SW_F_0101-MSWLF-1979_05-13-2013_RM_GW

I pENR USE:ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are 'Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for Inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must Include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off-site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby, the
facility (NCAC 136.1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.x.,
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Buxton Environmental, Inc.
Contact for questions about data formatting. Include data preparers name, telephone number and E-mail address:
Name: Ross Klingman, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Alamance County - Closed Alfred Road 0104 .0500 March 28, 2013
Swepsonville Landfill Graham, NC 27253
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring Q Detection Monitoring ❑ Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data
Surface water monitoring data ❑
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Ross Klingman, P.G. President 704-344-1450
-Facilitytepresentative Name (Print) Title (Area Code) Telephone Number
-_ S& _r 3 Affix NC Licensed/ Professional Geologist Seal
Date
1101 South Blvd., Suite 101; Charlotte, NC 28203
Facility Representative Address
C-278
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
,',��11�IRIi1�fye
SEAL

FIRST SEMI-ANNUAL 2013
GROUNDWATER AND SURFACE WATER MONITORING EVENT
CLOSED SWEPSOAWILLE LANDFILL
ALAMANCE COUNTY, NORTH CAROLINA
TABLE OF CONTENTS
1.0 Introduction
2.0 Background Information
1
1
3.0 Groundwater and Surface Water Monitoring Activities 1
4.0 Groundwater and Surface Water Analytical Results 2
5.0 Conclusions
6.0 Recommendations
LIST OF FIGURES
1. Site Layout Map
LIST OF TABLES
1. Groundwater Gauging Data
2. Groundwater and Surface Water Field Parameter Data
3. Groundwater Analytical Results
4. Surface Water Analytical Results
APPENDICES
A. Laboratory Data Sheets
3
3

FIRST SEMI-ANNUAL 2013
GROUNDWATER AND SURFACE WATER MONITORING EVENT
CLOSED SWEPSONVILLE LANDFILL
ALAMANCE COUNTY, NORTH CAROLINA
1.0 INTRODUCTION
Buxton Environmental, Inc. respectfully submits the methods and results of the first semi-annual
2013 groundwater and surface water monitoring activities conducted at the closed Swepsonville
Landfill located in Alamance County, North Carolina. The purpose for conducting the
assessment was to monitor water quality at the subject site. A site layout map is provided in
Figure 1.
The monitoring activities were conducted in general accordance with the North Carolina
Department of Environment and Natural Resources, Division of Waste Management -Solid
Waste Section (NCSWS) rules, and NCDWM memorandums dated October 27, 2006, February
23, 2007 and October 16, 2007 concerning changes to laboratory detection limits and reporting
requirements, and the NCDWM groundwater and surface water sampling guidelines dated April
2008. In addition, the North Carolina Ground Water Protection Standards (NCGPS's) presented
in this report have been updated to reflect current standards.
A summary of background information, and the methods, results, conclusions and
recommendations of this investigation are outlined below.
2.0 BACKGROUND INFORMATION
The Swepsonville Landfill operated as a municipal solid waste landfill until it was closed in
1993. To comply with NCDWM rules, semi-annual groundwater and surface water monitoring
has been conducted at the site since October 1995. Water samples have been analyzed for
Appendix I volatile organic compounds (VOC's) and metals plus mercury. Historical
groundwater samples have indicated VOC's and metals above the North Carolina Groundwater
Protection Standards (NCGPS's).
3.0 GROUNDWATER AND SURFACE WATER MONITORING ACTIVITIES
On March 28, 2013, Buxton Environmental, Inc. conducted the second first semi-annual 2013
groundwater and surface water monitoring event at the subject site. Groundwater monitoring
activities were conducted at eleven monitor wells MW -1, MW -2, MW -3, MW -4, MW -5, MW -6,
MW -7A, MW -7B, MW -8A, MW -8B and MW -9. Two surface water samples SW -1 and SW -2
were collected from Haw Creek located to the east the landfill.
Prior to conducting the sampling activities, groundwater levels were obtained from each monitor
well with a depth -to -water electrode to the nearest 0.01 foot. Following the gauging activities,
each well was purged of three well bore volumes of water or until dryness with a disposable
Teflon bailer attached to new nylon rope. Field parameters including pH, conductivity and
Page 1

temperature were collected at each well following purging and at surface water sample locations.
Purge water was poured on the ground surface at respective well heads. Groundwater gauging
and field parameter data are provided in Tables 1 and 2, respectively.
The groundwater and surface water samples were analyzed for Appendix I VOC's by EPA
Method 826013, Appendix I metals by EPA Method 6020A, and mercury by EPA Method
7470A. For quality control purposes, one trip blank was analyzed for Appendix I VOC's. The
trip blank was prepared by the laboratory. The laboratory analyses were conducted by Shealy
Environmental Services, Inc. in West Columbia, South Carolina. The water samples were
collected in general accordance with accepted protocol, including chain -of -custody
documentation.
4.0 GROUNDWATER AND SURFACE WATER ANALYTICAL RESULTS
The groundwater and surface water analytical results for the second semi-annual 2012 event are
presented in Tables 2 and 3, respectively. Laboratory data sheets are presented in Appendix A.
Groundwater Analytical Results
Groundwater samples MW -1, MW -2, MW -4, MW -7A, MW -7B and MW -8B indicated target
constituents above NCGPS's, which are summarized below.
Groundwater sample MW -1 indicated the presence of 1.2 micrograms per liter (ug/1)
tetrachloroethene.
Groundwater sample MW -2 indicated the presence of 2.2 ug/1 1,2-dichloroethane, 12 ug/l 1,1-
dichloroethene, 80 ug/l cis-1,2-dichlroethene, 5.2 ug/l 1,2-dichloropropane, 28 ug/1
tetrachloroethene, 54 ug/1 trichloroethene and 6.2 ug/1 vinyl chloride.
Groundwater sample MW -4 indicated the presence of 1 ug/1 benzene, 12 ug/l 1,4 -
dichlorobenzene, 72 ug/l 1,1-dichloroethane, 1.2 ug/1 1,2-dichloroethane, 280 ug/1 cis-1,2-
dichlroethene, 1.7 ug/l 1,2-dichloropropane, 17 ug/l vinyl chloride and 86 ug/l cobalt.
Groundwater sample MW -7A indicated the presence of 2.9 ug/l benzene, 14 ug/1 1,1-
dichloroethane, 10 ug/l tetrachloroethene, 11 ug/1 trichloroethene and 2.6 ug/1 vinyl chloride.
Groundwater sample MW -7B indicated the presence of 4.1 ug/1 benzene, 19 ug/1 1,1-
dichloroethane, 9.7 ug/1 tetrachloroethene, 14 ug/1 trichloroethene and 3.4 ug/l vinyl chloride.
Groundwater sample MW -8B indicated the presence of 43 ug/l cobalt and 9 ug/l vanadium.
The remaining groundwater samples MW -3, MW -5, MW -6, MW -8A and MW -9 did not indicate
target constituents above NCGPS's.
Page 2

Surface Water Analytical Results
Surface water samples SW -1 and SW -2 did not indicated the presence of Appendix I constituents
above established North Carolina Surface Water and Wetland Standards (15A NCAC 02B) for
Haw Creek (Class WS -V water) or EPA National Criteria standards (utilized by North Carolina
Division of Water Quality as default standards for non listed parameters) (NCSWWS's).
Quality Control Analytical Results
The trip blank indicated the presence of 0.7J ug/l methylene chloride. A J -flag indicates an
estimated result (<Solid Waste Section Limit (SWSL) (a.k.a Practical Quantitation Limit (PQL))
and >=Method Detection Limit (MDL)).
S.0 CONCL USIONS
On March 28, 2013, Buxton Environmental, Inc. conducted the first semi-annual 2013
groundwater and surface water monitoring activities at the closed Swepsonville Landfill located
in Alamance County, North Carolina. A summary of the findings of this investigation is
provided below.
• Groundwater samples collected at MW -1, MW -2, MW -4, MW -7A, MW -7B and MW -813
indicated target constituents above NCGPS's.
• The surface water samples did not indicate target constituents above the NCSWWS's.
6.0 RECOMMENDATIONS
Based on the findings of this assessment, Buxton Environmental, Inc. makes the following
recommendations.
• Semi-annual groundwater and surface water monitoring should continue to be conducted at
the closed Swepsonville Landfill. The next sampling event is anticipated to be conducted in
September 2013.
• A copy of this report should be forwarded to the NCSWS for their review.
rk:reports:swepsonville.313
Page 3

FIGURES

/® MW-
/
MW -SA
MW -7B \ SW -1
/ I
ClosedMunkipal
Solid Waste Landfill ,
MW -6 I
_ 1
MW -1\
yard waste
forncer
scale house
I A
communication I U
tower
asbestos
I tire collection disposal
%MW 9
MW -5
=1andingstrip �
&MW -4 -
I
MW -2
. r
r
.I
t
I
P
Legend
11 Monitor Well Location
t
Surface Water Sample Location
MW -3 I
Scale
SW -2
U Feet 725
Source: "Monitoring Well and Surface Water Locations"
map prepared by MACTEC Engineering & Consulting, Inc.
in May 2004
IClosed Swepsonville LandfillI Buxton Environmental, Inc. I Figure 1.
Alamance County, NC Site Layout Map

TABLES

TABLE 1
GROUNDWATER GAUGING DATA
CLOSED SWEPSONVILLE LANDFILL
ALAMANCE COUNTY, NORTH CAROLINA
MARCH 28, 2013
We11ID
MW -1
TO
BTOC (ft)
33.00
TOC
Elevation (ft)
574.67
DTW
BTOC (ft)
22.76
DTW
Elevation (ft)
551.91
MW -2
29.90
510.67
27.50
483.17
MW -3
24.10
466.63
8.42
458.21
MW -4
50.00
497.57
29.81
467.76
MW -5
19.00
476.56
8.73
467.83
MW -6
50.00
529.50
22.51
506.99
MW -7A
31.05
554.12
19.36
534.76
MW -7B
64.02
553.09
22.06
531.03
MW -8A
65.00
591.08
25.22
565.86
MW -8B
26.00
591.25
24.67
566.58
MW -9
27.50
568.78
22.28
546.50
Notes:
Depth to water measurements obtained on March 28, 2013 to the nearest 0.01 foot with a depth to water meter.
TD --total depth;BTOC=below top of casing;TOCrtop of casing;DTW=depth to water;ft=feet
TD and TOC elevation data obtained from the "Report of Semi -Annual Water Quality Monitoring, Swepsonville
Landfill, Graham, Alamance Co., North Carolina" report prepared by MACTEC in April 2005
rk:tab1e:swepsonvi11egag.313

TABLE 2
GROUNDWATER AND SURFACE WATER FIELD PARAMETER DATA
CLOSED SWEPSONVILLE LANDFILL
ALAMANCE COUNTY, NORTH CAROLINA
MARCH 28, 2013
Sample ID
MW -1
pH (standard units)
6.12
Field Parameters
K (us)
120
T (fahrenheit)
60.2
MW -2
6.22
342
61.1
MW -3
6.05
114
61.3
MW -4
6.20
1,000
60.5
MW -5
6.35
200
60.4
MW -6
6.37
175
60.1
MW -7A
6.02
158
62.4
MW -7B
6.32
250
61.1
MW -8A
6.40
60
60.8
MW -8B
6.22
175
62.3
MW -9
5.90
65
60.2
SW -1
7.24
75
54.2
SW -2
7.19
70
56.5
Notes:
Field parameters collected on March 28, 2013 by Buxton Environmental, Inc. utilizing EXTECH ExStik
and ExStik H meters. Field parameters at monitor wells collected after purging 3 well volumes of water.
Leachate and surface water field parameters collected immediately prior to sampling.
K = conductivity
T = temperature
uS = microsiemens
rkAables:swepsonvillePar.313

TABLE 3
GR 0 UND WA TER ANAL YTICAL DATA
CLOSED SWEPSONVILLELANDFILL
ALAMANCE COUNTY, NORTH CAROLINA
MARCH 28, 2013
Sample ID
VOCIS
MW -1
MW -2
MW -3
MW -4
MW -5
MW -6
MW -7A
MW -7B MW -8A MW -8B
MW -9
NCGPS
Benzene
BDL
0.66J
BDL
,
BDL
BDLR
_:
BDL
BDL
BDL
1
Chlorobenzene
BDL
0.84J
BDL
1.6
BDL
BDL
BDL
0.41J
BDL
BDL
BDL
50
Chloroethane
BDL
1.6J
BDL
7.5
BDL
BDL
1.97
2.7
BDL
BDL
BDL
3,000
1,2 -Dichlorobenzene
BDL
0.52J
BDL
2
BDL
BDL
BDL
BDL
BDL
BDL
BDL
20
1,4 -Dichlorobenzene
BDL
3.7
BDL
-=4=
BDL
BDL
1.1
2.8
BDL
BDL
BDL
6
1,1-Dichloroethane
BDL
140
BDL
E
BDL
BDL
BDL
BDL
BDL
6
1,2-Dichloroethane
BDL
Y
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.4
1,1-Dichloroethene
BDL
BDL
0.35J
BDL
BDL
BDL
0.16J
BDL
BDL
BDL
7
cis-1,2-Dichloroethene
BDL
=
BDL
r,�K-%0
BDL
BDL
30
49
BDL
BDL
BDL
70
trans-1,2-Dichloroethene
BDL
2.1
BDL
BDL
BDL
BDL
BDL
0.26J
BDL
BDL
BDL
100
1,2-Dichloro ro ane
BDL
_
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.6
Methylene Chloride
BDL
1.1
BDL
1.1
BDL
BDL
1.1
1.2
BDL
BDL
BDL
5
Tetrachloroethene
12
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.7
Toluene
BDL
0.35J
BDL
0.36J
BDL
BDL
BDL
BDL
BDL
BDL
BDL
600
1,1,1 -Trichloroethane
BDL
0.37
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
200
1,1,2 -Trichloroethane
BDL
0.59J
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.6
Trichloroethene
BDL
BDL
1.2
BDL
BDL
_=
._ q
BDL
BDL
BDL
3
Vinyl Chloride
BDL
BDL
7=
BDL
BDL
R
BDL
BDL
BDL
0.03
X leases
Metals
BDL
BDL
BDL
0.42J
BDL
BDL
I BDL
BDL
BDL
BDL
BDL
500
Antimony
BDL
BDL
BDL
BDL
0.36J
BDL
BDL
BDL
BDL
BDL
BDL
1
Arsenic
BDL
0.42J
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
10
Barium
110B
170B
49B
120B
68B
69B
74B
120B
13B
98B
57B
700
Beryllium
0.39J
0.029)
BDL
BDL
BDL
0.04J
BDL
BDL
BDL
0.24J
0.069)
4
Cadmium
0.58
0.67
BDL
0.39
BDL
0.26
0.26
0.41
0.41
1.3
0.5
2
Chromium
0.6J
1.2J
0.83J
BDL
BDL
BDL
0.35J
BDL
0.61J
7.1
0.91J
10
Cobalt
0.63J
0.99J
0.13J
0.167
1.7J
2.9J
1J
BDL
1.4J
1
Copper
1
1.7
0.25J
0.69J
2.7
0.4J
0.4J
1.1
0.16J
31
1.2
11000
Lead
0.3 113J.
5.9B
0.41BJ
0.12BJ 0.071BJ
0.26BJ
BDL
0.04913J
BDL
2.2B
0.43BJ
15
Mercury
0.053) I
BDL
BDL
0.015J
BDL
0.017J
0.021)
0.023J
BDL
0.26
BDL
1
Nickel
0.41BJ
7B
0.66BJ
5AB
0.41BJ
0.42BJ
0.68BJ
0.9213J
BDL
5.7B
1.4BJ
100
Selenium
BDL
0.53J
BDL
0.687
BDL
BDL
BDL
BDL
BDL
BDL
BDL
20
Silver
0.013BJ
BDL 0.016BJ
0.021BJ,
BDL
BDL
BDL
BDL
BDL
0.031BJ
BDL
20
Thallium
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.49J
BDL
0.2
Vanadium
BDL
4.67
3.9J
BDL
BDL
1.87
1.57
2.1J
2.11
v,_
4.7J
0.3
Zinc
7.87
7.67
BDL
4.2J
28
3.47
3.27
3AJ
2.1J
17J
7.77
1,000
Notes:
Groundwater samples collected on March 28, 2013 and analyzed for Appendix 1 volatile organic compounds (VOC's) by
EPA Method 8260B, Appendix I metals by EPA 6020A and mercury by EPA Method 7470A.
Analyses by Shealy Environmental Services, Inc. in West Columbia, SC.
NCGPS=North Carolina Groundwater Protection Standard (J-tlagged data not considered)
BDL=below detection limit
Bold and'shade denotes above NCGPS
data presented in micrograms per liter (ug/1)
NT = not tested (limited water or dry well)
B = detected in method blank
J = estimated result <PQL and >=MDL

TABLE 4
SURFACE WATER ANALYTICAL DATA
CLOSED SWEPSONVILLE LANDFILL
ALAMANCE COUNTY, NORTH CAROLINA
MARCH 28, 2013
Sample ID
Volatile Organic Compounds
SW --1
SW -2
NCSWWS
cis-1,2-Dichloroethene
Metals
BDL
0.22J
330
Barium
23B
23B
1,000
Cadmium
BDL
0.1
2
Chromium
0.51J
0.56J
50
Cobalt
0.23J
0.31J
3
Copper
1
1.1
7
Lead
0.21BJ
0.22BJ
25
Mercury
BDL
BDL
0.012
Nickel
0.28BJ
0.3BJ
25
Vanadium
3J
2.2J
NS
zinc
1.8J
2.1 J
50
Notes:
Surface water samples collected on March 28, 2013 and analyzed for Appendix I volatile organic
compounds (VOC's) by EPA Method 8260B, Appendix I metals by EPA 6020A,
& mercury by EPA Method 7470A. Analyses by Shealy Environmental Services, Inc. in West Columbia, SC.
BDL=below detection limit; NA = not applicable
NCGPS=North Carolina Groundwater Protection Standard
NCSWWS = North Carolina Surface Water and Wetland Standards (15A NCAC 02B) for Haw
Creek (Class WS -V Water) or are EPA National Criteria.
Bold and shade denotes above established NCSWWS (J -flagged data not considered)
data presented in micrograms per liter (ug/1)
B = detected in method blank
J = estimated result <PQL and >=MDL
NS = no standard
NA = not applicable
rkAables:swepsonvillesw.313

APPENDIX A
LABORATORYDATA SHEETS

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Buxton Environmental
PO Box 11550
Charlotte, NC 28220
Attention: Ross Klingman
Project Name: Alamace - Swepsonville Landfill
Lot Number:OC29021
Date Completed:04/09/2013
/V.
Nisreen Saikaly ,
Project Manager
\,�O �N ACCOgO'y
�w 4
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329
Case Narrative
Buxton Environmental
Lot Number: OC29021
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Pian (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 61
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Buxton Environmental
Lot Number: OC29021
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
MW -1
Aqueous
03/28/20131645
03/29/2013
002
MW -2
Aqueous
03/28/20131745
03/29/2013
003
MW -3
Aqueous
03/28/20131800
03/29/2013
004
MW -4
Aqueous
03/28/20131830
03/29/2013
005
MW 6
Aqueous
03/2812813 18846
0312912013
006
MW -6
Aqueous
03/28/20131715
03/29/2013
007
MW -7A
Aqueous
03/28/20131600
03/29/2013
008
MW -76
Aqueous
03/28/20131630
03/29/2013
009
MW -8A
Aqueous
03/28/20131530
03/29/2013
010
MW -813
Aqueous
03/28/20131545
03/29/2013
011
MW -9
Aqueous
03/28/20131700
03/29/2013
012
SW -1
Aqueous
03/28/20131730
03/29/2013
013
SW -2
Aqueous
03/28/20131815
03/29/2013
014
TRIP BLANK
Aqueous
03/28/2013
03/29/2013
(14 samples)
Shealy Environmental Services, Inc. Page: 3 of 61
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Buxton Environmental
Lot Number: OC29021
Sample Sample ID Matrix Parameter Method Result Q Units Page
001
MW -1
Aqueous
Tetrachloroethene
8260B
1.2
ug/L
8
001
MW -1
Aqueous
Barium
6020A
110
B
ug/L
10
001
MW -1
Aqueous
Beryllium
6020A
0.39
J
ug/L
10
001
MW -1
Aqueous
Cadmium
6020A
0.58
ug/L
10
0
esus
Ghremium
60200.
080
J
ug&
1D
001
MW -1
Aqueous
Cobalt
6020A
0.63
J
ug/L
10
001
MW -1
Aqueous
Copper
6020A
1.0
ug/L
10
001
MW -1
Aqueous
Lead
6020A
0.31
BJ
ug/L
10
001
MW -1
Aqueous
Nickel
6020A
0.41
BJ
ug/L
10
001
MW -1
Aqueous
Silver
6020A
0.013
BJ
ug/L
10
001
MW -1
Aqueous
Zinc
6020A
7.8
J
ug/L
10
001
MW -1
Aqueous
Mercury
7470A
0.000053
J
mg/L
11
002
MW -2
Aqueous
Benzene
8260B
0.66
J
ug/L
12
002
MW -2
Aqueous
Chlorobenzene
8260B
0.84
J
ug/L
12
002
MW -2
Aqueous
Chloroethane
82608
1.6
J
ug/L
12
002
MW -2
Aqueous
1,2 -Dichlorobenzene
82608
0.52
J
ug/L
12
002
MW -2
Aqueous
1,4 -Dichlorobenzene
8260B
3.7
ug/L
12
002
MW -2
Aqueous
1,1-Dichloroethane
82608
140
ug/L
12
002
MW -2
Aqueous
1,2-Dichloroethane
8260B
2.2
ug/L
12
002
MW -2
Aqueous
1,1-Dichloroethene
8260B
12
ug/L
12
002
MW -2
Aqueous
cis-1,2-Dichloroethene
8260B
80
ug/L
12
002
MW -2
Aqueous
trans-1,2-Dichloroethene
8260B
2.1
ug/L
12
002
MW -2
Aqueous
1,2-Dichloropropane
8260B
5.2
ug/L
12
002
MW -2
Aqueous
Methylene chloride
8260B
1.1
ug/L
12
002
MW -2
Aqueous
Tetrachloroethene
8260B
28
ug/L
12
002
MW -2
Aqueous
Toluene
8260B
0.35
J
ug/L
12
002
MW -2
Aqueous
1,1,1 -Trichloroethane
8260B
0.30
J
ug/L
12
002
MW -2
Aqueous
1,1,2 Trichloroethane
8260B
0.59
J
ug/L
12
002
MW -2
Aqueous
Trichloroethene
8260B
54
ug/L
12
002
MW -2
Aqueous
Vinyl chloride
8260B
6.2
ug/L
13
002
MW -2
Aqueous
Arsenic
6020A
0.42
J
ug/L
14
002
MW -2
Aqueous
Barium
6020A
170
B
ug/L
14
002
MW -2
Aqueous
Beryllium
6020A
0.029
J
ug/L
14
002
MW -2
Aqueous
Cadmium
6020A
0.67
ug/L
14
002
MW -2
Aqueous
Chromium
6020A
1.2
J
ug/L
14
002
MW -2
Aqueous
Cobalt
6020A
0.99
J
ug/L
14
002
MW -2
Aqueous
Copper
6020A
1.7
ug/L
14
002
MW -2
Aqueous
Lead
6020A
5.9
B
ug/L
14
002
MW -2
Aqueous
Nickel
6020A
7.0
B
ug/L
14
002
MW -2
Aqueous
Selenium
6020A
0.53
J
ug/L
14
002
MW -2
Aqueous
Vanadium
6020A
4.6
J
ug/L
14
002
MW -2
Aqueous
Zinc
6020A
7.6
J
ug/L
14
003
MW -3
Aqueous
Barium
6020A
49
B
ug/L
18
003
MW -3
Aqueous
Chromium
6020A
0.83
J
ug/L
18
003
MW -3
Aqueous
Cobalt
6020A
0.13
J
ug/L
18
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Executive Summary (Continued)
Lot Number: OC29021
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
003
MW -3
Aqueous
Copper
6020A
0.25
J
ug/L
18
003
MW -3
Aqueous
Lead
6020A
0.41
BJ
ug/L
18
003
MW -3
Aqueous
Nickel
6020A
0.66
BJ
ug/L
18
003
MW -3
Aqueous
Silver
6020A
0.016
BJ
ug/L
18
003
MW -3
Aqueous
Vanadium
6020A
3.9
J
ug/L
18
004
MW -4
Aqueous
Benzene
8260B
1.0
ug/L
20
004
MW -4
Aqueous
Chlorobenzene
8260B
1.6
ug/L
20
004
MW -4
Aqueous
Chloroethane
8260B
7.5
ug/L
20
004
MW -4
Aqueous
1,2 -Dichlorobenzene
8260B
2.0
ug/L
20
004
MW -4
Aqueous
1,4 -Dichlorobenzene
8260B
12
ug/L
20
004
MW -4
Aqueous
1,1-Dichloroethane
8260B
72
ug/L
20
004
MW -4
Aqueous
1,2-Dichloroethane
8260B
1.2
ug/L
20
004
MW -4
Aqueous
1,1-Dichloroethene
8260B
0.35
J
ug/L
20
004
MW -4
Aqueous
cis-1,2-Dichloroethene
8260B
280
ug/L
20
004
MW -4
Aqueous
1,2-Dichloropropane
8260B
1.7
ug/L
20
004
MW -4
Aqueous
Methylene chloride
8260B
1.1
ug/L
20
004
MW -4
Aqueous
Toluene
8260B
0.36
J
ug/L
20
004
MW -4
Aqueous
Trichloroethene
8260B
1.2
ug/L
20
004
MW -4
Aqueous
Vinyl chloride
8260B
17
ug/L
21
004
MW -4
Aqueous
Xylenes (total)
8260B
0.42
J
ug/L
21
004
MW -4
Aqueous
Barium
6020A
120
B
ug/L
22
004
MW -4
Aqueous
Cadmium
6020A
0.39
ug/L
22
004
MW -4
Aqueous
Cobalt
6020A
86
ug/L
22
004
MW -4
Aqueous
Copper
6020A
0.69
J
ug/L
22
004
MW -4
Aqueous
Lead
6020A
0.12
BJ
ug/L
22
004
MW -4
Aqueous
Nickel
6020A
5.4
B
ug/L
22
004
MW -4
Aqueous
Selenium
6020A
0.68
J
ug/L
22
004
MW -4
Aqueous
Silver
6020A
0.021
BJ
ug/L
22
004
MW -4
Aqueous
Zinc
6020A
4.2
J
ug/L
22
004
MW -4
Aqueous
Mercury
7470A
0.000015
J
mg/L
23
005
MW -5
Aqueous
Antimony
6020A
0.36
J
ug/L
26
005
MW -5
Aqueous
Barium
6020A
68
B
ug/L
26
005
MW -5
Aqueous
Cobalt
6020A
0.16
J
ug/L
26
005
MW -5
Aqueous
Copper
6020A
2.7
ug/L
26
005
MW -5
Aqueous
Lead
6020A
0.071
BJ
ug/L
26
005
MW -5
Aqueous
Nickel
6020A
0.41
BJ
ug/L
26
005
MW -5
Aqueous
Zinc
6020A
28
ug/L
26
006
MW -6
Aqueous
Barium
6020A
69
B
ug/L
30
006
MW -6
Aqueous
Beryllium
6020A
0.040
J
ug/L
30
006
MW -6
Aqueous
Cadmium
6020A
0.26
ug/L
30
006
MW -6
Aqueous
Cobalt
6020A
1.7
J
ug/L
30
006
MW -6
Aqueous
Copper
6020A
0.40
J
ug/L
30
006
MW -6
Aqueous
Lead
6020A
0.26
BJ
ug/L
30
006
MW -6
Aqueous
Nickel
6020A
0.42
BJ
ug/L
30
006
MW -6
Aqueous
Vanadium
6020A
1.8
J
ug/L
30
006
MW -6
Aqueous
Zinc
6020A
3.4
J
ug/L
30
006
MW -6
Aqueous
Mercury
7470A
0.000017
J
mg/L
31
007
MW -7A
Aqueous
Benzene
8260B
2.9
ug/L
32
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Executive Summary (Continued)
Lot Number: OC29021
Sample Sample ID Matrix Parameter Method Result 0 Units Page
007
MW -7A
Aqueous
Chloroethane
8260B
1.9
J
ug/L
32
007
MW -7A
Aqueous
1,4 -Dichlorobenzene
8260B
1.1
ug/L
32
007
MW -7A
Aqueous
1,1-Dichloroethane
8260B
14
ug/L
32
007
MW -7A
Aqueous
cis-1,2-Dichloroethene
8260B
30
ug/L
32
007
MW -7A
Aqueous
Methylene chloride
8260B
1.1
ug/L
32
007
MW -7A
Aqueous
Tetrachloroethene
8260B
10
ug/L
32
007
MW -7A
Aqueous
Trichloroethene
8260B
11
ug/L
32
007
MW -7A
Aqueous
Vinyl chloride
8260B
2.6
ug/L
33
007
MW -7A
Aqueous
Barium
6020A
74
B
ug/L
34
007
MW -7A
Aqueous
Cadmium
6020A
0.26
ug/L
34
007
MW -7A
Aqueous
Chromium
6020A
0.35
J
ug/L
34
007
MW -7A
Aqueous
Cobalt
6020A
2.9
J
ug/L
34
007
MW -7A
Aqueous
Copper
6020A
0.40
J
ug/L
34
007
MW -7A
Aqueous
Nickel
6020A
0.68
BJ
ug/L
34
007
MW -7A
Aqueous
Vanadium
6020A
1.5
J
ug/L
34
007
MW -7A
Aqueous
Zinc
6020A
3.2
J
ug/L
34
007
MW -7A
Aqueous
Mercury
7470A
0.000021
J
mg/L
35
008
MW -7B
Aqueous
Benzene
8260B
4.1
ug/L
36
008
MW -7B
Aqueous
Chlorobenzene
82608
0.41
J
ug/L
36
008
MW -7B
Aqueous
Chloroethane
8260B
2.7
ug/L
36
008
MW -713
Aqueous
1,4 -Dichlorobenzene
8260B
2.8
ug/L
36
008
MW -713
Aqueous
1,1-Dichloroethane
8260B
19
ug/L
36
008
MW -7B
Aqueous
1,1-Dichforoethene
8260B
0.16
J
ug/L
36
008
MW -713
Aqueous
cis-1,2-Dichloroethene
82608
49
ug/L
36
008
MW -7B
Aqueous
trans-1,2-Dichloroethene
8260B
0.26
J
ug/L
36
008
MW -7B
Aqueous
Methylene chloride
8260B
1.2
ug/L
36
008
MW -7B
Aqueous
Tetrachloroethene
82608
9.7
ug/L
36
008
MW -7B
Aqueous
Trichloroethene
8260B
14
ug/L
36
008
MW -7B
Aqueous
Vinyl chloride
8260B
3.4
ug/L
37
008
MW -7B
Aqueous
Barium
6020A
120
B
ug/L
38
008
MW -76
Aqueous
Cadmium
6020A
0.41
ug/L
38
008
MW -7B
Aqueous
Cobalt
6020A
1.0
J
ug/L
38
008
MW -7B
Aqueous
Copper
6020A
1.1
ug/L
38
008
MW -713
Aqueous
Lead
6020A
0.049
BJ
ug/L
38
008
MW -713
Aqueous
Nickel
6020A
0.92
BJ
ug/L
38
008
MW -7B
Aqueous
Vanadium
6020A
2.1
J
ug/L
38
008
MW -76
Aqueous
Zinc
6020A
3.4
J
ug/L
38
008
MW -7B
Aqueous
Mercury
7470A
0.000023
J
mg/L
39
009
MW -8A
Aqueous
Barium
6020A
13
B
ug/L
42
009
MW -8A
Aqueous
Cadmium
6020A
0.41
ug/L
42
009
MW -8A
Aqueous
Chromium
6020A
0.61
J
ug/L
42
009
MW -8A
Aqueous
Copper
6020A
0.16
J
ug/L
42
009
MW -8A
Aqueous
Vanadium
6020A
2.1
J
ug/L
42
009
MW -8A
Aqueous
Zinc
6020A
2.1
J
ug/L
42
010
MW -86
Aqueous
Barium
6020A
98
B
ug/L
46
010
MW -813
Aqueous
Beryllium
6020A
0.24
J
ug/L
46
010
MW -813
Aqueous
Cadmium
6020A
1.3
ug/L
46
010
MW -8B
Aqueous
Chromium
6020A
7.1
ug/L
46
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Executive Summary (Continued)
Lot Number: OC29021
Sample Sample ID Matrix Parameter Method Result Q Units Page
010
MW -86
Aqueous
Cobalt
6020A
43
ug/L
46
010
MW -86
Aqueous
Copper
6020A
31
ug/L
46
010
MW -86
Aqueous
Lead
6020A
2.2
B
ug/L
46
010
MW -813
Aqueous
Nickel
6020A
5.7
B
ug/L
46
010
MW -8B
Aqueous
Silver
6020A
0.031
BJ
ug/L
46
010
MW -813
Aqueous
Thallium
6020A
0.49
J
ug/L
46
010
MW -8B
Aqueous
Vanadium
6020A
9.0
ug/L
46
010
MW -813
Aqueous
Zinc
6020A
17
J
ug/L
411-
010
MW -813
Aqueous
Mercury
7470A
0.00026
mg/L
47
011
MW -9
Aqueous
Barium
6020A
57
B
ug/L
50
011
MW -9
Aqueous
Beryllium
6020A
0.069
J
ug/L
50
011
MW -9
Aqueous
Cadmium
6020A
0.50
ug/L
50
011
MW -9
Aqueous
Chromium
6020A
0.91
J
ug/L
50
011
MW -9
Aqueous
Cobalt
6020A
1.4
J
ug/L
50
011
MW -9
Aqueous
Copper
6020A
1.2
ug/L
50
011
MW -9
Aqueous
Lead
6020A
0.43
BJ
ug/L
50
011
MW -9
Aqueous
Nickel
6020A
1.4
BJ
ug/L
50
011
MW -9
Aqueous
Vanadium
6020A
4.7
J
ug/L
50
011
MW -9
Aqueous
Zinc
6020A
7.7
J
ug/L
50
012
SW -1
Aqueous
Barium
6020A
23
B
ug/L
54
012
SW -1
Aqueous
Chromium
6020A
0.51
J
ug/L
54
012
SW -1
Aqueous
Cobalt
6020A
0.23
J
ug/L
54
012
SW -1
Aqueous
Copper
6020A
1.0
ug/L
54
012
SWA
Aqueous
Lead
6020A
0.21
BJ
ug/L
54
012
SW -1
Aqueous
Nickel
6020A
0.28
BJ
ug/L
54
012
SW -1
Aqueous
Vanadium
6020A
3.0
J
ug/L
54
012
SW -1
Aqueous
Zinc
6020A
1.8
J
ug/L
54
013
SW -2
Aqueous
cis-1,2-Dichloroethene
8260B
0.22
J
ug/L
56
013
SW -2
Aqueous
Barium
6020A
23
B
ug/L
58
013
SW -2
Aqueous
Cadmium
6020A
0.10
ug/L
58
013
SW -2
Aqueous
Chromium
6020A
0.56
J
ug/L
58
013
SW -2
Aqueous
Cobalt
6020A
0.31
J
ug/L
58
013
SW -2
Aqueous
Copper
6020A
1.1
ug/L
58
013
SW -2
Aqueous
Lead
6020A
0.22
BJ
ug/L
58
013
SW -2
Aqueous
Nickel
6020A
0.30
BJ
ug/L
58
013
SW -2
Aqueous
Vanadium
6020A
2.2
J
ug/L
58
013
SW -2
Aqueous
Zinc
6020A
2.1
J
ug/L
58
014
TRIP BLANK
Aqueous
Methylene chloride
82608
0.70
J
ug/L
60
(179 detections)
Shealy Environmental Services, Inc. Page: 7 of 61
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Volatile Organic Compounds by GC/MS
Client:Buxton Environmental Laboratory ID: OC29021-001
Description: MW -1 Matrix: Aqueous
Date Sampled:03/28/20131645
Date Received: 0312912013
Run Prep Method Analytical Method
Dilution Analysis Date
Analyst
Prep Date
Batch
1 5030B 8260B
1 04/05/2013 0122
JAC
17789
CAS Analytical
Parameter
Number Method
Result Q
PQL
MDL
Units
Run
Acetone
67-04-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
ND
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
82608
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
ND
2.0
0.47
ug/L
1
Chloroform
67-66-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
82608
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
82608
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
82608
ND
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
ND
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
ND
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
82608
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
82608
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
82608
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
82608
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
ND
1.0
0.33
ug/L
1
Styrene
100-42-5
82608
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
1.2
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
82608
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
82608
ND
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
82608
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
82608
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out
of holding time
Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and - MDL P = The RPD between two GC columns exceeds 40%
N =Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight
basis unless flagged with a "W'
S = MS/MSD failure
Shealy Environmental Services, Inc.
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Level 1 Report v2.1

Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-001
Description: MW -1 Matrix: Aqueous
Date Sampled:03/28/2013 1645
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/2013 0122 JAC 17789
PQL = Practical quantitation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC Columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 9 of 61
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CAS
Analytical
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
72
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4
8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4
8260B
ND
1.0
0.054
ug/L
1
Xylenes (total)
1330-20-7
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC Columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
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Run 1
Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
72
70-130
Bromofluorobenzene
83
70-130
Toluene -d8
81
70-130
PQL = Practical quantitation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC Columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 9 of 61
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ICP -MS
Client: Buxton Environmental Laboratory ID: OC29021-001
Description: MW -1 Matrix: Aqueous
Date Sampled:03/28/20131645
Date Received: 03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 03/30/2013 0220 BNW 03/29/2013 1424 17318
2 3005A 6020A 1 04/02/20131115 CDF 03/29/20131424 17318
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result <'PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria L = LCSILCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MSIMSD failure
Shealy Environmental Services, Inc. Page: 10 of 61
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CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Antimony
7440-36-0
6020A
ND
1.0
0.097
ug/L
1
Arsenic
7440-38-2
6020A
ND
1.0
0.26
ug/L
1
Barium
7440-39-3
6020A
110
B
5.0
0.045
ug/L
1
Beryllium
7440-01-7
6020A
0.39
J
0.40
0.028
ug/L
1
Cadmium
7440-43-9
6020A
0.58
0.10
0.059
ug/L
2
Chromium
7440-07-3
6020A
0.60
J
5.0
0.35
ug/L
1
Cobalt
7440-08-4
6020A
0.63
J
5.0
0.029
ug/L
1
Copper
7440-50-8
6020A
1.0
1.0
0.15
ug/L
1
Lead
7439-92-1
6020A
0.31
BJ
1.0
0.047
ug/L
1
Nickel
7440-02-0
6020A
0.41
BJ
5.0
0.28
ug/L
1
Selenium
7782-49-2
6020A
ND
1.0
0.25
ug/L
1
Silver
7440-22-4
6020A
0.013
BJ
1.0
0.011
ug/L
1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L
1
Vanadium
7440-62-2
6020A
ND
5.0
1.5
ug/L
1
Zinc
7440-06-6
6020A
7.8
J
10
1.5
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result <'PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria L = LCSILCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MSIMSD failure
Shealy Environmental Services, Inc. Page: 10 of 61
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CVAA
Client: Buxton Environmental Laboratory ID: OC29021-001
Description: MW -1 Matrix: Aqueous
Date Sampled:03/28/2013 1645
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2106 FCJ 04/02/2013 1622 17551
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A 0.000053 J 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-002
Description: MW -2 Matrix: Aqueous
Date Sampled:03/28/2013 1745
Date Received: 0312912013
Run Prep Method AnaWical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/2013 0144 JAC 17789
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless gagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 12 of 61
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CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
0.66
J
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
0.84
J
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
1.6
J
2.0
0.47
ug/L
1
Chloroform
67-66-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
82608
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
82608
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoelhane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
0.52
J
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
3.7
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
140
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
2.2
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
12
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
80
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
2.1
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
5.2
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
82608
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
82608
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
1.1
1.0
0.33
ug/L
1
Styrene
100-42-5
8260B
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
28
1.0
0.13
ug/L
1
Toluene
108-88-3
82608
0.35
J
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-66-6
8260B
0.30
J
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
0.59
J
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
54
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-694
8260B
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless gagged with a'W' S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID:OC29021-002
Description: MW -2 Matrix: Aqueous
Date Sampled:03/28/2013 1745
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/2013 0144 JAC 17789
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a'W' S = MS/MSD failure
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CAS
Analytical
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-i4
72
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4
8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-0
8260B
6.2
1.0
0.054
ug/L
1
Xylenes (total)
1330-20-7
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a'W' S = MS/MSD failure
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Run 1
Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-i4
72
70-130
Bromofluorobenzene
83
70-130
Toluene -d8
80
70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 13 of 61
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ICP -MS
Client:Buxton Environmental Laboratory ID:OC29021-002
Description: MW -2 Matrix: Aqueous
Date Sampled:03/28/2013 1745
Date Received: 03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 03/30/2013 0256 BNW 03/29/2013 1424 17318
2 3005A 6020A 1 04/02/20131152 CDF 03/29/20131424 17318
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 14 of 61
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CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Antimony
7440-36-0
6020A
ND
1.0
0.097
ug/L
1
Arsenic
7440-38-2
6020A
0.42
J
1.0
0.26
ug/L
1
Barium
7440-39-3
6020A
170
B
5.0
0.045
ug/L
1
Beryllium
7440-41-7
6020A
0.029
J
0.40
0.028
ug/L
1
Cadmium
7440-43-9
6020A
0.67
0.10
0.059
ug/L
2
Chromium
7440-47-3
6020A
1.2
J
5.0
0.35
ug/L
1
Cobalt
7440-08-4
6020A
0.99
J
5.0
0.029
ug/L
1
Copper
7440-50-8
6020A
1.7
1.0
0.15
ug/L
1
Lead
7439-92-1
6020A
5.9
B
1.0
0.047
ug/L
1
Nickel
7440-02-0
6020A
7.0
B
5.0
0.28
ug/L
1
Selenium
7782-49-2
6020A
0.53
J
1.0
0.25
ug/L
1
Silver
7440-22-4
6020A
ND
1.0
0.011
ug/L
1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L
1
Vanadium
7440-02-2
6020A
4.6
J
5.0
1.5
ug/L
1
Zinc
7440-06-0
6020A
7.6
J
10
1.5
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
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CVAA
Client: Buxton Environmental Laboratory ID:OC29021-002
Description: MW -2 Matrix: Aqueous
Date Sampled:03/28/2013 1745
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2109 FCJ 04/02/2013 1622 17551
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A ND 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure
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Volatile Organic Compounds by GUMS
Client: Buxton Environmental Laboratory ID:OC29021-003
Description: MW -3 Matrix: Aqueous
Date Sampled:03/28120131800
Date Received: 03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/2013 0207 JAC 17789
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 16 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
ND
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
ND
2.0
0.47
ug/L
1
Chloroform
67-06-3
82608
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
ND
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
ND
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-00-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethyibenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
ND
1.0
0.33
ug/L
1
Styrene
100-42-5
8260B
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
ND
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 16 of 61
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID:OC29021-003
Description: MW -3 Matrix: Aqueous
Date Sampled:03/2812013 1800
Date Received:03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 82608 1 04/05/2013 0207 JAC 17789
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
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CAS Analytical
Parameter
Number Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4 8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4 8260B
ND
1.0
0.054
ug/L
1
Xylenes (total)
1330-20-7 8260B
ND
1.0
0.33
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
73 70-130
Bromofluorobenzene
83 70-130
Toluene -d8
80 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
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ICP -MS
Client: Buxton Environmental Laboratory ID: OC29021-003
Description: MW -3 Matrix: Aqueous
Date Sampled:03/28/2013 1800
)ate Received: 0312912013
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
0.40
0.028
1 3005A
6020A 1 04/02/20131210 CDF
03/29/20131424
17318
ND
0.10
0.059
CAS Analytical
Chromium
7440-07-3
6020A
0.83
J
Parameter
Number Method
Result Q
PQL
MDL
Units
Run
Antimony
7440-36-0 6020A
ND
1.0
0.097
ug/L
1
Arsenic
7440-38-2 6020A
ND
1.0
0.26
ug/L
1
Barium
7440-39-3 6020A
49 B
5.0
0.045
ug/L
1
Beryllium
7440-41-7
6020A
ND
0.40
0.028
ug/L 1
Cadmium
7440-43-9
6020A
ND
0.10
0.059
ug/L 1
Chromium
7440-07-3
6020A
0.83
J
5.0
0.35
ug/L 1
Cobalt
7440-08-4
6020A
0.13
J
5.0
0.029
ug/L 1
Copper
7440-50-8
6020A
0.25
J
1.0
0.15
ug/L 1
Lead
7439-92-1
6020A
0.41
BJ
1.0
0.047
ug/L 1
Nickel
7440-02-0
6020A
0.66
BJ
5.0
0.28
ug/L 1
Selenium
7782-49-2
6020A
ND
1.0
0.25
ug/L 1
Silver
7440-22-4
6020A
0.016
BJ
1.0
0.011
ug/L 1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L 1
Vanadium
7440-62-2
6020A
3.9
J
5.0
1.5
ug/L 1
Zinc
7440-66-6
6020A
ND
10
1.5
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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CVAA
Client: Buxton Environmental Laboratory ID: OC29021-003
Description: MW -3 Matrix: Aqueous
Date Sampled:03/28/2013 1800
Date Received: 03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2111 FCJ 04/02/2013 1622 17551
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A ND 0.00010 0.000015 mg/L 1
PQL = Practical quantilation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding lime Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 19 of 61
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-004
Description: MW -4 Matrix: Aqueous
Date Sampled:03/28/20131830
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/2013 0235 JAC 17789
2 5030B 8260B 5 04/08/20131624 JAC 17949
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 20 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level t Reportv2.1
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
1.0
1.0
0.13
ug/L.
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
6260B
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
82608
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
1.6
1.0
0.33
ug/L
1
Chloroethane
75-00-3
82608
7.5
2.0
0.47
ug/L
1
Chloroform
67-66-3
82608
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
82608
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug%L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
2.0
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
12
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
72
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
82608
1.2
1.0
0.15
ug/L
1
1,1-Dichloroethene
7545-4
8260B
0.35 J
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
280
5.0
0.61
ug/L
2
trans-1,2-Dichloroethene
156-00-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
1.7
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
1.1
1.0
0.33
ug/L
1
Styrene
100-42-5
8260B
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
82608
ND
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
0.36 J
1.0
0.33
ug/l-
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
82608
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
82608
1.2
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-09-4
8260B
ND
1.0
0.30
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 20 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level t Reportv2.1

Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID:OC29021-004
Description: MW -4 Matrix: Aqueous
Date Sampled:03/28/2013 1830
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 50308 8260B 1 04/05/2013 0235 JAC 17789
2 5030B 82608 5 04/08/20131624 JAC 17949
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 21 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1
CAS Analytical
Parameter
Number Method
Result
Q
PQL
MDL
Units
Run
1,2,3-Trichloropropane
96-18-4 8260B
ND
1.0
0.33
ug/L
1
Vinyl acetate
108-05-4 8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4 8260B
17
1.0
0.054
ug/L
1
Xylenes (total)
1330-20-7 82608
0.42
J
1.0
0.33
ug/L
1
Run 1 Acceptance
Run 2 Acceptance
Surrogate
Q e% Recovery Limits Q % Recovery
Limits
1,2-Dichloroethane-d4
74 70-130
104
70-130
Bromofluorobenzene
84 70-130
104
70-130
Toluene -d8
80 70-130
105
70-130
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 21 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1

ICP -MS
Client: Buxton Environmental Laboratory ID: OC29021-004
Description: MW -4 Matrix: Aqueous
Date Sampled:03/28/2013 1830
)ate Received: 0312912013
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
B
1 3005A
6020A 1 03/31/2013 0859 BNW
03/29/2013 1424
17318
7440-41-7
2 3005A
6020A 1 04/02/20131237 CDF
03/29/20131424
17318
0.028
ug/L 1
CAS Analytical
7440-43-9
6020A
0.39
Parameter
Number Method
Result Q
PQL MDL
Units Run
Antimony
7440-36-0 6020A
ND
1.0 0.097
ug/L 1
Arsenic
7440-38-2 6020A
ND
1.0 0.26
ug/L 1
Barium
7440-39-3
6020A
120
B
5.0
0.045
ug/L 1
Beryllium
7440-41-7
6020A
ND
0.40
0.028
ug/L 1
Cadmium
7440-43-9
6020A
0.39
0.10
0.059
ug/L 2
Chromium
7440-47-3
6020A
ND
5.0
0.35
ug/L 1
Cobalt
7440-48-4
6020A
86
5.0
0.029
ug/L 1
Copper
7440-50-8
6020A
0.69
J
1.0
0.15
ug/L 1
Lead
7439-92-1
6020A
0.12
BJ
1.0
0.047
ug/L 1
Nickel
7440-02-0
6020A
5.4
B
5.0
0.28
ug/L 1
Selenium
7782-49-2
6020A
0.68
J
1.0
0.25
ug/L 1
Silver
7440-22-4
6020A
0.021
BJ
1.0
0.011
ug/L 1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L 1
Vanadium
7440-62-2
6020A
ND
5.0
1.5
ug/L 1
Zinc
7440-66-6
6020A
4.2
J
10
1.5
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at orabove the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W* S = MS/MSD failure
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CVAA
Client: Buxton Environmental Laboratory ID: OC29021-004
Description: MW -4 Matrix: Aqueous
Date Sampled:03/28/2013 1830
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2114 FCJ 04/02/20131622 17551
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A 0.000015 J 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 23 of 61
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Volatile Organic Compounds by GUMS
Client:Buxton Environmental Laboratory ID: OC29021-005
Description: MW -5 Matrix: Aqueous
Date Sampled:03/28/2013 1845
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131458 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 24 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
ND
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
82606
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
82608
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
82608
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
82608
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
ND
2.0
0.47
ug/L
1
Chloroform
67-66-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
82606
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
1.0
0.33
ug/L
1
1,1-Dirhloroethane
75-34-3
8260B
ND
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
82606
ND
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
ND
1.0
0.33
ug/L
1
Styrene
100-42-5
8260B
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
82606
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
ND
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 24 of 61
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-005
Description: MW -5 Matrix: Aqueous
Date Sampled:03/28/2013 1845
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131458 JAC 17854
1,2-Dichloroethane-d4 73 70-130
Bromofluorobenzene 81 70-130
Toluene -d8 79 70-130
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 25 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
MDL
Units Run
Vinyl acetate
108-05-4 8260B
ND
5.0
1.3
ug/L 1
Vinyl chloride
75-01-4 8260B
ND
1.0
0.054
ug/L 1
Xylenes (total)
1330-20-7 8260B
ND
1.0
0.33
ug/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4 73 70-130
Bromofluorobenzene 81 70-130
Toluene -d8 79 70-130
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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ICP -MS
Client:Buxton Environmental Laboratory ID:OC29021-005
Description: MW -5 Matrix: Aqueous
Date Sampled:03/28/2013 1845
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 03/31/2013 0908 BNW 03/29/2013 1424 17318
2 3005A 6020A 1 04/02/20131246 CDF 03/29/20131424 17318
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Servicesl Inc. Page: 26 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Antimony
7440-36-0
6020A
0.36
J
1.0
0.097
ug/L
1
Arsenic
7440-38-2
6020A
ND
1.0
0.26
ug/L
1
Barium
7440-39-3
6020A
68
B
5.0
0.045
ug/L
1
Beryllium
7440-41-7
6020A
ND
0.40
0.028
ug/L
1
Cadmium
7440-43-9
6020A
ND
0.10
0.059
ug/L
2
Chromium
7440117-3
6020A
ND
5.0
0.35
ug/L
1
Cobalt
7440-48-4
6020A
0.16
J
5.0
0.029
ug/L
1
Copper
7440-50-8
6020A
2.7
1.0
0.15
ug/L
1
Lead
7439-92-1
6020A
0.071
BJ
1.0
0.047
ug/L
1
Nickel
7440-02-0
6020A
0.41
BJ
5.0
0.28
ug/L
1
Selenium
7782-49-2
6020A
ND
1.0
0.25
ug/L
1
Silver
7440-22-4
6020A
ND
1.0
0.011
ug/L
1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L
1
Vanadium
7440-62-2
6020A
ND
5.0
1.5
ug/L
1
Zinc
7440-66-6
6020A
28
10
1.5
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Servicesl Inc. Page: 26 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

CVAA
Client: Buxton Environmental Laboratory ID: OC29021-005
Description: MW -5 Matrix: Aqueous
Date Sampled:03/28/2013 1845
Date Received: 03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date, Analyst Prep Date Batch
1 7470A 1 04/02/2013 2116 FCJ 04/02/2013 1622 17551
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A ND 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 27 Of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-006
Description: MW -6 Matrix: Aqueous
Date Sampled:03/28/20131715
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131520 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 28 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level t Report v2.1
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
NO
20
6.7
ug/i-
1
Acrylonitrile
107-13-1
8260B
NO
20
1.2
ug/L
1
Benzene
71143-2
8260B
NO
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
NO
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
8260B
NO
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
NO
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
NO
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
NO
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
NO
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
NO
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
NO
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
NO
2.0
0.47
ug/L
1
Chloroform
67-06-3
8260B
NO
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
82608
NO
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
NO
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
NO
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-9314
8260B
NO
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
NO
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
NO
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
NO
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
NO
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
82606
NO
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
NO
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-3514
8260B
NO
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
NO
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
NO
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
NO
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
NO
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
NO
1.0
0.11
ug/L
1
Ethylbenzene
100-4114
8260B
NO
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
NO
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
NO
5.0
1.2
ug/L
1
4-Methyl-2-penlanone
108-10-1
8260B
NO
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
NO
1.0
0.33
ug/L
1
Styrene
100142-5
8260B
NO
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
NO
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
NO
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
NO
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
NO
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
NO
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
NO
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
NO
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
NO
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
82608
NO
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 28 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level t Report v2.1

Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-006
Description: MW -6 Matrix: Aqueous
Date Sampled:03/28/2013 1715
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131520 JAC 17854
PQL= Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H =Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 29 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level t Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4 8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4 8260B
ND
1.0
0.054
ug/L
1
Xylenes (total)
1330-20-7 8260B
ND
1.0
0.33
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
74 70-130
Bromofluorobenzene
82 70-130
Toluene -d8
80 70-130
PQL= Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H =Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 29 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level t Report v2.1

ICP -MS
Client: Buxton Environmental Laboratory ID: OC29021-006
Description: MW -0 Matrix: Aqueous
Date Sampled:03/28/2013 1715
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 03/31/2013 0917 BNW 03/29/2013 1424 17318
2 3005A 6020A 1 04/02/20131255 CDF 03/29/20131424 17318
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Noldelected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 30 of 61
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CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Antimony
7440-36-0
6020A
ND
1.0
0.097
ug/L
1
Arsenic
7440-38-2
6020A
ND
1.0
0.26
ug/L
1
Barium
7440-39-3
6020A
69
B
5.0
0.045
ug/L
1
Beryllium
744041-7
6020A
0.040
J
0.40
0.028
ug/L
1
Cadmium
7440-43-9
6020A
0.26
0.10
0.059
ug/L
2
Chromium
7440-47-3
6020A
ND
5.0
0.35
ug/L
1
Cobalt
7440-48-4
6020A
1.7
J
5.0
0.029
ug/L
1
Copper
7440-50-8
6020A
0.40
J
1.0
0.15
ug/L
1
Lead
7439-92-1
6020A
0.26
BJ
1.0
0.047
ug/L
1
Nickel
7440-02-0
6020A
0.42
BJ
5.0
0.28
ug/L
1
Selenium
7782-49-2
6020A
ND
1.0
0.25
ug/L
1
Silver
7440-22-4
6020A
ND
1.0
0.011
ug/L
1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L
1
Vanadium
7440-62-2
6020A
1.8
J
5.0
1.5
ug/L
1
Zinc
7440-66-6
6020A
3.4
J
10
1.5
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Noldelected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure
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CVAA
Client: Buxton Environmental Laboratory ID: OC29021-006
Description: MW -6 Matrix: Aqueous
Date Sampled:03/28/2013 1715
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2119 FCJ 04/02/2013 1622 17551
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A 0.000017 J 0.00010 0.000015 mg/L 1
PQL = Practical quantltatian limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-007
Description: MW -7A Matrix: Aqueous
Date Sampled:03/28/20131600
Date Received: 03129/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 50308 8260B 1 04/05/20131543 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless gagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 32 of 61
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CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-04-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
2.9
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
82608
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
82608
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
82608
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
82608
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
82608
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
82608
1.9 J
2.0
0.47
ug/L
1
Chloroform
67-66-3
82608
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
82608
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
82608
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
1.1
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
14
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
30
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
82608
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
82608
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
82608
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
82608
1.1
1.0
0.33
ug/L
1
Styrene
100-42-5
82608
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
82608
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
10
1.0
0.13
uglL
1
Toluene
108-88-3
82608
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
82608
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
82608
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
11
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
82608
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless gagged with a'W' S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client:Buxton Environmental Laboratory ID: OC29021-007
Description: MW -7A Matrix: Aqueous
Date Sampled:03/28/20131600
Date Received:03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131543 JAC 17854
1,2-Dichloroethane-d4 74 70-130
Bromofluorobenzene 82 70-130
Toluene -d8 80 70-130
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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CAS Analytical
Parameter
Number Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4 8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4 8260B
2.6
1.0
0.054
ug/L
1
Xylenes (total)
1330-20-7 8260B
ND
1.0
0.33
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4 74 70-130
Bromofluorobenzene 82 70-130
Toluene -d8 80 70-130
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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ICP -MS
Client: Buxton Environmental Laboratory ID: OC29021-007
Description: MW -7A Matrix: Aqueous
Date Sampled:03/28/20131600
)ate Received: 0312912013
Run
Prep Method
Analytical Method
Dilution
Analysis Date
Analyst
Prep Date
Batch
1
3005A
6020A
1
03/31/2013 0926
BNW
03/29/2013 1424
17318
2
3005A
6020A
1
04/02/20131304
CDF
03/29/20131424
17318
Barium
CAS
Analytical.
74
Parameter
Number
Method Result Q
PQL MDL Units Run
Antimony
7440-36-0
6020A ND
1.0 0.097 ug/L 1
Arsenic
7440-38-2
6020A ND
1.0 0.26 ug/L 1
Barium
744039-3
6020A
74
B
5.0
0.045
ug/L 1
Beryllium
7440-41-7
6020A
ND
0.40
0.028
ug/L 1
Cadmium
7440-03-9
6020A
0.26
0.10
0.059
ug/l- 2
Chromium
7440-47-3
6020A
0.35
J
5.0
0.35
ug/L 1
Cobalt
7440-48-4
6020A
2.9
J
5.0
0.029
ug/L 1
Copper
7440-50-8
6020A
0.40
J
1.0
0.15
ug/L 1
Lead
7439-92-1
6020A
ND
1.0
0.047
ug/L 1
Nickel
7440-02-0
6020A
0.68
BJ
5.0
0.28
ug/L 1
Selenium
7782-49-2
6020A
ND
1.0
0.25
ug/L 1
Silver
7440-22-4
6020A
ND
1.0
0.011
ug/L 1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L 1
Vanadium
7440-62-2
6020A
1.5
J
5.0
1.5
ug/L 1
Zinc
7440-06-6
6020A
3.2
J
10
1.5
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
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CVAA
Client: Buxton Environmental Laboratory ID:OC29021-007
Description: MW -7A Matrix: Aqueous
Date Sampled:03/28/2013 1600
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2134 FCJ 04/02/2013 1622 17552
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A 0.000021 J 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID:OC29021-008
Description: MW -7B Matrix: Aqueous
Date Sampled:03/28/2013 1630
Date Received: 03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131605 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 36 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1
CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
82606
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
4.1
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
82608
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
0.41
J
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
2.7
2.0
0.47
ug/L
1
Chloroform
67-66-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
12448-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
2.8
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
19
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
7545-4
8260B
0.16
J
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
49
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
0.26
J
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
82608
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
1.2
1.0
0.33
ug/L
1
Styrene
100-42-5
8260B
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
12748-4
8260B
9.7
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
14
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 36 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1

Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-008
Description: MW -76 Matrix: Aqueous
Date Sampled:03128/2013 1630
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131605 JAC 17854
1,2-Dichloroethane-l4 74 70-130
Bromofluorobenzene 81 70-130
Toluene -d8 80 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 37 of 61
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CAS Analytical
Parameter
Number Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-1 8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4 8260B
3.4
1.0
0.054
ug/L
1
Xylenes (total)
1330-20-7 8260B
ND
1.0
0.33
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-l4 74 70-130
Bromofluorobenzene 81 70-130
Toluene -d8 80 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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ICP -MS
Client: Buxton Environmental Laboratory ID: OC29021-008
Description: MW -7B Matrix: Aqueous
Date Sampled:0312812013 1630
)ate Received: 0312912013
Run
Prep Method
Analytical Method
Dilution
Analysis Date
Analyst
Prep Date
Batch
1
3005A
6020A
1
03/31/2013 0935
BNW
03/29/2013 1424
17318
2
3005A
6020A
1
04/02/20131313
CDF
03/29/20131424
17318
CAS
Analytical
6020A
Parameter Number
Method Result Q
PQL MDL Units Run
Antimony 7440-36-0
6020A ND
1.0 0.097 ug/L 1
Arsenic 7440-38-2
6020A ND
1.0 0.26 ug/L 1
Barium
7440-39-3
6020A
120
B
5.0
0.045
ug/L 1
Beryllium
7440-41-7
6020A
ND
0.40
0.028
ug/L 1
Cadmium
7440-13-9
6020A
0.41
0.10
0.059
ug/L 2
Chromium
7440-47-3
6020A
ND
5.0
0.35
ug/L 1
Cobalt
7440-48-4
6020A
1.0
J
5.0
0.029
ug/L 1
Copper
7440-50-8
6020A
1.1
1.0
0.15
ug/L 1
Lead
7439-92-1
6020A
0.049
BJ
1.0
0.047
ug/L 1
Nickel
7440-02-0
6020A
0.92
BJ
5.0
0.28
ug/L 1
Selenium
7782-49-2
6020A
ND
1.0
0.25
ug/L 1
Silver
7440-22-4
6020A
ND
1.0
0.011
ug/L 1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L 1
Vanadium
7440-62-2
6020A
2.1
J
5.0
1.5
ug/L 1
Zinc
7440-66-6
6020A
3.4
J
10
1.5
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCSILCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless gagged with a'W' S = MS/MSD failure
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CVAA
Client: Buxton Environmental Laboratory ID: OC29021-008
Description: MW -7B - Matrix: Aqueous
Date Sampled:03/28/2013 1630
Date Received: 03129/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2144 FCJ 04/02/2013 1622 17552
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A 0.000023 J 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless gagged with a'W' S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client:Buxton Environmental Laboratory ID: OC29021-009
Description: MW -8A Matrix: Aqueous
Date Sampled:03/28/2013 1530
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131627 JAC 17854
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 40 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-04-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
ND
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
82608
ND
2.0
0.47
ug/L
1
Chloroform
67-66-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
ND
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
ND
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
ND
1.0
0.33
ug/L
1
Styrene
100-42-5
8260B
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
0.33
ug/L
1
1,,1,1 -Trichloroethane
71-55-6
82608
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
ND
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-009
Description: MW -8A Matrix: Aqueous
Date Sampled:03/28/20131530
Date Received:03129/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Data Batch
1 5030B 8260B 1 04/05/20131627 JAC 17854
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
No =Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 41 of 61
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CAS
Analytical
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
73
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4
8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4
8260B
ND
1.0
0.054
ug/L
1
Xvlenes (total)
1330-20-7
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
No =Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 41 of 61
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Run 1
Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
73
70-130
Bromofluorobenzene
80
70-130
Toluene -d8
79
70-130
PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
No =Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 41 of 61
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ICP -MS
Client: Buxton Environmental Laboratory ID:OC29021-009
Description: MW -8A Matrix: Aqueous
Date Sampled:03/28/2013 1530
Date Received: 0312912013
Run
Prep Method
Analytical Method
Dilution
Analysis Date
Analyst
Prep Date
Batch
1
3005A
6020A
1
03/31/2013 0944
BNW
03/29/2013 1424
17318
2
3005A
6020A
1
04/02/20131323
CDF
03/29/20131424
17318
CAS
Analytical
6020A
Parameter Number
Method Result Q
PQL MDL Units Run
Antimony 7440-36-0
6020A ND
1.0 0.097 ug/L 1
Arsenic 7440-38-2
6020A ND
1.0 0.26 ug/L 1
Barium
7440-39-3
6020A
13
B
5.0
0.045
ug/L 1
Beryllium
7440-41-7
6020A
ND
0.40
0.028
ug/L 1
Cadmium
744043-9
6020A
0.41
0.10
0.059
ug/L 2
Chromium
7440-47-3
6020A
0.61
J
5.0
0.35
ug/L 1
Cobalt
7440-48-4
6020A
ND
5.0
0.029
ug/L 1
Copper
7440-50-8
6020A
0.16
J
1.0
0.15
ug/L 1
Lead
7439-92-1
6020A
ND
1.0
0.047
ug/L 1
Nickel
7440-02-0
6020A
ND
5.0
0.28
ug/L 1
Selenium
7782149-2
6020A
ND
1.0
0.25
ug/L 1
Silver
7440-22-4
6020A
ND
1.0
0.011
ug/L 1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L 1
Vanadium
7440-02-2
6020A
2.1
J
5.0
1.5
ug/L 1
Zinc
7440-66-6
6020A
2.1
J
10
1.5
ug/L. 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
No = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure
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CVAA
Client: Buxton Environmental Laboratory ID: OC29021-009
Description: MW -8A Matrix: Aqueous
Date Sampled:03/28/2013 1530
Date Received: 03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2150 FCJ 04/02/2013 1622 17552
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A ND 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 43 of 61
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-010
Description: MW -8B Matrix: Aqueous
Date Sampled:03/28/2013 1545
Date Received: 03129/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131757 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 44 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
ND
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
82608
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
82608
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
82608
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
82608
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
82608
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
82608
ND
2.0
0.47
ug/L
1
Chloroform
67-66-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
12448-1
82608
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
82608
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
82608
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
82608
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
ND
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
82608
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
ND
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
82608
ND
1.0
0.092
ug/L
1
trans-11,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
82608
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
82608
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
82608
ND
1.0
0.33
ug/L
1
Styrene
100-42-5
82608
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
82608
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
82608
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
82608
ND
1.0
0.13
ug/L
1
Toluene
108-88-3
82608
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
82608
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
82608
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
82608
ND
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
82608
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
82608
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 44 of 61
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID:OC29021-010
Description: MW -8B Matrix: Aqueous
Date Sampled:03/28/2013 1546
Date Received:03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131757 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out,of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 45 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS
Analytical
Surrogate
Q e% Recovery
Limits
1,2-Dichloroethane-d4
74
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4
8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4
8260B
ND
1.0
0.054
ug/L
1
XvlpnPs (total►
1330-20-7
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out,of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 45 of 61
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Run 1
Acceptance
Surrogate
Q e% Recovery
Limits
1,2-Dichloroethane-d4
74
70-130
Bromofluorobenzene
80
70-130
Toluene -d8
79
70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out,of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 45 of 61
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ICP -MS
Client: Buxton Environmental Laboratory ID: OC29021-010
Description: MW -8B Matrix: Aqueous
Date Sampled:03128/20131546
Date Received: 0312912013
Run
Prep Method
Analytical Method
Dilution
Analysis Date
Analyst
Prep Date
Batch
1
3005A
6020A
1
03/31/2013 0953
BNW
03/29/2013 1424
17318
2
3005A
6020A
1
04/02/20131341
CDF
03/29/20131424
17318
3
3005A
6020A
5
04/02/20131332
CDF
03/29/20131424
17318
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and —> MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 46 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Antimony
7440-36-0
6020A
ND
1.0
0.097
ug/L
1
Arsenic
7440-38-2
6020A
ND
5.0
1.3
ug/L
3
Barium
7440-39-3
6020A
98
B
5.0
0.045
ug/L
1
Beryllium
7440-41-7
6020A
0.24
J
0.40
0.028
ug/L
1
Cadmium
7440-43-9
6020A
1.3
0.10
0.059
ug/L
2
Chromium
7440-47-3
6020A
7.1
5.0
0.35
ug/L
1
Cobalt
7440-48-4
6020A
43
5.0
0.029
ug/L
1
Copper
7440-50-8
6020A
31
1.0
0.15
ug/L
1
Lead
7439-92-1
6020A
2.2
B
1.0
0.047
ug/L
1
Nickel
7440-02-0
6020A
5.7
B
5.0
0.28
ug/L
1
Selenium
7782-49-2
6020A
ND
5.0
1.3
ug/L
3
Silver
7440-22-4
6020A
0.031
BJ
1.0
0.011
ug/L
1
Thallium
7440-28-0
6020A
0.49
J
0.50
0.076
ug/L
1
Vanadium
7440-62-2
6020A
9.0
5.0
1.5
ug/L
1
Zinc
7440-66-6
6020A
17
J
50
7.3
ug/L
3
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and —> MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 46 of 61
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CVAA
Client:Buxton Environmental Laboratory ID: OC29021-010
Description: MW -86 Matrix: Aqueous
Date Sampled:03/28/20131645
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2153 FCJ 04/02/2013 1622 17552
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A 0.00026 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 47 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021 -011
Description: MW -9 Matrix: Aqueous
Date Sampled:03/28/2013 1700
Date Received: 0312912013
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260B
1 04/05/20131650 JAC
17854
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
82608
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
ND
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
82608
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
ND
2.0
0.47
ug/L
1
Chloroform
67-66-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
ND
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
82608
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
ND
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
ND
1.0
0.33
ug/L
1
Styrene
100-42-5
8260B
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
ND
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H =
Out of holding time
Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40%
N =Recovery
is out of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight
basis unless gagged with a "W'
S = MS/MSD failure
Shealy Environmental Services, Inc.
Page: 48 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]
www.shealylab.com
Level 1 Report v2.1

Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID:OC29021-011
Description: MW -9 Matrix: Aqueous
Date Sampled:03/28/2013 1700
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 82608 1 04/05/20131650 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 49 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1
CAS
Analytical
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
74
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4
8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4
8260B
ND
1.0
0.054
ug/L
1
xulanPc (fnfall
1330-20-7
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 49 of 61
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Run 1
Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
74
70-130
Bromofluorobenzene
82
70-130
Toluene -i8
79
70-130
t
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 49 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1

ICP -MS
Client: Buxton Environmental Laboratory ID: OC29021-011
Description: MW -9 Matrix: Aqueous
Date Sampled:03/28/20131700
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 03/31/20131002 BNW 03/29/20131424 17318
2 3005A 6020A 1 04/02/20131350 CDF 03/29/20131424 17318
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 50 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Antimony
7440-36-0
6020A
ND
1.0
0.097
ug/L
1
Arsenic
7440-38-2
6020A
ND
1.0
0.26
ug/L
1
Barium
7440-39-3
6020A
57
B
5.0
0.045
ug/L
1
Beryllium
7440-41-7
6020A
0.069
J
0.40
0.028
ug/L
1
Cadmium
7440-43-9
6020A
0.50
0.10
0.059
ug/L
2
Chromium
7440-47-3
6020A
0.91
J
5.0
0.35
ug/L
1
Cobalt
7440-48-4
6020A
1.4
J
5.0
0.029
ug/L
1
Copper
7440-50-8
6020A
1.2
1.0
0.15
ug/l-
1
Lead
7439-92-1
6020A
0.43
BJ
1.0
0.047
ug/L
1
Nickel
7440-02-0
6020A
1.4
BJ
5.0
0.28
ug/L
1
Selenium
7782-49-2
6020A
ND
1.0
0.25
ug/L
1
Silver
7440-22-4
6020A
ND
1.0
0.011
ug/L
1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L
1
Vanadium
7440-62-2
6020A
4.7
J
5.0
1.5
ug/L
1
Zinc
7440-06-6
6020A
7.7
J
10
1.5
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 50 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Client: Buxton Environmental Laboratory ID: OC29021-011
Description: MW -9 Matrix: Aqueous
Date Sampled:03/28/2013 1700
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2156 FCJ 04/02/2013 1622 17552
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A ND 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 51 of 61
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-012
Description: SW -1 Matrix: Aqueous
Date Sampled:03/28/2013 1730
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131712 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at orabove the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 52 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 7 Report v2.1
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-04-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
82608
ND
20
1.2
ug/L
1
Benzene
71-43-2
82608
ND
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
82608
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
82608
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
82608
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
82608
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
ND
2.0
0.47
ug/L
1
Chloroform
67-66-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
82608
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
82608
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
ND
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
ND
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
ND
1.0
0.33
ug/L
1
Styrene
100-42-5
82608
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
82608
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
1.0
0.13
ug/L
1
Toluene
108-88-3
82608
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
82608
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
82608
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
82608
ND
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
82608
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at orabove the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021412
Description: SW -1 Matrix: Aqueous
Date Sampled:03/28/2013 1730
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131712 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 53 of 61
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CAS
Analytical
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
Parameter
Number
Method
Result Q
PQL
MDL
Units Run
Vinyl acetate
108-05-4
8260B
ND
5.0
1.3
ug/L 1
Vinyl chloride
75-01-4
82608
ND
1.0
0.054
ug/L 1
Xylenes (total)
1330-20-7
8260B
ND
1.0
0.33
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure
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Run 1
Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
75
70-130
Bromofluorobenzene
81
70-130
Toluene -d8
79
70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 53 of 61
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ICP -MS
Client: Buxton Environmental Laboratory ID:OC29021-012
Description: SW -1 Matrix: Aqueous
Date Sampled:03/28/20131730
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 03/31/20131011 BNW 03/29/20131424 17318
2 3005A 6020A 1 04/02/20131359 CDF 03/29/20131424 17318
PQL= Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis an: reported on a dry weight basis unless gagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 54 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheelylab.com Level 1 Report v2.1
CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Antimony
7440-36-0
6020A
ND
1.0
0.097
ug/L
1
Arsenic
7440-38-2
6020A
ND
1.0
0.26
ug/L
1
Barium
7440-39-3
6020A
23
B
5.0
0.045
ug/L
1
Beryllium
7440-41-7
6020A
ND
0.40
0.028
ug/L
1
Cadmium
7440-43-9
6020A
ND
0.10
0.059
ug/L
2
Chromium
7440-47-3
6020A
0.51
J
5.0
0.35
ug/L
1
Cobalt
7440-48-4
6020A
0.23
J
5.0
0.029
ug/L
1
Copper
7440-50-8
6020A
1.0
1.0
0.15
ug/L
1
Lead
7439-92-1
6020A
0.21
BJ
1.0
0.047
ug/L
1
Nickel
7440-02-0
6020A
0.28
BJ
5.0
0.28
ug/L
1
Selenium
7782-49-2
6020A
ND
1.0
0.25
ug/L
1
Silver
7440-22-4
6020A
ND
1.0
0.011
ug/L
1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L
1
Vanadium
7440-62-2
6020A
3.0
J
5.0
1.5
ug/L
1
Zinc
7440-66-6
6020A
1.8
J
10
1.5
ug/L
1
PQL= Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L= LCS/LCSD failure
Where applicable, all soil sample analysis an: reported on a dry weight basis unless gagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 54 of 61
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CVAA
Client: Buxton Environmental Laboratory ID: OC29021-012
Description: SW -1 Matrix: Aqueous
Date Sampled:03/28120131730
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2158 FCJ 04/02/2013 1622 17552
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A ND 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L= LCSILCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-013
Description: SW -2 Matrix: Aqueous
Date Sampled:03/28/2013 1815
Date Received: 03/29/2013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 82608 1 04/05120131734 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCSILCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 56 of 61
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CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
ND
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
1.0
0.33
ug/L
1
Bromoform
7525-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
ND
2.0
0.47
ug/L
1
Chloroform
67-66-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
82608
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
82608
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
ND
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
0.22 J
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
82608
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
ND
1.0
0.33
ug/L
1
Styrene
100-42-5
8260B
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
ND
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCSILCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-013
Description: SW -2 Matrix: Aqueous
Date Sampled:03/28/20131815
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/05/20131734 JAC 17854
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitatton of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 57 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS
Analytical
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
74
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4
8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4
8260B
ND
1.0
0.054
ug/L
1
Xylenes (total)
1330-20-7
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitatton of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
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Run 1
Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
74
70-130
Bromofluorobenzene
80
70-130
Toluene -d8
79
70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitatton of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 57 of 61
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ICP -MS
Client: Buxton Environmental Laboratory ID: OC29021-013
Description: SW -2 Matrix: Aqueous
Date Sampled:03/28/20131815
Date Received: 0312912013
Run
Prep Method
Analytical Method
Dilution
Analysis Date
Analyst
Prep Date
Batch
1
3005A
6020A
1
03/31/20131020
BNW
03/29/20131424
17318
2
3005A
6020A
1
04/02/20131426
CDF
03/29/20131424
17318
CAS
Analytical
6020A
Parameter Number
Method Result Q
PQL MDL Units Run
Antimony 7440-36-0
6020A ND
1.0 0.097 ug/L 1
Arsenic 7440-38-2
6020A ND
1.0 0.26 ug/L 1
Barium
7440.39-3
6020A
23
B
5.0
0.045
ug/L 1
Beryllium
7440-41-7
6020A
ND
0.40
0.028
ug/L 1
Cadmium
7440-43-9
6020A
0.10
0.10
0.059
ug/L 2
Chromium
7440-47-3
6020A
0.56
J
5.0
0.35
ug/L 1
Cobalt
7440-48-4
6020A
0.31
J
5.0
0.029
ug/L 1
Copper
7440-50-8
6020A
1.1
1.0
0.15
ug/L 1
Lead
7439-92-1
6020A
0.22
BJ
1.0
0.047
ug/L 1
Nickel
7440-02-0
6020A
0.30
BJ
5.0
0.28
ug/L 1
Selenium
7782-49-2
6020A
ND
1.0
0.25
ug/L 1
Silver
7440-22-4
6020A
ND
1.0
0.011
ug/L 1
Thallium
7440-28-0
6020A
ND
0.50
0.076
ug/L 1
Vanadium
7440-62-2
6020A
2.2
J
5.0
1.5
ug/L 1
Zinc
7440-66-6
6020A
2.1
J
10
1.5
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a'NW S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 58 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1

CVAA
Client: Buxton Environmental Laboratory ID: OC29021-013
Description: SW -2 Matrix: Aqueous
Date Sampled:03/28/2013 1815
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/02/2013 2206 FCJ 04/02/2013 1622 17552
CAS Analytical
Parameter Number Method Result Q PQL MDL Units Run
Mercury 7439-97-6 7470A ND 0.00010 0.000015 mg/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at orabove the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 59 of 61
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Volatile Organic Compounds by GC/MS
Client: Buxton Environmental Laboratory ID: OC29021-014
Description: TRIP BLANK Matrix: Aqueous
Date Sampled:03128/2013
Date Received: 03/29/2013
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260B
1 04/05/2013 0253 TAF
17829
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Acetone
67-64-1
8260B
ND
20
6.7
ug/L
1
Acrylonitrile
107-13-1
8260B
ND
20
1.2
ug/L
1
Benzene
71-43-2
8260B
ND
1.0
0.13
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
1.0
0.16
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
1.0
0.33
ug/L
1
Bromoform
75-25-2
8260B
ND
1.0
0.66
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
2.0
0.80
ug/L
1
2-Butanone (MEK)
78-93-3
8260B
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260B
ND
1.0
0.097
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
1.0
0.14
ug/L
1
Chlorobenzene
108-90-7
82608
ND
1.0
0.33
ug/L
1
Chloroethane
75-00-3
8260B
ND
2.0
0.47
ug/L
1
Chloroform
67-06-3
8260B
ND
1.0
0.33
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1.0
0.35
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1.0
0.60
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
1.0
0.33
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
0.30
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
1.0
0.35
ug/L
1
trans-1,4-Dichloro-2-butene
110-57-6
8260B
ND
2.0
0.83
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
1.0
0.33
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
1.0
0.33
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
ND
1.0
0.13
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
1.0
0.15
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
1.0
0.16
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
ND
1.0
0.12
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1.0
0.21
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
1.0
0.19
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
8260B
ND
1.0
0.092
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
8260B
ND
1.0
0.11
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
0.33
ug/L
1
2-Hexanone
591-78-6
8260B
ND
10
0.27
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260B
ND
5.0
1.2
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260B
ND
10
0.31
ug/L
1
Methylene chloride
75-09-2
8260B
0.70 J
1.0
0.33
ug/L
1
Styrene
100-42-5
8260B
ND
1.0
0.12
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
1.0
0.20
ug/L
1
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
1.0
0.16
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
1.0
0.13
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
0.33
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND
1.0
0.074
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
1.0
0.21
ug/L
1
Trichloroethene
79-01-6
8260B
ND
1.0
0.18
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
1.0
0.30
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
1.0
0.33
ug/L
1
PQL= Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria L
= LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
S = MS/MSD failure
Shealy Environmental Services, Inc.
Page: 60 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Level 1 Report v2.1

Volatile Organic Compounds by GC/MS
Client:Buxton Environmental Laboratory ID: OC29021-014
Description: TRIP BLANK Matrix: Aqueous
Date Sampled. -0312812013
Date Received: 0312912013
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 82608 1 04/05/2013 0253 TAF 17829
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 61 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.11
CAS
Analytical
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-04
113
Parameter
Number
Method
Result Q
PQL
MDL
Units
Run
Vinyl acetate
108-05-4
8260B
ND
5.0
1.3
ug/L
1
Vinyl chloride
75-01-4
82606
ND
1.0
0.054
ug/L
1
Xylenes (total)
1330-20-7
8260B
ND
1.0
0.33
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 61 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.11
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-04
113
70-130
Bromofluorobenzene
111
70-130
Toluene -d8
116
70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 61 of 61
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.11

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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Environrnentrd Services. Inc.
Do:urreot Numb=r: F -,1n-016
Revision Number. IC
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Reo:aces Date. iCt: I(1 I
ERee,n a Det: 0ICt':3
Sample Receipt Checklist (SRC)
Client: Y,7/ 07N Cooler Inspected by/date: LA L .- tzi t.':
Means of recei L-8 SESI
Client 0 UPS FedEx P Airbr)rn--
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1, Were custody seals present on the cooler?
Yes
N
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Cooler ID, temperarure upon receipt -C; I -C `C =C
Method., ❑ Temperature Blan)� Against 13ot-.les
Nfethod of coolant: ,_Q -Wet Ice ❑ Blue Ice ❑ Dry Ice ❑ None
If res onsc is No (or Yes for 14, 15,16). an ezplanatimiresoludon must he movid--c.
Yes ❑
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No 11Nrart�
3. If temperature of any cooler excouded 6.0"(, was Project Manaager notified?
Ph -f notified by SRC, phone, note (curc+lc one), other:__ . (For
c:oulers received via commercial courier, PMs are to be notified irrmediatcly.
Yes
No ❑ N
4. is the eoalmercial courier's packing slip atwched (o this farm^
1 Yes Jj.
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6. W. -re sample s ti,; tod?
j 'r. 'IVa -S collnctior. date & tirne listed?
Yes -a ' No Lj
ti. Were tests to be perfo mcd listed on the COC?
Yes
No Ll 1
9. Dia all samples arrive. in !ae proper conmin_ers for each test? --_—
Yes
Ycs.-_�
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No ❑
lU. Jid ali container Inhel irrl'urn:x:ion (Ill, date, :iiiie agree with COC?
11. Did a?1 coo laincrs arrive in good condition (unbroken, lids. on, etc.)? I
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14. Wert any samp:cs containers missing' _
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15. Were there at,,., excess sanlples :tot listed on COC?
.6. Were bubbles present =