6004_DukeMcGuireLF2_June2016_1stSemiAnnual_DIN26721_20160909

June 13, 2016

McGuire Nuclear Station - Landfill #2
(Synthetically Lined) Permit No. 6004
Semiannual Groundwater
Monitoring Report
June 2016 Sampling Event

September 2, 2016

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004
June 2016 Sampling Event CONTENTS

ii

Contents
Page
Report Verification i
Contents ii
Section 1 - Background 1
Section 2 - Methods 3
2.1 Sampling and Analysis Methods 3
2.2 Statement of Work 3
Section 3 - Results 5
3.1 Site Groundwater Flow 5
3.2 Analytical Results 5

FIGURES
1. Site Location Map
2. Sample Locations
3. Generalized Groundwater Surface Contours
TABLES
1. Well Construction Information
2. Groundwater Flow Velocities
3. Field Data Parameters
4. Groundwater Field and Analytical Results
5. Field and Analytical Results that Equal or Exceed 15A NCAC 2L Groundwater Quality
Standards
6. Surface Water Field and Analytical Results
7. Leachate Sample Field and Analytical Results
8. Radiological Analytical Results
APPENDICES
A. Field Sampling Forms
B. Laboratory Report and Chain-of-Custody Forms

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004
June 2016 Sampling Event SECTION 1 - BACKGROUND

1

Section 1 - Background
The McGuire Nuclear Station Landfill #2 (Synthetically Lined)1 is located at the Duke Energy
Carolinas, LLC (Duke Energy) McGuire Nuclear Station in Mecklenburg County, North Carolina.
The landfill is permitted to accept waste specified by the Permit to Operate. The landfill was
constructed with a high-density polyethylene (HDPE) synthetic liner and leachate collection and
removal system. Leachate and contact stormwater are collected in a lined leachate collection
basin and pumped to the McGuire Nuclear Station wastewater treatment system. The landfill is
permitted under the North Carolina Department of Environmental Quality (NCDEQ) Solid Waste
Permit No. 6004.
The landfill and nearby area are depicted on Figures 1 and 2. The landfill is located south of
North Carolina Highway 73, north of Cashion Road, and to the west of Linderman Road.
Cashion Road runs along a surface water divide, with surface flow draining to the northwest and
to the southeast. A surface water drainage feature is located to the northeast of the landfill. This
feature drains to the northwest to a perennial unnamed stream. Surface water sample location
SW-1 is located in this unnamed stream (north of the landfill) and is upstream from the
confluence with the surface water drainage feature. Surface water sample location SW-2 is also
located in this unnamed stream, downstream from SW-1 and west of the landfill. The unnamed
stream drains to the west to the Catawba River. A second surface water drainage feature is
located to the southwest of the landfill, draining to the northwest into the unnamed stream.
As described in the Sampling and Analysis Plan2 (SAP), the monitoring system at the landfill
consists of the following:
Monitoring Wells: MW-5 MW-5A
MW-6 MW-6A
MW-7 MW-7A
MW-8 MW-8A
MW-9 MW-9A
MW-10A

Surface Water Sample Locations SW-1 SW-2

Leachate Sample Locations: Leachate
Pond

1 In response to the North Carolina Division of Public Health, Radiation Protection Section, November 17,
2006 letter to Duke Energy, LLC, Duke Energy offered to indicate the McGuire Nuclear Station Landfill #2
as “(Synthetically Lined)” in reports.
2 Groundwater Monitoring Program Sampling and Analysis Plan, McGuire Nuclear Station, Landfill #2
(Synthetically Lined), Permit No. 6004-INDUS, March 28, 2014.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004
June 2016 Sampling Event SECTION 1 - BACKGROUND

2

The leachate sample is collected from the outfall of the leachate pipe which conveys leachate
from the landfill to the leachate collection basin. The locations of the monitoring wells, the
surface water sample locations, and the leachate collection basin are shown on Figure 2.
With the exception of well MW-10A, the wells are installed as well pairs with one shallow well
and one deeper well adjacent to one another. The well with the “A” designation is the deeper
well in each well pair. Well pair MW-9 and MW-9A are installed adjacent to and downgradient
from the leachate collection basin. The remaining wells are installed adjacent to the landfill.
Well construction information is provided in Table 1.
According to the SAP, monitoring wells MW-5 and MW-5A are the upgradient wells and are
considered the background wells for the site. Surface water sample location SW-1 is considered
the upgradient or background surface water sample location.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004
June 2016 Sampling Event SECTION 2 - METHODS

3

Section 2 - Methods
2.1 Sampling and Analysis Methods
Sample collection and documentation of sampling activities was performed by Duke Energy
personnel (Duke Energy Carolinas Field Certification #5193) in accordance with the North
Carolina Solid Waste Management Guidelines. Copies of the field sampling forms are included
in Appendix A. The parameters and constituents sampled were selected by Duke Energy and
the NCDEQ Division of Solid Waste. Alkalinity, chloride, sulfate, and metals were analyzed by
the Duke Energy Analytical Laboratory (North Carolina Laboratory Certification #248). Volatile
organic compounds (VOCs) and total petroleum hydrocarbons (TPHs) were analyzed by
TestAmerica Laboratories, Inc. (North Carolina Laboratory Certification #387). The laboratory
reports and chain-of-custody forms are included in Appendix B.
The groundwater, surface water, and leachate samples were analyzed for the following
constituents:
 Barium, chromium, and silver using Solid Waste (SW) Method 6010D
 Arsenic, cadmium, lead, and selenium using SW 6020B
 Mercury using Environmental Protection Agency (EPA) Method 7470A
 Chloride and sulfate using EPA Method 9056A
 VOCs using SW846 Method 8260B
 TPHs diesel range organics (DRO) using SW846 Method 8015C Modified
In addition, the following analyses were performed in accordance with the requirements of the
Radioactive Materials License No. 060-0379-7 issued by the North Carolina Department of
Health and Human Services Radiation Protection Section:
 Gross alpha radioactivity using EPA Method 900
 Gross beta radioactivity using EPA Method 900
 Tritium using EPA Method 906.0 Modified
 Gamma radioactivity for select isotopes
2.2 Statement of Work
HDR completed the following tasks:
 Received field sampling information provided by Duke Energy (performed by Duke
Energy personnel) for monitoring wells MW-5, MW-5A, MW-6, MW-6A, MW-7, MW-7A,
MW-8, MW-8A, MW-9, MW-9A, and MW-10A. Data were also received for surface water
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004
June 2016 Sampling Event SECTION 2 - METHODS

4

sample locations SW-1 and SW-2 as well as for the leachate pond sample. The samples
were collected on June 13, 2016, and HDR received the data on July 6, 2016.
 Reviewed the laboratory analytical results for the samples noted above. The Electronic
Data Deliverable (EDD), provided by Duke Energy, was adapted to conform to the
format requirements of the NCDEQ EDD template. HDR added an italicized J data
qualifier (J) to indicate a concentration that equals or is greater than the laboratory’s
method reporting limit (MRL), but less than the Solid Waste Section Limit3 (SWSL), and
retained the laboratory-supplied qualifier J to indicate values that equal or are greater
than the laboratory’s method detection limit (MDL) but are less than the MRL. A copy of
the original EDD is retained in HDR’s files.
 Developed a generalized groundwater surface contour map using map data and
groundwater elevation data supplied by Duke Energy.
 Prepared and submitted this Semiannual Groundwater Monitoring Report to Duke
Energy.
3 The Solid Waste Section Limit (SWSL) is defined by NCDEQ as the lowest amount of analyte in a
sample that can be quantitatively determined with suitable precision and accuracy. The SWSL is the
concentration below which reported results must be qualified as estimated. NCDEQ Division of Waste
Management Memorandum dated February 23, 2007.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004
June 2016 Sampling Event SECTION 3 - RESULTS

5

Section 3 - Results
3.1 Site Groundwater Flow
Generalized groundwater surface contours and groundwater flow direction arrows for the site
are shown on Figure 3. These contours were developed using groundwater elevations
measured at the shallow wells on the date of sampling. Calculated groundwater flow velocities
are presented in Table 2.
Groundwater flow in the area of the landfill is generally from the southeast end of the landfill
toward the northwest and the unnamed stream described in Section 1. Groundwater flow on the
east side of the landfill is towards the northeast toward wells MW-6, MW-6A, MW-10A, and the
surface water drainage feature located northeast of the wells.
3.2 Analytical Results
The measured field data parameters are presented in Table 3.
The groundwater sampling field and analytical results are summarized in Table 4. The analysis
results for the constituents are compared to the groundwater standards found in Title 15A
NCAC 02L .0202 (g) (2L Standards). Concentrations that attain or exceed the 2L Standards are
noted on Table 4 by bold font. A summary of the analytical results that attain or exceed the 2L
Standards and a preliminary analysis of the cause and significance of the exceedances are
presented in Table 5.
Surface water sample locations SW-1 and SW-2 are located on an unnamed stream. The
unnamed stream is a tributary of the Catawba River, which is classified by the NCDEQ Division
of Water Quality as Class WS-IV surface water at the confluence with the unnamed stream. As
a result, the field and analytical results from these locations are compared to Title 15A, NCAC,
Subchapter 2B Standards (2B Standards) for Class WS-IV water. The field and analytical
results of surface water sampling are summarized in Table 6.
The MDL was greater than the respective 2L Standard for the following constituents:
 1,2,3-Trichloropropane
 1,2-Dibromo-3-chloropropane (DBCP)
 1,2-Dibromoethane (EDB)
 Vinyl chloride
The MDL was greater than the respective 2B Standard for the following constituents:
 Silver
 Mercury
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004
June 2016 Sampling Event SECTION 3 - RESULTS

6

The MDLs for the listed constituents were all below their corresponding SWSLs as required by
the February 23, 2007, NCDEQ memo. These constituents were not detected above the MDL in
the analyzed samples and are not considered to exceed their respective 2L or 2B Standards.
The field and analytical results for leachate sampling are summarized in Table 7.
Concentrations with values that equal to or greater than the SWSLs are noted in Table 7 by
gray-shaded cells.
Selected samples were diluted as is normal laboratory practice to bring samples within the
calibrated range of the analysis. Specifics regarding the samples that were diluted, including the
dilution amount, are reported in the EDD.
The results of the radiological analyses are presented in Table 8. A copy of this report has been
submitted to the North Carolina Department of Health and Human Services Radiation Protection
Section for reference. HDR did not evaluate this data.

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b
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D
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E
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o
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J
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6
,

2
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1
6
.
Sc
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d

I
n
t
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r
v
a
l

be
l
o
w

T
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C
(f
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.
)
Geology of Screened IntervalWell Diameter (in.)Casing Type
We
l
l

S
t
i
c
k
-
u
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He
i
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h
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A
b
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Gr
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(f
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)
Gr
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d
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W
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be
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(ft
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To
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De
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b
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TO
C
(f
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f
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T
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(f
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)
We
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In
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Ele
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(
f
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Gr
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n
d

S
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f
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Ele
v
a
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n
(f
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.
)
Page  1  of  1
Ta
b
l
e

2
–
G
r
o
u
n
d
w
a
t
e
r

F
l
o
w

V
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l
o
c
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s
Du
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E
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C
a
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N
u
c
l
e
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a
t
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La
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d
f
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#
2

(
S
y
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t
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e
t
i
c
a
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l
y

L
i
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d
)

-

P
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N
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6
0
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4
We
l
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I
D
Up
g
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Gr
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Co
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El
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v
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(f
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D
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Gr
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w
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Co
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El
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(f
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Li
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t
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th
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(f
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d
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Gr
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(f
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f
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Po
r
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s
i
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(%
/
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)
Groundwater Velocity (ft/day)
MW
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9

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No
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s
:
1
.

L
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d
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t
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g
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3
.

A
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m
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w
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w
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u
p
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c
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a
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p
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g
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4
.

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w
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a
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l
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w
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i
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f
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a
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t
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c
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v
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.
5
.

H
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d
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g
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a
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g
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c
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a
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p
p
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x
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m
a
t
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.
6
.

H
y
d
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c
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v
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p
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f
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t
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a
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h
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d
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l
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m
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c
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d
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v
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d
a
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a

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H
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R

C
o
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d
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y

D
a
t
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b
a
s
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(
u
n
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b
l
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s
h
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d

d
a
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f
r
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P
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d
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a
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s
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w
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f
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d
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l
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b
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d
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k
)
.
7
.

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f
f
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t
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v
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p
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s
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y

p
r
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s
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n
t
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d

f
o
r

t
h
e

a
l
l
u
v
i
u
m
/
s
o
i
l
/
s
a
p
r
o
l
i
t
e

h
y
d
r
o
s
t
r
a
t
i
g
r
a
p
h
i
c

l
a
y
e
r

i
s

t
h
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m
e
a
n

v
a
l
u
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e
s
t
i
m
a
t
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d

f
r
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m

g
r
a
i
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s
i
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d
a
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u
s
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g

F
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t
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/
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D
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g
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m
s
.

8
.

T
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h
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d
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l
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f
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n

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s

n
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a
v
a
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l
a
b
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f
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m
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n
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M
W
-
5
.

T
h
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s

w
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l

i
s

a
s
s
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d

t
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b
e

s
c
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d

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a
l
l
u
v
i
u
m
/
s
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/
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a
p
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l
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y
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r
.
9
.

H
y
d
r
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u
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g
r
a
d
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n
t
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a
n
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g
r
o
u
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d
w
a
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e
r

v
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l
o
c
i
t
i
e
s

b
a
s
e
d

o
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g
r
o
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n
d
w
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t
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r

d
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p
t
h
s

m
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a
s
u
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d

o
n

J
u
n
e

1
3
,

2
0
1
6
.
Page 1 of 1
Ta
b
l
e

3
–
F
i
e
l
d

D
a
t
a

P
a
r
a
m
e
t
e
r
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
2

(
S
y
n
t
h
e
t
i
c
a
l
l
y

L
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
6/
1
3
/
2
0
1
6
MW
-
5
63
.
9
0

6
0
.
8
7

7
0
7
.
4
4

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

0
.
4
9

0
.
5
0

Y
E
S

1
9
.
8
0
15
5.4

4
.
3
412

1
0
.
3
9
6/
1
3
/
2
0
1
6
MW
-
5
A

9
6
.
0
0

6
1
.
6
3

7
0
6
.
7
9

N
o
r
m
a
l

N
o
n
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C
P

N
/
A

5
.
6
1

1
7
.
2
5

N
O

1
6
.
4
7
56
6.4

0
.
5
420

8
.
4
2
6/
1
3
/
2
0
1
6
MW
-
6
37
.
2
0

3
0
.
2
7

6
9
8
.
1
8

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

1
.
1
3

6
.
2
5

N
O

1
6
.
3
4
11
4
5.9

2
.
2
386

6
.
6
7
6/
1
3
/
2
0
1
6
MW
-
6
A

4
7
.
9
0

2
9
.
5
4

6
9
9
.
4
4

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

2
.
9
9

1
0
.
0
0

N
O

1
6
.
3
4
56
5.5

0
.
6
389

8
.
1
5
6/1
3
/
2
0
1
6
MW
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7
37
.
3
0

3
2
.
9
1

6
9
2
.
9
5

N
o
r
m
a
l

N
o
n
e

E
O
P

N
/
A

0
.
7
2

0
.
3
4

N
/
A

1
9
.
4
2
38
5.9

1
7
.
4

3
6
5

8
.
8
9
6/
1
3
/
2
0
1
6
MW
-
7
A

5
9
.
4
0

3
1
.
8
6

6
9
2
.
8
0

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

4
.
4
9

1
3
.
5
0

N
O

1
6
.
6
5
12
0
6.5

3
.
8
365

6
.
6
2
6/
1
3
/
2
0
1
6
MW
-
8
71
.
5
0

6
1
.
7
9

6
9
7
.
8
1

N
o
r
m
a
l

N
o
n
e

E
O
P

N
/
A

1
.
5
8

0
.
5
4

N
/
A

1
6
.
6
0
12
3
6.3

1
6
.
0

N
/
A

N
/
A
6/
1
3
/
2
0
1
6
MW
-
8
A

8
4
.
4
0

6
1
.
7
6

6
9
7
.
9
2

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

3
.
6
9

1
1
.
2
5

N
O

1
6
.
0
6
94
6.7

2
.
2
356

7
.
9
7
6/
1
3
/
2
0
1
6
MW
-
9
30
.
8
0

2
4
.
1
7

6
8
7
.
7
0

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

1
.
0
8

6
.
2
5

N
O

1
8
.
6
9
74
5.7

3
.
1
400

3
.
8
9
6/
1
3
/
2
0
1
6
MW
-
9
A

4
7
.
8
0

2
4
.
5
1

6
8
7
.
6
2

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

3
.
8
0

1
6
.
0
0

N
O

1
7
.
7
9
10
3
6.4

3
.
4
374

4
.
7
7
6/
1
3
/
2
0
1
6
MW
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No
t
e
s
:

1
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P
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r
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e

M
e
t
h
o
d
s
;

L
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=
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o
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F
l
o
w
,

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=
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n
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n
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P
u
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g
e

(
3
-
5

w
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l
l

v
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l
u
m
e
s
)
,

N
P
=
N
o

P
u
r
g
e

(
H
y
d
r
a
S
l
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e
v
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)
,

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q
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p
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O
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l
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g
e
.

P
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p

r
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a
p
p
l
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a
b
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t
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L
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p
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i
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g

o
n
l
y
.

2
.

F
i
e
l
d

s
a
m
p
l
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g

p
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m
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d

b
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D
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k
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E
n
e
r
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y

C
a
r
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l
i
n
a
s
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C

p
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3
.

E
V
A
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i
n
d
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w
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w
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l
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v
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i
n

t
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w
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l
l

w
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s

d
r
a
w
n

d
o
w
n

t
o

t
h
e

l
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v
e
l

o
f

t
h
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p
u
m
p

d
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n
g

p
u
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g
i
n
g
.

4
.

µ
Լ /c
m

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n
d
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c
a
t
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m
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p
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t
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r
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5
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6
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7
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m
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E

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m
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N
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H
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8
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WA
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(f
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Page 1 of 1
Ta
b
l
e

4
–
G
r
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d
w
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r

F
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a
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(
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14
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µ
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t
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.
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6
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17
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Page 1 of 2
Ta
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4
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Page 1 of 1
Ta
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A
Appendix A
Field Sampling Forms
ANALYZER SERIAL #:
WEATHER CONDITIONS:
DATE:TIME:DATE:TIME:
Calibation Instrument Standard Instrument Standard
Standard Value Value Value Value
SS 0.0 ▬▬►0.0 0.0 ▬/▬►0.0
SS 230.9 ▬▬►227 221.1 ▬/▬►227
SS 75.0 ▬/▬►75 77.7 ▬/▬►75
SS ▬/▬►1410 ▬/▬►1410
B (7.00)7.00 ▬▬►7.02 7.04 ▬/▬►7.02
B (4.00)4.03 ▬▬►4.00 4.03 ▬/▬►4.00
B (10.00)10.08 ▬/▬►10.04 10.09 ▬/▬►10.04
21.22 20.96
pH Check B (7.00)▬▬►7.13
Time:0.00
435 ▬▬►439 439 ▬/▬►439
N/A ▬/▬►N/A N/A ▬/▬►N/A
Zobell's 21.04 20.72
TEMP (CO)
BP (mmHg)
COND
100 % mg/L 8.77 ▬▬►8.75 8.90 ▬/▬►8.80
After Cal 8.79 100.42 8.85 100.58
LCS 8.71 99.51 8.81 100.13
LCSD 8.74 0.34 8.83 0.23
SS 54.2 ▬/▬►54.5 53.2 ▬/▬►54.5
NIST N/A ▬/▬►N/A N/A ▬/▬►N/A
KEY:
NOTES:
FIELD SAMPLING CALIBRATION FORM
STUDY:McGUIRE NUCLEAR STATION - LANDFILL 2 GROUNDWATER MONITORING
DATE (s):June 13, 2016 SURFACE UNIT READER:LDC
OTHER EQUIPMENT:TURBIDIMETER NO.2 - 3260-GW Clear, calm, 70 to 85 deg F
COLLECTORS:LDC, PSP SURFACE UNIT SERIAL #:3858
ANALYZER MODEL#:MS5 66121
Calibration Date / Time 13-Jun-16 440 14-Jun-16 440
PROCEDURE #:HYDROLAB 3210.6 VALIDATED BY:
Parameter Calibration Results Calibration Results
CALIBRATION BP (mmHg)740.19 CALIBRATION BP (mmHg)739.94
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
INSTRUMENT ZEROED INSTRUMENT ZEROED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
CHECK (uS/cm)
SPEC. COND.
(uS/cm)
pH
(units)
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Buffer Temp.Buffer Temp.
ORP Temp.ORP Temp.
ORP CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Buffer Temp.
89
CALIBRATION PASS CALIBRATION PASS
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
After Cal % SAT After Cal % SAT
TURB
(ntu)CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION PASS CALIBRATION PASS
DO
(mg/L)
20.54 20.26
740.19 739.94
89
Temp Cert Device #
TEMP
(deg C)Adjustment Not Available Adjustment Not Available
Tested - OK Replaced ref Electrode KCL
See Notes Replaced Ref. Electrode Tip
INSTRUMENT MAINTENANCE DATE / TIME
Conductance Subsystem pH Subsystem
Cleaned Electrodes Cleaned Electrodes
Tested - OK See Notes Tested - OK See Notes
Dissolved Oxygen Subsystem
Replaced Teflon Membrane Cleaned Electrode
Tested - OK See Notes
Oxidation Reduction Subsystem Temperature Subsystem
Cleaned Electrode Cleaned Electrode
Replaced DO electrolyte See Notes
Field Barometric Pressure
Beginning BP 741.2 (mmHg)Ending BP 742.2
SS = Standard solution AW = Average Winkler ▬/▬►= Not Adjusted To
(mmHg)
B = Buffer W = Winkler ▬▬► = Adjusted To N/A = Not Applicable
ANALYZER SERIAL #:
WEATHER CONDITIONS:
DATE:TIME:DATE:TIME:
Calibation Instrument Standard Instrument Standard
Standard Value Value Value Value
SS 0.0 ▬▬►0.0 0.0 ▬/▬►0.0
SS 225.0 ▬▬►227 220.1 ▬/▬►227
SS 75.6 ▬/▬►75 72.9 ▬/▬►75
SS ▬/▬►1410 ▬/▬►1410
B (7.00)7.02 ▬▬►7.02 7.08 ▬/▬►7.02
B (4.00)4.02 ▬▬►4.00 4.07 ▬/▬►4.00
B (10.00)10.03 ▬/▬►10.04 10.07 ▬/▬►10.04
21.18 20.96
pH Check B (7.00)▬▬►7.13
Time:0.00
437 ▬▬►439 439 ▬/▬►439
N/A ▬/▬►N/A N/A ▬/▬►N/A
Zobell's 21.03 20.64
TEMP (CO)
BP (mmHg)
COND
100 % mg/L 8.74 ▬▬►8.76 8.84 ▬/▬►8.81
After Cal 8.75 99.84 8.82 100.16
LCS 8.67 98.93 8.78 99.71
LCSD 8.69 0.23 8.76 -0.23
SS 53.2 ▬/▬►53.5 53.1 ▬/▬►53.5
NIST N/A ▬/▬►N/A N/A ▬/▬►N/A
KEY:
NOTES:
FIELD SAMPLING CALIBRATION FORM
STUDY:McGUIRE NUCLEAR STATION - LANDFILL 2 GROUNDWATER MONITORING
DATE (s):June 13, 2016 SURFACE UNIT READER:PSP
OTHER EQUIPMENT:TURBIDIMETER NO.1 - 3260-GW Clear, calm, 70 to 85 deg F
COLLECTORS:LDC, PSP SURFACE UNIT SERIAL #:0730
ANALYZER MODEL#:HL4 400440
Calibration Date / Time 13-Jun-16 500 14-Jun-16 345
PROCEDURE #:HYDROLAB 3210.6 VALIDATED BY:
Parameter Calibration Results Calibration Results
CALIBRATION BP (mmHg)740.19 CALIBRATION BP (mmHg)739.94
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
INSTRUMENT ZEROED INSTRUMENT ZEROED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
CHECK (uS/cm)
SPEC. COND.
(uS/cm)
pH
(units)
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Buffer Temp.Buffer Temp.
ORP Temp.ORP Temp.
ORP CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Buffer Temp.
85.3
CALIBRATION PASS CALIBRATION PASS
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
After Cal % SAT After Cal % SAT
TURB
(ntu)CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION PASS CALIBRATION PASS
DO
(mg/L)
20.48 20.22
740.19 739.94
85
Temp Cert Device #
TEMP
(deg C)Adjustment Not Available Adjustment Not Available
Tested - OK Replaced ref Electrode KCL
See Notes Replaced Ref. Electrode Tip
INSTRUMENT MAINTENANCE DATE / TIME
Conductance Subsystem pH Subsystem
Cleaned Electrodes Cleaned Electrodes
Tested - OK See Notes Tested - OK See Notes
Dissolved Oxygen Subsystem
Replaced Teflon Membrane Cleaned Electrode
Tested - OK See Notes
Oxidation Reduction Subsystem Temperature Subsystem
Cleaned Electrode Cleaned Electrode
Replaced DO electrolyte See Notes
Field Barometric Pressure
Beginning BP 741.2 (mmHg)Ending BP 742.2
SS = Standard solution AW = Average Winkler ▬/▬►= Not Adjusted To
(mmHg)
B = Buffer W = Winkler ▬▬► = Adjusted To N/A = Not Applicable
49.90 63.90
45 (psi)10 (sec)(sec)
(gal)
0.49 (gal)
@
QC By:
SAMPLING NOTES
ADDITIONAL WELL CONDITION NOTES
Good Tag
WELL CONDITION
PROTECTIVE CASING
WELL PAD
WELL TAG
Good Condition
Good Condition
Good ConditionWELL CASING
PSP 0
TOTAL PURGE
VOLUME
0.50
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY
(recalculates on
current water
level)(deg C)(umho/cm)(SU)(NTU)(mV-NHE)(mg/L)
4.3 412 10.39
SAMPLING EQUIPMENT
TUBING DIAMETER (in)1/2 OD
QED T1200
PURGE COMPLETE TEMP SPECIFIC pH TURBIDITY
WATER ELEVATION (ft msl)707.44
APPEARANCE
DETECTED ODOR None
Normal
WATER LEVEL
AFTER PURGE *
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27
WELL DEPTH (ft TOC)
WELL DIAMETER (in)MIDDLE OF WETTED SCREEN (ft toc)
WELL VOL
SCREEN INTERVAL (ft TOC)TO
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)60.87 WATER COLUMN (ft)3.03
EQUIPMENT INFORMATION
LEVEL METER SERIAL#26055
62.90PUMP INTAKE DEPTH (ft TOC)63.90
TOC ELEV (ft msl)
GS ELEV (ft msl)
768.31
766.42
WELL/LOCATION NAME MW-5
FIELD CREW LDC, PSP
MONITORING WELL INFORMATION
2
N/A
PROCEDURE NO 3175.4DUKE ENERGY
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING
SAMPLING DATE(s)13-Jun-2016
62.39
PURGE METHOD
Conventional
DISCHARGERECHARGEPRESSURE 10
PUMP CONTROLLER SETTINGS
0.1631CONVERSION FACTOR
Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
0.49WELL VOLUME
(gal)
ORP
(ft)(YES/NO)
0.50 YES 19.80 15 5.38
VOLUME EVACUATION COND.
6/13/2016 0940
Sample preservation verified to pH
(units)< 2.0
DATE TIME
DISSOLVED
OXYGEN
82.00 96.00
50 (psi)10 (sec)(sec)
(gal)
5.61 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-5A
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)768.42 MIDDLE OF WETTED SCREEN (ft toc)89.00
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)96.00 GS ELEV (ft msl)766.45 PUMP INTAKE DEPTH (ft TOC)95.00
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)61.63 WATER COLUMN (ft)34.37 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)706.79 WELL VOLUME 5.61
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
5.75 NO 16.49 56 6.36 1.3 419
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
8.41
5.75 NO 16.47 56 6.35 0.5 420 8.42
5.75 NO 16.48 56 6.37 1.4 417 8.45
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
17.25 PSP 6/13/2016 1005 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
23.20 37.20
20 (psi)10 (sec)(sec)
(gal)
1.13 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
6.25 PSP 6/13/2016 0705 0
1.25 NO 16.34 114 5.93 2.2 386 6.67
1.25 NO 16.34 110 5.89 1.6 377 6.74
1.25 NO 16.27 109 5.87 0.7 371 6.78
1.25 NO 16.32 102 5.85 0.6 363 6.92
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
1.25 NO 16.35 92 5.79 1.1 346
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
7.17
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)30.27 WATER COLUMN (ft)6.93 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)698.18 WELL VOLUME 1.13
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)728.45 MIDDLE OF WETTED SCREEN (ft toc)33.74
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)37.20 GS ELEV (ft msl)726.79 PUMP INTAKE DEPTH (ft TOC)36.20
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-6
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
33.90 47.90
25 (psi)13 (sec)(sec)
(gal)
2.99 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
10.00 PSP 6/13/2016 0715 0
4.00 NO 16.34 56 5.52 0.6 389 8.15
3.00 NO 16.33 56 5.45 0.8 375 8.20
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
3.00 NO 16.33 55 5.48 1.7 359
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
8.23
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)29.54 WATER COLUMN (ft)18.36 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)699.44 WELL VOLUME 2.99
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)728.98 MIDDLE OF WETTED SCREEN (ft toc)40.90
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)47.90 GS ELEV (ft msl)727.54 PUMP INTAKE DEPTH (ft TOC)46.90
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-6A
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
23.30 37.30
55 (psi)25 (sec)(sec)
(gal)
788 (ml)
495 (ml)
1283 (ml)=0.34 (gal)@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition Grass was very tall around well.
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
NA
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
SAMPLE COLLECTED BY DATE TIME
Total Purge Volume LDC 6/13/2016 0815
Sample preservation verified to pH
(units)< 2.0
17.4 365 8.89 N/A
Tubing Volume Removed 0.5 gal.EQUIPMENT PURGE ONLY SAMPLE CHLORINE
(mg/l)Pump (Bladder) Volume
32.91 N/A Below pump 19.42 38 5.91
(ft)(ml/min)(ft)(deg C)(umho/cm)(SU)(NTU)(mV -NEH)(mg/L)
WATER LEVEL RATE WATER LEVEL COND.OXYGEN
INITIAL FLOW FINAL TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)32.91 WATER COLUMN (ft)4.39 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)692.95 WELL VOLUME 0.72
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 5
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Equip. Only Purge
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)725.86 MIDDLE OF WETTED SCREEN (ft toc)35.11
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)37.30 GS ELEV (ft msl)723.72 PUMP INTAKE DEPTH (ft TOC)36.30
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-7
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR EQUIPMENT PURGE ONLY SAMPLING
45.40 59.40
30 (psi)10 (sec)(sec)
(gal)
4.49 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition Grass was very tall around well.
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
13.50 LDC 6/13/2016 0845 0
4.50 NO 16.65 120 6.51 3.8 365 6.62
4.50 NO 16.56 119 6.48 4.3 361 6.63
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
4.50 NO 16.67 120 6.49 7.2 354
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
6.70
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)31.86 WATER COLUMN (ft)27.54 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)692.80 WELL VOLUME 4.49
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)724.66 MIDDLE OF WETTED SCREEN (ft toc)52.40
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)59.40 GS ELEV (ft msl)722.74 PUMP INTAKE DEPTH (ft TOC)58.40
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-7A
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
57.50 71.50
35 (psi)10 (sec)(sec)
(gal)
1531 (ml)
495 (ml)
2026 (ml)=0.54 (gal)@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition Grass was very tall around well.
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
0
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
SAMPLE COLLECTED BY DATE TIME
Total Purge Volume LDC 6/13/2016 0635
Sample preservation verified to pH
(units)< 2.0
16.0 342 8.45 N/A
Tubing Volume Removed 0.75 gal EQUIPMENT PURGE ONLY SAMPLE CHLORINE
(mg/l)Pump (Bladder) Volume
61.79 N/A Below pump 16.60 123 6.32
(ft)(ml/min)(ft)(deg C)(umho/cm)(SU)(NTU)(mV-NHE)(mg/L)
WATER LEVEL RATE WATER LEVEL COND.OXYGEN
INITIAL FLOW FINAL TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)61.79 WATER COLUMN (ft)9.71 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)697.81 WELL VOLUME 1.58
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Equip. Only Purge
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)759.60 MIDDLE OF WETTED SCREEN (ft toc)66.65
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)71.50 GS ELEV (ft msl)757.30 PUMP INTAKE DEPTH (ft TOC)70.50
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-8
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR EQUIPMENT PURGE ONLY SAMPLING
70.40 84.40
45 (psi)10 (sec)(sec)
(gal)
3.69 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition Grass was very tall around well.
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
11.25 LDC 6/13/2016 0730 0
3.75 NO 16.06 94 6.69 2.2 356 7.97
3.75 NO 16.05 94 6.70 2.7 351 7.96
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
3.75 NO 16.20 94 6.63 3.5 341
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
7.96
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)61.76 WATER COLUMN (ft)22.64 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)697.92 WELL VOLUME 3.69
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)759.68 MIDDLE OF WETTED SCREEN (ft toc)77.40
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)84.40 GS ELEV (ft msl)757.61 PUMP INTAKE DEPTH (ft TOC)83.40
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-8A
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
16.80 30.80
15 (psi)10 (sec)(sec)
(gal)
1.08 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition Grass was very tall around well.
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
6.25 LDC 6/13/2016 1030 0
1.25 NO 18.69 74 5.70 3.1 400 3.89
1.25 NO 18.48 71 5.70 2.8 402 3.97
1.25 NO 18.45 67 5.65 2.3 404 4.08
1.25 NO 18.34 40 5.59 2.5 404 4.28
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
1.25 NO 18.15 53 5.49 2.6 409
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
4.64
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)24.17 WATER COLUMN (ft)6.63 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)687.70 WELL VOLUME 1.08
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 5
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)711.87 MIDDLE OF WETTED SCREEN (ft toc)27.49
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)30.80 GS ELEV (ft msl)710.27 PUMP INTAKE DEPTH (ft TOC)29.80
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-9
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
33.80 47.80
25 (psi)10 (sec)(sec)
(gal)
3.80 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition Grass was very tall around well.
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
16.00 LDC 6/13/2016 1015 0
4.00 NO 17.79 103 6.41 3.4 374 4.77
4.00 NO 17.81 103 6.39 2.4 376 4.68
4.00 NO 17.58 106 6.37 2.0 375 4.46
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
4.00 NO 17.62 78 6.32 2.3 380
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
4.07
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)24.51 WATER COLUMN (ft)23.29 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)687.62 WELL VOLUME 3.80
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)712.13 MIDDLE OF WETTED SCREEN (ft toc)40.80
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)47.80 GS ELEV (ft msl)710.30 PUMP INTAKE DEPTH (ft TOC)46.80
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-9A
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
44.23 59.23
30 (psi)10 (sec)(sec)
(gal)
1.36 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
6.00 PSP 6/13/2016 0835 0
1.50 NO 16.66 25 5.47 3.8 407 7.58
1.50 NO 16.70 25 5.46 3.4 395 7.58
1.50 NO 16.72 25 5.44 21.4 376 7.57
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
1.50 NO 16.70 27 5.42 59.7 386
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
7.26
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)50.87 WATER COLUMN (ft)8.36 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)704.91 WELL VOLUME 1.36
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)755.78 MIDDLE OF WETTED SCREEN (ft toc)55.05
SCREEN LENGTH (ft)15.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)59.23 GS ELEV (ft msl)753.87 PUMP INTAKE DEPTH (ft TOC)58.23
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME MW-10A
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
0.00 0.00
N/A (psi)N/A (sec)(sec)
(gal)
(ft)=(in)@
QC By:
SAMPLING NOTES
PROTECTIVE CASING
WELL PAD
WELL CASING
WELL TAG
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
1130
200 7.69
0
N/A
Deployed Water Column In Screen
Above Top Of Hydrasleeve
NO PURGE SAMPLE CHLORINE
(mg/l)Top Weight SAMPLE COLLECTED BY DATE
(NTU)(mV-NHE)(mg/L)
N/A N/A N/A 21.07 117 7.37 20.8
TIME
PSP 6/13/2016
LENGTH DEPTH (top)DEPLOYED COND.OXYGEN
(inches)(ft TOC)(deg C)(umho/cm)(SU)
HYDRASLEEVE DEPLOYED DATE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
DETECTED ODOR CONVERSION FACTOR
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)N/A WATER COLUMN (ft)Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)WELL VOLUME
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE N/A
N/A SAMPLING EQUIPMENT PERISTALTIC PUMP PURGE METHOD
TUBING DIAMETER (in)3/8 OD No Purge
MONITORING WELL INFORMATION
WELL DIAMETER (in)TOC ELEV (ft msl)N/A MIDDLE OF WETTED SCREEN (ft toc)
SCREEN LENGTH (ft)ELEV REF SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)GS ELEV (ft msl)PUMP INTAKE DEPTH (ft TOC)N/A
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME SW-1
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR NO PURGE SAMPLING
0.00 0.00
(psi)(sec)(sec)
(gal)
(ft)=(in)@
QC By:
SAMPLING NOTES
PROTECTIVE CASING
WELL PAD
WELL CASING
WELL TAG
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
1110
230 7.97
0
N/A
Deployed Water Column In Screen
Above Top Of Hydrasleeve
NO PURGE SAMPLE CHLORINE
(mg/l)Top Weight SAMPLE COLLECTED BY DATE
(NTU)(mV-NHE)(mg/L)
N/A N/A N/A 20.89 121 7.34 12.3
TIME
LDC 6/13/2016
LENGTH DEPTH (top)DEPLOYED COND.OXYGEN
(inches)(ft TOC)(deg C)(umho/cm)(SU)
HYDRASLEEVE DEPLOYED DATE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
DETECTED ODOR CONVERSION FACTOR
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)N/A WATER COLUMN (ft)Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)WELL VOLUME
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE
N/A SAMPLING EQUIPMENT PERISTALTIC PUMP PURGE METHOD
TUBING DIAMETER (in)3/8 OD No Purge
MONITORING WELL INFORMATION
WELL DIAMETER (in)TOC ELEV (ft msl)N/A MIDDLE OF WETTED SCREEN (ft toc)
SCREEN LENGTH (ft)ELEV REF SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)GS ELEV (ft msl)PUMP INTAKE DEPTH (ft TOC)N/A
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME SW-2
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR NO PURGE SAMPLING
0.00 0.00
(psi)(sec)(sec)
(gal)
(ft)=(in)@
QC By:
Pipe discharge flow rate =0.25 gal / min
SAMPLING NOTES
PROTECTIVE CASING
WELL PAD
WELL CASING
WELL TAG
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
1145
307 7.07
0
N/A
Deployed Water Column In Screen
Above Top Of Hydrasleeve
NO PURGE SAMPLE CHLORINE
(mg/l)Top Weight SAMPLE COLLECTED BY DATE
(NTU)(mV-NHE)(mg/L)
N/A N/A N/A 22.12 1393 7.26 9.5
TIME
LDC 6/13/2016
LENGTH DEPTH (top)DEPLOYED COND.OXYGEN
(inches)(ft TOC)(deg C)(umho/cm)(SU)
HYDRASLEEVE DEPLOYED DATE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
DETECTED ODOR CONVERSION FACTOR
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)N/A WATER COLUMN (ft)Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)WELL VOLUME
SCREEN LENGTH (ft)ELEV REF SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)GS ELEV (ft msl)PUMP INTAKE DEPTH (ft TOC)N/A
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE
N/A SAMPLING EQUIPMENT GRAB
MONITORING WELL INFORMATION
WELL DIAMETER (in)TOC ELEV (ft msl)N/A MIDDLE OF WETTED SCREEN (ft toc)
TUBING DIAMETER (in)No Purge
PURGE METHOD
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jun-2016 WELL/LOCATION NAME LEACHATE POND
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR NO PURGE SAMPLING
PERMIT #
MW-5 MW-5A MW-6 MW-6A MW-7 MW-7A MW-8 MW-8A MW-9 MW-9A MW-10A SW-1 SW-2
YES YES YES YES YES YES YES YES YES YES YES YES YES
SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE
SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE SEE NOTE
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
NORTH CAROLINA GROUNDWATER SAMPLING SITE CHECKLIST
LOCATION / SITE McGUIRE NUCLEAR STATION - LANDFILL #2 GROUNDWATER MONITORING 60-04 SAMPLE DATE June 13, 2016
SITE CONTACT John Williamson FIELD CREW LDC, PSP
WEATHER Clear, calm, 70 to 85 deg F.
WELL LOCK CONDITION
PAGE 1 OF 1
ACCESS TO WELLS
Access cleared into well
Access cleared around well
Tall grass or weeds - needs mowing
Road washing out / muddy / needs grading
Fallen tree blocking access
WELL SECURITY
Well found locked
Well found unlocked
Undermined / washing out
Lock in good condition
Lock rusted, difficult to open / needs replacing
Replaced damaged lock
WELL CASINGS
Casing in good condition
Damaged casing / still functional
Damaged casing / repair required
CONCRETE PADS
Pad in good condition
Minor cracks
Major cracks / broken / repair required
Replaced damaged well cap
Fire ants around concrete pad
WELL PROTECTIVE CASINGS
Casing in good condition
Damaged casing / still functional
Damaged casing / repair required
Broken hinge on protective lid
Wasp nest inside protective casing
Ants inside protective casing
WELL CAPS
Well cap in good conditon
Damaged / needs replacement
Lacks required information - Completion date
FLUSH MOUNT WELLS
Vault in good condition
Water inside vault
Vault bolt holes broken or stripped
Bolts stripped
Vault lid cracked or broken
WELL ID TAGS
Well tag in good condition
Well tag missing
Well tag damaged / illegible
Lacks required information - Driller Reg #
Lacks required information - Total well depth
Lacks required information - Depth to screen
Lacks required information - Non potable tag
NOTE:Grass was very tall around all locations.
WELL DEPTH TO WATER Purge AVG *WELL EVAC SPECIFIC
WELL DEPTH WATER ELEV.Method PMP RATE VOL VOL EVAC TEMP CONDUCTANCE pH TURBIDITY ORP DO
DATE NO.(feet-toc)(feet-toc)(feet)APPEARANCE ODOR (ml/min)(gal)(gal)(yes/no)(deg C)(umho/cm)(units)(NTU)(mV-NHE)(mg/l)
6/13/2016 MW-5 63.90 60.87 707.44 Normal None C N/A 0.49 0.50 YES 19.80 15 5.4 4.3 412 10.39
6/13/2016 MW-5A 96.00 61.63 706.79 Normal None C N/A 5.61 17.25 NO 16.47 56 6.4 0.5 420 8.42
6/13/2016 MW-6 37.20 30.27 698.18 Normal None C N/A 1.13 6.25 NO 16.34 114 5.9 2.2 386 6.67
6/13/2016 MW-6A 47.90 29.54 699.44 Normal None C N/A 2.99 10.00 NO 16.34 56 5.5 0.6 389 8.15
6/13/2016 MW-7 37.30 32.91 692.95 Normal None EOP N/A 0.72 0.34 N/A 19.42 38 5.9 17.4 365 8.89
6/13/2016 MW-7A 59.40 31.86 692.80 Normal None C N/A 4.49 13.50 NO 16.65 120 6.5 3.8 365 6.62
6/13/2016 MW-8 71.50 61.79 697.81 Normal None EOP N/A 1.58 0.54 N/A 16.60 123 6.3 16.0 N/A N/A
6/13/2016 MW-8A 84.40 61.76 697.92 Normal None C N/A 3.69 11.25 NO 16.06 94 6.7 2.2 356 7.97
6/13/2016 MW-9 30.80 24.17 687.70 Normal None C N/A 1.08 6.25 NO 18.69 74 5.7 3.1 400 3.89
6/13/2016 MW-9A 47.80 24.51 687.62 Normal None C N/A 3.80 16.00 NO 17.79 103 6.4 3.4 374 4.77
6/13/2016 MW-10A 59.23 50.87 704.91 Normal None C N/A 1.36 6.00 NO 16.66 25 5.5 3.8 407 7.58
6/13/2016 SW-1 N/A N/A N/A Normal None NP N/A N/A N/A N/A 21.07 117 7.4 20.8 200 7.69
6/13/2016 SW-2 N/A N/A N/A Normal None NP N/A N/A N/A N/A 20.89 121 7.3 12.3 230 7.97
6/13/2016 LEACHATE POND N/A N/A N/A Normal None NP N/A N/A N/A N/A 22.12 1393 7.3 9.5 307 7.07
Purge Methods
LF = Low Flow
LF(M) = Low Flow (Mod.)
C = Connventional
NP = No Purge
EOP = Equip. Only Purge
LO = Level Only
* = Applicable to LF & LF(M) Purging Only
McGUIRE NUCLEAR STATION
LANDFILL 2 GROUNDWATER MONITORING
GROUNDWATER MONITORING FIELD DATA
PERMIT #60-04
B
Appendix B
Laboratory Report and
Chain-of-Custody Forms
13339 Hagers Ferry RoadHuntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J16060002
Project Name:MCGUIRE - GW LF2
Lab Contact: Anne Pridgeon
Date:6/29/2016
Customer Address:13225 Hagers Ferry Rd
Customer Name(s):TIM HUNSUCKER, CHUCK CAMPBELL
Mail Code: MG01CH
Huntersville, NC 28078-8985
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Method 8260: Please note that sample volume for volatile analysis was preserved with HCl which degrades constituents that are
sensitive to acid including Acrylonitrile.
Method 8015: Surrogate failure for Leachate Pond and associated matrix spike/spike duplicate samples was attributed to matrix
interference.
LCS associated with 8015 prep batch recovered slightly low for C10-C28. Due to limited volume, reanalysis was not performed however data has been qualified.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis, Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods.
Anne Pridgeon
Duke Energy Analytical Lab
Page 1 of 88
Reason: I have reviewed this
document.
Date: 2016.06.29 17:40:07
-04'00'
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection Date and Time Collected By Sample Description
2016015534 MCGUIRE 13-Jun-16 5:10 AM PSP TRIP BLANK
2016015535 MCGUIRE 13-Jun-16 9:40 AM PSP MW-5
2016015536 MCGUIRE 13-Jun-16 10:05 AM PSP MW-5A
2016015537 MCGUIRE 13-Jun-16 7:05 AM PSP MW-6
2016015538 MCGUIRE 13-Jun-16 7:15 AM PSP MW-6A
2016015539 MCGUIRE 13-Jun-16 8:15 AM LDC MW-7
2016015540 MCGUIRE 13-Jun-16 8:45 AM LDC MW-7A
2016015541 MCGUIRE 13-Jun-16 6:35 AM LDC MW-8
2016015542 MCGUIRE 13-Jun-16 7:30 AM LDC MW-8A
2016015543 MCGUIRE 13-Jun-16 10:30 AM LDC MW-9
2016015544 MCGUIRE 13-Jun-16 10:15 AM LDC MW-9A
2016015545 MCGUIRE 13-Jun-16 8:35 AM PSP MW-10A
2016015546 MCGUIRE 13-Jun-16 11:30 AM PSP SW-1
2016015547 MCGUIRE 13-Jun-16 11:10 AM LDC SW-2
2016015548 MCGUIRE 13-Jun-16 11:45 AM LDC LEACHATE POND
2016015549 MCGUIRE 13-Jun-16 11:45 AM LDC QC - WELL #
2016015550 MCGUIRE 13-Jun-16 12:00 PM PSP FIELD BLANK
17 Total Samples
Duke Energy Analytical Lab
Page 2 of 88
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:Anne Pridgeon Date:6/29/2016
Electronic Data Deliverable (EDD) Sent Separatel
Duke Energy Analytical Lab
Page 3 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015534
Collection Date:13-Jun-16 5:10 AM
Site:TRIP BLANK
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 4 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015535
Collection Date:13-Jun-16 9:40 AM
Site:MW-5
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)< 5 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride 1.3 mg/L EPA 9056A 06/14/2016 13:16 BGN90340.1 1
Sulfate 0.84 mg/L EPA 9056A 06/14/2016 13:16 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:16 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.014 mg/L SW 6010D 06/16/2016 13:29 JJMACKE0.005 1
Calcium (Ca)0.847 mg/L SW 6010D 06/16/2016 13:29 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 13:29 JJMACKE0.005 1
Magnesium (Mg)0.709 mg/L SW 6010D 06/16/2016 13:29 JJMACKE0.005 1
Potassium (K)0.668 mg/L SW 6010D 06/16/2016 13:29 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 13:29 JJMACKE0.005 1
Sodium (Na)0.711 mg/L SW 6010D 06/16/2016 13:29 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 19:18 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 19:18 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 19:18 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 19:18 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
GROs Complete Vendor Method V_T. America
DROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 5 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015536
Collection Date:13-Jun-16 10:05 AM
Site:MW-5A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)24 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride 1.4 mg/L EPA 9056A 06/14/2016 13:33 BGN90340.1 1
Sulfate 1.8 mg/L EPA 9056A 06/14/2016 13:33 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:18 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.025 mg/L SW 6010D 06/16/2016 13:40 JJMACKE0.005 1
Calcium (Ca)3.75 mg/L SW 6010D 06/16/2016 13:40 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 13:40 JJMACKE0.005 1
Magnesium (Mg)1.78 mg/L SW 6010D 06/16/2016 13:40 JJMACKE0.005 1
Potassium (K)0.896 mg/L SW 6010D 06/16/2016 13:40 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 13:40 JJMACKE0.005 1
Sodium (Na)4.79 mg/L SW 6010D 06/16/2016 13:40 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 19:04 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 19:04 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 19:04 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 19:04 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
GROs Complete Vendor Method V_T. America
DROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 6 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015537
Collection Date:13-Jun-16 7:05 AM
Site:MW-6
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)43 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride 11 mg/L EPA 9056A 06/14/2016 14:24 BGN90340.2 2
Sulfate 0.39 mg/L EPA 9056A 06/14/2016 14:24 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:21 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.053 mg/L SW 6010D 06/16/2016 13:44 JJMACKE0.005 1
Calcium (Ca)11.2 mg/L SW 6010D 06/16/2016 13:44 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 13:44 JJMACKE0.005 1
Magnesium (Mg)4.74 mg/L SW 6010D 06/16/2016 13:44 JJMACKE0.005 1
Potassium (K)0.574 mg/L SW 6010D 06/16/2016 13:44 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 13:44 JJMACKE0.005 1
Sodium (Na)4.52 mg/L SW 6010D 06/16/2016 13:44 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 19:22 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 19:22 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 19:22 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 19:22 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 7 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015538
Collection Date:13-Jun-16 7:15 AM
Site:MW-6A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)10 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride 5.5 mg/L EPA 9056A 06/14/2016 14:07 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 9056A 06/14/2016 14:07 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:40 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.051 mg/L SW 6010D 06/16/2016 13:48 JJMACKE0.005 1
Calcium (Ca)4.46 mg/L SW 6010D 06/16/2016 13:48 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 13:48 JJMACKE0.005 1
Magnesium (Mg)1.49 mg/L SW 6010D 06/16/2016 13:48 JJMACKE0.005 1
Potassium (K)0.241 mg/L SW 6010D 06/16/2016 13:48 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 13:48 JJMACKE0.005 1
Sodium (Na)3.82 mg/L SW 6010D 06/16/2016 13:48 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 19:27 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 19:27 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 19:27 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 19:27 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 8 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015539
Collection Date:13-Jun-16 8:15 AM
Site:MW-7
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)14 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride 1.8 mg/L EPA 9056A 06/15/2016 13:10B2 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 9056A 06/15/2016 13:10 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:42 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.031 mg/L SW 6010D 06/16/2016 13:52 JJMACKE0.005 1
Calcium (Ca)2.54 mg/L SW 6010D 06/16/2016 13:52 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 13:52 JJMACKE0.005 1
Magnesium (Mg)2.19 mg/L SW 6010D 06/16/2016 13:52 JJMACKE0.005 1
Potassium (K)0.249 mg/L SW 6010D 06/16/2016 13:52 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 13:52 JJMACKE0.005 1
Sodium (Na)1.08 mg/L SW 6010D 06/16/2016 13:52 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 19:32 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 19:32 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 19:32 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 19:32 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 9 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015540
Collection Date:13-Jun-16 8:45 AM
Site:MW-7A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)63 mg/L
(CaCO3)
SM 2320B 06/14/2016 12:44 CJELLIO201
INORGANIC IONS BY IC
Chloride 1.4 mg/L EPA 9056A 06/15/2016 14:32B2 BGN90340.1 1
Sulfate 0.35 mg/L EPA 9056A 06/15/2016 14:32 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:45 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.005 mg/L SW 6010D 06/16/2016 13:56 JJMACKE0.005 1
Calcium (Ca)14.9 mg/L SW 6010D 06/16/2016 13:56 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 13:56 JJMACKE0.005 1
Magnesium (Mg)4.06 mg/L SW 6010D 06/16/2016 13:56 JJMACKE0.005 1
Potassium (K)0.470 mg/L SW 6010D 06/16/2016 13:56 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 13:56 JJMACKE0.005 1
Sodium (Na)4.15 mg/L SW 6010D 06/16/2016 13:56 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 19:51 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 19:51 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 19:51 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 19:51 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 10 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015541
Collection Date:13-Jun-16 6:35 AM
Site:MW-8
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)64 mg/L
(CaCO3)
SM 2320B 06/14/2016 12:44 CJELLIO201
INORGANIC IONS BY IC
Chloride 1.5 mg/L EPA 9056A 06/15/2016 14:49B2 BGN90340.1 1
Sulfate 0.60 mg/L EPA 9056A 06/15/2016 14:49 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:47 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.023 mg/L SW 6010D 06/16/2016 14:17 JJMACKE0.005 1
Calcium (Ca)15.6 mg/L SW 6010D 06/16/2016 14:17 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 14:17 JJMACKE0.005 1
Magnesium (Mg)3.36 mg/L SW 6010D 06/16/2016 14:17 JJMACKE0.005 1
Potassium (K)1.04 mg/L SW 6010D 06/16/2016 14:17 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 14:17 JJMACKE0.005 1
Sodium (Na)6.25 mg/L SW 6010D 06/16/2016 14:17 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 19:55 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 19:55 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 19:55 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 19:55 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 11 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015542
Collection Date:13-Jun-16 7:30 AM
Site:MW-8A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)45 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride 2.0 mg/L EPA 9056A 06/15/2016 15:06B2 BGN90340.1 1
Sulfate 0.95 mg/L EPA 9056A 06/15/2016 15:06 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:50 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.025 mg/L SW 6010D 06/16/2016 14:21 JJMACKE0.005 1
Calcium (Ca)9.87 mg/L SW 6010D 06/16/2016 14:21 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 14:21 JJMACKE0.005 1
Magnesium (Mg)3.21 mg/L SW 6010D 06/16/2016 14:21 JJMACKE0.005 1
Potassium (K)1.17 mg/L SW 6010D 06/16/2016 14:21 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 14:21 JJMACKE0.005 1
Sodium (Na)4.44 mg/L SW 6010D 06/16/2016 14:21 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 20:00 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 20:00 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 20:00 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 20:00 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 12 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015543
Collection Date:13-Jun-16 10:30 AM
Site:MW-9
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)30 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride 2.1 mg/L EPA 9056A 06/15/2016 15:23B2 BGN90340.1 1
Sulfate 0.32 mg/L EPA 9056A 06/15/2016 15:23 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:52 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.032 mg/L SW 6010D 06/16/2016 14:25 JJMACKE0.005 1
Calcium (Ca)6.25 mg/L SW 6010D 06/16/2016 14:25 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 14:25 JJMACKE0.005 1
Magnesium (Mg)2.80 mg/L SW 6010D 06/16/2016 14:25 JJMACKE0.005 1
Potassium (K)0.523 mg/L SW 6010D 06/16/2016 14:25 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 14:25 JJMACKE0.005 1
Sodium (Na)4.38 mg/L SW 6010D 06/16/2016 14:25 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 20:05 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 20:05 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 20:05 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 20:05 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 13 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015544
Collection Date:13-Jun-16 10:15 AM
Site:MW-9A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)50 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride 1.7 mg/L EPA 9056A 06/15/2016 15:40B2 BGN90340.1 1
Sulfate 0.24 mg/L EPA 9056A 06/15/2016 15:40 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:55 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.010 mg/L SW 6010D 06/16/2016 14:28 JJMACKE0.005 1
Calcium (Ca)10.4 mg/L SW 6010D 06/16/2016 14:28 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 14:28 JJMACKE0.005 1
Magnesium (Mg)4.52 mg/L SW 6010D 06/16/2016 14:28 JJMACKE0.005 1
Potassium (K)0.526 mg/L SW 6010D 06/16/2016 14:28 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 14:28 JJMACKE0.005 1
Sodium (Na)5.22 mg/L SW 6010D 06/16/2016 14:28 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 20:10 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 20:10 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 20:10 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 20:10 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 14 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015545
Collection Date:13-Jun-16 8:35 AM
Site:MW-10A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)5.6 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride 1.4 mg/L EPA 9056A 06/15/2016 15:57B2 BGN90340.1 1
Sulfate 0.54 mg/L EPA 9056A 06/15/2016 15:57 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 13:57 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.016 mg/L SW 6010D 06/16/2016 14:32 JJMACKE0.005 1
Calcium (Ca)1.24 mg/L SW 6010D 06/16/2016 14:32 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 14:32 JJMACKE0.005 1
Magnesium (Mg)1.06 mg/L SW 6010D 06/16/2016 14:32 JJMACKE0.005 1
Potassium (K)0.575 mg/L SW 6010D 06/16/2016 14:32 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 14:32 JJMACKE0.005 1
Sodium (Na)1.54 mg/L SW 6010D 06/16/2016 14:32 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 20:14 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 20:14 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 20:14 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 20:14 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
GROs Complete Vendor Method V_T. America
DROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 15 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015546
Collection Date:13-Jun-16 11:30 AM
Site:SW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)59 mg/L
(CaCO3)
SM 2320B 06/14/2016 12:44 CJELLIO201
INORGANIC IONS BY IC
Chloride 2.1 mg/L EPA 9056A 06/15/2016 16:14B2 BGN90340.1 1
Sulfate 1.0 mg/L EPA 9056A 06/15/2016 16:14 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 14:00 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.029 mg/L SW 6010D 06/16/2016 14:36 JJMACKE0.005 1
Calcium (Ca)11.6 mg/L SW 6010D 06/16/2016 14:36 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 14:36 JJMACKE0.005 1
Magnesium (Mg)4.62 mg/L SW 6010D 06/16/2016 14:36 JJMACKE0.005 1
Potassium (K)0.936 mg/L SW 6010D 06/16/2016 14:36 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 14:36 JJMACKE0.005 1
Sodium (Na)5.82 mg/L SW 6010D 06/16/2016 14:36 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 20:19 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 20:19 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 20:19 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 20:19 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 16 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015547
Collection Date:13-Jun-16 11:10 AM
Site:SW-2
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)59 mg/L
(CaCO3)
SM 2320B 06/14/2016 12:44 CJELLIO201
INORGANIC IONS BY IC
Chloride 2.3 mg/L EPA 9056A 06/15/2016 16:31B2 BGN90340.1 1
Sulfate 2.3 mg/L EPA 9056A 06/15/2016 16:31 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 14:50 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.026 mg/L SW 6010D 06/16/2016 14:40 JJMACKE0.005 1
Calcium (Ca)12.2 mg/L SW 6010D 06/16/2016 14:40 JJMACKE0.01 1
Chromium (Cr)0.005 mg/L SW 6010D 06/16/2016 14:40 JJMACKE0.005 1
Magnesium (Mg)4.70 mg/L SW 6010D 06/16/2016 14:40 JJMACKE0.005 1
Potassium (K)1.08 mg/L SW 6010D 06/16/2016 14:40 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 14:40 JJMACKE0.005 1
Sodium (Na)6.02 mg/L SW 6010D 06/16/2016 14:40 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 20:24 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 20:24 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 20:24 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 20:24 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 17 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015548
Collection Date:13-Jun-16 11:45 AM
Site:LEACHATE POND
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)400 mg/L
(CaCO3)
SM 2320B 06/14/2016 12:44 CJELLIO201
INORGANIC IONS BY IC
Chloride 180 mg/L EPA 9056A 06/15/2016 13:58B2 BGN9034220
Sulfate 68 mg/L EPA 9056A 06/15/2016 13:58 BGN9034220
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 14:55 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.110 mg/L SW 6010D 06/16/2016 14:44 JJMACKE0.005 1
Calcium (Ca)111 mg/L SW 6010D 06/16/2016 14:44 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 14:44 JJMACKE0.005 1
Magnesium (Mg)23.1 mg/L SW 6010D 06/16/2016 14:44 JJMACKE0.005 1
Potassium (K)14.5 mg/L SW 6010D 06/16/2016 14:44 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 14:44 JJMACKE0.005 1
Sodium (Na)124 mg/L SW 6010D 06/16/2016 14:44 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 20:28 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 20:28 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 20:28 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 20:28 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 18 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015549
Collection Date:13-Jun-16 11:45 AM
Site:QC - WELL #
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
GROs Complete Vendor Method V_T. America
DROs Complete Vendor Method V_T. America
Duke Energy Analytical Lab
Page 19 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
2016015550
Collection Date:13-Jun-16 12:00 PM
Site:FIELD BLANK
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)< 5 mg/L
(CaCO3)
SM 2320B 06/16/2016 10:26 CJELLIO51
INORGANIC IONS BY IC
Chloride < 0.1 mg/L EPA 9056A 06/15/2016 16:48B2 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 9056A 06/15/2016 16:48 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 06/23/2016 14:57 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)< 0.005 mg/L SW 6010D 06/16/2016 14:47 JJMACKE0.005 1
Calcium (Ca)< 0.01 mg/L SW 6010D 06/16/2016 14:47 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/16/2016 14:47 JJMACKE0.005 1
Magnesium (Mg)< 0.005 mg/L SW 6010D 06/16/2016 14:47 JJMACKE0.005 1
Potassium (K)< 0.1 mg/L SW 6010D 06/16/2016 14:47 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/16/2016 14:47 JJMACKE0.005 1
Sodium (Na)< 0.05 mg/L SW 6010D 06/16/2016 14:47 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/14/2016 20:33 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/14/2016 20:33 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/14/2016 20:33 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 06/14/2016 20:33 CWSPEN311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
DROs Complete Vendor Method V_T. America
GROs Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Qualifiers:
B2 Target analyte was detected in blank(s) at a concentration greater than ½ the reporting limit but less than the reporting limit. Analyte concentration in sample is valid and may be used for compliance purposes.
Duke Energy Analytical Lab
Page 20 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
Q16060366 ALK_FIX4.5 ALKALINITY (FIXED END POINT 4.5)
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 1
RPD
Parent Sample: J16060290 -- 2016016803
Alkalinity (mg/L CaCO3)0.0494mg/L (CaCO3)-1241
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3) 44.3 98.5mg/L (CaCO3)-12080143.6
Duke Energy Analytical Lab
Page 21 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
Q16060435 ALK_LL_Fix LOW LEVEL ALKALINITY (FIXED END POINT)
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 1
RPD
Parent Sample: J16060002 -- 2016015535
Alkalinity (mg/L CaCO3)1.7mg/L (CaCO3)-14.55
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3) 11.08 85.5mg/L (CaCO3)-1208019.47
Duke Energy Analytical Lab
Page 22 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
Q16060353 Dionex INORGANIC IONS BY IC
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Chloride 0.0259 mg/L -10.0259 0.1 < 1/2 RDL
Sulfate 0.0041 mg/L -10.0041 0.1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
IS # 1
% Recovery LCL UCLSpike
Chloride 6.48 5 107mg/L -1208016.48
Sulfate 8.55 5 101mg/L -1208018.55
Final QualifierDilMeasuredUnits:Parameter
ISD # 1
RPD% Recovery LCL UCLSpike
Chloride 6.46 5 107 0.278mg/L -1208016.46
Sulfate 8.54 5 101 0.222mg/L -1208018.54
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Chloride 5.28 5 106mg/L -1109015.28
Sulfate 5.1 5 102mg/L -1109015.1
Duke Energy Analytical Lab
Page 23 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
Q16060381 Dionex INORGANIC IONS BY IC
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Chloride 0.0535 mg/L -10.0535 0.1 > 1/2 RDL
Sulfate 0.0085 mg/L -10.0085 0.1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
IS # 1
% Recovery LCL UCLSpike
Chloride 6.48 5 93.2mg/L -1208016.48
Sulfate 5.05 5 99.8mg/L -1208015.05
Final QualifierDilMeasuredUnits:Parameter
ISD # 1
RPD% Recovery LCL UCLSpike
Chloride 6.5 5 93.6 0.415mg/L -1208016.5
Sulfate 5.05 5 99.9 0.0941mg/L -1208015.05
Final QualifierDilMeasuredUnits:Parameter
IS # 2
% Recovery LCL UCLSpike
Chloride 6.33 5 99.8mg/L -1208016.33
Sulfate 6.48 5 96.7mg/L -1208016.48
Final QualifierDilMeasuredUnits:Parameter
ISD # 2
RPD% Recovery LCL UCLSpike
Chloride 6.31 5 99.5 0.351mg/L -1208016.31
Sulfate 6.49 5 96.9 0.217mg/L -1208016.49
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Chloride 4.95 5 99mg/L -1208014.95
Sulfate 4.97 5 99.3mg/L -1208014.97
Duke Energy Analytical Lab
Page 24 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
Q16060655 HG 7470 MERCURY (COLD VAPOR) IN WATER
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Mercury (Hg) 0.018 ug/L -10.018 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
Blank # 2
RDL Relative Concentration
Mercury (Hg) 0.02 ug/L -10.02 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
Blank # 3
RDL Relative Concentration
Mercury (Hg) 0.022 ug/L -10.022 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
Blank # 4
RDL Relative Concentration
Mercury (Hg) 0.021 ug/L -10.021 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
IS # 1
% Recovery LCL UCLSpike
Mercury (Hg) 0.884 20 87ug/L -125752017.7
Final QualifierDilMeasuredUnits:Parameter
ISD # 1
RPD% Recovery LCL UCLSpike
Mercury (Hg) 0.892 20 87.8 0.916ug/L -2017.8
Final QualifierDilMeasuredUnits:Parameter
IS # 2
% Recovery LCL UCLSpike
Mercury (Hg) 0.929 100 90.6ug/L -1257510092.9
Final QualifierDilMeasuredUnits:Parameter
ISD # 2
RPD% Recovery LCL UCLSpike
Mercury (Hg) 0.93 100 90.7 0.0882ug/L -10093
Final QualifierDilMeasuredUnits:Parameter
IS # 3
% Recovery LCL UCLSpike
Mercury (Hg) 2.02 100 90ug/L -12575100203
Final QualifierDilMeasuredUnits:Parameter
ISD # 3
RPD% Recovery LCL UCLSpike
Mercury (Hg) 2 100 87.1 3.27ug/L -100200
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Mercury (Hg) 2 2 99.8ug/L -1158512
Final QualifierDilMeasuredUnits:Parameter
LCS # 2
% Recovery LCL UCLSpike
Mercury (Hg) 1.91 2 95.3ug/L -1158511.91
Duke Energy Analytical Lab
Page 25 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
Q16060655 HG 7470 MERCURY (COLD VAPOR) IN WATER
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
LCS # 3
% Recovery LCL UCLSpike
Mercury (Hg) 1.86 2 93.1ug/L -1158511.86
Duke Energy Analytical Lab
Page 26 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
Q16060357 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Barium (Ba) 0.000068 mg/L -10.000068 0.005 < 1/2 RDL
Calcium (Ca) 0.00193 mg/L -10.00193 0.01 < 1/2 RDL
Chromium (Cr) -0.000509 mg/L -1-0.000509 0.005 < 1/2 RDL
Magnesium (Mg) 0.000089 mg/L -10.000089 0.005 < 1/2 RDL
Potassium (K) 0.00139 mg/L -10.00139 0.1 < 1/2 RDL
Silver (Ag) -0.000357 mg/L -1-0.000357 0.005 < 1/2 RDL
Sodium (Na) 0.00106 mg/L -10.00106 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Barium (Ba) 5.05 5 101mg/L -1208015.05
Calcium (Ca) 4.82 5 96.4mg/L -1208014.82
Chromium (Cr) 4.86 5 97.2mg/L -1208014.86
Magnesium (Mg) 5.07 5 101mg/L -1208015.07
Potassium (K) 4.96 5 99.1mg/L -1208014.96
Silver (Ag) 0.509 0.5 102mg/L -1208010.509
Sodium (Na) 4.94 5 98.9mg/L -1208014.94
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16060002 -- 2016015535
Barium (Ba) 5.05 5 101mg/L -1257515.05
Calcium (Ca) 5.56 5 94.3mg/L -1257515.56
Chromium (Cr) 4.86 5 97.2mg/L -1257514.86
Magnesium (Mg) 5.75 5 101mg/L -1257515.75
Potassium (K) 5.58 5 98.2mg/L -1257515.58
Silver (Ag) 0.503 0.5 101mg/L -1257510.503
Sodium (Na) 5.68 5 99.4mg/L -1257515.68
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16060002 -- 2016015535
Barium (Ba) 5.08 5 101 0.574mg/L -1257515.08
Calcium (Ca) 5.61 5 95.2 0.887mg/L -1257515.61
Chromium (Cr) 4.89 5 97.7 0.533mg/L -1257514.89
Magnesium (Mg) 5.79 5 102 0.712mg/L -1257515.79
Potassium (K) 5.59 5 98.4 0.203mg/L -1257515.59
Silver (Ag) 0.507 0.5 101 0.678mg/L -1257510.507
Sodium (Na) 5.72 5 100 0.702mg/L -1257515.72
Duke Energy Analytical Lab
Page 27 of 88
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060002
Q16060359 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Arsenic (As) -0.0011 ug/L -1-0.0011 1 < 1/2 RDL
Cadmium (Cd) 0.0042 ug/L -10.0042 1 < 1/2 RDL
Lead (Pb) 0.0091 ug/L -10.0091 1 < 1/2 RDL
Selenium (Se) -0.0604 ug/L -1-0.0604 1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Arsenic (As) 48.8 50 97.7ug/L -12080148.8
Cadmium (Cd) 49 50 98ug/L -12080149
Lead (Pb) 48.7 50 97.5ug/L -12080148.7
Selenium (Se) 48.8 50 97.6ug/L -12080148.8
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16060002 -- 2016015536
Arsenic (As) 48.8 50 97.1ug/L -12080148.8
Cadmium (Cd) 49 50 97.9ug/L -12080149
Lead (Pb) 48.3 50 96.5ug/L -12080148.3
Selenium (Se) 47.7 50 95.3ug/L -12080147.7
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16060002 -- 2016015536
Arsenic (As) 48.7 50 96.9 0.228ug/L -12080148.7
Cadmium (Cd) 49.1 50 98.2 0.239ug/L -12080149.1
Lead (Pb) 48.2 50 96.4 0.182ug/L -12080148.2
Selenium (Se) 47.6 50 95.2 0.113ug/L -12080147.6
Duke Energy Analytical Lab
Page 28 of 88
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-105735-1
Client Project/Site: MNS Landfill #2 J16060002
For:
Duke Energy Corporation
13339 Hagers Ferry Road
Huntersville, North Carolina 28078
Attn: Lab Customer
Authorized for release by:
6/27/2016 3:07:12 PM
Shali Brown, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J16060002
TestAmerica Job ID: 490-105735-1
Page 2 of 59 TestAmerica Nashville6/27/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .48
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .54
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59
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Duke Energy Analytical Lab
Page 87 of 88
Duke Energy Analytical Lab Page 88 of 88
13339 Hagers Ferry RoadHuntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J16060006
Project Name:MCGUIRE -
Lab Contact: Anne Pridgeon
Date:7/5/2016
Customer Address:13225 Hagers Ferry Rd
Customer Name(s):TIM HUNSUCKER, CHUCK CAMPBELL
Mail Code: MG01CH
Huntersville, NC 28078-8985
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Anne Pridgeon) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results) under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods.
Anne Pridgeon
Duke Energy Analytical Lab
Page 1 of 8
Reason: I have reviewed this
document.
Date: 2016.07.05 11:22:11
-04'00'
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection Date and Time Collected By Sample Description
2016015553 MCGUIRE 13-Jun-16 11:30 AM PSP SW-1
2016015554 MCGUIRE 13-Jun-16 11:25 AM LDC SW-2
2 Total Samples
Duke Energy Analytical Lab
Page 2 of 8
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:Anne Pridgeon Date:6/30/2016
Electronic Data Deliverable (EDD) Sent Separatel
Duke Energy Analytical Lab
Page 3 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060006
2016015553
Collection Date:13-Jun-16 11:30 AM
Site:SW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP
Barium (Ba)0.024 mg/L SW 6010D 06/27/2016 13:48 JJMACKE0.005 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/27/2016 13:48 JJMACKE0.005 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/27/2016 13:48 JJMACKE0.005 1
DISSOLVED METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/20/2016 12:32 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/20/2016 12:32 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/20/2016 12:32 CWSPEN311
Duke Energy Analytical Lab
Page 4 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060006
2016015554
Collection Date:13-Jun-16 11:25 AM
Site:SW-2
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP
Barium (Ba)0.020 mg/L SW 6010D 06/27/2016 14:08 JJMACKE0.005 1
Chromium (Cr)< 0.005 mg/L SW 6010D 06/27/2016 14:08 JJMACKE0.005 1
Silver (Ag)< 0.005 mg/L SW 6010D 06/27/2016 14:08 JJMACKE0.005 1
DISSOLVED METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 06/20/2016 12:46 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 06/20/2016 12:46 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 06/20/2016 12:46 CWSPEN311
Duke Energy Analytical Lab
Page 5 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060006
Q16060759 ICP Dissolved DISSOLVED METALS BY ICP
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Barium (Ba) -0.000123 mg/L -1-0.000123 0.005 < 1/2 RDL
Chromium (Cr) -0.000371 mg/L -1-0.000371 0.005 < 1/2 RDL
Silver (Ag) -0.000328 mg/L -1-0.000328 0.005 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Barium (Ba) 0.98 1 98mg/L -1158510.98
Chromium (Cr) 1 1 100mg/L -1158511
Silver (Ag) 0.99 1 99mg/L -1158510.99
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16060006 -- 2016015553
Barium (Ba) 5.02 5 100mg/L -1307015.02
Chromium (Cr) 4.86 5 97.2mg/L -1307014.86
Silver (Ag) 0.549 0.5 110mg/L -1307010.549
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16060006 -- 2016015553
Barium (Ba) 5.02 5 99.9 0.04mg/L -1307015.02
Chromium (Cr) 4.85 5 97 0.288mg/L -1307014.85
Silver (Ag) 0.541 0.5 108 1.48mg/L -1307010.541
Duke Energy Analytical Lab
Page 6 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16060006
Q16060546 IMS Dissolved DISSOLVED METALS BY ICP-MS
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Arsenic (As) 79.8 80 99.8ug/L -12080179.8
Cadmium (Cd) 8.26 8 103ug/L -1208018.26
Lead (Pb) 80.8 80 101ug/L -12080180.8
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Arsenic (As) 47.5 50ug/L -12575147.5
Cadmium (Cd) 48.3 50ug/L -12575148.3
Lead (Pb) 47.7 50ug/L -12575147.7
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Arsenic (As) 47.6 50ug/L -13070147.6
Cadmium (Cd) 48.5 50ug/L -13070148.5
Lead (Pb) 48 50ug/L -13070148
Duke Energy Analytical Lab
Page 7 of 8
Duke Energy Analytical Lab Page 8 of 8
Radiological Data for MCGUIRE
413558Sample #:Station:MCGUIRE
Collection End: 6/13/2016 09:40:00
Collection Start:6/13/2016 09:40:00Location:MNS_MW-5 [ MNS Landfill 2 / MW-5 ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-4.4E-03 0.00E+00 8.89E-01
Beta 1.20E+00 7.67E-01 1.24E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.12E+00 0.00E+00 5.12E+00 <1000 LLD OK<15
Co-58 <4.37E+00 0.00E+00 4.37E+00 <1000 LLD OK<15
Fe-59 <1.32E+01 0.00E+00 1.32E+01 <400 LLD OK<30
Co-60 <7.64E+00 0.00E+00 7.64E+00 <300 LLD OK<15
Zn-65 <1.17E+01 0.00E+00 1.17E+01 <300 LLD OK<30
Zr-95 <9.52E+00 0.00E+00 9.52E+00 <400 LLD OK<15
Nb-95 <5.99E+00 0.00E+00 5.99E+00 <400 LLD OK<15
I-131 <5.99E+00 0.00E+00 5.99E+00 LLD OK<15
Cs-134 <6.22E+00 0.00E+00 6.22E+00 <30 LLD OK<15
Cs-137 <5.22E+00 0.00E+00 5.22E+00 <50 LLD OK<18
BaLa-140 <6.44E+00 0.00E+00 6.44E+00 <200 LLD OK<15
Be-7 <4.30E+01 0.00E+00 4.30E+01
K-40 8.90E+01 6.14E+01 8.89E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-5.3E+01 0.00E+00 2.03E+02 <20000 LLD OK<250
413559Sample #:Station:MCGUIRE
Collection End: 6/13/2016 10:05:00
Collection Start:6/13/2016 10:05:00Location:MNS_MW-5A [ MNS Landfill 2 / MW-5A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-3.3E-01 0.00E+00 9.99E-01
Beta 1.59E+00 7.94E-01 1.26E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.44E+00 0.00E+00 5.44E+00 <1000 LLD OK<15
Co-58 <4.04E+00 0.00E+00 4.04E+00 <1000 LLD OK<15
Fe-59 <8.43E+00 0.00E+00 8.43E+00 <400 LLD OK<30
Page 1 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 1 of 12 06.30.2016
Radiological Data for MCGUIRE
413559Sample #:Station:MCGUIRE
Collection End: 6/13/2016 10:05:00
Collection Start:6/13/2016 10:05:00Location:MNS_MW-5A [ MNS Landfill 2 / MW-5A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <5.42E+00 0.00E+00 5.42E+00 <300 LLD OK<15
Zn-65 <1.02E+01 0.00E+00 1.02E+01 <300 LLD OK<30
Zr-95 <9.02E+00 0.00E+00 9.02E+00 <400 LLD OK<15
Nb-95 <6.49E+00 0.00E+00 6.49E+00 <400 LLD OK<15
I-131 <4.11E+00 0.00E+00 4.11E+00 LLD OK<15
Cs-134 <4.89E+00 0.00E+00 4.89E+00 <30 LLD OK<15
Cs-137 <6.36E+00 0.00E+00 6.36E+00 <50 LLD OK<18
BaLa-140 <6.85E+00 0.00E+00 6.85E+00 <200 LLD OK<15
Be-7 <4.68E+01 0.00E+00 4.68E+01
K-40 <9.74E+01 0.00E+00 9.74E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-1.1E+02 0.00E+00 2.01E+02 <20000 LLD OK<250
413560Sample #:Station:MCGUIRE
Collection End: 6/13/2016 07:05:00
Collection Start:6/13/2016 07:05:00Location:MNS_MW-6 [ MNS Landfill 2 / MW-6 ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-4.3E-01 0.00E+00 1.16E+00
Beta 1.40E+00 8.10E-01 1.30E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.70E+00 0.00E+00 6.70E+00 <1000 LLD OK<15
Co-58 <6.27E+00 0.00E+00 6.27E+00 <1000 LLD OK<15
Fe-59 <1.04E+01 0.00E+00 1.04E+01 <400 LLD OK<30
Co-60 <6.70E+00 0.00E+00 6.70E+00 <300 LLD OK<15
Zn-65 <1.24E+01 0.00E+00 1.24E+01 <300 LLD OK<30
Zr-95 <8.13E+00 0.00E+00 8.13E+00 <400 LLD OK<15
Nb-95 <6.41E+00 0.00E+00 6.41E+00 <400 LLD OK<15
I-131 <5.30E+00 0.00E+00 5.30E+00 LLD OK<15
Cs-134 <6.89E+00 0.00E+00 6.89E+00 <30 LLD OK<15
Cs-137 <6.21E+00 0.00E+00 6.21E+00 <50 LLD OK<18
BaLa-140 <8.97E+00 0.00E+00 8.97E+00 <200 LLD OK<15
Page 2 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 2 of 12 06.30.2016
Radiological Data for MCGUIRE
413560Sample #:Station:MCGUIRE
Collection End: 6/13/2016 07:05:00
Collection Start:6/13/2016 07:05:00Location:MNS_MW-6 [ MNS Landfill 2 / MW-6 ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.92E+01 0.00E+00 4.92E+01
K-40 <1.07E+02 0.00E+00 1.07E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-1.0E+02 0.00E+00 2.05E+02 <20000 LLD OK<250
413561Sample #:Station:MCGUIRE
Collection End: 6/13/2016 07:15:00
Collection Start:6/13/2016 07:15:00Location:MNS_MW-6A [ MNS Landfill 2 / MW-6A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-4.8E-02 0.00E+00 9.71E-01
Beta 1.04E+00 7.67E-01 1.26E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.82E+00 0.00E+00 4.82E+00 <1000 LLD OK<15
Co-58 <5.40E+00 0.00E+00 5.40E+00 <1000 LLD OK<15
Fe-59 <9.66E+00 0.00E+00 9.66E+00 <400 LLD OK<30
Co-60 <6.89E+00 0.00E+00 6.89E+00 <300 LLD OK<15
Zn-65 <1.21E+01 0.00E+00 1.21E+01 <300 LLD OK<30
Zr-95 <9.69E+00 0.00E+00 9.69E+00 <400 LLD OK<15
Nb-95 <6.05E+00 0.00E+00 6.05E+00 <400 LLD OK<15
I-131 <5.09E+00 0.00E+00 5.09E+00 LLD OK<15
Cs-134 <6.55E+00 0.00E+00 6.55E+00 <30 LLD OK<15
Cs-137 <5.87E+00 0.00E+00 5.87E+00 <50 LLD OK<18
BaLa-140 <6.29E+00 0.00E+00 6.29E+00 <200 LLD OK<15
Be-7 <4.60E+01 0.00E+00 4.60E+01
K-40 4.90E+01 5.24E+01 8.34E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-8.1E+01 0.00E+00 2.05E+02 <20000 LLD OK<250
Page 3 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 3 of 12 06.30.2016
Radiological Data for MCGUIRE
413562Sample #:Station:MCGUIRE
Collection End: 6/13/2016 08:15:00
Collection Start:6/13/2016 08:15:00Location:MNS_MW-7 [ MNS Landfill 2 / MW-7 ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <2.97E-01 0.00E+00 9.39E-01
Beta 7.65E-01 7.54E-01 1.25E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.08E+00 0.00E+00 5.08E+00 <1000 LLD OK<15
Co-58 <6.94E+00 0.00E+00 6.94E+00 <1000 LLD OK<15
Fe-59 <9.89E+00 0.00E+00 9.89E+00 <400 LLD OK<30
Co-60 <6.03E+00 0.00E+00 6.03E+00 <300 LLD OK<15
Zn-65 <1.11E+01 0.00E+00 1.11E+01 <300 LLD OK<30
Zr-95 <9.38E+00 0.00E+00 9.38E+00 <400 LLD OK<15
Nb-95 <4.66E+00 0.00E+00 4.66E+00 <400 LLD OK<15
I-131 <4.72E+00 0.00E+00 4.72E+00 LLD OK<15
Cs-134 <5.71E+00 0.00E+00 5.71E+00 <30 LLD OK<15
Cs-137 <6.31E+00 0.00E+00 6.31E+00 <50 LLD OK<18
BaLa-140 <6.10E+00 0.00E+00 6.10E+00 <200 LLD OK<15
Be-7 <3.11E+01 0.00E+00 3.11E+01
K-40 8.09E+01 4.12E+01 4.20E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-8.7E+01 0.00E+00 2.04E+02 <20000 LLD OK<250
413563Sample #:Station:MCGUIRE
Collection End: 6/13/2016 08:45:00
Collection Start:6/13/2016 08:45:00Location:MNS_MW-7A [ MNS Landfill 2 / MW-7A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-5.5E-01 0.00E+00 1.20E+00
Beta 1.52E+00 8.21E-01 1.31E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.14E+00 0.00E+00 6.14E+00 <1000 LLD OK<15
Co-58 <5.41E+00 0.00E+00 5.41E+00 <1000 LLD OK<15
Fe-59 <9.36E+00 0.00E+00 9.36E+00 <400 LLD OK<30
Page 4 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 4 of 12 06.30.2016
Radiological Data for MCGUIRE
413563Sample #:Station:MCGUIRE
Collection End: 6/13/2016 08:45:00
Collection Start:6/13/2016 08:45:00Location:MNS_MW-7A [ MNS Landfill 2 / MW-7A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <6.37E+00 0.00E+00 6.37E+00 <300 LLD OK<15
Zn-65 <9.91E+00 0.00E+00 9.91E+00 <300 LLD OK<30
Zr-95 <8.74E+00 0.00E+00 8.74E+00 <400 LLD OK<15
Nb-95 <5.21E+00 0.00E+00 5.21E+00 <400 LLD OK<15
I-131 <5.62E+00 0.00E+00 5.62E+00 LLD OK<15
Cs-134 <5.94E+00 0.00E+00 5.94E+00 <30 LLD OK<15
Cs-137 <6.02E+00 0.00E+00 6.02E+00 <50 LLD OK<18
BaLa-140 <6.11E+00 0.00E+00 6.11E+00 <200 LLD OK<15
Be-7 <4.39E+01 0.00E+00 4.39E+01
K-40 7.90E+01 5.90E+01 8.76E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-6.1E+01 0.00E+00 2.05E+02 <20000 LLD OK<250
413564Sample #:Station:MCGUIRE
Collection End: 6/13/2016 06:35:00
Collection Start:6/13/2016 06:35:00Location:MNS_MW-8 [ MNS Landfill 2 / MW-8 ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-2.3E-01 0.00E+00 1.22E+00
Beta 1.49E+00 8.26E-01 1.32E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.98E+00 0.00E+00 4.98E+00 <1000 LLD OK<15
Co-58 <4.67E+00 0.00E+00 4.67E+00 <1000 LLD OK<15
Fe-59 <8.35E+00 0.00E+00 8.35E+00 <400 LLD OK<30
Co-60 <4.80E+00 0.00E+00 4.80E+00 <300 LLD OK<15
Zn-65 <1.36E+01 0.00E+00 1.36E+01 <300 LLD OK<30
Zr-95 <8.58E+00 0.00E+00 8.58E+00 <400 LLD OK<15
Nb-95 <5.65E+00 0.00E+00 5.65E+00 <400 LLD OK<15
I-131 <5.63E+00 0.00E+00 5.63E+00 LLD OK<15
Cs-134 <6.16E+00 0.00E+00 6.16E+00 <30 LLD OK<15
Cs-137 <7.72E+00 0.00E+00 7.72E+00 <50 LLD OK<18
BaLa-140 <6.07E+00 0.00E+00 6.07E+00 <200 LLD OK<15
Page 5 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 5 of 12 06.30.2016
Radiological Data for MCGUIRE
413564Sample #:Station:MCGUIRE
Collection End: 6/13/2016 06:35:00
Collection Start:6/13/2016 06:35:00Location:MNS_MW-8 [ MNS Landfill 2 / MW-8 ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.15E+01 0.00E+00 4.15E+01
K-40 <1.00E+02 0.00E+00 1.00E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-4.6E+01 0.00E+00 2.06E+02 <20000 LLD OK<250
413565Sample #:Station:MCGUIRE
Collection End: 6/13/2016 07:30:00
Collection Start:6/13/2016 07:30:00Location:MNS_MW-8A [ MNS Landfill 2 / MW-8A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-6.2E-01 0.00E+00 1.12E+00
Beta 1.88E+00 8.23E-01 1.29E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.09E+00 0.00E+00 5.09E+00 <1000 LLD OK<15
Co-58 <5.23E+00 0.00E+00 5.23E+00 <1000 LLD OK<15
Fe-59 <1.09E+01 0.00E+00 1.09E+01 <400 LLD OK<30
Co-60 <8.08E+00 0.00E+00 8.08E+00 <300 LLD OK<15
Zn-65 <1.12E+01 0.00E+00 1.12E+01 <300 LLD OK<30
Zr-95 <8.04E+00 0.00E+00 8.04E+00 <400 LLD OK<15
Nb-95 <7.09E+00 0.00E+00 7.09E+00 <400 LLD OK<15
I-131 <5.68E+00 0.00E+00 5.68E+00 LLD OK<15
Cs-134 <6.15E+00 0.00E+00 6.15E+00 <30 LLD OK<15
Cs-137 <6.02E+00 0.00E+00 6.02E+00 <50 LLD OK<18
BaLa-140 <7.68E+00 0.00E+00 7.68E+00 <200 LLD OK<15
Be-7 <4.97E+01 0.00E+00 4.97E+01
K-40 8.51E+01 5.44E+01 7.56E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-4.6E+01 0.00E+00 2.06E+02 <20000 LLD OK<250
Page 6 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 6 of 12 06.30.2016
Radiological Data for MCGUIRE
413566Sample #:Station:MCGUIRE
Collection End: 6/13/2016 10:30:00
Collection Start:6/13/2016 10:30:00Location:MNS_MW-9 [ MNS Landfill 2 / MW-9 ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-1.5E-01 0.00E+00 1.05E+00
Beta 1.47E+00 7.97E-01 1.27E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.14E+00 0.00E+00 6.14E+00 <1000 LLD OK<15
Co-58 <5.18E+00 0.00E+00 5.18E+00 <1000 LLD OK<15
Fe-59 <9.60E+00 0.00E+00 9.60E+00 <400 LLD OK<30
Co-60 <4.42E+00 0.00E+00 4.42E+00 <300 LLD OK<15
Zn-65 <1.01E+01 0.00E+00 1.01E+01 <300 LLD OK<30
Zr-95 <7.00E+00 0.00E+00 7.00E+00 <400 LLD OK<15
Nb-95 <5.37E+00 0.00E+00 5.37E+00 <400 LLD OK<15
I-131 <5.60E+00 0.00E+00 5.60E+00 LLD OK<15
Cs-134 <5.15E+00 0.00E+00 5.15E+00 <30 LLD OK<15
Cs-137 <4.93E+00 0.00E+00 4.93E+00 <50 LLD OK<18
BaLa-140 <9.80E+00 0.00E+00 9.80E+00 <200 LLD OK<15
Be-7 <4.60E+01 0.00E+00 4.60E+01
K-40 <9.01E+01 0.00E+00 9.01E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <2.58E+01 0.00E+00 2.02E+02 <20000 LLD OK<250
413567Sample #:Station:MCGUIRE
Collection End: 6/13/2016 10:15:00
Collection Start:6/13/2016 10:15:00Location:MNS_MW-9A [ MNS Landfill 2 / MW-9A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-5.9E-01 0.00E+00 1.17E+00
Beta 1.23E+00 8.03E-01 1.31E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.14E+00 0.00E+00 6.14E+00 <1000 LLD OK<15
Co-58 <6.09E+00 0.00E+00 6.09E+00 <1000 LLD OK<15
Fe-59 <1.16E+01 0.00E+00 1.16E+01 <400 LLD OK<30
Page 7 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 7 of 12 06.30.2016
Radiological Data for MCGUIRE
413567Sample #:Station:MCGUIRE
Collection End: 6/13/2016 10:15:00
Collection Start:6/13/2016 10:15:00Location:MNS_MW-9A [ MNS Landfill 2 / MW-9A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <5.05E+00 0.00E+00 5.05E+00 <300 LLD OK<15
Zn-65 <9.43E+00 0.00E+00 9.43E+00 <300 LLD OK<30
Zr-95 <7.87E+00 0.00E+00 7.87E+00 <400 LLD OK<15
Nb-95 <5.54E+00 0.00E+00 5.54E+00 <400 LLD OK<15
I-131 <5.85E+00 0.00E+00 5.85E+00 LLD OK<15
Cs-134 <6.92E+00 0.00E+00 6.92E+00 <30 LLD OK<15
Cs-137 <5.33E+00 0.00E+00 5.33E+00 <50 LLD OK<18
BaLa-140 <4.82E+00 0.00E+00 4.82E+00 <200 LLD OK<15
Be-7 <4.13E+01 0.00E+00 4.13E+01
K-40 3.97E+01 4.87E+01 7.92E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <7.88E+00 0.00E+00 2.01E+02 <20000 LLD OK<250
413568Sample #:Station:MCGUIRE
Collection End: 6/13/2016 08:35:00
Collection Start:6/13/2016 08:35:00Location:MNS_MW-10A [ MNS Landfill 2 / MW-10A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-2.9E-01 0.00E+00 8.95E-01
Beta 8.58E-01 7.50E-01 1.24E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.80E+00 0.00E+00 5.80E+00 <1000 LLD OK<15
Co-58 <5.75E+00 0.00E+00 5.75E+00 <1000 LLD OK<15
Fe-59 <1.17E+01 0.00E+00 1.17E+01 <400 LLD OK<30
Co-60 <5.26E+00 0.00E+00 5.26E+00 <300 LLD OK<15
Zn-65 <1.05E+01 0.00E+00 1.05E+01 <300 LLD OK<30
Zr-95 <1.13E+01 0.00E+00 1.13E+01 <400 LLD OK<15
Nb-95 <6.43E+00 0.00E+00 6.43E+00 <400 LLD OK<15
I-131 <6.48E+00 0.00E+00 6.48E+00 LLD OK<15
Cs-134 <5.25E+00 0.00E+00 5.25E+00 <30 LLD OK<15
Cs-137 <5.16E+00 0.00E+00 5.16E+00 <50 LLD OK<18
BaLa-140 <7.18E+00 0.00E+00 7.18E+00 <200 LLD OK<15
Page 8 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 8 of 12 06.30.2016
Radiological Data for MCGUIRE
413568Sample #:Station:MCGUIRE
Collection End: 6/13/2016 08:35:00
Collection Start:6/13/2016 08:35:00Location:MNS_MW-10A [ MNS Landfill 2 / MW-10A ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.38E+01 0.00E+00 4.38E+01
K-40 1.53E+02 6.39E+01 7.42E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-5.9E+01 0.00E+00 2.02E+02 <20000 LLD OK<250
413569Sample #:Station:MCGUIRE
Collection End: 6/13/2016 11:30:00
Collection Start:6/13/2016 11:30:00Location:MNS_SW-1 [ MNS Landfill 2 / SW-1 ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-1.7E-01 0.00E+00 1.21E+00
Beta 1.81E+00 8.38E-01 1.32E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.34E+00 0.00E+00 4.34E+00 <1000 LLD OK<15
Co-58 <4.99E+00 0.00E+00 4.99E+00 <1000 LLD OK<15
Fe-59 <1.12E+01 0.00E+00 1.12E+01 <400 LLD OK<30
Co-60 <4.97E+00 0.00E+00 4.97E+00 <300 LLD OK<15
Zn-65 <1.21E+01 0.00E+00 1.21E+01 <300 LLD OK<30
Zr-95 <5.35E+00 0.00E+00 5.35E+00 <400 LLD OK<15
Nb-95 <4.60E+00 0.00E+00 4.60E+00 <400 LLD OK<15
I-131 <4.96E+00 0.00E+00 4.96E+00 LLD OK<15
Cs-134 <4.89E+00 0.00E+00 4.89E+00 <30 LLD OK<15
Cs-137 <5.52E+00 0.00E+00 5.52E+00 <50 LLD OK<18
BaLa-140 <6.28E+00 0.00E+00 6.28E+00 <200 LLD OK<15
Be-7 <3.70E+01 0.00E+00 3.70E+01
K-40 <9.30E+01 0.00E+00 9.30E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <3.95E+00 0.00E+00 2.01E+02 <20000 LLD OK<250
Page 9 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 9 of 12 06.30.2016
Radiological Data for MCGUIRE
413570Sample #:Station:MCGUIRE
Collection End: 6/13/2016 11:10:00
Collection Start:6/13/2016 11:10:00Location:MNS_SW-2 [ MNS Landfill 2 / SW-2 ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-6.7E-01 0.00E+00 1.20E+00
Beta 1.92E+00 8.39E-01 1.32E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.51E+00 0.00E+00 6.51E+00 <1000 LLD OK<15
Co-58 <5.56E+00 0.00E+00 5.56E+00 <1000 LLD OK<15
Fe-59 <1.06E+01 0.00E+00 1.06E+01 <400 LLD OK<30
Co-60 <6.84E+00 0.00E+00 6.84E+00 <300 LLD OK<15
Zn-65 <1.14E+01 0.00E+00 1.14E+01 <300 LLD OK<30
Zr-95 <9.65E+00 0.00E+00 9.65E+00 <400 LLD OK<15
Nb-95 <4.58E+00 0.00E+00 4.58E+00 <400 LLD OK<15
I-131 <5.33E+00 0.00E+00 5.33E+00 LLD OK<15
Cs-134 <5.41E+00 0.00E+00 5.41E+00 <30 LLD OK<15
Cs-137 <5.13E+00 0.00E+00 5.13E+00 <50 LLD OK<18
BaLa-140 <8.60E+00 0.00E+00 8.60E+00 <200 LLD OK<15
Be-7 <4.02E+01 0.00E+00 4.02E+01
K-40 5.43E+01 4.21E+01 5.96E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-9.4E+01 0.00E+00 2.00E+02 <20000 LLD OK<250
413571Sample #:Station:MCGUIRE
Collection End: 6/13/2016 11:45:00
Collection Start:6/13/2016 11:45:00Location:MNS_LEACHP [ MNS Landfill 2 / Leachate Pond ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-4.1E-01 0.00E+00 2.47E+00
Beta 1.12E+01 1.96E+00 2.95E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.91E+00 0.00E+00 5.91E+00 <1000 LLD OK<15
Co-58 <4.39E+00 0.00E+00 4.39E+00 <1000 LLD OK<15
Fe-59 <6.45E+00 0.00E+00 6.45E+00 <400 LLD OK<30
Page 10 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 10 of 12 06.30.2016
Radiological Data for MCGUIRE
413571Sample #:Station:MCGUIRE
Collection End: 6/13/2016 11:45:00
Collection Start:6/13/2016 11:45:00Location:MNS_LEACHP [ MNS Landfill 2 / Leachate Pond ( LANDFILL ) ]
MNS_2JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <5.85E+00 0.00E+00 5.85E+00 <300 LLD OK<15
Zn-65 <1.36E+01 0.00E+00 1.36E+01 <300 LLD OK<30
Zr-95 <9.42E+00 0.00E+00 9.42E+00 <400 LLD OK<15
Nb-95 <4.51E+00 0.00E+00 4.51E+00 <400 LLD OK<15
I-131 <5.27E+00 0.00E+00 5.27E+00 LLD OK<15
Cs-134 <4.25E+00 0.00E+00 4.25E+00 <30 LLD OK<15
Cs-137 <6.21E+00 0.00E+00 6.21E+00 <50 LLD OK<18
BaLa-140 <6.77E+00 0.00E+00 6.77E+00 <200 LLD OK<15
Be-7 <4.27E+01 0.00E+00 4.27E+01
K-40 <1.07E+02 0.00E+00 1.07E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW 1.93E+03 1.62E+02 2.04E+02 <20000 LLD OK<250
Page 11 of 11Report Generated @ 6/30/2016 06:13:15
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 11 of 12 06.30.2016
EnRad Laboratory Page 12 of 12 06.30.2016