3420_OmniSource_GWMReport_DIN23658_20151014

2211 W. Meadowview Rd., #101
Greensboro, NC 27409
tel: [phone]
fax: [phone]
www.JoyceEngineering.com

January 29, 2016

Ms. Jaclynne Drummond
Compliance Hydrogeologist
NC Department of Environmental Quality
Division of Waste Management – Solid Waste Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

RE: Second Semiannual Water Quality Monitoring Report of 2015
OmniSource Kernersville Landfill, Permit No. 34-20
Kernersville, North Carolina
JOYCE Project No. 00799.1501.12 Task No. 02

Dear Ms. Drummond:

On behalf of OmniSource Southeast, Joyce Engineering is submitting the Second
Semiannual Water Quality Monitoring Report of 2015 for the OmniSource Kernersville Landfill,
Permit No. 34-20. The attached report contains electronic versions of the complete report and all
appendices for the October 2015 sampling event. Also attached is the North Carolina
Environmental Monitoring Reporting Form and the associated laboratory EDDs.

If you wish to have a hard copy of the report, drawings, or appendices, we will be happy to
provide it upon your request. Please feel free to contact me or Alex Everhart at [phone] if
you have any questions regarding this report.

Sincerely,
JOYCE ENGINEERING

Van Burbach, Ph.D., P.G.
Senior Technical Consultant

Attachment

C: James Winegar, OmniSource Southeast, LLC
Gary Cosentino, OmniSource Kernersville

PREPARED FOR:

OMNISOURCE SOUTHEAST, LLC
2233 WAL-PAT ROAD
SMITHFIELD, NC 27577

OMNISOURCE SOUTHEAST
KERNERSVILLE LANDFILL
PERMIT NO. 34-20

SECOND SEMIANNUAL WATER QUALITY
MONITORING REPORT OF 2015

JANUARY 2016

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER C-0782
PHONE: [phone]
FAX: [phone]
JOYCE PROJECT NO. 799.1501.12

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
OmniSource Kernersville Landfill, Permit No. 34-20 January 2016

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Second Semiannual Water Quality Monitoring Report of 2015
OmniSource Southeast Landfill, Permit No. 34-20
Kernersville, North Carolina

TABLE OF CONTENTS

1.0 INTRODUCTION ..................................................................................................................1
1.1 Site Information .............................................................................................................. 1
1.2 Site Geology and Hydrogeology ..................................................................................... 1
1.3 Regulatory Status ............................................................................................................ 2

2.0 FACILITY MONITORING PROGRAM ...............................................................................2
2.1 Groundwater Monitoring Program ................................................................................. 2
2.2 Surface Water Monitoring Program ................................................................................ 2

3.0 SECOND SEMIANNUAL SAMPLING EVENT OF 2015 ..................................................3
3.1 Field Work and Visual Inspection .................................................................................. 3
3.2 Laboratory Analysis and Quality Control ....................................................................... 4
3.3 Verification Sampling ..................................................................................................... 4

4.0 DATA ANALYSIS .................................................................................................................5
4.1 Groundwater Data Analysis and Comparisons to Standards .......................................... 5
4.2 Surface Water Data Analysis and Comparisons to Standards ........................................ 5

5.0 CONCLUSIONS.....................................................................................................................6

6.0 REFERENCES .......................................................................................................................6

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
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TABLE OF CONTENCTS (Continued)

Tables
Table 1 Historical Groundwater Elevation Data
Table 2 Groundwater Gradients and Calculated Flow Rates
Table 3 Quantified Detections (October 2015)
Table 4 Exceedances (October 2015)
Table 5 Field Parameter Data (October 2015)
Table 6 Historical Detected Groundwater Constituents
Table 7 Historical Detected Surface Water Constituents

Figure
Figure 1 Site Location Map

Drawing
Drawing 1 Groundwater Potentiometric Surface Map

Appendices
Appendix A Field Data Logs
Appendix B Laboratory Analytical Reports and Chains of Custody

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
OmniSource Kernersville Landfill, Permit No. 34-20 January 2016

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1.0 INTRODUCTION
1.1 Site Information
The OmniSource Landfill is owned and operated by OmniSource Southeast, LLC and is located
in Kernersville, Forsyth County, North Carolina. The existing landfill was initially permitted in
the early 1970’s by the state of North Carolina as a private industrial landfill used to dispose of
residue from the automobile shredder under Permit Number 34-17, and was owned and operated
by Atlantic Scrap and Processing, LLC. The landfill received automotive shredder residue
(ASR, or “fluff”) consisting of plastic, glass, rubber, foam, fabric, etc., that was generated by the
on-site operations. The landfill stopped receiving waste and was closed in the mid-1990s. In
2005, the facility received a permit for a mining operation to recover additional metal from the
ASR waste. Currently the facility is operating a landfill mining operation under Permit Number
34-20.

The OmniSource Landfill includes approximately 14 acres located within OmniSource-Southeast
property located at 1426 West Mountain Street in Kernersville, North Carolina. Access to the
landfill area is limited from the southern end by means of the fenced scrap processing area and
from other directions by berms, topography, and the side-slopes of the landfill. The site location
is shown on Figure 1 on an excerpt from the 7.5-minute USGS topographic map for the area.

1.2 Site Geology and Hydrogeology
The OmniSource Landfill is located in the Piedmont physiographic providence of North Carolina
and is underlain by intrusive granitic rocks of Pennsylvanian to Permian age, which are part of
the Carolina Slate Belt Geologic Unit.

The groundwater level measurements taken on October 14, 2015 were used to construct the
groundwater surface contours shown in Drawing 1. Historical static water levels are provided in
Table 1. Groundwater flow at the site is toward the northeast.

Using the hydraulic gradients along the flow paths shown on Drawing 1, the linear flow velocity
(V) was estimated using the modified Darcy equation: V=Ki/n. The average hydraulic gradient
(i) based on the flow paths shown on Drawing 1 is 0.0633 ft/ft. An effective porosity (n) of 30%
was estimated based on typical values for piedmont aquifers. Hydraulic conductivity (K) of 1.73
ft/day was estimated from slug testing done by JOYCE at nearby site is Kernersville, NC in
November of 2013. The calculated groundwater flow rate averages approximately 133.2 ft/yr.
A summary of the hydraulic gradients and linear flow velocities is provided in Table 2.

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
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1.3 Regulatory Status
The OmniSource Landfill is currently monitoring groundwater in accordance with criteria set
forth in Title 15A Subchapter 13B .0500 of the North Carolina Solid Waste Management Rules
(NCSWMR) as well as, the approved sampling and analysis plan dated October 2011.

2.0 FACILITY MONITORING PROGRAM
2.1 Groundwater Monitoring Program
The original groundwater monitoring network consisted of 4 monitoring wells installed in 1989;
MW-1, MW-2, MW-3 and MW-4. In 2001, MW-4R was installed to replace MW-4 and
MW-1R replaced MW-1 to further expanding scrap metal processing activities. Monitoring
wells MW-2, MW-3, MW-4, and MW-4R were destroyed during mining operations.
Replacement wells MW-12, MW-13, and MW-14 were installed in 2012.

The current groundwater compliance monitoring network consists of four monitoring wells,
including one upgradient well (MW-1R) and three downgradient wells (MW-12, MW-13, and
MW-14). These wells are summarized below, along with their current monitoring program
status. The locations of the monitoring wells are shown on Drawing No. 1.

Monitoring Well Classification Monitoring Program Total Depth from TOC (ft)
MW-1R Upgradient Detection 104.73
MW-12 Downgradient Detection 28.82
MW-13 Downgradient Detection 26.15
MW-14 Downgradient Detection 33.68
TOC = Top of casing.
Groundwater samples are collected semiannually during the second and fourth quarters. Samples
are analyzed for all constituents listed in the NCSWMR Appendix I during the first and second
semiannual events.

2.2 Surface Water Monitoring Program
Surface water at the OmniSource Kernersville Landfill is monitored semiannually in conjunction
with the groundwater sampling events. Samples are collected from two surface water monitoring
points (SW-1 and SW-2). The locations of the surface water monitoring points are shown on
Drawing 1.

Surface water samples are collected and analyzed for the NCSWMR Appendix I list of
constituents during both semiannual monitoring events. The results are compared to the 15A
NCAC 2B (NC 2B) Surface Water Standards in a value-to-value comparison. These surface
water monitoring points are summarized below, along with their current monitoring program
status.

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
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Surface Point Classification Monitoring Program
SW-1 Upstream/Compliance Surface Water
SW-2 Downstream/Compliance Surface Water

3.0 SECOND SEMIANNUAL SAMPLING EVENT OF 2015
3.1 Field Work and Visual Inspection
In order to detect potential releases of leachate in a timely manner, a visual inspection program
has been implemented at the OmniSource Kernersville Landfill. This inspection program
involves field personnel making the following observations:

 Observation of stress induced on the biological community (e.g., dead or dying vegetation);
 Indications of leachate impact (e.g., seeps, impacted surface water);
 Observations of erosion; and
 Negative changes around the waste facility.

On October 14, 2015, Joyce Engineering (JOYCE) personnel visited the facility to purge and
sample the facility’s monitoring wells MW-1R, MW-12, MW-13, and MW-14. Prior to purging,
the depth to static water level was measured for all monitoring wells with an electronic water
level indicator, accurate to 0.01 foot.

Monitoring wells were purged and sampled, in accordance with the October 2011 Sampling &
Analysis Plan, using either a 12-volt submersible pump or disposable bailer. Measurements of
temperature, pH, specific conductivity, and turbidity were recorded in the site log book prior to
purging, after each purge volume, and during sampling. Prior to sampling, laboratory-supplied
containers were prepared with the following information:

 Monitoring well number (completed by field personnel);
 Date and time of sample collection (completed by field personnel);
 Initials of sampling personnel (completed by field personnel);
 Project name and number (completed by the laboratory);
 Chemical preservative (completed by the laboratory); and
 Requested chemical analysis (completed by the laboratory).

Groundwater samples from each monitoring well were collected directly from the 12-volt pump
or disposable bailers in the provided laboratory containers either immediately after purging or
within 24 hours of the final purge volume. Immediately after collection, the samples were
placed in a laboratory-provided cooler and chilled on ice. Field data logs are provided in
Appendix A.

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Surface water samples from SW-1 and SW-2 were collected directly from stream flow, by
lowering the prepared sample containers into the stream flow. Care was taken not to overflow
the sample containers (which could lead to preservative loss) and to avoid sampling-induced
turbidity. At the time of sampling, surface water was also measured for temperature, pH,
specific conductivity, and turbidity. After sample collection, the sampled were placed in a
laboratory-provided cooler and chilled on ice. Field data logs are provided in Appendix A.

3.2 Laboratory Analysis and Quality Control
The October 14, 2015, groundwater and surface water samples were submitted to Pace
Analytical Services of Huntersville, North Carolina. The samples were analyzed for the
NCSWMR Appendix I constituents. JOYCE requested a Level II data report for the final
laboratory report. The samples were received by the laboratory on October 15, 2015, in good
condition, properly preserved, and within analysis hold times.

In addition to samples collected for compliance monitoring at the OmniSource Kernersville
Landfill, a Field Blank was collected by JOYCE personnel as part of the October 2015 sampling
event. Also, a Trip Blank was prepared by the laboratory to accompany the volatile sampling
containers during shipment to and from the laboratory. The October 2015 Field Blank was
analyzed for the NCSWMR Appendix I constituents while the October 2015 Trip Blank was
analyzed for the NCSWMR Appendix I volatile organics only.

Upon receipt of the laboratory data package, the data was reviewed by JOYCE personnel for the
following:

 General typographical errors;
 Correct analyses performed and within method specified hold times;
 Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate;
and Laboratory Control Samples;
 Blank qualified data (B-flags);
 Detections above the groundwater and surface water standards; and
 Detections that are above historical levels.

3.3 Verification Sampling
Due to a detection of benzene in the October 2015 sample, the facility background well,
MW-1R, was resampled on November 11, 2015. The sample was sent to Pace Analytical to be
analyzed for benzene. Field data logs are provided in Appendix A.

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
OmniSource Kernersville Landfill, Permit No. 34-20 January 2016

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4.0 DATA ANALYSIS
4.1 Groundwater Data Analysis and Comparisons to Standards
The Laboratory Analytical Report from the October 2015 sampling event was received
November 19, 2015 from Pace Analytical and is included in Appendix B with the chains-of-
custody. Constituents that were detected at quantified concentrations above the North Carolina
Department of Environmental Quality (NCDEQ) Solid Waste Section Limits (SWSL) in
groundwater during the October 2015 sampling event are summarized in Table 3.

Analytical results from monitoring wells were compared directly to the North Carolina
Groundwater Standards found in 15A NCAC 02L.0202 (NC 2L Standards) or the NCDEQ Solid
Waste Section Groundwater Protection Standards (GWPS) for constituents with no listed NC 2L
standard. Analytical results for surface water samples were compared directly to either the
Freshwater Aquatic Surface Water Standards or Human Health Surface Water Standards
(whichever is lower) found in 15A NCAC 02B (NC 2B Standards). Constituents in exceedance
of the appropriate standards are summarized in Table 4. Field parameter data for the October
2015 sampling event are summarized in Table 5.

Benzene was detected at 1.8 µg/L in the October 2015 sample from the facility background well,
MW-1R, which exceeds the NC 2L standard of 1.0 µg/L. A resampling event was conducted on
November 11, 2015, and the results found benzene at 1.0 µg/L (equal to, but not exceeding the
NC2L standard.) The results of the November resampling event did not indicate an exceedance
of the NC 2L standard.

Well MW-1R is located approximately 345 feet upgradient from the edge of waste for the
landfill; therefore, it is very unlikely that the landfill is the source of the benzene detected in
MW-1R. This is an old industrial site with a long history of various activities, as well as ongoing
activities, which could be the source of the benzene. A reconnaissance of the area immediately
surrounding MW-1R observed semi-trailers, discarded equipment, and small piles of debris, but
no obvious spills, stained soil, or other indications of a recent release; therefore, the specific
source of the benzene is unknown.

With the exception of the benzene detected in MW-1R, the organic and inorganic groundwater
results are consistent with historical data. Historical groundwater data can be found in Table 6.

4.2 Surface Water Data Analysis and Comparisons to Standards
The results for the upstream surface water sample, SW-1, indicated one inorganic constituent
with a quantified concentration above the SWSL during the October 2015 sampling event. Zinc
was quantified at a concentration of 52 µg/L, which is above the respective NC 2B standard for
freshwater aquatic life that is 50 µg/L. In addition, three organic constituents were detected in
SW-1. Carbon Tetrachloride, Chloroform, and Tetrachloroethene (PCE) were detected above the
SWSL. Carbon Tetrachloride was found at a concentration of 4.5 µg/L and PCE was found at a

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
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concentration of 4.4 µg/L, which puts both constituents above their NC 2B human health
standards. The NC 2B human health standard for Carbon Tetrachloride is 1.6 µg/L. The NC 2B
human health standard for PCE is 3.3 µg/L.

Since surface water sampling point SW-1 is upstream of the OmniSource landfill, it is highly
unlikely that the constituents detected in SW-1 are due to a release from the landfill. The most
likely source of the PCE detected in SW-1 is the former Destructo-Chemway/ChemLawn
property, which is directly upstream of the SW-1 location. This property is a NC Inactive
Hazardous Site, which was the source of a major spill of hazardous material, including
chlorinated solvents, in 1977. The spill flowed down the creek where SW-1 is located and
eventually contaminated the Kernersville Reservoir. We believe the PCE and possibly some of
the inorganic constituents detected in SW-1 are residuals from this incident.

Barium and Zinc were the only constituents detected in the downstream surface water sample,
SW-2, at quantified concentrations above their respective SWSL during the October 2015
sampling event. Neither of the constituents detected were higher than the NC2B standard for
freshwater aquatic life. The October 2015 result is not higher than historical values for zinc in
SW-2 and it is lower than the concentration of zinc detected in the upstream sample, SW-1,
which had a zinc concentration of 52 µg/L. Historical surface water data can be found in Table
7.

5.0 CONCLUSIONS
Benzene was detected above the NC 2L Groundwater Standard in the upgradient monitoring well
MW-1R and a resampling event did not indicate an exceedance of the NC 2L standard. JOYCE
recommends continued semiannual monitoring to determine whether the benzene concentrations
remain below the NC 2L standard or return to exceedance levels before determining whether
further action or investigation is necessary. Since we do not believe the landfill to be the source
of the benzene, we recommend that the landfill remain in detection monitoring.

There were no exceedances of groundwater protection standards in any of the downgradient
monitoring wells during the October 2015 sampling event. The next scheduled semiannual
sampling event is tentatively scheduled for April 2016.

6.0 REFERENCES
Brown, Philip M., Chief Geologist, 1985, Geologic Map of North Carolina, The North Carolina
Geologic Survey, scale 1:500,000.

Fetter, C.W., 2001, Applied Hydrogeology, Fourth Edition: Prentice-Hall, Inc..

Johnson, A.I., 1967, Specific Yield - Compilation of Specific Yields For Various Materials: U.S.
Geological Survey Water Supply Paper 1662-D.

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
OmniSource Kernersville Landfill, Permit No. 34-20 January 2016

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Joyce Engineering, Inc. 2014. 2014 Operations Plan, OmniSource – Kernersville Landfill
Reclamation Project. May 2014.

North Carolina Department of Environment and Natural Resources, 1990-2012, Solid Waste
Management Regulations.

USEPA, 1981. Neely, N., D. Gillespie, F. Schauf, and J. Walsh. Remedial Actions at
Hazardous Sites, Survey and Case Studies: Section 5, Site D – Destructo/CaroLawn,
Kernersville, NC. EPA-430-9-81-005. January 1981.

USEPA, 1986. RCRA Ground Water Monitoring Technical Enforcement Guidance Document
(TEGD).

USEPA, 1992. Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities,
Addendum to Interim Final Guidance, Chapter 2, July.

W.Z Baumgartner & Associates, Inc. 2011. Sampling & Analysis Plan For Groundwater
Monitoring, OmniSource Southeast Industriall Landfill. October 2011.

W.Z Baumgartner & Associates, Inc. 2013. Groundwater Monitoirng Report, April 10, 2013
Sampling Event, OmniSource Southeast Landfill, Permit: 3417-TP. May 2014.

Tables

Table 1 Historical Groundwater Elevation Data
Table 2 Groundwater Gradients and Calculated Flow Rates
Table 3 Quantified Detections (October-November 2015)
Table 4 Exceedances (October-November 2015)
Table 5 Field Parameter Data (October-November 2015)
Table 6 Historical Detected Groundwater Constituents
Table 7 Historical Detected Surface Water Constituents

TABLE 1:
HISTORICAL GROUNDWATER ELEVATION DATA
Background
MW-1R MW-12 MW-13 MW-14
Well TOC Elev.:988.67 855.85 838.45 847.45
Well Total Depth:104.73 28.82 26.15 33.68
10-Apr-13 952.17 847.73 832.84 835.05
11-Sep-13 949.72 847.69 832.55 834.20
24-Apr-14 953.02 847.60 833.12 834.96
02-Oct-14 949.11 847.80 832.76 834.22
29-Apr-15 950.99 847.82 833.13 835.29
14-Oct-15 946.27 847.85 832.90 834.73
Notes:
TOC = top of casing.
Water levels are measured from TOC.
All elevations are in feet above mean sea level.
Downgradient
OmniSource Kernersville Landfill
Permit No. 34-20
Joyce Engineering
August 2015
TABLE 2:
GROUNDWATER GRADIENTS AND CALCULATED FLOW RATES
GROUND-HORIZ.HYDRAULIC EFFECTIVE LINEAR
FLOW WATER GRADIENT,CONDUCTIVITY,POROSITY VELOCITY,
DIRECTION ELEVATION i K n e V
(feet)(ft/ft)(ft/day)(ft/year)
940
860
940
860
Average:0.0633 Average:133.2
Notes:
Linear flow velocity is caculated by: V = Ki/ne
Hydraulic conductivity (K ) value based on slug tests at another site locaed approxiamtely 10 miles from the facility in a simialr geologic seting.
Effective porosity (n e ) is estimated at 30% (0.30), which is typical for saprolite aquifiers in the North Carolina Piedmont.
Refer to Drawling 1 for gradient calculation segments.
0.30
0.0594
October 14, 2015
GRADIENT
CALCULATION
SEGMENT
FLOW LINE
LENGTH
(feet)
i 2 1192 NE
i 1 1347 NE 1.73E+00 0.30 125.1
141.40.0671 1.73E+00
OmniSource - Kernersville Landfill
Permit No. 34-20 Joyce Engineering
TABLE 3:
Quantified Detections (October- November 2015)
WELL ID PARAMETER RESULT UNITS SWSL DATE
3420-MW1R Benzene 1.80 µg/L 1 10/14/2015
3420-MW1R*Benzene 1.00 µg/L 1 11/11/2015
3420-MW12 Barium 179 µg/L 100 10/14/2015
3420-MW14 Barium 121 µg/L 100 10/14/2015
3420-MW14 Beryllium 1.4 µg/L 1 10/14/2015
3420-SW1 Zinc 52 µg/L 10 10/14/2015
3420-SW1 Carbon Tetrachloride 4.5 µg/L 1 10/14/2015
3420-SW1 Chloroform 13.9 µg/L 5 10/14/2015
3420-SW1 Tetrachloroethene 4.4 µg/L 1 10/14/2015
3420-SW2 Barium 101 µg/L 100 10/14/2015
3420-SW2 Zinc 29.7 µg/L 10 10/14/2015
NOTES:All results in micorgrams per liter (µg/L).
SWSL = NC Soild Waste Section Reporting Limit.
* = Resample 11/11/15
OmniSource Kernersville
Permit No. 34-20
Joyce Engineering
TABLE 4:
Exceedances (October-November 2015)
WELL ID PARAMETER RESULT UNITS SWSL NC 2L / GWPS / NC 2B GPS DATE
3420-MW1R Benzene 1.8 µg/L 1.0 1 1 10/14/2015
3420-MW1R*Benzene 1.0 µg/L 1.0 1 1 10/15/2015
3420-SW1 Carbon tetrachloride 4.5 µg/L 1.0 1.6 HH 10/14/2015
3420-SW1 Tetrachloroethene 4.4 µg/L 1.0 3.3 HH 10/14/2015
3420-SW1 Zinc 52 µg/L 10.0 50 FAL 10/14/2015
NOTES:All results in micorgrams per liter (µg/L).
SWSL = NC Soild Waste Section Reporting Limit.
NC 2L = NC Groundwater Standard from 15A NCAC 2L.0202.
GWPS = NC Solid Waste Section Groundwater Protection Standard (for constituents with no NC2L).
NC 2B = NC Surface Water Standard from 15A NCAC 2B.
FAL = Freshwater Aquatic Life Standard.
HH = Human Health Standard.
GPS = Groundwater Protection Standard as defined by 15A NCAC 13B.1634(g).
Bold results are in exceednace of the pertinent standard.
An ASD for Iron and Manganese approved by DENR-SWS on June 9, 2011.
*= Resample Event 11/11/2015
OmniSource Kernersville
Permit No. 34-20
Joyce Engineering
TABLE 5:
Summary of Field Parameter Data
WELL ID PARAMETER RESULT UNITS COLLECT DATE
3420-MW1R pH 10.84 S.U.10/14/2015
3420-MW1R Temperature 18.3 °C 10/14/2015
3420-MW1R Conductivity 232 µS 10/14/2015
3420-MW1R Turbididty 13.60 NTU 10/14/2015
3420-MW1R Static Water Level 42.40 ft 10/14/2015
3420-MW1R Well Depth 104.73 ft 10/14/2015
3420-MW1R*pH 9.92 S.U.11/11/2015
3420-MW1R*Temperature 14.5 °C 11/11/2015
3420-MW1R*Conductivity 214 µS 11/11/2015
3420-MW1R*Turbididty 20.70 NTU 11/11/2015
3420-MW1R*Static Water Level 47.83 ft 11/11/2015
3420-MW1R*Well Depth 104.73 ft 11/11/2015
3420-MW12 pH 6.70 S.U.10/14/2015
3420-MW12 Temperature 19.9 °C 10/14/2015
3420-MW12 Conductivity 291 µS 10/14/2015
3420-MW12 Turbididty 35.90 NTU 10/14/2015
3420-MW12 Static Water Level 20.82 ft 10/14/2015
3420-MW12 Well Depth 28.82 ft 10/14/2015
3420-MW13 pH 6.20 S.U.10/14/2015
3420-MW13 Temperature 20.5 °C 10/14/2015
3420-MW13 Conductivity 568 µS 10/14/2015
3420-MW13 Turbididty 10.26 NTU 10/14/2015
3420-MW13 Static Water Level 20.6 ft 10/14/2015
3420-MW13 Well Depth 26.15 ft 10/14/2015
OmniSource Kernersville
Permit No. 34-20 1 of 2 Joyce Engineering
TABLE 5:
Summary of Field Parameter Data
WELL ID PARAMETER RESULT UNITS COLLECT DATE
3420-MW14 pH 5.48 S.U.10/14/2015
3420-MW14 Temperature 14.9 °C 10/14/2015
3420-MW14 Conductivity 170 µS 10/14/2015
3420-MW14 Turbididty 11.16 NTU 10/14/2015
3420-MW14 Static Water Level 12.72 ft 10/14/2015
3420-MW14 Well Depth 33.68 ft 10/14/2015
3420-SW1 pH 7.05 S.U.10/14/2015
3420-SW1 Temperature 16.5 °C 10/14/2015
3420-SW1 Conductivity 113 µS 10/14/2015
3420-SW1 Turbididty 8.61 NTU 10/14/2015
3420-SW2 pH 6.74 S.U.10/14/2015
3420-SW2 Temperature 16.0 °C 10/14/2015
3420-SW2 Conductivity 406 µS 10/14/2015
3420-SW2 Turbididty 6.59 NTU 10/14/2015
NOTES:ºC = degrees Centigrade
S.U.= Standard Units
µS = microsemens
NTU = Nephelometric Turbidity Units
*= Resample November 2015
OmniSource Kernersville
Permit No. 34-20 2 of 2 Joyce Engineering
TABLE 6:
HISTORICAL DETECTED GROUND WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1R MW-12 MW-13 MW-14 Blanks
Inorganic Compounds
Antimony 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------7.70 ND ND ND ---
GWPS = 1 µg/L (10/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 5.0 6.0 ND ND ND ND ND
2-Oct-14 5.0 6.0 6.5 ND ND ND ND
29-Apr-15 0.5 6.0 1.01 J ND ND ND ND
14-Oct-15 3.8 6.0 ND ND ND ND ND
Arsenic 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------10.7 ND 3.40 ND ---
NC 2L = 100 µg/L (1/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 5.0 10.0 ND ND ND ND ND
2-Oct-14 5.0 10.0 ND ND ND ND ND
29-Apr-15 0.25 10.0 1.59 J ND ND ND ND
14-Oct-15 2.50 10.0 ND ND ND ND ND
Barium 12-Apr-12 ------41.5 166 41.0 118 ---
10-Oct-12 ------37.6 170 26.9 107 ---
NC 2L = 700 µg/L (1/01/10)10-Apr-13 ------26.9 166 27.5 98.2 ---
11-Sep-13 ------39.4 196 29.8 100 ---
24-Apr-14 5.0 100 21.2 J 184 39.3 J 88.8 J ND
2-Oct-14 5.0 100 15.5 J 195 43.5 J 106 ND
29-Apr-15 0.25 100 27.2 J 181 46.1 J 125 ND
14-Oct-15 2.50 100 17.2 J 179 43.1 J 121 ND
Beryllium 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND 1.10 ---
GWPS = 4 µg/L (10/23/07)10-Apr-13 ------ND ND ND 1.10 ---
11-Sep-13 ------ND ND ND 0.800 ---
24-Apr-14 1.0 1.0 ND ND ND 1.1 ND
2-Oct-14 1.0 1.0 ND ND 1.2 1.4 ND
29-Apr-15 0.25 1.0 ND 0.30 J 0.38 J 1.26 ND
14-Oct-15 0.50 1.0 ND ND ND 1.4 ND
Chromium 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------2.50 ND ND ND ---
NC2B= 50 µg/L (05/01/07)10-Apr-13 ------2.30 ND ND ND ---
11-Sep-13 ------1.80 ND ND ND ---
24-Apr-14 5.0 10.0 ND ND ND ND ND
2-Oct-14 5.0 10.0 ND ND ND ND ND
29-Apr-15 0.25 10.0 ND 0.73 J 1.34 J ND ---
14-Oct-15 2.50 10.0 ND ND 2.8 J ND ND
OmniSource Kernersville Landfill
Permit No. 34-20 1 of 4
Joyce Engineering
TABLE 6:
HISTORICAL DETECTED GROUND WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1R MW-12 MW-13 MW-14 Blanks
Cobalt 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------0.700 3.10 3.90 5.70 ---
GWPS = 1 µg/L (10/01/10)10-Apr-13 ------ND 1.90 2.80 3.80 ---
11-Sep-13 ------ND 2.60 4.10 ND ---
24-Apr-14 5.0 10.0 ND ND 5.5 J ND ND
2-Oct-14 5.0 10.0 ND ND 10.4 5.2 J ND
29-Apr-15 0.25 10.0 ND 3.02 J 7.91 J 5.08 J ND
14-Oct-15 2.50 10.0 ND ND 7.2 J 5.4 J ND
Copper 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
NC 2L = 1,000 µg/L (10/23/07)10-Apr-13 ------8.8 ND ND ND ---
11-Sep-13 ------10.0 ND ND ND ---
24-Apr-14 5.00 10.0 ND ND 7.5 J ND ND
2-Oct-14 5.00 10.0 ND ND 8.9 J ND ND
29-Apr-15 0.25 10.0 0.39 J 2.73 J 3.43 J 0.92 J ND
14-Oct-15 2.50 10.0 ND 3.5 J 4.3 J ND ND
Lead 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------4.9 ND ND ND ---
NC 2L = 15 µg/L (10/23/07)10-Apr-13 ------4.2 ND ND ND ---
11-Sep-13 ------6.2 ND ND ND ---
24-Apr-14 5.0 10.0 ND ND ND ND ND
2-Oct-14 5.0 10.0 ND ND ND ND ND
29-Apr-15 0.3 10.0 ND 1.60 J 1.26 J ND ND
14-Oct-15 2.5 10.0 ND 3.5 J ND ND ND
Nickel 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND 2.30 ND 2.00 ---
NC 2L = 100 µg/L (10/23/07)10-Apr-13 ------ND 2.90 ND ND ---
11-Sep-13 ------ND ND ND 2.20 ---
24-Apr-14 5.0 50.0 ND ND ND ND ND
2-Oct-14 5.0 50.0 ND ND ND ND ND
29-Apr-15 0.5 50.0 ND 4.44 J 4.07 J 2.58 J ND
14-Oct-15 2.5 50.0 ND 5.8 J 4.9 J 2.6 J ND
Selenium 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
NC 2L = 20 µg/L (1/01/10)10-Apr-13 ------ND ND ND 4.90 ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 10.0 10.0 ND ND ND ND ND
2-Oct-14 10.0 10.0 ND ND ND ND ND
29-Apr-15 0.25 10.0 ND ND ND ND ND
14-Oct-15 5.00 10.0 ND ND ND ND ND
Vanadium 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
GWPS = 0.3 µg/L (10/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 5.00 25.0 ND ND 9.2 J ND ND
2-Oct-14 5.00 25.0 ND 5.0 J 20.1 J ND ND
29-Apr-15 0.25 25.0 4.12 J 2.54 J 5.42 J 0.31 J ND
14-Oct-15 2.50 25.0 ND 5.4 J 8.5 J ND ND
OmniSource Kernersville Landfill
Permit No. 34-20 2 of 4
Joyce Engineering
TABLE 6:
HISTORICAL DETECTED GROUND WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1R MW-12 MW-13 MW-14 Blanks
Zinc 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------27.3 ND ND ND ---
NC 2L = 1,000 µg/L (1/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------29.4 ND ND ND ---
24-Apr-14 10.0 10.0 ND 15.3 ND ND ND
2-Oct-14 10.0 10.0 ND ND ND ND ND
29-Apr-15 5.0 10.0 20.2 24.3 23.1 26.2 ND
14-Oct-15 5.0 10.0 7.1 J 8.9 J 7.6 J 5.1 J ND
Organic Compounds
Acetone 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------12 20.9 ND ND ---
NC 2L = 6,000 µg/L (1/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 10.0 100 ND ND ND ND ND
2-Oct-14 10.0 100 ND ND ND ND ND
29-Apr-15 10.0 100 ND ND ND ND ND
14-Oct-15 10.0 100 ND ND ND ND ND
Benzene 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND 0.406 0.280 ND ---
NC 2L = 1 µg/L (10/23/07)10-Apr-13 ------ND 0.365 ND ND ---
11-Sep-13 ------ND 0.411 0.203 ND ---
24-Apr-14 0.25 1.0 ND 0.350 J ND ND ND
2-Oct-14 0.25 1.0 ND ND ND ND ND
29-Apr-15 0.20 1.0 1.43 ND ND ND ND
GCAL resample 27-May-15 0.20 1.0 1.45 ------------
Pace resample 24-Jun-15 0.25 1.0 0.88 J ------------
GCAL resample 24-Jun-15 0.20 1.0 0.96 J ------------
14-Oct-15 0.25 1.0 1.8 ND ND ND ND
Pace resample 11-Nov-15 0.30 1.0 1.0 ---------ND
Carbon disulfide 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND 1.9 ---
NC 2L = 700 µg/L (10/23/07)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 1.2 100 ND ND ND ND ND
2-Oct-14 1.2 100 ND ND ND ND ND
29-Apr-15 1.2 100 ND ND ND ND ND
14-Oct-15 1.2 100 ND ND ND ND ND
Cis-1,2-Dichloroethene 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
NC 2L = 70 µg/L (10/23/07)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 0.19 5.0 ND 0.200 J ND ND ND
2-Oct-14 0.19 5.0 ND ND ND ND ND
29-Apr-15 0.19 5.0 ND ND ND ND ND
14-Oct-15 0.19 5.0 ND 0.20 J ND ND ND
OmniSource Kernersville Landfill
Permit No. 34-20 3 of 4
Joyce Engineering
TABLE 6:
HISTORICAL DETECTED GROUND WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1R MW-12 MW-13 MW-14 Blanks
Methylene Chloride 14-Oct-15 0.97 1 ND ND ND ND 3.6
NC 2L = 5 µg/L (10/23/07)
Styrene 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
NC 2L = 70 µg/L (10/23/07)10-Apr-13 ------0.515 ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 0.26 1.0 ND ND ND ND ND
2-Oct-14 0.26 1.0 ND ND ND ND ND
29-Apr-15 0.26 1.0 ND ND ND ND ND
14-Oct-15 0.26 1.0 ND ND ND ND ND
Tetrachloroethene 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND 0.319 ND ND ---
NC 2L = 0.7 µg/L (10/23/07)10-Apr-13 ------ND 0.525 ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 0.46 1.0 ND ND ND ND ND
2-Oct-14 0.46 1.0 ND ND ND ND ND
29-Apr-15 0.20 1.0 ND ND ND ND ND
14-Oct-15 0.46 1.0 ND ND ND ND ND
Notes:
All concentrations are in micrograms per liter (µg/L).
NC 2L = North Carolina Groundwater Standards established under 15A NCAC 2L.0202.
GWPS = Groundwater Protection Standards established by the DENR-SWS for constituents with ne NC 2L standard.
RL = Laboratory reporting limit (NC SWSL or lower).
DL = Laboratory detection limit.
J = Estimated value between the DL and the SWSL.
B = Blank-qualified data; result is expected to be biased high based on concentrations in the blanks.
ND = Not detected above the DL.
--- = Data not available.
Data prior to May 2014 provided by W.Z. Baumgartner & Associates, Inc.
Bold values are above the NC 2L Standards or GWPS.
OmniSource Kernersville Landfill
Permit No. 34-20 4 of 4
Joyce Engineering
TABLE 7:
HISTORICAL DETECTED SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL RL SW-1 SW-2 Blanks
Inorganic Compounds
Antimony 29-Apr-15 0.5 6 1.69 J ND ND
14-Oct-15 3.8 6 ND ND ND
NC 2B = 640 µg/L (HH)
Arsenic 12-Apr-12 ------ND ND ---
10-Oct-12 ------ND 69.0 ---
NC 2B = 10 µg/L (HH)10-Apr-13 ------44.3 ND ---
11-Sep-13 ------ND ND ---
24-Apr-14 5.0 10.0 Dry ND ND
2-Oct-14 5.0 10.0 Dry ND ND
29-Apr-15 0.3 10.0 0.39 J 0.27 J ND
14-Oct-15 2.5 10.0 ND ND ND
Barium 12-Apr-12 ------52.4 79.1 ---
10-Oct-12 ------52.6 87.4 ---
NC 2B = 200,000 µg/L (HH)10-Apr-13 ------44.3 84.2 ---
11-Sep-13 ------52.7 99.3 ---
24-Apr-14 5.0 100 Dry 79.6 J ND
2-Oct-14 5.0 100 Dry 79.9 J ND
29-Apr-15 0.3 100 174 98.2 J ND
14-Oct-15 2.5 100 59.6 J 101 ND
Beryllium 12-Apr-12 ------ND ND ---
10-Oct-12 ------ND ND ---
NC 2B = 6.5 µg/L (FAL)10-Apr-13 ------ND ND ---
11-Sep-13 ------ND ND ---
24-Apr-14 1.0 1.0 Dry ND ND
2-Oct-14 1.0 1.0 Dry ND ND
29-Apr-15 0.3 1.0 0.43 J ND ND
14-Oct-15 0.5 1.0 ND ND ND
Cadmium 29-Apr-15 0.3 1.0 1.40 ND ND
14-Oct-15 0.5 1.0 ND ND ND
NC 2B = 2 µg/L (05/01/07) (FAL)
Chromium 12-Apr-12 ------ND ND ---
10-Oct-12 ------ND ND ---
NC 2B = 50 µg/L (FAL)10-Apr-13 ------1.6 2.1 ---
11-Sep-13 ------ND ND ---
24-Apr-14 5.0 10.0 Dry ND ND
2-Oct-14 5.0 10.0 Dry ND ND
29-Apr-15 0.3 10.0 5.40 J 0.39 J ND
14-Oct-15 2.5 10.0 ND ND ND
OmniSource Kernersville Landfill
Permit No. 34-20 1 of 3
Joyce Engineering
TABLE 7:
HISTORICAL DETECTED SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL RL SW-1 SW-2 Blanks
Cobalt 12-Apr-12 ------ND ND ---
10-Oct-12 ------ND 1.0 ---
NC 2B = 4 µg/L (HH)10-Apr-13 ------ND ND ---
11-Sep-13 ------ND ND ---
24-Apr-14 5.0 10.0 Dry ND ND
2-Oct-14 5.0 10.0 Dry ND ND
29-Apr-15 0.3 10.0 1.83 J 1.39 J ND
14-Oct-15 2.5 10.0 ND ND ND
Copper 12-Apr-12 ------ ND ND ---
10-Oct-12 ------11.8 13.5 ---
NC 2B = 7 µg/L (FAL)10-Apr-13 ------ND ND ---
11-Sep-13 ------ND ND ---
24-Apr-14 5.00 10.0 Dry 6.8 J ND
2-Oct-14 5.00 10.0 Dry ND ND
29-Apr-15 0.25 10.0 43.8 4.72 J ND
14-Oct-15 2.50 10.0 2.8 J 3.2 J ND
Lead 29-Apr-15 0.25 10.0 69.2 0.92 J ND
14-Oct-15 2.50 10.0 ND ND ND
NC 2B = 25 µg/L (05/01/07) (FAL)
Nickel 12-Apr-12 ------ND ND ---
10-Oct-12 ------ND 7.6 ---
NC 2B = 88 µg/L (FAL) 10-Apr-13 ------ND 5.1 ---
11-Sep-13 ------ND 4.5 ---
24-Apr-14 5.0 50.0 Dry 6.7 J ND
2-Oct-14 5.0 50.0 Dry ND ND
29-Apr-15 0.5 50.0 9.67 J 5.43 J ND
14-Oct-15 2.5 50.0 ND 4.4 J ND
Vanadium 29-Apr-15 0.25 25 3.01 J 0.40 J ND
14-Oct-15 2.5 25 ND ND ND
NC 2B = NE (05/01/07)
Zinc 12-Apr-12 ------ND ND ---
10-Oct-12 ------0.051 24.2 ---
NC 2B = 50 µg/L (FAL)10-Apr-13 ------ND 29.4 ---
11-Sep-13 ------0.169 23.2 ---
24-Apr-14 10.0 10.0 Dry 27.7 ND
2-Oct-14 10.0 10.0 Dry 10.6 ND
29-Apr-15 5.0 10.0 438 62.0 ND
14-Oct-15 5.0 10.0 52.0 29.7 ND
OmniSource Kernersville Landfill
Permit No. 34-20 2 of 3
Joyce Engineering
TABLE 7:
HISTORICAL DETECTED SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL RL SW-1 SW-2 Blanks
Organic Compounds
Acetone 12-Apr-12 ------ND ND ---
10-Oct-12 ------ND 2.88 ---
NC 2B = 2,000 µg/L (FAL)10-Apr-13 ------ND 8.34 ---
11-Sep-13 ------ND ND ---
24-Apr-14 10.0 100.0 Dry ND ND
2-Oct-14 10.0 100.0 Dry ND ND
29-Apr-15 0.5 100.0 ND ND ND
14-Oct-15 10.0 100.0 ND ND ND
Benzene 12-Apr-12 ------ND ND ---
10-Oct-12 ------ND 0.509 ---
NC 2B = 51 µg/L (HH)10-Apr-13 ------ND 0.369 ---
11-Sep-13 ------ND 0.481 ---
24-Apr-14 1.2 1.0 Dry 0.31 J ND
2-Oct-14 0.3 1.0 Dry ND ND
29-Apr-15 0.2 1.0 ND ND ND
14-Oct-15 0.3 1.0 ND 0.45 J ND
Carbon tetrachloride 14-Oct-15 0.25 1.0 4.5 ND ND
NC 2B = 1.6 µg/L (HH)
cis-1,2-Dichloroethene 14-Oct-15 0.19 5 0.7 J ND ND
NC 2B = NE
Chloroform 14-Oct-15 0.14 5 13.9 ND ND
NC 2B = NE
Tetrachloroethene
NC 2B = 3.3 µg/L (10/23/07) (HH)29-Apr-15 0.2 1.0 8.1 ND ND
Resample >27-May-15 0.2 1.0 3.5 ---ND
14-Oct-15 0.46 1.0 4.4 ND ND
Toluene 12-Apr-12 ------ND ND ---
10-Oct-12 ------ND 0.257 ---
NC 2B = 11 µg/L (HH)10-Apr-13 ------ND ND ---
11-Sep-13 ------ND ND ---
24-Apr-14 0.26 1.0 Dry ND ND
2-Oct-14 0.26 1.0 Dry ND ND
29-Apr-15 0.20 1.0 ND ND ND
14-Oct-15 0.26 1.0 ND ND ND
Notes:
All concentrations are in micrograms per liter (µg/L).
NC 2B = North Carolina Surface Water Standards established under 15A NCAC 2B.
(NC 2B shown is the lowest of "Freshwater Aquatic Life" (FAL) or "Human Health" (HH) standard.)
RL = Laboratory reporting limit (NC SWSL or lower).
DL = Laboratory detection limit.
J = Estimated value between the DL and the SWSL.
B = Blank-qualified data; result is suspected to be biased high based on concentrations in the blanks.
ND = Not detected above the DL.
--- = Data not available.
Data prior to May 2014 provided by W.Z. Baumgartner & Associates, Inc.
Bold values exceed the NC 2B standard.
OmniSource Kernersville Landfill
Permit No. 34-20 3 of 3
Joyce Engineering

Figure

Figure 1 Site Location Map

Drawing

Drawing 1 Groundwater Potentiometric Surface Map

APPENDICES

Appendix A

Field Data Logs

Appendix B

Laboratory Analytical Reports
and Chains of Custody

#=CL#
October 28, 2015
LIMS USE: FR - ALEX EVERHART
LIMS OBJECT ID: 92272115
92272115
Project:
Pace Project No.:
RE:
Mr. Alex Everhart
Joyce Engineering-NC
2211 W. Meadowview Road
Suite 101
Greensboro, NC 27407
OMNISOURCE/KERNERSVILLE LF
Dear Mr. Everhart:
Enclosed are the analytical results for sample(s) received by the laboratory on October 15, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
cc:Mr. Van Burbach, Joyce Engineering-NC
Alex Everhart, Joyce Engineering-NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 34
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 34
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Lab ID Sample ID Matrix Date Collected Date Received
92272115001 3420-FIELD BLANK Water 10/14/15 14:15 10/15/15 11:29
92272115002 3420-MW12 Water 10/14/15 13:15 10/15/15 11:29
92272115003 3420-MW13 Water 10/14/15 13:44 10/15/15 11:29
92272115004 3420-MW14 Water 10/14/15 11:25 10/15/15 11:29
92272115005 3420-MW1R Water 10/14/15 14:00 10/15/15 11:29
92272115006 3420-SW1 Water 10/14/15 13:30 10/15/15 11:29
92272115007 3420-SW2 Water 10/14/15 12:00 10/15/15 11:29
92272115008 3420-TRIP BLANK Water 10/14/15 08:00 10/15/15 11:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92272115001 3420-FIELD BLANK EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92272115002 3420-MW12 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92272115003 3420-MW13 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92272115004 3420-MW14 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92272115005 3420-MW1R EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92272115006 3420-SW1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92272115007 3420-SW2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92272115008 3420-TRIP BLANK EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 34
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92272115001 3420-FIELD BLANK
Methylene Chloride 3.6 ug/L 10/27/15 03:061.0EPA 8260
92272115002 3420-MW12
Barium 179 ug/L 10/20/15 21:04100EPA 6010
Copper 3.5J ug/L 10/20/15 21:0410.0EPA 6010
Lead 3.5J ug/L 10/20/15 21:0410.0EPA 6010
Nickel 5.8J ug/L 10/20/15 21:0450.0EPA 6010
Vanadium 5.4J ug/L 10/20/15 21:0425.0EPA 6010
Zinc 8.9J ug/L 10/20/15 21:0410.0EPA 6010
cis-1,2-Dichloroethene 0.20J ug/L 10/27/15 03:235.0EPA 8260
92272115003 3420-MW13
Barium 43.1J ug/L 10/20/15 21:07100EPA 6010
Chromium 2.8J ug/L 10/20/15 21:0710.0EPA 6010
Cobalt 7.2J ug/L 10/20/15 21:0710.0EPA 6010
Copper 4.3J ug/L 10/20/15 21:0710.0EPA 6010
Nickel 4.9J ug/L 10/20/15 21:0750.0EPA 6010
Vanadium 8.5J ug/L 10/20/15 21:0725.0EPA 6010
Zinc 7.6J ug/L 10/20/15 21:0710.0EPA 6010
92272115004 3420-MW14
Barium 121 ug/L 10/20/15 21:19100EPA 6010
Beryllium 1.4 ug/L 10/20/15 21:191.0EPA 6010
Cobalt 5.4J ug/L 10/20/15 21:1910.0EPA 6010
Nickel 2.6J ug/L 10/20/15 21:1950.0EPA 6010
Zinc 5.1J ug/L 10/20/15 21:1910.0EPA 6010
92272115005 3420-MW1R
Barium 17.2J ug/L 10/20/15 21:22100EPA 6010
Zinc 7.1J ug/L 10/20/15 21:2210.0EPA 6010
Benzene 1.8 ug/L 10/27/15 04:151.0EPA 8260
92272115006 3420-SW1
Barium 59.6J ug/L 10/20/15 21:25100EPA 6010
Copper 2.8J ug/L 10/20/15 21:2510.0EPA 6010
Zinc 52.0 ug/L 10/20/15 21:2510.0EPA 6010
Carbon tetrachloride 4.5 ug/L 10/27/15 04:321.0EPA 8260
Chloroform 13.9 ug/L 10/27/15 04:325.0EPA 8260
cis-1,2-Dichloroethene 0.70J ug/L 10/27/15 04:325.0EPA 8260
Tetrachloroethene 4.4 ug/L 10/27/15 04:321.0EPA 8260
92272115007 3420-SW2
Barium 101 ug/L 10/20/15 21:28100EPA 6010
Copper 3.2J ug/L 10/20/15 21:2810.0EPA 6010
Nickel 4.4J ug/L 10/20/15 21:2850.0EPA 6010
Zinc 29.7 ug/L 10/20/15 21:2810.0EPA 6010
Benzene 0.45J ug/L 10/27/15 04:501.0EPA 8260
92272115008 3420-TRIP BLANK
Methylene Chloride 1.7 ug/L 10/27/15 05:071.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-FIELD BLANK Lab ID:92272115001 Collected:10/14/15 14:15 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/20/15 23:56 7440-36-010/16/15 19:006.0 3.8 1
Arsenic ND ug/L 10/20/15 23:56 7440-38-210/16/15 19:0010.0 2.5 1
Barium ND ug/L 10/20/15 23:56 7440-39-310/16/15 19:001002.5 1
Beryllium ND ug/L 10/20/15 23:56 7440-41-710/16/15 19:001.0 0.50 1
Cadmium ND ug/L 10/20/15 23:56 7440-43-910/16/15 19:001.0 0.50 1
Chromium ND ug/L 10/20/15 23:56 7440-47-310/16/15 19:0010.0 2.5 1
Cobalt ND ug/L 10/20/15 23:56 7440-48-410/16/15 19:0010.0 2.5 1
Copper ND ug/L 10/20/15 23:56 7440-50-810/16/15 19:0010.0 2.5 1
Lead ND ug/L 10/20/15 23:56 7439-92-110/16/15 19:0010.0 2.5 1
Nickel ND ug/L 10/20/15 23:56 7440-02-010/16/15 19:0050.0 2.5 1
Selenium ND ug/L 10/20/15 23:56 7782-49-210/16/15 19:0010.0 5.0 1
Silver ND ug/L 10/20/15 23:56 7440-22-410/16/15 19:0010.0 2.5 1
Thallium ND ug/L 10/20/15 23:56 7440-28-010/16/15 19:005.5 5.0 1
Vanadium ND ug/L 10/20/15 23:56 7440-62-210/16/15 19:0025.0 2.5 1
Zinc ND ug/L 10/20/15 23:56 7440-66-610/16/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/27/15 03:06 67-64-110010.0 1
Acrylonitrile ND ug/L 10/27/15 03:06 107-13-12001.9 1
Benzene ND ug/L 10/27/15 03:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/27/15 03:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/27/15 03:06 75-27-41.0 0.18 1
Bromoform ND ug/L 10/27/15 03:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/27/15 03:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/27/15 03:06 78-93-31000.96 1
Carbon disulfide ND ug/L 10/27/15 03:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/27/15 03:06 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/27/15 03:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/27/15 03:06 75-00-310.0 0.54 1
Chloroform ND ug/L 10/27/15 03:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/27/15 03:06 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/27/15 03:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/27/15 03:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/27/15 03:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/27/15 03:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/27/15 03:06 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/27/15 03:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/27/15 03:06 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/27/15 03:06 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/27/15 03:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/27/15 03:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/27/15 03:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/27/15 03:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/27/15 03:06 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/27/15 03:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/27/15 03:06 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-FIELD BLANK Lab ID:92272115001 Collected:10/14/15 14:15 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/27/15 03:06 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/27/15 03:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/27/15 03:06 74-88-410.0 0.32 1
Methylene Chloride 3.6 ug/L 10/27/15 03:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/27/15 03:06 108-10-11000.33 1
Styrene ND ug/L 10/27/15 03:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/27/15 03:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/27/15 03:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/27/15 03:06 127-18-41.0 0.46 1
Toluene ND ug/L 10/27/15 03:06 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/27/15 03:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/27/15 03:06 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/27/15 03:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/27/15 03:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/27/15 03:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/27/15 03:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/27/15 03:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/27/15 03:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %10/27/15 03:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %10/27/15 03:06 17060-07-070-130 1
Toluene-d8 (S)101 %10/27/15 03:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW12 Lab ID:92272115002 Collected:10/14/15 13:15 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/20/15 21:04 7440-36-010/19/15 19:306.0 3.8 1
Arsenic ND ug/L 10/20/15 21:04 7440-38-210/19/15 19:3010.0 2.5 1
Barium 179 ug/L 10/20/15 21:04 7440-39-310/19/15 19:301002.5 1
Beryllium ND ug/L 10/20/15 21:04 7440-41-710/19/15 19:301.0 0.50 1
Cadmium ND ug/L 10/20/15 21:04 7440-43-910/19/15 19:301.0 0.50 1
Chromium ND ug/L 10/20/15 21:04 7440-47-310/19/15 19:3010.0 2.5 1
Cobalt ND ug/L 10/20/15 21:04 7440-48-410/19/15 19:3010.0 2.5 1
Copper 3.5J ug/L 10/20/15 21:04 7440-50-810/19/15 19:3010.0 2.5 1
Lead 3.5J ug/L 10/20/15 21:04 7439-92-110/19/15 19:3010.0 2.5 1
Nickel 5.8J ug/L 10/20/15 21:04 7440-02-010/19/15 19:3050.0 2.5 1
Selenium ND ug/L 10/20/15 21:04 7782-49-210/19/15 19:3010.0 5.0 1
Silver ND ug/L 10/20/15 21:04 7440-22-410/19/15 19:3010.0 2.5 1
Thallium ND ug/L 10/20/15 21:04 7440-28-010/19/15 19:305.5 5.0 1
Vanadium 5.4J ug/L 10/20/15 21:04 7440-62-210/19/15 19:3025.0 2.5 1
Zinc 8.9J ug/L 10/20/15 21:04 7440-66-610/19/15 19:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/27/15 03:23 67-64-110010.0 1
Acrylonitrile ND ug/L 10/27/15 03:23 107-13-12001.9 1
Benzene ND ug/L 10/27/15 03:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/27/15 03:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/27/15 03:23 75-27-41.0 0.18 1
Bromoform ND ug/L 10/27/15 03:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/27/15 03:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/27/15 03:23 78-93-31000.96 1
Carbon disulfide ND ug/L 10/27/15 03:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/27/15 03:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/27/15 03:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/27/15 03:23 75-00-310.0 0.54 1
Chloroform ND ug/L 10/27/15 03:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/27/15 03:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/27/15 03:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/27/15 03:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/27/15 03:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/27/15 03:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/27/15 03:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/27/15 03:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/27/15 03:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/27/15 03:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/27/15 03:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/27/15 03:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.20J ug/L 10/27/15 03:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/27/15 03:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/27/15 03:23 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/27/15 03:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/27/15 03:23 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW12 Lab ID:92272115002 Collected:10/14/15 13:15 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/27/15 03:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/27/15 03:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/27/15 03:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/27/15 03:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/27/15 03:23 108-10-11000.33 1
Styrene ND ug/L 10/27/15 03:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/27/15 03:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/27/15 03:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/27/15 03:23 127-18-41.0 0.46 1
Toluene ND ug/L 10/27/15 03:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/27/15 03:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/27/15 03:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/27/15 03:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/27/15 03:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/27/15 03:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/27/15 03:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/27/15 03:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/27/15 03:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/27/15 03:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %10/27/15 03:23 17060-07-070-130 1
Toluene-d8 (S)101 %10/27/15 03:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW13 Lab ID:92272115003 Collected:10/14/15 13:44 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/20/15 21:07 7440-36-010/19/15 19:306.0 3.8 1
Arsenic ND ug/L 10/20/15 21:07 7440-38-210/19/15 19:3010.0 2.5 1
Barium 43.1J ug/L 10/20/15 21:07 7440-39-310/19/15 19:301002.5 1
Beryllium ND ug/L 10/20/15 21:07 7440-41-710/19/15 19:301.0 0.50 1
Cadmium ND ug/L 10/20/15 21:07 7440-43-910/19/15 19:301.0 0.50 1
Chromium 2.8J ug/L 10/20/15 21:07 7440-47-310/19/15 19:3010.0 2.5 1
Cobalt 7.2J ug/L 10/20/15 21:07 7440-48-410/19/15 19:3010.0 2.5 1
Copper 4.3J ug/L 10/20/15 21:07 7440-50-810/19/15 19:3010.0 2.5 1
Lead ND ug/L 10/20/15 21:07 7439-92-110/19/15 19:3010.0 2.5 1
Nickel 4.9J ug/L 10/20/15 21:07 7440-02-010/19/15 19:3050.0 2.5 1
Selenium ND ug/L 10/20/15 21:07 7782-49-210/19/15 19:3010.0 5.0 1
Silver ND ug/L 10/20/15 21:07 7440-22-410/19/15 19:3010.0 2.5 1
Thallium ND ug/L 10/20/15 21:07 7440-28-010/19/15 19:305.5 5.0 1
Vanadium 8.5J ug/L 10/20/15 21:07 7440-62-210/19/15 19:3025.0 2.5 1
Zinc 7.6J ug/L 10/20/15 21:07 7440-66-610/19/15 19:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/27/15 03:40 67-64-110010.0 1
Acrylonitrile ND ug/L 10/27/15 03:40 107-13-12001.9 1
Benzene ND ug/L 10/27/15 03:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/27/15 03:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/27/15 03:40 75-27-41.0 0.18 1
Bromoform ND ug/L 10/27/15 03:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/27/15 03:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/27/15 03:40 78-93-31000.96 1
Carbon disulfide ND ug/L 10/27/15 03:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/27/15 03:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/27/15 03:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/27/15 03:40 75-00-310.0 0.54 1
Chloroform ND ug/L 10/27/15 03:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/27/15 03:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/27/15 03:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/27/15 03:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/27/15 03:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/27/15 03:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/27/15 03:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/27/15 03:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/27/15 03:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/27/15 03:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/27/15 03:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/27/15 03:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/27/15 03:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/27/15 03:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/27/15 03:40 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/27/15 03:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/27/15 03:40 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW13 Lab ID:92272115003 Collected:10/14/15 13:44 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/27/15 03:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/27/15 03:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/27/15 03:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/27/15 03:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/27/15 03:40 108-10-11000.33 1
Styrene ND ug/L 10/27/15 03:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/27/15 03:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/27/15 03:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/27/15 03:40 127-18-41.0 0.46 1
Toluene ND ug/L 10/27/15 03:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/27/15 03:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/27/15 03:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/27/15 03:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/27/15 03:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/27/15 03:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/27/15 03:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/27/15 03:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/27/15 03:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %10/27/15 03:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %10/27/15 03:40 17060-07-070-130 1
Toluene-d8 (S)102 %10/27/15 03:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW14 Lab ID:92272115004 Collected:10/14/15 11:25 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/20/15 21:19 7440-36-010/19/15 19:306.0 3.8 1
Arsenic ND ug/L 10/20/15 21:19 7440-38-210/19/15 19:3010.0 2.5 1
Barium 121 ug/L 10/20/15 21:19 7440-39-310/19/15 19:301002.5 1
Beryllium 1.4 ug/L 10/20/15 21:19 7440-41-710/19/15 19:301.0 0.50 1
Cadmium ND ug/L 10/20/15 21:19 7440-43-910/19/15 19:301.0 0.50 1
Chromium ND ug/L 10/20/15 21:19 7440-47-310/19/15 19:3010.0 2.5 1
Cobalt 5.4J ug/L 10/20/15 21:19 7440-48-410/19/15 19:3010.0 2.5 1
Copper ND ug/L 10/20/15 21:19 7440-50-810/19/15 19:3010.0 2.5 1
Lead ND ug/L 10/20/15 21:19 7439-92-110/19/15 19:3010.0 2.5 1
Nickel 2.6J ug/L 10/20/15 21:19 7440-02-010/19/15 19:3050.0 2.5 1
Selenium ND ug/L 10/20/15 21:19 7782-49-210/19/15 19:3010.0 5.0 1
Silver ND ug/L 10/20/15 21:19 7440-22-410/19/15 19:3010.0 2.5 1
Thallium ND ug/L 10/20/15 21:19 7440-28-010/19/15 19:305.5 5.0 1
Vanadium ND ug/L 10/20/15 21:19 7440-62-210/19/15 19:3025.0 2.5 1
Zinc 5.1J ug/L 10/20/15 21:19 7440-66-610/19/15 19:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/27/15 03:58 67-64-110010.0 1
Acrylonitrile ND ug/L 10/27/15 03:58 107-13-12001.9 1
Benzene ND ug/L 10/27/15 03:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/27/15 03:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/27/15 03:58 75-27-41.0 0.18 1
Bromoform ND ug/L 10/27/15 03:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/27/15 03:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/27/15 03:58 78-93-31000.96 1
Carbon disulfide ND ug/L 10/27/15 03:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/27/15 03:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/27/15 03:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/27/15 03:58 75-00-310.0 0.54 1
Chloroform ND ug/L 10/27/15 03:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/27/15 03:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/27/15 03:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/27/15 03:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/27/15 03:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/27/15 03:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/27/15 03:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/27/15 03:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/27/15 03:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/27/15 03:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/27/15 03:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/27/15 03:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/27/15 03:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/27/15 03:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/27/15 03:58 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/27/15 03:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/27/15 03:58 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW14 Lab ID:92272115004 Collected:10/14/15 11:25 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/27/15 03:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/27/15 03:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/27/15 03:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/27/15 03:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/27/15 03:58 108-10-11000.33 1
Styrene ND ug/L 10/27/15 03:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/27/15 03:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/27/15 03:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/27/15 03:58 127-18-41.0 0.46 1
Toluene ND ug/L 10/27/15 03:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/27/15 03:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/27/15 03:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/27/15 03:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/27/15 03:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/27/15 03:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/27/15 03:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/27/15 03:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/27/15 03:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/27/15 03:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %10/27/15 03:58 17060-07-070-130 1
Toluene-d8 (S)101 %10/27/15 03:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW1R Lab ID:92272115005 Collected:10/14/15 14:00 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/20/15 21:22 7440-36-010/19/15 19:306.0 3.8 1
Arsenic ND ug/L 10/20/15 21:22 7440-38-210/19/15 19:3010.0 2.5 1
Barium 17.2J ug/L 10/20/15 21:22 7440-39-310/19/15 19:301002.5 1
Beryllium ND ug/L 10/20/15 21:22 7440-41-710/19/15 19:301.0 0.50 1
Cadmium ND ug/L 10/20/15 21:22 7440-43-910/19/15 19:301.0 0.50 1
Chromium ND ug/L 10/20/15 21:22 7440-47-310/19/15 19:3010.0 2.5 1
Cobalt ND ug/L 10/20/15 21:22 7440-48-410/19/15 19:3010.0 2.5 1
Copper ND ug/L 10/20/15 21:22 7440-50-810/19/15 19:3010.0 2.5 1
Lead ND ug/L 10/20/15 21:22 7439-92-110/19/15 19:3010.0 2.5 1
Nickel ND ug/L 10/20/15 21:22 7440-02-010/19/15 19:3050.0 2.5 1
Selenium ND ug/L 10/20/15 21:22 7782-49-210/19/15 19:3010.0 5.0 1
Silver ND ug/L 10/20/15 21:22 7440-22-410/19/15 19:3010.0 2.5 1
Thallium ND ug/L 10/20/15 21:22 7440-28-010/19/15 19:305.5 5.0 1
Vanadium ND ug/L 10/20/15 21:22 7440-62-210/19/15 19:3025.0 2.5 1
Zinc 7.1J ug/L 10/20/15 21:22 7440-66-610/19/15 19:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/27/15 04:15 67-64-110010.0 1
Acrylonitrile ND ug/L 10/27/15 04:15 107-13-12001.9 1
Benzene 1.8 ug/L 10/27/15 04:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/27/15 04:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/27/15 04:15 75-27-41.0 0.18 1
Bromoform ND ug/L 10/27/15 04:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/27/15 04:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/27/15 04:15 78-93-31000.96 1
Carbon disulfide ND ug/L 10/27/15 04:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/27/15 04:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/27/15 04:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/27/15 04:15 75-00-310.0 0.54 1
Chloroform ND ug/L 10/27/15 04:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/27/15 04:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/27/15 04:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/27/15 04:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/27/15 04:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/27/15 04:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/27/15 04:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/27/15 04:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/27/15 04:15 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/27/15 04:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/27/15 04:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/27/15 04:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/27/15 04:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/27/15 04:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/27/15 04:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/27/15 04:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/27/15 04:15 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW1R Lab ID:92272115005 Collected:10/14/15 14:00 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/27/15 04:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/27/15 04:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/27/15 04:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/27/15 04:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/27/15 04:15 108-10-11000.33 1
Styrene ND ug/L 10/27/15 04:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/27/15 04:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/27/15 04:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/27/15 04:15 127-18-41.0 0.46 1
Toluene ND ug/L 10/27/15 04:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/27/15 04:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/27/15 04:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/27/15 04:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/27/15 04:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/27/15 04:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/27/15 04:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/27/15 04:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/27/15 04:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/27/15 04:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %10/27/15 04:15 17060-07-070-130 1
Toluene-d8 (S)101 %10/27/15 04:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW1 Lab ID:92272115006 Collected:10/14/15 13:30 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/20/15 21:25 7440-36-010/19/15 19:306.0 3.8 1
Arsenic ND ug/L 10/20/15 21:25 7440-38-210/19/15 19:3010.0 2.5 1
Barium 59.6J ug/L 10/20/15 21:25 7440-39-310/19/15 19:301002.5 1
Beryllium ND ug/L 10/20/15 21:25 7440-41-710/19/15 19:301.0 0.50 1
Cadmium ND ug/L 10/20/15 21:25 7440-43-910/19/15 19:301.0 0.50 1
Chromium ND ug/L 10/20/15 21:25 7440-47-310/19/15 19:3010.0 2.5 1
Cobalt ND ug/L 10/20/15 21:25 7440-48-410/19/15 19:3010.0 2.5 1
Copper 2.8J ug/L 10/20/15 21:25 7440-50-810/19/15 19:3010.0 2.5 1
Lead ND ug/L 10/20/15 21:25 7439-92-110/19/15 19:3010.0 2.5 1
Nickel ND ug/L 10/20/15 21:25 7440-02-010/19/15 19:3050.0 2.5 1
Selenium ND ug/L 10/20/15 21:25 7782-49-210/19/15 19:3010.0 5.0 1
Silver ND ug/L 10/20/15 21:25 7440-22-410/19/15 19:3010.0 2.5 1
Thallium ND ug/L 10/20/15 21:25 7440-28-010/19/15 19:305.5 5.0 1
Vanadium ND ug/L 10/20/15 21:25 7440-62-210/19/15 19:3025.0 2.5 1
Zinc 52.0 ug/L 10/20/15 21:25 7440-66-610/19/15 19:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/27/15 04:32 67-64-110010.0 1
Acrylonitrile ND ug/L 10/27/15 04:32 107-13-12001.9 1
Benzene ND ug/L 10/27/15 04:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/27/15 04:32 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/27/15 04:32 75-27-41.0 0.18 1
Bromoform ND ug/L 10/27/15 04:32 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/27/15 04:32 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/27/15 04:32 78-93-31000.96 1
Carbon disulfide ND ug/L 10/27/15 04:32 75-15-01001.2 1
Carbon tetrachloride 4.5 ug/L 10/27/15 04:32 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/27/15 04:32 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/27/15 04:32 75-00-310.0 0.54 1
Chloroform 13.9 ug/L 10/27/15 04:32 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/27/15 04:32 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/27/15 04:32 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/27/15 04:32 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/27/15 04:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/27/15 04:32 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/27/15 04:32 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/27/15 04:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/27/15 04:32 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/27/15 04:32 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/27/15 04:32 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/27/15 04:32 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.70J ug/L 10/27/15 04:32 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/27/15 04:32 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/27/15 04:32 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/27/15 04:32 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/27/15 04:32 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW1 Lab ID:92272115006 Collected:10/14/15 13:30 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/27/15 04:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/27/15 04:32 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/27/15 04:32 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/27/15 04:32 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/27/15 04:32 108-10-11000.33 1
Styrene ND ug/L 10/27/15 04:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/27/15 04:32 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/27/15 04:32 79-34-53.0 0.40 1
Tetrachloroethene 4.4 ug/L 10/27/15 04:32 127-18-41.0 0.46 1
Toluene ND ug/L 10/27/15 04:32 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/27/15 04:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/27/15 04:32 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/27/15 04:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/27/15 04:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/27/15 04:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/27/15 04:32 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/27/15 04:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/27/15 04:32 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %10/27/15 04:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %10/27/15 04:32 17060-07-070-130 1
Toluene-d8 (S)101 %10/27/15 04:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW2 Lab ID:92272115007 Collected:10/14/15 12:00 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/20/15 21:28 7440-36-010/19/15 19:306.0 3.8 1
Arsenic ND ug/L 10/20/15 21:28 7440-38-210/19/15 19:3010.0 2.5 1
Barium 101 ug/L 10/20/15 21:28 7440-39-310/19/15 19:301002.5 1
Beryllium ND ug/L 10/20/15 21:28 7440-41-710/19/15 19:301.0 0.50 1
Cadmium ND ug/L 10/20/15 21:28 7440-43-910/19/15 19:301.0 0.50 1
Chromium ND ug/L 10/20/15 21:28 7440-47-310/19/15 19:3010.0 2.5 1
Cobalt ND ug/L 10/20/15 21:28 7440-48-410/19/15 19:3010.0 2.5 1
Copper 3.2J ug/L 10/20/15 21:28 7440-50-810/19/15 19:3010.0 2.5 1
Lead ND ug/L 10/20/15 21:28 7439-92-110/19/15 19:3010.0 2.5 1
Nickel 4.4J ug/L 10/20/15 21:28 7440-02-010/19/15 19:3050.0 2.5 1
Selenium ND ug/L 10/20/15 21:28 7782-49-210/19/15 19:3010.0 5.0 1
Silver ND ug/L 10/20/15 21:28 7440-22-410/19/15 19:3010.0 2.5 1
Thallium ND ug/L 10/20/15 21:28 7440-28-010/19/15 19:305.5 5.0 1
Vanadium ND ug/L 10/20/15 21:28 7440-62-210/19/15 19:3025.0 2.5 1
Zinc 29.7 ug/L 10/20/15 21:28 7440-66-610/19/15 19:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/27/15 04:50 67-64-1 M110010.0 1
Acrylonitrile ND ug/L 10/27/15 04:50 107-13-12001.9 1
Benzene 0.45J ug/L 10/27/15 04:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/27/15 04:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/27/15 04:50 75-27-41.0 0.18 1
Bromoform ND ug/L 10/27/15 04:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/27/15 04:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/27/15 04:50 78-93-31000.96 1
Carbon disulfide ND ug/L 10/27/15 04:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/27/15 04:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/27/15 04:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/27/15 04:50 75-00-310.0 0.54 1
Chloroform ND ug/L 10/27/15 04:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/27/15 04:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/27/15 04:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/27/15 04:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/27/15 04:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/27/15 04:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/27/15 04:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/27/15 04:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/27/15 04:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/27/15 04:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/27/15 04:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/27/15 04:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/27/15 04:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/27/15 04:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/27/15 04:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/27/15 04:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/27/15 04:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
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[phone]
Page 18 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW2 Lab ID:92272115007 Collected:10/14/15 12:00 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/27/15 04:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/27/15 04:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/27/15 04:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/27/15 04:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/27/15 04:50 108-10-11000.33 1
Styrene ND ug/L 10/27/15 04:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/27/15 04:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/27/15 04:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/27/15 04:50 127-18-41.0 0.46 1
Toluene ND ug/L 10/27/15 04:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/27/15 04:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/27/15 04:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/27/15 04:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/27/15 04:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/27/15 04:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/27/15 04:50 108-05-4 M150.0 0.35 1
Vinyl chloride ND ug/L 10/27/15 04:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/27/15 04:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/27/15 04:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %10/27/15 04:50 17060-07-070-130 1
Toluene-d8 (S)102 %10/27/15 04:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
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Page 19 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-TRIP BLANK Lab ID:92272115008 Collected:10/14/15 08:00 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/27/15 05:07 67-64-110010.0 1
Acrylonitrile ND ug/L 10/27/15 05:07 107-13-12001.9 1
Benzene ND ug/L 10/27/15 05:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/27/15 05:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/27/15 05:07 75-27-41.0 0.18 1
Bromoform ND ug/L 10/27/15 05:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/27/15 05:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/27/15 05:07 78-93-31000.96 1
Carbon disulfide ND ug/L 10/27/15 05:07 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/27/15 05:07 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/27/15 05:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/27/15 05:07 75-00-310.0 0.54 1
Chloroform ND ug/L 10/27/15 05:07 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/27/15 05:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/27/15 05:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/27/15 05:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/27/15 05:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/27/15 05:07 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/27/15 05:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/27/15 05:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/27/15 05:07 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/27/15 05:07 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/27/15 05:07 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/27/15 05:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/27/15 05:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/27/15 05:07 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/27/15 05:07 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/27/15 05:07 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/27/15 05:07 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/27/15 05:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/27/15 05:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/27/15 05:07 74-88-410.0 0.32 1
Methylene Chloride 1.7 ug/L 10/27/15 05:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/27/15 05:07 108-10-11000.33 1
Styrene ND ug/L 10/27/15 05:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/27/15 05:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/27/15 05:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/27/15 05:07 127-18-41.0 0.46 1
Toluene ND ug/L 10/27/15 05:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/27/15 05:07 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/27/15 05:07 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/27/15 05:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/27/15 05:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/27/15 05:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/27/15 05:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/27/15 05:07 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Sample:3420-TRIP BLANK Lab ID:92272115008 Collected:10/14/15 08:00 Received:10/15/15 11:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 10/27/15 05:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/27/15 05:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %10/27/15 05:07 17060-07-070-130 1
Toluene-d8 (S)101 %10/27/15 05:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19828
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92272115001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1584686
Associated Lab Samples:92272115001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 10/20/15 22:193.8
Arsenic ug/L ND 10.0 10/20/15 22:192.5
Barium ug/L ND 100 10/20/15 22:192.5
Beryllium ug/L ND 1.0 10/20/15 22:190.50
Cadmium ug/L ND 1.0 10/20/15 22:190.50
Chromium ug/L ND 10.0 10/20/15 22:192.5
Cobalt ug/L ND 10.0 10/20/15 22:192.5
Copper ug/L ND 10.0 10/20/15 22:192.5
Lead ug/L ND 10.0 10/20/15 22:192.5
Nickel ug/L ND 50.0 10/20/15 22:192.5
Selenium ug/L ND 10.0 10/20/15 22:195.0
Silver ug/L ND 10.0 10/20/15 22:192.5
Thallium ug/L ND 5.5 10/20/15 22:195.0
Vanadium ug/L ND 25.0 10/20/15 22:192.5
Zinc ug/L ND 10.0 10/20/15 22:195.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1584687LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 468500 94 80-120
Arsenic ug/L 450500 90 80-120
Barium ug/L 468500 94 80-120
Beryllium ug/L 464500 93 80-120
Cadmium ug/L 466500 93 80-120
Chromium ug/L 462500 92 80-120
Cobalt ug/L 462500 92 80-120
Copper ug/L 475500 95 80-120
Lead ug/L 454500 91 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 451500 90 80-120
Silver ug/L 230250 92 80-120
Thallium ug/L 451500 90 80-120
Vanadium ug/L 459500 92 80-120
Zinc ug/L 448500 90 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1584688MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272094005
1584689
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 92 75-12589 3 25500ND461446
Arsenic ug/L 500 90 75-12588 2 25500ND449440
Barium ug/L 500 94 75-12592 2 2550041.2 513 501
Beryllium ug/L 500 93 75-12591 3 25500ND467455
Cadmium ug/L 500 93 75-12591 3 25500ND465453
Chromium ug/L 500 92 75-12591 2 25500ND464455
Cobalt ug/L 500 93 75-12590 3 25500ND464452
Copper ug/L 500 94 75-12593 1 25500ND474469
Lead ug/L 500 91 75-12588 3 25500ND455443
Nickel ug/L 500 93 75-12591 2 25500ND465454
Selenium ug/L 500 90 75-12588 2 25500ND452441
Silver ug/L 250 91 75-12589 2 25250ND227223
Thallium ug/L 500 90 75-12588 2 25500ND450440
Vanadium ug/L 500 92 75-12590 2 255004.3J 463 456
Zinc ug/L 500 90 75-12588 2 255005.5J 453 444
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19840
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92272115002, 92272115003, 92272115004, 92272115005, 92272115006, 92272115007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1585679
Associated Lab Samples:92272115002, 92272115003, 92272115004, 92272115005, 92272115006, 92272115007
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 10/20/15 20:033.8
Arsenic ug/L ND 10.0 10/20/15 20:032.5
Barium ug/L ND 100 10/20/15 20:032.5
Beryllium ug/L ND 1.0 10/20/15 20:030.50
Cadmium ug/L ND 1.0 10/20/15 20:030.50
Chromium ug/L ND 10.0 10/20/15 20:032.5
Cobalt ug/L ND 10.0 10/20/15 20:032.5
Copper ug/L ND 10.0 10/20/15 20:032.5
Lead ug/L ND 10.0 10/20/15 20:032.5
Nickel ug/L ND 50.0 10/20/15 20:032.5
Selenium ug/L ND 10.0 10/20/15 20:035.0
Silver ug/L ND 10.0 10/20/15 20:032.5
Thallium ug/L ND 5.5 10/20/15 20:035.0
Vanadium ug/L ND 25.0 10/20/15 20:032.5
Zinc ug/L ND 10.0 10/20/15 20:035.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1585680LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 511500 102 80-120
Arsenic ug/L 488500 98 80-120
Barium ug/L 514500 103 80-120
Beryllium ug/L 510500 102 80-120
Cadmium ug/L 509500 102 80-120
Chromium ug/L 507500 101 80-120
Cobalt ug/L 501500 100 80-120
Copper ug/L 516500 103 80-120
Lead ug/L 495500 99 80-120
Nickel ug/L 505500 101 80-120
Selenium ug/L 495500 99 80-120
Silver ug/L 249250 100 80-120
Thallium ug/L 491500 98 80-120
Vanadium ug/L 495500 99 80-120
Zinc ug/L 485500 97 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1585681MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272154001
1585682
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12594 1 25500ND480474
Arsenic ug/L 500 95 75-12593 2 25500ND478470
Barium ug/L 500 96 75-12593 3 2550070.7 551 535
Beryllium ug/L 500 94 75-12591 2 25500ND468457
Cadmium ug/L 500 95 75-12594 1 25500ND477471
Chromium ug/L 500 94 75-12593 2 25500ND474465
Cobalt ug/L 500 96 75-12595 1 255005.2 485 478
Copper ug/L 500 98 75-12596 2 255006.7 495 487
Lead ug/L 500 94 75-12593 1 25500ND474468
Nickel ug/L 500 94 75-12593 2 25500ND476467
Selenium ug/L 500 94 75-12592 2 25500ND468460
Silver ug/L 250 94 75-12592 2 25250ND235231
Thallium ug/L 500 91 75-12590 1 25500ND457453
Vanadium ug/L 500 95 75-12593 2 255006.9 483 473
Zinc ug/L 500 99 75-12597 1 2550018.8 512 505
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2015 04:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33996
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92272115001, 92272115002, 92272115003, 92272115004, 92272115005, 92272115006, 92272115007,
92272115008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1591707
Associated Lab Samples:92272115001, 92272115002, 92272115003, 92272115004, 92272115005, 92272115006, 92272115007,
92272115008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/27/15 02:310.33
1,1,1-Trichloroethane ug/L ND 1.0 10/27/15 02:310.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 10/27/15 02:310.40
1,1,2-Trichloroethane ug/L ND 1.0 10/27/15 02:310.29
1,1-Dichloroethane ug/L ND 5.0 10/27/15 02:310.32
1,1-Dichloroethene ug/L ND 5.0 10/27/15 02:310.56
1,2,3-Trichloropropane ug/L ND 1.0 10/27/15 02:310.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 10/27/15 02:312.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/27/15 02:310.27
1,2-Dichlorobenzene ug/L ND 5.0 10/27/15 02:310.30
1,2-Dichloroethane ug/L ND 1.0 10/27/15 02:310.24
1,2-Dichloropropane ug/L ND 1.0 10/27/15 02:310.27
1,4-Dichlorobenzene ug/L ND 1.0 10/27/15 02:310.33
2-Butanone (MEK)ug/L ND 100 10/27/15 02:310.96
2-Hexanone ug/L ND 50.0 10/27/15 02:310.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 10/27/15 02:310.33
Acetone ug/L ND 100 10/27/15 02:3110.0
Acrylonitrile ug/L ND 200 10/27/15 02:311.9
Benzene ug/L ND 1.0 10/27/15 02:310.25
Bromochloromethane ug/L ND 3.0 10/27/15 02:310.17
Bromodichloromethane ug/L ND 1.0 10/27/15 02:310.18
Bromoform ug/L ND 3.0 10/27/15 02:310.26
Bromomethane ug/L ND 10.0 10/27/15 02:310.29
Carbon disulfide ug/L ND 100 10/27/15 02:311.2
Carbon tetrachloride ug/L ND 1.0 10/27/15 02:310.25
Chlorobenzene ug/L ND 3.0 10/27/15 02:310.23
Chloroethane ug/L ND 10.0 10/27/15 02:310.54
Chloroform ug/L ND 5.0 10/27/15 02:310.14
Chloromethane ug/L ND 1.0 10/27/15 02:310.11
cis-1,2-Dichloroethene ug/L ND 5.0 10/27/15 02:310.19
cis-1,3-Dichloropropene ug/L ND 1.0 10/27/15 02:310.13
Dibromochloromethane ug/L ND 3.0 10/27/15 02:310.21
Dibromomethane ug/L ND 10.0 10/27/15 02:310.21
Ethylbenzene ug/L ND 1.0 10/27/15 02:310.30
Iodomethane ug/L ND 10.0 10/27/15 02:310.32
Methylene Chloride ug/L ND 1.0 10/27/15 02:310.97
Styrene ug/L ND 1.0 10/27/15 02:310.26
Tetrachloroethene ug/L ND 1.0 10/27/15 02:310.46
Toluene ug/L ND 1.0 10/27/15 02:310.26
trans-1,2-Dichloroethene ug/L ND 5.0 10/27/15 02:310.49
REPORT OF LABORATORY ANALYSIS
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Page 26 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1591707
Associated Lab Samples:92272115001, 92272115002, 92272115003, 92272115004, 92272115005, 92272115006, 92272115007,
92272115008
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 10/27/15 02:310.26
trans-1,4-Dichloro-2-butene ug/L ND 100 10/27/15 02:311.0
Trichloroethene ug/L ND 1.0 10/27/15 02:310.47
Trichlorofluoromethane ug/L ND 1.0 10/27/15 02:310.20
Vinyl acetate ug/L ND 50.0 10/27/15 02:310.35
Vinyl chloride ug/L ND 1.0 10/27/15 02:310.62
Xylene (Total)ug/L ND 5.0 10/27/15 02:310.66
1,2-Dichloroethane-d4 (S)%107 70-130 10/27/15 02:31
4-Bromofluorobenzene (S)%100 70-130 10/27/15 02:31
Toluene-d8 (S)%102 70-130 10/27/15 02:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1591708LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.850 100 80-125
1,1,1-Trichloroethane ug/L 58.850 118 71-129
1,1,2,2-Tetrachloroethane ug/L 59.250 118 79-124
1,1,2-Trichloroethane ug/L 54.750 109 85-125
1,1-Dichloroethane ug/L 56.550 113 73-126
1,1-Dichloroethene ug/L 57.550 115 66-135
1,2,3-Trichloropropane ug/L 57.650 115 75-130
1,2-Dibromo-3-chloropropane ug/L 50.450 101 71-133
1,2-Dibromoethane (EDB)ug/L 57.550 115 83-124
1,2-Dichlorobenzene ug/L 54.750 109 80-133
1,2-Dichloroethane ug/L 52.350 105 67-128
1,2-Dichloropropane ug/L 53.850 108 75-132
1,4-Dichlorobenzene ug/L 54.850 110 78-130
2-Butanone (MEK)ug/L 123100 123 61-144
2-Hexanone ug/L 133100 133 68-143
4-Methyl-2-pentanone (MIBK)ug/L 122100 122 72-135
Acetone ug/L 128100 128 48-146
Acrylonitrile ug/L 306250 122 40-160
Benzene ug/L 55.750 111 80-125
Bromochloromethane ug/L 59.850 120 71-125
Bromodichloromethane ug/L 52.050 104 78-124
Bromoform ug/L 43.550 87 71-128
Bromomethane ug/L 51.650 103 40-160
Carbon disulfide ug/L 52.5J50 105 50-160
Carbon tetrachloride ug/L 49.550 99 69-131
Chlorobenzene ug/L 54.350 109 81-122
Chloroethane ug/L 53.950 108 39-148
Chloroform ug/L 58.450 117 73-127
Chloromethane ug/L 54.050 108 44-146
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1591708LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 54.150 108 74-124
cis-1,3-Dichloropropene ug/L 51.350 103 72-132
Dibromochloromethane ug/L 47.850 96 78-125
Dibromomethane ug/L 56.750 113 82-120
Ethylbenzene ug/L 56.050 112 79-121
Iodomethane ug/L 102100 102 39-154
Methylene Chloride ug/L 53.350 107 64-133
Styrene ug/L 59.050 118 84-126
Tetrachloroethene ug/L 53.350 107 78-122
Toluene ug/L 54.850 110 80-121
trans-1,2-Dichloroethene ug/L 54.650 109 71-127
trans-1,3-Dichloropropene ug/L 50.350 101 69-141
trans-1,4-Dichloro-2-butene ug/L 55.6J50 111 40-160
Trichloroethene ug/L 52.650 105 78-122
Trichlorofluoromethane ug/L 54.350 109 53-137
Vinyl acetate ug/L 121100 121 40-160
Vinyl chloride ug/L 58.450 117 58-137
Xylene (Total)ug/L 170150 113 81-126
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1591709MATRIX SPIKE SAMPLE:
MSSpike
Result
92272115007
1,1,1,2-Tetrachloroethane ug/L 21.020 105 70-130ND
1,1,1-Trichloroethane ug/L 25.120 125 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.420 112 70-130ND
1,1,2-Trichloroethane ug/L 21.620 108 70-130ND
1,1-Dichloroethane ug/L 24.020 120 70-130ND
1,1-Dichloroethene ug/L 25.420 127 70-166ND
1,2,3-Trichloropropane ug/L 22.120 110 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.320 102 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.420 112 70-130ND
1,2-Dichlorobenzene ug/L 22.520 112 70-130ND
1,2-Dichloroethane ug/L 21.420 106 70-130ND
1,2-Dichloropropane ug/L 21.720 108 70-130ND
1,4-Dichlorobenzene ug/L 22.420 112 70-130ND
2-Butanone (MEK)ug/L 48.0J40 120 70-130ND
2-Hexanone ug/L 50.240 125 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 46.3J40 116 70-130ND
Acetone ug/L 62.4J M14015670-130ND
Acrylonitrile ug/L 116J100 116 70-130ND
Benzene ug/L 24.420 120 70-1480.45J
Bromochloromethane ug/L 24.120 120 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 28 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1591709MATRIX SPIKE SAMPLE:
MSSpike
Result
92272115007
Bromodichloromethane ug/L 21.620 108 70-130ND
Bromoform ug/L 18.320 91 70-130ND
Bromomethane ug/L 20.920 104 70-130ND
Carbon disulfide ug/L 24.1J20 120 70-130ND
Carbon tetrachloride ug/L 22.120 111 70-130ND
Chlorobenzene ug/L 22.720 114 70-146ND
Chloroethane ug/L 23.920 120 70-130ND
Chloroform ug/L 24.520 122 70-130ND
Chloromethane ug/L 24.220 121 70-130ND
cis-1,2-Dichloroethene ug/L 23.220 116 70-130ND
cis-1,3-Dichloropropene ug/L 16.920 84 70-130ND
Dibromochloromethane ug/L 19.820 99 70-130ND
Dibromomethane ug/L 22.720 114 70-130ND
Ethylbenzene ug/L 23.520 117 70-130ND
Iodomethane ug/L 42.240 105 70-130ND
Methylene Chloride ug/L 22.120 108 70-130ND
Styrene ug/L 22.820 114 70-130ND
Tetrachloroethene ug/L 22.620 113 70-130ND
Toluene ug/L 23.320 116 70-155ND
trans-1,2-Dichloroethene ug/L 23.320 116 70-130ND
trans-1,3-Dichloropropene ug/L 16.720 83 70-130ND
trans-1,4-Dichloro-2-butene ug/L 16.6J20 83 70-130ND
Trichloroethene ug/L 22.520 112 69-151ND
Trichlorofluoromethane ug/L 23.820 119 70-130ND
Vinyl acetate ug/L 11.6J M1402970-130ND
Vinyl chloride ug/L 25.820 129 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92272492003
1591710SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 29 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92272492003
1591710SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%111 0111
4-Bromofluorobenzene (S)%99 0100
Toluene-d8 (S)%101 1102
REPORT OF LABORATORY ANALYSIS
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Page 30 of 34
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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Page 31 of 34
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92272115
OMNISOURCE/KERNERSVILLE LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92272115001 MPRP/19828 ICP/178823420-FIELD BLANK EPA 3010 EPA 6010
92272115002 MPRP/19840 ICP/178913420-MW12 EPA 3010 EPA 6010
92272115003 MPRP/19840 ICP/178913420-MW13 EPA 3010 EPA 6010
92272115004 MPRP/19840 ICP/178913420-MW14 EPA 3010 EPA 6010
92272115005 MPRP/19840 ICP/178913420-MW1R EPA 3010 EPA 6010
92272115006 MPRP/19840 ICP/178913420-SW1 EPA 3010 EPA 6010
92272115007 MPRP/19840 ICP/178913420-SW2 EPA 3010 EPA 6010
92272115001 MSV/339963420-FIELD BLANK EPA 8260
92272115002 MSV/339963420-MW12 EPA 8260
92272115003 MSV/339963420-MW13 EPA 8260
92272115004 MSV/339963420-MW14 EPA 8260
92272115005 MSV/339963420-MW1R EPA 8260
92272115006 MSV/339963420-SW1 EPA 8260
92272115007 MSV/339963420-SW2 EPA 8260
92272115008 MSV/339963420-TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 32 of 34
Page 33 of 34
Page 34 of 34
#=CL#
November 19, 2015
LIMS USE: FR - ALEX EVERHART
LIMS OBJECT ID: 92275941
92275941
Project:
Pace Project No.:
RE:
Mr. Alex Everhart
Joyce Engineering-NC
2211 W. Meadowview Road
Suite 101
Greensboro, NC 27407
OMNISOURCE/KERNERSVILLE LF
Dear Mr. Everhart:
Enclosed are the analytical results for sample(s) received by the laboratory on November 12, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
cc:Mr. Van Burbach, Joyce Engineering-NC
Alex Everhart, Joyce Engineering-NC
REPORT OF LABORATORY ANALYSIS
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Page 1 of 12
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92275941
OMNISOURCE/KERNERSVILLE LF
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 12
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92275941
OMNISOURCE/KERNERSVILLE LF
Lab ID Sample ID Matrix Date Collected Date Received
92275941001 3420-MW1R Water 11/11/15 15:50 11/12/15 11:17
92275941002 3420-TRIP BLANK Water 11/11/15 13:00 11/12/15 11:17
REPORT OF LABORATORY ANALYSIS
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Page 3 of 12
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275941
OMNISOURCE/KERNERSVILLE LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92275941001 3420-MW1R EPA 8260 4 PASI-CNB
92275941002 3420-TRIP BLANK EPA 8260 4 PASI-CNB
REPORT OF LABORATORY ANALYSIS
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92275941
OMNISOURCE/KERNERSVILLE LF
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92275941001 3420-MW1R
Benzene 1.0 ug/L 11/13/15 06:391.0EPA 8260
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275941
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW1R Lab ID:92275941001 Collected:11/11/15 15:50 Received:11/12/15 11:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene 1.0 ug/L 11/13/15 06:39 71-43-21.0 0.25 1
Surrogates
4-Bromofluorobenzene (S)102 %11/13/15 06:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)122 %11/13/15 06:39 17060-07-070-130 1
Toluene-d8 (S)105 %11/13/15 06:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 12
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275941
OMNISOURCE/KERNERSVILLE LF
Sample:3420-TRIP BLANK Lab ID:92275941002 Collected:11/11/15 13:00 Received:11/12/15 11:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 11/13/15 06:56 71-43-21.0 0.25 1
Surrogates
4-Bromofluorobenzene (S)103 %11/13/15 06:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)127 %11/13/15 06:56 17060-07-070-130 1
Toluene-d8 (S)105 %11/13/15 06:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 7 of 12
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275941
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34262
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92275941001, 92275941002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1605472
Associated Lab Samples:92275941001, 92275941002
Matrix:Water
AnalyzedMDL
Benzene ug/L ND 1.0 11/13/15 01:090.25
1,2-Dichloroethane-d4 (S)%118 70-130 11/13/15 01:09
4-Bromofluorobenzene (S)%102 70-130 11/13/15 01:09
Toluene-d8 (S)%104 70-130 11/13/15 01:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1605473LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/L 51.950 104 80-125
1,2-Dichloroethane-d4 (S)%112 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%103 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1605474MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275823005
1605475
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene ug/L 20 115 70-148113 2 3020ND23.1 22.7
1,2-Dichloroethane-d4 (S)%114 70-130115
4-Bromofluorobenzene (S)%102 70-130101
Toluene-d8 (S)%102 70-130102
REPORT OF LABORATORY ANALYSIS
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Page 8 of 12
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92275941
OMNISOURCE/KERNERSVILLE LF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 10:59 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 12
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275941
OMNISOURCE/KERNERSVILLE LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275941001 MSV/342623420-MW1R EPA 8260
92275941002 MSV/342623420-TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 10:59 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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