0401_AnsonCounty_GWMAnnualReport_DIN26438_20150518

WATER QUALITY MONITORING REPORT
2015 ANNUAL SAMPLING EVENT
ANSON COUNTY LANDFILL
FACILITY PERMIT NO. 04-01

Prepared for:
ANSON COUNTY

Anson County Utilities Department
907 North Washington Street
Wadesboro, North Carolina 28170
[phone]

Prepared by:

SCS ENGINEERS, PC
2520 Whitehall Park Drive, Suite 450
Charlotte, North Carolina 28273
[phone]
License Number C-1837

Date: December 23, 2015
File No.: 02209366.04

Offices Nationwide
www.scsengineers.com
Water Quality Monitoring Report
2015 Annual Sampling Event
i
Table of Contents

Section Page

1 BACKGROUND ................................................................................................................. 1
2 FIELD ACTIVITIES .............................................................................................................. 2
3 GROUNDWATER LEVELS AND FLOW ............................................................................... 2
4 WATER QUALITY .............................................................................................................. 3
4.1 GROUNDWATER ANALYTICAL RESULTS ............................................................... 3
4.1.1 Organic Constituents ................................................................................ 3
4.1.2 Inorganic Constituents.............................................................................. 4
5 SUMMARY AND ANALYSIS ............................................................................................. 4
5.1 Organics Detection Summary ................................................................................. 4
5.2 Inorganics Detection Summary .............................................................................. 4
5.3 Analysis ................................................................................................................. 9

List of Tables

Table 1 – Groundwater Level and Flow Data............................................................................ 2
Table 2 – Summary of Groundwater Quality Data – Appendix I Constituents ......................... 3
Table 3 – Historical Groundwater Monitoring Results ............................................................... 5

List of Figures

Figure No. 1 – Groundwater Surface Contour Map

Attachments

Attachment 1 – Monitoring Well Sampling Logs
Attachment 2 – Constituents for Detection Monitoring 40 CFR 258, Appendix I
Attachment 3 – Laboratory Analytical Results
Attachment 4 – Relevant Documentation and Correspondence

Water Quality Monitoring Report
2015 Annual Sampling Event
1
SCS Engineers, PC (SCS) is submitting this Water Quality Monitoring Report for the closed
Anson County Landfill, a.k.a. Lilesville Landfill, on behalf of the Anson County Utilities
Department. The Landfill’s North Carolina Department of Natural Resources (NCDENR)
facility permit number is 04-01. This report provides background information, description of
field activities, data, and summary and analysis of the laboratory analytical results from the
groundwater monitoring sampling event conducted on May 18, 2015.
This monitoring event is the fourth (4th) annual monitoring event for a five (5) year period as
requested in a letter dated May 16, 2011 from Mr. Ervin Lane, Compliance Hydrogeologist with
NCDENR (currently NCDEQ); Division of Waste Management; Solid Waste Section.
1 BACKGROUND
There are two (2) solid waste landfills, approximately 49.7 and 11.6-acres in size that previously
operated along Haileys Ferry Road (SR 1801) in Lilesville, North Carolina. See attached Figure
No. 1 for the landfill locations and approximate landfilled waste extents. The 49.7-acre landfill
began operations before 1972 and was closed prior to 1978. The 11.6-acre landfill which is
permitted and subjected to groundwater monitoring was closed with a final cover system in the
fall of 1994 with landfill operations dating back to 1978. The 11.6-acre landfill facility permit
number is 04-01. Both landfills are unlined.
Based on a letter dated January 18, 1996 from Mr. James Coffey with the Department of
Environment, Health and Natural Resources - DEHNR (currently NCDEQ) to Anson County, the
permitted 11.6-acre landfill was considered officially closed subject to post-closure conditions
including groundwater monitoring. This letter is included in Attachment 4 for reference. Since
1996, the landfill has been in a post-closure care period. Based on review of previously prepared
documentation, groundwater monitoring has been conducted at the permitted landfill since 1992.
Currently, the groundwater monitoring program at the landfill consists of four monitoring wells:
one (1) background well and three (3) compliance wells. The background well is designated as
MW-A with the compliance wells being designated as MW- B, MW-C, and MW-D.
A Groundwater Monitoring Evaluation Report dated March 18, 2011 was prepared and
submitted to NCDENR by Engineering & Environmental Science Company (E2S) of Raleigh,
North Carolina on behalf of Anson County. This report outlined the historical groundwater
monitoring results at the landfill from 1992 to 2006, evaluated the need to continue with
groundwater monitoring and a request to stop further groundwater monitoring at the landfill.
The County received a letter dated May 16, 2011 from Mr. Ervin Lane with NCDENR (currently
NCDEQ), Division of Waste Management stating that the Division had reviewed the
Groundwater Monitoring Evaluation Report including the request to stop the groundwater
monitoring and determined that the County needs to continue groundwater monitoring on an
annual basis for the next five (5) years. The letter also stated after five (5) years of additional
monitoring, the monitoring results will be re-evaluated by the NCDENR to determine the need
for continued groundwater monitoring at the landfill. The letter from NCDENR is included in
Attachment 4 for reference.

Water Quality Monitoring Report
2015 Annual Sampling Event
2
2 FIELD ACTIVITIES
On May 18, 2015, SCS personnel collected groundwater samples from the four (4) existing
monitoring wells at the Anson County Landfill for laboratory analysis of constituents listed in
Appendix I of the 40 Code of Federal Regulations (CFR) Part 258. The list of Appendix I
constituents is included for reference in Attachment 2. The wells are designated as MW-A,
MW-B, MW-C, and MW-D. Groundwater was purged and samples were collected from the
monitoring wells using low flow sampling procedures. During the purging process for MW-A
and MW-D three well volumes was not able to be removed from the wells due to the wells going
dry before purging was complete. In addition, both wells had minimal well recharge.
SCS’s field sampling logs containing field measurements for pH, conductivity, temperature,
water levels, and dissolved oxygen are included in Attachment 1.
3 GROUNDWATER LEVELS AND FLOW
Water level data for the May 18, 2015 sampling event is summarized in Table 1. Based on the
water level data, a Groundwater Surface Contour Map is presented as Figure 1. The
groundwater flow direction is primarily towards the eastern property boundary. The calculated
groundwater flow velocity and estimated values for hydraulic conductivity and porosity are
included below in Table 1. Please note that for all the monitoring wells, the estimated values for
hydraulic conductivity and effective porosity in Table 1 are from the Groundwater Monitoring
Evaluation Report prepared by Engineering & Environmental Science Company (E2S) dated
March 18, 2011.
TABLE 1
Groundwater Level and Flow Data
Closed Anson County Landfill (Lilesville Landfill) - Facility Permit No. 04-01

Well
ID Date GS Well TOC K n DTW WL-Elev. I V
Elevation Depth Elevation (ft/yr) (feet) (feet) (ft/ft) (ft/yr)
MW-A 5-18-2015 NM 27.8 462.63 517.21 0.25 11.61 451.02 0.023 48.53
MW-B 5-18-2015 NM 28.1 451.20 517.21 0.25 16.60 434.60 0.023 48.53
MW-C 5-18-2015 NM 22.57 438.19 517.21 0.25 5.25 432.94 0.004 8.18
MW-D 5-18-2015 NM 35.52 436.16 517.21 0.25 5.25 430.91 0.003 5.53

Legend:
GS = ground surface TOC = top of casing NM = Not Measured
WL-Elev = water level elevation DTW = depth to water from TOC
(measured)
V = groundwater flow rate
(calculated); V = (K*I)/n
n = effective porosity (estimated
based on previous GW monitoring
reports and site conditions)
K = hydraulic conductivity (estimated
based on previous GW monitoring
reports and site conditions)
I = hydraulic gradient (calculated);
I = WL-elev. difference / horizontal
distance
Water Quality Monitoring Report
2015 Annual Sampling Event
3
4 WATER QUALITY
40 CFR Part 258 Appendix I detected constituents with their analytical concentration were
compared against the North Carolina Department of Environment and Natural Resources
(NCDENR) rule 15A NCAC 02L .0202 Groundwater Quality Standards (2L). When a 15A
NCAC 02L .0202 Groundwater Quality Standard is not available for a detected constituent, the
result is compared against the North Carolina Groundwater Protection Standard (GWP). The
following Table 2 lists the Appendix I detected constituents analytical results from the May
2015 annual water quality monitoring event. In Table 2, constituent analytical results that
exceed their associated 2L or GWP compliance limit are shaded. A hard copy of the laboratory
report from Pace Analytical Services, Inc. with a copy of the chain-of-custody form is included
in Attachment 3.
TABLE 2
Summary of Groundwater Quality Data - Appendix I Constituents
Closed Anson County Landfill (Lilesville Landfill) - Facility Permit No. 04-01
Parameter Sampling
Date
Compliance Limit (µg/L) Analytical Results for Sample Locations
(in µg/L)
SWSL 15A NCAC 02L MW-A MW-B MW-C MW-D
Barium 05-18-2015 100 700 18.2 14.6 46.0 48.5
Nickel 05-18-2015 50 100 ND<5 ND<5 ND<5 5.2
Zinc 05-18-2015 10 1000 ND<10 ND<10 ND<10 16.3

Legend:
µg/L = Micrograms per Liter Bold font indicates analyte detection.
Shaded field denotes result that exceeds Compliance Limit. SWSL = Solid Waste Section Limit
GWP = Groundwater Protection Standard (2L Standard not established) NE = Not established
J = Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
4.1 GROUNDWATER ANALYTICAL RESULTS
The description of the Appendix I organic and inorganic constituents detected during the 2015
annual groundwater monitoring event are as follows:
4.1.1 ORGANIC CONSTITUENTS
No Appendix I organic constituents were detected during the monitoring event.

Water Quality Monitoring Report
2015 Annual Sampling Event
4
4.1.2 INORGANIC CONSTITUENTS
Barium, Nickel, and Zinc were the only Appendix I inorganic constituents detected in one or
more of the monitoring wells during the monitoring event although were detected below their
respective compliance limit. These detections are summarized as follows:
 Barium was detected in all four (4) monitoring wells below its 2L compliance limit
of 700 g/L. In background monitoring well MW-A the concentration was 18.2
g/L. In compliance well MW-B the concentration was 14.6 g/L, MW-C was 46.0
g/L, and MW-D was 48.5 g/L.
 Nickel was only detected in monitoring well MW-D at a concentration of 5.2 g/L
which is less than its 2L compliance limit of 100 g/L.
 Zinc was only detected in monitoring well MW-D at a concentration of 16.3 g/L
which is less than its 2L compliance limit of 1000 g/L.
5 SUMMARY AND ANALYSIS
A summary of the 2015 annual water quality monitoring event results as well as historical
monitoring results is a follows:
5.1 ORGANICS DETECTION SUMMARY
During the 2015 annual monitoring event, no Appendix I organic constituents were detected in
the monitoring wells. No detection of Appendix I organic constituents occurred during the 2014
annual monitoring event as well.
The monitoring wells historical Appendix I organics analytical results are presented in Table 3.
5.2 INORGANICS DETECTION SUMMARY
During the 2015 annual monitoring event no Appendix I inorganic constituents were detected
above their respective compliance limits in the monitoring wells. During this monitoring event
Barium was detected below its respective compliance limit of 700 g/L in all four (4) monitoring
wells. Barium has historically been detected in all the monitoring wells but below the 2L
compliance limit.
Nickel and Zinc was detected during this monitoring event in monitoring well MW-D only at
levels below their respective compliance limit. Since 2012 Nickel has been infrequently detected
in MW-D only and Zinc has only been detected in monitoring well MW-D, always below the
compliance limit.
The monitoring wells historical Appendix I inorganics analytical results are presented in Table
3.

Water Quality Monitoring Report
2015 Annual Sampling Event
5
TABLE 3
Historical Groundwater Monitoring Results
Closed Anson County Landfill (Lilesville Landfill) - Facility Permit No. 04-01

Sample
Date
Detection
Limit
Compliance Limit
15A NCAC 02L or
Groundwater Protection
Standard
Analytical Results (µg/L)
MW-A MW-B MW-C MW-D
Parameter: Benzene
Apr-99 2 ND<2 ND<2 ND<2 ND<2
Oct-00 1 ND<1 ND<1 2.1 ND<1
Oct-01 2 ND<2 ND<2 2.7 ND<2
Apr-02 1 ND<1 ND<1 1.5 ND<1
Oct-03 1 ND<1 ND<1 1.3 ND<1
May-04 1 ND<1 ND<1 ND<1 ND<1
Oct-04 5 ND<5 ND<5 ND<5 ND<5
May-05 5 ND<5 ND<5 ND<5 ND<5
Oct-06 5 ND<5 ND<5 ND<5 ND<5
Oct-12 1 1 ND<1 ND<1 1.3 ND<1
Apr-13 1 1 ND<1 ND<1 ND<1 ND<1
Nov-14 1 1 ND<1 ND<1 ND<1 ND<1
May-15 1 1 ND<1 ND<1 ND<1 ND<1
Parameter: Chlorobenzene
Apr-99 2 ND<2 ND<2 ND<2 ND<2
Oct-00 1 ND<1 ND<1 14 ND<1
Oct-01 2 ND<2 ND<2 17 ND<2
Apr-02 1 ND<1 ND<1 11 ND<1
Oct-03 1 ND<1 ND<1 6 ND<1
May-04 1 ND<1 ND<1 ND<1 ND<1
Oct-04 5 ND<5 ND<5 ND<5 ND<5
May-05 5 ND<5 ND<5 ND<5 ND<5
Oct-06 5 ND<5 ND<5 9 ND<5
Oct-12 1 50 ND<1 ND<1 5.2 ND<1
Apr-13 1 50 ND<1 ND<1 1.4 ND<1
Nov-14 1 50 ND<1 ND<1 ND<1 ND<1
May-15 1 50 ND<1 ND<1 ND<1 ND<1
ND = Not Detected (below detection limit)

Water Quality Monitoring Report
2015 Annual Sampling Event
6
TABLE 3
Historical Groundwater Monitoring Results
Closed Anson County Landfill (Lilesville Landfill) - Facility Permit No. 04-01

Sample
Date
Detection
Limit
Compliance Limit
15A NCAC 02L or
Groundwater Protection
Standard
Analytical Results (µg/L)
MW-A MW-B MW-C MW-D
Parameter: Arsenic
Apr-99 5 ND<5 ND<5 ND<5 ND<5
Oct-00 5 ND<5 ND<5 6 ND<5
Oct-01 5 ND<5 27 ND<5 ND<5
Apr-02 5 ND<5 ND<5 8 ND<5
Oct-03 5 ND<5 ND<5 7 ND<5
May-04 5 8 5 5 ND<5
Oct-04 20 ND<20 ND<20 ND<20 ND<20
May-05 20 16 31 81 72
Oct-06 20 ND<20 ND<20 ND<20 ND<20
Oct-12 5 10 ND<5 ND<5 5.4 ND<5
Apr-13 10 10 ND<10 ND<10 ND<10 ND<10
Nov-14 10 10 ND<10 ND<10 ND<10 ND<10
May-15 10 10 ND<10 ND<10 ND<10 ND<10
Parameter: Barium
Apr-99 20 20 14 76 66
Oct-00 20 21 150 211 53
Oct-01 20 21 26 238 66
Apr-02 20 23 18 18 52
Oct-03 20 17 17 205 49
May-04 20 23 24 91 51
Oct-04 40 ND<40 45 150 70
May-05 40 28 31 81 72
Oct-06 40 ND<40 52 260 65
Oct-12 5 700 18.1 19.6 176 69.4
Apr-13 5 700 21.4 15.5 83.8 74.1
Nov-14 5 700 62.8 18.4 18.6 40.3
May-15 5 700 18.2 14.6 46 48.5
ND = Not Detected (below detection limit)

Water Quality Monitoring Report
2015 Annual Sampling Event
7
TABLE 3
Historical Groundwater Monitoring Results
Closed Anson County Landfill (Lilesville Landfill) - Facility Permit No. 04-01

Sample
Date
Detection
Limit
Compliance Limit
15A NCAC 02L or
Groundwater Protection
Standard
Analytical Results (µg/L)
MW-A MW-B MW-C MW-D
Parameter: Chromium
Apr-99 5 ND<5 ND<5 ND<5 ND<5
Oct-00 5 ND<5 ND<5 ND<5 ND<5
Oct-01 5 ND<5 ND<5 ND<5 10
Apr-02 5 ND<5 ND<5 ND<5 ND<5
Oct-03 5 ND<5 ND<5 ND<5 6
May-04 5 ND<5 ND<5 ND<5 ND<5
Oct-04 20 ND<20 ND<20 ND<20 ND<20
May-05 20 ND<20 ND<20 ND<20 ND<20
Oct-06 20 ND<20 ND<20 ND<20 ND<20
Oct-12 5 10 ND<5 ND<5 ND<5 176
Apr-13 5 10 ND<5 ND<5 ND<5 350
Nov-14 5 10 ND<5 ND<5 ND<5 ND<5
May-15 5 10 ND<5 ND<5 ND<5 ND<5
Parameter: Lead
Apr-99 3 ND<3 ND<3 ND<3 8
Oct-00 3 ND<3 ND<3 3 34
Oct-01 3 ND<3 5 ND<3 24
Apr-02 2 ND<2 ND<2 4 4
Oct-03 2 ND<2 ND<2 ND<2 3
May-04 2 6 4 ND<2 ND<2
Oct-04 15 ND<15 ND<15 ND<15 ND<15
May-05 10 ND<10 ND<10 ND<10 ND<10
Oct-06 40 ND<40 ND<40 ND<40 ND<40
Oct-12 5 15 ND<5 ND<5 ND<5 24.8
Apr-13 5 15 ND<5 ND<5 ND<5 28.2
Nov-14 5 15 ND<5 ND<5 ND<5 ND<5
May-15 5 15 ND<5 ND<5 ND<5 ND<5
ND = Not Detected (below detection limit)

Water Quality Monitoring Report
2015 Annual Sampling Event
8
TABLE 3
Historical Groundwater Monitoring Results
Closed Anson County Landfill (Lilesville Landfill) - Facility Permit No. 04-01

Sample
Date
Detection
Limit
Compliance Limit
15A NCAC 02L or
Groundwater Protection
Standard
Analytical Results (µg/L)
MW-A MW-B MW-C MW-D
Parameter: Beryllium
Oct-12 1 4 ND<1 ND<1 ND<1 ND<1
Apr-13 1 4 ND<1 ND<1 ND<1 1.4
Nov-14 1 4 ND<1 ND<1 ND<1 ND<1
May-15 1 4 ND<1 ND<1 ND<1 ND<1
Parameter: Cobalt
Oct-12 5 1 ND<5 ND<5 ND<5 6
Apr-13 5 1 ND<5 19.3 48.4 13.3
Nov-14 5 1 ND<5 ND<5 ND<5 ND<5
May-15 5 1 ND<5 ND<5 ND<5 ND<5
Parameter: Copper
Oct-12 5 1000 ND<5 ND<5 ND<5 26.6
Apr-13 5 1000 ND<5 ND<5 ND<5 25
Nov-14 5 1000 ND<5 ND<5 ND<5 ND<5
May-15 5 1000 ND<5 ND<5 ND<5 ND<5
Parameter: Nickel
Oct-12 5 100 ND<5 ND<5 ND<5 86.6
Apr-13 5 100 ND<5 ND<5 ND<5 160
Nov-14 5 100 ND<5 ND<5 ND<5 ND<5
May-15 5 100 ND<5 ND<5 ND<5 5.2
Parameter: Vanadium
Oct-12 5 0.3 ND<5 ND<5 ND<5 18
Apr-13 5 0.3 ND<5 ND<5 ND<5 22.3
Nov-14 5 0.3 ND<5 ND<5 ND<5 ND<5
May-15 5 0.3 ND<5 ND<5 ND<5 ND<5
ND = Not Detected (below detection limit)

Water Quality Monitoring Report
2015 Annual Sampling Event
9
TABLE 3
Historical Groundwater Monitoring Results
Closed Anson County Landfill (Lilesville Landfill) - Facility Permit No. 04-01

Sample
Date
Detection
Limit
Compliance Limit
15A NCAC 02L or
Groundwater Protection
Standard
Analytical Results (µg/L)
MW-A MW-B MW-C MW-D
Parameter: Zinc
Oct-12 10 1000 ND<10 ND<10 ND<10 31
Apr-13 10 1000 ND<10 ND<10 ND<10 27.5
Nov-14 10 1000 ND<10 ND<10 ND<10 13.5
May-15 10 1000 ND<10 ND<10 ND<10 16.3
ND = Not Detected (below detection limit)

5.3 ANALYSIS
During the 2015 annual monitoring event, no 40 CFR Part 258 Appendix I organic constituents
or metals were detected above their respective compliance limits in the monitoring wells. As
stated in previous monitoring reports certain Appendix I inorganics or metals are considered
natural occurring within the in-situ soils and not caused by a release from a landfill. An example
of this is a closed MSW landfill located in Union County, North Carolina where groundwater
alternate source demonstrations(1) for metals were completed and the metals Barium, Beryllium,
Chromium, Cobalt, Copper, Lead, Nickel, Vanadium and Zinc were determined to be natural
occurring at considerable levels in the in-situ soils. The landfill located in Union County is
within the vicinity of and has similar geologic conditions to the closed Anson County - Lilesville
Landfill. So the existence of these metals in the in-situ soils at the Anson County - Lilesville
Landfill is probable. Further investigation of the in-situ soils does not seem warranted at this
time since only Barium, Nickel, and Zinc were detected during the monitoring event at levels
below their respective compliance limit.
No Appendix I organics or volatile organic compounds (VOCs) were detected during the
monitoring event. A VOC was last detected in April 2013 during the 2013 annual monitoring
event. The detected VOC was Chlorobenzene in monitoring well MW-C and was at a
concentration below the compliance limit.
There is one (1) remaining regulatory requested annual monitoring event to occur in the fall of
2016.

(1) Reference: Alternate Source Demonstration Report, Union County Landfill, Wingate North Carolina dated July
2008 and Revised Alternate Source Demonstration for the Union County Landfill dated November 2012.
Water Quality Monitoring Report
2015 Annual Sampling Event

FIGURE NO. 1
Groundwater Surface Contour Map

OLD LANDFILL AREA(APPROX. 49.7 ACRES)CLOSED PRIOR TO 1978
P
E
R
M
I
T
T
E
D

L
A
N
D
F
I
L
L

A
R
E
A
F
A
C
I
L
I
T
Y

P
E
R
M
I
T

N
O
.

0
4
-
0
1
(
A
P
P
R
O
X
.

1
1
.
6

A
C
R
E
S
)
O
F
F
I
C
I
A
L
L
Y

C
L
O
S
E
D

J
A
N
U
A
R
Y

1
8
,

1
9
9
6
APP BY
CHK BY
DES BY
CAD FILE
SCALE
FIGURE
PROJECT NO.DATE
Environmental Consultants and Contractors
PHONE: [phone] FAX: [phone]
2520 WHITEHALL PARK DRIVE, SUITE 450
CHARLOTTE, NORTH CAROLINA 28273
02209366.04
AS SHOWN
POT. MAP
DMC
ADG
ADG
CLOSED ANSON COUNTY LANDFILL 04-01
GROUNDWATER SURFACE CONTOUR MAP
LILESVILLE, NC
5/18/2015
1
Water Quality Monitoring Report
2015 Annual Sampling Event

ATTACHMENT 1
Monitoring Well Sampling Logs

ANSON COUNTY LANDFILL ‐ CLOSED LILESVILLE LANDFILL
ANSON COUNTY, NORTH CAROLINA
MONITORING WELL SAMPLE LOG
WELL ID: MW‐A WEATHER: Clear, Upper 80s
DATE: 5/18/2015
PERSONNEL: Michael Cobb; SCS Engineers, PC
Adam Smith; SCS Engineers, PC
Compliance.
Total Well Depth: 27.8 ft.
Depth to Water: 11.61 ft.
Water Column: 16.19 ft.
Well Volume: 2.62 gal.
Field Readings 1 2 3 4
Time
Turbidity
pH
DO Mg/L
Temperature
Sp. Conductivity 5 gal
5 6 7 8 9 101112
Time
Turbidity
pH
DO Mg/L
Temperature
Sp. Conductivity
Notes:
Sampled after purging 5 gallons due to minimal recharge.
Sample ID: MW‐A
Sample Time: 1525
Laboratory: Pace Analytical
Shipping Date: 5/19/2015
Total purged from well:
REASON FOR SAMPLING:
ANSON COUNTY LANDFILL ‐ CLOSED LILESVILLE LANDFILL
ANSON COUNTY, NORTH CAROLINA
MONITORING WELL SAMPLE LOG
WELL ID: MW‐B WEATHER: Clear, Upper 80s
DATE: 5/18/2015
PERSONNEL: Michael Cobb; SCS Engineers, PC
Adam Smith; SCS Engineers, PC
Compliance.
Total Well Depth: 28.1 ft.
Depth to Water: 16.6 ft.
Water Column: 11.5 ft.
Well Volume: 1.86 gal.
Field Readings 1 2 3 4
Time 1337 1342 1347 1352
Turbidity 7.1 9.8 6.22 5.1
pH 6.17 6.11 6.1 6.11
DO Mg/L 0.67 0.52 0.57 0.58
Temperature 16.1 15.8 15.6 15.4
Sp. Conductivity 92.9 72.7 68.7 66.4 52 gal
5 678 910
Time 1357 1402 1407 1412 1417 1422
Turbidity 6.23 4.97 2.67 4.74 2.8 2.51
pH 6.1 6.09 6.11 6.09 6.1 6.11
DO Mg/L 0.51 0.51 0.55 0.53 0.52 0.54
Temperature 15.4 15.4 15.4 15.4 15.4 15.4
Sp. Conductivity 65.5 65.9 64.9 63.8 64.2 63.4
Notes:
Purged 3 well volumes before taking measurements
Sample ID: MW‐B
Sample Time: 1425
Laboratory: Pace Analytical
Shipping Date: 5/19/2015
Total purged from well:
REASON FOR SAMPLING:
ANSON COUNTY LANDFILL ‐ CLOSED LILESVILLE LANDFILL
ANSON COUNTY, NORTH CAROLINA
MONITORING WELL SAMPLE LOG
WELL ID: MW‐C WEATHER: Clear, Upper 80s
DATE: 5/18/2015
PERSONNEL: Michael Cobb; SCS Engineers, PC
Adam Smith; SCS Engineers, PC
Compliance.
Total Well Depth: 22.57 ft.
Depth to Water: 5.25 ft.
Water Column: 17.32 ft.
Well Volume: 2.80 gal.
Field Readings 1 2 3 4
Time 1110 1115 1120 1125
Turbidity 7.28 5.92 5.03 5.52
pH 6.55 6.48 6.46 6.45
DO Mg/L 0.6 0.62 0.64 0.43
Temperature 17.4 17 16.9 16.9
Sp. Conductivity 437.7 262.6 254.9 214.7 37.5 gal
5
Time 1130
Turbidity 5.11
pH 6.45
DO Mg/L 0.54
Temperature 16.8
Sp. Conductivity 219
Notes:
Purged 3 well volumes before taking measurements.
Sample ID: MW‐C
Sample Time: 1135
Laboratory: Pace Analytical
Shipping Date: 5/19/2015
Total purged from well:
REASON FOR SAMPLING:
ANSON COUNTY LANDFILL ‐ CLOSED LILESVILLE LANDFILL
ANSON COUNTY, NORTH CAROLINA
MONITORING WELL SAMPLE LOG
WELL ID: MW‐D WEATHER: Clear, Upper 80s
DATE: 5/18/2015
PERSONNEL: Michael Cobb; SCS Engineers, PC
Adam Smith; SCS Engineers, PC
Compliance.
Total Well Depth: 35.52 ft.
Depth to Water: 5.25 ft.
Water Column: 30.27 ft.
Well Volume: 5.14 gal.
Field Readings 1 2 3 4
Time
Turbidity
pH
Sp. Conductivity
DO Mg/L
Temp.6 gal
Notes:
Well dry before initial purge completed.
Waited for well to recharge and then sampled.
Sample ID: MW‐D
Sample Time: 1545
Laboratory: Pace Analytical
Shipping Date: 5/19/2015
Total purged from well:
REASON FOR SAMPLING:
Water Quality Monitoring Report
2015 Annual Sampling Event

ATTACHMENT 2
Constituents for Detection Monitoring 40 CFR 258, Appendix I

Constituents for Detection Monitoring
(40 CFR 258, Appendix I)
Common name CAS RN
Antimony (Total)
Arsenic (Total)
Barium (Total)
Beryllium (Total)
Cadmium (Total)
Chromium (Total)
Cobalt (Total)
Copper (Total)
Lead (Total)
Nickel (Total)
Selenium (Total)
Silver (Total)
Thallium (Total)
Vanadium (Total)
Zinc (Total)
Acetone 67-64-1
Acrylonitrile 107-13-1
Benzene 71-43-2
Bromochloromethane 74-97-5
Bromodichloromethane 75-27-4
Bromoform; Tribromomethane 75-25-2
Carbon disulfide 75-15-0
Carbon tetrachloride 56-23-5
Chlorobenzene 108-90-7
Chloroethane; Ethyl chloride 75-00-3
Chloroform; Trichloromethane 67-66-3
Dibromochloromethane; Chlorodibromomethane 124-48-1
1,2-Dibromo-3-chlorpropane; DBCP 96-12-8
1,2-Dibromoethane; Ethylene dibromide; EDB 106-93-4
o-Dichlorobenzene; 1,2-Dichlorobenzene 95-50-1
p-Dichlorobenzene; 1,4-Dichlorobenzene 106-46-7
trans-1,4-Dichloro-2-butene 110-57-6
1,1-Dichloroethane; Ethylidene chloride 75-34-3
1,2-Dichloroethane; Ethlyene dichloride 107-06-2
1,1-Dichloroethylene; 1-1-Dichloroethene; Vinylidene
chloride
75-35-4
cis-1,2-Dichloroethylene; cis-1,2-Dichloroethene 156-59-2
trans-1,2-Dichloroethylene; trans-1,2-Dichloroethene 156-60-5
1,2-Dichlorpropane; Propylene dichloride 78-87-5
cis-1,3-Dichlorpropene 10061-01-5
trans-1,3-Dichlorpropene 10061-02-6
Ethylbenzene 100-41-4
2-hexanone; Methyl butyl ketone 591-78-6
Methyl bromide; Bromomethane 74-83-9
Methyl chloride; Chloromethane 74-87-3
Methylene bromide Dibromomethane 74-95-3
Methylene chloride; Dichloromethane 75-09-2
Methyl ethyl ketone; MEK; 2-Butanone 78-93-3
Methyl iodide; Iodomethane 74-88-4
4-Methyl-2-pentanone; Methyl isobutyl isobutyl
ketone
108-10-1
Styrene 100-42-5
1,1,1,2-Tetrachloroethane 630-20-6
1,1,2,2-Tetrachloroethane 79-34-5
Tetrachloroethylene; Tetracholorethene;
Perchloroethylene
127-18-4
Toluene 108-88-3
1,1,1-Trochlorethane; Methylchloroform 71-55-6
1,1,2-Trichloroethane 79-00-5
Trichloroethylene; Trichlorethene 79-01-6
Trichlorofluoromethane; CFC-11 75-69-4
1,2,3-Trichloropropane 96-18-4
Vinyl acetate 108-05-4
Vinyl chloride 75-01-4
Xylenes 1330-20-7
NC Department of Environment and Natural Resources
Waste Management - Constituent List
Sections and Programs » Solid Waste Section » Environmental Monitoring » List
Solid Waste Environmental Monitoring Reporting Limits and Standards
All units are in (ug/L) unless noted.
NE = Not Established
CAS numbers that begin with "SW" are not real CAS numbers, instead this represents the Solid Waste Section's ID
number.
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
630-20-6 1,1,1,2-Tetrachloroethane Ethane, 1,1,1,2-tetrachloro- NE 1 5 190 I
71-55-6 1,1,1-Trichloroethane; Ethane, 1,1,1-trichloro- 200 -- 1 200 I
79-34-5 1,1,2,2-Tetrachloroethane Ethane, 1,1,2,2-tetrachloro- 0.2 0.18 3 191 I
79-00-5 1,1,2-Trichloroethane Ethane, 1,1,2-trichloro- NE 0.6 1 202 I
76-13-1 1,1,2-Trichlorotrifluoroethane CFC-113 200000 NE NE 398
92-52-4 1,1-biphenyl 1,1-biphenyl 400 -- 10 421
75-34-3 1,1-Dichloroethane; Ethyldidene Ethane, 1,1-dichloro- 6 -- 5 75 I
75-35-4 1,1-Dichloroethylene; 1,1- Ethene, 1,1-dichloro- 7 -- 5 77 I
563-58-6 1,1-Dichloropropene 1-Propene, 1,1-dichloro- NE NE 5 85
96-18-4 1,2,3-Trichloropropane Propane, 1,2,3-trichloro- 0.005 -- 1 206 I
95-94-3 1,2,4,5-Tetrachlorobenzene Benzene, 1,2,4,5-tetrachloro- NE 2 10 189
120-82-1 1,2,4-Trichlorobenzene Benzene, 1,2,4-trichloro- 70 70 10 199
95-63-6 1,2,4-Trimethylbenzene Pseudocumene 400 NE NE 372
226-36-8 1,2,5,6-Dibenzacridine NE NE NE 385
96-12-8 1,2-Dibromo-3-chloropropane; DBCP Propane, 1,2-dibromo-3-chloro- 0.04 -- 13 67 I
106-93-4 1,2-Dibromoethane; Ethylene dibromide; Ethane, 1,2-dibromo- 0.02 -- 1 68 I
107-06-2 1,2-Dichloroethane; Ethylene Ethane, 1,2-dichloro- 0.4 -- 1 76 I
540-59-0 1,2-Dichloroethylene mixed isomers Mixed Isomers NE 60 NE 481
78-87-5 1,2-Dichloropropane Propane, 1,2-dichloro- 0.6 -- 1 82 I
122-66-7 1,2-Diphenylhydrazine NE NE NE 394
108-67-8 1,3,5-Trimethylbenzene) Mesitylene 400 NE NE 373
142-28-9 1,3-Dichloropropane; Trimethylene Propane, 1,3-dichloro- NE NE 1 83
106-37-6 1,4-Dibromobenzene p-Dibromobenzene, p-Bromobenzene 70 471
123-91-1 1,4-dioxane 1,4-dioxane 3 -- 10 422
130-15-4 1,4-Naphthoquinone 1,4-Naphthalenedione NE NE 10 149
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 1 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
87-61-6 1-2-3-Trichlorobenzene NE NE NE 371
90-12-0 1-Methylnaphthalene α-methylnaphthalene NE 1 NE 503
134-32-7 1-Naphthylamine 1-Naphthalenamine NE NE 10 150
120-36-5 2-(2-4-dichlorophenoxy)propionic NE NE NE 352
594-20-7 2,2-Dichloropropane; Isopropylidene Propane, 2,2-dichloro- NE NE 15 84
58-90-2 2,3,4,6-Tetrachlorophenol Phenol, 2,3,4,6-tetrachloro- 200 -- 10 193
93-76-5 2,4,5-T; 2,4,5-Trichlorophenoxyacetic Acetic acid, (2,4,5-trichlorophenoxy)- NE NE 2 188
93-72-1 2,4,5-TP Acid Silvex 50 NE NE 452
95-95-4 2,4,5-Trichlorophenol Phenol, 2,4,5-trichloro- NE 63 10 204
88-06-2 2,4,6-Trichlorophenol Phenol, 2,4,6-trichloro- NE 4 10 205
94-75-7 2,4-D; 2,4-Dichlorophenoxyacetic Acetic acid, (2,4-dichlorophenoxy)- 70 -- 2 59
120-83-2 2,4-Dichlorophenol Phenol, 2,4-dichloro- NE 0.98 10 80
105-67-9 2,4-Dimethylphenol; m-Xylenol Phenol, 2,4-dimethyl- 100 -- 10 95
51-28-5 2,4-Dinitrophenol Phenol, 2,4-dinitro- NE NE 50 99
121-14-2 2,4-Dinitrotoluene Benzene, 1-methyl-2,4-dinitro- NE 0.1 10 100
87-65-0 2,6-Dichlorophenol Phenol, 2,6-dichloro- NE NE 10 81
606-20-2 2,6-Dinitrotoluene Benzene, 2-methyl-1,3-dinitro- NE NE 10 101
94-82-6 2-4 DB NE NE NE 350
53-96-3 2-Acetylaminofluorene; 2-AAF Acetamide, N-9H-fluoren-2-yl- NE NE 20 6
110-75-8 2-Chloroethylvinyl ether NE NE NE 358
91-58-7 2-Chloronaphthalene Naphthalene, 2-chloro- NE NE 10 47
95-57-8 2-Chlorophenol Phenol, 2-chloro- 0.4 -- 10 48
591-78-6 2-Hexanone; Methyl butyl ketone 2-Hexanone NE 40 50 124 I
91-57-6 2-Methylnaphthalene Naphthalene, 2-methyl- 30 -- 10 145
91-59-8 2-Naphthylamine 2-Naphthalenamine NE NE 10 151
109-06-8 2-Picoline NE NE NE 390
91-94-1 3,3'-Dichlorobenzidine [1,1'-Biphenyl]-4,4'-diamine,3,3'- NE NE 20 72
119-93-7 3,3'-Dimethylbenzidine [1,1'-Biphenyl]-4,4'-diamine,3,3'- NE NE 10 94
56-49-5 3-Methylcholanthrene Benz[j]aceanthrylene,1,2-dihydro-3- NE NE 10 138
72-54-8 4,4'-DDD Benzene 1,1'-(2,2- 0.1 -- 0.1 60
72-55-9 4,4'-DDE Benzene, 1,1'- NE NE 0.1 61
50-29-3 4,4'-DDT Benzene, 1,1'-(2,2,2- 0.1 -- 0.1 62
534-52-1 4,6-Dinitro-o-cresol; 4,6-Dinitro-2- Phenol, 2-methyl-4,6-dinitro- NE NE 50 98
92-67-1 4-Aminobiphenyl [1,1'-Biphenyl]-4-amine NE NE 20 11
460-00-4 4-Bromofluorobenzene NE NE NE 463
101-55-3 4-Bromophenyl phenyl ether Benzene, 1-bromo-4-phenoxy- NE NE 10 31
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 2 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
7005-72-3 4-Chlorophenyl phenyl ether Benzene, 1-chloro-4-phenoxy- NE NE 10 49
108-10-1 4-Methyl-2-pentanone; Methyl isobutyl 2-Pentanone, 4-methyl- NE 560 100 147 I
56-57-5 4-nitroquinoline-1-oxide NE NE NE 388
99-55-8 5-Nitro-o-toluidine Benzenamine, 2-methyl-5-nitro- NE NE 10 157
57-97-6 7,12-Dimethylbenz[a]anthracene Benz[a]anthracene, 7,12-dimethyl- NE NE 10 93
83-32-9 Acenaphthene Acenaphthylene, 1,2-dihydro- 80 -- 10 1
208-96-8 Acenaphthylene Acenaphthylene 200 -- 10 2
SW416 Acetic Acid Acetic Acid NE NE NE 416
34256-82-1 Acetochlor 100 490
187022-11-3 Acetochlor ESA 1000 491
184992-44-4 Acetochlor OXA 1000 492
67-64-1 Acetone 2-Propanone 6000 -- 100 3 I
75-05-8 Acetonitrile; Methyl cyanide Acetonitrile NE 42 55 4
98-86-2 Acetophenone Ethanone, 1-phenyl- NE 700 10 5
50594-66-6 Acifluorofen Acifluorofen 453
107-02-8 Acrolein 2-Propenal NE 4 53 7
79-06-1 Acrylamide Acrylamide 0.008 -- NE 429
107-13-1 Acrylonitrile 2-Propenenitrile NE NE 200 8 I
15972-60-8 Alachlor 0.4 469
309-00-2 Aldrin 1,4:5,8- NE 0.002 0.05 9
SW337 Alkalinity NE NE NE 337
107-05-1 Allyl chloride 1-Propene, 3-chloro- NE NE 10 10
319-84-6 alpha-BHC Cyclohexane,1,2,3,4,5,6-hexachloro- NE 0.006 0.05 24
319-84-6 alpha-Hexachlorocyclohexane α-Benzenehexachloride NE 0.006 NE 501
-- Aluminum Aluminum NE 3500 NE 454
7429-90-5 Aluminum NE 3500 NE 438
7664-41-7 Ammonia Ammonia NE 1500 NE 435
62-53-3 Aniline NE NE NE 381
120-12-7 Anthracene Anthracene 2000 -- 10 12
7440-36-0 Antimony Antimony NE 1 6 13 I
140-57-8 Aramite NE NE NE 382
12674-11-2 Aroclor 1016 congener of PCB; see (1336-36-3) NE NE NE 401
11104-28-2 Aroclor 1221 congener of PCB; see (1336-36-3) NE NE NE 402
11141-16-5 Aroclor 1232 congener of PCB; see (1336-36-3) NE NE NE 403
53469-21-9 Aroclor 1242 congener of PCB; see (1336-36-3) NE NE NE 404
12672-29-6 Aroclor 1248 congener of PCB; see (1336-36-3) NE NE NE 405
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 3 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
11097-69-1 Aroclor 1254 congener of PCB; see (1336-36-3) NE NE NE 406
11096-82-5 Aroclor 1260 congener of PCB; see (1336-36-3) NE NE NE 407
7440-38-2 Arsenic Arsenic 10 -- 10 14 I
7440-39-3 Barium Barium 700 -- 100 15 I
25057-89-0 Bentazon NE NE NE 462
100-52-7 Benzaldehyde Phenylmethanal, NE 700 NE 496
71-43-2 Benzene Benzene 1 -- 1 16 I
122-09-8 Benzeneethanamine, alpha,alpha- NE NE NE 386
92-87-5 Benzidine NE NE NE 383
56-55-3 Benzo[a]anthracene; Benz[a]anthracene 0.05 -- 10 17
50-32-8 Benzo[a]pyrene Benzo[a]pyrene 0.005 -- 10 21
205-99-2 Benzo[b]fluoranthene Benz[e]acephenanthrylene 0.05 -- 10 18
191-24-2 Benzo[ghi]perylene Benzo[ghi]perylene 200 -- 10 20
207-08-9 Benzo[k]fluoranthene Benzo[k]fluoranthene 0.5 -- 10 19
65-85-0 Benzoic Acid 30000 28000 NE 395
100-51-6 Benzyl alcohol Benzenemethanol NE 700 20 22
7440-41-7 Beryllium Beryllium NE 4 1 23 I
319-85-7 beta-BHC Cyclohexane,1,2,3,4,5,6-hexachloro- NE 0.019 0.05 25
319-85-7 beta-Hexachlorocyclohexane β-Benzenehexachloride NE 0.02 NE 502
SW347 Bicarbonate (as CaCO3) NE NE NE 347
SW316 Biological Oxygen Demand BOD NE NE NE 316
101-84-8 biphenyl ether biphenyl ether NE NE 10 423
108-60-1 Bis(2-chloro-1-methylethyl) ether; 2,2'- Propane, 2,2'-oxybis[1-chloro- NE NE 10 46
111-91-1 Bis(2-chloroethoxy)methane Ethane, 1,1'-[methylenebis(oxy)]bis [2- NE NE 10 42
111-44-4 Bis(2-chloroethyl)ether; Dichloroethyl Ethane, 1,1'-oxybis[2-chloro- NE 0.031 10 43
39638-32-9 Bis(2-chloroisopropyl) ether 0.03 NE NE 384
117-81-7 Bis(2-ethylhexyl) phthalate 1,2-Benzenedicarboxylic acid, bis(2- 3 NE 15 111
7440-42-8 Boron Boron 700 -- NE 428
108-86-1 Bromobenzene NE NE NE 360
74-97-5 Bromochloromethane; Methane, bromochloro- NE 0.6 3 28 I
75-27-4 Bromodichloromethane; Methane, bromodichloro- 0.6 -- 1 29 I
75-25-2 Bromoform; Tribromomethane Methane, tribromo- 4 -- 3 30 I
71-36-3 Butanol n n-Butyl Alcohol NE 700 470
78-92-2 Butanol sec sec-Butyl Alcohol NE 10000 483
85-68-7 Butyl benzyl phthalate; Benzyl butyl 1,2-Benzenedicarboxylicacid, butyl 1000 -- 10 32
SW418 Butyric Acid Butyric Acid NE NE NE 418
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 4 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
7440-43-9 Cadmium Cadmium 2 -- 1 34 I
7440-70-2 Calcium NE NE NE 375
471-34-1 Calcium carbonate NE NE NE 464
105-60-2 Caprolactam 4000 NE NE 440
86-74-8 Carbazole dibenzopyrrole, diphenylenimine, NE 2 NE 497
1563-66-2 Carbofuran Carbofuran 40 NE NE 430
124-38-9 Carbon Dioxide NE NE NE 459
SW413 Carbon Dioxide (CO2) CO2 Gas NE NE NE 413
75-15-0 Carbon disulfide Carbon disulfide 700 -- 100 35 I
56-23-5 Carbon tetrachloride Methane, tetrachloro- 0.3 -- 1 36 I
SW348 Carbonate (as CaCO3) NE NE NE 348
7440-44-0 Charcoal NE NE NE 466
SW317 Chemical Oxygen Demand COD NE NE NE 317
57-74-9 Chlordane 4,7-Methano-1H-indene,1,2,4,5,6,7,8,8- 0.1 -- 0.5 339
12789-03-6 Chlordane (constituents) NE NE NE 400
5103-71-9 Chlordane, alpha cis-Chlordane NE NE NE 379
5103-74-2 Chlordane, beta trans-Chlordane NE NE NE 378
5566-34-7 Chlordane, gamma NE NE NE 399
16887-00-6 Chloride Chloride 455
SW301 Chloride 250000 -- NE 301
108-90-7 Chlorobenzene Benzene, chloro- 50 -- 3 39 I
510-15-6 Chlorobenzilate Benzeneacetic acid, 4-chloro-(4- NE NE 10 40
75-00-3 Chloroethane; Ethyl chloride Ethane, chloro- 3000 -- 10 41 I
67-66-3 Chloroform; Trichloromethane Methane, trichloro- 70 -- 5 44 I
126-99-8 Chloroprene 1,3-Butadiene, 2-chloro- NE NE 20 50
7440-47-3 Chromium Chromium 10 -- 10 51 I
218-01-9 Chrysene Chrysene 5 -- 10 52
156-59-2 cis-1,2-Dichloroethylene; cis-1,2- Ethene, 1,2-dichloro-,(Z)- 70 -- 5 78 I
10061-01-5 cis-1,3-Dichloropropene 1-Propene, 1,3-dichloro-, (Z)- 0.4 -- 1 86 I
7440-48-4 Cobalt Cobalt NE 1 10 53 I
SW309 Coliform (total)1 NE NE 309
SW310 Color (color units) 15 NE NE 310
7440-50-8 Copper Copper 1000 -- 10 54 I
57-12-5 Cyanide Cyanide 70 -- 10 58
75-99-0 Dalapon NE 200 NE 355
3424-82-6 DDE o,p-DDE 0.1 472
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 5 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
319-86-8 delta-BHC Cyclohexane,1,2,3,4,5,6-hexachloro- NE 0.019 0.05 26
SW318 Depth To Water (ft) DTW NE NE NE 318
117-81-7 Di(2-ethylhexyl)phthalate Di(2-ethylhexyl)phthalate, DEHP 2.5 -- NE 431
2303-16-4 Diallate Carbamothioic acid,bis(1-methylethyl)-, NE NE 10 63
53-70-3 Dibenz[a,h]anthracene Dibenz[a,h]anthracene 0.005 -- 10 64
132-64-9 Dibenzofuran Dibenzofuran NE 28 10 65
124-48-1 Dibromochloromethane; Methane, dibromochloro- 0.4 0.41 3 66 I
1918-00-9 Dicamba NE NE NE 353
79-43-6 Dichloroacetic Acid NE 0.7 NE 480
75-71-8 Dichlorodifluoromethane; CFC 12 Methane,dichlorodifluoro- 1000 -- 5 74
60-57-1 Dieldrin 2,7:3,6-Dimethanonaphth[2,3- 0.002 -- 0.075 88
84-66-2 Diethyl phthalate 1,2-Benzenedicarboxylicacid, diethyl 6000 -- 10 90
60-51-5 Dimethoate Phosphorodithioic acid,O,O-dimethyl S- NE NE 20 91
131-11-3 Dimethyl phthalate 1,2-Benzenedicarboxylicacid, dimethyl NE NE 10 96
84-74-2 Di-n-butyl phthalate 1,2-Benzenedicarboxylic acid, dibutyl 700 -- 10 33
117-84-0 Di-n-octyl phthalate 1,2-Benzenedicarboxylicacid, dioctyl 100 -- 10 168
88-85-7 Dinoseb; DNBP; 2-sec-Butyl-4,6- Phenol, 2-(1-methylpropyl)-4,6-dinitro- NE 7 1 102
1746-01-6 Dioxin 2,3,7,8-TCDD 0.2 NE NE 441
101-84-8 Diphenyl ether Diphenyl oxide; 1,1'-Oxybisbenzene; NE 100 NE 498
122-39-4 Diphenylamine Benzenamine, N-phenyl- NE NE 10 103
85-00-7 Diquat 20 473
74-82-8 Dissolved Methane Dissolved Methane 456
7782-44-7 Dissolved Oxygen NE NE NE 356
298-04-4 Disulfoton Phosphorodithioic acid,O,O-diethyl S-[2- 0.3 -- 10 104
3648-20-2 Diundecyl phthalate Santicizer 711 100 NE NE 442
959-98-8 Endosulfan I 6,9-Methano-2,4,3-benzodiox- 40 NE 0.1 105
33213-65-9 Endosulfan II 6,9-Methano-2,4,3- -- 42 0.1 106
1031-07-8 Endosulfan sulfate 6,9-Methano-2,4,3- NE 40 0.1 107
145-73-3 Endothall 100 474
72-20-8 Endrin 2,7:3,6-Dimethanonaphth[2,3-b]oxirene, 2 -- 0.1 108
7421-93-4 Endrin aldehyde 1,2,4-Methenocyclo-penta[cd]pentalene- 2 -- 0.1 109
106-89-8 Epichlorohydrin 4 NE NE 443
74-84-0 Ethane- Dissolved NE NE NE 331
64-17-5 Ethanol Ethyl alcohol, Ethyl hydrate, NE 4000 NE 499
74-85-1 Ethene- Dissolved NE NE NE 332
141-78-6 Ethyl acetate 3000 NE NE 444
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 6 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
97-63-2 Ethyl methacrylate 2-Propenoic acid, 2-methyl-, ethyl NE NE 10 112
62-50-0 Ethyl methanesulfonate Methanesulfonic acid,ethyl ester NE NE 20 113
637-92-3 Ethyl tert-butyl ether ETBE, Ethyl tertiary butyl ether NE 47 NE 500
100-41-4 Ethylbenzene Benzene, ethyl- 600 -- 1 110 I
107-21-1 ethylene glycol ethylene glycol 10000 -- 10,000 424
52-85-7 Famphur Phosphorothioic acid, O-[4- NE NE 20 114
SW334 Ferrous Iron- Dissolved NE NE NE 334
206-44-0 Fluoranthene Fluoranthene 300 -- 10 115
86-73-7 Fluorene 9H-Fluorene 300 -- 10 116
16984-48-8 Fluoride 2000 -- 2000 312
SW313 Foaming Agents 500 -- NE 313
50-00-0 Formaldehyde 600 NE NE 445
59-89-9 gamma-BHC (Lindane) gamma-BHC (Lindane) 457
58-89-9 gamma-BHC; Lindane Cyclohexane,1,2,3,4,5,6-hexachloro- 0.03 -- 0.05 27
SW314 Gross Alpha 15 NE NE 314
SW427 Groundwater Elevation (feet) GW Elevation (feet) NE NE NE 427
SW319 Head (ft mean sea level) NE NE NE 319
76-44-8 Heptachlor 4,7-Methano-1H-indene,1,4,5,6,7,8,8- 0.008 -- 0.05 117
1024-57-3 Heptachlor epoxide 2,5-Methano-2H-indeno[1,2- 0.004 -- 0.075 118
142-82-5 Heptane Heptane 400 -- NE 432
118-74-1 Hexachlorobenzene Benzene, hexachloro- 0.02 -- 10 119
87-68-3 Hexachlorobutadiene 1,3-Butadiene,1,1,2,3,4,4-hexachloro- 0.4 0.44 10 120
608-73-1 Hexachlorocyclohexane isomers 0.02 NE NE 446
77-47-4 Hexachlorocyclopentadiene 1,3-Cyclopentadiene,1,2,3,4,5,5- NE 50 10 121
67-72-1 Hexachloroethane Ethane, hexachloro- NE 2.5 10 122
70-30-4 Hexachlorophene NE NE NE 387
1888-71-7 Hexachloropropene 1-Propene, 1,1,2,3,3,3-hexachloro- NE NE 10 123
142-62-1 Hexanoic Acid NE NE NE 485
133-74-0 Hydrogen Gas Dissolved Hydrogen Gas NE NE NE 420
SW338 Hydrogen Sulfide NE NE NE 338
646-07-1 i-Hexonic Acid NE NE NE 486
193-39-5 Indeno(1,2,3-cd)pyrene Indeno[1,2,3-cd]pyrene 0.05 -- 10 125
503-74-2 i-Pentanoic Acid NE NE NE 488
7439-89-6 Iron 300 -- 300 340
78-83-1 Isobutyl alcohol 1-Propanol, 2-methyl- NE NE 100 126
465-73-6 Isodrin 1,4,5,8-Dimethanonaphthalene,1,2,3,4,1 NE NE 20 127
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 7 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
78-59-1 Isophorone 2-Cyclohexen-1-one,3,5,5-trimethyl- 40 -- 10 128
108-20-3 Isopropyl ether 70 -- NE 366
98-82-8 Isopropylbenzene 70 -- NE 367
120-58-1 Isosafrole 1,3-Benzodioxole, 5-(1-propenyl)- NE NE 10 129
143-50-0 Kepone 1,3,4-Metheno-2H-cyclobuta- NE NE 20 130
SW415 Lactic Acid Lactic Acid NE NE NE 415
SW329 Landfill Gas LFG NE NE NE 329
7439-92-1 Lead Lead 15 -- 10 131 I
SW374 m-&p-Cresol (combined) NE NE NE 374
SW359 m-&p-Xylene (combined) NE NE NE 359
7439-95-4 Magnesium NE NE NE 376
7439-96-5 Manganese 50 -- 50 342
SW335 Manganese- Dissolved 50 -- 50 335
94-74-6 MCPA NE NE NE 351
108-39-4 m-Cresol; 3-Methylphenol Phenol, 3-methyl- 400 -- 10 345
541-73-1 m-Dichlorobenzene; 1,3- Benzene, 1,3-dichloro- 200 -- 5 70
99-65-0 m-Dinitrobenzene Benzene, 1,3-dinitro- NE NE 20 97
93-65-2 Mecopop, MCPP NE NE NE 354
7439-97-6 Mercury Mercury 1 -- 0.2 132
126-98-7 Methacrylonitrile 2-Propenenitrile, 2-methyl- NE NE 100 133
SW333 Methane- Dissolved NE NE NE 333
67-56-1 Methanol 4000 NE NE 448
91-80-5 Methapyrilene 1,2,Ethanediamine, N,N-dimethyl-N'-2- NE NE 100 134
72-43-5 Methoxychlor Benzene, 1,1'- 40 -- 1 135
72-43-5 Methoxychlor 40 NE NE 449
74-83-9 Methyl bromide; Bromomethane Methane, bromo- NE 10 10 136 I
74-87-3 Methyl chloride; Chloromethane Methane, chloro- 3 -- 1 137 I
78-93-3 Methyl ethyl ketone; MEK; 2- 2-Butanone 4000 -- 100 141 I
74-88-4 Methyl iodide; Iodomethane Methane, iodo- NE NE 10 142 I
108-10-1 Methyl Isobutyl Ketone 100 493
80-62-6 Methyl methacrylate 2-Propenoic acid, 2-methyl-, methyl NE 25 30 143
66-27-3 Methyl methanesulfonate Methanesulfonic acid,methyl ester NE NE 10 144
298-00-0 Methyl parathion; Parathion methyl Phosphorothioic acid,O,O-dimethyl NE NE 10 146
2037-26-5 Methylbenzene NE NE NE 461
74-95-3 Methylene bromide; Methane, dibromo- NE 70 10 139 I
75-09-2 Methylene chloride; Methane, dichloro- 5 -- 1 140 I
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 8 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
1634-04-4 Methyl-tert-butyl ether (MTBE) 20 -- NE 369
99-09-2 m-Nitroaniline; 3-Nitroaniline Benzenamine, 3-nitro- NE NE 50 153
7439-98-7 Molybdenum NE NE NE 397
108-38-3 m-Xylene NE NE NE 409
91-20-3 Naphthalene Naphthalene 6 -- 10 148
104-51-8 n-Butylbenzene 70 -- NE 361
110-54-3 n-Hexane 400 NE NE 447
7440-02-0 Nickel Nickel 100 -- 50 152 I
14797-55-8 Nitrate (as N)10000 -- 10000 303
14797-65-0 Nitrite (as N)1000 -- 1000 304
98-95-3 Nitrobenzene Benzene, nitro- NE NE 10 156
7727-37-9 Nitrogen NE NE NE 467
55-18-5 N-Nitrosodiethylamine Ethanamine, N-ethyl-N-nitroso- NE NE 20 160
62-75-9 N-Nitrosodimethylamine Methanamine, N-methyl-N-nitroso- 0.0007 -- 10 161
924-16-3 N-Nitrosodi-n-butylamine 1-Butanamine, N-butyl-N-nitroso- NE NE 10 162
86-30-6 N-Nitrosodiphenylamine Benzenamine, N-nitroso-N-phenyl- NE NE 10 163
SW426 N- N- NE NE 10 426
SW439 N-NE NE NE 439
621-64-7 N-Nitrosodipropylamine; N-Nitroso-N- 1-Propanamine, N-nitroso-N-propyl- NE NE 10 164
10595-95-6 N-Nitrosomethylethalamine Ethanamine, N-methyl-N-nitroso- NE NE 10 165
59-89-2 N-Nitrosomorpholine NE NE NE 389
100-75-4 N-Nitrosopiperidine Piperidine, 1-nitroso- NE NE 20 166
930-55-2 N-Nitrosopyrrolidine Pyrrolidine, 1-nitroso- NE NE 10 167
SW419 No2/No3 (nitrate & nitrite reported NOX NE NE NE 419
103-65-1 n-Propylbenzene 70 NE NE 370
126-68-1 O,O,O-Triethyl phosphorothioate Phosphorothioic acid,O,O,O-triethyl NE NE 10 207
297-97-2 O,O-Diethyl O-2-pyrazinyl Phosphorothioic acid,O,O-diethyl O- NE NE 20 89
136777-61-2 o,p-Xylene NE NE NE 460
95-49-8 o-Chlorotoluene 2-chlorotoluene 100 NE NE 364
95-48-7 o-Cresol; 2-Methylphenol Phenol, 2-methyl- NE 400 10 56
95-50-1 o-Dichlorobenzene; 1,2- Benzene, 1,2-dichloro- 20 -- 5 69 I
88-74-4 o-Nitroaniline; 2-Nitroaniline Benzenamine, 2-nitro- NE NE 50 154
88-75-5 o-Nitrophenol; 2-Nitrophenol Phenol, 2-nitro- NE NE 10 158
SW437 Orthophosphate Phosphorus NE NE NE 437
95-53-4 o-Toluidine Benzenamine, 2-methyl- NE NE 10 197
23135-22-0 Oxamyl 200 NE NE 450
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 9 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
SW336 Oxygen Reduction Potential (mV) ORP NE NE NE 336
96-47-6 o-Xylene NE NE NE 408
60-11-7 p-(Dimethylamino)azobenzene Benzenamine, N,N-dimethyl-4- NE NE 10 92
56-38-2 Parathion Phosphorothioic acid,O,O-diethyl-O-(4- NE NE 10 169
106-47-8 p-Chloroaniline Benzenamine, 4-chloro- NE NE 20 38
59-50-7 p-Chloro-m-cresol; 4-Chloro-3- Phenol, 4-chloro-3-methyl- NE NE 20 45
106-43-4 p-Chlorotoluene NE 24 NE 365
106-44-5 p-Cresol; 4-Methylphenol Phenol, 4-methyl- 40 NE-- 10 344
99-87-6 p-Cymene NE 25 NE 368
106-46-7 p-Dichlorobenzene; 1,4- Benzene, 1,4-dichloro- 6 -- 1 71 I
608-93-5 Pentachlorobenzene Benzene, pentachloro- NE NE 10 171
76-01-7 Pentachloroethane NE NE NE 380
82-68-8 Pentachloronitrobenzene Benzene,pentachloronitro- NE NE 20 172
87-86-5 Pentachlorophenol Phenol, pentachloro- 0.3 -- 25 173
109-52-4 Pentanoic Acid NE NE NE 487
7790-98-9 Perchlorate and Perchlorate Salts 2 494
335-67-1 Perfluorooctanoic acid PFOA, C8 2 484
SW307 petroleum aliphatic carbon fraction class 10000 -- NE 307
SW305 petroleum aliphatic carbon fraction class 400 -- NE 305
SW306 petroleum aliphatic carbon fraction class 700 -- NE 306
SW308 petroleum aromatics carbon fraction 200 -- NE 308
SW320 pH (field)NE NE NE 320
SW321 pH (lab)NE NE NE 321
62-44-2 Phenacetin Acetamide, N-(4-ethoxyphenyl) NE NE 20 174
85-01-8 Phenanthrene Phenanthrene 200 -- 10 175
108-95-2 Phenol Phenol 30 -- 10 177
298-02-2 Phorate Phosphorodithioic acid,O,O-diethyl S- 1 -- 10 178
96-91-3 Picramic Acid 2-amino-4,6-dinitiphenol NE 0.7 NE 482
100-01-6 p-Nitroaniline; 4-Nitroaniline Benzenamine, 4-nitro- NE NE 20 155
100-02-7 p-Nitrophenol; 4-Nitrophenol Phenol, 4-nitro- NE NE 50 159
1336-36-3 Polychlorinated biphenyls; PCBs 1,1'-Biphenyl,chloro derivatives Method NE 0.09 2 434
7440-09-7 Potassium NE NE NE 377
106-50-3 p-Phenylenediamine 1,4-Benzenediamine NE NE 10 176
23950-58-5 Pronamide Benzamide, 3,5-dichloro-N-(1,1- NE NE 10 179
SW417 Propionic Acid Propionic Acid NE NE NE 417
107-12-0 Propionitrile; Ethyl cyanide Propanenitrile NE NE 150 180
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 10 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
57-55-6 Propylene Glycol NE 140,000 NE 507
106-42-3 p-Xylene NE NE NE 410
129-00-0 Pyrene Pyrene 200 -- 10 181
110-86-1 Pyridine NE 7 NE 391
SW414 Pyruvic Acid Pyruvic Acid NE NE NE 414
94-59-7 Safrole 1,3-Benzodioxole, 5-(2-propenyl)- NE NE 10 182
135-98-8 sec-Butylbenzene 70 -- NE 362
7782-49-2 Selenium Selenium 20 -- 10 183 I
7440-22-4 Silver Silver 20 -- 10 184 I
93-72-1 Silvex; 2,4,5-TP Propanoic acid, 2-(2,4,5- 50 -- 2 185
122-34-9 Simazine 4 NE NE 451
7440-23-5 Sodium NE 20000 NE 322
SW323 SpecCond (field)NE NE NE 323
SW324 SpecCond (lab)NE NE NE 324
7440-24-6 Strontium NE NE NE 465
100-42-5 Styrene Benzene, ethenyl- 70 -- 1 186 I
14808-79-8 Sulfate 250000 -- 250000 315
18496-25-8 Sulfide Sulfide NE NE 1000 187
3689-24-5 Sulfotep NE NE NE 392
99-35-4 sym-Trinitrobenzene Benzene, 1,3,5-trinitro- NE NE 10 208
SW325 Temp (oC)NE NE NE 325
994-05-8 tert-Amyl methyl ether TAME, 2-methoxy-2-methylbutane NE 128 NE 504
98-06-6 tert-Butylbenzene 70 -- NE 363
75-65-0 Tertiary Butyl Alcohol tert-butanol NE 10 NE 505
127-18-4 Tetrachloroethylene; Tetrachloroethene; Ethene, tetrachloro- 0.7 -- 1 192 I
109-99-9 Tetrahydrofuran NE NE NE 458
7440-28-0 Thallium Thallium NE 0.28 5.5 194 I
7440-31-5 Tin Tin NE 2000 100 195
108-88-3 Toluene Benzene, methyl- 600 -- 1 196 I
SW328 Top Of Casing (ft mean sea level) TOC NE NE NE 328
SW425 Total BHC NE 0.019 NE 425
SW311 Total Dissolved Solids TDS 500000 -- NE 311
SW436 Total Fatty Acids Total Fatty Acids NE NE NE 436
E-10195 Total Organic Carbon NE NE NE 357
SW396 Total Organic Halides NE NE NE 396
7723-14-0 Total Phosphorus Total Phosphorus NE NE NE 412
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
Page 11 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
CAS Number Name Other Names 2L Std. GWP* Std. SWSL** SW ID App I
SW343 Total Suspended Solids NE NE NE 343
SW411 Total Well Depth (ft) TD NE NE NE 411
8001-35-2 Toxaphene Toxaphene 0.03 -- 1.5 198
156-60-5 trans-1,2-Dichloroethylene; trans-1,2- Ethene, 1,2-dichloro-,(E)- 100 -- 5 79 I
10061-02-6 trans-1,3-Dichloropropene 1-Propene, 1,3-dichloro-, (E)- 0.4 -- 1 87 I
110-57-6 trans-1,4-Dichloro-2-butene 2-Butene, 1,4-dichloro-, (E)- NE NE 100 73 I
79-01-6 Trichloroethylene; Trichloroethene Ethene, trichloro- 3 -- 1 201 I
75-69-4 Trichlorofluoromethane; CFC-11 Methane,trichlorofluoro- 2000 -- 1 203 I
SW330 Turbidity NE NE NE 330
7440-62-2 Vanadium Vanadium NE 0.3 25 209 I
108-05-4 Vinyl acetate Acetic acid, ethenylester NE 88 50 210 I
75-01-4 Vinyl chloride; Chloroethene Ethene, chloro- 0.03 -- 1 211 I
1330-20-7 Xylene (total) (o-,m-,and p-, Benzene, dimethyl 500 -- 5 346 I
7440-66-6 Zinc Zinc 1000 -- 10 213 I
* GWP = Groundwater Protection
** SWSL = Solid Waste
Last updated: 6/13/2011 8:19:15 AM
N.C. Department of Environment and Natural Resources
1601 Mail Service Center, Raleigh, NC 27699-1601
Headquarters (Environment and Natural Resources Building): 217 W. Jones St.
Archdale Building: 512 N. Salisbury St.
Toll Free:[phone]
Page 12 of 12NCDENR - Constituent List
5/5/2015http://portal.ncdenr.org/web/wm/sw/envmonitoringlist
Water Quality Monitoring Report
2015 Annual Sampling Event

ATTACHMENT 3
Laboratory Analytical Results
Pace Analytical Services, Inc.

#=CL#
June 12, 2015
LIMS USE: FR - MICHAEL COBB
LIMS OBJECT ID: 92250449
92250449
Project:
Pace Project No.:
RE:
Mr. Michael Cobb
SCS Engineers
2520 Whitehall Park Drive
Suite 450
Charlotte, NC 28273
ANSON LILESVILLE GW
Dear Mr. Cobb:
Enclosed are the analytical results for sample(s) received by the laboratory on May 19, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 47
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 47
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92250449001 MW-A EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AHVK
EPA 8260 50 PASI-CGAW
SM 4500-S2D 1 PASI-AMAB
SM 5210B 1 PASI-AMLS
EPA 300.0 2 PASI-AAES2
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ASER
SM 5220D 1 PASI-AMAB
SM 5310B 1 PASI-AAES2
92250449002 MW-B EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AHVK
EPA 8260 50 PASI-CGAW
SM 4500-S2D 1 PASI-AMAB
SM 5210B 1 PASI-AMLS
EPA 300.0 2 PASI-AAES2
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ASER
SM 5220D 1 PASI-AMAB
SM 5310B 1 PASI-AAES2
92250449003 MW-C EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AHVK
EPA 8260 50 PASI-CGAW
SM 4500-S2D 1 PASI-AMAB
SM 5210B 1 PASI-AMLS
EPA 300.0 2 PASI-AAES2
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ASER
SM 5220D 1 PASI-AMAB
SM 5310B 1 PASI-AAES2
92250449004 MW-D EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AHVK
EPA 8260 50 PASI-CGAW
SM 4500-S2D 1 PASI-AMAB
SM 5210B 1 PASI-AMLS
EPA 300.0 2 PASI-AAES2
EPA 353.2 1 PASI-ADMN
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 47
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-Cl-E 1 PASI-ASER
SM 5220D 1 PASI-AMAB
SM 5310B 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-A Lab ID:92250449001 Collected:05/18/15 15:25 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 05/22/15 19:37 7440-36-005/21/15 16:205.0 1
Arsenic ND ug/L 05/22/15 19:37 7440-38-205/21/15 16:2010.0 1
Barium 18.2 ug/L 05/22/15 19:37 7440-39-305/21/15 16:205.0 1
Beryllium ND ug/L 05/22/15 19:37 7440-41-705/21/15 16:201.0 1
Cadmium ND ug/L 05/22/15 19:37 7440-43-905/21/15 16:201.0 1
Chromium ND ug/L 05/22/15 19:37 7440-47-305/21/15 16:205.0 1
Cobalt ND ug/L 05/22/15 19:37 7440-48-405/21/15 16:205.0 1
Copper ND ug/L 05/22/15 19:37 7440-50-805/21/15 16:205.0 1
Lead ND ug/L 05/22/15 19:37 7439-92-105/21/15 16:205.0 1
Nickel ND ug/L 05/22/15 19:37 7440-02-005/21/15 16:205.0 1
Selenium ND ug/L 05/22/15 19:37 7782-49-205/21/15 16:2010.0 1
Silver ND ug/L 05/22/15 19:37 7440-22-405/21/15 16:205.0 1
Thallium ND ug/L 05/22/15 19:37 7440-28-005/21/15 16:205.4 1
Vanadium ND ug/L 05/22/15 19:37 7440-62-205/21/15 16:205.0 1
Zinc ND ug/L 05/22/15 19:37 7440-66-605/21/15 16:2010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/26/15 15:27 7439-97-605/23/15 17:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/23/15 14:56 67-64-125.0 1
Acrylonitrile ND ug/L 05/23/15 14:56 107-13-110.0 1
Benzene ND ug/L 05/23/15 14:56 71-43-21.0 1
Bromochloromethane ND ug/L 05/23/15 14:56 74-97-51.0 1
Bromodichloromethane ND ug/L 05/23/15 14:56 75-27-41.0 1
Bromoform ND ug/L 05/23/15 14:56 75-25-21.0 1
Bromomethane ND ug/L 05/23/15 14:56 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/23/15 14:56 78-93-35.0 1
Carbon disulfide ND ug/L 05/23/15 14:56 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/23/15 14:56 56-23-51.0 1
Chlorobenzene ND ug/L 05/23/15 14:56 108-90-71.0 1
Chloroethane ND ug/L 05/23/15 14:56 75-00-31.0 1
Chloroform ND ug/L 05/23/15 14:56 67-66-31.0 1
Chloromethane ND ug/L 05/23/15 14:56 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/23/15 14:56 96-12-82.0 1
Dibromochloromethane ND ug/L 05/23/15 14:56 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/23/15 14:56 106-93-41.0 1
Dibromomethane ND ug/L 05/23/15 14:56 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/23/15 14:56 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/23/15 14:56 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/23/15 14:56 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/23/15 14:56 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/23/15 14:56 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/23/15 14:56 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/23/15 14:56 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/23/15 14:56 156-60-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-A Lab ID:92250449001 Collected:05/18/15 15:25 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 05/23/15 14:56 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/23/15 14:56 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/23/15 14:56 10061-02-61.0 1
Ethylbenzene ND ug/L 05/23/15 14:56 100-41-41.0 1
2-Hexanone ND ug/L 05/23/15 14:56 591-78-65.0 1
Iodomethane ND ug/L 05/23/15 14:56 74-88-45.0 1
Methylene Chloride ND ug/L 05/23/15 14:56 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/23/15 14:56 108-10-15.0 1
Styrene ND ug/L 05/23/15 14:56 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/23/15 14:56 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/23/15 14:56 79-34-51.0 1
Tetrachloroethene ND ug/L 05/23/15 14:56 127-18-41.0 1
Toluene ND ug/L 05/23/15 14:56 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/23/15 14:56 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/23/15 14:56 79-00-51.0 1
Trichloroethene ND ug/L 05/23/15 14:56 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/23/15 14:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/23/15 14:56 96-18-41.0 1
Vinyl acetate ND ug/L 05/23/15 14:56 108-05-42.0 1
Vinyl chloride ND ug/L 05/23/15 14:56 75-01-41.0 1
Xylene (Total)ND ug/L 05/23/15 14:56 1330-20-72.0 1
Surrogates
4-Bromofluorobenzene (S)97 %05/23/15 14:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %05/23/15 14:56 17060-07-070-130 1
Toluene-d8 (S)97 %05/23/15 14:56 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 05/21/15 16:00 18496-25-81001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 05/25/15 13:3505/20/15 11:0220001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Fluoride ND ug/L 05/23/15 02:23 16984-48-85001
Sulfate 3520 ug/L 05/23/15 02:23 14808-79-820001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 05/19/15 23:1220.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3610 ug/L 05/21/15 05:45 16887-00-610001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 05/27/15 14:10250001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-A Lab ID:92250449001 Collected:05/18/15 15:25 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon ND ug/L 05/24/15 04:27 7440-44-010001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-B Lab ID:92250449002 Collected:05/18/15 14:25 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 05/22/15 19:40 7440-36-005/21/15 16:205.0 1
Arsenic ND ug/L 05/22/15 19:40 7440-38-205/21/15 16:2010.0 1
Barium 14.6 ug/L 05/22/15 19:40 7440-39-305/21/15 16:205.0 1
Beryllium ND ug/L 05/22/15 19:40 7440-41-705/21/15 16:201.0 1
Cadmium ND ug/L 05/22/15 19:40 7440-43-905/21/15 16:201.0 1
Chromium ND ug/L 05/22/15 19:40 7440-47-305/21/15 16:205.0 1
Cobalt ND ug/L 05/22/15 19:40 7440-48-405/21/15 16:205.0 1
Copper ND ug/L 05/22/15 19:40 7440-50-805/21/15 16:205.0 1
Lead ND ug/L 05/22/15 19:40 7439-92-105/21/15 16:205.0 1
Nickel ND ug/L 05/22/15 19:40 7440-02-005/21/15 16:205.0 1
Selenium ND ug/L 05/22/15 19:40 7782-49-205/21/15 16:2010.0 1
Silver ND ug/L 05/22/15 19:40 7440-22-405/21/15 16:205.0 1
Thallium ND ug/L 05/22/15 19:40 7440-28-005/21/15 16:205.4 1
Vanadium ND ug/L 05/22/15 19:40 7440-62-205/21/15 16:205.0 1
Zinc ND ug/L 05/22/15 19:40 7440-66-605/21/15 16:2010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/26/15 15:30 7439-97-605/23/15 17:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/23/15 15:13 67-64-125.0 1
Acrylonitrile ND ug/L 05/23/15 15:13 107-13-110.0 1
Benzene ND ug/L 05/23/15 15:13 71-43-21.0 1
Bromochloromethane ND ug/L 05/23/15 15:13 74-97-51.0 1
Bromodichloromethane ND ug/L 05/23/15 15:13 75-27-41.0 1
Bromoform ND ug/L 05/23/15 15:13 75-25-21.0 1
Bromomethane ND ug/L 05/23/15 15:13 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/23/15 15:13 78-93-35.0 1
Carbon disulfide ND ug/L 05/23/15 15:13 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/23/15 15:13 56-23-51.0 1
Chlorobenzene ND ug/L 05/23/15 15:13 108-90-71.0 1
Chloroethane ND ug/L 05/23/15 15:13 75-00-31.0 1
Chloroform ND ug/L 05/23/15 15:13 67-66-31.0 1
Chloromethane ND ug/L 05/23/15 15:13 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/23/15 15:13 96-12-82.0 1
Dibromochloromethane ND ug/L 05/23/15 15:13 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/23/15 15:13 106-93-41.0 1
Dibromomethane ND ug/L 05/23/15 15:13 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/23/15 15:13 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/23/15 15:13 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/23/15 15:13 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/23/15 15:13 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/23/15 15:13 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/23/15 15:13 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/23/15 15:13 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/23/15 15:13 156-60-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-B Lab ID:92250449002 Collected:05/18/15 14:25 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 05/23/15 15:13 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/23/15 15:13 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/23/15 15:13 10061-02-61.0 1
Ethylbenzene ND ug/L 05/23/15 15:13 100-41-41.0 1
2-Hexanone ND ug/L 05/23/15 15:13 591-78-65.0 1
Iodomethane ND ug/L 05/23/15 15:13 74-88-45.0 1
Methylene Chloride ND ug/L 05/23/15 15:13 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/23/15 15:13 108-10-15.0 1
Styrene ND ug/L 05/23/15 15:13 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/23/15 15:13 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/23/15 15:13 79-34-51.0 1
Tetrachloroethene ND ug/L 05/23/15 15:13 127-18-41.0 1
Toluene ND ug/L 05/23/15 15:13 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/23/15 15:13 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/23/15 15:13 79-00-51.0 1
Trichloroethene ND ug/L 05/23/15 15:13 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/23/15 15:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/23/15 15:13 96-18-41.0 1
Vinyl acetate ND ug/L 05/23/15 15:13 108-05-42.0 1
Vinyl chloride ND ug/L 05/23/15 15:13 75-01-41.0 1
Xylene (Total)ND ug/L 05/23/15 15:13 1330-20-72.0 1
Surrogates
4-Bromofluorobenzene (S)98 %05/23/15 15:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %05/23/15 15:13 17060-07-070-130 1
Toluene-d8 (S)97 %05/23/15 15:13 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide 113 ug/L 05/21/15 16:00 18496-25-81001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 05/25/15 13:3505/20/15 11:0220001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Fluoride ND ug/L 05/23/15 02:56 16984-48-85001
Sulfate ND ug/L 05/23/15 02:56 14808-79-820001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 05/19/15 23:1120.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4360 ug/L 05/21/15 05:47 16887-00-610001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 05/27/15 14:10250001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-B Lab ID:92250449002 Collected:05/18/15 14:25 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon ND ug/L 05/24/15 04:38 7440-44-010001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-C Lab ID:92250449003 Collected:05/18/15 11:05 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 05/22/15 19:43 7440-36-005/21/15 16:205.0 1
Arsenic ND ug/L 05/22/15 19:43 7440-38-205/21/15 16:2010.0 1
Barium 46.0 ug/L 05/22/15 19:43 7440-39-305/21/15 16:205.0 1
Beryllium ND ug/L 05/22/15 19:43 7440-41-705/21/15 16:201.0 1
Cadmium ND ug/L 05/22/15 19:43 7440-43-905/21/15 16:201.0 1
Chromium ND ug/L 05/22/15 19:43 7440-47-305/21/15 16:205.0 1
Cobalt ND ug/L 05/22/15 19:43 7440-48-405/21/15 16:205.0 1
Copper ND ug/L 05/22/15 19:43 7440-50-805/21/15 16:205.0 1
Lead ND ug/L 05/22/15 19:43 7439-92-105/21/15 16:205.0 1
Nickel ND ug/L 05/22/15 19:43 7440-02-005/21/15 16:205.0 1
Selenium ND ug/L 05/22/15 19:43 7782-49-205/21/15 16:2010.0 1
Silver ND ug/L 05/22/15 19:43 7440-22-405/21/15 16:205.0 1
Thallium ND ug/L 05/22/15 19:43 7440-28-005/21/15 16:205.4 1
Vanadium ND ug/L 05/22/15 19:43 7440-62-205/21/15 16:205.0 1
Zinc ND ug/L 05/22/15 19:43 7440-66-605/21/15 16:2010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/26/15 15:32 7439-97-605/23/15 17:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/23/15 15:30 67-64-125.0 1
Acrylonitrile ND ug/L 05/23/15 15:30 107-13-110.0 1
Benzene ND ug/L 05/23/15 15:30 71-43-21.0 1
Bromochloromethane ND ug/L 05/23/15 15:30 74-97-51.0 1
Bromodichloromethane ND ug/L 05/23/15 15:30 75-27-41.0 1
Bromoform ND ug/L 05/23/15 15:30 75-25-21.0 1
Bromomethane ND ug/L 05/23/15 15:30 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/23/15 15:30 78-93-35.0 1
Carbon disulfide ND ug/L 05/23/15 15:30 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/23/15 15:30 56-23-51.0 1
Chlorobenzene ND ug/L 05/23/15 15:30 108-90-71.0 1
Chloroethane ND ug/L 05/23/15 15:30 75-00-31.0 1
Chloroform ND ug/L 05/23/15 15:30 67-66-31.0 1
Chloromethane ND ug/L 05/23/15 15:30 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/23/15 15:30 96-12-82.0 1
Dibromochloromethane ND ug/L 05/23/15 15:30 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/23/15 15:30 106-93-41.0 1
Dibromomethane ND ug/L 05/23/15 15:30 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/23/15 15:30 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/23/15 15:30 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/23/15 15:30 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/23/15 15:30 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/23/15 15:30 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/23/15 15:30 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/23/15 15:30 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/23/15 15:30 156-60-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-C Lab ID:92250449003 Collected:05/18/15 11:05 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 05/23/15 15:30 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/23/15 15:30 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/23/15 15:30 10061-02-61.0 1
Ethylbenzene ND ug/L 05/23/15 15:30 100-41-41.0 1
2-Hexanone ND ug/L 05/23/15 15:30 591-78-65.0 1
Iodomethane ND ug/L 05/23/15 15:30 74-88-45.0 1
Methylene Chloride ND ug/L 05/23/15 15:30 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/23/15 15:30 108-10-15.0 1
Styrene ND ug/L 05/23/15 15:30 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/23/15 15:30 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/23/15 15:30 79-34-51.0 1
Tetrachloroethene ND ug/L 05/23/15 15:30 127-18-41.0 1
Toluene ND ug/L 05/23/15 15:30 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/23/15 15:30 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/23/15 15:30 79-00-51.0 1
Trichloroethene ND ug/L 05/23/15 15:30 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/23/15 15:30 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/23/15 15:30 96-18-41.0 1
Vinyl acetate ND ug/L 05/23/15 15:30 108-05-42.0 1
Vinyl chloride ND ug/L 05/23/15 15:30 75-01-41.0 1
Xylene (Total)ND ug/L 05/23/15 15:30 1330-20-72.0 1
Surrogates
4-Bromofluorobenzene (S)99 %05/23/15 15:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %05/23/15 15:30 17060-07-070-130 1
Toluene-d8 (S)97 %05/23/15 15:30 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 05/21/15 16:00 18496-25-81001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 6810 ug/L 05/25/15 13:3505/20/15 11:0220001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Fluoride ND ug/L 05/23/15 04:33 16984-48-85001
Sulfate ND ug/L 05/23/15 04:33 14808-79-820001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 05/19/15 23:06 M120.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 12500 ug/L 05/21/15 05:48 16887-00-610001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 05/27/15 14:10250001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-C Lab ID:92250449003 Collected:05/18/15 11:05 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 5200 ug/L 05/24/15 04:48 7440-44-010001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-D Lab ID:92250449004 Collected:05/18/15 15:45 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 05/22/15 19:46 7440-36-005/21/15 16:205.0 1
Arsenic ND ug/L 05/22/15 19:46 7440-38-205/21/15 16:2010.0 1
Barium 48.5 ug/L 05/22/15 19:46 7440-39-305/21/15 16:205.0 1
Beryllium ND ug/L 05/22/15 19:46 7440-41-705/21/15 16:201.0 1
Cadmium ND ug/L 05/22/15 19:46 7440-43-905/21/15 16:201.0 1
Chromium ND ug/L 05/22/15 19:46 7440-47-305/21/15 16:205.0 1
Cobalt ND ug/L 05/22/15 19:46 7440-48-405/21/15 16:205.0 1
Copper ND ug/L 05/22/15 19:46 7440-50-805/21/15 16:205.0 1
Lead ND ug/L 05/22/15 19:46 7439-92-105/21/15 16:205.0 1
Nickel 5.2 ug/L 05/22/15 19:46 7440-02-005/21/15 16:205.0 1
Selenium ND ug/L 05/22/15 19:46 7782-49-205/21/15 16:2010.0 1
Silver ND ug/L 05/22/15 19:46 7440-22-405/21/15 16:205.0 1
Thallium ND ug/L 05/22/15 19:46 7440-28-005/21/15 16:205.4 1
Vanadium ND ug/L 05/22/15 19:46 7440-62-205/21/15 16:205.0 1
Zinc 16.3 ug/L 05/22/15 19:46 7440-66-605/21/15 16:2010.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/26/15 15:34 7439-97-605/23/15 17:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/23/15 15:47 67-64-125.0 1
Acrylonitrile ND ug/L 05/23/15 15:47 107-13-110.0 1
Benzene ND ug/L 05/23/15 15:47 71-43-21.0 1
Bromochloromethane ND ug/L 05/23/15 15:47 74-97-51.0 1
Bromodichloromethane ND ug/L 05/23/15 15:47 75-27-41.0 1
Bromoform ND ug/L 05/23/15 15:47 75-25-21.0 1
Bromomethane ND ug/L 05/23/15 15:47 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/23/15 15:47 78-93-35.0 1
Carbon disulfide ND ug/L 05/23/15 15:47 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/23/15 15:47 56-23-51.0 1
Chlorobenzene ND ug/L 05/23/15 15:47 108-90-71.0 1
Chloroethane ND ug/L 05/23/15 15:47 75-00-31.0 1
Chloroform ND ug/L 05/23/15 15:47 67-66-31.0 1
Chloromethane ND ug/L 05/23/15 15:47 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/23/15 15:47 96-12-82.0 1
Dibromochloromethane ND ug/L 05/23/15 15:47 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/23/15 15:47 106-93-41.0 1
Dibromomethane ND ug/L 05/23/15 15:47 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/23/15 15:47 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/23/15 15:47 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/23/15 15:47 110-57-61.0 1
1,1-Dichloroethane ND ug/L 05/23/15 15:47 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/23/15 15:47 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/23/15 15:47 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/23/15 15:47 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/23/15 15:47 156-60-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-D Lab ID:92250449004 Collected:05/18/15 15:45 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 05/23/15 15:47 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/23/15 15:47 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/23/15 15:47 10061-02-61.0 1
Ethylbenzene ND ug/L 05/23/15 15:47 100-41-41.0 1
2-Hexanone ND ug/L 05/23/15 15:47 591-78-65.0 1
Iodomethane ND ug/L 05/23/15 15:47 74-88-45.0 1
Methylene Chloride ND ug/L 05/23/15 15:47 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/23/15 15:47 108-10-15.0 1
Styrene ND ug/L 05/23/15 15:47 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/23/15 15:47 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/23/15 15:47 79-34-51.0 1
Tetrachloroethene ND ug/L 05/23/15 15:47 127-18-41.0 1
Toluene ND ug/L 05/23/15 15:47 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/23/15 15:47 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/23/15 15:47 79-00-51.0 1
Trichloroethene ND ug/L 05/23/15 15:47 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/23/15 15:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/23/15 15:47 96-18-41.0 1
Vinyl acetate ND ug/L 05/23/15 15:47 108-05-42.0 1
Vinyl chloride ND ug/L 05/23/15 15:47 75-01-41.0 1
Xylene (Total)ND ug/L 05/23/15 15:47 1330-20-72.0 1
Surrogates
4-Bromofluorobenzene (S)99 %05/23/15 15:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %05/23/15 15:47 17060-07-070-130 1
Toluene-d8 (S)98 %05/23/15 15:47 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 05/21/15 16:00 18496-25-81001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 05/25/15 13:3505/20/15 11:0220001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Fluoride ND ug/L 05/23/15 05:06 16984-48-85001
Sulfate 2660 ug/L 05/23/15 05:06 14808-79-820001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 61.3 ug/L 05/19/15 23:1720.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 1940 ug/L 05/21/15 05:49 16887-00-610001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 05/27/15 14:10250001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Sample:MW-D Lab ID:92250449004 Collected:05/18/15 15:45 Received:05/19/15 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon ND ug/L 05/24/15 05:10 7440-44-010001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/7853
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1467312
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 05/26/15 14:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1467313LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.32.5 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1467314MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248802020
1467315
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 81 75-12583 32.5ND 2.0 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18529
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1465350
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 05/22/15 19:22
Arsenic ug/L ND 10.0 05/22/15 19:22
Barium ug/L ND 5.0 05/22/15 19:22
Beryllium ug/L ND 1.0 05/22/15 19:22
Cadmium ug/L ND 1.0 05/22/15 19:22
Chromium ug/L ND 5.0 05/22/15 19:22
Cobalt ug/L ND 5.0 05/22/15 19:22
Copper ug/L ND 5.0 05/22/15 19:22
Lead ug/L ND 5.0 05/22/15 19:22
Nickel ug/L ND 5.0 05/22/15 19:22
Selenium ug/L ND 10.0 05/22/15 19:22
Silver ug/L ND 5.0 05/22/15 19:22
Thallium ug/L ND 5.4 05/22/15 19:22
Vanadium ug/L ND 5.0 05/22/15 19:22
Zinc ug/L ND 10.0 05/22/15 19:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1465351LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 454500 91 80-120
Arsenic ug/L 457500 91 80-120
Barium ug/L 451500 90 80-120
Beryllium ug/L 455500 91 80-120
Cadmium ug/L 458500 92 80-120
Chromium ug/L 440500 88 80-120
Cobalt ug/L 452500 90 80-120
Copper ug/L 438500 88 80-120
Lead ug/L 451500 90 80-120
Nickel ug/L 453500 91 80-120
Selenium ug/L 433500 87 80-120
Silver ug/L 228250 91 80-120
Thallium ug/L 461500 92 80-120
Vanadium ug/L 432500 86 80-120
Zinc ug/L 463500 93 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1465352MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250143012
1465353
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 92 75-12590 2500ND463453
Arsenic ug/L 500 94 75-12592 2500ND468460
Barium ug/L 500 92 75-12590 250016.1J 474 466
Beryllium ug/L 500 93 75-12591 2500ND463456
Cadmium ug/L 500 93 75-12592 2500ND466458
Chromium ug/L 500 90 75-12588 1500ND448442
Cobalt ug/L 500 92 75-12590 2500ND458450
Copper ug/L 500 89 75-12587 1500ND444437
Lead ug/L 500 91 75-12589 2500ND456448
Nickel ug/L 500 92 75-12590 2500ND459452
Selenium ug/L 500 88 75-12586 2500ND439430
Silver ug/L 250 92 75-12591 1250ND231228
Thallium ug/L 500 94 75-12593 2500ND473465
Vanadium ug/L 500 88 75-12586 2500ND443433
Zinc ug/L 500 93 75-12593 1500ND472468
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31818
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1466655
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/23/15 10:44
1,1,1-Trichloroethane ug/L ND 1.0 05/23/15 10:44
1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/23/15 10:44
1,1,2-Trichloroethane ug/L ND 1.0 05/23/15 10:44
1,1-Dichloroethane ug/L ND 1.0 05/23/15 10:44
1,1-Dichloroethene ug/L ND 1.0 05/23/15 10:44
1,2,3-Trichloropropane ug/L ND 1.0 05/23/15 10:44
1,2-Dibromo-3-chloropropane ug/L ND 2.0 05/23/15 10:44
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/23/15 10:44
1,2-Dichlorobenzene ug/L ND 1.0 05/23/15 10:44
1,2-Dichloroethane ug/L ND 1.0 05/23/15 10:44
1,2-Dichloropropane ug/L ND 1.0 05/23/15 10:44
1,4-Dichlorobenzene ug/L ND 1.0 05/23/15 10:44
2-Butanone (MEK)ug/L ND 5.0 05/23/15 10:44
2-Hexanone ug/L ND 5.0 05/23/15 10:44
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 05/23/15 10:44
Acetone ug/L ND 25.0 05/23/15 10:44
Acrylonitrile ug/L ND 10.0 05/23/15 10:44
Benzene ug/L ND 1.0 05/23/15 10:44
Bromochloromethane ug/L ND 1.0 05/23/15 10:44
Bromodichloromethane ug/L ND 1.0 05/23/15 10:44
Bromoform ug/L ND 1.0 05/23/15 10:44
Bromomethane ug/L ND 2.0 05/23/15 10:44
Carbon disulfide ug/L ND 2.0 05/23/15 10:44
Carbon tetrachloride ug/L ND 1.0 05/23/15 10:44
Chlorobenzene ug/L ND 1.0 05/23/15 10:44
Chloroethane ug/L ND 1.0 05/23/15 10:44
Chloroform ug/L ND 1.0 05/23/15 10:44
Chloromethane ug/L ND 1.0 05/23/15 10:44
cis-1,2-Dichloroethene ug/L ND 1.0 05/23/15 10:44
cis-1,3-Dichloropropene ug/L ND 1.0 05/23/15 10:44
Dibromochloromethane ug/L ND 1.0 05/23/15 10:44
Dibromomethane ug/L ND 1.0 05/23/15 10:44
Ethylbenzene ug/L ND 1.0 05/23/15 10:44
Iodomethane ug/L ND 5.0 05/23/15 10:44
Methylene Chloride ug/L ND 1.0 05/23/15 10:44
Styrene ug/L ND 1.0 05/23/15 10:44
Tetrachloroethene ug/L ND 1.0 05/23/15 10:44
Toluene ug/L ND 1.0 05/23/15 10:44
trans-1,2-Dichloroethene ug/L ND 1.0 05/23/15 10:44
trans-1,3-Dichloropropene ug/L ND 1.0 05/23/15 10:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1466655
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
trans-1,4-Dichloro-2-butene ug/L ND 1.0 05/23/15 10:44
Trichloroethene ug/L ND 1.0 05/23/15 10:44
Trichlorofluoromethane ug/L ND 1.0 05/23/15 10:44
Vinyl acetate ug/L ND 2.0 05/23/15 10:44
Vinyl chloride ug/L ND 1.0 05/23/15 10:44
Xylene (Total)ug/L ND 2.0 05/23/15 10:44
1,2-Dichloroethane-d4 (S)%95 70-130 05/23/15 10:44
4-Bromofluorobenzene (S)%95 70-130 05/23/15 10:44
Toluene-d8 (S)%100 70-130 05/23/15 10:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1466656LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.950 98 80-125
1,1,1-Trichloroethane ug/L 42.650 85 71-129
1,1,2,2-Tetrachloroethane ug/L 48.750 97 79-124
1,1,2-Trichloroethane ug/L 47.750 95 85-125
1,1-Dichloroethane ug/L 44.950 90 73-126
1,1-Dichloroethene ug/L 48.350 97 66-135
1,2,3-Trichloropropane ug/L 49.050 98 75-130
1,2-Dibromo-3-chloropropane ug/L 44.250 88 71-133
1,2-Dibromoethane (EDB)ug/L 48.850 98 83-124
1,2-Dichlorobenzene ug/L 50.050 100 80-133
1,2-Dichloroethane ug/L 43.050 86 67-128
1,2-Dichloropropane ug/L 48.850 98 75-132
1,4-Dichlorobenzene ug/L 50.250 100 78-130
2-Butanone (MEK)ug/L 82.2100 82 61-144
2-Hexanone ug/L 93.3100 93 68-143
4-Methyl-2-pentanone (MIBK)ug/L 93.4100 93 72-135
Acetone ug/L 79.9100 80 48-146
Acrylonitrile ug/L 218250 87 40-160
Benzene ug/L 47.750 95 80-125
Bromochloromethane ug/L 44.950 90 71-125
Bromodichloromethane ug/L 45.550 91 78-124
Bromoform ug/L 43.950 88 71-128
Bromomethane ug/L 49.350 99 40-160
Carbon disulfide ug/L 45.350 91 50-160
Carbon tetrachloride ug/L 43.750 87 69-131
Chlorobenzene ug/L 50.450 101 81-122
Chloroethane ug/L 28.850 58 39-148
Chloroform ug/L 43.650 87 73-127
Chloromethane ug/L 43.550 87 44-146
cis-1,2-Dichloroethene ug/L 45.450 91 74-124
cis-1,3-Dichloropropene ug/L 48.450 97 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1466656LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 48.250 96 78-125
Dibromomethane ug/L 47.550 95 82-120
Ethylbenzene ug/L 50.150 100 79-121
Iodomethane ug/L 115100 115 39-154
Methylene Chloride ug/L 43.450 87 64-133
Styrene ug/L 50.250 100 84-126
Tetrachloroethene ug/L 49.150 98 78-122
Toluene ug/L 49.050 98 80-121
trans-1,2-Dichloroethene ug/L 46.850 94 71-127
trans-1,3-Dichloropropene ug/L 47.550 95 69-141
trans-1,4-Dichloro-2-butene ug/L 48.750 97 40-160
Trichloroethene ug/L 47.150 94 78-122
Trichlorofluoromethane ug/L 42.050 84 53-137
Vinyl acetate ug/L 89.7100 90 40-160
Vinyl chloride ug/L 41.650 83 58-137
Xylene (Total)ug/L 148150 99 81-126
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1466657MATRIX SPIKE SAMPLE:
MSSpike
Result
92250143001
1,1,1,2-Tetrachloroethane ug/L 20.420 102 70-130ND
1,1,1-Trichloroethane ug/L 16.820 84 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.620 103 70-130ND
1,1,2-Trichloroethane ug/L 19.420 97 70-130ND
1,1-Dichloroethane ug/L 16.920 85 70-130ND
1,1-Dichloroethene ug/L 15.220 76 70-166ND
1,2,3-Trichloropropane ug/L 22.220 111 70-130ND
1,2-Dibromo-3-chloropropane ug/L 14.020 70 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.020 95 70-130ND
1,2-Dichlorobenzene ug/L 20.820 104 70-130ND
1,2-Dichloroethane ug/L 16.920 85 70-130ND
1,2-Dichloropropane ug/L 20.520 103 70-130ND
1,4-Dichlorobenzene ug/L 22.520 111 70-1300.36J
2-Butanone (MEK)ug/L 31.740 79 70-130ND
2-Hexanone ug/L 40.740 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.640 99 70-130ND
Acetone ug/L 31.840 80 70-130ND
Acrylonitrile ug/L 85.4100 85 70-130ND
Benzene ug/L 20.220 101 70-148ND
Bromochloromethane ug/L 17.820 89 70-130ND
Bromodichloromethane ug/L 16.520 83 70-130ND
Bromoform ug/L 17.020 85 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1466657MATRIX SPIKE SAMPLE:
MSSpike
Result
92250143001
Bromomethane ug/L 14.120 70 70-130ND
Carbon disulfide ug/L 12.7 M1206370-130ND
Carbon tetrachloride ug/L 17.320 86 70-130ND
Chlorobenzene ug/L 22.420 112 70-146ND
Chloroethane ug/L 15.420 77 70-130ND
Chloroform ug/L 15.520 78 70-130ND
Chloromethane ug/L 6.1 M1203170-130ND
cis-1,2-Dichloroethene ug/L 18.420 87 70-1300.99J
cis-1,3-Dichloropropene ug/L 18.620 93 70-130ND
Dibromochloromethane ug/L 17.220 86 70-130ND
Dibromomethane ug/L 19.420 97 70-130ND
Ethylbenzene ug/L 21.720 108 70-130ND
Iodomethane ug/L 20.4 M1405170-130ND
Methylene Chloride ug/L 17.020 85 70-130ND
Styrene ug/L 21.620 108 70-130ND
Tetrachloroethene ug/L 21.620 108 70-130ND
Toluene ug/L 20.720 103 70-155ND
trans-1,2-Dichloroethene ug/L 16.420 82 70-130ND
trans-1,3-Dichloropropene ug/L 18.220 91 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.520 98 70-130ND
Trichloroethene ug/L 20.920 104 69-151ND
Trichlorofluoromethane ug/L 13.7 M1206970-130ND
Vinyl acetate ug/L 28.640 71 70-130ND
Vinyl chloride ug/L 8.3 M1204170-130ND
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92250143002
1466658SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L .73J0.66J
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L 5.3 25.2
1,2-Dichloroethane ug/L ND0.43J
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L 10.4 210.1
2-Butanone (MEK)ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92250143002
1466658SAMPLE DUPLICATE:
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L 1.70.73J
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L 8.2 D6614.3
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
Methylene Chloride ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L .35JND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%94 094
4-Bromofluorobenzene (S)%97 196
Toluene-d8 (S)%99 099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/37589
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1464569
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
Sulfide ug/L ND 100 05/21/15 16:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1464570LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 537500 107 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1464571MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250449001
1464572
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 105 90-110105 0500ND530530
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/37555
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1463376
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
BOD, 5 day ug/L ND 2000 05/25/15 13:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1463377LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 214000198000 108 84.6-115.4
Parameter Units
Dup
Result QualifiersRPDResult
92250449003
1463378SAMPLE DUPLICATE:
BOD, 5 day ug/L 6810 06810
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23035
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1466679
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
Fluoride ug/L ND 500 05/22/15 22:04
Sulfate ug/L ND 2000 05/22/15 22:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1466680LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoride ug/L 24102500 97 90-110
Sulfate ug/L 1980020000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1466681MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250550001
1466682
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Fluoride ug/L 2500 102 90-110103 12500ND26902710
Sulfate ug/L 20000 105 90-110105 02000013.2
mg/L
34200 34200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/22991
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1463237
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
Nitrogen, Nitrate ug/L ND 20.0 05/19/15 23:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1463238LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24302500 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1463239MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250449003
1463240
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L M125007990-11079 02500ND19801980
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23002
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1463611
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
Chloride ug/L ND 1000 05/21/15 05:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1463612LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 1960020000 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1463613MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250449001
1463614
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 20000 95 90-11098 22000036102270023300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23058
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1467494
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
Chemical Oxygen Demand ug/L ND 25000 05/27/15 14:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1467495LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 795000750000 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1467496MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250449001
1467497
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 100 90-110100 0750000ND752000752000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23049
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1467306
Associated Lab Samples:92250449001, 92250449002, 92250449003, 92250449004
Matrix:Water
Analyzed
Total Organic Carbon ug/L ND 1000 05/24/15 00:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1467307LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2430025000 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1467308MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250991004
1467309
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Total Organic Carbon ug/L M1250009390-11088 4250008.2
mg/L 31500 30200
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1467310MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250991014
1467311
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 98 90-11097 0250003.0
mg/L 27400 27300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 47
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 47
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92250449
ANSON LILESVILLE GW
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92250449001 MPRP/18529 ICP/16623MW-A EPA 3010 EPA 6010
92250449002 MPRP/18529 ICP/16623MW-B EPA 3010 EPA 6010
92250449003 MPRP/18529 ICP/16623MW-C EPA 3010 EPA 6010
92250449004 MPRP/18529 ICP/16623MW-D EPA 3010 EPA 6010
92250449001 MERP/7853 MERC/7538MW-A EPA 7470 EPA 7470
92250449002 MERP/7853 MERC/7538MW-B EPA 7470 EPA 7470
92250449003 MERP/7853 MERC/7538MW-C EPA 7470 EPA 7470
92250449004 MERP/7853 MERC/7538MW-D EPA 7470 EPA 7470
92250449001 MSV/31818MW-A EPA 8260
92250449002 MSV/31818MW-B EPA 8260
92250449003 MSV/31818MW-C EPA 8260
92250449004 MSV/31818MW-D EPA 8260
92250449001 WET/37589MW-A SM 4500-S2D
92250449002 WET/37589MW-B SM 4500-S2D
92250449003 WET/37589MW-C SM 4500-S2D
92250449004 WET/37589MW-D SM 4500-S2D
92250449001 WET/37555 WET/37560MW-A SM 5210B SM 5210B
92250449002 WET/37555 WET/37560MW-B SM 5210B SM 5210B
92250449003 WET/37555 WET/37560MW-C SM 5210B SM 5210B
92250449004 WET/37555 WET/37560MW-D SM 5210B SM 5210B
92250449001 WETA/23035MW-A EPA 300.0
92250449002 WETA/23035MW-B EPA 300.0
92250449003 WETA/23035MW-C EPA 300.0
92250449004 WETA/23035MW-D EPA 300.0
92250449001 WETA/22991MW-A EPA 353.2
92250449002 WETA/22991MW-B EPA 353.2
92250449003 WETA/22991MW-C EPA 353.2
92250449004 WETA/22991MW-D EPA 353.2
92250449001 WETA/23002MW-A SM 4500-Cl-E
92250449002 WETA/23002MW-B SM 4500-Cl-E
92250449003 WETA/23002MW-C SM 4500-Cl-E
92250449004 WETA/23002MW-D SM 4500-Cl-E
92250449001 WETA/23058MW-A SM 5220D
92250449002 WETA/23058MW-B SM 5220D
92250449003 WETA/23058MW-C SM 5220D
92250449004 WETA/23058MW-D SM 5220D
92250449001 WETA/23049MW-A SM 5310B
92250449002 WETA/23049MW-B SM 5310B
92250449003 WETA/23049MW-C SM 5310B
92250449004 WETA/23049MW-D SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 47
Page 34 of 47
Page 35 of 47
June 04, 2015
Pace Analytical Services Inc
Kevin Godwin
Dear Kevin Godwin:
RE:92250449
Order No.:15052168
FAX:[phone]
TEL:[phone]
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Website: http://www.settek.com
TEL: [phone] FAX: [phone]
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Summit Environmental Technologies, Inc. received 4 sample(s) on 5/20/2015 for the
analyses presented in the following report.
Page 1 of 9
A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC
E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank)
3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099,
New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma
9940, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5,
Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West
Virginia 248 and 9957C and E87688, Wisconsin 399013010
Page 36 of 47
Project:92250449
CLIENT:Pace Analytical Services Inc
6/4/2015
Case Narrative
15052168
Date:
WO#:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Website: http://www.settek.com
TEL: [phone] FAX: [phone]
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this
sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway
Haddock, GA 31033
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
This report is believed to meet all of the requirements of NELAC or the accrediting / certifying agency.
Any comments or problems with the analytical events associated with this report are noted below.
Page 2 of 9
Original
Page 37 of 47
6/4/2015
Qualifiers and Acronyms
15052168
Date:
WO#:
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Website: http://www.settek.com
TEL: [phone] FAX: [phone]
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Qualifiers

U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.

Acronyms

ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor

Page 3 of 9
Original
Page 38 of 47
Project:92250449
CLIENT:Pace Analytical Services Inc
Lab SampleID Client Sample ID Tag No Date ReceivedDate Collected
04-Jun-15
Workorder
Sample Summary
15052168WO#:
Matrix
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Website: http://www.settek.com
TEL: [phone] FAX: [phone]
15052168-001 92250449001 5/18/2015 3:25:00 PM 5/20/2015 9:40:00 AM Non-Potable
Water
15052168-002 92250449002 5/18/2015 2:25:00 PM 5/20/2015 9:40:00 AM Non-Potable
Water
15052168-003 92250449003 5/18/2015 11:05:00 AM 5/20/2015 9:40:00 AM Non-Potable
Water
15052168-004 92250449004 5/18/2015 3:45:00 PM 5/20/2015 9:40:00 AM Non-Potable
Water
Page 4 of 9
Page 39 of 47
Project:92250449
Client Sample ID 92250449001
Collection Date:5/18/2015 3:25:00 PMMatrix:NON-POTABLE WATER
Analyses Result QualUnits Date Analyzed
CLIENT:Pace Analytical Services Inc
Lab ID:15052168-001A
DF
Tag Number:
RL
6/4/2015
Analytical Report
15052168
Date Reported:
WO#:
(base report)
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Website: http://www.settek.com
TEL: [phone] FAX: [phone]
TOTAL ORGANIC HALIDES (TOX) (9020)SW9020 Analyst:CJM
Total Organic Halides 6/3/2015 6:30:00 PM0.100 mg/L 1ND
Page 5 of 9
Qualifiers:
Original
*Value exceeds Maximum Contaminant Level.E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.N Tentatively identified compounds
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
U Samples with CalcVal < MDL
Page 40 of 47
Project:92250449
Client Sample ID 92250449002
Collection Date:5/18/2015 2:25:00 PMMatrix:NON-POTABLE WATER
Analyses Result QualUnits Date Analyzed
CLIENT:Pace Analytical Services Inc
Lab ID:15052168-002A
DF
Tag Number:
RL
6/4/2015
Analytical Report
15052168
Date Reported:
WO#:
(base report)
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Website: http://www.settek.com
TEL: [phone] FAX: [phone]
TOTAL ORGANIC HALIDES (TOX) (9020)SW9020 Analyst:CJM
Total Organic Halides 6/3/2015 7:16:00 PM0.100 mg/L 1ND
Page 6 of 9
Qualifiers:
Original
*Value exceeds Maximum Contaminant Level.E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.N Tentatively identified compounds
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
U Samples with CalcVal < MDL
Page 41 of 47
Project:92250449
Client Sample ID 92250449003
Collection Date:5/18/2015 11:05:00 AMMatrix:NON-POTABLE WATER
Analyses Result QualUnits Date Analyzed
CLIENT:Pace Analytical Services Inc
Lab ID:15052168-003A
DF
Tag Number:
RL
6/4/2015
Analytical Report
15052168
Date Reported:
WO#:
(base report)
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Website: http://www.settek.com
TEL: [phone] FAX: [phone]
TOTAL ORGANIC HALIDES (TOX) (9020)SW9020 Analyst:CJM
Total Organic Halides 6/3/2015 7:28:00 PM0.100 mg/L 1ND
Page 7 of 9
Qualifiers:
Original
*Value exceeds Maximum Contaminant Level.E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.N Tentatively identified compounds
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
U Samples with CalcVal < MDL
Page 42 of 47
Project:92250449
Client Sample ID 92250449004
Collection Date:5/18/2015 3:45:00 PMMatrix:NON-POTABLE WATER
Analyses Result QualUnits Date Analyzed
CLIENT:Pace Analytical Services Inc
Lab ID:15052168-004A
DF
Tag Number:
RL
6/4/2015
Analytical Report
15052168
Date Reported:
WO#:
(base report)
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Website: http://www.settek.com
TEL: [phone] FAX: [phone]
TOTAL ORGANIC HALIDES (TOX) (9020)SW9020 Analyst:CJM
Total Organic Halides 6/3/2015 7:51:00 PM0.100 mg/L 1ND
Page 8 of 9
Qualifiers:
Original
*Value exceeds Maximum Contaminant Level.E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.N Tentatively identified compounds
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
U Samples with CalcVal < MDL
Page 43 of 47
Project:92250449
Client:Pace Analytical Services Inc
BatchID:R38200
04-Jun-15
QC SUMMARY REPORT
15052168WO#:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Website: http://www.settek.com
TEL: [phone] FAX: [phone]
Sample ID MB-R38200
Batch ID:R38200 TestNo:SW9020 Analysis Date:6/3/2015
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual
Units:mg/L
PQL
Client ID:PBW
RunNo:38200
SeqNo:556442
MBLKSampType:TestCode:TOX_NPW(90
Total Organic Halides 0.100ND
Sample ID LCS-R38200
Batch ID:R38200 TestNo:SW9020 Analysis Date:6/3/2015
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual
Units:mg/L
PQL
Client ID:LCSW
RunNo:38200
SeqNo:556443
LCSSampType:TestCode:TOX_NPW(90
Total Organic Halides 0.3000 102 90 1100.100 00.307
Qualifiers:
Page 9 of 9
Original
*Value exceeds Maximum Contaminant Level.B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 44 of 47
Page 45 of 47
Page 46 of 47
Page 47 of 47
Water Quality Monitoring Report
2015 Annual Sampling Event

ATTACHMENT 4
Relevant Documentation and Correspondence