ND<-0.693147 ND<-0.693147 0 48 0
0.875469 ND<-0.693147 1.56862 49 0
0.0953102 ND<-0.693147 0.788457 50 0
-0.400478 J ND<-0.693147 0.29267 51 0
0.405465 ND<-0.693147 1.09861 52 0
0.530628 ND<-0.693147 1.22378 53 0
1.16315 ND<-0.693147 1.8563 54 0
0.993252 ND<-0.693147 1.6864 55 0

ND<-0.693147 ND<-0.693147 0 55 0
ND<-0.693147 ND<-0.693147 0 55 0
ND<0 J ND<-0.693147 0.693147 56 0
ND<0 J ND<-0.693147 0.693147 57 0
ND<0 J ND<-0.693147 0.693147 58 0
ND<-0.693147 ND<-0.693147 0 58 0
ND<0 J ND<-0.693147 0.693147 59 0
ND<-0.693147 ND<-0.693147 0 59 0
ND<-0.693147 ND<-0.693147 0 59 0
0.875469 ND<-0.693147 1.56862 60 0
0.0953102 ND<-0.693147 0.788457 61 0
-0.400478 J ND<-0.693147 0.29267 62 0
0.405465 ND<-0.693147 1.09861 63 0
0.530628 ND<-0.693147 1.22378 64 0
1.16315 ND<-0.693147 1.8563 65 0
0.993252 ND<-0.693147 1.6864 66 0

ND<-0.693147 ND<-0.693147 0 66 0
ND<0 J ND<-0.693147 0.693147 67 0
ND<0 J ND<-0.693147 0.693147 68 0
ND<0 J ND<-0.693147 0.693147 69 0
ND<-0.693147 ND<-0.693147 0 69 0
ND<0 J ND<-0.693147 0.693147 70 0
ND<-0.693147 ND<-0.693147 0 70 0
ND<-0.693147 ND<-0.693147 0 70 0
0.875469 ND<-0.693147 1.56862 71 0
0.0953102 ND<-0.693147 0.788457 72 0
-0.400478 J ND<-0.693147 0.29267 73 0
0.405465 ND<-0.693147 1.09861 74 0
0.530628 ND<-0.693147 1.22378 75 0
1.16315 ND<-0.693147 1.8563 76 0
0.993252 ND<-0.693147 1.6864 77 0

ND<0 J ND<-0.693147 0.693147 78 0
ND<0 J ND<-0.693147 0.693147 79 0
ND<0 J ND<-0.693147 0.693147 80 0
ND<-0.693147 ND<-0.693147 0 80 0
ND<0 J ND<-0.693147 0.693147 81 0
ND<-0.693147 ND<-0.693147 0 81 0
ND<-0.693147 ND<-0.693147 0 81 0
0.875469 ND<-0.693147 1.56862 82 0
0.0953102 ND<-0.693147 0.788457 83 0
-0.400478 J ND<-0.693147 0.29267 84 0
0.405465 ND<-0.693147 1.09861 85 0
0.530628 ND<-0.693147 1.22378 86 0
1.16315 ND<-0.693147 1.8563 87 0
0.993252 ND<-0.693147 1.6864 88 0

ND<0 J ND<0 J 0 88 0
ND<0 J ND<0 J 0 88 0
ND<-0.693147 ND<0 J -0.693147 88 1
ND<0 J ND<0 J 0 88 1
ND<-0.693147 ND<0 J -0.693147 88 2
ND<-0.693147 ND<0 J -0.693147 88 3
0.875469 ND<0 J 0.875469 89 3
0.0953102 ND<0 J 0.0953102 90 3
-0.400478 J ND<0 J -0.400478 90 4
0.405465 ND<0 J 0.405465 91 4
0.530628 ND<0 J 0.530628 92 4
1.16315 ND<0 J 1.16315 93 4
0.993252 ND<0 J 0.993252 94 4

ND<0 J ND<0 J 0 94 4
ND<-0.693147 ND<0 J -0.693147 94 5
ND<0 J ND<0 J 0 94 5
ND<-0.693147 ND<0 J -0.693147 94 6
ND<-0.693147 ND<0 J -0.693147 94 7
0.875469 ND<0 J 0.875469 95 7
0.0953102 ND<0 J 0.0953102 96 7
-0.400478 J ND<0 J -0.400478 96 8
0.405465 ND<0 J 0.405465 97 8
0.530628 ND<0 J 0.530628 98 8
1.16315 ND<0 J 1.16315 99 8
0.993252 ND<0 J 0.993252 100 8

ND<-0.693147 ND<0 J -0.693147 100 9
ND<0 J ND<0 J 0 100 9
ND<-0.693147 ND<0 J -0.693147 100 10
ND<-0.693147 ND<0 J -0.693147 100 11
0.875469 ND<0 J 0.875469 101 11
0.0953102 ND<0 J 0.0953102 102 11
-0.400478 J ND<0 J -0.400478 102 12
0.405465 ND<0 J 0.405465 103 12
0.530628 ND<0 J 0.530628 104 12
1.16315 ND<0 J 1.16315 105 12
0.993252 ND<0 J 0.993252 106 12

ND<0 J ND<-0.693147 0.693147 107 12
ND<-0.693147 ND<-0.693147 0 107 12
ND<-0.693147 ND<-0.693147 0 107 12
0.875469 ND<-0.693147 1.56862 108 12
0.0953102 ND<-0.693147 0.788457 109 12
-0.400478 J ND<-0.693147 0.29267 110 12
0.405465 ND<-0.693147 1.09861 111 12
0.530628 ND<-0.693147 1.22378 112 12
1.16315 ND<-0.693147 1.8563 113 12
0.993252 ND<-0.693147 1.6864 114 12

ND<-0.693147 ND<0 J -0.693147 114 13
ND<-0.693147 ND<0 J -0.693147 114 14
0.875469 ND<0 J 0.875469 115 14
0.0953102 ND<0 J 0.0953102 116 14
-0.400478 J ND<0 J -0.400478 116 15
0.405465 ND<0 J 0.405465 117 15
0.530628 ND<0 J 0.530628 118 15
1.16315 ND<0 J 1.16315 119 15
0.993252 ND<0 J 0.993252 120 15

ND<-0.693147 ND<-0.693147 0 120 15
0.875469 ND<-0.693147 1.56862 121 15
0.0953102 ND<-0.693147 0.788457 122 15
-0.400478 J ND<-0.693147 0.29267 123 15
0.405465 ND<-0.693147 1.09861 124 15
0.530628 ND<-0.693147 1.22378 125 15
1.16315 ND<-0.693147 1.8563 126 15
0.993252 ND<-0.693147 1.6864 127 15

0.875469 ND<-0.693147 1.56862 128 15
0.0953102 ND<-0.693147 0.788457 129 15
-0.400478 J ND<-0.693147 0.29267 130 15
0.405465 ND<-0.693147 1.09861 131 15
0.530628 ND<-0.693147 1.22378 132 15
1.16315 ND<-0.693147 1.8563 133 15
0.993252 ND<-0.693147 1.6864 134 15

0.0953102 0.875469 -0.780159 134 16
-0.400478 J 0.875469 -1.27595 134 17
0.405465 0.875469 -0.470004 134 18
0.530628 0.875469 -0.34484 134 19
1.16315 0.875469 0.287682 135 19
0.993252 0.875469 0.117783 136 19

-0.400478 J 0.0953102 -0.495788 136 20
0.405465 0.0953102 0.310155 137 20
0.530628 0.0953102 0.435318 138 20
1.16315 0.0953102 1.06784 139 20
0.993252 0.0953102 0.897942 140 20

0.405465 -0.400478 J 0.805943 141 20
0.530628 -0.400478 J 0.931106 142 20
1.16315 -0.400478 J 1.56363 143 20
0.993252 -0.400478 J 1.39373 144 20

0.530628 0.405465 0.125163 145 20
1.16315 0.405465 0.757686 146 20
0.993252 0.405465 0.587787 147 20

1.16315 0.530628 0.632523 148 20
0.993252 0.530628 0.462624 149 20

0.993252 1.16315 -0.169899 149 21

S Statistic = 149 - 21 = 128

Tied Group Value Members
1 -0.693147 11
2 0 4

Time Period Observations
1/16/1998 1
3/16/1999 1
9/23/1999 1
3/14/2000 1
9/23/2003 1
3/10/2004 1
10/12/2004 1
4/1/2005 1
10/26/2005 1
6/19/2006 1
11/18/2006 1
6/2/2007 1
11/15/2007 1
5/20/2008 1
11/20/2008 1
6/11/2009 1
6/30/2010 1
11/17/2010 1
7/6/2011 1
11/22/2011 1
5/16/2012 1
11/16/2012 1
There are 0 time periods with multiple data

A = 3126
B = 0
C = 1014
D = 0
E = 122
F = 0
a = 22638
b = 83160
c = 924
Group Variance = 1084
Z-Score = 3.85735
Comparison Level at 1.0 - (0.05 / 2) = 97.5% confidence level = 1.97737 (two-tailed)
|3.85735| > 1.97737 indicating a trend

Shewhart-CUSUM Control Chart
Parameter: 1,2-cis-Dichloroethylene
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Baseline mean = -1.29678
Baseline Std Dev = 0.904416
k = 1
h = 5
SCL = 4.5

Date Value CuSum Std Mean
1/16/1998 -0.693147 0 0.667424
1/16/1998 -0.693147 0 0.667424
3/16/1999 -0.693147 0 0.667424
3/16/1999 -0.693147 0 0.667424
9/23/1999 -0.693147 0 0.667424
9/23/1999 -0.693147 0 0.667424
3/14/2000 -0.693147 0 0.667424
3/14/2000 -0.693147 0 0.667424
9/23/2003 -0.693147 0 0.667424
9/23/2003 -0.693147 0 0.667424
3/10/2004 -0.693147 0 0.667424
3/10/2004 -0.693147 0 0.667424
10/12/2004 -0.693147 0 0.667424
10/12/2004 -0.693147 0 0.667424
4/1/2005 -0.693147 0 0.667424
4/1/2005 -0.693147 0 0.667424
10/26/2005 0 0.433826 1.43383
10/26/2005 0 0.433826 1.43383
6/19/2006 0 0.867653 1.43383
6/19/2006 0 0.867653 1.43383
11/18/2006 0 1.30148 1.43383
11/18/2006 0 1.30148 1.43383
6/2/2007 -0.693147 0.968903 0.667424
6/2/2007 -0.693147 0.968903 0.667424
11/15/2007 0 1.40273 1.43383
11/15/2007 0 1.40273 1.43383
5/20/2008 -0.693147 1.07015 0.667424
5/20/2008 -0.693147 1.07015 0.667424
11/20/2008 -0.693147 0.737577 0.667424
11/20/2008 -0.693147 0.737577 0.667424
6/11/2009 0.875469 2.1394 2.40182
6/11/2009 0.875469 2.1394 2.40182
6/30/2010 0.0953102 2.67861 1.53921
6/30/2010 0.0953102 2.67861 1.53921
11/17/2010 -0.400478 2.66963 0.991024
11/17/2010 -0.400478 2.66963 0.991024
7/6/2011 0.405465 3.55177 1.88214
7/6/2011 0.405465 3.55177 1.88214
11/22/2011 0.530628 4.57231 2.02053
11/22/2011 0.530628 4.57231 2.02053
5/16/2012 1.16315 6.29221 2.71991
5/16/2012 1.16315 6.29221 2.71991
11/16/2012 0.993252 7.82426 2.53205
11/16/2012 0.993252 7.82426 2.53205
Concentrations (ppb)
Parameter: 4-Isopropyltoluene
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements: 13
Total Non-Detect: 10
Percent Non-Detects: 76.9231%
Total Background Measurements: 1
There is 1 background location

Loc. Meas. ND Date Conc. Original

LMW-4 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

There are 12 compliance locations

Loc. Meas. ND Date Conc. Original

LMW-10 1 0 (0%) 11/16/2012 0.22 J 0.22 J

LMW-14R 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

LMW-15R 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

LMW-16 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

LMW-3 1 0 (0%) 11/16/2012 0.95 J 0.95 J

LMW-3S 1 0 (0%) 11/16/2012 0.44 J 0.44 J

LMW-6 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

LMW-7 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

LMW-8 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

LMW-9 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

LMW-9D 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

LMW-9S 1 1 (100%) 11/16/2012 ND<0.13 U ND<0.13 U

There are 0 unused locations

Loc. Meas. ND Date Conc. Original

Shapiro-Wilks Test of Normality
Parameter: 4-Isopropyltoluene
All Locations
Normality Test of Parameter Concentrations
Original Data (Not Transformed)
Non-Detects Replaced with 1/2 DL
K = 6 for 13 measurements

i x(i) x(n-i+1) x(n-1+1)-x(i) a(n-i+1) b(i)
1 0.065 0.95 0.885 0.5359 0.474272
2 0.065 0.44 0.375 0.3325 0.124688
3 0.065 0.22 0.155 0.2412 0.037386
4 0.065 0.065 0 0.1707 0
5 0.065 0.065 0 0.1099 0
6 0.065 0.065 0 0.0539 0
7 0.065 0.065 0
8 0.065 0.065 0
9 0.065 0.065 0
10 0.065 0.065 0
11 0.22 0.065 -0.155
12 0.44 0.065 -0.375
13 0.95 0.065 -0.885

Sum of b values = 0.636345
Sample Standard Deviation = 0.257206
W Statistic = 0.510085

5% Critical value of 0.866 exceeds 0.510085
Evidence of non-normality at 95% level of significance

1% Critical value of 0.814 exceeds 0.510085
Evidence of non-normality at 99% level of significance

Probability Plot
Parameter: 4-Isopropyltoluene
Original Data (Not Transformed)
Non-Detects Replaced with 1/2 DL

Probability Plot
Correlation Coefficient = 0.69604
0.69604 < 0.931 -- Normality test fails at 95% level

Plotted Data Points

Datum Value Prob. Quantile. x y
1 0.065 0.0714286 -1.46838 73.775 322.059
2 0.065 0.142857 -1.07138 73.775 292.978
3 0.065 0.214286 -0.792618 73.775 272.559
4 0.065 0.285714 -0.568052 73.775 256.11
5 0.065 0.357143 -0.36649 73.775 241.345
6 0.065 0.428571 -0.181468 73.775 227.793
7 0.065 0.5 0 73.775 214.5
8 0.065 0.571429 0.181468 73.775 201.207
9 0.065 0.642857 0.36649 73.775 187.655
10 0.065 0.714286 0.568052 73.775 172.89
11 0.22 0.785714 0.792618 156.7 156.441
12 0.44 0.857143 1.07138 274.4 136.022
13 0.95 0.928571 1.46838 547.25 106.941

Shapiro-Wilks Test of Normality
Parameter: 4-Isopropyltoluene
All Locations
Normality Test of Parameter Concentrations
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL
K = 6 for 13 measurements

i x(i) x(n-i+1) x(n-1+1)-x(i) a(n-i+1) b(i)
1 -2.73337 -0.0512933 2.68207 0.5359 1.43732
2 -2.73337 -0.820981 1.91239 0.3325 0.635869
3 -2.73337 -1.51413 1.21924 0.2412 0.294081
4 -2.73337 -2.73337 0 0.1707 0
5 -2.73337 -2.73337 0 0.1099 0
6 -2.73337 -2.73337 0 0.0539 0
7 -2.73337 -2.73337 0
8 -2.73337 -2.73337 0
9 -2.73337 -2.73337 0
10 -2.73337 -2.73337 0
11 -1.51413 -2.73337 -1.21924
12 -0.820981 -2.73337 -1.91239
13 -0.0512933 -2.73337 -2.68207

Sum of b values = 2.36727
Sample Standard Deviation = 0.900804
W Statistic = 0.575513

5% Critical value of 0.866 exceeds 0.575513
Evidence of non-normality at 95% level of significance

1% Critical value of 0.814 exceeds 0.575513
Evidence of non-normality at 99% level of significance

Probability Plot
Parameter: 4-Isopropyltoluene
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Probability Plot
Correlation Coefficient = 0.752997
0.752997 < 0.931 -- Normality test fails at 95% level

Plotted Data Points

Datum Value Prob. Quantile. x y
1 -2.73337 0.0714286 -1.46838 86.5494 322.059
2 -2.73337 0.142857 -1.07138 86.5494 292.978
3 -2.73337 0.214286 -0.792618 86.5494 272.559
4 -2.73337 0.285714 -0.568052 86.5494 256.11
5 -2.73337 0.357143 -0.36649 86.5494 241.345
6 -2.73337 0.428571 -0.181468 86.5494 227.793
7 -2.73337 0.5 0 86.5494 214.5
8 -2.73337 0.571429 0.181468 86.5494 201.207
9 -2.73337 0.642857 0.36649 86.5494 187.655
10 -2.73337 0.714286 0.568052 86.5494 172.89
11 -1.51413 0.785714 0.792618 303.981 156.441
12 -0.820981 0.857143 1.07138 427.592 136.022
13 -0.0512933 0.928571 1.46838 564.853 106.941

Kruskal-Wallis Non-Parametric Test
Parameter: 4-Isopropyltoluene
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Kruskal Wallis Ranks

Background Locations

Loc. ID Date Value Rank
LMW-4 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

Background Rank Sum = 5.5
Background Rank Mean = 5.5

Compliance Locations

Loc. ID Date Value Rank
LMW-10 11/16/2012 -1.51413 J 11
Rank Sum = 11
Rank Mean = 11

LMW-14R 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

LMW-15R 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

LMW-16 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

LMW-3 11/16/2012 -0.0512933 J 13
Rank Sum = 13
Rank Mean = 13

LMW-3S 11/16/2012 -0.820981 J 12
Rank Sum = 12
Rank Mean = 12

LMW-6 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

LMW-7 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

LMW-8 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

LMW-9 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

LMW-9D 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

LMW-9S 11/16/2012 ND<-2.73337 U 5.5
Rank Sum = 5.5
Rank Mean = 5.5

Calculation Results:
Kruskal-Wallis H Statistic = 6.56044
Kruskal-Wallis H Statistic (adjusted for tied non-detects) = 12
95% Confidence comparison value is 21.0261 at 12 degrees of freedom
6.56044 < 21.0261 indicating no significant group difference at 5% significance level
12 < 21.0261 indicating no significant group difference at 5% significance level when adjusted for ties

Concentrations (ppb)
Parameter: Arsenic
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements: 284
Total Non-Detect: 207
Percent Non-Detects: 72.8873%
Total Background Measurements: 23
There is 1 background location

Loc. Meas. ND Date Conc. Original

LMW-4 23 21 (91.3043%) 1/16/1998 ND<2 ND<2 3/16/1999 ND<2 ND<2 9/23/1999 ND<2 ND<2 3/14/2000 ND<2 ND<2
9/23/2003 ND<2 ND<2 3/10/2004 ND<2 ND<2
10/12/2004 ND<2 ND<2 4/1/2005 ND<2 ND<2 10/26/2005 ND<2 ND<2
6/19/2006 ND<2 ND<2 11/18/2006 ND<2 ND<2 6/2/2007 1 J 1 J
11/15/2007 1 J 1 J 5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2
6/11/2009 ND<0.4 U ND<0.4 U 11/16/2009 ND<0.4 U ND<0.4 U 6/30/2010 ND<0.4 U ND<0.4 U
11/17/2010 ND<0.4 U ND<0.4 U 7/6/2011 ND<0.4 U ND<0.4 U
11/22/2011 ND<0.4 U ND<0.4 U 5/16/2012 ND<0.4 U ND<0.4 U 11/16/2012 ND<0.4 U ND<0.4 U

There are 16 compliance locations

Loc. Meas. ND Date Conc. Original

LMW-10 20 17 (85%) 3/14/2000 23 23
9/23/2003 ND<2 ND<2 3/10/2004 25 25 10/12/2004 ND<2 ND<2
4/1/2005 ND<2 ND<2 10/26/2005 ND<2 ND<2 6/19/2006 ND<2 ND<2
11/18/2006 ND<2 ND<2 6/2/2007 1 J 1 J 11/15/2007 ND<2 ND<2
5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2 6/11/2009 ND<0.4 U ND<0.4 U
11/16/2009 ND<0.4 U ND<0.4 U 6/30/2010 ND<0.4 U ND<0.4 U
11/17/2010 ND<0.4 U ND<0.4 U 7/6/2011 ND<0.4 U ND<0.4 U 11/22/2011 ND<0.4 U ND<0.4 U 5/16/2012 ND<0.4 U ND<0.4 U
11/16/2012 ND<0.4 U ND<0.4 U

LMW-11 11 9 (81.8182%) 3/14/2000 12 12
9/23/2003 ND<2 ND<2 3/10/2004 18 18
10/12/2004 ND<2 ND<2 4/1/2005 ND<2 ND<2 10/26/2005 ND<2 ND<2 6/19/2006 ND<2 ND<2
6/2/2007 ND<2 ND<2 11/15/2007 ND<2 ND<2
5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2

LMW-12 11 10 (90.9091%) 3/14/2000 57 57 9/23/2003 ND<2 ND<2 3/10/2004 ND<2 ND<2
10/12/2004 ND<2 ND<2 4/1/2005 ND<2 ND<2
10/26/2005 ND<2 ND<2 6/19/2006 ND<2 ND<2 6/2/2007 ND<2 ND<2
11/15/2007 ND<2 ND<2 5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2

LMW-13 11 10 (90.9091%) 3/14/2000 16 16 9/23/2003 ND<2 ND<2
3/10/2004 ND<2 ND<2 10/12/2004 ND<2 ND<2
4/1/2005 ND<2 ND<2 10/26/2005 ND<2 ND<2 6/19/2006 ND<2 ND<2
6/2/2007 ND<2 ND<2 11/15/2007 ND<2 ND<2 5/20/2008 ND<2 ND<2
11/20/2008 ND<2 ND<2

LMW-14R 14 10 (71.4286%) 6/2/2007 1 J 1 J
11/15/2007 ND<2 ND<2 5/20/2008 ND<2 ND<2
11/20/2008 9 9 6/11/2009 0.41 J 0.41 J 11/16/2009 ND<0.4 U ND<0.4 U
11/16/2009 ND<0.4 U ND<0.4 U 11/16/2009 0.47 J 0.47 J 6/30/2010 ND<0.4 U ND<0.4 U
11/17/2010 ND<0.4 U ND<0.4 U 7/6/2011 ND<0.4 U ND<0.4 U 11/22/2011 ND<0.4 U ND<0.4 U
5/16/2012 ND<0.4 U ND<0.4 U 11/16/2012 ND<0.4 U ND<0.4 U

LMW-15R 15 14 (93.3333%) 11/18/2006 ND<2 ND<2 6/2/2007 ND<2 ND<2
11/15/2007 ND<2 ND<2 11/15/2007 ND<2 ND<2 5/20/2008 ND<2 ND<2
5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2
6/11/2009 2.5 2.5 6/30/2010 ND<0.4 U ND<0.4 U
11/17/2010 ND<0.4 U ND<0.4 U 7/6/2011 ND<0.4 U ND<0.4 U
11/22/2011 ND<0.4 U ND<0.4 U 5/16/2012 ND<0.4 U ND<0.4 U 11/16/2012 ND<0.4 U ND<0.4 U

LMW-16 13 3 (23.0769%) 11/18/2006 ND<2 ND<2 6/2/2007 2 2
11/15/2007 ND<2 ND<2 5/20/2008 ND<2 ND<2
11/20/2008 9 9 6/11/2009 0.56 J 0.56 J 11/16/2009 0.59 J 0.59 J
6/30/2010 0.5 J 0.5 J 11/17/2010 0.54 J 0.54 J 7/6/2011 1 1
11/22/2011 0.54 J 0.54 J 5/16/2012 1.8 1.8 11/16/2012 1.1 1.1

LMW-3 25 23 (92%) 11/19/1996 ND<2 ND<2
3/24/1997 ND<2 ND<2 1/16/1998 ND<2 ND<2 3/16/1999 ND<2 ND<2
9/23/1999 ND<2 ND<2 3/14/2000 ND<2 ND<2 9/23/2003 ND<2 ND<2
3/10/2004 ND<2 ND<2 10/12/2004 ND<2 ND<2 4/1/2005 ND<2 ND<2
10/26/2005 ND<2 ND<2 6/19/2006 ND<2 ND<2 11/18/2006 ND<2 ND<2
6/2/2007 ND<2 ND<2 11/15/2007 ND<2 ND<2
5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2 6/11/2009 0.42 J B 0.42 J B 11/16/2009 ND<0.4 U ND<0.4 U
6/30/2010 ND<0.4 U ND<0.4 U 11/17/2010 0.44 J 0.44 J
7/6/2011 ND<0.4 U ND<0.4 U 11/22/2011 ND<0.4 U ND<0.4 U 5/16/2012 ND<0.4 U ND<0.4 U
11/16/2012 ND<0.4 U ND<0.4 U

LMW-3S 13 10 (76.9231%) 11/18/2006 ND<2 ND<2
6/2/2007 ND<2 ND<2 11/15/2007 ND<2 ND<2
5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2 6/11/2009 0.73 J B 0.73 J B
11/16/2009 ND<0.4 U ND<0.4 U 6/30/2010 ND<0.4 U ND<0.4 U 11/17/2010 1 1
7/6/2011 0.84 J 0.84 J 11/22/2011 ND<0.4 U ND<0.4 U 5/16/2012 ND<0.4 U ND<0.4 U
11/16/2012 ND<0.4 U ND<0.4 U

LMW-6 23 19 (82.6087%) 1/16/1998 ND<2 ND<2 3/16/1999 ND<2 ND<2
9/23/1999 ND<2 ND<2 3/14/2000 ND<2 ND<2
9/23/2003 ND<2 ND<2 3/10/2004 ND<2 ND<2 10/12/2004 ND<2 ND<2
4/1/2005 ND<2 ND<2 10/26/2005 ND<2 ND<2 6/19/2006 ND<2 ND<2
11/18/2006 ND<2 ND<2 6/2/2007 1 J 1 J 11/15/2007 ND<2 ND<2
5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2 6/11/2009 0.65 J B 0.65 J B
11/16/2009 ND<0.4 U ND<0.4 U 6/30/2010 0.46 J 0.46 J
11/17/2010 0.52 J 0.52 J 7/6/2011 ND<0.4 U ND<0.4 U 11/22/2011 ND<0.4 U ND<0.4 U
5/16/2012 ND<0.4 U ND<0.4 U 11/16/2012 ND<0.4 U ND<0.4 U

LMW-7 21 16 (76.1905%) 1/16/1998 ND<2 ND<2 3/16/1999 ND<2 ND<2 9/23/1999 ND<2 ND<2
3/14/2000 10 10 9/23/2003 ND<2 ND<2 3/10/2004 ND<2 ND<2 10/12/2004 ND<2 ND<2 4/1/2005 ND<2 ND<2
10/26/2005 ND<2 ND<2 6/19/2006 ND<2 ND<2 11/18/2006 ND<2 ND<2
6/2/2007 1 J 1 J 11/15/2007 ND<2 ND<2 5/20/2008 ND<2 ND<2
11/20/2008 10 10 6/11/2009 1.1 J B 1.1 J B 11/17/2010 ND<0.4 U ND<0.4 U
7/6/2011 1.8 1.8 11/22/2011 ND<0.4 U ND<0.4 U 5/16/2012 ND<0.4 U ND<0.4 U
11/16/2012 ND<0.4 U ND<0.4 U

LMW-8 23 15 (65.2174%) 1/16/1998 ND<2 ND<2 3/16/1999 ND<2 ND<2 9/23/1999 ND<2 ND<2
3/14/2000 ND<2 ND<2 9/23/2003 ND<2 ND<2 3/10/2004 ND<2 ND<2
10/12/2004 ND<2 ND<2 4/1/2005 ND<2 ND<2 10/26/2005 ND<2 ND<2
6/19/2006 ND<2 ND<2 11/18/2006 ND<2 ND<2
6/2/2007 ND<2 ND<2 11/15/2007 ND<2 ND<2 5/20/2008 ND<2 ND<2
11/20/2008 ND<2 ND<2 6/11/2009 0.49 J 0.49 J 11/16/2009 0.53 J 0.53 J
6/30/2010 0.43 J 0.43 J
11/17/2010 0.48 J 0.48 J 7/6/2011 0.81 J 0.81 J
11/22/2011 1.2 1.2 5/16/2012 1.3 1.3 11/16/2012 1.7 1.7

LMW-9 23 15 (65.2174%) 1/16/1998 ND<2 ND<2 3/16/1999 ND<2 ND<2
9/23/1999 3 3 3/14/2000 ND<2 ND<2
9/23/2003 ND<2 ND<2 3/10/2004 ND<2 ND<2 10/12/2004 ND<2 ND<2
4/1/2005 1 J 1 J 10/26/2005 ND<2 ND<2 6/19/2006 1 J 1 J
11/18/2006 ND<2 ND<2 6/2/2007 1 J 1 J 11/15/2007 ND<2 ND<2
5/20/2008 ND<2 ND<2 11/20/2008 8 8 6/11/2009 1.1 J 1.1 J
11/16/2009 ND<0.4 U ND<0.4 U 6/30/2010 0.58 J 0.58 J 11/17/2010 1.6 1.6
7/6/2011 ND<0.4 U ND<0.4 U 11/22/2011 ND<0.4 U ND<0.4 U 5/16/2012 ND<0.4 U ND<0.4 U 11/16/2012 ND<0.4 U ND<0.4 U

LMW-9D 13 1 (7.69231%) 11/18/2006 7 7 6/2/2007 7 7 11/15/2007 ND<2 ND<2
5/20/2008 3 3 11/20/2008 3 3
6/11/2009 2.1 2.1 11/16/2009 2 2 6/30/2010 1.8 1.8 11/17/2010 2 2
7/6/2011 3.2 3.2 11/22/2011 2.5 2.5
5/16/2012 2.6 2.6 11/16/2012 5.3 5.3

LMW-9S 12 3 (25%) 11/18/2006 ND<2 ND<2 6/2/2007 1 J 1 J 11/15/2007 4 4
5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2
6/11/2009 0.46 J 0.46 J 6/30/2010 0.57 J 0.57 J 11/17/2010 1.2 1.2
7/6/2011 0.46 J 0.46 J 11/22/2011 0.47 J 0.47 J 5/16/2012 0.54 J 0.54 J
11/16/2012 1.2 1.2

MW-5 13 11 (84.6154%) 1/16/1998 ND<2 ND<2
3/16/1999 ND<2 ND<2 9/23/1999 ND<2 ND<2
3/14/2000 34 34 9/23/2003 ND<2 ND<2
3/10/2004 60 60 10/12/2004 ND<2 ND<2
4/1/2005 ND<2 ND<2 10/26/2005 ND<2 ND<2 6/19/2006 ND<2 ND<2
11/15/2007 ND<2 ND<2 5/20/2008 ND<2 ND<2 11/20/2008 ND<2 ND<2

There are 0 unused locations

Loc. Meas. ND Date Conc. Original

Shapiro-Francia Test of Normality
Parameter: Arsenic
All Locations
Normality Test of Parameter Concentrations
Original Data (Not Transformed)
Non-Detects Replaced with 1/2 DL
Total Number of Measurements = 284

i x(i) m(i) sum(m^2) sum(mx)
1 0.2 -2.74777 7.55021 -0.549553
2 0.2 -2.45727 13.5884 -1.04101
3 0.2 -2.32634 19.0003 -1.50628
4 0.2 -2.19728 23.8283 -1.94573
5 0.2 -2.12007 28.323 -2.36975
6 0.2 -2.03352 32.4582 -2.77645
7 0.2 -1.97737 36.3682 -3.17192
8 0.2 -1.91103 40.0203 -3.55413
9 0.2 -1.86629 43.5033 -3.92739
10 0.2 -1.81191 46.7863 -4.28977
11 0.2 -1.77438 49.9348 -4.64465
12 0.2 -1.72793 52.9205 -4.99023
13 0.2 -1.6954 55.7949 -5.32931
14 0.2 -1.65463 58.5327 -5.66024
15 0.2 -1.62576 61.1758 -5.98539
16 0.2 -1.58927 63.7015 -6.30324
17 0.2 -1.56322 66.1452 -6.61589
18 0.2 -1.53007 68.4863 -6.9219
19 0.2 -1.50626 70.7551 -7.22315
20 0.2 -1.47579 72.9331 -7.51831
21 0.2 -1.4538 75.0466 -7.80907
22 0.2 -1.42554 77.0788 -8.09418
23 0.2 -1.40507 79.053 -8.3752
24 0.2 -1.37866 80.9537 -8.65093
25 0.2 -1.35946 82.8019 -8.92282
26 0.2 -1.33462 84.5831 -9.18975
27 0.2 -1.31652 86.3163 -9.45305
28 0.2 -1.29303 87.9883 -9.71166
29 0.2 -1.27588 89.6161 -9.96683
30 0.2 -1.25357 91.1875 -10.2175
31 0.2 -1.23724 92.7183 -10.465
32 0.2 -1.21596 94.1969 -10.7082
33 0.2 -1.20036 95.6377 -10.9483
34 0.2 -1.18 97.0301 -11.1843
35 0.2 -1.16505 98.3875 -11.4173
36 0.2 -1.1455 99.6996 -11.6464
37 0.2 -1.13113 100.979 -11.8726
38 0.2 -1.11232 102.216 -12.0951
39 0.2 -1.09847 103.423 -12.3148
40 0.2 -1.08032 104.59 -12.5308
41 0.2 -1.06694 105.728 -12.7442
42 0.2 -1.04939 106.83 -12.9541
43 0.2 -1.03643 107.904 -13.1614
44 0.2 -1.01943 108.943 -13.3653
45 0.2 -1.00687 109.957 -13.5666
46 0.2 -0.990356 110.938 -13.7647
47 0.2 -0.97815 111.894 -13.9603
48 0.2 -0.9621 112.82 -14.1527
49 0.2 -0.950222 113.723 -14.3428
50 0.2 -0.93459 114.596 -14.5297
51 0.2 -0.923014 115.448 -14.7143
52 0.2 -0.907769 116.272 -14.8959
53 0.2 -0.896473 117.076 -15.0752
54 0.2 -0.881587 117.853 -15.2515
55 0.2 -0.87055 118.611 -15.4256
56 0.41 -0.855996 119.344 -15.7765
57 0.42 -0.841621 120.052 -16.13
58 0.43 -0.830953 120.743 -16.4873
59 0.44 -0.816874 121.41 -16.8468
60 0.46 -0.806422 122.06 -17.2177
61 0.46 -0.792618 122.689 -17.5823
62 0.46 -0.782366 123.301 -17.9422
63 0.47 -0.768821 123.892 -18.3036
64 0.47 -0.758753 124.467 -18.6602
65 0.48 -0.745449 125.023 -19.018
66 0.49 -0.735557 125.564 -19.3784
67 0.5 -0.722479 126.086 -19.7396
68 0.52 -0.712751 126.594 -20.1103
69 0.53 -0.699883 127.084 -20.4812
70 0.54 -0.690309 127.561 -20.854
71 0.54 -0.677639 128.02 -21.2199
72 0.54 -0.668209 128.466 -21.5807
73 0.56 -0.655726 128.896 -21.9479
74 0.57 -0.646431 129.314 -22.3164
75 0.58 -0.634124 129.716 -22.6842
76 0.59 -0.624956 130.107 -23.0529
77 0.65 -0.612813 130.482 -23.4513
78 0.73 -0.603765 130.847 -23.892
79 0.81 -0.591776 131.197 -24.3713
80 0.84 -0.582841 131.537 -24.8609
81 1 -0.570999 131.863 -25.4319
82 1 -0.56217 132.179 -25.9941
83 1 -0.550465 132.482 -26.5446
84 1 -0.541736 132.775 -27.0863
85 1 -0.530162 133.056 -27.6165
86 1 -0.521527 133.328 -28.138
87 1 -0.510074 133.589 -28.6481
88 1 -0.501527 133.84 -29.1496
89 1 -0.490189 134.08 -29.6398
90 1 -0.481728 134.312 -30.1215
91 1 -0.470498 134.534 -30.592
92 1 -0.462114 134.747 -31.0541
93 1 -0.450985 134.951 -31.5051
94 1 -0.442676 135.147 -31.9478
95 1 -0.431644 135.333 -32.3794
96 1 -0.423405 135.512 -32.8028
97 1 -0.412463 135.682 -33.2153
98 1 -0.40429 135.846 -33.6196
99 1 -0.393433 136.001 -34.013
100 1 -0.385321 136.149 -34.3983
101 1 -0.374544 136.289 -34.7729
102 1 -0.36649 136.424 -35.1394
103 1 -0.355788 136.55 -35.4952
104 1 -0.347787 136.671 -35.8429
105 1 -0.337155 136.785 -36.1801
106 1 -0.329206 136.893 -36.5093
107 1 -0.318639 136.995 -36.8279
108 1 -0.310738 137.091 -37.1387
109 1 -0.300232 137.182 -37.4389
110 1 -0.292375 137.267 -37.7313
111 1 -0.281926 137.346 -38.0132
112 1 -0.27411 137.422 -38.2873
113 1 -0.263715 137.491 -38.551
114 1 -0.253347 137.555 -38.8044
115 1 -0.24559 137.616 -39.05
116 1 -0.235269 137.671 -39.2852
117 1 -0.227545 137.723 -39.5128
118 1 -0.217267 137.77 -39.7301
119 1 -0.209575 137.814 -39.9396
120 1 -0.199336 137.854 -40.139
121 1 -0.191671 137.89 -40.3306
122 1 -0.181468 137.923 -40.5121
123 1 -0.173829 137.954 -40.6859
124 1 -0.163659 137.98 -40.8496
125 1 -0.156042 138.005 -41.0056
126 1 -0.1459 138.026 -41.1515
127 1 -0.138305 138.045 -41.2898
128 1 -0.128189 138.062 -41.418
129 1 -0.12061 138.076 -41.5386
130 1 -0.110516 138.088 -41.6492
131 1 -0.102953 138.099 -41.7521
132 1 -0.0928787 138.108 -41.845
133 1 -0.0853288 138.115 -41.9303
134 1 -0.0752698 138.12 -42.0056
135 1 -0.0677301 138.125 -42.0733
136 1 -0.0576847 138.128 -42.131
137 1 -0.0501541 138.131 -42.1812
138 1 -0.0401167 138.132 -42.2213
139 1 -0.0325917 138.134 -42.2539
140 1 -0.0225612 138.134 -42.2764
141 1 -0.0150408 138.134 -42.2915
142 1 -0.00501359 138.134 -42.2965
143 1 0.00501359 138.134 -42.2915
144 1 0.0150408 138.135 -42.2764
145 1 0.0225612 138.135 -42.2539
146 1 0.0325917 138.136 -42.2213
147 1 0.0401167 138.138 -42.1812
148 1 0.0501541 138.14 -42.131
149 1 0.0576847 138.144 -42.0733
150 1 0.0677301 138.148 -42.0056
151 1 0.0752698 138.154 -41.9303
152 1 0.0853288 138.161 -41.845
153 1 0.0928787 138.17 -41.7521
154 1 0.102953 138.18 -41.6492
155 1 0.110516 138.193 -41.5386
156 1 0.12061 138.207 -41.418
157 1 0.128189 138.224 -41.2898
158 1 0.138305 138.243 -41.1515
159 1 0.1459 138.264 -41.0056
160 1 0.156042 138.288 -40.8496
161 1 0.163659 138.315 -40.6859
162 1 0.173829 138.345 -40.5121
163 1 0.181468 138.378 -40.3306
164 1 0.191671 138.415 -40.139
165 1 0.199336 138.455 -39.9396
166 1 0.209575 138.499 -39.7301
167 1 0.217267 138.546 -39.5128
168 1 0.227545 138.598 -39.2852
169 1 0.235269 138.653 -39.05
170 1 0.24559 138.713 -38.8044
171 1 0.253347 138.777 -38.551
172 1 0.263715 138.847 -38.2873
173 1 0.27411 138.922 -38.0132
174 1 0.281926 139.002 -37.7313
175 1 0.292375 139.087 -37.4389
176 1 0.300232 139.177 -37.1387
177 1 0.310738 139.274 -36.8279
178 1 0.318639 139.375 -36.5093
179 1 0.329206 139.484 -36.1801
180 1 0.337155 139.597 -35.8429
181 1 0.347787 139.718 -35.4952
182 1 0.355788 139.845 -35.1394
183 1 0.36649 139.979 -34.7729
184 1 0.374544 140.12 -34.3983
185 1 0.385321 140.268 -34.013
186 1 0.393433 140.423 -33.6196
187 1 0.40429 140.586 -33.2153
188 1 0.412463 140.756 -32.8028
189 1 0.423405 140.936 -32.3794
190 1 0.431644 141.122 -31.9478
191 1 0.442676 141.318 -31.5051
192 1 0.450985 141.521 -31.0541
193 1 0.462114 141.735 -30.592
194 1 0.470498 141.956 -30.1215
195 1 0.481728 142.188 -29.6398
196 1 0.490189 142.429 -29.1496
197 1 0.501527 142.68 -28.6481
198 1 0.510074 142.94 -28.138
199 1 0.521527 143.212 -27.6165
200 1 0.530162 143.493 -27.0863
201 1 0.541736 143.787 -26.5446
202 1 0.550465 144.09 -25.9941
203 1 0.56217 144.406 -25.4319
204 1 0.570999 144.732 -24.8609
205 1 0.582841 145.072 -24.2781
206 1 0.591776 145.422 -23.6863
207 1 0.603765 145.786 -23.0825
208 1 0.612813 146.162 -22.4697
209 1 0.624956 146.552 -21.8448
210 1 0.634124 146.955 -21.2107
211 1 0.646431 147.372 -20.5642
212 1 0.655726 147.802 -19.9085
213 1 0.668209 148.249 -19.2403
214 1 0.677639 148.708 -18.5626
215 1 0.690309 149.185 -17.8723
216 1 0.699883 149.674 -17.1725
217 1 0.712751 150.182 -16.4597
218 1 0.722479 150.704 -15.7372
219 1 0.735557 151.245 -15.0017
220 1 0.745449 151.801 -14.2562
221 1 0.758753 152.377 -13.4975
222 1 0.768821 152.968 -12.7286
223 1 0.782366 153.58 -11.9463
224 1 0.792618 154.208 -11.1537
225 1 0.806422 154.859 -10.3472
226 1 0.816874 155.526 -9.53037
227 1 0.830953 156.216 -8.69941
228 1 0.841621 156.925 -7.85779
229 1 0.855996 157.657 -7.0018
230 1 0.87055 158.415 -6.13125
231 1 0.881587 159.193 -5.24966
232 1 0.896473 159.996 -4.35319
233 1 0.907769 160.82 -3.44542
234 1 0.923014 161.672 -2.5224
235 1 0.93459 162.546 -1.58781
236 1 0.950222 163.449 -0.637592
237 1 0.9621 164.374 0.324508
238 1 0.97815 165.331 1.30266
239 1 0.990356 166.312 2.29301
240 1 1.00687 167.326 3.29988
241 1 1.01943 168.365 4.31931
242 1 1.03643 169.439 5.35574
243 1 1.04939 170.54 6.40513
244 1 1.06694 171.679 7.47206
245 1.1 1.08032 172.846 8.66042
246 1.1 1.09847 174.052 9.86873
247 1.1 1.11232 175.29 11.0923
248 1.2 1.13113 176.569 12.4496
249 1.2 1.1455 177.881 13.8242
250 1.2 1.16505 179.239 15.2223
251 1.3 1.18 180.631 16.7563
252 1.6 1.20036 182.072 18.6769
253 1.7 1.21596 183.55 20.744
254 1.8 1.23724 185.081 22.971
255 1.8 1.25357 186.653 25.2275
256 1.8 1.27588 188.28 27.524
257 2 1.29303 189.952 30.1101
258 2 1.31652 191.686 32.7431
259 2 1.33462 193.467 35.4124
260 2.1 1.35946 195.315 38.2673
261 2.5 1.37866 197.216 41.7139
262 2.5 1.40507 199.19 45.2266
263 2.6 1.42554 201.222 48.933
264 3 1.4538 203.336 53.2944
265 3 1.47579 205.514 57.7218
266 3 1.50626 207.782 62.2406
267 3.2 1.53007 210.123 67.1368
268 4 1.56322 212.567 73.3897
269 5.3 1.58927 215.093 81.8128
270 7 1.62576 217.736 93.1931
271 7 1.65463 220.474 104.776
272 8 1.6954 223.348 118.339
273 9 1.72793 226.334 133.89
274 9 1.77438 229.482 149.859
275 10 1.81191 232.765 167.979
276 10 1.86629 236.248 186.642
277 12 1.91103 239.9 209.574
278 16 1.97737 243.81 241.212
279 18 2.03352 247.946 277.815
280 23 2.12007 252.44 326.577
281 25 2.19728 257.268 381.509
282 34 2.32634 262.68 460.605
283 57 2.45727 268.718 600.669
284 60 2.74777 276.269 765.535

Data Set Standard Deviation = 5.8445
Numerator = 586044
Denominator = 2.67063e+006
W Statistic = 0.219441 = 586044 / 2.67063e+006

5% Critical value of 0.976 exceeds 0.219441
Evidence of non-normality at 95% level of significance

1% Critical value of 0.967 exceeds 0.219441
Evidence of non-normality at 99% level of significance

Probability Plot
Parameter: Arsenic
Original Data (Not Transformed)
Non-Detects Replaced with 1/2 DL

Probability Plot
Correlation Coefficient = 0.475572
0.475572 < 0.987 -- Normality test fails at 95% level

Plotted Data Points

Datum Value Prob. Quantile. x y
1 0.2 0.00350877 -2.74777 40.7833 348.683
2 0.2 0.00701754 -2.45727 40.7833 334.497
3 0.2 0.0105263 -2.32634 40.7833 328.103
4 0.2 0.0140351 -2.19728 40.7833 321.801
5 0.2 0.0175439 -2.12007 40.7833 318.03
6 0.2 0.0210526 -2.03352 40.7833 313.804
7 0.2 0.0245614 -1.97737 40.7833 311.062
8 0.2 0.0280702 -1.91103 40.7833 307.822
9 0.2 0.0315789 -1.86629 40.7833 305.637
10 0.2 0.0350877 -1.81191 40.7833 302.982
11 0.2 0.0385965 -1.77438 40.7833 301.149
12 0.2 0.0421053 -1.72793 40.7833 298.881
13 0.2 0.045614 -1.6954 40.7833 297.292
14 0.2 0.0491228 -1.65463 40.7833 295.301
15 0.2 0.0526316 -1.62576 40.7833 293.891
16 0.2 0.0561404 -1.58927 40.7833 292.109
17 0.2 0.0596491 -1.56322 40.7833 290.837
18 0.2 0.0631579 -1.53007 40.7833 289.218
19 0.2 0.0666667 -1.50626 40.7833 288.056
20 0.2 0.0701754 -1.47579 40.7833 286.568
21 0.2 0.0736842 -1.4538 40.7833 285.494
22 0.2 0.077193 -1.42554 40.7833 284.114
23 0.2 0.0807018 -1.40507 40.7833 283.114
24 0.2 0.0842105 -1.37866 40.7833 281.824
25 0.2 0.0877193 -1.35946 40.7833 280.887
26 0.2 0.0912281 -1.33462 40.7833 279.674
27 0.2 0.0947368 -1.31652 40.7833 278.79
28 0.2 0.0982456 -1.29303 40.7833 277.643
29 0.2 0.101754 -1.27588 40.7833 276.805
30 0.2 0.105263 -1.25357 40.7833 275.716
31 0.2 0.108772 -1.23724 40.7833 274.918
32 0.2 0.112281 -1.21596 40.7833 273.879
33 0.2 0.115789 -1.20036 40.7833 273.118
34 0.2 0.119298 -1.18 40.7833 272.123
35 0.2 0.122807 -1.16505 40.7833 271.393
36 0.2 0.126316 -1.1455 40.7833 270.439
37 0.2 0.129825 -1.13113 40.7833 269.737
38 0.2 0.133333 -1.11232 40.7833 268.818
39 0.2 0.136842 -1.09847 40.7833 268.142
40 0.2 0.140351 -1.08032 40.7833 267.256
41 0.2 0.14386 -1.06694 40.7833 266.602
42 0.2 0.147368 -1.04939 40.7833 265.745
43 0.2 0.150877 -1.03643 40.7833 265.112
44 0.2 0.154386 -1.01943 40.7833 264.282
45 0.2 0.157895 -1.00687 40.7833 263.669
46 0.2 0.161404 -0.990356 40.7833 262.862
47 0.2 0.164912 -0.97815 40.7833 262.266
48 0.2 0.168421 -0.9621 40.7833 261.483
49 0.2 0.17193 -0.950222 40.7833 260.903
50 0.2 0.175439 -0.93459 40.7833 260.139
51 0.2 0.178947 -0.923014 40.7833 259.574
52 0.2 0.182456 -0.907769 40.7833 258.829
53 0.2 0.185965 -0.896473 40.7833 258.278
54 0.2 0.189474 -0.881587 40.7833 257.551
55 0.2 0.192982 -0.87055 40.7833 257.012
56 0.41 0.196491 -0.855996 42.6558 256.301
57 0.42 0.2 -0.841621 42.745 255.599
58 0.43 0.203509 -0.830953 42.8342 255.078
59 0.44 0.207018 -0.816874 42.9233 254.391
60 0.46 0.210526 -0.806422 43.1017 253.88
61 0.46 0.214035 -0.792618 43.1017 253.206
62 0.46 0.217544 -0.782366 43.1017 252.706
63 0.47 0.221053 -0.768821 43.1908 252.044
64 0.47 0.224561 -0.758753 43.1908 251.552
65 0.48 0.22807 -0.745449 43.28 250.903
66 0.49 0.231579 -0.735557 43.3692 250.42
67 0.5 0.235088 -0.722479 43.4583 249.781
68 0.52 0.238596 -0.712751 43.6367 249.306
69 0.53 0.242105 -0.699883 43.7258 248.678
70 0.54 0.245614 -0.690309 43.815 248.21
71 0.54 0.249123 -0.677639 43.815 247.591
72 0.54 0.252632 -0.668209 43.815 247.131
73 0.56 0.25614 -0.655726 43.9933 246.521
74 0.57 0.259649 -0.646431 44.0825 246.067
75 0.58 0.263158 -0.634124 44.1717 245.466
76 0.59 0.266667 -0.624956 44.2608 245.019
77 0.65 0.270175 -0.612813 44.7958 244.426
78 0.73 0.273684 -0.603765 45.5092 243.984
79 0.81 0.277193 -0.591776 46.2225 243.398
80 0.84 0.280702 -0.582841 46.49 242.962
81 1 0.284211 -0.570999 47.9167 242.384
82 1 0.287719 -0.56217 47.9167 241.953
83 1 0.291228 -0.550465 47.9167 241.381
84 1 0.294737 -0.541736 47.9167 240.955
85 1 0.298246 -0.530162 47.9167 240.39
86 1 0.301754 -0.521527 47.9167 239.968
87 1 0.305263 -0.510074 47.9167 239.409
88 1 0.308772 -0.501527 47.9167 238.991
89 1 0.312281 -0.490189 47.9167 238.438
90 1 0.315789 -0.481728 47.9167 238.024
91 1 0.319298 -0.470498 47.9167 237.476
92 1 0.322807 -0.462114 47.9167 237.067
93 1 0.326316 -0.450985 47.9167 236.523
94 1 0.329825 -0.442676 47.9167 236.117
95 1 0.333333 -0.431644 47.9167 235.579
96 1 0.336842 -0.423405 47.9167 235.176
97 1 0.340351 -0.412463 47.9167 234.642
98 1 0.34386 -0.40429 47.9167 234.243
99 1 0.347368 -0.393433 47.9167 233.713
100 1 0.350877 -0.385321 47.9167 233.317
101 1 0.354386 -0.374544 47.9167 232.79
102 1 0.357895 -0.36649 47.9167 232.397
103 1 0.361404 -0.355788 47.9167 231.874
104 1 0.364912 -0.347787 47.9167 231.484
105 1 0.368421 -0.337155 47.9167 230.964
106 1 0.37193 -0.329206 47.9167 230.576
107 1 0.375439 -0.318639 47.9167 230.06
108 1 0.378947 -0.310738 47.9167 229.674
109 1 0.382456 -0.300232 47.9167 229.161
110 1 0.385965 -0.292375 47.9167 228.778
111 1 0.389474 -0.281926 47.9167 228.267
112 1 0.392982 -0.27411 47.9167 227.886
113 1 0.396491 -0.263715 47.9167 227.378
114 1 0.4 -0.253347 47.9167 226.872
115 1 0.403509 -0.24559 47.9167 226.493
116 1 0.407018 -0.235269 47.9167 225.989
117 1 0.410526 -0.227545 47.9167 225.612
118 1 0.414035 -0.217267 47.9167 225.11
119 1 0.417544 -0.209575 47.9167 224.734
120 1 0.421053 -0.199336 47.9167 224.234
121 1 0.424561 -0.191671 47.9167 223.86
122 1 0.42807 -0.181468 47.9167 223.362
123 1 0.431579 -0.173829 47.9167 222.989
124 1 0.435088 -0.163659 47.9167 222.492
125 1 0.438596 -0.156042 47.9167 222.12
126 1 0.442105 -0.1459 47.9167 221.625
127 1 0.445614 -0.138305 47.9167 221.254
128 1 0.449123 -0.128189 47.9167 220.76
129 1 0.452632 -0.12061 47.9167 220.39
130 1 0.45614 -0.110516 47.9167 219.897
131 1 0.459649 -0.102953 47.9167 219.528
132 1 0.463158 -0.0928787 47.9167 219.036
133 1 0.466667 -0.0853288 47.9167 218.667
134 1 0.470175 -0.0752698 47.9167 218.176
135 1 0.473684 -0.0677301 47.9167 217.807
136 1 0.477193 -0.0576847 47.9167 217.317
137 1 0.480702 -0.0501541 47.9167 216.949
138 1 0.484211 -0.0401167 47.9167 216.459
139 1 0.487719 -0.0325917 47.9167 216.092
140 1 0.491228 -0.0225612 47.9167 215.602
141 1 0.494737 -0.0150408 47.9167 215.234
142 1 0.498246 -0.00501359 47.9167 214.745
143 1 0.501754 0.00501359 47.9167 214.255
144 1 0.505263 0.0150408 47.9167 213.766
145 1 0.508772 0.0225612 47.9167 213.398
146 1 0.512281 0.0325917 47.9167 212.908
147 1 0.515789 0.0401167 47.9167 212.541
148 1 0.519298 0.0501541 47.9167 212.051
149 1 0.522807 0.0576847 47.9167 211.683
150 1 0.526316 0.0677301 47.9167 211.193
151 1 0.529825 0.0752698 47.9167 210.824
152 1 0.533333 0.0853288 47.9167 210.333
153 1 0.536842 0.0928787 47.9167 209.964
154 1 0.540351 0.102953 47.9167 209.472
155 1 0.54386 0.110516 47.9167 209.103
156 1 0.547368 0.12061 47.9167 208.61
157 1 0.550877 0.128189 47.9167 208.24
158 1 0.554386 0.138305 47.9167 207.746
159 1 0.557895 0.1459 47.9167 207.375
160 1 0.561404 0.156042 47.9167 206.88
161 1 0.564912 0.163659 47.9167 206.508
162 1 0.568421 0.173829 47.9167 206.011
163 1 0.57193 0.181468 47.9167 205.638
164 1 0.575439 0.191671 47.9167 205.14
165 1 0.578947 0.199336 47.9167 204.766
166 1 0.582456 0.209575 47.9167 204.266
167 1 0.585965 0.217267 47.9167 203.89
168 1 0.589474 0.227545 47.9167 203.388
169 1 0.592982 0.235269 47.9167 203.011
170 1 0.596491 0.24559 47.9167 202.507
171 1 0.6 0.253347 47.9167 202.128
172 1 0.603509 0.263715 47.9167 201.622
173 1 0.607018 0.27411 47.9167 201.114
174 1 0.610526 0.281926 47.9167 200.733
175 1 0.614035 0.292375 47.9167 200.222
176 1 0.617544 0.300232 47.9167 199.839
177 1 0.621053 0.310738 47.9167 199.326
178 1 0.624561 0.318639 47.9167 198.94
179 1 0.62807 0.329206 47.9167 198.424
180 1 0.631579 0.337155 47.9167 198.036
181 1 0.635088 0.347787 47.9167 197.516
182 1 0.638596 0.355788 47.9167 197.126
183 1 0.642105 0.36649 47.9167 196.603
184 1 0.645614 0.374544 47.9167 196.21
185 1 0.649123 0.385321 47.9167 195.683
186 1 0.652632 0.393433 47.9167 195.287
187 1 0.65614 0.40429 47.9167 194.757
188 1 0.659649 0.412463 47.9167 194.358
189 1 0.663158 0.423405 47.9167 193.824
190 1 0.666667 0.431644 47.9167 193.421
191 1 0.670175 0.442676 47.9167 192.883
192 1 0.673684 0.450985 47.9167 192.477
193 1 0.677193 0.462114 47.9167 191.933
194 1 0.680702 0.470498 47.9167 191.524
195 1 0.684211 0.481728 47.9167 190.976
196 1 0.687719 0.490189 47.9167 190.562
197 1 0.691228 0.501527 47.9167 190.009
198 1 0.694737 0.510074 47.9167 189.591
199 1 0.698246 0.521527 47.9167 189.032
200 1 0.701754 0.530162 47.9167 188.61
201 1 0.705263 0.541736 47.9167 188.045
202 1 0.708772 0.550465 47.9167 187.619
203 1 0.712281 0.56217 47.9167 187.047
204 1 0.715789 0.570999 47.9167 186.616
205 1 0.719298 0.582841 47.9167 186.038
206 1 0.722807 0.591776 47.9167 185.602
207 1 0.726316 0.603765 47.9167 185.016
208 1 0.729825 0.612813 47.9167 184.574
209 1 0.733333 0.624956 47.9167 183.981
210 1 0.736842 0.634124 47.9167 183.534
211 1 0.740351 0.646431 47.9167 182.933
212 1 0.74386 0.655726 47.9167 182.479
213 1 0.747368 0.668209 47.9167 181.869
214 1 0.750877 0.677639 47.9167 181.409
215 1 0.754386 0.690309 47.9167 180.79
216 1 0.757895 0.699883 47.9167 180.322
217 1 0.761404 0.712751 47.9167 179.694
218 1 0.764912 0.722479 47.9167 179.219
219 1 0.768421 0.735557 47.9167 178.58
220 1 0.77193 0.745449 47.9167 178.097
221 1 0.775439 0.758753 47.9167 177.448
222 1 0.778947 0.768821 47.9167 176.956
223 1 0.782456 0.782366 47.9167 176.294
224 1 0.785965 0.792618 47.9167 175.794
225 1 0.789474 0.806422 47.9167 175.12
226 1 0.792982 0.816874 47.9167 174.609
227 1 0.796491 0.830953 47.9167 173.922
228 1 0.8 0.841621 47.9167 173.401
229 1 0.803509 0.855996 47.9167 172.699
230 1 0.807018 0.87055 47.9167 171.988
231 1 0.810526 0.881587 47.9167 171.449
232 1 0.814035 0.896473 47.9167 170.722
233 1 0.817544 0.907769 47.9167 170.171
234 1 0.821053 0.923014 47.9167 169.426
235 1 0.824561 0.93459 47.9167 168.861
236 1 0.82807 0.950222 47.9167 168.097
237 1 0.831579 0.9621 47.9167 167.517
238 1 0.835088 0.97815 47.9167 166.734
239 1 0.838596 0.990356 47.9167 166.138
240 1 0.842105 1.00687 47.9167 165.331
241 1 0.845614 1.01943 47.9167 164.718
242 1 0.849123 1.03643 47.9167 163.888
243 1 0.852632 1.04939 47.9167 163.255
244 1 0.85614 1.06694 47.9167 162.398
245 1.1 0.859649 1.08032 48.8083 161.744
246 1.1 0.863158 1.09847 48.8083 160.858
247 1.1 0.866667 1.11232 48.8083 160.182
248 1.2 0.870175 1.13113 49.7 159.263
249 1.2 0.873684 1.1455 49.7 158.561
250 1.2 0.877193 1.16505 49.7 157.607
251 1.3 0.880702 1.18 50.5917 156.877
252 1.6 0.884211 1.20036 53.2667 155.882
253 1.7 0.887719 1.21596 54.1583 155.121
254 1.8 0.891228 1.23724 55.05 154.082
255 1.8 0.894737 1.25357 55.05 153.284
256 1.8 0.898246 1.27588 55.05 152.195
257 2 0.901754 1.29303 56.8333 151.357
258 2 0.905263 1.31652 56.8333 150.21
259 2 0.908772 1.33462 56.8333 149.326
260 2.1 0.912281 1.35946 57.725 148.113
261 2.5 0.915789 1.37866 61.2917 147.176
262 2.5 0.919298 1.40507 61.2917 145.886
263 2.6 0.922807 1.42554 62.1833 144.886
264 3 0.926316 1.4538 65.75 143.506
265 3 0.929825 1.47579 65.75 142.432
266 3 0.933333 1.50626 65.75 140.944
267 3.2 0.936842 1.53007 67.5333 139.782
268 4 0.940351 1.56322 74.6667 138.163
269 5.3 0.94386 1.58927 86.2583 136.891
270 7 0.947368 1.62576 101.417 135.109
271 7 0.950877 1.65463 101.417 133.699
272 8 0.954386 1.6954 110.333 131.708
273 9 0.957895 1.72793 119.25 130.119
274 9 0.961404 1.77438 119.25 127.851
275 10 0.964912 1.81191 128.167 126.018
276 10 0.968421 1.86629 128.167 123.363
277 12 0.97193 1.91103 146 121.178
278 16 0.975439 1.97737 181.667 117.938
279 18 0.978947 2.03352 199.5 115.196
280 23 0.982456 2.12007 244.083 110.97
281 25 0.985965 2.19728 261.917 107.199
282 34 0.989474 2.32634 342.167 100.897
283 57 0.992982 2.45727 547.25 94.5032
284 60 0.996491 2.74777 574 80.3175

Shapiro-Francia Test of Normality
Parameter: Arsenic
All Locations
Normality Test of Parameter Concentrations
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL
Total Number of Measurements = 284

i x(i) m(i) sum(m^2) sum(mx)
1 -1.60944 -2.74777 7.55021 4.42236
2 -1.60944 -2.45727 13.5884 8.37719
3 -1.60944 -2.32634 19.0003 12.1213
4 -1.60944 -2.19728 23.8283 15.6577
5 -1.60944 -2.12007 28.323 19.0698
6 -1.60944 -2.03352 32.4582 22.3426
7 -1.60944 -1.97737 36.3682 25.5251
8 -1.60944 -1.91103 40.0203 28.6008
9 -1.60944 -1.86629 43.5033 31.6044
10 -1.60944 -1.81191 46.7863 34.5206
11 -1.60944 -1.77438 49.9348 37.3764
12 -1.60944 -1.72793 52.9205 40.1574
13 -1.60944 -1.6954 55.7949 42.886
14 -1.60944 -1.65463 58.5327 45.549
15 -1.60944 -1.62576 61.1758 48.1656
16 -1.60944 -1.58927 63.7015 50.7234
17 -1.60944 -1.56322 66.1452 53.2393
18 -1.60944 -1.53007 68.4863 55.7019
19 -1.60944 -1.50626 70.7551 58.1261
20 -1.60944 -1.47579 72.9331 60.5013
21 -1.60944 -1.4538 75.0466 62.8411
22 -1.60944 -1.42554 77.0788 65.1354
23 -1.60944 -1.40507 79.053 67.3968
24 -1.60944 -1.37866 80.9537 69.6157
25 -1.60944 -1.35946 82.8019 71.8036
26 -1.60944 -1.33462 84.5831 73.9516
27 -1.60944 -1.31652 86.3163 76.0705
28 -1.60944 -1.29303 87.9883 78.1515
29 -1.60944 -1.27588 89.6161 80.205
30 -1.60944 -1.25357 91.1875 82.2225
31 -1.60944 -1.23724 92.7183 84.2138
32 -1.60944 -1.21596 94.1969 86.1708
33 -1.60944 -1.20036 95.6377 88.1027
34 -1.60944 -1.18 97.0301 90.0018
35 -1.60944 -1.16505 98.3875 91.8769
36 -1.60944 -1.1455 99.6996 93.7205
37 -1.60944 -1.13113 100.979 95.541
38 -1.60944 -1.11232 102.216 97.3312
39 -1.60944 -1.09847 103.423 99.0991
40 -1.60944 -1.08032 104.59 100.838
41 -1.60944 -1.06694 105.728 102.555
42 -1.60944 -1.04939 106.83 104.244
43 -1.60944 -1.03643 107.904 105.912
44 -1.60944 -1.01943 108.943 107.553
45 -1.60944 -1.00687 109.957 109.173
46 -1.60944 -0.990356 110.938 110.767
47 -1.60944 -0.97815 111.894 112.341
48 -1.60944 -0.9621 112.82 113.89
49 -1.60944 -0.950222 113.723 115.419
50 -1.60944 -0.93459 114.596 116.923
51 -1.60944 -0.923014 115.448 118.409
52 -1.60944 -0.907769 116.272 119.87
53 -1.60944 -0.896473 117.076 121.313
54 -1.60944 -0.881587 117.853 122.732
55 -1.60944 -0.87055 118.611 124.133
56 -0.891598 -0.855996 119.344 124.896
57 -0.867501 -0.841621 120.052 125.626
58 -0.84397 -0.830953 120.743 126.327
59 -0.820981 -0.816874 121.41 126.998
60 -0.776529 -0.806422 122.06 127.624
61 -0.776529 -0.792618 122.689 128.24
62 -0.776529 -0.782366 123.301 128.847
63 -0.755023 -0.768821 123.892 129.428
64 -0.755023 -0.758753 124.467 130
65 -0.733969 -0.745449 125.023 130.548
66 -0.71335 -0.735557 125.564 131.072
67 -0.693147 -0.722479 126.086 131.573
68 -0.653926 -0.712751 126.594 132.039
69 -0.634878 -0.699883 127.084 132.484
70 -0.616186 -0.690309 127.561 132.909
71 -0.616186 -0.677639 128.02 133.326
72 -0.616186 -0.668209 128.466 133.738
73 -0.579818 -0.655726 128.896 134.118
74 -0.562119 -0.646431 129.314 134.482
75 -0.544727 -0.634124 129.716 134.827
76 -0.527633 -0.624956 130.107 135.157
77 -0.430783 -0.612813 130.482 135.421
78 -0.314711 -0.603765 130.847 135.611
79 -0.210721 -0.591776 131.197 135.736
80 -0.174353 -0.582841 131.537 135.837
81 0 -0.570999 131.863 135.837
82 0 -0.56217 132.179 135.837
83 0 -0.550465 132.482 135.837
84 0 -0.541736 132.775 135.837
85 0 -0.530162 133.056 135.837
86 0 -0.521527 133.328 135.837
87 0 -0.510074 133.589 135.837
88 0 -0.501527 133.84 135.837
89 0 -0.490189 134.08 135.837
90 0 -0.481728 134.312 135.837
91 0 -0.470498 134.534 135.837
92 0 -0.462114 134.747 135.837
93 0 -0.450985 134.951 135.837
94 0 -0.442676 135.147 135.837
95 0 -0.431644 135.333 135.837
96 0 -0.423405 135.512 135.837
97 0 -0.412463 135.682 135.837
98 0 -0.40429 135.846 135.837
99 0 -0.393433 136.001 135.837
100 0 -0.385321 136.149 135.837
101 0 -0.374544 136.289 135.837
102 0 -0.36649 136.424 135.837
103 0 -0.355788 136.55 135.837
104 0 -0.347787 136.671 135.837
105 0 -0.337155 136.785 135.837
106 0 -0.329206 136.893 135.837
107 0 -0.318639 136.995 135.837
108 0 -0.310738 137.091 135.837
109 0 -0.300232 137.182 135.837
110 0 -0.292375 137.267 135.837
111 0 -0.281926 137.346 135.837
112 0 -0.27411 137.422 135.837
113 0 -0.263715 137.491 135.837
114 0 -0.253347 137.555 135.837
115 0 -0.24559 137.616 135.837
116 0 -0.235269 137.671 135.837
117 0 -0.227545 137.723 135.837
118 0 -0.217267 137.77 135.837
119 0 -0.209575 137.814 135.837
120 0 -0.199336 137.854 135.837
121 0 -0.191671 137.89 135.837
122 0 -0.181468 137.923 135.837
123 0 -0.173829 137.954 135.837
124 0 -0.163659 137.98 135.837
125 0 -0.156042 138.005 135.837
126 0 -0.1459 138.026 135.837
127 0 -0.138305 138.045 135.837
128 0 -0.128189 138.062 135.837
129 0 -0.12061 138.076 135.837
130 0 -0.110516 138.088 135.837
131 0 -0.102953 138.099 135.837
132 0 -0.0928787 138.108 135.837
133 0 -0.0853288 138.115 135.837
134 0 -0.0752698 138.12 135.837
135 0 -0.0677301 138.125 135.837
136 0 -0.0576847 138.128 135.837
137 0 -0.0501541 138.131 135.837
138 0 -0.0401167 138.132 135.837
139 0 -0.0325917 138.134 135.837
140 0 -0.0225612 138.134 135.837
141 0 -0.0150408 138.134 135.837
142 0 -0.00501359 138.134 135.837
143 0 0.00501359 138.134 135.837
144 0 0.0150408 138.135 135.837
145 0 0.0225612 138.135 135.837
146 0 0.0325917 138.136 135.837
147 0 0.0401167 138.138 135.837
148 0 0.0501541 138.14 135.837
149 0 0.0576847 138.144 135.837
150 0 0.0677301 138.148 135.837
151 0 0.0752698 138.154 135.837
152 0 0.0853288 138.161 135.837
153 0 0.0928787 138.17 135.837
154 0 0.102953 138.18 135.837
155 0 0.110516 138.193 135.837
156 0 0.12061 138.207 135.837
157 0 0.128189 138.224 135.837
158 0 0.138305 138.243 135.837
159 0 0.1459 138.264 135.837
160 0 0.156042 138.288 135.837
161 0 0.163659 138.315 135.837
162 0 0.173829 138.345 135.837
163 0 0.181468 138.378 135.837
164 0 0.191671 138.415 135.837
165 0 0.199336 138.455 135.837
166 0 0.209575 138.499 135.837
167 0 0.217267 138.546 135.837
168 0 0.227545 138.598 135.837
169 0 0.235269 138.653 135.837
170 0 0.24559 138.713 135.837
171 0 0.253347 138.777 135.837
172 0 0.263715 138.847 135.837
173 0 0.27411 138.922 135.837
174 0 0.281926 139.002 135.837
175 0 0.292375 139.087 135.837
176 0 0.300232 139.177 135.837
177 0 0.310738 139.274 135.837
178 0 0.318639 139.375 135.837
179 0 0.329206 139.484 135.837
180 0 0.337155 139.597 135.837
181 0 0.347787 139.718 135.837
182 0 0.355788 139.845 135.837
183 0 0.36649 139.979 135.837
184 0 0.374544 140.12 135.837
185 0 0.385321 140.268 135.837
186 0 0.393433 140.423 135.837
187 0 0.40429 140.586 135.837
188 0 0.412463 140.756 135.837
189 0 0.423405 140.936 135.837
190 0 0.431644 141.122 135.837
191 0 0.442676 141.318 135.837
192 0 0.450985 141.521 135.837
193 0 0.462114 141.735 135.837
194 0 0.470498 141.956 135.837
195 0 0.481728 142.188 135.837
196 0 0.490189 142.429 135.837
197 0 0.501527 142.68 135.837
198 0 0.510074 142.94 135.837
199 0 0.521527 143.212 135.837
200 0 0.530162 143.493 135.837
201 0 0.541736 143.787 135.837
202 0 0.550465 144.09 135.837
203 0 0.56217 144.406 135.837
204 0 0.570999 144.732 135.837
205 0 0.582841 145.072 135.837
206 0 0.591776 145.422 135.837
207 0 0.603765 145.786 135.837
208 0 0.612813 146.162 135.837
209 0 0.624956 146.552 135.837
210 0 0.634124 146.955 135.837
211 0 0.646431 147.372 135.837
212 0 0.655726 147.802 135.837
213 0 0.668209 148.249 135.837
214 0 0.677639 148.708 135.837
215 0 0.690309 149.185 135.837
216 0 0.699883 149.674 135.837
217 0 0.712751 150.182 135.837
218 0 0.722479 150.704 135.837
219 0 0.735557 151.245 135.837
220 0 0.745449 151.801 135.837
221 0 0.758753 152.377 135.837
222 0 0.768821 152.968 135.837
223 0 0.782366 153.58 135.837
224 0 0.792618 154.208 135.837
225 0 0.806422 154.859 135.837
226 0 0.816874 155.526 135.837
227 0 0.830953 156.216 135.837
228 0 0.841621 156.925 135.837
229 0 0.855996 157.657 135.837
230 0 0.87055 158.415 135.837
231 0 0.881587 159.193 135.837
232 0 0.896473 159.996 135.837
233 0 0.907769 160.82 135.837
234 0 0.923014 161.672 135.837
235 0 0.93459 162.546 135.837
236 0 0.950222 163.449 135.837
237 0 0.9621 164.374 135.837
238 0 0.97815 165.331 135.837
239 0 0.990356 166.312 135.837
240 0 1.00687 167.326 135.837
241 0 1.01943 168.365 135.837
242 0 1.03643 169.439 135.837
243 0 1.04939 170.54 135.837
244 0 1.06694 171.679 135.837
245 0.0953102 1.08032 172.846 135.94
246 0.0953102 1.09847 174.052 136.045
247 0.0953102 1.11232 175.29 136.151
248 0.182322 1.13113 176.569 136.357
249 0.182322 1.1455 177.881 136.566
250 0.182322 1.16505 179.239 136.778
251 0.262364 1.18 180.631 137.088
252 0.470004 1.20036 182.072 137.652
253 0.530628 1.21596 183.55 138.297
254 0.587787 1.23724 185.081 139.025
255 0.587787 1.25357 186.653 139.761
256 0.587787 1.27588 188.28 140.511
257 0.693147 1.29303 189.952 141.408
258 0.693147 1.31652 191.686 142.32
259 0.693147 1.33462 193.467 143.245
260 0.741937 1.35946 195.315 144.254
261 0.916291 1.37866 197.216 145.517
262 0.916291 1.40507 199.19 146.805
263 0.955511 1.42554 201.222 148.167
264 1.09861 1.4538 203.336 149.764
265 1.09861 1.47579 205.514 151.385
266 1.09861 1.50626 207.782 153.04
267 1.16315 1.53007 210.123 154.82
268 1.38629 1.56322 212.567 156.987
269 1.66771 1.58927 215.093 159.637
270 1.94591 1.62576 217.736 162.801
271 1.94591 1.65463 220.474 166.021
272 2.07944 1.6954 223.348 169.546
273 2.19722 1.72793 226.334 173.343
274 2.19722 1.77438 229.482 177.241
275 2.30259 1.81191 232.765 181.414
276 2.30259 1.86629 236.248 185.711
277 2.48491 1.91103 239.9 190.46
278 2.77259 1.97737 243.81 195.942
279 2.89037 2.03352 247.946 201.82
280 3.13549 2.12007 252.44 208.467
281 3.21888 2.19728 257.268 215.54
282 3.52636 2.32634 262.68 223.743
283 4.04305 2.45727 268.718 233.678
284 4.09434 2.74777 276.269 244.929

Data Set Standard Deviation = 0.998224
Numerator = 59990
Denominator = 77906.5
W Statistic = 0.770025 = 59990 / 77906.5

5% Critical value of 0.976 exceeds 0.770025
Evidence of non-normality at 95% level of significance

1% Critical value of 0.967 exceeds 0.770025
Evidence of non-normality at 99% level of significance

Probability Plot
Parameter: Arsenic
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Probability Plot
Correlation Coefficient = 0.878963
0.878963 < 0.987 -- Normality test fails at 95% level

Plotted Data Points

Datum Value Prob. Quantile. x y
1 -1.60944 0.00350877 -2.74777 68.8501 348.683
2 -1.60944 0.00701754 -2.45727 68.8501 334.497
3 -1.60944 0.0105263 -2.32634 68.8501 328.103
4 -1.60944 0.0140351 -2.19728 68.8501 321.801
5 -1.60944 0.0175439 -2.12007 68.8501 318.03
6 -1.60944 0.0210526 -2.03352 68.8501 313.804
7 -1.60944 0.0245614 -1.97737 68.8501 311.062
8 -1.60944 0.0280702 -1.91103 68.8501 307.822
9 -1.60944 0.0315789 -1.86629 68.8501 305.637
10 -1.60944 0.0350877 -1.81191 68.8501 302.982
11 -1.60944 0.0385965 -1.77438 68.8501 301.149
12 -1.60944 0.0421053 -1.72793 68.8501 298.881
13 -1.60944 0.045614 -1.6954 68.8501 297.292
14 -1.60944 0.0491228 -1.65463 68.8501 295.301
15 -1.60944 0.0526316 -1.62576 68.8501 293.891
16 -1.60944 0.0561404 -1.58927 68.8501 292.109
17 -1.60944 0.0596491 -1.56322 68.8501 290.837
18 -1.60944 0.0631579 -1.53007 68.8501 289.218
19 -1.60944 0.0666667 -1.50626 68.8501 288.056
20 -1.60944 0.0701754 -1.47579 68.8501 286.568
21 -1.60944 0.0736842 -1.4538 68.8501 285.494
22 -1.60944 0.077193 -1.42554 68.8501 284.114
23 -1.60944 0.0807018 -1.40507 68.8501 283.114
24 -1.60944 0.0842105 -1.37866 68.8501 281.824
25 -1.60944 0.0877193 -1.35946 68.8501 280.887
26 -1.60944 0.0912281 -1.33462 68.8501 279.674
27 -1.60944 0.0947368 -1.31652 68.8501 278.79
28 -1.60944 0.0982456 -1.29303 68.8501 277.643
29 -1.60944 0.101754 -1.27588 68.8501 276.805
30 -1.60944 0.105263 -1.25357 68.8501 275.716
31 -1.60944 0.108772 -1.23724 68.8501 274.918
32 -1.60944 0.112281 -1.21596 68.8501 273.879
33 -1.60944 0.115789 -1.20036 68.8501 273.118
34 -1.60944 0.119298 -1.18 68.8501 272.123
35 -1.60944 0.122807 -1.16505 68.8501 271.393
36 -1.60944 0.126316 -1.1455 68.8501 270.439
37 -1.60944 0.129825 -1.13113 68.8501 269.737
38 -1.60944 0.133333 -1.11232 68.8501 268.818
39 -1.60944 0.136842 -1.09847 68.8501 268.142
40 -1.60944 0.140351 -1.08032 68.8501 267.256
41 -1.60944 0.14386 -1.06694 68.8501 266.602
42 -1.60944 0.147368 -1.04939 68.8501 265.745
43 -1.60944 0.150877 -1.03643 68.8501 265.112
44 -1.60944 0.154386 -1.01943 68.8501 264.282
45 -1.60944 0.157895 -1.00687 68.8501 263.669
46 -1.60944 0.161404 -0.990356 68.8501 262.862
47 -1.60944 0.164912 -0.97815 68.8501 262.266
48 -1.60944 0.168421 -0.9621 68.8501 261.483
49 -1.60944 0.17193 -0.950222 68.8501 260.903
50 -1.60944 0.175439 -0.93459 68.8501 260.139
51 -1.60944 0.178947 -0.923014 68.8501 259.574
52 -1.60944 0.182456 -0.907769 68.8501 258.829
53 -1.60944 0.185965 -0.896473 68.8501 258.278
54 -1.60944 0.189474 -0.881587 68.8501 257.551
55 -1.60944 0.192982 -0.87055 68.8501 257.012
56 -0.891598 0.196491 -0.855996 123.714 256.301
57 -0.867501 0.2 -0.841621 125.555 255.599
58 -0.84397 0.203509 -0.830953 127.354 255.078
59 -0.820981 0.207018 -0.816874 129.111 254.391
60 -0.776529 0.210526 -0.806422 132.508 253.88
61 -0.776529 0.214035 -0.792618 132.508 253.206
62 -0.776529 0.217544 -0.782366 132.508 252.706
63 -0.755023 0.221053 -0.768821 134.152 252.044
64 -0.755023 0.224561 -0.758753 134.152 251.552
65 -0.733969 0.22807 -0.745449 135.761 250.903
66 -0.71335 0.231579 -0.735557 137.337 250.42
67 -0.693147 0.235088 -0.722479 138.881 249.781
68 -0.653926 0.238596 -0.712751 141.878 249.306
69 -0.634878 0.242105 -0.699883 143.334 248.678
70 -0.616186 0.245614 -0.690309 144.763 248.21
71 -0.616186 0.249123 -0.677639 144.763 247.591
72 -0.616186 0.252632 -0.668209 144.763 247.131
73 -0.579818 0.25614 -0.655726 147.542 246.521
74 -0.562119 0.259649 -0.646431 148.895 246.067
75 -0.544727 0.263158 -0.634124 150.224 245.466
76 -0.527633 0.266667 -0.624956 151.531 245.019
77 -0.430783 0.270175 -0.612813 158.933 244.426
78 -0.314711 0.273684 -0.603765 167.804 243.984
79 -0.210721 0.277193 -0.591776 175.752 243.398
80 -0.174353 0.280702 -0.582841 178.532 242.962
81 0 0.284211 -0.570999 191.857 242.384
82 0 0.287719 -0.56217 191.857 241.953
83 0 0.291228 -0.550465 191.857 241.381
84 0 0.294737 -0.541736 191.857 240.955
85 0 0.298246 -0.530162 191.857 240.39
86 0 0.301754 -0.521527 191.857 239.968
87 0 0.305263 -0.510074 191.857 239.409
88 0 0.308772 -0.501527 191.857 238.991
89 0 0.312281 -0.490189 191.857 238.438
90 0 0.315789 -0.481728 191.857 238.024
91 0 0.319298 -0.470498 191.857 237.476
92 0 0.322807 -0.462114 191.857 237.067
93 0 0.326316 -0.450985 191.857 236.523
94 0 0.329825 -0.442676 191.857 236.117
95 0 0.333333 -0.431644 191.857 235.579
96 0 0.336842 -0.423405 191.857 235.176
97 0 0.340351 -0.412463 191.857 234.642
98 0 0.34386 -0.40429 191.857 234.243
99 0 0.347368 -0.393433 191.857 233.713
100 0 0.350877 -0.385321 191.857 233.317
101 0 0.354386 -0.374544 191.857 232.79
102 0 0.357895 -0.36649 191.857 232.397
103 0 0.361404 -0.355788 191.857 231.874
104 0 0.364912 -0.347787 191.857 231.484
105 0 0.368421 -0.337155 191.857 230.964
106 0 0.37193 -0.329206 191.857 230.576
107 0 0.375439 -0.318639 191.857 230.06
108 0 0.378947 -0.310738 191.857 229.674
109 0 0.382456 -0.300232 191.857 229.161
110 0 0.385965 -0.292375 191.857 228.778
111 0 0.389474 -0.281926 191.857 228.267
112 0 0.392982 -0.27411 191.857 227.886
113 0 0.396491 -0.263715 191.857 227.378
114 0 0.4 -0.253347 191.857 226.872
115 0 0.403509 -0.24559 191.857 226.493
116 0 0.407018 -0.235269 191.857 225.989
117 0 0.410526 -0.227545 191.857 225.612
118 0 0.414035 -0.217267 191.857 225.11
119 0 0.417544 -0.209575 191.857 224.734
120 0 0.421053 -0.199336 191.857 224.234
121 0 0.424561 -0.191671 191.857 223.86
122 0 0.42807 -0.181468 191.857 223.362
123 0 0.431579 -0.173829 191.857 222.989
124 0 0.435088 -0.163659 191.857 222.492
125 0 0.438596 -0.156042 191.857 222.12
126 0 0.442105 -0.1459 191.857 221.625
127 0 0.445614 -0.138305 191.857 221.254
128 0 0.449123 -0.128189 191.857 220.76
129 0 0.452632 -0.12061 191.857 220.39
130 0 0.45614 -0.110516 191.857 219.897
131 0 0.459649 -0.102953 191.857 219.528
132 0 0.463158 -0.0928787 191.857 219.036
133 0 0.466667 -0.0853288 191.857 218.667
134 0 0.470175 -0.0752698 191.857 218.176
135 0 0.473684 -0.0677301 191.857 217.807
136 0 0.477193 -0.0576847 191.857 217.317
137 0 0.480702 -0.0501541 191.857 216.949
138 0 0.484211 -0.0401167 191.857 216.459
139 0 0.487719 -0.0325917 191.857 216.092
140 0 0.491228 -0.0225612 191.857 215.602
141 0 0.494737 -0.0150408 191.857 215.234
142 0 0.498246 -0.00501359 191.857 214.745
143 0 0.501754 0.00501359 191.857 214.255
144 0 0.505263 0.0150408 191.857 213.766
145 0 0.508772 0.0225612 191.857 213.398
146 0 0.512281 0.0325917 191.857 212.908
147 0 0.515789 0.0401167 191.857 212.541
148 0 0.519298 0.0501541 191.857 212.051
149 0 0.522807 0.0576847 191.857 211.683
150 0 0.526316 0.0677301 191.857 211.193
151 0 0.529825 0.0752698 191.857 210.824
152 0 0.533333 0.0853288 191.857 210.333
153 0 0.536842 0.0928787 191.857 209.964
154 0 0.540351 0.102953 191.857 209.472
155 0 0.54386 0.110516 191.857 209.103
156 0 0.547368 0.12061 191.857 208.61
157 0 0.550877 0.128189 191.857 208.24
158 0 0.554386 0.138305 191.857 207.746
159 0 0.557895 0.1459 191.857 207.375
160 0 0.561404 0.156042 191.857 206.88
161 0 0.564912 0.163659 191.857 206.508
162 0 0.568421 0.173829 191.857 206.011
163 0 0.57193 0.181468 191.857 205.638
164 0 0.575439 0.191671 191.857 205.14
165 0 0.578947 0.199336 191.857 204.766
166 0 0.582456 0.209575 191.857 204.266
167 0 0.585965 0.217267 191.857 203.89
168 0 0.589474 0.227545 191.857 203.388
169 0 0.592982 0.235269 191.857 203.011
170 0 0.596491 0.24559 191.857 202.507
171 0 0.6 0.253347 191.857 202.128
172 0 0.603509 0.263715 191.857 201.622
173 0 0.607018 0.27411 191.857 201.114
174 0 0.610526 0.281926 191.857 200.733
175 0 0.614035 0.292375 191.857 200.222
176 0 0.617544 0.300232 191.857 199.839
177 0 0.621053 0.310738 191.857 199.326
178 0 0.624561 0.318639 191.857 198.94
179 0 0.62807 0.329206 191.857 198.424
180 0 0.631579 0.337155 191.857 198.036
181 0 0.635088 0.347787 191.857 197.516
182 0 0.638596 0.355788 191.857 197.126
183 0 0.642105 0.36649 191.857 196.603
184 0 0.645614 0.374544 191.857 196.21
185 0 0.649123 0.385321 191.857 195.683
186 0 0.652632 0.393433 191.857 195.287
187 0 0.65614 0.40429 191.857 194.757
188 0 0.659649 0.412463 191.857 194.358
189 0 0.663158 0.423405 191.857 193.824
190 0 0.666667 0.431644 191.857 193.421
191 0 0.670175 0.442676 191.857 192.883
192 0 0.673684 0.450985 191.857 192.477
193 0 0.677193 0.462114 191.857 191.933
194 0 0.680702 0.470498 191.857 191.524
195 0 0.684211 0.481728 191.857 190.976
196 0 0.687719 0.490189 191.857 190.562
197 0 0.691228 0.501527 191.857 190.009
198 0 0.694737 0.510074 191.857 189.591
199 0 0.698246 0.521527 191.857 189.032
200 0 0.701754 0.530162 191.857 188.61
201 0 0.705263 0.541736 191.857 188.045
202 0 0.708772 0.550465 191.857 187.619
203 0 0.712281 0.56217 191.857 187.047
204 0 0.715789 0.570999 191.857 186.616
205 0 0.719298 0.582841 191.857 186.038
206 0 0.722807 0.591776 191.857 185.602
207 0 0.726316 0.603765 191.857 185.016
208 0 0.729825 0.612813 191.857 184.574
209 0 0.733333 0.624956 191.857 183.981
210 0 0.736842 0.634124 191.857 183.534
211 0 0.740351 0.646431 191.857 182.933
212 0 0.74386 0.655726 191.857 182.479
213 0 0.747368 0.668209 191.857 181.869
214 0 0.750877 0.677639 191.857 181.409
215 0 0.754386 0.690309 191.857 180.79
216 0 0.757895 0.699883 191.857 180.322
217 0 0.761404 0.712751 191.857 179.694
218 0 0.764912 0.722479 191.857 179.219
219 0 0.768421 0.735557 191.857 178.58
220 0 0.77193 0.745449 191.857 178.097
221 0 0.775439 0.758753 191.857 177.448
222 0 0.778947 0.768821 191.857 176.956
223 0 0.782456 0.782366 191.857 176.294
224 0 0.785965 0.792618 191.857 175.794
225 0 0.789474 0.806422 191.857 175.12
226 0 0.792982 0.816874 191.857 174.609
227 0 0.796491 0.830953 191.857 173.922
228 0 0.8 0.841621 191.857 173.401
229 0 0.803509 0.855996 191.857 172.699
230 0 0.807018 0.87055 191.857 171.988
231 0 0.810526 0.881587 191.857 171.449
232 0 0.814035 0.896473 191.857 170.722
233 0 0.817544 0.907769 191.857 170.171
234 0 0.821053 0.923014 191.857 169.426
235 0 0.824561 0.93459 191.857 168.861
236 0 0.82807 0.950222 191.857 168.097
237 0 0.831579 0.9621 191.857 167.517
238 0 0.835088 0.97815 191.857 166.734
239 0 0.838596 0.990356 191.857 166.138
240 0 0.842105 1.00687 191.857 165.331
241 0 0.845614 1.01943 191.857 164.718
242 0 0.849123 1.03643 191.857 163.888
243 0 0.852632 1.04939 191.857 163.255
244 0 0.85614 1.06694 191.857 162.398
245 0.0953102 0.859649 1.08032 199.142 161.744
246 0.0953102 0.863158 1.09847 199.142 160.858
247 0.0953102 0.866667 1.11232 199.142 160.182
248 0.182322 0.870175 1.13113 205.792 159.263
249 0.182322 0.873684 1.1455 205.792 158.561
250 0.182322 0.877193 1.16505 205.792 157.607
251 0.262364 0.880702 1.18 211.909 156.877
252 0.470004 0.884211 1.20036 227.779 155.882
253 0.530628 0.887719 1.21596 232.412 155.121
254 0.587787 0.891228 1.23724 236.781 154.082
255 0.587787 0.894737 1.25357 236.781 153.284
256 0.587787 0.898246 1.27588 236.781 152.195
257 0.693147 0.901754 1.29303 244.833 151.357
258 0.693147 0.905263 1.31652 244.833 150.21
259 0.693147 0.908772 1.33462 244.833 149.326
260 0.741937 0.912281 1.35946 248.562 148.113
261 0.916291 0.915789 1.37866 261.888 147.176
262 0.916291 0.919298 1.40507 261.888 145.886
263 0.955511 0.922807 1.42554 264.886 144.886
264 1.09861 0.926316 1.4538 275.823 143.506
265 1.09861 0.929825 1.47579 275.823 142.432
266 1.09861 0.933333 1.50626 275.823 140.944
267 1.16315 0.936842 1.53007 280.755 139.782
268 1.38629 0.940351 1.56322 297.81 138.163
269 1.66771 0.94386 1.58927 319.318 136.891
270 1.94591 0.947368 1.62576 340.58 135.109
271 1.94591 0.950877 1.65463 340.58 133.699
272 2.07944 0.954386 1.6954 350.786 131.708
273 2.19722 0.957895 1.72793 359.788 130.119
274 2.19722 0.961404 1.77438 359.788 127.851
275 2.30259 0.964912 1.81191 367.84 126.018
276 2.30259 0.968421 1.86629 367.84 123.363
277 2.48491 0.97193 1.91103 381.775 121.178
278 2.77259 0.975439 1.97737 403.762 117.938
279 2.89037 0.978947 2.03352 412.764 115.196
280 3.13549 0.982456 2.12007 431.498 110.97
281 3.21888 0.985965 2.19728 437.871 107.199
282 3.52636 0.989474 2.32634 461.372 100.897
283 4.04305 0.992982 2.45727 500.862 94.5032
284 4.09434 0.996491 2.74777 504.782 80.3175

Kruskal-Wallis Non-Parametric Test
Parameter: Arsenic
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Kruskal Wallis Ranks

Background Locations

Loc. ID Date Value Rank
LMW-4 1/16/1998 ND<0 104 3/16/1999 ND<0 104 9/23/1999 ND<0 104
3/14/2000 ND<0 104 9/23/2003 ND<0 104 3/10/2004 ND<0 104
10/12/2004 ND<0 104 4/1/2005 ND<0 104 10/26/2005 ND<0 104
6/19/2006 ND<0 104 11/18/2006 ND<0 104 6/2/2007 0 J 233
11/15/2007 0 J 234 5/20/2008 ND<0 104 11/20/2008 ND<0 104
6/11/2009 ND<-1.60944 U 104 11/16/2009 ND<-1.60944 U 104
6/30/2010 ND<-1.60944 U 104 11/17/2010 ND<-1.60944 U 104 7/6/2011 ND<-1.60944 U 104
11/22/2011 ND<-1.60944 U 104 5/16/2012 ND<-1.60944 U 104 11/16/2012 ND<-1.60944 U 104
Rank Sum = 2651
Rank Mean = 115.261

Background Rank Sum = 2651
Background Rank Mean = 115.261

Compliance Locations

Loc. ID Date Value Rank
LMW-10 3/14/2000 3.13549 280 9/23/2003 ND<0 104
3/10/2004 3.21888 281 10/12/2004 ND<0 104
4/1/2005 ND<0 104 10/26/2005 ND<0 104 6/19/2006 ND<0 104
11/18/2006 ND<0 104 6/2/2007 0 J 235 11/15/2007 ND<0 104
5/20/2008 ND<0 104 11/20/2008 ND<0 104 6/11/2009 ND<-1.60944 U 104
11/16/2009 ND<-1.60944 U 104 6/30/2010 ND<-1.60944 U 104 11/17/2010 ND<-1.60944 U 104
7/6/2011 ND<-1.60944 U 104
11/22/2011 ND<-1.60944 U 104 5/16/2012 ND<-1.60944 U 104
11/16/2012 ND<-1.60944 U 104
Rank Sum = 2564
Rank Mean = 128.2

LMW-11 3/14/2000 2.48491 277 9/23/2003 ND<0 104
3/10/2004 2.89037 279 10/12/2004 ND<0 104
4/1/2005 ND<0 104 10/26/2005 ND<0 104 6/19/2006 ND<0 104
6/2/2007 ND<0 104 11/15/2007 ND<0 104 5/20/2008 ND<0 104
11/20/2008 ND<0 104
Rank Sum = 1492
Rank Mean = 135.636

LMW-12 3/14/2000 4.04305 283
9/23/2003 ND<0 104 3/10/2004 ND<0 104 10/12/2004 ND<0 104
4/1/2005 ND<0 104 10/26/2005 ND<0 104 6/19/2006 ND<0 104
6/2/2007 ND<0 104 11/15/2007 ND<0 104 5/20/2008 ND<0 104
11/20/2008 ND<0 104
Rank Sum = 1323
Rank Mean = 120.273

LMW-13 3/14/2000 2.77259 278
9/23/2003 ND<0 104 3/10/2004 ND<0 104 10/12/2004 ND<0 104
4/1/2005 ND<0 104 10/26/2005 ND<0 104 6/19/2006 ND<0 104
6/2/2007 ND<0 104 11/15/2007 ND<0 104 5/20/2008 ND<0 104
11/20/2008 ND<0 104
Rank Sum = 1318
Rank Mean = 119.818

LMW-14R 6/2/2007 0 J 236
11/15/2007 ND<0 104 5/20/2008 ND<0 104 11/20/2008 2.19722 273
6/11/2009 -0.891598 J 208 11/16/2009 ND<-1.60944 U 104 11/16/2009 ND<-1.60944 U 104
11/16/2009 -0.755023 J 215 6/30/2010 ND<-1.60944 U 104 11/17/2010 ND<-1.60944 U 104
7/6/2011 ND<-1.60944 U 104 11/22/2011 ND<-1.60944 U 104
5/16/2012 ND<-1.60944 U 104 11/16/2012 ND<-1.60944 U 104
Rank Sum = 1972
Rank Mean = 140.857

LMW-15R 11/18/2006 ND<0 104
6/2/2007 ND<0 104 11/15/2007 ND<0 104 11/15/2007 ND<0 104 5/20/2008 ND<0 104
5/20/2008 ND<0 104 11/20/2008 ND<0 104
11/20/2008 ND<0 104 6/11/2009 0.916291 261 6/30/2010 ND<-1.60944 U 104
11/17/2010 ND<-1.60944 U 104 7/6/2011 ND<-1.60944 U 104 11/22/2011 ND<-1.60944 U 104
5/16/2012 ND<-1.60944 U 104 11/16/2012 ND<-1.60944 U 104
Rank Sum = 1717
Rank Mean = 114.467

LMW-16 11/18/2006 ND<0 104 6/2/2007 0.693147 257 11/15/2007 ND<0 104
5/20/2008 ND<0 104 11/20/2008 2.19722 274 6/11/2009 -0.579818 J 225
11/16/2009 -0.527633 J 228 6/30/2010 -0.693147 J 219 11/17/2010 -0.616186 J 222
7/6/2011 0 237 11/22/2011 -0.616186 J 223 5/16/2012 0.587787 254
11/16/2012 0.0953102 245
Rank Sum = 2696
Rank Mean = 207.385

LMW-3 11/19/1996 ND<0 104
3/24/1997 ND<0 104 1/16/1998 ND<0 104 3/16/1999 ND<0 104
9/23/1999 ND<0 104 3/14/2000 ND<0 104 9/23/2003 ND<0 104
3/10/2004 ND<0 104 10/12/2004 ND<0 104 4/1/2005 ND<0 104
10/26/2005 ND<0 104 6/19/2006 ND<0 104
11/18/2006 ND<0 104 6/2/2007 ND<0 104 11/15/2007 ND<0 104
5/20/2008 ND<0 104 11/20/2008 ND<0 104 6/11/2009 -0.867501 J B 209
11/16/2009 ND<-1.60944 U 104 6/30/2010 ND<-1.60944 U 104 11/17/2010 -0.820981 J 211
7/6/2011 ND<-1.60944 U 104 11/22/2011 ND<-1.60944 U 104 5/16/2012 ND<-1.60944 U 104
11/16/2012 ND<-1.60944 U 104
Rank Sum = 2812
Rank Mean = 112.48

LMW-3S 11/18/2006 ND<0 104
6/2/2007 ND<0 104 11/15/2007 ND<0 104 5/20/2008 ND<0 104 11/20/2008 ND<0 104
6/11/2009 -0.314711 J B 230 11/16/2009 ND<-1.60944 U 104
6/30/2010 ND<-1.60944 U 104 11/17/2010 0 238 7/6/2011 -0.174353 J 232
11/22/2011 ND<-1.60944 U 104 5/16/2012 ND<-1.60944 U 104 11/16/2012 ND<-1.60944 U 104
Rank Sum = 1740
Rank Mean = 133.846

LMW-6 1/16/1998 ND<0 104 3/16/1999 ND<0 104
9/23/1999 ND<0 104 3/14/2000 ND<0 104 9/23/2003 ND<0 104
3/10/2004 ND<0 104 10/12/2004 ND<0 104 4/1/2005 ND<0 104
10/26/2005 ND<0 104 6/19/2006 ND<0 104 11/18/2006 ND<0 104
6/2/2007 0 J 239 11/15/2007 ND<0 104 5/20/2008 ND<0 104
11/20/2008 ND<0 104 6/11/2009 -0.430783 J B 229
11/16/2009 ND<-1.60944 U 104 6/30/2010 -0.776529 J 212 11/17/2010 -0.653926 J 220 7/6/2011 ND<-1.60944 U 104
11/22/2011 ND<-1.60944 U 104 5/16/2012 ND<-1.60944 U 104
11/16/2012 ND<-1.60944 U 104
Rank Sum = 2876
Rank Mean = 125.043

LMW-7 1/16/1998 ND<0 104 3/16/1999 ND<0 104
9/23/1999 ND<0 104 3/14/2000 2.30259 275
9/23/2003 ND<0 104 3/10/2004 ND<0 104 10/12/2004 ND<0 104
4/1/2005 ND<0 104 10/26/2005 ND<0 104 6/19/2006 ND<0 104
11/18/2006 ND<0 104 6/2/2007 0 J 240 11/15/2007 ND<0 104
5/20/2008 ND<0 104 11/20/2008 2.30259 276 6/11/2009 0.0953102 J B 246
11/17/2010 ND<-1.60944 U 104
7/6/2011 0.587787 255 11/22/2011 ND<-1.60944 U 104
5/16/2012 ND<-1.60944 U 104 11/16/2012 ND<-1.60944 U 104
Rank Sum = 2956
Rank Mean = 140.762

LMW-8 1/16/1998 ND<0 104
3/16/1999 ND<0 104 9/23/1999 ND<0 104
3/14/2000 ND<0 104 9/23/2003 ND<0 104 3/10/2004 ND<0 104
10/12/2004 ND<0 104 4/1/2005 ND<0 104 10/26/2005 ND<0 104
6/19/2006 ND<0 104 11/18/2006 ND<0 104 6/2/2007 ND<0 104
11/15/2007 ND<0 104 5/20/2008 ND<0 104 11/20/2008 ND<0 104
6/11/2009 -0.71335 J 218 11/16/2009 -0.634878 J 221 6/30/2010 -0.84397 J 210
11/17/2010 -0.733969 J 217 7/6/2011 -0.210721 J 231 11/22/2011 0.182322 248 5/16/2012 0.262364 251 11/16/2012 0.530628 253
Rank Sum = 3409
Rank Mean = 148.217

LMW-9 1/16/1998 ND<0 104 3/16/1999 ND<0 104
9/23/1999 1.09861 264 3/14/2000 ND<0 104 9/23/2003 ND<0 104 3/10/2004 ND<0 104
10/12/2004 ND<0 104 4/1/2005 0 J 241
10/26/2005 ND<0 104 6/19/2006 0 J 242 11/18/2006 ND<0 104
6/2/2007 0 J 243 11/15/2007 ND<0 104 5/20/2008 ND<0 104
11/20/2008 2.07944 272 6/11/2009 0.0953102 J 247 11/16/2009 ND<-1.60944 U 104
6/30/2010 -0.544727 J 227 11/17/2010 0.470004 252 7/6/2011 ND<-1.60944 U 104
11/22/2011 ND<-1.60944 U 104 5/16/2012 ND<-1.60944 U 104
11/16/2012 ND<-1.60944 U 104
Rank Sum = 3548
Rank Mean = 154.261

LMW-9D 11/18/2006 1.94591 270 6/2/2007 1.94591 271
11/15/2007 ND<0 104
5/20/2008 1.09861 265 11/20/2008 1.09861 266
6/11/2009 0.741937 260 11/16/2009 0.693147 258 6/30/2010 0.587787 256
11/17/2010 0.693147 259 7/6/2011 1.16315 267 11/22/2011 0.916291 262
5/16/2012 0.955511 263 11/16/2012 1.66771 269
Rank Sum = 3270
Rank Mean = 251.538

LMW-9S 11/18/2006 ND<0 104 6/2/2007 0 J 244 11/15/2007 1.38629 268
5/20/2008 ND<0 104 11/20/2008 ND<0 104 6/11/2009 -0.776529 J 213
6/30/2010 -0.562119 J 226 11/17/2010 0.182322 249 7/6/2011 -0.776529 J 214
11/22/2011 -0.755023 J 216 5/16/2012 -0.616186 J 224 11/16/2012 0.182322 250
Rank Sum = 2416
Rank Mean = 201.333

MW-5 1/16/1998 ND<0 104 3/16/1999 ND<0 104
9/23/1999 ND<0 104 3/14/2000 3.52636 282 9/23/2003 ND<0 104
3/10/2004 4.09434 284 10/12/2004 ND<0 104
4/1/2005 ND<0 104 10/26/2005 ND<0 104 6/19/2006 ND<0 104 11/15/2007 ND<0 104
5/20/2008 ND<0 104 11/20/2008 ND<0 104
Rank Sum = 1710
Rank Mean = 131.538

Calculation Results:
Kruskal-Wallis H Statistic = 49.1464
Kruskal-Wallis H Statistic (adjusted for tied non-detects) = 80.2016
95% Confidence comparison value is 26.2962 at 16 degrees of freedom
49.1464 > 26.2962 indicating a significant group difference at 5% significance level
80.2016 > 26.2962 indicating a significant group difference at 5% significance level when adjusted for ties

Individual Well Comparisons at 1% Significance Level per Comparison
1% Z score is 2.32634
Mean background rank is 115.261
Well Mean Rank Dif from Bkg Critical Value
LMW-10 128.2 12.9391 58.4144
LMW-11 135.636 20.3755 70.0396
LMW-12 120.273 5.01186 70.0396
LMW-13 119.818 4.55731 70.0396
LMW-14R 140.857 25.5963 64.7646
LMW-15R 114.467 -0.794203 63.4084
LMW-16 207.385 92.1237 66.2949
LMW-3 112.48 -2.78087 55.2015
LMW-3S 133.846 18.5853 66.2949
LMW-6 125.043 9.78261 56.3398
LMW-7 140.762 25.501 57.6657
LMW-8 148.217 32.9565 56.3398
LMW-9 154.261 39 56.3398
LMW-9D251.538 136.278 66.2949
LMW-9S 201.333 86.0725 68.0368
MW-5 131.538 16.2776 66.2949

Individual Well Comparisons at Groupwise 5% Significance Level
(0.3125% Significance Level per comparison)
0.3125% Z score is 2.74777
Mean background rank is 115.261
Well Mean Rank Dif from Bkg Critical Value
LMW-10 128.2 12.9391 68.9963
LMW-11 135.636 20.3755 82.7275
LMW-12 120.273 5.01186 82.7275
LMW-13 119.818 4.55731 82.7275
LMW-14R 140.857 25.5963 76.4969
LMW-15R 114.467 -0.794203 74.895
LMW-16 207.385 92.1237 78.3044
LMW-3 112.48 -2.78087 65.2015
LMW-3S 133.846 18.5853 78.3044
LMW-6 125.043 9.78261 66.546
LMW-7 140.762 25.501 68.112
LMW-8 148.217 32.9565 66.546
LMW-9 154.261 39 66.546
LMW-9D251.538 136.278 78.3044
LMW-9S 201.333 86.0725 80.3619
MW-5 131.538 16.2776 78.3044

Mann-Kendall Trend Analysis
Parameter: Arsenic
Location: LMW-16
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

95% Confidence Level

Xj Xk Xj - Xk Positives Negatives
0.693147 ND<0 0.693147 1 0
ND<0 ND<0 0 1 0
ND<0 ND<0 0 1 0
2.19722 ND<0 2.19722 2 0
-0.579818 J ND<0 -0.579818 2 1
-0.527633 J ND<0 -0.527633 2 2
-0.693147 J ND<0 -0.693147 2 3
-0.616186 J ND<0 -0.616186 2 4
0 ND<0 0 2 4
-0.616186 J ND<0 -0.616186 2 5
0.587787 ND<0 0.587787 3 5
0.0953102 ND<0 0.0953102 4 5

ND<0 0.693147 -0.693147 4 6
ND<0 0.693147 -0.693147 4 7
2.19722 0.693147 1.50408 5 7
-0.579818 J 0.693147 -1.27297 5 8
-0.527633 J 0.693147 -1.22078 5 9
-0.693147 J 0.693147 -1.38629 5 10
-0.616186 J 0.693147 -1.30933 5 11
0 0.693147 -0.693147 5 12
-0.616186 J 0.693147 -1.30933 5 13
0.587787 0.693147 -0.105361 5 14
0.0953102 0.693147 -0.597837 5 15

ND<0 ND<0 0 5 15
2.19722 ND<0 2.19722 6 15
-0.579818 J ND<0 -0.579818 6 16
-0.527633 J ND<0 -0.527633 6 17
-0.693147 J ND<0 -0.693147 6 18
-0.616186 J ND<0 -0.616186 6 19
0 ND<0 0 6 19
-0.616186 J ND<0 -0.616186 6 20
0.587787 ND<0 0.587787 7 20
0.0953102 ND<0 0.0953102 8 20

2.19722 ND<0 2.19722 9 20
-0.579818 J ND<0 -0.579818 9 21
-0.527633 J ND<0 -0.527633 9 22
-0.693147 J ND<0 -0.693147 9 23
-0.616186 J ND<0 -0.616186 9 24
0 ND<0 0 9 24
-0.616186 J ND<0 -0.616186 9 25
0.587787 ND<0 0.587787 10 25
0.0953102 ND<0 0.0953102 11 25

-0.579818 J 2.19722 -2.77704 11 26
-0.527633 J 2.19722 -2.72486 11 27
-0.693147 J 2.19722 -2.89037 11 28
-0.616186 J 2.19722 -2.81341 11 29
0 2.19722 -2.19722 11 30
-0.616186 J 2.19722 -2.81341 11 31
0.587787 2.19722 -1.60944 11 32
0.0953102 2.19722 -2.10191 11 33

-0.527633 J -0.579818 J 0.0521858 12 33
-0.693147 J -0.579818 J -0.113329 12 34
-0.616186 J -0.579818 J -0.0363676 12 35
0 -0.579818 J 0.579818 13 35
-0.616186 J -0.579818 J -0.0363676 13 36
0.587787 -0.579818 J 1.16761 14 36
0.0953102 -0.579818 J 0.675129 15 36

-0.693147 J -0.527633 J -0.165514 15 37
-0.616186 J -0.527633 J -0.0885534 15 38
0 -0.527633 J 0.527633 16 38
-0.616186 J -0.527633 J -0.0885534 16 39
0.587787 -0.527633 J 1.11542 17 39
0.0953102 -0.527633 J 0.622943 18 39

-0.616186 J -0.693147 J 0.076961 19 39
0 -0.693147 J 0.693147 20 39
-0.616186 J -0.693147 J 0.076961 21 39
0.587787 -0.693147 J 1.28093 22 39
0.0953102 -0.693147 J 0.788457 23 39

0 -0.616186 J 0.616186 24 39
-0.616186 J -0.616186 J 0 24 39
0.587787 -0.616186 J 1.20397 25 39
0.0953102 -0.616186 J 0.711496 26 39

-0.616186 J 0 -0.616186 26 40
0.587787 0 0.587787 27 40
0.0953102 0 0.0953102 28 40

0.587787 -0.616186 J 1.20397 29 40
0.0953102 -0.616186 J 0.711496 30 40

0.0953102 0.587787 -0.492476 30 41

S Statistic = 30 - 41 = -11

Tied Group Value Members
1 0 4
2 -0.616186 2

Time Period Observations
11/18/2006 1
6/2/2007 1
11/15/2007 1
5/20/2008 1
11/20/2008 1
6/11/2009 1
11/16/2009 1
6/30/2010 1
11/17/2010 1
7/6/2011 1
11/22/2011 1
5/16/2012 1
11/16/2012 1
There are 0 time periods with multiple data

A = 174
B = 0
C = 24
D = 0
E = 14
F = 0
a = 4836
b = 15444
c = 312
Group Variance = 259
Z-Score = -0.62137
Comparison Level at 1.0 - (0.05 / 2) = 97.5% confidence level = 1.97737 (two-tailed)
|-0.62137| <= 1.97737 indicating no evidence of a trend

Mann-Kendall Trend Analysis
Parameter: Arsenic
Location: LMW-9D
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

95% Confidence Level

Xj Xk Xj - Xk Positives Negatives
1.94591 1.94591 0 0 0
ND<0 1.94591 -1.94591 0 1
1.09861 1.94591 -0.847298 0 2
1.09861 1.94591 -0.847298 0 3
0.741937 1.94591 -1.20397 0 4
0.693147 1.94591 -1.25276 0 5
0.587787 1.94591 -1.35812 0 6
0.693147 1.94591 -1.25276 0 7
1.16315 1.94591 -0.782759 0 8
0.916291 1.94591 -1.02962 0 9
0.955511 1.94591 -0.990399 0 10
1.66771 1.94591 -0.278203 0 11

ND<0 1.94591 -1.94591 0 12
1.09861 1.94591 -0.847298 0 13
1.09861 1.94591 -0.847298 0 14
0.741937 1.94591 -1.20397 0 15
0.693147 1.94591 -1.25276 0 16
0.587787 1.94591 -1.35812 0 17
0.693147 1.94591 -1.25276 0 18
1.16315 1.94591 -0.782759 0 19
0.916291 1.94591 -1.02962 0 20
0.955511 1.94591 -0.990399 0 21
1.66771 1.94591 -0.278203 0 22

1.09861 ND<0 1.09861 1 22
1.09861 ND<0 1.09861 2 22
0.741937 ND<0 0.741937 3 22
0.693147 ND<0 0.693147 4 22
0.587787 ND<0 0.587787 5 22
0.693147 ND<0 0.693147 6 22
1.16315 ND<0 1.16315 7 22
0.916291 ND<0 0.916291 8 22
0.955511 ND<0 0.955511 9 22
1.66771 ND<0 1.66771 10 22

1.09861 1.09861 0 10 22
0.741937 1.09861 -0.356675 10 23
0.693147 1.09861 -0.405465 10 24
0.587787 1.09861 -0.510826 10 25
0.693147 1.09861 -0.405465 10 26
1.16315 1.09861 0.0645385 11 26
0.916291 1.09861 -0.182322 11 27
0.955511 1.09861 -0.143101 11 28
1.66771 1.09861 0.569095 12 28

0.741937 1.09861 -0.356675 12 29
0.693147 1.09861 -0.405465 12 30
0.587787 1.09861 -0.510826 12 31
0.693147 1.09861 -0.405465 12 32
1.16315 1.09861 0.0645385 13 32
0.916291 1.09861 -0.182322 13 33
0.955511 1.09861 -0.143101 13 34
1.66771 1.09861 0.569095 14 34

0.693147 0.741937 -0.0487902 14 35
0.587787 0.741937 -0.154151 14 36
0.693147 0.741937 -0.0487902 14 37
1.16315 0.741937 0.421213 15 37
0.916291 0.741937 0.174353 16 37
0.955511 0.741937 0.213574 17 37
1.66771 0.741937 0.925769 18 37

0.587787 0.693147 -0.105361 18 38
0.693147 0.693147 0 18 38
1.16315 0.693147 0.470004 19 38
0.916291 0.693147 0.223144 20 38
0.955511 0.693147 0.262364 21 38
1.66771 0.693147 0.97456 22 38

0.693147 0.587787 0.105361 23 38
1.16315 0.587787 0.575364 24 38
0.916291 0.587787 0.328504 25 38
0.955511 0.587787 0.367725 26 38
1.66771 0.587787 1.07992 27 38

1.16315 0.693147 0.470004 28 38
0.916291 0.693147 0.223144 29 38
0.955511 0.693147 0.262364 30 38
1.66771 0.693147 0.97456 31 38

0.916291 1.16315 -0.24686 31 39
0.955511 1.16315 -0.207639 31 40
1.66771 1.16315 0.504556 32 40

0.955511 0.916291 0.0392207 33 40
1.66771 0.916291 0.751416 34 40

1.66771 0.955511 0.712195 35 40

S Statistic = 35 - 40 = -5

Tied Group Value Members
1 1.94591 2
2 1.09861 2
3 0.693147 2

Time Period Observations
11/18/2006 1
6/2/2007 1
11/15/2007 1
5/20/2008 1
11/20/2008 1
6/11/2009 1
11/16/2009 1
6/30/2010 1
11/17/2010 1
7/6/2011 1
11/22/2011 1
5/16/2012 1
11/16/2012 1
There are 0 time periods with multiple data

A = 54
B = 0
C = 0
D = 0
E = 6
F = 0
a = 4836
b = 15444
c = 312
Group Variance = 265.667
Z-Score = -0.24541
Comparison Level at 1.0 - (0.05 / 2) = 97.5% confidence level = 1.97737 (two-tailed)
|-0.24541| <= 1.97737 indicating no evidence of a trend

Mann-Kendall Trend Analysis
Parameter: Arsenic
Location: LMW-9S
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

95% Confidence Level

Xj Xk Xj - Xk Positives Negatives
0 J ND<0 0 0 0
1.38629 ND<0 1.38629 1 0
ND<0 ND<0 0 1 0
ND<0 ND<0 0 1 0
-0.776529 J ND<0 -0.776529 1 1
-0.562119 J ND<0 -0.562119 1 2
0.182322 ND<0 0.182322 2 2
-0.776529 J ND<0 -0.776529 2 3
-0.755023 J ND<0 -0.755023 2 4
-0.616186 J ND<0 -0.616186 2 5
0.182322 ND<0 0.182322 3 5

1.38629 0 J 1.38629 4 5
ND<0 0 J 0 4 5
ND<0 0 J 0 4 5
-0.776529 J 0 J -0.776529 4 6
-0.562119 J 0 J -0.562119 4 7
0.182322 0 J 0.182322 5 7
-0.776529 J 0 J -0.776529 5 8
-0.755023 J 0 J -0.755023 5 9
-0.616186 J 0 J -0.616186 5 10
0.182322 0 J 0.182322 6 10

ND<0 1.38629 -1.38629 6 11
ND<0 1.38629 -1.38629 6 12
-0.776529 J 1.38629 -2.16282 6 13
-0.562119 J 1.38629 -1.94841 6 14
0.182322 1.38629 -1.20397 6 15
-0.776529 J 1.38629 -2.16282 6 16
-0.755023 J 1.38629 -2.14132 6 17
-0.616186 J 1.38629 -2.00248 6 18
0.182322 1.38629 -1.20397 6 19

ND<0 ND<0 0 6 19
-0.776529 J ND<0 -0.776529 6 20
-0.562119 J ND<0 -0.562119 6 21
0.182322 ND<0 0.182322 7 21
-0.776529 J ND<0 -0.776529 7 22
-0.755023 J ND<0 -0.755023 7 23
-0.616186 J ND<0 -0.616186 7 24
0.182322 ND<0 0.182322 8 24

-0.776529 J ND<0 -0.776529 8 25
-0.562119 J ND<0 -0.562119 8 26
0.182322 ND<0 0.182322 9 26
-0.776529 J ND<0 -0.776529 9 27
-0.755023 J ND<0 -0.755023 9 28
-0.616186 J ND<0 -0.616186 9 29
0.182322 ND<0 0.182322 10 29

-0.562119 J -0.776529 J 0.21441 11 29
0.182322 -0.776529 J 0.95885 12 29
-0.776529 J -0.776529 J 0 12 29
-0.755023 J -0.776529 J 0.0215062 13 29
-0.616186 J -0.776529 J 0.160343 14 29
0.182322 -0.776529 J 0.95885 15 29

0.182322 -0.562119 J 0.74444 16 29
-0.776529 J -0.562119 J -0.21441 16 30
-0.755023 J -0.562119 J -0.192904 16 31
-0.616186 J -0.562119 J -0.0540672 16 32
0.182322 -0.562119 J 0.74444 17 32

-0.776529 J 0.182322 -0.95885 17 33
-0.755023 J 0.182322 -0.937344 17 34
-0.616186 J 0.182322 -0.798508 17 35
0.182322 0.182322 0 17 35

-0.755023 J -0.776529 J 0.0215062 18 35
-0.616186 J -0.776529 J 0.160343 19 35
0.182322 -0.776529 J 0.95885 20 35

-0.616186 J -0.755023 J 0.138836 21 35
0.182322 -0.755023 J 0.937344 22 35

0.182322 -0.616186 J 0.798508 23 35

S Statistic = 23 - 35 = -12

Tied Group Value Members
1 0 4
2 -0.776529 2
3 0.182322 2

Time Period Observations
11/18/2006 1
6/2/2007 1
11/15/2007 1
5/20/2008 1
11/20/2008 1
6/11/2009 1
6/30/2010 1
11/17/2010 1
7/6/2011 1
11/22/2011 1
5/16/2012 1
11/16/2012 1
There are 0 time periods with multiple data

A = 192
B = 0
C = 24
D = 0
E = 16
F = 0
a = 3828
b = 11880
c = 264
Group Variance = 202
Z-Score = -0.773957
Comparison Level at 1.0 - (0.05 / 2) = 97.5% confidence level = 1.97737 (two-tailed)
|-0.773957| <= 1.97737 indicating no evidence of a trend

Shewhart-CUSUM Control Chart
Parameter: Arsenic
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Baseline mean = -0.559804
Baseline Std Dev = 0.783772
k = 1
h = 5
SCL = 4.5

Date Value CuSum Std Mean
11/18/2006 1.94591 2.197 3.197
11/18/2006 1.94591 2.197 3.197
6/2/2007 1.94591 4.39399 3.197
6/2/2007 1.94591 4.39399 3.197
11/15/2007 0 4.10824 0.714244
11/15/2007 0 4.10824 0.714244
5/20/2008 1.09861 5.22418 2.11594
5/20/2008 1.09861 5.22418 2.11594
11/20/2008 1.09861 6.34012 2.11594
11/20/2008 1.09861 6.34012 2.11594
6/11/2009 0.741937 7.00099 1.66087
6/11/2009 0.741937 7.00099 1.66087
11/16/2009 0.693147 7.59961 1.59862
11/16/2009 0.693147 7.59961 1.59862
6/30/2010 0.587787 8.0638 1.46419
6/30/2010 0.587787 8.0638 1.46419
11/17/2010 0.693147 8.66242 1.59862
11/17/2010 0.693147 8.66242 1.59862
7/6/2011 1.16315 9.8607 2.19829
7/6/2011 1.16315 9.8607 2.19829
11/22/2011 0.916291 10.744 1.88332
11/22/2011 0.916291 10.744 1.88332
5/16/2012 0.955511 11.6774 1.93336
5/16/2012 0.955511 11.6774 1.93336
11/16/2012 1.66771 13.5194 2.84204
11/16/2012 1.66771 13.5194 2.84204
Shewhart-CUSUM Control Chart
Parameter: Arsenic
Natural Logarithm Transformation
Non-Detects Replaced with 1/2 DL

Baseline mean = -0.559804
Baseline Std Dev = 0.783772
k = 1
h = 5
SCL = 4.5

Date Value CuSum Std Mean
11/18/2006 0 0 0.714244
11/18/2006 0 0 0.714244
6/2/2007 0 0 0.714244
6/2/2007 0 0 0.714244
11/15/2007 1.38629 1.48299 2.48299
11/15/2007 1.38629 1.48299 2.48299
5/20/2008 0 1.19724 0.714244
5/20/2008 0 1.19724 0.714244
11/20/2008 0 0.911481 0.714244
11/20/2008 0 0.911481 0.714244
6/11/2009 -0.776529 0 -0.276515
6/11/2009 -0.776529 0 -0.276515
6/30/2010 -0.562119 0 -0.00295293
6/30/2010 -0.562119 0 -0.00295293
11/17/2010 0.182322 0 0.946865
11/17/2010 0.182322 0 0.946865
7/6/2011 -0.776529 0 -0.276515
7/6/2011 -0.776529 0 -0.276515
11/22/2011 -0.755023 0 -0.249075
11/22/2011 -0.755023 0 -0.249075
5/16/2012 -0.616186 0 -0.0719363
5/16/2012 -0.616186 0 -0.0719363
11/16/2012 0.182322 0 0.946865
11/16/2012 0.182322 0 0.946865
Concentrations (ppb)
Parameter: Barium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements: 284
Total Non-Detect: 88
Percent Non-Detects: 30.9859%
Total Background Measurements: 23
There is 1 background location

Loc. Meas. ND Date Conc. Original

LMW-4 23 5 (21.7391%) 1/16/1998 ND<10 ND<10 3/16/1999 20 20 9/23/1999 8 J 8 J 3/14/2000 ND<10 ND<10
9/23/2003 ND<10 ND<10 3/10/2004 ND<10 ND<10
10/12/2004 ND<10 ND<10 4/1/2005 14 14 10/26/2005 12 12
6/19/2006 10 10 11/18/2006 13 13 6/2/2007 24 24
11/15/2007 13 13 5/20/2008 11 11 11/20/2008 14 14
6/11/2009 13 13 11/16/2009 13 13 6/30/2010 15 15
11/17/2010 14 14 7/6/2011 14 14
11/22/2011 16 16 5/16/2012 15 15 11/16/2012 13 13

There are 16 compliance locations

Loc. Meas. ND Date Conc. Original

LMW-10 20 6 (30%) 3/14/2000 ND<10 ND<10
9/23/2003 ND<10 ND<10 3/10/2004 ND<10 ND<10 10/12/2004 ND<10 ND<10
4/1/2005 13 13 10/26/2005 ND<10 ND<10 6/19/2006 20 20
11/18/2006 11 11 6/2/2007 21 21 11/15/2007 ND<10 ND<10
5/20/2008 12 12 11/20/2008 12 12 6/11/2009 13 13
11/16/2009 12 12 6/30/2010 12 12
11/17/2010 14 14 7/6/2011 21 21 11/22/2011 23 23 5/16/2012 23 23
11/16/2012 25 25

LMW-11 11 11 (100%) 3/14/2000 ND<10 ND<10
9/23/2003 ND<10 ND<10 3/10/2004 ND<10 ND<10
10/12/2004 ND<10 ND<10 4/1/2005 ND<10 ND<10 10/26/2005 ND<10 ND<10 6/19/2006 ND<10 ND<10
6/2/2007 ND<10 ND<10 11/15/2007 ND<10 ND<10
5/20/2008 ND<10 ND<10 11/20/2008 ND<10 ND<10

LMW-12 11 11 (100%) 3/14/2000 ND<10 ND<10 9/23/2003 ND<10 ND<10 3/10/2004 ND<10 ND<10
10/12/2004 ND<10 ND<10 4/1/2005 ND<10 ND<10
10/26/2005 ND<10 ND<10 6/19/2006 ND<10 ND<10 6/2/2007 ND<10 ND<10
11/15/2007 ND<10 ND<10 5/20/2008 ND<10 ND<10 11/20/2008 ND<10 ND<10

LMW-13 11 11 (100%) 3/14/2000 ND<10 ND<10 9/23/2003 ND<10 ND<10
3/10/2004 ND<10 ND<10 10/12/2004 ND<10 ND<10
4/1/2005 ND<10 ND<10 10/26/2005 ND<10 ND<10 6/19/2006 ND<10 ND<10
6/2/2007 ND<10 ND<10 11/15/2007 ND<10 ND<10 5/20/2008 ND<10 ND<10
11/20/2008 ND<10 ND<10

LMW-14R 14 0 (0%) 6/2/2007 14 14
11/15/2007 12 12 5/20/2008 9 J 9 J
11/20/2008 13 13 6/11/2009 13 13 11/16/2009 48 48
11/16/2009 14 14 11/16/2009 12 12 6/30/2010 13 13
11/17/2010 12 12 7/6/2011 11 11 11/22/2011 14 14
5/16/2012 13 13 11/16/2012 13 13

LMW-15R 15 3 (20%) 11/18/2006 37 37 6/2/2007 38 38
11/15/2007 ND<10 ND<10 11/15/2007 27 27 5/20/2008 ND<10 ND<10
5/20/2008 24 24 11/20/2008 ND<10 ND<10 11/20/2008 38 38
6/11/2009 42 42 6/30/2010 36 36
11/17/2010 30 30 7/6/2011 25 25
11/22/2011 32 32 5/16/2012 32 32 11/16/2012 30 30

LMW-16 13 0 (0%) 11/18/2006 23 23 6/2/2007 41 41
11/15/2007 35 35 5/20/2008 22 22
11/20/2008 23 23 6/11/2009 14 14 11/16/2009 13 13
6/30/2010 8.8 8.8 11/17/2010 10 10 7/6/2011 11 11
11/22/2011 8.8 8.8 5/16/2012 9.2 9.2 11/16/2012 9.2 9.2

LMW-3 25 9 (36%) 11/19/1996 ND<10 ND<10
3/24/1997 ND<10 ND<10 1/16/1998 ND<10 ND<10 3/16/1999 8 J 8 J
9/23/1999 7 J 7 J 3/14/2000 ND<10 ND<10 9/23/2003 ND<10 ND<10
3/10/2004 ND<10 ND<10 10/12/2004 ND<10 ND<10 4/1/2005 ND<10 ND<10
10/26/2005 7 J 7 J 6/19/2006 5 J 5 J 11/18/2006 7 J 7 J
6/2/2007 5 5 11/15/2007 ND<10 ND<10
5/20/2008 5 J 5 J 11/20/2008 5 J 5 J 6/11/2009 7.2 7.2 11/16/2009 6.4 6.4
6/30/2010 5 5 11/17/2010 13 13
7/6/2011 3.5 3.5 11/22/2011 12 12 5/16/2012 4.6 4.6
11/16/2012 4.5 4.5

LMW-3S 13 0 (0%) 11/18/2006 5 J 5 J
6/2/2007 18 18 11/15/2007 13 13
5/20/2008 8 J 8 J 11/20/2008 13 13 6/11/2009 12 12
11/16/2009 10 10 6/30/2010 12 12 11/17/2010 16 16
7/6/2011 14 14 11/22/2011 5.4 5.4 5/16/2012 13 13
11/16/2012 14 14

LMW-6 23 5 (21.7391%) 1/16/1998 ND<10 ND<10 3/16/1999 8 J 8 J
9/23/1999 18 18 3/14/2000 ND<10 ND<10
9/23/2003 ND<10 ND<10 3/10/2004 ND<10 ND<10 10/12/2004 ND<10 ND<10
4/1/2005 9 J 9 J 10/26/2005 12 12 6/19/2006 20 20
11/18/2006 33 33 6/2/2007 52 52 11/15/2007 42 42
5/20/2008 49 49 11/20/2008 73 73 6/11/2009 92 92
11/16/2009 74 74 6/30/2010 77 77
11/17/2010 79 79 7/6/2011 55 55 11/22/2011 44 J 44 J
5/16/2012 36 36 11/16/2012 33 33

LMW-7 21 5 (23.8095%) 1/16/1998 ND<10 ND<10 3/16/1999 20 20 9/23/1999 22 22
3/14/2000 ND<10 ND<10 9/23/2003 ND<10 ND<10 3/10/2004 ND<10 ND<10 10/12/2004 ND<10 ND<10 4/1/2005 31 31
10/26/2005 30 30 6/19/2006 20 20 11/18/2006 11 11
6/2/2007 27 27 11/15/2007 6 J 6 J 5/20/2008 5 J 5 J
11/20/2008 7 J 7 J 6/11/2009 12 12 11/17/2010 5.2 5.2
7/6/2011 13 13 11/22/2011 8.5 8.5 5/16/2012 7.6 7.6
11/16/2012 6.9 6.9

LMW-8 23 5 (21.7391%) 1/16/1998 ND<10 ND<10 3/16/1999 10 10 9/23/1999 109 109
3/14/2000 ND<10 ND<10 9/23/2003 ND<10 ND<10 3/10/2004 ND<10 ND<10
10/12/2004 ND<10 ND<10 4/1/2005 48 48 10/26/2005 38 38
6/19/2006 40 40 11/18/2006 32 32
6/2/2007 34 34 11/15/2007 41 41 5/20/2008 34 34
11/20/2008 29 29 6/11/2009 40 40 11/16/2009 40 40
6/30/2010 30 30
11/17/2010 44 44 7/6/2011 32 32
11/22/2011 45 45 5/16/2012 39 39 11/16/2012 38 38

LMW-9 23 7 (30.4348%) 1/16/1998 ND<10 ND<10 3/16/1999 10 10
9/23/1999 22 22 3/14/2000 ND<10 ND<10
9/23/2003 ND<10 ND<10 3/10/2004 ND<10 ND<10 10/12/2004 ND<10 ND<10
4/1/2005 ND<10 ND<10 10/26/2005 ND<10 ND<10 6/19/2006 10 10
11/18/2006 3 J 3 J 6/2/2007 6 6 11/15/2007 3 J 3 J
5/20/2008 2 J 2 J 11/20/2008 4 J 4 J 6/11/2009 3.1 3.1
11/16/2009 2.9 2.9 6/30/2010 2.8 2.8 11/17/2010 4 4
7/6/2011 3.3 3.3 11/22/2011 3.4 3.4 5/16/2012 13 13 11/16/2012 21 21

LMW-9D 13 0 (0%) 11/18/2006 13 13 6/2/2007 5 5 11/15/2007 120 120
5/20/2008 10 10 11/20/2008 3 J 3 J
6/11/2009 3.1 3.1 11/16/2009 2.9 2.9 6/30/2010 2.1 2.1 11/17/2010 2.8 2.8
7/6/2011 3.8 3.8 11/22/2011 2.8 2.8
5/16/2012 2.5 2.5 11/16/2012 1.9 1.9

LMW-9S 12 0 (0%) 11/18/2006 77 77 6/2/2007 80 80 11/15/2007 2 J 2 J
5/20/2008 75 75 11/20/2008 61 61
6/11/2009 28 28 6/30/2010 38 38 11/17/2010 53 53
7/6/2011 59 59 11/22/2011 66 66 5/16/2012 39 39
11/16/2012 68 68

MW-5 13 10 (76.9231%) 1/16/1998 ND<10 ND<10
3/16/1999 20 20 9/23/1999 9 J 9 J
3/14/2000 ND<10 ND<10 9/23/2003 ND<10 ND<10