IH1473_20230811_Limited GW Mon Report - June 2023 Trial Event

Mount Pleasant, South Carolina 29464
843-884-0029 | 843-856-0107
www.ensafe.com

creative thinking. custom solutions. ®
LIMITED GROUNDWATER MONITORING REPORT
JUNE 2023 TRIAL RUN EVENT

PACTIV EVERGREEN
CANTON MILL
CANTON, NORTH CAROLINA

EnSafe Project Number
0888834351

Prepared for:

Pactiv Evergreen
175 Main Street
Canton, North Carolina 28716

August 11, 2023

Mount Pleasant, South Carolina 29464
843-884-0029 | 843-856-0107
www.ensafe.com

creative thinking. custom solutions. ®
LIMITED GROUNDWATER MONITORING REPORT
JUNE 2023 TRIAL RUN EVENT

PACTIV EVERGREEN
CANTON MILL
CANTON, NORTH CAROLINA

EnSafe Project Number
0888834351

Prepared for:

Pactiv Evergreen
175 Main Street
Canton, North Carolina 28716

August 11, 2023

Prepared by: Reviewed by:

Travis Darden, PG, Project Manager Bridget Morello, PE, Principal

i
TABLE OF CONTENTS
LIST OF ACRONYMS ................................................................................................................. ii

1.0 INTRODUCTION ......................................................................................................... 1-1 1.1 Objectives ....................................................................................................... 1-1
1.2 Organization ................................................................................................... 1-1

2.0 BACKGROUND............................................................................................................ 2-1 2.1 Site History ..................................................................................................... 2-1
2.2 Previous Investigations .................................................................................... 2-1

3.0 LIMITED GROUNDWATER MONITORING ACTIVITIES — JUNE 2023 ............................... 3-1
3.1 Well Inspection and Purging ............................................................................. 3-1
3.2 Groundwater Sampling and Analysis .................................................................. 3-2
3.3 Analytical Results ............................................................................................. 3-9 3.4 Investigation Derived Waste ........................................................................... 3-10

4.0 CONCLUSIONS AND RECOMMENDATIONS.................................................................... 4-1

5.0 REFERENCES ............................................................................................................. 5-1

FIGURES

Figure 1 Site Location Map
Figure 2 Existing Well Network Map

TABLES
Table 3-1 Groundwater Sample Locations ......................................................................... 3-1
Table 3-2 Limited Well Inventory ..................................................................................... 3-2
Table 3-3 Groundwater Analytes and Screening Levels ...................................................... 3-2 Table 3-4 Analytical Summary Table .............................................................................. 3-10

APPENDICES
Appendix A Groundwater Field Sampling Forms
Appendix B Data Validation and Laboratory Analytical Reports

ii
LIST OF ACRONYMS
µg/L micrograms per liter
µS/cm = microsiemens per centimeter
bgs Below ground surface

CAS No. Chemical Abstracts Service number
CSA Comprehensive Site Assessment

DWR Division of Water Resources
ft feet

IP International Paper

mg/L milligrams per liter
mV millivolts

N/A Not applicable NC GW North Carolina 15A NCAC 02L .0202 Groundwater Standards (April 2022) NCDEQ North Carolina Department of Environmental Quality NOV Notice of Violation
NS not specified
NTU Nephelometric Turbidity Unit

pg/L picogram per liter
ppm parts per million

PTVE Pactiv Evergreen

QA/QC Quality and Assurance and Quality Control

SVOCs semi-volatile organic compound
TBD To be determined

U.S. EPA United States Environmental Protection Agency

Unk Unknown
VOCs volatile organic compound

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Pactiv Evergreen Canton Mill
Canton, North Carolina
August 2023

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1.0 INTRODUCTION
Due to its composition, black liquor has proven to be a difficult matrix for characterizing contaminants
of potential concern by conventional analytical methods. As such, EnSafe Inc., on behalf of
Pactiv Evergreen (PTVE), conducted a limited groundwater sampling event as a “trial run” at the
former Canton Mill facility in Canton, North Carolina (Site) in advance of a Site-wide sampling event
to ensure the proposed analytical methods are viable to meet the objectives of the Interim Work Plan
Addendum (EnSafe, June 2023).

1.1 Objectives
The objectives of the trial run were two-fold: 1) determine a laboratory analytical method capable
of achieving lower detection limits for contaminants of potential concern than methods used by other
consultants’ efforts for this Site, and 2) determine the monitoring well network integrity/ability to
produce representative samples of the aquifers of concern.

During the limited sampling event two of the more impacted wells (RW-5 and PZ-4) and
one background well (PZ-21) were sampled. The preliminary data set for RW-5, PZ-4, and PZ-21 will
allow for amendments and optimization of groundwater sampling protocols related to the upcoming
Site-wide event.

Activities described herein were performed in accordance with the Site Sampling and Analyses Plan
and Quality Assurance Project Plan. All work was performed in consultation with the
United States Environmental Protection Agency (U.S. EPA), the North Carolina Department of
Environmental Quality (NCDEQ) Division of Waste Management’s Superfund Section, Inactive
Hazardous Sites Branch guidance, and in general accordance with the U.S. EPA Region 4, Science
and Ecosystem Support Division Field Branches Quality System and Technical Procedures, available
at https://www.epa.gov/quality/quality-system-and-technical-procedures-lsasd-field-branches.

1.2 Organization
This report is organized into the following sections:

Section 1 — Introduction
Section 2 — Site Background
Section 3 — June 2023 Groundwater Monitoring Activities
Section 4 — Conclusions and Recommendations
Section 5 — References
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Canton, North Carolina
August 2023

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2.0 BACKGROUND
The Canton Mill has been producing paper at its current location via the kraft method since 1908.
The mill campus is bisected by the Pigeon River and surrounded by the town of Canton, North Carolina
as depicted in Figure 1, all figures are located behind the Figures tab. The mill was shut down in
June 2023, and decommissioning is ongoing.

2.1 Site History
A seep of black liquor into the Pigeon River was reported to the North Carolina Department of
Environment and Natural Resources (NCDENR), now NCDEQ, in 1994 by Champion Paper (who
owned the Mill at that time). A series of subsequent Comprehensive Site Assessments were
conducted by Champion Paper to assess impacts to groundwater and included the installation of the
existing monitoring and recovery well network (Figure 1). Initial efforts to contain black liquor and
mitigate the seep included a pump and treat system that proved to be ineffective for several plausible
reasons. In 1999, Champion, who retained liability for the black liquor release, sold the mill to
Carolina Paper which later became Blue Ridge Paper Products. Champion Paper was acquired by
International Paper (IP) in 2000. From 2007 to present, IP conducted semi-annual groundwater
monitoring events targeting a limited analyte suite (AECOM various dates). In 2007,
Evergreen Packaging (now a wholly-owned subsidiary of PTVE) purchased the Canton Mill from
Blue Ridge Paper Products and has operated the mill since. At the request of the U.S. EPA and the
NCDEQ, PTVE has chosen to move forward with the assessment of potential impacts to groundwater
associated with historic releases of black liquor at the Site without the assistance of other potentially
responsible parties.

An apparent re-activation of the black liquor seep was reported to NCDEQ on January 28, 2022.
On April 11, 2022, NCDEQ Division of Water Resources (DWR) issued a Notice of Violation (NOV) to
IP, requiring IP to sample surface waters and sediments of the Pigeon River proximal to the
black liquor seep as well as to provide a summary of historical efforts to treat or contain impacted
groundwater. The Inactive Hazardous Sites Branch of NCDEQ followed up with the issuance of a
Notice of Regulatory Requirements to IP on April 22, 2022, mandating a similar suite of assessment
actions. NCDEQ DWR subsequently issued an NOV to PTVE on October 20, 2022, which mirrored the
requirements of the NOV sent to IP in April 2022.

2.2 Previous Investigations
Based on a review of publicly available information, while focused semiannual sampling events have
been performed by AECOM on behalf of IP, the most recent comprehensive site-wide groundwater
Limited Groundwater Monitoring Report June 2023 Trial Run Event
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Canton, North Carolina
August 2023

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sampling event was conducted in 1997 by Roy F. Weston Inc. as part of a Phase III Site Assessment
on behalf of Champion Paper. A Site-wide Groundwater Sampling Work Plan will be provided under
separate cover for review/approval by U.S. EPA and NCDEQ, and that sampling event is anticipated
for September 2023 following associated well network inspection and redevelopment/rehabilitation
work, as needed.

Limited Groundwater Monitoring Report June 2023 Trial Run Event
Pactiv Evergreen Canton Mill
Canton, North Carolina
August 2023

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3.0 LIMITED GROUNDWATER MONITORING ACTIVITIES — JUNE 2023
The limited groundwater monitoring activities completed at the Site in June 2023 as part of the
“trial run” are outlined below. Per paragraph three, Section 2.0 of the Interim Work Plan Addendum
(EnSafe, June 2023), groundwater sampling was performed at two of the more impacted wells (RW-5
and PZ-4) and one background well (PZ-21). Sample locations and rationale for this “trial run” event
are summarized in Table 3-1. The complete analyte list is displayed in Table 3-2. Figure 2 depicts
the select wells included in this “trial run” event.

Table 3-1
PZ-21 PZ21WG-MMDDYY UNK
PZ-04 PZ04WG-MMDDYY 9-24
RW-05 RW05WG-MMDDYY 9-49
QA/QC TBD TBD
QA/QC TBD TBD
QA/QC EB-MMDDYY N/A
ID = Identification
ft = feet
bgs = below ground surface MMDDYY = Month, day, and year, ex. February 3, 2023 will be identified as 020323 N/A = not applicable UNK = Unknown
TBD = To be determined
QA/QC = Quality assurance/quality control
EB = Equipment blank
3.1 Well Inspection and Purging
The objective of any groundwater monitoring event is to collect a sample that is representative of
the current aquifer conditions. Although semi-annual monitoring events have been conducted at the
Site by other contractors on behalf of IP since February 2007, the existing well network dates to the
mid-1990s and many wells have historically been prone to scaling (CSAIII Weston 1997). Therefore,
prior to groundwater sampling efforts, the three select wells were inventoried by EnSafe field
personnel for any visual or inferred deficiencies. Table 3-2 summarizes monitoring well deficiencies
(implied or) observed by the sampling team, notes any implications to the validity of the data
collected, and offers resolutions.
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Canton, North Carolina
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Table 3-2 Limited Well Inventory
Location Deficiencies Likely Cause Implication/Resolution
PZ-04
recharge
Measured well depth less than
published depth.

Fine sediment intrusion

locale if purged dry — low flow sample after 24-hour
equilibration/recharge period. Hydrogeologic data collected from well may not be indicative of aquifer conditions.

Well should be redeveloped and rehabilitated to ensure
RW-05
recharge

Measured well
depth less than
published depth.

Fine sediment
intrusion

locale if purged dry — low flow sample after 24-hour equilibration/recharge period.

Hydrogeologic data collected from well may not be
indicative of aquifer conditions.
Well should be redeveloped and rehabilitated to ensure

NA = Not applicable

3.2 Groundwater Sampling and Analysis
From June 22 through June 23, 2023, EnSafe personnel collected groundwater samples from the
select monitoring wells listed in Table 3-1. Pursuant to Table 3-2, impacted wells PZ-04 and RW-05
were purged dry on June 22, 2023, allowed to recharge overnight, and sampled on June 23, 2023.
All groundwater samples were collected utilizing low flow techniques as described in the initial
Sampling and Analyses Plan and Quality Assurance Project Plan. The samples were shipped under a
strict chain of custody to Pace Analytical Laboratories, LLC, a NCDEQ-certified laboratory, and were
analyzed for the constituents listed in Table 3-3. Groundwater sampling logs are included in
Appendix A.

Table 3-3 Groundwater Analytes and Screening Levels
Analyte CAS No. NC GW
Laboratory Method Detection
Method Quantitation (Reporting)
1,1,1-Trichloroethane 71-55-6 200 0.332 1 µg/L
1,1,2,2-Tetrachloroethane 79-34-5 0.2 0.225 1 µg/L
1,1,2-Trichloroethane 79-00-5 0.6 0.325 1 µg/L
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Canton, North Carolina
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Table 3-3
Groundwater Analytes and Screening Levels
Analyte CAS No. NC GW
Laboratory Method Detection
Method Quantitation (Reporting)
1,1-Dichloroethane 75-34-3 6 0.367 1 µg/L
1,1-Dichloroethene 75-35-4 350 0.367 1 µg/L
1,2,4-Trichlorobenzene 120-82-1 70 0.639 1 µg/L
1,2-Dibromo-3-chloropropane 96-12-8 0.04 0.34 2 µg/L
1,2-Dibromoethane 106-93-4 0.02 0.272 1 µg/L
1,2-Dichlorobenzene 95-50-1 20 0.339 1 µg/L
1,2-Dichloroethane 107-06-2 0.4 0.322 1 µg/L
1,2-Dichloropropane 78-87-5 0.6 0.355 1 µg/L
1,3-Dichlorobenzene 541-73-1 200 0.34 1 µg/L
1,4-Dichlorobenzene 106-46-7 6 0.333 1 µg/L
2-Butanone 78-93-3 4,000 3.96 5 µg/L
2-Hexanone 591-78-6 40 0.476 5 µg/L
4-Methyl-2-pentanone 108-10-1 100 2.71 5 µg/L
Benzene 71-43-2 1 0.345 1 µg/L
Bromomethane 74-83-9 10 1.66 2 µg/L
Chloroethane 75-00-3 3,000 0.649 1 µg/L
Chloromethane 74-87-3 3 0.649 1 µg/L
cis-1,2-Dichloroethene 156-59-2 70 0.384 1 µg/L
cis-1,3-Dichloropropene 10061-01-5 0.4 0.365 1 µg/L
Ethylbenzene 100-41-4 600 0.304 1 µg/L
m,p-Xylene 179601-23-1 500 0.709 2 µg/L
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Canton, North Carolina
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Table 3-3
Groundwater Analytes and Screening Levels
Analyte CAS No. NC GW
Laboratory Method Detection
Method Quantitation (Reporting)
Methylcyclohexane 108-87-2 NS 1.51 10 µg/L
Methylene chloride 75-09-2 5 1.95 5 µg/L
o-Xylene 95-47-6 500 0.338 1 µg/L
Toluene 108-88-3 600 0.239 1 µg/L
trans-1,2-Dichloroethene 156-60-5 100 0.396 1 µg/L
trans-1,3-Dichloropropene 10061-02-6 0.4 0.363 1 µg/L
Trichloroethene 79-01-6 3 0.383 1 µg/L
SVOCs by SW-846 Method 8270E
1,1-Biphenyl 92-52-4 400 1.82 10 µg/L
2,4,5-Trichlorophenol 95-95-4 63 1.42 10 µg/L
2,4,6-Trichlorophenol 88-06-2 4 1.55 10 µg/L
2,4-Dichlorophenol 120-83-2 0.98 1.7 10 µg/L
2,4-Dinitrophenol 51-28-5 NS 26 50 µg/L
2-Chlorophenol 95-57-8 0.4 1.2 10 µg/L
2-Methylnaphthalene 91-57-6 30 1.87 10 µg/L
2-Nitroaniline 88-74-4 NS 2.98 20 µg/L
3-Nitroaniline 99-09-2 NS 3.75 20 µg/L
4,6-Dinitro-2-methylphenol 497-56-3 NS 7.78 20 µg/L
4-Bromophenyl phenyl ether 101-55-3 NS 1.77 10 µg/L
4-Chloro-3-methylphenol 59-50-7 NS 3.34 10 µg/L
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Canton, North Carolina
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Table 3-3
Groundwater Analytes and Screening Levels
Analyte CAS No. NC GW
Laboratory Method Detection
Method Quantitation (Reporting)
4-Nitrophenol 100-02-7 NS 6.59 50 µg/L
Acetophenone 98-86-2 700 1.5 10 µg/L
Benzaldehyde 100-52-7 NS 3.6 10 µg/L
Benzo(a)pyrene 50-32-8 0.005 2.78 10 µg/L
Benzo(b)fluoranthene 205-99-2 0.05 2.6 10 µg/L
Benzo(g,h,i)perylene 191-24-2 200 2.84 10 µg/L
Caprolactam 105-60-2 4,000 6.94 10 µg/L
Dibenzofuran 132-64-9 NS 2.1 10 µg/L
Dimethyl phthalate 131-11-3 NS 2.13 10 µg/L
Isophorone 78-59-1 40 1.66 10 µg/L
N-Nitrosodi-n-propylamine 621-64-7 NS 1.33 10 µg/L
N-Nitrosodiphenylamine 86-30-6 NS 3 10 µg/L
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Canton, North Carolina
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Table 3-3
Groundwater Analytes and Screening Levels
Analyte CAS No. NC GW
Laboratory Method Detection
Method Quantitation (Reporting)
Naphthalene 91-20-3 6 2.09 10 µg/L
Pyrene 129-00-0 200 2.2 10 µg/L
Metals by SW-846 Method 6010D
Arsenic 7440-38-2 0.01 0.0034 0.015 mg/L

Chromium 7440-47-3 0.01 0.0017 0.005 mg/L
Manganese 7439-95-4 0.05 0.084 0.005 mg/L
Selenium 7782-49-2 0.02 0.0039 0.015 mg/L
Dissolved Metals (Field-Filtered) by SW-846 Method 6010D
Barium 7440-39-3 0.7 0.00084 0.01 mg/L
Cadmium 7440-43-9 0.002 0.00033 0.001 mg/L
Cobalt 7440-48-4 0.001 0.00096 0.01 mg/L
Nickel 7442-02-0 0.1 0.001 0.005 mg/L
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Canton, North Carolina
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Table 3-3
Groundwater Analytes and Screening Levels
Analyte CAS No. NC GW
Laboratory Method Detection
Method Quantitation (Reporting)
Selenium 7782-49-2 0.02 0.0039 0.015 mg/L
Silver 7440-22-4 0.02 0.001 0.005 mg/L
Mercury by SW-846 Method 7470A
Mercury 7439-97-6 0.001 0.000125 0.0002 mg/L
Mercury 7439-97-6 0.001 0.000125 0.0002 mg/L
Boron by U.S. EPA Method 200.7
Boron 7440-42-8 0.7 0.00975 0.04 mg/L
Dissolved Boron (Field-Filtered) by U.S. EPA Method 200.7
Boron 7440-42-8 0.7 0.00975 0.04 mg/L
Color by Standard Method 2120B
Color COLOR 15 25 25 Color
Alkalinity by Standard Method 2320B
Alkalinity, Total (As CaCO3) 471-34-1 NS 5 5 mg/L
Anions by SW-846 Method 9056
Chloride 16887-00-6 250 0.6 1 mg/L
Sulfate 14808-79-8 250 0.5 1 mg/L
Sulfide by Standard Method 4500S2-D
Field Measurements
Dissolved Oxygen NS NS NS NS mg/L
Oxidation-Reduction Potential NS NS NS NS mV
(1) NS 6.5-8.5 NS NS pH
Specific Conductance NS NS NS NS µS/cm
Turbidity NS NS NS NS NTU
Dissolved Oxygen NS NS NS NS mg/L
Dioxins/Furans by SW-846 8290A
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Canton, North Carolina
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Table 3-3
Groundwater Analytes and Screening Levels
Analyte CAS No. NC GW
Laboratory Method Detection
Method Quantitation (Reporting)
1,2,3,7,8-PeCDD 40321-76-4 NS 2.07 50 pg/L
1,2,3,4,7,8-HxCDF 70648-26-9 NS 4.99 50 pg/L
1,2,3,6,7,8-HxCDF 57117-44-9 NS 4.39 50 pg/L
1,2,3,6,7,8-HxCDD 57653-85-7 NS 4.49 50 pg/L
1,2,3,4,6,7,8-HpCDD 35822-46-9 NS 4.27 50 pg/L

(1) Due to the short holding time requirement for pH (15 minutes), pH will be measured in the field. CAS No. = Chemical Abstracts Service number NC GW = North Carolina 15A NCAC 02L .0202 Groundwater Standards (April 2022) VOCs = volatile organic compounds µg/L = micrograms per liter
NS = not specified SVOCs = semivolatile organic compounds mg/L = milligram per liter
mV = millivolts
ppm = parts per million
µS/cm = microsiemens per centimeter NTU = Nephelometric Turbidity Unit
pg/L = picogram per liter
U.S. EPA = United States Environmental Protection Agency

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Canton, North Carolina
August 2023

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3.3 Analytical Results
Pursuant to discussions with the stakeholders and in accordance with the Interim Work Plan
Addendum (EnSafe, June 2023), two of the more impacted wells (RW-5 and PZ-4) and one
background well (PZ-21) were sampled as part of a “trial run” in advance of a Site-wide sampling
event. As previously mentioned, the purpose of this limited groundwater sampling event is to ensure
the proposed analytical methods are viable to meet the investigative objectives. Samples from the
three select wells were analyzed for Color (by Standard Method 2120B), Alkalinity (by
Standard Method 2320B), Anions (by SW-846 Method 9056), Sulfide (by Standard Method
4500S2-D), Metals (total and dissolved by SW-846 Method 6010D), Boron (total and dissolved by
U.S. EPA Method 200.7), Mercury (total and dissolved by SW-846 Method 7470A), Volatile Organic
Compounds (by SW-846 Method 8260D), Semi-volatile Organic Compounds (by SW-846 Method
8270E), and Dioxins/Furans (by SW-846 8290A). Field measurements for Dissolved Oxygen,
Oxidation-Reduction Potential, pH, Specific Conductance, and Turbidity were also collected. A
summary of the analytical results is presented in Table 3-4. Field measurements were recorded on
the sampling logs in Appendix A. The data validation report and the analytical laboratory reports for
this limited sampling event are included in Appendix B.

3.3.1 Exceedances of North Caroline Groundwater Standards
Exceedances of North Carolina groundwater standards, organized by general analyte suites, are noted
below. The North Carolina 15A NCAC 02L .0202 Groundwater Standards (April 2022) are noted in
parentheses, followed by identification of the wells and results exceeding the respective standards.

Dissolved Metals
Arsenic (10 micrograms per Liter µg/L) — PZ-4 (37.4 µ/L), RW-5 (550 µ/L)
Boron (700 µg/L) — RW-5 (2980 µg/L)
Chromium (10 µg/L) — PZ-4 (43.1 µg/L), RW-5 (81.3 µg/L)
Lead (15 µg/L) — PZ-4 (20 µg/L), RW-5 (34.8 µg/L)
Nickel (100 µg/L) — PZ-4 (109 µg/L), RW-5 (138 µg/L)
Selenium (20 µg/L) — PZ-4 (22 µg/L)
Vanadium (7 µg/L) — PZ-4 (1400 µg/L), RW-5 (1300 µg/L)
Mercury (1 µg/L) — PZ-4 (12.7J µg/L)

Volatile Organic Compounds
Benzene (1 µg/L) RW-5 (1.5 J ug/L)

Semi-Volatile Organic Compounds
Naphthalene (6 µg/L) RW-5 (92.4 µg/L)
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Canton, North Carolina
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Table 3-4
Analytical Summary Table
Sample Location: Sample Sample Date:Sample Type:
PZ21 PZ21WG-062223 06/22/2023
Normal
PZ4WG-062323 06/23/2023
Normal
RW5WG-062323 06/23/2023
Normal
Method CAS No. Analyte NC GW Units Result Result Result
5000 2000
6.3 11.62 11.86
129 5450 25300
13 J 39.8
Arsenic 10 364 794
106 84.8 351
Boron 700 266 4310 Cadmium 2 16.1
Chromium 10 166 183
35.8
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Canton, North Carolina
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Table 3-4
Analytical Summary Table
Sample Location: Sample Sample Date:Sample Type:
PZ21 PZ21WG-062223 06/22/2023
Normal
PZ4WG-062323 06/23/2023
Normal
RW5WG-062323 06/23/2023
Normal
Method CAS No. Analyte NC GW Units Result Result Result
Lead 15 37.4 221
Nickel 100 207 404
Selenium 20 122
Vanadium 7 1900 1900
810
Arsenic (Dissolved) 10 37.4 550
114 69.1 179
Boron (Dissolved) 700 348 2980
1.1
Chromium (Dissolved) 10 43.1 81.3
Lead (Dissolved) 15 20 34.8
Nickel (Dissolved) 100 109 138
Selenium (Dissolved) 20 22
9 J
Vanadium (Dissolved) 7 1400 1300
Mercury 1 2.6 0.21
Mercury (Dissolved) 1 12.7 J 0.2 J
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Canton, North Carolina
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Table 3-4
Analytical Summary Table
Sample Location: Sample Sample Date:Sample Type:
PZ21 PZ21WG-062223 06/22/2023
Normal
PZ4WG-062323 06/23/2023
Normal
RW5WG-062323 06/23/2023
Normal
Method CAS No. Analyte NC GW Units Result Result Result
5.4 13.3
47.3 92.7
Benzene 1 0.41 J 1.5 J
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Canton, North Carolina
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Table 3-4
Analytical Summary Table
Sample Location: Sample Sample Date:Sample Type:
PZ21 PZ21WG-062223 06/22/2023
Normal
PZ4WG-062323 06/23/2023
Normal
RW5WG-062323 06/23/2023
Normal
Method CAS No. Analyte NC GW Units Result Result Result
1.7 2.1
6 3.8 J
2.8 1.8 J
1.1 3.4
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Canton, North Carolina
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Table 3-4
Analytical Summary Table
Sample Location: Sample Sample Date:Sample Type:
PZ21 PZ21WG-062223 06/22/2023
Normal
PZ4WG-062323 06/23/2023
Normal
RW5WG-062323 06/23/2023
Normal
Method CAS No. Analyte NC GW Units Result Result Result
2.3 J
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Canton, North Carolina
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Table 3-4
Analytical Summary Table
Sample Location: Sample Sample Date:Sample Type:
PZ21 PZ21WG-062223 06/22/2023
Normal
PZ4WG-062323 06/23/2023
Normal
RW5WG-062323 06/23/2023
Normal
Method CAS No. Analyte NC GW Units Result Result Result
Naphthalene 6 92.4
7.4 J
0.0000085
0.000012 0.0000098
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Canton, North Carolina
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Table 3-4
Analytical Summary Table
Sample Location: Sample Sample Date:Sample Type:
PZ21 PZ21WG-062223 06/22/2023
Normal
PZ4WG-062323 06/23/2023
Normal
RW5WG-062323 06/23/2023
Normal
Method CAS No. Analyte NC GW Units Result Result Result
0.0000087
0.000055
0.000005 0.0000043
0.000015 0.0000034
0.000045 0.0000055
0.00047
0.000033

Notes:
AECOM = Sample was collected by AECOM CAS No. = Chemical Abstracts Service number NC GW = North Carolina 2L Groundwater Standards (2020)
NE = Not established
NA = Not analyzed SU = Standard Units µg/L = micrograms per liter
mg/L = milligrams per liter
pH = Potential of Hydrogen Bold = Detected Value J = Estimated
UJ = Nondetect, estimated
U = Non detect, shown with method detection limit = Shaded/Bold = exceeds NC GW

Limited Groundwater Monitoring Report June 2023 Trial Run Event
Pactiv Evergreen Canton Mill
Canton, North Carolina
August 2023

3-17
3.4 Investigation Derived Waste
Classification/characterization activities were based on Site knowledge, field observations, and
archival analytical data. A determination was made by the stakeholders present during sampling that
disposal of purge water into the onsite WWTP was acceptable.

Limited Groundwater Monitoring Report June 2023 Trial Run Event
Pactiv Evergreen Canton Mill
Canton, North Carolina
August 2023

4-1
4.0 CONCLUSIONS AND RECOMMENDATIONS
Prior to this trial run event, data quality concerns were voiced by various stakeholders, specifically
regarding laboratory detection limits for certain compounds and the overall
integrity/representativeness of the existing well network.

Existing Well Network
As discussed in Section 3.1 above, the samples collected from the existing well network appear to be
indicative of current aquifer conditions so long as the wells are adequately purged. Prior to the
upcoming Site-wide groundwater monitoring effort, the monitoring well network will be inspected
and wells redeveloped/rehabilitated as needed. The well inspections and continued proper purging
techniques will ensure representative sample collection.

Laboratory Detection Limits
Laboratory detection limits for certain organic compounds remain above North Carolina groundwater
standards. However, the laboratory was able to achieve a 50% improvement in detection limits when
compared to results from other consultants’ laboratories. The data generated during this limited
groundwater sampling event was scrutinized by scientists from various disciplines and compared to
historical data sets collected by other environmental firms to assess validity. The consensus among
the technical working group is that the sampling techniques and analytical methods employed during
this limited sampling event have produced a data set representative of current aquifer conditions at
the Canton Mill. Given the complexity and sample matrix interferences posed by black liquor, the
detection limits achieved by Pace for this trial run are deemed acceptable, and these methods will be
incorporated in the upcoming Site-wide groundwater monitoring effort.

Comprehensive Site-Wide Groundwater Sampling Event
A Site-wide Groundwater Sampling Work Plan will be provided under separate cover for
review/approval by U.S. EPA and NCDEQ, and that sampling event is anticipated for September 2023
following associated well network inspection and redevelopment/rehabilitation work (both anticipated
for August/September 2023), as needed.
Limited Groundwater Monitoring Report June 2023 Trial Run Event
Pactiv Evergreen Canton Mill
Canton, North Carolina
August 2023

5-1
5.0 REFERENCES
AECOM/Earth Tech. Semi-Annual Groundwater Sampling Reports, Pactiv Evergreen Site.
Various Dates.
— Groundwater Sampling Plan, to North Carolina Department of Environment and
Natural Resources. 2006, November 28.

EnSafe Inc. Technical Memorandum Summary of Response Actions. Pactiv Evergreen Canton Mill,
Canton, North Carolina. March 2023.

— Initial Work Plan (i.e., Fuel Oil Investigation Work Plan). Pactiv Evergreen Canton Mill,
Canton, North Carolina. April 2023.

— Initial Quality Assurance Project Plan (i.e., Fuel Oil Investigation Quality Assurance
Project Plan). Pactiv Evergreen Canton Mill, Canton, North Carolina. April 2023.

— Initial Sampling and Analysis Plan (i.e., Fuel Oil Investigation Sampling and
Analysis Plan). Pactiv Evergreen Canton Mill, Canton, North Carolina. April 2023.

— Initial Health and Safety Plan (i.e., Fuel Oil Investigation Health and Safety Plan).
Pactiv Evergreen Canton Mill, Canton, North Carolina. April 2023.

— Position Paper — Assessment of Black Liquor Impacts to Groundwater.
Pactiv Evergreen Canton Mill, Canton, North Carolina. May 2023.

— Interim Work Plan Addendum — Comprehensive Sampling and Assessment of Black
Liquor Impacts to Groundwater. Pactiv Evergreen Canton Mill, Canton, North Carolina.
June 2023.

International Paper. North Carolina Department of Environment and Natural Resources Meeting
Agenda. 2003, February 20.

— Path forward on the corrective action at the Blue Ridge Paper Products, Inc. Site,
Canton Haywood County Letter from Mr. Thomas C. Richardson to Mr. Qu Qi,
North Carolina Department of Environment and Natural Resources. 2006, March 27.

Limited Groundwater Monitoring Report June 2023 Trial Run Event
Pactiv Evergreen Canton Mill
Canton, North Carolina
August 2023

5-2
— Voluntary Cleanup Checklist for Blue Ridge Paper Products, Inc. Site, Canton Haywood
County Letter from Mr. Thomas C. Richardson to Mr. Collin Day, North Carolina
Department of Environment and Natural Resources. 2007, October 31.

— Response to Notice of Regulatory Requirements - Blue Ridge Paper Products, Inc. Site,
Canton Haywood County, Groundwater Incident #12680 Letter from Mr. Thomas C.
Richardson to Mr. Kim Caulk, North Carolina Department of Environment and
Natural Resources. 2008, May 23.

North Carolina Department of Environmental Quality (formerly Department of Environment and
Natural Resources) Asheville Regional Office to IP Groundwater Sampling Plan — Approval.
2006, December 21.

— North Carolina Department of Environmental Quality IHSB Letter to International
Paper RE; Requirements for Containment Assessment and Cleanup (Agency
Restructuring & Voluntary Cleanup/REC Program). 2007, September 21.

— Notice of Regulatory Requirements to International Paper. 2008, March 17.

— Notice of Regulatory Requirements to International Paper. 2022, April 22.

— Notice of Violation to Pactiv Evergreen. 2022, October 20.

Roy. F. Weston, Inc. Groundwater Assessment at the Canton Pulp and Paper Mill.
1994, December 15.
— Comprehensive Site Assessment Report Canton Pulp and Paper Mill, Canton
North Carolina. 1995, June 1.

— Comprehensive Site Assessment Addendum Report Canton Pulp and Paper Mill,
Canton North Carolina. 1996, January 18.

— Comprehensive Site Assessment Phase III Report Canton Pulp and Paper Mill,
Canton North Carolina. 1997, July 10.

Limited Groundwater Monitoring Report June 2023 Trial Run Event
Pactiv Evergreen Canton Mill
Canton, North Carolina
August 2023

5-3
United States Environmental Protection Agency. Quality System and Technical Procedures for
LSASD Field Branches. https://www.epa.gov/quality/quality-system-and-technical-
procedures-lsasd-field-branches. Last Update 2022, February 7.

Figures
X:\EvergreenPackaging\SiteLocMap.mxd
FIGURE 1
SITE LOCATION MAP
PACTIV EVERGREEN CANTON MILLCANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:LEGEND
APPROXIMATE SUBJECT PROPERTY BOUNDARY
Source: U.S. Geological Survey. Canton Quadrangle, North Carolina[Map]. Photorevised 2022. 1:24,000. 7.5 Minute Series.
TD
MS
3/31/2023
Z000000005
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RW-3 PZ-3
PZ-13
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FIGURE 2
EXISTING WELL NETWORK MAPPACTIV EVERGREEN CANTON MILL CANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:LEGEND
&>WELL LOCATION
Source: Google Earth Pro Imagery - 04/2022
TD
RK4/28/2023
0888834351
0 100 200
SCALE IN FEET
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NAD 1983 STATE PLANENORTH CAROLINA FEET
800.588.7962 www.ensafe.com
Creative thinking.Custom solutions.

Appendix A
Field Sampling Forms

DATE: EQUIPMENT (Make/Model #/Serial #):
EVENT:
WELL ID: LOCATION:
WEATHER CONDITIONS: AMBIENT TEMP:
REVIEWED BY: PERSONNEL:
WELL DIAMETER (in): 4 0.652 gal/ft
SCREEN LENGTH (ft): 30 START: FINISH:
TOTAL DEPTH from TOC (ft.): 40.29 VOLUME PURGED (gal):
DEPTH TO WATER from TOC (ft.): 8.71
LENGTH OF WATER COL. (ft.):31.55 START: FINISH:
1 VOLUME OF WATER (gal):20.50 Total Vol Purged (gal):
3 VOLUMES OF WATER (gal):61.50
Temperature: 1.0 ° C Temperature: ± 0.5 °C
pH:± 0.5 standard units pH: ± 0.5 standard units
Specific Conductance:± 10%Specific Conductance: ± 10% of the past 3 measurement
Turbidity: relatively stable DO:±0.3 mg/L saturation
ORP: ± 10.0 millivolts
Turbidity:≤10 NTUs
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:
Time (hh:mm):9:45 9:50 9:55 10:00 10:05
Temperature (Co):18.96 18.90 18.94 19.00 19.05
Spec Cond (mS/cm):31.790 30.980 30.460 30.210 29.620
pH (units):11.91 11.90 11.88 11.86 11.86
ORP (mV):-456.6 -473.8 -476.9 -481.3 -485.2
Turbidity (NTU):112.00 102.00 101.30 98.80 92.80
DO % Sat: YSI 556 11.4% 5.2% 4.5% 3.3% 2.9%
DO (mg/L): YSI 556 0.91 0.42 0.33 0.27 0.24
Depth to Water (ft):9.23 9.45 9.73 9.92 10.07
Volume Purged (gal):0.25 0.25 0.25 0.25 0.25
Cumulative Vol (gal):0.25 0.50 0.75 1.00 1.25 1.25 1.25 1.25 1.25 1.25 1.25 1.25
Purge Rate (gpm)0.00 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
Well Goes Dry While Purging
SAMPLE DATA Bailer Pump Description:
Purging/Sampling Device Decon Process:
COMMENTS:
Peri Pump, soda straw for VOC's
6-22-23 Well Purge - purged dry with "tornado" pump, 20.1 gal removed, will return on 6-23-23 to sample
Low flow Peri pump 6-23-23 Purged ~ 1.25 gal dark amber to black color
RW05WG-062323 6/23/2023 10:10 13 y
Sample ID Date Time Bottles Filtered Remarks(mm/dd/yyyy) (hh:mm) (total to lab)(0.45 m)
WELL DEVELOPMENT PARAMETERS GROUNDWATER SAMPLING PARAMETERS
of the past measurement
IN-SITU TESTING
GROUNDWATER SAMPLING
9:40 8:55
1.25
ANALYSIS:
ML/EP
WELL DEVELOPMENT
RW-05 Canton NC Geotech # 23054658
Cloudy 65
WELL DEVELOPMENT & GROUNDWATER SAMPLING FORM
6/23/2023
PROJECT: Pactiv Evergreen YSI 556 MPS #8303592
JOB NUMBER: 0888834351.03.03.003
GW Sampling
DATE: JOB NUMBER: EQUIPMENT (Make/Model #/Serial #):
EVENT:
WELL ID: LOCATION:
WEATHER CONDITIONS: AMBIENT TEMP:
REVIEWED BY: PERSONNEL:
WELL DIAMETER (in): 2 0.163 gal/ft
SCREEN LENGTH (ft): START: FINISH:
TOTAL DEPTH from TOC (ft.): 23.90 VOLUME PURGED (gal):
DEPTH TO WATER from TOC (ft.): 5.06
LENGTH OF WATER COL. (ft.):18.84 START: FINISH:
1 VOLUME OF WATER (gal):3.07 Total Vol Purged (gal):
3 VOLUMES OF WATER (gal):9.21
Temperature: 1.0 ° C Temperature: ± 0.5 °C
pH:± 0.5 standard units pH: ± 0.5 standard units
Specific Conductance:± 10%Specific Conductance: ± 10% of the past 3 measurement
Turbidity: relatively stable DO:±0.3 mg/L saturation
ORP: ± 10.0 millivolts
Turbidity:≤10 NTUs
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:
Time (hh:mm):8:05 8:10
Temperature (Co):20.46 20.48
Spec Cond (mS/cm):32.480 31.360
pH (units):11.60 11.62
ORP (mV):-427.9 -462.4
Turbidity (NTU):0.02 0.02
DO % Sat: YSI 556 2.2% 1.9%
DO (mg/L): YSI 556 0.17 0.15
Depth to Water (ft):5.96 7.65
Volume Purged (gal):0.25 0.50
Cumulative Vol (gal):0.00 0.00 0.00 0.00 0.00 0.00 0.00
Purge Rate (gpm)#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
Well Goes Dry While Purging
SAMPLE DATA Bailer Pump Description:
Purging/Sampling Device Decon Process:
COMMENTS:
Peri Pump, soda straw for VOC's
6-22-23 Well Purge started and drawdown occured, decided to purge dry, 3.5 gal removed, will return on 6-23-23 to sample
6-23-23 Purged ~ 0.5 gal dark amber to black color
PZ04WG-062323 6/23/2023 8:15 13 y
DUP01WG-062323 6/23/2023 8:15 13 y
Sample ID Date Time Bottles Filtered Remarks(mm/dd/yyyy) (hh:mm) (total to lab)(0.45 m)
WELL DEVELOPMENT PARAMETERS GROUNDWATER SAMPLING PARAMETERS
of the past measurement
IN-SITU TESTING
GROUNDWATER SAMPLING
8:00 8:55
0.00
ANALYSIS:
ML/EP
WELL DEVELOPMENT
PZ-04 Canton NC Geotech # 23054658
Cloudy 65
WELL DEVELOPMENT & GROUNDWATER SAMPLING FORM
6/23/2023 0888834351.03.03.003
PROJECT: PTVE Canton GW Sampling YSI 556 MPS #8303592
DATE: JOB NUMBER: EQUIPMENT (Make/Model #/Serial #):
EVENT:
WELL ID: LOCATION:
WEATHER CONDITIONS: AMBIENT TEMP:
REVIEWED BY: PERSONNEL:
WELL DIAMETER (in): 2 0.163 gal/ft
SCREEN LENGTH (ft): START: FINISH:
TOTAL DEPTH from TOC (ft.): 14.80 VOLUME PURGED (gal):
DEPTH TO WATER from TOC (ft.): 4.49
LENGTH OF WATER COL. (ft.): START: FINISH:
1 VOLUME OF WATER (gal): Total Vol Purged (gal):
3 VOLUMES OF WATER (gal):0.00
Temperature: 1.0 ° C Temperature: ± 0.5 °C
pH:± 0.5 standard units pH: ± 0.5 standard units
Specific Conductance:± 10%Specific Conductance: ± 10% of the past 3 measurement
Turbidity: relatively stable DO:±0.3 mg/L saturation
ORP: ± 10.0 millivolts
Turbidity:≤10 NTUs
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:
Time (hh:mm):14:00 14:05 14:10 14:15 14:20
Temperature (Co):17.85 17.83 17.56 17.40 17.42
Spec Cond (mS/cm):0.779 0.770 0.741 0.757 0.763
pH (units):6.04 6.08 6.09 6.10 6.11
ORP (mV):234.8 233.1 231.3 232.2 230.6
Turbidity (NTU):8.75 10.80 7.00 6.50 6.84
DO % Sat: YSI 556 8.7% 9.5% 8.2% 7.9% 8.7%
DO (mg/L): YSI 556 0.81 0.90 0.84 0.76 0.84
Depth to Water (ft):5.41 5.68 5.74 5.81 5.93
Volume Purged (gal):0.00 0.50 0.50 0.50 0.50
Cumulative Vol (gal):0.00 0.50 1.00 1.50 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00
Purge Rate (gpm)0.10 0.10 0.10 0.10 0.00 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
Well Goes Dry While Purging
SAMPLE DATA Bailer Pump Description:
Purging/Sampling Device Decon Process:
COMMENTS:
ML/EP
PROJECT:
Cloudy
Geotech # 23054658Canton NC
Date
WELL DEVELOPMENT
GROUNDWATER SAMPLING
WELL DEVELOPMENT PARAMETERS GROUNDWATER SAMPLING PARAMETERS
14:25
IN-SITU TESTING
ANALYSIS:
of the past measurement
WELL DEVELOPMENT & GROUNDWATER SAMPLING FORM
Remarks(total to lab)(0.45 m)
Time Bottles Filtered
(hh:mm)Sample ID (mm/dd/yyyy)
6/22/2023
PZ-21
0888834351.03.03.003
GW Sampling
65
6/22/2023
6/22/2023
YSI 556 MPS #8303592
13:55
2.00

Appendix B
Data Validation and Analytical Report
Data Validation Summary Report Pactiv Evergreen
Canton, North Carolina
Sampling Event: June 2023

1
VALIDATION SUMMARY
This report summarizes data validation findings for the June 2023 sampling event at the
Pactiv Evergreen Canton Mill in Canton, North Carolina. Data were evaluated independently from the
laboratory to assess data quality. Samples discussed in this report were collected on June 22 and
23, 2023. Samples were received by Pace Analytical Services, LLC in Huntersville, North Carolina.
The samples were shipped to Pace Analytical Services laboratories located in Ashville, North Carolina,
Charlotte, North Carolina, Eden, North Carolina, West Columbia, South Carolina, and Minneapolis,
Minnesota. EnSafe Inc. validated the analytical data discussed in this report.

The quality assurance criteria used to assess all data were established by the analytical methods and
relevant standards in the following guidance documents:

• National Functional Guidelines for Organic Superfund Methods Data Review,
EPA-540-R-20-005 (United States Environmental Protection Agency [U.S. EPA],
November 2020)

• National Functional Guidelines for Inorganic Superfund Methods Data Review,
EPA-542-R-20-006 (U.S. EPA, November 2020)

U.S. EPA Stage 2A electronic and manual data validation, consisting of analytical results review and
quality control summaries, were performed on samples from sample delivery groups 92674166,
10659324, 92674238, 10661874, and YF23032. Table A-1 in Attachment A provides a summary of
all samples collected.

The analytes were validated for the following parameters, as applicable to the method:

* Data completeness
* Sample receipt and preservation
* Holding times
Laboratory control sample
Surrogates
Matrix spike/matrix spike duplicate
* Laboratory duplicates
Laboratory blanks
* Trip blank
Field duplicate

Data Validation Summary Report Pactiv Evergreen
Canton, North Carolina
Sampling Event: June 2023

2
When the quality control parameters did not fall within the specific method or data review guidelines,
the data reviewer qualified the corresponding compounds. Acceptable data parameters for which all
criteria were met, or no qualification was performed are indicated above with an asterisk (*).

Surrogates
Surrogates were within the acceptable percent recovery (%R) with the exceptions noted in Table 1
with the resulting qualification.

Table 1
Surrogate Percent Recovery Outliers
Method Sample ID Surrogate %R
Control
Limit
Associated
Analytes Qualifier RC
8270E DUP01WG-062323 2-Fluorophenol 5 10-130 All acid SVOCs UJ s

Notes:
%R = percent recovery RC = reason code
SVOCs = semivolatile organic compounds
UJ = Nondetected result was qualified as estimated.
s = surrogates percent recovery outlier

Laboratory Control Samples
Laboratory control samples were within the acceptable %R, with the exceptions noted in Table 2.

Table 2
Laboratory Control Sample Percent Recovery Outliers
Method Sample ID Analyte
LCS
%R
Control
Limit
Affected
Samples Qualifier RC
8270E LCS-4060995 4,6-Dinitro-2-methylphenol 24 39-158 PZ4WG-062323
DUP01WG-062323 UJ l 4-Nitrophenol 13 17-130
Notes:
LCS = laboratory control sample
%R = percent recovery
RC = reason code
UJ = Nondetected result was qualified as estimated.
l = laboratory control sample percent recovery outlier

Matrix Spike/Matrix Spike Duplicates
Matrix spike and matrix spike duplicates were within the acceptable %R, with the exceptions noted
in Table 3. All relative percent differences were within the acceptance criteria. When the native
sample was greater than four times the spike concentration, sample qualification was not necessary.
Data Validation Summary Report Pactiv Evergreen
Canton, North Carolina
Sampling Event: June 2023

3
Only the native sample, and if applicable the field duplicate, were qualified due to the outlier. Table
3 displays the qualified results.

Table 3
Matrix Spike/Matrix Spike Duplicate Percent Recovery Outliers
Method Sample ID Analyte
MS
%R
MSD
%R
Control
Limit Qualifier RC
8270E PZ21WG-062223
4-Nitrophenol 0 0 10-130 UJ m
4,6-Dinitro-2-methylphenol 6 8 10-187 UJ m
Pentachlorophenol 7 — 10-188 UJ m
Chrysene 42 — 43-159 UJ m
Dibenz(a,h)anthracene 39 — 40-171 UJ m
Pyrene 41 — 42-163 UJ m
2,4-Dinitrophenol 0 0 10-172 UJ m
Di-n-butylphthalate 41 — 42-160 UJ m
Di-n-octylphthalate 41 — 42-171 UJ m

Notes:
MS = matrix spike
%R = percent recovery
MSD = matrix spike duplicate RC = reason code
UJ = Nondetected result was qualified as estimated.
m = matrix spike/matrix spike duplicate percent recovery outlier
— = The analyte recovered within the acceptance criteria.

Although 4-nitrophenol and 2,4-nitrophenol recovered at 0%, the data were qualified as estimated
(UJ) due to these compounds being known poor-performers subjected to erratic chromatographic
behavior.

Laboratory Blanks
Laboratory blanks were free from contamination with the exceptions noted in Table 4 with the
resulting qualifications.

Data Validation Summary Report Pactiv Evergreen
Canton, North Carolina
Sampling Event: June 2023

4
Table 4
Laboratory Blank Outliers
SDG Method Blank ID Analyte
Blank Result (pg/L) Samples
qualified
Sample
Result
(pg/L)
Sample
RL
(pg/L) Qualifier RC
10661874 U.S. EPA
8290 BLANK-107396
1,2,3,7,8,9-
HxCDF 1.4 PZ4WG-062323
RW5WG-062323
9.8
5.5
100
99
U
U bl
1,2,3,4,7,8-
HxCDD 2.5 DUP01WG-062323 7.6 99 U bl
OCDD 6.6 PZ4WG-062323
DUP01WG-062323
140
120
200
200
U
U bl

Notes:
SDG = sample delivery group
pg/L = picograms per liter
RL = reporting limit
RC = reason code
U.S. EPA = United States Environmental Protection Agency
U = The result was qualified as not detected at the reporting limit.
bl = laboratory blank outlier

Field Duplicates
The relative percent difference of field duplicate samples were evaluated against an acceptance
criterion of 30% when both the results were greater than 5-times the reporting limit. Table 5 notes
the field duplicate results that required qualification.

Table 5
Field Duplicate Outliers
Method
Sample / Field
Duplicate ID Analyte
Sample
Result
Field
Duplicate
Result

Unit RPD Qualifier RC
7470A PZ4WG-062323 /
DUP01WG-062323
Dissolved mercury 12.7 4.4 µg/L 97 J fd
SM 4500-
S2D-2011 Sulfide 13 51 mg/L 119 J fd
Notes:
RPD = relative percent difference
RC = reason code
µg/L = micrograms per liter
mg/L = milligrams per liter
J = Detected result was qualified as estimated and the bias is indeterminable.
fd = field duplicate precision outlier

Sample Dilution Summary
All samples were analyzed undiluted.

Data Validation Summary Report Pactiv Evergreen
Canton, North Carolina
Sampling Event: June 2023

5
Overall Assessment
The data from the June 2023 sampling event were validated independently from the laboratory to
assess data quality. All analytes detected at concentrations less than the reporting limit but greater
than the method detection limit were qualified by the laboratory as estimated (J). This J-qualifier
was retained during data validation. Table B-1 in Attachment B provides a summary of the results
qualified during data validation.

Attachment A
Sample and Analysis Summary

A-1
Table A-1
Sample and Analysis Summary
SDG Sample ID
Sample
Date Sample Type
U.S. EPA 6010D (total and
dissolved)
U.S. EPA
7470A (total and
dissolved)
U.S. EPA
8260D
U.S. EPA
8270E
SM 2320B-
2011
SM 2120B-
2011
SM 4500-S2D-
2011
U.S. EPA
8290A
92674166 /
10659324 PZ21WG-062223 6/22/2023 Ground water X X X X X X X
92674238/
YF23032/
10661874
PZ4WG-062323 6/23/2023 Ground water X X X X X X X X
92674238/
YF23032/ 10661874 DUP01WG-062323 6/23/2023 Duplicate of
PZ4WG-062323 X X X X X X X X
92674238/
YF23032/ 10661874 RW5WG-062323 6/23/2023 Ground water X X X X X X X X
92674238/
YF23032 TRIP BLANK 6/23/2023 Trip blank X
Notes:
SDG = sample delivery group
U.S. EPA = United States Environmental Protection Agency 6010D = total and dissolved metals via SW-846 Method 6010D
7470A = total and dissolved mercury via SW-846 Method 7470A 8260D = volatile organic compounds via SW-846 Method 8260D
8270E = semivolatile organic compounds via SW-846 Method 8270E
SM 2320B-2011 = alkalinity via Standard Method 2320B-2011 SM 2120B-2011 = true color via Standard Method 2120B-2011 SM 4500-S2D-2011 = sulfide via Standard Method 4500-S2D-2011
8290A = polychlorinated dibenzodioxins and polychlorinated dibenzofurans via SW-846 Method 8290A X = Sample was analyzed for the method indicated in the column header.

Attachment B
Qualified Results Summary

B-1
Table B-1
Qualified Results Summary
SDG Method Sample ID Analyte Result Unit Reporting Limit Validation Qualifier RC
92674166 U.S. EPA
8270E PZ21WG-062223 Di-n-octylphthalate 9.1 µg/L 9.1 UJ m
92674166 U.S. EPA
8270E PZ21WG-062223 Pyrene 9.1 µg/L 9.1 UJ m
92674166 U.S. EPA
8270E PZ21WG-062223 4,6-Dinitro-2-
methylphenol 18.2 µg/L 18.2 UJ m
92674166 U.S. EPA 8270E PZ21WG-062223 2,4-Dinitrophenol 45.5 µg/L 45.5 UJ m
92674166 U.S. EPA 8270E PZ21WG-062223 Chrysene 9.1 µg/L 9.1 UJ m
92674166 U.S. EPA 8270E PZ21WG-062223 Di-n-butylphthalate 9.1 µg/L 9.1 UJ m
92674166 U.S. EPA 8270E PZ21WG-062223 Dibenz(a,h)anthracene 9.1 µg/L 9.1 UJ m
92674166 U.S. EPA 8270E PZ21WG-062223 Pentachlorophenol 18.2 µg/L 18.2 UJ m
92674166 U.S. EPA 8270E PZ21WG-062223 4-Nitrophenol 45.5 µg/L 45.5 UJ m
92674238 U.S. EPA 7470A PZ4WG-062323 Mercury, Dissolved 12.7 µg/L 1 J fd
92674238 U.S. EPA
7470A DUP01WG-062323 Mercury, Dissolved 4.4 µg/L 0.2 J fd
92674238 U.S. EPA
8270E PZ4WG-062323 4-Nitrophenol 250 µg/L 250 UJ l
92674238 U.S. EPA
8270E PZ4WG-062323 4,6-Dinitro-2-
methylphenol 100 µg/L 100 UJ l
92674238 U.S. EPA
8270E DUP01WG-062323 2,4,6-Trichlorophenol 50 µg/L 50 UJ s
92674238 U.S. EPA
8270E DUP01WG-062323 2,4-Dichlorophenol 50 µg/L 50 UJ s
92674238 U.S. EPA
8270E DUP01WG-062323 Pentachlorophenol 100 µg/L 100 UJ s
92674238 U.S. EPA
8270E DUP01WG-062323 2,4,5-Trichlorophenol 50 µg/L 50 UJ s
92674238 U.S. EPA
8270E DUP01WG-062323 2,4-Dinitrophenol 250 µg/L 250 UJ s
92674238 U.S. EPA 8270E DUP01WG-062323 2-Chlorophenol 50 µg/L 50 UJ s
92674238 U.S. EPA 8270E DUP01WG-062323 4-Nitrophenol 250 µg/L 250 UJ l,s
92674238 U.S. EPA 8270E DUP01WG-062323 2-Methylphenol(o-Cresol) 50 µg/L 50 UJ s
92674238 U.S. EPA 8270E DUP01WG-062323 2-Nitrophenol 50 µg/L 50 UJ s
92674238 U.S. EPA 8270E DUP01WG-062323 4,6-Dinitro-2-methylphenol 100 µg/L 100 UJ l,s
92674238 U.S. EPA 8270E DUP01WG-062323 4-Chloro-3-methylphenol 50 µg/L 50 UJ s
92674238 U.S. EPA 8270E DUP01WG-062323 2,4-Dimethylphenol 50 µg/L 50 UJ s
92674238 U.S. EPA
8270E DUP01WG-062323 Phenol 50 µg/L 50 UJ s
92674238 U.S. EPA
8270E DUP01WG-062323 3&4-Methylphenol(m&p
Cresol) 50 µg/L 50 UJ s
92674238 SM 4500-
S2D-2011 PZ4WG-062323 Sulfide 13 mg/L 2.5 J fd
92674238 SM 4500-
S2D-2011 DUP01WG-062323 Sulfide 51 mg/L 10 J fd
10661874 U.S. EPA
8290A PZ4WG-062323 1,2,3,7,8,9-HxCDF 100 pg/L 100 U bl

B-2
Table B-1
Qualified Results Summary
SDG Method Sample ID Analyte Result Unit Reporting Limit Validation Qualifier RC
10661874 U.S. EPA 8290A PZ4WG-062323 OCDD 200 pg/L 200 U bl
10661874 U.S. EPA 8290A DUP01WG-062323 1,2,3,4,7,8-HxCDD 99 pg/L 99 U bl
10661874 U.S. EPA 8290A DUP01WG-062323 OCDD 200 pg/L 200 U bl
10661874 U.S. EPA 8290A RW5WG-062323 1,2,3,7,8,9-HxCDF 99 pg/L 99 U bl

Notes:
SDG = sample delivery group
RC = reason code
U.S. EPA = United States Environmental Protection Agency µg/L = micrograms per liter
mg/L = milligrams per liter
pg/L = picograms per liter

Qualifier Definitions:
UJ = Not detected result was qualified as estimated.
J = Detected result was qualified as estimated and the bias is indeterminable.
U = The result was qualified as not detected at the reporting limit.

Reason Code Definitions:
m = matrix spike/matrix spike duplicate percent recovery outlier
fd = field duplicate precision outlier
l = laboratory control sample percent recovery outlier
s = surrogate percent recovery outlier
bl = laboratory blank outlier
#=CL#
July 18, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92674166
92674166
Project:
Pace Project No.:
RE:
Christina Ashdown
ENSAFE
313 Wingo Way
Mount Pleasant, SC 29464
PACTIV EVERGREEN-Revised Report
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on June 22, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
This revision was issued on 07/18/23 to report all requested analytes.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
cc:Phil Coop, ENSAFE Inc.
Travis Darden, ENSAFE Inc.
Lab, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 52
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 52
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Lab ID Sample ID Matrix Date Collected Date Received
92674166001 PZ21WG-062223 Water 06/22/23 14:25 06/22/23 16:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 3 of 52
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92674166001 PZ21WG-062223 SM 2120B-2011 2 PASI-EAED
EPA 6010D 16 PASI-ADBB1
EPA 6010D 16 PASI-ADBB1
EPA 7470A 1 PASI-ANMP
EPA 7470A 1 PASI-ANMP
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Sample:PZ21WG-062223 Lab ID:92674166001 Collected:06/22/23 14:25 Received:06/22/23 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.3 Std. Units 06/23/23 11:171
True Color ND units 06/23/23 11:175.0 5.0 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 06/29/23 14:20 7440-36-006/27/23 11:475.0 3.0 1
Arsenic ND ug/L 06/29/23 14:20 7440-38-206/27/23 11:4710.0 4.7 1
Barium 106 ug/L 06/29/23 14:20 7440-39-306/27/23 11:475.0 3.5 1
Beryllium ND ug/L 06/29/23 14:20 7440-41-706/27/23 11:471.0 0.70 1
Boron ND ug/L 06/29/23 14:20 7440-42-806/27/23 11:4750.0 32.4 1
Cadmium ND ug/L 06/29/23 14:20 7440-43-906/27/23 11:471.0 0.40 1
Chromium ND ug/L 06/29/23 14:20 7440-47-306/27/23 11:475.0 3.7 1
Cobalt ND ug/L 06/29/23 14:20 7440-48-406/27/23 11:475.0 3.6 1
Copper ND ug/L 06/29/23 14:20 7440-50-806/27/23 11:475.0 4.3 1
Lead ND ug/L 06/29/23 14:20 7439-92-106/27/23 11:475.0 4.5 1
Nickel ND ug/L 06/29/23 14:20 7440-02-006/27/23 11:475.0 3.5 1
Selenium ND ug/L 06/29/23 14:20 7782-49-206/27/23 11:4710.0 4.7 1
Silver ND ug/L 06/29/23 14:20 7440-22-406/27/23 11:475.0 2.5 1
Thallium ND ug/L 06/29/23 14:20 7440-28-006/27/23 11:4710.0 8.1 1
Vanadium ND ug/L 06/29/23 14:20 7440-62-206/27/23 11:475.0 3.9 1
Zinc ND ug/L 06/29/23 14:20 7440-66-606/27/23 11:4710.0 9.5 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 06/29/23 15:39 7440-36-006/25/23 20:145.0 3.0 1
Arsenic, Dissolved ND ug/L 06/29/23 15:39 7440-38-206/25/23 20:1410.0 4.7 1
Barium, Dissolved 114 ug/L 06/29/23 15:39 7440-39-306/25/23 20:145.0 3.5 1
Beryllium, Dissolved ND ug/L 06/29/23 15:39 7440-41-706/25/23 20:141.0 0.70 1
Boron, Dissolved ND ug/L 06/29/23 15:39 7440-42-806/25/23 20:1450.0 32.4 1
Cadmium, Dissolved ND ug/L 06/29/23 15:39 7440-43-906/25/23 20:141.0 0.40 1
Chromium, Dissolved ND ug/L 06/29/23 15:39 7440-47-306/25/23 20:145.0 3.7 1
Cobalt, Dissolved ND ug/L 06/29/23 15:39 7440-48-406/25/23 20:145.0 3.6 1
Copper, Dissolved ND ug/L 06/29/23 15:39 7440-50-806/25/23 20:145.0 4.3 1
Lead, Dissolved ND ug/L 06/29/23 15:39 7439-92-106/25/23 20:145.0 4.5 1
Nickel, Dissolved ND ug/L 06/29/23 15:39 7440-02-006/25/23 20:145.0 3.5 1
Selenium, Dissolved ND ug/L 06/29/23 15:39 7782-49-206/25/23 20:1410.0 4.7 1
Silver, Dissolved ND ug/L 06/29/23 15:39 7440-22-406/25/23 20:145.0 2.5 1
Thallium, Dissolved ND ug/L 06/29/23 15:39 7440-28-006/25/23 20:1410.0 8.1 1
Vanadium, Dissolved ND ug/L 06/29/23 15:39 7440-62-206/25/23 20:145.0 3.9 1
Zinc, Dissolved ND ug/L 06/29/23 15:39 7440-66-606/25/23 20:1410.0 9.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 07/13/23 11:03 7439-97-607/12/23 09:140.20 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Sample:PZ21WG-062223 Lab ID:92674166001 Collected:06/22/23 14:25 Received:06/22/23 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 07/14/23 11:28 7439-97-607/13/23 12:140.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 06/25/23 17:50 83-32-906/23/23 15:339.1 1.8 1
Acenaphthylene ND ug/L 06/25/23 17:50 208-96-806/23/23 15:339.1 1.8 1
Acetophenone ND ug/L 06/25/23 17:50 98-86-206/23/23 15:339.1 1.4 1
Anthracene ND ug/L 06/25/23 17:50 120-12-706/23/23 15:339.1 2.1 1
Atrazine ND ug/L 06/25/23 17:50 1912-24-906/23/23 15:339.1 2.9 1
Benzaldehyde ND ug/L 06/25/23 17:50 100-52-706/23/23 15:339.1 3.3 1
Benzo(a)anthracene ND ug/L 06/25/23 17:50 56-55-306/23/23 15:339.1 2.4 1
Benzo(a)pyrene ND ug/L 06/25/23 17:50 50-32-806/23/23 15:339.1 2.5 1
Benzo(b)fluoranthene ND ug/L 06/25/23 17:50 205-99-206/23/23 15:339.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 06/25/23 17:50 191-24-206/23/23 15:339.1 2.6 1
Benzo(k)fluoranthene ND ug/L 06/25/23 17:50 207-08-906/23/23 15:339.1 2.5 1
Biphenyl (Diphenyl)ND ug/L 06/25/23 17:50 92-52-406/23/23 15:339.1 1.7 1
4-Bromophenylphenyl ether 2.3J ug/L 06/25/23 17:50 101-55-306/23/23 15:339.1 1.6 1
Butylbenzylphthalate ND ug/L 06/25/23 17:50 85-68-706/23/23 15:339.1 2.9 1
Caprolactam ND ug/L 06/25/23 17:50 105-60-206/23/23 15:339.1 6.3 1
Carbazole ND ug/L 06/25/23 17:50 86-74-806/23/23 15:339.1 2.1 1
4-Chloro-3-methylphenol ND ug/L 06/25/23 17:50 59-50-706/23/23 15:339.1 3.0 1
4-Chloroaniline ND ug/L 06/25/23 17:50 106-47-806/23/23 15:3318.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 06/25/23 17:50 111-91-106/23/23 15:339.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/25/23 17:50 111-44-406/23/23 15:339.1 1.7 1
2-Chloronaphthalene ND ug/L 06/25/23 17:50 91-58-706/23/23 15:339.1 1.6 1
2-Chlorophenol ND ug/L 06/25/23 17:50 95-57-806/23/23 15:339.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 06/25/23 17:50 7005-72-306/23/23 15:339.1 1.8 1
Chrysene ND ug/L 06/25/23 17:50 218-01-9 M106/23/23 15:339.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 06/25/23 17:50 53-70-3 M106/23/23 15:339.1 2.7 1
Dibenzofuran ND ug/L 06/25/23 17:50 132-64-906/23/23 15:339.1 1.9 1
3,3'-Dichlorobenzidine ND ug/L 06/25/23 17:50 91-94-106/23/23 15:3318.2 7.4 1
2,4-Dichlorophenol ND ug/L 06/25/23 17:50 120-83-206/23/23 15:339.1 1.3 1
Diethylphthalate ND ug/L 06/25/23 17:50 84-66-206/23/23 15:339.1 1.9 1
2,4-Dimethylphenol ND ug/L 06/25/23 17:50 105-67-9 L106/23/23 15:339.1 1.5 1
Dimethylphthalate ND ug/L 06/25/23 17:50 131-11-306/23/23 15:339.1 1.9 1
Di-n-butylphthalate ND ug/L 06/25/23 17:50 84-74-2 M106/23/23 15:339.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/25/23 17:50 534-52-1 M106/23/23 15:3318.2 7.1 1
2,4-Dinitrophenol ND ug/L 06/25/23 17:50 51-28-5 M106/23/23 15:3345.5 23.6 1
2,4-Dinitrotoluene ND ug/L 06/25/23 17:50 121-14-206/23/23 15:339.1 1.5 1
2,6-Dinitrotoluene ND ug/L 06/25/23 17:50 606-20-206/23/23 15:339.1 1.6 1
Di-n-octylphthalate ND ug/L 06/25/23 17:50 117-84-0 M106/23/23 15:339.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/25/23 17:50 117-81-706/23/23 15:335.5 3.4 1
Fluoranthene ND ug/L 06/25/23 17:50 206-44-006/23/23 15:339.1 2.0 1
Fluorene ND ug/L 06/25/23 17:50 86-73-706/23/23 15:339.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 06/25/23 17:50 87-68-306/23/23 15:339.1 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Sample:PZ21WG-062223 Lab ID:92674166001 Collected:06/22/23 14:25 Received:06/22/23 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Hexachlorobenzene ND ug/L 06/25/23 17:50 118-74-106/23/23 15:339.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 06/25/23 17:50 77-47-406/23/23 15:339.1 1.4 1
Hexachloroethane ND ug/L 06/25/23 17:50 67-72-106/23/23 15:339.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/25/23 17:50 193-39-506/23/23 15:339.1 2.6 1
Isophorone ND ug/L 06/25/23 17:50 78-59-106/23/23 15:339.1 1.5 1
2-Methylnaphthalene ND ug/L 06/25/23 17:50 91-57-606/23/23 15:339.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 06/25/23 17:50 95-48-706/23/23 15:339.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/25/23 17:50 15831-10-406/23/23 15:339.1 1.1 1
Naphthalene ND ug/L 06/25/23 17:50 91-20-306/23/23 15:339.1 1.9 1
2-Nitroaniline ND ug/L 06/25/23 17:50 88-74-406/23/23 15:3318.2 2.7 1
3-Nitroaniline ND ug/L 06/25/23 17:50 99-09-206/23/23 15:3318.2 3.4 1
4-Nitroaniline ND ug/L 06/25/23 17:50 100-01-606/23/23 15:3318.2 4.6 1
Nitrobenzene ND ug/L 06/25/23 17:50 98-95-306/23/23 15:339.1 1.7 1
2-Nitrophenol ND ug/L 06/25/23 17:50 88-75-506/23/23 15:339.1 1.3 1
4-Nitrophenol ND ug/L 06/25/23 17:50 100-02-7 M106/23/23 15:3345.5 6.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/25/23 17:50 621-64-706/23/23 15:339.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 06/25/23 17:50 86-30-606/23/23 15:339.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/25/23 17:50 108-60-106/23/23 15:339.1 1.0 1
Pentachlorophenol ND ug/L 06/25/23 17:50 87-86-5 M106/23/23 15:3318.2 3.4 1
Phenanthrene ND ug/L 06/25/23 17:50 85-01-806/23/23 15:339.1 1.8 1
Phenol ND ug/L 06/25/23 17:50 108-95-206/23/23 15:339.1 1.2 1
Pyrene ND ug/L 06/25/23 17:50 129-00-0 M106/23/23 15:339.1 2.0 1
2,4,5-Trichlorophenol ND ug/L 06/25/23 17:50 95-95-406/23/23 15:339.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 06/25/23 17:50 88-06-206/23/23 15:339.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)94 %06/25/23 17:50 4165-60-006/23/23 15:3310-138 1
2-Fluorobiphenyl (S)87 %06/25/23 17:50 321-60-806/23/23 15:3310-130 1
Terphenyl-d14 (S)101 %06/25/23 17:50 1718-51-006/23/23 15:3319-191 1
Phenol-d6 (S)44 %06/25/23 17:50 13127-88-306/23/23 15:3310-130 1
2-Fluorophenol (S)57 %06/25/23 17:50 367-12-406/23/23 15:3310-130 1
2,4,6-Tribromophenol (S)91 %06/25/23 17:50 118-79-606/23/23 15:3310-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/02/23 14:32 67-64-125.0 5.1 1
Benzene ND ug/L 07/02/23 14:32 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 07/02/23 14:32 75-27-41.0 0.31 1
Bromoform ND ug/L 07/02/23 14:32 75-25-21.0 0.34 1
Bromomethane ND ug/L 07/02/23 14:32 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 07/02/23 14:32 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 07/02/23 14:32 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 07/02/23 14:32 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 07/02/23 14:32 108-90-71.0 0.28 1
Chloroethane ND ug/L 07/02/23 14:32 75-00-31.0 0.65 1
Chloroform ND ug/L 07/02/23 14:32 67-66-31.0 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Sample:PZ21WG-062223 Lab ID:92674166001 Collected:06/22/23 14:25 Received:06/22/23 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 07/02/23 14:32 74-87-31.0 0.54 1
Cyclohexane ND ug/L 07/02/23 14:32 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 07/02/23 14:32 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 07/02/23 14:32 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 07/02/23 14:32 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 07/02/23 14:32 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 07/02/23 14:32 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 07/02/23 14:32 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 07/02/23 14:32 75-71-8 L11.0 0.35 1
1,1-Dichloroethane ND ug/L 07/02/23 14:32 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 07/02/23 14:32 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 07/02/23 14:32 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 07/02/23 14:32 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 07/02/23 14:32 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 07/02/23 14:32 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 07/02/23 14:32 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 07/02/23 14:32 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 07/02/23 14:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/02/23 14:32 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 07/02/23 14:32 98-82-81.0 0.33 1
Methyl acetate ND ug/L 07/02/23 14:32 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 07/02/23 14:32 108-87-2 M110.0 1.5 1
Methylene Chloride ND ug/L 07/02/23 14:32 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/02/23 14:32 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 07/02/23 14:32 1634-04-41.0 0.42 1
Styrene ND ug/L 07/02/23 14:32 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 07/02/23 14:32 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 07/02/23 14:32 127-18-41.0 0.29 1
Toluene ND ug/L 07/02/23 14:32 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 07/02/23 14:32 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 07/02/23 14:32 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 07/02/23 14:32 79-00-51.0 0.32 1
Trichloroethene ND ug/L 07/02/23 14:32 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 07/02/23 14:32 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 07/02/23 14:32 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 07/02/23 14:32 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 07/02/23 14:32 179601-23-12.0 0.71 1
o-Xylene ND ug/L 07/02/23 14:32 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)95 %07/02/23 14:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %07/02/23 14:32 17060-07-070-130 1
Toluene-d8 (S)101 %07/02/23 14:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Sample:PZ21WG-062223 Lab ID:92674166001 Collected:06/22/23 14:25 Received:06/22/23 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 129 mg/L 07/01/23 18:445.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 06/27/23 04:54 18496-25-80.10 0.022 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782635
SM 2120B-2011
SM 2120B-2011
2120B True Color EDEN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples:92674166001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4059650
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
True Color units ND 5.0 06/23/23 11:155.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4059651LABORATORY CONTROL SAMPLE:
LCSSpike
True Color units 35.035 100 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674166001
4059652SAMPLE DUPLICATE:
pH Std. Units 6.3 0 106.3
True Color units ND 10ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
786136
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674166001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4075898
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 07/13/23 10:590.12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4075899LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4075900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4075901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 99 75-12597 2 252.5ND 2.5 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
786528
EPA 7470A
EPA 7470A
7470 Mercury Dissolved
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674166001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4077942
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 07/14/23 11:230.12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4077943LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.72.5 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4077944MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4077945
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2.5 99 75-125104 4 252.5ND 2.5 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783225
EPA 3010A
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674166001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4062107
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/29/23 13:133.0
Arsenic ug/L ND 10.0 06/29/23 13:134.7
Barium ug/L ND 5.0 06/29/23 13:133.5
Beryllium ug/L ND 1.0 06/29/23 13:130.70
Boron ug/L ND 50.0 06/29/23 13:1332.4
Cadmium ug/L ND 1.0 06/29/23 13:130.40
Chromium ug/L ND 5.0 06/29/23 13:133.7
Cobalt ug/L ND 5.0 06/29/23 13:133.6
Copper ug/L ND 5.0 06/29/23 13:134.3
Lead ug/L ND 5.0 06/29/23 13:134.5
Nickel ug/L ND 5.0 06/29/23 13:133.5
Selenium ug/L ND 10.0 06/29/23 13:134.7
Silver ug/L ND 5.0 06/29/23 13:132.5
Thallium ug/L ND 10.0 06/29/23 13:138.1
Vanadium ug/L ND 5.0 06/29/23 13:133.9
Zinc ug/L ND 10.0 06/29/23 13:139.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4062108LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 494500 99 80-120
Arsenic ug/L 495500 99 80-120
Barium ug/L 503500 101 80-120
Beryllium ug/L 503500 101 80-120
Boron ug/L 505500 101 80-120
Cadmium ug/L 502500 100 80-120
Chromium ug/L 509500 102 80-120
Cobalt ug/L 505500 101 80-120
Copper ug/L 505500 101 80-120
Lead ug/L 502500 100 80-120
Nickel ug/L 509500 102 80-120
Selenium ug/L 489500 98 80-120
Silver ug/L 249250 100 80-120
Thallium ug/L 508500 102 80-120
Vanadium ug/L 507500 101 80-120
Zinc ug/L 498500 100 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062109MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4062110
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 102 75-125102 0 20500ND509509
Arsenic ug/L 500 103 75-125103 0 20500ND513514
Barium ug/L 500 101 75-125100 1 20500106612607
Beryllium ug/L 500 103 75-125103 0 20500ND513515
Boron ug/L 500 103 75-125103 0 20500ND547547
Cadmium ug/L 500 100 75-125100 0 20500ND499501
Chromium ug/L 500 100 75-125101 0 20500ND503503
Cobalt ug/L 500 100 75-125100 0 20500ND502502
Copper ug/L 500 103 75-125103 0 20500ND516514
Lead ug/L 500 99 75-12599 0 20500ND495495
Nickel ug/L 500 101 75-125101 0 20500ND504505
Selenium ug/L 500 105 75-125105 0 20500ND523523
Silver ug/L 250 101 75-125100 0 20250ND252251
Thallium ug/L 500 100 75-125100 1 20500ND498501
Vanadium ug/L 500 103 75-125103 0 20500ND516515
Zinc ug/L 500 99 75-12599 0 20500ND498498
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782484
EPA 3010A
EPA 6010D
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674166001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4059237
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
Antimony, Dissolved ug/L ND 5.0 06/29/23 15:253.0
Arsenic, Dissolved ug/L ND 10.0 06/29/23 15:254.7
Barium, Dissolved ug/L ND 5.0 06/29/23 15:253.5
Beryllium, Dissolved ug/L ND 1.0 06/29/23 15:250.70
Boron, Dissolved ug/L ND 50.0 06/29/23 15:2532.4
Cadmium, Dissolved ug/L ND 1.0 06/29/23 15:250.40
Chromium, Dissolved ug/L ND 5.0 06/29/23 15:253.7
Cobalt, Dissolved ug/L ND 5.0 06/29/23 15:253.6
Copper, Dissolved ug/L ND 5.0 06/29/23 15:254.3
Lead, Dissolved ug/L ND 5.0 06/29/23 15:254.5
Nickel, Dissolved ug/L ND 5.0 06/29/23 15:253.5
Selenium, Dissolved ug/L ND 10.0 06/29/23 15:254.7
Silver, Dissolved ug/L ND 5.0 06/29/23 15:252.5
Thallium, Dissolved ug/L ND 10.0 06/29/23 15:258.1
Vanadium, Dissolved ug/L ND 5.0 06/29/23 15:253.9
Zinc, Dissolved ug/L ND 10.0 06/29/23 15:259.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4059238LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 492500 98 80-120
Arsenic, Dissolved ug/L 493500 99 80-120
Barium, Dissolved ug/L 499500 100 80-120
Beryllium, Dissolved ug/L 498500 100 80-120
Boron, Dissolved ug/L 497500 99 80-120
Cadmium, Dissolved ug/L 494500 99 80-120
Chromium, Dissolved ug/L 498500 100 80-120
Cobalt, Dissolved ug/L 496500 99 80-120
Copper, Dissolved ug/L 488500 98 80-120
Lead, Dissolved ug/L 495500 99 80-120
Nickel, Dissolved ug/L 502500 100 80-120
Selenium, Dissolved ug/L 518500 104 80-120
Silver, Dissolved ug/L 243250 97 80-120
Thallium, Dissolved ug/L 501500 100 80-120
Vanadium, Dissolved ug/L 497500 99 80-120
Zinc, Dissolved ug/L 496500 99 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4059239MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4059240
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 500 100 75-125100 1 20500ND498502
Arsenic, Dissolved ug/L 500 99 75-125101 1 20500ND498504
Barium, Dissolved ug/L 500 97 75-12598 0 20500114600603
Beryllium, Dissolved ug/L 500 100 75-125101 1 20500ND501507
Boron, Dissolved ug/L 500 101 75-125102 1 20500ND533538
Cadmium, Dissolved ug/L 500 96 75-12597 0 20500ND481484
Chromium, Dissolved ug/L 500 98 75-12599 1 20500ND490495
Cobalt, Dissolved ug/L 500 97 75-12598 1 20500ND488492
Copper, Dissolved ug/L 500 101 75-125102 1 20500ND507511
Lead, Dissolved ug/L 500 96 75-12596 1 20500ND480484
Nickel, Dissolved ug/L 500 98 75-12599 1 20500ND490495
Selenium, Dissolved ug/L 500 103 75-125104 1 20500ND515520
Silver, Dissolved ug/L 250 98 75-12599 1 20250ND245248
Thallium, Dissolved ug/L 500 91 75-12592 1 20500ND454458
Vanadium, Dissolved ug/L 500 100 75-125101 1 20500ND500504
Zinc, Dissolved ug/L 500 95 75-12596 0 20500ND479481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783374
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674166001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4062974
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 06/28/23 12:430.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/28/23 12:430.22
1,1,2-Trichloroethane ug/L ND 1.0 06/28/23 12:430.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 v106/28/23 12:430.32
1,1-Dichloroethane ug/L ND 1.0 06/28/23 12:430.37
1,1-Dichloroethene ug/L ND 1.0 06/28/23 12:430.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/28/23 12:430.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/28/23 12:430.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/28/23 12:430.27
1,2-Dichlorobenzene ug/L ND 1.0 06/28/23 12:430.34
1,2-Dichloroethane ug/L ND 1.0 06/28/23 12:430.32
1,2-Dichloropropane ug/L ND 1.0 06/28/23 12:430.36
1,3-Dichlorobenzene ug/L ND 1.0 06/28/23 12:430.34
1,4-Dichlorobenzene ug/L ND 1.0 06/28/23 12:430.33
2-Butanone (MEK)ug/L ND 5.0 06/28/23 12:434.0
2-Hexanone ug/L ND 5.0 06/28/23 12:430.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/28/23 12:432.7
Acetone ug/L ND 25.0 06/28/23 12:435.1
Benzene ug/L ND 1.0 06/28/23 12:430.34
Bromodichloromethane ug/L ND 1.0 06/28/23 12:430.31
Bromoform ug/L ND 1.0 06/28/23 12:430.34
Bromomethane ug/L ND 2.0 v106/28/23 12:431.7
Carbon disulfide ug/L ND 2.0 06/28/23 12:430.36
Carbon tetrachloride ug/L ND 1.0 06/28/23 12:430.33
Chlorobenzene ug/L ND 1.0 06/28/23 12:430.28
Chloroethane ug/L ND 1.0 v106/28/23 12:430.65
Chloroform ug/L ND 1.0 06/28/23 12:430.43
Chloromethane ug/L ND 1.0 v106/28/23 12:430.54
cis-1,2-Dichloroethene ug/L ND 1.0 06/28/23 12:430.38
cis-1,3-Dichloropropene ug/L ND 1.0 06/28/23 12:430.36
Cyclohexane ug/L ND 1.0 06/28/23 12:430.35
Dibromochloromethane ug/L ND 1.0 06/28/23 12:430.36
Dichlorodifluoromethane ug/L ND 1.0 v106/28/23 12:430.35
Ethylbenzene ug/L ND 1.0 06/28/23 12:430.30
Isopropylbenzene (Cumene)ug/L ND 1.0 06/28/23 12:430.33
m&p-Xylene ug/L ND 2.0 06/28/23 12:430.71
Methyl acetate ug/L ND 10.0 06/28/23 12:432.4
Methyl-tert-butyl ether ug/L ND 1.0 06/28/23 12:430.42
Methylcyclohexane ug/L ND 10.0 v106/28/23 12:431.5
Methylene Chloride ug/L ND 5.0 06/28/23 12:432.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4062974
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 06/28/23 12:430.34
Styrene ug/L ND 1.0 06/28/23 12:430.29
Tetrachloroethene ug/L ND 1.0 06/28/23 12:430.29
Toluene ug/L ND 1.0 06/28/23 12:430.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/28/23 12:430.40
trans-1,3-Dichloropropene ug/L ND 1.0 06/28/23 12:430.36
Trichloroethene ug/L ND 1.0 06/28/23 12:430.38
Trichlorofluoromethane ug/L ND 1.0 v106/28/23 12:430.30
Vinyl chloride ug/L ND 1.0 06/28/23 12:430.39
1,2-Dichloroethane-d4 (S)%98 70-130 06/28/23 12:43
4-Bromofluorobenzene (S)%96 70-130 06/28/23 12:43
Toluene-d8 (S)%100 70-130 06/28/23 12:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4062975LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.720 104 70-130
1,1,2,2-Tetrachloroethane ug/L 19.820 99 70-130
1,1,2-Trichloroethane ug/L 19.620 98 70-130
1,1,2-Trichlorotrifluoroethane ug/L 26.0 v12013070-130
1,1-Dichloroethane ug/L 19.920 100 70-130
1,1-Dichloroethene ug/L 22.220 111 70-130
1,2,4-Trichlorobenzene ug/L 18.420 92 70-130
1,2-Dibromo-3-chloropropane ug/L 17.820 89 70-131
1,2-Dibromoethane (EDB)ug/L 20.020 100 70-130
1,2-Dichlorobenzene ug/L 19.020 95 70-130
1,2-Dichloroethane ug/L 18.820 94 70-130
1,2-Dichloropropane ug/L 19.720 99 70-130
1,3-Dichlorobenzene ug/L 19.320 96 70-130
1,4-Dichlorobenzene ug/L 19.320 96 70-130
2-Butanone (MEK)ug/L 36.540 91 70-134
2-Hexanone ug/L 37.340 93 70-131
4-Methyl-2-pentanone (MIBK)ug/L 35.740 89 70-130
Acetone ug/L 37.540 94 70-133
Benzene ug/L 20.320 102 70-130
Bromodichloromethane ug/L 19.020 95 70-130
Bromoform ug/L 19.920 100 70-130
Bromomethane ug/L 16.8 v1208445-151
Carbon disulfide ug/L 23.320 116 70-130
Carbon tetrachloride ug/L 21.320 107 70-130
Chlorobenzene ug/L 20.120 100 70-130
Chloroethane ug/L 22.4 v12011239-152
Chloroform ug/L 19.820 99 70-130
Chloromethane ug/L 24.9 v12012458-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4062975LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 19.620 98 70-130
cis-1,3-Dichloropropene ug/L 19.320 96 70-130
Cyclohexane ug/L 23.720 119 70-130
Dibromochloromethane ug/L 19.420 97 70-130
Dichlorodifluoromethane ug/L 31.2 L1,v12015654-133
Ethylbenzene ug/L 19.920 100 70-130
Isopropylbenzene (Cumene)ug/L 20.620 103 70-130
m&p-Xylene ug/L 40.340 101 70-130
Methyl acetate ug/L 17.620 88 70-130
Methyl-tert-butyl ether ug/L 17.720 89 70-130
Methylcyclohexane ug/L 24.4 v12012270-130
Methylene Chloride ug/L 19.120 96 66-130
o-Xylene ug/L 19.920 100 70-130
Styrene ug/L 20.020 100 70-130
Tetrachloroethene ug/L 20.720 104 70-130
Toluene ug/L 19.720 98 70-130
trans-1,2-Dichloroethene ug/L 20.720 103 70-130
trans-1,3-Dichloropropene ug/L 18.520 93 70-130
Trichloroethene ug/L 20.520 102 70-130
Trichlorofluoromethane ug/L 23.5 v12011862-130
Vinyl chloride ug/L 19.020 95 62-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062976MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674120008
4062977
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 120 70-150132 9 3020ND23.9 26.3
1,1,2,2-Tetrachloroethane ug/L 20 108 69-142118 9 3020ND21.7 23.7
1,1,2-Trichloroethane ug/L 20 111 70-138119 7 3020ND22.2 23.8
1,1,2-
Trichlorotrifluoroethane ug/L M12014370-157158 10 3020ND28.5 31.5
1,1-Dichloroethane ug/L 20 116 70-150125 8 3020ND23.1 25.0
1,1-Dichloroethene ug/L 20 126 70-156139 9 3020ND25.3 27.7
1,2,4-Trichlorobenzene ug/L 20 101 70-146111 9 3020ND20.2 22.1
1,2-Dibromo-3-
chloropropane ug/L 20 104 68-146111 6 3020ND20.9 22.3
1,2-Dibromoethane (EDB)ug/L 20 109 70-138120 10 3020ND21.8 24.1
1,2-Dichlorobenzene ug/L 20 104 70-141116 11 3020ND20.8 23.1
1,2-Dichloroethane ug/L 20 103 69-143114 10 3020ND20.6 22.8
1,2-Dichloropropane ug/L 20 114 68-156122 7 3020ND22.8 24.4
1,3-Dichlorobenzene ug/L 20 107 70-143117 9 3020ND21.3 23.4
1,4-Dichlorobenzene ug/L 20 106 70-142117 9 3020ND21.3 23.3
2-Butanone (MEK)ug/L 40 108 60-157115 7 3040ND43.1 46.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062976MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674120008
4062977
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 103 68-146111 7 3040ND41.4 44.3
4-Methyl-2-pentanone
(MIBK)ug/L 40 101 70-141109 8 3040ND40.3 43.6
Acetone ug/L 40 99 58-157102 2 3040ND44.1 45.0
Benzene ug/L 20 118 70-142127 8 3020ND23.5 25.5
Bromodichloromethane ug/L 20 109 70-139118 8 3020ND21.8 23.5
Bromoform ug/L 20 111 64-140120 8 3020ND22.1 24.0
Bromomethane ug/L 20 96 28-192102 6 3020ND19.2 20.4
Carbon disulfide ug/L 20 131 70-151142 8 3020ND26.2 28.5
Carbon tetrachloride ug/L 20 122 70-148134 9 3020ND24.4 26.7
Chlorobenzene ug/L 20 113 70-141125 10 3020ND22.7 25.0
Chloroethane ug/L 20 126 58-191137 8 3020ND25.2 27.4
Chloroform ug/L 20 110 70-148118 7 3020ND22.4 24.0
Chloromethane ug/L 20 139 43-162151 8 3020ND27.8 30.1
cis-1,2-Dichloroethene ug/L 20 114 68-151121 6 3020ND22.8 24.2
cis-1,3-Dichloropropene ug/L 20 108 70-139118 9 3020ND21.5 23.6
Cyclohexane ug/L 20 136 77-149148 9 3020ND27.1 29.7
Dibromochloromethane ug/L 20 109 70-144121 10 3020ND21.8 24.2
Dichlorodifluoromethane ug/L M02016239-171178 9 3020ND32.4 35.7
Ethylbenzene ug/L 20 113 70-143125 10 3020ND22.7 25.0
Isopropylbenzene
(Cumene)ug/L 20 117 70-145128 9 3020ND23.4 25.6
m&p-Xylene ug/L 40 113 70-144125 9 3040ND45.3 49.8
Methyl acetate ug/L 20 99 63-146106 6 3020ND19.9 21.2
Methyl-tert-butyl ether ug/L 20 101 65-143111 9 3020ND20.2 22.2
Methylcyclohexane ug/L M12014470-144157 9 3020ND28.7 31.4
Methylene Chloride ug/L 20 103 62-149113 9 3020ND20.9 23.0
o-Xylene ug/L 20 111 70-145124 11 3020ND22.3 24.8
Styrene ug/L 20 112 70-143124 11 3020ND22.3 24.9
Tetrachloroethene ug/L 20 116 70-145128 9 3020ND24.0 26.4
Toluene ug/L 20 115 70-142124 8 3020ND23.0 24.9
trans-1,2-Dichloroethene ug/L 20 119 70-151131 10 3020ND23.8 26.2
trans-1,3-Dichloropropene ug/L 20 107 70-139115 8 3020ND21.3 23.1
Trichloroethene ug/L 20 119 62-146129 8 3020ND23.8 25.8
Trichlorofluoromethane ug/L 20 131 63-153143 9 3020ND26.2 28.6
Vinyl chloride ug/L 20 109 61-163119 9 3020ND21.8 23.7
1,2-Dichloroethane-d4 (S)%94 70-13096
4-Bromofluorobenzene (S)%97 70-13098
Toluene-d8 (S)%101 70-130101
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062978MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4062979
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 124 70-150118 5 3020ND24.9 23.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062978MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4062979
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,2,2-Tetrachloroethane ug/L 20 111 69-142107 3 3020ND22.1 21.4
1,1,2-Trichloroethane ug/L 20 112 70-138107 5 3020ND22.5 21.4
1,1,2-
Trichlorotrifluoroethane ug/L 20 147 70-157140 5 3020ND29.4 27.9
1,1-Dichloroethane ug/L 20 120 70-150113 6 3020ND24.0 22.7
1,1-Dichloroethene ug/L 20 130 70-156126 4 3020ND26.1 25.2
1,2,4-Trichlorobenzene ug/L 20 102 70-14696 7 3020ND20.5 19.2
1,2-Dibromo-3-
chloropropane ug/L 20 105 68-14698 7 3020ND21.1 19.6
1,2-Dibromoethane (EDB)ug/L 20 113 70-138109 4 3020ND22.6 21.7
1,2-Dichlorobenzene ug/L 20 109 70-141102 6 3020ND21.7 20.4
1,2-Dichloroethane ug/L 20 106 69-14399 7 3020ND21.3 19.9
1,2-Dichloropropane ug/L 20 114 68-156110 4 3020ND22.9 21.9
1,3-Dichlorobenzene ug/L 20 110 70-143103 6 3020ND22.0 20.6
1,4-Dichlorobenzene ug/L 20 109 70-142103 6 3020ND21.8 20.5
2-Butanone (MEK)ug/L 40 109 60-157102 7 3040ND43.6 40.8
2-Hexanone ug/L 40 107 68-146101 6 3040ND42.7 40.3
4-Methyl-2-pentanone
(MIBK)
ug/L 40 102 70-14196 5 3040ND40.7 38.5
Acetone ug/L 40 99 58-15795 4 3040ND40.7 39.2
Benzene ug/L 20 119 70-142115 4 3020ND23.8 23.0
Bromodichloromethane ug/L 20 110 70-139106 4 3020ND22.1 21.1
Bromoform ug/L 20 116 64-140111 5 3020ND23.3 22.2
Bromomethane ug/L 20 99 28-19296 3 3020ND19.8 19.2
Carbon disulfide ug/L 20 135 70-151127 6 3020ND27.0 25.4
Carbon tetrachloride ug/L 20 130 70-148122 6 3020ND25.9 24.4
Chlorobenzene ug/L 20 117 70-141113 4 3020ND23.5 22.5
Chloroethane ug/L 20 130 58-191126 3 3020ND26.0 25.2
Chloroform ug/L 20 110 70-148111 0 3020ND22.4 22.5
Chloromethane ug/L 20 143 43-162138 3 3020ND28.6 27.7
cis-1,2-Dichloroethene ug/L 20 114 68-151111 3 3020ND22.9 22.2
cis-1,3-Dichloropropene ug/L 20 111 70-139104 6 3020ND22.1 20.8
Cyclohexane ug/L 20 138 77-149133 4 3020ND27.7 26.5
Dibromochloromethane ug/L 20 114 70-144109 5 3020ND22.8 21.7
Dichlorodifluoromethane ug/L 20 169 39-171161 5 3020ND33.8 32.2
Ethylbenzene ug/L 20 116 70-143113 3 3020ND23.3 22.5
Isopropylbenzene
(Cumene)
ug/L 20 120 70-145116 3 3020ND24.1 23.3
m&p-Xylene ug/L 40 117 70-144113 4 3040ND46.8 45.1
Methyl acetate ug/L 20 101 63-14688 14 3020ND20.3 17.6
Methyl-tert-butyl ether ug/L 20 102 65-14398 5 3020ND20.5 19.5
Methylcyclohexane ug/L M12014970-144141 6 3020ND29.7 28.1
Methylene Chloride ug/L 20 106 62-149100 5 3020ND21.7 20.6
o-Xylene ug/L 20 115 70-145110 4 3020ND23.0 22.0
Styrene ug/L 20 116 70-143111 4 3020ND23.1 22.1
Tetrachloroethene ug/L 20 121 70-145115 4 3020ND24.1 23.1
Toluene ug/L 20 117 70-142112 4 3020ND23.3 22.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062978MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4062979
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
trans-1,2-Dichloroethene ug/L 20 122 70-151118 3 3020ND24.4 23.6
trans-1,3-Dichloropropene ug/L 20 108 70-139102 6 3020ND21.7 20.5
Trichloroethene ug/L 20 124 62-146117 6 3020ND24.7 23.4
Trichlorofluoromethane ug/L 20 138 63-153129 6 3020ND27.6 25.9
Vinyl chloride ug/L 20 112 61-163107 4 3020ND22.3 21.5
1,2-Dichloroethane-d4 (S)%95 70-13093
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%100 70-130100
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062980MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674382011
4062981
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 129 70-150125 3 3020ND25.8 25.0
1,1,2,2-Tetrachloroethane ug/L 20 117 69-142115 2 3020ND23.4 22.9
1,1,2-Trichloroethane ug/L 20 117 70-138116 1 3020ND23.4 23.2
1,1,2-
Trichlorotrifluoroethane ug/L 20 155 70-157149 4 3020ND31.6 30.5
1,1-Dichloroethane ug/L 20 122 70-150121 1 3020ND24.4 24.2
1,1-Dichloroethene ug/L 20 135 70-156132 3 3020ND27.1 26.4
1,2,4-Trichlorobenzene ug/L 20 104 70-146103 0 3020ND20.8 20.7
1,2-Dibromo-3-
chloropropane ug/L 20 109 68-146106 2 3020ND21.7 21.2
1,2-Dibromoethane (EDB)ug/L 20 118 70-138115 2 3020ND23.5 23.0
1,2-Dichlorobenzene ug/L 20 111 70-141109 2 3020ND22.2 21.8
1,2-Dichloroethane ug/L 20 109 69-143108 2 3020ND21.9 21.5
1,2-Dichloropropane ug/L 20 119 68-156118 0 3020ND23.7 23.6
1,3-Dichlorobenzene ug/L 20 112 70-143111 1 3020ND22.4 22.2
1,4-Dichlorobenzene ug/L 20 113 70-142111 3 3020ND22.7 22.1
2-Butanone (MEK)ug/L 40 113 60-157112 0 3040ND45.0 44.9
2-Hexanone ug/L 40 111 68-146109 2 3040ND44.4 43.6
4-Methyl-2-pentanone
(MIBK)ug/L 40 109 70-141105 3 3040ND43.5 42.1
Acetone ug/L 40 106 58-157102 4 3040ND43.5 41.9
Benzene ug/L 20 125 70-142121 3 3020ND25.0 24.3
Bromodichloromethane ug/L 20 116 70-139113 3 3020ND23.2 22.6
Bromoform ug/L 20 120 64-140116 4 3020ND24.0 23.1
Bromomethane ug/L 20 91 28-19294 3 3020ND18.2 18.8
Carbon disulfide ug/L 20 140 70-151136 3 3020ND28.0 27.2
Carbon tetrachloride ug/L 20 136 70-148131 4 30201.6 28.7 27.7
Chlorobenzene ug/L 20 121 70-141118 2 3020ND24.1 23.6
Chloroethane ug/L 20 132 58-191127 4 3020ND26.5 25.4
Chloroform ug/L 20 118 70-148114 3 30201.2 24.7 24.0
Chloromethane ug/L 20 146 43-162144 2 3020ND29.2 28.7
cis-1,2-Dichloroethene ug/L 20 120 68-151117 3 3020ND24.4 23.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062980MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674382011
4062981
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
cis-1,3-Dichloropropene ug/L 20 116 70-139112 3 3020ND23.1 22.4
Cyclohexane ug/L 20 143 77-149140 2 3020ND28.7 28.0
Dibromochloromethane ug/L 20 120 70-144115 4 3020ND23.9 23.1
Dichlorodifluoromethane ug/L M02017739-171167 6 3020ND35.4 33.5
Ethylbenzene ug/L 20 121 70-143118 2 3020ND24.1 23.6
Isopropylbenzene
(Cumene)ug/L 20 126 70-145121 4 3020ND25.3 24.3
m&p-Xylene ug/L 40 122 70-144117 4 3040ND48.7 46.9
Methyl acetate ug/L 20 106 63-146103 2 3020ND21.2 20.7
Methyl-tert-butyl ether ug/L 20 107 65-143105 3 3020ND21.8 21.2
Methylcyclohexane ug/L M12015670-144153 2 3020ND31.1 30.6
Methylene Chloride ug/L 20 109 62-149107 2 3020ND22.1 21.7
o-Xylene ug/L 20 120 70-145114 4 3020ND23.9 22.9
Styrene ug/L 20 121 70-143117 3 3020ND24.2 23.4
Tetrachloroethene ug/L 20 126 70-145121 4 3020ND25.5 24.5
Toluene ug/L 20 122 70-142118 3 3020ND24.4 23.7
trans-1,2-Dichloroethene ug/L 20 128 70-151125 2 3020ND25.5 25.0
trans-1,3-Dichloropropene ug/L 20 115 70-139110 4 3020ND22.9 22.0
Trichloroethene ug/L 20 131 62-146127 2 302029.4 55.7 54.8
Trichlorofluoromethane ug/L 20 142 63-153139 2 3020ND28.3 27.7
Vinyl chloride ug/L 20 115 61-163113 2 3020ND23.1 22.7
1,2-Dichloroethane-d4 (S)%93 70-13095
4-Bromofluorobenzene (S)%98 70-13097
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782534
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674166001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4059340
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/23/23 20:271.2
2,4,5-Trichlorophenol ug/L ND 10.0 06/23/23 20:271.4
2,4,6-Trichlorophenol ug/L ND 10.0 06/23/23 20:271.6
2,4-Dichlorophenol ug/L ND 10.0 06/23/23 20:271.4
2,4-Dimethylphenol ug/L ND 10.0 06/23/23 20:271.7
2,4-Dinitrophenol ug/L ND 50.0 06/23/23 20:2726.0
2,4-Dinitrotoluene ug/L ND 10.0 06/23/23 20:271.6
2,6-Dinitrotoluene ug/L ND 10.0 06/23/23 20:271.7
2-Chloronaphthalene ug/L ND 10.0 06/23/23 20:271.7
2-Chlorophenol ug/L ND 10.0 06/23/23 20:271.2
2-Methylnaphthalene ug/L ND 10.0 06/23/23 20:271.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/23/23 20:271.9
2-Nitroaniline ug/L ND 20.0 06/23/23 20:273.0
2-Nitrophenol ug/L ND 10.0 06/23/23 20:271.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/23/23 20:271.2
3,3'-Dichlorobenzidine ug/L ND 20.0 06/23/23 20:278.1
3-Nitroaniline ug/L ND 20.0 06/23/23 20:273.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 v106/23/23 20:277.8
4-Bromophenylphenyl ether ug/L ND 10.0 06/23/23 20:271.8
4-Chloro-3-methylphenol ug/L ND 10.0 06/23/23 20:273.3
4-Chloroaniline ug/L ND 20.0 06/23/23 20:273.6
4-Chlorophenylphenyl ether ug/L ND 10.0 06/23/23 20:272.0
4-Nitroaniline ug/L ND 20.0 06/23/23 20:275.1
4-Nitrophenol ug/L ND 50.0 06/23/23 20:276.6
Acenaphthene ug/L ND 10.0 06/23/23 20:272.0
Acenaphthylene ug/L ND 10.0 06/23/23 20:272.0
Acetophenone ug/L ND 10.0 06/23/23 20:271.5
Anthracene ug/L ND 10.0 06/23/23 20:272.3
Atrazine ug/L ND 10.0 06/23/23 20:273.2
Benzaldehyde ug/L ND 10.0 06/23/23 20:273.6
Benzo(a)anthracene ug/L ND 10.0 06/23/23 20:272.7
Benzo(a)pyrene ug/L ND 10.0 06/23/23 20:272.8
Benzo(b)fluoranthene ug/L ND 10.0 06/23/23 20:272.6
Benzo(g,h,i)perylene ug/L ND 10.0 06/23/23 20:272.8
Benzo(k)fluoranthene ug/L ND 10.0 06/23/23 20:272.7
Biphenyl (Diphenyl)ug/L ND 10.0 06/23/23 20:271.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/23/23 20:271.8
bis(2-Chloroethyl) ether ug/L ND 10.0 06/23/23 20:271.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/23/23 20:273.7
Butylbenzylphthalate ug/L ND 10.0 06/23/23 20:273.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4059340
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
Caprolactam ug/L 8.7J 10.0 06/23/23 20:276.9
Carbazole ug/L ND 10.0 06/23/23 20:272.4
Chrysene ug/L ND 10.0 06/23/23 20:272.8
Di-n-butylphthalate ug/L ND 10.0 06/23/23 20:272.2
Di-n-octylphthalate ug/L ND 10.0 06/23/23 20:273.9
Dibenz(a,h)anthracene ug/L ND 10.0 06/23/23 20:273.0
Dibenzofuran ug/L ND 10.0 06/23/23 20:272.1
Diethylphthalate ug/L ND 10.0 06/23/23 20:272.0
Dimethylphthalate ug/L ND 10.0 06/23/23 20:272.1
Fluoranthene ug/L ND 10.0 06/23/23 20:272.2
Fluorene ug/L ND 10.0 06/23/23 20:272.1
Hexachloro-1,3-butadiene ug/L ND 10.0 06/23/23 20:271.8
Hexachlorobenzene ug/L ND 10.0 06/23/23 20:272.2
Hexachlorocyclopentadiene ug/L ND 10.0 06/23/23 20:271.6
Hexachloroethane ug/L ND 10.0 06/23/23 20:271.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/23/23 20:272.9
Isophorone ug/L ND 10.0 06/23/23 20:271.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/23/23 20:271.3
N-Nitrosodiphenylamine ug/L ND 10.0 06/23/23 20:273.0
Naphthalene ug/L ND 10.0 06/23/23 20:272.1
Nitrobenzene ug/L ND 10.0 06/23/23 20:271.9
Pentachlorophenol ug/L ND 20.0 06/23/23 20:273.8
Phenanthrene ug/L ND 10.0 06/23/23 20:272.0
Phenol ug/L ND 10.0 06/23/23 20:271.4
Pyrene ug/L ND 10.0 06/23/23 20:272.2
2,4,6-Tribromophenol (S)%65 10-164 06/23/23 20:27
2-Fluorobiphenyl (S)%89 10-130 06/23/23 20:27
2-Fluorophenol (S)%37 10-130 06/23/23 20:27
Nitrobenzene-d5 (S)%97 10-138 06/23/23 20:27
Phenol-d6 (S)%41 10-130 06/23/23 20:27
Terphenyl-d14 (S)%115 19-191 06/23/23 20:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4059341LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 52.150 104 21-135
2,4,5-Trichlorophenol ug/L 44.350 89 38-147
2,4,6-Trichlorophenol ug/L 38.450 77 34-142
2,4-Dichlorophenol ug/L 48.550 97 36-136
2,4-Dimethylphenol ug/L 76.8 L15015438-134
2,4-Dinitrophenol ug/L 114250 46 10-169
2,4-Dinitrotoluene ug/L 55.850 112 44-154
2,6-Dinitrotoluene ug/L 57.150 114 44-156
2-Chloronaphthalene ug/L 46.650 93 25-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4059341LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 42.250 84 29-130
2-Methylnaphthalene ug/L 47.250 94 23-130
2-Methylphenol(o-Cresol)ug/L 45.650 91 31-130
2-Nitroaniline ug/L 97.9100 98 39-145
2-Nitrophenol ug/L 47.350 95 29-142
3&4-Methylphenol(m&p Cresol)ug/L 46.650 93 30-130
3,3'-Dichlorobenzidine ug/L 108100 108 44-158
3-Nitroaniline ug/L 107100 107 45-152
4,6-Dinitro-2-methylphenol ug/L 59.3 v11005939-158
4-Bromophenylphenyl ether ug/L 49.050 98 47-147
4-Chloro-3-methylphenol ug/L 99.5100 100 40-138
4-Chloroaniline ug/L 89.3100 89 35-130
4-Chlorophenylphenyl ether ug/L 51.650 103 36-139
4-Nitroaniline ug/L 105100 105 46-157
4-Nitrophenol ug/L 97.2250 39 17-130
Acenaphthene ug/L 51.050 102 34-135
Acenaphthylene ug/L 49.550 99 35-137
Acetophenone ug/L 45.050 90 30-137
Anthracene ug/L 45.750 91 47-146
Atrazine ug/L 59.650 119 30-130
Benzaldehyde ug/L 54.850 110 17-167
Benzo(a)anthracene ug/L 51.050 102 48-160
Benzo(a)pyrene ug/L 50.550 101 47-165
Benzo(b)fluoranthene ug/L 56.150 112 49-171
Benzo(g,h,i)perylene ug/L 50.750 101 46-166
Benzo(k)fluoranthene ug/L 51.350 103 55-162
Biphenyl (Diphenyl)ug/L 46.250 92 28-130
bis(2-Chloroethoxy)methane ug/L 46.950 94 33-136
bis(2-Chloroethyl) ether ug/L 47.250 94 30-142
bis(2-Ethylhexyl)phthalate ug/L 52.150 104 46-173
Butylbenzylphthalate ug/L 55.950 112 53-169
Caprolactam ug/L 38.650 77 13-130
Carbazole ug/L 50.650 101 48-157
Chrysene ug/L 49.350 99 54-152
Di-n-butylphthalate ug/L 50.450 101 49-161
Di-n-octylphthalate ug/L 54.650 109 50-166
Dibenz(a,h)anthracene ug/L 51.750 103 46-166
Dibenzofuran ug/L 50.450 101 37-136
Diethylphthalate ug/L 52.750 105 45-149
Dimethylphthalate ug/L 51.450 103 43-145
Fluoranthene ug/L 53.350 107 50-153
Fluorene ug/L 52.750 105 42-142
Hexachloro-1,3-butadiene ug/L 40.950 82 10-130
Hexachlorobenzene ug/L 47.750 95 44-138
Hexachlorocyclopentadiene ug/L 44.150 88 10-130
Hexachloroethane ug/L 37.450 75 10-130
Indeno(1,2,3-cd)pyrene ug/L 51.250 102 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4059341LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 49.450 99 36-135
N-Nitroso-di-n-propylamine ug/L 49.350 99 33-140
N-Nitrosodiphenylamine ug/L 46.150 92 46-144
Naphthalene ug/L 45.450 91 20-130
Nitrobenzene ug/L 47.450 95 33-133
Pentachlorophenol ug/L 50.7100 51 21-163
Phenanthrene ug/L 48.950 98 47-146
Phenol ug/L 32.250 64 19-130
Pyrene ug/L 51.550 103 53-155
2,4,6-Tribromophenol (S)%78 10-164
2-Fluorobiphenyl (S)%93 10-130
2-Fluorophenol (S)%56 10-130
Nitrobenzene-d5 (S)%94 10-138
Phenol-d6 (S)%53 10-130
Terphenyl-d14 (S)%99 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4059342MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673251003
4059343
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-
chloropropane)ug/L 50 119 11-143100 17 3050ND59.3 50.1
2,4,5-Trichlorophenol ug/L 50 130 10-170114 12 3050ND64.8 57.2
2,4,6-Trichlorophenol ug/L 50 130 10-166114 12 3050ND64.8 57.2
2,4-Dichlorophenol ug/L 50 128 10-153109 16 3050ND64.2 54.7
2,4-Dimethylphenol ug/L M05018720-147163 14 3050ND93.6 81.5
2,4-Dinitrophenol ug/L 250 128 10-172123 4 30250ND321308
2,4-Dinitrotoluene ug/L 50 130 30-164120 8 3050ND64.9 60.1
2,6-Dinitrotoluene ug/L 50 135 31-163119 13 3050ND67.6 59.4
2-Chloronaphthalene ug/L 50 101 15-13487 15 3050ND50.6 43.7
2-Chlorophenol ug/L 50 108 10-13993 14 3050ND53.9 46.7
2-Methylnaphthalene ug/L 50 97 12-13086 11 3050ND48.3 43.1
2-Methylphenol(o-Cresol)ug/L 50 111 19-13299 12 3050ND55.7 49.5
2-Nitroaniline ug/L 100 116 23-154102 13 30100ND116102
2-Nitrophenol ug/L 50 127 10-159111 13 3050ND63.3 55.3
3&4-Methylphenol(m&p
Cresol)
ug/L 50 112 13-13698 13 3050ND55.8 49.0
3,3'-Dichlorobenzidine ug/L 100 134 10-178111 18 30100ND134111
3-Nitroaniline ug/L 100 126 20-166112 12 30100ND126112
4,6-Dinitro-2-methylphenol ug/L v110013510-187119 12 30100ND135119
4-Bromophenylphenyl ether ug/L 50 115 31-15796 19 3050ND57.7 47.8
4-Chloro-3-methylphenol ug/L 100 122 27-146110 10 30100ND122110
4-Chloroaniline ug/L 100 110 13-14395 15 30100ND11095.3
4-Chlorophenylphenyl ether ug/L 50 119 23-149106 12 3050ND59.6 53.0
4-Nitroaniline ug/L 100 123 24-171112 10 30100ND123112
4-Nitrophenol ug/L 250 79 10-13073 8 30250ND197182
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4059342MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673251003
4059343
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L 50 116 21-147100 15 3050ND57.8 49.9
Acenaphthylene ug/L 50 112 19-150100 12 3050ND56.0 49.8
Acetophenone ug/L 50 109 22-14593 15 3050ND54.4 46.7
Anthracene ug/L 50 108 36-15291 16 3050ND53.9 45.7
Atrazine ug/L 50 86 18-17384 2 3050ND43.0 42.0
Benzaldehyde ug/L 50 117 16-163111 6 3050ND58.6 55.4
Benzo(a)anthracene ug/L 50 123 42-163104 16 3050ND61.5 52.2
Benzo(a)pyrene ug/L 50 118 40-169101 16 3050ND59.1 50.3
Benzo(b)fluoranthene ug/L 50 133 40-177113 16 3050ND66.7 56.7
Benzo(g,h,i)perylene ug/L 50 118 38-174102 15 3050ND59.1 50.9
Benzo(k)fluoranthene ug/L 50 123 41-171102 18 3050ND61.3 51.1
Biphenyl (Diphenyl)ug/L 50 100 14-13787 13 3050ND49.8 43.5
bis(2-
Chloroethoxy)methane ug/L 50 116 19-146100 15 3050ND57.9 49.9
bis(2-Chloroethyl) ether ug/L 50 109 19-15196 14 3050ND54.7 47.8
bis(2-Ethylhexyl)phthalate ug/L 50 128 42-168106 19 3050ND63.8 52.8
Butylbenzylphthalate ug/L 50 136 42-177109 22 3050ND67.8 54.5
Caprolactam ug/L 50 43 10-13052 17 3050ND21.7 25.8
Carbazole ug/L 50 121 38-164103 16 3050ND60.5 51.7
Chrysene ug/L 50 118 43-159100 16 3050ND58.9 50.1
Di-n-butylphthalate ug/L 50 119 42-160103 15 3050ND59.5 51.3
Di-n-octylphthalate ug/L 50 134 42-171113 17 3050ND67.0 56.7
Dibenz(a,h)anthracene ug/L 50 121 40-171103 16 3050ND60.3 51.6
Dibenzofuran ug/L 50 117 23-147103 12 3050ND58.4 51.7
Diethylphthalate ug/L 50 122 33-157109 11 3050ND61.1 54.5
Dimethylphthalate ug/L 50 120 27-154106 12 3050ND59.9 53.1
Fluoranthene ug/L 50 125 42-157108 15 3050ND62.5 54.0
Fluorene ug/L 50 122 25-155108 12 3050ND61.2 54.1
Hexachloro-1,3-butadiene ug/L 50 40 10-13042 6 3050ND19.8 21.0
Hexachlorobenzene ug/L 50 112 32-14595 16 3050ND56.0 47.5
Hexachlorocyclopentadiene ug/L 50 76 10-13067 13 3050ND38.1 33.5
Hexachloroethane ug/L 50 29 10-13034 17 3050ND14.4 17.1
Indeno(1,2,3-cd)pyrene ug/L 50 123 39-174104 16 3050ND61.4 52.1
Isophorone ug/L 50 122 19-146108 12 3050ND61.1 54.1
N-Nitroso-di-n-propylamine ug/L 50 118 20-150104 13 3050ND58.9 51.9
N-Nitrosodiphenylamine ug/L 50 111 33-14993 18 3050ND55.4 46.4
Naphthalene ug/L 50 78 10-12875 5 3050ND39.2 37.5
Nitrobenzene ug/L 50 113 19-14599 13 3050ND56.3 49.6
Pentachlorophenol ug/L 100 133 10-188109 19 30100ND133109
Phenanthrene ug/L 50 116 38-15098 17 3050ND58.0 48.8
Phenol ug/L 50 78 10-13069 13 3050ND39.2 34.5
Pyrene ug/L 50 122 42-163102 18 3050ND61.2 51.0
2,4,6-Tribromophenol (S)%110 10-164113
2-Fluorobiphenyl (S)%90 10-13091
2-Fluorophenol (S)%72 10-13073
Nitrobenzene-d5 (S)%101 10-138108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4059342MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673251003
4059343
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%59 10-13062
Terphenyl-d14 (S)%105 19-191105
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4060053MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4060054
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-
chloropropane)ug/L 90.9 42 11-14347 11 3090.9ND 38.5 43.0
2,4,5-Trichlorophenol ug/L 90.9 29 10-17037 22 3090.9ND 26.6 33.2
2,4,6-Trichlorophenol ug/L 90.9 18 10-16624 3090.9ND 16.8J 21.9
2,4-Dichlorophenol ug/L 90.9 32 10-15339 20 3090.9ND 28.9 35.2
2,4-Dimethylphenol ug/L 90.9 60 20-14773 20 3090.9ND 54.6 66.4
2,4-Dinitrophenol ug/L M1455010-1720 30455NDNDND
2,4-Dinitrotoluene ug/L 90.9 38 30-16448 23 3090.9ND 34.7 43.7
2,6-Dinitrotoluene ug/L 90.9 43 31-16355 23 3090.9ND 39.4 49.6
2-Chloronaphthalene ug/L 90.9 38 15-13445 17 3090.9ND 34.6 41.1
2-Chlorophenol ug/L 90.9 30 10-13936 19 3090.9ND 26.9 32.5
2-Methylnaphthalene ug/L 90.9 38 12-13046 18 3090.9ND 34.6 41.5
2-Methylphenol(o-Cresol)ug/L 90.9 33 19-13240 19 3090.9ND 29.9 36.3
2-Nitroaniline ug/L 182 37 23-15446 20 30182ND67.9 82.9
2-Nitrophenol ug/L 90.9 34 10-15942 21 3090.9ND 30.7 38.0
3&4-Methylphenol(m&p
Cresol)ug/L 90.9 34 13-13641 18 3090.9ND 31.0 37.1
3,3'-Dichlorobenzidine ug/L 182 43 10-17854 23 30182ND77.3 97.7
3-Nitroaniline ug/L 182 40 20-16648 20 30182ND72.2 87.9
4,6-Dinitro-2-methylphenol ug/L M1182610-1878 30182NDNDND
4-Bromophenylphenyl ether ug/L 90.9 39 31-15748 19 3090.92.3J 37.7 45.7
4-Chloro-3-methylphenol ug/L 182 37 27-14645 17 30182ND68.2 81.2
4-Chloroaniline ug/L 182 34 13-14342 22 30182ND61.9 77.0
4-Chlorophenylphenyl ether ug/L 90.9 42 23-14949 16 3090.9ND 38.1 45.0
4-Nitroaniline ug/L 182 37 24-17144 17 30182ND67.7 80.3
4-Nitrophenol ug/L M1455010-1300 30455NDNDND
Acenaphthene ug/L 90.9 41 21-14748 17 3090.9ND 37.1 44.0
Acenaphthylene ug/L 90.9 40 19-15047 17 3090.9ND 36.4 43.0
Acetophenone ug/L 90.9 35 22-14541 16 3090.9ND 31.7 37.3
Anthracene ug/L 90.9 38 36-15246 18 3090.9ND 34.5 41.5
Atrazine ug/L 90.9 54 18-17363 15 3090.9ND 49.0 57.1
Benzaldehyde ug/L 90.9 45 16-16353 16 3090.9ND 40.9 48.1
Benzo(a)anthracene ug/L 90.9 42 42-16351 20 3090.9ND 38.2 46.5
Benzo(a)pyrene ug/L 90.9 41 40-16951 21 3090.9ND 37.4 46.3
Benzo(b)fluoranthene ug/L 90.9 43 40-17754 24 3090.9ND 38.8 49.2
Benzo(g,h,i)perylene ug/L 90.9 41 38-17451 23 3090.9ND 36.9 46.5
Benzo(k)fluoranthene ug/L 90.9 41 41-17154 27 3090.9ND 37.3 48.6
Biphenyl (Diphenyl)ug/L 90.9 36 14-13744 19 3090.9ND 32.9 39.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4060053MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4060054
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
bis(2-
Chloroethoxy)methane ug/L 90.9 37 19-14645 19 3090.9ND 33.9 40.9
bis(2-Chloroethyl) ether ug/L 90.9 36 19-15141 12 3090.9ND 33.1 37.3
bis(2-Ethylhexyl)phthalate ug/L 90.9 42 42-16853 23 3090.9ND 38.0 47.7
Butylbenzylphthalate ug/L 90.9 44 42-17756 25 3090.9ND 39.8 51.0
Caprolactam ug/L 90.9 21 10-13028 29 3090.9ND 18.9 25.3
Carbazole ug/L 90.9 41 38-16451 21 3090.9ND 37.0 45.9
Chrysene ug/L M190.9 42 43-15951 19 3090.9ND 38.6 46.4
Di-n-butylphthalate ug/L M190.9 41 42-16049 18 3090.9ND 37.4 44.9
Di-n-octylphthalate ug/L M190.9 41 42-17152 23 3090.9ND 37.7 47.5
Dibenz(a,h)anthracene ug/L M190.9 39 40-17151 28 3090.9ND 35.0 46.4
Dibenzofuran ug/L 90.9 41 23-14748 17 3090.9ND 36.8 43.5
Diethylphthalate ug/L 90.9 41 33-15751 20 3090.9ND 37.7 45.9
Dimethylphthalate ug/L 90.9 41 27-15450 21 3090.9ND 37.1 45.7
Fluoranthene ug/L 90.9 44 42-15752 18 3090.9ND 39.6 47.5
Fluorene ug/L 90.9 42 25-15549 16 3090.9ND 38.0 44.6
Hexachloro-1,3-butadiene ug/L 90.9 34 10-13043 22 3090.9ND 31.1 38.7
Hexachlorobenzene ug/L 90.9 41 32-14550 20 3090.9ND 37.0 45.1
Hexachlorocyclopentadiene ug/L 90.9 35 10-13043 20 3090.9ND 31.7 38.9
Hexachloroethane ug/L 90.9 31 10-13037 17 3090.9ND 28.1 33.3
Indeno(1,2,3-cd)pyrene ug/L 90.9 41 39-17451 23 3090.9ND 36.9 46.6
Isophorone ug/L 90.9 40 19-14648 19 3090.9ND 36.3 43.9
N-Nitroso-di-n-propylamine ug/L 90.9 37 20-15042 13 3090.9ND 34.0 38.6
N-Nitrosodiphenylamine ug/L 90.9 39 33-14947 19 3090.9ND 35.4 43.1
Naphthalene ug/L 90.9 38 10-12845 16 3090.9ND 34.5 40.6
Nitrobenzene ug/L 90.9 39 19-14548 22 3090.9ND 35.0 43.5
Pentachlorophenol ug/L M1182710-18810 30182ND13.1J 18.0J
Phenanthrene ug/L 90.9 40 38-15049 19 3090.9ND 36.6 44.5
Phenol ug/L 90.9 19 10-13027 3090.9ND 17.3J 24.2
Pyrene ug/L M190.9 41 42-16352 22 3090.9ND 37.7 47.0
2,4,6-Tribromophenol (S)%32 10-16440
2-Fluorobiphenyl (S)%41 10-13049
2-Fluorophenol (S)%19 10-13023
Nitrobenzene-d5 (S)%43 10-13851
Phenol-d6 (S)%21 10-13025
Terphenyl-d14 (S)%42 19-19153
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
784254
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674166001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4067550
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 07/01/23 14:205.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4067551LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.650 103 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4067552LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 52.450 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4067553MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4067554
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 111 80-120116 1 2550129185187
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4067655MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674362001
4067656
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M15011680-120121 2 255092.4 151 153
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783153
SM 4500-S2D-2011
SM 4500-S2D-2011
4500S2D Sulfide Water
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674166001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4061905
Associated Lab Samples:92674166001
Matrix:Water
AnalyzedMDL
Sulfide mg/L ND 0.10 06/27/23 04:520.022
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4061906LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide mg/L 0.520.5 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4061907MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4061908
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 99 80-120106 6 100.5ND 0.50 0.53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 52
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 52
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92674166
PACTIV EVERGREEN-Revised Report
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92674166001 782635PZ21WG-062223 SM 2120B-2011
92674166001 783225 783277PZ21WG-062223 EPA 3010A EPA 6010D
92674166001 782484 782895PZ21WG-062223 EPA 3010A EPA 6010D
92674166001 786136 786221PZ21WG-062223 EPA 7470A EPA 7470A
92674166001 786528 786802PZ21WG-062223 EPA 7470A EPA 7470A
92674166001 782534 782695PZ21WG-062223 EPA 3510C EPA 8270E
92674166001 783374PZ21WG-062223 EPA 8260D
92674166001 784254PZ21WG-062223 SM 2320B-2011
92674166001 783153PZ21WG-062223 SM 4500-S2D-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/18/2023 06:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 52
Page 35 of 52
Page 36 of 52
Page 37 of 52
Thisreportshouldnotbereproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamplesincludedinthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,LLC.
1700 Elm Street
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
Client - Charlotte
PACE Charlotte
9800 Kincey Ave.
Huntersville NC 28078
REPORT OF
LABORATORY
ANALYSIS FOR
PCDD/PCDF
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
July 18, 2023
Pace Project #: 10659324
Sample Receipt Date: 06/28/2023
Client Project #: 92674166
Client Sub PO #: N/A
The report provided has been invoiced as a Level 2
PCDD/PCDF Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questionstoIsaac Johnson,your Pace
Project Manager.
State Cert #: 530
Suite 100
Report Prepared for:
Page 1 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
July 18, 2023
Isaac Johnson, Project Manager
[phone]
[phone] (fax)
[e-mail]
Page 38 of 52
Pace Analytical Services,LLC.
1700 Elm Street
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
This report presents the results from the analysis performed on one sample submitted by a representative
of Pace Analytical Services, LLC. The sample was analyzed for the presence or absence of
polychlorodibenzo-p-dioxins (PCDDs) and polychlorodibenzofurans (PCDFs) using a modified version of
USEPA Method 8290A. The reporting limits were set to correspond to the lowest calibration points and a
nominal 1-liter sample amount, and the sensitivity was verified by signal-to-noise measurements. The
quantitation limits, adjusted for sample extraction amount, may be somewhat higher or lower than the
reporting limits provided in this report. This report was revised to provide results for all tetra through
octa-chlorinated PCDDs and PCDFs.
The recoveries of the isotopically-labeled PCDD/PCDF internal standards in the sample extract ranged
from 53-91%. All of the labeled internal standard recoveries obtained for this project were within the
40-135% target range specified in Method 8290A. Also, since the quantification of the native
2,3,7,8-substituted congeners was based on isotope dilution, the data were automatically corrected for
recovery and accurate values were obtained.
A laboratory method blank was prepared and analyzed with the sample batch as part of our routine quality
control procedures. The results show the blank to be free of PCDDs and PCDFs at the reporting limits.
Laboratory and matrix spike samples were also prepared using clean reference matrix or sample matrix
that had been fortified with native standard materials. The results show that the spiked native compounds
were recovered at 82-110% with relative percent differences of 0.2-6.1%. These results were within the
target ranges for the method.
The responses obtained for the labeled OCDD in calibration standard analysis U230703A_18 was outside
the target range. As specified in our procedures for this method, the average of the daily response factors
for this compound was used in the calculations for the samples from this runshift. The affected values
were flagged "Y" on the results tables.
DISCUSSION
Page 2 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 39 of 52
REPORT OF LABORATORY ANALYSIS
This report shallnot bereproduced,except in full,
withoutthe written consentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 40 of 52
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 41 of 52
Page 5 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 42 of 52
6/28/23
Page 6 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 43 of 52
Page 7 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 44 of 52
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
A =

B =

C =

D =

E =

H2 =

I =

J =

L =

Nn =

P =

R =

S =

U =

V =

X =

Y =

* =
Reporting Limit based on signal to noise (EDL)

Less than 10x higher than method blank level

Result obtained from confirmation analysis

Result obtained from analysis of diluted sample

Exceeds calibration range

Extracted outside of holding time

Isotope ratio out of specification

Estimated value

Suppressive interference, analyte may be biased low

Value obtained from additional analysis

PCDE Interference

Recovery outside target range

Peak saturated

Analyte not detected

Result verified by confirmation analysis

%D Exceeds limits

Calculated using average of daily RFs

See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 45 of 52
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 46 of 52
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted% MoistureDry Weight Extracted
ICAL ID
CCal Filename(s)
Method Blank ID
Client's Sample ID PZ21WG-06222392674166001
U230705B_13
SMT
NA959 mL
NA
U230524
U230705A_17 & U230705B_17
BLANK-107107
MatrixDilutionCollected
Received
Extracted
Analyzed
WATERNA06/22/2023 14:25
06/28/2023 08:50
06/29/2023 10:25
07/06/2023 06:31
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L RL
2,3,7,8-TCDF ND 10 2,3,7,8-TCDF-13C 2.00 75-----Total TCDF ND 10 2,3,7,8-TCDD-13C 2.00 77-----1,2,3,7,8-PeCDF-13C 2.00 742,3,7,8-TCDD ND 10 2,3,4,7,8-PeCDF-13C 2.00 63-----Total TCDD ND 10 1,2,3,7,8-PeCDD-13C 2.00 77-----1,2,3,4,7,8-HxCDF-13C 2.00 801,2,3,7,8-PeCDF ND 50 1,2,3,6,7,8-HxCDF-13C 2.00 87-----2,3,4,7,8-PeCDF ND 50 2,3,4,6,7,8-HxCDF-13C 2.00 80-----Total PeCDF ND 50 1,2,3,7,8,9-HxCDF-13C 2.00 84-----1,2,3,4,7,8-HxCDD-13C 2.00 801,2,3,7,8-PeCDD ND 50 1,2,3,6,7,8-HxCDD-13C 2.00 90-----Total PeCDD ND 50 1,2,3,4,6,7,8-HpCDF-13C 2.00 73-----1,2,3,4,7,8,9-HpCDF-13C 2.00 76
1,2,3,4,7,8-HxCDF ND 50 1,2,3,4,6,7,8-HpCDD-13C 2.00 91-----1,2,3,6,7,8-HxCDF ND 50 OCDD-13C 4.00 53-----2,3,4,6,7,8-HxCDF ND 50-----1,2,3,7,8,9-HxCDF ND 50 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 50 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 50 2,3,7,8-TCDD-37Cl4 0.20 85-----1,2,3,6,7,8-HxCDD ND 50-----1,2,3,7,8,9-HxCDD ND 50-----Total HxCDD ND 50-----
1,2,3,4,6,7,8-HpCDF ND 50 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 50 Equivalence: 0.00 pg/L-----Total HpCDF ND 50 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD ND 50-----Total HpCDD ND 50-----
OCDF ND 100-----OCDD ND 100-----
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not Applicable
NC = Not CalculatedRL = Reporting Limit
Page 10 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 47 of 52
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL IDCCal Filename(s)
BLANK-107107
U230703A_07
SMT
1020 mL
U230524U230703A_02 & U230703A_18
Matrix
Dilution
Extracted
Analyzed
Water
06/29/2023 10:25
07/03/2023 13:52
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKZG
Native
Isomers pg/L
Conc EMPC
pg/L pg/L
Internal
Standards Added
ng's Percent
Recovery
RL
2,3,7,8-TCDF ND -----10 2,3,7,8-TCDF-13C 2.00 110Total TCDF ND -----10 2,3,7,8-TCDD-13C 2.00 981,2,3,7,8-PeCDF-13C 2.00 1292,3,7,8-TCDD ND -----10 2,3,4,7,8-PeCDF-13C 2.00 117Total TCDD ND -----10 1,2,3,7,8-PeCDD-13C 2.00 1231,2,3,4,7,8-HxCDF-13C 2.00 1031,2,3,7,8-PeCDF ND -----50 1,2,3,6,7,8-HxCDF-13C 2.00 1192,3,4,7,8-PeCDF ND -----50 2,3,4,6,7,8-HxCDF-13C 2.00 107Total PeCDF ND -----50 1,2,3,7,8,9-HxCDF-13C 2.00 1081,2,3,4,7,8-HxCDD-13C 2.00 971,2,3,7,8-PeCDD ND -----50 1,2,3,6,7,8-HxCDD-13C 2.00 108Total PeCDD ND -----50 1,2,3,4,6,7,8-HpCDF-13C 2.00 831,2,3,4,7,8,9-HpCDF-13C 2.00 891,2,3,4,7,8-HxCDF ND -----50 1,2,3,4,6,7,8-HpCDD-13C 2.00 901,2,3,6,7,8-HxCDF ND -----50 OCDD-13C 4.00 103 Y2,3,4,6,7,8-HxCDF ND -----501,2,3,7,8,9-HxCDF ND -----50 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF ND -----50 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD ND -----50 2,3,7,8-TCDD-37Cl4 0.20 981,2,3,6,7,8-HxCDD ND -----501,2,3,7,8,9-HxCDD ND -----50Total HxCDD ND -----50
1,2,3,4,6,7,8-HpCDF ND -----50 Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----50 Equivalence: 0.00 pg/LTotal HpCDF ND -----50 (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD ND -----50Total HpCDD ND -----50
OCDF ND -----100OCDDND-----100
Conc=Concentration (Totalsinclude2,3,7,8-substitutedisomers).
EMPC=EstimatedMaximumPossibleConcentration
Y =Calculated using average of daily RFs
RL =Reporting Limit
Page 11 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 48 of 52
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL IDCCal Filename(s)
LCS-107108
U230703A_05
SMT
1020 mL
U230524U230703A_02 & U230703A_18
Matrix
Dilution
ExtractedAnalyzed
Water
06/29/2023 10:2507/03/2023 12:19
NA
Method Blank ID BLANK-107107
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's Percent
RecoveryIsomersStandardsAdded
%
Rec.(ng)(ng)
2,3,7,8-TCDF 0.20 0.20 2,3,7,8-TCDF-13C 2.0 94102Total TCDF 2,3,7,8-TCDD-13C 2.0 861,2,3,7,8-PeCDF-13C 2.0 1182,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.0 104105Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 1091,2,3,4,7,8-HxCDF-13C 2.0 901,2,3,7,8-PeCDF 1.0 0.99 1,2,3,6,7,8-HxCDF-13C 2.0 103992,3,4,7,8-PeCDF 1.0 1.0 2,3,4,6,7,8-HxCDF-13C 2.0 92100Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 931,2,3,4,7,8-HxCDD-13C 2.0 821,2,3,7,8-PeCDD 1.0 0.90 1,2,3,6,7,8-HxCDD-13C 2.0 9290Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 671,2,3,4,7,8,9-HpCDF-13C 2.0 671,2,3,4,7,8-HxCDF 1.0 0.96 1,2,3,4,6,7,8-HpCDD-13C 2.0 71961,2,3,6,7,8-HxCDF 1.0 1.0 OCDD-13C 4.0 74102 Y2,3,4,6,7,8-HxCDF 1.0 1.0 1021,2,3,7,8,9-HxCDF 1.0 1.0 1,2,3,4-TCDD-13C 2.0 NA100Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.0 2,3,7,8-TCDD-37Cl4 0.20 861011,2,3,6,7,8-HxCDD 1.0 0.94 941,2,3,7,8,9-HxCDD 1.0 1.1 106Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.98 981,2,3,4,7,8,9-HpCDF 1.0 1.0 103Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.89 89Total HpCDD
OCDF 2.0 2.2 110OCDD2.0 2.1 107
Qs = Quantity Spiked
Qm = Quantity Measured
Rec.=Recovery (Expressedas Percent)
R=Recoveryoutsideof target range
Y =RF averaging used in calculations
Nn =Value obtained from additional analysis
NA = Not Applicable
*=See Discussion
Page 12 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 49 of 52
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL ID
CCal Filename(s)
92674166001-MS
U230705B_14
SMT
947 mLU230524
U230705A_17 & U230705B_17
MatrixDilutionExtracted
Analyzed
WATER
06/29/2023 10:25
07/06/2023 07:17
Client - PACE Charlotte
NA
Method Blank ID BLANK-107107
Client's Sample ID PZ21WG-062223-MS
Method 8290A Spiked Sample Report
Native Qs Qm Internal ng's Percent
RecoveryIsomersStandardsAdded%
Rec.(ng)(ng)
2,3,7,8-TCDF 0.20 0.19 2,3,7,8-TCDF-13C 2.00 80972,3,7,8-TCDD-13C 2.00 841,2,3,7,8-PeCDF-13C 2.00 73
2,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.00 671031,2,3,7,8-PeCDD-13C 2.00 791,2,3,4,7,8-HxCDF-13C 2.00 821,2,3,7,8-PeCDF 1.00 0.95 1,2,3,6,7,8-HxCDF-13C 2.00 86952,3,4,7,8-PeCDF 1.00 1.02 2,3,4,6,7,8-HxCDF-13C 2.00 801021,2,3,7,8,9-HxCDF-13C 2.00 841,2,3,4,7,8-HxCDD-13C 2.00 811,2,3,7,8-PeCDD 1.00 0.85 1,2,3,6,7,8-HxCDD-13C 2.00 88851,2,3,4,6,7,8-HpCDF-13C 2.00 721,2,3,4,7,8,9-HpCDF-13C 2.00 781,2,3,4,7,8-HxCDF 1.00 1.01 1,2,3,4,6,7,8-HpCDD-13C 2.00 871011,2,3,6,7,8-HxCDF 1.00 1.02 OCDD-13C 4.00 521022,3,4,6,7,8-HxCDF 1.00 1.07 1071,2,3,7,8,9-HxCDF 1.00 1.03 1,2,3,4-TCDD-13C 2.00 NA1031,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 1.00 0.99 2,3,7,8-TCDD-37Cl4 0.20 83991,2,3,6,7,8-HxCDD 1.00 0.95 951,2,3,7,8,9-HxCDD 1.00 1.05 105
1,2,3,4,6,7,8-HpCDF 1.00 0.99 991,2,3,4,7,8,9-HpCDF 1.00 1.02 102
1,2,3,4,6,7,8-HpCDD 1.00 0.89 89
OCDF 2.00 1.82 91OCDD2.00 2.06 103
Qs = Quantity Spiked Qm = Quantity Measured Rec. = Recovery (Expressed as Percent)
Page 13 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 50 of 52
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL ID
CCal Filename(s)
92674166001-MSD
U230705B_15
SMT
981 mLU230524
U230705A_17 & U230705B_17
MatrixDilutionExtracted
Analyzed
WATER
06/29/2023 10:25
07/06/2023 08:03
Client - PACE Charlotte
NA
Method Blank ID BLANK-107107
Client's Sample ID PZ21WG-062223-MSD
Method 8290A Spiked Sample Report
Native Qs Qm Internal ng's Percent
RecoveryIsomersStandardsAdded%
Rec.(ng)(ng)
2,3,7,8-TCDF 0.20 0.20 2,3,7,8-TCDF-13C 2.00 76982,3,7,8-TCDD-13C 2.00 781,2,3,7,8-PeCDF-13C 2.00 66
2,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.00 581031,2,3,7,8-PeCDD-13C 2.00 701,2,3,4,7,8-HxCDF-13C 2.00 771,2,3,7,8-PeCDF 1.00 1.01 1,2,3,6,7,8-HxCDF-13C 2.00 801012,3,4,7,8-PeCDF 1.00 1.01 2,3,4,6,7,8-HxCDF-13C 2.00 761011,2,3,7,8,9-HxCDF-13C 2.00 771,2,3,4,7,8-HxCDD-13C 2.00 771,2,3,7,8-PeCDD 1.00 0.82 1,2,3,6,7,8-HxCDD-13C 2.00 84821,2,3,4,6,7,8-HpCDF-13C 2.00 691,2,3,4,7,8,9-HpCDF-13C 2.00 751,2,3,4,7,8-HxCDF 1.00 1.04 1,2,3,4,6,7,8-HpCDD-13C 2.00 841041,2,3,6,7,8-HxCDF 1.00 1.07 OCDD-13C 4.00 511072,3,4,6,7,8-HxCDF 1.00 1.01 1011,2,3,7,8,9-HxCDF 1.00 1.07 1,2,3,4-TCDD-13C 2.00 NA1071,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 1.00 1.00 2,3,7,8-TCDD-37Cl4 0.20 801001,2,3,6,7,8-HxCDD 1.00 0.92 921,2,3,7,8,9-HxCDD 1.00 1.08 108
1,2,3,4,6,7,8-HpCDF 1.00 1.05 1051,2,3,4,7,8,9-HpCDF 1.00 1.01 101
1,2,3,4,6,7,8-HpCDD 1.00 0.89 89
OCDF 2.00 1.87 93OCDD2.00 2.18 109
Qs = Quantity Spiked Qm = Quantity Measured Rec. = Recovery (Expressed as Percent)
Page 14 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 51 of 52
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]Method 8290A Spike Sample Results
Client - PACE Charlotte
Client Sample ID
Lab Sample ID
MS ID
MSD ID
PZ21WG-062223
92674166001
92674166001-MS
92674166001-MSD
Sample Filename
MS Filename
MSD Filename
U230705B_13
U230705B_14
U230705B_15
Analyte
Quantity Unspiked Sample Contribution
to MS to MSD
Quantity Measured
MS MSD
RPD
Spiked
(ng)
Subtracted Recovery
MS MSD
(ng)(ng)(ng)(ng)(%)(%)
2,3,7,8-TCDF 0.20 ND ND 0.19 0.20 97 981.1
2,3,7,8-TCDD 0.20 ND ND 0.21 0.21 103 1030.2
1,2,3,7,8-PeCDF 1.00 ND ND 0.95 1.01 95 1016.1
2,3,4,7,8-PeCDF 1.00 ND ND 1.02 1.01 102 1010.7
1,2,3,7,8-PeCDD 1.00 ND ND 0.85 0.82 85 823.5
1,2,3,4,7,8-HxCDF 1.00 ND ND 1.01 1.04 101 1043.1
1,2,3,6,7,8-HxCDF 1.00 ND ND 1.02 1.07 102 1074.8
2,3,4,6,7,8-HxCDF 1.00 ND ND 1.07 1.01 107 1015.0
1,2,3,7,8,9-HxCDF 1.00 ND ND 1.03 1.07 103 1074.4
1,2,3,4,7,8-HxCDD 1.00 ND ND 0.99 1.00 99 1001.5
1,2,3,6,7,8-HxCDD 1.00 ND ND 0.95 0.92 95 923.1
1,2,3,7,8,9-HxCDD 1.00 ND ND 1.05 1.08 105 1082.5
1,2,3,4,6,7,8-HpCDF 1.00 ND ND 0.99 1.05 99 1055.4
1,2,3,4,7,8,9-HpCDF 1.00 ND ND 1.02 1.01 102 1011.2
1,2,3,4,6,7,8-HpCDD 1.00 ND ND 0.89 0.89 89 890.2
OCDF 2.00 ND ND 1.82 1.87 91 932.7
OCDD 2.00 ND ND 2.06 2.18 103 1095.6
Quantity Spiked - the amount of analyte spiked into the spiked samples
Unspiked Sample Contribution - calculated based on the amount found in the sample and the extracted amounts of the spiked and unspiked samples
Quantity Measured - the total amount of analyte measured in the spiked samples
RPD - the Relative Percent Difference of the spiked sample Quantity Measured values
Subtracted Recovery - calculated after subtracting the unspiked sample contribution
Page 15 of 15Report No.....10659324_SW8290AFC_L2_R1_dfr Revision 1
Page 52 of 52
#=CL#
July 31, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92674238
92674238
Project:
Pace Project No.:
RE:
Christina Ashdown
ENSAFE
313 Wingo Way
Mount Pleasant, SC 29464
PACTIV EVERGREEN-Revised Report
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on June 23, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
This revision was issued on 07/21/23 to include all requested analytes.
This revision was issued on 07/31/23 to include Dioxin/Furan results.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
cc:Phil Coop, ENSAFE Inc.
Travis Darden, ENSAFE Inc.
Lab, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 90
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 90
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Lab ID Sample ID Matrix Date Collected Date Received
92674238001 PZ4WG-062323 Water 06/23/23 08:15 06/23/23 11:25
92674238002 DUP01WG-062323 Water 06/23/23 08:15 06/23/23 11:25
92674238003 RW5WG-062323 Water 06/23/23 10:10 06/23/23 11:25
92674238004 TRIP BLANK Water 06/23/23 11:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 90
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92674238001 PZ4WG-062323 EPA 6010D 16 PASI-ADBB1
EPA 6010D 16 PASI-ADBB1
EPA 7470A 1 PASI-ANMP
EPA 7470A 1 PASI-ANMP
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CCL
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
92674238002 DUP01WG-062323 EPA 6010D 16 PASI-ADBB1
EPA 6010D 16 PASI-ADBB1
EPA 7470A 1 PASI-ANMP
EPA 7470A 1 PASI-ANMP
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CCL
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
92674238003 RW5WG-062323 EPA 6010D 16 PASI-ADBB1
EPA 6010D 16 PASI-ADBB1
EPA 7470A 1 PASI-ANMP
EPA 7470A 1 PASI-ANMP
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CCL
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
92674238004 TRIP BLANK EPA 8260D 52 PASI-CJJK
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:PZ4WG-062323 Lab ID:92674238001 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 06/30/23 15:52 7440-36-0 D306/27/23 11:4725015010
Arsenic 364 ug/L 06/29/23 14:32 7440-38-206/27/23 11:4750.0 23.5 1
Barium 84.8 ug/L 06/29/23 14:32 7440-39-306/27/23 11:4725.0 17.4 1
Beryllium ND ug/L 06/29/23 14:32 7440-41-706/27/23 11:475.0 3.5 1
Boron 266 ug/L 06/29/23 14:32 7440-42-806/27/23 11:472501621
Cadmium ND ug/L 06/29/23 14:32 7440-43-906/27/23 11:475.0 2.0 1
Chromium 166 ug/L 06/29/23 14:32 7440-47-306/27/23 11:4725.0 18.3 1
Cobalt ND ug/L 06/29/23 14:32 7440-48-406/27/23 11:4725.0 18.2 1
Copper ND ug/L 06/29/23 14:32 7440-50-806/27/23 11:4725.0 21.3 1
Lead 37.4 ug/L 06/29/23 14:32 7439-92-106/27/23 11:4725.0 22.7 1
Nickel 207 ug/L 06/29/23 14:32 7440-02-006/27/23 11:4725.0 17.3 1
Selenium ND ug/L 06/29/23 14:32 7782-49-206/27/23 11:4750.0 23.5 1
Silver ND ug/L 06/29/23 14:32 7440-22-406/27/23 11:4725.0 12.5 1
Thallium ND ug/L 06/29/23 14:32 7440-28-006/27/23 11:4750.0 40.7 1
Vanadium 1900 ug/L 06/29/23 14:32 7440-62-206/27/23 11:4725.0 19.7 1
Zinc ND ug/L 06/29/23 14:32 7440-66-606/27/23 11:4750.0 47.3 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 06/30/23 15:58 7440-36-0 D306/25/23 20:1412575.0 25
Arsenic, Dissolved 37.4 ug/L 06/29/23 15:51 7440-38-206/25/23 20:1410.0 4.7 1
Barium, Dissolved 69.1 ug/L 06/29/23 15:51 7440-39-306/25/23 20:145.0 3.5 1
Beryllium, Dissolved ND ug/L 06/29/23 15:51 7440-41-706/25/23 20:141.0 0.70 1
Boron, Dissolved 348 ug/L 06/29/23 15:51 7440-42-806/25/23 20:1450.0 32.4 1
Cadmium, Dissolved 1.1 ug/L 06/29/23 15:51 7440-43-906/25/23 20:141.0 0.40 1
Chromium, Dissolved 43.1 ug/L 06/29/23 15:51 7440-47-306/25/23 20:145.0 3.7 1
Cobalt, Dissolved ND ug/L 06/29/23 15:51 7440-48-406/25/23 20:145.0 3.6 1
Copper, Dissolved ND ug/L 06/29/23 15:51 7440-50-806/25/23 20:145.0 4.3 1
Lead, Dissolved 20.0 ug/L 06/29/23 15:51 7439-92-106/25/23 20:145.0 4.5 1
Nickel, Dissolved 109 ug/L 06/29/23 15:51 7440-02-006/25/23 20:145.0 3.5 1
Selenium, Dissolved 22.0 ug/L 06/29/23 15:51 7782-49-206/25/23 20:1410.0 4.7 1
Silver, Dissolved ND ug/L 06/29/23 15:51 7440-22-406/25/23 20:145.0 2.5 1
Thallium, Dissolved 9.0J ug/L 06/29/23 15:51 7440-28-006/25/23 20:1410.0 8.1 1
Vanadium, Dissolved 1400 ug/L 06/29/23 15:51 7440-62-206/25/23 20:145.0 3.9 1
Zinc, Dissolved ND ug/L 06/29/23 15:51 7440-66-606/25/23 20:1410.0 9.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury 2.6 ug/L 07/13/23 11:10 7439-97-607/12/23 09:140.20 0.12 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury, Dissolved
Mercury, Dissolved 12.7 ug/L 07/14/23 11:49 7439-97-607/13/23 12:141.0 0.61 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:PZ4WG-062323 Lab ID:92674238001 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 06/26/23 21:42 83-32-906/26/23 09:1850.0 10.0 1
Acenaphthylene ND ug/L 06/26/23 21:42 208-96-806/26/23 09:1850.0 9.8 1
Acetophenone ND ug/L 06/26/23 21:42 98-86-206/26/23 09:1850.0 7.5 1
Anthracene ND ug/L 06/26/23 21:42 120-12-706/26/23 09:1850.0 11.6 1
Atrazine ND ug/L 06/26/23 21:42 1912-24-9 L106/26/23 09:1850.0 15.9 1
Benzaldehyde ND ug/L 06/26/23 21:42 100-52-706/26/23 09:1850.0 18.0 1
Benzo(a)anthracene ND ug/L 06/26/23 21:42 56-55-306/26/23 09:1850.0 13.4 1
Benzo(a)pyrene ND ug/L 06/26/23 21:42 50-32-806/26/23 09:1850.0 13.9 1
Benzo(b)fluoranthene ND ug/L 06/26/23 21:42 205-99-206/26/23 09:1850.0 13.0 1
Benzo(g,h,i)perylene ND ug/L 06/26/23 21:42 191-24-206/26/23 09:1850.0 14.2 1
Benzo(k)fluoranthene ND ug/L 06/26/23 21:42 207-08-906/26/23 09:1850.0 13.6 1
Biphenyl (Diphenyl)ND ug/L 06/26/23 21:42 92-52-406/26/23 09:1850.0 9.1 1
4-Bromophenylphenyl ether ND ug/L 06/26/23 21:42 101-55-306/26/23 09:1850.0 8.8 1
Butylbenzylphthalate ND ug/L 06/26/23 21:42 85-68-706/26/23 09:1850.0 15.7 1
Caprolactam ND ug/L 06/26/23 21:42 105-60-206/26/23 09:1850.0 34.7 1
Carbazole ND ug/L 06/26/23 21:42 86-74-806/26/23 09:1850.0 11.8 1
4-Chloro-3-methylphenol ND ug/L 06/26/23 21:42 59-50-706/26/23 09:1850.0 16.7 1
4-Chloroaniline ND ug/L 06/26/23 21:42 106-47-806/26/23 09:1810018.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/26/23 21:42 111-91-106/26/23 09:1850.0 9.1 1
bis(2-Chloroethyl) ether ND ug/L 06/26/23 21:42 111-44-406/26/23 09:1850.0 9.6 1
2-Chloronaphthalene ND ug/L 06/26/23 21:42 91-58-706/26/23 09:1850.0 8.6 1
2-Chlorophenol ND ug/L 06/26/23 21:42 95-57-806/26/23 09:1850.0 6.0 1
4-Chlorophenylphenyl ether ND ug/L 06/26/23 21:42 7005-72-306/26/23 09:1850.0 10.0 1
Chrysene ND ug/L 06/26/23 21:42 218-01-906/26/23 09:1850.0 13.8 1
Dibenz(a,h)anthracene ND ug/L 06/26/23 21:42 53-70-306/26/23 09:1850.0 14.8 1
Dibenzofuran ND ug/L 06/26/23 21:42 132-64-906/26/23 09:1850.0 10.5 1
3,3'-Dichlorobenzidine ND ug/L 06/26/23 21:42 91-94-106/26/23 09:1810040.6 1
2,4-Dichlorophenol ND ug/L 06/26/23 21:42 120-83-206/26/23 09:1850.0 7.0 1
Diethylphthalate ND ug/L 06/26/23 21:42 84-66-206/26/23 09:1850.0 10.2 1
2,4-Dimethylphenol ND ug/L 06/26/23 21:42 105-67-9 L106/26/23 09:1850.0 8.5 1
Dimethylphthalate ND ug/L 06/26/23 21:42 131-11-306/26/23 09:1850.0 10.6 1
Di-n-butylphthalate ND ug/L 06/26/23 21:42 84-74-206/26/23 09:1850.0 11.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/26/23 21:42 534-52-1 L2,v106/26/23 09:1810038.9 1
2,4-Dinitrophenol ND ug/L 06/26/23 21:42 51-28-506/26/23 09:182501301
2,4-Dinitrotoluene ND ug/L 06/26/23 21:42 121-14-206/26/23 09:1850.0 8.1 1
2,6-Dinitrotoluene ND ug/L 06/26/23 21:42 606-20-206/26/23 09:1850.0 8.6 1
Di-n-octylphthalate ND ug/L 06/26/23 21:42 117-84-006/26/23 09:1850.0 19.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/26/23 21:42 117-81-706/26/23 09:1830.0 18.6 1
Fluoranthene ND ug/L 06/26/23 21:42 206-44-006/26/23 09:1850.0 11.0 1
Fluorene ND ug/L 06/26/23 21:42 86-73-706/26/23 09:1850.0 10.4 1
Hexachloro-1,3-butadiene ND ug/L 06/26/23 21:42 87-68-306/26/23 09:1850.0 8.8 1
Hexachlorobenzene ND ug/L 06/26/23 21:42 118-74-106/26/23 09:1850.0 10.8 1
Hexachlorocyclopentadiene ND ug/L 06/26/23 21:42 77-47-406/26/23 09:1850.0 8.0 1
Hexachloroethane ND ug/L 06/26/23 21:42 67-72-106/26/23 09:1850.0 6.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/26/23 21:42 193-39-506/26/23 09:1850.0 14.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 6 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:PZ4WG-062323 Lab ID:92674238001 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 06/26/23 21:42 78-59-106/26/23 09:1850.0 8.3 1
2-Methylnaphthalene ND ug/L 06/26/23 21:42 91-57-606/26/23 09:1850.0 9.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/26/23 21:42 95-48-706/26/23 09:1850.0 9.4 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/26/23 21:42 15831-10-406/26/23 09:1850.0 6.1 1
Naphthalene ND ug/L 06/26/23 21:42 91-20-306/26/23 09:1850.0 10.4 1
2-Nitroaniline ND ug/L 06/26/23 21:42 88-74-406/26/23 09:1810014.9 1
3-Nitroaniline ND ug/L 06/26/23 21:42 99-09-206/26/23 09:1810018.8 1
4-Nitroaniline ND ug/L 06/26/23 21:42 100-01-606/26/23 09:1810025.5 1
Nitrobenzene ND ug/L 06/26/23 21:42 98-95-306/26/23 09:1850.0 9.4 1
2-Nitrophenol ND ug/L 06/26/23 21:42 88-75-506/26/23 09:1850.0 7.0 1
4-Nitrophenol ND ug/L 06/26/23 21:42 100-02-7 L206/26/23 09:1825033.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/26/23 21:42 621-64-706/26/23 09:1850.0 6.6 1
N-Nitrosodiphenylamine ND ug/L 06/26/23 21:42 86-30-606/26/23 09:1850.0 15.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/26/23 21:42 108-60-106/26/23 09:1850.0 5.8 1
Pentachlorophenol ND ug/L 06/26/23 21:42 87-86-506/26/23 09:1810018.8 1
Phenanthrene ND ug/L 06/26/23 21:42 85-01-806/26/23 09:1850.0 10.0 1
Phenol ND ug/L 06/26/23 21:42 108-95-206/26/23 09:1850.0 6.8 1
Pyrene ND ug/L 06/26/23 21:42 129-00-006/26/23 09:1850.0 11.0 1
2,4,5-Trichlorophenol ND ug/L 06/26/23 21:42 95-95-406/26/23 09:1850.0 7.1 1
2,4,6-Trichlorophenol ND ug/L 06/26/23 21:42 88-06-206/26/23 09:1850.0 7.8 1
Surrogates
Nitrobenzene-d5 (S)43 %06/26/23 21:42 4165-60-006/26/23 09:1810-138 1
2-Fluorobiphenyl (S)20 %06/26/23 21:42 321-60-806/26/23 09:1810-130 1
Terphenyl-d14 (S)32 %06/26/23 21:42 1718-51-006/26/23 09:1819-191 1
Phenol-d6 (S)18 %06/26/23 21:42 13127-88-306/26/23 09:1810-130 1
2-Fluorophenol (S)20 %06/26/23 21:42 367-12-406/26/23 09:1810-130 1
2,4,6-Tribromophenol (S)18 %06/26/23 21:42 118-79-606/26/23 09:1810-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 47.3 ug/L 06/30/23 13:35 67-64-125.0 5.1 1
Benzene 0.41J ug/L 06/30/23 13:35 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 06/30/23 13:35 75-27-41.0 0.31 1
Bromoform ND ug/L 06/30/23 13:35 75-25-2 v21.0 0.34 1
Bromomethane ND ug/L 06/30/23 13:35 74-83-92.0 1.7 1
2-Butanone (MEK)5.4 ug/L 06/30/23 13:35 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 06/30/23 13:35 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 06/30/23 13:35 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 06/30/23 13:35 108-90-71.0 0.28 1
Chloroethane ND ug/L 06/30/23 13:35 75-00-31.0 0.65 1
Chloroform ND ug/L 06/30/23 13:35 67-66-31.0 0.43 1
Chloromethane ND ug/L 06/30/23 13:35 74-87-31.0 0.54 1
Cyclohexane ND ug/L 06/30/23 13:35 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 06/30/23 13:35 96-12-8 v22.0 0.34 1
Dibromochloromethane ND ug/L 06/30/23 13:35 124-48-11.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:PZ4WG-062323 Lab ID:92674238001 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 06/30/23 13:35 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 06/30/23 13:35 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 06/30/23 13:35 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 06/30/23 13:35 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 06/30/23 13:35 75-71-8 v11.0 0.35 1
1,1-Dichloroethane ND ug/L 06/30/23 13:35 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 06/30/23 13:35 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 06/30/23 13:35 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 06/30/23 13:35 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 06/30/23 13:35 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 06/30/23 13:35 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 06/30/23 13:35 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 06/30/23 13:35 10061-02-61.0 0.36 1
Ethylbenzene 1.7 ug/L 06/30/23 13:35 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/30/23 13:35 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 06/30/23 13:35 98-82-81.0 0.33 1
Methyl acetate ND ug/L 06/30/23 13:35 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 06/30/23 13:35 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 06/30/23 13:35 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/30/23 13:35 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 06/30/23 13:35 1634-04-41.0 0.42 1
Styrene ND ug/L 06/30/23 13:35 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 06/30/23 13:35 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/30/23 13:35 127-18-41.0 0.29 1
Toluene 1.1 ug/L 06/30/23 13:35 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 06/30/23 13:35 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 06/30/23 13:35 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 06/30/23 13:35 79-00-51.0 0.32 1
Trichloroethene ND ug/L 06/30/23 13:35 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 06/30/23 13:35 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 06/30/23 13:35 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 06/30/23 13:35 75-01-41.0 0.39 1
m&p-Xylene 6.0 ug/L 06/30/23 13:35 179601-23-12.0 0.71 1
o-Xylene 2.8 ug/L 06/30/23 13:35 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)101 %06/30/23 13:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)116 %06/30/23 13:35 17060-07-070-130 1
Toluene-d8 (S)100 %06/30/23 13:35 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 5450 mg/L 07/06/23 17:295.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:PZ4WG-062323 Lab ID:92674238001 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 13.0 mg/L 06/27/23 04:56 18496-25-82.5 0.55 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:DUP01WG-062323 Lab ID:92674238002 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 06/30/23 15:55 7440-36-0 D306/27/23 11:4725015010
Arsenic 289 ug/L 06/29/23 14:35 7440-38-206/27/23 11:4750.0 23.5 1
Barium 86.6 ug/L 06/29/23 14:35 7440-39-306/27/23 11:4725.0 17.4 1
Beryllium ND ug/L 06/29/23 14:35 7440-41-706/27/23 11:475.0 3.5 1
Boron 244J ug/L 06/29/23 14:35 7440-42-806/27/23 11:472501621
Cadmium ND ug/L 06/29/23 14:35 7440-43-906/27/23 11:475.0 2.0 1
Chromium 189 ug/L 06/29/23 14:35 7440-47-306/27/23 11:4725.0 18.3 1
Cobalt ND ug/L 06/29/23 14:35 7440-48-406/27/23 11:4725.0 18.2 1
Copper ND ug/L 06/29/23 14:35 7440-50-806/27/23 11:4725.0 21.3 1
Lead 34.3 ug/L 06/29/23 14:35 7439-92-106/27/23 11:4725.0 22.7 1
Nickel 194 ug/L 06/29/23 14:35 7440-02-006/27/23 11:4725.0 17.3 1
Selenium ND ug/L 06/29/23 14:35 7782-49-206/27/23 11:4750.0 23.5 1
Silver ND ug/L 06/29/23 14:35 7440-22-406/27/23 11:4725.0 12.5 1
Thallium ND ug/L 06/29/23 14:35 7440-28-006/27/23 11:4750.0 40.7 1
Vanadium 1840 ug/L 06/29/23 14:35 7440-62-206/27/23 11:4725.0 19.7 1
Zinc ND ug/L 06/29/23 14:35 7440-66-606/27/23 11:4750.0 47.3 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 06/30/23 15:46 7440-36-0 D3,P406/26/23 20:3362537525
Arsenic, Dissolved 119 ug/L 06/29/23 16:17 7440-38-206/26/23 20:3350.0 23.5 1
Barium, Dissolved 66.2 ug/L 06/29/23 16:17 7440-39-306/26/23 20:3325.0 17.4 1
Beryllium, Dissolved ND ug/L 06/29/23 16:17 7440-41-706/26/23 20:335.0 3.5 1
Boron, Dissolved 355 ug/L 06/29/23 16:17 7440-42-806/26/23 20:332501621
Cadmium, Dissolved ND ug/L 06/29/23 16:17 7440-43-906/26/23 20:335.0 2.0 1
Chromium, Dissolved 47.3 ug/L 06/29/23 16:17 7440-47-306/26/23 20:3325.0 18.3 1
Cobalt, Dissolved ND ug/L 06/29/23 16:17 7440-48-406/26/23 20:3325.0 18.2 1
Copper, Dissolved ND ug/L 06/29/23 16:17 7440-50-806/26/23 20:3325.0 21.3 1
Lead, Dissolved 26.4 ug/L 06/29/23 16:17 7439-92-106/26/23 20:3325.0 22.7 1
Nickel, Dissolved 134 ug/L 06/29/23 16:17 7440-02-006/26/23 20:3325.0 17.3 1
Selenium, Dissolved ND ug/L 06/29/23 16:17 7782-49-206/26/23 20:3350.0 23.5 1
Silver, Dissolved ND ug/L 06/29/23 16:17 7440-22-406/26/23 20:3325.0 12.5 1
Thallium, Dissolved ND ug/L 06/29/23 16:17 7440-28-006/26/23 20:3350.0 40.7 1
Vanadium, Dissolved 1320 ug/L 06/29/23 16:17 7440-62-206/26/23 20:3325.0 19.7 1
Zinc, Dissolved ND ug/L 06/29/23 16:17 7440-66-606/26/23 20:3350.0 47.3 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury 2.2 ug/L 07/13/23 11:17 7439-97-607/12/23 09:140.20 0.12 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury, Dissolved
Mercury, Dissolved 4.4 ug/L 07/14/23 11:37 7439-97-607/13/23 12:140.20 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:DUP01WG-062323 Lab ID:92674238002 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 06/26/23 22:08 83-32-906/26/23 09:1850.0 10.0 1
Acenaphthylene ND ug/L 06/26/23 22:08 208-96-806/26/23 09:1850.0 9.8 1
Acetophenone ND ug/L 06/26/23 22:08 98-86-206/26/23 09:1850.0 7.5 1
Anthracene ND ug/L 06/26/23 22:08 120-12-706/26/23 09:1850.0 11.6 1
Atrazine ND ug/L 06/26/23 22:08 1912-24-9 L106/26/23 09:1850.0 15.9 1
Benzaldehyde ND ug/L 06/26/23 22:08 100-52-706/26/23 09:1850.0 18.0 1
Benzo(a)anthracene ND ug/L 06/26/23 22:08 56-55-306/26/23 09:1850.0 13.4 1
Benzo(a)pyrene ND ug/L 06/26/23 22:08 50-32-806/26/23 09:1850.0 13.9 1
Benzo(b)fluoranthene ND ug/L 06/26/23 22:08 205-99-206/26/23 09:1850.0 13.0 1
Benzo(g,h,i)perylene ND ug/L 06/26/23 22:08 191-24-206/26/23 09:1850.0 14.2 1
Benzo(k)fluoranthene ND ug/L 06/26/23 22:08 207-08-906/26/23 09:1850.0 13.6 1
Biphenyl (Diphenyl)ND ug/L 06/26/23 22:08 92-52-406/26/23 09:1850.0 9.1 1
4-Bromophenylphenyl ether ND ug/L 06/26/23 22:08 101-55-306/26/23 09:1850.0 8.8 1
Butylbenzylphthalate ND ug/L 06/26/23 22:08 85-68-706/26/23 09:1850.0 15.7 1
Caprolactam ND ug/L 06/26/23 22:08 105-60-206/26/23 09:1850.0 34.7 1
Carbazole ND ug/L 06/26/23 22:08 86-74-806/26/23 09:1850.0 11.8 1
4-Chloro-3-methylphenol ND ug/L 06/26/23 22:08 59-50-706/26/23 09:1850.0 16.7 1
4-Chloroaniline ND ug/L 06/26/23 22:08 106-47-806/26/23 09:1810018.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/26/23 22:08 111-91-106/26/23 09:1850.0 9.1 1
bis(2-Chloroethyl) ether ND ug/L 06/26/23 22:08 111-44-406/26/23 09:1850.0 9.6 1
2-Chloronaphthalene ND ug/L 06/26/23 22:08 91-58-706/26/23 09:1850.0 8.6 1
2-Chlorophenol ND ug/L 06/26/23 22:08 95-57-806/26/23 09:1850.0 6.0 1
4-Chlorophenylphenyl ether ND ug/L 06/26/23 22:08 7005-72-306/26/23 09:1850.0 10.0 1
Chrysene ND ug/L 06/26/23 22:08 218-01-906/26/23 09:1850.0 13.8 1
Dibenz(a,h)anthracene ND ug/L 06/26/23 22:08 53-70-306/26/23 09:1850.0 14.8 1
Dibenzofuran ND ug/L 06/26/23 22:08 132-64-906/26/23 09:1850.0 10.5 1
3,3'-Dichlorobenzidine ND ug/L 06/26/23 22:08 91-94-106/26/23 09:1810040.6 1
2,4-Dichlorophenol ND ug/L 06/26/23 22:08 120-83-206/26/23 09:1850.0 7.0 1
Diethylphthalate ND ug/L 06/26/23 22:08 84-66-206/26/23 09:1850.0 10.2 1
2,4-Dimethylphenol ND ug/L 06/26/23 22:08 105-67-9 L106/26/23 09:1850.0 8.5 1
Dimethylphthalate ND ug/L 06/26/23 22:08 131-11-306/26/23 09:1850.0 10.6 1
Di-n-butylphthalate ND ug/L 06/26/23 22:08 84-74-206/26/23 09:1850.0 11.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/26/23 22:08 534-52-1 L2,v106/26/23 09:1810038.9 1
2,4-Dinitrophenol ND ug/L 06/26/23 22:08 51-28-506/26/23 09:182501301
2,4-Dinitrotoluene ND ug/L 06/26/23 22:08 121-14-206/26/23 09:1850.0 8.1 1
2,6-Dinitrotoluene ND ug/L 06/26/23 22:08 606-20-206/26/23 09:1850.0 8.6 1
Di-n-octylphthalate ND ug/L 06/26/23 22:08 117-84-006/26/23 09:1850.0 19.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/26/23 22:08 117-81-706/26/23 09:1830.0 18.6 1
Fluoranthene ND ug/L 06/26/23 22:08 206-44-006/26/23 09:1850.0 11.0 1
Fluorene ND ug/L 06/26/23 22:08 86-73-706/26/23 09:1850.0 10.4 1
Hexachloro-1,3-butadiene ND ug/L 06/26/23 22:08 87-68-306/26/23 09:1850.0 8.8 1
Hexachlorobenzene ND ug/L 06/26/23 22:08 118-74-106/26/23 09:1850.0 10.8 1
Hexachlorocyclopentadiene ND ug/L 06/26/23 22:08 77-47-406/26/23 09:1850.0 8.0 1
Hexachloroethane ND ug/L 06/26/23 22:08 67-72-106/26/23 09:1850.0 6.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/26/23 22:08 193-39-506/26/23 09:1850.0 14.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:DUP01WG-062323 Lab ID:92674238002 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 06/26/23 22:08 78-59-106/26/23 09:1850.0 8.3 1
2-Methylnaphthalene ND ug/L 06/26/23 22:08 91-57-606/26/23 09:1850.0 9.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/26/23 22:08 95-48-706/26/23 09:1850.0 9.4 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/26/23 22:08 15831-10-406/26/23 09:1850.0 6.1 1
Naphthalene ND ug/L 06/26/23 22:08 91-20-306/26/23 09:1850.0 10.4 1
2-Nitroaniline ND ug/L 06/26/23 22:08 88-74-406/26/23 09:1810014.9 1
3-Nitroaniline ND ug/L 06/26/23 22:08 99-09-206/26/23 09:1810018.8 1
4-Nitroaniline ND ug/L 06/26/23 22:08 100-01-606/26/23 09:1810025.5 1
Nitrobenzene ND ug/L 06/26/23 22:08 98-95-306/26/23 09:1850.0 9.4 1
2-Nitrophenol ND ug/L 06/26/23 22:08 88-75-506/26/23 09:1850.0 7.0 1
4-Nitrophenol ND ug/L 06/26/23 22:08 100-02-7 L206/26/23 09:1825033.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/26/23 22:08 621-64-706/26/23 09:1850.0 6.6 1
N-Nitrosodiphenylamine ND ug/L 06/26/23 22:08 86-30-606/26/23 09:1850.0 15.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/26/23 22:08 108-60-106/26/23 09:1850.0 5.8 1
Pentachlorophenol ND ug/L 06/26/23 22:08 87-86-506/26/23 09:1810018.8 1
Phenanthrene ND ug/L 06/26/23 22:08 85-01-806/26/23 09:1850.0 10.0 1
Phenol ND ug/L 06/26/23 22:08 108-95-206/26/23 09:1850.0 6.8 1
Pyrene ND ug/L 06/26/23 22:08 129-00-006/26/23 09:1850.0 11.0 1
2,4,5-Trichlorophenol ND ug/L 06/26/23 22:08 95-95-406/26/23 09:1850.0 7.1 1
2,4,6-Trichlorophenol ND ug/L 06/26/23 22:08 88-06-206/26/23 09:1850.0 7.8 1
Surrogates
Nitrobenzene-d5 (S)69 %06/26/23 22:08 4165-60-006/26/23 09:1810-138 1
2-Fluorobiphenyl (S)48 %06/26/23 22:08 321-60-806/26/23 09:1810-130 1
Terphenyl-d14 (S)83 %06/26/23 22:08 1718-51-006/26/23 09:1819-191 1
Phenol-d6 (S)11 %06/26/23 22:08 13127-88-306/26/23 09:1810-130 1
2-Fluorophenol (S)5 %06/26/23 22:08 367-12-4 S006/26/23 09:1810-130 1
2,4,6-Tribromophenol (S)14 %06/26/23 22:08 118-79-606/26/23 09:1810-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 45.5 ug/L 06/30/23 13:54 67-64-125.0 5.1 1
Benzene 0.41J ug/L 06/30/23 13:54 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 06/30/23 13:54 75-27-41.0 0.31 1
Bromoform ND ug/L 06/30/23 13:54 75-25-2 v21.0 0.34 1
Bromomethane ND ug/L 06/30/23 13:54 74-83-92.0 1.7 1
2-Butanone (MEK)5.5 ug/L 06/30/23 13:54 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 06/30/23 13:54 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 06/30/23 13:54 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 06/30/23 13:54 108-90-71.0 0.28 1
Chloroethane ND ug/L 06/30/23 13:54 75-00-31.0 0.65 1
Chloroform ND ug/L 06/30/23 13:54 67-66-31.0 0.43 1
Chloromethane ND ug/L 06/30/23 13:54 74-87-31.0 0.54 1
Cyclohexane ND ug/L 06/30/23 13:54 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 06/30/23 13:54 96-12-8 v22.0 0.34 1
Dibromochloromethane ND ug/L 06/30/23 13:54 124-48-11.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:DUP01WG-062323 Lab ID:92674238002 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 06/30/23 13:54 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 06/30/23 13:54 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 06/30/23 13:54 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 06/30/23 13:54 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 06/30/23 13:54 75-71-8 v11.0 0.35 1
1,1-Dichloroethane ND ug/L 06/30/23 13:54 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 06/30/23 13:54 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 06/30/23 13:54 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 06/30/23 13:54 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 06/30/23 13:54 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 06/30/23 13:54 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 06/30/23 13:54 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 06/30/23 13:54 10061-02-61.0 0.36 1
Ethylbenzene 1.7 ug/L 06/30/23 13:54 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/30/23 13:54 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 06/30/23 13:54 98-82-81.0 0.33 1
Methyl acetate ND ug/L 06/30/23 13:54 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 06/30/23 13:54 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 06/30/23 13:54 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/30/23 13:54 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 06/30/23 13:54 1634-04-41.0 0.42 1
Styrene ND ug/L 06/30/23 13:54 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 06/30/23 13:54 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/30/23 13:54 127-18-41.0 0.29 1
Toluene 1.0 ug/L 06/30/23 13:54 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 06/30/23 13:54 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 06/30/23 13:54 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 06/30/23 13:54 79-00-51.0 0.32 1
Trichloroethene ND ug/L 06/30/23 13:54 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 06/30/23 13:54 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 06/30/23 13:54 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 06/30/23 13:54 75-01-41.0 0.39 1
m&p-Xylene 6.1 ug/L 06/30/23 13:54 179601-23-12.0 0.71 1
o-Xylene 2.6 ug/L 06/30/23 13:54 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)101 %06/30/23 13:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %06/30/23 13:54 17060-07-070-130 1
Toluene-d8 (S)100 %06/30/23 13:54 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 4940 mg/L 07/06/23 17:295.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:DUP01WG-062323 Lab ID:92674238002 Collected:06/23/23 08:15 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 51.0 mg/L 06/27/23 05:03 18496-25-810.0 2.2 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:RW5WG-062323 Lab ID:92674238003 Collected:06/23/23 10:10 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 06/29/23 14:38 7440-36-006/27/23 11:4725.0 15.0 1
Arsenic 794 ug/L 06/29/23 14:38 7440-38-206/27/23 11:4750.0 23.5 1
Barium 351 ug/L 06/29/23 14:38 7440-39-306/27/23 11:4725.0 17.4 1
Beryllium ND ug/L 06/29/23 14:38 7440-41-706/27/23 11:475.0 3.5 1
Boron 4310 ug/L 06/29/23 14:38 7440-42-806/27/23 11:472501621
Cadmium 16.1 ug/L 06/29/23 14:38 7440-43-906/27/23 11:475.0 2.0 1
Chromium 183 ug/L 06/29/23 14:38 7440-47-306/27/23 11:4725.0 18.3 1
Cobalt ND ug/L 06/29/23 14:38 7440-48-406/27/23 11:4725.0 18.2 1
Copper 35.8 ug/L 06/29/23 14:38 7440-50-806/27/23 11:4725.0 21.3 1
Lead 221 ug/L 06/29/23 14:38 7439-92-106/27/23 11:4725.0 22.7 1
Nickel 404 ug/L 06/29/23 14:38 7440-02-006/27/23 11:4725.0 17.3 1
Selenium 122 ug/L 06/29/23 14:38 7782-49-206/27/23 11:4750.0 23.5 1
Silver ND ug/L 06/29/23 14:38 7440-22-406/27/23 11:4725.0 12.5 1
Thallium ND ug/L 06/29/23 14:38 7440-28-006/27/23 11:4750.0 40.7 1
Vanadium 1900 ug/L 06/29/23 14:38 7440-62-206/27/23 11:4725.0 19.7 1
Zinc 810 ug/L 06/29/23 14:38 7440-66-606/27/23 11:4750.0 47.3 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 06/30/23 15:49 7440-36-0 D3,P406/26/23 20:3362537525
Arsenic, Dissolved 550 ug/L 06/29/23 16:20 7440-38-2 P406/26/23 20:3350.0 23.5 1
Barium, Dissolved 179 ug/L 06/29/23 16:20 7440-39-3 P406/26/23 20:3325.0 17.4 1
Beryllium, Dissolved ND ug/L 06/29/23 16:20 7440-41-7 P406/26/23 20:335.0 3.5 1
Boron, Dissolved 2980 ug/L 06/29/23 16:20 7440-42-8 P406/26/23 20:332501621
Cadmium, Dissolved ND ug/L 06/29/23 16:20 7440-43-9 P406/26/23 20:335.0 2.0 1
Chromium, Dissolved 81.3 ug/L 06/29/23 16:20 7440-47-3 P406/26/23 20:3325.0 18.3 1
Cobalt, Dissolved ND ug/L 06/29/23 16:20 7440-48-4 P406/26/23 20:3325.0 18.2 1
Copper, Dissolved ND ug/L 06/29/23 16:20 7440-50-8 P406/26/23 20:3325.0 21.3 1
Lead, Dissolved 34.8 ug/L 06/29/23 16:20 7439-92-1 P406/26/23 20:3325.0 22.7 1
Nickel, Dissolved 138 ug/L 06/29/23 16:20 7440-02-0 P406/26/23 20:3325.0 17.3 1
Selenium, Dissolved ND ug/L 06/29/23 16:20 7782-49-2 P406/26/23 20:3350.0 23.5 1
Silver, Dissolved ND ug/L 06/29/23 16:20 7440-22-4 P406/26/23 20:3325.0 12.5 1
Thallium, Dissolved ND ug/L 06/29/23 16:20 7440-28-0 P406/26/23 20:3350.0 40.7 1
Vanadium, Dissolved 1300 ug/L 06/29/23 16:20 7440-62-2 P406/26/23 20:3325.0 19.7 1
Zinc, Dissolved ND ug/L 06/29/23 16:20 7440-66-6 P406/26/23 20:3350.0 47.3 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury 0.21 ug/L 07/13/23 11:19 7439-97-607/12/23 09:140.20 0.12 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury, Dissolved
Mercury, Dissolved 0.20J ug/L 07/14/23 11:40 7439-97-607/13/23 12:140.20 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:RW5WG-062323 Lab ID:92674238003 Collected:06/23/23 10:10 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 07/01/23 20:15 83-32-906/29/23 12:2150.0 10.0 1
Acenaphthylene ND ug/L 07/01/23 20:15 208-96-806/29/23 12:2150.0 9.8 1
Acetophenone ND ug/L 07/01/23 20:15 98-86-206/29/23 12:2150.0 7.5 1
Anthracene ND ug/L 07/01/23 20:15 120-12-706/29/23 12:2150.0 11.6 1
Atrazine ND ug/L 07/01/23 20:15 1912-24-906/29/23 12:2150.0 15.9 1
Benzaldehyde ND ug/L 07/01/23 20:15 100-52-706/29/23 12:2150.0 18.0 1
Benzo(a)anthracene ND ug/L 07/01/23 20:15 56-55-306/29/23 12:2150.0 13.4 1
Benzo(a)pyrene ND ug/L 07/01/23 20:15 50-32-806/29/23 12:2150.0 13.9 1
Benzo(b)fluoranthene ND ug/L 07/01/23 20:15 205-99-206/29/23 12:2150.0 13.0 1
Benzo(g,h,i)perylene ND ug/L 07/01/23 20:15 191-24-206/29/23 12:2150.0 14.2 1
Benzo(k)fluoranthene ND ug/L 07/01/23 20:15 207-08-906/29/23 12:2150.0 13.6 1
Biphenyl (Diphenyl)ND ug/L 07/01/23 20:15 92-52-406/29/23 12:2150.0 9.1 1
4-Bromophenylphenyl ether ND ug/L 07/01/23 20:15 101-55-306/29/23 12:2150.0 8.8 1
Butylbenzylphthalate ND ug/L 07/01/23 20:15 85-68-706/29/23 12:2150.0 15.7 1
Caprolactam ND ug/L 07/01/23 20:15 105-60-206/29/23 12:2150.0 34.7 1
Carbazole ND ug/L 07/01/23 20:15 86-74-806/29/23 12:2150.0 11.8 1
4-Chloro-3-methylphenol ND ug/L 07/01/23 20:15 59-50-706/29/23 12:2150.0 16.7 1
4-Chloroaniline ND ug/L 07/01/23 20:15 106-47-806/29/23 12:2110018.2 1
bis(2-Chloroethoxy)methane ND ug/L 07/01/23 20:15 111-91-106/29/23 12:2150.0 9.1 1
bis(2-Chloroethyl) ether ND ug/L 07/01/23 20:15 111-44-406/29/23 12:2150.0 9.6 1
2-Chloronaphthalene ND ug/L 07/01/23 20:15 91-58-706/29/23 12:2150.0 8.6 1
2-Chlorophenol ND ug/L 07/01/23 20:15 95-57-806/29/23 12:2150.0 6.0 1
4-Chlorophenylphenyl ether ND ug/L 07/01/23 20:15 7005-72-306/29/23 12:2150.0 10.0 1
Chrysene ND ug/L 07/01/23 20:15 218-01-906/29/23 12:2150.0 13.8 1
Dibenz(a,h)anthracene ND ug/L 07/01/23 20:15 53-70-306/29/23 12:2150.0 14.8 1
Dibenzofuran ND ug/L 07/01/23 20:15 132-64-906/29/23 12:2150.0 10.5 1
3,3'-Dichlorobenzidine ND ug/L 07/01/23 20:15 91-94-106/29/23 12:2110040.6 1
2,4-Dichlorophenol ND ug/L 07/01/23 20:15 120-83-206/29/23 12:2150.0 7.0 1
Diethylphthalate ND ug/L 07/01/23 20:15 84-66-206/29/23 12:2150.0 10.2 1
2,4-Dimethylphenol ND ug/L 07/01/23 20:15 105-67-9 v106/29/23 12:2150.0 8.5 1
Dimethylphthalate ND ug/L 07/01/23 20:15 131-11-306/29/23 12:2150.0 10.6 1
Di-n-butylphthalate ND ug/L 07/01/23 20:15 84-74-206/29/23 12:2150.0 11.0 1
4,6-Dinitro-2-methylphenol ND ug/L 07/01/23 20:15 534-52-106/29/23 12:2110038.9 1
2,4-Dinitrophenol ND ug/L 07/01/23 20:15 51-28-506/29/23 12:212501301
2,4-Dinitrotoluene ND ug/L 07/01/23 20:15 121-14-206/29/23 12:2150.0 8.1 1
2,6-Dinitrotoluene ND ug/L 07/01/23 20:15 606-20-206/29/23 12:2150.0 8.6 1
Di-n-octylphthalate ND ug/L 07/01/23 20:15 117-84-006/29/23 12:2150.0 19.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/01/23 20:15 117-81-706/29/23 12:2130.0 18.6 1
Fluoranthene ND ug/L 07/01/23 20:15 206-44-006/29/23 12:2150.0 11.0 1
Fluorene ND ug/L 07/01/23 20:15 86-73-706/29/23 12:2150.0 10.4 1
Hexachloro-1,3-butadiene ND ug/L 07/01/23 20:15 87-68-306/29/23 12:2150.0 8.8 1
Hexachlorobenzene ND ug/L 07/01/23 20:15 118-74-106/29/23 12:2150.0 10.8 1
Hexachlorocyclopentadiene ND ug/L 07/01/23 20:15 77-47-406/29/23 12:2150.0 8.0 1
Hexachloroethane ND ug/L 07/01/23 20:15 67-72-106/29/23 12:2150.0 6.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/01/23 20:15 193-39-506/29/23 12:2150.0 14.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:RW5WG-062323 Lab ID:92674238003 Collected:06/23/23 10:10 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 07/01/23 20:15 78-59-106/29/23 12:2150.0 8.3 1
2-Methylnaphthalene ND ug/L 07/01/23 20:15 91-57-606/29/23 12:2150.0 9.4 1
2-Methylphenol(o-Cresol)ND ug/L 07/01/23 20:15 95-48-706/29/23 12:2150.0 9.4 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/01/23 20:15 15831-10-406/29/23 12:2150.0 6.1 1
Naphthalene 92.4 ug/L 07/01/23 20:15 91-20-306/29/23 12:2150.0 10.4 1
2-Nitroaniline ND ug/L 07/01/23 20:15 88-74-406/29/23 12:2110014.9 1
3-Nitroaniline ND ug/L 07/01/23 20:15 99-09-206/29/23 12:2110018.8 1
4-Nitroaniline ND ug/L 07/01/23 20:15 100-01-606/29/23 12:2110025.5 1
Nitrobenzene ND ug/L 07/01/23 20:15 98-95-306/29/23 12:2150.0 9.4 1
2-Nitrophenol ND ug/L 07/01/23 20:15 88-75-506/29/23 12:2150.0 7.0 1
4-Nitrophenol ND ug/L 07/01/23 20:15 100-02-706/29/23 12:2125033.0 1
N-Nitroso-di-n-propylamine ND ug/L 07/01/23 20:15 621-64-706/29/23 12:2150.0 6.6 1
N-Nitrosodiphenylamine ND ug/L 07/01/23 20:15 86-30-606/29/23 12:2150.0 15.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/01/23 20:15 108-60-106/29/23 12:2150.0 5.8 1
Pentachlorophenol ND ug/L 07/01/23 20:15 87-86-506/29/23 12:2110018.8 1
Phenanthrene ND ug/L 07/01/23 20:15 85-01-806/29/23 12:2150.0 10.0 1
Phenol 7.4J ug/L 07/01/23 20:15 108-95-206/29/23 12:2150.0 6.8 1
Pyrene ND ug/L 07/01/23 20:15 129-00-006/29/23 12:2150.0 11.0 1
2,4,5-Trichlorophenol ND ug/L 07/01/23 20:15 95-95-406/29/23 12:2150.0 7.1 1
2,4,6-Trichlorophenol ND ug/L 07/01/23 20:15 88-06-206/29/23 12:2150.0 7.8 1
Surrogates
Nitrobenzene-d5 (S)68 %07/01/23 20:15 4165-60-006/29/23 12:2110-138 1
2-Fluorobiphenyl (S)60 %07/01/23 20:15 321-60-806/29/23 12:2110-130 1
Terphenyl-d14 (S)101 %07/01/23 20:15 1718-51-006/29/23 12:2119-191 1
Phenol-d6 (S)41 %07/01/23 20:15 13127-88-306/29/23 12:2110-130 1
2-Fluorophenol (S)47 %07/01/23 20:15 367-12-406/29/23 12:2110-130 1
2,4,6-Tribromophenol (S)92 %07/01/23 20:15 118-79-606/29/23 12:2110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 92.7 ug/L 06/29/23 21:18 67-64-150.0 10.2 2
Benzene 1.5J ug/L 06/29/23 21:18 71-43-22.0 0.69 2
Bromodichloromethane ND ug/L 06/29/23 21:18 75-27-42.0 0.61 2
Bromoform ND ug/L 06/29/23 21:18 75-25-2 v22.0 0.68 2
Bromomethane ND ug/L 06/29/23 21:18 74-83-94.0 3.3 2
2-Butanone (MEK)13.3 ug/L 06/29/23 21:18 78-93-310.0 7.9 2
Carbon disulfide ND ug/L 06/29/23 21:18 75-15-04.0 0.71 2
Carbon tetrachloride ND ug/L 06/29/23 21:18 56-23-52.0 0.67 2
Chlorobenzene ND ug/L 06/29/23 21:18 108-90-72.0 0.57 2
Chloroethane ND ug/L 06/29/23 21:18 75-00-32.0 1.3 2
Chloroform ND ug/L 06/29/23 21:18 67-66-32.0 0.86 2
Chloromethane ND ug/L 06/29/23 21:18 74-87-32.0 1.1 2
Cyclohexane ND ug/L 06/29/23 21:18 110-82-72.0 0.71 2
1,2-Dibromo-3-chloropropane ND ug/L 06/29/23 21:18 96-12-8 v24.0 0.68 2
Dibromochloromethane ND ug/L 06/29/23 21:18 124-48-12.0 0.72 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
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Page 17 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:RW5WG-062323 Lab ID:92674238003 Collected:06/23/23 10:10 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 06/29/23 21:18 106-93-42.0 0.54 2
1,2-Dichlorobenzene ND ug/L 06/29/23 21:18 95-50-12.0 0.68 2
1,3-Dichlorobenzene ND ug/L 06/29/23 21:18 541-73-12.0 0.68 2
1,4-Dichlorobenzene ND ug/L 06/29/23 21:18 106-46-72.0 0.67 2
Dichlorodifluoromethane ND ug/L 06/29/23 21:18 75-71-8 v12.0 0.69 2
1,1-Dichloroethane ND ug/L 06/29/23 21:18 75-34-32.0 0.73 2
1,2-Dichloroethane ND ug/L 06/29/23 21:18 107-06-22.0 0.64 2
1,1-Dichloroethene ND ug/L 06/29/23 21:18 75-35-42.0 0.70 2
cis-1,2-Dichloroethene ND ug/L 06/29/23 21:18 156-59-22.0 0.77 2
trans-1,2-Dichloroethene ND ug/L 06/29/23 21:18 156-60-52.0 0.79 2
1,2-Dichloropropane ND ug/L 06/29/23 21:18 78-87-52.0 0.71 2
cis-1,3-Dichloropropene ND ug/L 06/29/23 21:18 10061-01-52.0 0.73 2
trans-1,3-Dichloropropene ND ug/L 06/29/23 21:18 10061-02-62.0 0.73 2
Ethylbenzene 2.1 ug/L 06/29/23 21:18 100-41-42.0 0.61 2
2-Hexanone ND ug/L 06/29/23 21:18 591-78-610.0 0.95 2
Isopropylbenzene (Cumene)ND ug/L 06/29/23 21:18 98-82-82.0 0.67 2
Methyl acetate ND ug/L 06/29/23 21:18 79-20-920.0 4.8 2
Methylcyclohexane ND ug/L 06/29/23 21:18 108-87-220.0 3.0 2
Methylene Chloride ND ug/L 06/29/23 21:18 75-09-210.0 3.9 2
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/23 21:18 108-10-110.0 5.4 2
Methyl-tert-butyl ether ND ug/L 06/29/23 21:18 1634-04-42.0 0.84 2
Styrene ND ug/L 06/29/23 21:18 100-42-52.0 0.58 2
1,1,2,2-Tetrachloroethane ND ug/L 06/29/23 21:18 79-34-52.0 0.45 2
Tetrachloroethene ND ug/L 06/29/23 21:18 127-18-42.0 0.58 2
Toluene 3.4 ug/L 06/29/23 21:18 108-88-32.0 0.48 2
1,2,4-Trichlorobenzene ND ug/L 06/29/23 21:18 120-82-12.0 1.3 2
1,1,1-Trichloroethane ND ug/L 06/29/23 21:18 71-55-62.0 0.66 2
1,1,2-Trichloroethane ND ug/L 06/29/23 21:18 79-00-52.0 0.65 2
Trichloroethene ND ug/L 06/29/23 21:18 79-01-62.0 0.77 2
Trichlorofluoromethane ND ug/L 06/29/23 21:18 75-69-42.0 0.60 2
1,1,2-Trichlorotrifluoroethane ND ug/L 06/29/23 21:18 76-13-12.0 0.63 2
Vinyl chloride ND ug/L 06/29/23 21:18 75-01-42.0 0.77 2
m&p-Xylene 3.8J ug/L 06/29/23 21:18 179601-23-14.0 1.4 2
o-Xylene 1.8J ug/L 06/29/23 21:18 95-47-62.0 0.68 2
Surrogates
4-Bromofluorobenzene (S)101 %06/29/23 21:18 460-00-470-130 2
1,2-Dichloroethane-d4 (S)113 %06/29/23 21:18 17060-07-070-130 2
Toluene-d8 (S)101 %06/29/23 21:18 2037-26-570-130 2
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 25300 mg/L 07/06/23 17:295.0 5.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:RW5WG-062323 Lab ID:92674238003 Collected:06/23/23 10:10 Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 39.8 mg/L 06/27/23 05:04 18496-25-810.0 2.2 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
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Page 19 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:TRIP BLANK Lab ID:92674238004 Collected:Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/27/23 20:50 67-64-125.0 5.1 1
Benzene ND ug/L 06/27/23 20:50 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 06/27/23 20:50 75-27-41.0 0.31 1
Bromoform ND ug/L 06/27/23 20:50 75-25-21.0 0.34 1
Bromomethane ND ug/L 06/27/23 20:50 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 06/27/23 20:50 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 06/27/23 20:50 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 06/27/23 20:50 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 06/27/23 20:50 108-90-71.0 0.28 1
Chloroethane ND ug/L 06/27/23 20:50 75-00-31.0 0.65 1
Chloroform ND ug/L 06/27/23 20:50 67-66-31.0 0.43 1
Chloromethane ND ug/L 06/27/23 20:50 74-87-3 L1,v11.0 0.54 1
Cyclohexane ND ug/L 06/27/23 20:50 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 06/27/23 20:50 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 06/27/23 20:50 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 06/27/23 20:50 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 06/27/23 20:50 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 06/27/23 20:50 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 06/27/23 20:50 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 06/27/23 20:50 75-71-8 L11.0 0.35 1
1,1-Dichloroethane ND ug/L 06/27/23 20:50 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 06/27/23 20:50 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 06/27/23 20:50 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 06/27/23 20:50 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 06/27/23 20:50 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 06/27/23 20:50 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 06/27/23 20:50 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 06/27/23 20:50 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 06/27/23 20:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/27/23 20:50 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 06/27/23 20:50 98-82-81.0 0.33 1
Methyl acetate ND ug/L 06/27/23 20:50 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 06/27/23 20:50 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 06/27/23 20:50 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/27/23 20:50 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 06/27/23 20:50 1634-04-41.0 0.42 1
Styrene ND ug/L 06/27/23 20:50 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 06/27/23 20:50 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/27/23 20:50 127-18-41.0 0.29 1
Toluene ND ug/L 06/27/23 20:50 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 06/27/23 20:50 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 06/27/23 20:50 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 06/27/23 20:50 79-00-51.0 0.32 1
Trichloroethene ND ug/L 06/27/23 20:50 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 06/27/23 20:50 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Sample:TRIP BLANK Lab ID:92674238004 Collected:Received:06/23/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 06/27/23 20:50 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 06/27/23 20:50 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 06/27/23 20:50 179601-23-12.0 0.71 1
o-Xylene ND ug/L 06/27/23 20:50 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)96 %06/27/23 20:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %06/27/23 20:50 17060-07-070-130 1
Toluene-d8 (S)99 %06/27/23 20:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
786136
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674238001, 92674238002, 92674238003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4075898
Associated Lab Samples:92674238001, 92674238002, 92674238003
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 07/13/23 10:590.12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4075899LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4075900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4075901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 99 75-12597 2 252.5ND 2.5 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
786528
EPA 7470A
EPA 7470A
7470 Mercury Dissolved
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674238001, 92674238002, 92674238003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4077942
Associated Lab Samples:92674238001, 92674238002, 92674238003
Matrix:Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 07/14/23 11:230.12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4077943LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.72.5 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4077944MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4077945
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2.5 99 75-125104 4 252.5ND 2.5 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783225
EPA 3010A
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674238001, 92674238002, 92674238003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4062107
Associated Lab Samples:92674238001, 92674238002, 92674238003
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/29/23 13:133.0
Arsenic ug/L ND 10.0 06/29/23 13:134.7
Barium ug/L ND 5.0 06/29/23 13:133.5
Beryllium ug/L ND 1.0 06/29/23 13:130.70
Boron ug/L ND 50.0 06/29/23 13:1332.4
Cadmium ug/L ND 1.0 06/29/23 13:130.40
Chromium ug/L ND 5.0 06/29/23 13:133.7
Cobalt ug/L ND 5.0 06/29/23 13:133.6
Copper ug/L ND 5.0 06/29/23 13:134.3
Lead ug/L ND 5.0 06/29/23 13:134.5
Nickel ug/L ND 5.0 06/29/23 13:133.5
Selenium ug/L ND 10.0 06/29/23 13:134.7
Silver ug/L ND 5.0 06/29/23 13:132.5
Thallium ug/L ND 10.0 06/29/23 13:138.1
Vanadium ug/L ND 5.0 06/29/23 13:133.9
Zinc ug/L ND 10.0 06/29/23 13:139.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4062108LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 494500 99 80-120
Arsenic ug/L 495500 99 80-120
Barium ug/L 503500 101 80-120
Beryllium ug/L 503500 101 80-120
Boron ug/L 505500 101 80-120
Cadmium ug/L 502500 100 80-120
Chromium ug/L 509500 102 80-120
Cobalt ug/L 505500 101 80-120
Copper ug/L 505500 101 80-120
Lead ug/L 502500 100 80-120
Nickel ug/L 509500 102 80-120
Selenium ug/L 489500 98 80-120
Silver ug/L 249250 100 80-120
Thallium ug/L 508500 102 80-120
Vanadium ug/L 507500 101 80-120
Zinc ug/L 498500 100 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062109MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4062110
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 102 75-125102 0 20500ND509509
Arsenic ug/L 500 103 75-125103 0 20500ND513514
Barium ug/L 500 101 75-125100 1 20500106612607
Beryllium ug/L 500 103 75-125103 0 20500ND513515
Boron ug/L 500 103 75-125103 0 20500ND547547
Cadmium ug/L 500 100 75-125100 0 20500ND499501
Chromium ug/L 500 100 75-125101 0 20500ND503503
Cobalt ug/L 500 100 75-125100 0 20500ND502502
Copper ug/L 500 103 75-125103 0 20500ND516514
Lead ug/L 500 99 75-12599 0 20500ND495495
Nickel ug/L 500 101 75-125101 0 20500ND504505
Selenium ug/L 500 105 75-125105 0 20500ND523523
Silver ug/L 250 101 75-125100 0 20250ND252251
Thallium ug/L 500 100 75-125100 1 20500ND498501
Vanadium ug/L 500 103 75-125103 0 20500ND516515
Zinc ug/L 500 99 75-12599 0 20500ND498498
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782484
EPA 3010A
EPA 6010D
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674238001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4059237
Associated Lab Samples:92674238001
Matrix:Water
AnalyzedMDL
Antimony, Dissolved ug/L ND 5.0 06/29/23 15:253.0
Arsenic, Dissolved ug/L ND 10.0 06/29/23 15:254.7
Barium, Dissolved ug/L ND 5.0 06/29/23 15:253.5
Beryllium, Dissolved ug/L ND 1.0 06/29/23 15:250.70
Boron, Dissolved ug/L ND 50.0 06/29/23 15:2532.4
Cadmium, Dissolved ug/L ND 1.0 06/29/23 15:250.40
Chromium, Dissolved ug/L ND 5.0 06/29/23 15:253.7
Cobalt, Dissolved ug/L ND 5.0 06/29/23 15:253.6
Copper, Dissolved ug/L ND 5.0 06/29/23 15:254.3
Lead, Dissolved ug/L ND 5.0 06/29/23 15:254.5
Nickel, Dissolved ug/L ND 5.0 06/29/23 15:253.5
Selenium, Dissolved ug/L ND 10.0 06/29/23 15:254.7
Silver, Dissolved ug/L ND 5.0 06/29/23 15:252.5
Thallium, Dissolved ug/L ND 10.0 06/29/23 15:258.1
Vanadium, Dissolved ug/L ND 5.0 06/29/23 15:253.9
Zinc, Dissolved ug/L ND 10.0 06/29/23 15:259.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4059238LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 492500 98 80-120
Arsenic, Dissolved ug/L 493500 99 80-120
Barium, Dissolved ug/L 499500 100 80-120
Beryllium, Dissolved ug/L 498500 100 80-120
Boron, Dissolved ug/L 497500 99 80-120
Cadmium, Dissolved ug/L 494500 99 80-120
Chromium, Dissolved ug/L 498500 100 80-120
Cobalt, Dissolved ug/L 496500 99 80-120
Copper, Dissolved ug/L 488500 98 80-120
Lead, Dissolved ug/L 495500 99 80-120
Nickel, Dissolved ug/L 502500 100 80-120
Selenium, Dissolved ug/L 518500 104 80-120
Silver, Dissolved ug/L 243250 97 80-120
Thallium, Dissolved ug/L 501500 100 80-120
Vanadium, Dissolved ug/L 497500 99 80-120
Zinc, Dissolved ug/L 496500 99 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4059239MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4059240
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 500 100 75-125100 1 20500ND498502
Arsenic, Dissolved ug/L 500 99 75-125101 1 20500ND498504
Barium, Dissolved ug/L 500 97 75-12598 0 20500114600603
Beryllium, Dissolved ug/L 500 100 75-125101 1 20500ND501507
Boron, Dissolved ug/L 500 101 75-125102 1 20500ND533538
Cadmium, Dissolved ug/L 500 96 75-12597 0 20500ND481484
Chromium, Dissolved ug/L 500 98 75-12599 1 20500ND490495
Cobalt, Dissolved ug/L 500 97 75-12598 1 20500ND488492
Copper, Dissolved ug/L 500 101 75-125102 1 20500ND507511
Lead, Dissolved ug/L 500 96 75-12596 1 20500ND480484
Nickel, Dissolved ug/L 500 98 75-12599 1 20500ND490495
Selenium, Dissolved ug/L 500 103 75-125104 1 20500ND515520
Silver, Dissolved ug/L 250 98 75-12599 1 20250ND245248
Thallium, Dissolved ug/L 500 91 75-12592 1 20500ND454458
Vanadium, Dissolved ug/L 500 100 75-125101 1 20500ND500504
Zinc, Dissolved ug/L 500 95 75-12596 0 20500ND479481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782892
EPA 3010A
EPA 6010D
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674238002, 92674238003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4060927
Associated Lab Samples:92674238002, 92674238003
Matrix:Water
AnalyzedMDL
Antimony, Dissolved ug/L ND 5.0 06/29/23 15:593.0
Arsenic, Dissolved ug/L ND 10.0 06/29/23 15:594.7
Barium, Dissolved ug/L ND 5.0 06/29/23 15:593.5
Beryllium, Dissolved ug/L ND 1.0 06/29/23 15:590.70
Boron, Dissolved ug/L ND 50.0 06/29/23 15:5932.4
Cadmium, Dissolved ug/L ND 1.0 06/29/23 15:590.40
Chromium, Dissolved ug/L ND 5.0 06/29/23 15:593.7
Cobalt, Dissolved ug/L ND 5.0 06/29/23 15:593.6
Copper, Dissolved ug/L ND 5.0 06/29/23 15:594.3
Lead, Dissolved ug/L ND 5.0 06/29/23 15:594.5
Nickel, Dissolved ug/L ND 5.0 06/29/23 15:593.5
Selenium, Dissolved ug/L ND 10.0 06/29/23 15:594.7
Silver, Dissolved ug/L ND 5.0 06/29/23 15:592.5
Thallium, Dissolved ug/L ND 10.0 06/29/23 15:598.1
Vanadium, Dissolved ug/L ND 5.0 06/29/23 15:593.9
Zinc, Dissolved ug/L ND 10.0 06/29/23 15:599.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4060928LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 480500 96 80-120
Arsenic, Dissolved ug/L 484500 97 80-120
Barium, Dissolved ug/L 484500 97 80-120
Beryllium, Dissolved ug/L 490500 98 80-120
Boron, Dissolved ug/L 491500 98 80-120
Cadmium, Dissolved ug/L 484500 97 80-120
Chromium, Dissolved ug/L 491500 98 80-120
Cobalt, Dissolved ug/L 483500 97 80-120
Copper, Dissolved ug/L 475500 95 80-120
Lead, Dissolved ug/L 483500 97 80-120
Nickel, Dissolved ug/L 493500 99 80-120
Selenium, Dissolved ug/L 506500 101 80-120
Silver, Dissolved ug/L 240250 96 80-120
Thallium, Dissolved ug/L 491500 98 80-120
Vanadium, Dissolved ug/L 483500 97 80-120
Zinc, Dissolved ug/L 479500 96 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4060929MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673461001
4060930
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 500 96 75-12595 1 20500ND480474
Arsenic, Dissolved ug/L 500 96 75-12595 2 20500ND481474
Barium, Dissolved ug/L 500 97 75-12596 1 20500159645640
Beryllium, Dissolved ug/L 500 99 75-12597 2 20500ND494487
Boron, Dissolved ug/L 500 99 75-12597 2 20500ND498490
Cadmium, Dissolved ug/L 500 96 75-12595 1 20500ND478473
Chromium, Dissolved ug/L 500 98 75-12597 1 20500ND493487
Cobalt, Dissolved ug/L 500 97 75-12595 2 20500ND484477
Copper, Dissolved ug/L 500 98 75-12596 2 20500ND491480
Lead, Dissolved ug/L 500 96 75-12594 1 20500ND480473
Nickel, Dissolved ug/L 500 98 75-12596 2 20500ND491483
Selenium, Dissolved ug/L 500 101 75-12599 1 20500ND504496
Silver, Dissolved ug/L 250 96 75-12594 2 20250ND240235
Thallium, Dissolved ug/L 500 98 75-12596 2 20500ND488481
Vanadium, Dissolved ug/L 500 97 75-12596 2 20500ND487480
Zinc, Dissolved ug/L 500 95 75-12594 1 2050012.0 488 481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783375
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674238004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4062986
Associated Lab Samples:92674238004
Matrix:Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 06/27/23 13:340.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/27/23 13:340.22
1,1,2-Trichloroethane ug/L ND 1.0 06/27/23 13:340.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 06/27/23 13:340.32
1,1-Dichloroethane ug/L ND 1.0 06/27/23 13:340.37
1,1-Dichloroethene ug/L ND 1.0 06/27/23 13:340.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/27/23 13:340.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/27/23 13:340.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/27/23 13:340.27
1,2-Dichlorobenzene ug/L ND 1.0 06/27/23 13:340.34
1,2-Dichloroethane ug/L ND 1.0 06/27/23 13:340.32
1,2-Dichloropropane ug/L ND 1.0 06/27/23 13:340.36
1,3-Dichlorobenzene ug/L ND 1.0 06/27/23 13:340.34
1,4-Dichlorobenzene ug/L ND 1.0 06/27/23 13:340.33
2-Butanone (MEK)ug/L ND 5.0 06/27/23 13:344.0
2-Hexanone ug/L ND 5.0 06/27/23 13:340.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/27/23 13:342.7
Acetone ug/L ND 25.0 06/27/23 13:345.1
Benzene ug/L ND 1.0 06/27/23 13:340.34
Bromodichloromethane ug/L ND 1.0 06/27/23 13:340.31
Bromoform ug/L ND 1.0 06/27/23 13:340.34
Bromomethane ug/L ND 2.0 06/27/23 13:341.7
Carbon disulfide ug/L ND 2.0 06/27/23 13:340.36
Carbon tetrachloride ug/L ND 1.0 06/27/23 13:340.33
Chlorobenzene ug/L ND 1.0 06/27/23 13:340.28
Chloroethane ug/L ND 1.0 06/27/23 13:340.65
Chloroform ug/L ND 1.0 06/27/23 13:340.43
Chloromethane ug/L ND 1.0 v106/27/23 13:340.54
cis-1,2-Dichloroethene ug/L ND 1.0 06/27/23 13:340.38
cis-1,3-Dichloropropene ug/L ND 1.0 06/27/23 13:340.36
Cyclohexane ug/L ND 1.0 06/27/23 13:340.35
Dibromochloromethane ug/L ND 1.0 06/27/23 13:340.36
Dichlorodifluoromethane ug/L ND 1.0 06/27/23 13:340.35
Ethylbenzene ug/L ND 1.0 06/27/23 13:340.30
Isopropylbenzene (Cumene)ug/L ND 1.0 06/27/23 13:340.33
m&p-Xylene ug/L ND 2.0 06/27/23 13:340.71
Methyl acetate ug/L ND 10.0 06/27/23 13:342.4
Methyl-tert-butyl ether ug/L ND 1.0 06/27/23 13:340.42
Methylcyclohexane ug/L ND 10.0 06/27/23 13:341.5
Methylene Chloride ug/L ND 5.0 06/27/23 13:342.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4062986
Associated Lab Samples:92674238004
Matrix:Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 06/27/23 13:340.34
Styrene ug/L ND 1.0 06/27/23 13:340.29
Tetrachloroethene ug/L ND 1.0 06/27/23 13:340.29
Toluene ug/L ND 1.0 06/27/23 13:340.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/27/23 13:340.40
trans-1,3-Dichloropropene ug/L ND 1.0 06/27/23 13:340.36
Trichloroethene ug/L ND 1.0 06/27/23 13:340.38
Trichlorofluoromethane ug/L ND 1.0 06/27/23 13:340.30
Vinyl chloride ug/L ND 1.0 06/27/23 13:340.39
1,2-Dichloroethane-d4 (S)%97 70-130 06/27/23 13:34
4-Bromofluorobenzene (S)%98 70-130 06/27/23 13:34
Toluene-d8 (S)%100 70-130 06/27/23 13:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4062987LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 21.220 106 70-130
1,1,2,2-Tetrachloroethane ug/L 21.120 106 70-130
1,1,2-Trichloroethane ug/L 20.520 103 70-130
1,1,2-Trichlorotrifluoroethane ug/L 22.620 113 70-130
1,1-Dichloroethane ug/L 21.120 105 70-130
1,1-Dichloroethene ug/L 22.320 111 70-130
1,2,4-Trichlorobenzene ug/L 19.920 100 70-130
1,2-Dibromo-3-chloropropane ug/L 19.120 96 70-131
1,2-Dibromoethane (EDB)ug/L 20.720 103 70-130
1,2-Dichlorobenzene ug/L 20.220 101 70-130
1,2-Dichloroethane ug/L 19.220 96 70-130
1,2-Dichloropropane ug/L 20.820 104 70-130
1,3-Dichlorobenzene ug/L 20.620 103 70-130
1,4-Dichlorobenzene ug/L 20.720 104 70-130
2-Butanone (MEK)ug/L 37.440 94 70-134
2-Hexanone ug/L 40.440 101 70-131
4-Methyl-2-pentanone (MIBK)ug/L 38.040 95 70-130
Acetone ug/L 37.640 94 70-133
Benzene ug/L 21.220 106 70-130
Bromodichloromethane ug/L 19.920 100 70-130
Bromoform ug/L 20.620 103 70-130
Bromomethane ug/L 19.120 95 45-151
Carbon disulfide ug/L 24.020 120 70-130
Carbon tetrachloride ug/L 22.020 110 70-130
Chlorobenzene ug/L 21.320 106 70-130
Chloroethane ug/L 22.420 112 39-152
Chloroform ug/L 20.420 102 70-130
Chloromethane ug/L 27.3 L1,v12013658-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4062987LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 20.620 103 70-130
cis-1,3-Dichloropropene ug/L 20.220 101 70-130
Cyclohexane ug/L 21.820 109 70-130
Dibromochloromethane ug/L 20.720 104 70-130
Dichlorodifluoromethane ug/L 29.0 L12014554-133
Ethylbenzene ug/L 21.220 106 70-130
Isopropylbenzene (Cumene)ug/L 21.820 109 70-130
m&p-Xylene ug/L 42.740 107 70-130
Methyl acetate ug/L 18.320 92 70-130
Methyl-tert-butyl ether ug/L 18.820 94 70-130
Methylcyclohexane ug/L 23.420 117 70-130
Methylene Chloride ug/L 19.520 98 66-130
o-Xylene ug/L 21.120 106 70-130
Styrene ug/L 21.220 106 70-130
Tetrachloroethene ug/L 21.420 107 70-130
Toluene ug/L 20.920 105 70-130
trans-1,2-Dichloroethene ug/L 21.720 109 70-130
trans-1,3-Dichloropropene ug/L 19.720 98 70-130
Trichloroethene ug/L 21.620 108 70-130
Trichlorofluoromethane ug/L 21.920 110 62-130
Vinyl chloride ug/L 20.220 101 62-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062988MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674494017
4062989
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 123 70-150132 8 3020ND24.5 26.5
1,1,2,2-Tetrachloroethane ug/L 20 115 69-142122 5 3020ND23.1 24.4
1,1,2-Trichloroethane ug/L 20 114 70-138125 9 3020ND22.8 25.0
1,1,2-
Trichlorotrifluoroethane ug/L M1,v12015170-157159 5 3020ND30.3 31.9
1,1-Dichloroethane ug/L 20 118 70-150127 8 3020ND23.5 25.4
1,1-Dichloroethene ug/L 20 130 70-156139 7 3020ND26.0 27.8
1,2,4-Trichlorobenzene ug/L 20 106 70-146111 4 3020ND21.3 22.2
1,2-Dibromo-3-
chloropropane ug/L 20 103 68-146113 9 3020ND20.7 22.5
1,2-Dibromoethane (EDB)ug/L 20 115 70-138124 8 3020ND22.9 24.8
1,2-Dichlorobenzene ug/L 20 110 70-141116 6 3020ND21.9 23.2
1,2-Dichloroethane ug/L 20 107 69-143115 7 3020ND21.5 23.1
1,2-Dichloropropane ug/L 20 115 68-156125 8 3020ND23.1 24.9
1,3-Dichlorobenzene ug/L 20 112 70-143117 5 3020ND22.4 23.4
1,4-Dichlorobenzene ug/L 20 112 70-142117 4 3020ND22.5 23.4
2-Butanone (MEK)ug/L 40 113 60-157120 6 3040ND45.2 48.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062988MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674494017
4062989
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 115 68-146122 6 3040ND46.0 48.9
4-Methyl-2-pentanone
(MIBK)ug/L 40 107 70-141117 10 3040ND42.7 47.0
Acetone ug/L 40 104 58-157112 7 3040ND43.1 46.3
Benzene ug/L 20 120 70-142131 9 3020ND23.9 26.1
Bromodichloromethane ug/L 20 112 70-139121 8 3020ND22.3 24.2
Bromoform ug/L 20 112 64-140122 9 3020ND22.3 24.4
Bromomethane ug/L v12010328-192112 8 3020ND20.6 22.4
Carbon disulfide ug/L 20 135 70-151143 6 3020ND26.9 28.7
Carbon tetrachloride ug/L 20 129 70-148135 5 3020ND25.7 27.1
Chlorobenzene ug/L 20 120 70-141126 5 3020ND24.1 25.3
Chloroethane ug/L v12012358-191129 4 3020ND24.7 25.8
Chloroform ug/L 20 109 70-148118 7 3020ND22.1 23.7
Chloromethane ug/L M0,v12015343-162163 6 3020ND30.8 32.7
cis-1,2-Dichloroethene ug/L 20 114 68-151123 7 3020ND22.8 24.6
cis-1,3-Dichloropropene ug/L 20 108 70-139119 10 3020ND21.7 23.9
Cyclohexane ug/L 20 139 77-149148 6 3020ND27.9 29.7
Dibromochloromethane ug/L 20 112 70-144122 9 3020ND22.4 24.4
Dichlorodifluoromethane ug/L M0,v12018339-171193 6 3020ND36.6 38.7
Ethylbenzene ug/L 20 119 70-143126 5 3020ND23.8 25.1
Isopropylbenzene
(Cumene)ug/L 20 123 70-145130 5 3020ND24.7 26.0
m&p-Xylene ug/L 40 120 70-144125 4 3040ND47.9 49.9
Methyl acetate ug/L 20 104 63-146110 5 3020ND20.8 21.9
Methyl-tert-butyl ether ug/L 20 104 65-143113 9 3020ND20.8 22.7
Methylcyclohexane ug/L M1,v12015370-144163 7 3020ND30.5 32.6
Methylene Chloride ug/L 20 105 62-149113 8 3020ND21.1 22.8
o-Xylene ug/L 20 115 70-145124 7 3020ND23.1 24.8
Styrene ug/L 20 118 70-143126 7 3020ND23.6 25.2
Tetrachloroethene ug/L 20 123 70-145129 5 3020ND24.5 25.8
Toluene ug/L 20 118 70-142128 8 3020ND23.6 25.5
trans-1,2-Dichloroethene ug/L 20 121 70-151131 8 3020ND24.3 26.2
trans-1,3-Dichloropropene ug/L 20 108 70-139119 10 3020ND21.6 23.8
Trichloroethene ug/L 20 121 62-146130 7 3020ND24.3 26.0
Trichlorofluoromethane ug/L v12012863-153146 13 3020ND25.6 29.2
Vinyl chloride ug/L 20 117 61-163126 7 3020ND23.4 25.2
1,2-Dichloroethane-d4 (S)%97 70-13097
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%100 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783895
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674238003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4065548
Associated Lab Samples:92674238003
Matrix:Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 06/29/23 16:180.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/29/23 16:180.22
1,1,2-Trichloroethane ug/L ND 1.0 06/29/23 16:180.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 06/29/23 16:180.32
1,1-Dichloroethane ug/L ND 1.0 06/29/23 16:180.37
1,1-Dichloroethene ug/L ND 1.0 06/29/23 16:180.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/29/23 16:180.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 v206/29/23 16:180.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/29/23 16:180.27
1,2-Dichlorobenzene ug/L ND 1.0 06/29/23 16:180.34
1,2-Dichloroethane ug/L ND 1.0 06/29/23 16:180.32
1,2-Dichloropropane ug/L ND 1.0 06/29/23 16:180.36
1,3-Dichlorobenzene ug/L ND 1.0 06/29/23 16:180.34
1,4-Dichlorobenzene ug/L ND 1.0 06/29/23 16:180.33
2-Butanone (MEK)ug/L ND 5.0 06/29/23 16:184.0
2-Hexanone ug/L ND 5.0 06/29/23 16:180.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/29/23 16:182.7
Acetone ug/L ND 25.0 06/29/23 16:185.1
Benzene ug/L ND 1.0 06/29/23 16:180.34
Bromodichloromethane ug/L ND 1.0 06/29/23 16:180.31
Bromoform ug/L ND 1.0 v206/29/23 16:180.34
Bromomethane ug/L ND 2.0 06/29/23 16:181.7
Carbon disulfide ug/L ND 2.0 06/29/23 16:180.36
Carbon tetrachloride ug/L ND 1.0 06/29/23 16:180.33
Chlorobenzene ug/L ND 1.0 06/29/23 16:180.28
Chloroethane ug/L ND 1.0 06/29/23 16:180.65
Chloroform ug/L ND 1.0 06/29/23 16:180.43
Chloromethane ug/L ND 1.0 06/29/23 16:180.54
cis-1,2-Dichloroethene ug/L ND 1.0 06/29/23 16:180.38
cis-1,3-Dichloropropene ug/L ND 1.0 06/29/23 16:180.36
Cyclohexane ug/L ND 1.0 06/29/23 16:180.35
Dibromochloromethane ug/L ND 1.0 06/29/23 16:180.36
Dichlorodifluoromethane ug/L ND 1.0 v106/29/23 16:180.35
Ethylbenzene ug/L ND 1.0 06/29/23 16:180.30
Isopropylbenzene (Cumene)ug/L ND 1.0 06/29/23 16:180.33
m&p-Xylene ug/L ND 2.0 06/29/23 16:180.71
Methyl acetate ug/L ND 10.0 06/29/23 16:182.4
Methyl-tert-butyl ether ug/L ND 1.0 06/29/23 16:180.42
Methylcyclohexane ug/L ND 10.0 06/29/23 16:181.5
Methylene Chloride ug/L ND 5.0 06/29/23 16:182.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
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Page 34 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4065548
Associated Lab Samples:92674238003
Matrix:Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 06/29/23 16:180.34
Styrene ug/L ND 1.0 06/29/23 16:180.29
Tetrachloroethene ug/L ND 1.0 06/29/23 16:180.29
Toluene ug/L ND 1.0 06/29/23 16:180.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/29/23 16:180.40
trans-1,3-Dichloropropene ug/L ND 1.0 06/29/23 16:180.36
Trichloroethene ug/L ND 1.0 06/29/23 16:180.38
Trichlorofluoromethane ug/L ND 1.0 06/29/23 16:180.30
Vinyl chloride ug/L ND 1.0 06/29/23 16:180.39
1,2-Dichloroethane-d4 (S)%113 70-130 06/29/23 16:18
4-Bromofluorobenzene (S)%100 70-130 06/29/23 16:18
Toluene-d8 (S)%100 70-130 06/29/23 16:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4065549LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.620 98 70-130
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130
1,1,2-Trichloroethane ug/L 19.120 96 70-130
1,1,2-Trichlorotrifluoroethane ug/L 20.920 105 70-130
1,1-Dichloroethane ug/L 19.520 97 70-130
1,1-Dichloroethene ug/L 21.720 108 70-130
1,2,4-Trichlorobenzene ug/L 19.020 95 70-130
1,2-Dibromo-3-chloropropane ug/L 15.7 v3207970-131
1,2-Dibromoethane (EDB)ug/L 18.720 93 70-130
1,2-Dichlorobenzene ug/L 20.020 100 70-130
1,2-Dichloroethane ug/L 21.420 107 70-130
1,2-Dichloropropane ug/L 18.720 93 70-130
1,3-Dichlorobenzene ug/L 20.020 100 70-130
1,4-Dichlorobenzene ug/L 19.320 97 70-130
2-Butanone (MEK)ug/L 33.640 84 70-134
2-Hexanone ug/L 34.640 87 70-131
4-Methyl-2-pentanone (MIBK)ug/L 35.440 89 70-130
Acetone ug/L 37.440 94 70-133
Benzene ug/L 18.920 94 70-130
Bromodichloromethane ug/L 18.120 91 70-130
Bromoform ug/L 15.9 v3207970-130
Bromomethane ug/L 19.920 100 45-151
Carbon disulfide ug/L 20.520 102 70-130
Carbon tetrachloride ug/L 19.220 96 70-130
Chlorobenzene ug/L 19.420 97 70-130
Chloroethane ug/L 21.820 109 39-152
Chloroform ug/L 20.420 102 70-130
Chloromethane ug/L 19.820 99 58-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4065549LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 19.820 99 70-130
cis-1,3-Dichloropropene ug/L 18.020 90 70-130
Cyclohexane ug/L 19.320 97 70-130
Dibromochloromethane ug/L 17.420 87 70-130
Dichlorodifluoromethane ug/L 26.0 v12013054-133
Ethylbenzene ug/L 19.520 97 70-130
Isopropylbenzene (Cumene)ug/L 20.020 100 70-130
m&p-Xylene ug/L 39.340 98 70-130
Methyl acetate ug/L 17.120 85 70-130
Methyl-tert-butyl ether ug/L 18.220 91 70-130
Methylcyclohexane ug/L 19.420 97 70-130
Methylene Chloride ug/L 19.820 99 66-130
o-Xylene ug/L 18.820 94 70-130
Styrene ug/L 19.120 96 70-130
Tetrachloroethene ug/L 19.120 95 70-130
Toluene ug/L 19.120 96 70-130
trans-1,2-Dichloroethene ug/L 20.020 100 70-130
trans-1,3-Dichloropropene ug/L 17.820 89 70-130
Trichloroethene ug/L 19.420 97 70-130
Trichlorofluoromethane ug/L 22.220 111 62-130
Vinyl chloride ug/L 17.720 88 62-130
1,2-Dichloroethane-d4 (S)%113 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4065550MATRIX SPIKE SAMPLE:
MSSpike
Result
92674930002
1,1,1-Trichloroethane ug/L 21.220 106 70-150<1.0
1,1,2,2-Tetrachloroethane ug/L 21.620 108 69-142<1.0
1,1,2-Trichloroethane ug/L 21.520 107 70-138<1.0
1,1,2-Trichlorotrifluoroethane ug/L 26.020 130 70-157<1.0
1,1-Dichloroethane ug/L 20.220 101 70-150<1.0
1,1-Dichloroethene ug/L 22.720 113 70-156<1.0
1,2,4-Trichlorobenzene ug/L 22.920 115 70-146<1.0
1,2-Dibromo-3-chloropropane ug/L 19.920 99 68-146<2.0
1,2-Dibromoethane (EDB)ug/L 22.020 110 70-138<1.0
1,2-Dichlorobenzene ug/L 21.220 106 70-141<1.0
1,2-Dichloroethane ug/L 19.920 99 69-143<1.0
1,2-Dichloropropane ug/L 21.220 106 68-156<1.0
1,3-Dichlorobenzene ug/L 21.620 108 70-143<1.0
1,4-Dichlorobenzene ug/L 20.920 105 70-142<1.0
2-Butanone (MEK)ug/L 38.540 96 60-157<5.0
2-Hexanone ug/L 42.740 107 68-146<5.0
4-Methyl-2-pentanone (MIBK)ug/L 39.540 99 70-141<5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4065550MATRIX SPIKE SAMPLE:
MSSpike
Result
92674930002
Acetone ug/L 38.940 97 58-157<25.0
Benzene ug/L 22.620 110 70-1420.57J
Bromodichloromethane ug/L 20.020 100 70-139<1.0
Bromoform ug/L 20.820 104 64-140<1.0
Bromomethane ug/L 16.8 v3208428-192<2.0
Carbon disulfide ug/L 23.820 119 70-151<2.0
Carbon tetrachloride ug/L 22.820 114 70-148<1.0
Chlorobenzene ug/L 22.420 112 70-141<1.0
Chloroethane ug/L 19.3 v3209658-191<1.0
Chloroform ug/L 20.720 104 70-148<1.0
Chloromethane ug/L 18.9 v3209543-162<1.0
cis-1,2-Dichloroethene ug/L 23.920 98 68-1514.4
cis-1,3-Dichloropropene ug/L 20.420 102 70-139<1.0
Cyclohexane ug/L 23.620 118 77-149<1.0
Dibromochloromethane ug/L 21.020 105 70-144<1.0
Dichlorodifluoromethane ug/L 25.920 129 39-171<1.0
Ethylbenzene ug/L 21.920 110 70-143<1.0
Isopropylbenzene (Cumene)ug/L 22.920 115 70-145<1.0
m&p-Xylene ug/L 44.440 111 70-144<2.0
Methyl acetate ug/L 17.620 88 63-146<10.0
Methyl-tert-butyl ether ug/L 18.120 88 65-1430.45J
Methylcyclohexane ug/L 28.020 140 70-144<10.0
Methylene Chloride ug/L 19.720 98 62-149<5.0
o-Xylene ug/L 22.020 110 70-145<1.0
Styrene ug/L 22.220 111 70-143<1.0
Tetrachloroethene ug/L 22.420 112 70-145<1.0
Toluene ug/L 21.620 108 70-142<1.0
trans-1,2-Dichloroethene ug/L 22.620 113 70-151<1.0
trans-1,3-Dichloropropene ug/L 20.520 103 70-139<1.0
Trichloroethene ug/L 22.820 111 62-1460.58J
Trichlorofluoromethane ug/L 22.520 113 63-153<1.0
Vinyl chloride ug/L 17.6 v3208461-1630.71J
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674930003
4065551SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30<1.0
1,1,2,2-Tetrachloroethane ug/L ND 30<1.0
1,1,2-Trichloroethane ug/L ND 30<1.0
1,1,2-Trichlorotrifluoroethane ug/L ND 30<1.0
1,1-Dichloroethane ug/L ND 30<1.0
1,1-Dichloroethene ug/L ND 30<1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674930003
4065551SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30<1.0
1,2-Dibromo-3-chloropropane ug/L ND 30<2.0
1,2-Dibromoethane (EDB)ug/L ND 30<1.0
1,2-Dichlorobenzene ug/L ND 30<1.0
1,2-Dichloroethane ug/L ND 30<1.0
1,2-Dichloropropane ug/L ND 30<1.0
1,3-Dichlorobenzene ug/L ND 30<1.0
1,4-Dichlorobenzene ug/L ND 30<1.0
2-Butanone (MEK)ug/L ND 30<5.0
2-Hexanone ug/L ND 30<5.0
4-Methyl-2-pentanone (MIBK)ug/L ND 30<5.0
Acetone ug/L ND 30<25.0
Benzene ug/L ND 30<1.0
Bromodichloromethane ug/L ND 30<1.0
Bromoform ug/L ND 30<1.0
Bromomethane ug/L ND v230<2.0
Carbon disulfide ug/L ND 30<2.0
Carbon tetrachloride ug/L ND 30<1.0
Chlorobenzene ug/L ND 30<1.0
Chloroethane ug/L ND v230<1.0
Chloroform ug/L ND 30<1.0
Chloromethane ug/L ND v230<1.0
cis-1,2-Dichloroethene ug/L ND 30<1.0
cis-1,3-Dichloropropene ug/L ND 30<1.0
Cyclohexane ug/L ND 30<1.0
Dibromochloromethane ug/L ND 30<1.0
Dichlorodifluoromethane ug/L ND 30<1.0
Ethylbenzene ug/L ND 30<1.0
Isopropylbenzene (Cumene)ug/L ND 30<1.0
m&p-Xylene ug/L ND 30<2.0
Methyl acetate ug/L ND 30<10.0
Methyl-tert-butyl ether ug/L 0.74J 300.80J
Methylcyclohexane ug/L ND 30<10.0
Methylene Chloride ug/L ND 30<5.0
o-Xylene ug/L ND 30<1.0
Styrene ug/L ND 30<1.0
Tetrachloroethene ug/L ND 30<1.0
Toluene ug/L ND 30<1.0
trans-1,2-Dichloroethene ug/L ND 30<1.0
trans-1,3-Dichloropropene ug/L ND 30<1.0
Trichloroethene ug/L ND 30<1.0
Trichlorofluoromethane ug/L ND 30<1.0
Vinyl chloride ug/L ND v230<1.0
1,2-Dichloroethane-d4 (S)%94112
4-Bromofluorobenzene (S)%9598
Toluene-d8 (S)%98100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783899
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674238001, 92674238002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4065562
Associated Lab Samples:92674238001, 92674238002
Matrix:Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 06/30/23 04:480.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/30/23 04:480.22
1,1,2-Trichloroethane ug/L ND 1.0 06/30/23 04:480.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 06/30/23 04:480.32
1,1-Dichloroethane ug/L ND 1.0 06/30/23 04:480.37
1,1-Dichloroethene ug/L ND 1.0 06/30/23 04:480.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/30/23 04:480.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 v206/30/23 04:480.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/30/23 04:480.27
1,2-Dichlorobenzene ug/L ND 1.0 06/30/23 04:480.34
1,2-Dichloroethane ug/L ND 1.0 06/30/23 04:480.32
1,2-Dichloropropane ug/L ND 1.0 06/30/23 04:480.36
1,3-Dichlorobenzene ug/L ND 1.0 06/30/23 04:480.34
1,4-Dichlorobenzene ug/L ND 1.0 06/30/23 04:480.33
2-Butanone (MEK)ug/L ND 5.0 06/30/23 04:484.0
2-Hexanone ug/L ND 5.0 06/30/23 04:480.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/30/23 04:482.7
Acetone ug/L ND 25.0 06/30/23 04:485.1
Benzene ug/L ND 1.0 06/30/23 04:480.34
Bromodichloromethane ug/L ND 1.0 06/30/23 04:480.31
Bromoform ug/L ND 1.0 v206/30/23 04:480.34
Bromomethane ug/L ND 2.0 06/30/23 04:481.7
Carbon disulfide ug/L ND 2.0 06/30/23 04:480.36
Carbon tetrachloride ug/L ND 1.0 06/30/23 04:480.33
Chlorobenzene ug/L ND 1.0 06/30/23 04:480.28
Chloroethane ug/L ND 1.0 06/30/23 04:480.65
Chloroform ug/L ND 1.0 06/30/23 04:480.43
Chloromethane ug/L ND 1.0 06/30/23 04:480.54
cis-1,2-Dichloroethene ug/L ND 1.0 06/30/23 04:480.38
cis-1,3-Dichloropropene ug/L ND 1.0 06/30/23 04:480.36
Cyclohexane ug/L ND 1.0 06/30/23 04:480.35
Dibromochloromethane ug/L ND 1.0 06/30/23 04:480.36
Dichlorodifluoromethane ug/L ND 1.0 v106/30/23 04:480.35
Ethylbenzene ug/L ND 1.0 06/30/23 04:480.30
Isopropylbenzene (Cumene)ug/L ND 1.0 06/30/23 04:480.33
m&p-Xylene ug/L ND 2.0 06/30/23 04:480.71
Methyl acetate ug/L ND 10.0 06/30/23 04:482.4
Methyl-tert-butyl ether ug/L ND 1.0 06/30/23 04:480.42
Methylcyclohexane ug/L ND 10.0 06/30/23 04:481.5
Methylene Chloride ug/L ND 5.0 06/30/23 04:482.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4065562
Associated Lab Samples:92674238001, 92674238002
Matrix:Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 06/30/23 04:480.34
Styrene ug/L ND 1.0 06/30/23 04:480.29
Tetrachloroethene ug/L ND 1.0 06/30/23 04:480.29
Toluene ug/L ND 1.0 06/30/23 04:480.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/30/23 04:480.40
trans-1,3-Dichloropropene ug/L ND 1.0 06/30/23 04:480.36
Trichloroethene ug/L ND 1.0 06/30/23 04:480.38
Trichlorofluoromethane ug/L ND 1.0 06/30/23 04:480.30
Vinyl chloride ug/L ND 1.0 06/30/23 04:480.39
1,2-Dichloroethane-d4 (S)%113 70-130 06/30/23 04:48
4-Bromofluorobenzene (S)%101 70-130 06/30/23 04:48
Toluene-d8 (S)%100 70-130 06/30/23 04:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4065563LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.920 99 70-130
1,1,2,2-Tetrachloroethane ug/L 18.720 93 70-130
1,1,2-Trichloroethane ug/L 19.420 97 70-130
1,1,2-Trichlorotrifluoroethane ug/L 19.920 100 70-130
1,1-Dichloroethane ug/L 19.720 98 70-130
1,1-Dichloroethene ug/L 21.320 106 70-130
1,2,4-Trichlorobenzene ug/L 19.020 95 70-130
1,2-Dibromo-3-chloropropane ug/L 15.2 v3207670-131
1,2-Dibromoethane (EDB)ug/L 18.320 91 70-130
1,2-Dichlorobenzene ug/L 19.520 98 70-130
1,2-Dichloroethane ug/L 21.620 108 70-130
1,2-Dichloropropane ug/L 19.020 95 70-130
1,3-Dichlorobenzene ug/L 19.520 98 70-130
1,4-Dichlorobenzene ug/L 18.920 94 70-130
2-Butanone (MEK)ug/L 32.840 82 70-134
2-Hexanone ug/L 32.940 82 70-131
4-Methyl-2-pentanone (MIBK)ug/L 35.540 89 70-130
Acetone ug/L 37.340 93 70-133
Benzene ug/L 19.220 96 70-130
Bromodichloromethane ug/L 18.420 92 70-130
Bromoform ug/L 15.8 v3207970-130
Bromomethane ug/L 17.920 89 45-151
Carbon disulfide ug/L 20.020 100 70-130
Carbon tetrachloride ug/L 19.520 97 70-130
Chlorobenzene ug/L 19.120 95 70-130
Chloroethane ug/L 22.220 111 39-152
Chloroform ug/L 20.320 102 70-130
Chloromethane ug/L 19.520 97 58-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4065563LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 19.820 99 70-130
cis-1,3-Dichloropropene ug/L 17.820 89 70-130
Cyclohexane ug/L 19.020 95 70-130
Dibromochloromethane ug/L 17.320 86 70-130
Dichlorodifluoromethane ug/L 24.7 v12012454-133
Ethylbenzene ug/L 19.020 95 70-130
Isopropylbenzene (Cumene)ug/L 19.120 95 70-130
m&p-Xylene ug/L 38.040 95 70-130
Methyl acetate ug/L 16.620 83 70-130
Methyl-tert-butyl ether ug/L 18.520 93 70-130
Methylcyclohexane ug/L 18.920 94 70-130
Methylene Chloride ug/L 20.220 101 66-130
o-Xylene ug/L 18.020 90 70-130
Styrene ug/L 18.520 93 70-130
Tetrachloroethene ug/L 18.220 91 70-130
Toluene ug/L 19.320 96 70-130
trans-1,2-Dichloroethene ug/L 19.720 99 70-130
trans-1,3-Dichloropropene ug/L 17.520 88 70-130
Trichloroethene ug/L 19.220 96 70-130
Trichlorofluoromethane ug/L 22.120 111 62-130
Vinyl chloride ug/L 17.620 88 62-130
1,2-Dichloroethane-d4 (S)%109 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4065564MATRIX SPIKE SAMPLE:
MSSpike
Result
92674941001
1,1,1-Trichloroethane ug/L 20.920 105 70-150<1.0
1,1,2,2-Tetrachloroethane ug/L 21.920 110 69-142<1.0
1,1,2-Trichloroethane ug/L 21.220 106 70-138<1.0
1,1,2-Trichlorotrifluoroethane ug/L 25.620 128 70-157<1.0
1,1-Dichloroethane ug/L 20.420 102 70-150<1.0
1,1-Dichloroethene ug/L 22.920 114 70-156<1.0
1,2,4-Trichlorobenzene ug/L 23.120 115 70-146<1.0
1,2-Dibromo-3-chloropropane ug/L 20.920 104 68-146<2.0
1,2-Dibromoethane (EDB)ug/L 22.420 112 70-138<1.0
1,2-Dichlorobenzene ug/L 21.620 108 70-141<1.0
1,2-Dichloroethane ug/L 19.220 96 69-143<1.0
1,2-Dichloropropane ug/L 21.220 106 68-156<1.0
1,3-Dichlorobenzene ug/L 21.820 109 70-143<1.0
1,4-Dichlorobenzene ug/L 21.420 107 70-142<1.0
2-Butanone (MEK)ug/L 40.540 101 60-157<5.0
2-Hexanone ug/L 43.740 109 68-146<5.0
4-Methyl-2-pentanone (MIBK)ug/L 40.540 101 70-141<5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4065564MATRIX SPIKE SAMPLE:
MSSpike
Result
92674941001
Acetone ug/L 39.040 97 58-157<25.0
Benzene ug/L 21.720 108 70-142<1.0
Bromodichloromethane ug/L 20.420 102 70-139<1.0
Bromoform ug/L 21.220 106 64-140<1.0
Bromomethane ug/L 17.0 v3208528-192<2.0
Carbon disulfide ug/L 21.920 110 70-151<2.0
Carbon tetrachloride ug/L 22.820 114 70-148<1.0
Chlorobenzene ug/L 22.920 115 70-141<1.0
Chloroethane ug/L 19.4 v3209758-191<1.0
Chloroform ug/L 20.320 102 70-148<1.0
Chloromethane ug/L 18.9 v3209543-162<1.0
cis-1,2-Dichloroethene ug/L 20.920 105 68-151<1.0
cis-1,3-Dichloropropene ug/L 20.620 103 70-139<1.0
Cyclohexane ug/L 24.120 121 77-149<1.0
Dibromochloromethane ug/L 21.720 109 70-144<1.0
Dichlorodifluoromethane ug/L 26.020 130 39-171<1.0
Ethylbenzene ug/L 22.420 112 70-143<1.0
Isopropylbenzene (Cumene)ug/L 23.320 117 70-145<1.0
m&p-Xylene ug/L 45.040 112 70-144<2.0
Methyl acetate ug/L 18.020 90 63-146<10.0
Methyl-tert-butyl ether ug/L 18.920 95 65-143<1.0
Methylcyclohexane ug/L 28.720 143 70-144<10.0
Methylene Chloride ug/L 19.420 97 62-149<5.0
o-Xylene ug/L 22.620 113 70-145<1.0
Styrene ug/L 22.920 114 70-143<1.0
Tetrachloroethene ug/L 23.420 117 70-145<1.0
Toluene ug/L 21.520 107 70-142<1.0
trans-1,2-Dichloroethene ug/L 20.820 104 70-151<1.0
trans-1,3-Dichloropropene ug/L 20.820 104 70-139<1.0
Trichloroethene ug/L 22.720 113 62-146<1.0
Trichlorofluoromethane ug/L 22.820 114 63-153<1.0
Vinyl chloride ug/L 17.1 v3208561-163<1.0
1,2-Dichloroethane-d4 (S)%87 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674930015
4065565SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30<1.0
1,1,2,2-Tetrachloroethane ug/L ND 30<1.0
1,1,2-Trichloroethane ug/L ND 30<1.0
1,1,2-Trichlorotrifluoroethane ug/L ND 30<1.0
1,1-Dichloroethane ug/L ND 30<1.0
1,1-Dichloroethene ug/L ND 30<1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674930015
4065565SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30<1.0
1,2-Dibromo-3-chloropropane ug/L ND 30<2.0
1,2-Dibromoethane (EDB)ug/L ND 30<1.0
1,2-Dichlorobenzene ug/L 1.8 6 301.7
1,2-Dichloroethane ug/L ND 30<1.0
1,2-Dichloropropane ug/L ND 30<1.0
1,3-Dichlorobenzene ug/L 2.7 1 302.7
1,4-Dichlorobenzene ug/L 2.2 2 302.3
2-Butanone (MEK)ug/L ND 30<5.0
2-Hexanone ug/L ND 30<5.0
4-Methyl-2-pentanone (MIBK)ug/L ND 30<5.0
Acetone ug/L ND 30<25.0
Benzene ug/L ND 30<1.0
Bromodichloromethane ug/L ND 30<1.0
Bromoform ug/L ND 30<1.0
Bromomethane ug/L ND v230<2.0
Carbon disulfide ug/L ND 30<2.0
Carbon tetrachloride ug/L ND 30<1.0
Chlorobenzene ug/L 0.38J 300.31J
Chloroethane ug/L ND v230<1.0
Chloroform ug/L ND 30<1.0
Chloromethane ug/L ND v230<1.0
cis-1,2-Dichloroethene ug/L 3.8 5 303.9
cis-1,3-Dichloropropene ug/L ND 30<1.0
Cyclohexane ug/L ND 30<1.0
Dibromochloromethane ug/L ND 30<1.0
Dichlorodifluoromethane ug/L ND 30<1.0
Ethylbenzene ug/L ND 30<1.0
Isopropylbenzene (Cumene)ug/L ND 30<1.0
m&p-Xylene ug/L ND 30<2.0
Methyl acetate ug/L ND 30<10.0
Methyl-tert-butyl ether ug/L 3.1 8 303.4
Methylcyclohexane ug/L ND 30<10.0
Methylene Chloride ug/L ND 30<5.0
o-Xylene ug/L ND 30<1.0
Styrene ug/L ND 30<1.0
Tetrachloroethene ug/L ND 30<1.0
Toluene ug/L ND 30<1.0
trans-1,2-Dichloroethene ug/L 0.62J 300.55J
trans-1,3-Dichloropropene ug/L ND 30<1.0
Trichloroethene ug/L 7.0 1 306.9
Trichlorofluoromethane ug/L ND 30<1.0
Vinyl chloride ug/L ND v230<1.0
1,2-Dichloroethane-d4 (S)%93111
4-Bromofluorobenzene (S)%94101
Toluene-d8 (S)%100101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782933
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674238001, 92674238002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4060994
Associated Lab Samples:92674238001, 92674238002
Matrix:Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/26/23 16:321.2
2,4,5-Trichlorophenol ug/L ND 10.0 06/26/23 16:321.4
2,4,6-Trichlorophenol ug/L ND 10.0 06/26/23 16:321.6
2,4-Dichlorophenol ug/L ND 10.0 06/26/23 16:321.4
2,4-Dimethylphenol ug/L ND 10.0 06/26/23 16:321.7
2,4-Dinitrophenol ug/L ND 50.0 06/26/23 16:3226.0
2,4-Dinitrotoluene ug/L ND 10.0 06/26/23 16:321.6
2,6-Dinitrotoluene ug/L ND 10.0 06/26/23 16:321.7
2-Chloronaphthalene ug/L ND 10.0 06/26/23 16:321.7
2-Chlorophenol ug/L ND 10.0 06/26/23 16:321.2
2-Methylnaphthalene ug/L ND 10.0 06/26/23 16:321.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/26/23 16:321.9
2-Nitroaniline ug/L ND 20.0 06/26/23 16:323.0
2-Nitrophenol ug/L ND 10.0 06/26/23 16:321.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/26/23 16:321.2
3,3'-Dichlorobenzidine ug/L ND 20.0 06/26/23 16:328.1
3-Nitroaniline ug/L ND 20.0 06/26/23 16:323.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 v106/26/23 16:327.8
4-Bromophenylphenyl ether ug/L ND 10.0 06/26/23 16:321.8
4-Chloro-3-methylphenol ug/L ND 10.0 06/26/23 16:323.3
4-Chloroaniline ug/L ND 20.0 06/26/23 16:323.6
4-Chlorophenylphenyl ether ug/L ND 10.0 06/26/23 16:322.0
4-Nitroaniline ug/L ND 20.0 06/26/23 16:325.1
4-Nitrophenol ug/L ND 50.0 06/26/23 16:326.6
Acenaphthene ug/L ND 10.0 06/26/23 16:322.0
Acenaphthylene ug/L ND 10.0 06/26/23 16:322.0
Acetophenone ug/L ND 10.0 06/26/23 16:321.5
Anthracene ug/L ND 10.0 06/26/23 16:322.3
Atrazine ug/L ND 10.0 06/26/23 16:323.2
Benzaldehyde ug/L ND 10.0 06/26/23 16:323.6
Benzo(a)anthracene ug/L ND 10.0 06/26/23 16:322.7
Benzo(a)pyrene ug/L ND 10.0 06/26/23 16:322.8
Benzo(b)fluoranthene ug/L ND 10.0 06/26/23 16:322.6
Benzo(g,h,i)perylene ug/L ND 10.0 06/26/23 16:322.8
Benzo(k)fluoranthene ug/L ND 10.0 06/26/23 16:322.7
Biphenyl (Diphenyl)ug/L ND 10.0 06/26/23 16:321.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/26/23 16:321.8
bis(2-Chloroethyl) ether ug/L ND 10.0 06/26/23 16:321.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/26/23 16:323.7
Butylbenzylphthalate ug/L ND 10.0 06/26/23 16:323.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4060994
Associated Lab Samples:92674238001, 92674238002
Matrix:Water
AnalyzedMDL
Caprolactam ug/L 9.3J 10.0 06/26/23 16:326.9
Carbazole ug/L ND 10.0 06/26/23 16:322.4
Chrysene ug/L ND 10.0 06/26/23 16:322.8
Di-n-butylphthalate ug/L ND 10.0 06/26/23 16:322.2
Di-n-octylphthalate ug/L ND 10.0 06/26/23 16:323.9
Dibenz(a,h)anthracene ug/L ND 10.0 06/26/23 16:323.0
Dibenzofuran ug/L ND 10.0 06/26/23 16:322.1
Diethylphthalate ug/L ND 10.0 06/26/23 16:322.0
Dimethylphthalate ug/L ND 10.0 06/26/23 16:322.1
Fluoranthene ug/L ND 10.0 06/26/23 16:322.2
Fluorene ug/L ND 10.0 06/26/23 16:322.1
Hexachloro-1,3-butadiene ug/L ND 10.0 06/26/23 16:321.8
Hexachlorobenzene ug/L ND 10.0 06/26/23 16:322.2
Hexachlorocyclopentadiene ug/L ND 10.0 06/26/23 16:321.6
Hexachloroethane ug/L ND 10.0 06/26/23 16:321.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/26/23 16:322.9
Isophorone ug/L ND 10.0 06/26/23 16:321.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/26/23 16:321.3
N-Nitrosodiphenylamine ug/L ND 10.0 06/26/23 16:323.0
Naphthalene ug/L ND 10.0 06/26/23 16:322.1
Nitrobenzene ug/L ND 10.0 06/26/23 16:321.9
Pentachlorophenol ug/L ND 20.0 06/26/23 16:323.8
Phenanthrene ug/L ND 10.0 06/26/23 16:322.0
Phenol ug/L ND 10.0 06/26/23 16:321.4
Pyrene ug/L ND 10.0 06/26/23 16:322.2
2,4,6-Tribromophenol (S)%92 10-164 06/26/23 16:32
2-Fluorobiphenyl (S)%18 10-130 06/26/23 16:32
2-Fluorophenol (S)%32 10-130 06/26/23 16:32
Nitrobenzene-d5 (S)%36 10-138 06/26/23 16:32
Phenol-d6 (S)%26 10-130 06/26/23 16:32
Terphenyl-d14 (S)%103 19-191 06/26/23 16:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4060995LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 58.450 117 21-135
2,4,5-Trichlorophenol ug/L 43.150 86 38-147
2,4,6-Trichlorophenol ug/L 32.150 64 34-142
2,4-Dichlorophenol ug/L 52.650 105 36-136
2,4-Dimethylphenol ug/L 98.2 L15019638-134
2,4-Dinitrophenol ug/L 33.7J250 13 10-169
2,4-Dinitrotoluene ug/L 61.550 123 44-154
2,6-Dinitrotoluene ug/L 65.850 132 44-156
2-Chloronaphthalene ug/L 56.450 113 25-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4060995LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 45.250 90 29-130
2-Methylnaphthalene ug/L 56.650 113 23-130
2-Methylphenol(o-Cresol)ug/L 55.550 111 31-130
2-Nitroaniline ug/L 112100 112 39-145
2-Nitrophenol ug/L 49.550 99 29-142
3&4-Methylphenol(m&p Cresol)ug/L 49.950 100 30-130
3,3'-Dichlorobenzidine ug/L 137100 137 44-158
3-Nitroaniline ug/L 118100 118 45-152
4,6-Dinitro-2-methylphenol ug/L 23.8 L2,v11002439-158
4-Bromophenylphenyl ether ug/L 62.650 125 47-147
4-Chloro-3-methylphenol ug/L 123100 123 40-138
4-Chloroaniline ug/L 100100 100 35-130
4-Chlorophenylphenyl ether ug/L 59.350 119 36-139
4-Nitroaniline ug/L 106100 106 46-157
4-Nitrophenol ug/L 33.6J L22501317-130
Acenaphthene ug/L 59.050 118 34-135
Acenaphthylene ug/L 58.350 117 35-137
Acetophenone ug/L 52.650 105 30-137
Anthracene ug/L 54.550 109 47-146
Atrazine ug/L 66.5 L15013330-130
Benzaldehyde ug/L 64.650 129 17-167
Benzo(a)anthracene ug/L 66.750 133 48-160
Benzo(a)pyrene ug/L 61.450 123 47-165
Benzo(b)fluoranthene ug/L 69.550 139 49-171
Benzo(g,h,i)perylene ug/L 57.150 114 46-166
Benzo(k)fluoranthene ug/L 61.950 124 55-162
Biphenyl (Diphenyl)ug/L 54.750 109 28-130
bis(2-Chloroethoxy)methane ug/L 55.450 111 33-136
bis(2-Chloroethyl) ether ug/L 55.250 110 30-142
bis(2-Ethylhexyl)phthalate ug/L 71.450 143 46-173
Butylbenzylphthalate ug/L 75.250 150 53-169
Caprolactam ug/L 40.650 81 13-130
Carbazole ug/L 58.450 117 48-157
Chrysene ug/L 60.950 122 54-152
Di-n-butylphthalate ug/L 60.550 121 49-161
Di-n-octylphthalate ug/L 73.150 146 50-166
Dibenz(a,h)anthracene ug/L 59.350 119 46-166
Dibenzofuran ug/L 58.450 117 37-136
Diethylphthalate ug/L 58.650 117 45-149
Dimethylphthalate ug/L 58.750 117 43-145
Fluoranthene ug/L 60.150 120 50-153
Fluorene ug/L 60.250 120 42-142
Hexachloro-1,3-butadiene ug/L 51.850 104 10-130
Hexachlorobenzene ug/L 61.950 124 44-138
Hexachlorocyclopentadiene ug/L 53.650 107 10-130
Hexachloroethane ug/L 38.650 77 10-130
Indeno(1,2,3-cd)pyrene ug/L 59.950 120 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4060995LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 59.150 118 36-135
N-Nitroso-di-n-propylamine ug/L 56.050 112 33-140
N-Nitrosodiphenylamine ug/L 59.250 118 46-144
Naphthalene ug/L 54.050 108 20-130
Nitrobenzene ug/L 57.150 114 33-133
Pentachlorophenol ug/L 34.0100 34 21-163
Phenanthrene ug/L 58.150 116 47-146
Phenol ug/L 35.550 71 19-130
Pyrene ug/L 69.550 139 53-155
2,4,6-Tribromophenol (S)%92 10-164
2-Fluorobiphenyl (S)%102 10-130
2-Fluorophenol (S)%48 10-130
Nitrobenzene-d5 (S)%107 10-138
Phenol-d6 (S)%63 10-130
Terphenyl-d14 (S)%127 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4060996MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35807863001
4060997
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-
chloropropane)ug/L 50 47 11-14352 11 30501.2U 23.3 26.0
2,4,5-Trichlorophenol ug/L M150910-17067 30501.4U 4.4J 33.7
2,4,6-Trichlorophenol ug/L M150310-16659 30501.6U 1.6J 29.5
2,4-Dichlorophenol ug/L M150910-15349 30501.4U 4.4J 24.7
2,4-Dimethylphenol ug/L 50 62 20-14783 28 30501.7U 31.1 41.3
2,4-Dinitrophenol ug/L M1250010-17264 3025026.0U ND 161
2,4-Dinitrotoluene ug/L 50 80 30-16478 2 30501.6U 39.8 38.9
2,6-Dinitrotoluene ug/L 50 73 31-16371 2 30501.7U 36.5 35.7
2-Chloronaphthalene ug/L 50 35 15-13438 8 30501.7U 17.6 19.1
2-Chlorophenol ug/L M150910-13946 30501.2U 4.3J 23.2
2-Methylnaphthalene ug/L 50 36 12-13032 9 30501.9U 17.8 16.2
2-Methylphenol(o-Cresol)ug/L R1503319-13249 40 30501.9U 16.4 24.7
2-Nitroaniline ug/L 100 60 23-15464 7 301003.0U 60.0 64.5
2-Nitrophenol ug/L M150710-15951 30501.4U 3.7J 25.5
3&4-Methylphenol(m&p
Cresol)
ug/L R1502713-13645 49 30501.2U 13.6 22.6
3,3'-Dichlorobenzidine ug/L 100 93 10-17870 28 301008.1U 93.1 70.2
3-Nitroaniline ug/L 100 76 20-16671 7 301003.8U 76.0 70.8
4,6-Dinitro-2-methylphenol ug/L M0,v1100010-18772 301007.8U ND 72.3
4-Bromophenylphenyl ether ug/L 50 67 31-15765 3 30501.8U 33.4 32.5
4-Chloro-3-methylphenol ug/L R11004327-14661 35 301003.3U 43.0 61.3
4-Chloroaniline ug/L R11004013-14329 32 301003.6U 39.6 28.6
4-Chlorophenylphenyl ether ug/L 50 53 23-14962 14 30502.0U 26.7 30.8
4-Nitroaniline ug/L 100 79 24-17175 5 301005.1U 79.2 75.1
4-Nitrophenol ug/L M0250010-13054 302506.6U ND 135
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4060996MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35807863001
4060997
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L 50 41 21-14750 20 30502.0U 21.8 26.7
Acenaphthylene ug/L 50 41 19-15049 19 30502.0U 20.4 24.7
Acetophenone ug/L 50 41 22-14549 16 30501.5U 20.7 24.3
Anthracene ug/L 50 71 36-15264 10 30502.3U 35.6 32.1
Atrazine ug/L R1509318-17350 61 30503.2U 46.4 24.8
Benzaldehyde ug/L 50 56 16-16358 5 30503.6U 27.9 29.2
Benzo(a)anthracene ug/L 50 89 42-16375 17 30502.7U 44.5 37.5
Benzo(a)pyrene ug/L 50 83 40-16973 13 30502.8U 41.6 36.7
Benzo(b)fluoranthene ug/L 50 91 40-17781 11 30502.6U 45.3 40.7
Benzo(g,h,i)perylene ug/L 50 81 38-17469 16 30502.8U 40.5 34.6
Benzo(k)fluoranthene ug/L 50 85 41-17171 19 30502.7U 42.7 35.3
Biphenyl (Diphenyl)ug/L 50 35 14-13739 10 30501.8U 17.4 19.3
bis(2-
Chloroethoxy)methane ug/L 50 43 19-14650 14 30501.8U 21.5 24.8
bis(2-Chloroethyl) ether ug/L 50 42 19-15148 13 30501.9U 21.0 24.0
bis(2-Ethylhexyl)phthalate ug/L 50 92 42-16880 15 30503.7U 46.2 39.8
Butylbenzylphthalate ug/L 50 98 42-17779 22 30503.1U 49.0 39.5
Caprolactam ug/L R1503410-13049 35 30506.9U 17.1 24.5
Carbazole ug/L 50 85 38-16473 15 30502.4U 42.5 36.5
Chrysene ug/L 50 84 43-15972 15 30502.8U 41.9 36.1
Di-n-butylphthalate ug/L 50 88 42-16076 14 30502.2U 43.9 38.2
Di-n-octylphthalate ug/L 50 98 42-17181 19 30503.9U 49.1 40.7
Dibenz(a,h)anthracene ug/L 50 82 40-17171 14 30503.0U 41.2 35.7
Dibenzofuran ug/L 50 46 23-14756 19 30502.1U 23.0 27.9
Diethylphthalate ug/L 50 79 33-15774 6 30502.0U 39.5 37.2
Dimethylphthalate ug/L 50 64 27-15467 3 30502.1U 32.2 33.3
Fluoranthene ug/L 50 88 42-15777 13 30502.2U 43.9 38.5
Fluorene ug/L 50 56 25-15564 12 30502.1U 28.2 31.8
Hexachloro-1,3-butadiene ug/L 50 30 10-13013 30501.8U 14.9 6.6J
Hexachlorobenzene ug/L 50 70 32-14562 11 30502.2U 34.8 31.1
Hexachlorocyclopentadiene ug/L 50 26 10-13018 30501.6U 12.8 8.8J
Hexachloroethane ug/L 50 27 10-13013 30501.4U 13.7 6.6J
Indeno(1,2,3-cd)pyrene ug/L 50 83 39-17473 13 30502.9U 41.4 36.4
Isophorone ug/L 50 46 19-14652 14 30501.7U 22.9 26.2
N-Nitroso-di-n-propylamine ug/L 50 43 20-15051 17 30501.3U 21.3 25.4
N-Nitrosodiphenylamine ug/L 50 71 33-14966 8 30503.0U 35.7 32.9
Naphthalene ug/L 50 36 10-12829 20 30502.1U 17.9 14.6
Nitrobenzene ug/L 50 45 19-14549 7 30501.9U 22.7 24.3
Pentachlorophenol ug/L M1100410-18870 301003.8U 3.8J 70.4
Phenanthrene ug/L 50 75 38-15068 10 30502.0U 37.5 34.0
Phenol ug/L 50 11 10-13032 30501.4U 5.3J 16.1
Pyrene ug/L 50 90 42-16374 19 30502.2U 45.1 37.1
2,4,6-Tribromophenol (S)%10 10-16478
2-Fluorobiphenyl (S)%33 10-13047
2-Fluorophenol (S)%S0210-13040
Nitrobenzene-d5 (S)%43 10-13855
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4060996MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35807863001
4060997
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%S0810-13033
Terphenyl-d14 (S)%78 19-19173
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783788
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674238003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4064951
Associated Lab Samples:92674238003
Matrix:Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 07/01/23 14:421.2
2,4,5-Trichlorophenol ug/L ND 10.0 07/01/23 14:421.4
2,4,6-Trichlorophenol ug/L ND 10.0 07/01/23 14:421.6
2,4-Dichlorophenol ug/L ND 10.0 07/01/23 14:421.4
2,4-Dimethylphenol ug/L ND 10.0 v107/01/23 14:421.7
2,4-Dinitrophenol ug/L ND 50.0 07/01/23 14:4226.0
2,4-Dinitrotoluene ug/L ND 10.0 07/01/23 14:421.6
2,6-Dinitrotoluene ug/L ND 10.0 07/01/23 14:421.7
2-Chloronaphthalene ug/L ND 10.0 07/01/23 14:421.7
2-Chlorophenol ug/L ND 10.0 07/01/23 14:421.2
2-Methylnaphthalene ug/L ND 10.0 07/01/23 14:421.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 07/01/23 14:421.9
2-Nitroaniline ug/L ND 20.0 07/01/23 14:423.0
2-Nitrophenol ug/L ND 10.0 07/01/23 14:421.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/01/23 14:421.2
3,3'-Dichlorobenzidine ug/L ND 20.0 07/01/23 14:428.1
3-Nitroaniline ug/L ND 20.0 07/01/23 14:423.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/01/23 14:427.8
4-Bromophenylphenyl ether ug/L ND 10.0 07/01/23 14:421.8
4-Chloro-3-methylphenol ug/L ND 10.0 07/01/23 14:423.3
4-Chloroaniline ug/L ND 20.0 07/01/23 14:423.6
4-Chlorophenylphenyl ether ug/L ND 10.0 07/01/23 14:422.0
4-Nitroaniline ug/L ND 20.0 07/01/23 14:425.1
4-Nitrophenol ug/L ND 50.0 07/01/23 14:426.6
Acenaphthene ug/L ND 10.0 07/01/23 14:422.0
Acenaphthylene ug/L ND 10.0 07/01/23 14:422.0
Acetophenone ug/L ND 10.0 07/01/23 14:421.5
Anthracene ug/L ND 10.0 07/01/23 14:422.3
Atrazine ug/L ND 10.0 07/01/23 14:423.2
Benzaldehyde ug/L ND 10.0 07/01/23 14:423.6
Benzo(a)anthracene ug/L ND 10.0 07/01/23 14:422.7
Benzo(a)pyrene ug/L ND 10.0 07/01/23 14:422.8
Benzo(b)fluoranthene ug/L ND 10.0 07/01/23 14:422.6
Benzo(g,h,i)perylene ug/L ND 10.0 07/01/23 14:422.8
Benzo(k)fluoranthene ug/L ND 10.0 07/01/23 14:422.7
Biphenyl (Diphenyl)ug/L ND 10.0 07/01/23 14:421.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 07/01/23 14:421.8
bis(2-Chloroethyl) ether ug/L ND 10.0 07/01/23 14:421.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 07/01/23 14:423.7
Butylbenzylphthalate ug/L ND 10.0 07/01/23 14:423.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4064951
Associated Lab Samples:92674238003
Matrix:Water
AnalyzedMDL
Caprolactam ug/L ND 10.0 07/01/23 14:426.9
Carbazole ug/L ND 10.0 07/01/23 14:422.4
Chrysene ug/L ND 10.0 07/01/23 14:422.8
Di-n-butylphthalate ug/L ND 10.0 07/01/23 14:422.2
Di-n-octylphthalate ug/L ND 10.0 07/01/23 14:423.9
Dibenz(a,h)anthracene ug/L ND 10.0 07/01/23 14:423.0
Dibenzofuran ug/L ND 10.0 07/01/23 14:422.1
Diethylphthalate ug/L ND 10.0 07/01/23 14:422.0
Dimethylphthalate ug/L ND 10.0 07/01/23 14:422.1
Fluoranthene ug/L ND 10.0 07/01/23 14:422.2
Fluorene ug/L ND 10.0 07/01/23 14:422.1
Hexachloro-1,3-butadiene ug/L ND 10.0 07/01/23 14:421.8
Hexachlorobenzene ug/L ND 10.0 07/01/23 14:422.2
Hexachlorocyclopentadiene ug/L ND 10.0 07/01/23 14:421.6
Hexachloroethane ug/L ND 10.0 07/01/23 14:421.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/01/23 14:422.9
Isophorone ug/L ND 10.0 07/01/23 14:421.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 07/01/23 14:421.3
N-Nitrosodiphenylamine ug/L ND 10.0 07/01/23 14:423.0
Naphthalene ug/L ND 10.0 07/01/23 14:422.1
Nitrobenzene ug/L ND 10.0 07/01/23 14:421.9
Pentachlorophenol ug/L ND 20.0 07/01/23 14:423.8
Phenanthrene ug/L ND 10.0 07/01/23 14:422.0
Phenol ug/L ND 10.0 07/01/23 14:421.4
Pyrene ug/L ND 10.0 07/01/23 14:422.2
2,4,6-Tribromophenol (S)%31 10-164 07/01/23 14:42
2-Fluorobiphenyl (S)%13 10-130 07/01/23 14:42
2-Fluorophenol (S)%14 10-130 07/01/23 14:42
Nitrobenzene-d5 (S)%18 10-138 07/01/23 14:42
Phenol-d6 (S)%11 10-130 07/01/23 14:42
Terphenyl-d14 (S)%74 19-191 07/01/23 14:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4064952LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 35.550 71 21-135
2,4,5-Trichlorophenol ug/L 43.750 87 38-147
2,4,6-Trichlorophenol ug/L 43.850 88 34-142
2,4-Dichlorophenol ug/L 40.350 81 36-136
2,4-Dimethylphenol ug/L 59.9 v15012038-134
2,4-Dinitrophenol ug/L 218250 87 10-169
2,4-Dinitrotoluene ug/L 41.950 84 44-154
2,6-Dinitrotoluene ug/L 44.250 88 44-156
2-Chloronaphthalene ug/L 27.650 55 25-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4064952LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 33.750 67 29-130
2-Methylnaphthalene ug/L 26.050 52 23-130
2-Methylphenol(o-Cresol)ug/L 37.050 74 31-130
2-Nitroaniline ug/L 79.0100 79 39-145
2-Nitrophenol ug/L 37.350 75 29-142
3&4-Methylphenol(m&p Cresol)ug/L 37.250 74 30-130
3,3'-Dichlorobenzidine ug/L 89.1100 89 44-158
3-Nitroaniline ug/L 83.3100 83 45-152
4,6-Dinitro-2-methylphenol ug/L 91.0100 91 39-158
4-Bromophenylphenyl ether ug/L 39.050 78 47-147
4-Chloro-3-methylphenol ug/L 82.8100 83 40-138
4-Chloroaniline ug/L 62.0100 62 35-130
4-Chlorophenylphenyl ether ug/L 34.650 69 36-139
4-Nitroaniline ug/L 77.8100 78 46-157
4-Nitrophenol ug/L 134250 54 17-130
Acenaphthene ug/L 33.550 67 34-135
Acenaphthylene ug/L 33.650 67 35-137
Acetophenone ug/L 34.450 69 30-137
Anthracene ug/L 37.150 74 47-146
Atrazine ug/L 40.250 80 30-130
Benzaldehyde ug/L 37.150 74 17-167
Benzo(a)anthracene ug/L 41.750 83 48-160
Benzo(a)pyrene ug/L 41.150 82 47-165
Benzo(b)fluoranthene ug/L 45.750 91 49-171
Benzo(g,h,i)perylene ug/L 42.050 84 46-166
Benzo(k)fluoranthene ug/L 41.150 82 55-162
Biphenyl (Diphenyl)ug/L 27.650 55 28-130
bis(2-Chloroethoxy)methane ug/L 35.450 71 33-136
bis(2-Chloroethyl) ether ug/L 35.150 70 30-142
bis(2-Ethylhexyl)phthalate ug/L 45.150 90 46-173
Butylbenzylphthalate ug/L 44.550 89 53-169
Caprolactam ug/L 23.950 48 13-130
Carbazole ug/L 41.750 83 48-157
Chrysene ug/L 40.550 81 54-152
Di-n-butylphthalate ug/L 42.150 84 49-161
Di-n-octylphthalate ug/L 43.750 87 50-166
Dibenz(a,h)anthracene ug/L 42.650 85 46-166
Dibenzofuran ug/L 34.550 69 37-136
Diethylphthalate ug/L 40.850 82 45-149
Dimethylphthalate ug/L 40.250 80 43-145
Fluoranthene ug/L 42.850 86 50-153
Fluorene ug/L 37.950 76 42-142
Hexachloro-1,3-butadiene ug/L 18.750 37 10-130
Hexachlorobenzene ug/L 40.550 81 44-138
Hexachlorocyclopentadiene ug/L 20.150 40 10-130
Hexachloroethane ug/L 18.850 38 10-130
Indeno(1,2,3-cd)pyrene ug/L 43.450 87 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4064952LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 38.550 77 36-135
N-Nitroso-di-n-propylamine ug/L 37.350 75 33-140
N-Nitrosodiphenylamine ug/L 39.550 79 46-144
Naphthalene ug/L 27.150 54 20-130
Nitrobenzene ug/L 34.350 69 33-133
Pentachlorophenol ug/L 90.4100 90 21-163
Phenanthrene ug/L 39.750 79 47-146
Phenol ug/L 25.550 51 19-130
Pyrene ug/L 42.950 86 53-155
2,4,6-Tribromophenol (S)%109 10-164
2-Fluorobiphenyl (S)%72 10-130
2-Fluorophenol (S)%57 10-130
Nitrobenzene-d5 (S)%80 10-138
Phenol-d6 (S)%52 10-130
Terphenyl-d14 (S)%93 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4065163MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35809128001
4065164
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-
chloropropane)ug/L 45.5 84 11-14389 6 3045.51.0U 38.2 40.5
2,4,5-Trichlorophenol ug/L 45.5 98 10-170102 4 3045.51.3U 44.5 46.5
2,4,6-Trichlorophenol ug/L 45.5 95 10-166101 5 3045.51.4U 43.3 45.7
2,4-Dichlorophenol ug/L 45.5 86 10-15398 13 3045.51.3U 39.3 44.7
2,4-Dimethylphenol ug/L v145.5 135 20-147135 0 3045.51.5U 61.2 61.5
2,4-Dinitrophenol ug/L 227 95 10-172109 14 3022723.6U 216 247
2,4-Dinitrotoluene ug/L 45.5 94 30-164106 12 3045.51.5U 42.9 48.2
2,6-Dinitrotoluene ug/L 45.5 98 31-163102 4 3045.51.6U 44.5 46.3
2-Chloronaphthalene ug/L 45.5 70 15-13475 8 3045.51.6U 31.6 34.3
2-Chlorophenol ug/L 45.5 80 10-13989 10 3045.51.1U 36.6 40.3
2-Methylnaphthalene ug/L 45.5 64 12-13073 14 3045.51.7U 29.1 33.3
2-Methylphenol(o-Cresol)ug/L 45.5 81 19-13293 14 3045.51.7U 36.7 42.1
2-Nitroaniline ug/L 90.9 85 23-15486 1 3090.92.7U 77.4 78.1
2-Nitrophenol ug/L 45.5 93 10-159101 8 3045.51.3U 42.2 45.7
3&4-Methylphenol(m&p
Cresol)
ug/L 45.5 79 13-13693 16 3045.51.1U 35.8 42.1
3,3'-Dichlorobenzidine ug/L 90.9 85 10-17887 2 3090.97.4U 77.4 78.9
3-Nitroaniline ug/L 90.9 88 20-16698 10 3090.93.4U 80.2 88.8
4,6-Dinitro-2-methylphenol ug/L 90.9 102 10-187111 9 3090.97.1U 92.4 101
4-Bromophenylphenyl ether ug/L 45.5 88 31-15791 3 3045.51.6U 39.9 41.2
4-Chloro-3-methylphenol ug/L 90.9 92 27-146101 9 3090.93.0U 83.6 91.8
4-Chloroaniline ug/L 90.9 73 13-14381 11 3090.93.3U 66.2 73.6
4-Chlorophenylphenyl ether ug/L 45.5 84 23-14989 6 3045.51.8U 38.2 40.5
4-Nitroaniline ug/L 90.9 82 24-17191 10 3090.94.6U 74.6 82.4
4-Nitrophenol ug/L 227 60 10-13070 17 302276.0U 135 160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4065163MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35809128001
4065164
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L 45.5 81 21-14787 6 3045.51.8U 37.0 39.3
Acenaphthylene ug/L 45.5 80 19-15086 7 3045.51.8U 36.2 38.9
Acetophenone ug/L 45.5 76 22-14585 11 3045.51.4U 34.7 38.6
Anthracene ug/L 45.5 82 36-15286 5 3045.52.1U 37.4 39.3
Atrazine ug/L 45.5 82 18-17384 2 3045.52.9U 37.2 38.1
Benzaldehyde ug/L 45.5 90 16-16391 2 3045.53.3U 40.9 41.6
Benzo(a)anthracene ug/L 45.5 94 42-16396 2 3045.52.4U 42.8 43.7
Benzo(a)pyrene ug/L 45.5 90 40-16992 2 3045.52.5U 41.1 42.0
Benzo(b)fluoranthene ug/L 45.5 100 40-177103 4 3045.52.4U 45.3 47.0
Benzo(g,h,i)perylene ug/L 45.5 88 38-17484 5 3045.52.6U 40.1 38.3
Benzo(k)fluoranthene ug/L 45.5 95 41-17195 0 3045.52.5U 43.1 43.0
Biphenyl (Diphenyl)ug/L 45.5 69 14-13775 8 3045.51.7U 31.4 34.1
bis(2-
Chloroethoxy)methane ug/L 45.5 82 19-14693 12 3045.51.7U 37.3 42.2
bis(2-Chloroethyl) ether ug/L 45.5 85 19-15191 6 3045.51.7U 38.7 41.1
bis(2-Ethylhexyl)phthalate ug/L 45.5 103 42-168108 4 3045.53.4U 46.9 49.1
Butylbenzylphthalate ug/L 45.5 104 42-177108 4 3045.52.9U 47.1 49.0
Caprolactam ug/L 45.5 60 10-13073 20 3045.56.3U 27.3 33.4
Carbazole ug/L 45.5 90 38-16497 7 3045.52.1U 41.1 43.9
Chrysene ug/L 45.5 90 43-15991 1 3045.52.5U 40.7 41.3
Di-n-butylphthalate ug/L 45.5 92 42-160100 9 3045.52.0U 41.6 45.5
Di-n-octylphthalate ug/L 45.5 104 42-171111 7 3045.53.6U 47.3 50.6
Dibenz(a,h)anthracene ug/L 45.5 91 40-17189 2 3045.52.7U 41.4 40.5
Dibenzofuran ug/L 45.5 84 23-14790 6 3045.51.9U 38.3 40.8
Diethylphthalate ug/L 45.5 90 33-15797 7 3045.51.9U 41.0 43.9
Dimethylphthalate ug/L 45.5 88 27-15494 7 3045.51.9U 39.9 42.8
Fluoranthene ug/L 45.5 91 42-15799 9 3045.52.0U 41.4 45.2
Fluorene ug/L 45.5 89 25-15594 6 3045.51.9U 40.4 42.7
Hexachloro-1,3-butadiene ug/L 45.5 47 10-13046 3 3045.51.6U 21.3 20.7
Hexachlorobenzene ug/L 45.5 87 32-14589 2 3045.52.0U 39.6 40.5
Hexachlorocyclopentadiene ug/L 45.5 49 10-13049 0 3045.51.4U 22.5 22.4
Hexachloroethane ug/L 45.5 48 10-13047 2 3045.51.3U 21.8 21.5
Indeno(1,2,3-cd)pyrene ug/L 45.5 92 39-17490 1 3045.52.6U 41.6 41.0
Isophorone ug/L 45.5 84 19-14698 14 3045.51.5U 38.4 44.3
N-Nitroso-di-n-propylamine ug/L 45.5 86 20-15093 8 3045.51.2U 39.1 42.4
N-Nitrosodiphenylamine ug/L 45.5 88 33-14989 2 3045.52.7U 39.8 40.6
Naphthalene ug/L 45.5 66 10-12873 10 3045.51.9U 30.1 33.1
Nitrobenzene ug/L 45.5 83 19-14593 11 3045.51.7U 37.9 42.2
Pentachlorophenol ug/L 90.9 97 10-188108 11 3090.93.4U 88.6 98.6
Phenanthrene ug/L 45.5 88 38-15090 3 3045.51.8U 39.9 40.9
Phenol ug/L 45.5 59 10-13067 14 3045.51.2U 26.7 30.7
Pyrene ug/L 45.5 100 42-16398 2 3045.52.0U 45.4 44.7
2,4,6-Tribromophenol (S)%114 10-164111
2-Fluorobiphenyl (S)%79 10-13083
2-Fluorophenol (S)%67 10-13071
Nitrobenzene-d5 (S)%121 10-138100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4065163MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35809128001
4065164
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%55 10-13062
Terphenyl-d14 (S)%103 19-19199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
785082
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674238001, 92674238002, 92674238003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4070865
Associated Lab Samples:92674238001, 92674238002, 92674238003
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 07/06/23 20:095.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4070866LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 53.050 106 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4070867LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 53.750 107 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4070868MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674597001
4070869
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 108 80-120106 1 255071.0 125 124
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4070870MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674597002
4070871
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 105 80-120104 1 255068.8 121 121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783153
SM 4500-S2D-2011
SM 4500-S2D-2011
4500S2D Sulfide Water
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674238001, 92674238002, 92674238003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4061905
Associated Lab Samples:92674238001, 92674238002, 92674238003
Matrix:Water
AnalyzedMDL
Sulfide mg/L ND 0.10 06/27/23 04:520.022
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4061906LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide mg/L 0.520.5 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4061907MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674166001
4061908
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 99 80-120106 6 100.5ND 0.50 0.53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 90
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Sample field preservation does not meet EPA or method recommendations for this analysis.P4
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 90
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92674238
PACTIV EVERGREEN-Revised Report
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92674238001 783225 783277PZ4WG-062323 EPA 3010A EPA 6010D
92674238002 783225 783277DUP01WG-062323 EPA 3010A EPA 6010D
92674238003 783225 783277RW5WG-062323 EPA 3010A EPA 6010D
92674238001 782484 782895PZ4WG-062323 EPA 3010A EPA 6010D
92674238002 782892 783137DUP01WG-062323 EPA 3010A EPA 6010D
92674238003 782892 783137RW5WG-062323 EPA 3010A EPA 6010D
92674238001 786136 786221PZ4WG-062323 EPA 7470A EPA 7470A
92674238002 786136 786221DUP01WG-062323 EPA 7470A EPA 7470A
92674238003 786136 786221RW5WG-062323 EPA 7470A EPA 7470A
92674238001 786528 786802PZ4WG-062323 EPA 7470A EPA 7470A
92674238002 786528 786802DUP01WG-062323 EPA 7470A EPA 7470A
92674238003 786528 786802RW5WG-062323 EPA 7470A EPA 7470A
92674238001 782933 783069PZ4WG-062323 EPA 3510C EPA 8270E
92674238002 782933 783069DUP01WG-062323 EPA 3510C EPA 8270E
92674238003 783788 784171RW5WG-062323 EPA 3510C EPA 8270E
92674238001 783899PZ4WG-062323 EPA 8260D
92674238002 783899DUP01WG-062323 EPA 8260D
92674238003 783895RW5WG-062323 EPA 8260D
92674238004 783375TRIP BLANK EPA 8260D
92674238001 785082PZ4WG-062323 SM 2320B-2011
92674238002 785082DUP01WG-062323 SM 2320B-2011
92674238003 785082RW5WG-062323 SM 2320B-2011
92674238001 783153PZ4WG-062323 SM 4500-S2D-2011
92674238002 783153DUP01WG-062323 SM 4500-S2D-2011
92674238003 783153RW5WG-062323 SM 4500-S2D-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2023 03:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 90
Page 60 of 90
Page 61 of 90
Page 62 of 90
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC.
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Report of Analysis
Pace Analytical Services,LLC
9800 Kincey Avenue
Suite 100
Huntersville,NC 28078
Attention:Matthew Brainard
Project Name:Pactiv Evergreen
Project Number:92674238
Lot Number:YF23032
Date Completed:06/26/2023
06/28/2023 3:47 PM
Approved and released by:
Project Coordinator 1:Jenna S.Holliday
Page 1 of 11
Page 63 of 90
PACE ANALYTICAL SERVICES,LLC
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Pace Analytical Services,LLC
Lot Number:YF23032
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.Where
sampling is conducted by the client,results relate to the accuracy of the information provided,and as the
samples are received.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace")
Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to
the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory;however,the following analyses are currently not listed on our TNI
scope of accreditation:Drinking Water:VOC (excluding BTEX,MTBE,Naphthalene,&1,2-
dichloroethane)EPA 524.2,E.coli and Total coliforms SM 9223 B-2004,Solid Chemical Material:TOC
Walkley-Black,Biological Tissue:All,Non-Potable Water:SGT-HEM EPA 1664B,Silica EPA 200.7,
Boron,Calcium,Silicon,Strontium EPA 200.8,Bicarbonate,Carbonate,and Hydroxide Alkalinity SM 2320
B-2011,SM 9221 C E-2006 &SM 9222D-2006,Strontium SW-846 6010D,VOC SM 6200 B-2011,Fecal
Coliform Colilert-18,PFAS by Isotope Dilution SOP.
Pace is a DoD/DoE and TNI accredited laboratory;however,Pace is not accredited for PFAS Direct
Aqueous Injection or Method D8421.
If you have any questions regarding this report,please contact the Pace Project Manager listed on the
cover page.
Page 2 of 11
Page 64 of 90
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical Services, LLC
Lot Number: YF23032

Project Name: Pactiv Evergreen
Project Number: 92674238
Sample Number Sample ID Matrix Date Sampled Date Received
001 06/23/2023 0815PZ4WG-062323 Aqueous 06/23/2023
002 06/23/2023 0815DUP01WG-062323 Aqueous 06/23/2023
003 06/23/2023 1010RW5WG-062323 Aqueous 06/23/2023
(3 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 11
Page 65 of 90
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical Services, LLC
Lot Number: YF23032

Project Name: Pactiv Evergreen
Project Number: 92674238
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 PZ4WG-062323 Aqueous Platinum-Cobalt Color SM 2120B-5000 color units 5
002 DUP01WG-062323 Aqueous Platinum-Cobalt Color SM 2120B-4000 color units 6
003 RW5WG-062323 Aqueous Platinum-Cobalt Color SM 2120B-2000 color units 7
(3 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 11
Page 66 of 90
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
PZ4WG-062323
YF23032-001
06/23/2023 0815
06/23/2023
Aqueous
Project Name: Pactiv Evergreen
Project Number: 92674238
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 1 06/23/2023 1708 MSG
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 5000 1color units5.05.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 11
Page 67 of 90
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
DUP01WG-062323
YF23032-002
06/23/2023 0815
06/23/2023
Aqueous
Project Name: Pactiv Evergreen
Project Number: 92674238
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 1 06/23/2023 1708 MSG
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 4000 1color units5.05.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 11
Page 68 of 90
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
RW5WG-062323
YF23032-003
06/23/2023 1010
06/23/2023
Aqueous
Project Name: Pactiv Evergreen
Project Number: 92674238
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 1 06/23/2023 1708 MSG
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 2000 1color units5.05.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 11
Page 69 of 90
QC Summary
QC Data for Lot Number: YF23032
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 11
Page 70 of 90
Chain of Custody
and
Miscellaneous Documents
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 11
Page 71 of 90
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 11
Page 72 of 90
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 11
Page 73 of 90
Thisreportshouldnotbereproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamplesincludedinthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,Inc.
1700 Elm Street
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
Client - Charlotte
PACE Charlotte
9800 Kincey Ave.
Huntersville NC 28078
REPORT OF
LABORATORY
ANALYSIS FOR
PCDD/PCDF
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
July 31, 2023
Pace Project #: 10661874
Sample Receipt Date: 07/19/2023
Client Project #: 92674238
Client Sub PO #: N/A
The report provided has been invoiced as a Level 2
PCDD/PCDF Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questionstoIsaac Johnson,your Pace
Project Manager.
State Cert #: 530
Suite 100
Report Prepared for:
Page 1 of 17Report No.....10661874_SW8290AFC_L2_dfr
July 31, 2023
Isaac Johnson, Project Manager
[phone]
[phone] (fax)
[e-mail]
Page 74 of 90
Pace Analytical Services,Inc.
1700 Elm Street
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
This report presents the results from the analyses performed on three samples submitted by a
representative of Pace Analytical Services, LLC. The samples were analyzed for the presence or absence
of polychlorodibenzo-p-dioxins (PCDDs) and polychlorodibenzofurans (PCDFs) using a modified version
of USEPA Method 8290A. The estimated detection limits (EDLs) were based on signal-to-noise
measurements. Estimated maximum possible concentration (EMPC) values were treated as positives in
the toxic equivalence calculations.
Second column confirmation analyses of 2,3,7,8-TCDF values obtained from the primary (DB5-MS)
column are performed only when specifically requested for a project and only when the values are above
the concentration of the lowest calibration standard. Typical resolution for this isomer using the DB5-MS
column ranges from 25-30%.
The isotopically-labeled PCDD/PCDF internal standards in the sample extracts were recovered at
28-86%. Except for four low values, which were flagged "R" on the results tables, the labeled internal
standard recoveries obtained for this project were within the 40-135% target range specified in Method
8290A. Since the quantification of the native 2,3,7,8-substituted congeners was based on isotope dilution,
the data were automatically corrected for recovery and accurate values were obtained.
Values were flagged "I" where incorrect isotope ratios were obtained. Concentrations below the calibration
range were flagged "J" and should be regarded as estimates.
A laboratory method blank was prepared and analyzed with the sample batch as part of our routine quality
control procedures. The results show the blank to contain trace levels of one or more selected congeners.
These levels were below the calibration range of the method. Sample concentrations similar to the
corresponding blank levels were flagged "B" on the results tables and may be, at least partially, attributed
to the background.
Laboratory spike samples were also prepared using clean reference matrix that had been fortified with
native standard materials. The results show that the spiked native compounds were recovered at
76-105% with relative percent differences of 0.0-18.8%. These results were within the target ranges for
the method. Matrix spikes were not prepared with the sample batch.
The responses obtained for selected labeled congeners in calibration standard analyses L230725A_15
and U230725A_18 were outside the target ranges. As specified in our procedures for this method, the
averages of the daily response factors for these compounds were used in the calculations for the samples
from these runshifts. The affected values were flagged "Y" on the results tables.
DISCUSSION
Page 2 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 75 of 90
REPORT OF LABORATORY ANALYSIS
This report shallnot bereproduced,except in full,
withoutthe written consentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Report No.....10660525
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 17Report No.....10661874_SW8290AFC_L2_dfr
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Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 77 of 90
Page 5 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 78 of 90
7/19/23
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Page 79 of 90
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Page 80 of 90
Page 8 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 81 of 90
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
A =

B =

C =

D =

E =

H2 =

I =

J =

L =

Nn =

P =

R =

S =

U =

V =

X =

Y =

* =
Reporting Limit based on signal to noise (EDL)

Less than 10x higher than method blank level

Result obtained from confirmation analysis

Result obtained from analysis of diluted sample

Exceeds calibration range

Extracted outside of holding time

Isotope ratio out of specification

Estimated value

Suppressive interference, analyte may be biased low

Value obtained from additional analysis

PCDE Interference

Recovery outside target range

Peak saturated

Analyte not detected

Result verified by confirmation analysis

%D Exceeds limits

Calculated using average of daily RFs

See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 82 of 90
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 83 of 90
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted% MoistureDry Weight Extracted
ICAL ID
CCal Filename(s)
Method Blank ID
Client's Sample ID PZ4WG-06232392674238001
L230725A_06
SMT
NA500 mL
NA
L230613
L230724A_17 & L230725A_15
BLANK-107396
MatrixDilutionCollected
Received
Extracted
Analyzed
WATERNA06/23/2023 08:15
07/19/2023 08:50
07/20/2023 10:52
07/25/2023 12:35
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF 45 4.2 2,3,7,8-TCDF-13C 2.00 61-----Total TCDF 94 4.2 2,3,7,8-TCDD-13C 2.00 55-----1,2,3,7,8-PeCDF-13C 2.00 412,3,7,8-TCDD ND 4.8 2,3,4,7,8-PeCDF-13C 2.00 45-----Total TCDD ND 4.8 1,2,3,7,8-PeCDD-13C 2.00 45-----1,2,3,4,7,8-HxCDF-13C 2.00 861,2,3,7,8-PeCDF -----6.2 1,2,3,6,7,8-HxCDF-13C 2.00 43IJ8.72,3,4,7,8-PeCDF 15 3.3 2,3,4,6,7,8-HxCDF-13C 2.00 81J-----Total PeCDF 39 3.3 1,2,3,7,8,9-HxCDF-13C 2.00 73J-----1,2,3,4,7,8-HxCDD-13C 2.00 781,2,3,7,8-PeCDD ND 3.7 1,2,3,6,7,8-HxCDD-13C 2.00 74-----Total PeCDD ND 3.7 1,2,3,4,6,7,8-HpCDF-13C 2.00 60-----1,2,3,4,7,8,9-HpCDF-13C 2.00 36 R
1,2,3,4,7,8-HxCDF -----5.9 1,2,3,4,6,7,8-HpCDD-13C 2.00 65IJ121,2,3,6,7,8-HxCDF ND 11 OCDD-13C 4.00 59-----Y2,3,4,6,7,8-HxCDF -----4.4 IJ5.01,2,3,7,8,9-HxCDF 9.8 6.4 1,2,3,4-TCDD-13C 2.00 NAJ-----Total HxCDF 9.8 4.4 1,2,3,7,8,9-HxCDD-13C 2.00 NAJ-----
1,2,3,4,7,8-HxCDD ND 7.2 2,3,7,8-TCDD-37Cl4 0.20 86-----1,2,3,6,7,8-HxCDD ND 4.9-----1,2,3,7,8,9-HxCDD ND 5.8-----Total HxCDD 17 4.9 BJ-----
1,2,3,4,6,7,8-HpCDF ND 18 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 26 Equivalence: 12 pg/L-----Total HpCDF ND 18 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD ND 7.4-----Total HpCDD 27 7.4 J-----
OCDF ND 18-----OCDD 140 32 J-----
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not Applicable
NC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank level
R =Recovery outside target range
I=Isotope ratio out of specification
Y =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 11 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 84 of 90
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted% MoistureDry Weight Extracted
ICAL ID
CCal Filename(s)
Method Blank ID
Client's Sample ID DUP01WG-06232392674238002
L230725A_07
SMT
NA505 mL
NA
L230613
L230724A_17 & L230725A_15
BLANK-107396
MatrixDilutionCollected
Received
Extracted
Analyzed
WATERNA06/23/2023 08:15
07/19/2023 08:50
07/20/2023 10:52
07/25/2023 13:20
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF 34 3.8 2,3,7,8-TCDF-13C 2.00 52-----Total TCDF 51 3.8 2,3,7,8-TCDD-13C 2.00 46-----1,2,3,7,8-PeCDF-13C 2.00 402,3,7,8-TCDD ND 2.9 2,3,4,7,8-PeCDF-13C 2.00 45-----Total TCDD ND 2.9 1,2,3,7,8-PeCDD-13C 2.00 46-----1,2,3,4,7,8-HxCDF-13C 2.00 741,2,3,7,8-PeCDF 13 5.2 1,2,3,6,7,8-HxCDF-13C 2.00 56J-----2,3,4,7,8-PeCDF 12 4.2 2,3,4,6,7,8-HxCDF-13C 2.00 70J-----Total PeCDF 35 4.2 1,2,3,7,8,9-HxCDF-13C 2.00 63J-----1,2,3,4,7,8-HxCDD-13C 2.00 671,2,3,7,8-PeCDD ND 2.8 1,2,3,6,7,8-HxCDD-13C 2.00 60-----Total PeCDD ND 2.8 1,2,3,4,6,7,8-HpCDF-13C 2.00 51-----1,2,3,4,7,8,9-HpCDF-13C 2.00 32 R
1,2,3,4,7,8-HxCDF 12 4.7 1,2,3,4,6,7,8-HpCDD-13C 2.00 54J-----1,2,3,6,7,8-HxCDF ND 5.0 OCDD-13C 4.00 50-----Y2,3,4,6,7,8-HxCDF ND 2.6-----1,2,3,7,8,9-HxCDF ND 4.3 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF 12 2.6 1,2,3,7,8,9-HxCDD-13C 2.00 NAJ-----
1,2,3,4,7,8-HxCDD -----3.2 2,3,7,8-TCDD-37Cl4 0.20 83IJ7.61,2,3,6,7,8-HxCDD ND 3.9-----1,2,3,7,8,9-HxCDD ND 3.7-----Total HxCDD 11 3.2 BJ-----
1,2,3,4,6,7,8-HpCDF ND 6.9 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 15 Equivalence: 9.4 pg/L-----Total HpCDF ND 6.9 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----7.3 IJ15Total HpCDD 28 7.3 J-----
OCDF ND 12-----OCDD -----23 IJ120
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not Applicable
NC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank level
R =Recovery outside target range
I=Isotope ratio out of specification
Y =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 12 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 85 of 90
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted% MoistureDry Weight Extracted
ICAL ID
CCal Filename(s)
Method Blank ID
Client's Sample ID RW5WG-06232392674238003
L230725A_08
SMT
NA506 mL
NA
L230613
L230724A_17 & L230725A_15
BLANK-107396
MatrixDilutionCollected
Received
Extracted
Analyzed
WATERNA06/23/2023 10:10
07/19/2023 08:50
07/20/2023 10:52
07/25/2023 14:06
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF 5.5 3.9 2,3,7,8-TCDF-13C 2.00 67J-----Total TCDF 5.5 3.9 2,3,7,8-TCDD-13C 2.00 54J-----1,2,3,7,8-PeCDF-13C 2.00 462,3,7,8-TCDD ND 2.5 2,3,4,7,8-PeCDF-13C 2.00 53-----Total TCDD ND 2.5 1,2,3,7,8-PeCDD-13C 2.00 49-----1,2,3,4,7,8-HxCDF-13C 2.00 701,2,3,7,8-PeCDF ND 4.7 1,2,3,6,7,8-HxCDF-13C 2.00 59-----2,3,4,7,8-PeCDF -----1.9 2,3,4,6,7,8-HxCDF-13C 2.00 71IJ3.4Total PeCDF ND 1.9 1,2,3,7,8,9-HxCDF-13C 2.00 60-----1,2,3,4,7,8-HxCDD-13C 2.00 601,2,3,7,8-PeCDD ND 2.7 1,2,3,6,7,8-HxCDD-13C 2.00 54-----Total PeCDD ND 2.7 1,2,3,4,6,7,8-HpCDF-13C 2.00 44-----1,2,3,4,7,8,9-HpCDF-13C 2.00 28 R
1,2,3,4,7,8-HxCDF -----2.8 1,2,3,4,6,7,8-HpCDD-13C 2.00 45IJ9.81,2,3,6,7,8-HxCDF ND 3.4 OCDD-13C 4.00 39-----RY2,3,4,6,7,8-HxCDF -----2.3 IJ4.31,2,3,7,8,9-HxCDF -----1.8 1,2,3,4-TCDD-13C 2.00 NAIJ5.5Total HxCDF ND 1.8 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 9.1 2,3,7,8-TCDD-37Cl4 0.20 83-----1,2,3,6,7,8-HxCDD ND 7.4-----1,2,3,7,8,9-HxCDD ND 5.3-----Total HxCDD ND 5.3-----
1,2,3,4,6,7,8-HpCDF -----6.7 Total 2,3,7,8-TCDDIJ8.51,2,3,4,7,8,9-HpCDF ND 16 Equivalence: 4.3 pg/L-----Total HpCDF ND 6.7 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD 55 6.1 J-----Total HpCDD 260 6.1-----
OCDF -----23 IJ33OCDD47030-----
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not Applicable
NC = Not Calculated
J = Estimated value
R =Recovery outside target range
I=Isotope ratio out of specification
Y =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 13 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 86 of 90
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL IDCCal Filename(s)
BLANK-107396
U230725A_06
SM
1020 mL
U230524U230725A_02 & U230725A_18
Matrix
Dilution
Extracted
Analyzed
Water
07/20/2023 10:52
07/25/2023 15:37
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKCR
Native
Isomers pg/L
Conc EMPC
pg/L pg/L
Internal
Standards Added
ng's Percent
Recovery
EDL
2,3,7,8-TCDF ND -----0.40 2,3,7,8-TCDF-13C 2.00 92Total TCDF ND -----0.40 2,3,7,8-TCDD-13C 2.00 881,2,3,7,8-PeCDF-13C 2.00 992,3,7,8-TCDD ND -----0.67 2,3,4,7,8-PeCDF-13C 2.00 84 YTotal TCDD ND -----0.67 1,2,3,7,8-PeCDD-13C 2.00 85 Y1,2,3,4,7,8-HxCDF-13C 2.00 122 Y1,2,3,7,8-PeCDF ND -----0.64 1,2,3,6,7,8-HxCDF-13C 2.00 492,3,4,7,8-PeCDF ND -----0.45 2,3,4,6,7,8-HxCDF-13C 2.00 106Total PeCDF ND -----0.45 1,2,3,7,8,9-HxCDF-13C 2.00 981,2,3,4,7,8-HxCDD-13C 2.00 991,2,3,7,8-PeCDD ND -----0.68 1,2,3,6,7,8-HxCDD-13C 2.00 102Total PeCDD ND -----0.68 1,2,3,4,6,7,8-HpCDF-13C 2.00 711,2,3,4,7,8,9-HpCDF-13C 2.00 491,2,3,4,7,8-HxCDF ND -----0.75 1,2,3,4,6,7,8-HpCDD-13C 2.00 861,2,3,6,7,8-HxCDF ND -----2.1 OCDD-13C 4.00 682,3,4,6,7,8-HxCDF ND -----0.601,2,3,7,8,9-HxCDF -----1.4 0.77 IJ 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF ND -----0.60 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD -----2.5 1.5 IJ 2,3,7,8-TCDD-37Cl4 0.20 791,2,3,6,7,8-HxCDD ND -----0.881,2,3,7,8,9-HxCDD ND -----1.4Total HxCDD 2.0 -----0.88 J
1,2,3,4,6,7,8-HpCDF ND -----3.1 Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----9.6 Equivalence: 0.39 pg/LTotal HpCDF ND -----3.1 (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD ND -----1.1Total HpCDD ND -----1.1
OCDF ND -----2.8OCDD6.6 -----4.0 J
Conc=Concentration (Totalsinclude2,3,7,8-substitutedisomers).
EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
I =Isotope ratio out of specification
Y =Calculated using average of daily RFs
EDL =EstimatedDetection Limit
Page 14 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 87 of 90
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL IDCCal Filename(s)
LCS-107397
F230726A_03
SMT
1000 mL
F230720F230726A_02 & F230726A_06
Matrix
Dilution
ExtractedAnalyzed
Water
07/20/2023 10:5207/26/2023 10:13
NA
Method Blank ID BLANK-107396
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's Percent
RecoveryIsomersStandardsAdded
%
Rec.(ng)(ng)
2,3,7,8-TCDF 0.20 0.17 2,3,7,8-TCDF-13C 2.0 7784Total TCDF 2,3,7,8-TCDD-13C 2.0 771,2,3,7,8-PeCDF-13C 2.0 732,3,7,8-TCDD 0.20 0.17 2,3,4,7,8-PeCDF-13C 2.0 7486Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 801,2,3,4,7,8-HxCDF-13C 2.0 921,2,3,7,8-PeCDF 1.0 0.83 1,2,3,6,7,8-HxCDF-13C 2.0 93832,3,4,7,8-PeCDF 1.0 0.85 2,3,4,6,7,8-HxCDF-13C 2.0 9485Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 861,2,3,4,7,8-HxCDD-13C 2.0 891,2,3,7,8-PeCDD 1.0 0.81 1,2,3,6,7,8-HxCDD-13C 2.0 9181Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 821,2,3,4,7,8,9-HpCDF-13C 2.0 721,2,3,4,7,8-HxCDF 1.0 0.88 1,2,3,4,6,7,8-HpCDD-13C 2.0 91881,2,3,6,7,8-HxCDF 1.0 0.91 OCDD-13C 4.0 63912,3,4,6,7,8-HxCDF 1.0 0.90 901,2,3,7,8,9-HxCDF 1.0 0.88 1,2,3,4-TCDD-13C 2.0 NA88Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 0.92 2,3,7,8-TCDD-37Cl4 0.20 76921,2,3,6,7,8-HxCDD 1.0 0.86 861,2,3,7,8,9-HxCDD 1.0 0.87 87Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.83 831,2,3,4,7,8,9-HpCDF 1.0 0.82 82Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.79 79Total HpCDD
OCDF 2.0 1.5 76OCDD2.0 1.6 82
Qs = Quantity Spiked
Qm = Quantity Measured
Rec.=Recovery (Expressedas Percent)
R=Recoveryoutsideof target range
Y =RF averaging used in calculations
Nn =Value obtained from additional analysis
NA = Not Applicable
*=See Discussion
Page 15 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 88 of 90
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL IDCCal Filename(s)
LCSD-107398
F230726A_04
SMT
1000 mL
F230720F230726A_02 & F230726A_06
Matrix
Dilution
ExtractedAnalyzed
Water
07/20/2023 10:5207/26/2023 10:58
NA
Method Blank ID BLANK-107396
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's Percent
RecoveryIsomersStandardsAdded
%
Rec.(ng)(ng)
2,3,7,8-TCDF 0.20 0.17 2,3,7,8-TCDF-13C 2.0 6787Total TCDF 2,3,7,8-TCDD-13C 2.0 671,2,3,7,8-PeCDF-13C 2.0 602,3,7,8-TCDD 0.20 0.18 2,3,4,7,8-PeCDF-13C 2.0 6392Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 671,2,3,4,7,8-HxCDF-13C 2.0 741,2,3,7,8-PeCDF 1.0 0.88 1,2,3,6,7,8-HxCDF-13C 2.0 76882,3,4,7,8-PeCDF 1.0 0.91 2,3,4,6,7,8-HxCDF-13C 2.0 8091Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 711,2,3,4,7,8-HxCDD-13C 2.0 531,2,3,7,8-PeCDD 1.0 0.86 1,2,3,6,7,8-HxCDD-13C 2.0 7286Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 561,2,3,4,7,8,9-HpCDF-13C 2.0 551,2,3,4,7,8-HxCDF 1.0 0.93 1,2,3,4,6,7,8-HpCDD-13C 2.0 73931,2,3,6,7,8-HxCDF 1.0 0.97 OCDD-13C 4.0 54972,3,4,6,7,8-HxCDF 1.0 0.98 981,2,3,7,8,9-HxCDF 1.0 0.94 1,2,3,4-TCDD-13C 2.0 NA94Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.1 2,3,7,8-TCDD-37Cl4 0.20 861051,2,3,6,7,8-HxCDD 1.0 0.95 951,2,3,7,8,9-HxCDD 1.0 1.1 105Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.87 871,2,3,4,7,8,9-HpCDF 1.0 0.89 89Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.79 79Total HpCDD
OCDF 2.0 1.6 78OCDD2.0 1.7 85
Qs = Quantity Spiked
Qm = Quantity Measured
Rec.=Recovery (Expressedas Percent)
R=Recoveryoutsideof target range
Y =RF averaging used in calculations
Nn =Value obtained from additional analysis
NA = Not Applicable
*=See Discussion
Page 16 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 89 of 90
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,
without thewrittenconsentof PaceAnalyticalServices,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Client
Spike 1 ID
Spike 1 Filename F230726A_03
LCS-107397
PACE Charlotte
Spike Recovery Relative Percent Difference (RPD) Results
Spike 2 ID
Spike 2 Filename F230726A_04
LCSD-107398
Method 8290A
Spike 1 Spike 2
Compound %REC %REC %RPD
2,3,7,8-TCDF 84 87 3.52,3,7,8-TCDD 86 92 6.71,2,3,7,8-PeCDF 83 88 5.82,3,4,7,8-PeCDF 85 91 6.81,2,3,7,8-PeCDD 81 86 6.01,2,3,4,7,8-HxCDF 88 93 5.51,2,3,6,7,8-HxCDF 91 97 6.42,3,4,6,7,8-HxCDF 90 98 8.51,2,3,7,8,9-HxCDF 88 94 6.61,2,3,4,7,8-HxCDD 92 105 13.21,2,3,6,7,8-HxCDD 86 95 9.91,2,3,7,8,9-HxCDD 87 105 18.81,2,3,4,6,7,8-HpCDF 83 87 4.71,2,3,4,7,8,9-HpCDF 82 89 8.21,2,3,4,6,7,8-HpCDD 79 79 0.0OCDF76782.6OCDD82853.6
%REC = Percent Recovered
RPD =The difference betweenthetwo valuesdivided by the mean value
Page 17 of 17Report No.....10661874_SW8290AFC_L2_dfr
Page 90 of 90