SW_F_1803-CDLF-_09-16-2014_RM_GW.pdf

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TABLEOFCONTENTS
EXECUTIVESUMMARY……………………………………..……..…………..1
1.0 INTRODUCTION……………………………………………………………......6
2.0 SITEDESCRIPTION….………………………………………………………......7
2.1PhysicalSetting…………………………………………………………………7
2.2GeologyandHydrogeology……………………….………………….….…….7
2.3MonitoringNetwork………………………….………………..………….8
3.0 HYDROLOGICEVALUATION………………………………………………….8
3.1StaticWaterLevelsandGroundwater Elevations ...……………………….8
3.2GroundwaterFlowRateandDirection ..…………………………………....8
4.0 SAMPLINGANDLABORATORYANALYSIS……………….……………….10
4.1FieldSamplingSummary…………..………………………………………….10
4.2LaboratoryAnalysisSummary .……………………………………………....11
4.3QualityAssurance/QualityControl…....………………………………….12
4.4AnalyticalResults ..…………………………………………………………….12
5.0 FINDINGSANDCONCLUSIONS ..…………….……………….……………….15
5.1SummaryofFindings ..….…………..………………………………………….15
5.2Conclusions…….……………….……………………………………………....15
FIGURES
GroundwaterPotentiometricContours–UppermostAquifer
GroundwaterPotentiometricContours–DeeperAquifer
APPENDICES
AppendixA StaticWaterLevelSummary
AppendixB SubtitleD–Unit2andUnit3
1.2ndSemi-Annual2014SummaryofDetections
2.SummaryofDissolvedMetalsandTSSDetections
3.HistoricalSummaryofDetections
4.LeachateAnalysisSummary
5.SummaryofDataPre-DatingUnit3Construction/WastePlacement
6.AnalyticalReportandChain-of-CustodyRecord
7.FieldSamplingSummaryandFieldSampleLogs
8.HistoricalResults
AppendixC ClosedPortion–Unit1
1.2ndSemi-Annual2014SummaryofDetections
2.SummaryofDissolvedMetalsandTSSDetections
3.HistoricalSummaryofDetections
4.AnalyticalReportandChain-of-CustodyRecord
5.FieldSamplingSummaryandFieldSampleLogs
6.HistoricalResults
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TABLEOFCONTENTS(cont’d)
AppendixD C&D–Unit1andUnit2
1.2ndSemi-Annual2014SummaryofDetections
2.SummaryofDissolvedMetalsandTSSDetections
3.HistoricalSummaryofDetections
4.AnalyticalReportandChain-of-CustodyRecord
5.FieldSamplingSummaryandFieldSampleLogs
6.HistoricalResults
AppendixE AlternateSourceDemonstration
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EXECUTIVESUMMARY
REIConsultants,Inc.(REIC)haspreparedthisreportforthe 2nd semi-annual2014water
qualitymonitoringeventfortheBlackburnResourceRecoveryFacility,operatedbyCatawba
County,NorthCarolina.ThemonitoringeventwasperformedinaccordancewithNorth
Carolinaregulationsin15ANCAC13B,directivesandapprovalsfromtheNorthCarolina
DepartmentofEnvironmentandNaturalResources(NCDENR),andthefacilityWaterQuality
MonitoringPlan.
BlackburnResourceRecoveryFacilityconsistsoffourmainareas,aSubtitleDLandfill(Units
2and3),aClosedPortion(Unit1),andaConstructionandDemolitionLandfill(C&DUnit2
Landfill),allofwhichoperateunderPermit#18-03,andaformerC&DLandfill(C&DUnit
1Landfill).
Waterqualitymonitoringisconductedonasemi-annualbasisatthefacility.Fieldsampling
forthe 2nd semi-annualeventwasconductedbyREIConSeptember16,2014.Samplesfrom
theSubtitleDandC&Dareas,currentlyindetectionmonitoring,andsamplesfromthe
ClosedPortion,currentlyinassessmentmonitoring,wereanalyzedforconstituentsappropriate
totherespectiveprograms.GroundwatersamplesassociatedwiththeC&Dlandfillswere
analyzedfortetrahydrofuraninadditiontotheroutinemonitoringparameterlistpertheJune
25,2010memofromNCDENR.
ResultsfromallwellswerecompareddirectlytoNorthCarolinagroundwaterstandards.The
regulationsat15ANCAC13Bnolongerrequirestatisticalanalysistobeperformedduring
detectionandassessmentmonitoring.However,duetometalsdetectionsthatexceeded
groundwaterstandards,statisticalanalysiswasutilizedtodemonstratethatmetals
concentrationswerelessthanbackgroundlevels.Theresultsofthe 2nd semi-annual2014
monitoringeventforeachareaofthefacilityarediscussedbelow.
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SubtitleDUnit2
SampleswerecollectedfromallwaterqualitymonitoringlocationsassociatedwiththeSubtitle
DUnit2areaduringtheeventwiththeexceptionofunderdrainU-1,whichwasdry.Allwell
purgingandsamplingwasperformedwithnounusualcharacteristicsobservedwiththe
exceptionof significantsuspendedsolidsinseveralgroundwatersamples.
LaboratoryanalysesforNorthCarolinaAppendixIparametersyieldednodetectionsabovethe
NCDENRSolidWasteSectionLimits(SWSLs)forallvolatileorganiccompounds(VOCs).
NometalsconstituentsweredetectedaboveNorthCarolinagroundwaterstandardswiththe
exceptionofcobaltinwellsMW-12andMW-16,andvanadiuminwellMW-16.Astatistical
evaluationwasperformedutilizingpredictionintervals,whichwereconstructedfrom
backgroundhistoricaldataandcomparedtoindividualwellconstituentresultsfromthe 2nd
semi-annual2014monitoringevent.Thisevaluationindicatesthatthemetalsobservedin
compliancewellsarenotstatisticallyelevatedoverbackgroundlevels(see“AlternateSource
Demonstration”intheappendix).
Basedontheresultsofthecurrentgroundwatermonitoringevent,andpursuanttoNorth
CarolinaSub-Chapter13B,Rule .1633,itisrecommendedthattheBlackburnSubtitleDUnit2
Landfillremaininadetectionmonitoringprogramforthe 1st semi-annualmonitoringeventof
2015.
SubtitleDUnit 3
SampleswerecollectedfromallwaterqualitymonitoringlocationsassociatedwiththeSubtitle
DUnit3areaduringtheevent.Allwellpurgingandsamplingwasperformedwithnounusual
characteristicsobservedwiththeexceptionofsignificantsuspendedsolidsinseveral
groundwatersamples.
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LaboratoryanalysesforNorthCarolinaAppendixIconstituentsyieldednodetectionsabove
NCDENRSWSLsforVOCsinanyofthewells.MetalsparametersthatexceededNorth
CarolinagroundwaterstandardsintheUnit3monitoringwellsincludedchromiumand
vanadiuminwellsMW-31,MW-32,MW-33,andMW-34;andcobaltinwellsMW-32and
MW-33.Astatisticalevaluationwasperformedutilizingpredictionintervals,whichwere
constructedfrombackgroundhistoricaldataandcomparedtoindividualwellconstituent
resultsfromthe 2nd semi-annualmonitoringeventof2014.Thisevaluationindicatesthatthe
metalsobservedincompliancewellsarenotstatisticallyelevatedoverbackgroundlevels(see
“AlternateSourceDemonstration”intheappendix).
Basedontheresultsofthecurrentgroundwatermonitoringevent,andpursuanttoNorth
CarolinaSub-Chapter13B,Rule .1633,itisrecommendedthattheBlackburnSubtitleDUnit3
landfillremaininadetectionmonitoringprogramforthe 1st semi-annualmonitoringeventof
2015.
ClosedUnit1
SampleswerecollectedfromallwaterqualitymonitoringlocationsassociatedwiththeClosed
Unit1areaduringtheevent.Allwellpurgingandsamplingwasperformedwithnounusual
characteristicsobservedwiththeexceptionofsignificantsuspendedsolidsinseveral
groundwatersamples.
SampleswereanalyzedforNorthCarolinaAppendixIIconstituents.Parametersobservedat
concentrationsaboveNorthCarolinagroundwaterstandardsincompliancewellsareas
follows:
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Parameter MonitoringWell
Benzene MW-5A, MW-6,MW-7, MW-11
Chromium MW-5,MW-7
Cobalt MW-6,MW-7,MW-11
1,4-Dichlorobenzene MW-7
1,1-Dichloroethane MW-5A, MW-6
Tetrachloroethene MW-5A, MW-7
Trichloroethene MW-5A
Vinylchloride MW-7
AllotherparameterswereeithernotdetectedorwerebelowNorthCarolinagroundwater
standards.
The 2nd semi-annualassessmentmonitoringeventof2014includedanalysisofNorthCarolina
AppendixIconstituents.PerthefacilityWaterQualityMonitoringPlan,theClosedPortion
facilitywillcontinueassessmentmonitoringduringthe 1st semi-annualsamplingeventof
2015,withanalysisofAppendixIIparameters.
C&DUnits1and2
SampleswerecollectedfromallwaterqualitymonitoringlocationsassociatedwiththeC&D
Unit1andUnit2areasduringtheevent.Allwellpurgingandsamplingwasperformedwith
nounusualcharacteristicsobservedwiththeexceptionofsignificantsuspendedsolidsin
severalgroundwatersamples.
AreviewofthegroundwaterdatafortheC&DLandfillsyieldeddetectionsabovetheNorth
CarolinagroundwaterstandardofchromiuminwellsMW-21,MW-29andMW-30(notethat
wellMW-21isanupgradientbackgroundwell).Astatisticalevaluationwasperformed
utilizingpredictionintervals,whichwereconstructedfrombackgroundhistoricaldataand
comparedtoindividualwellconstituentresultsfromthe 2nd semi-annualmonitoringeventof
2014.Thisevaluationindicatesthatthemetalsobservedincompliancewellsarenot
statisticallyelevatedoverbackgroundlevels(see“AlternateSourceDemonstration”inthe
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appendix).Tetrahydrofuranwasnotdetectedabovethelaboratorypracticalquantitationlimit
(PQL)inanyoftheC&Dwellsamples.
Basedontheresultsofthecurrentgroundwatermonitoringevent,andperthefacility’sWater
QualityMonitoringPlan,itisrecommendedthattheBlackburnC&DUnit1andUnit 2
landfillsremaininadetectionmonitoringprogramforthe 1st semi-annualmonitoringeventof
2015.
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1.0 INTRODUCTION
REIConsultants,Inc.(REIC)haspreparedthe 2nd Semi-AnnualGroundwaterMonitoring
Reportfor2014fortheBlackburnResourceRecoveryFacility,anactivemunicipalsolidwaste
(MSW)andconstructionanddemolition(C&D)landfilllocatedinCatawbaCounty,North
Carolina.ThreesolidwastedisposalfacilitiesaremaintainedbyCatawbaCountyunderNorth
CarolinaSolidWastePermit#18-03. The sitesincludedinthepermitareasfollows:
·BlackburnSubtitleDFacility(Units2and3):anactiveMSW
landfillonthesouth sideofNorthCarolinaRoute2019.
·BlackburnClosedPortion(Unit1):aclosedlandfillarea,whichis
contiguouswiththesoutheast sideofUnit2andsouth sideofUnit3.
·BlackburnNewC&DFacility(C&DUnit2):aC&Dlandfill
locatedtothesouthoftheactiveSubtitleDdisposalareaandwestofthe
ClosedPortion.
Inaddition,CatawbaCountymaintainstheOldC&DFacility(C&DUnit1),aformerC&
DlandfilllocatedacrossRoute2019tothenorthoftheactiveSubtitleDdisposalarea.
Overtheyears,thewaterqualitymonitoringnetworkatBlackburnResourceRecoveryFacility
hasevolvedandadaptedasthefacilityhasundergonechangesandexpansions.NCDENRhas
beeninvolvedthroughoutthemonitoringhistory,throughmeetingsandperiodicdiscussions,
toissuerecommendations,requirements,andapprovalstochangesinthemonitoringprogram.
In2003,REICpreparedacomprehensiveWaterQualityMonitoringPlanattherequestof
NCDENRinordertoincorporateallpriordiscussions,directives,andrequirementsforthe
individualsitesintoonedocument.REICsubmittedanupdatedWaterQualityMonitoring
PlaninJune2013(approvedbyNCDENRinJuly2013)toincorporateprogramchangesand
amendmentstotheNorthCarolinaSolidWasteManagementRulesthathadoccurredsince
2003.MonitoringisconductedonasemiannualbasisperthemostrecentWaterQuality
MonitoringPlan.
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Forthe 2nd semiannual2014event,REICcollectedgroundwatersamplesfromtwenty-six(26)
monitoringwells,two(2)piezometers,andsix(6)surfacewaterlocationsatthefacility.In
addition,asamplewascollectedfromthefacility’sleachate.
2.0 SITEDESCRIPTION
2.1 PhysicalSetting
BlackburnResourceRecoveryFacilityislocatedonRockyFordRoadapproximatelysixmiles
southwestofNewton,NorthCarolina.Localtopographyinthevicinityofthefacilityis
characterizedbygentlyrollinghills.Elevationsintheareaofthelandfillrangefrom
approximately930feetabovemeansealevel(MSL)onknollstoaminimumelevationatan
unnamedtributarystreamtoSouthForkCatawbaRiverthatexitsthepropertyat
approximately790feetaboveMSL.Landusesurroundingthefacilityisindustrialtothe
north,residentialtothesouthandwest,andagriculturaltotheeast.
2.2 GeologyandHydrogeology
ThefacilityislocatedwithintheInnerPiedmontBeltofthePiedmontPhysiographicProvince
ofNorthCarolina.GeologyintheregionischaracterizedbyCambrian/Proterozoic
amphibolitewithbiotitegneiss. Extensivecharacterizationofon-sitesoilsandrockhavebeen
performedthroughcoringprogramsandloggingofboringsconductedatthefacility.Soilsin
thevicinitybeginwithclayeysiltnearthesurface,whiledeepersoilsaremoresiltyandsandy.
Thetransitionalboundaryfromsoiltorockistypicallycharacterizedbypartiallyweathered
rockabovebedrock.Thissoiltorockboundaryinthevicinityofthelandfillgenerallyranges
fromapproximately10to70feetdeep.Groundwateroftheupper-mostaquiferexistsunder
watertableconditions.Infiltrationofprecipitationistheprimarysourceofrechargeof
groundwater.Hydraulicgradientsaregenerallyinthedirectionofthetopographicsurface
gradients,resultinginadischargeconditionatstreams,wherethewatertableintersectsthe
topographiclowpointsinthearea.
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2.3 MonitoringNetwork
TheUnit1monitoringnetworkincludeswellsMW-5,MW-5A,MW-6,MW-6D,MW-7,and
MW-11,andsurfacewaterlocationsSW-1andSW-3. Twopiezometers,PZ-85BandPZ-86B,
locatedalongtheeasternsideofUnit1,areincludedinthenetworkinordertomonitor
impactsoflandfillgasfromtheclosedareatogroundwaterinthevicinity.TheUnit2
monitoringnetworkincludeswellsMW-12,MW-13,MW-14,MW-15,MW-16,andMW-17,
andunderdrainsU-1,U-2,andU-3.TheUnit3monitoringnetworkincludeswellsMW-31,
MW-32, MW-33,and MW-34,andsurfacewaterlocationsSW-4andSW-5.TheC&DUnit1
monitoringsystemincludeswellsMW-2,MW-26,andMW-27.WellMW-20servesasthe
backgroundmonitoringwellforUnit1,Unit2,Unit3,andC&DUnit1.TheC&DUnit2
monitoringsystemincludeswellMW-21,thebackgroundwell,andwellsMW-24,MW-25,
MW-28,MW-29,andMW-30.Inadditiontotheabovegroundwatersamplingpoints,several
wellsacrossthesiteareutilizedonlyforwaterlevelmonitoring.Samplinglocationsare
indicatedongroundwaterpotentiometricmapsincludedinthisreport.
3.0 HYDROLOGICEVALUATION
3.1 StaticWaterLevelsandGroundwaterElevations
Staticwaterlevelsweremeasuredfromthetopofcasingpriortopurginginallwellson
September16,2014.Thesewaterlevelmeasurements,inconjunctionwithsurveyedcasing
elevationdata,wereusedtocalculategroundwaterelevationsineachwell.Thisdatais
presentedinAppendixA.
3.2 Groundwater FlowRateandDirection
Theelevationdatahavebeenutilizedtodeveloppotentiometricmapsforthefacility.The
BlackburnSubtitleD(Units2and3),ClosedPortion(Unit1),NewC&D(C&DUnit2),
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andOldC&D(C&DUnit1)facilitiesareshowntogetherontheresultingmapsthatare
includedinthisreport.Separatemapsareprovidedfortheshalloworupper-mostaquiferand
thepotentiometricsurfacedefinedbythedeeperwellscreens.
Theshallowaquiferisthemost significantwater-bearingzoneoftheprogramandthemajority
ofthewellscreensaresetinthislayer.Theaquiferlithologyconsistsofsandwithminorsilt,
althoughtwoofthewellshavescreenswithextremelowerportionspenetratingthebedrock.
Theshallowaquiferisunconfinedandthephreaticsurfacegenerallyfollowstopographical
contours.Therefore,theinfluenceofsurfacetopographyandelevationsalongthecreek,the
localdischargepoint,wereutilizedindevelopingthepotentiometricmapfortheshallow
aquifer.
Thepotentiometricmapconstructedfromwaterlevelmeasurementstakenatthedeeperwell
screensisbasedonfourdatapoints.Thefourwellsutilizedarethosewithrelativelydeeper
wellscreenslocatedatclusteredwellsetsintheSubtitleDandClosedPortionareas.These
wellshavescreensthatarefullylocatedinthebedrockorhavescreenslocatedinweathered
bedrock.Noclearlydefinedaquitardsarediscernablebetweentheshallowanddeeperwell
screenzones.Thegeneraldeepergroundwaterflowdirectionissimilartothatoftheshallow
aquifer.
Thepotentiometricmapscreatedfortheupper-mostaquiferanddeeperwellscreenzoneare
includedinthisreport.Thehorizontalcomponentsofthehydraulicgradientshavebeen
determinedbyfollowingflowpathsthatarenormaltotheshallowpotentiometriccontours.
Theseflowpathsareshownontheshallowpotentiometricmap.Hydraulicgradientsand
groundwatervelocitieswerenotcalculatedforthedeeperwellscreenzone.
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GroundwaterhorizontalflowvelocitieswereestimatedusingaformofDarcy’s Law:
V=(Kh *i)/ ne
where:
V=groundwatervelocity
Kh=horizontalhydraulicconductivity
i=hydraulicgradient
ne=effectiveporosity
Hydraulicparametersandestimatedflowvelocitiesoftheupper-mostaquiferforeachareaare
providedinthefollowingtable:
Area
Groundwater
Velocity
(ft/yr)
Hydraulic
Conductivity
(cm/sec)
Hydraulic
Gradient
(ft/ft)
Effective
Porosity
(unitless)
ClosedUnit1 250 1.9x10-3 0.027 0.21
SubtitleDUnit2 100 7.7x10-4 0.027 0.21
C&DUnit1 360 1.9x10-3 0.038 0.21
C&DUnit2 490 1.9x10-3 0.053 0.21
Thehorizontalplacementofdowngradientwellsisdeemedsufficienttoprovideearlydetection
ofpotentialreleasesfromthewasteunits.Verticalplacementofwatertablewellscreens
allowsmonitoringofgroundwateroftheuppermostaquifer.WellsMW-5AandMW-6D
allowmonitoringofverticalflowconditionsandverticaldistributionofgroundwater
constituentsinthedischargeregionalongthestreamdowngradientofUnit1.Thewellsinthe
monitoringnetworkoftheBlackburnResourceRecoveryFacilityappeartobeadequateto
monitorgroundwaterhydraulicallyupgradientanddowngradientofthelandfillunitsatthe
facility.
4.0 SAMPLINGANDLABORATORYANALYSIS
4.1 FieldSamplingSummary
The 2nd semi-annual2014samplingeventwasperformedattheBlackburnResourceRecovery
FacilityonSeptember16,2014.Alllocationsinthemonitoringnetworkweresampledduring
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themonitoringeventwiththeexceptionofunderdrainU-1associatedwithSubtitleDUnit2,
whichwasdryduringthesamplingevent.Aleachatesamplewascollectedfromthefacility’s
leachatecollection systemduringtheevent.Fieldsamplingwasperformedinaccordancewith
stateandfederalguidelinesandthefacility’sWaterQualityMonitoringPlan.Monitoring
wellswereinspectedpriortosampling,andnosecurityissuesordamagetothewellswere
notedwiththeexceptionofabentinnercasingatwellMW-28.Staticwaterlevelswere
measuredineachwellpriortopurgingutilizingadecontaminatedelectronicmeasuringtape.
Monitoringwellswerepurgedandsampledusinglaboratorydecontaminatedpolytetra-
fluoroethylenebailers.FieldtestingofpH,temperature,conductivity,andturbiditywere
measuredtoensureadequatepurgingandtoverifystabilization.Sampleswerecollectedinto
pre-cleanedandappropriatelypreservedcontainers,placedinicedcoolers,andtransported
underproperchain-of-custodyprotocoltothelaboratory.SamplepH,temperature,
conductivity,andturbidityweremeasuredinthefieldusingcalibratedinstruments.Allwell
purgingandsamplingwasperformedwithnounusualcharacteristicsobservedwiththe
exceptionofsignificantsuspendedsolidsinseveralgroundwatersamples.Fieldsamplinglogs
areincludedinAppendixB(SubtitleDUnits2and3),AppendixC(ClosedUnit1),and
AppendixD(C&DUnits1and2).
4.2 LaboratoryAnalysisSummary
Samplescollectedduringthe 2nd semi-annual2014eventwereanalyzedbyREIC.Allsamples
collectedduringthemonitoringeventwerereceivedbythelaboratoryingoodconditionandat
propertemperatures.SampleswereanalyzedutilizingU.S.EPAapprovedmethodswithin
requiredholdingtimes.SamplesassociatedwiththeSubtitleDUnits2and3andClosedUnit
1areaswereanalyzedforNorthCarolinaAppendixIparameters.Groundwatersamples
associatedwiththeC&DlandfillswereanalyzedforNorthCarolinaAppendixIVOCsand
eightRCRAmetalspertheWaterQualityMonitoringPlan,inadditiontotetrahydrofuranper
theJune25,2010memofromNCDENR.
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4.3 QualityAssurance/QualityControl
Fieldqualitycontrolsamplesincludedduplicatesamplesandtripblanks.Duplicatesample
resultsgenerallyagreedwellwithparentsampleresults.Analysisofthetripblanksampledid
notindicateanycontaminationissuesviathefieldsampling,sampletransportation,or
laboratoryhandlingprocesses.
Thelaboratoryqualityassurance/qualitycontrol(QA/QC)programincludedallappropriate,
methodspecificqualitycontrols.Laboratorydatametthenecessaryqualitycontrolcriteria.
Laboratorycontrolsamplespikerecoveriesandsurrogaterecoverieswerewithinrequired
limits,andlaboratoryduplicate,matrixspike,andmethodblankanalyseswereacceptable.
4.4 AnalyticalResults
Laboratoryreportsandchain-of-custodyrecordsareincludedinAppendixB(SubtitleDUnits
2and3),AppendixC(ClosedUnit1),andAppendixD(C&DUnits1and2).Datahave
beenreportedtomethoddetectionlimits(MDLs)asrequestedbyNCDENR.However,note
thatanyvaluesreportedbelowSolidWasteSectionLimits(SWSLs),flaggedwitha“J”
qualifier,areonlyestimates,arenotquantitative,andshouldnotbeusednumericallyinany
way.
LaboratoryanalysisforsamplesassociatedwithSubtitleDUnit2indicatedthatno
constituentsweredetectedaboveNorthCarolinagroundwaterstandardsinmonitoringwells
withtheexceptionofcobaltinwellsMW-12andMW-16,andvanadiuminwellMW-16.
SeveralmetalsweredetectedaboveSWSLsinunderdrainsampleU-3.
ParametersthatexceededNorthCarolinagroundwaterstandardsintheSubtitleDUnit3
monitoringwellsincludedchromiumandvanadiuminwellsMW-31,MW-32,MW-33,and
MW-34;andcobaltinwellsMW-32andMW-33.NoparametersexceededNorthCarolina
groundwaterstandardsinthesurfacewatersamplesSW-4andSW-5.
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ParametersobservedatconcentrationsaboveNorthCarolinagroundwaterstandardsin
compliancewellsassociatedwithClosedUnit1areasfollows:
Parameter MonitoringWell
Benzene MW-5A, MW-6,MW-7, MW-11
Chromium MW-5,MW-7
Cobalt MW-6,MW-7,MW-11
1,4-Dichlorobenzene MW-7
1,1-Dichloroethane MW-5A, MW-6
Tetrachloroethene MW-5A, MW-7
Trichloroethene MW-5A
Vinylchloride MW-7
Theparametersandconcentrationsobservedduringthe 2nd semiannual2014eventinwells
associatedwithClosedUnit1aregenerallyconsistentwithrecenthistoricaldata.Inaddition,
VOCsobservedduringthe 2nd semiannual2014eventinpiezometersPZ-85BandPZ-86Bare
consistentwithrecenthistoricaldata.NoparametersweredetectedaboveSWSLsinthe
surfacewatersamplesSW-1andSW-3.
AreviewofthegroundwaterdatafortheC&DLandfillsindicateddetectionsabovetheNorth
CarolinagroundwaterstandardofchromiuminwellsMW-21,MW-29andMW-30(notethat
well MW-21isanupgradientbackgroundwell).
AnalyticalparametersthatweredetectedaboveSWSLsaresummarizedintablesincludedin
AppendixB(SubtitleDUnits2and3),AppendixC(ClosedUnit1),andAppendixD(C&D
Units1and2).Asummaryofdetectionstableisincludedforeacharea.Valuesgreaterthan
theNorthCarolinagroundwaterstandardsareshowninredprint.Dissolvedmetalsdetections
andtotalsuspendedsolidsresults,aswellashistoricaldatasummaries,areincludedinthe
appendicesforeachareaofthefacility.
DuetochangesinNorthCarolinasolidwasterules,statisticalanalysisofgroundwaterdatais
nolongerrequired.However,statisticalanalysiswasutilizedtodemonstratethatmetals
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concentrationsexceedinggroundwaterstandardswereactuallylessthanbackgroundlevels.
Thisevaluationindicatesthatthemetalsobservedabovegroundwaterstandardsincompliance
wellsassociatedwiththeSubtitleDUnit2,SubtitleDUnit3,C&DUnit1,andC&DUnit2
areasarenotstatisticallyelevatedoverbackgroundlevels.TheStatisticalAnalysisSummary
isincludedinAppendix E, “AlternateSourceDemonstration”.
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5.0 FINDINGSANDCONCLUSIONS
5.1 SummaryofFindings
·The 2nd semi-annual2014waterqualitymonitoringeventatBlackburnResource
RecoveryFacilityhasbeenperformedinaccordancewithNorthCarolinaregulations
andthefacility’sWaterQualityMonitoringPlan.
·Thehorizontalgroundwaterflowrateoftheuppermostaquiferhasbeenestimatedto
rangefrom100to490ft/yearthroughoutthe site.Thewellsinthemonitoringnetwork
appeartobeadequatetomonitorgroundwaterhydraulicallyupgradientand
downgradientofthefacility.
·Fieldsamplingandlaboratoryanalysisactivitieswereperformedwithnosignificant
proceduraldeviationsandwithinacceptableQA/QCparameters.
·Severalparametersexceededgroundwaterstandardsinwellsassociatedwiththe
ClosedUnit1area.However,resultsareconsistentwithdatafrompreviousevents.
·Severalmetalsparametersexceededgroundwaterstandardsinwellsassociatedwith
theSubtitleDUnit2and3andC&DUnit1and2areas.However,statistical
analysisindicatedthatthemetalsconcentrationswerelessthanbackgroundlevels.
5.2 Conclusions
Areviewofthemonitoringwellnetwork,fieldsamplingandlaboratoryanalysisactivities,and
QA/QCprogramindicatesthatthe 2nd semi-annual2014groundwatermonitoringeventatthe
BlackburnResourceRecoveryFacilityyieldedsamplesrepresentativeoftheuppermostaquifer
inthevicinityofthefacility.Basedontheresultsofthecurrentgroundwatermonitoring
event,andpursuanttoNorthCarolinaSub-Chapter13B,Rule.1633,itisrecommendedthat
theBlackburnSubtitleDlandfillsremaininadetectionmonitoringprogramforthe 1st semi-
2nd Semi-Annual2014Groundwater MonitoringReport
___________________________________________________________________________________________
REIConsultants,Inc.P.O.Box286,Beaver,WV25813800-999-0105 www.reiclabs.com
16
annualmonitoringeventof2015.Inaddition,itisrecommendedthattheC&DLandfills
remaininadetectionmonitoringprogramforthe 1st semi-annualmonitoringeventof2015.It
isalsorecommendedthatassessmentmonitoringcontinueattheClosedUnit1facilityduring
the 1st semi-annualeventof2015,withannualanalysisofallAppendixIIparameters.
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
Potentiometric Contour Maps
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
AppendixA:
Static Water Level Summary
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
Subtitle D
AppendixB1:
2nd Semi-Annual 2014
Summary of Detections
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
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CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
Subtitle D
AppendixB2:
Summary ofDissolvedMetalsand
TotalSuspendedSolid(TSS)
Detections
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Su
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in
m g /L.
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a nd
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F OO
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T E S:
1.
S W SL
-
S o l id
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2.
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A ll
d a ta
re
p o r t ed
in
m g /L.
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB3:
HistoricalSummaryofDetections
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Subtitle D -Unit 2
HistoricalSummary ofDetections
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB3-Page 1
Subtitle D -Unit 3
HistoricalSummary ofDetections
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB3-Page21
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB4:
LeachateAnalysisSummary
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
REICJobNumber:1409J30
SampleDate:9-2014
Units PQL Result
Volatiles by GCMS
1 1,1,1,2-Tetrachloroethane mg/L 0.005 ND
2 1,1,1-Trichloroethane mg/L 0.001 ND
3 1,1,2,2-Tetrachloroethane mg/L 0.003 ND
4 1,1,2-Trichloroethane mg/L 0.001 ND
5 1,1-Dichloroethane mg/L 0.005 ND
6 1,1-Dichloroethene mg/L 0.005 ND
7 1,2,3-Trichloropropane mg/L 0.001 ND
8 1,2-Dibromo-3-Chloropropane (DBCP)mg/L 0.013 ND
9 1,2-Dibromoethane (EDB)mg/L 0.001 ND
10 1,2-Dichlorobenzene mg/L 0.005 ND
11 1,2-Dichloroethane mg/L 0.001 ND
12 1,2-Dichloropropane mg/L 0.001 ND
13 1,4-Dichlorobenzene mg/L 0.001 ND
14 2-Butanone(Methylethylketone)mg/L 0.100 ND
15 2-Hexanone mg/L 0.050 ND
16 4-Methyl-2-pentanone mg/L 0.100 ND
17 Acetone mg/L 0.100 ND
18 Acrylonitrile mg/L 0.20 ND
19 Benzene mg/L 0.001 ND
20 Bromochloromethane mg/L 0.003 ND
21 Bromodichloromethane mg/L 0.001 ND
22 Bromoform mg/L 0.003 ND
23 Bromomethane (Methyl bromide)mg/L 0.010 ND
24 Carbon disulfide mg/L 0.100 ND
25 Carbon tetrachloride mg/L 0.001 ND
26 Chlorobenzene mg/L 0.003 ND
27 Chloroethane mg/L 0.010 ND
28 Chloroform mg/L 0.005 ND
29 Chloromethane (Methyl chloride)mg/L 0.001 ND
30 cis-1,2-Dichloroethene mg/L 0.005 ND
31 cis-1,3-Dichloropropene mg/L 0.001 ND
32 Dibromochloromethane mg/L 0.003 ND
33 Dibromomethane(Methylenebromide)mg/L 0.010 ND
34 Ethylbenzene mg/L 0.001 0.0040
35 Iodomethane(Methyliodide)mg/L 0.010 ND
36 Methylene chloride mg/L 0.001 ND
37 Styrene mg/L 0.001 ND
38 Tetrachloroethene mg/L 0.001 ND
39 Toluene mg/L 0.001 ND
40 trans-1,2-Dichloroethene mg/L 0.005 ND
41 trans-1,3-Dichloropropene mg/L 0.001 ND
42 trans-1,4-Dichloro-2-butene mg/L 0.100 ND
43 Trichloroethene mg/L 0.001 ND
44 Trichlorofluoromethane mg/L 0.001 ND
45 Vinyl acetate mg/L 0.050 ND
46 Vinyl chloride mg/L 0.001 ND
47 Xylenes mg/L 0.005 0.0038
DATA SUMMARY
CatawbaCounty,NC-SubtitleD Landfill- Leachate
Parameter
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB4-Page 1
REICJobNumber:1409J30
SampleDate:9-2014
Units PQL Result
DATA SUMMARY
CatawbaCounty,NC-SubtitleD Landfill- Leachate
Parameter
Inorganics (Metals)
48 Antimony mg/L 0.006 ND
49 Arsenic mg/L 0.010 ND
50 Barium mg/L 0.100 0.105
51 Beryllium mg/L 0.001 ND
52 Cadmium mg/L 0.001 ND
53 Chromium mg/L 0.010 0.0296
54 Cobalt mg/L 0.010 0.0167
55 Copper mg/L 0.010 0.0123
56 Lead mg/L 0.010 ND
57 Nickel mg/L 0.050 0.0781
58 Selenium mg/L 0.010 ND
59 Silver mg/L 0.010 ND
60 Thallium mg/L 0.006 ND
61 Vanadium mg/L 0.025 ND
62 Zinc mg/L 0.010 0.0588
Additional Parameters
Biochemical OxygenDemand(BOD)mg/L 2.0 23
Chemical OxygenDemand(COD)mg/L 10.0 354
Nitrate mg/L 0.1 ND
ortho-Phosphate mg/L 0.1 0.12
Sulfate mg/L 5.0 18.4
NOTES:
ND-NotDetectedatPQL
PQL-PracticalQuantitationLimits (PQLs)arethe lowestconcentraitonofanalytes ingroundwaterthatcanbereliably
determinedwithinspecified limitsofprecisionandaccuracybyaparticularmethodunderroutine laboratoryconditions.
IfthePQL foraparticularmethod isahighervaluethanthegroundwaterstandard forthatparameter, itmustbenbe
equalorbe lessthanthePQLsstated intheNorthCarolinaAppendixIIMonitoringandAppendixIOrganicConsituents
Guidelines.
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB4-Page 2
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB5:
SummaryofDataPre-DatingUnit3
Construction/Waste Placement
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
SUMMARY OF VOC DATA
PRE-DATING UNIT 3 CONSTRUCTION/WASTE PLACEMENT
Blackburn Landfill
Permit:#18-03
Analyte SWSL Units Sep-04 Mar-05 Sep-05 Mar-06 Sep-06 Mar-07 Sep-07
Acetone 0.1 mg/L ND ND ND ND ND ND ND
Acrylonitrile 0.2 mg/L ND ND ND ND ND ND ND
Benzene 0.001 mg/L ND ND ND ND ND ND ND
Bromochloromethane 0.003 mg/L ND ND ND ND ND ND ND
Bromodichloromethane 0.001 mg/L ND ND ND ND ND ND ND
Bromoform 0.003 mg/L ND ND ND ND ND ND ND
Bromomethane 0.01 mg/L ND ND ND ND ND ND ND
2-Butanone 0.1 mg/L ND ND ND ND ND ND ND
Carbondisulfide 0.1 mg/L ND ND ND ND ND ND ND
Carbontetrachloride 0.001 mg/L ND ND ND ND ND ND ND
Chlorobenzene 0.003 mg/L ND ND ND ND ND ND ND
Chloroethane 0.01 mg/L ND ND ND ND ND ND ND
Chloroform 0.005 mg/L ND ND ND ND ND ND ND
Chloromethane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dibromo-3-chloropropane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dibromoethane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dichlorobenzene 0.005 mg/L ND ND ND ND ND ND ND
1,4-Dichlorobenzene 0.001 mg/L ND ND ND ND ND ND ND
trans-1,4-Dichloro-2-butene 0.1 mg/L ND ND ND ND ND ND ND
1,1-Dichloroethane 0.005 mg/L ND 0.007 0.014 0.019 0.025 0.0134 0.007
1,2-Dichloroethane 0.001 mg/L ND ND ND ND ND ND ND
1,1-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
cis-1,2-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
trans-1,2-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
1,2-Dichloropropane 0.001 mg/L ND ND ND ND ND ND ND
cis-1,3-Dichloropropene 0.001 mg/L ND ND ND ND ND ND ND
trans-1,3-Dichloropropene 0.001 mg/L ND ND ND ND ND ND ND
Dibromochloromethane 0.001 mg/L ND ND ND ND ND ND ND
Dibromomethane 0.01 mg/L ND ND ND ND ND ND ND
Ethylbenzene 0.001 mg/L ND ND ND ND ND ND ND
2-Hexanone 0.05 mg/L ND ND ND ND ND ND ND
Iodomethane 0.01 mg/L ND ND ND ND ND ND ND
Methylenechloride 0.001 mg/L ND ND ND ND ND ND ND
4-Methyl-2-pentanone 0.1 mg/L ND ND ND ND ND ND ND
Styrene 0.001 mg/L ND ND ND ND ND ND ND
1,1,1,2-Tetrachloroethane 0.005 mg/L ND ND ND ND ND ND ND
1,1,2,2-Tetrachloroethane 0.001 mg/L ND ND ND ND ND ND ND
Tetrachloroethene 0.001 mg/L 0.025 0.031 0.024 0.034 0.039 0.035 0.018
Toluene 0.001 mg/L ND ND ND ND ND ND ND
1,1,1-Trichloroethane 0.001 mg/L ND ND ND ND ND ND ND
1,1,2-Trichloroethane 0.005 mg/L ND ND ND ND ND ND ND
Trichloroethene 0.001 mg/L 0.030 0.055 0.042 0.061 0.070 0.039 0.018
Trichlorofluoromethane 0.001 mg/L ND ND ND ND ND ND ND
1,2,3-Trichloropropane 0.001 mg/L ND ND ND ND ND ND ND
Vinylacetate 0.05 mg/L ND ND ND ND ND ND ND
Vinylchloride 0.001 mg/L ND ND 0.005 0.002 ND ND ND
Xylenes,Total 0.003 mg/L ND ND ND ND ND ND ND
FOOTNOTES:
SWSL-SolidWasteSectionLimits(mg/L)
ND-notdetectedatorabovetheSWSL
PZ-83B
SUMMARY OF VOC DATA
PRE-DATING UNIT 3 CONSTRUCTION/WASTE PLACEMENT
Blackburn Landfill
Permit:#18-03
Analyte SWSL Units Sep-04 Mar-05 Sep-05 Mar-06 Sep-06 Mar-07 Sep-07
Acetone 0.1 mg/L ND ND ND ND ND ND ND
Acrylonitrile 0.2 mg/L ND ND ND ND ND ND ND
Benzene 0.001 mg/L 0.010 0.008 0.010 0.009 0.011 0.0106 0.0108
Bromochloromethane 0.003 mg/L ND ND ND ND ND ND ND
Bromodichloromethane 0.001 mg/L ND ND ND ND ND ND ND
Bromoform 0.003 mg/L ND ND ND ND ND ND ND
Bromomethane 0.01 mg/L ND ND ND ND ND ND ND
2-Butanone 0.1 mg/L ND ND ND ND ND ND ND
Carbondisulfide 0.1 mg/L ND ND ND ND ND ND ND
Carbontetrachloride 0.001 mg/L ND ND ND ND ND ND ND
Chlorobenzene 0.003 mg/L ND ND ND 0.006 0.007 0.007 0.008
Chloroethane 0.01 mg/L ND ND ND ND ND ND ND
Chloroform 0.005 mg/L ND ND ND ND ND ND ND
Chloromethane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dibromo-3-chloropropane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dibromoethane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dichlorobenzene 0.005 mg/L ND ND ND ND ND ND ND
1,4-Dichlorobenzene 0.001 mg/L 0.013 0.015 0.017 0.018 0.018 0.015 0.015
trans-1,4-Dichloro-2-butene 0.1 mg/L ND ND ND ND ND ND ND
1,1-Dichloroethane 0.005 mg/L 0.090 0.087 0.075 0.075 0.081 0.052 0.034
1,2-Dichloroethane 0.001 mg/L ND ND 0.002 ND ND ND ND
1,1-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
cis-1,2-Dichloroethene 0.005 mg/L 0.094 0.098 0.091 0.163 0.213 0.16 0.142
trans-1,2-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
1,2-Dichloropropane 0.001 mg/L 0.009 0.007 0.008 0.006 0.006 0.005 0.004
cis-1,3-Dichloropropene 0.001 mg/L ND ND ND ND ND ND ND
trans-1,3-Dichloropropene 0.001 mg/L ND ND ND ND ND ND ND
Dibromochloromethane 0.001 mg/L ND ND ND ND ND ND ND
Dibromomethane 0.01 mg/L ND ND ND ND ND ND ND
Ethylbenzene 0.001 mg/L ND ND ND ND ND ND ND
2-Hexanone 0.05 mg/L ND ND ND ND ND ND ND
Iodomethane 0.01 mg/L ND ND ND ND ND ND ND
Methylenechloride 0.001 mg/L 0.235 0.105 0.082 ND 0.026 0.030 0.015
4-Methyl-2-pentanone 0.1 mg/L ND ND ND ND ND ND ND
Styrene 0.001 mg/L ND ND ND ND ND ND ND
1,1,1,2-Tetrachloroethane 0.005 mg/L ND ND ND ND ND ND ND
1,1,2,2-Tetrachloroethane 0.001 mg/L ND ND ND ND ND ND ND
Tetrachloroethene 0.001 mg/L 0.154 0.092 0.107 0.028 0.023 0.0198 0.011
Toluene 0.001 mg/L ND ND ND ND ND 0.0033 0.0047
1,1,1-Trichloroethane 0.001 mg/L ND ND ND ND ND ND ND
1,1,2-Trichloroethane 0.005 mg/L ND ND ND ND ND ND ND
Trichloroethene 0.001 mg/L 0.160 0.156 0.111 0.048 0.030 0.017 0.014
Trichlorofluoromethane 0.001 mg/L ND ND ND ND ND ND ND
1,2,3-Trichloropropane 0.001 mg/L ND ND ND ND ND ND ND
Vinylacetate 0.05 mg/L ND ND ND ND ND ND ND
Vinylchloride 0.001 mg/L ND ND 0.005 0.003 0.003 ND ND
Xylenes,Total 0.003 mg/L 0.059 0.044 0.067 0.052 0.061 0.070 0.070
FOOTNOTES:
SWSL-SolidWasteSectionLimits(mg/L)
ND-notdetectedatorabovetheSWSL
PZ-84B
SUMMARY OF VOC DATA
PRE-DATING UNIT 3 CONSTRUCTION/WASTE PLACEMENT
Blackburn Landfill
Permit:#18-03
Analyte SWSL Units Mar-08 Sep-08 Mar-09 Apr-09
1,1,1,2-Tetrachloroethane 0.005 mg/L ND ND ND ND
1,1,1-Trichloroethane 0.001 mg/L ND ND ND ND
1,1,2,2-Tetrachloroethane 0.001 mg/L ND ND ND ND
1,1,2-Trichloroethane 0.005 mg/L ND ND ND ND
1,1-Dichloroethane 0.005 mg/L ND 0.0070 0.0128 0.0182
1,1-Dichloroethene 0.005 mg/L ND ND ND ND
1,2,3-Trichloropropane 0.001 mg/L ND ND ND ND
1,2-Dibromo-3-chloropropane 0.001 mg/L ND ND ND ND
1,2-Dibromoethane 0.001 mg/L ND ND ND ND
1,2-Dichlorobenzene 0.005 mg/L ND ND ND ND
1,2-Dichloroethane 0.001 mg/L ND ND ND ND
1,2-Dichloropropane 0.001 mg/L ND ND ND ND
1,4-Dichlorobenzene 0.001 mg/L ND 0.0033 0.0044 0.0039
2-Butanone 0.1 mg/L ND ND ND ND
2-Hexanone 0.05 mg/L ND ND ND ND
4-Methyl-2-pentanone 0.1 mg/L ND ND ND ND
Acetone 0.1 mg/L ND ND ND ND
Acrylonitrile 0.2 mg/L ND ND ND ND
Benzene 0.001 mg/L ND ND 0.0011 0.0017
Bromochloromethane 0.003 mg/L ND ND ND ND
Bromodichloromethane 0.001 mg/L ND ND ND ND
Bromoform 0.003 mg/L ND ND ND ND
Bromomethane 0.01 mg/L ND ND ND ND
Carbondisulfide 0.1 mg/L ND ND ND ND
Carbontetrachloride 0.001 mg/L ND ND ND ND
Chlorobenzene 0.003 mg/L ND ND ND ND
Chloroethane 0.01 mg/L ND ND ND ND
Chloroform 0.005 mg/L ND ND ND ND
Chloromethane 0.001 mg/L ND ND ND ND
cis-1,2-Dichloroethene 0.005 mg/L ND 0.0081 0.0160 0.0243
cis-1,3-Dichloropropene 0.001 mg/L ND ND ND ND
Dibromochloromethane 0.001 mg/L ND ND ND ND
Dibromomethane 0.01 mg/L ND ND ND ND
Ethylbenzene 0.001 mg/L ND ND ND ND
Iodomethane 0.01 mg/L ND ND ND ND
Methylenechloride 0.001 mg/L ND 0.0020 0.0056 0.0079
Styrene 0.001 mg/L ND ND ND ND
Tetrachloroethene 0.001 mg/L ND 0.0039 0.0076 0.0157
Toluene 0.001 mg/L ND ND ND ND
trans-1,2-Dichloroethene 0.005 mg/L ND ND ND ND
trans-1,3-Dichloropropene 0.001 mg/L ND ND ND ND
trans-1,4-Dichloro-2-butene 0.1 mg/L ND ND ND ND
Trichloroethene 0.001 mg/L ND 0.0045 0.0120 0.0200
Trichlorofluoromethane 0.001 mg/L ND ND ND ND
Vinylacetate 0.05 mg/L ND ND ND ND
Vinylchloride 0.001 mg/L ND ND 0.0015 ND
Xylenes,Total 0.003 mg/L ND ND ND ND
FOOTNOTES:
SWSL-SolidWasteSectionLimits(mg/L)
ND-notdetectedatorabovetheSWSL
MW-31
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB6:
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Unit 2
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver, WV 25813 800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Monday, September 29, 2014
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:BLACKBURN SUBTITLE D
Work Order #:1409J28
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 10 sample(s) on 9/17/2014 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Case Narrative
Client:
Project:BLACKBURN SUBTITLE D
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:55:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-01A Matrix:Groundwater
MW-12Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/19/2014 2:49 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 2:49 PM
Barium 0.103 0.100 mg/L0.0010 NA PA/VA9/19/2014 2:49 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 2:49 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 2:49 PM
Chromium 0.0021 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 2:49 PM
Cobalt 0.109 0.0100 mg/L0.0010 NA PA/VA9/19/2014 2:49 PM
Copper 0.0084 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 2:49 PM
Lead 0.0007 0.0100 J mg/L0.0002 NA PA/VA9/19/2014 2:49 PM
Nickel 0.0056 0.0500 J mg/L0.0020 NA PA/VA9/19/2014 2:49 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 2:49 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 2:49 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/19/2014 2:49 PM
Vanadium 0.0111 0.0250 J mg/L0.0010 NA PA/VA9/19/2014 2:49 PM
Zinc 0.0139 0.0100 mg/L0.0030 NA PA/VA9/19/2014 2:49 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/20/2014 5:36 AM
Acetone 60.6 100 J µg/L4.88 NA PA/VA9/20/2014 5:36 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/20/2014 5:36 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/20/2014 5:36 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/20/2014 5:36 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/20/2014 5:36 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/20/2014 5:36 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/20/2014 5:36 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/20/2014 5:36 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/20/2014 5:36 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/20/2014 5:36 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/20/2014 5:36 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/20/2014 5:36 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/20/2014 5:36 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/20/2014 5:36 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/20/2014 5:36 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/20/2014 5:36 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/20/2014 5:36 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/20/2014 5:36 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/20/2014 5:36 AM
Page 3 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:55:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-01A Matrix:Groundwater
MW-12Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/20/2014 5:36 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/20/2014 5:36 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/20/2014 5:36 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/20/2014 5:36 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/20/2014 5:36 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/20/2014 5:36 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/20/2014 5:36 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/20/2014 5:36 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/20/2014 5:36 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/20/2014 5:36 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/20/2014 5:36 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/20/2014 5:36 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/20/2014 5:36 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/20/2014 5:36 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/20/2014 5:36 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/20/2014 5:36 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/20/2014 5:36 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/20/2014 5:36 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/20/2014 5:36 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/20/2014 5:36 AM
1,1,2-Trichloroethane 0.960 1.00 J µg/L0.492 NA PA/VA9/20/2014 5:36 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/20/2014 5:36 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/20/2014 5:36 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/20/2014 5:36 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/20/2014 5:36 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/20/2014 5:36 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/20/2014 5:36 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/20/2014 5:36 AM
Surr: 1,2-Dichloroethane-d4 93.8 68.7-129 %RECNANA 9/20/2014 5:36 AM
Surr: 4-Bromofluorobenzene 112 71.8-127 %RECNANA 9/20/2014 5:36 AM
Surr: Dibromofluoromethane 102 74.3-124 %RECNANA 9/20/2014 5:36 AM
Surr: Toluene-d8 104 71.4-129 %RECNANA 9/20/2014 5:36 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 21.0 10 mg/L2.0 NA PA/VA9/18/2014 8:20 AM
Page 4 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:28:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-02A Matrix:Groundwater
MW-13Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/19/2014 2:54 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 2:54 PM
Barium 0.0990 0.100 J mg/L0.0010 NA PA/VA9/19/2014 2:54 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 2:54 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 2:54 PM
Chromium 0.0089 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 2:54 PM
Cobalt 0.0026 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 2:54 PM
Copper 0.0188 0.0100 mg/L0.0010 NA PA/VA9/19/2014 2:54 PM
Lead 0.0005 0.0100 J mg/L0.0002 NA PA/VA9/19/2014 2:54 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA9/19/2014 2:54 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 2:54 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 2:54 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/19/2014 2:54 PM
Vanadium 0.0202 0.0250 J mg/L0.0010 NA PA/VA9/19/2014 2:54 PM
Zinc 0.0205 0.0100 mg/L0.0030 NA PA/VA9/19/2014 2:54 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/20/2014 11:38 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/20/2014 11:38 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/20/2014 11:38 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/20/2014 11:38 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/20/2014 11:38 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/20/2014 11:38 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/20/2014 11:38 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/20/2014 11:38 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/20/2014 11:38 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/20/2014 11:38 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/20/2014 11:38 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/20/2014 11:38 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/20/2014 11:38 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/20/2014 11:38 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/20/2014 11:38 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/20/2014 11:38 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/20/2014 11:38 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/20/2014 11:38 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/20/2014 11:38 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/20/2014 11:38 AM
Page 5 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:28:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-02A Matrix:Groundwater
MW-13Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/20/2014 11:38 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/20/2014 11:38 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/20/2014 11:38 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/20/2014 11:38 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/20/2014 11:38 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/20/2014 11:38 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/20/2014 11:38 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/20/2014 11:38 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/20/2014 11:38 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/20/2014 11:38 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/20/2014 11:38 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/20/2014 11:38 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/20/2014 11:38 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/20/2014 11:38 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/20/2014 11:38 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/20/2014 11:38 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/20/2014 11:38 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/20/2014 11:38 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/20/2014 11:38 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/20/2014 11:38 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/20/2014 11:38 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/20/2014 11:38 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/20/2014 11:38 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/20/2014 11:38 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/20/2014 11:38 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/20/2014 11:38 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/20/2014 11:38 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/20/2014 11:38 AM
Surr: 1,2-Dichloroethane-d4 89.0 68.7-129 %RECNANA 9/20/2014 11:38 AM
Surr: 4-Bromofluorobenzene 104 71.8-127 %RECNANA 9/20/2014 11:38 AM
Surr: Dibromofluoromethane 100 74.3-124 %RECNANA 9/20/2014 11:38 AM
Surr: Toluene-d8 102 71.4-129 %RECNANA 9/20/2014 11:38 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 37.0 10 mg/L2.0 NA PA/VA9/18/2014 8:20 AM
Page 6 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:07:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-03A Matrix:Groundwater
MW-14Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/19/2014 3:00 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:00 PM
Barium 0.0586 0.100 J mg/L0.0010 NA PA/VA9/19/2014 3:00 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:00 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:00 PM
Chromium 0.0027 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:00 PM
Cobalt 0.0014 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:00 PM
Copper 0.0064 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:00 PM
Lead 0.0004 0.0100 J mg/L0.0002 NA PA/VA9/19/2014 3:00 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA9/19/2014 3:00 PM
Selenium 0.0013 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:00 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:00 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/19/2014 3:00 PM
Vanadium 0.0136 0.0250 J mg/L0.0010 NA PA/VA9/19/2014 3:00 PM
Zinc 0.0056 0.0100 J mg/L0.0030 NA PA/VA9/19/2014 3:00 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/20/2014 12:11 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/20/2014 12:11 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/20/2014 12:11 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/20/2014 12:11 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/20/2014 12:11 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/20/2014 12:11 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/20/2014 12:11 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/20/2014 12:11 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/20/2014 12:11 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/20/2014 12:11 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/20/2014 12:11 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/20/2014 12:11 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/20/2014 12:11 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/20/2014 12:11 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/20/2014 12:11 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/20/2014 12:11 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/20/2014 12:11 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/20/2014 12:11 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/20/2014 12:11 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/20/2014 12:11 PM
Page 7 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:07:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-03A Matrix:Groundwater
MW-14Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/20/2014 12:11 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/20/2014 12:11 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/20/2014 12:11 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/20/2014 12:11 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/20/2014 12:11 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/20/2014 12:11 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/20/2014 12:11 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/20/2014 12:11 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/20/2014 12:11 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/20/2014 12:11 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/20/2014 12:11 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/20/2014 12:11 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/20/2014 12:11 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/20/2014 12:11 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/20/2014 12:11 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/20/2014 12:11 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/20/2014 12:11 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/20/2014 12:11 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/20/2014 12:11 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/20/2014 12:11 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/20/2014 12:11 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/20/2014 12:11 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/20/2014 12:11 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/20/2014 12:11 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/20/2014 12:11 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/20/2014 12:11 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/20/2014 12:11 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/20/2014 12:11 PM
Surr: 1,2-Dichloroethane-d4 88.1 68.7-129 %RECNANA 9/20/2014 12:11 PM
Surr: 4-Bromofluorobenzene 110 71.8-127 %RECNANA 9/20/2014 12:11 PM
Surr: Dibromofluoromethane 99.8 74.3-124 %RECNANA 9/20/2014 12:11 PM
Surr: Toluene-d8 104 71.4-129 %RECNANA 9/20/2014 12:11 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 14.0 10 mg/L2.0 NA PA/VA9/18/2014 8:20 AM
Page 8 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 3:38:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-04A Matrix:Groundwater
MW-15Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/19/2014 3:06 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:06 PM
Barium 0.0221 0.100 J mg/L0.0010 NA PA/VA9/19/2014 3:06 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:06 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:06 PM
Chromium 0.0035 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:06 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:06 PM
Copper 0.0033 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:06 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/19/2014 3:06 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA9/19/2014 3:06 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:06 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:06 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/19/2014 3:06 PM
Vanadium 0.0018 0.0250 J mg/L0.0010 NA PA/VA9/19/2014 3:06 PM
Zinc 0.0077 0.0100 J mg/L0.0030 NA PA/VA9/19/2014 3:06 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/24/2014 4:33 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/24/2014 4:33 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/24/2014 4:33 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/24/2014 4:33 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/24/2014 4:33 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/24/2014 4:33 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/24/2014 4:33 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/24/2014 4:33 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/24/2014 4:33 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/24/2014 4:33 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/24/2014 4:33 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/24/2014 4:33 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/24/2014 4:33 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/24/2014 4:33 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/24/2014 4:33 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/24/2014 4:33 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/24/2014 4:33 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/24/2014 4:33 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/24/2014 4:33 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/24/2014 4:33 PM
Page 9 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 3:38:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-04A Matrix:Groundwater
MW-15Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/24/2014 4:33 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/24/2014 4:33 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/24/2014 4:33 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/24/2014 4:33 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/24/2014 4:33 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/24/2014 4:33 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/24/2014 4:33 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/24/2014 4:33 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/24/2014 4:33 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/24/2014 4:33 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/24/2014 4:33 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/24/2014 4:33 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/24/2014 4:33 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/24/2014 4:33 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/24/2014 4:33 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/24/2014 4:33 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/24/2014 4:33 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/24/2014 4:33 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/24/2014 4:33 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/24/2014 4:33 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/24/2014 4:33 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/24/2014 4:33 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/24/2014 4:33 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/24/2014 4:33 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/24/2014 4:33 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/24/2014 4:33 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/24/2014 4:33 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/24/2014 4:33 PM
Surr: 1,2-Dichloroethane-d4 107 68.7-129 %RECNANA 9/24/2014 4:33 PM
Surr: 4-Bromofluorobenzene 108 71.8-127 %RECNANA 9/24/2014 4:33 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 9/24/2014 4:33 PM
Surr: Toluene-d8 102 71.4-129 %RECNANA 9/24/2014 4:33 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 7.0 5.0 mg/L1.0 NA PA/VA9/18/2014 8:20 AM
Page 10 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:55:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-05A Matrix:Groundwater
MW-16Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/19/2014 3:11 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:11 PM
Barium 0.217 0.100 mg/L0.0010 NA PA/VA9/19/2014 3:11 PM
Beryllium 0.0008 0.0010 J mg/L0.0002 NA PA/VA9/19/2014 3:11 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:11 PM
Chromium 0.0093 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:11 PM
Cobalt 0.0214 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:11 PM
Copper 0.0168 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:11 PM
Lead 0.0025 0.0100 J mg/L0.0002 NA PA/VA9/19/2014 3:11 PM
Nickel 0.0023 0.0500 J mg/L0.0020 NA PA/VA9/19/2014 3:11 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:11 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:11 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/19/2014 3:11 PM
Vanadium 0.0387 0.0250 mg/L0.0010 NA PA/VA9/19/2014 3:11 PM
Zinc 0.0393 0.0100 mg/L0.0030 NA PA/VA9/19/2014 3:11 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/24/2014 5:06 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/24/2014 5:06 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/24/2014 5:06 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/24/2014 5:06 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/24/2014 5:06 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/24/2014 5:06 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/24/2014 5:06 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/24/2014 5:06 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/24/2014 5:06 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/24/2014 5:06 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/24/2014 5:06 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/24/2014 5:06 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/24/2014 5:06 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/24/2014 5:06 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/24/2014 5:06 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/24/2014 5:06 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/24/2014 5:06 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/24/2014 5:06 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/24/2014 5:06 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/24/2014 5:06 PM
Page 11 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:55:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-05A Matrix:Groundwater
MW-16Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/24/2014 5:06 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/24/2014 5:06 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/24/2014 5:06 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/24/2014 5:06 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/24/2014 5:06 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/24/2014 5:06 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/24/2014 5:06 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/24/2014 5:06 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/24/2014 5:06 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/24/2014 5:06 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/24/2014 5:06 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/24/2014 5:06 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/24/2014 5:06 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/24/2014 5:06 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/24/2014 5:06 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/24/2014 5:06 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/24/2014 5:06 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/24/2014 5:06 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/24/2014 5:06 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/24/2014 5:06 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/24/2014 5:06 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/24/2014 5:06 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/24/2014 5:06 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/24/2014 5:06 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/24/2014 5:06 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/24/2014 5:06 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/24/2014 5:06 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/24/2014 5:06 PM
Surr: 1,2-Dichloroethane-d4 107 68.7-129 %RECNANA 9/24/2014 5:06 PM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 9/24/2014 5:06 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 9/24/2014 5:06 PM
Surr: Toluene-d8 102 71.4-129 %RECNANA 9/24/2014 5:06 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 135 10 mg/L2.0 NA PA/VA9/18/2014 8:20 AM
Page 12 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:30:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-06A Matrix:Groundwater
MW-17Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/19/2014 3:17 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:17 PM
Barium 0.0639 0.100 J mg/L0.0010 NA PA/VA9/19/2014 3:17 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:17 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:17 PM
Chromium 0.0027 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:17 PM
Cobalt 0.0054 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:17 PM
Copper 0.0066 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:17 PM
Lead 0.0007 0.0100 J mg/L0.0002 NA PA/VA9/19/2014 3:17 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA9/19/2014 3:17 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:17 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:17 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/19/2014 3:17 PM
Vanadium 0.0085 0.0250 J mg/L0.0010 NA PA/VA9/19/2014 3:17 PM
Zinc 0.0093 0.0100 J mg/L0.0030 NA PA/VA9/19/2014 3:17 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/24/2014 5:39 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/24/2014 5:39 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/24/2014 5:39 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/24/2014 5:39 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/24/2014 5:39 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/24/2014 5:39 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/24/2014 5:39 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/24/2014 5:39 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/24/2014 5:39 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/24/2014 5:39 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/24/2014 5:39 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/24/2014 5:39 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/24/2014 5:39 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/24/2014 5:39 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/24/2014 5:39 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/24/2014 5:39 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/24/2014 5:39 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/24/2014 5:39 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/24/2014 5:39 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/24/2014 5:39 PM
Page 13 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:30:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-06A Matrix:Groundwater
MW-17Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/24/2014 5:39 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/24/2014 5:39 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/24/2014 5:39 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/24/2014 5:39 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/24/2014 5:39 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/24/2014 5:39 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/24/2014 5:39 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/24/2014 5:39 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/24/2014 5:39 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/24/2014 5:39 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/24/2014 5:39 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/24/2014 5:39 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/24/2014 5:39 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/24/2014 5:39 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/24/2014 5:39 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/24/2014 5:39 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/24/2014 5:39 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/24/2014 5:39 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/24/2014 5:39 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/24/2014 5:39 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/24/2014 5:39 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/24/2014 5:39 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/24/2014 5:39 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/24/2014 5:39 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/24/2014 5:39 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/24/2014 5:39 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/24/2014 5:39 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/24/2014 5:39 PM
Surr: 1,2-Dichloroethane-d4 104 68.7-129 %RECNANA 9/24/2014 5:39 PM
Surr: 4-Bromofluorobenzene 108 71.8-127 %RECNANA 9/24/2014 5:39 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 9/24/2014 5:39 PM
Surr: Toluene-d8 102 71.4-129 %RECNANA 9/24/2014 5:39 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 33.0 10 mg/L2.0 NA PA/VA9/18/2014 8:20 AM
Page 14 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 3:08:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-07A Matrix:Groundwater
U-2Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/19/2014 3:23 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:23 PM
Barium 0.0815 0.100 J mg/L0.0010 NA PA/VA9/19/2014 3:23 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:23 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:23 PM
Chromium ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:23 PM
Cobalt 0.0065 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:23 PM
Copper 0.0017 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:23 PM
Lead 0.0002 0.0100 J mg/L0.0002 NA PA/VA9/19/2014 3:23 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA9/19/2014 3:23 PM
Selenium 0.0011 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:23 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:23 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/19/2014 3:23 PM
Vanadium 0.0014 0.0250 J mg/L0.0010 NA PA/VA9/19/2014 3:23 PM
Zinc 0.0066 0.0100 J mg/L0.0030 NA PA/VA9/19/2014 3:23 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/24/2014 6:12 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/24/2014 6:12 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/24/2014 6:12 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/24/2014 6:12 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/24/2014 6:12 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/24/2014 6:12 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/24/2014 6:12 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/24/2014 6:12 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/24/2014 6:12 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/24/2014 6:12 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/24/2014 6:12 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/24/2014 6:12 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/24/2014 6:12 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/24/2014 6:12 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/24/2014 6:12 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/24/2014 6:12 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/24/2014 6:12 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/24/2014 6:12 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/24/2014 6:12 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/24/2014 6:12 PM
Page 15 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 3:08:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-07A Matrix:Groundwater
U-2Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/24/2014 6:12 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/24/2014 6:12 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/24/2014 6:12 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/24/2014 6:12 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/24/2014 6:12 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/24/2014 6:12 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/24/2014 6:12 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/24/2014 6:12 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/24/2014 6:12 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/24/2014 6:12 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/24/2014 6:12 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/24/2014 6:12 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/24/2014 6:12 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/24/2014 6:12 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/24/2014 6:12 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/24/2014 6:12 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/24/2014 6:12 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/24/2014 6:12 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/24/2014 6:12 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/24/2014 6:12 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/24/2014 6:12 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/24/2014 6:12 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/24/2014 6:12 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/24/2014 6:12 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/24/2014 6:12 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/24/2014 6:12 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/24/2014 6:12 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/24/2014 6:12 PM
Surr: 1,2-Dichloroethane-d4 105 68.7-129 %RECNANA 9/24/2014 6:12 PM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 9/24/2014 6:12 PM
Surr: Dibromofluoromethane 104 74.3-124 %RECNANA 9/24/2014 6:12 PM
Surr: Toluene-d8 101 71.4-129 %RECNANA 9/24/2014 6:12 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 24.0 10 mg/L2.0 NA PA/VA9/18/2014 8:20 AM
Page 16 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 3:16:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-08A Matrix:Groundwater
U-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony 0.0004 0.0060 J mg/L0.0002 NA PA/VA9/19/2014 3:40 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:40 PM
Barium 0.162 0.100 mg/L0.0010 NA PA/VA9/19/2014 3:40 PM
Beryllium 0.0005 0.0010 J mg/L0.0002 NA PA/VA9/19/2014 3:40 PM
Cadmium 0.0004 0.0010 J mg/L0.0002 NA PA/VA9/19/2014 3:40 PM
Chromium 0.0432 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:40 PM
Cobalt 0.0083 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:40 PM
Copper 0.0279 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:40 PM
Lead 0.0098 0.0100 J mg/L0.0002 NA PA/VA9/19/2014 3:40 PM
Nickel 0.0077 0.0500 J mg/L0.0020 NA PA/VA9/19/2014 3:40 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:40 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:40 PM
Thallium 0.0002 0.0055 J mg/L0.0002 NA PA/VA9/19/2014 3:40 PM
Vanadium 0.0845 0.0250 mg/L0.0010 NA PA/VA9/19/2014 3:40 PM
Zinc 0.0628 0.0100 mg/L0.0030 NA PA/VA9/19/2014 3:40 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/24/2014 6:45 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/24/2014 6:45 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/24/2014 6:45 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/24/2014 6:45 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/24/2014 6:45 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/24/2014 6:45 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/24/2014 6:45 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/24/2014 6:45 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/24/2014 6:45 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/24/2014 6:45 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/24/2014 6:45 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/24/2014 6:45 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/24/2014 6:45 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/24/2014 6:45 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/24/2014 6:45 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/24/2014 6:45 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/24/2014 6:45 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/24/2014 6:45 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/24/2014 6:45 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/24/2014 6:45 PM
Page 17 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 3:16:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-08A Matrix:Groundwater
U-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/24/2014 6:45 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/24/2014 6:45 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/24/2014 6:45 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/24/2014 6:45 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/24/2014 6:45 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/24/2014 6:45 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/24/2014 6:45 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/24/2014 6:45 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/24/2014 6:45 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/24/2014 6:45 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/24/2014 6:45 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/24/2014 6:45 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/24/2014 6:45 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/24/2014 6:45 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/24/2014 6:45 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/24/2014 6:45 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/24/2014 6:45 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/24/2014 6:45 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/24/2014 6:45 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/24/2014 6:45 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/24/2014 6:45 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/24/2014 6:45 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/24/2014 6:45 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/24/2014 6:45 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/24/2014 6:45 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/24/2014 6:45 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/24/2014 6:45 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/24/2014 6:45 PM
Surr: 1,2-Dichloroethane-d4 105 68.7-129 %RECNANA 9/24/2014 6:45 PM
Surr: 4-Bromofluorobenzene 108 71.8-127 %RECNANA 9/24/2014 6:45 PM
Surr: Dibromofluoromethane 103 74.3-124 %RECNANA 9/24/2014 6:45 PM
Surr: Toluene-d8 101 71.4-129 %RECNANA 9/24/2014 6:45 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 489 10 mg/L2.0 NA PA/VA9/18/2014 8:20 AM
Page 18 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 3:38:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-09A Matrix:Groundwater
MW-15 DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/19/2014 3:45 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:45 PM
Barium 0.0233 0.100 J mg/L0.0010 NA PA/VA9/19/2014 3:45 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:45 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/19/2014 3:45 PM
Chromium 0.0030 0.0100 J mg/L0.0010 NA PA/VA9/19/2014 3:45 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:45 PM
Copper 0.0019 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 11:24 AM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/19/2014 3:45 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA9/19/2014 3:45 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:45 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/19/2014 3:45 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/19/2014 3:45 PM
Vanadium 0.0015 0.0250 J mg/L0.0010 NA PA/VA9/19/2014 3:45 PM
Zinc 0.0031 0.0100 J mg/L0.0030 NA PA/VA9/24/2014 11:24 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/24/2014 7:18 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/24/2014 7:18 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/24/2014 7:18 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/24/2014 7:18 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/24/2014 7:18 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/24/2014 7:18 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/24/2014 7:18 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/24/2014 7:18 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/24/2014 7:18 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/24/2014 7:18 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/24/2014 7:18 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/24/2014 7:18 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/24/2014 7:18 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/24/2014 7:18 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/24/2014 7:18 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/24/2014 7:18 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/24/2014 7:18 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/24/2014 7:18 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/24/2014 7:18 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/24/2014 7:18 PM
Page 19 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 3:38:00 PM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-09A Matrix:Groundwater
MW-15 DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/24/2014 7:18 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/24/2014 7:18 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/24/2014 7:18 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/24/2014 7:18 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/24/2014 7:18 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/24/2014 7:18 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/24/2014 7:18 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/24/2014 7:18 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/24/2014 7:18 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/24/2014 7:18 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/24/2014 7:18 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/24/2014 7:18 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/24/2014 7:18 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/24/2014 7:18 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/24/2014 7:18 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/24/2014 7:18 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/24/2014 7:18 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/24/2014 7:18 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/24/2014 7:18 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/24/2014 7:18 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/24/2014 7:18 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/24/2014 7:18 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/24/2014 7:18 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/24/2014 7:18 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/24/2014 7:18 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/24/2014 7:18 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/24/2014 7:18 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/24/2014 7:18 PM
Surr: 1,2-Dichloroethane-d4 108 68.7-129 %RECNANA 9/24/2014 7:18 PM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 9/24/2014 7:18 PM
Surr: Dibromofluoromethane 106 74.3-124 %RECNANA 9/24/2014 7:18 PM
Surr: Toluene-d8 102 71.4-129 %RECNANA 9/24/2014 7:18 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 11.5 5.0 mg/L1.0 NA PA/VA9/18/2014 8:20 AM
Page 20 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:00:00 AM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-10A Matrix:Trip Blank
TRIP BLANKClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/20/2014 11:04 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/20/2014 11:04 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/20/2014 11:04 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/20/2014 11:04 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/20/2014 11:04 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/20/2014 11:04 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/20/2014 11:04 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/20/2014 11:04 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/20/2014 11:04 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/20/2014 11:04 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/20/2014 11:04 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/20/2014 11:04 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/20/2014 11:04 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/20/2014 11:04 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/20/2014 11:04 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/20/2014 11:04 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/20/2014 11:04 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/20/2014 11:04 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/20/2014 11:04 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/20/2014 11:04 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/20/2014 11:04 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/20/2014 11:04 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/20/2014 11:04 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/20/2014 11:04 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/20/2014 11:04 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/20/2014 11:04 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/20/2014 11:04 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/20/2014 11:04 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/20/2014 11:04 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/20/2014 11:04 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/20/2014 11:04 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/20/2014 11:04 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/20/2014 11:04 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/20/2014 11:04 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/20/2014 11:04 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/20/2014 11:04 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/20/2014 11:04 AM
Page 21 of 22
WO#: 1409J28
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:00:00 AM
Project:BLACKBURN SUBTITLE D
Lab ID:1409J28-10A Matrix:Trip Blank
TRIP BLANKClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.C.Site ID:
NELAP
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/20/2014 11:04 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/20/2014 11:04 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/20/2014 11:04 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/20/2014 11:04 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/20/2014 11:04 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/20/2014 11:04 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/20/2014 11:04 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/20/2014 11:04 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/20/2014 11:04 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/20/2014 11:04 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/20/2014 11:04 AM
Surr: 1,2-Dichloroethane-d4 86.1 68.7-129 %RECNANA 9/20/2014 11:04 AM
Surr: 4-Bromofluorobenzene 111 71.8-127 %RECNANA 9/20/2014 11:04 AM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 9/20/2014 11:04 AM
Surr: Toluene-d8 103 71.4-129 %RECNANA 9/20/2014 11:04 AM
Page 22 of 22
DB
P i x
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Unit 3
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver, WV 25813 800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Monday, September 29, 2014
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:UNIT 3
Work Order #:1409J47
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 8 sample(s) on 9/17/2014 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Case Narrative
Client:
Project:UNIT 3
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 1:27:00 PM
Project:UNIT 3
Lab ID:1409J47-01A Matrix:Groundwater
MW-31Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 3:10 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:10 PM
Barium 0.335 0.100 mg/L0.0010 NA PA/VA9/24/2014 3:10 PM
Beryllium 0.0002 0.0010 J mg/L0.0002 NA PA/VA9/24/2014 3:10 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:10 PM
Chromium 0.0227 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:10 PM
Cobalt 0.0075 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 3:10 PM
Copper 0.0358 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:10 PM
Lead 0.0026 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 3:10 PM
Nickel 0.0132 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 3:10 PM
Selenium 0.0014 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 3:10 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:10 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 3:10 PM
Vanadium 0.0254 0.0250 mg/L0.0010 NA PA/VA9/24/2014 3:10 PM
Zinc 0.0167 0.0100 mg/L0.0030 NA PA/VA9/24/2014 3:10 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 4:08 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/25/2014 4:08 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/25/2014 4:08 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/25/2014 4:08 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/25/2014 4:08 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/25/2014 4:08 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/25/2014 4:08 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/25/2014 4:08 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/25/2014 4:08 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/25/2014 4:08 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/25/2014 4:08 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/25/2014 4:08 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/25/2014 4:08 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/25/2014 4:08 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/25/2014 4:08 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/25/2014 4:08 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/25/2014 4:08 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/25/2014 4:08 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/25/2014 4:08 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/25/2014 4:08 AM
Page 3 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 1:27:00 PM
Project:UNIT 3
Lab ID:1409J47-01A Matrix:Groundwater
MW-31Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/25/2014 4:08 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/25/2014 4:08 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 4:08 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/25/2014 4:08 AM
cis-1,2-Dichloroethene 0.440 5.00 J µg/L0.226 NA PA/VA9/25/2014 4:08 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/25/2014 4:08 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/25/2014 4:08 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/25/2014 4:08 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/25/2014 4:08 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/25/2014 4:08 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/25/2014 4:08 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/25/2014 4:08 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/25/2014 4:08 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/25/2014 4:08 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/25/2014 4:08 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/25/2014 4:08 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/25/2014 4:08 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/25/2014 4:08 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/25/2014 4:08 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/25/2014 4:08 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/25/2014 4:08 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/25/2014 4:08 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/25/2014 4:08 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/25/2014 4:08 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/25/2014 4:08 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/25/2014 4:08 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/25/2014 4:08 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/25/2014 4:08 AM
Surr: 1,2-Dichloroethane-d4 111 68.7-129 %RECNANA 9/25/2014 4:08 AM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 9/25/2014 4:08 AM
Surr: Dibromofluoromethane 106 74.3-124 %RECNANA 9/25/2014 4:08 AM
Surr: Toluene-d8 100 71.4-129 %RECNANA 9/25/2014 4:08 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 363 10 mg/L2.0 NA PA/VA9/18/2014 8:45 AM
Page 4 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 1:55:00 PM
Project:UNIT 3
Lab ID:1409J47-02A Matrix:Groundwater
MW-32Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 3:16 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:16 PM
Barium 0.373 0.100 mg/L0.0010 NA PA/VA9/24/2014 3:16 PM
Beryllium 0.0011 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:16 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:16 PM
Chromium 0.0411 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:16 PM
Cobalt 0.0144 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:16 PM
Copper 0.0183 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:16 PM
Lead 0.0086 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 3:16 PM
Nickel 0.0105 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 3:16 PM
Selenium ND 0.0100 mg/L0.0050 NA PA/VA9/24/2014 3:16 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:16 PM
Thallium 0.0002 0.0055 J mg/L0.0002 NA PA/VA9/24/2014 3:16 PM
Vanadium 0.0940 0.0250 mg/L0.0010 NA PA/VA9/24/2014 3:16 PM
Zinc 0.0250 0.0100 mg/L0.0030 NA PA/VA9/24/2014 3:16 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 4:41 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/25/2014 4:41 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/25/2014 4:41 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/25/2014 4:41 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/25/2014 4:41 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/25/2014 4:41 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/25/2014 4:41 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/25/2014 4:41 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/25/2014 4:41 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/25/2014 4:41 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/25/2014 4:41 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/25/2014 4:41 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/25/2014 4:41 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/25/2014 4:41 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/25/2014 4:41 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/25/2014 4:41 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/25/2014 4:41 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/25/2014 4:41 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/25/2014 4:41 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/25/2014 4:41 AM
Page 5 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 1:55:00 PM
Project:UNIT 3
Lab ID:1409J47-02A Matrix:Groundwater
MW-32Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/25/2014 4:41 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/25/2014 4:41 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 4:41 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/25/2014 4:41 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/25/2014 4:41 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/25/2014 4:41 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/25/2014 4:41 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/25/2014 4:41 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/25/2014 4:41 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/25/2014 4:41 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/25/2014 4:41 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/25/2014 4:41 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/25/2014 4:41 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/25/2014 4:41 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/25/2014 4:41 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/25/2014 4:41 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/25/2014 4:41 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/25/2014 4:41 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/25/2014 4:41 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/25/2014 4:41 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/25/2014 4:41 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/25/2014 4:41 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/25/2014 4:41 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/25/2014 4:41 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/25/2014 4:41 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/25/2014 4:41 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/25/2014 4:41 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/25/2014 4:41 AM
Surr: 1,2-Dichloroethane-d4 110 68.7-129 %RECNANA 9/25/2014 4:41 AM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/25/2014 4:41 AM
Surr: Dibromofluoromethane 107 74.3-124 %RECNANA 9/25/2014 4:41 AM
Surr: Toluene-d8 98.4 71.4-129 %RECNANA 9/25/2014 4:41 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 8,560 20.0 mg/L4.0 NA PA/VA9/18/2014 8:45 AM
Page 6 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:23:00 PM
Project:UNIT 3
Lab ID:1409J47-03A Matrix:Groundwater
MW-33Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 3:22 PM
Arsenic ND 0.0100 mg/L0.0050 NA PA/VA9/24/2014 3:22 PM
Barium 0.289 0.100 mg/L0.0010 NA PA/VA9/24/2014 3:22 PM
Beryllium 0.0018 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:22 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:22 PM
Chromium 0.0283 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:22 PM
Cobalt 0.0206 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:22 PM
Copper 0.0172 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:22 PM
Lead 0.0108 0.0100 mg/L0.0002 NA PA/VA9/24/2014 3:22 PM
Nickel 0.0101 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 3:22 PM
Selenium ND 0.0100 mg/L0.0050 NA PA/VA9/24/2014 3:22 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:22 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 3:22 PM
Vanadium 0.153 0.0250 mg/L0.0010 NA PA/VA9/24/2014 3:22 PM
Zinc 0.0342 0.0100 mg/L0.0030 NA PA/VA9/24/2014 3:22 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 5:15 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/25/2014 5:15 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/25/2014 5:15 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/25/2014 5:15 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/25/2014 5:15 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/25/2014 5:15 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/25/2014 5:15 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/25/2014 5:15 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/25/2014 5:15 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/25/2014 5:15 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/25/2014 5:15 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/25/2014 5:15 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/25/2014 5:15 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/25/2014 5:15 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/25/2014 5:15 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/25/2014 5:15 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/25/2014 5:15 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/25/2014 5:15 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/25/2014 5:15 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/25/2014 5:15 AM
Page 7 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:23:00 PM
Project:UNIT 3
Lab ID:1409J47-03A Matrix:Groundwater
MW-33Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/25/2014 5:15 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/25/2014 5:15 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 5:15 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/25/2014 5:15 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/25/2014 5:15 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/25/2014 5:15 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/25/2014 5:15 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/25/2014 5:15 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/25/2014 5:15 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/25/2014 5:15 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/25/2014 5:15 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/25/2014 5:15 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/25/2014 5:15 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/25/2014 5:15 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/25/2014 5:15 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/25/2014 5:15 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/25/2014 5:15 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/25/2014 5:15 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/25/2014 5:15 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/25/2014 5:15 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/25/2014 5:15 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/25/2014 5:15 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/25/2014 5:15 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/25/2014 5:15 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/25/2014 5:15 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/25/2014 5:15 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/25/2014 5:15 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/25/2014 5:15 AM
Surr: 1,2-Dichloroethane-d4 109 68.7-129 %RECNANA 9/25/2014 5:15 AM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/25/2014 5:15 AM
Surr: Dibromofluoromethane 107 74.3-124 %RECNANA 9/25/2014 5:15 AM
Surr: Toluene-d8 99.3 71.4-129 %RECNANA 9/25/2014 5:15 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 1,310 10 mg/L2.0 NA PA/VA9/18/2014 8:45 AM
Page 8 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:50:00 PM
Project:UNIT 3
Lab ID:1409J47-04A Matrix:Groundwater
MW-34Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 3:39 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:39 PM
Barium 0.306 0.100 mg/L0.0010 NA PA/VA9/24/2014 3:39 PM
Beryllium 0.0004 0.0010 J mg/L0.0002 NA PA/VA9/24/2014 3:39 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:39 PM
Chromium 0.0322 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:39 PM
Cobalt 0.0097 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 3:39 PM
Copper 0.0213 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:39 PM
Lead 0.0025 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 3:39 PM
Nickel 0.0155 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 3:39 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:39 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:39 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 3:39 PM
Vanadium 0.0327 0.0250 mg/L0.0010 NA PA/VA9/24/2014 3:39 PM
Zinc 0.0215 0.0100 mg/L0.0030 NA PA/VA9/24/2014 3:39 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 5:47 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/25/2014 5:47 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/25/2014 5:47 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/25/2014 5:47 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/25/2014 5:47 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/25/2014 5:47 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/25/2014 5:47 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/25/2014 5:47 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/25/2014 5:47 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/25/2014 5:47 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/25/2014 5:47 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/25/2014 5:47 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/25/2014 5:47 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/25/2014 5:47 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/25/2014 5:47 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/25/2014 5:47 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/25/2014 5:47 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/25/2014 5:47 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/25/2014 5:47 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/25/2014 5:47 AM
Page 9 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:50:00 PM
Project:UNIT 3
Lab ID:1409J47-04A Matrix:Groundwater
MW-34Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/25/2014 5:47 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/25/2014 5:47 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 5:47 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/25/2014 5:47 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/25/2014 5:47 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/25/2014 5:47 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/25/2014 5:47 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/25/2014 5:47 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/25/2014 5:47 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/25/2014 5:47 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/25/2014 5:47 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/25/2014 5:47 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/25/2014 5:47 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/25/2014 5:47 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/25/2014 5:47 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/25/2014 5:47 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/25/2014 5:47 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/25/2014 5:47 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/25/2014 5:47 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/25/2014 5:47 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/25/2014 5:47 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/25/2014 5:47 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/25/2014 5:47 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/25/2014 5:47 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/25/2014 5:47 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/25/2014 5:47 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/25/2014 5:47 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/25/2014 5:47 AM
Surr: 1,2-Dichloroethane-d4 108 68.7-129 %RECNANA 9/25/2014 5:47 AM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 9/25/2014 5:47 AM
Surr: Dibromofluoromethane 109 74.3-124 %RECNANA 9/25/2014 5:47 AM
Surr: Toluene-d8 99.7 71.4-129 %RECNANA 9/25/2014 5:47 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 238 10 mg/L2.0 NA PA/VA9/18/2014 8:45 AM
Page 10 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:05:00 PM
Project:UNIT 3
Lab ID:1409J47-05A Matrix:Groundwater
SW-4Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 3:44 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:44 PM
Barium 0.0349 0.100 J mg/L0.0010 NA PA/VA9/24/2014 3:44 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:44 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:44 PM
Chromium 0.0012 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 3:44 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:44 PM
Copper 0.0016 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 3:44 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/24/2014 3:44 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA9/24/2014 3:44 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:44 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:44 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 3:44 PM
Vanadium 0.0021 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 3:44 PM
Zinc 0.0036 0.0100 J mg/L0.0030 NA PA/VA9/24/2014 3:44 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 6:21 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/25/2014 6:21 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/25/2014 6:21 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/25/2014 6:21 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/25/2014 6:21 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/25/2014 6:21 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/25/2014 6:21 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/25/2014 6:21 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/25/2014 6:21 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/25/2014 6:21 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/25/2014 6:21 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/25/2014 6:21 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/25/2014 6:21 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/25/2014 6:21 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/25/2014 6:21 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/25/2014 6:21 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/25/2014 6:21 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/25/2014 6:21 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/25/2014 6:21 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/25/2014 6:21 AM
Page 11 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:05:00 PM
Project:UNIT 3
Lab ID:1409J47-05A Matrix:Groundwater
SW-4Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/25/2014 6:21 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/25/2014 6:21 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 6:21 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/25/2014 6:21 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/25/2014 6:21 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/25/2014 6:21 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/25/2014 6:21 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/25/2014 6:21 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/25/2014 6:21 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/25/2014 6:21 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/25/2014 6:21 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/25/2014 6:21 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/25/2014 6:21 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/25/2014 6:21 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/25/2014 6:21 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/25/2014 6:21 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/25/2014 6:21 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/25/2014 6:21 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/25/2014 6:21 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/25/2014 6:21 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/25/2014 6:21 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/25/2014 6:21 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/25/2014 6:21 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/25/2014 6:21 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/25/2014 6:21 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/25/2014 6:21 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/25/2014 6:21 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/25/2014 6:21 AM
Surr: 1,2-Dichloroethane-d4 114 68.7-129 %RECNANA 9/25/2014 6:21 AM
Surr: 4-Bromofluorobenzene 108 71.8-127 %RECNANA 9/25/2014 6:21 AM
Surr: Dibromofluoromethane 109 74.3-124 %RECNANA 9/25/2014 6:21 AM
Surr: Toluene-d8 99.3 71.4-129 %RECNANA 9/25/2014 6:21 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 11.0 10 mg/L2.0 NA PA/VA9/18/2014 8:45 AM
Page 12 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:32:00 PM
Project:UNIT 3
Lab ID:1409J47-06A Matrix:Groundwater
SW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 3:50 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:50 PM
Barium 0.0566 0.100 J mg/L0.0010 NA PA/VA9/24/2014 3:50 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:50 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:50 PM
Chromium 0.0037 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 3:50 PM
Cobalt 0.0013 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 3:50 PM
Copper 0.0025 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 3:50 PM
Lead 0.0004 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 3:50 PM
Nickel 0.0021 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 3:50 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:50 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:50 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 3:50 PM
Vanadium 0.0063 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 3:50 PM
Zinc 0.0032 0.0100 J mg/L0.0030 NA PA/VA9/24/2014 3:50 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 6:54 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/25/2014 6:54 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/25/2014 6:54 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/25/2014 6:54 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/25/2014 6:54 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/25/2014 6:54 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/25/2014 6:54 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/25/2014 6:54 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/25/2014 6:54 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/25/2014 6:54 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/25/2014 6:54 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/25/2014 6:54 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/25/2014 6:54 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/25/2014 6:54 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/25/2014 6:54 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/25/2014 6:54 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/25/2014 6:54 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/25/2014 6:54 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/25/2014 6:54 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/25/2014 6:54 AM
Page 13 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 4:32:00 PM
Project:UNIT 3
Lab ID:1409J47-06A Matrix:Groundwater
SW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/25/2014 6:54 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/25/2014 6:54 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 6:54 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/25/2014 6:54 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/25/2014 6:54 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/25/2014 6:54 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/25/2014 6:54 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/25/2014 6:54 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/25/2014 6:54 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/25/2014 6:54 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/25/2014 6:54 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/25/2014 6:54 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/25/2014 6:54 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/25/2014 6:54 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/25/2014 6:54 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/25/2014 6:54 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/25/2014 6:54 AM
Tetrachloroethene 0.370 1.00 J µg/L0.196 NA PA/VA9/25/2014 6:54 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/25/2014 6:54 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/25/2014 6:54 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/25/2014 6:54 AM
Trichloroethene 1.01 1.00 µg/L0.302 NA PA/VA9/25/2014 6:54 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/25/2014 6:54 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/25/2014 6:54 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/25/2014 6:54 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/25/2014 6:54 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/25/2014 6:54 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/25/2014 6:54 AM
Surr: 1,2-Dichloroethane-d4 108 68.7-129 %RECNANA 9/25/2014 6:54 AM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 9/25/2014 6:54 AM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 9/25/2014 6:54 AM
Surr: Toluene-d8 100 71.4-129 %RECNANA 9/25/2014 6:54 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 17.0 10 mg/L2.0 NA PA/VA9/18/2014 8:45 AM
Page 14 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:50:00 PM
Project:UNIT 3
Lab ID:1409J47-07A Matrix:Groundwater
MW- 34 DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 3:55 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:55 PM
Barium 0.309 0.100 mg/L0.0010 NA PA/VA9/24/2014 3:55 PM
Beryllium 0.0006 0.0010 J mg/L0.0002 NA PA/VA9/24/2014 3:55 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 3:55 PM
Chromium 0.0464 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:55 PM
Cobalt 0.0108 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:55 PM
Copper 0.0313 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:55 PM
Lead 0.0035 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 3:55 PM
Nickel 0.0215 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 3:55 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:55 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 3:55 PM
Thallium 0.0003 0.0055 J mg/L0.0002 NA PA/VA9/24/2014 3:55 PM
Vanadium 0.0519 0.0250 mg/L0.0010 NA PA/VA9/24/2014 3:55 PM
Zinc 0.0280 0.0100 mg/L0.0030 NA PA/VA9/24/2014 3:55 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 8:00 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/25/2014 8:00 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/25/2014 8:00 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/25/2014 8:00 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/25/2014 8:00 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/25/2014 8:00 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/25/2014 8:00 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/25/2014 8:00 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/25/2014 8:00 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/25/2014 8:00 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/25/2014 8:00 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/25/2014 8:00 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/25/2014 8:00 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/25/2014 8:00 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/25/2014 8:00 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/25/2014 8:00 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/25/2014 8:00 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/25/2014 8:00 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/25/2014 8:00 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/25/2014 8:00 AM
Page 15 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 2:50:00 PM
Project:UNIT 3
Lab ID:1409J47-07A Matrix:Groundwater
MW- 34 DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/25/2014 8:00 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/25/2014 8:00 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 8:00 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/25/2014 8:00 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/25/2014 8:00 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/25/2014 8:00 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/25/2014 8:00 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/25/2014 8:00 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/25/2014 8:00 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/25/2014 8:00 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/25/2014 8:00 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/25/2014 8:00 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/25/2014 8:00 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/25/2014 8:00 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/25/2014 8:00 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/25/2014 8:00 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/25/2014 8:00 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/25/2014 8:00 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/25/2014 8:00 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/25/2014 8:00 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/25/2014 8:00 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/25/2014 8:00 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/25/2014 8:00 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/25/2014 8:00 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/25/2014 8:00 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/25/2014 8:00 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/25/2014 8:00 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/25/2014 8:00 AM
Surr: 1,2-Dichloroethane-d4 113 68.7-129 %RECNANA 9/25/2014 8:00 AM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/25/2014 8:00 AM
Surr: Dibromofluoromethane 109 74.3-124 %RECNANA 9/25/2014 8:00 AM
Surr: Toluene-d8 98.6 71.4-129 %RECNANA 9/25/2014 8:00 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 373 10 mg/L2.0 NA PA/VA9/18/2014 8:45 AM
Page 16 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:00:00 AM
Project:UNIT 3
Lab ID:1409J47-08A Matrix:Trip Blank
TRIP BLANK #5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 7:27 AM
Acetone 13.2 100 J µg/L4.88 NA PA/VA9/25/2014 7:27 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/25/2014 7:27 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/25/2014 7:27 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/25/2014 7:27 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/25/2014 7:27 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/25/2014 7:27 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/25/2014 7:27 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/25/2014 7:27 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/25/2014 7:27 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/25/2014 7:27 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/25/2014 7:27 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/25/2014 7:27 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/25/2014 7:27 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/25/2014 7:27 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/25/2014 7:27 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/25/2014 7:27 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/25/2014 7:27 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/25/2014 7:27 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/25/2014 7:27 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/25/2014 7:27 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/25/2014 7:27 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 7:27 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/25/2014 7:27 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/25/2014 7:27 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/25/2014 7:27 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/25/2014 7:27 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/25/2014 7:27 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/25/2014 7:27 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/25/2014 7:27 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/25/2014 7:27 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/25/2014 7:27 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/25/2014 7:27 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/25/2014 7:27 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/25/2014 7:27 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/25/2014 7:27 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/25/2014 7:27 AM
Page 17 of 18
WO#: 1409J47
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:00:00 AM
Project:UNIT 3
Lab ID:1409J47-08A Matrix:Trip Blank
TRIP BLANK #5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/25/2014 7:27 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/25/2014 7:27 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/25/2014 7:27 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/25/2014 7:27 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/25/2014 7:27 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/25/2014 7:27 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/25/2014 7:27 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/25/2014 7:27 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/25/2014 7:27 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/25/2014 7:27 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/25/2014 7:27 AM
Surr: 1,2-Dichloroethane-d4 111 68.7-129 %RECNANA 9/25/2014 7:27 AM
Surr: 4-Bromofluorobenzene 104 71.8-127 %RECNANA 9/25/2014 7:27 AM
Surr: Dibromofluoromethane 106 74.3-124 %RECNANA 9/25/2014 7:27 AM
Surr: Toluene-d8 100 71.4-129 %RECNANA 9/25/2014 7:27 AM
Page 18 of 18
DB
P i x
E v a l u a t i on
w w w.a mm a r a .c om
Leachate
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver, WV 25813 800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Monday, September 29, 2014
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:SUBTITLE LEACHATE
Work Order #:1409J30
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 1 sample(s) on 9/17/2014 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 6
WO#: 1409J30
Date Reported: 9/29/2014
REI Consultants, Inc. - Case Narrative
Client:
Project:SUBTITLE LEACHATE
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 6
WO#: 1409J30
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 5:10:00 PM
Project:SUBTITLE LEACHATE
Lab ID:1409J30-01A Matrix:Waste Water
LEACHATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony 0.0060 0.0060 J mg/L0.0002 NA PA/VA9/24/2014 11:47 AM
Arsenic 0.0069 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 11:47 AM
Barium 0.105 0.100 mg/L0.0010 NA PA/VA9/24/2014 11:47 AM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 11:47 AM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 11:47 AM
Chromium 0.0296 0.0100 mg/L0.0010 NA PA/VA9/24/2014 11:47 AM
Cobalt 0.0167 0.0100 mg/L0.0010 NA PA/VA9/24/2014 11:47 AM
Copper 0.0123 0.0100 mg/L0.0010 NA PA/VA9/24/2014 11:47 AM
Lead 0.0010 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 11:47 AM
Nickel 0.0781 0.0500 mg/L0.0020 NA PA/VA9/24/2014 11:47 AM
Selenium 0.0010 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 11:47 AM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 11:47 AM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 11:47 AM
Vanadium 0.0154 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 11:47 AM
Zinc 0.0588 0.0100 mg/L0.0030 NA PA/VA9/24/2014 11:47 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/24/2014 7:51 PM
Acetone 94.3 100 J µg/L4.88 NA PA/VA9/24/2014 7:51 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/24/2014 7:51 PM
Benzene 0.940 1.00 J µg/L0.129 NA PA/VA9/24/2014 7:51 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/24/2014 7:51 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/24/2014 7:51 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/24/2014 7:51 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/24/2014 7:51 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/24/2014 7:51 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/24/2014 7:51 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/24/2014 7:51 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/24/2014 7:51 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/24/2014 7:51 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/24/2014 7:51 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/24/2014 7:51 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/24/2014 7:51 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/24/2014 7:51 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/24/2014 7:51 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/24/2014 7:51 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/24/2014 7:51 PM
Page 3 of 6
WO#: 1409J30
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 5:10:00 PM
Project:SUBTITLE LEACHATE
Lab ID:1409J30-01A Matrix:Waste Water
LEACHATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene 0.820 1.00 J µg/L0.287 NA PA/VA9/24/2014 7:51 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/24/2014 7:51 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/24/2014 7:51 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/24/2014 7:51 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/24/2014 7:51 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/24/2014 7:51 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/24/2014 7:51 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/24/2014 7:51 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/24/2014 7:51 PM
Ethylbenzene 4.03 1.00 µg/L0.178 NA PA/VA9/24/2014 7:51 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/24/2014 7:51 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/24/2014 7:51 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/24/2014 7:51 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/24/2014 7:51 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/24/2014 7:51 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/24/2014 7:51 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/24/2014 7:51 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/24/2014 7:51 PM
Toluene 0.390 1.00 J µg/L0.167 NA PA/VA9/24/2014 7:51 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/24/2014 7:51 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/24/2014 7:51 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/24/2014 7:51 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/24/2014 7:51 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/24/2014 7:51 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/24/2014 7:51 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/24/2014 7:51 PM
o-Xylene 1.31 1.00 µg/L0.186 NA PA/VA9/24/2014 7:51 PM
m,p-Xylene 2.46 2.00 µg/L0.287 NA PA/VA9/24/2014 7:51 PM
Surr: 1,2-Dichloroethane-d4 114 68.7-129 %RECNANA 9/24/2014 7:51 PM
Surr: 4-Bromofluorobenzene 103 71.8-127 %RECNANA 9/24/2014 7:51 PM
Surr: Dibromofluoromethane 110 74.3-124 %RECNANA 9/24/2014 7:51 PM
Surr: Toluene-d8 98.5 71.4-129 %RECNANA 9/24/2014 7:51 PM
BOD, 5 Day, 20°C Method: SM5210 B-2001 Analyst: VR
Biochemical Oxygen Demand 23 5 mg/L2NA PA/VA9/17/2014 1:28 PM
Chemical Oxygen Demand Method: EPA 410.4, Rev. 2
(1993)
Analyst: SF
Chemical Oxygen Demand 354 50 mg/L20NA PA/VA9/18/2014 9:15 AM
Page 4 of 6
WO#: 1409J30
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 5:10:00 PM
Project:SUBTITLE LEACHATE
Lab ID:1409J30-01A Matrix:Waste Water
LEACHATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
ANIONS by ION CHROMATOGRAPHY Method: EPA 300.0, Rev.2.1
(1993)
Analyst: CF
Sulfate 18.4 5.00 mg/L1.00 NA PA/VA9/17/2014 11:45 AM
ANIONS by ION CHROMATOGRAPHY-48 HOUR Method: EPA 300.0, Rev.2.1
(1993)
Analyst: CF
Nitrogen, Nitrate ND 0.10 mg/L0.02 NA PA/VA9/17/2014 11:45 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 23.0 10 mg/L2.0 NA PA/VA9/18/2014 8:20 AM
Page 5 of 6
WO#: 1409J30
Date Reported: 9/29/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 5:10:00 PM
Project:SUBTITLE LEACHATE
Lab ID:1409J30-01B Matrix:Waste Water
LEACHATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
ANIONS by ION CHROMATOGRAPHY-48 HOUR Method: EPA 300.0, Rev.2.1
(1993)
Analyst: CF
Orthophosphate (As P)0.12 0.10 mg/L0.05 NA PA/VA9/17/2014 12:03 PM
Page 6 of 6
DB
P i x
E v a l u a t i on
w w w.a mm a r a .c om
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB7:
FieldSamplingSummaries
and
FieldSampleLogs
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Unit 2
FieldSamplingSummaries
and
FieldSampleLogs
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB7-Page 1
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Sunny / PartlySunny83-88°F
Property Units MW-12 MW-13 MW-14 MW-15
SamplingDepth Feet 19.75 6.67 7.05 4.12
StaticDepth Feet 16.48 5.98 5.91 3.78
WellDepth Feet 22.95 18.60 14.60 14.50
WaterColumnHeight Feet 6.47 12.62 8.69 10.72
VolumePurged Liters 24 22 15 20
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-12 MW-13 MW-14 MW-15
pH SU 5.81 5.57 5.80 5.82Dup5.85
Temperature oC 18.6 18.4 21.2 22.1Dup22.1
Conductivity umhos/cm 356 145 255 73.9Dup74.1
Turbidity NTU 20.5 55.1 30.1 9.08Dup9.13
Appearance -Cloudy Cloudy Cloudy Clear
Odor -Slight Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 21 37 14 7
Property Units MW-16 MW-17
SamplingDepth Feet 7.19 16.04
StaticDepth Feet 6.14 7.28
WellDepth Feet 21.77 20.60
WaterColumnHeight Feet 15.63 13.32
VolumePurged Liters 28 10
PurgingStatus -FinishedPurging PurgedDry
PhysicalProperty Units MW-16 MW-17
pH SU 5.49 5.38
Temperature oC 20.7 20.1
Conductivity umhos/cm 90.6 59.9
Turbidity NTU 157 41.8
Appearance -Cloudy Cloudy
Odor -No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 135 33
SAMPLINGLOGSUMMARY
CountyofCatawba
1409J28
9/16/2014
SubtitleD-Unit2(Permit:#18-03)
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB7-Page 2
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Sunny / PartlySunny83-88°F
SAMPLINGLOGSUMMARY
CountyofCatawba
1409J28
9/16/2014
SubtitleD-Unit2(Permit:#18-03)
Property Units U-1 U-2 U-3 Leachate
SamplingDepth Feet ----
StaticDepth Feet ----
WellDepth Feet ----
WaterColumnHeight Feet ----
VolumePurged Liters ----
PurgingStatus -----
PhysicalProperty Units U-1 U-2 U-3 Leachate
pH SU -5.99 5.90 7.71
Temperature oC -23.3 23.3 33.6
Conductivity umhos/cm -196.1 110.2 5290
Turbidity NTU -62.8 322 33.9
Appearance --Cloudy Cloudy Cloudy
Odor --No Odor No Odor Strong Odor
TotalSuspendedSolids(TSS)mg/L -24 489 23
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB7-Page 3
ProjectName:Project :Well#:MW-12
ContactPerson:Phone#:
Y N Y N
x x
X x
x x
Comments:
Date/Time:Sunny 86 °F
16.48 (Ft)3.74 (Liters)
22.95 (Ft)11.23 (Liters)
6.47 (Ft)24.00 (Liters)
pH
Time (SU)
16:42 5.91
16:43 5.94
16:45 5.94
16:47 5.93
16:49 5.92
16:51 5.84
16:53
Date:Time:16:55
Method:SamplingDepth:19.75'
pH:5.81 (SU)Conductivity:356 (umhos/cm)
Temperature:18.6 (o C)Turbidity:20.5 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
RodneyHamby 704-462-1348
BlackburnSubtitleD-Unit 2 2ndSemi2014
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELLCONDITIONDATA
Cap onWellRiser 2"PVCCasing
PURGINGDATA
9/16/201416:35 WeatherConditions:
StaticDepth(DepthtoWater)Volume
WaterColumnHeight VolumePurged
WellDepth 3Volumes
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected VolumePurgedTemperatureTurbidity
Conductivity(umhos/cm)(oC)(NTU)(Liters)
461.0 20.9 7.58 1
496.0 19.3 11.81 4
18.9 13.57 8489.0
474.0 18.7 15.82 12
444.0 18.7 17.92 16
389.0 18.5 25.8 20
FinishedPurging 24
TeflonBailer
SAMPLINGDATA
9/16/2014
Odor:SlightOdor
PHYSICALCHARACTERISTICSOFSAMPLE
Appearance:Cloudy
9/16/2014
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB7-Page 4
ProjectName:Project :Well#:MW-13
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:PartlySunny85 °F
5.98 (Ft)7.30 (Liters)
18.60 (Ft)21.92 (Liters)
12.62 (Ft)22.00 (Liters)
pH
Time (SU)
16:18 6.03
16:20 5.71
16:21 5.62
16:22 5.64
16:23 5.59
16:24 5.61
16:25
Date:Time:16:28
Method:SamplingDepth:6.67'
pH:5.57 (SU)Conductivity:144.5 (umhos/cm)
Temperature:18.4 (o C)Turbidity:55.1 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
ProtectiveCasingPresent PhysicalDamage
2ndSemi2014BlackburnSubtitleD-Unit 2
ProtectiveCasingLocked Concrete/GroutPadPresent
RodneyHamby 704-462-1348
WELLCONDITIONDATA
Volume
2"PVCCasingCap onWellRiser
PURGINGDATA
WeatherConditions:9/16/201416:15
StaticDepth(DepthtoWater)
WaterColumnHeight
WellDepth 3Volumes
VolumePurged
EVACUATION/STABILIZATIONTESTDATA
VolumePurged
(NTU)(Liters)
Turbidity
Conductivity(umhos/cm)
76.5
TemperatureCorrected
(oC)
Temperature
21.4
105.5 45.1 4
3.78 1
20.3
144.6 17.8 1272.9
134.1 18.2 104 8
16142.3 17.6 69.3
FinishedPurging
144.4 17.5 67.4 20
22
TeflonBailer
SAMPLINGDATA
9/16/2014
NoOdorOdor:
PHYSICALCHARACTERISTICSOFSAMPLE
Appearance:Cloudy
9/16/2014
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB7-Page 5
ProjectName:Project :Well#:MW-14
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:PartlySunny85 °F
5.91 (Ft)5.03 (Liters)
14.60 (Ft)15.09 (Liters)
8.69 (Ft)15.00 (Liters)
pH
Time (SU)
15:56 6.08
15:58 5.87
16:00 5.81
16:01 5.76
16:03 5.78
16:04 5.82
16:04
Date:Time:16:07
Method:SamplingDepth:7.05'
pH:5.80 (SU)Conductivity:255 (umhos/cm)
Temperature:21.2 (o C)Turbidity:30.1 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 2 2ndSemi2014
704-462-1348
WELLCONDITIONDATA
RodneyHamby
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
StaticDepth(DepthtoWater)Volume
2"PVCCasingCap onWellRiser
9/16/201415:55 WeatherConditions:
PURGINGDATA
WellDepth 3Volumes
VolumePurgedWaterColumnHeight
TemperatureCorrected
EVACUATION/STABILIZATIONTESTDATA
VolumePurgedTurbidity
(Liters)Conductivity(umhos/cm)(oC)(NTU)
Temperature
24.0 130.8133.3
169.8 22.5 133 3
21.4 85
248.0 921.6 75.4
245.0
1247.7
243.0 6
250.0 20.7
15
20.9 55.6 15
SAMPLINGDATA
9/16/2014
TeflonBailer
FinishedPurging
Appearance:Cloudy Odor:
PHYSICALCHARACTERISTICSOFSAMPLE
NoOdor
9/16/2014
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB7-Page 6
ProjectName:Project :Well#:MW-15
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:PartlySunny88 °F
3.78 (Ft)6.20 (Liters)
14.50 (Ft)18.62 (Liters)
10.72 (Ft)20.00 (Liters)
pH
Time (SU)
15:29 6.42
15:31 5.94
15:32 5.85
15:33 5.81
15:34 5.82
15:35 5.79
15:35
Date:Time:15:38
Method:SamplingDepth:4.12'
pH:5.82Dup5.85 (SU)Conductivity:73.9Dup74.1 (umhos/cm)
Temperature:22.1Dup22.1 (o C)Turbidity:9.08Dup9.13 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 2 2ndSemi2014
704-462-1348RodneyHamby
Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELLCONDITIONDATA
ProtectiveCasingLocked
Cap onWellRiser 2"PVCCasing
9/16/201415:25 WeatherConditions:
PURGINGDATA
StaticDepth(DepthtoWater)Volume
3Volumes
WaterColumnHeight VolumePurged
WellDepth
VolumePurgedTemperatureTurbidity
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected
Conductivity(umhos/cm)(oC)(NTU)(Liters)
71.4 25.1 12.06
8.4772.1
8
23.1 4
73.6 21.3 7.7
74.0
12
72.7 21.7 8.66
1621.2 8.34
2021.2 8.0273.9
SAMPLINGDATA
PHYSICALCHARACTERISTICSOFSAMPLE
9/16/2014
20
TeflonBailer
FinishedPurging
Appearance:NoOdorClearOdor:
9/16/2014
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB7-Page 7
ProjectName:Project :Well#:MW-16
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:PartlySunny83 °F
6.14 (Ft)9.04 (Liters)
21.77 (Ft)27.14 (Liters)
15.63 (Ft)28.00 (Liters)
pH
Time (SU)
14:43 5.34
14:45 5.34
14:46 5.46
14:47 5.47
14:50 5.44
14:52 5.48
14:53
Date:Time:14:55
Method:SamplingDepth:7.19'
pH:5.49 (SU)Conductivity:90.6 (umhos/cm)
Temperature:20.7 (o C)Turbidity:157 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
704-462-1348
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 2 2ndSemi2014
RodneyHamby
WELLCONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
Concrete/GroutPadPresentProtectiveCasingLocked
9/16/201414:40
Volume
WeatherConditions:
2"PVCCasingCap onWellRiser
PURGINGDATA
StaticDepth(DepthtoWater)
VolumePurged
3VolumesWellDepth
WaterColumnHeight
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity VolumePurged
Conductivity(umhos/cm)
1
(oC)(NTU)(Liters)
76.5 24.3 3.47
22.1
87.3 21.6
79.1 28.3 5
15
53.9 10
67.690.3 20.3
90.7
20.3
20.3 123 25
10090.4 20
SAMPLINGDATA
PHYSICALCHARACTERISTICSOFSAMPLE
FinishedPurging 28
TeflonBailer
9/16/2014
Appearance:Cloudy NoOdor
9/16/2014
Odor:
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB7-Page 8
ProjectName:Project :Well#:MW-17
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 87 °F
7.28 (Ft)7.71 (Liters)
20.60 (Ft)23.13 (Liters)
13.32 (Ft)10.00 (Liters)
pH
Time (SU)
14:17 4.78
14:18 4.84
14:20 4.98
14:21
Date:Time:14:30
Method:SamplingDepth:16.04'
pH:5.38 (SU)Conductivity:59.9 (umhos/cm)
Temperature:20.1 (o C)Turbidity:41.8 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
704-462-1348RodneyHamby
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 2 2ndSemi2014
ProtectiveCasingLocked Concrete/GroutPadPresent
Volume
Cap onWellRiser
WeatherConditions:
PhysicalDamage
WELLCONDITIONDATA
ProtectiveCasingPresent
PURGINGDATA
StaticDepth(DepthtoWater)
9/16/201414:13
2"PVCCasing
3Volumes
VolumePurgedWaterColumnHeight
WellDepth
EVACUATION/STABILIZATIONTESTDATA
VolumePurgedTemperatureCorrectedTemperatureTurbidity
53.5 22.1
(Liters)Conductivity(umhos/cm)(oC)(NTU)
42.3 1
422.1 >80052.4
852.8 19.5 >800
PHYSICALCHARACTERISTICSOFSAMPLE
SAMPLINGDATA
TeflonBailer
10PurgedDry
9/16/2014
9/16/2014
NoOdorOdor:Appearance:Cloudy
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB7-Page 9
Outlet:
Date:14:23
pH:Conductivity:umhos/cm
Flow:DRY Temperature:o C
/
Turbidity=NTU
Outlet:
Date:15:08
pH:5.99 Conductivity:196.1 umhos/cm
Flow:N/A Temperature:23.3 o C
Cloudy /NoOdor
Turbidity=62.8NTU
Outlet:
Date:15:16
pH:5.90 Conductivity:110.2 umhos/cm
Flow:N/A Temperature:23.3 o C
Cloudy /NoOdor
Turbidity=322NTU
Time:
SampleOdorand PhysicalAppearance:
Comments:
U-3
U-2
SurfaceWaterSampling Log
REIConsultants,Inc.
ProjectName:BlackburnSubtitleD-Unit 2
SampleOdorand PhysicalAppearance:
Contact Person:
SampleOdorand PhysicalAppearance:
9/16/2014 Time:
Comments:
Comments:
9/16/2014
RodneyHamby Phone/Fax:
U-1
704-462-1348
NoSample Time:
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com AppendixB7-Page10
Outlet:
Date:17:10
pH:7.71 Conductivity:5290 umhos/cm
Flow:N/A Temperature:33.6 o C
Cloudy /StrongOdor
Turbidity=33.9NTU
Outlet:
Date:
pH:Conductivity:umhos/cm
Flow:Temperature:o C
/
Turbidity=NTU
Outlet:
Date:
pH:Conductivity:umhos/cm
Flow:Temperature:o C
/
Turbidity=NTU
Comments:
SampleOdorand PhysicalAppearance:
Time:
Comments:
SampleOdorand PhysicalAppearance:
Comments:
Leachate
9/16/2014 Time:
SurfaceWaterSampling Log
REIConsultants,Inc.
ProjectName:BlackburnSubtitleD-Unit 2
Contact Person:RodneyHamby Phone/Fax:[phone]
Time:
SampleOdorand PhysicalAppearance:
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com AppendixB7-Page11
Unit 3
FieldSamplingSummaries
and
FieldSampleLogs
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com AppendixB7-Page12
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Sunny83-86°F
Property Units MW-31 MW-32 MW-33 MW-34
SamplingDepth Feet 22.87 24.98 26.11 21.35
StaticDepth Feet 22.25 24.90 21.15 20.50
WellDepth Feet 32.70 32.75 29.75 28.05
WaterColumnHeight Feet 10.45 7.85 8.60 7.55
VolumePurged Liters 20 15 15 14
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-31 MW-32 MW-33 MW-34
pH SU 5.65 5.49 5.73 5.94Dup5.94
Temperature oC 17.2 16.9 17.6 18.2Dup18.1
Conductivity umhos/cm 151 67 34 57.7Dup57.0
Turbidity NTU 397.0 >800 >800 657Dup651
Appearance -Cloudy Muddy Muddy Cloudy
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 363 8560 1310 238
Property Units SW-4 SW-5
SamplingDepth Feet --
StaticDepth Feet --
WellDepth Feet --
WaterColumnHeight Feet --
VolumePurged Liters --
PurgingStatus ---
PhysicalProperty Units SW-4 SW-5
pH SU 6.89 6.95
Temperature oC 22.2 20.4
Conductivity umhos/cm 80.5 105.2
Turbidity NTU 20.3 20.8
Appearance -Clear Clear
Odor -No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 11 17
9/16/2014
SAMPLINGLOGSUMMARY
CountyofCatawba
SubtitleD-Unit3(Permit:#18-03)
1409J47
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com AppendixB7-Page13
ProjectName:Project :Well#:MW-31
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 83 °F
22.25 (Ft)6.05 (Liters)
32.70 (Ft)18.15 (Liters)
10.45 (Ft)20.00 (Liters)
pH
Time (SU)
13:15 5.67
13:17 5.71
13:18 5.70
13:19 5.70
13:21 5.72
13:23 5.71
13:23
Date:Time:13:27
Method:SamplingDepth:22.87'
pH:5.65 (SU)Conductivity:151.1 (umhos/cm)
Temperature:17.2 (o C)Turbidity:397 (NTU)
Comments:
SampledBy:RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
Sampler'sSignature:Date:
SAMPLINGDATA
9/16/2014
NoOdor
Conductivity(umhos/cm)
>800 12
VolumePurged
FinishedPurging 20
TeflonBailer
PHYSICALCHARACTERISTICSOFSAMPLE
Appearance:Cloudy Odor:
9/16/2014
157.5
8
143.5 16.9
>800 12
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
PURGINGDATA
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity
BlackburnSubtitleD-Unit 3 2ndSemi2014
WELLCONDITIONDATA
RodneyHamby 704-462-1348
Cap onWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
146.4 16.9 >800 20
152.3 16.8
17.6
16.9 >800152.1
9/16/201413:07 WeatherConditions:
WellDepth 3Volumes
WaterColumnHeight VolumePurged
710 4
(oC)(NTU)(Liters)
152.9 18.5 26.9 1
StaticDepth(DepthtoWater)Volume
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com AppendixB7-Page14
ProjectName:Project :Well#:MW-32
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 83 °F
24.90 (Ft)4.54 (Liters)
32.75 (Ft)13.63 (Liters)
7.85 (Ft)15.00 (Liters)
pH
Time (SU)
13:44 5.34
13:45 5.45
13:46 5.47
13:47 5.79
13:48 5.49
13:49 5.53
13:49
Date:Time:13:55
Method:SamplingDepth:24.98'
pH:5.49 (SU)Conductivity:66.5 (umhos/cm)
Temperature:16.9 (o C)Turbidity:>800 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
WELLCONDITIONDATA
RodneyHamby 704-462-1348
ProtectiveCasingPresent PhysicalDamage
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 3 2ndSemi2014
ProtectiveCasingLocked Concrete/GroutPadPresent
66.3 16.4
Cap onWellRiser 2"PVCCasing
>800
>800
>800
>800
>800
64.7 18.1
FinishedPurging
17.166.4
69.8 16.7
66.9 16.1
66.5 16.7
9/16/201413:37 WeatherConditions:
Temperature
WellDepth
Conductivity(umhos/cm)(oC)
PURGINGDATA
TemperatureCorrected VolumePurged
StaticDepth(DepthtoWater)Volume
EVACUATION/STABILIZATIONTESTDATA
3Volumes
(NTU)(Liters)
WaterColumnHeight VolumePurged
Turbidity
17.62 1
3
6
9
12
15
TeflonBailer
PHYSICALCHARACTERISTICSOFSAMPLE
15
SAMPLINGDATA
9/16/2014
Appearance:Muddy Odor:NoOdor
9/16/2014
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com AppendixB7-Page15
ProjectName:Project :Well#:MW-33
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 85 °F
21.15 (Ft)4.94 (Liters)
29.75 (Ft)14.93 (Liters)
8.60 (Ft)15.00 (Liters)
pH
Time (SU)
14:10 5.60
14:13 5.60
14:15 5.79
14:16 5.82
14:18 5.84
14:19 5.82
14:19
Date:Time:14:23
Method:SamplingDepth:26.11'
pH:5.73 (SU)Conductivity:34.1 (umhos/cm)
Temperature:17.6 (o C)Turbidity:>800 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
ProtectiveCasingLocked
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
RodneyHamby 704-462-1348
BlackburnSubtitleD-Unit 3 2ndSemi2014
Cap onWellRiser 2"PVCCasing
Concrete/GroutPadPresent
WELLCONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
9/16/201414:05 WeatherConditions:
PURGINGDATA
TemperatureCorrected Temperature
EVACUATION/STABILIZATIONTESTDATA
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
WaterColumnHeight VolumePurged
Conductivity(umhos/cm)(oC)(NTU)
33.3 19.4 4.39
(Liters)
37.6 18.0
1
>800 3
Turbidity VolumePurged
17.4
640.1 17.7 >800
38.8 >800 9
17.8 >800 1236.7
35.0
FinishedPurging
1517.4 >800
15
TeflonBailer
PHYSICALCHARACTERISTICSOFSAMPLE
Odor:NoOdor
SAMPLINGDATA
9/16/2014
Appearance:Muddy
9/16/2014
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com AppendixB7-Page16
ProjectName:Project :Well#:MW-34
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 86 °F
20.50 (Ft)4.37 (Liters)
28.05 (Ft)13.11 (Liters)
7.55 (Ft)14.00 (Liters)
pH
Time (SU)
14:39 6.26
14:40 6.20
14:41 6.13
14:43 6.01
14:44 5.92
14:45
Date:Time:14:50
Method:SamplingDepth:21.35'
pH:5.94Dup5.94 (SU)Conductivity:57.7Dup57.0 (umhos/cm)
Temperature:18.2Dup18.1 (o C)Turbidity:657Dup651 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
WELLCONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
Cap onWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
RodneyHamby 704-462-1348
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 3 2ndSemi2014
9/16/201414:30 WeatherConditions:
PURGINGDATA
StaticDepth(DepthtoWater)Volume
(Liters)
WellDepth 3Volumes
Turbidity
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
VolumePurgedTemperature
(oC)
55.2 19.0
(NTU)
TemperatureCorrected
Conductivity(umhos/cm)
6
9
54.2 18.0 180 3
473
12
0.94 1
17.6
17.4
53.4
55.1
57.2
256
17.7 700
14FinishedPurging
PHYSICALCHARACTERISTICSOFSAMPLE
TeflonBailer
9/16/2014
SAMPLINGDATA
Appearance:Cloudy Odor:NoOdor
9/16/2014
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com AppendixB7-Page17
Outlet:
Date:16:05
pH:6.89 Conductivity:80.5 umhos/cm
Flow:N/A Temperature:22.2 o C
Clear /NoOdor
Turbidity=20.3NTU
Outlet:
Date:16:32
pH:6.95 Conductivity:105.2 umhos/cm
Flow:N/A Temperature:20.4 o C
Clear /NoOdor
Turbidity=20.8NTU
Outlet:
Date:
pH:Conductivity:umhos/cm
Flow:Temperature:o C
/
Turbidity=NTU
SurfaceWaterSampling Log
REIConsultants,Inc.
ProjectName:BlackburnSubtitleD-Unit 3
9/16/2014 Time:
9/16/2014 Time:
Contact Person:RodneyHamby Phone/Fax:
SW-4
704-462-1348
Comments:
Comments:
Time:
SampleOdorand PhysicalAppearance:
SampleOdorand PhysicalAppearance:
Comments:
SW-5
SampleOdorand PhysicalAppearance:
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com AppendixB7-Page18
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
Subtitle D
AppendixB8:
HistoricalDataSummary
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-10
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page 1
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-12
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page 8
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-13
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page13
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-14
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page18
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-15
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page23
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-16
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page28
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-17
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page33
SubtitleD-Unit 2
HistoricalDataSummary
Underdrain:U-1
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page38
SubtitleD-Unit 2
HistoricalDataSummary
Underdrain:U-2
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page43
SubtitleD-Unit 2
HistoricalDataSummary
Underdrain:U-3
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page48
SubtitleD-Unit 3
HistoricalDataSummary
MonitoringWell:MW-31
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page53
B l ac
kb
u
r n
L a nd
f il
l
:
Su
b
ti
t
l
e
D U
n it
3
(P e r m it
:
#18
-0 3)
B l ac
kb
u
r n
L a nd
f il
l
:
Su
b
ti
t
l
e
D U
n it
3
(P e r m it
:
#18
-0 3)
SubtitleD-Unit 3
HistoricalDataSummary
MonitoringWell:MW-32
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page56
SubtitleD-Unit 3
HistoricalDataSummary
MonitoringWell:MW-33
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page59
SubtitleD-Unit 3
HistoricalDataSummary
MonitoringWell:MW-34
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page62
Subtitle D -Unit 3
HistoricalDataSummary
SurfaceWater:SW-4
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page65
Subtitle D -Unit 3
HistoricalDataSummary
SurfaceWater:SW-5
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixB8-Page68
CatawbaCounty,NorthCarolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
Appendix C1:
2ndSemi-Annual2014
Summary of Detections
REIConsultants,Inc.P.OBox 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com
P a r a m e t er
G W S
td
1
S W SL
2
M W -5
M W-
5A
M W -6
M W-
6D
M W -7
M W-
11
M W-
20
S W -1
S W -3 P Z-85B P Z-86B
1
30
5
13
<5
29
58
6
<10
<10 --
F OO
T NO
T E S:
S PE
CI
A L
NO
T E S:
1
G W S
t d
-
N o rt
h Ca
r o li
na
g r o u nd
w a t e r
s t a n da
r d s (m g /L ).
-O n l y
r es
u lt
s
a b ov
e
S W SL
's
s ho
wn
2
S W S L
- So
li
d
W a s t e S
ec
t i on
L i m i t s
(m g /L)
-A
ll
c on
ce
n tr
a t i on
s d
e t ec
t e d a
b ov
e t h e
G W S
t d a
r e h
i g h li
g h t e d
i n
r e d an d b o l d t e x t.
-A
ll
da
t a r e po
rt
e d
i n
m g /L.
-T r i p
Bl
a nk
r es
u l t s
f o r a
ll
vo
l a t il
e an
a
l y se
s
w e r e
ND
(no
t d
e t ec
t e d ) a t t h e P Q L.
T o t a l
S us
p en
d e d
S o li
d s
(T SS
)
CatawbaCounty,NorthCarolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
Appendix C2:
Summary of Dissolved Metals and
TotalSuspendedSolid(TSS)
Detections
REIConsultants,Inc.P.OBox 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com
Su
mm
a r y
o f
Di
ss
o lv
e d
Me
t a l s
a nd
T SS
D e t e c ti
o
ns
B l a c kb
u
r n
L
a nd
f il
l
:
C l o s e d
P
o r ti
on
P e r m i t :
#18
-03
R E I C
J o b
N u m b e r :
1 4 09
J 33
S a m p l e
D a t e :
9 -2 0 14
A n t i m o n y ,
D i ss
o l v ed
0 .0 06
A r s e n i c ,
D i ss
o l v ed
0 .01
B a r i um
,
D i ss
o l v ed
0 .1
0 .1 63
0 .1 89
0 .2 05
0 .2 83
0 .1 64
B e ry
ll
i
um
,
D i ss
o l v ed
0 .0 01
C a d m i um
,
D i ss
o l v ed
0 .0 01
C h r o m i um
,
D i ss
o l v ed
0 .01
C o b a l t ,
D i ss
o l v ed
0 .01
0 .0 3 74
0 .0 5 29
C o p pe
r ,
D i ss
o l v ed
0 .01
L ea
d,
D i ss
o l v ed
0 .01
Ni
c k e l,
D i ss
o l v ed
0 .05
S e l e n i um
,
D i ss
o l v ed
0 .01
S il
v e r ,
D i ss
o l v ed
0 .01
T h a ll
i
um
,
D i ss
o l v ed
0 .0 0 55
V a n a di
um
,
D i ss
o l v ed
0 .0 25
Z i n c ,
D i ss
o l v ed
0 .01
0 .0 4 31
0 .0 1 35
T o t a l S
u
s p e nd
e d
S
o li
d s
(T SS
)
1
30
5 .0
13
2
29
58
6
<2 4
F OO
T NO
T E S:
1.
S W SL
-
S o l id
W a s te
Se
c ti
on
L i m it
(m
g /L)
2.
O n ly
re
su
l ts
a b o ve
S WS
Ls
sh
o wn
S P E CI
AL
NO
T E S:
A ll
d a ta
re
p o r t ed
in
m g /L.
CatawbaCounty,NorthCarolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
Appendix C3:
HistoricalSummary ofDetections
REIConsultants,Inc.P.OBox 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
AppendixC4:
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Tuesday, September 30, 2014
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:BLACKBURN CLOSED
Work Order #:1409J33
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 13 sample(s) on 9/17/2014 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Case Narrative
Client:
Project:BLACKBURN CLOSED
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:55:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-01A Matrix:Groundwater
MW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 11:58 AM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 11:58 AM
Barium 0.248 0.100 mg/L0.0010 NA PA/VA9/24/2014 11:58 AM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 11:58 AM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 11:58 AM
Chromium 0.0104 0.0100 mg/L0.0010 NA PA/VA9/24/2014 11:58 AM
Cobalt 0.0032 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 11:58 AM
Copper 0.0118 0.0100 mg/L0.0010 NA PA/VA9/24/2014 11:58 AM
Lead 0.0012 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 11:58 AM
Nickel 0.0038 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 11:58 AM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 11:58 AM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 11:58 AM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 11:58 AM
Vanadium 0.0163 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 11:58 AM
Zinc 0.0075 0.0100 J mg/L0.0030 NA PA/VA9/24/2014 11:58 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/19/2014 9:16 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/19/2014 9:16 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/19/2014 9:16 PM
Benzene 0.730 1.00 J µg/L0.129 NA PA/VA9/19/2014 9:16 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/19/2014 9:16 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/19/2014 9:16 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/19/2014 9:16 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/19/2014 9:16 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/19/2014 9:16 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/19/2014 9:16 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/19/2014 9:16 PM
Chlorobenzene 2.12 3.00 J µg/L0.177 NA PA/VA9/19/2014 9:16 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/19/2014 9:16 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/19/2014 9:16 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/19/2014 9:16 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/19/2014 9:16 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/19/2014 9:16 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/19/2014 9:16 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/19/2014 9:16 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/19/2014 9:16 PM
Page 3 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:55:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-01A Matrix:Groundwater
MW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene 2.20 1.00 µg/L0.287 NA PA/VA9/19/2014 9:16 PM
1,1-Dichloroethane 3.21 5.00 J µg/L0.383 NA PA/VA9/19/2014 9:16 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/19/2014 9:16 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/19/2014 9:16 PM
cis-1,2-Dichloroethene 1.68 5.00 J µg/L0.226 NA PA/VA9/19/2014 9:16 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/19/2014 9:16 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/19/2014 9:16 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/19/2014 9:16 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/19/2014 9:16 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/19/2014 9:16 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/19/2014 9:16 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/19/2014 9:16 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/19/2014 9:16 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/19/2014 9:16 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/19/2014 9:16 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/19/2014 9:16 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/19/2014 9:16 PM
Tetrachloroethene 0.560 1.00 J µg/L0.196 NA PA/VA9/19/2014 9:16 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/19/2014 9:16 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/19/2014 9:16 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/19/2014 9:16 PM
Trichloroethene 1.80 1.00 µg/L0.302 NA PA/VA9/19/2014 9:16 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/19/2014 9:16 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/19/2014 9:16 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/19/2014 9:16 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/19/2014 9:16 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/19/2014 9:16 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/19/2014 9:16 PM
Surr: 1,2-Dichloroethane-d4 99.8 68.7-129 %RECNANA 9/19/2014 9:16 PM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/19/2014 9:16 PM
Surr: Dibromofluoromethane 101 74.3-124 %RECNANA 9/19/2014 9:16 PM
Surr: Toluene-d8 99.6 71.4-129 %RECNANA 9/19/2014 9:16 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 30.0 5.0 mg/L1.0 NA PA/VA9/18/2014 8:20 AM
Page 4 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:30:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-02A Matrix:Groundwater
MW-5AClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 12:15 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:15 PM
Barium 0.195 0.100 mg/L0.0010 NA PA/VA9/24/2014 12:15 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:15 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:15 PM
Chromium 0.0015 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:15 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:15 PM
Copper 0.0031 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:15 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/24/2014 12:15 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA9/24/2014 12:15 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:15 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:15 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 12:15 PM
Vanadium 0.0075 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 12:15 PM
Zinc 0.0262 0.0100 mg/L0.0030 NA PA/VA9/24/2014 12:15 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/19/2014 9:49 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/19/2014 9:49 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/19/2014 9:49 PM
Benzene 1.96 1.00 µg/L0.129 NA PA/VA9/19/2014 9:49 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/19/2014 9:49 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/19/2014 9:49 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/19/2014 9:49 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/19/2014 9:49 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/19/2014 9:49 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/19/2014 9:49 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/19/2014 9:49 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/19/2014 9:49 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/19/2014 9:49 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/19/2014 9:49 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/19/2014 9:49 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/19/2014 9:49 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/19/2014 9:49 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/19/2014 9:49 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/19/2014 9:49 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/19/2014 9:49 PM
Page 5 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:30:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-02A Matrix:Groundwater
MW-5AClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene 0.950 1.00 J µg/L0.287 NA PA/VA9/19/2014 9:49 PM
1,1-Dichloroethane 19.2 5.00 µg/L0.383 NA PA/VA9/19/2014 9:49 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/19/2014 9:49 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/19/2014 9:49 PM
cis-1,2-Dichloroethene 18.2 5.00 µg/L0.226 NA PA/VA9/19/2014 9:49 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/19/2014 9:49 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/19/2014 9:49 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/19/2014 9:49 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/19/2014 9:49 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/19/2014 9:49 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/19/2014 9:49 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/19/2014 9:49 PM
Methylene chloride 1.28 1.00 µg/L0.539 NA PA/VA9/19/2014 9:49 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/19/2014 9:49 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/19/2014 9:49 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/19/2014 9:49 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/19/2014 9:49 PM
Tetrachloroethene 8.55 1.00 µg/L0.196 NA PA/VA9/19/2014 9:49 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/19/2014 9:49 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/19/2014 9:49 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/19/2014 9:49 PM
Trichloroethene 17.9 1.00 µg/L0.302 NA PA/VA9/19/2014 9:49 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/19/2014 9:49 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/19/2014 9:49 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/19/2014 9:49 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/19/2014 9:49 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/19/2014 9:49 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/19/2014 9:49 PM
Surr: 1,2-Dichloroethane-d4 101 68.7-129 %RECNANA 9/19/2014 9:49 PM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/19/2014 9:49 PM
Surr: Dibromofluoromethane 101 74.3-124 %RECNANA 9/19/2014 9:49 PM
Surr: Toluene-d8 101 71.4-129 %RECNANA 9/19/2014 9:49 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 5.0 5.0 mg/L1.0 NA PA/VA9/18/2014 8:20 AM
Page 6 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 10:00:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-03A Matrix:Groundwater
MW-6Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 12:21 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:21 PM
Barium 0.271 0.100 mg/L0.0010 NA PA/VA9/24/2014 12:21 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:21 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:21 PM
Chromium 0.0030 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:21 PM
Cobalt 0.0378 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:21 PM
Copper 0.0015 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:21 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/24/2014 12:21 PM
Nickel 0.0093 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 12:21 PM
Selenium 0.0017 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:21 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:21 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 12:21 PM
Vanadium 0.0012 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 12:21 PM
Zinc 0.0070 0.0100 J mg/L0.0030 NA PA/VA9/24/2014 12:21 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/19/2014 10:22 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/19/2014 10:22 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/19/2014 10:22 PM
Benzene 3.24 1.00 µg/L0.129 NA PA/VA9/19/2014 10:22 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/19/2014 10:22 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/19/2014 10:22 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/19/2014 10:22 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/19/2014 10:22 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/19/2014 10:22 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/19/2014 10:22 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/19/2014 10:22 PM
Chlorobenzene 2.16 3.00 J µg/L0.177 NA PA/VA9/19/2014 10:22 PM
Chloroethane 1.89 10.0 J µg/L0.942 NA PA/VA9/19/2014 10:22 PM
Chloroform 1.02 5.00 J µg/L0.253 NA PA/VA9/19/2014 10:22 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/19/2014 10:22 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/19/2014 10:22 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/19/2014 10:22 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/19/2014 10:22 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/19/2014 10:22 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/19/2014 10:22 PM
Page 7 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 10:00:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-03A Matrix:Groundwater
MW-6Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene 5.01 1.00 µg/L0.287 NA PA/VA9/19/2014 10:22 PM
1,1-Dichloroethane 12.0 5.00 µg/L0.383 NA PA/VA9/19/2014 10:22 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/19/2014 10:22 PM
1,1-Dichloroethene 1.18 5.00 J µg/L0.328 NA PA/VA9/19/2014 10:22 PM
cis-1,2-Dichloroethene 3.72 5.00 J µg/L0.226 NA PA/VA9/19/2014 10:22 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/19/2014 10:22 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/19/2014 10:22 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/19/2014 10:22 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/19/2014 10:22 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/19/2014 10:22 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/19/2014 10:22 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/19/2014 10:22 PM
Methylene chloride 0.970 1.00 J µg/L0.539 NA PA/VA9/19/2014 10:22 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/19/2014 10:22 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/19/2014 10:22 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/19/2014 10:22 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/19/2014 10:22 PM
Tetrachloroethene 0.770 1.00 J µg/L0.196 NA PA/VA9/19/2014 10:22 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/19/2014 10:22 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/19/2014 10:22 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/19/2014 10:22 PM
Trichloroethene 1.86 1.00 µg/L0.302 NA PA/VA9/19/2014 10:22 PM
Trichlorofluoromethane 16.9 1.00 µg/L0.299 NA PA/VA9/19/2014 10:22 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/19/2014 10:22 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/19/2014 10:22 PM
Vinyl chloride 0.890 1.00 J µg/L0.223 NA PA/VA9/19/2014 10:22 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/19/2014 10:22 PM
m,p-Xylene 0.500 2.00 J µg/L0.287 NA PA/VA9/19/2014 10:22 PM
Surr: 1,2-Dichloroethane-d4 103 68.7-129 %RECNANA 9/19/2014 10:22 PM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/19/2014 10:22 PM
Surr: Dibromofluoromethane 102 74.3-124 %RECNANA 9/19/2014 10:22 PM
Surr: Toluene-d8 100 71.4-129 %RECNANA 9/19/2014 10:22 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 13.0 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 8 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 9:42:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-04A Matrix:Groundwater
MW-6DClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 12:27 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:27 PM
Barium 0.0726 0.100 J mg/L0.0010 NA PA/VA9/24/2014 12:27 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:27 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:27 PM
Chromium 0.0018 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:27 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:27 PM
Copper 0.0027 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:27 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/24/2014 12:27 PM
Nickel 0.0025 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 12:27 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:27 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:27 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 12:27 PM
Vanadium 0.0099 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 12:27 PM
Zinc 0.0054 0.0100 J mg/L0.0030 NA PA/VA9/24/2014 12:27 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/19/2014 10:55 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/19/2014 10:55 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/19/2014 10:55 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/19/2014 10:55 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/19/2014 10:55 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/19/2014 10:55 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/19/2014 10:55 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/19/2014 10:55 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/19/2014 10:55 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/19/2014 10:55 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/19/2014 10:55 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/19/2014 10:55 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/19/2014 10:55 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/19/2014 10:55 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/19/2014 10:55 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/19/2014 10:55 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/19/2014 10:55 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/19/2014 10:55 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/19/2014 10:55 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/19/2014 10:55 PM
Page 9 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 9:42:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-04A Matrix:Groundwater
MW-6DClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene 0.460 1.00 J µg/L0.287 NA PA/VA9/19/2014 10:55 PM
1,1-Dichloroethane 0.660 5.00 J µg/L0.383 NA PA/VA9/19/2014 10:55 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/19/2014 10:55 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/19/2014 10:55 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/19/2014 10:55 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/19/2014 10:55 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/19/2014 10:55 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/19/2014 10:55 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/19/2014 10:55 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/19/2014 10:55 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/19/2014 10:55 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/19/2014 10:55 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/19/2014 10:55 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/19/2014 10:55 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/19/2014 10:55 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/19/2014 10:55 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/19/2014 10:55 PM
Tetrachloroethene 0.330 1.00 J µg/L0.196 NA PA/VA9/19/2014 10:55 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/19/2014 10:55 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/19/2014 10:55 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/19/2014 10:55 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/19/2014 10:55 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/19/2014 10:55 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/19/2014 10:55 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/19/2014 10:55 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/19/2014 10:55 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/19/2014 10:55 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/19/2014 10:55 PM
Surr: 1,2-Dichloroethane-d4 102 68.7-129 %RECNANA 9/19/2014 10:55 PM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/19/2014 10:55 PM
Surr: Dibromofluoromethane 104 74.3-124 %RECNANA 9/19/2014 10:55 PM
Surr: Toluene-d8 100 71.4-129 %RECNANA 9/19/2014 10:55 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 2.0 5.0 J mg/L1.0 NA PA/VA9/18/2014 8:40 AM
Page 10 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 10:44:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-05A Matrix:Groundwater
MW-7Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 12:32 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:32 PM
Barium 0.347 0.100 mg/L0.0010 NA PA/VA9/24/2014 12:32 PM
Beryllium 0.0008 0.0010 J mg/L0.0002 NA PA/VA9/24/2014 12:32 PM
Cadmium 0.0004 0.0010 J mg/L0.0002 NA PA/VA9/24/2014 12:32 PM
Chromium 0.0209 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:32 PM
Cobalt 0.0666 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:32 PM
Copper 0.0101 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:32 PM
Lead 0.0037 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 12:32 PM
Nickel 0.0347 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 12:32 PM
Selenium 0.0018 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:32 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:32 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 12:32 PM
Vanadium 0.0223 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 12:32 PM
Zinc 0.0577 0.0100 mg/L0.0030 NA PA/VA9/24/2014 12:32 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/23/2014 1:29 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/23/2014 1:29 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/23/2014 1:29 AM
Benzene 8.79 1.00 µg/L0.129 NA PA/VA9/23/2014 1:29 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/23/2014 1:29 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/23/2014 1:29 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/23/2014 1:29 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/23/2014 1:29 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/23/2014 1:29 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/23/2014 1:29 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/23/2014 1:29 AM
Chlorobenzene 2.73 3.00 J µg/L0.177 NA PA/VA9/23/2014 1:29 AM
Chloroethane 1.05 10.0 J µg/L0.942 NA PA/VA9/23/2014 1:29 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/23/2014 1:29 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/23/2014 1:29 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/23/2014 1:29 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/23/2014 1:29 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/23/2014 1:29 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/23/2014 1:29 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/23/2014 1:29 AM
Page 11 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 10:44:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-05A Matrix:Groundwater
MW-7Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene 10.3 1.00 µg/L0.287 NA PA/VA9/23/2014 1:29 AM
1,1-Dichloroethane 2.18 5.00 J µg/L0.383 NA PA/VA9/23/2014 1:29 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/23/2014 1:29 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/23/2014 1:29 AM
cis-1,2-Dichloroethene 9.14 5.00 µg/L0.226 NA PA/VA9/23/2014 1:29 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/23/2014 1:29 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/23/2014 1:29 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/23/2014 1:29 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/23/2014 1:29 AM
Ethylbenzene 0.350 1.00 J µg/L0.178 NA PA/VA9/23/2014 1:29 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/23/2014 1:29 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/23/2014 1:29 AM
Methylene chloride 0.610 1.00 J µg/L0.539 NA PA/VA9/23/2014 1:29 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/23/2014 1:29 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/23/2014 1:29 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/23/2014 1:29 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/23/2014 1:29 AM
Tetrachloroethene 1.02 1.00 µg/L0.196 NA PA/VA9/23/2014 1:29 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/23/2014 1:29 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/23/2014 1:29 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/23/2014 1:29 AM
Trichloroethene 1.50 1.00 µg/L0.302 NA PA/VA9/23/2014 1:29 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/23/2014 1:29 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/23/2014 1:29 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/23/2014 1:29 AM
Vinyl chloride 1.09 1.00 µg/L0.223 NA PA/VA9/23/2014 1:29 AM
o-Xylene 3.22 1.00 µg/L0.186 NA PA/VA9/23/2014 1:29 AM
m,p-Xylene 3.48 2.00 µg/L0.287 NA PA/VA9/23/2014 1:29 AM
Surr: 1,2-Dichloroethane-d4 102 68.7-129 %RECNANA 9/23/2014 1:29 AM
Surr: 4-Bromofluorobenzene 104 71.8-127 %RECNANA 9/23/2014 1:29 AM
Surr: Dibromofluoromethane 102 74.3-124 %RECNANA 9/23/2014 1:29 AM
Surr: Toluene-d8 98.6 71.4-129 %RECNANA 9/23/2014 1:29 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 29.0 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 12 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 11:08:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-06A Matrix:Groundwater
MW-11Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 12:38 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:38 PM
Barium 0.199 0.100 mg/L0.0010 NA PA/VA9/24/2014 12:38 PM
Beryllium 0.0002 0.0010 J mg/L0.0002 NA PA/VA9/24/2014 12:38 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:38 PM
Chromium 0.0026 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:38 PM
Cobalt 0.0126 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:38 PM
Copper 0.0063 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:38 PM
Lead 0.0006 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 12:38 PM
Nickel 0.0042 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 12:38 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:38 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:38 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 12:38 PM
Vanadium 0.0177 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 12:38 PM
Zinc 0.0117 0.0100 mg/L0.0030 NA PA/VA9/24/2014 12:38 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/23/2014 2:02 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/23/2014 2:02 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/23/2014 2:02 AM
Benzene 6.23 1.00 µg/L0.129 NA PA/VA9/23/2014 2:02 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/23/2014 2:02 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/23/2014 2:02 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/23/2014 2:02 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/23/2014 2:02 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/23/2014 2:02 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/23/2014 2:02 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/23/2014 2:02 AM
Chlorobenzene 2.16 3.00 J µg/L0.177 NA PA/VA9/23/2014 2:02 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/23/2014 2:02 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/23/2014 2:02 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/23/2014 2:02 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/23/2014 2:02 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/23/2014 2:02 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/23/2014 2:02 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/23/2014 2:02 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/23/2014 2:02 AM
Page 13 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 11:08:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-06A Matrix:Groundwater
MW-11Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene 5.31 1.00 µg/L0.287 NA PA/VA9/23/2014 2:02 AM
1,1-Dichloroethane 1.22 5.00 J µg/L0.383 NA PA/VA9/23/2014 2:02 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/23/2014 2:02 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/23/2014 2:02 AM
cis-1,2-Dichloroethene 6.69 5.00 µg/L0.226 NA PA/VA9/23/2014 2:02 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/23/2014 2:02 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/23/2014 2:02 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/23/2014 2:02 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/23/2014 2:02 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/23/2014 2:02 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/23/2014 2:02 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/23/2014 2:02 AM
Methylene chloride 2.42 1.00 µg/L0.539 NA PA/VA9/23/2014 2:02 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/23/2014 2:02 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/23/2014 2:02 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/23/2014 2:02 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/23/2014 2:02 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/23/2014 2:02 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/23/2014 2:02 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/23/2014 2:02 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/23/2014 2:02 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/23/2014 2:02 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/23/2014 2:02 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/23/2014 2:02 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/23/2014 2:02 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/23/2014 2:02 AM
o-Xylene 1.25 1.00 µg/L0.186 NA PA/VA9/23/2014 2:02 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/23/2014 2:02 AM
Surr: 1,2-Dichloroethane-d4 103 68.7-129 %RECNANA 9/23/2014 2:02 AM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/23/2014 2:02 AM
Surr: Dibromofluoromethane 103 74.3-124 %RECNANA 9/23/2014 2:02 AM
Surr: Toluene-d8 98.6 71.4-129 %RECNANA 9/23/2014 2:02 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 58.0 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 14 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 11:43:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-07A Matrix:Groundwater
MW-20Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 12:44 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:44 PM
Barium 0.0470 0.100 J mg/L0.0010 NA PA/VA9/24/2014 12:44 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:44 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:44 PM
Chromium 0.0028 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:44 PM
Cobalt 0.0012 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:44 PM
Copper 0.0066 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:44 PM
Lead 0.0003 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 12:44 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA9/24/2014 12:44 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:44 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:44 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 12:44 PM
Vanadium 0.0052 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 12:44 PM
Zinc 0.0094 0.0100 J mg/L0.0030 NA PA/VA9/24/2014 12:44 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/23/2014 2:36 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/23/2014 2:36 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/23/2014 2:36 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/23/2014 2:36 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/23/2014 2:36 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/23/2014 2:36 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/23/2014 2:36 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/23/2014 2:36 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/23/2014 2:36 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/23/2014 2:36 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/23/2014 2:36 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/23/2014 2:36 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/23/2014 2:36 AM
Chloroform 3.33 5.00 J µg/L0.253 NA PA/VA9/23/2014 2:36 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/23/2014 2:36 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/23/2014 2:36 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/23/2014 2:36 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/23/2014 2:36 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/23/2014 2:36 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/23/2014 2:36 AM
Page 15 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 11:43:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-07A Matrix:Groundwater
MW-20Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene 0.470 1.00 J µg/L0.287 NA PA/VA9/23/2014 2:36 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/23/2014 2:36 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/23/2014 2:36 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/23/2014 2:36 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/23/2014 2:36 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/23/2014 2:36 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/23/2014 2:36 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/23/2014 2:36 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/23/2014 2:36 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/23/2014 2:36 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/23/2014 2:36 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/23/2014 2:36 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/23/2014 2:36 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/23/2014 2:36 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/23/2014 2:36 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/23/2014 2:36 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/23/2014 2:36 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/23/2014 2:36 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/23/2014 2:36 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/23/2014 2:36 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/23/2014 2:36 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/23/2014 2:36 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/23/2014 2:36 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/23/2014 2:36 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/23/2014 2:36 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/23/2014 2:36 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/23/2014 2:36 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/23/2014 2:36 AM
Surr: 1,2-Dichloroethane-d4 102 68.7-129 %RECNANA 9/23/2014 2:36 AM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/23/2014 2:36 AM
Surr: Dibromofluoromethane 103 74.3-124 %RECNANA 9/23/2014 2:36 AM
Surr: Toluene-d8 99.3 71.4-129 %RECNANA 9/23/2014 2:36 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 6.0 5.0 mg/L1.0 NA PA/VA9/18/2014 8:40 AM
Page 16 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 9:04:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-08A Matrix:Groundwater
SW-1Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 12:49 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:49 PM
Barium 0.0663 0.100 J mg/L0.0010 NA PA/VA9/24/2014 12:49 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:49 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:49 PM
Chromium 0.0011 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:49 PM
Cobalt 0.0016 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:49 PM
Copper 0.0018 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:49 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/24/2014 12:49 PM
Nickel 0.0029 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 12:49 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:49 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:49 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 12:49 PM
Vanadium 0.0016 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 12:49 PM
Zinc 0.0050 0.0100 J mg/L0.0030 NA PA/VA9/24/2014 12:49 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/23/2014 3:09 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/23/2014 3:09 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/23/2014 3:09 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/23/2014 3:09 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/23/2014 3:09 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/23/2014 3:09 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/23/2014 3:09 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/23/2014 3:09 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/23/2014 3:09 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/23/2014 3:09 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/23/2014 3:09 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/23/2014 3:09 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/23/2014 3:09 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/23/2014 3:09 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/23/2014 3:09 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/23/2014 3:09 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/23/2014 3:09 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/23/2014 3:09 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/23/2014 3:09 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/23/2014 3:09 AM
Page 17 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 9:04:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-08A Matrix:Groundwater
SW-1Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/23/2014 3:09 AM
1,1-Dichloroethane 0.940 5.00 J µg/L0.383 NA PA/VA9/23/2014 3:09 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/23/2014 3:09 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/23/2014 3:09 AM
cis-1,2-Dichloroethene 0.800 5.00 J µg/L0.226 NA PA/VA9/23/2014 3:09 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/23/2014 3:09 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/23/2014 3:09 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/23/2014 3:09 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/23/2014 3:09 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/23/2014 3:09 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/23/2014 3:09 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/23/2014 3:09 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/23/2014 3:09 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/23/2014 3:09 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/23/2014 3:09 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/23/2014 3:09 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/23/2014 3:09 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/23/2014 3:09 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/23/2014 3:09 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/23/2014 3:09 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/23/2014 3:09 AM
Trichloroethene 0.590 1.00 J µg/L0.302 NA PA/VA9/23/2014 3:09 AM
Trichlorofluoromethane 0.340 1.00 J µg/L0.299 NA PA/VA9/23/2014 3:09 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/23/2014 3:09 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/23/2014 3:09 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/23/2014 3:09 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/23/2014 3:09 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/23/2014 3:09 AM
Surr: 1,2-Dichloroethane-d4 103 68.7-129 %RECNANA 9/23/2014 3:09 AM
Surr: 4-Bromofluorobenzene 104 71.8-127 %RECNANA 9/23/2014 3:09 AM
Surr: Dibromofluoromethane 102 74.3-124 %RECNANA 9/23/2014 3:09 AM
Surr: Toluene-d8 101 71.4-129 %RECNANA 9/23/2014 3:09 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids ND 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 18 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 1:58:00 PM
Project:BLACKBURN CLOSED
Lab ID:1409J33-09A Matrix:Groundwater
SW-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 12:55 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:55 PM
Barium 0.0279 0.100 J mg/L0.0010 NA PA/VA9/24/2014 12:55 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:55 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 12:55 PM
Chromium 0.0032 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:55 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:55 PM
Copper 0.0027 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 12:55 PM
Lead 0.0003 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 12:55 PM
Nickel 0.0021 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 12:55 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:55 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 12:55 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 12:55 PM
Vanadium 0.0045 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 12:55 PM
Zinc 0.0043 0.0100 J mg/L0.0030 NA PA/VA9/24/2014 12:55 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/23/2014 3:42 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/23/2014 3:42 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/23/2014 3:42 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/23/2014 3:42 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/23/2014 3:42 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/23/2014 3:42 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/23/2014 3:42 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/23/2014 3:42 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/23/2014 3:42 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/23/2014 3:42 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/23/2014 3:42 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/23/2014 3:42 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/23/2014 3:42 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/23/2014 3:42 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/23/2014 3:42 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/23/2014 3:42 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/23/2014 3:42 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/23/2014 3:42 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/23/2014 3:42 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/23/2014 3:42 AM
Page 19 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 1:58:00 PM
Project:BLACKBURN CLOSED
Lab ID:1409J33-09A Matrix:Groundwater
SW-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/23/2014 3:42 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/23/2014 3:42 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/23/2014 3:42 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/23/2014 3:42 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/23/2014 3:42 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/23/2014 3:42 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/23/2014 3:42 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/23/2014 3:42 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/23/2014 3:42 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/23/2014 3:42 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/23/2014 3:42 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/23/2014 3:42 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/23/2014 3:42 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/23/2014 3:42 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/23/2014 3:42 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/23/2014 3:42 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/23/2014 3:42 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/23/2014 3:42 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/23/2014 3:42 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/23/2014 3:42 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/23/2014 3:42 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/23/2014 3:42 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/23/2014 3:42 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/23/2014 3:42 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/23/2014 3:42 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/23/2014 3:42 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/23/2014 3:42 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/23/2014 3:42 AM
Surr: 1,2-Dichloroethane-d4 99.4 68.7-129 %RECNANA 9/23/2014 3:42 AM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 9/23/2014 3:42 AM
Surr: Dibromofluoromethane 103 74.3-124 %RECNANA 9/23/2014 3:42 AM
Surr: Toluene-d8 100 71.4-129 %RECNANA 9/23/2014 3:42 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 4.0 10 J mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 20 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:30:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-10A Matrix:Groundwater
MW-5 A DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA9/24/2014 1:01 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:01 PM
Barium 0.197 0.100 mg/L0.0010 NA PA/VA9/24/2014 1:01 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 1:01 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 1:01 PM
Chromium 0.0017 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 1:01 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:01 PM
Copper 0.0025 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 1:01 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/24/2014 1:01 PM
Nickel 0.0023 0.0500 J mg/L0.0020 NA PA/VA9/24/2014 1:01 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:01 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:01 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA9/24/2014 1:01 PM
Vanadium 0.0076 0.0250 J mg/L0.0010 NA PA/VA9/24/2014 1:01 PM
Zinc 0.0177 0.0100 mg/L0.0030 NA PA/VA9/24/2014 1:01 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/23/2014 4:15 AM
Acetone ND 100 µg/L4.88 NA PA/VA9/23/2014 4:15 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/23/2014 4:15 AM
Benzene 1.96 1.00 µg/L0.129 NA PA/VA9/23/2014 4:15 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/23/2014 4:15 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/23/2014 4:15 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/23/2014 4:15 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/23/2014 4:15 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/23/2014 4:15 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/23/2014 4:15 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/23/2014 4:15 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/23/2014 4:15 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/23/2014 4:15 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/23/2014 4:15 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/23/2014 4:15 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/23/2014 4:15 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/23/2014 4:15 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/23/2014 4:15 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/23/2014 4:15 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/23/2014 4:15 AM
Page 21 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:30:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-10A Matrix:Groundwater
MW-5 A DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene 0.760 1.00 J µg/L0.287 NA PA/VA9/23/2014 4:15 AM
1,1-Dichloroethane 19.8 5.00 µg/L0.383 NA PA/VA9/23/2014 4:15 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/23/2014 4:15 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/23/2014 4:15 AM
cis-1,2-Dichloroethene 18.9 5.00 µg/L0.226 NA PA/VA9/23/2014 4:15 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/23/2014 4:15 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/23/2014 4:15 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/23/2014 4:15 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/23/2014 4:15 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/23/2014 4:15 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/23/2014 4:15 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/23/2014 4:15 AM
Methylene chloride 1.36 1.00 µg/L0.539 NA PA/VA9/23/2014 4:15 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/23/2014 4:15 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/23/2014 4:15 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/23/2014 4:15 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/23/2014 4:15 AM
Tetrachloroethene 8.11 1.00 µg/L0.196 NA PA/VA9/23/2014 4:15 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/23/2014 4:15 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/23/2014 4:15 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/23/2014 4:15 AM
Trichloroethene 18.2 1.00 µg/L0.302 NA PA/VA9/23/2014 4:15 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/23/2014 4:15 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/23/2014 4:15 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/23/2014 4:15 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/23/2014 4:15 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/23/2014 4:15 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/23/2014 4:15 AM
Surr: 1,2-Dichloroethane-d4 103 68.7-129 %RECNANA 9/23/2014 4:15 AM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/23/2014 4:15 AM
Surr: Dibromofluoromethane 103 74.3-124 %RECNANA 9/23/2014 4:15 AM
Surr: Toluene-d8 98.8 71.4-129 %RECNANA 9/23/2014 4:15 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 4.0 5.0 J mg/L1.0 NA PA/VA9/18/2014 8:40 AM
Page 22 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 1:03:00 PM
Project:BLACKBURN CLOSED
Lab ID:1409J33-11A Matrix:Groundwater
PZ-85BClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/24/2014 8:58 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/24/2014 8:58 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/24/2014 8:58 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/24/2014 8:58 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/24/2014 8:58 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/24/2014 8:58 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/24/2014 8:58 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/24/2014 8:58 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/24/2014 8:58 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/24/2014 8:58 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/24/2014 8:58 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/24/2014 8:58 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/24/2014 8:58 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/24/2014 8:58 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/24/2014 8:58 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/24/2014 8:58 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/24/2014 8:58 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/24/2014 8:58 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/24/2014 8:58 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/24/2014 8:58 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/24/2014 8:58 PM
1,1-Dichloroethane 0.730 5.00 J µg/L0.383 NA PA/VA9/24/2014 8:58 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/24/2014 8:58 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/24/2014 8:58 PM
cis-1,2-Dichloroethene 2.21 5.00 J µg/L0.226 NA PA/VA9/24/2014 8:58 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/24/2014 8:58 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/24/2014 8:58 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/24/2014 8:58 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/24/2014 8:58 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/24/2014 8:58 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/24/2014 8:58 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/24/2014 8:58 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/24/2014 8:58 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/24/2014 8:58 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/24/2014 8:58 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/24/2014 8:58 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/24/2014 8:58 PM
Page 23 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 1:03:00 PM
Project:BLACKBURN CLOSED
Lab ID:1409J33-11A Matrix:Groundwater
PZ-85BClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
Tetrachloroethene 3.36 1.00 µg/L0.196 NA PA/VA9/24/2014 8:58 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/24/2014 8:58 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/24/2014 8:58 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/24/2014 8:58 PM
Trichloroethene 3.26 1.00 µg/L0.302 NA PA/VA9/24/2014 8:58 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/24/2014 8:58 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/24/2014 8:58 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/24/2014 8:58 PM
Vinyl chloride 0.620 1.00 J µg/L0.223 NA PA/VA9/24/2014 8:58 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/24/2014 8:58 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/24/2014 8:58 PM
Surr: 1,2-Dichloroethane-d4 107 68.7-129 %RECNANA 9/24/2014 8:58 PM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 9/24/2014 8:58 PM
Surr: Dibromofluoromethane 102 74.3-124 %RECNANA 9/24/2014 8:58 PM
Surr: Toluene-d8 101 71.4-129 %RECNANA 9/24/2014 8:58 PM
Page 24 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:24:00 PM
Project:BLACKBURN CLOSED
Lab ID:1409J33-12A Matrix:Groundwater
PZ-86BClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/24/2014 9:31 PM
Acetone ND 100 µg/L4.88 NA PA/VA9/24/2014 9:31 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/24/2014 9:31 PM
Benzene 4.34 1.00 µg/L0.129 NA PA/VA9/24/2014 9:31 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/24/2014 9:31 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/24/2014 9:31 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/24/2014 9:31 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/24/2014 9:31 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/24/2014 9:31 PM
Carbon disulfide ND 100 µg/L1.27 NA 9/24/2014 9:31 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/24/2014 9:31 PM
Chlorobenzene 0.460 3.00 J µg/L0.177 NA PA/VA9/24/2014 9:31 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/24/2014 9:31 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/24/2014 9:31 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/24/2014 9:31 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/24/2014 9:31 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/24/2014 9:31 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/24/2014 9:31 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/24/2014 9:31 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/24/2014 9:31 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/24/2014 9:31 PM
1,1-Dichloroethane 33.7 50.0 J µg/L3.83 NA PA/VA9/26/2014 11:18 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/24/2014 9:31 PM
1,1-Dichloroethene 0.460 5.00 J µg/L0.328 NA PA/VA9/24/2014 9:31 PM
cis-1,2-Dichloroethene 21.7 50.0 J µg/L2.26 NA PA/VA9/26/2014 11:18 PM
trans-1,2-Dichloroethene 0.690 5.00 J µg/L0.392 NA PA/VA9/24/2014 9:31 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/24/2014 9:31 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/24/2014 9:31 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/24/2014 9:31 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/24/2014 9:31 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/24/2014 9:31 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/24/2014 9:31 PM
Methylene chloride 22.1 10.0 µg/L5.39 NA PA/VA9/26/2014 11:18 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/24/2014 9:31 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/24/2014 9:31 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/24/2014 9:31 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/24/2014 9:31 PM
Page 25 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:24:00 PM
Project:BLACKBURN CLOSED
Lab ID:1409J33-12A Matrix:Groundwater
PZ-86BClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
Tetrachloroethene 27.7 10.0 µg/L1.96 NA PA/VA9/26/2014 11:18 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/24/2014 9:31 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/24/2014 9:31 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/24/2014 9:31 PM
Trichloroethene 25.1 10.0 µg/L3.02 NA PA/VA9/26/2014 11:18 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/24/2014 9:31 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/24/2014 9:31 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/24/2014 9:31 PM
Vinyl chloride 5.29 1.00 µg/L0.223 NA PA/VA9/24/2014 9:31 PM
o-Xylene 1.41 1.00 µg/L0.186 NA PA/VA9/24/2014 9:31 PM
m,p-Xylene 1.21 2.00 J µg/L0.287 NA PA/VA9/24/2014 9:31 PM
Surr: 1,2-Dichloroethane-d4 108 68.7-129 %RECNANA 9/24/2014 9:31 PM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 9/24/2014 9:31 PM
Surr: Dibromofluoromethane 106 74.3-124 %RECNANA 9/24/2014 9:31 PM
Surr: Toluene-d8 98.5 71.4-129 %RECNANA 9/24/2014 9:31 PM
Page 26 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:00:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-13A Matrix:Trip Blank
TRIP BLANKClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 3:35 AM
Acetone 11.9 100 J µg/L4.88 NA PA/VA9/25/2014 3:35 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA9/25/2014 3:35 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA9/25/2014 3:35 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA9/25/2014 3:35 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA9/25/2014 3:35 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA9/25/2014 3:35 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA9/25/2014 3:35 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA9/25/2014 3:35 AM
Carbon disulfide ND 100 µg/L1.27 NA 9/25/2014 3:35 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA9/25/2014 3:35 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA9/25/2014 3:35 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA9/25/2014 3:35 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA9/25/2014 3:35 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA9/25/2014 3:35 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA9/25/2014 3:35 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA9/25/2014 3:35 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA9/25/2014 3:35 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA9/25/2014 3:35 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA9/25/2014 3:35 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA9/25/2014 3:35 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA9/25/2014 3:35 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 3:35 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA9/25/2014 3:35 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA9/25/2014 3:35 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA9/25/2014 3:35 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA9/25/2014 3:35 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA9/25/2014 3:35 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA9/25/2014 3:35 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA9/25/2014 3:35 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA9/25/2014 3:35 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA9/25/2014 3:35 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA9/25/2014 3:35 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA9/25/2014 3:35 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA9/25/2014 3:35 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA9/25/2014 3:35 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA9/25/2014 3:35 AM
Page 27 of 28
WO#: 1409J33
Date Reported: 9/30/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:00:00 AM
Project:BLACKBURN CLOSED
Lab ID:1409J33-13A Matrix:Trip Blank
TRIP BLANKClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA9/25/2014 3:35 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA9/25/2014 3:35 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA9/25/2014 3:35 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA9/25/2014 3:35 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA9/25/2014 3:35 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA9/25/2014 3:35 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA9/25/2014 3:35 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA9/25/2014 3:35 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA9/25/2014 3:35 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA9/25/2014 3:35 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA9/25/2014 3:35 AM
Surr: 1,2-Dichloroethane-d4 109 68.7-129 %RECNANA 9/25/2014 3:35 AM
Surr: 4-Bromofluorobenzene 109 71.8-127 %RECNANA 9/25/2014 3:35 AM
Surr: Dibromofluoromethane 107 74.3-124 %RECNANA 9/25/2014 3:35 AM
Surr: Toluene-d8 99.2 71.4-129 %RECNANA 9/25/2014 3:35 AM
Page 28 of 28
DB
P i x
E v a l u a t i on
w w w.a mm a r a .c om
DB
P i x
E v a l u a t i on
w w w.a mm a r a .c om
CatawbaCounty,NorthCarolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
Appendix C5:
FieldSamplingSummaries
and
FieldSampleLogs
REIConsultants,Inc.P.OBox 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Cloudy / Sunny66-85°F
Property Units MW-5 MW-5A MW-6 MW-6D
SamplingDepth Feet 6.50 19.04 5.90 5.83
StaticDepth Feet 5.44 4.75 5.73 5.44
WellDepth Feet 17.69 48.40 17.60 53.35
WaterColumnHeight Feet 12.25 43.65 11.87 47.91
VolumePurged Liters 22 76 21 84
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-5 MW-5A MW-6 MW-6D
pH SU 5.54 6.53Dup6.51 5.99 6.77
Temperature oC 19.5 17.0Dup17.1 22.7 18.3
Conductivity umhos/cm 232 239Dup238 872 112
Turbidity NTU 54.4 4.33Dup4.29 15.3 3.71
Appearance -Cloudy Clear Clear Clear
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 30 5 13 2
Property Units MW-7 MW-11 MW-20 PZ-85B
SamplingDepth Feet 14.51 16.24 41.25 20.51
StaticDepth Feet 11.03 15.69 37.30 19.37
WellDepth Feet 17.40 26.60 50.63 44.00
WaterColumnHeight Feet 6.37 10.91 13.33 24.63
VolumePurged Liters 11 20 25 43
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-7 MW-11 MW-20 PZ-85B
pH SU 4.95 5.36 5.31 5.92
Temperature oC 18.2 17.4 17.6 17.6
Conductivity umhos/cm 401 184 78.2 136
Turbidity NTU 89.9 48.7 65.8 276
Appearance -Cloudy Cloudy Cloudy Cloudy
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 29 58 6 -
SAMPLINGLOGSUMMARY
Closed Portion(Permit:#18-03)
1409J33
9/16/2014
CountyofCatawba
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page 1
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Cloudy / Sunny66-85°F
SAMPLINGLOGSUMMARY
Closed Portion(Permit:#18-03)
1409J33
9/16/2014
CountyofCatawba
Property Units PZ-86B SW-1 SW-3
SamplingDepth Feet 33.99 --
StaticDepth Feet 31.86 --
WellDepth Feet 57.78 --
WaterColumnHeight Feet 25.92 --
VolumePurged Liters 46 --
PurgingStatus -FinishedPurging --
PhysicalProperty Units PZ-86B SW-1 SW-3
pH SU 5.99 6.51 6.58
Temperature oC 17.2 19.6 21.5
Conductivity umhos/cm 331 165.3 72.6
Turbidity NTU 19.61 12.53 20.8
Appearance -Clear Clear Clear
Odor -No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L -<2 4
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page 2
ProjectName:Project :Well #:MW-5
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Cloudy 72 °F
5.44 (Ft)7.09 (Liters)
17.69 (Ft)21.27 (Liters)
12.25 (Ft)22.00 (Liters)
pH
Time (SU)
08:47 5.65
08:48 5.55
08:49 5.56
08:50 5.58
08:51 5.58
08:52 5.58
08:53
Date:Time:08:55
Method:SamplingDepth:6.50'
pH:5.54 (SU)Conductivity:232 (umhos/cm)
Temperature:19.5 (oC)Turbidity:54.4 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnClosed Portion 2ndSemi2014
RodneyHamby 704-462-1348
WELL CONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
PURGINGDATA
9/16/201408:44 WeatherConditions:
StaticDepth(DepthtoWater)Volume
EVACUATION/STABILIZATIONTESTDATA
WellDepth 3Volumes
WaterColumnHeight VolumePurged
Conductivity(umhos/cm)(oC)(NTU)(Liters)
TemperatureCorrected Temperature Turbidity VolumePurged
127.2 22.6 5.39 1
129.9 21.5 33.60 4
183.5 19.7 38.40 8
233.0 19.2 51.20 12
233.0 19.0 63.10 16
192.6 19.6 57.90 20
9/16/2014
Finished Purging 22
SAMPLINGDATA
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
Appearance:Cloudy Odor:NoOdor
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page 3
ProjectName:Project :Well #:MW-5A
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Foggy 66 °F
4.75 (Ft)25.27 (Liters)
48.40 (Ft)75.82 (Liters)
43.65 (Ft)76.00 (Liters)
pH
Time (SU)
08:02 6.87
08:06 7.10
08:11 6.53
08:15 6.46
08:20 6.42
08:26 6.44
08:27
Date:Time:08:30
Method:SamplingDepth:19.04'
pH:6.53Dup6.51 (SU)Conductivity:239Dup238 (umhos/cm)
Temperature:17.0Dup17.1 (oC)Turbidity:4.33Dup4.29 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnClosed Portion 2ndSemi2014
RodneyHamby 704-462-1348
WELL CONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
PURGINGDATA
9/16/201407:56 WeatherConditions:
StaticDepth(DepthtoWater)Volume
WellDepth 3Volumes
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
Conductivity(umhos/cm)(oC)(NTU)(Liters)
TurbidityTemperatureCorrectedTemperature VolumePurged
130.0 22.7 0.72 1
129.0 17.4 3.01 14
194.6 16.8 7.50 28
241.0 16.8 7.69 42
240.0 17.0 8.97
239.0 16.8 567.57
70
76
9/16/2014
Finished Purging
SAMPLINGDATA
TeflonBailer
Odor:Appearance:Clear NoOdor
PHYSICAL CHARACTERISTICSOFSAMPLE
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page 4
ProjectName:Project :Well #:MW-6
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Cloudy 77 °F
5.73 (Ft)6.87 (Liters)
17.60 (Ft)20.61 (Liters)
11.87 (Ft)21.00 (Liters)
pH
Time (SU)
09:52 6.04
09:53 5.96
09:54 6.01
09:56 5.98
09:57 5.99
09:58 5.99
09:59
Date:Time:10:00
Method:SamplingDepth:5.90'
pH:5.99 (SU)Conductivity:872 (umhos/cm)
Temperature:22.7 (oC)Turbidity:15.25 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
RodneyHamby 704-462-1348
BlackburnClosed Portion 2ndSemi2014
WELL CONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
9/16/201409:49 WeatherConditions:
PURGINGDATA
StaticDepth(DepthtoWater)Volume
EVACUATION/STABILIZATIONTESTDATA
WellDepth 3Volumes
WaterColumnHeight VolumePurged
(oC)(NTU)Conductivity(umhos/cm)
TemperatureCorrected Temperature Turbidity VolumePurged
1
(Liters)
24.3 61.4455.0
75.3 4778.0 23.4
23.0 78 8831.0
1222.8 68.8856.0
75.4 16
22.8 36.8
22.8865.0
20876.0
Finished Purging 21
9/16/2014
SAMPLINGDATA
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
Clear Odor:NoOdorAppearance:
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page 5
ProjectName:Project :Well #:MW-6D
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Cloudy 72 °F
5.44 (Ft)27.73 (Liters)
53.35 (Ft)83.21 (Liters)
47.91 (Ft)84.00 (Liters)
pH
Time (SU)
09:19 6.78
09:23 6.74
09:26 6.75
09:31 6.79
09:35 6.80
09:39 6.81
09:40
Date:Time:09:42
Method:SamplingDepth:5.83'
pH:6.77 (SU)Conductivity:112.3 (umhos/cm)
Temperature:18.3 (oC)Turbidity:3.71 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
2ndSemi2014
RodneyHamby
BlackburnClosed Portion
WELL CONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
704-462-1348
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
PURGINGDATA
9/16/201409:15 WeatherConditions:
StaticDepth(DepthtoWater)Volume
WellDepth 3Volumes
TemperatureCorrected
WaterColumnHeight VolumePurged
EVACUATION/STABILIZATIONTESTDATA
Turbidity VolumePurgedTemperature
111.8 23.9 0.79 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
3.18 16111.0 19.0
113.6 18.3 6.16 32
112.8 18.2 6.28 48
113.3 18.2 5.4 64
113.0 18.0 5.39 80
84Finished Purging
9/16/2014
SAMPLINGDATA
TeflonBailer
Clear
PHYSICAL CHARACTERISTICSOFSAMPLE
Odor:Appearance:NoOdor
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page 6
ProjectName:Project :Well #:MW-7
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 78 °F
11.03 (Ft)3.68 (Liters)
17.40 (Ft)11.06 (Liters)
6.37 (Ft)11.00 (Liters)
pH
Time (SU)
10:35 5.15
10:37 4.96
10:38 4.89
10:39 4.92
10:40 4.92
10:41 4.96
10:41
Date:Time:10:44
Method:SamplingDepth:14.51'
pH:4.95 (SU)Conductivity:401 (umhos/cm)
Temperature:18.2 (oC)Turbidity:89.9 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
704-462-1348
2ndSemi2014BlackburnClosed Portion
WELL CONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
RodneyHamby
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
StaticDepth(DepthtoWater)
PURGINGDATA
9/16/201410:31 WeatherConditions:
Volume
WellDepth 3Volumes
VolumePurged
Turbidity VolumePurged
WaterColumnHeight
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature
20.6 21.6459.0
Conductivity(umhos/cm)(oC)(NTU)(Liters)
1
449.0 18.7 423 3
>800 5439.0 18.2
718.1 >800
455414.0 18.0
430.0
398.0
9
17.9 314 11
Finished Purging
SAMPLINGDATA
11
9/16/2014
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
NoOdorAppearance:Cloudy Odor:
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page 7
ProjectName:Project :Well #:MW-11
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:PartlyCloudy82 °F
15.69 (Ft)6.31 (Liters)
26.60 (Ft)18.95 (Liters)
10.91 (Ft)20.00 (Liters)
pH
Time (SU)
10:59 5.24
11:00 5.33
11:01 5.46
11:03 5.29
11:04 5.39
11:05 5.44
11:05
Date:Time:11:08
Method:SamplingDepth:16.24'
pH:5.36 (SU)Conductivity:183.8 (umhos/cm)
Temperature:17.4 (oC)Turbidity:48.7 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
2ndSemi2014
RodneyHamby
BlackburnClosed Portion
ProtectiveCasingPresent PhysicalDamage
704-462-1348
WELL CONDITIONDATA
Concrete/GroutPadPresentProtectiveCasingLocked
CaponWellRiser 2"PVCCasing
WeatherConditions:
PURGINGDATA
9/16/201410:53
StaticDepth(DepthtoWater)Volume
WaterColumnHeight
WellDepth 3Volumes
TemperatureCorrected
VolumePurged
EVACUATION/STABILIZATIONTESTDATA
Turbidity VolumePurgedTemperature
Conductivity(umhos/cm)(oC)(NTU)(Liters)
132.5 19.1 20 1
4164.1 18.2 57.8
190.4 17.7 50 8
162.5 17.2 10.39 12
16
197.8
187.1 17.2 32.9
17.2 25.6 20
9/16/2014
SAMPLINGDATA
Finished Purging 20
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
Appearance:Cloudy Odor:NoOdor
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page 8
ProjectName:Project :Well #:MW-20
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 82 °F
37.30 (Ft)7.71 (Liters)
50.63 (Ft)23.15 (Liters)
13.33 (Ft)25.00 (Liters)
pH
Time (SU)
11:27 5.28
11:30 5.30
11:32 5.35
11:34 5.50
11:36 5.54
11:38 5.57
11:38
Date:Time:11:43
Method:SamplingDepth:41.25'
pH:5.31 (SU)Conductivity:78.2 (umhos/cm)
Temperature:17.6 (oC)Turbidity:65.8 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnClosed Portion 2ndSemi2014
RodneyHamby 704-462-1348
WELL CONDITIONDATA
2"PVCCasingCaponWellRiser
PhysicalDamageProtectiveCasingPresent
ProtectiveCasingLocked Concrete/GroutPadPresent
WeatherConditions:
PURGINGDATA
9/16/201411:22
StaticDepth(DepthtoWater)Volume
WellDepth 3Volumes
EVACUATION/STABILIZATIONTESTDATA
VolumePurgedWaterColumnHeight
TemperatureCorrected Temperature Turbidity VolumePurged
(NTU)(Liters)Conductivity(umhos/cm)(oC)
154.8 18.6 27.4
69.0 17.6 557 5
374
79.4 17.3 429
85.9 17.2 15
10
88.5 17.2 189 20
89.6 17.2 195 25
25
9/16/2014
SAMPLINGDATA
Finished Purging
TeflonBailer
Cloudy
PHYSICAL CHARACTERISTICSOFSAMPLE
Appearance:Odor:NoOdor
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page 9
ProjectName:Project :Well #:PZ-85B
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 85 °F
19.37 (Ft)14.26 (Liters)
44.00 (Ft)42.78 (Liters)
24.63 (Ft)43.00 (Liters)
pH
Time (SU)
12:44 6.68
12:47 6.45
12:49 6.15
12:52 5.98
12:55 5.98
12:59 5.90
13:01
Date:Time:13:03
Method:SamplingDepth:20.51'
pH:5.92 (SU)Conductivity:136.3 (umhos/cm)
Temperature:17.6 (oC)Turbidity:276 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnClosed Portion 2ndSemi2014
RodneyHamby
WELL CONDITIONDATA
704-462-1348
CaponWellRiser 2"PVCCasing
PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent
WeatherConditions:9/16/201412:38
PURGINGDATA
StaticDepth(DepthtoWater)Volume
3Volumes
VolumePurged
WellDepth
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight
TemperatureCorrected Temperature Turbidity VolumePurged
(oC)(NTU)(Liters)Conductivity(umhos/cm)
134.9 19.6 12.8 1
27.6 7135.3 17.6
140.1
142.9 17.5 152
17.4 41.3 14
21
140.7 17.2 213 28
17.5 193 35139.6
Finished Purging 43
9/16/2014
SAMPLINGDATA
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
NoOdorAppearance:Cloudy Odor:
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page10
ProjectName:Project :Well #:PZ-86B
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 83 °F
31.86 (Ft)15.00 (Liters)
57.78 (Ft)45.02 (Liters)
25.92 (Ft)46.00 (Liters)
pH
Time (SU)
12:02 6.58
12:06 6.19
12:08 5.96
12:12 5.97
12:15 5.99
12:20 5.97
12:22
Date:Time:12:24
Method:SamplingDepth:33.99'
pH:5.99 (SU)Conductivity:331 (umhos/cm)
Temperature:17.2 (oC)Turbidity:19.61 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnClosed Portion 2ndSemi2014
RodneyHamby
WELL CONDITIONDATA
704-462-1348
ProtectiveCasingPresent PhysicalDamage
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
PURGINGDATA
9/16/201411:58 WeatherConditions:
WaterColumnHeight
3Volumes
StaticDepth(DepthtoWater)Volume
EVACUATION/STABILIZATIONTESTDATA
VolumePurged
WellDepth
TemperatureCorrected VolumePurgedTemperatureTurbidity
(Liters)Conductivity(umhos/cm)(oC)(NTU)
1
322.0
19.1
17.5 11.71
6.58315.0
8
20.1 24
16348.0 17.2 15.13
347.0 17.2
3223.3340.0 17.2
40334.0 17.1 17.43
46Finished Purging
9/16/2014
SAMPLINGDATA
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
Odor:NoOdorClearAppearance:
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page11
Outlet:
Date:09:04
pH:6.51 Conductivity:165.3 umhos/cm
Flow:N/A Temperature:19.6 o C
Clear /NoOdor
Turbidity=12.53NTU
Outlet:
Date:13:58
pH:6.58 Conductivity:72.6 umhos/cm
Flow:N/A Temperature:21.5 o C
Clear /NoOdor
Turbidity=20.8NTU
Outlet:
Date:
pH:Conductivity:umhos/cm
Flow:Temperature:o C
SurfaceWaterSampling Log
REIConsultants,Inc.
ProjectName:BlackburnClosedPortion
SampleOdorand PhysicalAppearance:
SW-3
Contact Person:RodneyHamby Phone/Fax:[phone]
SW-1
9/16/2014 Time:
SampleOdorand PhysicalAppearance:
Comments:
Comments:
9/16/2014 Time:
SampleOdorand PhysicalAppearance:
Comments:
Time:
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC5-Page12
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
AppendixC6:
Historical Results
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-5
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page 1
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-5A
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page17
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-6
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page33
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-6D
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page49
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-7
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page60
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-11
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page76
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-20
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page87
Closed Portion
HistoricalDataSummary
SurfaceWater:SW-1
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page98
Closed Portion
HistoricalDataSummary
SurfaceWater:SW-3
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page109
Closed Portion
Historical Data Summary
Piezometer:PZ-85B
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page120
Closed Portion
Historical Data Summary
Piezometer:PZ-86B
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixC6-Page125
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD1:
2ndSemi-Annual2014
Summary of Detections
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
1
-O n l y
re
s
u lt
s
a b ov
e
S W SL
's s ho
wn
2
1
2
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD2:
Summary of Dissolved Metals and
TotalSuspendedSolid(TSS)
Detections
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Su
mm
a r y
o f
Di
ss
o lv
e d
Me
t a l s
a nd
T SS
D e t e c ti
o
ns
B l a c kb
u
r n
L
a nd
f il
l
:
C
& D
P e r m i t :
#18
-03
R E I C
J o b
N u m b e r :
1 4 03
S 11
S a m p l e
D a t e :
9 -16
-2 0 14
A r s e n i c ,
D i ss
o l v ed
0 .01
B a r i um
,
D i ss
o l v ed
0 .1
0 .1 45
0 .2 93
0 .1 25
0 .2 20
C a d m i um
,
D i ss
o l v ed
0 .0 01
C h r o m i um
,
D i ss
o l v ed
0 .01
L ea
d,
D i ss
o l v ed
0 .01
S e l e n i um
,
D i ss
o l v ed
0 .01
S il
v e r ,
D i ss
o l v ed
0 .01
M e r cu
ry
,
D i ss
o l v ed
0 .0 0 02
T o t a l S
u
s p e nd
e d
S
o li
d s
(T SS
)
1
1 01
62
33
9 62
1 37
36
1 29
2 15 3 49
Ol
d
C
& D
N e w
C
& D
F OO
T NO
T E S:
1.
S W SL
-
S o l id
W a s te
Se
c ti
on
L i m it
(m
g /L)
2.
O n ly
re
su
l ts
a b o ve
S WS
Ls
sh
o wn
S P E CI
AL
NO
T E S:
A ll
d a ta
re
p o r t ed
in
m g /L.
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD3:
HistoricalSummaryofDetections
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
H I S TO
R IC
AL
SU
MM
A R Y
O F
D E T E C T I ON
S
M o n it
o r i ng
W e ll
:
MW
-
2
Bl
a c kb
u
rn
L a n d f il
l
:
C
& D
P a r a m e t er
G W S
t d.
1
P QL
2
J u l-
19
9
2
M a r-
19
9
6
S e p -19
9
6
A p r-
19
9
7
S e p -19
9
7
M a r-
19
9
8
S e p -19
9
8
M a r-
19
9
9
S e p -19
9
9
M a r-2000 S e p -2000 M a y -2001
B a ri
um
2 .0
0 .50
0
0 .649
C a d m i um
0 .00
1 75
0 .00
1
0 .00
9
Ch
r o m i um
0 .05
0 .05
0 .00
7
0 .03
7
0 .02
0
0 .04
3
0 .01
2
0 .105 0 .018 0 .033
T SS
1
P a r a m e t er
G W S
t d.
1
P QL
2
S e p -20
0
1
M a r-
20
0
2
S e p -20
0
2
M a r-
20
0
3
S e p -20
0
3
M a r-
20
0
4
S e p -20
0
4
M a r-
20
0
5
S e p -20
0
5
M a y -2006 S e p -2006
B a ri
um
2 .0
0 .50
0
0 .155
C a d m i um
0 .00
1 75
0 .00
1
Ch
r o m i um
0 .05
0 .05
0 .01
36
T SS
1
38
1
58
73
62
35
5
30
23
P a r a m e t er
G W S
t d.
1
S W SL
3
M a r-
20
0
7
S e p -20
0
7
M a r-
20
0
8
S e p -20
0
8
M a r-
20
0
9
S e p -20
0
9
G W S
t d.
1
S W SL
3
M a r-
20
1
0
S e p -2010 M a r-2011 S e p -2011
B a ri
um
2 .0
0 .10
0
0 .12
4
0 .22
1
0 .16
0
0 .18
1
0 .14
4
0 .19
8
0 .7
0 .10
0
0 .12
1
0 .172 0 .141 0 .198
C a d m i um
0 .00
1 75
0 .00
1
0 .00
2
0 .00
1
Ch
r o m i um
0 .05
0 .01
0
0 .01
0 .01
0
T SS
1
37
37
7
7
13
19
1
13
6 19 2
P a r a m e t er
G W S
t d.
1
S W SL
3
M a r-
20
1
2
S e p -20
1
2
M a r-
20
1
3
S e p -20
1
3
M a r-
20
1
4
S e p -20
1
4
B a ri
um
0 .7
0 .10
0
0 .17
5
0 .23
1
0 .17
1
0 .16
1
0 .21
1
0 .16
3
C a d m i um
0 .00
2
0 .00
1
Ch
r o m i um
0 .01
0 .01
0
T SS
1
-
30
12
13
17
10
1
F OO
T NO
T E S:
S PE
CI
A L
NO
T E S:
1
G W S
t d.
-
N o rt
h Ca
r o li
na
g r o u nd
w a t e r
s t a n da
r d s
(m g /L ).
-T SS
- To
t a l Su
s p e nd
e d So
li
ds
2
P Q L
-
P r a c t i c a l
Q u an
t i t a t i on
L i m i t s
(m g /L ).
-O n l y
r es
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S
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S
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S
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S
1
3
1
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1
3
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Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD4:
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Wednesday, October 01, 2014
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:BLACKBURN C&D
Work Order #:1409J34
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 11 sample(s) on 9/17/2014 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Case Narrative
Client:
Project:BLACKBURN C&D
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:35:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-01A Matrix:Groundwater
MW-2Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:29 PM
Barium 0.163 0.100 mg/L0.0010 NA PA/VA9/24/2014 1:29 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 1:29 PM
Chromium 0.0037 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 1:29 PM
Lead 0.0003 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 1:29 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:29 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:29 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury ND 0.0010 mg/L0.0001 NA PA/VA9/19/2014 9:55 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 4:36 PM
Acetone ND 100 µg/L5.00 NA PA/VA9/25/2014 4:36 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/25/2014 4:36 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 4:36 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/25/2014 4:36 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/25/2014 4:36 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/25/2014 4:36 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/25/2014 4:36 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/25/2014 4:36 PM
Carbon disulfide ND 100 µg/L2.25 NA 9/25/2014 4:36 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/25/2014 4:36 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/25/2014 4:36 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/25/2014 4:36 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/25/2014 4:36 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/25/2014 4:36 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/25/2014 4:36 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/25/2014 4:36 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/25/2014 4:36 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/25/2014 4:36 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/25/2014 4:36 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/25/2014 4:36 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/25/2014 4:36 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/25/2014 4:36 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/25/2014 4:36 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/25/2014 4:36 PM
Page 3 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:35:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-01A Matrix:Groundwater
MW-2Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/25/2014 4:36 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/25/2014 4:36 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/25/2014 4:36 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/25/2014 4:36 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/25/2014 4:36 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/25/2014 4:36 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/25/2014 4:36 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/25/2014 4:36 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/25/2014 4:36 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/25/2014 4:36 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/25/2014 4:36 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/25/2014 4:36 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/25/2014 4:36 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 4:36 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/25/2014 4:36 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/25/2014 4:36 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/25/2014 4:36 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/25/2014 4:36 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 4:36 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/25/2014 4:36 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/25/2014 4:36 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/25/2014 4:36 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/25/2014 4:36 PM
Surr: 1,2-Dichloroethane-d4 109 68.7-129 %RECNANA 9/25/2014 4:36 PM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 9/25/2014 4:36 PM
Surr: Dibromofluoromethane 101 74.3-124 %RECNANA 9/25/2014 4:36 PM
Surr: Toluene-d8 99.8 71.4-129 %RECNANA 9/25/2014 4:36 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 9/29/2014 7:59 PM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/25/2014 4:36 PM
Surr: 1,2-Dichloroethane-d4 97.3 80-120 %RECNANA 9/25/2014 4:36 PM
Surr: 4-Bromofluorobenzene 98.7 80-120 %RECNANA 9/25/2014 4:36 PM
Surr: Dibromofluoromethane 96.5 80-120 %RECNANA 9/25/2014 4:36 PM
Surr: Toluene-d8 95.5 80-120 %RECNANA 9/25/2014 4:36 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 101 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 4 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 10:27:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-02A Matrix:Groundwater
MW-21Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:34 PM
Barium 0.232 0.100 mg/L0.0010 NA PA/VA9/24/2014 1:34 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 1:34 PM
Chromium 0.0182 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:34 PM
Lead 0.0042 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 1:34 PM
Selenium 0.0012 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 1:34 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:34 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury ND 0.0010 mg/L0.0001 NA PA/VA9/19/2014 9:58 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 5:10 PM
Acetone ND 100 µg/L5.00 NA PA/VA9/25/2014 5:10 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/25/2014 5:10 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 5:10 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/25/2014 5:10 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/25/2014 5:10 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/25/2014 5:10 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/25/2014 5:10 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/25/2014 5:10 PM
Carbon disulfide ND 100 µg/L2.25 NA 9/25/2014 5:10 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/25/2014 5:10 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/25/2014 5:10 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/25/2014 5:10 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/25/2014 5:10 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/25/2014 5:10 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/25/2014 5:10 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/25/2014 5:10 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/25/2014 5:10 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/25/2014 5:10 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/25/2014 5:10 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/25/2014 5:10 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/25/2014 5:10 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/25/2014 5:10 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/25/2014 5:10 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/25/2014 5:10 PM
Page 5 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 10:27:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-02A Matrix:Groundwater
MW-21Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/25/2014 5:10 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/25/2014 5:10 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/25/2014 5:10 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/25/2014 5:10 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/25/2014 5:10 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/25/2014 5:10 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/25/2014 5:10 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/25/2014 5:10 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/25/2014 5:10 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/25/2014 5:10 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/25/2014 5:10 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/25/2014 5:10 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/25/2014 5:10 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 5:10 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/25/2014 5:10 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/25/2014 5:10 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/25/2014 5:10 PM
Trichlorofluoromethane 0.540 1.00 J µg/L0.223 NA PA/VA9/25/2014 5:10 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 5:10 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/25/2014 5:10 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/25/2014 5:10 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/25/2014 5:10 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/25/2014 5:10 PM
Surr: 1,2-Dichloroethane-d4 110 68.7-129 %RECNANA 9/25/2014 5:10 PM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 9/25/2014 5:10 PM
Surr: Dibromofluoromethane 108 74.3-124 %RECNANA 9/25/2014 5:10 PM
Surr: Toluene-d8 101 71.4-129 %RECNANA 9/25/2014 5:10 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 9/29/2014 8:32 PM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/25/2014 5:10 PM
Surr: 1,2-Dichloroethane-d4 99.7 80-120 %RECNANA 9/25/2014 5:10 PM
Surr: 4-Bromofluorobenzene 99.1 80-120 %RECNANA 9/25/2014 5:10 PM
Surr: Dibromofluoromethane 97.6 80-120 %RECNANA 9/25/2014 5:10 PM
Surr: Toluene-d8 96.3 80-120 %RECNANA 9/25/2014 5:10 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 962 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 6 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 10:59:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-03A Matrix:Groundwater
MW-24Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:40 PM
Barium 0.153 0.100 mg/L0.0010 NA PA/VA9/24/2014 1:40 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 1:40 PM
Chromium 0.0098 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 1:40 PM
Lead 0.0010 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 1:40 PM
Selenium 0.0010 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 1:40 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:40 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury ND 0.0010 mg/L0.0001 NA PA/VA9/19/2014 10:00 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 5:43 PM
Acetone 7.84 100 J µg/L5.00 NA PA/VA9/25/2014 5:43 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/25/2014 5:43 PM
Benzene 0.330 1.00 J µg/L0.250 NA PA/VA9/25/2014 5:43 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/25/2014 5:43 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/25/2014 5:43 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/25/2014 5:43 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/25/2014 5:43 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/25/2014 5:43 PM
Carbon disulfide ND 100 µg/L2.25 NA 9/25/2014 5:43 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/25/2014 5:43 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/25/2014 5:43 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/25/2014 5:43 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/25/2014 5:43 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/25/2014 5:43 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/25/2014 5:43 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/25/2014 5:43 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/25/2014 5:43 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/25/2014 5:43 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/25/2014 5:43 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/25/2014 5:43 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/25/2014 5:43 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/25/2014 5:43 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/25/2014 5:43 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/25/2014 5:43 PM
Page 7 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 10:59:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-03A Matrix:Groundwater
MW-24Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/25/2014 5:43 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/25/2014 5:43 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/25/2014 5:43 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/25/2014 5:43 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/25/2014 5:43 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/25/2014 5:43 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/25/2014 5:43 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/25/2014 5:43 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/25/2014 5:43 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/25/2014 5:43 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/25/2014 5:43 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/25/2014 5:43 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/25/2014 5:43 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 5:43 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/25/2014 5:43 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/25/2014 5:43 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/25/2014 5:43 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/25/2014 5:43 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 5:43 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/25/2014 5:43 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/25/2014 5:43 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/25/2014 5:43 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/25/2014 5:43 PM
Surr: 1,2-Dichloroethane-d4 109 68.7-129 %RECNANA 9/25/2014 5:43 PM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 9/25/2014 5:43 PM
Surr: Dibromofluoromethane 106 74.3-124 %RECNANA 9/25/2014 5:43 PM
Surr: Toluene-d8 99.7 71.4-129 %RECNANA 9/25/2014 5:43 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran 20.9 50.0 J µg/L12.5 NA 9/29/2014 9:05 PM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/25/2014 5:43 PM
Surr: 1,2-Dichloroethane-d4 99.0 80-120 %RECNANA 9/25/2014 5:43 PM
Surr: 4-Bromofluorobenzene 102 80-120 %RECNANA 9/25/2014 5:43 PM
Surr: Dibromofluoromethane 97.4 80-120 %RECNANA 9/25/2014 5:43 PM
Surr: Toluene-d8 95.3 80-120 %RECNANA 9/25/2014 5:43 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 137 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 8 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 11:20:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-04A Matrix:Groundwater
MW-25Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:46 PM
Barium 0.216 0.100 mg/L0.0010 NA PA/VA9/24/2014 1:46 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 1:46 PM
Chromium 0.0023 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 1:46 PM
Lead 0.0002 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 1:46 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:46 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:46 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury ND 0.0010 mg/L0.0001 NA PA/VA9/19/2014 10:02 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 6:16 PM
Acetone 5.01 100 J µg/L5.00 NA PA/VA9/25/2014 6:16 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/25/2014 6:16 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 6:16 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/25/2014 6:16 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/25/2014 6:16 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/25/2014 6:16 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/25/2014 6:16 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/25/2014 6:16 PM
Carbon disulfide ND 100 µg/L2.25 NA 9/25/2014 6:16 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/25/2014 6:16 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/25/2014 6:16 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/25/2014 6:16 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/25/2014 6:16 PM
Chloromethane 0.370 1.00 J µg/L0.350 NA PA/VA9/25/2014 6:16 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/25/2014 6:16 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/25/2014 6:16 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/25/2014 6:16 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/25/2014 6:16 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/25/2014 6:16 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/25/2014 6:16 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/25/2014 6:16 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/25/2014 6:16 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/25/2014 6:16 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/25/2014 6:16 PM
Page 9 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 11:20:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-04A Matrix:Groundwater
MW-25Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/25/2014 6:16 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/25/2014 6:16 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/25/2014 6:16 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/25/2014 6:16 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/25/2014 6:16 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/25/2014 6:16 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/25/2014 6:16 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/25/2014 6:16 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/25/2014 6:16 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/25/2014 6:16 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/25/2014 6:16 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/25/2014 6:16 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/25/2014 6:16 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 6:16 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/25/2014 6:16 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/25/2014 6:16 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/25/2014 6:16 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/25/2014 6:16 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 6:16 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/25/2014 6:16 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/25/2014 6:16 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/25/2014 6:16 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/25/2014 6:16 PM
Surr: 1,2-Dichloroethane-d4 111 68.7-129 %RECNANA 9/25/2014 6:16 PM
Surr: 4-Bromofluorobenzene 108 71.8-127 %RECNANA 9/25/2014 6:16 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 9/25/2014 6:16 PM
Surr: Toluene-d8 100 71.4-129 %RECNANA 9/25/2014 6:16 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran 23.1 50.0 J µg/L12.5 NA 9/29/2014 9:38 PM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/25/2014 6:16 PM
Surr: 1,2-Dichloroethane-d4 100 80-120 %RECNANA 9/25/2014 6:16 PM
Surr: 4-Bromofluorobenzene 99.5 80-120 %RECNANA 9/25/2014 6:16 PM
Surr: Dibromofluoromethane 97.3 80-120 %RECNANA 9/25/2014 6:16 PM
Surr: Toluene-d8 96.1 80-120 %RECNANA 9/25/2014 6:16 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 36.0 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 10 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 9:50:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-05A Matrix:Groundwater
MW-26Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:51 PM
Barium 0.0802 0.100 J mg/L0.0010 NA PA/VA9/24/2014 1:51 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 1:51 PM
Chromium 0.0030 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 1:51 PM
Lead 0.0004 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 1:51 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:51 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:51 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury ND 0.0010 mg/L0.0001 NA PA/VA9/19/2014 10:09 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 6:49 PM
Acetone ND 100 µg/L5.00 NA PA/VA9/25/2014 6:49 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/25/2014 6:49 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 6:49 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/25/2014 6:49 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/25/2014 6:49 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/25/2014 6:49 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/25/2014 6:49 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/25/2014 6:49 PM
Carbon disulfide ND 100 µg/L2.25 NA 9/25/2014 6:49 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/25/2014 6:49 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/25/2014 6:49 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/25/2014 6:49 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/25/2014 6:49 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/25/2014 6:49 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/25/2014 6:49 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/25/2014 6:49 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/25/2014 6:49 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/25/2014 6:49 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/25/2014 6:49 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/25/2014 6:49 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/25/2014 6:49 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/25/2014 6:49 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/25/2014 6:49 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/25/2014 6:49 PM
Page 11 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 9:50:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-05A Matrix:Groundwater
MW-26Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/25/2014 6:49 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/25/2014 6:49 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/25/2014 6:49 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/25/2014 6:49 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/25/2014 6:49 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/25/2014 6:49 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/25/2014 6:49 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/25/2014 6:49 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/25/2014 6:49 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/25/2014 6:49 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/25/2014 6:49 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/25/2014 6:49 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/25/2014 6:49 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 6:49 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/25/2014 6:49 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/25/2014 6:49 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/25/2014 6:49 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/25/2014 6:49 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 6:49 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/25/2014 6:49 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/25/2014 6:49 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/25/2014 6:49 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/25/2014 6:49 PM
Surr: 1,2-Dichloroethane-d4 110 68.7-129 %RECNANA 9/25/2014 6:49 PM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 9/25/2014 6:49 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 9/25/2014 6:49 PM
Surr: Toluene-d8 100 71.4-129 %RECNANA 9/25/2014 6:49 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 9/29/2014 10:11 PM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/25/2014 6:49 PM
Surr: 1,2-Dichloroethane-d4 98.9 80-120 %RECNANA 9/25/2014 6:49 PM
Surr: 4-Bromofluorobenzene 98.7 80-120 %RECNANA 9/25/2014 6:49 PM
Surr: Dibromofluoromethane 96.2 80-120 %RECNANA 9/25/2014 6:49 PM
Surr: Toluene-d8 95.7 80-120 %RECNANA 9/25/2014 6:49 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 62.0 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 12 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 9:17:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-06A Matrix:Groundwater
MW-27Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:57 PM
Barium 0.308 0.100 mg/L0.0010 NA PA/VA9/24/2014 1:57 PM
Cadmium 0.0004 0.0010 J mg/L0.0002 NA PA/VA9/24/2014 1:57 PM
Chromium 0.0038 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 1:57 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/24/2014 1:57 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:57 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 1:57 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury 0.0002 0.0010 J mg/L0.0001 NA PA/VA9/19/2014 10:11 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 7:22 PM
Acetone 5.82 100 J µg/L5.00 NA PA/VA9/25/2014 7:22 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/25/2014 7:22 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 7:22 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/25/2014 7:22 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/25/2014 7:22 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/25/2014 7:22 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/25/2014 7:22 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/25/2014 7:22 PM
Carbon disulfide ND 100 µg/L2.25 NA 9/25/2014 7:22 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/25/2014 7:22 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/25/2014 7:22 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/25/2014 7:22 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/25/2014 7:22 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/25/2014 7:22 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/25/2014 7:22 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/25/2014 7:22 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/25/2014 7:22 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/25/2014 7:22 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/25/2014 7:22 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/25/2014 7:22 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/25/2014 7:22 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/25/2014 7:22 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/25/2014 7:22 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/25/2014 7:22 PM
Page 13 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 9:17:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-06A Matrix:Groundwater
MW-27Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/25/2014 7:22 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/25/2014 7:22 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/25/2014 7:22 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/25/2014 7:22 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/25/2014 7:22 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/25/2014 7:22 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/25/2014 7:22 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/25/2014 7:22 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/25/2014 7:22 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/25/2014 7:22 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/25/2014 7:22 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/25/2014 7:22 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/25/2014 7:22 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 7:22 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/25/2014 7:22 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/25/2014 7:22 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/25/2014 7:22 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/25/2014 7:22 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 7:22 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/25/2014 7:22 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/25/2014 7:22 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/25/2014 7:22 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/25/2014 7:22 PM
Surr: 1,2-Dichloroethane-d4 115 68.7-129 %RECNANA 9/25/2014 7:22 PM
Surr: 4-Bromofluorobenzene 104 71.8-127 %RECNANA 9/25/2014 7:22 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 9/25/2014 7:22 PM
Surr: Toluene-d8 99.8 71.4-129 %RECNANA 9/25/2014 7:22 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 9/30/2014 3:08 AM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/25/2014 7:22 PM
Surr: 1,2-Dichloroethane-d4 102 80-120 %RECNANA 9/25/2014 7:22 PM
Surr: 4-Bromofluorobenzene 99.6 80-120 %RECNANA 9/25/2014 7:22 PM
Surr: Dibromofluoromethane 97.1 80-120 %RECNANA 9/25/2014 7:22 PM
Surr: Toluene-d8 95.0 80-120 %RECNANA 9/25/2014 7:22 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 33.0 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 14 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 11:39:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-07A Matrix:Groundwater
MW-28Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:03 PM
Barium 0.151 0.100 mg/L0.0010 NA PA/VA9/24/2014 2:03 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 2:03 PM
Chromium 0.0034 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 2:03 PM
Lead 0.0017 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 2:03 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:03 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:03 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury ND 0.0010 mg/L0.0001 NA PA/VA9/19/2014 10:13 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 7:55 PM
Acetone ND 100 µg/L5.00 NA PA/VA9/25/2014 7:55 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/25/2014 7:55 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 7:55 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/25/2014 7:55 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/25/2014 7:55 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/25/2014 7:55 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/25/2014 7:55 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/25/2014 7:55 PM
Carbon disulfide ND 100 µg/L2.25 NA 9/25/2014 7:55 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/25/2014 7:55 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/25/2014 7:55 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/25/2014 7:55 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/25/2014 7:55 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/25/2014 7:55 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/25/2014 7:55 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/25/2014 7:55 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/25/2014 7:55 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/25/2014 7:55 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/25/2014 7:55 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/25/2014 7:55 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/25/2014 7:55 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/25/2014 7:55 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/25/2014 7:55 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/25/2014 7:55 PM
Page 15 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 11:39:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-07A Matrix:Groundwater
MW-28Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/25/2014 7:55 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/25/2014 7:55 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/25/2014 7:55 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/25/2014 7:55 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/25/2014 7:55 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/25/2014 7:55 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/25/2014 7:55 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/25/2014 7:55 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/25/2014 7:55 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/25/2014 7:55 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/25/2014 7:55 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/25/2014 7:55 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/25/2014 7:55 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 7:55 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/25/2014 7:55 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/25/2014 7:55 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/25/2014 7:55 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/25/2014 7:55 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 7:55 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/25/2014 7:55 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/25/2014 7:55 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/25/2014 7:55 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/25/2014 7:55 PM
Surr: 1,2-Dichloroethane-d4 113 68.7-129 %RECNANA 9/25/2014 7:55 PM
Surr: 4-Bromofluorobenzene 104 71.8-127 %RECNANA 9/25/2014 7:55 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 9/25/2014 7:55 PM
Surr: Toluene-d8 101 71.4-129 %RECNANA 9/25/2014 7:55 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 9/30/2014 3:41 AM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/25/2014 7:55 PM
Surr: 1,2-Dichloroethane-d4 101 80-120 %RECNANA 9/25/2014 7:55 PM
Surr: 4-Bromofluorobenzene 99.6 80-120 %RECNANA 9/25/2014 7:55 PM
Surr: Dibromofluoromethane 96.4 80-120 %RECNANA 9/25/2014 7:55 PM
Surr: Toluene-d8 96.4 80-120 %RECNANA 9/25/2014 7:55 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 129 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 16 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:05:00 PM
Project:BLACKBURN C&D
Lab ID:1409J34-08A Matrix:Groundwater
MW-29Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:42 PM
Barium 0.140 0.100 mg/L0.0010 NA PA/VA9/24/2014 2:42 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 2:42 PM
Chromium 0.0342 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:42 PM
Lead 0.0026 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 2:42 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:42 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:42 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury ND 0.0010 mg/L0.0001 NA PA/VA9/19/2014 10:15 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 8:28 PM
Acetone ND 100 µg/L5.00 NA PA/VA9/25/2014 8:28 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/25/2014 8:28 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 8:28 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/25/2014 8:28 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/25/2014 8:28 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/25/2014 8:28 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/25/2014 8:28 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/25/2014 8:28 PM
Carbon disulfide ND 100 µg/L2.25 NA 9/25/2014 8:28 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/25/2014 8:28 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/25/2014 8:28 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/25/2014 8:28 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/25/2014 8:28 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/25/2014 8:28 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/25/2014 8:28 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/25/2014 8:28 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/25/2014 8:28 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/25/2014 8:28 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/25/2014 8:28 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/25/2014 8:28 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/25/2014 8:28 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/25/2014 8:28 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/25/2014 8:28 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/25/2014 8:28 PM
Page 17 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:05:00 PM
Project:BLACKBURN C&D
Lab ID:1409J34-08A Matrix:Groundwater
MW-29Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/25/2014 8:28 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/25/2014 8:28 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/25/2014 8:28 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/25/2014 8:28 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/25/2014 8:28 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/25/2014 8:28 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/25/2014 8:28 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/25/2014 8:28 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/25/2014 8:28 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/25/2014 8:28 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/25/2014 8:28 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/25/2014 8:28 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/25/2014 8:28 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 8:28 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/25/2014 8:28 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/25/2014 8:28 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/25/2014 8:28 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/25/2014 8:28 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 8:28 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/25/2014 8:28 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/25/2014 8:28 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/25/2014 8:28 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/25/2014 8:28 PM
Surr: 1,2-Dichloroethane-d4 110 68.7-129 %RECNANA 9/25/2014 8:28 PM
Surr: 4-Bromofluorobenzene 109 71.8-127 %RECNANA 9/25/2014 8:28 PM
Surr: Dibromofluoromethane 108 74.3-124 %RECNANA 9/25/2014 8:28 PM
Surr: Toluene-d8 99.3 71.4-129 %RECNANA 9/25/2014 8:28 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 9/30/2014 4:14 AM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/25/2014 8:28 PM
Surr: 1,2-Dichloroethane-d4 101 80-120 %RECNANA 9/25/2014 8:28 PM
Surr: 4-Bromofluorobenzene 101 80-120 %RECNANA 9/25/2014 8:28 PM
Surr: Dibromofluoromethane 97.2 80-120 %RECNANA 9/25/2014 8:28 PM
Surr: Toluene-d8 95.0 80-120 %RECNANA 9/25/2014 8:28 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 215 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 18 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:27:00 PM
Project:BLACKBURN C&D
Lab ID:1409J34-09A Matrix:Groundwater
MW-30Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:48 PM
Barium 0.386 0.100 mg/L0.0010 NA PA/VA9/24/2014 2:48 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 2:48 PM
Chromium 0.0460 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:48 PM
Lead 0.0067 0.0100 J mg/L0.0002 NA PA/VA9/24/2014 2:48 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:48 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:48 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury ND 0.0010 mg/L0.0001 NA PA/VA9/19/2014 10:17 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/26/2014 4:12 AM
Acetone ND 100 µg/L5.00 NA PA/VA9/26/2014 4:12 AM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/26/2014 4:12 AM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/26/2014 4:12 AM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/26/2014 4:12 AM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/26/2014 4:12 AM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/26/2014 4:12 AM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/26/2014 4:12 AM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/26/2014 4:12 AM
Carbon disulfide ND 100 µg/L2.25 NA 9/26/2014 4:12 AM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/26/2014 4:12 AM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/26/2014 4:12 AM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/26/2014 4:12 AM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/26/2014 4:12 AM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/26/2014 4:12 AM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/26/2014 4:12 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/26/2014 4:12 AM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/26/2014 4:12 AM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/26/2014 4:12 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/26/2014 4:12 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/26/2014 4:12 AM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/26/2014 4:12 AM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/26/2014 4:12 AM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/26/2014 4:12 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/26/2014 4:12 AM
Page 19 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:27:00 PM
Project:BLACKBURN C&D
Lab ID:1409J34-09A Matrix:Groundwater
MW-30Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/26/2014 4:12 AM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/26/2014 4:12 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/26/2014 4:12 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/26/2014 4:12 AM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/26/2014 4:12 AM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/26/2014 4:12 AM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/26/2014 4:12 AM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/26/2014 4:12 AM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/26/2014 4:12 AM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/26/2014 4:12 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/26/2014 4:12 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/26/2014 4:12 AM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/26/2014 4:12 AM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/26/2014 4:12 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/26/2014 4:12 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/26/2014 4:12 AM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/26/2014 4:12 AM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/26/2014 4:12 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/26/2014 4:12 AM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/26/2014 4:12 AM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/26/2014 4:12 AM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/26/2014 4:12 AM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/26/2014 4:12 AM
Surr: 1,2-Dichloroethane-d4 115 68.7-129 %RECNANA 9/26/2014 4:12 AM
Surr: 4-Bromofluorobenzene 104 71.8-127 %RECNANA 9/26/2014 4:12 AM
Surr: Dibromofluoromethane 107 74.3-124 %RECNANA 9/26/2014 4:12 AM
Surr: Toluene-d8 97.4 71.4-129 %RECNANA 9/26/2014 4:12 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 9/30/2014 4:47 AM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/26/2014 4:12 AM
Surr: 1,2-Dichloroethane-d4 103 80-120 %RECNANA 9/26/2014 4:12 AM
Surr: 4-Bromofluorobenzene 101 80-120 %RECNANA 9/26/2014 4:12 AM
Surr: Dibromofluoromethane 97.5 80-120 %RECNANA 9/26/2014 4:12 AM
Surr: Toluene-d8 93.4 80-120 %RECNANA 9/26/2014 4:12 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 349 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 20 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:35:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-10A Matrix:Groundwater
MW- 2 DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:53 PM
Barium 0.155 0.100 mg/L0.0010 NA PA/VA9/24/2014 2:53 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA9/24/2014 2:53 PM
Chromium 0.0016 0.0100 J mg/L0.0010 NA PA/VA9/24/2014 2:53 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA9/24/2014 2:53 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:53 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA9/24/2014 2:53 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: BG
Mercury ND 0.0010 mg/L0.0001 NA PA/VA9/19/2014 10:20 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/25/2014 9:01 PM
Acetone ND 100 µg/L5.00 NA PA/VA9/25/2014 9:01 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/25/2014 9:01 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 9:01 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/25/2014 9:01 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/25/2014 9:01 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/25/2014 9:01 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/25/2014 9:01 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/25/2014 9:01 PM
Carbon disulfide ND 100 µg/L2.25 NA 9/25/2014 9:01 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/25/2014 9:01 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/25/2014 9:01 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/25/2014 9:01 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/25/2014 9:01 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/25/2014 9:01 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/25/2014 9:01 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/25/2014 9:01 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/25/2014 9:01 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/25/2014 9:01 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/25/2014 9:01 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/25/2014 9:01 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/25/2014 9:01 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/25/2014 9:01 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/25/2014 9:01 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/25/2014 9:01 PM
Page 21 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 8:35:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-10A Matrix:Groundwater
MW- 2 DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/25/2014 9:01 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/25/2014 9:01 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/25/2014 9:01 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/25/2014 9:01 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/25/2014 9:01 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/25/2014 9:01 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/25/2014 9:01 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/25/2014 9:01 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/25/2014 9:01 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/25/2014 9:01 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/25/2014 9:01 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/25/2014 9:01 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/25/2014 9:01 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/25/2014 9:01 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/25/2014 9:01 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/25/2014 9:01 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/25/2014 9:01 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/25/2014 9:01 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/25/2014 9:01 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/25/2014 9:01 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/25/2014 9:01 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/25/2014 9:01 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/25/2014 9:01 PM
Surr: 1,2-Dichloroethane-d4 113 68.7-129 %RECNANA 9/25/2014 9:01 PM
Surr: 4-Bromofluorobenzene 104 71.8-127 %RECNANA 9/25/2014 9:01 PM
Surr: Dibromofluoromethane 108 74.3-124 %RECNANA 9/25/2014 9:01 PM
Surr: Toluene-d8 99.0 71.4-129 %RECNANA 9/25/2014 9:01 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 9/30/2014 5:20 AM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/25/2014 9:01 PM
Surr: 1,2-Dichloroethane-d4 101 80-120 %RECNANA 9/25/2014 9:01 PM
Surr: 4-Bromofluorobenzene 99.9 80-120 %RECNANA 9/25/2014 9:01 PM
Surr: Dibromofluoromethane 96.8 80-120 %RECNANA 9/25/2014 9:01 PM
Surr: Toluene-d8 94.8 80-120 %RECNANA 9/25/2014 9:01 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: JJ
Total Suspended Solids 96.0 10 mg/L2.0 NA PA/VA9/18/2014 8:40 AM
Page 22 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:00:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-11A Matrix:Trip Blank
TRIP BLANK # 3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 9/26/2014 4:45 AM
Acetone 10.8 100 J µg/L5.00 NA PA/VA9/26/2014 4:45 AM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA9/26/2014 4:45 AM
Benzene ND 1.00 µg/L0.250 NA PA/VA9/26/2014 4:45 AM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA9/26/2014 4:45 AM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA9/26/2014 4:45 AM
Bromoform ND 3.00 µg/L0.482 NA PA/VA9/26/2014 4:45 AM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA9/26/2014 4:45 AM
2-Butanone ND 100 µg/L4.74 NA PA/VA9/26/2014 4:45 AM
Carbon disulfide ND 100 µg/L2.25 NA 9/26/2014 4:45 AM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA9/26/2014 4:45 AM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA9/26/2014 4:45 AM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA9/26/2014 4:45 AM
Chloroform ND 5.00 µg/L0.400 NA PA/VA9/26/2014 4:45 AM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA9/26/2014 4:45 AM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA9/26/2014 4:45 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA9/26/2014 4:45 AM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA9/26/2014 4:45 AM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA9/26/2014 4:45 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA9/26/2014 4:45 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA9/26/2014 4:45 AM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA9/26/2014 4:45 AM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA9/26/2014 4:45 AM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA9/26/2014 4:45 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA9/26/2014 4:45 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA9/26/2014 4:45 AM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA9/26/2014 4:45 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA9/26/2014 4:45 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA9/26/2014 4:45 AM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA9/26/2014 4:45 AM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA9/26/2014 4:45 AM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA9/26/2014 4:45 AM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA9/26/2014 4:45 AM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA9/26/2014 4:45 AM
Styrene ND 1.00 µg/L0.346 NA PA/VA9/26/2014 4:45 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA9/26/2014 4:45 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA9/26/2014 4:45 AM
Page 23 of 24
WO#: 1409J34
Date Reported: 10/1/2014
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:9/16/2014 12:00:00 AM
Project:BLACKBURN C&D
Lab ID:1409J34-11A Matrix:Trip Blank
TRIP BLANK # 3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:9/17/2014
CATAWBA CO N.CSite ID:
NELAP
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA9/26/2014 4:45 AM
Toluene ND 1.00 µg/L0.250 NA PA/VA9/26/2014 4:45 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA9/26/2014 4:45 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA9/26/2014 4:45 AM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA9/26/2014 4:45 AM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA9/26/2014 4:45 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA9/26/2014 4:45 AM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA9/26/2014 4:45 AM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA9/26/2014 4:45 AM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA9/26/2014 4:45 AM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA9/26/2014 4:45 AM
Surr: 1,2-Dichloroethane-d4 113 68.7-129 %RECNANA 9/26/2014 4:45 AM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 9/26/2014 4:45 AM
Surr: Dibromofluoromethane 108 74.3-124 %RECNANA 9/26/2014 4:45 AM
Surr: Toluene-d8 99.9 71.4-129 %RECNANA 9/26/2014 4:45 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 9/29/2014 7:27 PM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA PA/VA9/26/2014 4:45 AM
Surr: 1,2-Dichloroethane-d4 102 80-120 %RECNANA 9/26/2014 4:45 AM
Surr: 4-Bromofluorobenzene 99.8 80-120 %RECNANA 9/26/2014 4:45 AM
Surr: Dibromofluoromethane 99.0 80-120 %RECNANA 9/26/2014 4:45 AM
Surr: Toluene-d8 95.4 80-120 %RECNANA 9/26/2014 4:45 AM
Page 24 of 24
DB
P i x
E v a l u a t i on
w w w.a mm a r a .c om
DB
P i x
E v a l u a t i on
w w w.a mm a r a .c om
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD5:
FieldSamplingSummaries
and
FieldSampleLogs
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Sunny70-83°F
Property Units MW-2 MW-21 MW-24 MW-25
SamplingDepth Feet 18.00 53.51 11.95 6.94
StaticDepth Feet 17.27 53.93 11.05 5.75
WellDepth Feet 23.99 62.63 22.78 13.94
WaterColumnHeight Feet 6.72 8.70 11.73 8.19
VolumePurged Liters 12 15 22 15
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-2 MW-21 MW-24 MW-25
pH SU 5.40Dup5.42 6.07 5.91 5.87
Temperature oC 17.4Dup17.3 17.1 19.2 20.2
Conductivity umhos/cm 215Dup199.1 47.5 614 388
Turbidity NTU 33.9Dup33.1 359 67.7 41.2
Appearance -Cloudy Cloudy Cloudy Cloudy
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 101 962 137 36
Property Units MW-26 MW-27 MW-28 MW-29
SamplingDepth Feet 4.95 12.90 4.90 12.13
StaticDepth Feet 4.30 12.62 4.90 11.22
WellDepth Feet 22.41 28.00 14.92 23.13
WaterColumnHeight Feet 18.11 15.38 10.02 11.91
VolumePurged Liters 33 27 0 21
PurgingStatus -FinishedPurgingFinishedPurging 0 FinishedPurging
PhysicalProperty Units MW-26 MW-27 MW-28 MW-29
pH SU 5.55 5.91 6.21 5.71
Temperature oC 19.8 17.6 23.3 17.5
Conductivity umhos/cm 112 566 322 125
Turbidity NTU 46.7 35.0 246 391
Appearance -Cloudy Cloudy Cloudy Cloudy
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 62 33 129 215
SAMPLINGLOGSUMMARY
BlackburnC&D Landfill(Permit:#18-03)
1409J34
9/16/2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page 1
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Sunny70-83°F
SAMPLINGLOGSUMMARY
BlackburnC&D Landfill(Permit:#18-03)
1409J34
9/16/2014
Property Units MW-30
SamplingDepth Feet 17.75
StaticDepth Feet 16.02
WellDepth Feet 22.85
WaterColumnHeight Feet 6.83
VolumePurged Liters 12
PurgingStatus -FinishedPurging
PhysicalProperty Units MW-30
pH SU 5.75
Temperature oC 17.3
Conductivity umhos/cm 138
Turbidity NTU 795
Appearance -Cloudy
Odor -No Odor
TotalSuspendedSolids(TSS)mg/L 349
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page 2
ProjectName:Project :Well #:MW-2
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 70 °F
17.27 (Ft)3.89 (Liters)
23.99 (Ft)11.67 (Liters)
6.72 (Ft)12.00 (Liters)
pH
Time (SU)
08:25 5.39
08:26 5.41
08:27 5.45
08:28 5.46
08:29 5.49
08:30 5.49
08:30
Date:Time:08:35
Method:SamplingDepth:18.00'
pH:5.40Dup5.42 (SU)Conductivity:215Dup199.1 (umhos/cm)
Temperature:17.4Dup17.3 (oC)Turbidity:33.9Dup33.1 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:9/16/2014
Appearance:NoOdor
RandyFarley /AllenMcBride / RickyTalley / J.D.Bennett
TeflonBailer
Cloudy Odor:
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
9/16/2014
Finished Purging 12
198.9 16.5 22.9 11
199.1 16.7 13.03 9
198.5 16.7 11.91 7
215.0 16.9 13.7 5
198.9 17.2 16.61 3
Conductivity(umhos/cm)(oC)(NTU)(Liters)
174.4 18.0 1.93 1
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity VolumePurged
WaterColumnHeight VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
PURGINGDATA
9/16/201408:15 WeatherConditions:
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 2ndSemi2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page 3
ProjectName:Project :Well #:MW-21
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 78 °F
53.93 (Ft)5.03 (Liters)
62.63 (Ft)15.11 (Liters)
8.70 (Ft)15.00 (Liters)
pH
Time (SU)
10:16 6.02
10:17 5.96
10:18 6.02
10:20 6.03
10:22 6.03
10:23 6.05
10:23
Date:Time:10:27
Method:SamplingDepth:53.51'
pH:6.07 (SU)Conductivity:47.5 (umhos/cm)
Temperature:17.1 (oC)Turbidity:359 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:9/16/2014
RandyFarley /AllenMcBride / RickyTalley / J.D.Bennett
TeflonBailer
Appearance:Cloudy Odor:NoOdor
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
9/16/2014
Finished Purging 15
46.7 16.8 461 15
47.1 16.9 478 12
48.0
46.8 16.9 390 9
17.2 320 6
47.4 17.6 222 3
45.3 18.0 45.3 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
EVACUATION/STABILIZATIONTESTDATA
Temperature Turbidity VolumePurgedTemperatureCorrected
WaterColumnHeight VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
PURGINGDATA
9/16/201410:10 WeatherConditions:
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
RodneyHamby 704-462-1348
WELL CONDITIONDATA
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 2ndSemi2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page 4
ProjectName:Project :Well #:MW-24
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 81 °F
11.05 (Ft)6.79 (Liters)
22.78 (Ft)20.37 (Liters)
11.73 (Ft)22.00 (Liters)
pH
Time (SU)
10:48 5.40
10:50 5.59
10:52 5.85
10:54 5.85
10:56 5.90
10:57
Date:Time:10:59
Method:SamplingDepth:11.95'
pH:5.91 (SU)Conductivity:614 (umhos/cm)
Temperature:19.2 (oC)Turbidity:67.7 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:9/16/2014
RandyFarley /AllenMcBride / RickyTalley / J.D.Bennett
TeflonBailer
Appearance:Cloudy Odor:NoOdor
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
9/16/2014
22Finished Purging
118 20720.0 18.7
714.0 18.9 64.2 15
663.0 18.9 39.5 10
32.5 5323.0 19.9
89.2 21.2 4.4 1
(oC)Conductivity(umhos/cm)(NTU)(Liters)
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity VolumePurged
WellDepth 3Volumes
WaterColumnHeight VolumePurged
PURGINGDATA
9/16/201410:43 WeatherConditions:
StaticDepth(DepthtoWater)Volume
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 2ndSemi2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page 5
ProjectName:Project :Well #:MW-25
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 83 °F
5.75 (Ft)4.74 (Liters)
13.94 (Ft)14.22 (Liters)
8.19 (Ft)15.00 (Liters)
pH
Time (SU)
11:13 5.53
11:14 5.82
11:15 5.77
11:16 5.78
11:17 5.77
11:18 5.83
11:18
Date:Time:11:20
Method:SamplingDepth:6.94'
pH:5.87 (SU)Conductivity:388 (umhos/cm)
Temperature:20.2 (oC)Turbidity:41.2 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:9/16/2014
Cloudy
RandyFarley /AllenMcBride / RickyTalley / J.D.Bennett
TeflonBailer
NoOdorOdor:Appearance:
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
9/16/2014
15Finished Purging
320.0 20.0 86.1 15
256.0 19.9 48 12
9240.0 20.3 46.9
257.0 20.7 36 6
312.0 21.8 160 3
1150.2 23.2 80.9
Conductivity(umhos/cm)(oC)(NTU)(Liters)
EVACUATION/STABILIZATIONTESTDATA
Temperature Turbidity VolumePurgedTemperatureCorrected
WaterColumnHeight VolumePurged
WellDepth 3Volumes
9/16/201411:09 WeatherConditions:
StaticDepth(DepthtoWater)Volume
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 2ndSemi2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page 6
ProjectName:Project :Well #:MW-26
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 74 °F
4.30 (Ft)10.48 (Liters)
22.41 (Ft)31.45 (Liters)
18.11 (Ft)33.00 (Liters)
pH
Time (SU)
09:37 5.65
09:39 5.60
09:41 5.58
09:42 5.56
09:44 5.57
09:46 5.60
09:47
Date:Time:09:50
Method:SamplingDepth:4.95'
pH:5.55 (SU)Conductivity:111.7 (umhos/cm)
Temperature:19.8 (oC)Turbidity:46.7 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:9/16/2014
RandyFarley /AllenMcBride / RickyTalley / J.D.Bennett
Odor:Appearance:Cloudy
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
NoOdor
9/16/2014
SAMPLINGDATA
Finished Purging 33
105.6 17.6 >800 30
24103.8 18.2 >800
105.2 17.8 18563
18.8 469 12104.9
6107.7 19.8 386
108.9 21.3 9.75 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
VolumePurged
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity
WaterColumnHeight VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
9/16/201409:31 WeatherConditions:
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
704-462-1348
WELL CONDITIONDATA
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
RodneyHamby
BlackburnC&D 2ndSemi2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page 7
ProjectName:Project :Well #:MW-27
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 74 °F
12.62 (Ft)8.90 (Liters)
28.00 (Ft)26.71 (Liters)
15.38 (Ft)27.00 (Liters)
pH
Time (SU)
09:05 5.90
09:07 6.04
09:09 6.00
09:10 5.91
09:11 5.96
09:12 5.97
09:13
Date:Time:09:17
Method:SamplingDepth:12.90'
pH:5.91 (SU)Conductivity:566 (umhos/cm)
Temperature:17.6 (oC)Turbidity:35 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:9/16/2014
Appearance:Cloudy
RandyFarley /AllenMcBride / RickyTalley / J.D.Bennett
Odor:NoOdor
TeflonBailer
9/16/2014
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
Finished Purging 27
17.3 43.1 25676.0
62.4 20832.0 17.3
15724.0 17.3 17.16
1017.7 39.51,048.0
32.3 51,055.0 18.1
688.0 19.2 8.08 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
TemperatureCorrected Temperature
EVACUATION/STABILIZATIONTESTDATA
Turbidity VolumePurged
WaterColumnHeight VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
9/16/201408:57 WeatherConditions:
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
RodneyHamby
WELL CONDITIONDATA
704-462-1348
2ndSemi2014BlackburnC&D
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page 8
ProjectName:Project :Well #:MW-28
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 80 °F
4.90 (Ft)5.80 (Liters)
14.92 (Ft)17.40 (Liters)
10.02 (Ft)0.00 (Liters)
pH
Time (SU)
Date:Time:11:39
Method:SamplingDepth:4.90'
pH:6.21 (SU)Conductivity:322 (umhos/cm)
Temperature:23.3 (oC)Turbidity:246 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:9/16/2014
RandyFarley /AllenMcBride / RickyTalley / J.D.Bennett
SampledOnly-DidNot Purge
Appearance:Cloudy Odor:NoOdor
9/16/2014
DisposableBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
TemperatureCorrected
(NTU)(Liters)(oC)Conductivity(umhos/cm)
EVACUATION/STABILIZATIONTESTDATA
Temperature Turbidity VolumePurged
WellDepth 3Volumes
WaterColumnHeight VolumePurged
StaticDepth(DepthtoWater)Volume
9/16/201411:32 WeatherConditions:
WellCasingBent-SampledOnly
PURGINGDATA
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 2ndSemi2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page 9
ProjectName:Project :Well #:MW-29
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 80 °F
11.22 (Ft)6.89 (Liters)
23.13 (Ft)20.68 (Liters)
11.91 (Ft)21.00 (Liters)
pH
Time (SU)
11:54 5.62
11:56 5.75
11:57 5.74
11:59 5.75
12:00 5.70
12:02 5.70
12:02
Date:Time:12:05
Method:SamplingDepth:12.13'
pH:5.71 (SU)Conductivity:124.5 (umhos/cm)
Temperature:17.5 (oC)Turbidity:391 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:9/16/2014
RandyFarley /AllenMcBride / RickyTalley / J.D.Bennett
NoOdor
TeflonBailer
Appearance:Cloudy Odor:
SAMPLINGDATA
9/16/2014
PHYSICAL CHARACTERISTICSOFSAMPLE
Finished Purging 21
123.4 2017.1 503
122.1 17.3
120.9 17.4 311 12
417 16
116.9 18.2
116.1 17.7 301 8
111.8 20.4 27 1
272 4
(oC)(NTU)(Liters)Conductivity(umhos/cm)
WaterColumnHeight VolumePurged
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
9/16/201411:50 WeatherConditions:
CaponWellRiser 2"PVCCasing
PURGINGDATA
ProtectiveCasingLocked Concrete/GroutPadPresent
PhysicalDamageProtectiveCasingPresent
WELL CONDITIONDATA
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 2ndSemi2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page10
ProjectName:Project :Well #:MW-30
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 81 °F
16.02 (Ft)3.95 (Liters)
22.85 (Ft)11.86 (Liters)
6.83 (Ft)12.00 (Liters)
pH
Time (SU)
12:18 5.96
12:19 5.80
12:20 5.75
12:22 5.70
12:23 5.71
12:23
Date:Time:12:27
Method:SamplingDepth:17.75'
pH:5.75 (SU)Conductivity:138.3 (umhos/cm)
Temperature:17.3 (oC)Turbidity:795 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:9/16/2014
RandyFarley /AllenMcBride / RickyTalley / J.D.Bennett
Appearance:Cloudy Odor:
PHYSICAL CHARACTERISTICSOFSAMPLE
NoOdor
SAMPLINGDATA
9/16/2014
TeflonBailer
12Finished Purging
1216.7 >800
735 916.8
144.1
143.7
317.3 491
6557137.1 17.1
10.31 118.3
123.6
112.7
(oC)Conductivity(umhos/cm)(Liters)(NTU)
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
VolumePurgedTemperatureCorrectedTemperatureTurbidity
3VolumesWellDepth
StaticDepth(DepthtoWater)Volume
WeatherConditions:9/16/201412:11
CaponWellRiser 2"PVCCasing
PURGINGDATA
Concrete/GroutPadPresentProtectiveCasingLocked
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
704-462-1348RodneyHamby
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 2ndSemi2014
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD5-Page11
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD6:
Historical Results
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-2
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD6-Page 1
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-21
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD6-Page 6
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-24
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD6-Page11
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-25
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD6-Page16
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-26
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD6-Page21
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C
& D
B l ac
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L a nd
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C
& D
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-27
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD6-Page24
B l ac
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& D
B l ac
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L a nd
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& D
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-28
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD6-Page27
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-29
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD6-Page30
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-30
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com AppendixD6-Page33
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
AppendixF:
AlternateSourceDemonstration
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
1
1.0 EXCEEDANCEDESCRIPTION
REIConsultantsofNorthCarolina,PLLC(REICofNC),onbehalfofCatawbaCounty,
issubmittingthisAlternateSourceDemonstration(ASD)forBlackburnResource
RecoveryFacility,PermitNo.18-03,pursuanttoNorthCarolinawastemanagement
regulations15NCAC13B.1633,duetoexceedancesofNorthCarolinagroundwater
protectionstandardsformetalsduringthe 2nd semi-annualmonitoringperiodof2014.
NorthCarolinagroundwaterprotectionstandardsincludebothgroundwaterstandardsand
interimmaximumallowableconcentrations(IMACs)givenin15ANCAC2L.0202,
effectiveApril1,2013.Thefollowingmetalsexceededgroundwaterprotection
standardsintheindicatedcompliancewells:
Parameter Well
SubtitleDUnit2
Cobalt MW-12,MW-16
Vanadium MW-16
SubtitleDUnit3
Chromium MW-31,MW-32,MW-33,MW-34
Cobalt MW-32,MW-33
Vanadium MW-31,MW-32,MW-33,MW-34
C&DUnit2
Chromium MW-29,MW-30
2.0 DATAEVALUATION
Statisticalanalysisofbackgrounddatafromupgradientwellsatthefacilityindicatesthat
alloftheaboveexceedancesarelowerthanbackgroundstatisticallimits.Statistical
analysisofgroundwaterdatawasconductedbyconstructingpredictionlimitsfrom
availableupgradientbackgrounddata.DatafromwellsMW-4andMW-10,whichhave
beenabandonedduetofacilityexpansion,andwellMW-20werepooledandutilizedfor
comparisontodatafromcompliancewellsassociatedwiththeSubtitleDUnit2andUnit
3landfills.DatafromwellMW-21wasutilizedforcomparisontodatafromcompliance
wellsassociatedwiththeC&DUnit2landfill. Thestatisticalanalysisisincludedinthis
report.Thefollowingtablessummarize,forthosecompliancewellsandparametersfor
2
whichgroundwaterprotectionstandardswereexceededduringthe 2nd semiannual2014
event,thesampleresults,reportinglimits,applicablegroundwaterprotectionstandards,
andbackgroundstatisticallimits:C&DUnit2
SubtitleDUnit 2
SWSL GPS UPL MW-12 MW-16
Cobalt 0.010 0.001 0.230 0.109 0.0214
Vanadium 0.025 0.0003 0.880 -0.0387
SubtitleDUnit 3
SWSL GPS UPL MW-31 MW-32 MW-33 MW-34
Chromium 0.010 0.01 0.860 0.0227 0.0411 0.0283 0.0322
Cobalt 0.010 0.001 0.230 -0.0144 0.0206 -
Vanadium 0.025 0.0003 0.880 0.0254 0.0940 0.153 0.0327
C&DUnit 2
SWSL GPS UPL MW-29 MW-30
Chromium 0.010 0.01 0.110 0.0287 0.0830
Notes:
Allvaluesinmg/L
SWSL–SolidWasteSectionLimit(reportinglimit)
GPS–15ANCAC2L.0202groundwaterprotectionstandard
UPL–upperpredictionlimit
“-“–notdetected aboveGPS
Notethatnoneoftheresultsexceededthestatisticalbackgroundlimits.Allofthe
parameterswhichexceededgroundwaterprotectionstandardshavebeenobservedinthe
upgradientbackgroundwellsatthefacilityathigherlevelsthanthoseexhibitedin
compliancewells.
3.0 CONCLUSIONS
ItistheprofessionalopinionofREICofNCthatthegroundwaterprotectionstandard
exceedancesofmetalsincompliancewellswerenottheresultofareleasefromthe
landfill,butratherareduetonaturalvariation.Thisconclusionisbaseduponthe
availabledatacollectedfrombackgroundandcompliancewellsatthefacility,and
applicationofstatisticalprocedurestocomparedataupgradientanddowngradientofthe
landfills.Chromium,cobalt,andvanadiumhavebeenobservedinsamplescollected
3
frombackgroundwellsatthefacility,whichindicatesthatthesemetalsarepresent
naturallyinareasofthefacilityupgradientofwasteunits.Inaddition,thestatistical
limitsderivedfromupgradientdataareconsiderablyhigherthanconcentrationsofthe
metalsobservedduringthe 2nd semiannual2014monitoringevent.Sincethemetalsin
theaffectedwellsdonotexceedbackground,thepresenceofthemetalsisattributedto
naturalvariation.
CatawbaCounty,NorthCarolina
BlackburnLandfill
PermitNumber:18-03
Units2& 3
StatisticalEvaluation
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
i xi i/(n+1)mi mi*xi mi2
1 0.005 0.017 -2.1144-0.01064.4706
2 0.005 0.034 -1.8186-0.00913.3075
3 0.005 0.052 -1.6284-0.00812.6516
4 0.005 0.069 -1.4835-0.00742.2009
5 0.005 0.086 -1.3645-0.00681.8618
6 0.0111 0.103 -1.2621-0.01401.5930
7 0.0121 0.121 -1.1715-0.01421.3725
8 0.0125 0.138 -1.0897-0.01361.1874
9 0.0134 0.155 -1.0145-0.01361.0292
10 0.0140 0.172 -0.9447-0.01320.8924
11 0.0161 0.190 -0.8792-0.01420.7729
12 0.0210 0.207 -0.8172-0.01720.6679
13 0.025 0.224 -0.7583-0.01900.5750
14 0.025 0.241 -0.7019-0.01750.4926
15 0.025 0.259 -0.6476-0.01620.4194
16 0.025 0.276 -0.5952-0.01490.3542
17 0.025 0.293 -0.5443-0.01360.2963
18 0.025 0.310 -0.4949-0.01240.2449
19 0.025 0.328 -0.4466-0.01120.1994
20 0.025 0.345 -0.3993-0.01000.1595
21 0.025 0.362 -0.3529-0.00880.1246
22 0.025 0.379 -0.3073-0.00770.0944
23 0.025 0.397 -0.2623-0.00660.0688
24 0.025 0.414 -0.2178-0.00540.0474
25 0.025 0.431 -0.1737-0.00430.0302
26 0.025 0.448 -0.1300-0.00330.0169
27 0.025 0.466 -0.0865-0.00220.0075
28 0.025 0.483 -0.0432-0.00110.0019
29 0.025 0.500 0.0000 0.0000 0.0000
30 0.025 0.517 0.0432 0.0011 0.0019
31 0.025 0.534 0.0865 0.0022 0.0075
32 0.025 0.552 0.1300 0.0033 0.0169
33 0.025 0.569 0.1737 0.0043 0.0302
34 0.0327 0.586 0.2178 0.0071 0.0474
35 0.0336 0.603 0.2623 0.0088 0.0688
36 0.0350 0.621 0.3073 0.0108 0.0944
37 0.0368 0.638 0.3529 0.0130 0.1246
38 0.053 0.655 0.3993 0.0212 0.1595
39 0.056 0.672 0.4466 0.0250 0.1994
40 0.059 0.690 0.4949 0.0292 0.2449
41 0.066 0.707 0.5443 0.0358 0.2963
42 0.078 0.724 0.5952 0.0461 0.3542
43 0.084 0.741 0.6476 0.0546 0.4194
44 0.086 0.759 0.7019 0.0604 0.4926
45 0.100 0.776 0.7583 0.0758 0.5750
46 0.109 0.793 0.8172 0.0891 0.6679
47 0.116 0.810 0.8792 0.1020 0.7729
48 0.130 0.828 0.9447 0.1228 0.8924
49 0.140 0.845 1.0145 0.1420 1.0292
50 0.200 0.862 1.0897 0.2184 1.1874
51 0.213 0.879 1.1715 0.2495 1.3725
52 0.220 0.897 1.2621 0.2777 1.5930
53 0.223 0.914 1.3645 0.3043 1.8618
54 0.252 0.931 1.4835 0.3739 2.2009
55 0.471 0.948 1.6284 0.7670 2.6516
56 0.680 0.966 1.8186 1.2367 3.3075
57 0.695 0.983 2.1144 1.4695 4.4706
sum 5.455350.2814
S.D.=0.142
W'=0.523 Þ less than0.944,normalassumptionrejected
Zinc
Shapiro-FranciaTest-NormalAssumption
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 4
Zinc
i yi i/(n+1)mi mi*yi mi2
1 -5.298 0.017 -2.114411.20274.4706
2 -5.298 0.034 -1.81869.6358 3.3075
3 -5.298 0.052 -1.62848.6276 2.6516
4 -5.298 0.069 -1.48357.8603 2.2009
5 -5.298 0.086 -1.36457.2295 1.8618
6 -4.501 0.103 -1.26215.6807 1.5930
7 -4.415 0.121 -1.17155.1718 1.3725
8 -4.382 0.138 -1.08974.7749 1.1874
9 -4.313 0.155 -1.01454.3750 1.0292
10 -4.269 0.172 -0.94474.0325 0.8924
11 -4.129 0.190 -0.87923.6300 0.7729
12 -3.863 0.207 -0.81723.1572 0.6679
13 -3.689 0.224 -0.75832.7972 0.5750
14 -3.689 0.241 -0.70192.5891 0.4926
15 -3.689 0.259 -0.64762.3889 0.4194
16 -3.689 0.276 -0.59522.1955 0.3542
17 -3.689 0.293 -0.54432.0080 0.2963
18 -3.689 0.310 -0.49491.8255 0.2449
19 -3.689 0.328 -0.44661.6474 0.1994
20 -3.689 0.345 -0.39931.4731 0.1595
21 -3.689 0.362 -0.35291.3019 0.1246
22 -3.689 0.379 -0.30731.1336 0.0944
23 -3.689 0.397 -0.26230.9675 0.0688
24 -3.689 0.414 -0.21780.8034 0.0474
25 -3.689 0.431 -0.17370.6409 0.0302
26 -3.689 0.448 -0.13000.4796 0.0169
27 -3.689 0.466 -0.08650.3192 0.0075
28 -3.689 0.483 -0.04320.1595 0.0019
29 -3.689 0.500 0.0000 0.0000 0.0000
30 -3.689 0.517 0.0432-0.15950.0019
31 -3.689 0.534 0.0865-0.31920.0075
32 -3.689 0.552 0.1300-0.47960.0169
33 -3.689 0.569 0.1737-0.64090.0302
34 -3.420 0.586 0.2178-0.74500.0474
35 -3.393 0.603 0.2623-0.89000.0688
36 -3.352 0.621 0.3073-1.03020.0944
37 -3.302 0.638 0.3529-1.16550.1246
38 -2.937 0.655 0.3993-1.17300.1595
39 -2.882 0.672 0.4466-1.28720.1994
40 -2.830 0.690 0.4949-1.40060.2449
41 -2.723 0.707 0.5443-1.48210.2963
42 -2.557 0.724 0.5952-1.52220.3542
43 -2.473 0.741 0.6476-1.60180.4194
44 -2.453 0.759 0.7019-1.72200.4926
45 -2.303 0.776 0.7583-1.74600.5750
46 -2.216 0.793 0.8172-1.81130.6679
47 -2.154 0.810 0.8792-1.89390.7729
48 -2.040 0.828 0.9447-1.92730.8924
49 -1.966 0.845 1.0145-1.99461.0292
50 -1.607 0.862 1.0897-1.75161.1874
51 -1.546 0.879 1.1715-1.81181.3725
52 -1.514 0.897 1.2621-1.91101.5930
53 -1.501 0.914 1.3645-2.04751.8618
54 -1.378 0.931 1.4835-2.04482.2009
55 -0.753 0.948 1.6284-1.22602.6516
56 -0.386 0.966 1.8186-0.70143.3075
57 -0.364 0.983 2.1144-0.76934.4706
sum 60.853350.2814
S.D.=1.189
W'=0.964 Þ greaterthan0.944,lognormalassumptionnotrejected
Shapiro-FranciaTest- LognormalAssumption
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Zinc
EPAUnifiedGuidance,Table19-1(15COCs,n=57,w=13):
10COCs:w/n 50 57 60
12 2.19 2.17 2.16
13 2.19
16 2.26 2.24 2.23
20COCs:w/n 50 57 60
12 2.35 2.33 2.32
13 2.35
16 2.44 2.43 2.42
COCs
10 2.19
15 2.27
20 2.35
mean=-3.261
s=1.189
=2.27
UPL=0.571
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CatawbaCounty,NorthCarolina
BlackburnLandfill
PermitNumber:18-03
C&D
StatisticalEvaluation
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WellNumber Date Barium Chromium Lead
MW-21 Jul-02 0.51 0.016 0.010
MW-21 Sep-02 1.19 0.050 0.021
MW-21 Mar-03 1.94 0.048 0.028
MW-21 Sep-03 1.03 0.032 0.005
MW-21 Mar-04 1.47 0.110 0.027
MW-21 Sep-04 <0.5 0.005 0.005
MW-21 Mar-05 <0.5 0.005 0.005
MW-21 Sep-05 <0.5 0.005 0.005
MW-21 Mar-06 <0.5 0.005 0.005
MW-21 Sep-06 0.260 0.005 0.005
MW-21 Mar-07 0.295 0.005 0.005
MW-21 Sep-07 0.440 0.005 0.005
MW-21 Mar-08 0.199 0.005 0.005
MW-21 Sep-08 0.119 0.0412 0.0143
MW-21 Mar-09 1.34 0.005 0.005
MW-21 Sep-09 0.492 0.005 0.005
MW-21 Mar-10 0.525 0.0157 0.005
MW-21 Sep-10 0.286 0.005 0.005
MW-21 Mar-11 0.414 0.0229 0.005
MW-21 Sep-11 0.366 0.0116 0.005
MW-21 Mar-12 0.336 0.005 0.005
MW-21 Sep-12 0.348 0.005 0.005
MW-21 Mar-13 0.215 0.005 0.005
MW-21 Sep-13 0.416 0.0102 0.005
MW-21 Mar-14 0.601 0.0477 0.005
MW-21 Sep-14 0.232 0.0182 0.005
26 26 26
4 14 21
15%54%81%
Parametric Non-parametricNon-parametric
UpperPredictionLimit 1.75 0.110 0.028
Method
HISTORICALBACKGROUNDDATA
#Observations
# Non-detects
% Non-detects
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Barium ln(Barium)Shapiro-Wilk Normality Test
0.119 -2.1286 0.6627 2.791 0.4450 1.242
0.199 -1.6145 0.3853 2.000 0.3069 0.614
0.215 -1.5371 0.2927 1.830 0.2543 0.465
0.25 -1.3863 0.1740 1.560 0.2148 0.335
0.25 -1.3863 0.0296 1.416 0.1822 0.258
0.25 -1.3863-0.5092 0.877 0.1539 0.135
0.25 -1.3863-0.6444 0.742 0.1283 0.095
0.26 -1.3471-0.6733 0.674 0.1046 0.070
0.286 -1.2518-0.7093 0.542 0.0823 0.045
0.295 -1.2208-0.8210 0.400 0.0610 0.024
0.336 -1.0906-0.8771 0.214 0.0403 0.009
0.348 -1.0556-0.8819 0.174 0.0200 0.003
0.366 -1.0051-1.0051 0.000 0.0000 0.000
0.414 -0.8819-1.0556 -0.174
0.416 -0.8771-1.0906 -0.214 b=3.296
0.44 -0.8210-1.2208 -0.400
0.492 -0.7093-1.2518 -0.542
0.51 -0.6733-1.3471 -0.674
0.525 -0.6444-1.3863 -0.742
0.601 -0.5092-1.3863 -0.877
1.03 0.0296-1.3863 -1.416
1.19 0.1740-1.3863 -1.560
1.34 0.2927-1.5371 -1.830
1.47 0.3853-1.6145 -2.000
1.94 0.6627-2.1286 -2.791
s=0.697
W=0.931greaterthan0.884,normalassumptionnotrejected
EPAUnified Guidance,Table19-1(8COCs,n=25,w=5):
COCs
5 1.90
8 2.03
10 2.11
mean=-0.855
s=0.697
=2.03
UPL=1.75
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