1701-MSWLF-1985_CaswellCountyLandfill_GWMReport_DIN26485_20160502

Caswell County Landfill – Permit 17-01
Semi-Annual Water Quality Monitoring
May 2016 Sampling Event
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
Prepared for:
Caswell County
Post Office Box 98
144 Court Square
Yanceyville, North Carolina 27379
Prepared by:
S&ME, Inc.
8646 W Market St, Suite 105
Greensboro, NC 27409
June 1, 2016
S&ME, Inc. | 8646 W Market St, Ste 105 | Greensboro, NC 27409 | p 336.288.7180 | f 336.288.8980 | www.smeinc.com
June 1, 2016
Caswell County
Post Office Box 98
144 Court Square
Yanceyville, North Carolina 27379
Attention:Tim Smith
Reference:Semi-Annual Monitoring Report – May 2016 Event
Caswell County Landfill, Permit No. 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
Dear Mr. Smith:
S&ME Inc. (S&ME) has completed the first semi-annual monitoring event for 2016 at the closed Caswell
County Landfill site. The monitoring activities were authorized by Caswell County, County Manager, Mr.
Bryan Miller and were completed in general accordance with S&ME proposal 43-1600164 dated February
16, 2016. This report summarizes our understanding of the project, our field services, and the results of
laboratory analyses performed on the samples collected. If you have any questions regarding this
document, and our associated findings and recommendations; please contact Edmund Henriques at your
convenience.
Sincerely,
S&ME, Inc.
Edmund Q.B. Henriques Amanda Bloom
Project Manager / Senior Geologist Staff Professional
NC Licensed Geologist No. 1216
Semi-Annual Monitoring Report – May 2016 Event
Caswell County Landfill, Permit No. 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
June 1, 2016 ii
Table of Contents
1.0 Executive Summary...............................................................................................1
2.0 Introduction............................................................................................................1
3.0 Scope Of Work.......................................................................................................2
4.0 Methods Employed...............................................................................................2
4.1 Monitoring Well Sampling..............................................................................................2
4.2 Surface Water Sampling..................................................................................................3
5.0 Results......................................................................................................................3
5.1 Groundwater Analytical Results....................................................................................3
5.2 Surface Water Analytical Results...................................................................................4
5.3 Groundwater Flow Direction..........................................................................................4
5.4 Quality Assurance............................................................................................................5
5.5 Preliminary Analysis of Cause and Significance of 2L Exceedances ........................5
6.0 References...............................................................................................................6
Appendices
Tables...................................................................................................................................................................ii
Figures............................................................................................................................................................... iii
Appendix I – Groundwater Sampling Field Data Sheets........................................................................... iv
Appendix II – Laboratory Analytical Reports ...............................................................................................v
Appendix III – NC DENR Electronic Data Deliverables............................................................................ vi
Semi-Annual Monitoring Report – May 2016 Event
Caswell County Landfill, Permit No. 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
June 1, 2016 1
1.0 Executive Summary
Six monitoring wells at the Caswell County Landfill were sampled on May 2, 2016. The six wells (MW-1,
MW-2, MW-3, MW-4, MW-5, and MW-6) comprise the groundwater monitoring system for the closed
Caswell County Landfill. This sampling event was conducted in general accordance with North Carolina
Solid Waste Management Guidelines. Samples collected from monitoring wells MW-1, MW-2, MW-3,
MW-4, MW-5, and MW-6 and surface water samples SW-1 and SW-2 were submitted for analysis of the
North Carolina Landfill Appendix I volatile organic constituents plus eight RCRA Metals. The samples were
analyzed by PACE Analytical Services, Inc. of Huntersville, North Carolina, a North Carolina certified
laboratory.
Analytical results of the six groundwater samples report that none of the 8-RCRA metals were detected at
concentrations greater than the corresponding 15A North Carolina Administrative Code (NCAC) 2L.0200
groundwater quality standards (2L Standard) during this event.
The volatile organic constituent benzene was detected in monitoring well MW-5 at a concentration equal
to the corresponding 2L Standard of 1 µg/L. Volatile organic constituent 1,4-dichlorobenzene was
detected in the groundwater samples collected from wells MW-2, MW-4, and MW-5 at concentrations
greater than the corresponding 2L Standard of 6 µg/L. During this event, no other volatile organic
compounds were detected in the monitoring wells sampled at concentrations greater than the
corresponding 2L Standards.
During this monitoring event, no targeted volatile organic constituents were detected at concentrations
greater than the method detection limit in either of the two stream sample locations. Barium was
detected in up-gradient background surface water sample SW-1 and down-gradient sample SW-2 at
similar concentrations. The reported concentrations are below their respective 15A NCAC 2B Surface
Water Standard for Class C surface waters. There were no other metals detected above the method
detection limit in the surface water samples collected during this sampling event.
It is believed that the cause of the 2L Standards exceedances for Benzene and 1,4-Dichlorobenzene at the
Caswell County Landfill is from percolation of landfill constituents from the waste management units into
the uppermost groundwater aquifer. Due to the detection of these exceedances above the 2L Standards
in the compliance wells, S&ME recommends that a water supply well receptor survey be completed for
the Caswell County Landfill and the development of an assessment plan to address the 2L Standards
exceedances in accordance with regulatory requirements.
2.0 Introduction
S&ME Inc. (S&ME) has completed the first semi-annual monitoring event for 2016 at the closed Caswell
County Landfill site. The monitoring activities were authorized by County Manager, Mr. Bryan Miller and
were completed in general accordance with S&ME proposal 43-1600164 dated February 16, 2016. This
report summarizes our understanding of the project, our field services, and the results of laboratory
analyses performed on the samples collected.
Semi-Annual Monitoring Report – May 2016 Event
Caswell County Landfill, Permit No. 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
June 1, 2016 2
The Caswell County Landfill (Permit No. 17-01) is a closed facility that currently monitors water quality
under a Post Closure Care Plan on a semi-annual basis. The facility uses a network of six (6) groundwater
monitoring wells to monitor groundwater quality at the Facility. The groundwater monitoring network is
made up of one up-gradient monitoring well (MW-1) and five down-gradient compliance monitoring
wells (MW-2, MW-3, MW-4, MW-5, and MW-6). The collected groundwater samples are analyzed in
accordance with 15A NCAC 13B .0500 et seq for the North Carolina Landfill Appendix I volatile organic
constituent suite plus the eight RCRA metals. Groundwater monitoring wells were purged and
groundwater samples were collected using new, disposable, Teflon bailers, or a sterile pump with new
Teflon tubing.
The facility also typically monitors surface water quality at the stream that crosses the down-gradient
region of the Facility. As conditions allow, during each semi-annual monitoring event, two surface water
samples are collected from this stream at designated sampling points. Stream sampling location SW-1 is
the upstream sampling location to the south of the waste management unit. Stream sampling location
SW-2 is the downstream sampling location. During the May 2, 2016 sampling event, stream samples were
collected from both surface water monitoring points SW-1 and SW-2.
This report discusses the field procedures, summarizes the field measurements and analytical results for
the first semi-annual water quality monitoring event for 2016.
3.0 Scope Of Work
S&ME has performed the first semi-annual groundwater sampling of the six (6) network groundwater
monitoring wells for the 2016 groundwater monitoring year. The groundwater monitoring wells were
purged, sampled, and the groundwater samples collected from MW-1 through MW-6 were analyzed (in
accordance with 15A NCAC 13B .0500 et seq) for the North Carolina Appendix I volatile organic
constituents and the eight RCRA metals. This semi-annual groundwater monitoring report has been
prepared to summarize the May 2, 2016, groundwater monitoring event and includes:
♦Summary Tables of the laboratory analytical data from each sampling event,
♦Development of a current potentiometric map,
♦A discussion of findings and results,
♦An electronic copy of this report will be sent to the North Carolina Department of Environmental
Quality (NC DEQ)
4.0 Methods Employed
4.1 Monitoring Well Sampling
Groundwater monitoring well sampling took place on May 2, 2016. The monitoring well locations with
respect to the Facility layout are shown on Figure 1. Prior to sample collection each well was opened and
the static water level measured relative to the top edge of the PVC well casing. The total well depth was
used to determine the volume of water in the wells at the time of sampling. These data are summarized
in Table 1 and Table 2.
Semi-Annual Monitoring Report – May 2016 Event
Caswell County Landfill, Permit No. 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
June 1, 2016 3
Monitor wells MW-1, MW-2 and MW-4 were manually purged using a new, sterile Teflon bailer prior to
collecting the water samples. Each well was purged of up to three times the well volume or purged until
the well went dry prior to the collection of the groundwater sample. The bailer was lowered, by hand,
using a nylon rope into the well in such a manner as to minimize agitation of the groundwater. The purge
water from each of these wells was monitored for pH, conductivity, and temperature. Table 2 provides a
summary of the measured field parameters.
Monitor wells MW-3, MW-5, and MW-6 were purged and sampled using a peristaltic pump. New Teflon
tubing was used at each well. Each well was purged of up to three times the well volume or purged until
the well was dry prior to the collection of the groundwater sample. The purge water from each of these
wells was monitored for pH, conductivity, and temperature. The field data collected during sampling was
recorded on the groundwater sampling field data sheets included in Appendix I of this report.
Immediately upon collection, each groundwater sample was placed in laboratory supplied containers,
place in a cooler with ice, and placed under chain-of custody. The sampling technician wore nitrile gloves
that were changed between wells to reduce the possibility of cross contamination.
All monitoring well samples were then sent to PACE Analytical Services, Inc. (PACE) in Huntersville, North
Carolina to be analyzed for Appendix I volatile organic constituents and the eight RCRA metals.
4.2 Surface Water Sampling
Surface water sampling took place on May 2, 2016. Two stream samples (SW-1 and SW-2) were collected
from an unnamed tributary of Bear Branch, which flows along the eastern portion of the Facility and flows
toward the north away from the Landfill. Surface water sample (SW-1) was collected from an upstream
position with respect to the waste management unit and SW-2 was collected downstream of the waste
management unit. The surface water samples were collected by immersing laboratory supplied containers
directly into the stream at the locations to be sampled. After collection, the surface water samples were
placed in a cooler with ice and placed under chain-of-custody. All stream samples were analyzed for the
North Carolina Appendix I volatile organic constituents as well as the 8 RCRA metals by PACE Analytical
Services, Inc.; a North Carolina certified laboratory.
5.0 Results
The following sections provide a discussion of the groundwater and surface water sampling results for the
May 2, 2016, semi-annual monitoring event. The laboratory analytical report is included in Appendix II.
Appendix III contains a CD with the field and analytical laboratory data provided in the NCDEQ electronic
data deliverable (EDD) format.
5.1 Groundwater Analytical Results
The results of the laboratory analyses for the groundwater monitoring well samples are summarized in
Table 3, which also provides the corresponding 15A North Carolina Administrative Code (NCAC) 2L.0200
groundwater quality standards (2L Standard) for reference. Table 4 provides a summary of the
constituents detected at concentrations greater than their respective 2L Standards. The following
summarizes the groundwater sample analyses for the six monitoring wells (MW-1, MW-2, MW-3, MW-4,
MW-5, and MW-6) sampled on May 2, 2016.
Semi-Annual Monitoring Report – May 2016 Event
Caswell County Landfill, Permit No. 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
June 1, 2016 4
Metals (8-RCRA):
♦Arsenic was detected in the sample collected from monitoring well MW-4 at a concentration less than
the corresponding 2L Standard.
♦Barium was detected in the samples collected from monitoring wells MW-1 through MW-6 at a
concentrations less than the corresponding 2L Standard.
♦Lead was detected in the sample collected from monitoring well MW-4 at a concentration less than
the corresponding 2L Standard.
There were no other metals detected above the method detection limit from any other groundwater
monitoring wells during the May 2, 2016, monitoring event. The analytical results for the detected metals
(totals) are summarized in Table 3.
Volatile Organic Compounds:
♦Benzene was detected in the groundwater samples collected from monitoring wells MW-2, MW-
3, MW-4, and MW-5. The reported concentrations in wells MW-2, MW-3, ad MW-4 were less
than the corresponding 2L Standard. The concentration reported in well MW-5 was equal to the
2L Standard of 1 µg/L for benzene.
♦1,4-Dichlorobenzene was detected in the groundwater samples collected from wells MW-2, MW-
3, MW-4, and MW-5. The concentrations reported at wells MW-2, MW-4, and MW-5 are greater
than the 2L Standard established at 6 µg/L.
♦Chlorobenzene, 1,2-dichlorobenzene, 1,1-dichloroethane, cis 1,2-dichloroethene, 2-hexanone,
toluene, and xylenes (total) were detected in one or more groundwater samples during this
monitoring event; however, each of the reported concentrations of these constituents were less
than their respective 2L Standard. An estimated concentration of O-xylenes was detected in the
Trip Blank sample that accompanied this sampling event. No other volatile organic compounds
were detected in the monitoring wells sampled during this event.
5.2 Surface Water Analytical Results
There were no volatile organic constituents detected above the method detection limits in the stream
samples SW-1 or SW-2 during the May 2, 2016, semi-annual monitoring event. The metal barium was
detected in samples SW-1 and SW-2, at similar concentrations. The reported concentrations are below
the respective 15A NCAC 2B Surface Water Standard for barium for Class C surface waters. There were no
other metals detected above the method detection limit in the surface water samples collected during this
sampling event. The results of the surface water sample analyses are summarized on Table 5 and Table 6.
5.3 Groundwater Flow Direction
The static water levels in the monitoring wells were measured on May 2, 2016. On this date, the depths to
the water table ranged from 6.67 feet below top of well casing at MW-6 to 21.33 feet below the top of
well casing at MW-4. Groundwater elevation data are presented in Table 1. Ground surface elevations
were taken from surface topography illustrated on Plan Sheet No. 3 of the Caswell County Landfill Closure
Plans prepared by Dewberry and Davis in March 1994. The groundwater elevation at each monitoring well
was approximated by taking the difference of the ground surface elevation (topography) and the depth to
static water in each monitoring well. A groundwater contour map was constructed using the calculated
Semi-Annual Monitoring Report – May 2016 Event
Caswell County Landfill, Permit No. 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
June 1, 2016 5
groundwater elevation data from the May 2, 2016, sampling event and is presented as Figure 2. The
groundwater elevation data collected during this monitoring event indicates that the groundwater
beneath the landfill generally flows easterly toward the unnamed tributary of Bear Branch.
5.4 Quality Assurance
A qualitative review of the data was performed to verify that the detected concentrations in the laboratory
report were of known quality. A formal, quantitative data validation was not performed. Laboratory-
assigned data qualifiers were evaluated to verify that rejected or unsupportable data were not included in
the dataset. Quality control data provided in the laboratory reports were also reviewed. No rejected or
otherwise unacceptable quality data were reported from the laboratory.
During this event a duplicate sample was collected from monitoring well MW-1 and the sample was
analyzed for the Appendix I Volatile Organic Compounds and the 8-RCRA metals. Barium was the only
target constituent detected in the duplicate sample. The detected barium concentrations in the sample
identified as MW-1 and the duplicate sample show very good correlation. A Trip Blank accompanied the
sample kit during shipment, sample collection, and shipment of the collected samples back to the
laboratory. The Trip Blank sample was analyzed for Appendix I Volatile Organic Compounds. No target
compounds were detected except for xylenes (total) at an estimated concentration of 0.26 ug/L. Similar
estimated concentrations of xylenes (total) were detected in samples MW-2, MW-4 and MW-5 during the
May 2, 2016 sampling event. The results of the duplicate, trip blank, and laboratory QC sample analyses
are included in Appendix II.
5.5 Preliminary Analysis of Cause and Significance of 2L Exceedances
It is believed that the cause of the 2L Standard exceedances reported for benzene and 1,4-
dichlorobenzene within the hydrogeologic regime at the Caswell County Landfill is caused from
percolation of landfill constituents from the waste management units into the uppermost groundwater
aquifer.
Previously, S&ME reviewed the 2000 aerial photograph of the Caswell County Landfill and surrounding
vicinity as a preliminary analysis of the proximity of potential receptor water well users to the compliance
monitoring wells in which 2L Standard exceedances occurred during the July 2010 groundwater
monitoring event. Based on the aerial photograph for the year 2000, the nearest suspect residential home
is located approximately 900 feet northeast of compliance monitoring well MW-5, which is the furthest
down-gradient monitoring well on the landfill side of the unnamed tributary of Bear Branch. The observed
suspect residential homes are topographically up-gradient and on the other side of the unnamed
tributary of Bear Branch from the Caswell County Landfill. At this time, S&ME has no information
regarding the current use of groundwater as a potable water source for these homes or the availability of
public water in the vicinity of the landfill.
Due to the detection of exceedances of the 2L Standard in the compliance wells, S&ME recommends that
a detailed water supply well receptor survey be completed for the Caswell County Landfill and the
development of an assessment plan to address the regulatory requirements associated with the 2L
Standard exceedances.
Semi-Annual Monitoring Report – May 2016 Event
Caswell County Landfill, Permit No. 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
June 1, 2016 6
6.0 References
Fetter, C. W., 1988, Applied Hydrogeology, New York; Macmillian Publishing Company, 1988, 592 pp.
North Carolina Administrative Code, Title 15A, Department of Environment, Health and Natural Resources,
Division of Environmental Management, Subchapter 2L, Classifications and Water Quality Standards
Applicable to the Groundwaters of North Carolina, Sections .0100, .0200, and .0300; from the
Environmental Management Commission Raleigh, North Carolina.
North Carolina Administrative Code, Title 15A, Department of Environment, Health and Natural Resources,
Division of Environmental Management, Subchapter 2B, Classifications and Water Quality Standards
Applicable to the Surface Waters of North Carolina, Section .0200; from the Environmental Management
Commission, Raleigh, North Carolina.
North Carolina Administrative Code, Title 15A, Department of Environment, Health and Natural Resources,
Division of Solid Waste Management, subchapter 13B, Solid Waste Management, Section .1600.
Appendices
Tables
TABLE 2
SUMMARY OF GROUNDWATER SAMPLING FIELD PARAMETERS
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
DATE WELL WELL DEPTH TO WATER ODOR PURGE PUMP WELL EVAC PURGED TEMP pH SPECIFIC
ID DEPTH WATER ELEVATION METHOD RATE VOLUME VOLUME DRY?CONDUCTANCE
(feet)(feet)(feet)(mL/min)(gallons)(gallons)(yes/no)(deg C)(SU)(μs/cm)
5/2/2016 MW-1 24.5 16.75 557.25 None bailer NA 1.26 4 No 16.50 6.33 801.0
5/2/2016 MW-2 22.3 17.62 510.38 None bailer NA 0.76 0.5 Yes 14.90 6.34 1400.0
5/2/2016 MW-3 17.8 9.20 503.80 None pump 100 1.40 1 No 15.00 6.00 686.0
5/2/2016 MW-4 36 21.33 506.07 None bailer NA 2.39 5 Yes 15.30 6.35 1428.0
5/2/2016 MW-5 24.7 8.18 491.92 None pump 200 2.69 2.5 No 17.50 6.60 1067.0
5/2/2016 MW-6 16.2 6.67 484.43 None pump 200 1.55 1.5 No 14.70 6.30 80.0
Notes:
1. TEMP = groundwater temperature, measured in degrees Celsius
2. Pump Rate, measured in milliliters/minute
3. Specific Conductance, measured in μs/cm indicates micro Siemens per centimeter.
4. SU indicates Standard Units.
5. EVAC = evacuated volume of groundwater
6. NA = not applicable
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
NC SWSL Report NCAC 2L NCDENR Federal
Well ID MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 Duplicate Limit Standards IMAC MCLs
Sample ID 1701-MW1 1701-MW2 1701-MW3 1701-MW4 1701-MW5 1701-MW61701-Duplicate
Date Collected 05/02/16 05/02/16 05/02/16 05/02/16 05/02/16 05/02/16 05/02/16
Detected Analytes (ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)
16 Benzene <1.0 0.66 J 0.40 J 0.97 J 1.0 <1.0 <1.0 1 1.0 1 --5
39 Chlorobenzene <1.0 17.7 4.2 26.5 6.6 <1.0 <1.0 3 1.0 50 --100
69 1,2-Dichlorobenzene <1.0 1.5 0.38 J 2.3 2.0 <1.0 <1.0 5 1.0 20 --600
71 1,4-Dichlorobenzene <1.0 8.9 2.4 11.4 11.8 <1.0 <1.0 1 1.0 6 --75
75 1,1-Dichloroethane <1.0 <1.0 <1.0 <1.0 0.38 J <1.0 <1.0 5 1.0 6 --ns
78 cis-1,2-Dichloroethene <1.0 <1.0 <1.0 <1.0 0.55 J <1.0 <1.0 5 1.0 70 --700
124 2-Hexanone <5.0 <5.0 <5.0 0.99 J <5.0 <5.0 <5.0 50 5.0 ns 40 ns
196 Toluene <1.0 0.49 J <1.0 <1.0 <1.0 <1.0 <1.0 1 1.0 600 --1
346 Xylenes <3.0 0.27 J <3.0 0.31 J 0.26 J <3.0 <3.0 5 3.0 500 --10
NC SWSL Report NCAC 2L NCDENR Federal
Well ID MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 Duplicate Limit Standards IMAC MCLs
Sample ID 1701-MW1 1701-MW2 1701-MW3 1701-MW4 1701-MW5 1701-MW61701-Duplicate
Date Collected 05/02/16 05/02/16 05/02/16 05/02/16 05/02/16 05/02/16 05/02/16
Detected Analytes (ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)
14 Arsenic <10.0 <10.0 <10.0 2.8 J <10.0 <10.0 <10.0 10 10 10 --ns
15 Barium 21.8 J 69.2J 64.3 J 50.1 J 46.3 J 8.9 J 21.9 J 100 10 700 --2,000
131 Lead <5.0 <5.0 <5.0 2.6 J <5.0 <5.0 <5.0 10 5 15 --ns
ug/L = concentrations reported in micrograms per liter (ug/L)
NC SWSL = North Carolina Solid Waste Section Limit
NCAC 2L Standards = 15A North Carolina Administrative Code 2L .0200, GW Quality Standards for Class GA groundwater.
concentrations in bold exceed the corresponding 2L Standard
NCDENR IMAC = Interim Maximum Allowed Concentration, NCDENR
Federal MCL = Maximum Concentration Levels, USEPA
ns = no MCL listed, USEPA
na = not analyzed
Solid
Waste
Section
ID #
Sample Locations
Sample Locations
TABLE 3
SUMMARY OF GROUNDWATER ANALYSES RESULTS - DETECTIONS
Appendix I Volatile Organic Compounds
Solid
Waste
Section
ID #
8-RCRA Metals
TABLE 4
SUMMARY OF GROUNDWATER STANDARD EXCEEDANCES
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
Well ID MW-2 MW-4 MW-5 NC SWSL NCAC 2L NCDENR Federal
Sample ID 1701-MW2 1701-MW4 1701-MW5 Standards IMAC MCLs
Date Collected 05/02/16 05/02/16 05/02/16
Detected Analytes (ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)
16 Benzene 1.0 1 1 --5
71 1,4-Dichlorobenzene 8.9 11.4 11.8 1 6 --75
ug/L = concentrations reported in micrograms per liter (ug/L)
NC SWSL = North Carolina Solid Waste Section Limit
NCAC 2L Standards = 15A North Carolina Administrative Code 2L .0200, GW Quality Standards
for Class GA groundwater.
Concentration greater than the NCAC 2L Standards are shown in bold
NCDENR IMAC = Interim Maximum Allowed Concentration, NCDENR
Federal MCL = Maximum Concentration Levels, USEPA
ns = no MCL listed, USEPA
na = not analyzed
Solid
Waste
Section
IDs
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
NC SWSL Report NCAC 2B
Sample Location SW-1 SW-2 Limit Standards
Sample ID 1701-SW1 1701-SW2
Date Collected 05/02/16 05/02/16
Detected Analytes (ug/L)(ug/L)(ug/L)(ug/L)(ug/L)
all target analytes < report limit < report limit analyte specific analyte specific analyte specific
NC SWSL Report NCAC 2B
Sample Location SW-1 SW-2 Limit Standards*
Sample ID 1701-SW1 1701-SW2
Date Collected 05/02/16 05/02/16
Detected Analytes (ug/L)(ug/L)(ug/L)(ug/L)(ug/L)
15 Barium 30.4 32.7 100 5.0 1000
ug/L = concentrations reported in micrograms per liter (ug/L)
NC SWSL = North Carolina Solid Waste Section Limit
8-RCRA Metals
Solid
Waste
Section
ID #
Sample Locations
TABLE 5
SUMMARY OF SURFACE WATER ANALYSES RESULTS - DETECTIONS
Appendix I Volatile Organic Compounds
Solid
Waste
Section
ID #
Sample Locations
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
Sample Location SW-1 SW-2 NC SWSL NCAC 2B
Sample ID 1701-SW1 1701-SW2 Standards*
Date Collected 05/02/16 05/02/16
Detected Analytes (ug/L)(ug/L)(ug/L)(ug/L)
ug/L = concentrations reported in micrograms per liter (ug/L)
NC SWSL = North Carolina Solid Waste Section Limit
No exceedances
Appendix I VOCs and 8-RCRA Metals
Solid
Waste
Section
IDs
TABLE 6
SUMMARY OF 2B SURFACE WATER STANDARD EXCEEDANCES
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3718 OLD BATTLEGROUND ROAD
GREENSBORO, NC. 27410
PH. 336-288-7180
FAX. [phone]
WWW.SMEINC.COM
SITE PLAN
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
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A
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D
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I
L
L

A
R
E
A
L
G
V
-
3
L
G
V
-
4
L
G
V
-
5
L
G
V
-
6
L
G
V
-
2
L
G
V
-
1
- APPROXIMATE LOCATION OF LANDFILL GAS VENTS
560570570570
5
6
0
55
0
540
530
5
2
0
5
1
0
5
0
0
4
9
0
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9
0
G
R
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A
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.
0
500
.
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0
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0
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0
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0
550.0
495
.
0
505.
0
515.
0
525.
0
535.
0
545.0555.0
JOB NO.
SCALE:
DATE:
DRAWN BY:CHECKED BY:
FIGURE NO.
3718 OLD BATTLEGROUND ROAD
GREENSBORO, NC. 27410
PH. 336-288-7180
FAX. [phone]
WWW.SMEINC.COM
GROUNDWATER CONTOUR MAP
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
AS SHOWN RDM EQBH
1584-07-034A MAY 2016 2
0
G
R
A
P
H
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=

1
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'
M
W
-
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-
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-
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-
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-
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(
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)
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(557.25)
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A
KEY- MONITORING WELL LOCATION- GROUNDWATER CONTOUR- GROUNDWATER ELEVATION MEASURED IN MONITORING WELL- GROUNDWATER FLOW DIRECTION (557.25)
Appendix I – Groundwater Sampling Field Data Sheets
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
7.75 feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
Note: Duplicate sample taken at this location. (0900)
2" well:
height:7.75 x .163 =1.26325
gallons x liters
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
1515 5/2/2016 16.10 6.23 797.000 1.00
1525 5/2/2016 16.50 6.33 801.000 1.00
Final Readings 1525 5/2/2016 16.50 6.33 801.000 1.00
* C units mS/cm mV mg/L NTU
Caswell County Landfill
1584-07-034A
1701-MW-1
Gary Simcox
Monday, May 02, 2016
Monday, May 02, 2016
Depth to well bottom from measuring point:24.50
Height of water column:
Bailer
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:16.75
1530
Sunny
Measuring point:Top of Casing
Well Purging & Sample Collection
Bailer Purge Time
80 *F
Sample Collection Time
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 2.0
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
4.68 feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
2" well:
height:4.68 x .163 =0.76284
gallons x liters
Yes x No
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
Final Readings 1000 5/2/2016 14.90 6.34 1400.000 2.00
* C units mS/cm mV mg/L
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 0.50
Bailer
Measuring point:Top of Casing
Well Purging & Sample Collection
Bailer Purge Time
Sample Collection Time
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:17.62
1000
Sunny
80*FGary Simcox
Depth to well bottom from measuring point:22.30
Height of water column:
Monday, May 02, 2016
Monday, May 02, 2016
Caswell County Landfill
1584-07-034A
1701-MW-2
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start 1015 Stop 1055
Purge Rate ml/min
Control Settings On:sec.Start 1055 Stop 1100
Off:sec.
Pressure:psi
2" well:
height:8.60 x .163 =1.4018
gallons liters x
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
1115 5/2/2016
1125 5/2/2016 16.20 6.10 702.00 1.00
1135 5/2/2016 15.40 6.07 685.00 1.00
1145 5/2/2016 15.40 6.01 687.00 1.00
1155 5/2/2016 15.00 6.00 686.00 1.00
Final Readings 1155 5/2/2016 15.00 6.00 686.00 1.00
* C units mS/cm mV mg/L
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:9.20
1200
Sunny
80 *F
Caswell County Landfill
1584-07-034A
1701-MW-3
Gary Simcox
Monday, May 02, 2016
Monday, May 02, 2016
Measuring point:Top of Casing
Well Purging & Sample Collection
Depth to well bottom from measuring point:17.80
Height of water column:8.60
Peristaltic Pump Purge Time
Peristaltic Pump
100 Sample Collection Time
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 4.0
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
2" well:
height:14.67 x .163 =2.39121
gallons x liters
Yes X No
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
1030 5/2/2016 16.40 6.23 1428.00 1.00
1040 5/2/2016 15.40 6.30 1419.00 1.00
1050 5/2/2016 15.30 6.35 1428.00 1.00
Final Readings 1050 5/2/2016 15.30 6.35 1428.00 1.00
* C units mS/cm mV mg/L
Height of water column:
Monday, May 02, 2016
14.67
Measuring point:Top of Casing
Depth to well bottom from measuring point:36.00
Field Analyses
Well Purging & Sample Collection
Bailer Purge Time
Volume of water in well
Volume of water removed 5.0
Was well purged dry
Sample Collection Time
Bailer
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:21.33
1100
Sunny
80*F
Caswell County Landfill
1584-07-034A
1701-MW-4
Gary Simcox
Monday, May 02, 2016
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start 1215 Stop 1255
Purge Rate ml/min
Control Settings On: 3.0 sec.Start 1255 Stop 1300
Off: 27.0 sec.
Pressure: 26 psi
2" well:
height:16.52 x .163 =2.69276
gallons liters x
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
1215 5/2/2016
1225 5/2/2016 18.00 6.75 1077.00 1.00
18 1235 5/2/2016 17.70 6.67 1067.00 2.00
1245 5/2/2016 17.40 6.62 1068.00 2.00
1255 5/2/2016 17.50 6.60 1067.00 2.00
Final Readings 1255 5/2/2016 17.50 6.60 1067.00 2.00
* C units mS/cm mV mg/L NTU
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:8.18
1300
Sunny
80 *F
Caswell County Landfill
1584-07-034A
1701-MW-5
Gary Simcox
Monday, May 02, 2016
Monday, May 02, 2016
Measuring point:Top of Casing
Well Purging & Sample Collection
Depth to well bottom from measuring point:24.70
Height of water column:16.52
Peristaltic Pump Purge Time
Peristaltic Pump
200 Sample Collection Time
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 10.0
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start 1325 Stop 1355
Purge Rate ml/min
Control Settings On:sec.Start 1355 Stop 1400
Off:sec.
Pressure:psi
2" well:
height:9.53 x .163 =1.55339
gallons liters x
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
1325 5/2/2016
1335 5/2/2016 15.00 6.45 83.00 1.00
1345 5/2/2016 14.70 6.31 81.00 2.00
1355 5/2/2016 14.70 6.30 80.00 2.00
Final Readings 1355 5/2/2016 14.70 6.30 80.00 2.00
* C units mS/cm mV mg/L
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:6.67
1400
Sunny
80 *F
Caswell County Landfill
1584-07-034A
1701-MW-6
Gary Simcox
Monday, May 02, 2016
Monday, May 02, 2016
Measuring point:Top of Casing
Well Purging & Sample Collection
Depth to well bottom from measuring point:16.20
Height of water column:9.53
Peristaltic Pump Purge Time
Peristaltic Pump
200 Sample Collection Time
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 5.0
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
2" well:
height:0 x .163 =0
gallons liters
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
Final Readings 1445 5/2/2016 20.90 7.04 112.000
* C units mS/cm mV mg/L NTU
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:
1445
Sunny
80 *F
Caswell County Landfill
1584-07-034A
1701-SW-1
Gary Simcox
Monday, May 02, 2016
Monday, May 02, 2016
Measuring point:
Well Purging & Sample Collection
Depth to well bottom from measuring point:
Height of water column:
Purge Time
Sample Collection Time
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
2" well:
height:0 x .163 =0
gallons liters x
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
Final Readings 1415 5/2/2016 20.10 7.26 117.000
* C units mS/cm mV mg/L NTU
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed
Measuring point:
Well Purging & Sample Collection
Purge Time
Sample Collection Time
Depth to well bottom from measuring point:
Monday, May 02, 2016
Height of water column:
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:
1415
Sunny
80 *F
Caswell County Landfill
1584-07-034A
1701-SW-2
Gary Simcox
Monday, May 02, 2016
Appendix II – Laboratory Analytical Reports
#=CL#
May 09, 2016
LIMS USE: FR - TIM SMITH
LIMS OBJECT ID: 92296128
92296128
Project:
Pace Project No.:
RE:
Tim Smith
Caswell County Landfill
162 Landfill Road
Yanceyville, NC 27379
CASWELL CO LF 1584-07-034A
Dear Tim Smith:
Enclosed are the analytical results for sample(s) received by the laboratory on May 03, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
cc:Mr. Ed Henriques, S&ME, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 29
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
Asheville Certification IDs2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 29
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92296128001 MW-1 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92296128002 MW-2 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92296128003 MW-3 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92296128004 MW-4 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92296128005 MW-5 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92296128006 MW-6 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92296128007 SW-1 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92296128008 SW-2 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92296128009 DUPLICATE EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92296128010 TRIP BLANK EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:MW-1 Lab ID:92296128001 Collected:05/02/16 15:30 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 06:15 7440-38-205/04/16 14:3010.0 1
Barium 21.8J ug/L 05/06/16 06:15 7440-39-305/04/16 14:301001
Cadmium ND ug/L 05/06/16 06:15 7440-43-905/04/16 14:301.0 1
Chromium ND ug/L 05/06/16 06:15 7440-47-305/04/16 14:305.0 1
Lead ND ug/L 05/06/16 06:15 7439-92-105/04/16 14:305.0 1
Selenium ND ug/L 05/06/16 06:15 7782-49-205/04/16 14:3010.0 1
Silver ND ug/L 05/06/16 06:15 7440-22-405/04/16 14:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/16 10:03 7439-97-605/04/16 16:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 17:39 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 17:39 107-13-110.0 1
Benzene ND ug/L 05/06/16 17:39 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 17:39 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 17:39 75-27-41.0 1
Bromoform ND ug/L 05/06/16 17:39 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 17:39 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 17:39 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 17:39 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/06/16 17:39 56-23-51.0 1
Chlorobenzene ND ug/L 05/06/16 17:39 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 17:39 75-00-31.0 1
Chloroform ND ug/L 05/06/16 17:39 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 17:39 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 17:39 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 17:39 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 17:39 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/06/16 17:39 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/06/16 17:39 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 17:39 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/06/16 17:39 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 17:39 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/06/16 17:39 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/06/16 17:39 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 17:39 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 17:39 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 17:39 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 17:39 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 17:39 100-41-41.0 1
2-Hexanone ND ug/L 05/06/16 17:39 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 17:39 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 17:39 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 17:39 108-10-15.0 1
Styrene ND ug/L 05/06/16 17:39 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 4 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:MW-1 Lab ID:92296128001 Collected:05/02/16 15:30 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 17:39 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 17:39 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 17:39 127-18-41.0 1
Toluene ND ug/L 05/06/16 17:39 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 17:39 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 17:39 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 17:39 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 17:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 17:39 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 17:39 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 17:39 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 17:39 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 17:39 179601-23-12.0 1
o-Xylene ND ug/L 05/06/16 17:39 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %05/06/16 17:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %05/06/16 17:39 17060-07-070-130 1
Toluene-d8 (S)100 %05/06/16 17:39 2037-26-570-130 1
Sample:MW-2 Lab ID:92296128002 Collected:05/02/16 10:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 06:24 7440-38-205/04/16 14:3010.0 1
Barium 69.2J ug/L 05/06/16 06:24 7440-39-305/04/16 14:301001
Cadmium ND ug/L 05/06/16 06:24 7440-43-905/04/16 14:301.0 1
Chromium ND ug/L 05/06/16 06:24 7440-47-305/04/16 14:305.0 1
Lead ND ug/L 05/06/16 06:24 7439-92-105/04/16 14:305.0 1
Selenium ND ug/L 05/06/16 06:24 7782-49-205/04/16 14:3010.0 1
Silver ND ug/L 05/06/16 06:24 7440-22-405/04/16 14:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/16 10:05 7439-97-605/04/16 16:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 17:56 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 17:56 107-13-110.0 1
Benzene 0.66J ug/L 05/06/16 17:56 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 17:56 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 17:56 75-27-41.0 1
Bromoform ND ug/L 05/06/16 17:56 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 17:56 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 17:56 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 17:56 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 5 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:MW-2 Lab ID:92296128002 Collected:05/02/16 10:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 05/06/16 17:56 56-23-51.0 1
Chlorobenzene 17.7 ug/L 05/06/16 17:56 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 17:56 75-00-31.0 1
Chloroform ND ug/L 05/06/16 17:56 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 17:56 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 17:56 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 17:56 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 17:56 74-95-31.0 1
1,2-Dichlorobenzene 1.5 ug/L 05/06/16 17:56 95-50-11.0 1
1,4-Dichlorobenzene 8.9 ug/L 05/06/16 17:56 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 17:56 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/06/16 17:56 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 17:56 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/06/16 17:56 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/06/16 17:56 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 17:56 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 17:56 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 17:56 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 17:56 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 17:56 100-41-41.0 1
2-Hexanone ND ug/L 05/06/16 17:56 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 17:56 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 17:56 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 17:56 108-10-15.0 1
Styrene ND ug/L 05/06/16 17:56 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 17:56 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 17:56 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 17:56 127-18-41.0 1
Toluene 0.49J ug/L 05/06/16 17:56 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 17:56 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 17:56 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 17:56 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 17:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 17:56 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 17:56 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 17:56 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 17:56 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 17:56 179601-23-12.0 1
o-Xylene 0.27J ug/L 05/06/16 17:56 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)108 %05/06/16 17:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %05/06/16 17:56 17060-07-070-130 1
Toluene-d8 (S)100 %05/06/16 17:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:MW-3 Lab ID:92296128003 Collected:05/02/16 12:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 06:27 7440-38-205/04/16 14:3010.0 1
Barium 64.3J ug/L 05/06/16 06:27 7440-39-305/04/16 14:301001
Cadmium ND ug/L 05/06/16 06:27 7440-43-905/04/16 14:301.0 1
Chromium ND ug/L 05/06/16 06:27 7440-47-305/04/16 14:305.0 1
Lead ND ug/L 05/06/16 06:27 7439-92-105/04/16 14:305.0 1
Selenium ND ug/L 05/06/16 06:27 7782-49-205/04/16 14:3010.0 1
Silver ND ug/L 05/06/16 06:27 7440-22-405/04/16 14:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/16 10:08 7439-97-605/04/16 16:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 18:13 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 18:13 107-13-110.0 1
Benzene 0.40J ug/L 05/06/16 18:13 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 18:13 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 18:13 75-27-41.0 1
Bromoform ND ug/L 05/06/16 18:13 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 18:13 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 18:13 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 18:13 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/06/16 18:13 56-23-51.0 1
Chlorobenzene 4.2 ug/L 05/06/16 18:13 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 18:13 75-00-31.0 1
Chloroform ND ug/L 05/06/16 18:13 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 18:13 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 18:13 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 18:13 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 18:13 74-95-31.0 1
1,2-Dichlorobenzene 0.38J ug/L 05/06/16 18:13 95-50-11.0 1
1,4-Dichlorobenzene 2.4 ug/L 05/06/16 18:13 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 18:13 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/06/16 18:13 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 18:13 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/06/16 18:13 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/06/16 18:13 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 18:13 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 18:13 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 18:13 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 18:13 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 18:13 100-41-41.0 1
2-Hexanone ND ug/L 05/06/16 18:13 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 18:13 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 18:13 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 18:13 108-10-15.0 1
Styrene ND ug/L 05/06/16 18:13 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:MW-3 Lab ID:92296128003 Collected:05/02/16 12:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 18:13 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 18:13 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 18:13 127-18-41.0 1
Toluene ND ug/L 05/06/16 18:13 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 18:13 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 18:13 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 18:13 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 18:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 18:13 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 18:13 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 18:13 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 18:13 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 18:13 179601-23-12.0 1
o-Xylene ND ug/L 05/06/16 18:13 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %05/06/16 18:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %05/06/16 18:13 17060-07-070-130 1
Toluene-d8 (S)95 %05/06/16 18:13 2037-26-570-130 1
Sample:MW-4 Lab ID:92296128004 Collected:05/02/16 11:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic 2.8J ug/L 05/06/16 06:30 7440-38-205/04/16 14:3010.0 1
Barium 50.1J ug/L 05/06/16 06:30 7440-39-305/04/16 14:301001
Cadmium ND ug/L 05/06/16 06:30 7440-43-905/04/16 14:301.0 1
Chromium ND ug/L 05/06/16 06:30 7440-47-305/04/16 14:305.0 1
Lead 2.6J ug/L 05/06/16 06:30 7439-92-105/04/16 14:305.0 1
Selenium ND ug/L 05/06/16 06:30 7782-49-205/04/16 14:3010.0 1
Silver ND ug/L 05/06/16 06:30 7440-22-405/04/16 14:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/16 10:10 7439-97-605/04/16 16:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 18:30 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 18:30 107-13-110.0 1
Benzene 0.97J ug/L 05/06/16 18:30 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 18:30 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 18:30 75-27-41.0 1
Bromoform ND ug/L 05/06/16 18:30 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 18:30 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 18:30 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 18:30 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:MW-4 Lab ID:92296128004 Collected:05/02/16 11:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 05/06/16 18:30 56-23-51.0 1
Chlorobenzene 26.5 ug/L 05/06/16 18:30 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 18:30 75-00-31.0 1
Chloroform ND ug/L 05/06/16 18:30 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 18:30 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 18:30 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 18:30 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 18:30 74-95-31.0 1
1,2-Dichlorobenzene 2.3 ug/L 05/06/16 18:30 95-50-11.0 1
1,4-Dichlorobenzene 11.4 ug/L 05/06/16 18:30 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 18:30 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/06/16 18:30 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 18:30 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/06/16 18:30 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/06/16 18:30 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 18:30 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 18:30 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 18:30 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 18:30 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 18:30 100-41-41.0 1
2-Hexanone 0.99J ug/L 05/06/16 18:30 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 18:30 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 18:30 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 18:30 108-10-15.0 1
Styrene ND ug/L 05/06/16 18:30 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 18:30 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 18:30 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 18:30 127-18-41.0 1
Toluene ND ug/L 05/06/16 18:30 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 18:30 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 18:30 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 18:30 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 18:30 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 18:30 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 18:30 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 18:30 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 18:30 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 18:30 179601-23-12.0 1
o-Xylene 0.31J ug/L 05/06/16 18:30 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %05/06/16 18:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %05/06/16 18:30 17060-07-070-130 1
Toluene-d8 (S)98 %05/06/16 18:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:MW-5 Lab ID:92296128005 Collected:05/02/16 13:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 06:33 7440-38-205/04/16 14:3010.0 1
Barium 46.3J ug/L 05/06/16 06:33 7440-39-305/04/16 14:301001
Cadmium ND ug/L 05/06/16 06:33 7440-43-905/04/16 14:301.0 1
Chromium ND ug/L 05/06/16 06:33 7440-47-305/04/16 14:305.0 1
Lead ND ug/L 05/06/16 06:33 7439-92-105/04/16 14:305.0 1
Selenium ND ug/L 05/06/16 06:33 7782-49-205/04/16 14:3010.0 1
Silver ND ug/L 05/06/16 06:33 7440-22-405/04/16 14:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/16 10:12 7439-97-605/04/16 16:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 18:48 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 18:48 107-13-110.0 1
Benzene 1.0 ug/L 05/06/16 18:48 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 18:48 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 18:48 75-27-41.0 1
Bromoform ND ug/L 05/06/16 18:48 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 18:48 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 18:48 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 18:48 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/06/16 18:48 56-23-51.0 1
Chlorobenzene 6.6 ug/L 05/06/16 18:48 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 18:48 75-00-31.0 1
Chloroform ND ug/L 05/06/16 18:48 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 18:48 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 18:48 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 18:48 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 18:48 74-95-31.0 1
1,2-Dichlorobenzene 2.0 ug/L 05/06/16 18:48 95-50-11.0 1
1,4-Dichlorobenzene 11.8 ug/L 05/06/16 18:48 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 18:48 110-57-61.0 1
1,1-Dichloroethane 0.38J ug/L 05/06/16 18:48 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 18:48 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/06/16 18:48 75-35-41.0 1
cis-1,2-Dichloroethene 0.55J ug/L 05/06/16 18:48 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 18:48 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 18:48 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 18:48 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 18:48 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 18:48 100-41-41.0 1
2-Hexanone ND ug/L 05/06/16 18:48 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 18:48 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 18:48 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 18:48 108-10-15.0 1
Styrene ND ug/L 05/06/16 18:48 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:MW-5 Lab ID:92296128005 Collected:05/02/16 13:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 18:48 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 18:48 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 18:48 127-18-41.0 1
Toluene ND ug/L 05/06/16 18:48 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 18:48 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 18:48 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 18:48 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 18:48 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 18:48 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 18:48 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 18:48 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 18:48 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 18:48 179601-23-12.0 1
o-Xylene 0.26J ug/L 05/06/16 18:48 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %05/06/16 18:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %05/06/16 18:48 17060-07-070-130 1
Toluene-d8 (S)97 %05/06/16 18:48 2037-26-570-130 1
Sample:MW-6 Lab ID:92296128006 Collected:05/02/16 14:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 06:37 7440-38-205/04/16 14:3010.0 1
Barium 8.9J ug/L 05/06/16 06:37 7440-39-305/04/16 14:301001
Cadmium ND ug/L 05/06/16 06:37 7440-43-905/04/16 14:301.0 1
Chromium ND ug/L 05/06/16 06:37 7440-47-305/04/16 14:305.0 1
Lead ND ug/L 05/06/16 06:37 7439-92-105/04/16 14:305.0 1
Selenium ND ug/L 05/06/16 06:37 7782-49-205/04/16 14:3010.0 1
Silver ND ug/L 05/06/16 06:37 7440-22-405/04/16 14:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/16 10:15 7439-97-605/04/16 16:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 19:05 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 19:05 107-13-110.0 1
Benzene ND ug/L 05/06/16 19:05 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 19:05 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 19:05 75-27-41.0 1
Bromoform ND ug/L 05/06/16 19:05 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 19:05 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 19:05 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 19:05 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:MW-6 Lab ID:92296128006 Collected:05/02/16 14:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 05/06/16 19:05 56-23-51.0 1
Chlorobenzene ND ug/L 05/06/16 19:05 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 19:05 75-00-31.0 1
Chloroform ND ug/L 05/06/16 19:05 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 19:05 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 19:05 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 19:05 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 19:05 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/06/16 19:05 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/06/16 19:05 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 19:05 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/06/16 19:05 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 19:05 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/06/16 19:05 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/06/16 19:05 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 19:05 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 19:05 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 19:05 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 19:05 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 19:05 100-41-41.0 1
2-Hexanone ND ug/L 05/06/16 19:05 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 19:05 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 19:05 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 19:05 108-10-15.0 1
Styrene ND ug/L 05/06/16 19:05 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 19:05 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 19:05 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 19:05 127-18-41.0 1
Toluene ND ug/L 05/06/16 19:05 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 19:05 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 19:05 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 19:05 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 19:05 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 19:05 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 19:05 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 19:05 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 19:05 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 19:05 179601-23-12.0 1
o-Xylene ND ug/L 05/06/16 19:05 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %05/06/16 19:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %05/06/16 19:05 17060-07-070-130 1
Toluene-d8 (S)97 %05/06/16 19:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 12 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:SW-1 Lab ID:92296128007 Collected:05/02/16 14:45 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 06:40 7440-38-205/04/16 14:3010.0 1
Barium 30.4 ug/L 05/06/16 06:40 7440-39-305/04/16 14:305.0 1
Cadmium ND ug/L 05/06/16 06:40 7440-43-905/04/16 14:301.0 1
Chromium ND ug/L 05/06/16 06:40 7440-47-305/04/16 14:305.0 1
Lead ND ug/L 05/06/16 06:40 7439-92-105/04/16 14:305.0 1
Selenium ND ug/L 05/06/16 06:40 7782-49-205/04/16 14:3010.0 1
Silver ND ug/L 05/06/16 06:40 7440-22-405/04/16 14:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/16 10:17 7439-97-605/04/16 16:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 19:22 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 19:22 107-13-110.0 1
Benzene ND ug/L 05/06/16 19:22 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 19:22 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 19:22 75-27-41.0 1
Bromoform ND ug/L 05/06/16 19:22 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 19:22 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 19:22 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 19:22 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/06/16 19:22 56-23-51.0 1
Chlorobenzene ND ug/L 05/06/16 19:22 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 19:22 75-00-31.0 1
Chloroform ND ug/L 05/06/16 19:22 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 19:22 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 19:22 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 19:22 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 19:22 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/06/16 19:22 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/06/16 19:22 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 19:22 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/06/16 19:22 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 19:22 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/06/16 19:22 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/06/16 19:22 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 19:22 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 19:22 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 19:22 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 19:22 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 19:22 100-41-41.0 1
2-Hexanone ND ug/L 05/06/16 19:22 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 19:22 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 19:22 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 19:22 108-10-15.0 1
Styrene ND ug/L 05/06/16 19:22 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:SW-1 Lab ID:92296128007 Collected:05/02/16 14:45 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 19:22 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 19:22 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 19:22 127-18-41.0 1
Toluene ND ug/L 05/06/16 19:22 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 19:22 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 19:22 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 19:22 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 19:22 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 19:22 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 19:22 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 19:22 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 19:22 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 19:22 179601-23-12.0 1
o-Xylene ND ug/L 05/06/16 19:22 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %05/06/16 19:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %05/06/16 19:22 17060-07-070-130 1
Toluene-d8 (S)97 %05/06/16 19:22 2037-26-570-130 1
Sample:SW-2 Lab ID:92296128008 Collected:05/02/16 14:15 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 06:52 7440-38-205/04/16 14:3010.0 1
Barium 32.7 ug/L 05/06/16 06:52 7440-39-305/04/16 14:305.0 1
Cadmium ND ug/L 05/06/16 06:52 7440-43-905/04/16 14:301.0 1
Chromium ND ug/L 05/06/16 06:52 7440-47-305/04/16 14:305.0 1
Lead ND ug/L 05/06/16 06:52 7439-92-105/04/16 14:305.0 1
Selenium ND ug/L 05/06/16 06:52 7782-49-205/04/16 14:3010.0 1
Silver ND ug/L 05/06/16 06:52 7440-22-405/04/16 14:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/16 10:19 7439-97-605/04/16 16:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 19:39 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 19:39 107-13-110.0 1
Benzene ND ug/L 05/06/16 19:39 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 19:39 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 19:39 75-27-41.0 1
Bromoform ND ug/L 05/06/16 19:39 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 19:39 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 19:39 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 19:39 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:SW-2 Lab ID:92296128008 Collected:05/02/16 14:15 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 05/06/16 19:39 56-23-51.0 1
Chlorobenzene ND ug/L 05/06/16 19:39 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 19:39 75-00-31.0 1
Chloroform ND ug/L 05/06/16 19:39 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 19:39 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 19:39 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 19:39 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 19:39 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/06/16 19:39 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/06/16 19:39 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 19:39 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/06/16 19:39 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 19:39 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/06/16 19:39 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/06/16 19:39 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 19:39 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 19:39 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 19:39 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 19:39 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 19:39 100-41-41.0 1
2-Hexanone ND ug/L 05/06/16 19:39 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 19:39 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 19:39 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 19:39 108-10-15.0 1
Styrene ND ug/L 05/06/16 19:39 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 19:39 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 19:39 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 19:39 127-18-41.0 1
Toluene ND ug/L 05/06/16 19:39 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 19:39 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 19:39 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 19:39 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 19:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 19:39 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 19:39 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 19:39 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 19:39 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 19:39 179601-23-12.0 1
o-Xylene ND ug/L 05/06/16 19:39 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %05/06/16 19:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %05/06/16 19:39 17060-07-070-130 1
Toluene-d8 (S)96 %05/06/16 19:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:DUPLICATE Lab ID:92296128009 Collected:05/02/16 09:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 06:55 7440-38-205/04/16 14:3010.0 1
Barium 21.9 ug/L 05/06/16 06:55 7440-39-305/04/16 14:305.0 1
Cadmium ND ug/L 05/06/16 06:55 7440-43-905/04/16 14:301.0 1
Chromium ND ug/L 05/06/16 06:55 7440-47-305/04/16 14:305.0 1
Lead ND ug/L 05/06/16 06:55 7439-92-105/04/16 14:305.0 1
Selenium ND ug/L 05/06/16 06:55 7782-49-205/04/16 14:3010.0 1
Silver ND ug/L 05/06/16 06:55 7440-22-405/04/16 14:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/16 10:22 7439-97-605/04/16 16:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 19:56 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 19:56 107-13-110.0 1
Benzene ND ug/L 05/06/16 19:56 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 19:56 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 19:56 75-27-41.0 1
Bromoform ND ug/L 05/06/16 19:56 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 19:56 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 19:56 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 19:56 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/06/16 19:56 56-23-51.0 1
Chlorobenzene ND ug/L 05/06/16 19:56 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 19:56 75-00-31.0 1
Chloroform ND ug/L 05/06/16 19:56 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 19:56 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 19:56 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 19:56 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 19:56 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/06/16 19:56 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/06/16 19:56 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 19:56 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/06/16 19:56 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 19:56 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/06/16 19:56 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/06/16 19:56 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 19:56 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 19:56 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 19:56 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 19:56 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 19:56 100-41-41.0 1
2-Hexanone ND ug/L 05/06/16 19:56 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 19:56 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 19:56 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 19:56 108-10-15.0 1
Styrene ND ug/L 05/06/16 19:56 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:DUPLICATE Lab ID:92296128009 Collected:05/02/16 09:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 19:56 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 19:56 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 19:56 127-18-41.0 1
Toluene ND ug/L 05/06/16 19:56 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 19:56 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 19:56 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 19:56 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 19:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 19:56 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 19:56 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 19:56 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 19:56 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 19:56 179601-23-12.0 1
o-Xylene ND ug/L 05/06/16 19:56 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %05/06/16 19:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %05/06/16 19:56 17060-07-070-130 1
Toluene-d8 (S)95 %05/06/16 19:56 2037-26-570-130 1
Sample:TRIP BLANK Lab ID:92296128010 Collected:05/02/16 00:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/06/16 16:30 67-64-125.0 1
Acrylonitrile ND ug/L 05/06/16 16:30 107-13-110.0 1
Benzene ND ug/L 05/06/16 16:30 71-43-21.0 1
Bromochloromethane ND ug/L 05/06/16 16:30 74-97-51.0 1
Bromodichloromethane ND ug/L 05/06/16 16:30 75-27-41.0 1
Bromoform ND ug/L 05/06/16 16:30 75-25-21.0 1
Bromomethane ND ug/L 05/06/16 16:30 74-83-9 L22.0 1
2-Butanone (MEK)ND ug/L 05/06/16 16:30 78-93-35.0 1
Carbon disulfide ND ug/L 05/06/16 16:30 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/06/16 16:30 56-23-51.0 1
Chlorobenzene ND ug/L 05/06/16 16:30 108-90-71.0 1
Chloroethane ND ug/L 05/06/16 16:30 75-00-31.0 1
Chloroform ND ug/L 05/06/16 16:30 67-66-31.0 1
Chloromethane ND ug/L 05/06/16 16:30 74-87-31.0 1
Dibromochloromethane ND ug/L 05/06/16 16:30 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/16 16:30 106-93-41.0 1
Dibromomethane ND ug/L 05/06/16 16:30 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/06/16 16:30 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/06/16 16:30 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/06/16 16:30 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/06/16 16:30 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/06/16 16:30 107-06-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 17 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Sample:TRIP BLANK Lab ID:92296128010 Collected:05/02/16 00:00 Received:05/03/16 11:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 05/06/16 16:30 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/06/16 16:30 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/06/16 16:30 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/06/16 16:30 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/06/16 16:30 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/06/16 16:30 10061-02-61.0 1
Ethylbenzene ND ug/L 05/06/16 16:30 100-41-41.0 1
2-Hexanone ND ug/L 05/06/16 16:30 591-78-65.0 1
Iodomethane ND ug/L 05/06/16 16:30 74-88-45.0 1
Methylene Chloride ND ug/L 05/06/16 16:30 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/16 16:30 108-10-15.0 1
Styrene ND ug/L 05/06/16 16:30 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/06/16 16:30 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/16 16:30 79-34-51.0 1
Tetrachloroethene ND ug/L 05/06/16 16:30 127-18-41.0 1
Toluene ND ug/L 05/06/16 16:30 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/06/16 16:30 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/06/16 16:30 79-00-51.0 1
Trichloroethene ND ug/L 05/06/16 16:30 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/06/16 16:30 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/06/16 16:30 96-18-41.0 1
Vinyl acetate ND ug/L 05/06/16 16:30 108-05-42.0 1
Vinyl chloride ND ug/L 05/06/16 16:30 75-01-41.0 1
Xylene (Total)ND ug/L 05/06/16 16:30 1330-20-72.0 1
m&p-Xylene ND ug/L 05/06/16 16:30 179601-23-12.0 1
o-Xylene 0.26J ug/L 05/06/16 16:30 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %05/06/16 16:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %05/06/16 16:30 17060-07-070-130 1
Toluene-d8 (S)93 %05/06/16 16:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 18 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/9355
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92296128001, 92296128002, 92296128003, 92296128004, 92296128005, 92296128006, 92296128007,
92296128008, 92296128009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1725311
Associated Lab Samples:92296128001, 92296128002, 92296128003, 92296128004, 92296128005, 92296128006, 92296128007,
92296128008, 92296128009
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 05/05/16 09:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1725312LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1725313MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92295819001
1725314
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 101 75-125102 22.5ND 2.5 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 19 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/21594
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92296128001, 92296128002, 92296128003, 92296128004, 92296128005, 92296128006, 92296128007,
92296128008, 92296128009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1725266
Associated Lab Samples:92296128001, 92296128002, 92296128003, 92296128004, 92296128005, 92296128006, 92296128007,
92296128008, 92296128009
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 05/06/16 06:00
Barium ug/L ND 5.0 05/06/16 06:00
Cadmium ug/L ND 1.0 05/06/16 06:00
Chromium ug/L ND 5.0 05/06/16 06:00
Lead ug/L ND 5.0 05/06/16 06:00
Selenium ug/L ND 10.0 05/06/16 06:00
Silver ug/L ND 5.0 05/06/16 06:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1725267LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 467500 93 80-120
Barium ug/L 499500 100 80-120
Cadmium ug/L 494500 99 80-120
Chromium ug/L 482500 96 80-120
Lead ug/L 498500 100 80-120
Selenium ug/L 498500 100 80-120
Silver ug/L 234250 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1725268MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92296128001
1725269
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 97 75-12596 1500ND484478
Barium ug/L 500 100 75-12597 250021.8J 521 508
Cadmium ug/L 500 100 75-12598 2500ND499490
Chromium ug/L 500 96 75-12594 2500ND481470
Lead ug/L 500 96 75-12594 2500ND482472
Selenium ug/L 500 99 75-12597 2500ND500490
Silver ug/L 250 95 75-12593 2250ND238233
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 20 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36725
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92296128001, 92296128002, 92296128003, 92296128004, 92296128005, 92296128006, 92296128007,
92296128008, 92296128009, 92296128010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1727800
Associated Lab Samples:92296128001, 92296128002, 92296128003, 92296128004, 92296128005, 92296128006, 92296128007,
92296128008, 92296128009, 92296128010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/06/16 11:54
1,1,1-Trichloroethane ug/L ND 1.0 05/06/16 11:54
1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/06/16 11:54
1,1,2-Trichloroethane ug/L ND 1.0 05/06/16 11:54
1,1-Dichloroethane ug/L ND 1.0 05/06/16 11:54
1,1-Dichloroethene ug/L ND 1.0 05/06/16 11:54
1,2,3-Trichloropropane ug/L ND 1.0 05/06/16 11:54
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/06/16 11:54
1,2-Dichlorobenzene ug/L ND 1.0 05/06/16 11:54
1,2-Dichloroethane ug/L ND 1.0 05/06/16 11:54
1,2-Dichloropropane ug/L ND 1.0 05/06/16 11:54
1,4-Dichlorobenzene ug/L ND 1.0 05/06/16 11:54
2-Butanone (MEK)ug/L ND 5.0 05/06/16 11:54
2-Hexanone ug/L ND 5.0 05/06/16 11:54
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 05/06/16 11:54
Acetone ug/L ND 25.0 05/06/16 11:54
Acrylonitrile ug/L ND 10.0 05/06/16 11:54
Benzene ug/L ND 1.0 05/06/16 11:54
Bromochloromethane ug/L ND 1.0 05/06/16 11:54
Bromodichloromethane ug/L ND 1.0 05/06/16 11:54
Bromoform ug/L ND 1.0 05/06/16 11:54
Bromomethane ug/L ND 2.0 05/06/16 11:54
Carbon disulfide ug/L ND 2.0 05/06/16 11:54
Carbon tetrachloride ug/L ND 1.0 05/06/16 11:54
Chlorobenzene ug/L ND 1.0 05/06/16 11:54
Chloroethane ug/L ND 1.0 05/06/16 11:54
Chloroform ug/L ND 1.0 05/06/16 11:54
Chloromethane ug/L ND 1.0 05/06/16 11:54
cis-1,2-Dichloroethene ug/L ND 1.0 05/06/16 11:54
cis-1,3-Dichloropropene ug/L ND 1.0 05/06/16 11:54
Dibromochloromethane ug/L ND 1.0 05/06/16 11:54
Dibromomethane ug/L ND 1.0 05/06/16 11:54
Ethylbenzene ug/L ND 1.0 05/06/16 11:54
Iodomethane ug/L ND 5.0 05/06/16 11:54
m&p-Xylene ug/L ND 2.0 05/06/16 11:54
Methylene Chloride ug/L ND 1.0 05/06/16 11:54
o-Xylene ug/L ND 1.0 05/06/16 11:54
Styrene ug/L ND 1.0 05/06/16 11:54
Tetrachloroethene ug/L ND 1.0 05/06/16 11:54
Toluene ug/L ND 1.0 05/06/16 11:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 21 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1727800
Associated Lab Samples:92296128001, 92296128002, 92296128003, 92296128004, 92296128005, 92296128006, 92296128007,
92296128008, 92296128009, 92296128010
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 1.0 05/06/16 11:54
trans-1,3-Dichloropropene ug/L ND 1.0 05/06/16 11:54
trans-1,4-Dichloro-2-butene ug/L ND 1.0 05/06/16 11:54
Trichloroethene ug/L ND 1.0 05/06/16 11:54
Trichlorofluoromethane ug/L ND 1.0 05/06/16 11:54
Vinyl acetate ug/L ND 2.0 05/06/16 11:54
Vinyl chloride ug/L ND 1.0 05/06/16 11:54
Xylene (Total)ug/L ND 2.0 05/06/16 11:54
1,2-Dichloroethane-d4 (S)%95 70-130 05/06/16 11:54
4-Bromofluorobenzene (S)%100 70-130 05/06/16 11:54
Toluene-d8 (S)%96 70-130 05/06/16 11:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1727801LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 45.750 91 80-125
1,1,1-Trichloroethane ug/L 46.450 93 71-129
1,1,2,2-Tetrachloroethane ug/L 48.550 97 79-124
1,1,2-Trichloroethane ug/L 49.150 98 85-125
1,1-Dichloroethane ug/L 46.250 92 73-126
1,1-Dichloroethene ug/L 51.050 102 66-135
1,2,3-Trichloropropane ug/L 46.050 92 75-130
1,2-Dibromoethane (EDB)ug/L 47.250 94 83-124
1,2-Dichlorobenzene ug/L 48.150 96 80-133
1,2-Dichloroethane ug/L 47.250 94 67-128
1,2-Dichloropropane ug/L 47.150 94 75-132
1,4-Dichlorobenzene ug/L 50.950 102 78-130
2-Butanone (MEK)ug/L 114100 114 61-144
2-Hexanone ug/L 101100 101 68-143
4-Methyl-2-pentanone (MIBK)ug/L 98.7100 99 72-135
Acetone ug/L 114100 114 48-146
Acrylonitrile ug/L 236250 95 40-160
Benzene ug/L 47.750 95 80-125
Bromochloromethane ug/L 48.350 97 71-125
Bromodichloromethane ug/L 52.150 104 78-124
Bromoform ug/L 48.750 97 71-128
Bromomethane ug/L 16.2 L0503240-160
Carbon disulfide ug/L 53.950 108 50-160
Carbon tetrachloride ug/L 51.150 102 69-131
Chlorobenzene ug/L 49.650 99 81-122
Chloroethane ug/L 48.950 98 39-148
Chloroform ug/L 48.550 97 73-127
Chloromethane ug/L 32.750 65 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 22 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1727801LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 45.550 91 74-124
cis-1,3-Dichloropropene ug/L 47.950 96 72-132
Dibromochloromethane ug/L 49.850 100 78-125
Dibromomethane ug/L 58.350 117 82-120
Ethylbenzene ug/L 48.250 96 79-121
Iodomethane ug/L 57.8100 58 39-154
m&p-Xylene ug/L 97.3100 97 81-124
Methylene Chloride ug/L 42.750 85 64-133
o-Xylene ug/L 46.650 93 79-131
Styrene ug/L 47.850 96 84-126
Tetrachloroethene ug/L 53.450 107 78-122
Toluene ug/L 50.250 100 80-121
trans-1,2-Dichloroethene ug/L 50.950 102 71-127
trans-1,3-Dichloropropene ug/L 47.150 94 69-141
trans-1,4-Dichloro-2-butene ug/L 45.950 92 40-160
Trichloroethene ug/L 50.750 101 78-122
Trichlorofluoromethane ug/L 50.950 102 53-137
Vinyl acetate ug/L 92.8100 93 40-160
Vinyl chloride ug/L 43.350 87 58-137
Xylene (Total)ug/L 144150 96 81-126
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1727803MATRIX SPIKE SAMPLE:
MSSpike
Result
92296179004
1,1,1,2-Tetrachloroethane ug/L 22.420 112 70-130ND
1,1,1-Trichloroethane ug/L 23.420 117 70-130ND
1,1,2,2-Tetrachloroethane ug/L 23.920 120 70-130ND
1,1,2-Trichloroethane ug/L 22.920 115 70-130ND
1,1-Dichloroethane ug/L 48.520 100 70-13028.4
1,1-Dichloroethene ug/L 24.920 123 70-166ND
1,2,3-Trichloropropane ug/L 22.620 113 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.420 117 70-130ND
1,2-Dichlorobenzene ug/L 24.220 118 70-1300.54J
1,2-Dichloroethane ug/L 22.720 114 70-130ND
1,2-Dichloropropane ug/L 24.120 120 70-130ND
1,4-Dichlorobenzene ug/L 39.020 120 70-13015.0
2-Butanone (MEK)ug/L 49.240 123 70-130ND
2-Hexanone ug/L 48.740 122 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 47.640 119 70-130ND
Acetone ug/L 53.2 M1402970-13041.5J
Acrylonitrile ug/L 109100 109 70-130ND
Benzene ug/L 38.920 124 70-14814.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 23 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1727803MATRIX SPIKE SAMPLE:
MSSpike
Result
92296179004
Bromochloromethane ug/L 22.520 113 70-130ND
Bromodichloromethane ug/L 21.720 109 70-130ND
Bromoform ug/L 22.120 111 70-130ND
Bromomethane ug/L 6.0 M0203070-130ND
Carbon disulfide ug/L 26.3 M12013270-130ND
Carbon tetrachloride ug/L 24.620 123 70-130ND
Chlorobenzene ug/L 24.620 119 70-1460.81J
Chloroethane ug/L 28.6 M12014370-130ND
Chloroform ug/L 22.820 114 70-130ND
Chloromethane ug/L 15.520 77 70-130ND
cis-1,2-Dichloroethene ug/L 44.120 101 70-13023.9
cis-1,3-Dichloropropene ug/L 23.220 116 70-130ND
Dibromochloromethane ug/L 22.020 110 70-130ND
Dibromomethane ug/L 27.4 M12013770-130ND
Ethylbenzene ug/L 30.220 128 70-1304.6
Iodomethane ug/L 11.6 M1402970-130ND
m&p-Xylene ug/L 95.7 M14013570-13041.6
Methylene Chloride ug/L 47.920 87 70-13030.5
o-Xylene ug/L 49.220 92 70-13030.8
Styrene ug/L 23.220 116 70-130ND
Tetrachloroethene ug/L 33.520 130 70-1307.6
Toluene ug/L 76.9 M12019470-15538.2
trans-1,2-Dichloroethene ug/L 22.720 113 70-130ND
trans-1,3-Dichloropropene ug/L 20.920 105 70-130ND
trans-1,4-Dichloro-2-butene ug/L 20.120 101 70-130ND
Trichloroethene ug/L 36.120 130 69-15110.1
Trichlorofluoromethane ug/L 25.720 128 70-130ND
Vinyl acetate ug/L 40.740 102 70-130ND
Vinyl chloride ug/L 22.720 114 70-130ND
1,2-Dichloroethane-d4 (S)%88 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92296179003
1727802SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L ND23.4
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 24 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92296179003
1727802SAMPLE DUPLICATE:
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L ND6.0
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L ND2.9
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L ND0.94J
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L ND9.6
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Ethylbenzene ug/L ND1.4
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L ND0.30J
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L ND1.8
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L ND0.74J
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%78 1692
4-Bromofluorobenzene (S)%72 3299
Toluene-d8 (S)%99 297
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 25 of 29
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 26 of 29
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92296128
CASWELL CO LF 1584-07-034A
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92296128001 MPRP/21594 ICP/19386MW-1 EPA 3010A EPA 6010
92296128002 MPRP/21594 ICP/19386MW-2 EPA 3010A EPA 6010
92296128003 MPRP/21594 ICP/19386MW-3 EPA 3010A EPA 6010
92296128004 MPRP/21594 ICP/19386MW-4 EPA 3010A EPA 6010
92296128005 MPRP/21594 ICP/19386MW-5 EPA 3010A EPA 6010
92296128006 MPRP/21594 ICP/19386MW-6 EPA 3010A EPA 6010
92296128007 MPRP/21594 ICP/19386SW-1 EPA 3010A EPA 6010
92296128008 MPRP/21594 ICP/19386SW-2 EPA 3010A EPA 6010
92296128009 MPRP/21594 ICP/19386DUPLICATEEPA 3010A EPA 6010
92296128001 MERP/9355 MERC/8997MW-1 EPA 7470 EPA 7470
92296128002 MERP/9355 MERC/8997MW-2 EPA 7470 EPA 7470
92296128003 MERP/9355 MERC/8997MW-3 EPA 7470 EPA 7470
92296128004 MERP/9355 MERC/8997MW-4 EPA 7470 EPA 7470
92296128005 MERP/9355 MERC/8997MW-5 EPA 7470 EPA 7470
92296128006 MERP/9355 MERC/8997MW-6 EPA 7470 EPA 7470
92296128007 MERP/9355 MERC/8997SW-1 EPA 7470 EPA 7470
92296128008 MERP/9355 MERC/8997SW-2 EPA 7470 EPA 7470
92296128009 MERP/9355 MERC/8997DUPLICATEEPA 7470 EPA 7470
92296128001 MSV/36725MW-1 EPA 8260
92296128002 MSV/36725MW-2 EPA 8260
92296128003 MSV/36725MW-3 EPA 8260
92296128004 MSV/36725MW-4 EPA 8260
92296128005 MSV/36725MW-5 EPA 8260
92296128006 MSV/36725MW-6 EPA 8260
92296128007 MSV/36725SW-1 EPA 8260
92296128008 MSV/36725SW-2 EPA 8260
92296128009 MSV/36725DUPLICATEEPA 8260
92296128010 MSV/36725TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 03:33 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 27 of 29
Page 28 of 29
Page 29 of 29
Appendix III – NC DENR Electronic Data Deliverables