IH1473_20240131_Q4 2023 Progress Report and Technical Memorandum

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ENGINEERING | ENVIRONMENTAL | HEALTH & SAFETY | TECHNOLOGY 
12402 N. 56th Street | Tampa, Florida 33617 | P 813‐930‐0669 | F 813‐930‐9809 | www.ensafe.com 
January 31, 2024

Mr. Kenneth B. Rhame via email: [e-mail]
United States Environmental Protection Agency — Region 4
61 Forsyth Street S.W. #9
Atlanta, Georgia 30303

Re: Project Progress Report for Fourth Quarter 2023
Pactiv Evergreen — Canton Mill, Canton, North Carolina

Dear Mr. Rhame:

This progress report provides a summary of Time Critical Removal Action (TCRA) activities undertaken
by or on behalf of Pactiv Evergreen (PTVE) at the former Canton Mill (the Site) in Canton, North Carolina.
This report complies with the requirements of Section VIII.25 of the Administrative Settlement
Agreement and Order on Consent for Removal Action (AOC), CERCLA-04-2024-7000, effective
October 24, 2023. This report covers the fourth quarter (Q4) of 2023.

DESCRIPTION OF WORK COMPLETED
A detailed Action Tracker (log) of TCRA activities is provided on the project-specific SharePoint site.
The following TCRA field activities were performed during Q4 2023 (corresponding documents are listed
below in Submittals/Deliverables):

1. Completed a one-time, site-wide comprehensive groundwater and surface water sampling event
performed in September and October 2023, pursuant to the United States Environmental
Protection Agency (U.S. EPA) approved Interim Work Plan Addendum — Comprehensive
Sampling and Assessment of Black Liquor Impacts to Groundwater (EnSafe Inc., June 2023), to
assess impacts to groundwater and surrounding surface water bodies as a baseline for the black
liquor interim removal action required by the AOC.
2. Completed surface water sampling at the Campground Branch on October 2, 2023, per the
approved work plan.
3. Completed removal of submerged fuel oil from the Pigeon River per the approved work plan.
4. Completed the Fuel Oil Area Interim Removal Action per the U.S. EPA approved Interim Removal
Action Work Plan for Petroleum-Impacted Soils (EnSafe, August 14, 2023), including
aboveground storage tank (AST) removal, soil excavation and disposal, dewatering/treatment
and disposal, confirmatory soil sampling, grouting of sewer line in former AST bunker to the
levee manhole, grouting of the levee manhole, and restoration of work areas.

SUBMITTALS/DELIVERABLES
1. The following correspondence was issued or received by or on behalf of PTVE in Q4 2023:
a. Received the executed Administrative Settlement Agreement and AOC for
Removal Action, CERCLA-04-2024-7000, effective October 24, 2023.
Mr. Kenneth Rhame January 31, 2024
Page 2

b. Submitted the Implementation of Recovery of Submerged Oil Plan dated
November 1, 2023); U.S. EPA approved the submittal via email dated November 2, 2023.
c. Submitted the Health and Safety Plan, Revision 1 dated November 14, 2023, pursuant
to the AOC.
d. Submitted the Implementation of Interim Work Plan Addendum to Address Vertical
Delineation Data Gaps via Limited Subsurface Investigations dated December 11, 2023;
U.S. EPA approved the submittal via email dated December 27, 2023.
e. Submitted the Implementation of Interim Work Plan Addendum to Replace Monitoring
Well PZ-16 dated December 14, 2023; U.S. EPA approved the submittal January 24,
2024. SUMMARY OF SAMPLING RESULTS/TESTS
1. Attachment 1 provides the Technical Memorandum — Summary of 2023 Groundwater and
Surface Water Sampling (EnSafe, January 2024) documenting the work and results from the
site-wide sampling and Campground Branch surface water sampling efforts in September and
October 2023. Key takeaways include:
a. Groundwater, seep, and surface water contaminants of potential concern have been
resolved, and future monitoring (scope to be determined when applicable) can focus on
the known contaminants of concern (COCs) in groundwater and seeps; no COCs were
identified in surface water and toxicity testing indicates no adverse ecological impacts to
the Pigeon River.
b. Historical thinking regarding groundwater COCs have been disproved as follows: dioxins
and furans typically related to pulp/paper mills are not a concern in site groundwater;
and volatile organic compounds and semi-volatile organic compounds are not prevalent
in site groundwater and only a few of each are considered COCs.
c. Groundwater impacts are primarily within the shallow unconsolidated aquiferat the Site.
There is no evidence of groundwater communication between the surficial aquifer and
bedrock aquifer.

2. Confirmatory soil sampling results from the former Fuel Oil AST bunker area will be documented
in the Fuel Oil Area Interim Removal Summary Report scheduled for submittal in February 2024.
Only one of 23 confirmatory samples exhibited results above soil screening levels (and that
location could not be further excavated due to bunker wall/obstacle).

WORK ANTICIPATED IN FOLLOWING QUARTER
The following TCRA activities are planned for the first quarter of 2024 (January — March):

1. Continue implementing work and deliverables as required per the AOC.
2. Submit the Black Liquor Interim Removal Action Work Plan per Section VIII.16.b of the AOC.
3. Commence data gap filling activities to refine the black liquor interim removal action design
basis, per the U.S. EPA approved Implementation of Interim Work Plan Addendum to Address
Vertical Delineation Data Gaps via Limited Subsurface Investigations (EnSafe, December 2023).
This includes soil borings to assess vertical lithology, determine which hydrogeologic formation
Mr. Kenneth Rhame January 31, 2024
Page 3

exhibit black liquor residuals in groundwater, collection of specific hydrogeologic data, and
installation of wells for aquifer testing.
4. Replace monitoring well PZ-16 per the U.S. EPA approved Implementation of Interim Work Plan
Addendum to Replace Monitoring Well PZ-16 (EnSafe, December 2023).
5. Implement the Black Liquor Interim Removal Action Work Plan once approved by U.S. EPA in
consultation with the North Carolina Department of Environmental Quality.
6. Participate in periodic status calls/meetings with stakeholders.
7. Support U.S. EPA’s community relations and outreach as applicable.

ISSUES/RESOLUTIONS
None.

COMMUNITY RELATIONS
Provided data and information as applicable to support U.S. EPA and North Carolina Department of
Environmental Quality in response to community inquiries.

If you have questions or need additional information, please contact me at 813-734-7985.

Sincerely,
EnSafe Inc.

By: Bridget Morello, PE
Principal

Attachments:
Attachment 1 — Technical Memorandum — Summary of 2023 Groundwater and Surface Water
Sampling (EnSafe, January 2024)

cc: Alison Vincent, Project Coordinator, PTVE
Project-specific SharePoint site
313 Wingo Way Mount Pleasant, South Carolina 29464 843-884-0029 | 843-856-0107www.ensafe.com
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TECHNICAL MEMORANDUM
SUMMARY OF 2023 GROUNDWATER
AND SURFACE WATER SAMPLING
PACTIV EVERGREEN
CANTON MILL
CANTON, NORTH CAROLINA
EnSafe Project Number
0888834351/003
Prepared for:
Pactiv Evergreen
175 Main Street
Canton, North Carolina 28716
Draft January 2024
Final February 2024
i
TABLE OF CONTENTS
1.0 INTRODUCTION .............................................................................................................. 1
2.0 OBJECTIVES ................................................................................................................... 1
3.0 SITE DESCRIPTION AND REGULATORY HISTORY ............................................................. 2
4.0 SITE-WIDE COMPREHENSIVE SAMPLING ACTIVITIES ....................................................... 4
4.1 Well Inventory, Inspection, and Redevelopment ..................................................... 5
4.2 Professional Well Survey ....................................................................................... 5
4.3 Groundwater Level Gauging .................................................................................. 6
4.4 Groundwater Sample Collection ............................................................................. 6
4.5 Surface Water Sample Collection ........................................................................... 7
5.0 GROUNDWATER ANALYTICAL RESULTS ........................................................................... 9
5.1 pH and Color Results ............................................................................................ 9
5.1.1 pH .............................................................................................................. 9
5.1.2 Color ......................................................................................................... 10
5.2 Metals ............................................................................................................... 10
5.3 Volatile Organic Compounds ............................................................................... 15
5.4 Semi-Volatile Organic Compounds ....................................................................... 16
5.5 Dioxins and Furans ............................................................................................. 16
5.6 Anions ............................................................................................................... 16
5.7 Additional Analytes ............................................................................................. 17
6.0 SURFACE WATER ANALYTICAL RESULTS ........................................................................ 18
6.1 pH and Color ...................................................................................................... 18
6.2 Metals ............................................................................................................... 18
6.3 Volatile Organic Compounds ............................................................................... 18
6.4 Semi-Volatile Organic Compounds ....................................................................... 19
6.5 Anions ............................................................................................................... 19
6.6 General Chemistry .............................................................................................. 19
7.0 ADDITIONAL VOLUNTARY ASSESSMENT WORK .............................................................. 20
8.0 CONCLUSIONS AND TIME CRITICAL REMOVAL ACTION (TCRA) PLAN .............................. 22
9.0 REFERENCES ................................................................................................................ 25
FIGURES
Figure 3 Site Location Map
Figure 4-2 Wells Network Map (Revised)
Figure 4-3.1 Groundwater Potentiometric Map September 2023
Figure 4-3.2 Groundwater Potentiometric Map November 2023
Figure 4-5 Surface Water Sample Locations
Figure 5-1.1 Groundwater pH Isocontour Map
Figure 5-1.2 Groundwater Color Isocontour Map
Figure 5-2 Exceedances for Metals in Groundwater
Figure 5-3 Exceedances for VOCs in Groundwater
Figure 5-4 Exceedances for SVOCs in Groundwater

ii
Figure 5-6 Exceedances of Chloride and Sulfate Anions in Groundwater
Figure 6 Exceedances in Surface Water and Seeps

TABLES

Table 3-1 Regulatory Data Gap Inquiries and Relevant Action Item Status
Table 4-2 Well Survey Data
Table 4-3 Groundwater Elevations September and November 2023
Table 4-4.1 Groundwater Sample Locations
Table 4-4.2 Field Parameters in Groundwater Table 4-5 Field Parameters in Surface Water and Seeps
Table 5-1 pH and Color in Groundwater
Table 5-2 Metals in Groundwater
Table 5-3 VOCs in Groundwater
Table 5-4 SVOCs in Groundwater
Table 5-5 Dioxins and Furans in Groundwater
Table 5-6 Anions in Groundwater
Table 5-7 Additional Analytes and General Chemistry of Site Groundwater
Table 6-1 pH and Color in Surface Water and Seeps
Table 6-2 Metals in Surface Water and Seeps
Table 6-3 VOCs in Surface Water and Seeps
Table 6-4 SVOCs in Surface Water and Seeps
Table 6-5 Anions in Surface Water and Seeps
Table 6-6 General Chemistry and Sulfur in Surface Water and Seeps

APPENDICES

Appendix A Photo Log and Fieldwork Documentation
Appendix B Field Sampling Logs
Appendix C Laboratory Analytical Reports
Appendix D Additional Voluntary PFAS Sampling and Analysis Documentation

Technical Memorandum
Summary of 2023 Groundwater and Surface Water Sampling
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

1
1.0 INTRODUCTION
EnSafe Inc., on behalf of Pactiv Evergreen (Pactiv or PTVE), prepared this Technical Memorandum
to document the field activities, hydrogeologic conditions, and results of a one-time comprehensive
sampling event of groundwater and surface water at the Pactiv Evergreen Canton Mill (Site or Mill)
in September and October 2023. The activities were conducted pursuant to the Initial Site Work Plan
(EnSafe, April 2023), and associated Sampling and Analyses Plan and Quality Assurance Project Plan,
the Interim Work Plan Addendum — Comprehensive Sampling and Assessment of Black Liquor
Impacts to Groundwater (EnSafe. June 2023), the Sampling and Evaluation Work Plan for Surface
Water, Seep, and Sediment Sampling (TRC, October 2022), and the Campground Branch Sampling
Technical Memorandum (EnSafe, September 2023) – as approved by the United States Environmental
Protection Agency (U.S. EPA).

Any deviations from the approved work plans are noted within this Technical Memorandum and
were communicated to the U.S. EPA and the North Carolina Department of Environmental Quality
(NCDEQ) Division of Waste Management’s Superfund Section, Inactive Hazardous Sites Branch
(IHSB) as applicable. Activities also were executed in a manner consistent with industry standards
and in general accordance with the U.S. EPA Region 4, Laboratory Services and Applied Sciences
Division (LSASD), available at https://www.epa.gov/quality/quality-system-and-technical-
procedures-lsasd-field-branches.

2.0 OBJECTIVES
The one-time, comprehensive Site-wide sampling event was developed based on consultation with
U.S. EPA to assess impacts to groundwater and surrounding surface water bodies as a baseline for
the black liquor interim removal action. The goals of this one-time comprehensive sampling event
included:

• Ensure groundwater samples collected are representative of current aquifer conditions by
rehabilitating and redeveloping the existing well network prior to sampling.

• Establish a baseline data set for Site groundwater quality.

• Fulfill requirements of Notice of Violation (NOV)/Notice of Regulatory Requirements issued by
NCDEQ mandating low flow surface water monitoring of the Pigeon River.

• Assess surface water quality in Pigeon River and Campground Branch.
Technical Memorandum
Summary of 2023 Groundwater and Surface Water Sampling
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

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• Update relevant portions of the Conceptual Site Model based on new well survey data.

• Utilize results in design basis for remedial strategies.

This Technical Memorandum presents the sampling logs and analytical reports, as well as summary
tables and maps depicting exceedances of applicable groundwater and surface water standards.
Conclusions and recommendations based on these results are documented separately in the
Black Liquor Interim Removal Action Work Plan (EnSafe, January 2024).

This Technical Memorandum summarizes the impacts of historical releases of black liquor at the Site,
and is organized as follows:

Section 1: Introduction
Section 2: Objectives
Section 3: Site Description and Regulatory History
Section 4: Site-wide Comprehensive Sampling Activities
Section 5: Groundwater Analytical Results
Section 6: Surface Water Analytical Results
Section 7: Additional Voluntary Assessment Work
Section 8: Conclusions and Time Critical Removal Action Plan
Section 9: References

Figures, tables, and supporting appendices are included at the conclusion of the text.

3.0 SITE DESCRIPTION AND REGULATORY HISTORY
The Canton Paper Mill (Site) has operated in this location since 1908. The Site is bisected by the
Pigeon River and surrounded by the town of Canton, North Carolina as depicted in Figure 3. A release
of black liquor into the Pigeon River was reported to the North Carolina Department of Environment
and Natural Resources, now NCDEQ, in 1994 by Champion Paper, the owner of the Canton Mill at
that time. A series of Comprehensive Site Assessments was conducted by Champion Paper to assess
impacts to groundwater and included installation of the existing monitoring and recovery well
network. Initial efforts to contain black liquor and mitigate the seep included a pump and treat
system that proved to be ineffective for several reasons. In 1999, Champion Paper sold the Canton
Technical Memorandum
Summary of 2023 Groundwater and Surface Water Sampling
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

3
Mill to Carolina Paper Products which later became Blue Ridge Paper Products LLC. 1 Champion
retained liability for the black liquor release. International Paper (“IP”) purchased Champion in 2000.
From 2007 to present, IP conducted semi-annual groundwater monitoring targeting a limited analyte
suite (AECOM various dates). In 2007, Evergreen Packaging (now PTVE) purchased the Canton Mill
from Blue Ridge Paper Products, and has operated the Mill until it ceased operating in 2023.

A new observation of the original black liquor seep was reported to NCDEQ on January 28, 2022.
On April 11, 2022, NCDEQ Division of Water Resources (DWR) issued an NOV to IP requiring IP to
sample surface waters and sediments of the Pigeon River proximal to the black liquor seep as well
as to provide a summary of historical efforts to treat or contain impacted groundwater. The NCDEQ
IHSB followed up with the issuance of a Notice of Regulatory Requirements letter to IP on April 22,
2022, mandating a similar suite of assessment actions. NCDEQ DWR subsequently issued a NOV to
PTVE on October 20, 2022, which mirrored the requirements of the NOV sent to IP in April 2022.
In consultation with NCDEQ DWR prior to receiving the October 2022 NOV, PTVE submitted a
sampling plan on October 17, 2022, which was approved the following day by NCDEQ DWR, and
outlined both riverbank reconnaissance and sampling of surface water, seep(s), and sediments
(i.e., requirements 1 and 2 of the October 2022 NOV). PTVE implemented this work during the first
quarter of 2023; however, the plan did not include groundwater sampling. Aside from the focused
semiannual groundwater sampling events performed by IP, the most recent comprehensive Site-wide
groundwater sampling event was conducted in 1997 by Roy F. Weston Inc. as part of a Phase III
Site Assessment on behalf of Champion Paper.

The U.S. EPA began inquiries at the Site on or around March 24, 2023, and published a Removal Site
Evaluation (RSE) Pollution Report on July 6, 2023, recommending Time Critical Removal Actions at
the Site. Prior to U.S. EPA’s issuance of the RSE/Pollution Report, and in consultation with U.S. EPA
and NCDEQ, PTVE voluntarily began to assess potential impacts to groundwater associated with
historic releases of black liquor at the Site without the assistance of other potentially responsible
parties. PTVE ceased all operations at the Mill in June 2023, and has since completed removal of all
stored black liquor, interim removal action for No. 6 Fuel Oil pursuant to a separate work plan
approved by U.S. EPA, and general cleanup of the Site.

1 Blue Ridge Paper Products LLC is a wholly owned subsidiary of Pactiv Evergreen LLC
Technical Memorandum
Summary of 2023 Groundwater and Surface Water Sampling
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

4
U.S. EPA and Blue Ridge Paper Products entered into an Administrative Settlement Agreement and
Order on Consent for Removal Action (AOC) on October 24, 2023. Among other things, the AOC
requires a Black Liquor Interim Removal Action Work Plan.

Work completed by PTVE prior to the AOC execution included a Black Liquor Position Paper (EnSafe
May 2023) documenting the difficulty historical black liquor releases pose when attempting to
characterize contaminants of potential concern (COPCs) in Site groundwater by conventional
analytical methods. As such, PTVE conducted a trial run sampling and analyses event in June 2023
during which two of the more impacted Site wells (RW-05 and PZ-04) were sampled to ensure the
proposed analytical methods were viable to meet the objectives of the Interim Work Plan Addendum
— Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
(EnSafe, June 2023). Additionally, an upgradient well (PZ-21) was sampled as a quality control
measure for laboratory detection limit evaluation and comparison. The trial run indicated the
proposed analytical methods were effective and could achieve reasonable detection limits for
comparison of results to applicable standards. Therefore, the Interim Work Plan Addendum —
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater (EnSafe, June
2023) outlined a one-time, comprehensive Site-wide sampling event to further assess impacts to
groundwater and surrounding surface water bodies as a baseline for the black liquor interim removal
action required by the AOC. Table 3-1 provides an overview of regulatory inquiries regarding data
gaps and associated assessment activities completed or being addressed by PTVE pursuant to the
NOV and AOC.

In addition to the Site-wide assessment, and at the request of NCDEQ, PTVE voluntarily collected
groundwater samples at select wells and surface water samples at specific locations for laboratory
analyses of per- and polyfluoroalkyl substances (PFAS). These samples were split with NCDEQ as
part of a quality assurance plan for the project. The results of PFAS sampling are discussed in Section
7.

4.0 SITE-WIDE COMPREHENSIVE SAMPLING ACTIVITIES
Per the Interim Work Plan Addendum — Comprehensive Sampling and Assessment of Black Liquor
Impacts to Groundwater (EnSafe, June 2023) and based on consultation with U.S. EPA and NCDEQ,
the Site-wide assessment event included:

• Inspection and redevelopment/repair (as needed) of Site monitoring wells;

Technical Memorandum
Summary of 2023 Groundwater and Surface Water Sampling
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

5
• Hydraulic water level gauging and resurveying of all Site monitoring wells;

• Groundwater sampling and analyses of COPCs as well as additional parameters to aid in
removal action decision-making; and

• Surface water sampling and analyses of COPCs in the Campground (Camp) Branch inlet and
outfall at the Site.

4.1 Well Inventory, Inspection, and Redevelopment
Semi-annual monitoring events have been conducted at the Site by other contractors on behalf of IP
since February 2007, however, due to the unusual Site groundwater chemistry and relative age of
the well network, the down hole integrity of the existing well network was unknown. Given that the
objective of any groundwater monitoring event is to collect samples that are representative of the
current aquifer conditions, PTVE requested all of the Site wells be properly inspected and redeveloped
by a licensed drilling contractor. More robust rehabilitation efforts were implemented at recovery
well locations where scaling issues had been historically documented. A photo log and table
summarizing the well redevelopment and rehabilitation activities conducted by licensed driller,
SADEACO, is included as Appendix A. The noted well deficiencies will be addressed in consultation
with the appropriate agencies.

4.2 Professional Well Survey
During well inventory activities some irregularities were noted regarding the physical locations of
certain wells with respect to the position shown on historical maps, specifically PZ-20. PZ-20 was not
part of original well survey conducted during the Comprehensive Site Assessments in February 1995
by Hampton, Hintz and Associates, Inc. At that time, North Carolina registered land surveyors
typically utilized the North Carolina Geodetic Survey coordinate system for horizontal refence and
mean-sea-level as the vertical reference. To confirm the accuracy of the location and elevation of
each existing well a Professional Survey team from JMT was contracted to re-survey the well network
utilizing the North American Vertical Datum (NAVD 88) GRID coordinates in conjunction with more
advanced survey methods. The revised well locations and top of casing elevations collected during
this assessment are summarized in Table 4-2. Figure 4-2 depicts the well locations at the Site
pursuant to the current survey data.

Technical Memorandum
Summary of 2023 Groundwater and Surface Water Sampling
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

6
4.3 Groundwater Level Gauging
On September 12, 2023, EnSafe personnel collected depth-to-groundwater measurements from the
16 shallow and three bedrock monitoring wells, and the seven former recovery wells using an
electric water level meter. Depth-to-water was measured in units of feet (to the nearest 0.01 foot)
from the marked location on the top of the inner well riser and recorded. The measuring device
was decontaminated between each monitoring well prior to obtaining measurements to avoid
cross contamination.

A follow-up gauging event was conducted on November 15, 2023, to confirm the findings of the
September data set after water use at the Mill had ceased the week prior. The follow-up gauging
event was focused on the surficial aquifer and did not include measurements from the bedrock aquifer
nor PZ-14R, which was obstructed at the time. Groundwater elevation data collected from the two
gauging events are displayed in Table 4-3. Maps depicting the potentiometric surface elevation and
inferred groundwater flow direction from September and November are attached as Figures 4-3.1
and 4-3.2 respectively.

4.4 Groundwater Sample Collection
From September 13 through September 21, 2023, EnSafe personnel collected groundwater samples
from the existing monitoring well network for laboratory analyses of COPCs and/or other parameters
as noted in Table 4-4.1.

The sample collected from RW-5 on September 20, 2023, was rejected by the laboratory due to
matrix interference and the well was subsequently re-sampled October 17, 2023, and submitted for
a limited analyte suite that would affect the performance of the laboratory equipment. The locations
of the wells included in the site-wide event are shown on Figure 4-2.

Prior to sampling, the wells were purged using the tubing-in-screened-interval/low-flow method with
a peristaltic pump in accordance with U.S. EPA SOP SESDPROC-301-R4 and SESDPROC-203-R4.
During the purging process, the following field parameters were recorded and monitored for
stabilization as specified in U.S. EPA SOP SESDPROC-111-R4:

• Dissolved Oxygen — U.S. EPA SOP LSASDPROC-106-R4
• Oxidation-Reduction Potential — U.S. EPA SOP LSASDPROC-113-R3
• pH — U.S. EPA SOP LSASDPROC-100-R5
• Specific Conductance — U.S. EPA SOP LSASDPROC-101-R7
• Temperature — U.S. EPA SOP SESDPROC-102-R5
Technical Memorandum
Summary of 2023 Groundwater and Surface Water Sampling
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

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• Turbidity — U.S. EPA SOP LSASDPROC-103-R5
• Sulfide — HACH Method 8131
• Ferrous Iron — HACH Method 8146

Once parameters stabilized, representative groundwater samples were collected into laboratory-
supplied bottles and placed immediately into coolers with ice. The samples were delivered or shipped
under a strict chain of custody to Pace Analytical Laboratories, LLC, a NCDEQ-certified laboratory, for
analysis as prescribed in the Interim Work Plan Addendum — Comprehensive Sampling and
Assessment of Black Liquor Impacts to Groundwater (EnSafe. June 2023); which included:

• VOCs by SW-846 Method 8260D
• SVOCs by SW-846 Method 8270E
• Metals by SW-846 Method 6010D
• Dissolved Metals (Field-Filtered) by SW-846 Method 6010D
• Mercury (total and dissolved) by SW-846 Method 7470A
• Boron (total and dissolved) by SW-846 Method 200.7
• Color by Standard Method 2120B
• Alkalinity by Standard Method 2320B
• Anions by SW-846 Method 9056
• Sulfide by SW-846 Method 4500S2-D
• Dioxins/Furans by SW-846 8290A

A summary of groundwater field measurements is displayed in Table 4-4.2. The field sampling logs
are included in Appendix B.

4.5 Surface Water Sample Collection
Surface water samples were collected from locations along the Pigeon River and Camp Branch at
locations depicted in Figure 4.5. Field measurements for select parameters were captured during
sample collection from both surface water bodies and are displayed in Table 4-5. Turbidity readings
were not collected at SW-UP and SW-DOWN locations due to logistical and safety concerns.

Samples from the Pigeon River were collected in accordance with the Sampling and Evaluation Work
Plan for Surface Water, Seep, the Sediment Sampling Plan (SWS Plan TRC, October 2022), which
prescribed two sampling events representative of variable seasonal flow conditions. Historical data
from the USGS Canton, North Carolina gauging station (#03456991) located upstream of the Site
Technical Memorandum
Summary of 2023 Groundwater and Surface Water Sampling
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

8
indicate higher flow regimes occur at the Pigeon River during the winter months and lower flow
conditions are typically observed in the early fall. The initial surface water sampling event was
conducted the week of January 9 to 13, 2023 by TRC personnel and was representative of higher
seasonal flow conditions with the river gauge averaging 2.4 feet at a flow rate of 550 cubic feet per
second. No black liquor seeps were observed during the January 2023 sampling event.

The second surface water sampling event conducted by EnSafe on September 20, 2023, was
representative of low river level and flow. In fact, the river level was near its historic low with the
USGS gauge reading 1.47 feet at a flow rate of 82.5 cubic feet per second. Black liquor was
observed along the east bank of the Pigeon River just downstream from the chip bridge (Seep 1)
and immediately upriver from the from the Mill rail-road bridge to the north (Seep 2) during
this event. Samples were collected via disposable syringes from both visible seeps during the
September 20 event.

At the request of NCDEQ and U.S. EPA additional surface water samples were collected on
October 2, 2023, from a small tributary of the Pigeon River referred to as Camp Branch. The creek
originates in the higher elevations east of the Mill campus, and currently enters a culvert immediately
upstream of the Mill flowing beneath the Site until it discharges into the Pigeon River downstream of
the railroad bridge. Samples were collected upstream of the Mill where the creek enters the culvert
and downstream of the Mill at the culvert outfall prior to mixing with waters of the Pigeon River.
The Camp Branch samples were analyzed for contaminants of concern specific to black liquor
pursuant to the U.S. EPA-approved Campground Branch Sampling Technical Memorandum (EnSafe,
September 2023). The field sampling logs for both surface water sampling events are included
in Appendix B.

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

9
5.0 GROUNDWATER ANALYTICAL RESULTS
Samples from the 27 existing monitoring wells were analyzed pursuant to the Interim Work Plan
Addendum — Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
(EnSafe, June 2023) with the following exceptions:

• The sample collected from RW-05 on September 20, 2023, was rejected by the laboratory
due to matrix interference and the well was subsequently re-sampled October 17, 2023 and
submitted for a more limited analyte suite that would not affect the performance of the
laboratory equipment.

• The volume of groundwater collected from BR-02 was insufficient to run the full suite of
analyses prescribed.

• A field decision was made to omit select analyses based on sample volumes required for a
particular laboratory method.

Laboratory results for the various analyte suites were screened against the North Carolina
Groundwater Quality Standards, Title 15A, North Carolina Administrative Code, Chapter 02,
Subchapter L, Section .0202, April 2022 (hereafter North Carolina 02L GWQS or NC2L) and are
discussed in greater detail in the sections below. Groundwater analytical results are summarized in
Tables 5-1 through 5-7. Laboratory analytical reports are presented in Appendix C.

5.1 pH and Color Results
When observed at the Site together, elevated pH and color measurements can be indicative of the
presence of black liquor in groundwater. A summary of pH and color results is presented in Table 5-1
and exceedances of NC2L GWQS are outlined below.

5.1.1 pH
The acceptable range for pH in groundwater pursuant to the NC2L standards is between 6.5 to 8.5
SU. Exceedances of the prescribed values of pH that may indicate the presence of black liquor
impacts to Site groundwater can be found in Table 5-1 and were measured at the following locations:

BR-01 (6.45), BR-03 (8.73), PZ-02 (10.13), PZ-03 (8.84), PZ-04 (10.94), PZ-05 (5.99), PZ-07
(8.90), PZ-08 (10.07), PZ-09 (5.66), PZ-11 (9.13), PZ-12 (9.02), PZ-17 (6.01), PZ-18 (6.3),
PZ-21 (5.97), RW-04 (10.28), RW-05 (12.15), and RW-07 (6.03)
Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

10
An iso-contour map depicting the distribution of pH values in exceedance of the NC2L standard is
presented as Figure 5-1.1.

5.1.2 Color
Measurements for color were identified at the laboratory and recorded as color units (CU). The NC2L
standard for color in groundwater is 15 CU. The locations below exceeded the NC2L standard of
15 CU for color in groundwater:

BR-01 (160) BR-03 (200), PZ-1 (375), PZ-2 (16,000), PZ-03 (2,000), PZ-04 (5,000), PZ-07
(16,000), PZ-08 (350 J), PZ-11 (9,000), PZ-12 (7,500), PZ-18 (500), PZ-20 (250), RW-01 (100)
RW-02 (4,000) RW-03 (875) RW-04 (1,500), and RW-05 (2,000).

An iso-contour map depicting the distribution of color concentrations in exceedance of the NC2L
standard is presented as Figure 5-1.2.

5.2 Metals
Several metals have been shown in prior sampling to be indicative of black liquor. These metals
largely originate in the wood processed at the Site to make paper but are concentrated in the process.
Groundwater samples were analyzed for total and dissolved metals as prescribed, except Bedrock
Well BR-02 where insufficient sample volume necessitated omitting analysis for dissolved metals.
A summary of the metals detected in groundwater can be viewed in Table 5-2. Figure 5-2 depicts
exceedances of NC2L standards in Site groundwater.

Metals were detected in exceedance of NC2L standards in all but one monitoring well (i.e., PZ-05),
and while some may stem from the Mill process, others are likely representative of natural aquifer
conditions at the Site and surrounding area. The list below reflects those total and dissolved metals
in exceedance of NC2L standards — all units are milligrams per liter (mg/L).

BR-01
Chromium total — 0.32; dissolved — 0.22
Cobalt total — 0.019 J (where J = flagged as estimated by the laboratory); dissolved — 0.021 J
Manganese total — 9.8; dissolved — 11.7
Nickel total — 0.55; dissolved — 0.4
Vanadium total — 0.0095 J

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

11
BR-02
Antimony total — 0.0071 J
Chromium total — 0.0912
Cobalt total — 0.0081 J
Manganese total — 0.216
Vanadium total — 0.0273

BR-03
Cobalt total — 0.0017 J; dissolved — 0.0022 J
Manganese — 0.097
Vanadium total — 0.11; dissolved — 0.1

PZ-01
Manganese total — 3.6; dissolved — 3.1
Vanadium total — 0.0463; dissolved — 0.0356

PZ-02
Arsenic total — 0.025 J; dissolved — 0.016
Chromium total — 0.04; dissolved — 0.029
Cobalt total — 0.0086 J; dissolved — 0.006 J
Iron total — 15.4; dissolved — 10.1
Manganese total — 0.13; dissolved — 0.089
Nickel total — 0.19; dissolved — 0.14
Vanadium total — 0.55; dissolved — 0.4

PZ-03
Chromium total — 0.0175; dissolved — 0.0146
Cobalt total — 0.0025 J; dissolved — 0.0017 J
Manganese total — 1.39; dissolved — 1.21
Vanadium total — 0.227; dissolved — 0.174

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

12
PZ-04
Antimony dissolved — 0.0179
Arsenic total — 0.254; dissolved — 0.297
Chromium total — 0.118; dissolved — 0.115
Cobalt total — 0.0036 J; dissolved — 0.004 J
Iron total — 5.09; dissolved — 3.55
Manganese total — 0.0823
Mercury total — 0.0032; dissolved — 0.0036
Nickel total — 0.117
Vanadium total — 1.32; dissolved — 1.34

PZ-05
No Exceedances

PZ-06
Cobalt total — 0.0019 J; dissolved — 0.0018 J
Manganese total — 3.2; dissolved — 2.8

PZ-07
Arsenic total — 0.021 J; dissolved — 0.013 J
Beryllium total — 0.0078 J; dissolved — 0.0057 J
Chromium total — 0.22; dissolved — 0.2
Cobalt total — 0.014 J; dissolved — 0.01 J
Iron total — 22.7; dissolved — 18.1
Lead total — 0.039 J; dissolved — 0.033
Manganese total — 0.12; dissolved — 0.086
Nickel total — 0.15; dissolved — 0.12
Vanadium total — 0.96; dissolved — 0.8

PZ-08
Chromium total — 0.0108
Cobalt total — 0.0031 J; dissolved — 0.0012 J
Vanadium total — 0.0389; dissolved — 0.0238

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

13
PZ-09
Cobalt total — 0.0013 J

PZ-11
Arsenic total — 0.046 J; dissolved — 0.06
Barium total — 0.72
Chromium total — 0.17; dissolved — 0.15
Cobalt dissolved — 0.0052 J
Manganese total — 0.23; dissolved — 0.18
Vanadium total — 0.84; dissolved — 0.73

PZ-12
Arsenic total — 0.042; dissolved — 0.042
Chromium total — 0.17; dissolved — 0.15
Cobalt total — 0.0035 J; dissolved — 0.003 J
Manganese total — 0.18; dissolved — 0.15
Vanadium total — 0.96; dissolved — 0.81

PZ-13
Cobalt total — 0.01; dissolved — 0.0078 J
Manganese total — 0.26; dissolved — 0.25

PZ-14R
Manganese total — 0.25; dissolved — 0.25

PZ-17
Manganese total — 2.43; dissolved — 2.07

PZ-18
Cobalt total — 0.0016 J; dissolved — 0.0033 J
Manganese total — 0.63; dissolved — 0.61

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

14
PZ-20
Cobalt total — 0.0027 J
Manganese total — 0.799; dissolved — 0.824
Vanadium total — 0.0178; dissolved — 0.0094 J

PZ-21
Cobalt total — 0.0012 J
Manganese total — 0.833; dissolved — 0.648

RW-01
Manganese total — 1.57; dissolved — 1.32
Vanadium total — 0.0115

RW-02
Chromium total — 0.0424; dissolved — 0.0135
Cobalt total — 0.0248 J; dissolved — 0.0158
Vanadium total — 0.556; dissolved — 0.423
Zinc total — 2.86; dissolved — 2.0

RW-03
Vanadium total — 0.0977; dissolved — 0.0577

RW-04
Arsenic total — 0.0303; dissolved — 0.0296
Chromium total — 0.0499; dissolved — 0.0334
Cobalt total — 0.0037 J; dissolved — 0.0017 J
Manganese total — 0.161; dissolved — 0.0725
Vanadium total — 0.493; dissolved — 0.322

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

15
RW-05
Arsenic total — 0.286 J; dissolved — 0.613
Boron total — 2.37 J; dissolved — 4.42
Chromium total — 0.191 J; dissolved — 0.219 J
Iron total — 3.86
Lead total — 0.278 J
Manganese total — 0.137 J
Nickel total — 0.146 J; dissolved — 0.257
Vanadium total — 1.24; dissolved — 1.91
Zinc total — 1.78

RW-06
Cobalt dissolved — 0.0012 J
Manganese total — 0.673; dissolved — 0.687

RW-07
Cobalt dissolved — 0.0012 J
Manganese total — 0.453; dissolved — 0.508

5.3 Volatile Organic Compounds
Volatile organic compounds (VOCs) were analyzed because one or more of these compounds was
reported in prior testing. Groundwater samples were analyzed for VOCs by U.S. EPA Method 8260.
Laboratory results indicate exceedances of NC2L standards for only three VOCs at six wells and one
duplicate sample. Table 5-3 displays a summary of the VOCs detected in Site groundwater. Figure
5-3 depicts the spatial extent of VOCs exceedances. The exceedances are listed below in micrograms
per liter and compared to their respective NC2L standard in parentheses.

PZ-02 Benzene — 10 (1)
PZ-06 Trichloroethene — 6.8 (3)
PZ-12 Benzene — 1.1 J (1)
PZ-14R (and duplicate) 2-Hexanone — 89.2 (40), Benzene — 106 (1)
RW-01 Benzene — 2.7 (1)
RW-04 Benzene — 1.3 J (1)

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

16
5.4 Semi-Volatile Organic Compounds
One or more semi-volatile compounds (SVOCs) were reported in prior tests. Groundwater samples
were analyzed for SVOCs by U.S. EPA Method 8270. Laboratory results indicate exceedances of NC2L
standards for only four SVOCs at six wells and two duplicate samples. Table 5-4 displays a summary
of the SVOCs detected in Site groundwater. Figure 5-4 depicts the spatial extent of SVOCs
exceedances. The exceedances are listed below in micrograms per liter and compared to their
respective NC2L standard in parentheses.

PZ-02 Phenol — 49.1 J (30)
PZ-08 Naphthalene — 15.1 (6)
PZ-12 Acenaphthene — 87.7 (80), Naphthalene — 108 (6)
PZ-14R (and duplicate) Naphthalene — 13.2 (6)
PZ-17 (duplicate only) bis(2-Ethylhexyl)phthalate — 4.4 J (3)
RW-04 Naphthalene — 130 (6)
RW-05 Naphthalene — 225 (6)

5.5 Dioxins and Furans
The Mill’s original bleaching process utilized elemental chlorine which could have generated dioxins
and furans. The mill converted its bleaching process to the use of chlorine dioxide in the early 1990’s.
Dioxin has been non-detect in the Canton Mill effluent since 1989. The presence of dioxins and furans
was evaluated to assess whether the legacy bleaching process contributed such contaminants to Site
groundwater. Groundwater samples were analyzed for Dioxins and Furans by U.S. EPA Method 8290.
Nine analytes were detected in the groundwater samples, ranging from 0.75 to 39,000 picograms
per liter (pg/L). No exceedances of NC2L standards were reported. Table 5-5 displays a summary
of the dioxins and furans results for Site groundwater.

5.6 Anions
Chlorides and sulfates have been reported in prior tests and are known to occur in black liquor.
Therefore, groundwater samples were analyzed for chloride and sulfate by U.S. EPA Method SW9056
for all sample locations except PZ-08 and PZ-09 which were analyzed by U.S. EPA Method E300 due
to a laboratory oversight. Insufficient sample volume from BR-02 and sample rejection of RW-05 by
the laboratory precluded analysis for anions at these locations. The NC2L standard for both chloride
and sulfate is 250 mg/L. A summary of the anion data set is attached in Table 5-6. Sample locations
where analytical results indicate exceedance of the standards are listed below and depicted spatially
in Figure 5-6.

BR-01 Chloride 15,900; Sulfate 540
BR-03 Chloride 8,910; Sulfate 500
Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

17
PZ-01 Chloride 282
PZ-02 Chloride 1,360
PZ-04 Chloride 4,960; Sulfate 824
PZ-08 Chloride 2,670
PZ-12 Chloride 1,530; Sulfate 630
RW-03 Sulfate 490
RW-04 Sulfate 432

5.7 Additional Analytes
To gain a more thorough understanding of the Site groundwater chemistry in support of removal
action options evaluation, additional analytical parameters were deemed appropriate at select
locations and are listed below. Data for each of the additional analyte suites is presented in Table 5-7.
North Carolina Water Quality Standards only exist for two of the additional parameters tested (Nitrate
at 10 mg/L and Fluoride at 2 mg/L) and data indicate neither threshold was exceeded.

General Chemistry Suite
Biochemical Oxygen Demand (BOD) via Method SM 5210B
Chemical Oxygen Demand (COD) via Method SM 5220D
Carbon (Total) via Method SM 5310B
Total Kjeldahl Nitrogen (TKN) via Method E351.2
Nitrate (as N) via Method E351.2
Oil and Grease, Gravimetric via Method 1664B
Alkalinity (as CaCO3) via Method SM 2320B
Total Dissolved Solids (TDS) via Method SM 2540C
Total Suspended Solids (TSS) via Method SM 2540D
Sulfide via Method SM 4500S
Dissolved gases (methane, ethane, and ethene) via Method RSK175
Diesel Range Organics/Gasoline Range Organics (C6-C12) via Method SW8015
Additional Anions — bromide and fluoride via Method E300
Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

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6.0 SURFACE WATER ANALYTICAL RESULTS
The nine Pigeon River surface water samples collected on September 20, 2023, were analyzed for
pH, color, metals, VOCs, SVOCs, select anions, and a suite of general chemistry analytes.
The additional surface water samples collected on October 2, 2023, from two locations along Camp
Branch and were analyzed pursuant to the Campground Branch Sampling Technical Memorandum
(EnSafe, September 2023). Analytical results were compared to the most recent North Carolina
Surface Water Quality Standards for Class C waterways, Title 15A, North Carolina Administrative
Code, Subchapter 02B, Section .0211, dated September 2022 (hereafter North Carolina 02B, NC2B,
or SWQS). The laboratory reports are included in Appendix B. Analytical results are summarized on
Tables 6-1 through 6-6. Sample locations and any exceedances or deviations from the applicable
NC2B surface water standards are depicted in Figure 6.

6.1 pH and Color
Values for pH and True Color derived for surface water samples are presented in Table 6-1.
Measurements for pH should fall between 6 — 9 standard units per NC2B standards. Values for pH
outside of that range were measured at Seep01 (10.2 J) and Seep02 (9.3 J). North Carolina has not
established a surface water standard for True Color.

6.2 Metals
Surface water analytical results for metals are displayed in Table 6-2. Concentrations of dissolved
metals indicated four exceedances when compared to NC2B standards (using default hardness
values) as noted below with the standard in parentheses and are depicted in Figure 6.

Pigeon River
SEEP-01 — Copper — 3.7 J (2.7); Zinc — 50.7 (36)
SEEP-02 — Copper — 4.2 J (2.7)

Camp Branch Outfall (CBOF) — Lead — 2.2 (0.54)

6.3 Volatile Organic Compounds
Laboratory results for VOCs in surface water are summarized in Table 6-3. Data indicate no
exceedances of NC2B standards for VOCs were detected in the Pigeon River or Camp Branch samples.

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

19
6.4 Semi-Volatile Organic Compounds
Laboratory results for SVOCs in surface water are summarized in Table 6-4. Data indicate
no exceedances of NC2B standards for SVOCs were detected in the Pigeon River or
Camp Branch samples.

6.5 Anions
Surface water samples were analyzed for chloride and sulfate and results are presented in Table 6-5.
Values for chloride did not exceed the NC2B standard of 230 mg/L; and North Carolina has not
established a standard for sulfate in surface water.

6.6 General Chemistry
Pursuant to the individually approved work plans, samples from the Pigeon River and Camp Branch
were analyzed for the following general chemistry parameters: Ammonia (as N), nitrogen, phenolics,
total recoverable, alkalinity (as CaCO3), total dissolved solids (TDS), chemical oxygen demand, and
orthophosphate. Additionally, samples from the culvert upstream and the outfall of Camp Branch
were tested for sulfur. The results of the general chemistry suite of analytes are summarized in
Table 6-6. The State of North Carolina has not set surface water quality standards for these general
chemistry parameters.
Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

20
7.0 ADDITIONAL VOLUNTARY ASSESSMENT WORK
In addition to the one-time, comprehensive Site-wide sampling to assess impacts to groundwater
and surrounding surface water bodies as a baseline for the black liquor interim removal action, PTVE
voluntarily agreed to a request from the NCDEQ and sampled groundwater at select wells for
laboratory analyses of PFAS. This PFAS assessment work was not associated with or required by the
TCRA. The selected sampling locations were mutually agreed to by U.S. EPA and NCDEQ as
representative sample locations for this effort.

The NCDEQ request stemmed from its Action Strategy for assessing the presence of PFAS in North
Carolina (https://www.deq.nc.gov/news/key-issues/emerging-compounds/action-strategy-pfas).
NCDEQ has not yet established criteria for PFAS in any media. Therefore, the purpose of the one-
time PFAS groundwater sampling effort was to evaluate presence of PFAS for future consideration.

PFAS are human-made chemicals found in many products used by consumers and industry, and can
be discharged or released to soil, groundwater, surface water, and air. However, no processes at
the Canton Mill were associated with PFAS chemicals.

PFAS are contaminants of emerging concern in some communities, and rules and regulations for
PFAS assessment and remediation are under development by U.S. EPA and states. U.S. EPA has
concluded that some PFAS may adversely impact human health, and has issued health advisories and
proposed drinking water maximum contaminant levels (MCLs) for specific PFAS; however, scientific
research is ongoing regarding toxicity and risk. Human health and ecological risk-based criteria have
not yet been developed.

PFAS are analyzed in a laboratory using methods approved by U.S. EPA. Results for liquid samples
(e.g., groundwater, surface water) are reported in units called parts per trillion (ppt). A ppt is a
miniscule amount. One ppt is equivalent to one drop of water in an Olympic-sized swimming pool
(one drop in pool containing about 660,000 gallons of water).

The samples for PFAS analyses were collected by EnSafe on behalf of PTVE, and split samples were
provided to NCDEQ for redundant analyses by their contract analytical laboratory. Groundwater
sampled were collected at wells PZ-04, PZ-21, RW-01 and RW-05; surface water samples were
collected at the Town of Canton’s water intake for its drinking water plant and a location downgradient
of the Site. The results from this voluntary PFAS sampling effort are summarized in Appendix D,
Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

21
including tabulated results and laboratory analytical reports (for EnSafe and NCDEQ split samples).
The takeaways from the PFAS sampling effort include:

• Groundwater – PFAS results ranged from non-detect to 101 ppt. A few groundwater samples
exceeded the U.S. EPA’s proposed MCLs for PFOS and PFOA including the upgradient location
considered representative of background conditions. PFAS detections in groundwater at the
Former Canton Mill are low levels similar to results NCDEQ observed for more than half of the
drinking water plant taps across North Carolina that were sampled in 2022. The NCDEQ split
sample results ranged from non-detect to 273 ppt.

• Surface Water – One PFAS was detected in surface water samples; result was 0.779 J ppt for
PFOS (which is an estimated result below the laboratory reporting limit). The NCDEQ split
sample results were all non-detect.

• The PFAS detected in Site groundwater and surface water are common, terminal stable PFAS
that have been commonly detected in many water bodies across the nation, and are not likely
associated with Canton Mill processes.

• The analytical results from the split sample analyses by NCDEQ are comparable to the results
obtained for PTVE’s samples. There are some variations in reported concentrations and
reporting limits, but none of the results indicate repeat sampling is necessary.

No further sampling for PFAS is planned for this Site at this time.
Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

22
8.0 CONCLUSIONS AND TIME CRITICAL REMOVAL ACTION (TCRA) PLAN
The results from this one-time, Site-wide, comprehensive sampling event served as a baseline for
the evaluation of options for the black liquor interim removal action, and enabled identification of
data gaps to be addressed. The overall conclusions from the summary of groundwater and surface
water data collected in 2023 include:

• Groundwater, seep, and surface water COPCs have been resolved, and future monitoring
(scope to be determined when applicable) can focus on the known contaminants of concern
(COCs) which include:

 Groundwater COCs – color, pH, chloride, sulfate, specific metals total and dissolved
(as listed in Section 5.2), specific VOCs (2-hexanone, benzene and trichloroethene),
and specific SVOCs (acenaphthene, bis(2-ethylhexyl)phthalate, naphthalene,
and phenol). Dioxins and furans were not detected at levels above NC2L standards,
but will remain as COCs while further evaluation/discussion of potential toxicity is
performed in coordination with U.S. EPA and NCDEQ.
 Seep COCs – pH, copper, zinc, and lead; and results dissipate within feet of the seeps.
 Surface Water COCs – None, surface water samples exhibited no detections above
SWQS. In addition, toxicity testing data (for water flea and minnows) do not indicate
any adverse ecological impacts to the Pigeon River based on comparison of
surface water quality data and sediment sample data to U.S. EPA Region 4 ecological
screening values.

• As noted above, and as expected, pH, color, chlorides, sulfates, and some metals were found
in black liquor impacted groundwater and will remain COCs for planned TCRA activities.

• COCs have been clarified and do not include:

 VOCs and SVOCs – are not widespread in Site groundwater and only a few of each,
principally benzene and naphthalene, are considered COCs as listed above.
 PAHs – Groundwater results for PAHs potentially stemming from former Fuel Oil No.
6 releases at the Site suggest there is no commingling of lack liquor COCs and Fuel
Oil components.

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

23
• Groundwater impacts are primarily within the shallow unconsolidated aquifer at the Site within
cobble and saprolitic zones. There is no evidence of groundwater communication between
the surficial aquifer and bedrock aquifer.

• The findings of the original (1990s) and 2023 receptor surveys and 2023 site-wide assessment
of groundwater and surface water confirm that potential receptors are limited and the legacy
releases of black liquor from the Site to the Pigeon River pose minimal current risk to potential
receptors based on the following: 1) groundwater beneath the Site is not a potable water
source, 2) no private potable water wells are located within a 0.5-mile radius of the Site, 3)
no industrial production wells are located at or in the vicinity of the Site, 4) potable and
industrial water is supplied to the area surrounding the Mill by the Canton, and 5) municipal
water service is the source of potable water to this area.

• The only surface water bodies in proximity to the Site are the Pigeon River and the
Campground Branch which was partially converted from a swale to a 72-inch concrete storm
sewer as it crosses the eastern portion of the Site. Groundwater flows from the Site toward
the Pigeon River. Stormwater collected from the Site flows either to the Campground
Branch/storm sewer and discharges to the Pigeon River, or to the WWTP via other Mill sewers.

• Surface water data and toxicity testing demonstrate that the black liquor seeps have not
degraded the Pigeon River water quality, and results meet NCDEQ’s Surface Water Quality
Standards in Title 15A North Carolina Administrative Code, Subchapter 2B.

The additional voluntary sampling of Site groundwater for PFAS was not associated with or required
by the AOC for the TCRA. Results presented in Section 7 show some PFAS detections in groundwater
and surface water. There are no U.S. EPA or NCDEQ regulatory criteria or requirements for PFAS
assessment or remediation at this time.

The Black Liquor Interim Removal Action Work Plan was submitted to U.S. EPA on January 22, 2024,
per the AOC. That work plan included an updated conceptual site model using the results
documented in this Technical Memorandum, and the TCRA Plan to address data gaps and develop
the final design for the selected black liquor removal action to meet the AOC objectives.

The anticipated schedule for implementation of the TCRA Plan was provided in Table 5 of the Black
Liquor Interim Removal Action Work Plan. The conceptual site model will continue to be refined as
Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

24
data gaps are filled. The final design for the black liquor interim removal action will be developed
once data gaps are filled and any U.S. EPA comments on the original work plan have been resolved.

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

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9.0 REFERENCES
AECOM/Earth Tech. Semi-Annual Groundwater Sampling Reports, Pactiv Evergreen Site.
Various Dates.

— Groundwater Sampling Plan, to North Carolina Department of Environment and
Natural Resources. 2006, November 28.

EnSafe Inc. Technical Memorandum Summary of Response Actions. Pactiv Evergreen Canton Mill,
Canton, North Carolina. March 2023.

— Initial Work Plan (i.e., Fuel Oil Investigation Work Plan). Pactiv Evergreen Canton Mill,
Canton, North Carolina. April 2023.

— Initial Quality Assurance Project Plan (i.e., Fuel Oil Investigation Quality Assurance
Project Plan). Pactiv Evergreen Canton Mill, Canton, North Carolina. April 2023.

— Initial Sampling and Analysis Plan (i.e., Fuel Oil Investigation Sampling and
Analysis Plan). Pactiv Evergreen Canton Mill, Canton, North Carolina. April 2023.

— Initial Health and Safety Plan (i.e., Fuel Oil Investigation Health and Safety Plan).
Pactiv Evergreen Canton Mill, Canton, North Carolina. April 2023.

— Position Paper — Assessment of Black Liquor Impacts to Groundwater.
Pactiv Evergreen Canton Mill, Canton, North Carolina. May 2023

— Interim Work Plan Addendum — Comprehensive Sampling and Assessment of Black
Liquor Impacts to Groundwater. Pactiv Evergreen Canton Mill, Canton, North Carolina.
June 2023

— Limited Groundwater Monitoring Report – June 2023 “Trial Run” Event. Pactiv
Evergreen Canton Mill, Canton, North Carolina. August 2023.

— Implementation of Interim Work Plan Addendum for Site-Wide Groundwater Sampling
and Monitoring Well Rehabilitation and Redevelopment Protocols at the Pactiv
Evergreen Corporation — Canton Mill, Canton, North Carolina. August 2023.

Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

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— Campground Branch Sampling Technical Memorandum (for Surface Water Sampling
at two locations along Campground Branch), at the Pactiv Evergreen Corporation —
Canton Mill, Canton, North Carolina. September 2023.

— Black Liquor Interim Removal Action Work Plan. Pactiv Evergreen Canton Mill, Canton,
North Carolina. January 2024.

International Paper. North Carolina Department of Environment and Natural Resources Meeting
Agenda. 2003, February 20.

— Path forward on the corrective action at the Blue Ridge Paper Products, Inc. Site,
Canton Haywood County Letter from Mr. Thomas C. Richardson to Mr. Qu Qi,
North Carolina Department of Environment and Natural Resources. 2006, March 27.

— Voluntary Cleanup Checklist for Blue Ridge Paper Products, Inc. Site, Canton Haywood
County Letter from Mr. Thomas C. Richardson to Mr. Collin Day, North Carolina
Department of Environment and Natural Resources. 2007, October 31.

— Response to Notice of Regulatory Requirements - Blue Ridge Paper Products, Inc. Site,
Canton Haywood County, Groundwater Incident #12680 Letter from Mr. Thomas C.
Richardson to Mr. Kim Caulk, North Carolina Department of Environment and
Natural Resources. 2008, May 23.

North Carolina Department of Environmental Quality (formerly Department of Environment and
Natural Resources) Asheville Regional Office to IP Groundwater Sampling Plan — Approval.
2006, December 21.

— North Carolina Department of Environmental Quality IHSB Letter to International
Paper RE; Requirements for Containment Assessment and Cleanup (Agency
Restructuring & Voluntary Cleanup/REC Program). 2007, September 21.

— Notice of Regulatory Requirements to International Paper. 2008, March 17.

— Notice of Regulatory Requirements to International Paper. 2022, April 22.

— Notice of Violation to Pactiv Evergreen. 2022, October 20.
Technical Memorandum
Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
February 2024

27

— Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L,
Section.0202, Groundwater Quality Standards (NC 02L GWQS). April 2022

— Title 15A, North Carolina Administrative Code, Subchapter 02B, Section .0211, Surface
Water Quality Standards (NC 02B SWQS). September 2022

Roy. F. Weston, Inc. Groundwater Assessment at the Canton Pulp and Paper Mill.
1994, December 15.

— Comprehensive Site Assessment Report Canton Pulp and Paper Mill, Canton
North Carolina. 1995, June 1.

— Comprehensive Site Assessment Addendum Report Canton Pulp and Paper Mill,
Canton North Carolina. 1996, January 18.

— Comprehensive Site Assessment Phase III Report Canton Pulp and Paper Mill,
Canton North Carolina. 1997, July 10.

United States Environmental Protection Agency. Quality System and Technical Procedures for
LSASD Field Branches. https://www.epa.gov/quality/quality-system-and-technical-
procedures-lsasd-field-branches. Last Update 2022, February 7.

— Enforcement Action Memorandum - Evergreen Packaging Site, Canton North Carolina.
2023, October 18.

— Administrative Settlement Agreement and Order on Consent for Removal Action -
Evergreen Packaging Site, Canton North Carolina. 2023, October 24.

Figures
FIGURE
SITE LOCATION MAP
PACTIV EVERGREEN CANTON MILL
CANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:LEGEND
APPROXIMATE SUBJECT PROPERTY BOUNDARY
Source: U.S. Geological Survey. Canton Quadrangle, North Carolina[Map]. Photorevised 2022. 1:24,000. 7.5 Minute Series.
TD
NR
11/27/2023
0888834351
0 1,000 2,000
SCALE IN FEET
o
NAD 1983 STATE PLANE
NORTH CAROLINA FEET
&
&
&&
&
&
&&
&
&&&
&&
&
&
&
&
&
&
&
&
&
&
&
&
&
PZ-5
RW-1
BR-1 PZ-14R
PZ-6
PZ-7
PZ-9 PZ-21
PZ-8
BR-3
PZ-2
PZ-1
BR-2RW-2
RW-3
PZ-3
PZ-13
RW-4
RW-5
RW-6
PZ-12
RW-7
PZ-11
PZ-20
PZ-4
PZ-17
PZ-18
C
FIBERVILLE RD STATE RD 1643
FIGURE
WELLS NETWORK MAP (REVISED)
PACTIV EVERGREEN CANTON MILL
CANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:LEGEND
&WELL LOCATION
Source: Google Earth Pro Imagery - 04/2022
TD
MS
11/27/2023
0888834351
0 100 200
SCALE IN FEET
o
NAD 1983 STATE PLANE
NORTH CAROLINA FEET
&
&
&&
&
&
&&
&
&&&
&&
&
&
&
&
&
&
&
&
&
&
&
&
&
ÛÚ
ÛÚ
ÛÚ
FIBERVILLE RD
STAT
579
2
PZ-5
2575.00
RW-1
2567.76
BR-1
2492.63
PZ-14R
2570.06
PZ-6
2573.36
PZ-7
2578.99
PZ-9
2577.86 PZ-21
2581.88
PZ-8
2577.70
BR-32573.65
PZ-2
2578.45
PZ-1
2570.00
BR-2
2482.40
RW-2
2568.54
RW-3
2567.38 PZ-3
2572.40
PZ-13
2579.39
RW-4
2569.57
RW-5
2571.50
RW-6
2571.09
PZ-12
2574.44
RW-7
2572.70
PZ-11
2577.19
PZ-20
2581.74
PZ-4
2576.88
PZ-17
2574.31
PZ-18
2575.95
2572.49
2570.00
2566.20
2565.00
FIGURE
GROUNDWATER POTENTIOMETRIC MAP
SEPTEMBER 2023
PACTIV EVERGREEN CANTON MILL
CANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:
LEGEND
&WELL LOCATION
ÛÚ RIVER ELEVATIONMEASUREMENT LOCATION
POTENTIOMETRIC SURFACE CONTOUR
(DASHED WHERE INFERRED)
GROUNDWATER FLOW LINE
Source: Google Earth Pro Imagery - 04/2022
TD
NR
12/5/2023
0888834351
0 100 200
SCALE IN FEET
o
NAD 1983 STATE PLANE
NORTH CAROLINA FEET
&
&
&&
&
&
&&
&
&&&
&&
&
&
&
&
&
&
&
&
&
&
&
&
&
ÛÚ
ÛÚ
ÛÚ
FIBERVILLE RD
STAT
PZ-5
2574.09
RW-1
2567.37
BR-1
NM
PZ-14R
NM
PZ-6
2572.73
PZ-7
2578.23
PZ-9
2577.20 PZ-21
2580.81
PZ-8
2576.96
BR-3
NM
PZ-2
2577.75
PZ-1
2569.43
BR-2
NMRW-2
2568.05
RW-3
2567.02 PZ-3
2571.78
PZ-13
2579.17
RW-4
2569.08
RW-5
2571.06
RW-6
2570.27
PZ-12
2574.25
RW-7
2572.69
PZ-11
2576.26
PZ-20
2581.60
PZ-4
2576.28
PZ-17
2574.44
PZ-18
2575.54
2572.49
2570
2566.20
2565
FIGURE
GROUNDWATER POTENTIOMETRIC MAP
NOVEMBER 2023
PACTIV EVERGREEN CANTON MILL
CANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:
LEGEND
&WELL LOCATION
ÛÚ RIVER ELEVATIONMEASUREMENT LOCATION
POTENTIOMETRIC SURFACE CONTOUR
(DASHED WHERE INFERRED)
GROUNDWATER FLOW LINE
Source: Google Earth Pro Imagery - 04/2022
TD
NR
12/5/2023
0888834351
0 100 200
SCALE IN FEET
o
NAD 1983 STATE PLANE
NORTH CAROLINA FEET
#*
#*
!(
!(!(
!(
!(!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
ED
ED
ED
ED
ED
ED
ED
@A
@A@A
!(
!(
!(
!(
!(
!(
BR-2 BR-3
PZ-5
RW-1
BR-1
PZ-14R PZ-6
PZ-7
PZ-9 PZ-21
PZ-8
PZ-2PZ-1RW-2
RW-3 PZ-3
PZ-13
RW-4
RW-5
RW-6
PZ-12
RW-7
PZ-11
PZ-20
PZ-4
PZ-17
PZ-18
SW-UP
SW-01
SW-02
SW-DOWN
SEEP-01
Camp Branch
Outfall(CBOF)
SEEP-02
Camp Branch
Upstream
(CBUS)
N MAIN ST
FIGURE
SURFACE WATER SAMPLEL OCATIONS
PACTIV EVERGREEN CANTON MILL
CANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:
LEGEND
!(SURFACE WATER SAMPLE LOCATION
#*SEEP SAMPLE LOCATION
!(PIEZOMETER
ED RECOVERY WELL
@A BEDROCK MONITORING WELL
RIVER FLOW DIRECTION
Source: Google Earth Pro Imagery - 04/2022
TD
NR
11/30/2023
0888834351
0 200 400
SCALE IN FEET
o
NAD 1983 STATE PLANE
NORTH CAROLINA FEET
&
&
&&
&
&
&&
&
&&&
&&
&
&
&
&
&
&
&
&
&
&
&
&
&
#*
#*
BR-1
BR-3BR-2
PZ-5
5.99
64.1
RW-1
7.17
-210.4 PZ-14R
6.6
-110.3
PZ-66.59
-11.9
PZ-7
8.90
-89.6
PZ-9
5.66
133.1
PZ-21
5.97
114.9
PZ-8
10.07
-311.4
PZ-2
10.13
-341.3PZ-1
8.25
-181.8
RW-2
6.82
-90.7
RW-3
6.61
-108.7 PZ-3
8.84
-267.8
PZ-13
6.54
36.7
RW-4
10.28
-372.2
RW-5
12.15
-533.3
RW-6
6.81
-16
PZ-12
9.02
-234.7
RW-7
6.03
64.8
PZ-119.13
-224.5
PZ-20
7.82
-228.5
PZ-4
10.94-432
PZ-17
6.01
49
PZ-18
6.3
-89.7
SEEP-01
9.3J
-269.6
SEEP-02
10.2J
35.3
STATE RD 1643
12 11
10
9
8
FIGURE -1.1
GROUNDWATER H ISOCONTOUR MAP
PACTIV EVERGREEN CANTON MILL
CANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:
LEGEND
&WELL LOCATION #*SEEP pH CONTOURS
Source: Google Earth Pro Imagery - 04/2022
TD
NR
12/5/2023
0888834351
0 100 200
SCALE IN FEET
o
NAD 1983 STATE PLANE
NORTH CAROLINA FEETNOTE- ORANGE = ORP IN
MEGAVOLTS (mV)pH IN STANDARD UNITS (SU)
1 2 3 4 5 6 7 8 9 10 11 12 13 14
&
&
&&
&
&
&&
&
&&&
&&
&
&
&
&
&
&
&
&
&
&
&
&
&
#*
#*
1000
5000
500
100
50 15
BR-1
BR-3BR-2 PZ-1
375
-181.8
PZ-55 U
64.1
RW-1
100
-210.4
PZ-14R
10
-110.3
PZ-610
-111.9
PZ-7
16000
-89.6
PZ-9
5 U
133.1
PZ-21
5
114.9
PZ-8
350 J
-311.4
PZ-2
16000
-341.3RW-2
4000
-90.7
RW-3
875
-108.7 PZ-3
2000
-267.8
PZ-13
15
36.7
RW-4
1500
-372.2
RW-5
2000
-533.3
RW-6
5
-16
PZ-12
7500-234.7
RW-7
5 U
64.8
PZ-11
9000
-224.5
PZ-20250
-228.5
PZ-4
5000-432
PZ-17
5 U
49
PZ-18
500
-89.7
SEEP-01
250
-269.6
SEEP-02
200
-35.3
10000
5000
1000
500
50
15
100
50
15
100
1000500
FIGURE -1.2
GROUNDWATER COLOR ISOCONTOUR MAP
SEPTEMBER 2023PACTIV EVERGREEN CANTON MILL
CANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:
LEGEND
&WELL LOCATION #*SEEP COLOR CONTOURS, DASHED WHERE INFERRED
Source: Google Earth Pro Imagery - 04/2022
TD
NR
12/8/2023
0888834351
0 100 200
SCALE IN FEET
o
NAD 1983 STATE PLANE
NORTH CAROLINA FEET
COLOR BY SM2120B-2011 COLOR IN PLATINUM COBALT UNITS
15 50 100 500 1000 5000 10000
NOTES- ORANGE = ORP IN MEGAVOLTS (mV)- J = ESTIMATED CONCENTRATION- U = NOT DETECTED AT THE
NUMERICAL DETECTION LIMIT
#*
#*
!(
!(!(
!(
!(!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
ED
ED
ED
ED
ED
ED
ED
@A
@A@A
!(
!(
!(
!(
!(
!(
BR-2 BR-3
SEEP-02pH - 9.3 J (6-9)
Copper - 4.2 J (2.7)
SEEP-01
pH - 10.2 J (6-9)
Copper - 3.7 J (2.7)
Zinc - 50.7 (36)
Camp Branch
Outfall (CBOF)
Lead - 2.2 (0.54)
PZ-5
RW-1 BR-1 PZ-14R
PZ-6
PZ-7
PZ-9 PZ-21
PZ-8
PZ-2PZ-1RW-2
RW-3 PZ-3
PZ-13
RW-4
RW-5
RW-6
PZ-12
RW-7
PZ-11
PZ-20
PZ-4
PZ-17
PZ-18
SW-UP
SW-01
SW-02
SW-DOWN
Camp Branch
Upstream
(CBUS)
FIGURE 6
NC 02B SWQS EXCEEDANCES IN
SURFACE WATER AND SEEPS
CLASS C WATER BODY EXCEEDANCES
PACTIV EVERGREEN CANTON MILLCANTON, NORTH CAROLINA
REQUESTED BY:
DATE:
PROJECT:
DRAWN BY:
LEGEND
!(SURFACE WATER
SAMPLE LOCATION
#*SEEP SAMPLE LOCATION
!(PIEZOMETER
ED RECOVERY WELL
@A BEDROCK MONITORING WELL
RIVER FLOW DIRECTION
Source: Google Earth Pro Imagery - 04/2022
TD
RC
1/12/2024
0888834351
0 200 400
SCALE IN FEET
o
NAD 1983 STATE PLANE
NORTH CAROLINA FEET
NOTES- DISSOLVED METALS IN MICROGRAMS PER LITER
- J = ESTIMATED VALUE
- PIGEON RIVER SAMPLES COLLECTED 9/20/23- CAMP BRANCH SAMPLES COLLECTED 10/02/23
- pH IN STANDARD UNITS
- (XX) = NC2B SW STANDARDS

Tables
Table 3-1
Regulatory Data Gap Inquiries and Action Item Status
Pactive Evergreen Canton Mill
Canton, North Carolina
Data Gap Inquiry Action Item
Ensure adequate laboratory detection limits achievable given complex sample matrix
Well Inventory Survey, Redevelopment and Rehabilitation, August 2023
Accuracy of existing well location and elevation surveys Professional Survey of all wells conducted in September 2023
Comprehensive Baseline Data Set for Groundwater and Surface Water
Assessment of Black Liquor Impacts to Groundwater (EnSafe, June 2023)
Ongoing groundwater monitoring is performed by IP semi-annually in response to historical NOV and reported NCDEQ IHSB (AECOM August 2023 is
Pigeon River water quality for various seasonal river conditions
Surface water and seep sampling was completed in September 2023 under low river flow/level conditions per the approved Interim Work Plan Addendum Comprehensive Sampling and Assessment of Black Liquor Impacts to Groundwater (EnSafe, June 2023)
Surface water sampling under high river flow/level conditions was completed by others in January 2023 (TRC, Jan 2023) along with toxicity
Campground Branch (Camp Branch) water quality Camp Branch surface water sampling event and evaluation of historical sewer installation in place of native feature; sampled upstream and outfall of
Status of potential black liquor sources within the Site Mill ceased operations in June 2023, and all stored black liquor was removed from the Site as part of the decommissioning process
Vertical delineation of black liquor in the subsurface and confirmation of Site Data gap filling to commence in January 2024 per the approved Interim Work Plan Addendum to Address Vertical Delineation Data Gaps via Limited
Identify contaminants of potential concern (COPCs) in groundwater related to historical
black liquor use/release at the Mill CSA data sets associated with the 1994 CSA Work Plan. Summary of black composition and COPCs Consensus was outlined in the Black Liquor Position
Page 1 of 1
Table 4-2
Well Survey Data
Pactiv Evergreen Canton Mill
Canton, North Carolina
BR-1 Bedrock 672421.31 856573.20 2582.73 672476.76 856644.34 2582.54
BR-2 Bedrock 672237.64 856490.14 2583.42 672292.88 856560.94 2583.39
BR-3 Bedrock 672239.98 856755.52 2584.67 672295.535 856826.641 2584.46
PZ-1 Shallow 672209.15 856493.91 2583.38 672268.84 856570.76 2583.32
PZ-2 Shallow 672226.71 856753.35 2584.63 672282.41 856824.25 2584.53
PZ-3 Shallow 671950.96 856599.12 2582.53 672006.38 856670.14 2582.29
PZ-4 Shallow 671757.76 857052.53 2581.62 671813.51 857123.76 2581.43
PZ-5 Shallow 672767.77 856517.40 2584.29 672823.20 856588.19 2585.24
PZ-6 Shallow 672450.45 856720.63 2581.20 672505.93 856791.48 2583.02
PZ-7 Shallow 672327.41 857257.71 2583.54 672383.15 857328.61 2583.03
PZ-8 Shallow 672067.83 857256.45 2582.00 672123.67 857327.61 2581.90
PZ-9 Shallow 672178.33 857412.95 2582.48 672234.06 857483.78 2583.21
PZ-11 Shallow 671570.29 857252.06 2581.25 671626.34 857323.20 2581.15
PZ-12 Shallow 671390.25 856995.59 2582.48 671446.20 857066.99 2583.37
PZ-13 Shallow 672015.82 856790.36 2585.18 672071.42 856861.44 2584.79
PZ-14R Shallow 672422.13 856579.47 2582.66 672479.16 856651.08 2582.52
PZ-16 Shallow 671187.21 856952.07 2581.16 Abandoned Abandoned Abandoned
PZ-17 Shallow 671115.43 857193.39 2583.20 671171.27 857264.19 2585.73
PZ-18 Shallow 671438.82 857457.85 2585.20 671494.94 857529.14 2581.83
PZ-20 Shallow 671738.64 856957.13 2581.87 671904.99 856922.68 2584.10
PZ-21 Shallow 672152.98 857706.24 2581.67 672216.39 857771.94 2587.25
RW-1 Recovery 672458.74 856380.64 2582.54 672514.25 856451.81 2581.68
RW-2 Recovery 672219.68 856380.29 2581.61 672274.97 856451.36 2580.84
RW-3 Recovery 671985.00 856427.98 2580.96 672040.31 856498.94 2579.93
RW-4 Recovery 671807.39 856524.08 2581.46 671862.98 856595.14 2579.97
RW-5 Recovery 671642.98 856636.53 2581.46 671698.32 856707.54 2580.51
RW-6 Recovery 671478.65 856764.52 2582.54 671534.19 856835.69 2581.42
RW-7 Recovery 671284.91 856896.34 2583.25 671340.46 856967.505 2582.19
Notes:
ft = feet
amsl = above mean sea level
btoc = below top of casing
TOC = top of casing
btoc = bottom from top of casing
* = Coordinates Not Available / Estimated TOC Elevation
Updated
Northing
Updated
Easting
Updated TOC
Elevation
(ft amsl)
Well Identification Type Historical
Northing Historical Easting
Historical
TOC Elevation
(ft amsl)
Page 1 of 2
Table 4-2
Well Survey Data
Pactiv Evergreen Canton Mill
Canton, North Carolina
Depth to Water
(ft btoc)
GW Elevation
(ft amsl)
Depth to Water from
TOC (ft)
GW Elevation
(ft amsl)
BR-1 2582.54 89.91 2492.63 NM NM
BR-2 2583.39 100.99 2482.40 NM NM
BR-3 2584.46 10.81 2573.65 NM NM
PZ-1 2583.32 13.32 2570.00 13.89 2569.43
PZ-2 2584.53 6.08 2578.45 6.78 2577.75
PZ-3 2582.29 9.89 2572.40 10.51 2571.78
PZ-4 2581.43 4.55 2576.88 5.15 2576.28
PZ-5 2585.24 10.24 2575.00 11.15 2574.09
PZ-6 2583.02 9.66 2573.36 10.29 2572.73
PZ-7 2583.03 4.04 2578.99 4.80 2578.23
PZ-8 2581.90 4.20 2577.70 4.94 2576.96
PZ-9 2583.21 5.35 2577.86 6.01 2577.20
PZ-11 2581.15 3.96 2577.19 4.89 2576.26
PZ-12 2583.37 8.93 2574.44 9.12 2574.25
PZ-13 2584.79 5.40 2579.39 5.62 2579.17
PZ-14R 2582.52 12.46 2570.06 NM NM
PZ-16 Abandoned Abandoned Abandoned Abandoned Abandoned
PZ-17 2585.73 11.42 2574.31 11.29 2574.44
PZ-18 2581.83 5.88 2575.95 6.29 2575.54
PZ-20 2584.10 2.36 2581.74 2.50 2581.60
PZ-21 2587.25 5.37 2581.88 6.44 2580.81
RW-1 2581.68 13.92 2567.76 14.31 2567.37
RW-2 2580.84 12.30 2568.54 12.79 2568.05
RW-3 2579.93 12.55 2567.38 12.91 2567.02
RW-4 2579.97 10.40 2569.57 10.89 2569.08
RW-5 2580.51 9.01 2571.50 9.45 2571.06
RW-6 2581.42 10.33 2571.09 11.15 2570.27
RW-7 2582.19 9.49 2572.70 9.50 2572.69
Notes:
ft = feet
amsl = above mean sea level
btoc = below top of casing
TOC = top of casing
* = Coordinates Not Available / Estimated TOC Elevation
NM = not measured
Well Identification Updated TOC Elevation
(ft amsl)
September 12, 2023 November 15, 2023
Page 2 of 2
Table 4-3
Well Survey Data
Pactiv Evergreen Canton Mill
Canton, North Carolina
Depth to Water
(ft btoc)
GW Elevation
(ft amsl)
Depth to Water from
TOC (ft)
GW Elevation
(ft amsl)
BR-1 2582.54 89.91 2492.63 NM NM
BR-2 2583.39 100.99 2482.40 NM NM
BR-3 2584.46 10.81 2573.65 NM NM
PZ-1 2583.32 13.32 2570.00 13.89 2569.43
PZ-2 2584.53 6.08 2578.45 6.78 2577.75
PZ-3 2582.29 9.89 2572.40 10.51 2571.78
PZ-4 2581.43 4.55 2576.88 5.15 2576.28
PZ-5 2585.24 10.24 2575.00 11.15 2574.09
PZ-6 2583.02 9.66 2573.36 10.29 2572.73
PZ-7 2583.03 4.04 2578.99 4.80 2578.23
PZ-8 2581.90 4.20 2577.70 4.94 2576.96
PZ-9 2583.21 5.35 2577.86 6.01 2577.20
PZ-11 2581.15 3.96 2577.19 4.89 2576.26
PZ-12 2583.37 8.93 2574.44 9.12 2574.25
PZ-13 2584.79 5.40 2579.39 5.62 2579.17
PZ-14R 2582.52 12.46 2570.06 NM NM
PZ-16 Abandoned Abandoned Abandoned Abandoned Abandoned
PZ-17 2585.73 11.42 2574.31 11.29 2574.44
PZ-18 2581.83 5.88 2575.95 6.29 2575.54
PZ-20 2584.10 2.36 2581.74 2.50 2581.60
PZ-21 2587.25 5.37 2581.88 6.44 2580.81
RW-1 2581.68 13.92 2567.76 14.31 2567.37
RW-2 2580.84 12.30 2568.54 12.79 2568.05
RW-3 2579.93 12.55 2567.38 12.91 2567.02
RW-4 2579.97 10.40 2569.57 10.89 2569.08
RW-5 2580.51 9.01 2571.50 9.45 2571.06
RW-6 2581.42 10.33 2571.09 11.15 2570.27
RW-7 2582.19 9.49 2572.70 9.50 2572.69
Notes:
ft = feet
amsl = above mean sea level
btoc = below top of casing
TOC = top of casing
* = Coordinates Not Available / Estimated TOC Elevation
NM = not measured
Updated TOC Elevation
Page 1 of 1
Table 4-4.1
Groundwater Sampling Locations
Pactiv Evergreen Canton Mill
Canton, North Carolina
Location Sample ID Notes
BR-1 BR01WG-MMDDYY 70-100 Bedrock Well Full analytical suite
BR-2 BR02WG-MMDDYY 93-103
BR-3 BR03WG-MMDDYY 36-56 Bedrock Well Full analytical suite
PZ-1 PZ01WG-MMDDYY 7.5-22.5 Full analytical suite
PZ-2 PZ02WG-MMDDYY 10-20
PZ-3 PZ03WG-MMDDYY 8-23 Full analytical suite
PZ-4 PZ04WG-MMDDYY 9-24
PZ-5 PZ05WG-MMDDYY 9-19 Full analytical suite
PZ-6 PZ06WG-MMDDYY 17-27 Full analytical suite
PZ-7 PZ07WG-MMDDYY 11-26
PZ-8 PZ08WG-MMDDYY 8.5-23.8 Full analytical suite
PZ-9 PZ09WG-MMDDYY 10-25 Full analytical suite
PZ-11 PZ11WG-MMDDYY 9-24 Full analytical suite
PZ-12 PZ12WG-MMDDYY 9-24 Full analytical suite
PZ-13 PZ13WG-MMDDYY 8.5-23.5 Full analytical suite
PZ-14R PZ14WG-MMDDYY 10-20 Full analytical suite
PZ-17 PZ17WG-MMDDYY 4-19 Full analytical suite
PZ-18 PZ18WG-MMDDYY 4.8-19.8 Full analytical suite
PZ-20 PZ20WG-MMDDYY UNK Full analytical suite
PZ-21 PZ21WG-MMDDYY UNK Full analytical suite
RW-1 RW01WG-MMDDYY 20-40 Full analytical suite
RW-2 RW02WG-MMDDYY 9-49 4-inch Recovery Well - Full analytical suite
RW-3 RW03WG-MMDDYY 9-49 4-inch Recovery Well - Full analytical suite
RW-4 RW04WG-MMDDYY 9-49 4-inch Recovery Well - Full analytical suite
RW-5 RW05WG-MMDDYY 9-49
RW-6 RW06WG-MMDDYY 10.5-30.5 4-inch Recovery Well - Full analytical suite
RW-7 RW07WG-MMDDYY 10-40 4-inch Recovery Well - Full analytical suite
Page 1 of 2
Table 4-4.1
Groundwater Sampling Locations
Pactiv Evergreen Canton Mill
Canton, North Carolina
Notes:
ID = Identification
ft = feet
bgs = below ground surface
MMDDYY = Month, day, and year, ex. February 3, 2023 will be identified as 020323
UNK = Unknown
*= Initial sample for full and remedial analytical suites was rejected by lab
Page 2 of 2
Table 4-4.2Field Parameters in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Well ID Date
pH Turbidity DO ORP
BR-1 9/14/2023 6.45 45.82 5.26 1.01 16.3 20.7
BR-2 9/12/2023 6.81 3.146 3.99 3.98 16.61 42.7
BR-3 9/14/2023 8.73 27.94 23 0.21 18.38 -173.3
PZ-1 9/13/2023 8.25 2.52 1.93 0.08 19.85 -181.8
PZ-2 9/14/2023 10.13 14.05 6.85 0.25 20 -341.3
PZ-3 9/13/2023 8.84 2.26 9.03 0.08 23.88 -267.8
PZ-4 9/19/2023 10.94 29.09 7.67 0.06 23.96 -432
PZ-5 9/13/2023 5.99 0.742 1.34 0.88 19.53 64.1
PZ-6 9/14/2023 6.59 0.814 13.2 0.38 21.33 -111.9
PZ-7 9/15/2024 8.9 5.908 9.79 0.34 19.76 -89.6
PZ-8 9/21/2023 10.07 9.02 29.6 0.1 22.05 -311.4
PZ-9 9/21/2023 5.66 0.655 1.98 1.41 19.1 133.1
PZ-11 9/14/2023 9.13 3.08 37.9 0.08 22.24 -224.5
PZ-12 9/14/2023 9.02 9.94 2.99 0.22 21.88 -234.7
PZ-13 9/15/2023 6.54 0.572 2.19 0.74 20.98 36.7
PZ-14/PZ-14R*9/14/2023 6.6 0.522 8.59 0.29 16.56 -110.3
PZ-17 9/17/2023 6.01 0.566 3.95 0.5 17.85 49
PZ-18 9/18/2023 6.3 0.446 4.24 0.65 23.46 -89.7
PZ-20 9/19/2023 7.82 1.277 5.66 0.2 22.24 -228.5
PZ-21 9/19/2023 5.97 0.791 2.49 1.49 17.93 114.9
RW-1 9/19/2023 7.17 0.872 13.8 0.29 19.77 -210.4
RW-2 9/12/2023 6.82 0.277 6.71 0.46 17.41 -90.7
RW-3 9/12/2023 6.61 2.06 5.41 0.59 18.07 -108.7
RW-4 9/13/2023 10.28 4.34 9.23 0.13 19.14 -372.2
RW-5 9/20/2023 12.15 46.95 13.3 0.16 17.71 -533.3
RW-6 9/13/2023 6.81 0.855 2.44 0.54 17.73 -16
RW-7 9/13/2023 6.03 0.682 3.86 0.51 20.92 64.8
Notes:
s.u.= Standard Units
mS/cm = MilliSiemens per centimeter
NTU = Nephelometric Turbidity Unit
mg/L = Milligrams per Liter
C = Celsius
Page 1 of 1
Table 4-5Field Parameters in Surface Water and Seeps
Pactiv Evergreen Canton Mill
Canton, North Carolina Date: 9/20/2023
Sample ID
Depth pH Conductivity Turbidity DO Temperature ORP
SW-Down 0-4"1305 9.24 128 NM 8.1 20.64 -38.7 First location sampled — sample
taken from river cobble bar at bridge.
SW-Up 0-4"1700 8.32 26 NM 12.6 19.38 -0.3 due to unsafe depths; sample taken
Seep-01 4"1530 10.38 2152 5.22 8.4 26.46 -269.6 Sample collected from pool
Seep-02 1.5"1415 9.68 485 10.3 12.8 26.52 -35.3 Sample collected from pool
0-4"1435 7.42 27 2.6 9.65 18.72 29.9 Sample taken at the riverbank
SW-01 (2')0-4"1450 6.01 29 1.54 9.3 18.72 36.2
SW-01 (5')0-4"1510 6.97 28 1.57 9.62 18.89 40.3 Sample taken 5-feet from riverbank
SW-01 (10')0-4"1520 7.62 28 1.69 9.99 19.58 43.5 Sample taken 10-feet from riverbank
SW-02 0-4"1550 7.7 27 1.72 11.41 19.13 9.4 Sample taken after SW-01/Seep-01
s.u.= Standard Units
mS/cm
NTU = Nephelometric Turbidity Unit
mg/L = Milligrams per Liter
C = Celsius
Page 1 of 1
Table 5-1
pH and Color in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
BR01 BR02 BR03 PZ01 PZ02 PZ03 PZ04 PZ04 PZ04 PZ05
BR01WG-091423 BR02 WG- 091323 BR03WG-091423 PZ01 WG- 091323 PZ02WG-091423 PZ03 WG- 091323 PZ4WG-062323 DUP01WG-062323 PZ04WG-091923 PZ05 WG- 091323
09/14/2023 09/13/2023 09/14/2023 09/13/2023 09/14/2023 09/13/2023 06/23/2023 06/23/2023 09/19/2023 09/13/2023
Normal Normal Normal Normal Normal Normal Normal Field Duplicate Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
Method CAS No.Analyte NC 02L GWQS Units
SM 2120B COLOR Color, True 15 color unit 160 5 200 375 16000 2000 5000 4000 NA 5 U
SW9040 9999900-09-4 pH 6.5 - 8.5 SU 6.45 6.81 8.73 8.25 10.13 8.84 NA NA 10.94 5.99
Notes:
Cas No.
NA
J
R
SU
U
UR
Bold
Highlighted
*pH values were collected as field parameters from the September 2023 Sampling Event
**pH values were collected on a different day than the correlating samples
= Title 15A, North Carolina Administrative Code, Chapter 02,
Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
Page 1 of 29
Table 5-1
pH and Color in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SM 2120B COLOR Color, True 15 color unit
SW9040 9999900-09-4 pH 6.5 - 8.5 SU
Cas No.
NA
J
R
SU
U
UR
Bold
Highlighted
*pH values were collected as field parameters from the September 2023 Sampling Event
**pH values were collected on a different day than the correlating samples
= Title 15A, North Carolina Administrative Code, Chapter 02,
Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
PZ06 PZ07 PZ08 PZ09 PZ11 PZ12 PZ13 PZ14 PZ14 PZ17
PZ06WG-091423 PZ07WG-091523 PZ08WG-092123 PZ09WG-092123 PZ11WG-091423 PZ12WG-091423 PZ13WG-091523 PZ14WG-091423 PZ14HG-091423 PZ17 WG- 091323
09/14/2023 09/15/2023 09/21/2023 09/21/2023 09/14/2023 09/14/2023 09/15/2023 09/14/2023 09/14/2023 09/13/2023
Normal Normal Normal Normal Normal Normal Normal Normal Field Duplicate Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
10 16000 350 J 5 R 9000 7500 15 10 10 5 U
6.59 8.9 10.07 5.66 9.13 9.02 6.54 6.6 6.6 NA
Page 2 of 29
Table 5-1
pH and Color in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SM 2120B COLOR Color, True 15 color unit
SW9040 9999900-09-4 pH 6.5 - 8.5 SU
Cas No.
NA
J
R
SU
U
UR
Bold
Highlighted
*pH values were collected as field parameters from the September 2023 Sampling Event
**pH values were collected on a different day than the correlating samples
= Title 15A, North Carolina Administrative Code, Chapter 02,
Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
PZ17 PZ17**PZ18 PZ20 PZ21 PZ21 RW01 RW02 RW03 RW04
PZ17 HG- 091323 NA PZ18WG-091823 PZ20WG-091923 PZ21WG-062223 PZ21WG-091923 RW01WG-091923 RW02W6-091223 RW03W6-091223 RW04 WG- 091323
09/13/2023 09/17/2023 09/18/2023 09/19/2023 06/22/2023 09/19/2023 09/19/2023 09/12/2023 09/12/2023 09/13/2023
Field Duplicate NA Normal Normal Normal Normal Normal Normal Normal Normal
Groundwater NA Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
5 U NA 500 250 5 U 5 J 100 4000 875 1500
NA 6.01 6.3 7.82 NA 5.97 7.17 6.82 6.61 10.28
Page 3 of 29
Table 5-1
pH and Color in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SM 2120B COLOR Color, True 15 color unit
SW9040 9999900-09-4 pH 6.5 - 8.5 SU
Cas No.
NA
J
R
SU
U
UR
Bold
Highlighted
*pH values were collected as field parameters from the September 2023 Sampling Event
**pH values were collected on a different day than the correlating samples
= Title 15A, North Carolina Administrative Code, Chapter 02,
Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
RW05 RW05**RW06 RW07
RW5WG-062323 NA RW06 WG- 091323 RW07 WG- 091323
06/23/2023 09/20/2023 09/13/2023 09/13/2023
Normal NA Normal Normal
Groundwater NA Groundwater Groundwater
2000 NA 5 5 U
NA 12.15 6.81 6.03
Page 4 of 29
Table 5-2
Metals in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
BR01 BR02 BR03 PZ01 PZ02 PZ03
BR01WG-091423 BR02 WG- 091323 BR03WG-091423 PZ01 WG- 091323 PZ02WG-091423 PZ03 WG- 091323
09/14/2023 09/13/2023 09/14/2023 09/13/2023 09/14/2023 09/13/2023
Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
Method CAS No.Analyte NC 02L GWQS Units
SW6010 7429-90-5 Aluminum NE mg/L NA NA NA NA NA NA
SW6010 7429-90-5 Aluminum (Dissolved)NE mg/L NA NA NA NA NA NA
SW6010 7440-36-0 Antimony 0.001 mg/L 0.015 U 0.0071 J 0.015 U 0.015 U 0.075 U 0.015 U
SW6010 7440-36-0 Antimony (Dissolved)0.001 mg/L 0.015 U NA 0.015 U 0.015 U 0.015 U 0.015 U
SW6010 7440-38-2 Arsenic 0.01 mg/L 0.01 U 0.01 U 0.01 U 0.01 U 0.025 J 0.0061 J
SW6010 7440-38-2 Arsenic (Dissolved)0.01 mg/L 0.01 U NA 0.0062 J 0.0042 J 0.016 0.0065 J
SW6010 7440-39-3 Barium 0.7 mg/L 0.34 0.196 0.21 0.0421 0.14 0.111
SW6010 7440-39-3 Barium (Dissolved)0.7 mg/L 0.36 NA 0.19 0.0347 0.11 0.0833
SW6010 7440-41-7 Beryllium 0.004 mg/L 0.004 U 0.004 U 0.004 U 0.004 U 0.0031 J 0.00058 J
SW6010 7440-41-7 Beryllium (Dissolved)0.004 mg/L 0.08 U NA 0.004 U 0.004 U 0.0018 J 0.00041 J
SW6010 7440-42-8 Boron 0.7 mg/L 0.05 U 0.0283 J 0.045 J 0.0846 0.14 J 0.116
SW6010 7440-42-8 Boron (Dissolved)0.7 mg/L 0.05 U NA 0.046 J 0.0855 0.095 0.114
SW6010 7440-43-9 Cadmium 0.002 mg/L 0.001 U 0.00047 J 0.001 U 0.001 U 0.005 U 0.001 U
SW6010 7440-43-9 Cadmium (Dissolved)0.002 mg/L 0.002 U NA 0.00052 J 0.001 U 0.001 U 0.001 U
SW6010 7440-70-2 Calcium NE mg/L NA NA NA NA 14.1 NA
SW6010 7440-70-2 Calcium (Dissolved)NE mg/L NA NA NA NA NA NA
SW6010 7440-47-3 Chromium 0.01 mg/L 0.32 0.0912 0.0039 J 0.008 0.04 0.0175
SW6010 7440-47-3 Chromium (Dissolved)0.01 mg/L 0.22 NA 0.003 J 0.0051 0.029 0.0146
SW6010 7440-48-4 Cobalt 0.001 mg/L 0.019 J 0.0081 J 0.0017 J 0.01 U 0.0086 J 0.0025 J
SW6010 7440-48-4 Cobalt (Dissolved)0.001 mg/L 0.021 J NA 0.0022 J 0.01 U 0.006 J 0.0017 J
SW6010 7440-50-8 Copper 1 mg/L 0.018 J 0.0072 0.0043 J 0.005 U 0.025 U 0.0041 J
SW6010 7440-50-8 Copper (Dissolved)1 mg/L 0.1 U NA 0.005 U 0.0081 0.005 U 0.0028 J
SW6010 7439-89-6 Iron 0.3 mg/L NA NA NA NA 15.4 NA
SW6010 7439-89-6 Iron (Dissolved)0.3 mg/L NA NA NA NA 10.1 NA
SW6010 7439-92-1 Lead 0.015 mg/L 0.05 U 0.007 J 0.01 U 0.01 U 0.05 U 0.0022 J
SW6010 7439-92-1 Lead (Dissolved)0.015 mg/L 0.02 U NA 0.01 U 0.01 U 0.0067 J 0.01 U
SW6010 7439-95-4 Magnesium NE mg/L NA NA NA NA 2.5 U NA
SW6010 7439-95-4 Magnesium (Dissolved)NE mg/L NA NA NA NA NA NA
SW6010 7439-96-5 Manganese 0.05 mg/L 9.8 0.216 0.097 3.6 0.13 1.39
SW6010 7439-96-5 Manganese (Dissolved)0.05 mg/L 11.7 NA 0.048 3.1 0.089 1.21
SW6010 7440-02-0 Nickel 0.1 mg/L 0.55 0.0309 0.032 0.0109 0.19 0.0064
SW6010 7440-02-0 Nickel (Dissolved)0.1 mg/L 0.4 NA 0.026 0.0093 0.14 0.0054
SW6010 7723-14-0 Phosphorus NE mg/L NA NA NA NA 13 NA
SW6010 7440-09-7 Potassium NE mg/L NA NA NA NA 24 NA
SW6010 7782-49-2 Selenium 0.02 mg/L 0.075 U 0.015 U 0.015 U 0.015 U 0.075 U 0.015 U
SW6010 7782-49-2 Selenium (Dissolved)0.02 mg/L 0.015 U NA 0.015 U 0.015 U 0.015 U 0.015 U
SW6010 7440-22-4 Silver 0.02 mg/L 0.005 U 0.005 U 0.005 U 0.005 U 0.025 U 0.005 U
SW6010 7440-22-4 Silver (Dissolved)0.02 mg/L 0.01 U NA 0.0029 J 0.005 U 0.005 U 0.005 U
SW6010 7440-23-5 Sodium NE mg/L NA NA NA NA NA NA
SW6010 7440-23-5 Sodium (Dissolved)NE mg/L NA NA NA NA NA NA
SW6010 7440-28-0 Thallium 0.002 mg/L 0.015 U 0.015 U 0.015 U 0.015 U 0.075 U 0.015 U
SW6010 7440-28-0 Thallium (Dissolved)0.002 mg/L 0.03 U NA 0.015 U 0.015 U 0.015 U 0.015 U
SW6010 7440-62-2 Vanadium 0.007 mg/L 0.0095 J 0.0273 0.11 0.0463 0.55 0.227
SW6010 7440-62-2 Vanadium (Dissolved)0.007 mg/L 0.2 U NA 0.1 0.0356 0.4 0.174
SW6010 7440-66-6 Zinc 1 mg/L 0.1 U 0.071 0.02 U 0.02 U 0.1 U 0.0114 J
SW6010 7440-66-6 Zinc (Dissolved)1 mg/L 0.67 NA 0.02 U 0.02 U 0.013 J 0.0281
SW7470 7439-97-6 Mercury 0.001 mg/L 0.0002 U 0.00031 0.0002 U 0.0002 U 0.0016 U 0.0002 U
SW7470 7439-97-6 Mercury (Dissolved)0.001 mg/L 0.0002 U NA 0.0002 U 0.0002 U 0.0008 U 0.0002 U
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter
Page 5 of 29
Table 5-2
Metals in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW6010 7429-90-5 Aluminum NE mg/L
SW6010 7429-90-5 Aluminum (Dissolved)NE mg/L
SW6010 7440-36-0 Antimony 0.001 mg/L
SW6010 7440-36-0 Antimony (Dissolved)0.001 mg/L
SW6010 7440-38-2 Arsenic 0.01 mg/L
SW6010 7440-38-2 Arsenic (Dissolved)0.01 mg/L
SW6010 7440-39-3 Barium 0.7 mg/L
SW6010 7440-39-3 Barium (Dissolved)0.7 mg/L
SW6010 7440-41-7 Beryllium 0.004 mg/L
SW6010 7440-41-7 Beryllium (Dissolved)0.004 mg/L
SW6010 7440-42-8 Boron 0.7 mg/L
SW6010 7440-42-8 Boron (Dissolved)0.7 mg/L
SW6010 7440-43-9 Cadmium 0.002 mg/L
SW6010 7440-43-9 Cadmium (Dissolved)0.002 mg/L
SW6010 7440-70-2 Calcium NE mg/L
SW6010 7440-70-2 Calcium (Dissolved)NE mg/L
SW6010 7440-47-3 Chromium 0.01 mg/L
SW6010 7440-47-3 Chromium (Dissolved)0.01 mg/L
SW6010 7440-48-4 Cobalt 0.001 mg/L
SW6010 7440-48-4 Cobalt (Dissolved)0.001 mg/L
SW6010 7440-50-8 Copper 1 mg/L
SW6010 7440-50-8 Copper (Dissolved)1 mg/L
SW6010 7439-89-6 Iron 0.3 mg/L
SW6010 7439-89-6 Iron (Dissolved)0.3 mg/L
SW6010 7439-92-1 Lead 0.015 mg/L
SW6010 7439-92-1 Lead (Dissolved)0.015 mg/L
SW6010 7439-95-4 Magnesium NE mg/L
SW6010 7439-95-4 Magnesium (Dissolved)NE mg/L
SW6010 7439-96-5 Manganese 0.05 mg/L
SW6010 7439-96-5 Manganese (Dissolved)0.05 mg/L
SW6010 7440-02-0 Nickel 0.1 mg/L
SW6010 7440-02-0 Nickel (Dissolved)0.1 mg/L
SW6010 7723-14-0 Phosphorus NE mg/L
SW6010 7440-09-7 Potassium NE mg/L
SW6010 7782-49-2 Selenium 0.02 mg/L
SW6010 7782-49-2 Selenium (Dissolved)0.02 mg/L
SW6010 7440-22-4 Silver 0.02 mg/L
SW6010 7440-22-4 Silver (Dissolved)0.02 mg/L
SW6010 7440-23-5 Sodium NE mg/L
SW6010 7440-23-5 Sodium (Dissolved)NE mg/L
SW6010 7440-28-0 Thallium 0.002 mg/L
SW6010 7440-28-0 Thallium (Dissolved)0.002 mg/L
SW6010 7440-62-2 Vanadium 0.007 mg/L
SW6010 7440-62-2 Vanadium (Dissolved)0.007 mg/L
SW6010 7440-66-6 Zinc 1 mg/L
SW6010 7440-66-6 Zinc (Dissolved)1 mg/L
SW7470 7439-97-6 Mercury 0.001 mg/L
SW7470 7439-97-6 Mercury (Dissolved)0.001 mg/L
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter
PZ04 PZ05 PZ06 PZ07 PZ08 PZ09
PZ04WG-091923 PZ05 WG- 091323 PZ06WG-091423 PZ07WG-091523 PZ08WG-092123 PZ09WG-092123
09/19/2023 09/13/2023 09/14/2023 09/15/2023 09/21/2023 09/21/2023
Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
NA NA NA NA NA NA
NA NA NA NA NA NA
0.015 U 0.015 U 0.015 U 0.075 U 0.015 U 0.015 U
0.0179 0.015 U 0.015 U 0.03 U 0.015 U 0.015 U
0.254 0.01 U 0.01 U 0.021 J 0.0049 J 0.01 U
0.297 0.01 U 0.01 U 0.013 J 0.0046 J 0.01 U
0.0713 0.0447 0.12 0.13 0.019 0.353
0.0537 0.043 0.1 0.11 0.0071 J 0.348
0.004 U 0.004 U 0.004 U 0.0078 J 0.00027 J 0.004 U
0.004 U 0.004 U 0.004 U 0.0057 J 0.004 U 0.004 U
0.19 0.0557 0.055 0.17 J 0.0674 0.05 U
0.199 0.0562 0.057 0.13 0.0779 0.05 U
0.00081 J 0.001 U 0.001 U 0.005 U 0.001 U 0.001 U
0.00034 J 0.001 U 0.0004 J 0.00072 J 0.001 U 0.001 U
5.62 NA NA 12.7 NA NA
NA NA NA NA NA NA
0.118 0.005 U 0.0027 J 0.22 0.0108 0.005 U
0.115 0.005 U 0.005 U 0.2 0.0043 J 0.005 U
0.0036 J 0.01 U 0.0019 J 0.014 J 0.0031 J 0.0013 J
0.004 J 0.01 U 0.0018 J 0.01 J 0.0012 J 0.01 U
0.0222 0.005 U 0.005 U 0.06 0.0053 0.005 U
0.005 U 0.005 U 0.005 U 0.049 0.005 U 0.005 U
5.09 NA NA 22.7 NA NA
3.55 NA NA 18.1 NA NA
0.01 U 0.01 U 0.01 U 0.039 J 0.0075 J 0.01 U
0.01 U 0.01 U 0.01 U 0.033 0.01 U 0.01 U
0.16 J NA NA 1.38 J NA NA
NA NA NA NA NA NA
0.0823 0.0112 3.2 0.12 0.0482 0.0061
0.023 0.0023 J 2.8 0.086 0.0105 0.005
0.117 0.005 U 0.005 U 0.15 0.014 0.0016 J
0.0956 0.005 U 0.005 U 0.12 0.0069 0.0018 J
14.6 NA NA 12.5 NA NA
18.5 NA NA 11.5 NA NA
0.0042 J 0.015 U 0.015 U 0.075 U 0.015 U 0.015 U
0.0061 J 0.015 U 0.015 U 0.03 U 0.015 U 0.015 U
0.005 U 0.005 U 0.005 U 0.025 U 0.005 U 0.005 U
0.005 U 0.005 U 0.005 U 0.01 U 0.005 U 0.005 U
NA NA NA NA NA NA
NA NA NA NA NA NA
0.03 U 0.015 U 0.015 U 0.075 U 0.015 U 0.015 U
0.015 U 0.015 U 0.015 U 0.03 U 0.015 U 0.015 U
1.32 0.01 U 0.0043 J 0.96 0.0389 0.01 U
1.34 0.01 U 0.0012 J 0.8 0.0238 0.01 U
0.0298 0.02 U 0.02 U 0.1 U 0.02 U 0.02 U
0.0154 J 0.02 U 0.02 U 0.028 J 0.02 U 0.02 U
0.0032 0.0002 U 0.0002 U 0.0016 U 0.00032 0.00016 J
0.0036 0.0002 U 0.0002 U 0.0008 U 0.00035 0.0002 U
Page 6 of 29
Table 5-2
Metals in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW6010 7429-90-5 Aluminum NE mg/L
SW6010 7429-90-5 Aluminum (Dissolved)NE mg/L
SW6010 7440-36-0 Antimony 0.001 mg/L
SW6010 7440-36-0 Antimony (Dissolved)0.001 mg/L
SW6010 7440-38-2 Arsenic 0.01 mg/L
SW6010 7440-38-2 Arsenic (Dissolved)0.01 mg/L
SW6010 7440-39-3 Barium 0.7 mg/L
SW6010 7440-39-3 Barium (Dissolved)0.7 mg/L
SW6010 7440-41-7 Beryllium 0.004 mg/L
SW6010 7440-41-7 Beryllium (Dissolved)0.004 mg/L
SW6010 7440-42-8 Boron 0.7 mg/L
SW6010 7440-42-8 Boron (Dissolved)0.7 mg/L
SW6010 7440-43-9 Cadmium 0.002 mg/L
SW6010 7440-43-9 Cadmium (Dissolved)0.002 mg/L
SW6010 7440-70-2 Calcium NE mg/L
SW6010 7440-70-2 Calcium (Dissolved)NE mg/L
SW6010 7440-47-3 Chromium 0.01 mg/L
SW6010 7440-47-3 Chromium (Dissolved)0.01 mg/L
SW6010 7440-48-4 Cobalt 0.001 mg/L
SW6010 7440-48-4 Cobalt (Dissolved)0.001 mg/L
SW6010 7440-50-8 Copper 1 mg/L
SW6010 7440-50-8 Copper (Dissolved)1 mg/L
SW6010 7439-89-6 Iron 0.3 mg/L
SW6010 7439-89-6 Iron (Dissolved)0.3 mg/L
SW6010 7439-92-1 Lead 0.015 mg/L
SW6010 7439-92-1 Lead (Dissolved)0.015 mg/L
SW6010 7439-95-4 Magnesium NE mg/L
SW6010 7439-95-4 Magnesium (Dissolved)NE mg/L
SW6010 7439-96-5 Manganese 0.05 mg/L
SW6010 7439-96-5 Manganese (Dissolved)0.05 mg/L
SW6010 7440-02-0 Nickel 0.1 mg/L
SW6010 7440-02-0 Nickel (Dissolved)0.1 mg/L
SW6010 7723-14-0 Phosphorus NE mg/L
SW6010 7440-09-7 Potassium NE mg/L
SW6010 7782-49-2 Selenium 0.02 mg/L
SW6010 7782-49-2 Selenium (Dissolved)0.02 mg/L
SW6010 7440-22-4 Silver 0.02 mg/L
SW6010 7440-22-4 Silver (Dissolved)0.02 mg/L
SW6010 7440-23-5 Sodium NE mg/L
SW6010 7440-23-5 Sodium (Dissolved)NE mg/L
SW6010 7440-28-0 Thallium 0.002 mg/L
SW6010 7440-28-0 Thallium (Dissolved)0.002 mg/L
SW6010 7440-62-2 Vanadium 0.007 mg/L
SW6010 7440-62-2 Vanadium (Dissolved)0.007 mg/L
SW6010 7440-66-6 Zinc 1 mg/L
SW6010 7440-66-6 Zinc (Dissolved)1 mg/L
SW7470 7439-97-6 Mercury 0.001 mg/L
SW7470 7439-97-6 Mercury (Dissolved)0.001 mg/L
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter
PZ11 PZ12 PZ13 PZ14 PZ14 PZ17
PZ11WG-091423 PZ12WG-091423 PZ13WG-091523 PZ14WG-091423 PZ14HG-091423
09/14/2023 09/14/2023 09/15/2023 09/14/2023 09/14/2023 09/13/2023
Normal Normal Normal Normal Field Duplicate Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
NA NA NA NA NA NA
NA NA NA NA NA NA
0.15 U 0.03 U 0.015 U 0.015 U 0.015 U 0.015 U
0.075 U 0.015 U 0.015 U 0.015 U 0.015 U 0.015 U
0.046 J 0.042 0.01 U 0.01 U 0.01 U 0.01 U
0.06 0.042 0.01 U 0.01 U 0.01 U 0.01 U
0.72 0.36 0.021 0.11 0.11 0.105
0.58 0.34 0.019 0.1 0.1 0.0983
0.04 U 0.0025 J 0.004 U 0.004 U 0.004 U 0.004 U
0.02 U 0.0019 J 0.004 U 0.004 U 0.004 U 0.004 U
0.34 J 0.44 0.043 J 0.036 J 0.037 J 0.0895
0.32 0.43 0.043 J 0.037 J 0.036 J 0.0879
0.01 U 0.002 U 0.001 U 0.001 U 0.001 U 0.001 U
0.005 U 0.001 U 0.001 U 0.001 U 0.001 U 0.00039 J
NA NA NA NA NA NA
NA NA NA NA NA NA
0.17 0.17 0.005 U 0.005 U 0.005 U 0.005 U
0.15 0.15 0.005 U 0.005 U 0.005 U 0.005 U
0.1 U 0.0035 J 0.01 0.01 U 0.01 U 0.01 U
0.0052 J 0.003 J 0.0078 J 0.01 U 0.01 U 0.01 U
0.066 0.01 U 0.036 0.005 U 0.005 U 0.005 U
0.044 0.005 U 0.0036 J 0.005 U 0.005 U 0.005 U
NA NA NA NA NA NA
NA NA NA NA NA NA
0.1 U 0.02 U 0.01 U 0.01 U 0.01 U 0.01 U
0.05 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U
NA NA NA NA NA NA
NA NA NA NA NA NA
0.23 0.18 0.26 0.25 0.26 2.43
0.18 0.15 0.25 0.25 0.25 2.07
0.02 J 0.055 0.03 0.005 U 0.005 U 0.005 U
0.016 J 0.046 0.023 0.005 U 0.005 U 0.005 U
NA NA NA NA NA NA
NA NA NA NA NA NA
0.15 U 0.03 U 0.015 U 0.015 U 0.015 U 0.015 U
0.075 U 0.015 U 0.015 U 0.015 U 0.015 U 0.015 U
0.05 U 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U
0.025 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U
NA NA NA NA NA NA
NA NA NA NA NA NA
0.15 U 0.03 U 0.015 U 0.015 U 0.015 U 0.015 U
0.075 U 0.015 U 0.015 U 0.015 U 0.015 U 0.015 U
0.84 0.96 0.0031 J 0.0012 J 0.0014 J 0.01 U
0.73 0.81 0.0021 J 0.0015 J 0.0016 J 0.01 U
0.2 U 0.04 U 0.1 0.02 U 0.02 U 0.0692
0.1 U 0.02 U 0.096 0.02 U 0.02 U 0.0644
0.0004 U 0.0008 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U
0.00018 J 0.0004 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U
Page 7 of 29
Table 5-2
Metals in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW6010 7429-90-5 Aluminum NE mg/L
SW6010 7429-90-5 Aluminum (Dissolved)NE mg/L
SW6010 7440-36-0 Antimony 0.001 mg/L
SW6010 7440-36-0 Antimony (Dissolved)0.001 mg/L
SW6010 7440-38-2 Arsenic 0.01 mg/L
SW6010 7440-38-2 Arsenic (Dissolved)0.01 mg/L
SW6010 7440-39-3 Barium 0.7 mg/L
SW6010 7440-39-3 Barium (Dissolved)0.7 mg/L
SW6010 7440-41-7 Beryllium 0.004 mg/L
SW6010 7440-41-7 Beryllium (Dissolved)0.004 mg/L
SW6010 7440-42-8 Boron 0.7 mg/L
SW6010 7440-42-8 Boron (Dissolved)0.7 mg/L
SW6010 7440-43-9 Cadmium 0.002 mg/L
SW6010 7440-43-9 Cadmium (Dissolved)0.002 mg/L
SW6010 7440-70-2 Calcium NE mg/L
SW6010 7440-70-2 Calcium (Dissolved)NE mg/L
SW6010 7440-47-3 Chromium 0.01 mg/L
SW6010 7440-47-3 Chromium (Dissolved)0.01 mg/L
SW6010 7440-48-4 Cobalt 0.001 mg/L
SW6010 7440-48-4 Cobalt (Dissolved)0.001 mg/L
SW6010 7440-50-8 Copper 1 mg/L
SW6010 7440-50-8 Copper (Dissolved)1 mg/L
SW6010 7439-89-6 Iron 0.3 mg/L
SW6010 7439-89-6 Iron (Dissolved)0.3 mg/L
SW6010 7439-92-1 Lead 0.015 mg/L
SW6010 7439-92-1 Lead (Dissolved)0.015 mg/L
SW6010 7439-95-4 Magnesium NE mg/L
SW6010 7439-95-4 Magnesium (Dissolved)NE mg/L
SW6010 7439-96-5 Manganese 0.05 mg/L
SW6010 7439-96-5 Manganese (Dissolved)0.05 mg/L
SW6010 7440-02-0 Nickel 0.1 mg/L
SW6010 7440-02-0 Nickel (Dissolved)0.1 mg/L
SW6010 7723-14-0 Phosphorus NE mg/L
SW6010 7440-09-7 Potassium NE mg/L
SW6010 7782-49-2 Selenium 0.02 mg/L
SW6010 7782-49-2 Selenium (Dissolved)0.02 mg/L
SW6010 7440-22-4 Silver 0.02 mg/L
SW6010 7440-22-4 Silver (Dissolved)0.02 mg/L
SW6010 7440-23-5 Sodium NE mg/L
SW6010 7440-23-5 Sodium (Dissolved)NE mg/L
SW6010 7440-28-0 Thallium 0.002 mg/L
SW6010 7440-28-0 Thallium (Dissolved)0.002 mg/L
SW6010 7440-62-2 Vanadium 0.007 mg/L
SW6010 7440-62-2 Vanadium (Dissolved)0.007 mg/L
SW6010 7440-66-6 Zinc 1 mg/L
SW6010 7440-66-6 Zinc (Dissolved)1 mg/L
SW7470 7439-97-6 Mercury 0.001 mg/L
SW7470 7439-97-6 Mercury (Dissolved)0.001 mg/L
Bold
Highlighted
= Chemical Abstracts Service number
= Exceeds the NC 02L GWQS
= Not analyzed
= Not detected, shown with reporting limit
= Estimated value
= milligrams per liter
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter
PZ17 PZ18 PZ20 PZ21 RW01 RW02
PZ17 HG- 091323 PZ18WG-091823 PZ20WG-091923 PZ21WG-091923 RW01WG-091923 RW02W6-091223
09/13/2023 09/18/2023 09/19/2023 09/19/2023 09/19/2023 09/12/2023
Field Duplicate Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
NA NA NA NA NA NA
NA NA NA NA NA NA
0.015 U 0.015 U 0.015 U 0.015 U 0.015 U 0.025 U
0.015 U 0.015 U 0.015 U 0.015 U 0.015 U 0.005 U
0.01 U 0.01 U 0.0049 J 0.01 U 0.01 U 0.05 U
0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.0075 J
0.105 0.168 0.0367 0.0913 0.0566 0.264
0.098 0.172 0.0343 0.0922 0.0344 0.211
0.004 U 0.00081 J 0.004 U 0.004 U 0.004 U 0.005 U
0.004 U 0.004 U 0.004 U 0.004 U 0.004 U 0.001 U
0.0885 0.05 U 0.11 0.0323 J 0.0609 0.25 U
0.0887 0.05 U 0.115 0.0375 J 0.0656 0.122
0.001 U 0.00089 J 0.00037 J 0.001 U 0.001 U 0.005 U
0.00033 J 0.00058 J 0.001 U 0.00045 J 0.001 U 0.001 U
NA NA NA NA NA NA
NA NA NA NA NA NA
0.005 U 0.005 U 0.0039 J 0.005 U 0.0036 J 0.0424
0.005 U 0.005 U 0.0021 J 0.005 U 0.005 U 0.0135
0.01 U 0.0016 J 0.0027 J 0.0012 J 0.00098 J 0.0248 J
0.01 U 0.0033 J 0.01 U 0.01 U 0.01 U 0.0158
0.005 U 0.005 U 0.0046 J 0.005 U 0.0038 J 0.025 U
0.005 U 0.005 U 0.005 U 0.004 J 0.005 U 0.005 U
NA NA NA NA NA NA
NA NA NA NA NA NA
0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.025 U
0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.005 U
NA NA NA NA NA NA
NA NA NA NA NA NA
2.32 0.63 0.799 0.833 1.57 NA
2.28 0.61 0.824 0.648 1.32 NA
0.005 U 0.005 U 0.0058 0.005 U 0.0027 J 0.025 U
0.005 U 0.005 U 0.0015 J 0.005 U 0.0016 J 0.0108
NA NA NA NA NA NA
NA NA NA NA NA NA
0.015 U 0.015 U 0.015 U 0.015 U 0.015 U 0.05 U
0.015 U 0.015 U 0.015 U 0.015 U 0.015 U 0.01 U
0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.025 U
0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U
NA NA NA NA NA NA
NA NA NA NA NA NA
0.015 U 0.015 U 0.015 U 0.015 U 0.015 U 0.05 U
0.015 U 0.015 U 0.015 U 0.015 U 0.015 U 0.01 U
0.01 U 0.01 U 0.0178 0.01 U 0.0115 0.556
0.01 U 0.0014 J 0.0094 J 0.01 U 0.0041 J 0.423
0.0671 0.02 U 0.0275 0.02 U 0.0796 2.86
0.0618 0.02 U 0.02 U 0.02 U 0.02 U 2
0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0004 U
0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U
Page 8 of 29
Table 5-2
Metals in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW6010 7429-90-5 Aluminum NE mg/L
SW6010 7429-90-5 Aluminum (Dissolved)NE mg/L
SW6010 7440-36-0 Antimony 0.001 mg/L
SW6010 7440-36-0 Antimony (Dissolved)0.001 mg/L
SW6010 7440-38-2 Arsenic 0.01 mg/L
SW6010 7440-38-2 Arsenic (Dissolved)0.01 mg/L
SW6010 7440-39-3 Barium 0.7 mg/L
SW6010 7440-39-3 Barium (Dissolved)0.7 mg/L
SW6010 7440-41-7 Beryllium 0.004 mg/L
SW6010 7440-41-7 Beryllium (Dissolved)0.004 mg/L
SW6010 7440-42-8 Boron 0.7 mg/L
SW6010 7440-42-8 Boron (Dissolved)0.7 mg/L
SW6010 7440-43-9 Cadmium 0.002 mg/L
SW6010 7440-43-9 Cadmium (Dissolved)0.002 mg/L
SW6010 7440-70-2 Calcium NE mg/L
SW6010 7440-70-2 Calcium (Dissolved)NE mg/L
SW6010 7440-47-3 Chromium 0.01 mg/L
SW6010 7440-47-3 Chromium (Dissolved)0.01 mg/L
SW6010 7440-48-4 Cobalt 0.001 mg/L
SW6010 7440-48-4 Cobalt (Dissolved)0.001 mg/L
SW6010 7440-50-8 Copper 1 mg/L
SW6010 7440-50-8 Copper (Dissolved)1 mg/L
SW6010 7439-89-6 Iron 0.3 mg/L
SW6010 7439-89-6 Iron (Dissolved)0.3 mg/L
SW6010 7439-92-1 Lead 0.015 mg/L
SW6010 7439-92-1 Lead (Dissolved)0.015 mg/L
SW6010 7439-95-4 Magnesium NE mg/L
SW6010 7439-95-4 Magnesium (Dissolved)NE mg/L
SW6010 7439-96-5 Manganese 0.05 mg/L
SW6010 7439-96-5 Manganese (Dissolved)0.05 mg/L
SW6010 7440-02-0 Nickel 0.1 mg/L
SW6010 7440-02-0 Nickel (Dissolved)0.1 mg/L
SW6010 7723-14-0 Phosphorus NE mg/L
SW6010 7440-09-7 Potassium NE mg/L
SW6010 7782-49-2 Selenium 0.02 mg/L
SW6010 7782-49-2 Selenium (Dissolved)0.02 mg/L
SW6010 7440-22-4 Silver 0.02 mg/L
SW6010 7440-22-4 Silver (Dissolved)0.02 mg/L
SW6010 7440-23-5 Sodium NE mg/L
SW6010 7440-23-5 Sodium (Dissolved)NE mg/L
SW6010 7440-28-0 Thallium 0.002 mg/L
SW6010 7440-28-0 Thallium (Dissolved)0.002 mg/L
SW6010 7440-62-2 Vanadium 0.007 mg/L
SW6010 7440-62-2 Vanadium (Dissolved)0.007 mg/L
SW6010 7440-66-6 Zinc 1 mg/L
SW6010 7440-66-6 Zinc (Dissolved)1 mg/L
SW7470 7439-97-6 Mercury 0.001 mg/L
SW7470 7439-97-6 Mercury (Dissolved)0.001 mg/L
Cas No.
NA
U
J
mg/L
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter
RW03 RW04 RW05 RW06 RW07
RW03W6-091223 RW04 WG- 091323 RW06 WG- 091323 RW07 WG- 091323
09/12/2023 09/13/2023 10/17/2023 09/13/2023 09/13/2023
Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater
NA NA 2.34 J NA NA
NA NA 4.42 J NA NA
0.025 U 0.015 U 0.75 UJ 0.015 U 0.015 U
0.005 U 0.015 U 0.75 UJ 0.015 U 0.015 U
0.05 U 0.0303 0.286 J 0.01 U 0.01 U
0.01 U 0.0296 0.613 0.01 U 0.01 U
0.11 0.152 0.181 J 0.0621 0.026
0.0888 0.0768 0.187 J 0.0596 0.0246
0.005 U 0.00066 J 0.2 UJ 0.004 U 0.004 U
0.001 U 0.00027 J 0.2 UJ 0.004 U 0.004 U
0.25 U 0.395 2.37 J 0.0829 0.114
0.114 0.383 4.42 0.086 0.114
0.005 U 0.001 U 0.05 UJ 0.001 U 0.001 U
0.001 U 0.001 U 0.05 UJ 0.0005 J 0.00052 J
NA NA 20.8 J NA NA
NA NA 25 UJ NA NA
0.025 U 0.0499 0.191 J 0.005 U 0.005 U
0.0042 J 0.0334 0.219 J 0.005 U 0.005 U
0.025 U 0.0037 J 0.5 UJ 0.01 U 0.001 J
0.005 U 0.0017 J 0.5 UJ 0.0012 J 0.0012 J
0.025 U 0.004 J 0.25 UJ 0.005 U 0.0046 J
0.005 U 0.005 U 0.25 UJ 0.005 U 0.0311
NA NA 3.86 NA NA
NA NA 2 UJ NA NA
0.025 U 0.01 U 0.278 J 0.01 U 0.01 U
0.005 U 0.01 U 0.5 UJ 0.01 U 0.01 U
NA NA 25 UJ NA NA
NA NA 25 UJ NA NA
NA 0.161 0.137 J 0.673 0.453
NA 0.0725 0.25 UJ 0.687 0.508
0.025 U 0.0199 0.146 J 0.0021 J 0.0026 J
0.005 U 0.0139 0.257 0.005 U 0.0039 J
NA NA NA NA NA
NA NA NA NA NA
0.05 U 0.015 U 0.75 UJ 0.015 U 0.015 U
0.01 U 0.015 U 0.75 UJ 0.015 U 0.015 U
0.025 U 0.005 U 0.25 UJ 0.005 U 0.005 U
0.005 U 0.005 U 0.25 UJ 0.005 U 0.005 U
NA NA 7820 NA NA
NA NA 14100 NA NA
0.05 U 0.015 U 0.75 UJ 0.015 U 0.015 U
0.01 U 0.015 U 0.75 UJ 0.015 U 0.015 U
0.0977 0.493 1.24 0.0035 J 0.01 U
0.0577 0.322 1.91 0.0041 J 0.01 U
0.082 0.0413 1.78 0.0798 0.586
0.0341 0.02 U 1 UJ 0.02 U 0.71
0.0002 U 0.0002 U 0.008 UJ 0.0002 U 0.0002 U
0.0002 U 0.0002 U 0.008 UJ 0.0002 U 0.0002 U
Page 9 of 29
Table 5-3
VOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
BR01 BR02 BR03 PZ01 PZ02
BR01WG-091423 BR02 WG- 091323 BR03WG-091423 PZ01 WG- 091323 PZ02WG-091423
09/14/2023 09/13/2023 09/14/2023 09/13/2023 09/14/2023
Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater
Method CAS No.Analyte NC 02L GWQS Units
SW8260 71-55-6 1,1,1-Trichloroethane 200 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 79-34-5 1,1,2,2-Tetrachloroethane 0.2 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 76-13-1 1,1,2-Trichloro-1,2,2-trifluoroethane 200000 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 79-00-5 1,1,2-Trichloroethane 0.6 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 75-34-3 1,1-Dichloroethane 6 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 75-35-4 1,1-Dichloroethene 350 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 120-82-1 1,2,4-Trichlorobenzene 70 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 96-12-8 1,2-Dibromo-3-Chloropropane 0.04 µg/L 2 U 2 U 2 U 2 U 2 U
SW8260 106-93-4 1,2-Dibromoethane (EDB)0.02 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 95-50-1 1,2-Dichlorobenzene 20 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 107-06-2 1,2-Dichloroethane 0.4 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 78-87-5 1,2-Dichloropropane 0.6 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 541-73-1 1,3-Dichlorobenzene 200 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 106-46-7 1,4-Dichlorobenzene 6 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 78-93-3 2-Butanone (MEK)4000 µg/L 5 U 5 U 5 U 5 U 68.6
SW8260 591-78-6 2-Hexanone 40 µg/L 5 U 5 U 5 U 5 U 0.74 J
SW8260 108-10-1 4-Methyl-2-Pentanone (MIBK)100 µg/L 5 U 5 U 3.3 J 5 U 14.9
SW8260 67-64-1 Acetone 6000 µg/L 25 U 25 U 16 J 25 U 188
SW8260 71-43-2 Benzene 1 µg/L 0.47 J 1 U 0.49 J 1 U 10
SW8260 75-27-4 Bromodichloromethane 0.6 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 75-25-2 Bromoform 4 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 74-83-9 Bromomethane 10 µg/L 2 U 2 U 2 U 2 U 2 U
SW8260 75-15-0 Carbon disulfide 700 µg/L 2 U 2 U 2 U 2 U 2 J
SW8260 56-23-5 Carbon tetrachloride 0.3 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 108-90-7 Chlorobenzene 50 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 75-00-3 Chloroethane 3000 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 67-66-3 Chloroform 70 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 74-87-3 Chloromethane 3 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 156-59-2 cis-1,2-Dichloroethene 70 µg/L 0.43 J 1 U 1 U 1 U 1 U
SW8260 10061-01-5 cis-1,3-Dichloropropene NE µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 110-82-7 Cyclohexane NE µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 124-48-1 Dibromochloromethane 0.4 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 75-71-8 Dichlorodifluoromethane 1000 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 100-41-4 Ethylbenzene 600 µg/L 1 U 1 U 21.5 5.3 22.1
SW8260 98-82-8 Isopropylbenzene 70 µg/L 1 U 1 U 1 U 1 U 0.4 J
SW8260 179601-23-1 m,p-Xylene NE µg/L 2 U 2 U 19.6 7.1 70.9
SW8260 79-20-9 Methyl acetate NE µg/L 10 U 10 U 10 U 10 U 10 U
SW8260 1634-04-4 Methyl tert-butyl ether 20 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 108-87-2 Methylcyclohexane NE µg/L 10 U 10 U 10 U 10 U 10 U
SW8260 75-09-2 Methylene chloride 5 µg/L 5 U 5 U 5 U 5 U 5 U
SW8260 95-47-6 o-Xylene NE µg/L 1 U 1 U 24.7 1.5 28.8
SW8260 100-42-5 Styrene 70 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 127-18-4 Tetrachloroethene 0.7 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 108-88-3 Toluene 600 µg/L 1 U 1 U 0.45 J 1 U 27.5
SW8260 156-60-5 trans-1,2-Dichloroethene 100 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 10061-02-6 trans-1,3-Dichloropropene NE µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 79-01-6 Trichloroethene 3 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 75-69-4 Trichlorofluoromethane 2000 µg/L 1 U 1 U 1 U 1 U 1 U
SW8260 75-01-4 Vinyl chloride 0.03 µg/L 1 U 1 U 1 U 1 U 1 U
Cas No.
NE
U
J
µg/L
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L,
Page 10 of 29
Table 5-3
VOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8260 71-55-6 1,1,1-Trichloroethane 200 µg/L
SW8260 79-34-5 1,1,2,2-Tetrachloroethane 0.2 µg/L
SW8260 76-13-1 1,1,2-Trichloro-1,2,2-trifluoroethane 200000 µg/L
SW8260 79-00-5 1,1,2-Trichloroethane 0.6 µg/L
SW8260 75-34-3 1,1-Dichloroethane 6 µg/L
SW8260 75-35-4 1,1-Dichloroethene 350 µg/L
SW8260 120-82-1 1,2,4-Trichlorobenzene 70 µg/L
SW8260 96-12-8 1,2-Dibromo-3-Chloropropane 0.04 µg/L
SW8260 106-93-4 1,2-Dibromoethane (EDB)0.02 µg/L
SW8260 95-50-1 1,2-Dichlorobenzene 20 µg/L
SW8260 107-06-2 1,2-Dichloroethane 0.4 µg/L
SW8260 78-87-5 1,2-Dichloropropane 0.6 µg/L
SW8260 541-73-1 1,3-Dichlorobenzene 200 µg/L
SW8260 106-46-7 1,4-Dichlorobenzene 6 µg/L
SW8260 78-93-3 2-Butanone (MEK)4000 µg/L
SW8260 591-78-6 2-Hexanone 40 µg/L
SW8260 108-10-1 4-Methyl-2-Pentanone (MIBK)100 µg/L
SW8260 67-64-1 Acetone 6000 µg/L
SW8260 71-43-2 Benzene 1 µg/L
SW8260 75-27-4 Bromodichloromethane 0.6 µg/L
SW8260 75-25-2 Bromoform 4 µg/L
SW8260 74-83-9 Bromomethane 10 µg/L
SW8260 75-15-0 Carbon disulfide 700 µg/L
SW8260 56-23-5 Carbon tetrachloride 0.3 µg/L
SW8260 108-90-7 Chlorobenzene 50 µg/L
SW8260 75-00-3 Chloroethane 3000 µg/L
SW8260 67-66-3 Chloroform 70 µg/L
SW8260 74-87-3 Chloromethane 3 µg/L
SW8260 156-59-2 cis-1,2-Dichloroethene 70 µg/L
SW8260 10061-01-5 cis-1,3-Dichloropropene NE µg/L
SW8260 110-82-7 Cyclohexane NE µg/L
SW8260 124-48-1 Dibromochloromethane 0.4 µg/L
SW8260 75-71-8 Dichlorodifluoromethane 1000 µg/L
SW8260 100-41-4 Ethylbenzene 600 µg/L
SW8260 98-82-8 Isopropylbenzene 70 µg/L
SW8260 179601-23-1 m,p-Xylene NE µg/L
SW8260 79-20-9 Methyl acetate NE µg/L
SW8260 1634-04-4 Methyl tert-butyl ether 20 µg/L
SW8260 108-87-2 Methylcyclohexane NE µg/L
SW8260 75-09-2 Methylene chloride 5 µg/L
SW8260 95-47-6 o-Xylene NE µg/L
SW8260 100-42-5 Styrene 70 µg/L
SW8260 127-18-4 Tetrachloroethene 0.7 µg/L
SW8260 108-88-3 Toluene 600 µg/L
SW8260 156-60-5 trans-1,2-Dichloroethene 100 µg/L
SW8260 10061-02-6 trans-1,3-Dichloropropene NE µg/L
SW8260 79-01-6 Trichloroethene 3 µg/L
SW8260 75-69-4 Trichlorofluoromethane 2000 µg/L
SW8260 75-01-4 Vinyl chloride 0.03 µg/L
Cas No.
NE
U
J
µg/L
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L,
PZ03 PZ04 PZ05 PZ06 PZ07
PZ03 WG- 091323 PZ04WG-091923 PZ05 WG- 091323 PZ06WG-091423 PZ07WG-091523
09/13/2023 09/19/2023 09/13/2023 09/14/2023 09/15/2023
Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
2 U 2 U 2 U 2 U 2 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
5 U 5 U 5 U 5 U 5 U
5 U 5 U 5 U 5 U 5 U
5 U 5 U 5 U 5 U 5 U
25 U 18 J 25 U 25 U 15.9 J
1 U 1 U 1 U 1 U 0.46 J
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
2 U 2 U 2 U 2 U 2 U
2 U 2 U 2 U 2 U 2 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 29.7 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 0.71 J 1 U
1 U 1 U 1 U 1 U 1 U
1 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 72.9 1 U 1 U 0.36 J
1 U 2.5 1 U 1 U 1 U
2 U 240 2 U 2 U 1.6 J
10 U 10 U 10 U 10 U 10 U
1 U 1 U 1 U 1 U 1 U
10 U 10 U 10 U 10 U 10 U
5 U 5 U 5 U 5 U 5 U
1 U 119 1 U 1 U 1.7
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1.1 1 U 1 U 2.8
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 6.8 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
Page 11 of 29
Table 5-3
VOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8260 71-55-6 1,1,1-Trichloroethane 200 µg/L
SW8260 79-34-5 1,1,2,2-Tetrachloroethane 0.2 µg/L
SW8260 76-13-1 1,1,2-Trichloro-1,2,2-trifluoroethane 200000 µg/L
SW8260 79-00-5 1,1,2-Trichloroethane 0.6 µg/L
SW8260 75-34-3 1,1-Dichloroethane 6 µg/L
SW8260 75-35-4 1,1-Dichloroethene 350 µg/L
SW8260 120-82-1 1,2,4-Trichlorobenzene 70 µg/L
SW8260 96-12-8 1,2-Dibromo-3-Chloropropane 0.04 µg/L
SW8260 106-93-4 1,2-Dibromoethane (EDB)0.02 µg/L
SW8260 95-50-1 1,2-Dichlorobenzene 20 µg/L
SW8260 107-06-2 1,2-Dichloroethane 0.4 µg/L
SW8260 78-87-5 1,2-Dichloropropane 0.6 µg/L
SW8260 541-73-1 1,3-Dichlorobenzene 200 µg/L
SW8260 106-46-7 1,4-Dichlorobenzene 6 µg/L
SW8260 78-93-3 2-Butanone (MEK)4000 µg/L
SW8260 591-78-6 2-Hexanone 40 µg/L
SW8260 108-10-1 4-Methyl-2-Pentanone (MIBK)100 µg/L
SW8260 67-64-1 Acetone 6000 µg/L
SW8260 71-43-2 Benzene 1 µg/L
SW8260 75-27-4 Bromodichloromethane 0.6 µg/L
SW8260 75-25-2 Bromoform 4 µg/L
SW8260 74-83-9 Bromomethane 10 µg/L
SW8260 75-15-0 Carbon disulfide 700 µg/L
SW8260 56-23-5 Carbon tetrachloride 0.3 µg/L
SW8260 108-90-7 Chlorobenzene 50 µg/L
SW8260 75-00-3 Chloroethane 3000 µg/L
SW8260 67-66-3 Chloroform 70 µg/L
SW8260 74-87-3 Chloromethane 3 µg/L
SW8260 156-59-2 cis-1,2-Dichloroethene 70 µg/L
SW8260 10061-01-5 cis-1,3-Dichloropropene NE µg/L
SW8260 110-82-7 Cyclohexane NE µg/L
SW8260 124-48-1 Dibromochloromethane 0.4 µg/L
SW8260 75-71-8 Dichlorodifluoromethane 1000 µg/L
SW8260 100-41-4 Ethylbenzene 600 µg/L
SW8260 98-82-8 Isopropylbenzene 70 µg/L
SW8260 179601-23-1 m,p-Xylene NE µg/L
SW8260 79-20-9 Methyl acetate NE µg/L
SW8260 1634-04-4 Methyl tert-butyl ether 20 µg/L
SW8260 108-87-2 Methylcyclohexane NE µg/L
SW8260 75-09-2 Methylene chloride 5 µg/L
SW8260 95-47-6 o-Xylene NE µg/L
SW8260 100-42-5 Styrene 70 µg/L
SW8260 127-18-4 Tetrachloroethene 0.7 µg/L
SW8260 108-88-3 Toluene 600 µg/L
SW8260 156-60-5 trans-1,2-Dichloroethene 100 µg/L
SW8260 10061-02-6 trans-1,3-Dichloropropene NE µg/L
SW8260 79-01-6 Trichloroethene 3 µg/L
SW8260 75-69-4 Trichlorofluoromethane 2000 µg/L
SW8260 75-01-4 Vinyl chloride 0.03 µg/L
Cas No.
NE
U
J
µg/L
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L,
PZ08 PZ09 PZ11 PZ12 PZ13
PZ08WG-092123 PZ09WG-092123 PZ11WG-091423 PZ12WG-091423 PZ13WG-091523
09/21/2023 09/21/2023 09/14/2023 09/14/2023 09/15/2023
Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
2 U 2 U 2 U 5 U 2 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
5 U 5 U 5 U 12.5 U 5 U
5 U 5 U 5 U 12.5 U 5 U
5 U 5 U 5 U 12.5 U 5 U
25 U 25 U 25 U 62.5 U 25 U
0.5 J 1 U 1 U 1.1 J 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
2 U 2 U 2 U 5 U 2 U
2 U 2 U 1.6 J 5 U 2 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 0.83 J 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1.1 1 U 2.5 U 2.3
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.4 J 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
87 1 U 0.37 J 15.9 1 U
1.7 1 U 1 U 1 J 1 U
333 2 U 2 J 11.9 2 U
10 U 10 U 10 U 25 U 10 U
1 U 1 U 1 U 2.5 U 1 U
10 U 10 U 10 U 25 U 10 U
5 U 5 U 5 U 12.5 U 5 U
106 1 U 1 7.9 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
3.2 1 U 0.52 J 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
1 U 1 U 1 U 2.5 U 1 U
Page 12 of 29
Table 5-3
VOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8260 71-55-6 1,1,1-Trichloroethane 200 µg/L
SW8260 79-34-5 1,1,2,2-Tetrachloroethane 0.2 µg/L
SW8260 76-13-1 1,1,2-Trichloro-1,2,2-trifluoroethane 200000 µg/L
SW8260 79-00-5 1,1,2-Trichloroethane 0.6 µg/L
SW8260 75-34-3 1,1-Dichloroethane 6 µg/L
SW8260 75-35-4 1,1-Dichloroethene 350 µg/L
SW8260 120-82-1 1,2,4-Trichlorobenzene 70 µg/L
SW8260 96-12-8 1,2-Dibromo-3-Chloropropane 0.04 µg/L
SW8260 106-93-4 1,2-Dibromoethane (EDB)0.02 µg/L
SW8260 95-50-1 1,2-Dichlorobenzene 20 µg/L
SW8260 107-06-2 1,2-Dichloroethane 0.4 µg/L
SW8260 78-87-5 1,2-Dichloropropane 0.6 µg/L
SW8260 541-73-1 1,3-Dichlorobenzene 200 µg/L
SW8260 106-46-7 1,4-Dichlorobenzene 6 µg/L
SW8260 78-93-3 2-Butanone (MEK)4000 µg/L
SW8260 591-78-6 2-Hexanone 40 µg/L
SW8260 108-10-1 4-Methyl-2-Pentanone (MIBK)100 µg/L
SW8260 67-64-1 Acetone 6000 µg/L
SW8260 71-43-2 Benzene 1 µg/L
SW8260 75-27-4 Bromodichloromethane 0.6 µg/L
SW8260 75-25-2 Bromoform 4 µg/L
SW8260 74-83-9 Bromomethane 10 µg/L
SW8260 75-15-0 Carbon disulfide 700 µg/L
SW8260 56-23-5 Carbon tetrachloride 0.3 µg/L
SW8260 108-90-7 Chlorobenzene 50 µg/L
SW8260 75-00-3 Chloroethane 3000 µg/L
SW8260 67-66-3 Chloroform 70 µg/L
SW8260 74-87-3 Chloromethane 3 µg/L
SW8260 156-59-2 cis-1,2-Dichloroethene 70 µg/L
SW8260 10061-01-5 cis-1,3-Dichloropropene NE µg/L
SW8260 110-82-7 Cyclohexane NE µg/L
SW8260 124-48-1 Dibromochloromethane 0.4 µg/L
SW8260 75-71-8 Dichlorodifluoromethane 1000 µg/L
SW8260 100-41-4 Ethylbenzene 600 µg/L
SW8260 98-82-8 Isopropylbenzene 70 µg/L
SW8260 179601-23-1 m,p-Xylene NE µg/L
SW8260 79-20-9 Methyl acetate NE µg/L
SW8260 1634-04-4 Methyl tert-butyl ether 20 µg/L
SW8260 108-87-2 Methylcyclohexane NE µg/L
SW8260 75-09-2 Methylene chloride 5 µg/L
SW8260 95-47-6 o-Xylene NE µg/L
SW8260 100-42-5 Styrene 70 µg/L
SW8260 127-18-4 Tetrachloroethene 0.7 µg/L
SW8260 108-88-3 Toluene 600 µg/L
SW8260 156-60-5 trans-1,2-Dichloroethene 100 µg/L
SW8260 10061-02-6 trans-1,3-Dichloropropene NE µg/L
SW8260 79-01-6 Trichloroethene 3 µg/L
SW8260 75-69-4 Trichlorofluoromethane 2000 µg/L
SW8260 75-01-4 Vinyl chloride 0.03 µg/L
Cas No.
NE
U
J
µg/L
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L,
PZ14 PZ14 PZ17 PZ17 PZ18
PZ14WG-091423 PZ14HG-091423 PZ17 HG- 091323 PZ17 WG- 091323 PZ18WG-091823
09/14/2023 09/14/2023 09/13/2023 09/13/2023 09/18/2023
Normal Field Duplicate Field Duplicate Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
8 U 8 U 2 U 2 U 2 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
56 54.7 5 U 5 U 5 U
89.2 87.4 5 U 5 U 5 U
16.7 J 16.7 J 5 U 5 U 5 U
318 301 25 U 25 U 25 U
106 106 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
8 U 8 U 2 U 2 U 2 U
8 U 8 U 2 U 2 U 2 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
189 190 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
187 183 1 U 1 U 1 U
20.7 20.4 1 U 1 U 1 U
590 576 2 U 2 U 2 U
40 U 40 U 10 U 10 U 10 U
4 U 4 U 1 U 1 U 1 U
119 125 10 U 10 U 10 U
20 U 20 U 5 U 5 U 5 U
120 119 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
55.9 53.8 1 U 1 U 1 U
26.9 J 69.5 J 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
4 U 4 U 1 U 1 U 1 U
Page 13 of 29
Table 5-3
VOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8260 71-55-6 1,1,1-Trichloroethane 200 µg/L
SW8260 79-34-5 1,1,2,2-Tetrachloroethane 0.2 µg/L
SW8260 76-13-1 1,1,2-Trichloro-1,2,2-trifluoroethane 200000 µg/L
SW8260 79-00-5 1,1,2-Trichloroethane 0.6 µg/L
SW8260 75-34-3 1,1-Dichloroethane 6 µg/L
SW8260 75-35-4 1,1-Dichloroethene 350 µg/L
SW8260 120-82-1 1,2,4-Trichlorobenzene 70 µg/L
SW8260 96-12-8 1,2-Dibromo-3-Chloropropane 0.04 µg/L
SW8260 106-93-4 1,2-Dibromoethane (EDB)0.02 µg/L
SW8260 95-50-1 1,2-Dichlorobenzene 20 µg/L
SW8260 107-06-2 1,2-Dichloroethane 0.4 µg/L
SW8260 78-87-5 1,2-Dichloropropane 0.6 µg/L
SW8260 541-73-1 1,3-Dichlorobenzene 200 µg/L
SW8260 106-46-7 1,4-Dichlorobenzene 6 µg/L
SW8260 78-93-3 2-Butanone (MEK)4000 µg/L
SW8260 591-78-6 2-Hexanone 40 µg/L
SW8260 108-10-1 4-Methyl-2-Pentanone (MIBK)100 µg/L
SW8260 67-64-1 Acetone 6000 µg/L
SW8260 71-43-2 Benzene 1 µg/L
SW8260 75-27-4 Bromodichloromethane 0.6 µg/L
SW8260 75-25-2 Bromoform 4 µg/L
SW8260 74-83-9 Bromomethane 10 µg/L
SW8260 75-15-0 Carbon disulfide 700 µg/L
SW8260 56-23-5 Carbon tetrachloride 0.3 µg/L
SW8260 108-90-7 Chlorobenzene 50 µg/L
SW8260 75-00-3 Chloroethane 3000 µg/L
SW8260 67-66-3 Chloroform 70 µg/L
SW8260 74-87-3 Chloromethane 3 µg/L
SW8260 156-59-2 cis-1,2-Dichloroethene 70 µg/L
SW8260 10061-01-5 cis-1,3-Dichloropropene NE µg/L
SW8260 110-82-7 Cyclohexane NE µg/L
SW8260 124-48-1 Dibromochloromethane 0.4 µg/L
SW8260 75-71-8 Dichlorodifluoromethane 1000 µg/L
SW8260 100-41-4 Ethylbenzene 600 µg/L
SW8260 98-82-8 Isopropylbenzene 70 µg/L
SW8260 179601-23-1 m,p-Xylene NE µg/L
SW8260 79-20-9 Methyl acetate NE µg/L
SW8260 1634-04-4 Methyl tert-butyl ether 20 µg/L
SW8260 108-87-2 Methylcyclohexane NE µg/L
SW8260 75-09-2 Methylene chloride 5 µg/L
SW8260 95-47-6 o-Xylene NE µg/L
SW8260 100-42-5 Styrene 70 µg/L
SW8260 127-18-4 Tetrachloroethene 0.7 µg/L
SW8260 108-88-3 Toluene 600 µg/L
SW8260 156-60-5 trans-1,2-Dichloroethene 100 µg/L
SW8260 10061-02-6 trans-1,3-Dichloropropene NE µg/L
SW8260 79-01-6 Trichloroethene 3 µg/L
SW8260 75-69-4 Trichlorofluoromethane 2000 µg/L
SW8260 75-01-4 Vinyl chloride 0.03 µg/L
Cas No.
NE
U
J
µg/L
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L,
PZ20 PZ21 RW01 RW02 RW03
PZ20WG-091923 PZ21WG-091923 RW01WG-091923 RW02W6-091223 RW03W6-091223
09/19/2023 09/19/2023 09/19/2023 09/12/2023 09/12/2023
Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
2 U 2 U 2 U 2 U 2 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
5 U 5 U 5 U 5 U 5 U
5 U 5 U 5 U 5 U 5 U
5 U 5 U 5 U 5 U 5 U
26.5 25 U 25 U 25 U 25 U
1 U 1 U 2.7 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
2 U 2 U 2 U 2 U 2 U
2 U 2 U 2 U 2 U 2 U
1 U 1 U 1 U 1 U 1 U
0.44 J 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 0.76 J 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
4.3 1 U 1 U 1 U 1 U
1 U 1 U 1 U 0.64 J 1 U
2 U 2 U 0.71 J 2 U 2 U
10 U 10 U 10 U 10 U 10 U
1 U 1 U 1 U 1 U 1 U
10 U 10 U 10 U 10 U 10 U
5 U 5 U 5 U 5 U 5 U
1 U 1 U 0.4 J 1 U 1 U
0.64 J 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
20.5 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
1 U 1 U 1 U 1 U 1 U
Page 14 of 29
Table 5-3
VOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8260 71-55-6 1,1,1-Trichloroethane 200 µg/L
SW8260 79-34-5 1,1,2,2-Tetrachloroethane 0.2 µg/L
SW8260 76-13-1 1,1,2-Trichloro-1,2,2-trifluoroethane 200000 µg/L
SW8260 79-00-5 1,1,2-Trichloroethane 0.6 µg/L
SW8260 75-34-3 1,1-Dichloroethane 6 µg/L
SW8260 75-35-4 1,1-Dichloroethene 350 µg/L
SW8260 120-82-1 1,2,4-Trichlorobenzene 70 µg/L
SW8260 96-12-8 1,2-Dibromo-3-Chloropropane 0.04 µg/L
SW8260 106-93-4 1,2-Dibromoethane (EDB)0.02 µg/L
SW8260 95-50-1 1,2-Dichlorobenzene 20 µg/L
SW8260 107-06-2 1,2-Dichloroethane 0.4 µg/L
SW8260 78-87-5 1,2-Dichloropropane 0.6 µg/L
SW8260 541-73-1 1,3-Dichlorobenzene 200 µg/L
SW8260 106-46-7 1,4-Dichlorobenzene 6 µg/L
SW8260 78-93-3 2-Butanone (MEK)4000 µg/L
SW8260 591-78-6 2-Hexanone 40 µg/L
SW8260 108-10-1 4-Methyl-2-Pentanone (MIBK)100 µg/L
SW8260 67-64-1 Acetone 6000 µg/L
SW8260 71-43-2 Benzene 1 µg/L
SW8260 75-27-4 Bromodichloromethane 0.6 µg/L
SW8260 75-25-2 Bromoform 4 µg/L
SW8260 74-83-9 Bromomethane 10 µg/L
SW8260 75-15-0 Carbon disulfide 700 µg/L
SW8260 56-23-5 Carbon tetrachloride 0.3 µg/L
SW8260 108-90-7 Chlorobenzene 50 µg/L
SW8260 75-00-3 Chloroethane 3000 µg/L
SW8260 67-66-3 Chloroform 70 µg/L
SW8260 74-87-3 Chloromethane 3 µg/L
SW8260 156-59-2 cis-1,2-Dichloroethene 70 µg/L
SW8260 10061-01-5 cis-1,3-Dichloropropene NE µg/L
SW8260 110-82-7 Cyclohexane NE µg/L
SW8260 124-48-1 Dibromochloromethane 0.4 µg/L
SW8260 75-71-8 Dichlorodifluoromethane 1000 µg/L
SW8260 100-41-4 Ethylbenzene 600 µg/L
SW8260 98-82-8 Isopropylbenzene 70 µg/L
SW8260 179601-23-1 m,p-Xylene NE µg/L
SW8260 79-20-9 Methyl acetate NE µg/L
SW8260 1634-04-4 Methyl tert-butyl ether 20 µg/L
SW8260 108-87-2 Methylcyclohexane NE µg/L
SW8260 75-09-2 Methylene chloride 5 µg/L
SW8260 95-47-6 o-Xylene NE µg/L
SW8260 100-42-5 Styrene 70 µg/L
SW8260 127-18-4 Tetrachloroethene 0.7 µg/L
SW8260 108-88-3 Toluene 600 µg/L
SW8260 156-60-5 trans-1,2-Dichloroethene 100 µg/L
SW8260 10061-02-6 trans-1,3-Dichloropropene NE µg/L
SW8260 79-01-6 Trichloroethene 3 µg/L
SW8260 75-69-4 Trichlorofluoromethane 2000 µg/L
SW8260 75-01-4 Vinyl chloride 0.03 µg/L
Cas No.
NE
U
J
µg/L
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L,
RW04 RW05 RW06 RW07
09/13/2023 10/17/2023 09/13/2023 09/13/2023
Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
7.6 10 U 1 U 1 U
4 U 20 U 2 U 2 U
2 U 10 U 1 U 1 U
3.1 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
9 10 U 1 U 1 U
3.1 10 U 1 U 1 U
10 U 50 U 5 U 5 U
10 U 50 U 5 U 5 U
10 U 50 U 5 U 5 U
50 U 85.5 J 25 U 25 U
1.3 J 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
4 U 20 U 2 U 2 U
4 U 20 U 2 U 2 U
2 U 10 U 1 U 1 U
3.2 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
3.5 4.6 J 1 U 1 U
2 U 10 U 1 U 1 U
10.2 9.1 J 2 U 2 U
20 U 100 U 10 U 10 U
2 U 10 U 1 U 1 U
20 U 100 U 10 U 10 U
10 U 50 U 5 U 5 U
4.8 4.5 J 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 8.8 J 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
2 U 10 U 1 U 1 U
Page 15 of 29
Table 5-4SVOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
BR01 BR02 BR03 PZ01 PZ02 PZ03 PZ04 PZ05
BR01WG-091423 BR03WG-091423 PZ02WG-091423 PZ04WG-091923
09/14/2023 09/13/2023 09/14/2023 09/13/2023 09/14/2023 09/13/2023 09/19/2023 09/13/2023
Normal Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
Method CAS No.Analyte NC 02L GWQS Units
SW8270 108-60-1 2,2-Oxybis(1-chloropropane)NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 95-95-4 2,4,5-Trichlorophenol 63 µg/L 10 UJ 10 U 10 UJ 10 U 50 U 10 UJ 50 U 8.3 U
SW8270 88-06-2 2,4,6-Trichlorophenol 4 µg/L 10 UJ 10 U 10 UR 10 U 50 U 10 UJ 50 U 8.3 U
SW8270 120-83-2 2,4-Dichlorophenol 0.98 µg/L 10 UJ 10 U 10 UJ 10 U 50 U 10 UJ 50 U 8.3 U
SW8270 105-67-9 2,4-Dimethylphenol 100 µg/L 10 UJ 10 U 10 UJ 10 U 50 U 10 UJ 50 U 8.3 U
SW8270 51-28-5 2,4-Dinitrophenol NE µg/L 50 UJ 50 U 50 UR 50 U 250 U 50 UJ 250 U 41.7 U
SW8270 121-14-2 2,4-Dinitrotoluene 0.05 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 606-20-2 2,6-Dinitrotoluene 0.05 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 91-58-7 2-Chloronaphthalene NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 95-57-8 2-Chlorophenol 0.4 µg/L 10 UJ 10 U 10 UJ 10 U 50 U 10 UJ 50 U 8.3 U
SW8270 534-52-1 2-Methyl-4,6-Dinitrophenol NE µg/L 20 UJ 20 U 20 UJ 20 U 100 U 20 UJ 100 U 16.7 U
SW8270 91-57-6 2-Methylnaphthalene 30 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 95-48-7 2-Methylphenol (o-Cresol)400 µg/L 10 UJ 10 U 10 UJ 10 U 50 U 10 UJ 50 U 8.3 U
SW8270 88-74-4 2-Nitroaniline NE µg/L 20 U 20 U 20 U 20 U 100 U 20 U 100 U 16.7 U
SW8270 88-75-5 2-Nitrophenol NE µg/L 10 UJ 10 U 10 UR 10 U 50 U 10 UJ 50 U 8.3 U
SW8270 91-94-1 3,3'-Dichlorobenzidine NE µg/L 20 U 20 U 20 U 20 U 100 U 20 U 100 U 16.7 U
SW8270 9999900-32-2 3-Methylphenol/4-Methylphenol NE µg/L 10 UJ 10 U 10 UJ 10 U 17 J 10 UJ 50 U 8.3 U
SW8270 99-09-2 3-Nitroaniline NE µg/L 20 U 20 U 20 U 20 U 100 U 20 U 100 U 16.7 U
SW8270 101-55-3 4-Bromophenyl-phenylether NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 59-50-7 4-Chloro-3-methylphenol NE µg/L 10 UJ 10 U 10 UJ 10 U 50 U 10 UJ 50 U 8.3 U
SW8270 106-47-8 4-Chloroaniline NE µg/L 20 U 20 U 20 U 20 U 100 U 20 U 100 U 16.7 U
SW8270 7005-72-3 4-Chlorophenylphenyl ether NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 100-01-6 4-Nitroaniline NE µg/L 20 U 20 U 20 U 20 U 100 U 20 U 100 U 16.7 U
SW8270 100-02-7 4-Nitrophenol NE µg/L 50 U 50 U 50 UR 50 U 250 U 50 U 250 U 41.7 UJ
SW8270 83-32-9 Acenaphthene 80 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 208-96-8 Acenaphthylene 200 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 98-86-2 Acetophenone 700 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 120-12-7 Anthracene 2000 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 1912-24-9 Atrazine 3 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 100-52-7 Benzaldehyde NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 56-55-3 Benzo(a)anthracene 0.05 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 50-32-8 Benzo(a)pyrene 0.005 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 205-99-2 Benzo(b)fluoranthene 0.05 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 191-24-2 Benzo(g,h,i)perylene 200 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 207-08-9 Benzo(k)fluoranthene 0.5 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 92-52-4 Biphenyl 400 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 111-91-1 bis(2-Chloroethoxy)methane NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 111-44-4 bis(2-Chloroethyl)ether 0.03 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 117-81-7 bis(2-Ethylhexyl)phthalate 3 µg/L 6 U 6 U 6 U 6 U 30 U 6 U 30 U 5 U
SW8270 85-68-7 Butylbenzylphthalate 1000 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 105-60-2 Caprolactam 4000 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 86-74-8 Carbazole NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 218-01-9 Chrysene 5 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 84-74-2 Di-n-butylphthalate 700 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 117-84-0 Di-n-octylphthalate 100 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 53-70-3 Dibenz(a,h)anthracene 0.005 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 132-64-9 Dibenzofuran NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 84-66-2 Diethylphthalate 6000 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 131-11-3 Dimethylphthalate NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 206-44-0 Fluoranthene 300 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 86-73-7 Fluorene 300 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 118-74-1 Hexachlorobenzene 0.02 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 87-68-3 Hexachlorobutadiene 0.4 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 77-47-4 Hexachlorocyclopentadiene NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 67-72-1 Hexachloroethane NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 193-39-5 Indeno(1,2,3-cd)pyrene 0.05 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 78-59-1 Isophorone 40 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 621-64-7 N-Nitroso-di-n-propylamine NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 86-30-6 N-Nitrosodiphenylamine NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 91-20-3 Naphthalene 6 µg/L 10 U 10 U 10 U 3.4 J 50 U 10 U 50 U 8.3 U
SW8270 98-95-3 Nitrobenzene NE µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 87-86-5 Pentachlorophenol 0.3 µg/L 20 U 20 U 20 UJ 20 U 100 U 20 U 100 U 16.7 U
SW8270 85-01-8 Phenanthrene 200 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
SW8270 108-95-2 Phenol 30 µg/L 10 UJ 10 U 10 UJ 10 U 49.1 J 10 UJ 50 U 8.3 U
SW8270 129-00-0 Pyrene 200 µg/L 10 U 10 U 10 U 10 U 50 U 10 U 50 U 8.3 U
Cas No. = Chemical Abstracts Service number
NE = Not established
U
UJ = Not detected and estimated, shown with reporting limit
J = Estimated value
J- = Estimated value, bias low
µg/L
Bold
Highlighted = Exceeds the NC 02L GWQS
= Not detected, shown with reporting limit
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
Page 16 of 29
Table 5-4SVOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8270 108-60-1 2,2-Oxybis(1-chloropropane)NE µg/L
SW8270 95-95-4 2,4,5-Trichlorophenol 63 µg/L
SW8270 88-06-2 2,4,6-Trichlorophenol 4 µg/L
SW8270 120-83-2 2,4-Dichlorophenol 0.98 µg/L
SW8270 105-67-9 2,4-Dimethylphenol 100 µg/L
SW8270 51-28-5 2,4-Dinitrophenol NE µg/L
SW8270 121-14-2 2,4-Dinitrotoluene 0.05 µg/L
SW8270 606-20-2 2,6-Dinitrotoluene 0.05 µg/L
SW8270 91-58-7 2-Chloronaphthalene NE µg/L
SW8270 95-57-8 2-Chlorophenol 0.4 µg/L
SW8270 534-52-1 2-Methyl-4,6-Dinitrophenol NE µg/L
SW8270 91-57-6 2-Methylnaphthalene 30 µg/L
SW8270 95-48-7 2-Methylphenol (o-Cresol)400 µg/L
SW8270 88-74-4 2-Nitroaniline NE µg/L
SW8270 88-75-5 2-Nitrophenol NE µg/L
SW8270 91-94-1 3,3'-Dichlorobenzidine NE µg/L
SW8270 9999900-32-2 3-Methylphenol/4-Methylphenol NE µg/L
SW8270 99-09-2 3-Nitroaniline NE µg/L
SW8270 101-55-3 4-Bromophenyl-phenylether NE µg/L
SW8270 59-50-7 4-Chloro-3-methylphenol NE µg/L
SW8270 106-47-8 4-Chloroaniline NE µg/L
SW8270 7005-72-3 4-Chlorophenylphenyl ether NE µg/L
SW8270 100-01-6 4-Nitroaniline NE µg/L
SW8270 100-02-7 4-Nitrophenol NE µg/L
SW8270 83-32-9 Acenaphthene 80 µg/L
SW8270 208-96-8 Acenaphthylene 200 µg/L
SW8270 98-86-2 Acetophenone 700 µg/L
SW8270 120-12-7 Anthracene 2000 µg/L
SW8270 1912-24-9 Atrazine 3 µg/L
SW8270 100-52-7 Benzaldehyde NE µg/L
SW8270 56-55-3 Benzo(a)anthracene 0.05 µg/L
SW8270 50-32-8 Benzo(a)pyrene 0.005 µg/L
SW8270 205-99-2 Benzo(b)fluoranthene 0.05 µg/L
SW8270 191-24-2 Benzo(g,h,i)perylene 200 µg/L
SW8270 207-08-9 Benzo(k)fluoranthene 0.5 µg/L
SW8270 92-52-4 Biphenyl 400 µg/L
SW8270 111-91-1 bis(2-Chloroethoxy)methane NE µg/L
SW8270 111-44-4 bis(2-Chloroethyl)ether 0.03 µg/L
SW8270 117-81-7 bis(2-Ethylhexyl)phthalate 3 µg/L
SW8270 85-68-7 Butylbenzylphthalate 1000 µg/L
SW8270 105-60-2 Caprolactam 4000 µg/L
SW8270 86-74-8 Carbazole NE µg/L
SW8270 218-01-9 Chrysene 5 µg/L
SW8270 84-74-2 Di-n-butylphthalate 700 µg/L
SW8270 117-84-0 Di-n-octylphthalate 100 µg/L
SW8270 53-70-3 Dibenz(a,h)anthracene 0.005 µg/L
SW8270 132-64-9 Dibenzofuran NE µg/L
SW8270 84-66-2 Diethylphthalate 6000 µg/L
SW8270 131-11-3 Dimethylphthalate NE µg/L
SW8270 206-44-0 Fluoranthene 300 µg/L
SW8270 86-73-7 Fluorene 300 µg/L
SW8270 118-74-1 Hexachlorobenzene 0.02 µg/L
SW8270 87-68-3 Hexachlorobutadiene 0.4 µg/L
SW8270 77-47-4 Hexachlorocyclopentadiene NE µg/L
SW8270 67-72-1 Hexachloroethane NE µg/L
SW8270 193-39-5 Indeno(1,2,3-cd)pyrene 0.05 µg/L
SW8270 78-59-1 Isophorone 40 µg/L
SW8270 621-64-7 N-Nitroso-di-n-propylamine NE µg/L
SW8270 86-30-6 N-Nitrosodiphenylamine NE µg/L
SW8270 91-20-3 Naphthalene 6 µg/L
SW8270 98-95-3 Nitrobenzene NE µg/L
SW8270 87-86-5 Pentachlorophenol 0.3 µg/L
SW8270 85-01-8 Phenanthrene 200 µg/L
SW8270 108-95-2 Phenol 30 µg/L
SW8270 129-00-0 Pyrene 200 µg/L
= Chemical Abstracts Service number
= Not established
= Not detected and estimated, shown with reporting limit
= Estimated value
= Estimated value, bias low
Bold
Highlighted = Exceeds the NC 02L GWQS
= Not detected, shown with reporting limit
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
PZ06 PZ07 PZ08 PZ09 PZ11 PZ12 PZ13
PZ06WG-091423 PZ07WG-091523 PZ08WG-092123 PZ09WG-092123 PZ11WG-091423 PZ12WG-091423 PZ13WG-091523
09/14/2023 09/15/2023 09/21/2023 09/21/2023 09/14/2023 09/14/2023 09/15/2023
Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
50 U 250 U 50 U 50 U 250 U 250 U 50 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
20 U 100 U 20 U 20 U 100 U 100 U 20 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
20 U 100 U 20 U 20 U 100 U 100 U 20 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
20 U 100 U 20 U 20 U 100 U 100 U 20 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
20 U 100 U 20 U 20 U 100 U 100 U 20 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
20 U 100 U 20 U 20 U 100 U 100 U 20 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
20 U 100 U 20 U 20 U 100 U 100 U 20 U
50 U 250 U 50 U 50 U 250 U 250 U 50 U
10 U 50 U 10 U 10 U 50 U 87.7 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 22.4 J 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
6 U 30 U 6 U 6 U 30 U 30 U 6 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 16.8 J 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 44.5 J 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 29.8 J 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 15.1 10 U 50 U 108 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
20 U 100 U 20 U 20 U 100 U 100 U 20 U
10 U 50 U 2.9 J 10 U 50 U 34.1 J 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
10 U 50 U 10 U 10 U 50 U 50 U 10 U
Page 17 of 29
Table 5-4SVOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8270 108-60-1 2,2-Oxybis(1-chloropropane)NE µg/L
SW8270 95-95-4 2,4,5-Trichlorophenol 63 µg/L
SW8270 88-06-2 2,4,6-Trichlorophenol 4 µg/L
SW8270 120-83-2 2,4-Dichlorophenol 0.98 µg/L
SW8270 105-67-9 2,4-Dimethylphenol 100 µg/L
SW8270 51-28-5 2,4-Dinitrophenol NE µg/L
SW8270 121-14-2 2,4-Dinitrotoluene 0.05 µg/L
SW8270 606-20-2 2,6-Dinitrotoluene 0.05 µg/L
SW8270 91-58-7 2-Chloronaphthalene NE µg/L
SW8270 95-57-8 2-Chlorophenol 0.4 µg/L
SW8270 534-52-1 2-Methyl-4,6-Dinitrophenol NE µg/L
SW8270 91-57-6 2-Methylnaphthalene 30 µg/L
SW8270 95-48-7 2-Methylphenol (o-Cresol)400 µg/L
SW8270 88-74-4 2-Nitroaniline NE µg/L
SW8270 88-75-5 2-Nitrophenol NE µg/L
SW8270 91-94-1 3,3'-Dichlorobenzidine NE µg/L
SW8270 9999900-32-2 3-Methylphenol/4-Methylphenol NE µg/L
SW8270 99-09-2 3-Nitroaniline NE µg/L
SW8270 101-55-3 4-Bromophenyl-phenylether NE µg/L
SW8270 59-50-7 4-Chloro-3-methylphenol NE µg/L
SW8270 106-47-8 4-Chloroaniline NE µg/L
SW8270 7005-72-3 4-Chlorophenylphenyl ether NE µg/L
SW8270 100-01-6 4-Nitroaniline NE µg/L
SW8270 100-02-7 4-Nitrophenol NE µg/L
SW8270 83-32-9 Acenaphthene 80 µg/L
SW8270 208-96-8 Acenaphthylene 200 µg/L
SW8270 98-86-2 Acetophenone 700 µg/L
SW8270 120-12-7 Anthracene 2000 µg/L
SW8270 1912-24-9 Atrazine 3 µg/L
SW8270 100-52-7 Benzaldehyde NE µg/L
SW8270 56-55-3 Benzo(a)anthracene 0.05 µg/L
SW8270 50-32-8 Benzo(a)pyrene 0.005 µg/L
SW8270 205-99-2 Benzo(b)fluoranthene 0.05 µg/L
SW8270 191-24-2 Benzo(g,h,i)perylene 200 µg/L
SW8270 207-08-9 Benzo(k)fluoranthene 0.5 µg/L
SW8270 92-52-4 Biphenyl 400 µg/L
SW8270 111-91-1 bis(2-Chloroethoxy)methane NE µg/L
SW8270 111-44-4 bis(2-Chloroethyl)ether 0.03 µg/L
SW8270 117-81-7 bis(2-Ethylhexyl)phthalate 3 µg/L
SW8270 85-68-7 Butylbenzylphthalate 1000 µg/L
SW8270 105-60-2 Caprolactam 4000 µg/L
SW8270 86-74-8 Carbazole NE µg/L
SW8270 218-01-9 Chrysene 5 µg/L
SW8270 84-74-2 Di-n-butylphthalate 700 µg/L
SW8270 117-84-0 Di-n-octylphthalate 100 µg/L
SW8270 53-70-3 Dibenz(a,h)anthracene 0.005 µg/L
SW8270 132-64-9 Dibenzofuran NE µg/L
SW8270 84-66-2 Diethylphthalate 6000 µg/L
SW8270 131-11-3 Dimethylphthalate NE µg/L
SW8270 206-44-0 Fluoranthene 300 µg/L
SW8270 86-73-7 Fluorene 300 µg/L
SW8270 118-74-1 Hexachlorobenzene 0.02 µg/L
SW8270 87-68-3 Hexachlorobutadiene 0.4 µg/L
SW8270 77-47-4 Hexachlorocyclopentadiene NE µg/L
SW8270 67-72-1 Hexachloroethane NE µg/L
SW8270 193-39-5 Indeno(1,2,3-cd)pyrene 0.05 µg/L
SW8270 78-59-1 Isophorone 40 µg/L
SW8270 621-64-7 N-Nitroso-di-n-propylamine NE µg/L
SW8270 86-30-6 N-Nitrosodiphenylamine NE µg/L
SW8270 91-20-3 Naphthalene 6 µg/L
SW8270 98-95-3 Nitrobenzene NE µg/L
SW8270 87-86-5 Pentachlorophenol 0.3 µg/L
SW8270 85-01-8 Phenanthrene 200 µg/L
SW8270 108-95-2 Phenol 30 µg/L
SW8270 129-00-0 Pyrene 200 µg/L
= Chemical Abstracts Service number
= Not established
= Not detected and estimated, shown with reporting limit
= Estimated value
= Estimated value, bias low
Bold
Highlighted = Exceeds the NC 02L GWQS
= Not detected, shown with reporting limit
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
PZ14 PZ14 PZ17 PZ17 PZ18 PZ20 PZ21
PZ14WG-091423 PZ14HG-091423 PZ17 HG- 091323 PZ18WG-091823 PZ20WG-091923 PZ21WG-091923
09/14/2023 09/14/2023 09/13/2023 09/13/2023 09/18/2023 09/19/2023 09/19/2023
Normal Field Duplicate Normal Field Duplicate Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 UJ 10 U 8.3 UJ 100 U 10 U
8.7 U 8.3 U 10 UJ 10 U 8.3 UJ 100 U 10 U
8.7 U 8.3 U 10 UJ 10 U 8.3 UJ 100 U 10 U
16.9 11.8 10 UJ 10 U 8.3 UJ 100 U 10 U
43.5 U 41.7 U 50 UJ 50 U 41.7 UJ 500 U 50 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 UJ 10 U 8.3 UJ 100 U 10 U
17.4 U 16.7 U 20 UJ 20 U 16.7 UJ 200 U 20 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 2.1 J 10 UJ 10 U 8.3 UJ 100 U 10 U
17.4 U 16.7 U 20 U 20 U 16.7 U 200 U 20 U
8.7 U 8.3 U 10 UJ 10 U 8.3 UJ 100 U 10 U
17.4 U 16.7 U 20 U 20 U 16.7 U 200 U 20 U
13.1 11.2 10 UJ 10 U 8.3 UJ 100 U 10 U
17.4 U 16.7 U 20 U 20 U 16.7 U 200 U 20 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 UJ 10 U 8.3 UJ 100 U 10 U
17.4 U 16.7 U 20 U 20 U 16.7 U 200 U 20 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
17.4 U 16.7 U 20 U 20 U 16.7 U 200 U 20 U
43.5 U 41.7 U 50 U 50 U 41.7 U 500 U 50 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
5.2 U 5 U 6 U 4.4 J 5 U 60 U 6 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
13.2 12.5 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
17.4 U 16.7 U 20 U 20 U 16.7 U 200 U 20 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
8.7 U 8.3 U 10 UJ 10 U 8.3 UJ 100 U 10 U
8.7 U 8.3 U 10 U 10 U 8.3 U 100 U 10 U
Page 18 of 29
Table 5-4SVOCs in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8270 108-60-1 2,2-Oxybis(1-chloropropane)NE µg/L
SW8270 95-95-4 2,4,5-Trichlorophenol 63 µg/L
SW8270 88-06-2 2,4,6-Trichlorophenol 4 µg/L
SW8270 120-83-2 2,4-Dichlorophenol 0.98 µg/L
SW8270 105-67-9 2,4-Dimethylphenol 100 µg/L
SW8270 51-28-5 2,4-Dinitrophenol NE µg/L
SW8270 121-14-2 2,4-Dinitrotoluene 0.05 µg/L
SW8270 606-20-2 2,6-Dinitrotoluene 0.05 µg/L
SW8270 91-58-7 2-Chloronaphthalene NE µg/L
SW8270 95-57-8 2-Chlorophenol 0.4 µg/L
SW8270 534-52-1 2-Methyl-4,6-Dinitrophenol NE µg/L
SW8270 91-57-6 2-Methylnaphthalene 30 µg/L
SW8270 95-48-7 2-Methylphenol (o-Cresol)400 µg/L
SW8270 88-74-4 2-Nitroaniline NE µg/L
SW8270 88-75-5 2-Nitrophenol NE µg/L
SW8270 91-94-1 3,3'-Dichlorobenzidine NE µg/L
SW8270 9999900-32-2 3-Methylphenol/4-Methylphenol NE µg/L
SW8270 99-09-2 3-Nitroaniline NE µg/L
SW8270 101-55-3 4-Bromophenyl-phenylether NE µg/L
SW8270 59-50-7 4-Chloro-3-methylphenol NE µg/L
SW8270 106-47-8 4-Chloroaniline NE µg/L
SW8270 7005-72-3 4-Chlorophenylphenyl ether NE µg/L
SW8270 100-01-6 4-Nitroaniline NE µg/L
SW8270 100-02-7 4-Nitrophenol NE µg/L
SW8270 83-32-9 Acenaphthene 80 µg/L
SW8270 208-96-8 Acenaphthylene 200 µg/L
SW8270 98-86-2 Acetophenone 700 µg/L
SW8270 120-12-7 Anthracene 2000 µg/L
SW8270 1912-24-9 Atrazine 3 µg/L
SW8270 100-52-7 Benzaldehyde NE µg/L
SW8270 56-55-3 Benzo(a)anthracene 0.05 µg/L
SW8270 50-32-8 Benzo(a)pyrene 0.005 µg/L
SW8270 205-99-2 Benzo(b)fluoranthene 0.05 µg/L
SW8270 191-24-2 Benzo(g,h,i)perylene 200 µg/L
SW8270 207-08-9 Benzo(k)fluoranthene 0.5 µg/L
SW8270 92-52-4 Biphenyl 400 µg/L
SW8270 111-91-1 bis(2-Chloroethoxy)methane NE µg/L
SW8270 111-44-4 bis(2-Chloroethyl)ether 0.03 µg/L
SW8270 117-81-7 bis(2-Ethylhexyl)phthalate 3 µg/L
SW8270 85-68-7 Butylbenzylphthalate 1000 µg/L
SW8270 105-60-2 Caprolactam 4000 µg/L
SW8270 86-74-8 Carbazole NE µg/L
SW8270 218-01-9 Chrysene 5 µg/L
SW8270 84-74-2 Di-n-butylphthalate 700 µg/L
SW8270 117-84-0 Di-n-octylphthalate 100 µg/L
SW8270 53-70-3 Dibenz(a,h)anthracene 0.005 µg/L
SW8270 132-64-9 Dibenzofuran NE µg/L
SW8270 84-66-2 Diethylphthalate 6000 µg/L
SW8270 131-11-3 Dimethylphthalate NE µg/L
SW8270 206-44-0 Fluoranthene 300 µg/L
SW8270 86-73-7 Fluorene 300 µg/L
SW8270 118-74-1 Hexachlorobenzene 0.02 µg/L
SW8270 87-68-3 Hexachlorobutadiene 0.4 µg/L
SW8270 77-47-4 Hexachlorocyclopentadiene NE µg/L
SW8270 67-72-1 Hexachloroethane NE µg/L
SW8270 193-39-5 Indeno(1,2,3-cd)pyrene 0.05 µg/L
SW8270 78-59-1 Isophorone 40 µg/L
SW8270 621-64-7 N-Nitroso-di-n-propylamine NE µg/L
SW8270 86-30-6 N-Nitrosodiphenylamine NE µg/L
SW8270 91-20-3 Naphthalene 6 µg/L
SW8270 98-95-3 Nitrobenzene NE µg/L
SW8270 87-86-5 Pentachlorophenol 0.3 µg/L
SW8270 85-01-8 Phenanthrene 200 µg/L
SW8270 108-95-2 Phenol 30 µg/L
SW8270 129-00-0 Pyrene 200 µg/L
Cas No. = Chemical Abstracts Service number
NE = Not established
U
UJ = Not detected and estimated, shown with reporting limit
J = Estimated value
J- = Estimated value, bias low
µg/L
Bold
Highlighted = Exceeds the NC 02L GWQS
= Not detected, shown with reporting limit
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
RW01 RW02 RW03 RW04 RW05 RW06 RW07
RW01WG-091923 RW02W6-091223 RW03W6-091223
09/19/2023 09/12/2023 09/12/2023 09/13/2023 10/17/2023 09/13/2023 09/13/2023
Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 UJ 10 UJ 10 U
10 U 8.7 U 8.3 U 10 U 8.7 UJ 10 UJ 10 U
10 U 8.7 U 8.3 U 10 U 8.7 UJ 10 UJ 10 U
10 U 8.7 U 8.3 U 2.2 J 1.7 J-10 UJ 10 U
50 U 43.5 U 41.7 U 50 U 43.5 UJ 50 UJ 50 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 UJ 10 UJ 10 U
20 U 17.4 U 16.7 U 20 U 17.4 UJ 20 UJ 20 U
10 U 8.7 U 8.3 U 18.5 17.7 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 UJ 10 UJ 10 U
20 U 17.4 U 16.7 U 20 U 17.4 U 20 U 20 U
10 U 8.7 U 8.3 U 10 U 8.7 UJ 10 UJ 10 U
20 U 17.4 U 16.7 U 20 U 17.4 U 20 U 20 U
10 U 8.7 U 8.3 U 10 U 8.7 UJ 10 UJ 10 U
20 U 17.4 U 16.7 U 20 U 17.4 U 20 U 20 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 UJ 10 UJ 10 U
20 U 17.4 U 16.7 U 20 U 17.4 U 20 U 20 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
20 U 17.4 U 16.7 U 20 U 17.4 U 20 U 20 U
50 U 43.5 U 41.7 U 50 U 43.5 UJ 50 U 50 U
10 U 1.9 J 8.3 U 19.2 12.4 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 3.4 J 2.3 J 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
6 U 5.2 U 5 U 6 U 5.2 U 6 U 6 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 11 12 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10.4 5 J 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 5.7 J 8.3 U 5.8 J 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10.8 4.3 J 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
10 U 8.7 U 8.3 U 130 225 10 U 10 U
10 U 8.7 U 8.3 U 10 U 8.7 U 10 U 10 U
20 U 17.4 U 16.7 U 20 U 17.4 UJ 20 U 20 U
10 U 8.7 U 8.3 U 20.6 2.4 J 10 U 10 U
10 U 8.7 U 8.3 U 10 U 6.2 J-10 UJ 10 U
10 U 4.6 J 8.3 U 3.7 J 8.7 U 10 U 10 U
Page 19 of 29
Table 5-5
Dioxins and Furans in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
BR01 BR03 PZ01 PZ02 PZ03 PZ04 PZ05 PZ06 PZ07 PZ08
BR01WG-091423 BR03WG-091423 PZ01 WG- 091323 PZ02WG-091423 PZ03 WG- 091323 PZ04WG-091923 PZ05 WG- 091323 PZ06WG-091423 PZ07WG-091523 PZ08WG-092123
09/14/2023 09/14/2023 09/13/2023 09/14/2023 09/13/2023 09/19/2023 09/13/2023 09/14/2023 09/15/2023 09/21/2023
Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
Method CAS No.Analyte NC 02L GWQS Units
SW8290 567562-39-4 1,2,3,4,6,7,8-HpCDF NE pg/L 1.4 U 1.9 U 1.8 U 97 J 5.6 U 110 1.2 U 1.5 U 120 J 53 U
SW8290 555673-89-7 1,2,3,4,7,8,9-HpCDF NE pg/L 2.6 U 3.1 U 3.3 U 100 U 10 U 86 U 2 U 2.5 U 110 U 53 U
SW8290 570648-26-9 1,2,3,4,7,8-HxCDF NE pg/L 0.84 U 1 U 1.7 U 45 U 3.9 U 47 U 0.89 U 0.76 U 38 U 53 U
SW8290 557653-85-7 1,2,3,6,7,8-HxCDD NE pg/L 0.86 U 1.3 U 0.87 U 46 U 3.7 U 31 U 0.98 U 0.85 U 33 U 4.6 J
SW8290 557117-44-9 1,2,3,6,7,8-HxCDF NE pg/L 0.81 U 1 U 1.1 U 45 U 2.3 U 34 U 0.68 U 0.72 U 38 U 1.5 J
SW8290 572918-21-9 1,2,3,7,8,9-HxCDF NE pg/L 1.1 U 1.4 U 1.3 U 72 U 3.1 U 51 U 0.91 U 1.1 U 57 U 53 U
SW8290 557117-41-6 1,2,3,7,8-PeCDF NE pg/L 0.82 U 1.1 U 0.65 U 19 U 1.8 U 14 U 0.43 U 1.3 U 35 U 53 U
SW8290 35822-46-9 1234678-HpCDD NE pg/L 1.2 U 2.1 U 1.4 U 57 U 5.2 U 74 1.5 U 1.8 U 770 53 U
SW8290 39227-28-6 123478-HxCDD NE pg/L 1 U 1.5 U 0.95 U 60 U 3.9 U 34 U 1.1 U 1.1 U 40 U 53 U
SW8290 40321-76-4 12378-PeCDD NE pg/L 0.85 U 2.1 U 0.51 U 18 U 1.7 U 13 U 0.42 U 0.93 U 27 U 53 U
SW8290 19408-74-3 123789-HxCDD NE pg/L 0.9 U 1.3 U 0.89 U 50 U 3.7 U 35 1 U 0.94 U 35 U 53 U
SW8290 560851-34-5 2,3,4,6,7,8-HxCDF NE pg/L 0.83 U 1 U 0.98 U 48 U 2.2 U 34 U 0.65 U 0.71 U 37 U 53 U
SW8290 557117-31-4 2,3,4,7,8-PeCDF NE pg/L 0.61 U 0.79 U 0.45 U 14 U 1.4 U 16 0.3 U 0.94 U 24 U 53 U
SW8290 1746-01-6 2378-TCDD 0.2 pg/L 1.4 U 1.6 U 1.1 U 28 U 4.4 U 11 U 0.86 U 1.9 U 35 U 11 U
SW8290 51207-31-9 2378-TCDF NE pg/L 0.96 U 1.4 U 0.71 U 19 U 2.4 U 42 0.54 U 0.86 U 26 U 27
SW8290 3268-87-9 OCDD NE pg/L 5.7 U 7.4 U 83 J 1100 160 J 110 U 24 J 8.8 U 1600 110 U
SW8290 39001-02-0 OCDF NE pg/L 2.9 U 5.8 U 2.9 U 310 U 9.6 U 130 U 2.9 U 5.2 U 140 U 110 U
Cas No.
NE
U
J
pg/L
Bold = Detected
= Chemical Abstracts Service number
= Not established
= Not detected, shown with reporting limit
= Estimated value
= picograms per liter
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April
Page 20 of 29
Table 5-5
Dioxins and Furans in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8290 567562-39-4 1,2,3,4,6,7,8-HpCDF NE pg/L
SW8290 555673-89-7 1,2,3,4,7,8,9-HpCDF NE pg/L
SW8290 570648-26-9 1,2,3,4,7,8-HxCDF NE pg/L
SW8290 557653-85-7 1,2,3,6,7,8-HxCDD NE pg/L
SW8290 557117-44-9 1,2,3,6,7,8-HxCDF NE pg/L
SW8290 572918-21-9 1,2,3,7,8,9-HxCDF NE pg/L
SW8290 557117-41-6 1,2,3,7,8-PeCDF NE pg/L
SW8290 35822-46-9 1234678-HpCDD NE pg/L
SW8290 39227-28-6 123478-HxCDD NE pg/L
SW8290 40321-76-4 12378-PeCDD NE pg/L
SW8290 19408-74-3 123789-HxCDD NE pg/L
SW8290 560851-34-5 2,3,4,6,7,8-HxCDF NE pg/L
SW8290 557117-31-4 2,3,4,7,8-PeCDF NE pg/L
SW8290 1746-01-6 2378-TCDD 0.2 pg/L
SW8290 51207-31-9 2378-TCDF NE pg/L
SW8290 3268-87-9 OCDD NE pg/L
SW8290 39001-02-0 OCDF NE pg/L
Cas No.
NE
U
J
pg/L
Bold = Detected
= Chemical Abstracts Service number
= Not established
= Not detected, shown with reporting limit
= Estimated value
= picograms per liter
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April
PZ09 PZ11 PZ12 PZ13 PZ14 PZ14 PZ17 PZ17 PZ18 PZ20
PZ09WG-092123 PZ11WG-091423 PZ12WG-091423 PZ13WG-091523 PZ14HG-091423 PZ14WG-091423 PZ17 HG- 091323 PZ17 WG- 091323 PZ18WG-091823 PZ20WG-091923
09/21/2023 09/14/2023 09/14/2023 09/15/2023 09/14/2023 09/14/2023 09/13/2023 09/13/2023 09/18/2023 09/19/2023
Normal Normal Normal Normal Field Duplicate Normal Field Duplicate Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
53 U 74 U 110 J 1.8 U 1.3 U 1.7 U 1.4 U 1.1 U 2.5 U 7.3 U
53 U 120 U 68 U 2.7 U 2.1 U 2.7 U 3.1 U 2.2 U 4.7 U 10 U
53 U 41 U 32 U 0.68 U 1.1 U 0.73 U 0.61 U 0.72 U 1.2 U 2.9 U
53 U 41 U 26 U 0.97 U 0.8 U 0.74 U 0.57 U 0.64 U 0.93 U 4.5 U
53 U 42 U 31 U 0.75 J 1.1 U 0.74 U 0.39 U 0.46 U 0.92 U 2.9 U
53 U 66 U 49 U 0.91 U 1.5 U 1 U 0.55 U 0.57 U 1.1 U 3.5 U
53 U 23 U 20 U 1.2 U 0.72 U 0.66 U 0.55 U 0.49 U 0.5 U 1.5 U
53 U 38 U 4200 1.4 U 0.87 U 1.6 U 1.9 U 0.97 U 1.8 U 7.5 U
53 U 57 U 35 U 1.2 U 0.93 U 0.9 U 0.63 U 0.68 U 1 U 5.6 U
53 U 21 U 23 U 1.2 U 0.95 U 0.69 U 0.45 U 0.3 U 0.63 U 2.5 U
53 U 46 U 29 U 1 U 0.83 U 0.78 U 0.58 U 0.65 U 0.94 U 4.8 U
53 U 45 U 32 U 0.66 U 1 U 0.68 U 0.37 U 0.43 U 0.8 U 3 U
53 U 16 U 15 U 0.83 U 0.5 U 0.48 U 0.38 U 0.34 U 0.35 U 0.95 U
11 U 21 U 21 U 2 U 1.7 U 1.1 U 0.48 U 0.68 U 3 U 3.1 U
11 U 15 U 21 U 1.1 U 1 U 0.69 U 0.53 U 0.55 U 0.61 U 4.1 J
110 U 1100 39000 4.2 U 6.1 U 3.5 U 20 J 25 J 5.5 U 25 U
110 U 230 U 160 U 3.7 U 3.3 U 3.4 U 3.6 U 2.3 U 4.9 U 23 J+
Page 21 of 29
Table 5-5
Dioxins and Furans in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW8290 567562-39-4 1,2,3,4,6,7,8-HpCDF NE pg/L
SW8290 555673-89-7 1,2,3,4,7,8,9-HpCDF NE pg/L
SW8290 570648-26-9 1,2,3,4,7,8-HxCDF NE pg/L
SW8290 557653-85-7 1,2,3,6,7,8-HxCDD NE pg/L
SW8290 557117-44-9 1,2,3,6,7,8-HxCDF NE pg/L
SW8290 572918-21-9 1,2,3,7,8,9-HxCDF NE pg/L
SW8290 557117-41-6 1,2,3,7,8-PeCDF NE pg/L
SW8290 35822-46-9 1234678-HpCDD NE pg/L
SW8290 39227-28-6 123478-HxCDD NE pg/L
SW8290 40321-76-4 12378-PeCDD NE pg/L
SW8290 19408-74-3 123789-HxCDD NE pg/L
SW8290 560851-34-5 2,3,4,6,7,8-HxCDF NE pg/L
SW8290 557117-31-4 2,3,4,7,8-PeCDF NE pg/L
SW8290 1746-01-6 2378-TCDD 0.2 pg/L
SW8290 51207-31-9 2378-TCDF NE pg/L
SW8290 3268-87-9 OCDD NE pg/L
SW8290 39001-02-0 OCDF NE pg/L
Bold = Detected
= Chemical Abstracts Service number
= Not established
= Not detected, shown with reporting limit
= Estimated value
= picograms per liter
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April
PZ21 RW01 RW02 RW03 RW04 RW06 RW07
PZ21WG-091923 RW01WG-091923 RW02W6-091223 RW03W6-091223 RW04 WG- 091323 RW06 WG- 091323 RW07 WG- 091323
09/19/2023 09/19/2023 09/12/2023 09/12/2023 09/13/2023 09/13/2023 09/13/2023
Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
2.9 3.1 U 8.7 U 2.5 U 1.7 U 0.87 U 1.2 U
4.2 U 4.5 U 17 U 6.1 U 3.3 U 1.9 U 2.2 U
1.7 U 0.69 U 5.5 U 1.8 U 1.6 U 2 U 0.8 U
1.4 U 1.9 U 3.6 U 3.2 U 2 U 0.7 U 0.54 U
1.6 U 0.69 U 3.5 U 1.5 U 0.97 U 0.72 U 0.47 U
1.9 U 0.8 U 4.8 U 1.7 U 1.2 U 0.58 U 0.64 U
2.1 U 1.4 U 4.4 U 1.3 U 0.93 U 0.59 U 0.6 U
3.9 U 4.1 U 10 U 2.5 U 1.7 U 0.99 U 1.3 U
1.9 U 2.1 U 4 U 3.5 U 2.4 U 0.71 U 0.61 U
2 U 2.1 U 4.1 U 1 U 0.9 U 0.61 U 0.62 U
1.6 U 1.9 U 3.7 U 3.3 U 2.1 U 0.69 U 0.56 U
1.6 U 0.64 U 3.3 U 1.2 U 0.89 U 0.65 U 0.44 U
1.5 U 1 U 3 U 0.88 U 0.7 U 0.55 U 0.43 U
2.2 U 2.3 U 3.2 U 2 U 1.8 U 0.62 U 0.77 U
1.2 U 1.2 U 3.4 U 1.4 U 1.1 U 0.44 U 0.59 U
7.2 U 8.7 U 780 7.9 U 140 25 J 28 J
18 J 9.2 J+14 U 4 U 3.7 U 1.7 U 2.5 U
Page 22 of 29
Table 5-6
Anions in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
BR01 BR03 PZ01 PZ02 PZ03 PZ04 PZ05 PZ06 PZ07 PZ08
BR01WG-091423 BR03WG-091423 PZ01 WG- 091323 PZ02WG-091423 PZ03 WG- 091323 PZ04WG-091923 PZ05 WG- 091323 PZ06WG-091423 PZ07WG-091523 PZ08WG-092123
09/14/2023 09/14/2023 09/13/2023 09/14/2023 09/13/2023 09/19/2023 09/13/2023 09/14/2023 09/15/2023 09/21/2023
Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
Method CAS No.Analyte NC 02L GWQS Units
SW9056 16887-00-6 Chloride 250 mg/L 15900 8910 282 1360 28.8 4960 70.3 J-150 206 NA
SW9056 14808-79-8 Sulfate 250 mg/L 540 500 165 89.8 178 824 146 19.8 20.1 NA
E300 16887-00-6 Chloride 250 mg/L NA NA NA NA NA NA NA NA NA 2670
E300 14808-79-8 Sulfate 250 mg/L NA NA NA NA NA NA NA NA NA 175
Notes:
Cas No.
J
J-
mg/L
NC 02L GWQS
Bold
Highlighted = Exceeds the NC 02L GWQS
= Chemical Abstracts Service number
= Estimated value
= Estimated value, bias low
= milligrams per liter
= Title 15A, North Carolina Administrative Code, Chapter 02,
2022
Page 23 of 29
Table 5-6
Anions in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW9056 16887-00-6 Chloride 250 mg/L
SW9056 14808-79-8 Sulfate 250 mg/L
E300 16887-00-6 Chloride 250 mg/L
E300 14808-79-8 Sulfate 250 mg/L
Bold
Highlighted = Exceeds the NC 02L GWQS
= Chemical Abstracts Service number
= Estimated value
= Estimated value, bias low
= milligrams per liter
= Title 15A, North Carolina Administrative Code, Chapter 02,
2022
PZ09 PZ11 PZ12 PZ13 PZ14 PZ14 PZ17 PZ17 PZ18 PZ20
PZ09WG-092123 PZ11WG-091423 PZ12WG-091423 PZ13WG-091523 PZ14WG-091423 PZ14HG-091423 PZ17 WG- 091323 PZ17 HG- 091323 PZ18WG-091823 PZ20WG-091923
09/21/2023 09/14/2023 09/14/2023 09/15/2023 09/14/2023 09/14/2023 09/13/2023 09/13/2023 09/18/2023 09/19/2023
Normal Normal Normal Normal Normal Field Duplicate Normal Field Duplicate Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
NA 201 1530 12.2 29.3 29.3 52.9 52.3 94.1 16.4
NA 9.5 J 630 138 14.3 14.2 66.4 66.3 23.8 19.3
147 NA NA NA NA NA NA NA NA NA
26.1 NA NA NA NA NA NA NA NA NA
Page 24 of 29
Table 5-6
Anions in Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SW9056 16887-00-6 Chloride 250 mg/L
SW9056 14808-79-8 Sulfate 250 mg/L
E300 16887-00-6 Chloride 250 mg/L
E300 14808-79-8 Sulfate 250 mg/L
Cas No.
J
J-
mg/L
NC 02L GWQS
Bold
Highlighted
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02,
2022
PZ21 RW01 RW02 RW03 RW04 RW06 RW07
PZ21WG-091923 RW01WG-091923 RW02W6-091223 RW03W6-091223 RW04 WG- 091323 RW06 WG- 091323
09/19/2023 09/19/2023 09/12/2023 09/12/2023 09/13/2023 09/13/2023 09/13/2023
Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
93.2 48 56.7 50.6 48.7 24.2 57.7
100 41.8 203 490 432 83.7 148
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
Page 25 of 29
Figure 5-7
Additional Analytes and General Chemistry of Site Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
BR01 BR03 PZ01 PZ02 PZ03 PZ04 PZ04 PZ04
BR01WG-091423 BR03WG-091423 PZ01 WG- 091323 PZ02WG-091423 PZ03 WG- 091323 DUP01WG-062323 DUP01WG-062323 PZ04WG-091923
09/14/2023 09/14/2023 09/13/2023 09/14/2023 09/13/2023 06/23/2023 06/23/2023 09/19/2023
Normal Normal Normal Normal Normal Field Duplicate Field Duplicate Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
Method CAS No.Analyte NC 02L GWQS Units
SM 5210 B 9999900-03-8 Biochemical Oxygen Demand (5-day)NE mg/L NA NA NA 66 J-NA NA NA 76.8
SM 5220 D 9999900-04-0 Chemical Oxygen Demand NE mg/L NA NA NA 1590 NA NA NA 1030
SM 5310B 7440-44-0 Carbon (Total)NE mg/L NA NA NA 504 NA NA NA 144
E351.2 7727-37-9 Total Kjeldahl Nitrogen NE mg/L NA NA 56.9 NA NA NA NA 7.4
E353.2 14797-55-8 Nitrate (as N)10 mg/L NA NA 0.5 UJ NA NA NA NA 0.04 U
1664B 9999000-89-5 Oil and Grease, Gravimetric NE mg/L NA NA 32.4 NA NA NA NA 5 U
SM 2320B 471-34-1 Alkalinity (as CaCO3)NE mg/L 768 81 813 5860 947 5450 4940 4180
SM 2540C 9999900-07-2 Total Dissolved Solids (TDS)NE mg/L NA NA NA 9880 NA NA NA 16200
SM 2540D TSS Total Suspended Solids NE mg/L NA NA NA 12.6 NA NA NA 12.3
SM 4500 S 18496-25-8 Sulfide NE mg/L 0.1 U 0.24 J-0.22 19.3 1.2 13 J 51 J 33
E300 16984-48-8 Fluoride 2 mg/L NA NA NA NA NA NA NA NA
E300 24959-67-9 Bromide NE mg/L NA NA NA NA NA NA NA NA
SW8015 9999000-93-1 Diesel Range Organics NE mg/L NA NA NA 5.1 UJ NA NA NA 4.2 UJ
SW8015 9999001-01-1 Gasoline Range Organics (C6-C12)NE mg/L NA NA NA 0.39 NA NA NA 0.41
RSK175 74-84-0 Ethane NE mg/L NA NA NA NA NA NA NA 0.013 U
RSK175 74-85-1 Ethene NE mg/L NA NA NA NA NA NA NA 0.013 U
RSK175 74-82-8 Methane NE mg/L NA NA NA NA NA NA NA 0.721
RSK175 74-98-6 Propane NE mg/L NA NA NA NA NA NA NA 0.0186 U
Cas No.
NA
NE
U
J
UJ
J-
mg/L
NC 02L GWQS
Bold
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
= Detected
= Chemical Abstracts Service number
= Not detected, shown with reporting limit
= Not detected and estimated, shown with reporting limit
Page 26 of 29
Figure 5-7
Additional Analytes and General Chemistry of Site Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SM 5210 B 9999900-03-8 Biochemical Oxygen Demand (5-day)NE mg/L
SM 5220 D 9999900-04-0 Chemical Oxygen Demand NE mg/L
SM 5310B 7440-44-0 Carbon (Total)NE mg/L
E351.2 7727-37-9 Total Kjeldahl Nitrogen NE mg/L
E353.2 14797-55-8 Nitrate (as N)10 mg/L
1664B 9999000-89-5 Oil and Grease, Gravimetric NE mg/L
SM 2320B 471-34-1 Alkalinity (as CaCO3)NE mg/L
SM 2540C 9999900-07-2 Total Dissolved Solids (TDS)NE mg/L
SM 2540D TSS Total Suspended Solids NE mg/L
SM 4500 S 18496-25-8 Sulfide NE mg/L
E300 16984-48-8 Fluoride 2 mg/L
E300 24959-67-9 Bromide NE mg/L
SW8015 9999000-93-1 Diesel Range Organics NE mg/L
SW8015 9999001-01-1 Gasoline Range Organics (C6-C12)NE mg/L
RSK175 74-84-0 Ethane NE mg/L
RSK175 74-85-1 Ethene NE mg/L
RSK175 74-82-8 Methane NE mg/L
RSK175 74-98-6 Propane NE mg/L
Cas No.
NA
NE
U
J
UJ
J-
mg/L
NC 02L GWQS
Bold
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
= Detected
= Chemical Abstracts Service number
= Not detected, shown with reporting limit
= Not detected and estimated, shown with reporting limit
PZ05 PZ06 PZ07 PZ08 PZ09 PZ11 PZ12 PZ13
PZ05 WG- 091323 PZ06WG-091423 PZ07WG-091523 PZ08WG-092123 PZ09WG-092123 PZ11WG-091423 PZ12WG-091423 PZ13WG-091523
09/13/2023 09/14/2023 09/15/2023 09/21/2023 09/21/2023 09/14/2023 09/14/2023 09/15/2023
Normal Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
NA NA 27 J-NA NA NA NA NA
NA NA 2160 NA NA NA NA NA
NA NA 436 NA NA NA NA NA
NA NA 97.8 NA NA NA NA NA
NA NA 0.5 U NA NA NA NA NA
NA NA 4.7 J NA NA NA NA NA
85.1 104 3220 1550 40.8 1460 3000 108
NA NA 5810 NA NA NA NA NA
NA NA 4.6 NA NA NA NA NA
0.1 U 0.032 J 0.08 J 5.2 0.1 U 0.31 0.3 0.1 U
NA NA NA 0.14 0.05 J NA NA NA
NA NA NA 0.35 0.16 NA NA NA
NA NA 5.4 U NA NA NA NA NA
NA NA 0.08 U NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
Page 27 of 29
Figure 5-7
Additional Analytes and General Chemistry of Site Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SM 5210 B 9999900-03-8 Biochemical Oxygen Demand (5-day)NE mg/L
SM 5220 D 9999900-04-0 Chemical Oxygen Demand NE mg/L
SM 5310B 7440-44-0 Carbon (Total)NE mg/L
E351.2 7727-37-9 Total Kjeldahl Nitrogen NE mg/L
E353.2 14797-55-8 Nitrate (as N)10 mg/L
1664B 9999000-89-5 Oil and Grease, Gravimetric NE mg/L
SM 2320B 471-34-1 Alkalinity (as CaCO3)NE mg/L
SM 2540C 9999900-07-2 Total Dissolved Solids (TDS)NE mg/L
SM 2540D TSS Total Suspended Solids NE mg/L
SM 4500 S 18496-25-8 Sulfide NE mg/L
E300 16984-48-8 Fluoride 2 mg/L
E300 24959-67-9 Bromide NE mg/L
SW8015 9999000-93-1 Diesel Range Organics NE mg/L
SW8015 9999001-01-1 Gasoline Range Organics (C6-C12)NE mg/L
RSK175 74-84-0 Ethane NE mg/L
RSK175 74-85-1 Ethene NE mg/L
RSK175 74-82-8 Methane NE mg/L
RSK175 74-98-6 Propane NE mg/L
Cas No.
NA
NE
U
J
UJ
J-
mg/L
NC 02L GWQS
Bold
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
= Detected
= Chemical Abstracts Service number
= Not detected, shown with reporting limit
= Not detected and estimated, shown with reporting limit
PZ14 PZ14 PZ17 PZ17 PZ18 PZ20 PZ21 PZ21
PZ14WG-091423 PZ14HG-091423 PZ17 WG- 091323 PZ17 HG- 091323 PZ18WG-091823 PZ20WG-091923 PZ21WG-062223 PZ21WG-091923
09/14/2023 09/14/2023 09/13/2023 09/13/2023 09/18/2023 09/19/2023 06/22/2023 09/19/2023
Normal Field Duplicate Normal Field Duplicate Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
242 236 108 97.1 8.2 633 129 115
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
0.81 0.74 0.1 U 0.1 U 0.1 U 11.5 0.1 U 0.1 U
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
Page 28 of 29
Figure 5-7
Additional Analytes and General Chemistry of Site Groundwater
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS Units
SM 5210 B 9999900-03-8 Biochemical Oxygen Demand (5-day)NE mg/L
SM 5220 D 9999900-04-0 Chemical Oxygen Demand NE mg/L
SM 5310B 7440-44-0 Carbon (Total)NE mg/L
E351.2 7727-37-9 Total Kjeldahl Nitrogen NE mg/L
E353.2 14797-55-8 Nitrate (as N)10 mg/L
1664B 9999000-89-5 Oil and Grease, Gravimetric NE mg/L
SM 2320B 471-34-1 Alkalinity (as CaCO3)NE mg/L
SM 2540C 9999900-07-2 Total Dissolved Solids (TDS)NE mg/L
SM 2540D TSS Total Suspended Solids NE mg/L
SM 4500 S 18496-25-8 Sulfide NE mg/L
E300 16984-48-8 Fluoride 2 mg/L
E300 24959-67-9 Bromide NE mg/L
SW8015 9999000-93-1 Diesel Range Organics NE mg/L
SW8015 9999001-01-1 Gasoline Range Organics (C6-C12)NE mg/L
RSK175 74-84-0 Ethane NE mg/L
RSK175 74-85-1 Ethene NE mg/L
RSK175 74-82-8 Methane NE mg/L
RSK175 74-98-6 Propane NE mg/L
Cas No.
NA
NE
U
J
UJ
J-
mg/L
NC 02L GWQS
Bold
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
= Detected
= Chemical Abstracts Service number
= Not detected, shown with reporting limit
= Not detected and estimated, shown with reporting limit
RW01 RW02 RW03 RW04 RW05 RW06 RW07
RW01WG-091923 RW02W6-091223 RW03W6-091223 RW04 WG- 091323 RW5WG-062323 RW06 WG- 091323 RW07 WG- 091323
09/19/2023 09/12/2023 09/12/2023 09/13/2023 06/23/2023 09/13/2023 09/13/2023
Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
370 1050 604 2000 25300 398 198
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
0.1 U 0.1 U 0.1 U 41.5 39.8 0.074 J 0.1 U
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
Page 29 of 29
Table 6-1
pH and Color in Surface Water and Seeps
Pactiv Evergreen Canton Mill
Canton, North Carolina
CBOF CBOF CBUS SW01-00 SW01-02 SW01-05 SW01-10 SW02
CBOF-10022023 CBOF-10022023 DUP CBUS-10022023 SW01-00-WS-092023 SW01-02-WS-092023 SW01-05-WS-092023 SW01-10-WS-092023 SW02-WS-092023
10/02/2023 10/02/2023 10/02/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023
Normal Field Duplicate Normal Normal Normal Normal Normal Normal
Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water
Method CAS No.Analyte NC 02L GWQS NC 02B SWQS Units Camp Branch Camp Branch Camp Branch Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River
SM 2120B COLOR Color, True 15 NE color unit 5 10 10 5 J 5 J 5 J 10 J 5 J
SM 2120B 9999900-09-4 pH 6.5 - 8.5 6.0 - 9.0 SU NA NA NA 6.7 J 6.6 J 6.6 J 6.4 J 6.6 J
SW9040 9999900-09-4 pH 6.5 - 8.5 6.0 - 9.0 SU 7.7 J 7.6 J 7.3 J NA NA NA NA NA
Cas No. = Chemical Abstracts Service number
NE = Not established
NA = Not analyzed
J = Estimated value
SU
NC 02L GWQS
NC 02B SWQS
Bold
Highlighted = Exceeds the NC 02L GWQS (Seep) or the NC 02B SWQS (Surface Water)
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Detected
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section
.0202, Groundwater Quality Standards, April 2022
Page 1 of 8
Table 6-1
pH and Color in Surface Water and Seeps
Pactiv Evergreen Canton Mill
Canton, North Carolina
Method CAS No.Analyte NC 02L GWQS NC 02B SWQS Units
SM 2120B COLOR Color, True 15 NE color unit
SM 2120B 9999900-09-4 pH 6.5 - 8.5 6.0 - 9.0 SU
SW9040 9999900-09-4 pH 6.5 - 8.5 6.0 - 9.0 SU
Cas No. = Chemical Abstracts Service number
NE = Not established
NA = Not analyzed
J = Estimated value
SU
NC 02L GWQS
NC 02B SWQS
Bold
Highlighted = Exceeds the NC 02L GWQS (Seep) or the NC 02B SWQS (Surface Water)
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Detected
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section
.0202, Groundwater Quality Standards, April 2022
SWDOWN SWDOWN SWUP SEEP01 SEEP02
SWDOWNWS-092023 SWDOWNH-092023 SWUP-WS-092023 SEEP01-WG-092023 SEEP02WG-092023
09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023
Normal Field Duplicate Normal Normal Normal
Surface Water Surface Water Surface Water Groundwater Groundwater
Pigeon River Pigeon River Pigeon River Seep Seep
10 J 10 J 5 J 250 J 200 J
6.8 J 6.7 J 6.6 J 10.2 J 9.3 J
NA NA NA NA NA
Page 2 of 8
Table 6-2Metals in Surface Water and SeepsPactiv Evergreen Canton MillCanton, North Carolina
CBOF CBOF CBUS SW01-00 SW01-02 SW01-05 SW01-10
CBOF-10022023 CBOF-10022023 DUP CBUS-10022023 SW01-00-WS-092023 SW01-02-WS-092023 SW01-05-WS-092023 SW01-10-WS-092023
10/02/2023 10/02/2023 10/02/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023
Normal Field Duplicate Normal Normal Normal Normal Normal
Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water
Method CAS No.Analyte NC 02L GWQS NC 02B SWQS Units Camp Branch Camp Branch Camp Branch Pigeon River Pigeon River Pigeon River Pigeon River
E200.7 7429-90-5 Aluminum NE NE µg/L NA NA NA 79.1 J 75.2 J 65.1 J 82 JE200.7 7440-38-2 Arsenic 10 NE µg/L NA NA NA 10 U 10 U 10 U 10 U
E200.7 7440-39-3 Barium 700 NE µg/L NA NA NA 14.7 14.6 14.7 15.1
E200.7 7440-41-7 Beryllium 4 NE µg/L NA NA NA 4 U 4 U 4 U 4 UE200.7 7440-42-8 Boron 700 NE µg/L 12.9 J 12.8 J 50 U 50 U 50 U 50 U 50 U
E200.7 7440-43-9 Cadmium 2 NE µg/L NA NA NA 1 U 1 U 1 U 1 U
E200.7 7440-70-2 Calcium NE NE µg/L 13500 13200 10100 2440 2440 2450 2440E200.7 7440-47-3 Chromium 10 NE µg/L NA NA NA 5 U 5 U 5 U 5 U
E200.7 7440-48-4 Cobalt 1 NE µg/L NA NA NA 10 U 10 U 10 U 10 U
E200.7 7440-50-8 Copper 1000 NE µg/L NA NA NA 5 U 5 U 5 U 5 UE200.7 7439-89-6 Iron 300 NE µg/L 151 149 225 285 297 262 289
E200.7 7439-92-1 Lead 15 NE µg/L NA NA NA 10 U 10 U 10 U 10 U
E200.7 7439-95-4 Magnesium NE NE µg/L 4350 4280 4080 751 748 751 759E200.7 7439-96-5 Manganese 50 NE µg/L NA NA NA 19 18.4 17.9 19.1
E200.7 7439-98-7 Molybdenum NE NE µg/L NA NA NA 10 U 10 U 10 U 10 U
E200.7 7440-02-0 Nickel 100 NE µg/L NA NA NA 5 U 5 U 5 U 5 UE200.7 7782-49-2 Selenium 20 NE µg/L NA NA NA 15 U 15 U 15 U 15 U
E200.7 7440-22-4 Silver 20 NE µg/L NA NA NA 5 U 5 U 5 U 5 U
E200.7 7440-23-5 Sodium NE NE µg/L 24300 24000 10900 2100 1940 J 2260 1900 JE200.7 7440-28-0 Thallium 2 NE µg/L NA NA NA 15 U 15 U 15 U 15 U
E200.7 7440-66-6 Zinc 1000 NE µg/L NA NA NA 20 U 20 U 20 U 20 U
E200.7 7429-90-5 Aluminum (Dissolved)NE NE µg/L NA NA NA 100 U 100 U 100 U 100 U
E200.7 7440-38-2 Arsenic (Dissolved)10 150 µg/L NA NA NA 10 U 10 U 10 U 10 U
E200.7 7440-39-3 Barium (Dissolved)700 NE µg/L NA NA NA 15.2 14.8 15.1 15.2
E200.7 7440-41-7 Beryllium (Dissolved)4 6.5 µg/L NA NA NA 4 U 4 U 4 U 4 U
E200.7 7440-42-8 Boron (Dissolved)700 NE µg/L 16.6 J 14.9 J 50 U 50 U 50 U 50 U 50 UE200.7 7440-43-9 Cadmium (Dissolved)2 NE µg/L NA NA NA 1 U 1 U 1 U 1 U
E200.7 7440-70-2 Calcium (Dissolved)NE NE µg/L 14200 14200 11000 2440 2440 2450 2420
E200.7 7440-47-3 Chromium (Dissolved)10 24 µg/L NA NA NA 5 U 5 U 5 U 5 UE200.7 7440-48-4 Cobalt (Dissolved)1 NE µg/L NA NA NA 10 U 10 U 10 U 10 U
E200.7 7440-50-8 Copper (Dissolved)1000 2.7 µg/L NA NA NA 5 U 5 U 5 U 5 U
E200.7 7439-89-6 Iron (Dissolved)300 NE µg/L 160 163 195 124 127 130 145E200.7 7439-92-1 Lead (Dissolved)15 0.54 µg/L NA NA NA 10 U 10 U 10 U 10 U
E200.7 7439-95-4 Magnesium (Dissolved)NE NE µg/L 4350 4340 4150 791 783 787 780
E200.7 7439-96-5 Manganese (Dissolved)50 NE µg/L NA NA NA 14.3 14.9 14.9 15.5E200.7 7439-98-7 Molybdenum (Dissolved)NE NE µg/L NA NA NA 10 U 10 U 10 U 10 U
E200.7 7440-02-0 Nickel (Dissolved)100 16 µg/L NA NA NA 5 U 1.7 J 5 U 5 U
E200.7 7782-49-2 Selenium (Dissolved)20 NE µg/L NA NA NA 15 U 15 U 15 U 15 UE200.7 7440-22-4 Silver (Dissolved)20 0.06 µg/L NA NA NA 5 U 5 U 5 U 5 U
E200.7 7440-23-5 Sodium (Dissolved)NE NE µg/L 21900 21900 9710 2420 2560 2520 2250
E200.7 7440-28-0 Thallium (Dissolved)2 NE µg/L NA NA NA 15 U 15 U 15 U 15 UE200.7 7440-66-6 Zinc (Dissolved)1000 36 µg/L NA NA NA 20 U 20 U 20 U 20 U
E245.1 7439-97-6 Mercury 1 0.012 µg/L 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U
E245.1 7439-97-6 Mercury (Dissolved)1 NE µg/L 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 UE200.8 7429-90-5 Aluminum NE NE µg/L 41.6 34.7 111 NA NA NA NA
E200.8 7440-38-2 Arsenic 10 NE µg/L 1 U 1 U 1 U NA NA NA NA
E200.8 7440-39-3 Barium 700 NE µg/L 53.5 52.6 53.1 NA NA NA NA
E200.8 7440-41-7 Beryllium 4 NE µg/L 0.1 U 0.1 U 0.1 U NA NA NA NA
E200.8 7440-43-9 Cadmium 2 NE µg/L 0.1 U 0.1 U 0.1 U NA NA NA NA
E200.8 7440-47-3 Chromium 10 NE µg/L 1 U 1 U 1 U NA NA NA NA
E200.8 7440-48-4 Cobalt 1 NE µg/L 1 U 1 U 1 U NA NA NA NAE200.8 7440-50-8 Copper 1000 NE µg/L 1 1.4 1.1 NA NA NA NA
E200.8 7439-92-1 Lead 15 NE µg/L 2.4 2.4 0.58 J NA NA NA NA
E200.8 7439-96-5 Manganese 50 NE µg/L 18 17.2 13.2 NA NA NA NAE200.8 7439-98-7 Molybdenum NE NE µg/L 1 U 1 U 1 U NA NA NA NA
E200.8 7440-02-0 Nickel 100 NE µg/L 0.5 J 0.45 J 0.5 J NA NA NA NA
E200.8 7782-49-2 Selenium 20 NE µg/L 0.29 J 0.26 J 2 U NA NA NA NAE200.8 7440-22-4 Silver 20 NE µg/L 0.5 U 0.5 U 0.5 U NA NA NA NA
E200.8 7440-28-0 Thallium 2 NE µg/L 1 U 1 U 1 U NA NA NA NA
E200.8 7440-66-6 Zinc 1000 NE µg/L 10 U 10 U 10 U NA NA NA NAE200.8 7429-90-5 Aluminum (Dissolved)NE NE µg/L 34.9 38.9 101 NA NA NA NA
E200.8 7440-38-2 Arsenic (Dissolved)10 150 µg/L 1 U 1 U 1 U NA NA NA NA
E200.8 7440-39-3 Barium (Dissolved)700 NE µg/L 50.9 50.2 51 NA NA NA NAE200.8 7440-41-7 Beryllium (Dissolved)4 NE µg/L 0.1 U 0.1 U 0.1 U NA NA NA NA
E200.8 7440-43-9 Cadmium (Dissolved)2 0.25 µg/L 0.1 U 0.1 U 0.1 U NA NA NA NA
E200.8 7440-47-3 Chromium (Dissolved)10 24 µg/L 1 U 1 U 1 U NA NA NA NAE200.8 7440-48-4 Cobalt (Dissolved)1 NE µg/L 1 U 1 U 1 U NA NA NA NA
E200.8 7440-50-8 Copper (Dissolved)1000 2.7 µg/L 1.4 1.4 1.3 NA NA NA NA
E200.8 7439-92-1 Lead (Dissolved)15 0.54 µg/L 2.2 2.2 0.49 J NA NA NA NAE200.8 7439-96-5 Manganese (Dissolved)50 NE µg/L 16.8 17 11.1 NA NA NA NA
E200.8 7439-98-7 Molybdenum (Dissolved)NE NE µg/L 1 U 1 U 1 U NA NA NA NA
E200.8 7440-02-0 Nickel (Dissolved)100 16 µg/L 0.41 J 0.35 J 1 U NA NA NA NA
E200.8 7782-49-2 Selenium (Dissolved)20 NE µg/L 0.2 J 2 U 2 U NA NA NA NA
E200.8 7440-22-4 Silver (Dissolved)20 0.06 µg/L 0.5 U 0.5 U 0.5 U NA NA NA NA
E200.8 7440-28-0 Thallium (Dissolved)2 NE µg/L 1 U 1 U 1 U NA NA NA NA
E200.8 7440-66-6 Zinc (Dissolved)1000 36 µg/L 10 U 10 U 7.2 J NA NA NA NA
Cas No. = Chemical Abstracts Service numberNE = Not established
NA = Not analyzed
UJ = Estimated value
µg/L
Bold
Highlighted = Exceeds the NC 02L GWQS (Seep) or the NC 02B SWQS (Surface Water)
= Detected
Sample Location:
Sample ID:Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section
Page 3 of 8
Table 6-2Metals in Surface Water and SeepsPactiv Evergreen Canton MillCanton, North Carolina
Method CAS No.Analyte NC 02L GWQS NC 02B SWQS Units
E200.7 7429-90-5 Aluminum NE NE µg/LE200.7 7440-38-2 Arsenic 10 NE µg/L
E200.7 7440-39-3 Barium 700 NE µg/L
E200.7 7440-41-7 Beryllium 4 NE µg/LE200.7 7440-42-8 Boron 700 NE µg/L
E200.7 7440-43-9 Cadmium 2 NE µg/L
E200.7 7440-70-2 Calcium NE NE µg/LE200.7 7440-47-3 Chromium 10 NE µg/L
E200.7 7440-48-4 Cobalt 1 NE µg/L
E200.7 7440-50-8 Copper 1000 NE µg/LE200.7 7439-89-6 Iron 300 NE µg/L
E200.7 7439-92-1 Lead 15 NE µg/L
E200.7 7439-95-4 Magnesium NE NE µg/LE200.7 7439-96-5 Manganese 50 NE µg/L
E200.7 7439-98-7 Molybdenum NE NE µg/L
E200.7 7440-02-0 Nickel 100 NE µg/LE200.7 7782-49-2 Selenium 20 NE µg/L
E200.7 7440-22-4 Silver 20 NE µg/L
E200.7 7440-23-5 Sodium NE NE µg/LE200.7 7440-28-0 Thallium 2 NE µg/L
E200.7 7440-66-6 Zinc 1000 NE µg/L
E200.7 7429-90-5 Aluminum (Dissolved)NE NE µg/L
E200.7 7440-38-2 Arsenic (Dissolved)10 150 µg/L
E200.7 7440-39-3 Barium (Dissolved)700 NE µg/L
E200.7 7440-41-7 Beryllium (Dissolved)4 6.5 µg/L
E200.7 7440-42-8 Boron (Dissolved)700 NE µg/LE200.7 7440-43-9 Cadmium (Dissolved)2 NE µg/L
E200.7 7440-70-2 Calcium (Dissolved)NE NE µg/L
E200.7 7440-47-3 Chromium (Dissolved)10 24 µg/LE200.7 7440-48-4 Cobalt (Dissolved)1 NE µg/L
E200.7 7440-50-8 Copper (Dissolved)1000 2.7 µg/L
E200.7 7439-89-6 Iron (Dissolved)300 NE µg/LE200.7 7439-92-1 Lead (Dissolved)15 0.54 µg/L
E200.7 7439-95-4 Magnesium (Dissolved)NE NE µg/L
E200.7 7439-96-5 Manganese (Dissolved)50 NE µg/LE200.7 7439-98-7 Molybdenum (Dissolved)NE NE µg/L
E200.7 7440-02-0 Nickel (Dissolved)100 16 µg/L
E200.7 7782-49-2 Selenium (Dissolved)20 NE µg/LE200.7 7440-22-4 Silver (Dissolved)20 0.06 µg/L
E200.7 7440-23-5 Sodium (Dissolved)NE NE µg/L
E200.7 7440-28-0 Thallium (Dissolved)2 NE µg/LE200.7 7440-66-6 Zinc (Dissolved)1000 36 µg/L
E245.1 7439-97-6 Mercury 1 0.012 µg/L
E245.1 7439-97-6 Mercury (Dissolved)1 NE µg/LE200.8 7429-90-5 Aluminum NE NE µg/L
E200.8 7440-38-2 Arsenic 10 NE µg/L
E200.8 7440-39-3 Barium 700 NE µg/L
E200.8 7440-41-7 Beryllium 4 NE µg/L
E200.8 7440-43-9 Cadmium 2 NE µg/L
E200.8 7440-47-3 Chromium 10 NE µg/L
E200.8 7440-48-4 Cobalt 1 NE µg/LE200.8 7440-50-8 Copper 1000 NE µg/L
E200.8 7439-92-1 Lead 15 NE µg/L
E200.8 7439-96-5 Manganese 50 NE µg/LE200.8 7439-98-7 Molybdenum NE NE µg/L
E200.8 7440-02-0 Nickel 100 NE µg/L
E200.8 7782-49-2 Selenium 20 NE µg/LE200.8 7440-22-4 Silver 20 NE µg/L
E200.8 7440-28-0 Thallium 2 NE µg/L
E200.8 7440-66-6 Zinc 1000 NE µg/LE200.8 7429-90-5 Aluminum (Dissolved)NE NE µg/L
E200.8 7440-38-2 Arsenic (Dissolved)10 150 µg/L
E200.8 7440-39-3 Barium (Dissolved)700 NE µg/LE200.8 7440-41-7 Beryllium (Dissolved)4 NE µg/L
E200.8 7440-43-9 Cadmium (Dissolved)2 0.25 µg/L
E200.8 7440-47-3 Chromium (Dissolved)10 24 µg/LE200.8 7440-48-4 Cobalt (Dissolved)1 NE µg/L
E200.8 7440-50-8 Copper (Dissolved)1000 2.7 µg/L
E200.8 7439-92-1 Lead (Dissolved)15 0.54 µg/LE200.8 7439-96-5 Manganese (Dissolved)50 NE µg/L
E200.8 7439-98-7 Molybdenum (Dissolved)NE NE µg/L
E200.8 7440-02-0 Nickel (Dissolved)100 16 µg/L
E200.8 7782-49-2 Selenium (Dissolved)20 NE µg/L
E200.8 7440-22-4 Silver (Dissolved)20 0.06 µg/L
E200.8 7440-28-0 Thallium (Dissolved)2 NE µg/L
E200.8 7440-66-6 Zinc (Dissolved)1000 36 µg/L
= Chemical Abstracts Service number = Not established
= Not analyzed
= Estimated value
Bold
Highlighted = Exceeds the NC 02L GWQS (Seep) or the NC 02B SWQS (Surface Water)
= Detected
Sample Location:
Sample ID:Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section
SW02-WS-092023 SWDOWNWS-092023 SWDOWNH-092023 SWUP-WS-092023 SEEP01-WG-092023 SEEP02WG-092023
09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023
Normal Normal Field Duplicate Normal Normal Normal
Surface Water Surface Water Surface Water Surface Water Groundwater Groundwater
Pigeon River Pigeon River Pigeon River Pigeon River Seep Seep67 J 68.9 J 75.7 J 84.5 J 1070 86610 U 10 U 10 U 10 U 10 U 10 U
14.2 15.3 15.1 14.4 75.6 30.1
4 U 4 U 4 U 4 U 4 U 4 U50 U 50 U 50 U 50 U 192 13.5 J
1 U 1 U 1 U 1 U 0.43 J 1 U
2400 3300 3240 2400 10700 45105 U 5 U 5 U 5 U 18.5 2.1 J
10 U 10 U 10 U 10 U 2.4 J 10 U
5 U 5 U 5 U 5 U 8.2 5.325125727629223901300
10 U 10 U 10 U 10 U 10 U 10 U
746 852 840 766 1210 96516.5 28.4 28.1 18.1 207 126
10 U 10 U 10 U 10 U 11.1 2.8 J
5 U 5 U 1.4 J 5 U 7 3.1 J15 U 15 U 15 U 15 U 15 U 15 U
5 U 5 U 5 U 5 U 5 U 5 U
1840 J 5080 4930 2140 485000 7900015 U 15 U 15 U 15 U 15 U 15 U
20 U 20 U 20 U 20 U 75.2 13.3 J
100 U 100 U 100 U 100 U 396 363
10 U 10 U 10 U 10 U 10 U 10 U
14.8 15.7 15.7 15 44.6 16
4 U 4 U 4 U 4 U 4 U 4 U
50 U 12.7 J 50 U 50 U 143 20.5 J1 U 1 U 1 U 1 U 1 U 1 U
2370 3210 3250 2380 7320 4060
5 U 5 U 5 U 5 U 13.7 5 U10 U 10 U 10 U 10 U 1.5 J 10 U
5 U 5 U 5 U 5 U 3.7 J 4.2 J
126 110 104 136 1160 32510 U 10 U 10 U 10 U 10 U 10 U
782 873 878 793 910 804
13.6 25.4 25.7 15.9 114 46.210 U 10 U 10 U 10 U 7.9 J 4 J
5 U 5 U 5 U 5 U 5.9 3.5 J
15 U 15 U 15 U 15 U 15 U 15 U5 U 5 U 5 U 5 U 5 U 5 U
2140 5900 5900 2020 372000 81400
15 U 15 U 15 U 15 U 15 U 15 U20 U 20 U 20 U 20 U 50.7 20 U
0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U
0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 UNANANANANANA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NANANANANANANA
NA NA NA NA NA NA
NA NA NA NA NA NANANANANANANA
NA NA NA NA NA NA
NA NA NA NA NA NANANANANANANA
NA NA NA NA NA NA
NA NA NA NA NA NANANANANANANA
NA NA NA NA NA NA
NA NA NA NA NA NANANANANANANA
NA NA NA NA NA NA
NA NA NA NA NA NANANANANANANA
NA NA NA NA NA NA
NA NA NA NA NA NANANANANANANA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
Page 4 of 8
Table 6-3VOCs in Surface Water and SeepsPactiv Evergreen Canton MillCanton, North Carolina
CBOF CBOF CBUS SW01-00 SW01-02 SW01-05 SW01-10 SW02 SWDOWN SWDOWN SWUP SEEP01 SEEP02
CBOF-10022023 CBOF-10022023 DUP CBUS-10022023 SW01-00-WS-092023 SW01-02-WS-092023 SW01-05-WS-092023 SW01-10-WS-092023 SW02-WS-092023 SWDOWNWS-092023 SWDOWNH-092023 SWUP-WS-092023 SEEP01-WG-092023 SEEP02WG-092023
10/02/2023 10/02/2023 10/02/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023
Normal Field Duplicate Normal Normal Normal Normal Normal Normal Normal Field Duplicate Normal Normal NormalSurface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Groundwater GroundwaterMethodCAS No.Analyte NC 02L GWQS NC 02B SWQS Units Camp Branch Camp Branch Camp Branch Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Seep Seep
SW8260 71-55-6 1,1,1-Trichloroethane 200 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826079-34-5 0.2 4 µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826076-13-1 200000 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826079-00-5 1,1,2-Trichloroethane 0.6 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 75-34-3 1,1-Dichloroethane 6 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 75-35-4 1,1-Dichloroethene 350 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW8260120-82-1 70 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826096-12-8 0.04 NE µg/L 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 USW8260106-93-4 0.02 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 95-50-1 1,2-Dichlorobenzene 20 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 107-06-2 1,2-Dichloroethane 0.4 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826078-87-5 1,2-Dichloropropane 0.6 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW8260541-73-1 1,3-Dichlorobenzene 200 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 106-46-7 1,4-Dichlorobenzene 6 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 78-93-3 2-Butanone (MEK)4000 NE µg/L 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U
SW8260 591-78-6 2-Hexanone 40 NE µg/L 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 USW8260108-10-1 100 NE µg/L 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 USW826067-64-1 Acetone 6000 NE µg/L 25 U 25 U 5.6 J 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 USW826071-43-2 Benzene 1 51 µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 75-27-4 0.6 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 75-25-2 Bromoform 4 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826074-83-9 Bromomethane 10 NE µg/L 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 USW826075-15-0 Carbon disulfide 700 NE µg/L 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 1.8 J 2 USW826056-23-5 Carbon tetrachloride 0.3 1.6 µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 108-90-7 Chlorobenzene 50 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 75-00-3 Chloroethane 3000 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826067-66-3 Chloroform 70 NE µg/L 0.62 J 0.63 J 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826074-87-3 Chloromethane 3 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW8260156-59-2 cis-1,2-Dichloroethene 70 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 10061-01-5 NE NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 110-82-7 Cyclohexane NE NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW8260124-48-1 0.4 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826075-71-8 1000 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW8260100-41-4 Ethylbenzene 600 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 0.9 J 1 U
SW8260 98-82-8 Isopropylbenzene 70 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 179601-23-1 m,p-Xylene NE NE µg/L 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2.2 2 USW826079-20-9 Methyl acetate NE NE µg/L 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 USW82601634-04-4 20 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW8260108-87-2 Methylcyclohexane NE NE µg/L 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U
SW8260 75-09-2 Methylene chloride 5 NE µg/L 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U
SW8260 95-47-6 o-Xylene NE NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 0.98 J 1 USW8260100-42-5 Styrene 70 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW8260127-18-4 Tetrachloroethene 0.7 3.3 µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 108-88-3 Toluene 600 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 156-60-5 100 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
SW8260 10061-02-6 NE NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826079-01-6 Trichloroethene 3 30 µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826075-69-4 2000 NE µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 USW826075-01-4 Vinyl chloride 0.03 2.4 µg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
= Chemical Abstracts Service number = Not established
= Estimated value
Bold = Detected
= micrograms per liter
= Not detected, shown with reporting limit
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
= Title 15A, North Carolina Administrative Code, Subchapter 02B, Section .0211, Surface Water Quality
Page 5 of 8
Table 6-4SVOCs in Surface Water and SeepsPactiv Evergreen Canton MillCanton, North Carolina
CBOF CBOF CBUS SW01-00 SW01-02 SW01-05 SW01-10 SW02 SWDOWN SWDOWN SWUP SEEP01 SEEP02CBOF-10022023 CBOF-10022023 DUP CBUS-10022023 SW01-00-WS-092023 SW01-02-WS-092023 SW01-05-WS-092023 SW01-10-WS-092023 SW02-WS-092023 SWDOWNWS-092023 SWDOWNH-092023 SWUP-WS-092023 SEEP01-WG-092023 SEEP02WG-092023
10/02/2023 10/02/2023 10/02/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023
Normal Field Duplicate Normal Normal Normal Normal Normal Normal Normal Field Duplicate Normal Normal Normal
Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Groundwater Groundwater
Method CAS No.Analyte NC 02L GWQS NC 02B SWQS Units Camp Branch Camp Branch Camp Branch Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Seep Seep
SW8270 108-60-1 2,2-Oxybis(1-chloropropane)NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 95-95-4 2,4,5-Trichlorophenol 63 NE µg/L 8.3 U 8.3 U 8.3 U 10 UJ 8.3 U 10 U 8.7 UJ 8.7 U 8.3 U 8.3 UJ 8.3 UJ 10 U 10 U
SW8270 88-06-2 2,4,6-Trichlorophenol 4 NE µg/L 8.3 U 8.3 U 8.3 U 10 UJ 8.3 U 10 U 8.7 UJ 8.7 U 8.3 U 8.3 UJ 8.3 UJ 10 U 10 U
SW8270 120-83-2 2,4-Dichlorophenol 0.98 NE µg/L 8.3 U 8.3 U 8.3 U 10 UJ 8.3 U 10 U 8.7 UJ 8.7 U 8.3 U 8.3 UJ 8.3 UJ 10 U 10 USW8270105-67-9 2,4-Dimethylphenol 100 NE µg/L 8.3 U 8.3 U 8.3 U 10 UJ 8.3 U 10 U 8.7 UJ 8.7 U 8.3 U 8.3 UJ 8.3 UJ 10 U 10 USW827051-28-5 2,4-Dinitrophenol NE NE µg/L 41.7 U 41.7 U 41.7 U 50 UJ 41.7 U 50 U 43.5 UJ 43.5 U 41.7 U 41.7 UJ 41.7 UJ 50 U 50 USW8270121-14-2 2,4-Dinitrotoluene 0.05 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW8270606-20-2 2,6-Dinitrotoluene 0.05 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW827091-58-7 2-Chloronaphthalene NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 95-57-8 2-Chlorophenol 0.4 NE µg/L 8.3 U 8.3 U 8.3 U 10 UJ 8.3 U 10 U 8.7 UJ 8.7 U 8.3 U 8.3 UJ 8.3 UJ 10 U 10 U
SW8270 534-52-1 2-Methyl-4,6-Dinitrophenol NE NE µg/L 16.7 U 16.7 U 16.7 U 20 U 16.7 U 20 U 17.4 U 17.4 U 16.7 U 16.7 U 16.7 U 20 U 20 U
SW8270 91-57-6 2-Methylnaphthalene 30 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 95-48-7 2-Methylphenol (o-Cresol)400 NE µg/L 8.3 U 8.3 U 8.3 U 10 UJ 8.3 U 10 U 8.7 UJ 8.7 U 8.3 U 8.3 UJ 8.3 UJ 10 U 10 U
SW8270 88-74-4 2-Nitroaniline NE NE µg/L 16.7 U 16.7 U 16.7 U 20 U 16.7 U 20 U 17.4 U 17.4 U 16.7 U 16.7 U 16.7 U 20 U 20 U
SW8270 88-75-5 2-Nitrophenol NE NE µg/L 8.3 U 8.3 U 8.3 U 10 UJ 8.3 U 10 U 8.7 UJ 8.7 U 8.3 U 8.3 UJ 8.3 UJ 10 U 10 U
SW8270 91-94-1 3,3'-Dichlorobenzidine NE NE µg/L 16.7 U 16.7 U 16.7 U 20 U 16.7 U 20 U 17.4 U 17.4 U 16.7 U 16.7 U 16.7 U 20 U 20 U
SW8270 9999900-32-2 3-Methylphenol/4-Methylphenol NE NE µg/L 8.3 U 8.3 U 8.3 U 10 UJ 8.3 U 10 U 8.7 UJ 8.7 U 8.3 U 8.3 UJ 8.3 UJ 10 U 10 U
SW8270 99-09-2 3-Nitroaniline NE NE µg/L 16.7 U 16.7 U 16.7 U 20 U 16.7 U 20 U 17.4 U 17.4 U 16.7 U 16.7 U 16.7 U 20 U 20 U
SW8270 101-55-3 4-Bromophenyl-phenylether NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 59-50-7 4-Chloro-3-methylphenol NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 106-47-8 4-Chloroaniline NE NE µg/L 16.7 U 16.7 U 16.7 U 20 U 16.7 U 20 U 17.4 U 17.4 U 16.7 U 16.7 U 16.7 UJ 20 U 20 U
SW8270 7005-72-3 4-Chlorophenylphenyl ether NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 100-01-6 4-Nitroaniline NE NE µg/L 16.7 U 16.7 U 16.7 U 20 U 16.7 U 20 U 17.4 U 17.4 U 16.7 U 16.7 U 16.7 U 20 U 20 U
SW8270 100-02-7 4-Nitrophenol NE NE µg/L 41.7 U 41.7 U 41.7 U 50 U 41.7 U 50 U 43.5 U 43.5 U 41.7 U 41.7 U 41.7 U 50 U 50 U
SW8270 83-32-9 Acenaphthene 80 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 208-96-8 Acenaphthylene 200 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 98-86-2 Acetophenone 700 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 120-12-7 Anthracene 2000 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 1912-24-9 Atrazine 3 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 100-52-7 Benzaldehyde NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW827056-55-3 Benzo(a)anthracene 0.05 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW827050-32-8 Benzo(a)pyrene 0.005 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW8270205-99-2 Benzo(b)fluoranthene 0.05 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW8270191-24-2 Benzo(g,h,i)perylene 200 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 207-08-9 Benzo(k)fluoranthene 0.5 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 92-52-4 Biphenyl 400 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 111-91-1 bis(2-Chloroethoxy)methane NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 111-44-4 bis(2-Chloroethyl)ether 0.03 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 117-81-7 bis(2-Ethylhexyl)phthalate 3 NE µg/L 5 U 5 U 5 U 6 U 5 U 6 U 5.2 U 5.2 U 5 U 5 U 5 U 6 U 6 U
SW8270 85-68-7 Butylbenzylphthalate 1000 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 105-60-2 Caprolactam 4000 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 86-74-8 Carbazole NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 218-01-9 Chrysene 5 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 84-74-2 Di-n-butylphthalate 700 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 117-84-0 Di-n-octylphthalate 100 NE µg/L 8.3 U 8.3 U 8.3 U v1 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 53-70-3 Dibenz(a,h)anthracene 0.005 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 132-64-9 Dibenzofuran NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 84-66-2 Diethylphthalate 6000 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 131-11-3 Dimethylphthalate NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 206-44-0 Fluoranthene 300 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 86-73-7 Fluorene 300 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 118-74-1 Hexachlorobenzene 0.02 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 87-68-3 Hexachlorobutadiene 0.4 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 77-47-4 Hexachlorocyclopentadiene NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW827067-72-1 Hexachloroethane NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW8270193-39-5 Indeno(1,2,3-cd)pyrene 0.05 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW827078-59-1 Isophorone 40 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW8270621-64-7 N-Nitroso-di-n-propylamine NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 USW827086-30-6 N-Nitrosodiphenylamine NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 91-20-3 Naphthalene 6 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 98-95-3 Nitrobenzene NE NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 87-86-5 Pentachlorophenol 0.3 NE µg/L 16.7 U 16.7 U 16.7 U 20 UJ 16.7 U 20 U 17.4 UJ 17.4 U 16.7 U 16.7 UJ 16.7 UJ 20 U 20 U
SW8270 85-01-8 Phenanthrene 200 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 8.3 U 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
SW8270 108-95-2 Phenol 30 NE µg/L 8.3 U 8.3 U 8.3 U 10 UJ 8.3 U 10 U 8.7 UJ 8.7 U 8.3 U 8.3 UJ 8.3 UJ 10 U 10 U
SW8270 129-00-0 Pyrene 200 NE µg/L 8.3 U 8.3 U 8.3 U 10 U 2.4 J 10 U 8.7 U 8.7 U 8.3 U 8.3 U 8.3 U 10 U 10 U
Cas No. = Chemical Abstracts Service number
NE = Not established
U
J = Estimated value
UJ = Not detected and estimated, shown with reporting limit
µg/L
NC 02B SWQS
Bold = Detected
= micrograms per liter
= Not detected, shown with reporting limit
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
Page 6 of 8
Table 6-5Anions in Surface Water and SeepsPactive Evergreen Canton MillCanton, North Carolina
SW01-00 SW01-02 SW01-05 SW01-10 SW02 SWDOWN SWDOWN SWUP SEEP01 SEEP02
SW01-00-WS-092023 SW01-02-WS-092023 SW01-05-WS-092023 SW01-10-WS-092023 SW02-WS-092023 SWDOWNWS-092023 SWDOWNH-092023 SWUP-WS-092023 SEEP01-WG-092023 SEEP02WG-092023
09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023
Normal Normal Normal Normal Normal Normal Field Duplicate Normal Normal Normal
Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water
Method CAS No.Analyte NC 02L GWQS NC 02B SWQS Units Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Seep Seep
E300 16887-00-6 Chloride 250000 230 mg/L 1.2 1.2 1.2 1.2 1.2 3.3 3.4 1.2 23.4 34.1
E300 14808-79-8 Sulfate 250000 NE mg/L 1.6 1.6 1.8 1.5 1.5 3 3 1.4 223 13.6
Notes:
Cas No. = Chemical Abstracts Service number
= Not analyzed
= Not established
= Estimated value
Bold = Detected
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater Quality Standards, April 2022
Page 7 of 8
Table 6-6General Chemistry and Sulfur in Surface Water and SeepsPactiv Evergreen Canton MillCanton, North Carolina
CBOF CBOF CBUS SW01-00 SW01-02 SW01-05 SW01-10 SW02 SWDOWN SWDOWN SWUP SEEP01 SEEP02
CBOF-10022023 CBOF-10022023 DUP CBUS-10022023 SW01-00-WS-092023 SW01-02-WS-092023 SW01-05-WS-092023 SW01-10-WS-092023 SW02-WS-092023 SWDOWNWS-092023 SWDOWNH-092023 SWUP-WS-092023 SEEP01-WG-092023 SEEP02WG-09202310/02/2023 10/02/2023 10/02/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023 09/20/2023
Normal Field Duplicate Normal Normal Normal Normal Normal Normal Normal Field Duplicate Normal Normal NormalSurface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water Surface Water
Method CAS No.Analyte NC 02L GWQS NC 02B SWQS Units Camp Branch Camp Branch Camp Branch Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Pigeon River Seep SeepE350.1 7664-41-7 Ammonia (as N)NE NE mg/L NA NA NA 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.031 J 0.1 U 0.33 0.04 J
E351.2 7727-37-9 Nitrogen NE NE mg/L NA NA NA 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 2 0.83E420.4 9999000-85-1 Phenolics, Total Recoverable NE NE mg/L NA NA NA 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.011 J 0.02 U
SM 2320B 471-34-1 Alkalinity (as CaCO3)NE NE mg/L NA NA NA 11.5 10.4 10.9 10.2 10.9 37.1 J-15.1 J-10.1 503 115
SM 2540C 9999900-07-2 Total Dissolved Solids (TDS)500 NE mg/L NA NA NA 25 U 25 U 25 U 25 U 25 U 35 40 25 U 1210 235SM 5220 D 9999900-04-0 Chemical Oxygen Demand NE NE mg/L NA NA NA 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 146 32.1
SM4500-P 9999000-80-6 orthophosphate NE NE mg/L NA NA NA 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.029 J 0.021 J 0.05 UJ 0.95 1.6ASTM D4239-05 63705-05-5 Sulfur NE NE %w/w 0.0535 0.051 0.0508 NA NA NA NA NA NA NA NA NA NA
= Chemical Abstracts Service number = Not analyzed
= Not established
= Estimated value
Bold
= Title 15A, North Carolina Administrative Code, Chapter 02, Subchapter L, Section .0202, Groundwater
= Title 15A, North Carolina Administrative Code, Subchapter 02B, Section .0211, Surface Water Quality Standards, September 2022
Sample Location:Sample ID:
Sample Date:Sample Type:
Matrix:
Page 8 of 8

Appendix A
Photo Log and Fieldwork Documentation
Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 1 DESCRIPTION: PZ-1 is in satisfactory condition. CONEX box has been removed
PHOTO NO. 2
DESCRIPTION: PZ-2 (foreground) is in satisfactory condition
Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 3 DESCRIPTION: PZ-3 is in satisfactory condition
PHOTO NO. 4 DESCRIPTION: PZ-4 is in satisfactory condition
Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 5 DESCRIPTION: PZ-5 is a 4-inch diameter well and is in satisfactory condition
PHOTO NO. 6 DESCRIPTION: Recommend constructing a flush mount vault and pad at PZ-6. Replacement/Updated well tag
Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 7 DESCRIPTION: PZ-7 is in satisfactory condition
PHOTO NO. 8 DESCRIPTION: PZ-8 is in satisfactory condition
Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 9 DESCRIPTION: PZ-9 is in satisfactory condition
PHOTO NO. 10
DESCRIPTION:

Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 11 DESCRIPTION: Recommend constructing a flush mount vault and pad at PZ-12. Replacement/Updated well tag
PHOTO NO. 12
DESCRIPTION: PZ-13 is in satisfactory condition
Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 13 DESCRIPTION: PZ-14R is in the distance (between bollards) and is paired with BR-1 in the foreground
PHOTO NO. 14
DESCRIPTION:
Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 15 DESCRIPTION: Prior to abandonment of PZ-16 - residual product was removed from the well via vac-truck and PVC stinger.

PHOTO NO. 16
DESCRIPTION:
PZ-16 was abandoned by a North Carolina licensed driller. Once excavations are complete a
replacement well will be installed in this location.

Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 17 DESCRIPTION: Recommend constructing a flush mount vault and pad at PZ-17. Replacement/Updated well tag and new bollards are also recommended

PHOTO NO. 18
DESCRIPTION: PZ-18 is in satisfactory condition.

Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 19 DESCRIPTION: PZ-20 is in satisfactory condition. Field observations of well location are not consistent with Well Location Maps from other contractors.

PHOTO NO. 20
DESCRIPTION: PZ-21 is in satisfactory condition and serves as an upgradient background well.

Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina

PHOTO NO. 21 DESCRIPTION:
PHOTO NO. 22 DESCRIPTION:
Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina

PHOTO NO. 23 DESCRIPTION: BR-3 (center-left) is paired with PZ-2 (foreground out of frame). BR-3 is in satisfactory condition.
PHOTO NO. 24 DESCRIPTION: Airlifting at RW-1. Recommend securing the casing within the vault.
Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina

PHOTO NO. 25 DESCRIPTION: RW-2 is in satisfactory condition.
PHOTO NO. 26 DESCRIPTION: RW-3 is in satisfactory condition.

Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina

PHOTO NO. 27 DESCRIPTION: RW-4 is in satisfactory condition.
PHOTO NO. 28 DESCRIPTION: RW-5 is in satisfactory condition.

Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 29 DESCRIPTION: RW-6 is in satisfactory condition.
PHOTO NO. 30
DESCRIPTION: Well maintenance at RW-6. A stainless-steel bladder pump was recovered from RW-6.

Appendix A - Photo Log Well Inspection Survey Pactiv Evergreen Canton Mill Canton, North Carolina

PHOTO NO. 31 DESCRIPTION: RW-7 is in satisfactory condition.
PHOTO NO. 32 DESCRIPTION: Example of coarse material removed from recovery wells 1 through 6.

Appendix A — Photo Log Well Maintenance Program Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 1 DESCRIPTION: RWs were redeveloped via surge block and rehabilitated by hydro jetting. Image above depicts surging at RW-1.

PHOTO NO. 2
DESCRIPTION:
After surging and hydro jetting liberated material and sediment were removed by air-lifting
techniques.
Appendix A — Photo Log Well Maintenance Program Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 3 DESCRIPTION: Compressed air is pumped into the well & tremie pipe via the clear tubing
PHOTO NO. 4 DESCRIPTION:
Appendix A — Photo Log Well Maintenance Program Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 5 DESCRIPTION: A sieve was used to collect samples of material liberated from RWs 1-6.
PHOTO NO. 6 DESCRIPTION: Example of material collected from RW-2
Appendix A — Photo Log Well Maintenance Program Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 7 DESCRIPTION: Overview of well rehabilitation process at RW-2
PHOTO NO. 8 DESCRIPTION: View from Cip Bridge of RW-6 maintenance
Appendix A — Photo Log Well Maintenance Program Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 9 DESCRIPTION: Bladder pump recovered from RW-6
PHOTO NO. 10
DESCRIPTION: Coarse grained sediment recovered from RW-5

Appendix A — Photo Log Well Maintenance Program Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 11 DESCRIPTION: Maintenance of shallow 2-inch MWs consisted of scrubbing surging and pumping
PHOTO NO. 12
DESCRIPTION: A “tornado” pump was used to remove fine sediments from the shallow MWs
Appendix A — Photo Log Well Maintenance Program Pactiv Evergreen Canton Mill Canton, North Carolina
PHOTO NO. 13 DESCRIPTION: Purge water from shallow wells was containerized
PHOTO NO. 14
DESCRIPTION: Wood chips were removed during surging at PZ-7 - above

Well Redevelopment Summary Table
Well ID
Screen Total Depth*
BR-01 70-100 100.3-(99.1) Surge Block, Reamed, & Pumping – very slow recharge
BR-02 93-103 103.5-(102.8)Surge Block, Reamed, & Pumping – negligible recharge
PZ-01 7.5-22.5 22.6-(22.4) Surge Block, Reamed, & Pumping – slow to moderate recharge
PZ-03 8-23 23.5-(22.4) Surge Block, Reamed, & Pumping – good recharge
PZ-04 9-24 23.4-(23.1) Surge Block, Reamed, & Pumping – slow recharge
PZ-05** 9-19 19.9-(18.8) Surge Block, Reamed, & Pumping – moderate recharge
PZ-06 17-27 29.5-(28.3) Surge Block, Reamed, & Pumping – good recharge
PZ-07 11-26 25.9-(24.8) Surge Block, Reamed, & Pumping – slow recharge
PZ-08 8.5-23.8 23.3-(23.1) Surge Block, Reamed, & Pumping – moderate recharge
PZ-09 10-25 24.8-(23.4) Surge Block, Reamed, & Pumping – moderate recharge
PZ-11 9-24 18.9-(18.1) Surge Block, Reamed, & Pumping – good recharge
PZ-12 9-24 25.2-(23.3) Surge Block, Reamed, & Pumping – good recharge
PZ-13 8.5-23.5 23.9-(23.6) Surge Block, Reamed, & Pumping – moderate recharge
PZ-14R 10-20 19.6-(19.1) Surge Block, Reamed, & Pumping – slow recharge
PZ-16 6-21 NA Abandoned 9/01/2023
PZ-17 4-19 18.7-(18.7) Surge Block, Reamed, & Pumping – good recharge
PZ-18 4.8-19.8 19.4-(19.1) Surge Block, Reamed, & Pumping – good recharge
PZ-20 UNK 19.6-(19.3) Surge Block, Reamed, & Pumping – good recharge
PZ-21 UNK 14.8-(14.8) Surge Block, Reamed, & Pumping – moderate recharge
RW-01** 20-40 36.5-(33.3) Surge Block, Hydro Jet, Reamed, & Air Lifting – slow recharge
RW-02** 9-49 47.9-(44.4)
RW-03** 9-49 47.0-(43.5) Surge Block, Hydro Jet, Reamed, & Air Lifting – moderate recharge
RW-05** 9-49 45.9-(40.3) Surge Block, Hydro Jet, Reamed, & Air Lifting – moderate recharge
RW-06** 10.5-30.5 28.2-(27.6) Surge Block, Hydro Jet, Reamed, & Air Lifting – moderate recharge
RW-07** 10-40 36.8-(36.2) Surge Block, Reamed, & Pumping – good recharge
ID = Identification
ft = feet
bgs = below ground surface
N/A = not applicable
UNK = Unknown ** = denotes 4 inch diameter well
Appendix B
Field Sampling Logs
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:Sampled with HDPE Dipper
Time (hh:mm):17:00
pH (units):8.32
Conductivity (mS/cm):26
Turbidity (NTU):NM
DO* (mg/L):12.6
ORP (mV):-0.3
Depth of Water (ft):2.5
*DO Range = 0 to 14.6 mg/L, max of 8.6 mg/L at 25°C
Sample Data MS/MSD Collected Bailer Pump Description:
SW-UP
COMMENTS:Sample collected at Park Street Bridge Upstream of Mill from river thalweg
Page ____ of ____
SURFACE WATER SAMPLING LOG
DATE: 9-20-23 JOB NUMBER:0888834350.03.03.003
IN-SITU TESTING
µm)
9/20/2023 17:00
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:Sampled with HDPE Dipper
Time (hh:mm):13:05
pH (units):9.24
Conductivity (mS/cm):128
Turbidity (NTU):NM
DO* (mg/L):8.1
ORP (mV):-38.7
Depth of Water (ft):0.75
*DO Range = 0 to 14.6 mg/L, max of 8.6 mg/L at 25°C
Sample Data MS/MSD Collected Bailer Pump Description:
SW-Down
COMMENTS:Sample collected at Hwy 215 bridge downstream of Mill from river thalweg
PFAS sample split with NCDEQ
Page ____ of ____
SURFACE WATER SAMPLING LOG
DATE: 9-20-23 JOB NUMBER:0888834350.03.03.003
IN-SITU TESTING
µm)
9/20/2023 13:05 Y
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:Sampled with large syringe
Time (hh:mm):14:15
pH (units):9.68
Conductivity (mS/cm):485
Turbidity (NTU):10.3
DO* (mg/L):12.8
ORP (mV):-35.3
Depth of Water (ft):0.5
*DO Range = 0 to 14.6 mg/L, max of 8.6 mg/L at 25°C
Sample Data MS/MSD Collected Bailer Pump Description:
Seep-02
COMMENTS:Sample collected from visible seep in standing pool
Page ____ of ____
SURFACE WATER SAMPLING LOG
DATE: 9-20-23 JOB NUMBER:0888834350.03.03.003
IN-SITU TESTING
µm)
9/20/2023 14:15
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:Sampled with HDPE Dipper
Time (hh:mm):14:35
pH (units):7.42
Conductivity (mS/cm):27
Turbidity (NTU):2.6
DO* (mg/L):9.65
ORP (mV):29.9
Depth of Water (ft):0.25
*DO Range = 0 to 14.6 mg/L, max of 8.6 mg/L at 25°C
Sample Data MS/MSD Collected Bailer Pump Description:
SW-01
COMMENTS:Sample collected at river bank
Page ____ of ____
SURFACE WATER SAMPLING LOG
DATE: 9-20-23 JOB NUMBER:0888834350.03.03.003
IN-SITU TESTING
µm)
9/20/2023 14:35
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:Sampled with HDPE Dipper
Time (hh:mm):14:50
pH (units):6.01
Conductivity (mS/cm):29
Turbidity (NTU):1.54
DO* (mg/L):9.3
ORP (mV):36.2
Depth of Water (ft):0.25
*DO Range = 0 to 14.6 mg/L, max of 8.6 mg/L at 25°C
Sample Data MS/MSD Collected Bailer Pump Description:
SW-01-2
COMMENTS:Collected 2ft from bank
Page ____ of ____
SURFACE WATER SAMPLING LOG
DATE: 9-20-23 JOB NUMBER:0888834350.03.03.003
IN-SITU TESTING
µm)
9/20/2023 14:50
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:Sampled with HDPE Dipper
Time (hh:mm):15:10
pH (units):6.97
Conductivity (mS/cm):28
Turbidity (NTU):1.57
DO* (mg/L):9.62
ORP (mV):40.3
Depth of Water (ft):0.5
*DO Range = 0 to 14.6 mg/L, max of 8.6 mg/L at 25°C
Sample Data MS/MSD Collected Bailer Pump Description:
SW-01-5
COMMENTS:Sample collected 5ft from bank
Page ____ of ____
SURFACE WATER SAMPLING LOG
DATE: 9-20-23 JOB NUMBER:0888834350.03.03.003
IN-SITU TESTING
µm)
9/20/2023 15:10
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:Sampled with HDPE Dipper
Time (hh:mm):15:20
pH (units):7.62
Conductivity (mS/cm):28
Turbidity (NTU):1.69
DO* (mg/L):9.99
ORP (mV):43.5
Depth of Water (ft):0.75
*DO Range = 0 to 14.6 mg/L, max of 8.6 mg/L at 25°C
Sample Data MS/MSD Collected Bailer Pump Description:
SW-01-10
COMMENTS:Sample collected 10ft from bank
Page ____ of ____
SURFACE WATER SAMPLING LOG
DATE: 9-20-23 JOB NUMBER:0888834350.03.03.003
IN-SITU TESTING
µm)
9/20/2023 15:20
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:Sampled with large syringe
Time (hh:mm):15:30
pH (units):10.38
Conductivity (mS/cm):2152
Turbidity (NTU):5.22
DO* (mg/L):8.4
ORP (mV):-269.6
Depth of Water (ft):0.75
*DO Range = 0 to 14.6 mg/L, max of 8.6 mg/L at 25°C
Sample Data MS/MSD Collected Bailer Pump Description:
Seep-01
COMMENTS:Sample collected from visible seep in standing pool
Page ____ of ____
SURFACE WATER SAMPLING LOG
DATE: 9-20-23 JOB NUMBER:0888834350.03.03.003
IN-SITU TESTING
µm)
9/20/2023 15:30
Circle one: DEVELOPMENT SAMPLING Bailer Pump Description:Sampled with HDPE Dipper
Time (hh:mm):15:50
pH (units):7.7
Conductivity (mS/cm):27
Turbidity (NTU):1.72
DO* (mg/L):11.41
ORP (mV):9.4
Depth of Water (ft):0.75
*DO Range = 0 to 14.6 mg/L, max of 8.6 mg/L at 25°C
Sample Data MS/MSD Collected Bailer Pump Description:
SW-02
COMMENTS:Sample collected from east bank near thalweg
Page ____ of ____
SURFACE WATER SAMPLING LOG
DATE: 9-20-23 JOB NUMBER:0888834350.03.03.003
IN-SITU TESTING
µm)
9/20/2023 15:50

Appendix C
Laboratory Analytical Reports
#=CL#
October 06, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92687719
92687719
Project:
Pace Project No.:
RE:
Christina AshdownENSAFE313 Wingo WayMount Pleasant, SC 29464
PACTIV EVERGREEN GROUNDWATER S
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on September 13, 2023. The results relate onlyto the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and thelaboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc: Jennings Kerr, ENSAFE Inc.
Lab, ENSAFE Inc.
David Warren, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 61
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 61
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Lab ID Sample ID Matrix Date Collected Date Received
92687719001 RW03W6-091223 Water 09/12/23 15:16 09/13/23 07:39
92687719002 RW02W6-091223 Water 09/12/23 14:50 09/13/23 07:39
92687719003 TRIP BLANK Water 09/12/23 12:00 09/13/23 07:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 61
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92687719001 RW03W6-091223 SM 2120B-2011 2 PASI-ELRB
EPA 6010D 16 PASI-ADBB1
EPA 6010D 16 PASI-ADBB1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CSAS
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92687719002 RW02W6-091223 SM 2120B-2011 2 PASI-ELRB
EPA 6010D 16 PASI-ADBB1
EPA 6010D 16 PASI-ADBB1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CSAS
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92687719003 TRIP BLANK EPA 8260D 52 PASI-CSAS
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW03W6-091223 Lab ID: 92687719001 Collected: 09/12/23 15:16 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.8 Std. Units 09/14/23 13:2325
True Color 875 units 09/14/23 13:23125 125 25
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 10/01/23 23:27 7440-36-009/27/23 13:1525.0 15.0 5
Arsenic ND ug/L 10/01/23 23:27 7440-38-209/27/23 13:1550.0 23.5 5
Barium 110 ug/L 10/01/23 23:27 7440-39-309/27/23 13:1525.0 17.4 5
Beryllium ND ug/L 10/01/23 23:27 7440-41-709/27/23 13:155.0 3.5 5
Boron ND ug/L 10/01/23 23:27 7440-42-809/27/23 13:15250 162 5
Cadmium ND ug/L 10/01/23 23:27 7440-43-909/27/23 13:155.0 2.0 5
Chromium ND ug/L 10/01/23 23:27 7440-47-309/27/23 13:1525.0 18.3 5
Cobalt ND ug/L 10/01/23 23:27 7440-48-409/27/23 13:1525.0 18.2 5
Copper ND ug/L 10/01/23 23:27 7440-50-809/27/23 13:1525.0 21.3 5
Lead ND ug/L 10/01/23 23:27 7439-92-109/27/23 13:1525.0 22.7 5
Nickel ND ug/L 10/01/23 23:27 7440-02-009/27/23 13:1525.0 17.3 5
Selenium ND ug/L 10/01/23 23:27 7782-49-209/27/23 13:1550.0 23.5 5
Silver ND ug/L 10/01/23 23:27 7440-22-409/27/23 13:1525.0 12.5 5
Thallium ND ug/L 10/01/23 23:27 7440-28-009/27/23 13:1550.0 40.7 5
Vanadium 97.7 ug/L 10/01/23 23:27 7440-62-209/27/23 13:1525.0 19.7 5
Zinc 82.0 ug/L 10/01/23 23:27 7440-66-609/27/23 13:1550.0 47.3 5
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/03/23 19:54 7440-36-009/27/23 20:305.0 3.0 1
Arsenic, Dissolved ND ug/L 10/03/23 19:54 7440-38-209/27/23 20:3010.0 4.7 1
Barium, Dissolved 88.8 ug/L 10/03/23 19:54 7440-39-309/27/23 20:305.0 3.5 1
Beryllium, Dissolved ND ug/L 10/03/23 19:54 7440-41-709/27/23 20:301.0 0.70 1
Boron, Dissolved 114 ug/L 10/03/23 19:54 7440-42-809/27/23 20:3050.0 32.4 1
Cadmium, Dissolved ND ug/L 10/03/23 19:54 7440-43-909/27/23 20:301.0 0.40 1
Chromium, Dissolved 4.2J ug/L 10/03/23 19:54 7440-47-309/27/23 20:305.0 3.7 1
Cobalt, Dissolved ND ug/L 10/03/23 19:54 7440-48-409/27/23 20:305.0 3.6 1
Copper, Dissolved ND ug/L 10/03/23 19:54 7440-50-809/27/23 20:305.0 4.3 1
Lead, Dissolved ND ug/L 10/03/23 19:54 7439-92-109/27/23 20:305.0 4.5 1
Nickel, Dissolved ND ug/L 10/03/23 19:54 7440-02-009/27/23 20:305.0 3.5 1
Selenium, Dissolved ND ug/L 10/03/23 19:54 7782-49-209/27/23 20:3010.0 4.7 1
Silver, Dissolved ND ug/L 10/03/23 19:54 7440-22-409/27/23 20:305.0 2.5 1
Thallium, Dissolved ND ug/L 10/03/23 19:54 7440-28-009/27/23 20:3010.0 8.1 1
Vanadium, Dissolved 57.7 ug/L 10/03/23 19:54 7440-62-209/27/23 20:305.0 3.9 1
Zinc, Dissolved 34.1 ug/L 10/03/23 19:54 7440-66-609/27/23 20:3010.0 9.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/04/23 09:37 7439-97-610/03/23 07:580.20 0.14 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW03W6-091223 Lab ID: 92687719001 Collected: 09/12/23 15:16 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/03/23 12:18 7439-97-610/02/23 15:100.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/18/23 15:10 83-32-909/15/23 16:548.3 1.7 1
Acenaphthylene ND ug/L 09/18/23 15:10 208-96-809/15/23 16:548.3 1.6 1
Acetophenone ND ug/L 09/18/23 15:10 98-86-209/15/23 16:548.3 1.2 1
Anthracene ND ug/L 09/18/23 15:10 120-12-709/15/23 16:548.3 1.9 1
Atrazine ND ug/L 09/18/23 15:10 1912-24-909/15/23 16:548.3 2.6 1
Benzaldehyde ND ug/L 09/18/23 15:10 100-52-709/15/23 16:548.3 3.0 1
Benzo(a)anthracene ND ug/L 09/18/23 15:10 56-55-309/15/23 16:548.3 2.2 1
Benzo(a)pyrene ND ug/L 09/18/23 15:10 50-32-809/15/23 16:548.3 2.3 1
Benzo(b)fluoranthene ND ug/L 09/18/23 15:10 205-99-209/15/23 16:548.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 09/18/23 15:10 191-24-209/15/23 16:548.3 2.4 1
Benzo(k)fluoranthene ND ug/L 09/18/23 15:10 207-08-909/15/23 16:548.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 09/18/23 15:10 92-52-409/15/23 16:548.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 09/18/23 15:10 101-55-309/15/23 16:548.3 1.5 1
Butylbenzylphthalate ND ug/L 09/18/23 15:10 85-68-709/15/23 16:548.3 2.6 1
Caprolactam ND ug/L 09/18/23 15:10 105-60-209/15/23 16:548.3 5.8 1
Carbazole ND ug/L 09/18/23 15:10 86-74-809/15/23 16:548.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/18/23 15:10 59-50-709/15/23 16:548.3 2.8 1
4-Chloroaniline ND ug/L 09/18/23 15:10 106-47-809/15/23 16:5416.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/18/23 15:10 111-91-109/15/23 16:548.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 09/18/23 15:10 111-44-409/15/23 16:548.3 1.6 1
2-Chloronaphthalene ND ug/L 09/18/23 15:10 91-58-709/15/23 16:548.3 1.4 1
2-Chlorophenol ND ug/L 09/18/23 15:10 95-57-809/15/23 16:548.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/18/23 15:10 7005-72-309/15/23 16:548.3 1.7 1
Chrysene ND ug/L 09/18/23 15:10 218-01-909/15/23 16:548.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 09/18/23 15:10 53-70-309/15/23 16:548.3 2.5 1
Dibenzofuran ND ug/L 09/18/23 15:10 132-64-909/15/23 16:548.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/18/23 15:10 91-94-109/15/23 16:5416.7 6.8 1
2,4-Dichlorophenol ND ug/L 09/18/23 15:10 120-83-209/15/23 16:548.3 1.2 1
Diethylphthalate ND ug/L 09/18/23 15:10 84-66-209/15/23 16:548.3 1.7 1
2,4-Dimethylphenol ND ug/L 09/18/23 15:10 105-67-909/15/23 16:548.3 1.4 1
Dimethylphthalate ND ug/L 09/18/23 15:10 131-11-309/15/23 16:548.3 1.8 1
Di-n-butylphthalate ND ug/L 09/18/23 15:10 84-74-209/15/23 16:548.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/18/23 15:10 534-52-109/15/23 16:5416.7 6.5 1
2,4-Dinitrophenol ND ug/L 09/18/23 15:10 51-28-509/15/23 16:5441.7 21.7 1
2,4-Dinitrotoluene ND ug/L 09/18/23 15:10 121-14-209/15/23 16:548.3 1.4 1
2,6-Dinitrotoluene ND ug/L 09/18/23 15:10 606-20-209/15/23 16:548.3 1.4 1
Di-n-octylphthalate ND ug/L 09/18/23 15:10 117-84-009/15/23 16:548.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/18/23 15:10 117-81-709/15/23 16:545.0 3.1 1
Fluoranthene ND ug/L 09/18/23 15:10 206-44-009/15/23 16:548.3 1.8 1
Fluorene ND ug/L 09/18/23 15:10 86-73-709/15/23 16:548.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 09/18/23 15:10 87-68-309/15/23 16:548.3 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW03W6-091223 Lab ID: 92687719001 Collected: 09/12/23 15:16 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Hexachlorobenzene ND ug/L 09/18/23 15:10 118-74-109/15/23 16:548.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 09/18/23 15:10 77-47-409/15/23 16:548.3 1.3 1
Hexachloroethane ND ug/L 09/18/23 15:10 67-72-109/15/23 16:548.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/18/23 15:10 193-39-509/15/23 16:548.3 2.4 1
Isophorone ND ug/L 09/18/23 15:10 78-59-109/15/23 16:548.3 1.4 1
2-Methylnaphthalene ND ug/L 09/18/23 15:10 91-57-609/15/23 16:548.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/18/23 15:10 95-48-709/15/23 16:548.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/18/23 15:10 15831-10-409/15/23 16:548.3 1.0 1
Naphthalene ND ug/L 09/18/23 15:10 91-20-309/15/23 16:548.3 1.7 1
2-Nitroaniline ND ug/L 09/18/23 15:10 88-74-409/15/23 16:5416.7 2.5 1
3-Nitroaniline ND ug/L 09/18/23 15:10 99-09-209/15/23 16:5416.7 3.1 1
4-Nitroaniline ND ug/L 09/18/23 15:10 100-01-609/15/23 16:5416.7 4.2 1
Nitrobenzene ND ug/L 09/18/23 15:10 98-95-309/15/23 16:548.3 1.6 1
2-Nitrophenol ND ug/L 09/18/23 15:10 88-75-509/15/23 16:548.3 1.2 1
4-Nitrophenol ND ug/L 09/18/23 15:10 100-02-709/15/23 16:5441.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 09/18/23 15:10 621-64-709/15/23 16:548.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 09/18/23 15:10 86-30-609/15/23 16:548.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/18/23 15:10 108-60-109/15/23 16:548.3 0.96 1
Pentachlorophenol ND ug/L 09/18/23 15:10 87-86-509/15/23 16:5416.7 3.1 1
Phenanthrene ND ug/L 09/18/23 15:10 85-01-809/15/23 16:548.3 1.7 1
Phenol ND ug/L 09/18/23 15:10 108-95-209/15/23 16:548.3 1.1 1
Pyrene ND ug/L 09/18/23 15:10 129-00-009/15/23 16:548.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 09/18/23 15:10 95-95-409/15/23 16:548.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/18/23 15:10 88-06-209/15/23 16:548.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)83 %09/18/23 15:10 4165-60-009/15/23 16:5410-138 1
2-Fluorobiphenyl (S)86 %09/18/23 15:10 321-60-809/15/23 16:5410-130 1
Terphenyl-d14 (S)107 %09/18/23 15:10 1718-51-009/15/23 16:5419-191 1
Phenol-d6 (S)49 %09/18/23 15:10 13127-88-309/15/23 16:5410-130 1
2-Fluorophenol (S)65 %09/18/23 15:10 367-12-409/15/23 16:5410-130 1
2,4,6-Tribromophenol (S)85 %09/18/23 15:10 118-79-609/15/23 16:5410-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/20/23 16:46 67-64-125.0 5.1 1
Benzene ND ug/L 09/20/23 16:46 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/20/23 16:46 75-27-41.0 0.31 1
Bromoform ND ug/L 09/20/23 16:46 75-25-2 v21.0 0.34 1
Bromomethane ND ug/L 09/20/23 16:46 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/20/23 16:46 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/20/23 16:46 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/20/23 16:46 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/20/23 16:46 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/20/23 16:46 75-00-31.0 0.65 1
Chloroform ND ug/L 09/20/23 16:46 67-66-31.0 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW03W6-091223 Lab ID: 92687719001 Collected: 09/12/23 15:16 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 09/20/23 16:46 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/20/23 16:46 110-82-7 IK1.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/20/23 16:46 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/20/23 16:46 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/20/23 16:46 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/20/23 16:46 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/20/23 16:46 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/20/23 16:46 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/20/23 16:46 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/20/23 16:46 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/20/23 16:46 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/20/23 16:46 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/20/23 16:46 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/20/23 16:46 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/20/23 16:46 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/20/23 16:46 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/20/23 16:46 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/20/23 16:46 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/20/23 16:46 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/20/23 16:46 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/20/23 16:46 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/20/23 16:46 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/20/23 16:46 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/20/23 16:46 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/20/23 16:46 1634-04-41.0 0.42 1
Styrene ND ug/L 09/20/23 16:46 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/20/23 16:46 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/20/23 16:46 127-18-41.0 0.29 1
Toluene ND ug/L 09/20/23 16:46 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/20/23 16:46 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/20/23 16:46 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/20/23 16:46 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/20/23 16:46 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/20/23 16:46 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/20/23 16:46 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/20/23 16:46 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/20/23 16:46 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/20/23 16:46 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %09/20/23 16:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %09/20/23 16:46 17060-07-070-130 1
Toluene-d8 (S)98 %09/20/23 16:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW03W6-091223 Lab ID: 92687719001 Collected: 09/12/23 15:16 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 604 mg/L 09/18/23 18:105.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/15/23 05:08 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 50.6 mg/L 09/15/23 06:20 16887-00-620.0 12.0 20
Sulfate 490 mg/L 09/15/23 06:20 14808-79-8 M120.0 10.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW02W6-091223 Lab ID: 92687719002 Collected: 09/12/23 14:50 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 7.2 Std. Units 09/14/23 13:18100
True Color 4000 units 09/14/23 13:18500 500 100
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 10/01/23 23:30 7440-36-009/27/23 13:1525.0 15.0 5
Arsenic ND ug/L 10/01/23 23:30 7440-38-209/27/23 13:1550.0 23.5 5
Barium 264 ug/L 10/01/23 23:30 7440-39-309/27/23 13:1525.0 17.4 5
Beryllium ND ug/L 10/01/23 23:30 7440-41-709/27/23 13:155.0 3.5 5
Boron ND ug/L 10/01/23 23:30 7440-42-809/27/23 13:15250 162 5
Cadmium ND ug/L 10/01/23 23:30 7440-43-909/27/23 13:155.0 2.0 5
Chromium 42.4 ug/L 10/01/23 23:30 7440-47-309/27/23 13:1525.0 18.3 5
Cobalt 24.8J ug/L 10/01/23 23:30 7440-48-409/27/23 13:1525.0 18.2 5
Copper ND ug/L 10/01/23 23:30 7440-50-809/27/23 13:1525.0 21.3 5
Lead ND ug/L 10/01/23 23:30 7439-92-109/27/23 13:1525.0 22.7 5
Nickel ND ug/L 10/01/23 23:30 7440-02-009/27/23 13:1525.0 17.3 5
Selenium ND ug/L 10/01/23 23:30 7782-49-209/27/23 13:1550.0 23.5 5
Silver ND ug/L 10/01/23 23:30 7440-22-409/27/23 13:1525.0 12.5 5
Thallium ND ug/L 10/01/23 23:30 7440-28-009/27/23 13:1550.0 40.7 5
Vanadium 556 ug/L 10/01/23 23:30 7440-62-209/27/23 13:1525.0 19.7 5
Zinc 2860 ug/L 10/01/23 23:30 7440-66-609/27/23 13:1550.0 47.3 5
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/03/23 20:06 7440-36-009/27/23 20:305.0 3.0 1
Arsenic, Dissolved 7.5J ug/L 10/03/23 20:06 7440-38-209/27/23 20:3010.0 4.7 1
Barium, Dissolved 211 ug/L 10/03/23 20:06 7440-39-309/27/23 20:305.0 3.5 1
Beryllium, Dissolved ND ug/L 10/03/23 20:06 7440-41-709/27/23 20:301.0 0.70 1
Boron, Dissolved 122 ug/L 10/03/23 20:06 7440-42-809/27/23 20:3050.0 32.4 1
Cadmium, Dissolved ND ug/L 10/03/23 20:06 7440-43-909/27/23 20:301.0 0.40 1
Chromium, Dissolved 13.5 ug/L 10/03/23 20:06 7440-47-309/27/23 20:305.0 3.7 1
Cobalt, Dissolved 15.8 ug/L 10/03/23 20:06 7440-48-409/27/23 20:305.0 3.6 1
Copper, Dissolved ND ug/L 10/03/23 20:06 7440-50-809/27/23 20:305.0 4.3 1
Lead, Dissolved ND ug/L 10/03/23 20:06 7439-92-109/27/23 20:305.0 4.5 1
Nickel, Dissolved 10.8 ug/L 10/03/23 20:06 7440-02-009/27/23 20:305.0 3.5 1
Selenium, Dissolved ND ug/L 10/03/23 20:06 7782-49-209/27/23 20:3010.0 4.7 1
Silver, Dissolved ND ug/L 10/03/23 20:06 7440-22-409/27/23 20:305.0 2.5 1
Thallium, Dissolved ND ug/L 10/03/23 20:06 7440-28-009/27/23 20:3010.0 8.1 1
Vanadium, Dissolved 423 ug/L 10/03/23 20:06 7440-62-209/27/23 20:305.0 3.9 1
Zinc, Dissolved 2000 ug/L 10/03/23 20:06 7440-66-609/27/23 20:3010.0 9.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/04/23 09:39 7439-97-6 D310/03/23 07:580.40 0.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW02W6-091223 Lab ID: 92687719002 Collected: 09/12/23 14:50 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/03/23 12:34 7439-97-610/02/23 15:100.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene 1.9J ug/L 09/18/23 15:36 83-32-909/15/23 16:548.7 1.7 1
Acenaphthylene ND ug/L 09/18/23 15:36 208-96-809/15/23 16:548.7 1.7 1
Acetophenone ND ug/L 09/18/23 15:36 98-86-209/15/23 16:548.7 1.3 1
Anthracene ND ug/L 09/18/23 15:36 120-12-709/15/23 16:548.7 2.0 1
Atrazine ND ug/L 09/18/23 15:36 1912-24-909/15/23 16:548.7 2.8 1
Benzaldehyde ND ug/L 09/18/23 15:36 100-52-709/15/23 16:548.7 3.1 1
Benzo(a)anthracene ND ug/L 09/18/23 15:36 56-55-309/15/23 16:548.7 2.3 1
Benzo(a)pyrene ND ug/L 09/18/23 15:36 50-32-809/15/23 16:548.7 2.4 1
Benzo(b)fluoranthene ND ug/L 09/18/23 15:36 205-99-209/15/23 16:548.7 2.3 1
Benzo(g,h,i)perylene ND ug/L 09/18/23 15:36 191-24-209/15/23 16:548.7 2.5 1
Benzo(k)fluoranthene ND ug/L 09/18/23 15:36 207-08-909/15/23 16:548.7 2.4 1
Biphenyl (Diphenyl)ND ug/L 09/18/23 15:36 92-52-409/15/23 16:548.7 1.6 1
4-Bromophenylphenyl ether ND ug/L 09/18/23 15:36 101-55-309/15/23 16:548.7 1.5 1
Butylbenzylphthalate ND ug/L 09/18/23 15:36 85-68-709/15/23 16:548.7 2.7 1
Caprolactam ND ug/L 09/18/23 15:36 105-60-209/15/23 16:548.7 6.0 1
Carbazole ND ug/L 09/18/23 15:36 86-74-809/15/23 16:548.7 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/18/23 15:36 59-50-709/15/23 16:548.7 2.9 1
4-Chloroaniline ND ug/L 09/18/23 15:36 106-47-809/15/23 16:5417.4 3.2 1
bis(2-Chloroethoxy)methane ND ug/L 09/18/23 15:36 111-91-109/15/23 16:548.7 1.6 1
bis(2-Chloroethyl) ether ND ug/L 09/18/23 15:36 111-44-409/15/23 16:548.7 1.7 1
2-Chloronaphthalene ND ug/L 09/18/23 15:36 91-58-709/15/23 16:548.7 1.5 1
2-Chlorophenol ND ug/L 09/18/23 15:36 95-57-809/15/23 16:548.7 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/18/23 15:36 7005-72-309/15/23 16:548.7 1.7 1
Chrysene ND ug/L 09/18/23 15:36 218-01-909/15/23 16:548.7 2.4 1
Dibenz(a,h)anthracene ND ug/L 09/18/23 15:36 53-70-309/15/23 16:548.7 2.6 1
Dibenzofuran ND ug/L 09/18/23 15:36 132-64-909/15/23 16:548.7 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/18/23 15:36 91-94-109/15/23 16:5417.4 7.1 1
2,4-Dichlorophenol ND ug/L 09/18/23 15:36 120-83-209/15/23 16:548.7 1.2 1
Diethylphthalate ND ug/L 09/18/23 15:36 84-66-209/15/23 16:548.7 1.8 1
2,4-Dimethylphenol ND ug/L 09/18/23 15:36 105-67-909/15/23 16:548.7 1.5 1
Dimethylphthalate ND ug/L 09/18/23 15:36 131-11-309/15/23 16:548.7 1.9 1
Di-n-butylphthalate ND ug/L 09/18/23 15:36 84-74-209/15/23 16:548.7 1.9 1
4,6-Dinitro-2-methylphenol ND ug/L 09/18/23 15:36 534-52-109/15/23 16:5417.4 6.8 1
2,4-Dinitrophenol ND ug/L 09/18/23 15:36 51-28-509/15/23 16:5443.5 22.6 1
2,4-Dinitrotoluene ND ug/L 09/18/23 15:36 121-14-209/15/23 16:548.7 1.4 1
2,6-Dinitrotoluene ND ug/L 09/18/23 15:36 606-20-209/15/23 16:548.7 1.5 1
Di-n-octylphthalate ND ug/L 09/18/23 15:36 117-84-009/15/23 16:548.7 3.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/18/23 15:36 117-81-709/15/23 16:545.2 3.2 1
Fluoranthene 5.7J ug/L 09/18/23 15:36 206-44-009/15/23 16:548.7 1.9 1
Fluorene ND ug/L 09/18/23 15:36 86-73-709/15/23 16:548.7 1.8 1
Hexachloro-1,3-butadiene ND ug/L 09/18/23 15:36 87-68-309/15/23 16:548.7 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW02W6-091223 Lab ID: 92687719002 Collected: 09/12/23 14:50 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Hexachlorobenzene ND ug/L 09/18/23 15:36 118-74-109/15/23 16:548.7 1.9 1
Hexachlorocyclopentadiene ND ug/L 09/18/23 15:36 77-47-409/15/23 16:548.7 1.4 1
Hexachloroethane ND ug/L 09/18/23 15:36 67-72-109/15/23 16:548.7 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/18/23 15:36 193-39-509/15/23 16:548.7 2.5 1
Isophorone ND ug/L 09/18/23 15:36 78-59-109/15/23 16:548.7 1.4 1
2-Methylnaphthalene ND ug/L 09/18/23 15:36 91-57-609/15/23 16:548.7 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/18/23 15:36 95-48-709/15/23 16:548.7 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/18/23 15:36 15831-10-409/15/23 16:548.7 1.1 1
Naphthalene ND ug/L 09/18/23 15:36 91-20-309/15/23 16:548.7 1.8 1
2-Nitroaniline ND ug/L 09/18/23 15:36 88-74-409/15/23 16:5417.4 2.6 1
3-Nitroaniline ND ug/L 09/18/23 15:36 99-09-209/15/23 16:5417.4 3.3 1
4-Nitroaniline ND ug/L 09/18/23 15:36 100-01-609/15/23 16:5417.4 4.4 1
Nitrobenzene ND ug/L 09/18/23 15:36 98-95-309/15/23 16:548.7 1.6 1
2-Nitrophenol ND ug/L 09/18/23 15:36 88-75-509/15/23 16:548.7 1.2 1
4-Nitrophenol ND ug/L 09/18/23 15:36 100-02-709/15/23 16:5443.5 5.7 1
N-Nitroso-di-n-propylamine ND ug/L 09/18/23 15:36 621-64-709/15/23 16:548.7 1.2 1
N-Nitrosodiphenylamine ND ug/L 09/18/23 15:36 86-30-609/15/23 16:548.7 2.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/18/23 15:36 108-60-109/15/23 16:548.7 1.0 1
Pentachlorophenol ND ug/L 09/18/23 15:36 87-86-509/15/23 16:5417.4 3.3 1
Phenanthrene ND ug/L 09/18/23 15:36 85-01-809/15/23 16:548.7 1.7 1
Phenol ND ug/L 09/18/23 15:36 108-95-209/15/23 16:548.7 1.2 1
Pyrene 4.6J ug/L 09/18/23 15:36 129-00-009/15/23 16:548.7 1.9 1
2,4,5-Trichlorophenol ND ug/L 09/18/23 15:36 95-95-409/15/23 16:548.7 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/18/23 15:36 88-06-209/15/23 16:548.7 1.3 1
Surrogates
Nitrobenzene-d5 (S)50 %09/18/23 15:36 4165-60-009/15/23 16:5410-138 1
2-Fluorobiphenyl (S)53 %09/18/23 15:36 321-60-809/15/23 16:5410-130 1
Terphenyl-d14 (S)62 %09/18/23 15:36 1718-51-009/15/23 16:5419-191 1
Phenol-d6 (S)30 %09/18/23 15:36 13127-88-309/15/23 16:5410-130 1
2-Fluorophenol (S)39 %09/18/23 15:36 367-12-409/15/23 16:5410-130 1
2,4,6-Tribromophenol (S)48 %09/18/23 15:36 118-79-609/15/23 16:5410-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/20/23 17:03 67-64-125.0 5.1 1
Benzene ND ug/L 09/20/23 17:03 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/20/23 17:03 75-27-41.0 0.31 1
Bromoform ND ug/L 09/20/23 17:03 75-25-2 v21.0 0.34 1
Bromomethane ND ug/L 09/20/23 17:03 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/20/23 17:03 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/20/23 17:03 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/20/23 17:03 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/20/23 17:03 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/20/23 17:03 75-00-31.0 0.65 1
Chloroform ND ug/L 09/20/23 17:03 67-66-31.0 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW02W6-091223 Lab ID: 92687719002 Collected: 09/12/23 14:50 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 09/20/23 17:03 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/20/23 17:03 110-82-7 IK1.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/20/23 17:03 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/20/23 17:03 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/20/23 17:03 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/20/23 17:03 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/20/23 17:03 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/20/23 17:03 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/20/23 17:03 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/20/23 17:03 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/20/23 17:03 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/20/23 17:03 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/20/23 17:03 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/20/23 17:03 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/20/23 17:03 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/20/23 17:03 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/20/23 17:03 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/20/23 17:03 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/20/23 17:03 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)0.64J ug/L 09/20/23 17:03 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/20/23 17:03 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/20/23 17:03 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/20/23 17:03 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/20/23 17:03 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/20/23 17:03 1634-04-41.0 0.42 1
Styrene ND ug/L 09/20/23 17:03 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/20/23 17:03 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/20/23 17:03 127-18-41.0 0.29 1
Toluene ND ug/L 09/20/23 17:03 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/20/23 17:03 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/20/23 17:03 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/20/23 17:03 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/20/23 17:03 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/20/23 17:03 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/20/23 17:03 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/20/23 17:03 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/20/23 17:03 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/20/23 17:03 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %09/20/23 17:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %09/20/23 17:03 17060-07-070-130 1
Toluene-d8 (S)98 %09/20/23 17:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: RW02W6-091223 Lab ID: 92687719002 Collected: 09/12/23 14:50 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 1050 mg/L 09/18/23 18:205.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/15/23 05:08 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 56.7 mg/L 09/15/23 07:31 16887-00-620.0 12.0 20
Sulfate 203 mg/L 09/15/23 07:31 14808-79-820.0 10.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: TRIP BLANK Lab ID: 92687719003 Collected: 09/12/23 12:00 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/16/23 05:23 67-64-125.0 5.1 1
Benzene ND ug/L 09/16/23 05:23 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/16/23 05:23 75-27-41.0 0.31 1
Bromoform ND ug/L 09/16/23 05:23 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/16/23 05:23 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/16/23 05:23 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/16/23 05:23 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/16/23 05:23 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/16/23 05:23 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/16/23 05:23 75-00-31.0 0.65 1
Chloroform ND ug/L 09/16/23 05:23 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/16/23 05:23 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/16/23 05:23 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/16/23 05:23 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/16/23 05:23 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/16/23 05:23 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/16/23 05:23 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/16/23 05:23 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/16/23 05:23 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/16/23 05:23 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/16/23 05:23 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/16/23 05:23 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/16/23 05:23 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/16/23 05:23 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/16/23 05:23 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/16/23 05:23 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/16/23 05:23 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/16/23 05:23 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/16/23 05:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/16/23 05:23 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/16/23 05:23 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/16/23 05:23 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/16/23 05:23 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/16/23 05:23 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/16/23 05:23 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/16/23 05:23 1634-04-41.0 0.42 1
Styrene ND ug/L 09/16/23 05:23 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/16/23 05:23 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/16/23 05:23 127-18-41.0 0.29 1
Toluene ND ug/L 09/16/23 05:23 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/16/23 05:23 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/16/23 05:23 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/16/23 05:23 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/16/23 05:23 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/16/23 05:23 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Sample: TRIP BLANK Lab ID: 92687719003 Collected: 09/12/23 12:00 Received: 09/13/23 07:39 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/16/23 05:23 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/16/23 05:23 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/16/23 05:23 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/16/23 05:23 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)96 %09/16/23 05:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %09/16/23 05:23 17060-07-070-130 1
Toluene-d8 (S)98 %09/16/23 05:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
799717
SM 2120B-2011
SM 2120B-2011
2120B True Color EDEN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4142127
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
True Color units ND 5.0 09/14/23 13:135.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4142128LABORATORY CONTROL SAMPLE:
LCSSpike
True Color units 35.035 100 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92687719002
4142129SAMPLE DUPLICATE:
pH Std. Units 7.2 0 107.2
True Color units 4000 0 104000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954517
EPA 7470
EPA 7470
7470 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5248824
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/04/23 08:420.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5248825LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.02 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5248826MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35830850002
5248827
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 96 75-12598 1 2020.14J 2.1 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954441
EPA 7470
EPA 7470
7470 Mercury Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5248254
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/03/23 12:130.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5248255LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 1.92 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5248256MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687719001
5248257
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2 94 85-11594 0 202ND1.9 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802282
EPA 3010A
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4155782
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
Antimony ug/L ND 5.0 10/01/23 22:493.0
Arsenic ug/L ND 10.0 10/01/23 22:494.7
Barium ug/L ND 5.0 10/01/23 22:493.5
Beryllium ug/L ND 1.0 10/01/23 22:490.70
Boron ug/L ND 50.0 10/01/23 22:4932.4
Cadmium ug/L ND 1.0 10/01/23 22:490.40
Chromium ug/L ND 5.0 10/01/23 22:493.7
Cobalt ug/L ND 5.0 10/01/23 22:493.6
Copper ug/L ND 5.0 10/01/23 22:494.3
Lead ug/L ND 5.0 10/01/23 22:494.5
Nickel ug/L ND 5.0 10/01/23 22:493.5
Selenium ug/L ND 10.0 10/01/23 22:494.7
Silver ug/L ND 5.0 10/01/23 22:492.5
Thallium ug/L ND 10.0 10/01/23 22:498.1
Vanadium ug/L ND 5.0 10/01/23 22:493.9
Zinc ug/L ND 10.0 10/01/23 22:499.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4155783LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 494500 99 80-120
Arsenic ug/L 492500 98 80-120
Barium ug/L 488500 98 80-120
Beryllium ug/L 498500 100 80-120
Boron ug/L 502500 100 80-120
Cadmium ug/L 495500 99 80-120
Chromium ug/L 498500 100 80-120
Cobalt ug/L 497500 99 80-120
Copper ug/L 490500 98 80-120
Lead ug/L 501500 100 80-120
Nickel ug/L 500500 100 80-120
Selenium ug/L 493500 99 80-120
Silver ug/L 242250 97 80-120
Thallium ug/L 490500 98 80-120
Vanadium ug/L 499500 100 80-120
Zinc ug/L 507500 101 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4155784MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687944007
4155785
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 100 75-12599 1 20500ND501 496
Arsenic ug/L 500 99 75-12598 1 20500ND494 489
Barium ug/L 500 96 75-12595 1 2050023.8 505 500
Beryllium ug/L 500 100 75-12599 1 20500ND498 494
Boron ug/L 500 100 75-125100 1 20500ND501 498
Cadmium ug/L 500 98 75-12597 1 20500ND489 485
Chromium ug/L 500 97 75-12596 1 20500ND486 483
Cobalt ug/L 500 97 75-12596 1 20500ND485 481
Copper ug/L 500 98 75-12596 1 20500ND488 481
Lead ug/L 500 97 75-12597 1 20500ND487 483
Nickel ug/L 500 97 75-12596 0 20500ND485 483
Selenium ug/L 500 102 75-125101 1 20500ND512 507
Silver ug/L 250 96 75-12595 1 20250ND240 238
Thallium ug/L 500 97 75-12596 1 20500ND484 479
Vanadium ug/L 500 99 75-12598 1 205007.4 504 500
Zinc ug/L 500 99 75-12599 1 20500ND502 499
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802409
EPA 3010A
EPA 6010D
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4156437
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
Antimony, Dissolved ug/L ND 5.0 10/03/23 19:373.0
Arsenic, Dissolved ug/L ND 10.0 10/03/23 19:374.7
Barium, Dissolved ug/L ND 5.0 10/03/23 19:373.5
Beryllium, Dissolved ug/L ND 1.0 10/03/23 19:370.70
Boron, Dissolved ug/L ND 50.0 10/03/23 19:3732.4
Cadmium, Dissolved ug/L ND 1.0 10/03/23 19:370.40
Chromium, Dissolved ug/L ND 5.0 10/03/23 19:373.7
Cobalt, Dissolved ug/L ND 5.0 10/03/23 19:373.6
Copper, Dissolved ug/L ND 5.0 10/03/23 19:374.3
Lead, Dissolved ug/L ND 5.0 10/03/23 19:374.5
Nickel, Dissolved ug/L ND 5.0 10/03/23 19:373.5
Selenium, Dissolved ug/L ND 10.0 10/03/23 19:374.7
Silver, Dissolved ug/L ND 5.0 10/03/23 19:372.5
Thallium, Dissolved ug/L ND 10.0 10/03/23 19:378.1
Vanadium, Dissolved ug/L ND 5.0 10/03/23 19:373.9
Zinc, Dissolved ug/L ND 10.0 10/03/23 19:379.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4156438LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 456500 91 80-120
Arsenic, Dissolved ug/L 448500 90 80-120
Barium, Dissolved ug/L 447500 89 80-120
Beryllium, Dissolved ug/L 453500 91 80-120
Boron, Dissolved ug/L 458500 92 80-120
Cadmium, Dissolved ug/L 452500 90 80-120
Chromium, Dissolved ug/L 446500 89 80-120
Cobalt, Dissolved ug/L 448500 90 80-120
Copper, Dissolved ug/L 439500 88 80-120
Lead, Dissolved ug/L 448500 90 80-120
Nickel, Dissolved ug/L 449500 90 80-120
Selenium, Dissolved ug/L 471500 94 80-120
Silver, Dissolved ug/L 225250 90 80-120
Thallium, Dissolved ug/L 452500 90 80-120
Vanadium, Dissolved ug/L 450500 90 80-120
Zinc, Dissolved ug/L 454500 91 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4156455MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687719001
4156456
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 500 89 75-12587 1 20500ND443 437
Arsenic, Dissolved ug/L 500 92 75-12590 2 20500ND464 453
Barium, Dissolved ug/L 500 90 75-12589 1 2050088.8 537 532
Beryllium, Dissolved ug/L 500 93 75-12591 2 20500ND464 457
Boron, Dissolved ug/L 500 95 75-12594 1 20500114592 583
Cadmium, Dissolved ug/L 500 88 75-12587 1 20500ND439 433
Chromium, Dissolved ug/L 500 89 75-12587 2 205004.2J 448 440
Cobalt, Dissolved ug/L 500 90 75-12589 1 20500ND451 447
Copper, Dissolved ug/L 500 98 75-12597 1 20500ND492 488
Lead, Dissolved ug/L 500 88 75-12587 1 20500ND444 438
Nickel, Dissolved ug/L 500 89 75-12587 2 20500ND446 439
Selenium, Dissolved ug/L 500 96 75-12594 1 20500ND478 472
Silver, Dissolved ug/L 250 94 75-12592 1 20250ND234 231
Thallium, Dissolved ug/L 500 88 75-12587 2 20500ND442 435
Vanadium, Dissolved ug/L 500 93 75-12592 1 2050057.7 525 519
Zinc, Dissolved ug/L 500 90 75-12589 1 2050034.1 485 480
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
799716
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92687719003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4142115
Associated Lab Samples:92687719003
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/15/23 23:280.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/15/23 23:280.22
1,1,2-Trichloroethane ug/L ND 1.0 09/15/23 23:280.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/15/23 23:280.32
1,1-Dichloroethane ug/L ND 1.0 09/15/23 23:280.37
1,1-Dichloroethene ug/L ND 1.0 09/15/23 23:280.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/15/23 23:280.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/15/23 23:280.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/15/23 23:280.27
1,2-Dichlorobenzene ug/L ND 1.0 09/15/23 23:280.34
1,2-Dichloroethane ug/L ND 1.0 09/15/23 23:280.32
1,2-Dichloropropane ug/L ND 1.0 09/15/23 23:280.36
1,3-Dichlorobenzene ug/L ND 1.0 09/15/23 23:280.34
1,4-Dichlorobenzene ug/L ND 1.0 09/15/23 23:280.33
2-Butanone (MEK)ug/L ND 5.0 09/15/23 23:284.0
2-Hexanone ug/L ND 5.0 09/15/23 23:280.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/15/23 23:282.7
Acetone ug/L ND 25.0 09/15/23 23:285.1
Benzene ug/L ND 1.0 09/15/23 23:280.34
Bromodichloromethane ug/L ND 1.0 09/15/23 23:280.31
Bromoform ug/L ND 1.0 09/15/23 23:280.34
Bromomethane ug/L ND 2.0 v209/15/23 23:281.7
Carbon disulfide ug/L ND 2.0 09/15/23 23:280.36
Carbon tetrachloride ug/L ND 1.0 09/15/23 23:280.33
Chlorobenzene ug/L ND 1.0 09/15/23 23:280.28
Chloroethane ug/L ND 1.0 09/15/23 23:280.65
Chloroform ug/L ND 1.0 09/15/23 23:280.43
Chloromethane ug/L ND 1.0 09/15/23 23:280.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/15/23 23:280.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/15/23 23:280.36
Cyclohexane ug/L ND 1.0 09/15/23 23:280.35
Dibromochloromethane ug/L ND 1.0 09/15/23 23:280.36
Dichlorodifluoromethane ug/L ND 1.0 09/15/23 23:280.35
Ethylbenzene ug/L ND 1.0 09/15/23 23:280.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/15/23 23:280.33
m&p-Xylene ug/L ND 2.0 09/15/23 23:280.71
Methyl acetate ug/L ND 10.0 09/15/23 23:282.4
Methyl-tert-butyl ether ug/L ND 1.0 09/15/23 23:280.42
Methylcyclohexane ug/L ND 10.0 09/15/23 23:281.5
Methylene Chloride ug/L ND 5.0 09/15/23 23:282.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4142115
Associated Lab Samples:92687719003
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/15/23 23:280.34
Styrene ug/L ND 1.0 09/15/23 23:280.29
Tetrachloroethene ug/L ND 1.0 09/15/23 23:280.29
Toluene ug/L ND 1.0 09/15/23 23:280.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/15/23 23:280.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/15/23 23:280.36
Trichloroethene ug/L ND 1.0 09/15/23 23:280.38
Trichlorofluoromethane ug/L ND 1.0 09/15/23 23:280.30
Vinyl chloride ug/L ND 1.0 09/15/23 23:280.39
1,2-Dichloroethane-d4 (S)%82 70-130 09/15/23 23:28
4-Bromofluorobenzene (S)%97 70-130 09/15/23 23:28
Toluene-d8 (S)%99 70-130 09/15/23 23:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4142116LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.220 96 70-130
1,1,2,2-Tetrachloroethane ug/L 22.020 110 70-130
1,1,2-Trichloroethane ug/L 22.820 114 70-130
1,1,2-Trichlorotrifluoroethane ug/L 19.820 99 70-132
1,1-Dichloroethane ug/L 17.320 86 70-130
1,1-Dichloroethene ug/L 18.620 93 69-131
1,2,4-Trichlorobenzene ug/L 23.520 117 70-130
1,2-Dibromo-3-chloropropane ug/L 23.420 117 70-130
1,2-Dibromoethane (EDB)ug/L 22.720 114 70-130
1,2-Dichlorobenzene ug/L 22.620 113 70-130
1,2-Dichloroethane ug/L 16.520 82 70-130
1,2-Dichloropropane ug/L 20.220 101 70-130
1,3-Dichlorobenzene ug/L 23.020 115 70-130
1,4-Dichlorobenzene ug/L 22.220 111 70-130
2-Butanone (MEK)ug/L 33.240 83 67-133
2-Hexanone ug/L 42.840 107 70-133
4-Methyl-2-pentanone (MIBK)ug/L 41.740 104 70-130
Acetone ug/L 34.840 87 67-130
Benzene ug/L 20.220 101 70-130
Bromodichloromethane ug/L 22.120 111 70-130
Bromoform ug/L 24.320 121 70-133
Bromomethane ug/L 15.5 v32078 41-148
Carbon disulfide ug/L 19.620 98 70-131
Carbon tetrachloride ug/L 21.720 108 70-130
Chlorobenzene ug/L 22.220 111 70-130
Chloroethane ug/L 16.920 84 41-157
Chloroform ug/L 18.020 90 70-130
Chloromethane ug/L 18.520 92 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4142116LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 17.220 86 70-130
cis-1,3-Dichloropropene ug/L 21.820 109 70-130
Cyclohexane ug/L 18.420 92 63-137
Dibromochloromethane ug/L 23.520 117 70-130
Dichlorodifluoromethane ug/L 20.520 103 54-147
Ethylbenzene ug/L 21.920 109 70-130
Isopropylbenzene (Cumene)ug/L 23.520 118 70-130
m&p-Xylene ug/L 44.840 112 70-130
Methyl acetate ug/L 17.520 88 70-130
Methyl-tert-butyl ether ug/L 17.020 85 70-130
Methylcyclohexane ug/L 19.920 100 70-130
Methylene Chloride ug/L 17.920 89 62-130
o-Xylene ug/L 22.820 114 70-130
Styrene ug/L 23.620 118 70-130
Tetrachloroethene ug/L 23.620 118 70-130
Toluene ug/L 21.520 108 70-130
trans-1,2-Dichloroethene ug/L 18.020 90 70-130
trans-1,3-Dichloropropene ug/L 22.220 111 70-130
Trichloroethene ug/L 22.120 110 70-130
Trichlorofluoromethane ug/L 20.620 103 57-130
Vinyl chloride ug/L 17.620 88 66-140
1,2-Dichloroethane-d4 (S)%80 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4144724MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687706005
4144725
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L M12014170-150161 13 3020ND28.3 32.2
1,1,2,2-Tetrachloroethane ug/L M12014466-144164 13 3020ND28.8 32.8
1,1,2-Trichloroethane ug/L M12012670-142148 16 3020ND25.2 29.6
1,1,2-Trichlorotrifluoroethane ug/L M1,v12019266-168177 8 3020ND38.4 35.4
1,1-Dichloroethane ug/L M12015768-150179 13 3020ND31.3 35.8
1,1-Dichloroethene ug/L M1,v12018164-162159 13 3020ND36.2 31.8
1,2,4-Trichlorobenzene ug/L 20 100 69-147113 12 3020ND20.0 22.5
1,2-Dibromo-3-chloropropane ug/L 20 109 62-146115 6 3020ND21.8 23.0
1,2-Dibromoethane (EDB) ug/L M12012870-143149 15 3020ND25.5 29.8
1,2-Dichlorobenzene ug/L 20 135 70-142135 0 3020ND27.0 27.0
1,2-Dichloroethane ug/L M12014068-145161 14 3020ND28.0 32.2
1,2-Dichloropropane ug/L M12014470-144169 16 3020ND28.9 33.7
1,3-Dichlorobenzene ug/L M12014070-142152 8 3020ND28.0 30.4
1,4-Dichlorobenzene ug/L M12013770-140154 11 3020ND27.5 30.8
2-Butanone (MEK)ug/L 40 141 57-156142 1 3040ND56.5 56.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4144724MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687706005
4144725
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L M14013762-153161 16 3040ND54.9 64.4
4-Methyl-2-pentanone(MIBK)ug/L 40 128 65-144144 12 3040ND51.1 57.8
Acetone ug/L v14014949-162153 2 3040ND59.6 61.1
Benzene ug/L M12014368-144165 15 3020ND28.6 33.1
Bromodichloromethane ug/L 20 122 70-141139 13 3020ND24.4 27.8
Bromoform ug/L 20 109 59-144126 14 3020ND21.8 25.2
Bromomethane ug/L 20 157 23-190188 18 3020ND31.4 37.6
Carbon disulfide ug/L M1,v12016764-160154 8 3020ND33.4 30.7
Carbon tetrachloride ug/L M12012970-147149 14 3020ND25.8 29.8
Chlorobenzene ug/L M12013870-143157 13 3020ND27.6 31.4
Chloroethane ug/L IK,M1,v12020555-190231 12 3020ND41.0 46.1
Chloroform ug/L M12014167-148164 15 3020ND28.2 32.7
Chloromethane ug/L 20 132 38-180149 13 3020ND26.3 29.9
cis-1,2-Dichloroethene ug/L M12015067-151171 13 3020ND30.1 34.3
cis-1,3-Dichloropropene ug/L 20 122 70-142139 13 3020ND24.3 27.7
Cyclohexane ug/L M1,v12019164-162217 13 3020ND38.2 43.5
Dibromochloromethane ug/L 20 119 68-140136 13 3020ND23.7 27.1
Dichlorodifluoromethane ug/L 20 177 15-200198 11 3020ND35.5 39.6
Ethylbenzene ug/L M12014170-145162 14 3020ND28.2 32.3Isopropylbenzene(Cumene)ug/L M12014070-144159 13 3020ND28.0 31.8
m&p-Xylene ug/L M14014070-148159 13 3040ND56.0 63.5
Methyl acetate ug/L M12013962-144151 8 3020ND27.8 30.2
Methyl-tert-butyl ether ug/L M12012564-146153 20 3020ND25.0 30.7
Methylcyclohexane ug/L M1,v12018370-155206 12 3020ND36.7 41.2
Methylene Chloride ug/L M1,v12016754-149173 3 3020ND33.5 34.6
o-Xylene ug/L M12012870-145149 15 3020ND25.6 29.9
Styrene ug/L M12013570-147155 14 3020ND26.9 31.0
Tetrachloroethene ug/L 20 130 70-145145 11 3020ND26.0 28.9
Toluene ug/L 20 131 65-146146 11 3020ND26.3 29.3
trans-1,2-Dichloroethene ug/L M1,v12017469-155192 10 3020ND34.9 38.4
trans-1,3-Dichloropropene ug/L 20 116 70-142137 17 3020ND23.2 27.3
Trichloroethene ug/L 20 131 70-152149 13 3020ND26.3 29.8
Trichlorofluoromethane ug/L M12016860-158186 10 3020ND33.6 37.2
Vinyl chloride ug/L 20 139 51-178158 13 3020ND27.7 31.7
1,2-Dichloroethane-d4 (S) %111 70-130113
4-Bromofluorobenzene (S) %99 70-130100
Toluene-d8 (S)%95 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800298
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4145134
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/20/23 13:310.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/20/23 13:310.22
1,1,2-Trichloroethane ug/L ND 1.0 09/20/23 13:310.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/20/23 13:310.32
1,1-Dichloroethane ug/L ND 1.0 09/20/23 13:310.37
1,1-Dichloroethene ug/L ND 1.0 09/20/23 13:310.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/20/23 13:310.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/20/23 13:310.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/20/23 13:310.27
1,2-Dichlorobenzene ug/L ND 1.0 09/20/23 13:310.34
1,2-Dichloroethane ug/L ND 1.0 09/20/23 13:310.32
1,2-Dichloropropane ug/L ND 1.0 09/20/23 13:310.36
1,3-Dichlorobenzene ug/L ND 1.0 09/20/23 13:310.34
1,4-Dichlorobenzene ug/L ND 1.0 09/20/23 13:310.33
2-Butanone (MEK)ug/L ND 5.0 09/20/23 13:314.0
2-Hexanone ug/L ND 5.0 09/20/23 13:310.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/20/23 13:312.7
Acetone ug/L ND 25.0 09/20/23 13:315.1
Benzene ug/L ND 1.0 09/20/23 13:310.34
Bromodichloromethane ug/L ND 1.0 09/20/23 13:310.31
Bromoform ug/L ND 1.0 v209/20/23 13:310.34
Bromomethane ug/L ND 2.0 v209/20/23 13:311.7
Carbon disulfide ug/L ND 2.0 09/20/23 13:310.36
Carbon tetrachloride ug/L ND 1.0 09/20/23 13:310.33
Chlorobenzene ug/L ND 1.0 09/20/23 13:310.28
Chloroethane ug/L ND 1.0 09/20/23 13:310.65
Chloroform ug/L ND 1.0 09/20/23 13:310.43
Chloromethane ug/L ND 1.0 09/20/23 13:310.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/20/23 13:310.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/20/23 13:310.36
Cyclohexane ug/L ND 1.0 IK09/20/23 13:310.35
Dibromochloromethane ug/L ND 1.0 09/20/23 13:310.36
Dichlorodifluoromethane ug/L ND 1.0 09/20/23 13:310.35
Ethylbenzene ug/L ND 1.0 09/20/23 13:310.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/20/23 13:310.33
m&p-Xylene ug/L ND 2.0 09/20/23 13:310.71
Methyl acetate ug/L ND 10.0 09/20/23 13:312.4
Methyl-tert-butyl ether ug/L ND 1.0 09/20/23 13:310.42
Methylcyclohexane ug/L ND 10.0 09/20/23 13:311.5
Methylene Chloride ug/L ND 5.0 09/20/23 13:312.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4145134
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/20/23 13:310.34
Styrene ug/L ND 1.0 09/20/23 13:310.29
Tetrachloroethene ug/L ND 1.0 09/20/23 13:310.29
Toluene ug/L ND 1.0 09/20/23 13:310.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/20/23 13:310.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/20/23 13:310.36
Trichloroethene ug/L ND 1.0 09/20/23 13:310.38
Trichlorofluoromethane ug/L ND 1.0 09/20/23 13:310.30
Vinyl chloride ug/L ND 1.0 09/20/23 13:310.39
1,2-Dichloroethane-d4 (S)%96 70-130 09/20/23 13:31
4-Bromofluorobenzene (S)%99 70-130 09/20/23 13:31
Toluene-d8 (S)%100 70-130 09/20/23 13:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4145135LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 21.220 106 70-130
1,1,2,2-Tetrachloroethane ug/L 19.520 97 70-130
1,1,2-Trichloroethane ug/L 20.420 102 70-130
1,1,2-Trichlorotrifluoroethane ug/L 21.520 108 70-132
1,1-Dichloroethane ug/L 21.220 106 70-130
1,1-Dichloroethene ug/L 21.020 105 69-131
1,2,4-Trichlorobenzene ug/L 21.420 107 70-130
1,2-Dibromo-3-chloropropane ug/L 18.820 94 70-130
1,2-Dibromoethane (EDB)ug/L 19.820 99 70-130
1,2-Dichlorobenzene ug/L 20.720 103 70-130
1,2-Dichloroethane ug/L 20.320 102 70-130
1,2-Dichloropropane ug/L 19.820 99 70-130
1,3-Dichlorobenzene ug/L 20.520 103 70-130
1,4-Dichlorobenzene ug/L 20.220 101 70-130
2-Butanone (MEK)ug/L 43.640 109 67-133
2-Hexanone ug/L 39.240 98 70-133
4-Methyl-2-pentanone (MIBK)ug/L 40.040 100 70-130
Acetone ug/L 38.140 95 67-130
Benzene ug/L 19.320 96 70-130
Bromodichloromethane ug/L 18.820 94 70-130
Bromoform ug/L 14.9 v32075 70-133
Bromomethane ug/L 13.0 v32065 41-148
Carbon disulfide ug/L 20.420 102 70-131
Carbon tetrachloride ug/L 20.320 101 70-130
Chlorobenzene ug/L 19.720 98 70-130
Chloroethane ug/L 16.720 84 41-157
Chloroform ug/L 20.120 100 70-130
Chloromethane ug/L 17.820 89 59-141
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
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Huntersville, NC 28078
[phone]
Page 29 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4145135LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 19.420 97 70-130
cis-1,3-Dichloropropene ug/L 19.520 98 70-130
Cyclohexane ug/L 21.8 IK20109 63-137
Dibromochloromethane ug/L 18.820 94 70-130
Dichlorodifluoromethane ug/L 21.620 108 54-147
Ethylbenzene ug/L 19.320 96 70-130
Isopropylbenzene (Cumene)ug/L 20.320 101 70-130
m&p-Xylene ug/L 39.240 98 70-130
Methyl acetate ug/L 17.420 87 70-130
Methyl-tert-butyl ether ug/L 19.320 96 70-130
Methylcyclohexane ug/L 21.620 108 70-130
Methylene Chloride ug/L 19.820 99 62-130
o-Xylene ug/L 19.520 97 70-130
Styrene ug/L 19.420 97 70-130
Tetrachloroethene ug/L 21.320 107 70-130
Toluene ug/L 19.620 98 70-130
trans-1,2-Dichloroethene ug/L 19.920 99 70-130
trans-1,3-Dichloropropene ug/L 17.120 86 70-130
Trichloroethene ug/L 21.620 108 70-130
Trichlorofluoromethane ug/L 19.720 98 57-130
Vinyl chloride ug/L 16.820 84 66-140
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4145136MATRIX SPIKE SAMPLE:
MSSpike
Result
92687719001
1,1,1-Trichloroethane ug/L 24.320 121 70-150ND
1,1,2,2-Tetrachloroethane ug/L 22.020 110 66-144ND
1,1,2-Trichloroethane ug/L 24.220 121 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 25.220 126 66-168ND
1,1-Dichloroethane ug/L 24.120 120 68-150ND
1,1-Dichloroethene ug/L 23.720 119 64-162ND
1,2,4-Trichlorobenzene ug/L 24.220 121 69-147ND
1,2-Dibromo-3-chloropropane ug/L 20.420 102 62-146ND
1,2-Dibromoethane (EDB)ug/L 23.420 117 70-143ND
1,2-Dichlorobenzene ug/L 23.620 118 70-142ND
1,2-Dichloroethane ug/L 21.720 109 68-145ND
1,2-Dichloropropane ug/L 24.120 120 70-144ND
1,3-Dichlorobenzene ug/L 23.720 118 70-142ND
1,4-Dichlorobenzene ug/L 22.520 113 70-140ND
2-Butanone (MEK)ug/L 44.340 111 57-156ND
2-Hexanone ug/L 42.640 107 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 44.540 111 65-144ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
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Huntersville, NC 28078
[phone]
Page 30 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4145136MATRIX SPIKE SAMPLE:
MSSpike
Result
92687719001
Acetone ug/L 37.140 93 49-162ND
Benzene ug/L 23.720 119 68-144ND
Bromodichloromethane ug/L 21.820 109 70-141ND
Bromoform ug/L 16.8 v32084 59-144ND
Bromomethane ug/L 18.820 94 23-190ND
Carbon disulfide ug/L 25.320 127 64-160ND
Carbon tetrachloride ug/L 23.020 115 70-147ND
Chlorobenzene ug/L 22.320 112 70-143ND
Chloroethane ug/L 23.620 118 55-190ND
Chloroform ug/L 23.220 116 67-148ND
Chloromethane ug/L 20.420 102 38-180ND
cis-1,2-Dichloroethene ug/L 22.720 113 67-151ND
cis-1,3-Dichloropropene ug/L 22.420 112 70-142ND
Cyclohexane ug/L 25.6 IK20128 64-162ND
Dibromochloromethane ug/L 21.220 106 68-140ND
Dichlorodifluoromethane ug/L 22.5 v120113 15-200ND
Ethylbenzene ug/L 22.620 113 70-145ND
Isopropylbenzene (Cumene)ug/L 24.220 121 70-144ND
m&p-Xylene ug/L 45.140 113 70-148ND
Methyl acetate ug/L 19.720 99 62-144ND
Methyl-tert-butyl ether ug/L 21.220 106 64-146ND
Methylcyclohexane ug/L 25.420 127 70-155ND
Methylene Chloride ug/L 22.220 111 54-149ND
o-Xylene ug/L 22.720 114 70-145ND
Styrene ug/L 23.220 116 70-147ND
Tetrachloroethene ug/L 23.120 116 70-145ND
Toluene ug/L 22.520 113 65-146ND
trans-1,2-Dichloroethene ug/L 23.320 117 69-155ND
trans-1,3-Dichloropropene ug/L 19.420 97 70-142ND
Trichloroethene ug/L 24.920 124 70-152ND
Trichlorofluoromethane ug/L 22.220 111 60-158ND
Vinyl chloride ug/L 20.120 101 51-178ND
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92687719002
4145137SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92687719002
4145137SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND v230ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND IK30ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND v130ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L 0.61J 300.64J
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9098
4-Bromofluorobenzene (S)%9699
Toluene-d8 (S)%10198
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
799912
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4143340
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/18/23 10:241.2
2,4,5-Trichlorophenol ug/L ND 10.0 09/18/23 10:241.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/18/23 10:241.6
2,4-Dichlorophenol ug/L ND 10.0 09/18/23 10:241.4
2,4-Dimethylphenol ug/L ND 10.0 09/18/23 10:241.7
2,4-Dinitrophenol ug/L ND 50.0 09/18/23 10:2426.0
2,4-Dinitrotoluene ug/L ND 10.0 09/18/23 10:241.6
2,6-Dinitrotoluene ug/L ND 10.0 09/18/23 10:241.7
2-Chloronaphthalene ug/L ND 10.0 09/18/23 10:241.7
2-Chlorophenol ug/L ND 10.0 09/18/23 10:241.2
2-Methylnaphthalene ug/L ND 10.0 09/18/23 10:241.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/18/23 10:241.9
2-Nitroaniline ug/L ND 20.0 09/18/23 10:243.0
2-Nitrophenol ug/L ND 10.0 09/18/23 10:241.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/18/23 10:241.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/18/23 10:248.1
3-Nitroaniline ug/L ND 20.0 09/18/23 10:243.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/18/23 10:247.8
4-Bromophenylphenyl ether ug/L ND 10.0 09/18/23 10:241.8
4-Chloro-3-methylphenol ug/L ND 10.0 09/18/23 10:243.3
4-Chloroaniline ug/L ND 20.0 09/18/23 10:243.6
4-Chlorophenylphenyl ether ug/L ND 10.0 09/18/23 10:242.0
4-Nitroaniline ug/L ND 20.0 09/18/23 10:245.1
4-Nitrophenol ug/L ND 50.0 09/18/23 10:246.6
Acenaphthene ug/L ND 10.0 09/18/23 10:242.0
Acenaphthylene ug/L ND 10.0 09/18/23 10:242.0
Acetophenone ug/L ND 10.0 09/18/23 10:241.5
Anthracene ug/L ND 10.0 09/18/23 10:242.3
Atrazine ug/L ND 10.0 09/18/23 10:243.2
Benzaldehyde ug/L ND 10.0 09/18/23 10:243.6
Benzo(a)anthracene ug/L ND 10.0 09/18/23 10:242.7
Benzo(a)pyrene ug/L ND 10.0 09/18/23 10:242.8
Benzo(b)fluoranthene ug/L ND 10.0 09/18/23 10:242.6
Benzo(g,h,i)perylene ug/L ND 10.0 09/18/23 10:242.8
Benzo(k)fluoranthene ug/L ND 10.0 09/18/23 10:242.7
Biphenyl (Diphenyl)ug/L ND 10.0 09/18/23 10:241.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/18/23 10:241.8
bis(2-Chloroethyl) ether ug/L ND 10.0 09/18/23 10:241.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/18/23 10:243.7
Butylbenzylphthalate ug/L ND 10.0 09/18/23 10:243.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4143340
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
Caprolactam ug/L ND 10.0 09/18/23 10:246.9
Carbazole ug/L ND 10.0 09/18/23 10:242.4
Chrysene ug/L ND 10.0 09/18/23 10:242.8
Di-n-butylphthalate ug/L ND 10.0 09/18/23 10:242.2
Di-n-octylphthalate ug/L ND 10.0 09/18/23 10:243.9
Dibenz(a,h)anthracene ug/L ND 10.0 09/18/23 10:243.0
Dibenzofuran ug/L ND 10.0 09/18/23 10:242.1
Diethylphthalate ug/L ND 10.0 09/18/23 10:242.0
Dimethylphthalate ug/L ND 10.0 09/18/23 10:242.1
Fluoranthene ug/L ND 10.0 09/18/23 10:242.2
Fluorene ug/L ND 10.0 09/18/23 10:242.1
Hexachloro-1,3-butadiene ug/L ND 10.0 09/18/23 10:241.8
Hexachlorobenzene ug/L ND 10.0 09/18/23 10:242.2
Hexachlorocyclopentadiene ug/L ND 10.0 09/18/23 10:241.6
Hexachloroethane ug/L ND 10.0 09/18/23 10:241.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/18/23 10:242.9
Isophorone ug/L ND 10.0 09/18/23 10:241.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/18/23 10:241.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/18/23 10:243.0
Naphthalene ug/L ND 10.0 09/18/23 10:242.1
Nitrobenzene ug/L ND 10.0 09/18/23 10:241.9
Pentachlorophenol ug/L ND 20.0 09/18/23 10:243.8
Phenanthrene ug/L ND 10.0 09/18/23 10:242.0
Phenol ug/L ND 10.0 09/18/23 10:241.4
Pyrene ug/L ND 10.0 09/18/23 10:242.2
2,4,6-Tribromophenol (S)%115 10-164 09/18/23 10:24
2-Fluorobiphenyl (S)%102 10-130 09/18/23 10:24
2-Fluorophenol (S)%80 10-130 09/18/23 10:24
Nitrobenzene-d5 (S)%107 10-138 09/18/23 10:24
Phenol-d6 (S)%58 10-130 09/18/23 10:24
Terphenyl-d14 (S)%141 19-191 09/18/23 10:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4143341LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 35.250 70 21-135
2,4,5-Trichlorophenol ug/L 46.750 93 38-147
2,4,6-Trichlorophenol ug/L 43.750 87 34-142
2,4-Dichlorophenol ug/L 41.750 83 36-136
2,4-Dimethylphenol ug/L 40.650 81 38-134
2,4-Dinitrophenol ug/L 185250 74 10-169
2,4-Dinitrotoluene ug/L 45.050 90 44-154
2,6-Dinitrotoluene ug/L 47.650 95 44-156
2-Chloronaphthalene ug/L 39.250 78 25-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4143341LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 41.950 84 29-130
2-Methylnaphthalene ug/L 37.550 75 23-130
2-Methylphenol(o-Cresol)ug/L 35.250 70 31-130
2-Nitroaniline ug/L 88.7100 89 39-145
2-Nitrophenol ug/L 44.650 89 29-142
3&4-Methylphenol(m&p Cresol)ug/L 37.750 75 30-130
3,3'-Dichlorobenzidine ug/L 102100 102 44-158
3-Nitroaniline ug/L 95.4100 95 45-152
4,6-Dinitro-2-methylphenol ug/L 80.9100 81 39-158
4-Bromophenylphenyl ether ug/L 44.750 89 47-147
4-Chloro-3-methylphenol ug/L 77.5100 78 40-138
4-Chloroaniline ug/L 84.2100 84 35-130
4-Chlorophenylphenyl ether ug/L 44.550 89 36-139
4-Nitroaniline ug/L 95.3100 95 46-157
4-Nitrophenol ug/L 122250 49 17-130
Acenaphthene ug/L 41.350 83 34-135
Acenaphthylene ug/L 42.050 84 35-137
Acetophenone ug/L 38.750 77 30-137
Anthracene ug/L 41.650 83 47-146
Atrazine ug/L 41.650 83 30-130
Benzaldehyde ug/L 44.250 88 17-167
Benzo(a)anthracene ug/L 44.750 89 48-160
Benzo(a)pyrene ug/L 45.050 90 47-165
Benzo(b)fluoranthene ug/L 50.750 101 49-171
Benzo(g,h,i)perylene ug/L 42.250 84 46-166
Benzo(k)fluoranthene ug/L 45.450 91 55-162
Biphenyl (Diphenyl)ug/L 39.650 79 28-130
bis(2-Chloroethoxy)methane ug/L 38.350 77 33-136
bis(2-Chloroethyl) ether ug/L 37.950 76 30-142
bis(2-Ethylhexyl)phthalate ug/L 51.250 102 46-173
Butylbenzylphthalate ug/L 50.450 101 53-169
Caprolactam ug/L 24.550 49 13-130
Carbazole ug/L 43.950 88 48-157
Chrysene ug/L 42.950 86 54-152
Di-n-butylphthalate ug/L 45.250 90 49-161
Di-n-octylphthalate ug/L 50.950 102 50-166
Dibenz(a,h)anthracene ug/L 41.850 84 46-166
Dibenzofuran ug/L 40.850 82 37-136
Diethylphthalate ug/L 44.550 89 45-149
Dimethylphthalate ug/L 43.950 88 43-145
Fluoranthene ug/L 43.150 86 50-153
Fluorene ug/L 42.850 86 42-142
Hexachloro-1,3-butadiene ug/L 28.050 56 10-130
Hexachlorobenzene ug/L 42.250 84 44-138
Hexachlorocyclopentadiene ug/L 33.850 68 10-130
Hexachloroethane ug/L 24.650 49 10-130
Indeno(1,2,3-cd)pyrene ug/L 41.450 83 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4143341LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 38.650 77 36-135
N-Nitroso-di-n-propylamine ug/L 40.350 81 33-140
N-Nitrosodiphenylamine ug/L 43.750 87 46-144
Naphthalene ug/L 34.250 68 20-130
Nitrobenzene ug/L 37.750 75 33-133
Pentachlorophenol ug/L 74.4100 74 21-163
Phenanthrene ug/L 41.950 84 47-146
Phenol ug/L 24.350 49 19-130
Pyrene ug/L 43.850 88 53-155
2,4,6-Tribromophenol (S)%122 10-164
2-Fluorobiphenyl (S)%97 10-130
2-Fluorophenol (S)%77 10-130
Nitrobenzene-d5 (S)%97 10-138
Phenol-d6 (S)%60 10-130
Terphenyl-d14 (S)%106 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4143342MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687716002
4143343
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-chloropropane)ug/L R1503011-14344 37 3050ND15.1 22.0
2,4,5-Trichlorophenol ug/L R1504010-17062 44 3050ND19.8 31.0
2,4,6-Trichlorophenol ug/L R1503610-16652 36 3050ND17.9 25.9
2,4-Dichlorophenol ug/L R1503310-15348 39 3050ND16.3 24.1
2,4-Dimethylphenol ug/L R1503320-14748 38 3050ND16.4 24.2
2,4-Dinitrophenol ug/L 250 43 10-17254 24 30250ND106 135
2,4-Dinitrotoluene ug/L 50 62 30-16472 15 3050ND30.9 35.9
2,6-Dinitrotoluene ug/L 50 48 31-16363 27 3050ND24.1 31.6
2-Chloronaphthalene ug/L R1503115-13446 37 3050ND15.7 22.8
2-Chlorophenol ug/L R1503810-13953 34 3050ND18.9 26.5
2-Methylnaphthalene ug/L R1502612-13043 49 3050ND13.1 21.5
2-Methylphenol(o-Cresol) ug/L R1503219-13247 37 3050ND16.2 23.6
2-Nitroaniline ug/L R11003923-15458 40 30100ND38.9 58.2
2-Nitrophenol ug/L R1503610-15958 47 3050ND18.0 28.93&4-Methylphenol(m&pCresol)ug/L R1503313-13647 37 3050ND16.3 23.6
3,3'-Dichlorobenzidine ug/L 100 81 10-17888 9 30100ND81.1 88.4
3-Nitroaniline ug/L 100 58 20-16674 25 30100ND58.0 74.3
4,6-Dinitro-2-methylphenol ug/L 100 57 10-18775 27 30100ND57.4 75.4
4-Bromophenylphenyl ether ug/L 50 45 31-15760 28 3050ND22.5 29.8
4-Chloro-3-methylphenol ug/L R11003027-14647 42 30100ND30.5 46.9
4-Chloroaniline ug/L R11003313-14351 43 30100ND32.8 50.8
4-Chlorophenylphenyl ether ug/L 50 38 23-14951 30 3050ND18.9 25.5
4-Nitroaniline ug/L 100 77 24-17189 15 30100ND77.0 89.4
4-Nitrophenol ug/L 250 38 10-13046 18 30250ND95.9 115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4143342MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687716002
4143343
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L R1503421-14748 35 3050ND16.9 24.1
Acenaphthylene ug/L R1503419-15048 34 3050ND17.1 24.2
Acetophenone ug/L R1503522-14549 33 3050ND17.4 24.3
Anthracene ug/L 50 57 36-15268 17 3050ND28.7 34.1
Atrazine ug/L R1506218-17389 36 3050ND30.8 44.3
Benzaldehyde ug/L R1503516-16355 45 3050ND17.5 27.7
Benzo(a)anthracene ug/L 50 75 42-16381 8 3050ND37.4 40.6
Benzo(a)pyrene ug/L 50 79 40-16989 12 3050ND39.3 44.5
Benzo(b)fluoranthene ug/L 50 88 40-17791 3 3050ND43.9 45.4
Benzo(g,h,i)perylene ug/L 50 75 38-17481 9 3050ND37.3 40.6
Benzo(k)fluoranthene ug/L 50 81 41-17198 19 3050ND40.5 48.9
Biphenyl (Diphenyl)ug/L R1503214-13747 39 3050ND15.8 23.4
bis(2-Chloroethoxy)methane ug/L R1503019-14648 45 3050ND15.1 24.0
bis(2-Chloroethyl) ether ug/L R1503419-15151 40 3050ND17.0 25.4
bis(2-Ethylhexyl)phthalate ug/L 50 85 42-16884 1 3050ND42.3 42.1
Butylbenzylphthalate ug/L 50 83 42-17789 6 3050ND41.6 44.3
Caprolactam ug/L 50 33 10-13044 29 3050ND16.4 22.0
Carbazole ug/L 50 73 38-16484 14 3050ND36.5 42.0
Chrysene ug/L 50 73 43-15987 17 3050ND36.7 43.7
Di-n-butylphthalate ug/L 50 76 42-16082 8 3050ND37.9 40.9
Di-n-octylphthalate ug/L 50 85 42-17184 2 3050ND42.7 42.1
Dibenz(a,h)anthracene ug/L 50 74 40-17177 4 3050ND37.0 38.6
Dibenzofuran ug/L R1503523-14748 31 3050ND17.6 24.2
Diethylphthalate ug/L 50 61 33-15767 10 3050ND30.4 33.6
Dimethylphthalate ug/L 50 46 27-15457 22 3050ND23.0 28.5
Fluoranthene ug/L 50 72 42-15780 10 3050ND36.0 39.8
Fluorene ug/L R1503825-15552 31 3050ND19.1 26.0
Hexachloro-1,3-butadiene ug/L R1502110-13030 34 3050ND10.7 15.1
Hexachlorobenzene ug/L 50 47 32-14559 22 3050ND23.6 29.6
Hexachlorocyclopentadiene ug/L R1502310-13039 53 3050ND11.5 19.6
Hexachloroethane ug/L 50 20 10-13025 21 3050ND10.2 12.7
Indeno(1,2,3-cd)pyrene ug/L 50 72 39-17479 10 3050ND35.9 39.5
Isophorone ug/L R1503119-14650 46 3050ND15.5 24.8
N-Nitroso-di-n-propylamine ug/L R1503520-15053 41 3050ND17.6 26.5
N-Nitrosodiphenylamine ug/L 50 50 33-14966 28 3050ND24.9 33.1
Naphthalene ug/L R1502410-12838 44 3050ND12.2 19.2
Nitrobenzene ug/L R1503119-14547 41 3050ND15.5 23.6
Pentachlorophenol ug/L 100 57 10-18868 17 30100ND57.1 68.0
Phenanthrene ug/L 50 58 38-15068 16 3050ND29.1 34.0
Phenol ug/L R1502210-13034 43 3050ND11.1 17.2
Pyrene ug/L 50 73 42-16385 15 3050ND36.5 42.4
2,4,6-Tribromophenol (S) %69 10-16490
2-Fluorobiphenyl (S)%43 10-13060
2-Fluorophenol (S)%34 10-13055
Nitrobenzene-d5 (S)%39 10-13865
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4143342MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687716002
4143343
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%27 10-13043
Terphenyl-d14 (S)%89 19-19199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800267
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4144892
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/18/23 13:515.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4144893LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.150 102 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4144894LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 52.950 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4144895MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687758002
4144896
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 99 80-12099 0 255038.2 87.5 87.8
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4144897MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687758004
4144898
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 102 80-120103 0 255092.6 143 144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
799850
SM 4500-S2D-2011
SM 4500-S2D-2011
4500S2D Sulfide Water
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4143148
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
Sulfide mg/L ND 0.10 09/15/23 05:020.022
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4143149LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide mg/L 0.530.5 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4143150MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687636005
4143151
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 97 80-12098 1 100.5ND 0.50 0.50
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4143169MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687839001
4143170
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 101 80-120100 1 100.5ND 0.52 0.52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
799601
EPA 9056A
EPA 9056A
9056 IC anions 28 Days
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92687719001, 92687719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4141634
Associated Lab Samples:92687719001, 92687719002
Matrix: Water
AnalyzedMDL
Chloride mg/L ND 1.0 09/15/23 05:510.60
Sulfate mg/L ND 1.0 09/15/23 05:510.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4141635LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 50.350 101 90-110
Sulfate mg/L 50.650 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4141636MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687719001
4141637
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L 50 93 90-11090 2 105050.6 97.2 95.8
Sulfate mg/L M1507490-11064 1 1050490527 522
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 61
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result shouldbe considered an estimated value.IK
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in theassociated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 61
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92687719
PACTIV EVERGREEN GROUNDWATER S
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92687719001 799717RW03W6-091223 SM 2120B-2011
92687719002 799717RW02W6-091223 SM 2120B-2011
92687719001 802282 802461RW03W6-091223 EPA 3010A EPA 6010D
92687719002 802282 802461RW02W6-091223 EPA 3010A EPA 6010D
92687719001 802409 802569RW03W6-091223 EPA 3010A EPA 6010D
92687719002 802409 802569RW02W6-091223 EPA 3010A EPA 6010D
92687719001 954517 954723RW03W6-091223 EPA 7470 EPA 7470
92687719002 954517 954723RW02W6-091223 EPA 7470 EPA 7470
92687719001 954441 954514RW03W6-091223 EPA 7470 EPA 7470
92687719002 954441 954514RW02W6-091223 EPA 7470 EPA 7470
92687719001 799912 800116RW03W6-091223 EPA 3510C EPA 8270E
92687719002 799912 800116RW02W6-091223 EPA 3510C EPA 8270E
92687719001 800298RW03W6-091223 EPA 8260D
92687719002 800298RW02W6-091223 EPA 8260D
92687719003 799716TRIP BLANK EPA 8260D
92687719001 800267RW03W6-091223 SM 2320B-2011
92687719002 800267RW02W6-091223 SM 2320B-2011
92687719001 799850RW03W6-091223 SM 4500-S2D-2011
92687719002 799850RW02W6-091223 SM 4500-S2D-2011
92687719001 799601RW03W6-091223 EPA 9056A
92687719002 799601RW02W6-091223 EPA 9056A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 61
Page 44 of 61
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Thisreportshouldnotbereproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamplesincludedinthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
Client - Charlotte
PACE Charlotte
9800 Kincey Ave.
Huntersville NC 28078
REPORT OF
LABORATORY
ANALYSIS FOR
PCDD/PCDF
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
October 6, 2023
Pace Project #: 10669205
Sample Receipt Date: 09/19/2023
Client Project #: 92687719 ENSAFE Inc.
Client Sub PO #: N/A
The report provided has been invoiced as a Level 2
PCDD/PCDF Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questionstoIsaac Johnson,your Pace
Project Manager.
State Cert #: 530
Suite 100
Report Prepared for:
Page 1 of 13Report No.....10669205_SW8290AFC_L2_dfr
October 06, 2023
Isaac Johnson, Project Manager
[phone]
[phone] (fax)
[e-mail]
Page 49 of 61
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
This report presents the results from the analyses performed on two samples submitted by a
representative of Pace Analytical Services, LLC. The samples were analyzed for the presence or absence
of polychlorodibenzo-p-dioxins (PCDDs) and polychlorodibenzofurans (PCDFs) using a modified version
of USEPA Method 8290A. The estimated detection limits (EDLs) were based on signal-to-noise
measurements. Estimated maximum possible concentration (EMPC) values were treated as positives inthe toxic equivalence calculations.
The isotopically-labeled PCDD/PCDF internal standards in the sample extracts were recovered at26-60%. Except for ten low values, which were flagged "R" on the results tables, the labeled internalstandard recoveries obtained for this project were within the 40-135% target range specified in Method8290A. Since the quantification of the native 2,3,7,8-substituted congeners was based on isotope dilution,the data were automatically corrected for recovery and accurate values were obtained.
Values were flagged "I" where incorrect isotope ratios were obtained. Concentrations below the calibrationrange were flagged "J" and should be regarded as estimates.
A laboratory method blank was prepared and analyzed with the sample batch as part of our routine quality
control procedures. The results show the blank to contain trace levels of one or more selected congeners.
These levels were below the calibration range of the method. Sample concentrations similar to the
corresponding blank levels were flagged "B" on the results tables and may be, at least partially, attributed
to the background.
A laboratory spike sample was also prepared with the sample batch using clean reference matrix that had
been fortified with native standard materials. The results show that the spiked native compounds were
recovered at 70-108%. These results were within the target range for the method. Matrix spikes were
prepared with the sample batch using sample material from a separate project; results from theseanalyses will be provided upon request.
DISCUSSION
Page 2 of 13Report No.....10669205_SW8290AFC_L2_dfr
Page 50 of 61
REPORT OF LABORATORY ANALYSIS
This report shallnot bereproduced,except in full,
withoutthe written consentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Report No.....10669611
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 13Report No.....10669205_SW8290AFC_L2_dfr
Page 51 of 61
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 4 of 13Report No.....10669205_SW8290AFC_L2_dfr
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10669205
Page 7 of 13Report No.....10669205_SW8290AFC_L2_dfr
Page 55 of 61
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
A =
B = C = D = E = H2 =
I =
J = L = Nn = P = R =
S =
U = V = X = Y = * =
Reporting Limit based on signal to noise (EDL)
Less than 10x higher than method blank level Result obtained from confirmation analysis Result obtained from analysis of diluted sample Exceeds calibration range Extracted outside of holding time
Isotope ratio out of specification
Estimated value Suppressive interference, analyte may be biased low Value obtained from additional analysis PCDE Interference Recovery outside target range
Peak saturated
Analyte not detected Result verified by confirmation analysis %D Exceeds limits Calculated using average of daily RFs See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 8 of 13Report No.....10669205_SW8290AFC_L2_dfr
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Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 9 of 13Report No.....10669205_SW8290AFC_L2_dfr
Page 57 of 61
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID RW03W6-09122392687719001L230924A_10BAL
NA939 mL
NAL230816L230924A_01 & L230924A_13BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/12/2023 15:1609/19/2023 08:5009/20/2023 12:0009/24/2023 22:03
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF 2.1 1.4 2,3,7,8-TCDF-13C 2.00 62J-----Total TCDF 6.9 1.4 2,3,7,8-TCDD-13C 2.00 52J-----1,2,3,7,8-PeCDF-13C 2.00 552,3,7,8-TCDD ND 2.0 2,3,4,7,8-PeCDF-13C 2.00 58-----Total TCDD ND 2.0 1,2,3,7,8-PeCDD-13C 2.00 58-----1,2,3,4,7,8-HxCDF-13C 2.00 39 R1,2,3,7,8-PeCDF 4.7 1.3 1,2,3,6,7,8-HxCDF-13C 2.00 49J-----2,3,4,7,8-PeCDF ND 0.88 2,3,4,6,7,8-HxCDF-13C 2.00 60-----Total PeCDF 4.7 0.88 1,2,3,7,8,9-HxCDF-13C 2.00 48J-----1,2,3,4,7,8-HxCDD-13C 2.00 521,2,3,7,8-PeCDD ND 1.0 1,2,3,6,7,8-HxCDD-13C 2.00 56-----Total PeCDD ND 1.0 1,2,3,4,6,7,8-HpCDF-13C 2.00 37-----R1,2,3,4,7,8,9-HpCDF-13C 2.00 26 R1,2,3,4,7,8-HxCDF -----1.8 1,2,3,4,6,7,8-HpCDD-13C 2.00 39IJ1.9 R1,2,3,6,7,8-HxCDF ND 1.5 OCDD-13C 4.00 37-----RY2,3,4,6,7,8-HxCDF ND 1.2-----1,2,3,7,8,9-HxCDF ND 1.7 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF 9.2 1.2 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD ND 3.5 2,3,7,8-TCDD-37Cl4 0.20 79-----1,2,3,6,7,8-HxCDD ND 3.2-----1,2,3,7,8,9-HxCDD ND 3.3-----Total HxCDD ND 3.2-----
1,2,3,4,6,7,8-HpCDF ND 2.5 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 6.1 Equivalence: 0.61 pg/L-----Total HpCDF ND 2.5 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----2.5 IJ5.0Total HpCDD 22 2.5 J-----
OCDF -----4.0 IJ4.6OCDD70 7.9 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelR=Recovery outside target rangeI=Isotope ratio out of specification
Y =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 10 of 13Report No.....10669205_SW8290AFC_L2_dfr
Page 58 of 61
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID RW02W6-09122392687719002L230924A_11BAL
NA252 mL
NAL230816L230924A_01 & L230924A_13BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/12/2023 14:5009/19/2023 08:5009/20/2023 12:0009/24/2023 22:47
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 3.4 2,3,7,8-TCDF-13C 2.00 57-----Total TCDF 26 3.4 2,3,7,8-TCDD-13C 2.00 50J-----1,2,3,7,8-PeCDF-13C 2.00 502,3,7,8-TCDD ND 3.2 2,3,4,7,8-PeCDF-13C 2.00 52-----Total TCDD ND 3.2 1,2,3,7,8-PeCDD-13C 2.00 53-----1,2,3,4,7,8-HxCDF-13C 2.00 36 R1,2,3,7,8-PeCDF -----4.4 1,2,3,6,7,8-HxCDF-13C 2.00 52IJ152,3,4,7,8-PeCDF ND 3.0 2,3,4,6,7,8-HxCDF-13C 2.00 51-----Total PeCDF ND 3.0 1,2,3,7,8,9-HxCDF-13C 2.00 43-----1,2,3,4,7,8-HxCDD-13C 2.00 451,2,3,7,8-PeCDD ND 4.1 1,2,3,6,7,8-HxCDD-13C 2.00 54-----Total PeCDD 22 4.1 1,2,3,4,6,7,8-HpCDF-13C 2.00 37J-----R1,2,3,4,7,8,9-HpCDF-13C 2.00 29 R1,2,3,4,7,8-HxCDF ND 5.5 1,2,3,4,6,7,8-HpCDD-13C 2.00 38-----R1,2,3,6,7,8-HxCDF ND 3.5 OCDD-13C 4.00 36-----RY2,3,4,6,7,8-HxCDF ND 3.3-----1,2,3,7,8,9-HxCDF ND 4.8 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF 10 3.3 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD -----4.0 2,3,7,8-TCDD-37Cl4 0.20 67IJ8.91,2,3,6,7,8-HxCDD ND 3.6-----1,2,3,7,8,9-HxCDD ND 3.7-----Total HxCDD 78 3.6 J-----
1,2,3,4,6,7,8-HpCDF 8.9 8.7 Total 2,3,7,8-TCDDBJ-----1,2,3,4,7,8,9-HpCDF ND 17 Equivalence: 2.4 pg/L-----Total HpCDF 28 8.7 (Lower-bound - Using 2005 WHO Factors)J-----
1,2,3,4,6,7,8-HpCDD 72 10 J-----Total HpCDD 620 10-----
OCDF 27 14 BJ-----OCDD 780 24-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelR=Recovery outside target rangeI=Isotope ratio out of specification
Y =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 11 of 13Report No.....10669205_SW8290AFC_L2_dfr
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REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
BLANK-108427L230922B_09
AH5
983 mLL230816L230922B_01 & L230922B_18
MatrixDilutionExtractedAnalyzed
Water
09/20/2023 12:0009/22/2023 21:05
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKOY
NativeIsomers pg/LConc EMPCpg/L pg/L InternalStandards Addedng's PercentRecoveryEDL
2,3,7,8-TCDF -----0.67 0.54 IJ 2,3,7,8-TCDF-13C 2.00 97Total TCDF ND -----0.54 2,3,7,8-TCDD-13C 2.00 901,2,3,7,8-PeCDF-13C 2.00 962,3,7,8-TCDD ND -----0.74 2,3,4,7,8-PeCDF-13C 2.00 91Total TCDD ND -----0.74 1,2,3,7,8-PeCDD-13C 2.00 1081,2,3,4,7,8-HxCDF-13C 2.00 791,2,3,7,8-PeCDF -----1.1 0.54 IJ 1,2,3,6,7,8-HxCDF-13C 2.00 1062,3,4,7,8-PeCDF -----0.72 0.40 IJ 2,3,4,6,7,8-HxCDF-13C 2.00 110Total PeCDF ND -----0.40 1,2,3,7,8,9-HxCDF-13C 2.00 1031,2,3,4,7,8-HxCDD-13C 2.00 1011,2,3,7,8-PeCDD 0.93 -----0.35 J 1,2,3,6,7,8-HxCDD-13C 2.00 114Total PeCDD 0.93 -----0.35 J 1,2,3,4,6,7,8-HpCDF-13C 2.00 901,2,3,4,7,8,9-HpCDF-13C 2.00 801,2,3,4,7,8-HxCDF 1.1 -----0.33 J 1,2,3,4,6,7,8-HpCDD-13C 2.00 1061,2,3,6,7,8-HxCDF -----0.73 0.23 IJ OCDD-13C 4.00 842,3,4,6,7,8-HxCDF -----0.49 0.22 IJ1,2,3,7,8,9-HxCDF 1.7 -----0.29 J 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF 2.7 -----0.22 J 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 2.9 -----0.55 J 2,3,7,8-TCDD-37Cl4 0.20 991,2,3,6,7,8-HxCDD -----0.73 0.50 IJ1,2,3,7,8,9-HxCDD -----1.1 0.51 IJTotal HxCDD 2.9 -----0.50 J
1,2,3,4,6,7,8-HpCDF 1.4 -----0.80 J Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----1.5 Equivalence: 2.1 pg/LTotal HpCDF 1.4 -----0.80 J (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD 1.7 -----0.83 JTotal HpCDD 1.7 -----0.83 J
OCDF 2.9 -----1.5 JOCDD12-----1.9 J
Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
I =Isotope ratio out of specification
EDL=EstimatedDetection Limit
Page 12 of 13Report No.....10669205_SW8290AFC_L2_dfr
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REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCS-108428L230922B_02
AH5
947 mLL230816L230922B_01 & L230922B_18
MatrixDilutionExtractedAnalyzed
Water
09/20/2023 12:0009/22/2023 16:00
NA
Method Blank ID BLANK-108427
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.21 2,3,7,8-TCDF-13C 2.0 81103Total TCDF 2,3,7,8-TCDD-13C 2.0 711,2,3,7,8-PeCDF-13C 2.0 852,3,7,8-TCDD 0.20 0.22 2,3,4,7,8-PeCDF-13C 2.0 78108Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 951,2,3,4,7,8-HxCDF-13C 2.0 781,2,3,7,8-PeCDF 1.0 0.95 1,2,3,6,7,8-HxCDF-13C 2.0 87952,3,4,7,8-PeCDF 1.0 0.99 2,3,4,6,7,8-HxCDF-13C 2.0 8599Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 861,2,3,4,7,8-HxCDD-13C 2.0 821,2,3,7,8-PeCDD 1.0 0.97 1,2,3,6,7,8-HxCDD-13C 2.0 8797Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 841,2,3,4,7,8,9-HpCDF-13C 2.0 761,2,3,4,7,8-HxCDF 1.0 0.92 1,2,3,4,6,7,8-HpCDD-13C 2.0 94921,2,3,6,7,8-HxCDF 1.0 0.98 OCDD-13C 4.0 79982,3,4,6,7,8-HxCDF 1.0 0.99 991,2,3,7,8,9-HxCDF 1.0 0.98 1,2,3,4-TCDD-13C 2.0 NA98Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.1 2,3,7,8-TCDD-37Cl4 0.20 771051,2,3,6,7,8-HxCDD 1.0 0.98 981,2,3,7,8,9-HxCDD 1.0 1.1 107Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.90 901,2,3,4,7,8,9-HpCDF 1.0 0.95 95Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.81 81Total HpCDD
OCDF 2.0 1.5 73OCDD2.0 1.4 70
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 13 of 13Report No.....10669205_SW8290AFC_L2_dfr
Page 61 of 61
#=CL#
October 31, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92688066
92688066
Project:
Pace Project No.:
RE:
Christina AshdownENSAFE313 Wingo WayMount Pleasant, SC 29464
Pactiv Evergreen GWS
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on September 14, 2023. The results relate onlyto the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and thelaboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc: Jennings Kerr, ENSAFE Inc.
Lab, ENSAFE Inc.
David Warren, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 116
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
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Pace Analytical Services Charlotte
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REPORT OF LABORATORY ANALYSIS
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[phone]
Page 2 of 116
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Lab ID Sample ID Matrix Date Collected Date Received
92688066001 RW04 WG- 091323 Water 09/13/23 09:50 09/14/23 07:53
92688066002 RW06 WG- 091323 Water 09/13/23 10:29 09/14/23 07:53
92688066003 RW07 WG- 091323 Water 09/13/23 12:27 09/14/23 07:53
92688066004 PZ01 WG- 091323 Water 09/13/23 12:54 09/14/23 07:53
92688066005 PZ05 WG- 091323 Water 09/13/23 14:46 09/14/23 07:53
92688066006 PZ03 WG- 091323 Water 09/13/23 15:27 09/14/23 07:53
92688066007 PZ17 WG- 091323 Water 09/13/23 16:56 09/14/23 07:53
92688066008 PZ17 HG- 091323 Water 09/13/23 16:58 09/14/23 07:53
92688066009 BR02 WG- 091323 Water 09/13/23 16:58 09/14/23 07:53
92688066010 Trip Blank Water 09/13/23 09:00 09/14/23 07:53
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 116
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92688066001 RW04 WG- 091323 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAAM1
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688066002 RW06 WG- 091323 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688066003 RW07 WG- 091323 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688066004 PZ01 WG- 091323 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAME, KC2
EPA 6010 17 PASI-OAAM1, KC2
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 116
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688066005 PZ05 WG- 091323 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688066006 PZ03 WG- 091323 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAAM1, KC2
EPA 6010 17 PASI-OAAM1, KC2
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688066007 PZ17 WG- 091323 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAAM1, AME
EPA 6010 17 PASI-OAAM1, KC2
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688066008 PZ17 HG- 091323 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAAM1, AME
EPA 6010 17 PASI-OAAM1, KC2
EPA 7470 1 PASI-OJNK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 116
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688066009 BR02 WG- 091323 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAME
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
92688066010 Trip Blank EPA 8260D 52 PASI-CTMH
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW04 WG- 091323 Lab ID: 92688066001 Collected: 09/13/23 09:50 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 10.2 Std. Units 09/15/23 10:24 H350
True Color 1500 units 09/15/23 10:24 H3250 250 50
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/05/23 17:45 7440-36-010/02/23 09:4615.0 5.5 1
Arsenic 30.3 ug/L 10/05/23 17:45 7440-38-210/02/23 09:4610.0 3.4 1
Barium 152 ug/L 10/05/23 17:45 7440-39-310/02/23 09:4610.0 0.84 1
Beryllium 0.66J ug/L 10/05/23 17:45 7440-41-710/02/23 09:464.0 0.17 1
Boron 395 ug/L 10/05/23 17:45 7440-42-810/02/23 09:4650.0 12.4 1
Cadmium ND ug/L 10/05/23 17:45 7440-43-910/02/23 09:461.0 0.33 1
Chromium 49.9 ug/L 10/05/23 17:45 7440-47-310/02/23 09:465.0 1.7 1
Cobalt 3.7J ug/L 10/05/23 17:45 7440-48-410/02/23 09:4610.0 0.96 1
Copper 4.0J ug/L 10/05/23 17:45 7440-50-810/02/23 09:465.0 2.6 1
Lead ND ug/L 10/05/23 17:45 7439-92-110/02/23 09:4610.0 2.1 1
Manganese 161 ug/L 10/05/23 17:45 7439-96-510/02/23 09:465.0 1.1 1
Nickel 19.9 ug/L 10/05/23 17:45 7440-02-010/02/23 09:465.0 1.0 1
Selenium ND ug/L 10/05/23 17:45 7782-49-210/02/23 09:4615.0 3.9 1
Silver ND ug/L 10/05/23 17:45 7440-22-410/02/23 09:465.0 1.0 1
Thallium ND ug/L 10/05/23 17:45 7440-28-010/02/23 09:4615.0 2.9 1
Vanadium 493 ug/L 10/05/23 17:45 7440-62-210/02/23 09:4610.0 1.0 1
Zinc 41.3 ug/L 10/05/23 17:45 7440-66-610/02/23 09:4620.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/05/23 14:20 7440-36-010/03/23 06:0415.0 5.5 1
Arsenic, Dissolved 29.6 ug/L 10/05/23 14:20 7440-38-210/03/23 06:0410.0 3.4 1
Barium, Dissolved 76.8 ug/L 10/05/23 14:20 7440-39-310/03/23 06:0410.0 0.84 1
Beryllium, Dissolved 0.27J ug/L 10/05/23 14:20 7440-41-710/03/23 06:044.0 0.17 1
Boron, Dissolved 383 ug/L 10/05/23 14:20 7440-42-810/03/23 06:0450.0 12.4 1
Cadmium, Dissolved ND ug/L 10/05/23 14:20 7440-43-910/03/23 06:041.0 0.33 1
Chromium, Dissolved 33.4 ug/L 10/05/23 14:20 7440-47-310/03/23 06:045.0 1.7 1
Cobalt, Dissolved 1.7J ug/L 10/05/23 14:20 7440-48-410/03/23 06:0410.0 0.96 1
Copper, Dissolved ND ug/L 10/05/23 14:20 7440-50-810/03/23 06:045.0 2.6 1
Lead, Dissolved ND ug/L 10/05/23 14:20 7439-92-110/03/23 06:0410.0 2.1 1
Manganese, Dissolved 72.5 ug/L 10/05/23 14:20 7439-96-510/03/23 06:045.0 1.1 1
Nickel, Dissolved 13.9 ug/L 10/05/23 14:20 7440-02-010/03/23 06:045.0 1.0 1
Selenium, Dissolved ND ug/L 10/05/23 14:20 7782-49-210/03/23 06:0415.0 3.9 1
Silver, Dissolved ND ug/L 10/05/23 14:20 7440-22-410/03/23 06:045.0 1.0 1
Thallium, Dissolved ND ug/L 10/05/23 14:20 7440-28-010/03/23 06:0415.0 2.9 1
Vanadium, Dissolved 322 ug/L 10/05/23 14:20 7440-62-210/03/23 06:0410.0 1.0 1
Zinc, Dissolved ND ug/L 10/05/23 14:20 7440-66-610/03/23 06:0420.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW04 WG- 091323 Lab ID: 92688066001 Collected: 09/13/23 09:50 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 09:46 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:22 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene 19.2 ug/L 09/20/23 17:46 83-32-909/19/23 10:3110.0 2.0 1
Acenaphthylene ND ug/L 09/20/23 17:46 208-96-809/19/23 10:3110.0 2.0 1
Acetophenone ND ug/L 09/20/23 17:46 98-86-209/19/23 10:3110.0 1.5 1
Anthracene ND ug/L 09/20/23 17:46 120-12-709/19/23 10:3110.0 2.3 1
Atrazine ND ug/L 09/20/23 17:46 1912-24-909/19/23 10:3110.0 3.2 1
Benzaldehyde ND ug/L 09/20/23 17:46 100-52-709/19/23 10:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/20/23 17:46 56-55-309/19/23 10:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/20/23 17:46 50-32-809/19/23 10:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/20/23 17:46 205-99-209/19/23 10:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/20/23 17:46 191-24-209/19/23 10:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/20/23 17:46 207-08-909/19/23 10:3110.0 2.7 1
Biphenyl (Diphenyl)3.4J ug/L 09/20/23 17:46 92-52-409/19/23 10:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/20/23 17:46 101-55-309/19/23 10:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/20/23 17:46 85-68-709/19/23 10:3110.0 3.1 1
Caprolactam ND ug/L 09/20/23 17:46 105-60-209/19/23 10:3110.0 6.9 1
Carbazole 11.0 ug/L 09/20/23 17:46 86-74-809/19/23 10:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/20/23 17:46 59-50-709/19/23 10:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/20/23 17:46 106-47-809/19/23 10:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/20/23 17:46 111-91-109/19/23 10:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/20/23 17:46 111-44-409/19/23 10:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/20/23 17:46 91-58-709/19/23 10:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/20/23 17:46 95-57-809/19/23 10:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/20/23 17:46 7005-72-309/19/23 10:3110.0 2.0 1
Chrysene ND ug/L 09/20/23 17:46 218-01-909/19/23 10:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/20/23 17:46 53-70-309/19/23 10:3110.0 3.0 1
Dibenzofuran 10.4 ug/L 09/20/23 17:46 132-64-909/19/23 10:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/20/23 17:46 91-94-109/19/23 10:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/20/23 17:46 120-83-209/19/23 10:3110.0 1.4 1
Diethylphthalate ND ug/L 09/20/23 17:46 84-66-209/19/23 10:3110.0 2.0 1
2,4-Dimethylphenol 2.2J ug/L 09/20/23 17:46 105-67-909/19/23 10:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/20/23 17:46 131-11-309/19/23 10:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/20/23 17:46 84-74-209/19/23 10:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/20/23 17:46 534-52-109/19/23 10:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/20/23 17:46 51-28-509/19/23 10:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/20/23 17:46 121-14-209/19/23 10:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/20/23 17:46 606-20-209/19/23 10:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/20/23 17:46 117-84-009/19/23 10:3110.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW04 WG- 091323 Lab ID: 92688066001 Collected: 09/13/23 09:50 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/20/23 17:46 117-81-709/19/23 10:316.0 3.7 1
Fluoranthene 5.8J ug/L 09/20/23 17:46 206-44-009/19/23 10:3110.0 2.2 1
Fluorene 10.8 ug/L 09/20/23 17:46 86-73-709/19/23 10:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/20/23 17:46 87-68-309/19/23 10:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/20/23 17:46 118-74-109/19/23 10:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/20/23 17:46 77-47-409/19/23 10:3110.0 1.6 1
Hexachloroethane ND ug/L 09/20/23 17:46 67-72-109/19/23 10:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/20/23 17:46 193-39-509/19/23 10:3110.0 2.9 1
Isophorone ND ug/L 09/20/23 17:46 78-59-109/19/23 10:3110.0 1.7 1
2-Methylnaphthalene 18.5 ug/L 09/20/23 17:46 91-57-609/19/23 10:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/20/23 17:46 95-48-709/19/23 10:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/20/23 17:46 15831-10-409/19/23 10:3110.0 1.2 1
Naphthalene 130 ug/L 09/20/23 17:46 91-20-309/19/23 10:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/20/23 17:46 88-74-409/19/23 10:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/20/23 17:46 99-09-209/19/23 10:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/20/23 17:46 100-01-609/19/23 10:3120.0 5.1 1
Nitrobenzene ND ug/L 09/20/23 17:46 98-95-309/19/23 10:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/20/23 17:46 88-75-509/19/23 10:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/20/23 17:46 100-02-709/19/23 10:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/20/23 17:46 621-64-709/19/23 10:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/20/23 17:46 86-30-609/19/23 10:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/20/23 17:46 108-60-109/19/23 10:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/20/23 17:46 87-86-509/19/23 10:3120.0 3.8 1
Phenanthrene 20.6 ug/L 09/20/23 17:46 85-01-809/19/23 10:3110.0 2.0 1
Phenol ND ug/L 09/20/23 17:46 108-95-209/19/23 10:3110.0 1.4 1
Pyrene 3.7J ug/L 09/20/23 17:46 129-00-009/19/23 10:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/20/23 17:46 95-95-409/19/23 10:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/20/23 17:46 88-06-209/19/23 10:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)77 %09/20/23 17:46 4165-60-009/19/23 10:3110-138 1
2-Fluorobiphenyl (S)79 %09/20/23 17:46 321-60-809/19/23 10:3110-130 1
Terphenyl-d14 (S)102 %09/20/23 17:46 1718-51-009/19/23 10:3119-191 1
Phenol-d6 (S)49 %09/20/23 17:46 13127-88-309/19/23 10:3110-130 1
2-Fluorophenol (S)63 %09/20/23 17:46 367-12-409/19/23 10:3110-130 1
2,4,6-Tribromophenol (S)98 %09/20/23 17:46 118-79-609/19/23 10:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/24/23 22:46 67-64-150.0 10.2 2
Benzene 1.3J ug/L 09/24/23 22:46 71-43-22.0 0.69 2
Bromodichloromethane ND ug/L 09/24/23 22:46 75-27-42.0 0.61 2
Bromoform ND ug/L 09/24/23 22:46 75-25-22.0 0.68 2
Bromomethane ND ug/L 09/24/23 22:46 74-83-94.0 3.3 2
2-Butanone (MEK)ND ug/L 09/24/23 22:46 78-93-310.0 7.9 2
Carbon disulfide ND ug/L 09/24/23 22:46 75-15-04.0 0.71 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW04 WG- 091323 Lab ID: 92688066001 Collected: 09/13/23 09:50 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/24/23 22:46 56-23-52.0 0.67 2
Chlorobenzene 3.2 ug/L 09/24/23 22:46 108-90-72.0 0.57 2
Chloroethane ND ug/L 09/24/23 22:46 75-00-32.0 1.3 2
Chloroform ND ug/L 09/24/23 22:46 67-66-32.0 0.86 2
Chloromethane ND ug/L 09/24/23 22:46 74-87-32.0 1.1 2
Cyclohexane ND ug/L 09/24/23 22:46 110-82-72.0 0.71 2
1,2-Dibromo-3-chloropropane ND ug/L 09/24/23 22:46 96-12-84.0 0.68 2
Dibromochloromethane ND ug/L 09/24/23 22:46 124-48-12.0 0.72 2
1,2-Dibromoethane (EDB)ND ug/L 09/24/23 22:46 106-93-42.0 0.54 2
1,2-Dichlorobenzene 3.1 ug/L 09/24/23 22:46 95-50-12.0 0.68 2
1,3-Dichlorobenzene 9.0 ug/L 09/24/23 22:46 541-73-12.0 0.68 2
1,4-Dichlorobenzene 3.1 ug/L 09/24/23 22:46 106-46-72.0 0.67 2
Dichlorodifluoromethane ND ug/L 09/24/23 22:46 75-71-82.0 0.69 2
1,1-Dichloroethane ND ug/L 09/24/23 22:46 75-34-32.0 0.73 2
1,2-Dichloroethane ND ug/L 09/24/23 22:46 107-06-22.0 0.64 2
1,1-Dichloroethene ND ug/L 09/24/23 22:46 75-35-42.0 0.70 2
cis-1,2-Dichloroethene ND ug/L 09/24/23 22:46 156-59-22.0 0.77 2
trans-1,2-Dichloroethene ND ug/L 09/24/23 22:46 156-60-52.0 0.79 2
1,2-Dichloropropane ND ug/L 09/24/23 22:46 78-87-52.0 0.71 2
cis-1,3-Dichloropropene ND ug/L 09/24/23 22:46 10061-01-52.0 0.73 2
trans-1,3-Dichloropropene ND ug/L 09/24/23 22:46 10061-02-62.0 0.73 2
Ethylbenzene 3.5 ug/L 09/24/23 22:46 100-41-42.0 0.61 2
2-Hexanone ND ug/L 09/24/23 22:46 591-78-610.0 0.95 2
Isopropylbenzene (Cumene)ND ug/L 09/24/23 22:46 98-82-82.0 0.67 2
Methyl acetate ND ug/L 09/24/23 22:46 79-20-920.0 4.8 2
Methylcyclohexane ND ug/L 09/24/23 22:46 108-87-220.0 3.0 2
Methylene Chloride ND ug/L 09/24/23 22:46 75-09-210.0 3.9 2
4-Methyl-2-pentanone (MIBK)ND ug/L 09/24/23 22:46 108-10-110.0 5.4 2
Methyl-tert-butyl ether ND ug/L 09/24/23 22:46 1634-04-42.0 0.84 2
Styrene ND ug/L 09/24/23 22:46 100-42-52.0 0.58 2
1,1,2,2-Tetrachloroethane ND ug/L 09/24/23 22:46 79-34-52.0 0.45 2
Tetrachloroethene ND ug/L 09/24/23 22:46 127-18-42.0 0.58 2
Toluene ND ug/L 09/24/23 22:46 108-88-32.0 0.48 2
1,2,4-Trichlorobenzene 7.6 ug/L 09/24/23 22:46 120-82-12.0 1.3 2
1,1,1-Trichloroethane ND ug/L 09/24/23 22:46 71-55-62.0 0.66 2
1,1,2-Trichloroethane ND ug/L 09/24/23 22:46 79-00-52.0 0.65 2
Trichloroethene ND ug/L 09/24/23 22:46 79-01-62.0 0.77 2
Trichlorofluoromethane ND ug/L 09/24/23 22:46 75-69-42.0 0.60 2
1,1,2-Trichlorotrifluoroethane ND ug/L 09/24/23 22:46 76-13-12.0 0.63 2
Vinyl chloride ND ug/L 09/24/23 22:46 75-01-42.0 0.77 2
m&p-Xylene 10.2 ug/L 09/24/23 22:46 179601-23-14.0 1.4 2
o-Xylene 4.8 ug/L 09/24/23 22:46 95-47-62.0 0.68 2
Surrogates
4-Bromofluorobenzene (S)99 %09/24/23 22:46 460-00-470-130 2
1,2-Dichloroethane-d4 (S)107 %09/24/23 22:46 17060-07-070-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW04 WG- 091323 Lab ID: 92688066001 Collected: 09/13/23 09:50 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)99 %09/24/23 22:46 2037-26-570-130 2
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 2000 mg/L 09/19/23 17:375.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 41.5 mg/L 09/20/23 02:46 18496-25-810.0 2.2 100
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 48.7 mg/L 09/15/23 21:42 16887-00-620.0 12.0 20
Sulfate 432 mg/L 09/15/23 21:42 14808-79-820.0 10.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW06 WG- 091323 Lab ID: 92688066002 Collected: 09/13/23 10:29 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 7.2 Std. Units 09/15/23 10:191
True Color 5.0 units 09/15/23 10:195.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/03/23 23:36 7440-36-010/02/23 09:4615.0 5.5 1
Arsenic ND ug/L 10/03/23 23:36 7440-38-210/02/23 09:4610.0 3.4 1
Barium 62.1 ug/L 10/03/23 23:36 7440-39-310/02/23 09:4610.0 0.84 1
Beryllium ND ug/L 10/03/23 23:36 7440-41-710/02/23 09:464.0 0.17 1
Boron 82.9 ug/L 10/03/23 23:36 7440-42-810/02/23 09:4650.0 12.4 1
Cadmium ND ug/L 10/03/23 23:36 7440-43-910/02/23 09:461.0 0.33 1
Chromium ND ug/L 10/03/23 23:36 7440-47-310/02/23 09:465.0 1.7 1
Cobalt ND ug/L 10/03/23 23:36 7440-48-410/02/23 09:4610.0 0.96 1
Copper ND ug/L 10/03/23 23:36 7440-50-810/02/23 09:465.0 2.6 1
Lead ND ug/L 10/03/23 23:36 7439-92-110/02/23 09:4610.0 2.1 1
Manganese 673 ug/L 10/03/23 23:36 7439-96-510/02/23 09:465.0 1.1 1
Nickel 2.1J ug/L 10/03/23 23:36 7440-02-010/02/23 09:465.0 1.0 1
Selenium ND ug/L 10/03/23 23:36 7782-49-210/02/23 09:4615.0 3.9 1
Silver ND ug/L 10/03/23 23:36 7440-22-410/02/23 09:465.0 1.0 1
Thallium ND ug/L 10/03/23 23:36 7440-28-010/02/23 09:4615.0 2.9 1
Vanadium 3.5J ug/L 10/03/23 23:36 7440-62-210/02/23 09:4610.0 1.0 1
Zinc 79.8 ug/L 10/03/23 23:36 7440-66-610/02/23 09:4620.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/05/23 14:24 7440-36-010/03/23 06:0415.0 5.5 1
Arsenic, Dissolved ND ug/L 10/05/23 14:24 7440-38-210/03/23 06:0410.0 3.4 1
Barium, Dissolved 59.6 ug/L 10/05/23 14:24 7440-39-310/03/23 06:0410.0 0.84 1
Beryllium, Dissolved ND ug/L 10/05/23 14:24 7440-41-710/03/23 06:044.0 0.17 1
Boron, Dissolved 86.0 ug/L 10/05/23 14:24 7440-42-810/03/23 06:0450.0 12.4 1
Cadmium, Dissolved 0.50J ug/L 10/05/23 14:24 7440-43-910/03/23 06:041.0 0.33 1
Chromium, Dissolved ND ug/L 10/05/23 14:24 7440-47-310/03/23 06:045.0 1.7 1
Cobalt, Dissolved 1.2J ug/L 10/05/23 14:24 7440-48-410/03/23 06:0410.0 0.96 1
Copper, Dissolved ND ug/L 10/05/23 14:24 7440-50-810/03/23 06:045.0 2.6 1
Lead, Dissolved ND ug/L 10/05/23 14:24 7439-92-110/03/23 06:0410.0 2.1 1
Manganese, Dissolved 687 ug/L 10/05/23 14:24 7439-96-510/03/23 06:045.0 1.1 1
Nickel, Dissolved ND ug/L 10/05/23 14:24 7440-02-010/03/23 06:045.0 1.0 1
Selenium, Dissolved ND ug/L 10/05/23 14:24 7782-49-210/03/23 06:0415.0 3.9 1
Silver, Dissolved ND ug/L 10/05/23 14:24 7440-22-410/03/23 06:045.0 1.0 1
Thallium, Dissolved ND ug/L 10/05/23 14:24 7440-28-010/03/23 06:0415.0 2.9 1
Vanadium, Dissolved 4.1J ug/L 10/05/23 14:24 7440-62-210/03/23 06:0410.0 1.0 1
Zinc, Dissolved ND ug/L 10/05/23 14:24 7440-66-610/03/23 06:0420.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW06 WG- 091323 Lab ID: 92688066002 Collected: 09/13/23 10:29 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 09:48 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:29 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/20/23 18:12 83-32-909/19/23 10:3110.0 2.0 1
Acenaphthylene ND ug/L 09/20/23 18:12 208-96-809/19/23 10:3110.0 2.0 1
Acetophenone ND ug/L 09/20/23 18:12 98-86-209/19/23 10:3110.0 1.5 1
Anthracene ND ug/L 09/20/23 18:12 120-12-709/19/23 10:3110.0 2.3 1
Atrazine ND ug/L 09/20/23 18:12 1912-24-909/19/23 10:3110.0 3.2 1
Benzaldehyde ND ug/L 09/20/23 18:12 100-52-709/19/23 10:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/20/23 18:12 56-55-309/19/23 10:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/20/23 18:12 50-32-809/19/23 10:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/20/23 18:12 205-99-209/19/23 10:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/20/23 18:12 191-24-209/19/23 10:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/20/23 18:12 207-08-909/19/23 10:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/20/23 18:12 92-52-409/19/23 10:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/20/23 18:12 101-55-309/19/23 10:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/20/23 18:12 85-68-709/19/23 10:3110.0 3.1 1
Caprolactam ND ug/L 09/20/23 18:12 105-60-209/19/23 10:3110.0 6.9 1
Carbazole ND ug/L 09/20/23 18:12 86-74-809/19/23 10:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/20/23 18:12 59-50-709/19/23 10:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/20/23 18:12 106-47-809/19/23 10:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/20/23 18:12 111-91-109/19/23 10:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/20/23 18:12 111-44-409/19/23 10:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/20/23 18:12 91-58-709/19/23 10:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/20/23 18:12 95-57-809/19/23 10:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/20/23 18:12 7005-72-309/19/23 10:3110.0 2.0 1
Chrysene ND ug/L 09/20/23 18:12 218-01-909/19/23 10:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/20/23 18:12 53-70-309/19/23 10:3110.0 3.0 1
Dibenzofuran ND ug/L 09/20/23 18:12 132-64-909/19/23 10:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/20/23 18:12 91-94-109/19/23 10:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/20/23 18:12 120-83-209/19/23 10:3110.0 1.4 1
Diethylphthalate ND ug/L 09/20/23 18:12 84-66-209/19/23 10:3110.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/20/23 18:12 105-67-909/19/23 10:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/20/23 18:12 131-11-309/19/23 10:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/20/23 18:12 84-74-209/19/23 10:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/20/23 18:12 534-52-109/19/23 10:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/20/23 18:12 51-28-509/19/23 10:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/20/23 18:12 121-14-209/19/23 10:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/20/23 18:12 606-20-209/19/23 10:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/20/23 18:12 117-84-009/19/23 10:3110.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW06 WG- 091323 Lab ID: 92688066002 Collected: 09/13/23 10:29 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/20/23 18:12 117-81-709/19/23 10:316.0 3.7 1
Fluoranthene ND ug/L 09/20/23 18:12 206-44-009/19/23 10:3110.0 2.2 1
Fluorene ND ug/L 09/20/23 18:12 86-73-709/19/23 10:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/20/23 18:12 87-68-309/19/23 10:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/20/23 18:12 118-74-109/19/23 10:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/20/23 18:12 77-47-409/19/23 10:3110.0 1.6 1
Hexachloroethane ND ug/L 09/20/23 18:12 67-72-109/19/23 10:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/20/23 18:12 193-39-509/19/23 10:3110.0 2.9 1
Isophorone ND ug/L 09/20/23 18:12 78-59-109/19/23 10:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/20/23 18:12 91-57-609/19/23 10:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/20/23 18:12 95-48-709/19/23 10:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/20/23 18:12 15831-10-409/19/23 10:3110.0 1.2 1
Naphthalene ND ug/L 09/20/23 18:12 91-20-309/19/23 10:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/20/23 18:12 88-74-409/19/23 10:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/20/23 18:12 99-09-209/19/23 10:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/20/23 18:12 100-01-609/19/23 10:3120.0 5.1 1
Nitrobenzene ND ug/L 09/20/23 18:12 98-95-309/19/23 10:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/20/23 18:12 88-75-509/19/23 10:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/20/23 18:12 100-02-709/19/23 10:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/20/23 18:12 621-64-709/19/23 10:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/20/23 18:12 86-30-609/19/23 10:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/20/23 18:12 108-60-109/19/23 10:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/20/23 18:12 87-86-509/19/23 10:3120.0 3.8 1
Phenanthrene ND ug/L 09/20/23 18:12 85-01-809/19/23 10:3110.0 2.0 1
Phenol ND ug/L 09/20/23 18:12 108-95-209/19/23 10:3110.0 1.4 1
Pyrene ND ug/L 09/20/23 18:12 129-00-009/19/23 10:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/20/23 18:12 95-95-409/19/23 10:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/20/23 18:12 88-06-209/19/23 10:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)102 %09/20/23 18:12 4165-60-009/19/23 10:3110-138 1
2-Fluorobiphenyl (S)98 %09/20/23 18:12 321-60-809/19/23 10:3110-130 1
Terphenyl-d14 (S)113 %09/20/23 18:12 1718-51-009/19/23 10:3119-191 1
Phenol-d6 (S)16 %09/20/23 18:12 13127-88-309/19/23 10:3110-130 1
2-Fluorophenol (S)3 %09/20/23 18:12 367-12-4 S009/19/23 10:3110-130 1
2,4,6-Tribromophenol (S)14 %09/20/23 18:12 118-79-609/19/23 10:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/23/23 08:11 67-64-125.0 5.1 1
Benzene ND ug/L 09/23/23 08:11 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/23/23 08:11 75-27-41.0 0.31 1
Bromoform ND ug/L 09/23/23 08:11 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/23/23 08:11 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/23/23 08:11 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/23/23 08:11 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW06 WG- 091323 Lab ID: 92688066002 Collected: 09/13/23 10:29 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/23/23 08:11 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/23/23 08:11 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/23/23 08:11 75-00-31.0 0.65 1
Chloroform ND ug/L 09/23/23 08:11 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/23/23 08:11 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/23/23 08:11 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/23/23 08:11 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/23/23 08:11 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/23/23 08:11 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/23/23 08:11 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/23/23 08:11 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/23/23 08:11 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/23/23 08:11 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/23/23 08:11 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/23/23 08:11 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/23/23 08:11 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/23/23 08:11 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/23/23 08:11 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/23/23 08:11 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/23/23 08:11 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/23/23 08:11 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/23/23 08:11 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/23/23 08:11 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/23/23 08:11 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/23/23 08:11 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/23/23 08:11 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/23/23 08:11 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/23/23 08:11 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/23/23 08:11 1634-04-41.0 0.42 1
Styrene ND ug/L 09/23/23 08:11 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/23/23 08:11 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/23/23 08:11 127-18-41.0 0.29 1
Toluene ND ug/L 09/23/23 08:11 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/23/23 08:11 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/23/23 08:11 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/23/23 08:11 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/23/23 08:11 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/23/23 08:11 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/23/23 08:11 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/23/23 08:11 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/23/23 08:11 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/23/23 08:11 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %09/23/23 08:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %09/23/23 08:11 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW06 WG- 091323 Lab ID: 92688066002 Collected: 09/13/23 10:29 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)99 %09/23/23 08:11 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 398 mg/L 09/20/23 08:135.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 0.074J mg/L 09/20/23 02:47 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 24.2 mg/L 09/15/23 21:55 16887-00-61.0 0.60 1
Sulfate 83.7 mg/L 09/15/23 21:55 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW07 WG- 091323 Lab ID: 92688066003 Collected: 09/13/23 12:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.4 Std. Units 09/15/23 10:551
True Color ND units 09/15/23 10:555.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/03/23 23:40 7440-36-010/02/23 09:4615.0 5.5 1
Arsenic ND ug/L 10/03/23 23:40 7440-38-210/02/23 09:4610.0 3.4 1
Barium 26.0 ug/L 10/03/23 23:40 7440-39-310/02/23 09:4610.0 0.84 1
Beryllium ND ug/L 10/03/23 23:40 7440-41-710/02/23 09:464.0 0.17 1
Boron 114 ug/L 10/03/23 23:40 7440-42-810/02/23 09:4650.0 12.4 1
Cadmium ND ug/L 10/03/23 23:40 7440-43-910/02/23 09:461.0 0.33 1
Chromium ND ug/L 10/03/23 23:40 7440-47-310/02/23 09:465.0 1.7 1
Cobalt 1.0J ug/L 10/03/23 23:40 7440-48-410/02/23 09:4610.0 0.96 1
Copper 4.6J ug/L 10/03/23 23:40 7440-50-810/02/23 09:465.0 2.6 1
Lead ND ug/L 10/03/23 23:40 7439-92-110/02/23 09:4610.0 2.1 1
Manganese 453 ug/L 10/03/23 23:40 7439-96-510/02/23 09:465.0 1.1 1
Nickel 2.6J ug/L 10/03/23 23:40 7440-02-010/02/23 09:465.0 1.0 1
Selenium ND ug/L 10/03/23 23:40 7782-49-210/02/23 09:4615.0 3.9 1
Silver ND ug/L 10/03/23 23:40 7440-22-410/02/23 09:465.0 1.0 1
Thallium ND ug/L 10/03/23 23:40 7440-28-010/02/23 09:4615.0 2.9 1
Vanadium ND ug/L 10/03/23 23:40 7440-62-210/02/23 09:4610.0 1.0 1
Zinc 586 ug/L 10/03/23 23:40 7440-66-610/02/23 09:4620.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/05/23 14:28 7440-36-010/03/23 06:0415.0 5.5 1
Arsenic, Dissolved ND ug/L 10/05/23 14:28 7440-38-210/03/23 06:0410.0 3.4 1
Barium, Dissolved 24.6 ug/L 10/05/23 14:28 7440-39-310/03/23 06:0410.0 0.84 1
Beryllium, Dissolved ND ug/L 10/05/23 14:28 7440-41-710/03/23 06:044.0 0.17 1
Boron, Dissolved 114 ug/L 10/05/23 14:28 7440-42-810/03/23 06:0450.0 12.4 1
Cadmium, Dissolved 0.52J ug/L 10/05/23 14:28 7440-43-910/03/23 06:041.0 0.33 1
Chromium, Dissolved ND ug/L 10/05/23 14:28 7440-47-310/03/23 06:045.0 1.7 1
Cobalt, Dissolved 1.2J ug/L 10/05/23 14:28 7440-48-410/03/23 06:0410.0 0.96 1
Copper, Dissolved 31.1 ug/L 10/05/23 14:28 7440-50-810/03/23 06:045.0 2.6 1
Lead, Dissolved ND ug/L 10/05/23 14:28 7439-92-110/03/23 06:0410.0 2.1 1
Manganese, Dissolved 508 ug/L 10/05/23 14:28 7439-96-510/03/23 06:045.0 1.1 1
Nickel, Dissolved 3.9J ug/L 10/05/23 14:28 7440-02-010/03/23 06:045.0 1.0 1
Selenium, Dissolved ND ug/L 10/05/23 14:28 7782-49-210/03/23 06:0415.0 3.9 1
Silver, Dissolved ND ug/L 10/05/23 14:28 7440-22-410/03/23 06:045.0 1.0 1
Thallium, Dissolved ND ug/L 10/05/23 14:28 7440-28-010/03/23 06:0415.0 2.9 1
Vanadium, Dissolved ND ug/L 10/05/23 14:28 7440-62-210/03/23 06:0410.0 1.0 1
Zinc, Dissolved 710 ug/L 10/05/23 14:28 7440-66-610/03/23 06:0420.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW07 WG- 091323 Lab ID: 92688066003 Collected: 09/13/23 12:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 09:51 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:31 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/20/23 18:38 83-32-909/19/23 10:3110.0 2.0 1
Acenaphthylene ND ug/L 09/20/23 18:38 208-96-809/19/23 10:3110.0 2.0 1
Acetophenone ND ug/L 09/20/23 18:38 98-86-209/19/23 10:3110.0 1.5 1
Anthracene ND ug/L 09/20/23 18:38 120-12-709/19/23 10:3110.0 2.3 1
Atrazine ND ug/L 09/20/23 18:38 1912-24-909/19/23 10:3110.0 3.2 1
Benzaldehyde ND ug/L 09/20/23 18:38 100-52-709/19/23 10:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/20/23 18:38 56-55-309/19/23 10:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/20/23 18:38 50-32-809/19/23 10:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/20/23 18:38 205-99-209/19/23 10:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/20/23 18:38 191-24-209/19/23 10:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/20/23 18:38 207-08-909/19/23 10:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/20/23 18:38 92-52-409/19/23 10:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/20/23 18:38 101-55-309/19/23 10:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/20/23 18:38 85-68-709/19/23 10:3110.0 3.1 1
Caprolactam ND ug/L 09/20/23 18:38 105-60-209/19/23 10:3110.0 6.9 1
Carbazole ND ug/L 09/20/23 18:38 86-74-809/19/23 10:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/20/23 18:38 59-50-709/19/23 10:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/20/23 18:38 106-47-809/19/23 10:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/20/23 18:38 111-91-109/19/23 10:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/20/23 18:38 111-44-409/19/23 10:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/20/23 18:38 91-58-709/19/23 10:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/20/23 18:38 95-57-809/19/23 10:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/20/23 18:38 7005-72-309/19/23 10:3110.0 2.0 1
Chrysene ND ug/L 09/20/23 18:38 218-01-909/19/23 10:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/20/23 18:38 53-70-309/19/23 10:3110.0 3.0 1
Dibenzofuran ND ug/L 09/20/23 18:38 132-64-909/19/23 10:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/20/23 18:38 91-94-109/19/23 10:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/20/23 18:38 120-83-209/19/23 10:3110.0 1.4 1
Diethylphthalate ND ug/L 09/20/23 18:38 84-66-209/19/23 10:3110.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/20/23 18:38 105-67-909/19/23 10:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/20/23 18:38 131-11-309/19/23 10:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/20/23 18:38 84-74-209/19/23 10:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/20/23 18:38 534-52-109/19/23 10:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/20/23 18:38 51-28-509/19/23 10:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/20/23 18:38 121-14-209/19/23 10:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/20/23 18:38 606-20-209/19/23 10:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/20/23 18:38 117-84-009/19/23 10:3110.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW07 WG- 091323 Lab ID: 92688066003 Collected: 09/13/23 12:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/20/23 18:38 117-81-709/19/23 10:316.0 3.7 1
Fluoranthene ND ug/L 09/20/23 18:38 206-44-009/19/23 10:3110.0 2.2 1
Fluorene ND ug/L 09/20/23 18:38 86-73-709/19/23 10:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/20/23 18:38 87-68-309/19/23 10:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/20/23 18:38 118-74-109/19/23 10:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/20/23 18:38 77-47-409/19/23 10:3110.0 1.6 1
Hexachloroethane ND ug/L 09/20/23 18:38 67-72-109/19/23 10:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/20/23 18:38 193-39-509/19/23 10:3110.0 2.9 1
Isophorone ND ug/L 09/20/23 18:38 78-59-109/19/23 10:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/20/23 18:38 91-57-609/19/23 10:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/20/23 18:38 95-48-709/19/23 10:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/20/23 18:38 15831-10-409/19/23 10:3110.0 1.2 1
Naphthalene ND ug/L 09/20/23 18:38 91-20-309/19/23 10:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/20/23 18:38 88-74-409/19/23 10:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/20/23 18:38 99-09-209/19/23 10:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/20/23 18:38 100-01-609/19/23 10:3120.0 5.1 1
Nitrobenzene ND ug/L 09/20/23 18:38 98-95-309/19/23 10:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/20/23 18:38 88-75-509/19/23 10:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/20/23 18:38 100-02-709/19/23 10:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/20/23 18:38 621-64-709/19/23 10:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/20/23 18:38 86-30-609/19/23 10:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/20/23 18:38 108-60-109/19/23 10:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/20/23 18:38 87-86-509/19/23 10:3120.0 3.8 1
Phenanthrene ND ug/L 09/20/23 18:38 85-01-809/19/23 10:3110.0 2.0 1
Phenol ND ug/L 09/20/23 18:38 108-95-209/19/23 10:3110.0 1.4 1
Pyrene ND ug/L 09/20/23 18:38 129-00-009/19/23 10:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/20/23 18:38 95-95-409/19/23 10:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/20/23 18:38 88-06-209/19/23 10:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)110 %09/20/23 18:38 4165-60-009/19/23 10:3110-138 1
2-Fluorobiphenyl (S)100 %09/20/23 18:38 321-60-809/19/23 10:3110-130 1
Terphenyl-d14 (S)113 %09/20/23 18:38 1718-51-009/19/23 10:3119-191 1
Phenol-d6 (S)61 %09/20/23 18:38 13127-88-309/19/23 10:3110-130 1
2-Fluorophenol (S)82 %09/20/23 18:38 367-12-409/19/23 10:3110-130 1
2,4,6-Tribromophenol (S)127 %09/20/23 18:38 118-79-609/19/23 10:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/23/23 08:29 67-64-125.0 5.1 1
Benzene ND ug/L 09/23/23 08:29 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/23/23 08:29 75-27-41.0 0.31 1
Bromoform ND ug/L 09/23/23 08:29 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/23/23 08:29 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/23/23 08:29 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/23/23 08:29 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW07 WG- 091323 Lab ID: 92688066003 Collected: 09/13/23 12:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/23/23 08:29 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/23/23 08:29 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/23/23 08:29 75-00-31.0 0.65 1
Chloroform ND ug/L 09/23/23 08:29 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/23/23 08:29 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/23/23 08:29 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/23/23 08:29 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/23/23 08:29 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/23/23 08:29 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/23/23 08:29 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/23/23 08:29 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/23/23 08:29 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/23/23 08:29 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/23/23 08:29 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/23/23 08:29 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/23/23 08:29 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/23/23 08:29 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/23/23 08:29 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/23/23 08:29 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/23/23 08:29 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/23/23 08:29 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/23/23 08:29 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/23/23 08:29 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/23/23 08:29 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/23/23 08:29 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/23/23 08:29 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/23/23 08:29 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/23/23 08:29 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/23/23 08:29 1634-04-41.0 0.42 1
Styrene ND ug/L 09/23/23 08:29 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/23/23 08:29 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/23/23 08:29 127-18-41.0 0.29 1
Toluene ND ug/L 09/23/23 08:29 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/23/23 08:29 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/23/23 08:29 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/23/23 08:29 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/23/23 08:29 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/23/23 08:29 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/23/23 08:29 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/23/23 08:29 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/23/23 08:29 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/23/23 08:29 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %09/23/23 08:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %09/23/23 08:29 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: RW07 WG- 091323 Lab ID: 92688066003 Collected: 09/13/23 12:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)98 %09/23/23 08:29 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 198 mg/L 09/19/23 18:015.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/20/23 02:47 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 57.7 mg/L 09/16/23 04:42 16887-00-61.0 0.60 1
Sulfate 148 mg/L 09/16/23 10:39 14808-79-83.0 1.5 3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ01 WG- 091323 Lab ID: 92688066004 Collected: 09/13/23 12:54 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 8.6 Std. Units 09/15/23 10:5825
True Color 375 units 09/15/23 10:58125 125 25
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/03/23 23:43 7440-36-010/02/23 09:4615.0 5.5 1
Arsenic ND ug/L 10/03/23 23:43 7440-38-210/02/23 09:4610.0 3.4 1
Barium 42.1 ug/L 10/03/23 23:43 7440-39-310/02/23 09:4610.0 0.84 1
Beryllium ND ug/L 10/03/23 23:43 7440-41-710/02/23 09:464.0 0.17 1
Boron 84.6 ug/L 10/03/23 23:43 7440-42-810/02/23 09:4650.0 12.4 1
Cadmium ND ug/L 10/03/23 23:43 7440-43-910/02/23 09:461.0 0.33 1
Chromium 8.0 ug/L 10/03/23 23:43 7440-47-310/02/23 09:465.0 1.7 1
Cobalt ND ug/L 10/03/23 23:43 7440-48-410/02/23 09:4610.0 0.96 1
Copper ND ug/L 10/03/23 23:43 7440-50-810/02/23 09:465.0 2.6 1
Lead ND ug/L 10/03/23 23:43 7439-92-110/02/23 09:4610.0 2.1 1
Manganese 3600 ug/L 10/06/23 07:28 7439-96-510/02/23 09:4650.0 11.0 10
Nickel 10.9 ug/L 10/03/23 23:43 7440-02-010/02/23 09:465.0 1.0 1
Selenium ND ug/L 10/03/23 23:43 7782-49-210/02/23 09:4615.0 3.9 1
Silver ND ug/L 10/03/23 23:43 7440-22-410/02/23 09:465.0 1.0 1
Thallium ND ug/L 10/03/23 23:43 7440-28-010/02/23 09:4615.0 2.9 1
Vanadium 46.3 ug/L 10/03/23 23:43 7440-62-210/02/23 09:4610.0 1.0 1
Zinc ND ug/L 10/03/23 23:43 7440-66-610/02/23 09:4620.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/05/23 14:32 7440-36-010/03/23 06:0415.0 5.5 1
Arsenic, Dissolved 4.2J ug/L 10/05/23 14:32 7440-38-210/03/23 06:0410.0 3.4 1
Barium, Dissolved 34.7 ug/L 10/05/23 14:32 7440-39-310/03/23 06:0410.0 0.84 1
Beryllium, Dissolved ND ug/L 10/05/23 14:32 7440-41-710/03/23 06:044.0 0.17 1
Boron, Dissolved 85.5 ug/L 10/05/23 14:32 7440-42-810/03/23 06:0450.0 12.4 1
Cadmium, Dissolved ND ug/L 10/05/23 14:32 7440-43-910/03/23 06:041.0 0.33 1
Chromium, Dissolved 5.1 ug/L 10/05/23 14:32 7440-47-310/03/23 06:045.0 1.7 1
Cobalt, Dissolved ND ug/L 10/05/23 14:32 7440-48-410/03/23 06:0410.0 0.96 1
Copper, Dissolved 8.1 ug/L 10/05/23 14:32 7440-50-810/03/23 06:045.0 2.6 1
Lead, Dissolved ND ug/L 10/05/23 14:32 7439-92-110/03/23 06:0410.0 2.1 1
Manganese, Dissolved 3100 ug/L 10/06/23 08:29 7439-96-510/03/23 06:0425.0 5.5 5
Nickel, Dissolved 9.3 ug/L 10/05/23 14:32 7440-02-010/03/23 06:045.0 1.0 1
Selenium, Dissolved ND ug/L 10/05/23 14:32 7782-49-210/03/23 06:0415.0 3.9 1
Silver, Dissolved ND ug/L 10/05/23 14:32 7440-22-410/03/23 06:045.0 1.0 1
Thallium, Dissolved ND ug/L 10/05/23 14:32 7440-28-010/03/23 06:0415.0 2.9 1
Vanadium, Dissolved 35.6 ug/L 10/05/23 14:32 7440-62-210/03/23 06:0410.0 1.0 1
Zinc, Dissolved ND ug/L 10/05/23 14:32 7440-66-610/03/23 06:0420.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ01 WG- 091323 Lab ID: 92688066004 Collected: 09/13/23 12:54 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 09:53 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:34 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/20/23 19:03 83-32-909/19/23 10:3110.0 2.0 1
Acenaphthylene ND ug/L 09/20/23 19:03 208-96-809/19/23 10:3110.0 2.0 1
Acetophenone ND ug/L 09/20/23 19:03 98-86-209/19/23 10:3110.0 1.5 1
Anthracene ND ug/L 09/20/23 19:03 120-12-709/19/23 10:3110.0 2.3 1
Atrazine ND ug/L 09/20/23 19:03 1912-24-909/19/23 10:3110.0 3.2 1
Benzaldehyde ND ug/L 09/20/23 19:03 100-52-709/19/23 10:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/20/23 19:03 56-55-309/19/23 10:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/20/23 19:03 50-32-809/19/23 10:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/20/23 19:03 205-99-209/19/23 10:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/20/23 19:03 191-24-209/19/23 10:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/20/23 19:03 207-08-909/19/23 10:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/20/23 19:03 92-52-409/19/23 10:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/20/23 19:03 101-55-309/19/23 10:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/20/23 19:03 85-68-709/19/23 10:3110.0 3.1 1
Caprolactam ND ug/L 09/20/23 19:03 105-60-209/19/23 10:3110.0 6.9 1
Carbazole ND ug/L 09/20/23 19:03 86-74-809/19/23 10:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/20/23 19:03 59-50-709/19/23 10:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/20/23 19:03 106-47-809/19/23 10:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/20/23 19:03 111-91-109/19/23 10:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/20/23 19:03 111-44-409/19/23 10:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/20/23 19:03 91-58-709/19/23 10:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/20/23 19:03 95-57-809/19/23 10:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/20/23 19:03 7005-72-309/19/23 10:3110.0 2.0 1
Chrysene ND ug/L 09/20/23 19:03 218-01-909/19/23 10:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/20/23 19:03 53-70-309/19/23 10:3110.0 3.0 1
Dibenzofuran ND ug/L 09/20/23 19:03 132-64-909/19/23 10:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/20/23 19:03 91-94-109/19/23 10:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/20/23 19:03 120-83-209/19/23 10:3110.0 1.4 1
Diethylphthalate ND ug/L 09/20/23 19:03 84-66-209/19/23 10:3110.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/20/23 19:03 105-67-909/19/23 10:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/20/23 19:03 131-11-309/19/23 10:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/20/23 19:03 84-74-209/19/23 10:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/20/23 19:03 534-52-109/19/23 10:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/20/23 19:03 51-28-509/19/23 10:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/20/23 19:03 121-14-209/19/23 10:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/20/23 19:03 606-20-209/19/23 10:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/20/23 19:03 117-84-009/19/23 10:3110.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ01 WG- 091323 Lab ID: 92688066004 Collected: 09/13/23 12:54 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/20/23 19:03 117-81-709/19/23 10:316.0 3.7 1
Fluoranthene ND ug/L 09/20/23 19:03 206-44-009/19/23 10:3110.0 2.2 1
Fluorene ND ug/L 09/20/23 19:03 86-73-709/19/23 10:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/20/23 19:03 87-68-309/19/23 10:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/20/23 19:03 118-74-109/19/23 10:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/20/23 19:03 77-47-409/19/23 10:3110.0 1.6 1
Hexachloroethane ND ug/L 09/20/23 19:03 67-72-109/19/23 10:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/20/23 19:03 193-39-509/19/23 10:3110.0 2.9 1
Isophorone ND ug/L 09/20/23 19:03 78-59-109/19/23 10:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/20/23 19:03 91-57-609/19/23 10:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/20/23 19:03 95-48-709/19/23 10:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/20/23 19:03 15831-10-409/19/23 10:3110.0 1.2 1
Naphthalene 3.4J ug/L 09/20/23 19:03 91-20-309/19/23 10:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/20/23 19:03 88-74-409/19/23 10:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/20/23 19:03 99-09-209/19/23 10:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/20/23 19:03 100-01-609/19/23 10:3120.0 5.1 1
Nitrobenzene ND ug/L 09/20/23 19:03 98-95-309/19/23 10:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/20/23 19:03 88-75-509/19/23 10:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/20/23 19:03 100-02-709/19/23 10:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/20/23 19:03 621-64-709/19/23 10:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/20/23 19:03 86-30-609/19/23 10:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/20/23 19:03 108-60-109/19/23 10:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/20/23 19:03 87-86-509/19/23 10:3120.0 3.8 1
Phenanthrene ND ug/L 09/20/23 19:03 85-01-809/19/23 10:3110.0 2.0 1
Phenol ND ug/L 09/20/23 19:03 108-95-209/19/23 10:3110.0 1.4 1
Pyrene ND ug/L 09/20/23 19:03 129-00-009/19/23 10:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/20/23 19:03 95-95-409/19/23 10:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/20/23 19:03 88-06-209/19/23 10:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)92 %09/20/23 19:03 4165-60-009/19/23 10:3110-138 1
2-Fluorobiphenyl (S)98 %09/20/23 19:03 321-60-809/19/23 10:3110-130 1
Terphenyl-d14 (S)118 %09/20/23 19:03 1718-51-009/19/23 10:3119-191 1
Phenol-d6 (S)49 %09/20/23 19:03 13127-88-309/19/23 10:3110-130 1
2-Fluorophenol (S)68 %09/20/23 19:03 367-12-409/19/23 10:3110-130 1
2,4,6-Tribromophenol (S)102 %09/20/23 19:03 118-79-609/19/23 10:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/23/23 08:48 67-64-125.0 5.1 1
Benzene ND ug/L 09/23/23 08:48 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/23/23 08:48 75-27-41.0 0.31 1
Bromoform ND ug/L 09/23/23 08:48 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/23/23 08:48 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/23/23 08:48 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/23/23 08:48 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ01 WG- 091323 Lab ID: 92688066004 Collected: 09/13/23 12:54 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/23/23 08:48 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/23/23 08:48 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/23/23 08:48 75-00-31.0 0.65 1
Chloroform ND ug/L 09/23/23 08:48 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/23/23 08:48 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/23/23 08:48 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/23/23 08:48 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/23/23 08:48 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/23/23 08:48 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/23/23 08:48 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/23/23 08:48 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/23/23 08:48 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/23/23 08:48 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/23/23 08:48 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/23/23 08:48 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/23/23 08:48 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/23/23 08:48 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/23/23 08:48 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/23/23 08:48 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/23/23 08:48 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/23/23 08:48 10061-02-61.0 0.36 1
Ethylbenzene 5.3 ug/L 09/23/23 08:48 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/23/23 08:48 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/23/23 08:48 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/23/23 08:48 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/23/23 08:48 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/23/23 08:48 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/23/23 08:48 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/23/23 08:48 1634-04-41.0 0.42 1
Styrene ND ug/L 09/23/23 08:48 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/23/23 08:48 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/23/23 08:48 127-18-41.0 0.29 1
Toluene ND ug/L 09/23/23 08:48 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/23/23 08:48 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/23/23 08:48 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/23/23 08:48 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/23/23 08:48 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/23/23 08:48 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/23/23 08:48 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/23/23 08:48 75-01-41.0 0.39 1
m&p-Xylene 7.1 ug/L 09/23/23 08:48 179601-23-12.0 0.71 1
o-Xylene 1.5 ug/L 09/23/23 08:48 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %09/23/23 08:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %09/23/23 08:48 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ01 WG- 091323 Lab ID: 92688066004 Collected: 09/13/23 12:54 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)98 %09/23/23 08:48 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 813 mg/L 09/21/23 16:325.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 0.22 mg/L 09/20/23 02:48 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 282 mg/L 09/16/23 04:56 16887-00-610.0 6.0 10
Sulfate 165 mg/L 09/16/23 04:56 14808-79-810.0 5.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ05 WG- 091323 Lab ID: 92688066005 Collected: 09/13/23 14:46 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 7.1 Std. Units 09/15/23 10:591
True Color ND units 09/15/23 10:595.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/03/23 23:46 7440-36-010/02/23 09:4615.0 5.5 1
Arsenic ND ug/L 10/03/23 23:46 7440-38-210/02/23 09:4610.0 3.4 1
Barium 44.7 ug/L 10/03/23 23:46 7440-39-310/02/23 09:4610.0 0.84 1
Beryllium ND ug/L 10/03/23 23:46 7440-41-710/02/23 09:464.0 0.17 1
Boron 55.7 ug/L 10/03/23 23:46 7440-42-810/02/23 09:4650.0 12.4 1
Cadmium ND ug/L 10/03/23 23:46 7440-43-910/02/23 09:461.0 0.33 1
Chromium ND ug/L 10/03/23 23:46 7440-47-310/02/23 09:465.0 1.7 1
Cobalt ND ug/L 10/03/23 23:46 7440-48-410/02/23 09:4610.0 0.96 1
Copper ND ug/L 10/03/23 23:46 7440-50-810/02/23 09:465.0 2.6 1
Lead ND ug/L 10/03/23 23:46 7439-92-110/02/23 09:4610.0 2.1 1
Manganese 11.2 ug/L 10/03/23 23:46 7439-96-510/02/23 09:465.0 1.1 1
Nickel ND ug/L 10/03/23 23:46 7440-02-010/02/23 09:465.0 1.0 1
Selenium ND ug/L 10/03/23 23:46 7782-49-210/02/23 09:4615.0 3.9 1
Silver ND ug/L 10/03/23 23:46 7440-22-410/02/23 09:465.0 1.0 1
Thallium ND ug/L 10/03/23 23:46 7440-28-010/02/23 09:4615.0 2.9 1
Vanadium ND ug/L 10/03/23 23:46 7440-62-210/02/23 09:4610.0 1.0 1
Zinc ND ug/L 10/03/23 23:46 7440-66-610/02/23 09:4620.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/05/23 10:53 7440-36-010/03/23 06:0415.0 5.5 1
Arsenic, Dissolved ND ug/L 10/05/23 10:53 7440-38-210/03/23 06:0410.0 3.4 1
Barium, Dissolved 43.0 ug/L 10/05/23 10:53 7440-39-310/03/23 06:0410.0 0.84 1
Beryllium, Dissolved ND ug/L 10/05/23 10:53 7440-41-710/03/23 06:044.0 0.17 1
Boron, Dissolved 56.2 ug/L 10/05/23 10:53 7440-42-810/03/23 06:0450.0 12.4 1
Cadmium, Dissolved ND ug/L 10/05/23 10:53 7440-43-910/03/23 06:041.0 0.33 1
Chromium, Dissolved ND ug/L 10/05/23 10:53 7440-47-310/03/23 06:045.0 1.7 1
Cobalt, Dissolved ND ug/L 10/05/23 10:53 7440-48-410/03/23 06:0410.0 0.96 1
Copper, Dissolved ND ug/L 10/05/23 10:53 7440-50-810/03/23 06:045.0 2.6 1
Lead, Dissolved ND ug/L 10/05/23 10:53 7439-92-110/03/23 06:0410.0 2.1 1
Manganese, Dissolved 2.3J ug/L 10/05/23 10:53 7439-96-510/03/23 06:045.0 1.1 1
Nickel, Dissolved ND ug/L 10/05/23 10:53 7440-02-010/03/23 06:045.0 1.0 1
Selenium, Dissolved ND ug/L 10/05/23 10:53 7782-49-210/03/23 06:0415.0 3.9 1
Silver, Dissolved ND ug/L 10/05/23 10:53 7440-22-410/03/23 06:045.0 1.0 1
Thallium, Dissolved ND ug/L 10/05/23 10:53 7440-28-010/03/23 06:0415.0 2.9 1
Vanadium, Dissolved ND ug/L 10/05/23 10:53 7440-62-210/03/23 06:0410.0 1.0 1
Zinc, Dissolved ND ug/L 10/05/23 10:53 7440-66-610/03/23 06:0420.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ05 WG- 091323 Lab ID: 92688066005 Collected: 09/13/23 14:46 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 10:00 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:36 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/20/23 19:29 83-32-909/19/23 10:318.3 1.7 1
Acenaphthylene ND ug/L 09/20/23 19:29 208-96-809/19/23 10:318.3 1.6 1
Acetophenone ND ug/L 09/20/23 19:29 98-86-209/19/23 10:318.3 1.2 1
Anthracene ND ug/L 09/20/23 19:29 120-12-709/19/23 10:318.3 1.9 1
Atrazine ND ug/L 09/20/23 19:29 1912-24-909/19/23 10:318.3 2.6 1
Benzaldehyde ND ug/L 09/20/23 19:29 100-52-709/19/23 10:318.3 3.0 1
Benzo(a)anthracene ND ug/L 09/20/23 19:29 56-55-309/19/23 10:318.3 2.2 1
Benzo(a)pyrene ND ug/L 09/20/23 19:29 50-32-809/19/23 10:318.3 2.3 1
Benzo(b)fluoranthene ND ug/L 09/20/23 19:29 205-99-209/19/23 10:318.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 09/20/23 19:29 191-24-209/19/23 10:318.3 2.4 1
Benzo(k)fluoranthene ND ug/L 09/20/23 19:29 207-08-909/19/23 10:318.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 09/20/23 19:29 92-52-409/19/23 10:318.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 09/20/23 19:29 101-55-309/19/23 10:318.3 1.5 1
Butylbenzylphthalate ND ug/L 09/20/23 19:29 85-68-709/19/23 10:318.3 2.6 1
Caprolactam ND ug/L 09/20/23 19:29 105-60-209/19/23 10:318.3 5.8 1
Carbazole ND ug/L 09/20/23 19:29 86-74-809/19/23 10:318.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/20/23 19:29 59-50-709/19/23 10:318.3 2.8 1
4-Chloroaniline ND ug/L 09/20/23 19:29 106-47-809/19/23 10:3116.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/20/23 19:29 111-91-109/19/23 10:318.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 09/20/23 19:29 111-44-409/19/23 10:318.3 1.6 1
2-Chloronaphthalene ND ug/L 09/20/23 19:29 91-58-709/19/23 10:318.3 1.4 1
2-Chlorophenol ND ug/L 09/20/23 19:29 95-57-809/19/23 10:318.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/20/23 19:29 7005-72-309/19/23 10:318.3 1.7 1
Chrysene ND ug/L 09/20/23 19:29 218-01-909/19/23 10:318.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 09/20/23 19:29 53-70-309/19/23 10:318.3 2.5 1
Dibenzofuran ND ug/L 09/20/23 19:29 132-64-909/19/23 10:318.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/20/23 19:29 91-94-109/19/23 10:3116.7 6.8 1
2,4-Dichlorophenol ND ug/L 09/20/23 19:29 120-83-2 R109/19/23 10:318.3 1.2 1
Diethylphthalate ND ug/L 09/20/23 19:29 84-66-209/19/23 10:318.3 1.7 1
2,4-Dimethylphenol ND ug/L 09/20/23 19:29 105-67-909/19/23 10:318.3 1.4 1
Dimethylphthalate ND ug/L 09/20/23 19:29 131-11-309/19/23 10:318.3 1.8 1
Di-n-butylphthalate ND ug/L 09/20/23 19:29 84-74-209/19/23 10:318.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/20/23 19:29 534-52-109/19/23 10:3116.7 6.5 1
2,4-Dinitrophenol ND ug/L 09/20/23 19:29 51-28-509/19/23 10:3141.7 21.7 1
2,4-Dinitrotoluene ND ug/L 09/20/23 19:29 121-14-209/19/23 10:318.3 1.4 1
2,6-Dinitrotoluene ND ug/L 09/20/23 19:29 606-20-209/19/23 10:318.3 1.4 1
Di-n-octylphthalate ND ug/L 09/20/23 19:29 117-84-009/19/23 10:318.3 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ05 WG- 091323 Lab ID: 92688066005 Collected: 09/13/23 14:46 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/20/23 19:29 117-81-709/19/23 10:315.0 3.1 1
Fluoranthene ND ug/L 09/20/23 19:29 206-44-009/19/23 10:318.3 1.8 1
Fluorene ND ug/L 09/20/23 19:29 86-73-709/19/23 10:318.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 09/20/23 19:29 87-68-309/19/23 10:318.3 1.5 1
Hexachlorobenzene ND ug/L 09/20/23 19:29 118-74-109/19/23 10:318.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 09/20/23 19:29 77-47-409/19/23 10:318.3 1.3 1
Hexachloroethane ND ug/L 09/20/23 19:29 67-72-109/19/23 10:318.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/20/23 19:29 193-39-509/19/23 10:318.3 2.4 1
Isophorone ND ug/L 09/20/23 19:29 78-59-109/19/23 10:318.3 1.4 1
2-Methylnaphthalene ND ug/L 09/20/23 19:29 91-57-609/19/23 10:318.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/20/23 19:29 95-48-709/19/23 10:318.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/20/23 19:29 15831-10-409/19/23 10:318.3 1.0 1
Naphthalene ND ug/L 09/20/23 19:29 91-20-309/19/23 10:318.3 1.7 1
2-Nitroaniline ND ug/L 09/20/23 19:29 88-74-409/19/23 10:3116.7 2.5 1
3-Nitroaniline ND ug/L 09/20/23 19:29 99-09-209/19/23 10:3116.7 3.1 1
4-Nitroaniline ND ug/L 09/20/23 19:29 100-01-609/19/23 10:3116.7 4.2 1
Nitrobenzene ND ug/L 09/20/23 19:29 98-95-309/19/23 10:318.3 1.6 1
2-Nitrophenol ND ug/L 09/20/23 19:29 88-75-5 R109/19/23 10:318.3 1.2 1
4-Nitrophenol ND ug/L 09/20/23 19:29 100-02-7 M109/19/23 10:3141.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 09/20/23 19:29 621-64-709/19/23 10:318.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 09/20/23 19:29 86-30-609/19/23 10:318.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/20/23 19:29 108-60-109/19/23 10:318.3 0.96 1
Pentachlorophenol ND ug/L 09/20/23 19:29 87-86-5 R109/19/23 10:3116.7 3.1 1
Phenanthrene ND ug/L 09/20/23 19:29 85-01-809/19/23 10:318.3 1.7 1
Phenol ND ug/L 09/20/23 19:29 108-95-209/19/23 10:318.3 1.1 1
Pyrene ND ug/L 09/20/23 19:29 129-00-009/19/23 10:318.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 09/20/23 19:29 95-95-4 R109/19/23 10:318.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/20/23 19:29 88-06-2 R109/19/23 10:318.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)90 %09/20/23 19:29 4165-60-009/19/23 10:3110-138 1
2-Fluorobiphenyl (S)91 %09/20/23 19:29 321-60-809/19/23 10:3110-130 1
Terphenyl-d14 (S)106 %09/20/23 19:29 1718-51-009/19/23 10:3119-191 1
Phenol-d6 (S)60 %09/20/23 19:29 13127-88-309/19/23 10:3110-130 1
2-Fluorophenol (S)74 %09/20/23 19:29 367-12-409/19/23 10:3110-130 1
2,4,6-Tribromophenol (S)110 %09/20/23 19:29 118-79-609/19/23 10:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/23/23 09:06 67-64-125.0 5.1 1
Benzene ND ug/L 09/23/23 09:06 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/23/23 09:06 75-27-41.0 0.31 1
Bromoform ND ug/L 09/23/23 09:06 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/23/23 09:06 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/23/23 09:06 78-93-3 R15.0 4.0 1
Carbon disulfide ND ug/L 09/23/23 09:06 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ05 WG- 091323 Lab ID: 92688066005 Collected: 09/13/23 14:46 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/23/23 09:06 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/23/23 09:06 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/23/23 09:06 75-00-31.0 0.65 1
Chloroform 29.7 ug/L 09/23/23 09:06 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/23/23 09:06 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/23/23 09:06 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/23/23 09:06 96-12-8 R12.0 0.34 1
Dibromochloromethane ND ug/L 09/23/23 09:06 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/23/23 09:06 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/23/23 09:06 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/23/23 09:06 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/23/23 09:06 106-46-7 R11.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/23/23 09:06 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/23/23 09:06 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/23/23 09:06 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/23/23 09:06 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/23/23 09:06 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/23/23 09:06 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/23/23 09:06 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/23/23 09:06 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/23/23 09:06 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/23/23 09:06 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/23/23 09:06 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/23/23 09:06 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/23/23 09:06 79-20-9 R110.0 2.4 1
Methylcyclohexane ND ug/L 09/23/23 09:06 108-87-2 M110.0 1.5 1
Methylene Chloride ND ug/L 09/23/23 09:06 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/23/23 09:06 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/23/23 09:06 1634-04-4 R11.0 0.42 1
Styrene ND ug/L 09/23/23 09:06 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/23/23 09:06 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/23/23 09:06 127-18-41.0 0.29 1
Toluene ND ug/L 09/23/23 09:06 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/23/23 09:06 120-82-1 R11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/23/23 09:06 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/23/23 09:06 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/23/23 09:06 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/23/23 09:06 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/23/23 09:06 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/23/23 09:06 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/23/23 09:06 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/23/23 09:06 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %09/23/23 09:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %09/23/23 09:06 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ05 WG- 091323 Lab ID: 92688066005 Collected: 09/13/23 14:46 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)98 %09/23/23 09:06 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 85.1 mg/L 09/21/23 12:475.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/20/23 02:48 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 70.3 mg/L 09/16/23 05:09 16887-00-6 M11.0 0.60 1
Sulfate 146 mg/L 09/16/23 10:53 14808-79-83.0 1.5 3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ03 WG- 091323 Lab ID: 92688066006 Collected: 09/13/23 15:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 8.8 Std. Units 09/15/23 11:0250
True Color 2000 units 09/15/23 11:02250 250 50
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/05/23 17:51 7440-36-010/02/23 09:4615.0 5.5 1
Arsenic 6.1J ug/L 10/05/23 17:51 7440-38-210/02/23 09:4610.0 3.4 1
Barium 111 ug/L 10/05/23 17:51 7440-39-310/02/23 09:4610.0 0.84 1
Beryllium 0.58J ug/L 10/05/23 17:51 7440-41-710/02/23 09:464.0 0.17 1
Boron 116 ug/L 10/05/23 17:51 7440-42-810/02/23 09:4650.0 12.4 1
Cadmium ND ug/L 10/05/23 17:51 7440-43-910/02/23 09:461.0 0.33 1
Chromium 17.5 ug/L 10/05/23 17:51 7440-47-310/02/23 09:465.0 1.7 1
Cobalt 2.5J ug/L 10/05/23 17:51 7440-48-410/02/23 09:4610.0 0.96 1
Copper 4.1J ug/L 10/05/23 17:51 7440-50-810/02/23 09:465.0 2.6 1
Lead 2.2J ug/L 10/05/23 17:51 7439-92-110/02/23 09:4610.0 2.1 1
Manganese 1390 ug/L 10/06/23 07:32 7439-96-510/02/23 09:4625.0 5.5 5
Nickel 6.4 ug/L 10/05/23 17:51 7440-02-010/02/23 09:465.0 1.0 1
Selenium ND ug/L 10/05/23 17:51 7782-49-210/02/23 09:4615.0 3.9 1
Silver ND ug/L 10/05/23 17:51 7440-22-410/02/23 09:465.0 1.0 1
Thallium ND ug/L 10/05/23 17:51 7440-28-010/02/23 09:4615.0 2.9 1
Vanadium 227 ug/L 10/05/23 17:51 7440-62-210/02/23 09:4610.0 1.0 1
Zinc 11.4J ug/L 10/05/23 17:51 7440-66-610/02/23 09:4620.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/05/23 14:43 7440-36-010/03/23 06:0415.0 5.5 1
Arsenic, Dissolved 6.5J ug/L 10/05/23 14:43 7440-38-210/03/23 06:0410.0 3.4 1
Barium, Dissolved 83.3 ug/L 10/05/23 14:43 7440-39-310/03/23 06:0410.0 0.84 1
Beryllium, Dissolved 0.41J ug/L 10/05/23 14:43 7440-41-710/03/23 06:044.0 0.17 1
Boron, Dissolved 114 ug/L 10/05/23 14:43 7440-42-810/03/23 06:0450.0 12.4 1
Cadmium, Dissolved ND ug/L 10/05/23 14:43 7440-43-910/03/23 06:041.0 0.33 1
Chromium, Dissolved 14.6 ug/L 10/05/23 14:43 7440-47-310/03/23 06:045.0 1.7 1
Cobalt, Dissolved 1.7J ug/L 10/05/23 14:43 7440-48-410/03/23 06:0410.0 0.96 1
Copper, Dissolved 2.8J ug/L 10/05/23 14:43 7440-50-810/03/23 06:045.0 2.6 1
Lead, Dissolved ND ug/L 10/05/23 14:43 7439-92-110/03/23 06:0410.0 2.1 1
Manganese, Dissolved 1210 ug/L 10/06/23 08:33 7439-96-510/03/23 06:0410.0 2.2 2
Nickel, Dissolved 5.4 ug/L 10/05/23 14:43 7440-02-010/03/23 06:045.0 1.0 1
Selenium, Dissolved ND ug/L 10/05/23 14:43 7782-49-210/03/23 06:0415.0 3.9 1
Silver, Dissolved ND ug/L 10/05/23 14:43 7440-22-410/03/23 06:045.0 1.0 1
Thallium, Dissolved ND ug/L 10/05/23 14:43 7440-28-010/03/23 06:0415.0 2.9 1
Vanadium, Dissolved 174 ug/L 10/05/23 14:43 7440-62-210/03/23 06:0410.0 1.0 1
Zinc, Dissolved 28.1 ug/L 10/05/23 14:43 7440-66-610/03/23 06:0420.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ03 WG- 091323 Lab ID: 92688066006 Collected: 09/13/23 15:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 10:39 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:47 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/20/23 20:46 83-32-909/19/23 10:3110.0 2.0 1
Acenaphthylene ND ug/L 09/20/23 20:46 208-96-809/19/23 10:3110.0 2.0 1
Acetophenone ND ug/L 09/20/23 20:46 98-86-209/19/23 10:3110.0 1.5 1
Anthracene ND ug/L 09/20/23 20:46 120-12-709/19/23 10:3110.0 2.3 1
Atrazine ND ug/L 09/20/23 20:46 1912-24-909/19/23 10:3110.0 3.2 1
Benzaldehyde ND ug/L 09/20/23 20:46 100-52-709/19/23 10:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/20/23 20:46 56-55-309/19/23 10:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/20/23 20:46 50-32-809/19/23 10:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/20/23 20:46 205-99-209/19/23 10:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/20/23 20:46 191-24-209/19/23 10:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/20/23 20:46 207-08-909/19/23 10:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/20/23 20:46 92-52-409/19/23 10:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/20/23 20:46 101-55-309/19/23 10:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/20/23 20:46 85-68-709/19/23 10:3110.0 3.1 1
Caprolactam ND ug/L 09/20/23 20:46 105-60-209/19/23 10:3110.0 6.9 1
Carbazole ND ug/L 09/20/23 20:46 86-74-809/19/23 10:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/20/23 20:46 59-50-709/19/23 10:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/20/23 20:46 106-47-809/19/23 10:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/20/23 20:46 111-91-109/19/23 10:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/20/23 20:46 111-44-409/19/23 10:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/20/23 20:46 91-58-709/19/23 10:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/20/23 20:46 95-57-809/19/23 10:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/20/23 20:46 7005-72-309/19/23 10:3110.0 2.0 1
Chrysene ND ug/L 09/20/23 20:46 218-01-909/19/23 10:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/20/23 20:46 53-70-309/19/23 10:3110.0 3.0 1
Dibenzofuran ND ug/L 09/20/23 20:46 132-64-909/19/23 10:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/20/23 20:46 91-94-109/19/23 10:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/20/23 20:46 120-83-209/19/23 10:3110.0 1.4 1
Diethylphthalate ND ug/L 09/20/23 20:46 84-66-209/19/23 10:3110.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/20/23 20:46 105-67-909/19/23 10:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/20/23 20:46 131-11-309/19/23 10:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/20/23 20:46 84-74-209/19/23 10:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/20/23 20:46 534-52-109/19/23 10:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/20/23 20:46 51-28-509/19/23 10:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/20/23 20:46 121-14-209/19/23 10:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/20/23 20:46 606-20-209/19/23 10:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/20/23 20:46 117-84-009/19/23 10:3110.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ03 WG- 091323 Lab ID: 92688066006 Collected: 09/13/23 15:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/20/23 20:46 117-81-709/19/23 10:316.0 3.7 1
Fluoranthene ND ug/L 09/20/23 20:46 206-44-009/19/23 10:3110.0 2.2 1
Fluorene ND ug/L 09/20/23 20:46 86-73-709/19/23 10:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/20/23 20:46 87-68-309/19/23 10:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/20/23 20:46 118-74-109/19/23 10:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/20/23 20:46 77-47-409/19/23 10:3110.0 1.6 1
Hexachloroethane ND ug/L 09/20/23 20:46 67-72-109/19/23 10:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/20/23 20:46 193-39-509/19/23 10:3110.0 2.9 1
Isophorone ND ug/L 09/20/23 20:46 78-59-109/19/23 10:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/20/23 20:46 91-57-609/19/23 10:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/20/23 20:46 95-48-709/19/23 10:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/20/23 20:46 15831-10-409/19/23 10:3110.0 1.2 1
Naphthalene ND ug/L 09/20/23 20:46 91-20-309/19/23 10:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/20/23 20:46 88-74-409/19/23 10:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/20/23 20:46 99-09-209/19/23 10:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/20/23 20:46 100-01-609/19/23 10:3120.0 5.1 1
Nitrobenzene ND ug/L 09/20/23 20:46 98-95-309/19/23 10:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/20/23 20:46 88-75-509/19/23 10:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/20/23 20:46 100-02-709/19/23 10:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/20/23 20:46 621-64-709/19/23 10:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/20/23 20:46 86-30-609/19/23 10:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/20/23 20:46 108-60-109/19/23 10:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/20/23 20:46 87-86-509/19/23 10:3120.0 3.8 1
Phenanthrene ND ug/L 09/20/23 20:46 85-01-809/19/23 10:3110.0 2.0 1
Phenol ND ug/L 09/20/23 20:46 108-95-209/19/23 10:3110.0 1.4 1
Pyrene ND ug/L 09/20/23 20:46 129-00-009/19/23 10:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/20/23 20:46 95-95-409/19/23 10:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/20/23 20:46 88-06-209/19/23 10:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)94 %09/20/23 20:46 4165-60-009/19/23 10:3110-138 1
2-Fluorobiphenyl (S)92 %09/20/23 20:46 321-60-809/19/23 10:3110-130 1
Terphenyl-d14 (S)111 %09/20/23 20:46 1718-51-009/19/23 10:3119-191 1
Phenol-d6 (S)26 %09/20/23 20:46 13127-88-309/19/23 10:3110-130 1
2-Fluorophenol (S)7 %09/20/23 20:46 367-12-4 S009/19/23 10:3110-130 1
2,4,6-Tribromophenol (S)20 %09/20/23 20:46 118-79-609/19/23 10:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/23/23 06:22 67-64-125.0 5.1 1
Benzene ND ug/L 09/23/23 06:22 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/23/23 06:22 75-27-41.0 0.31 1
Bromoform ND ug/L 09/23/23 06:22 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/23/23 06:22 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/23/23 06:22 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/23/23 06:22 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ03 WG- 091323 Lab ID: 92688066006 Collected: 09/13/23 15:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/23/23 06:22 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/23/23 06:22 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/23/23 06:22 75-00-31.0 0.65 1
Chloroform ND ug/L 09/23/23 06:22 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/23/23 06:22 74-87-31.0 0.54 1
Cyclohexane 1.0 ug/L 09/23/23 06:22 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/23/23 06:22 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/23/23 06:22 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/23/23 06:22 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/23/23 06:22 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/23/23 06:22 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/23/23 06:22 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/23/23 06:22 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/23/23 06:22 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/23/23 06:22 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/23/23 06:22 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/23/23 06:22 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/23/23 06:22 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/23/23 06:22 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/23/23 06:22 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/23/23 06:22 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/23/23 06:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/23/23 06:22 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/23/23 06:22 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/23/23 06:22 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/23/23 06:22 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/23/23 06:22 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/23/23 06:22 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/23/23 06:22 1634-04-41.0 0.42 1
Styrene ND ug/L 09/23/23 06:22 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/23/23 06:22 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/23/23 06:22 127-18-41.0 0.29 1
Toluene ND ug/L 09/23/23 06:22 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/23/23 06:22 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/23/23 06:22 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/23/23 06:22 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/23/23 06:22 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/23/23 06:22 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/23/23 06:22 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/23/23 06:22 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/23/23 06:22 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/23/23 06:22 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %09/23/23 06:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %09/23/23 06:22 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ03 WG- 091323 Lab ID: 92688066006 Collected: 09/13/23 15:27 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)99 %09/23/23 06:22 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 947 mg/L 09/21/23 13:085.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 1.2 mg/L 09/20/23 02:54 18496-25-81.0 0.22 10
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 28.8 mg/L 09/16/23 06:16 16887-00-620.0 12.0 20
Sulfate 178 mg/L 09/16/23 06:16 14808-79-820.0 10.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 WG- 091323 Lab ID: 92688066007 Collected: 09/13/23 16:56 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.6 Std. Units 09/15/23 11:051
True Color ND units 09/15/23 11:055.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/04/23 00:10 7440-36-010/02/23 09:4615.0 5.5 1
Arsenic ND ug/L 10/04/23 00:10 7440-38-210/02/23 09:4610.0 3.4 1
Barium 105 ug/L 10/04/23 00:10 7440-39-310/02/23 09:4610.0 0.84 1
Beryllium ND ug/L 10/04/23 00:10 7440-41-710/02/23 09:464.0 0.17 1
Boron 89.5 ug/L 10/04/23 00:10 7440-42-810/02/23 09:4650.0 12.4 1
Cadmium ND ug/L 10/04/23 00:10 7440-43-910/02/23 09:461.0 0.33 1
Chromium ND ug/L 10/04/23 00:10 7440-47-310/02/23 09:465.0 1.7 1
Cobalt ND ug/L 10/04/23 00:10 7440-48-410/02/23 09:4610.0 0.96 1
Copper ND ug/L 10/04/23 00:10 7440-50-810/02/23 09:465.0 2.6 1
Lead ND ug/L 10/04/23 00:10 7439-92-110/02/23 09:4610.0 2.1 1
Manganese 2430 ug/L 10/05/23 17:55 7439-96-510/02/23 09:4650.0 11.0 10
Nickel ND ug/L 10/04/23 00:10 7440-02-010/02/23 09:465.0 1.0 1
Selenium ND ug/L 10/04/23 00:10 7782-49-210/02/23 09:4615.0 3.9 1
Silver ND ug/L 10/04/23 00:10 7440-22-410/02/23 09:465.0 1.0 1
Thallium ND ug/L 10/04/23 00:10 7440-28-010/02/23 09:4615.0 2.9 1
Vanadium ND ug/L 10/04/23 00:10 7440-62-210/02/23 09:4610.0 1.0 1
Zinc 69.2 ug/L 10/04/23 00:10 7440-66-610/02/23 09:4620.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/05/23 14:47 7440-36-010/03/23 06:0415.0 5.5 1
Arsenic, Dissolved ND ug/L 10/05/23 14:47 7440-38-210/03/23 06:0410.0 3.4 1
Barium, Dissolved 98.3 ug/L 10/05/23 14:47 7440-39-310/03/23 06:0410.0 0.84 1
Beryllium, Dissolved ND ug/L 10/05/23 14:47 7440-41-710/03/23 06:044.0 0.17 1
Boron, Dissolved 87.9 ug/L 10/05/23 14:47 7440-42-810/03/23 06:0450.0 12.4 1
Cadmium, Dissolved 0.39J ug/L 10/05/23 14:47 7440-43-910/03/23 06:041.0 0.33 1
Chromium, Dissolved ND ug/L 10/05/23 14:47 7440-47-310/03/23 06:045.0 1.7 1
Cobalt, Dissolved ND ug/L 10/05/23 14:47 7440-48-410/03/23 06:0410.0 0.96 1
Copper, Dissolved ND ug/L 10/05/23 14:47 7440-50-810/03/23 06:045.0 2.6 1
Lead, Dissolved ND ug/L 10/05/23 14:47 7439-92-110/03/23 06:0410.0 2.1 1
Manganese, Dissolved 2070 ug/L 10/06/23 08:43 7439-96-510/03/23 06:0425.0 5.5 5
Nickel, Dissolved ND ug/L 10/05/23 14:47 7440-02-010/03/23 06:045.0 1.0 1
Selenium, Dissolved ND ug/L 10/05/23 14:47 7782-49-210/03/23 06:0415.0 3.9 1
Silver, Dissolved ND ug/L 10/05/23 14:47 7440-22-410/03/23 06:045.0 1.0 1
Thallium, Dissolved ND ug/L 10/05/23 14:47 7440-28-010/03/23 06:0415.0 2.9 1
Vanadium, Dissolved ND ug/L 10/05/23 14:47 7440-62-210/03/23 06:0410.0 1.0 1
Zinc, Dissolved 64.4 ug/L 10/05/23 14:47 7440-66-610/03/23 06:0420.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 WG- 091323 Lab ID: 92688066007 Collected: 09/13/23 16:56 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 10:41 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:50 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/20/23 21:12 83-32-909/19/23 10:3110.0 2.0 1
Acenaphthylene ND ug/L 09/20/23 21:12 208-96-809/19/23 10:3110.0 2.0 1
Acetophenone ND ug/L 09/20/23 21:12 98-86-209/19/23 10:3110.0 1.5 1
Anthracene ND ug/L 09/20/23 21:12 120-12-709/19/23 10:3110.0 2.3 1
Atrazine ND ug/L 09/20/23 21:12 1912-24-909/19/23 10:3110.0 3.2 1
Benzaldehyde ND ug/L 09/20/23 21:12 100-52-709/19/23 10:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/20/23 21:12 56-55-309/19/23 10:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/20/23 21:12 50-32-809/19/23 10:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/20/23 21:12 205-99-209/19/23 10:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/20/23 21:12 191-24-209/19/23 10:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/20/23 21:12 207-08-909/19/23 10:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/20/23 21:12 92-52-409/19/23 10:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/20/23 21:12 101-55-309/19/23 10:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/20/23 21:12 85-68-709/19/23 10:3110.0 3.1 1
Caprolactam ND ug/L 09/20/23 21:12 105-60-209/19/23 10:3110.0 6.9 1
Carbazole ND ug/L 09/20/23 21:12 86-74-809/19/23 10:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/20/23 21:12 59-50-709/19/23 10:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/20/23 21:12 106-47-809/19/23 10:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/20/23 21:12 111-91-109/19/23 10:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/20/23 21:12 111-44-409/19/23 10:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/20/23 21:12 91-58-709/19/23 10:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/20/23 21:12 95-57-809/19/23 10:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/20/23 21:12 7005-72-309/19/23 10:3110.0 2.0 1
Chrysene ND ug/L 09/20/23 21:12 218-01-909/19/23 10:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/20/23 21:12 53-70-309/19/23 10:3110.0 3.0 1
Dibenzofuran ND ug/L 09/20/23 21:12 132-64-909/19/23 10:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/20/23 21:12 91-94-109/19/23 10:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/20/23 21:12 120-83-209/19/23 10:3110.0 1.4 1
Diethylphthalate ND ug/L 09/20/23 21:12 84-66-209/19/23 10:3110.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/20/23 21:12 105-67-909/19/23 10:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/20/23 21:12 131-11-309/19/23 10:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/20/23 21:12 84-74-209/19/23 10:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/20/23 21:12 534-52-109/19/23 10:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/20/23 21:12 51-28-509/19/23 10:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/20/23 21:12 121-14-209/19/23 10:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/20/23 21:12 606-20-209/19/23 10:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/20/23 21:12 117-84-009/19/23 10:3110.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 WG- 091323 Lab ID: 92688066007 Collected: 09/13/23 16:56 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/20/23 21:12 117-81-709/19/23 10:316.0 3.7 1
Fluoranthene ND ug/L 09/20/23 21:12 206-44-009/19/23 10:3110.0 2.2 1
Fluorene ND ug/L 09/20/23 21:12 86-73-709/19/23 10:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/20/23 21:12 87-68-309/19/23 10:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/20/23 21:12 118-74-109/19/23 10:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/20/23 21:12 77-47-409/19/23 10:3110.0 1.6 1
Hexachloroethane ND ug/L 09/20/23 21:12 67-72-109/19/23 10:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/20/23 21:12 193-39-509/19/23 10:3110.0 2.9 1
Isophorone ND ug/L 09/20/23 21:12 78-59-109/19/23 10:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/20/23 21:12 91-57-609/19/23 10:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/20/23 21:12 95-48-709/19/23 10:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/20/23 21:12 15831-10-409/19/23 10:3110.0 1.2 1
Naphthalene ND ug/L 09/20/23 21:12 91-20-309/19/23 10:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/20/23 21:12 88-74-409/19/23 10:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/20/23 21:12 99-09-209/19/23 10:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/20/23 21:12 100-01-609/19/23 10:3120.0 5.1 1
Nitrobenzene ND ug/L 09/20/23 21:12 98-95-309/19/23 10:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/20/23 21:12 88-75-509/19/23 10:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/20/23 21:12 100-02-709/19/23 10:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/20/23 21:12 621-64-709/19/23 10:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/20/23 21:12 86-30-609/19/23 10:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/20/23 21:12 108-60-109/19/23 10:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/20/23 21:12 87-86-509/19/23 10:3120.0 3.8 1
Phenanthrene ND ug/L 09/20/23 21:12 85-01-809/19/23 10:3110.0 2.0 1
Phenol ND ug/L 09/20/23 21:12 108-95-209/19/23 10:3110.0 1.4 1
Pyrene ND ug/L 09/20/23 21:12 129-00-009/19/23 10:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/20/23 21:12 95-95-409/19/23 10:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/20/23 21:12 88-06-209/19/23 10:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)90 %09/20/23 21:12 4165-60-0 1g09/19/23 10:3110-138 1
2-Fluorobiphenyl (S)86 %09/20/23 21:12 321-60-809/19/23 10:3110-130 1
Terphenyl-d14 (S)100 %09/20/23 21:12 1718-51-009/19/23 10:3119-191 1
Phenol-d6 (S)21 %09/20/23 21:12 13127-88-309/19/23 10:3110-130 1
2-Fluorophenol (S)4 %09/20/23 21:12 367-12-4 S009/19/23 10:3110-130 1
2,4,6-Tribromophenol (S)2 %09/20/23 21:12 118-79-6 S009/19/23 10:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/23/23 09:42 67-64-125.0 5.1 1
Benzene ND ug/L 09/23/23 09:42 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/23/23 09:42 75-27-41.0 0.31 1
Bromoform ND ug/L 09/23/23 09:42 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/23/23 09:42 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/23/23 09:42 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/23/23 09:42 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 WG- 091323 Lab ID: 92688066007 Collected: 09/13/23 16:56 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/23/23 09:42 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/23/23 09:42 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/23/23 09:42 75-00-31.0 0.65 1
Chloroform ND ug/L 09/23/23 09:42 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/23/23 09:42 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/23/23 09:42 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/23/23 09:42 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/23/23 09:42 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/23/23 09:42 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/23/23 09:42 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/23/23 09:42 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/23/23 09:42 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/23/23 09:42 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/23/23 09:42 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/23/23 09:42 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/23/23 09:42 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/23/23 09:42 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/23/23 09:42 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/23/23 09:42 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/23/23 09:42 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/23/23 09:42 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/23/23 09:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/23/23 09:42 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/23/23 09:42 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/23/23 09:42 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/23/23 09:42 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/23/23 09:42 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/23/23 09:42 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/23/23 09:42 1634-04-41.0 0.42 1
Styrene ND ug/L 09/23/23 09:42 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/23/23 09:42 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/23/23 09:42 127-18-41.0 0.29 1
Toluene ND ug/L 09/23/23 09:42 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/23/23 09:42 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/23/23 09:42 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/23/23 09:42 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/23/23 09:42 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/23/23 09:42 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/23/23 09:42 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/23/23 09:42 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/23/23 09:42 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/23/23 09:42 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %09/23/23 09:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %09/23/23 09:42 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 WG- 091323 Lab ID: 92688066007 Collected: 09/13/23 16:56 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)98 %09/23/23 09:42 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 108 mg/L 09/21/23 13:205.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/20/23 02:55 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 52.9 mg/L 09/16/23 06:30 16887-00-61.0 0.60 1
Sulfate 66.4 mg/L 09/16/23 06:30 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 HG- 091323 Lab ID: 92688066008 Collected: 09/13/23 16:58 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.5 Std. Units 09/15/23 11:061
True Color ND units 09/15/23 11:065.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/04/23 00:14 7440-36-010/02/23 09:4615.0 5.5 1
Arsenic ND ug/L 10/04/23 00:14 7440-38-210/02/23 09:4610.0 3.4 1
Barium 105 ug/L 10/04/23 00:14 7440-39-310/02/23 09:4610.0 0.84 1
Beryllium ND ug/L 10/04/23 00:14 7440-41-710/02/23 09:464.0 0.17 1
Boron 88.5 ug/L 10/04/23 00:14 7440-42-810/02/23 09:4650.0 12.4 1
Cadmium ND ug/L 10/04/23 00:14 7440-43-910/02/23 09:461.0 0.33 1
Chromium ND ug/L 10/04/23 00:14 7440-47-310/02/23 09:465.0 1.7 1
Cobalt ND ug/L 10/04/23 00:14 7440-48-410/02/23 09:4610.0 0.96 1
Copper ND ug/L 10/04/23 00:14 7440-50-810/02/23 09:465.0 2.6 1
Lead ND ug/L 10/04/23 00:14 7439-92-110/02/23 09:4610.0 2.1 1
Manganese 2320 ug/L 10/05/23 17:58 7439-96-510/02/23 09:4650.0 11.0 10
Nickel ND ug/L 10/04/23 00:14 7440-02-010/02/23 09:465.0 1.0 1
Selenium ND ug/L 10/04/23 00:14 7782-49-210/02/23 09:4615.0 3.9 1
Silver ND ug/L 10/04/23 00:14 7440-22-410/02/23 09:465.0 1.0 1
Thallium ND ug/L 10/04/23 00:14 7440-28-010/02/23 09:4615.0 2.9 1
Vanadium ND ug/L 10/04/23 00:14 7440-62-210/02/23 09:4610.0 1.0 1
Zinc 67.1 ug/L 10/04/23 00:14 7440-66-610/02/23 09:4620.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/05/23 14:51 7440-36-010/03/23 06:0415.0 5.5 1
Arsenic, Dissolved ND ug/L 10/05/23 14:51 7440-38-210/03/23 06:0410.0 3.4 1
Barium, Dissolved 98.0 ug/L 10/05/23 14:51 7440-39-310/03/23 06:0410.0 0.84 1
Beryllium, Dissolved ND ug/L 10/05/23 14:51 7440-41-710/03/23 06:044.0 0.17 1
Boron, Dissolved 88.7 ug/L 10/05/23 14:51 7440-42-810/03/23 06:0450.0 12.4 1
Cadmium, Dissolved 0.33J ug/L 10/05/23 14:51 7440-43-910/03/23 06:041.0 0.33 1
Chromium, Dissolved ND ug/L 10/05/23 14:51 7440-47-310/03/23 06:045.0 1.7 1
Cobalt, Dissolved ND ug/L 10/05/23 14:51 7440-48-410/03/23 06:0410.0 0.96 1
Copper, Dissolved ND ug/L 10/05/23 14:51 7440-50-810/03/23 06:045.0 2.6 1
Lead, Dissolved ND ug/L 10/05/23 14:51 7439-92-110/03/23 06:0410.0 2.1 1
Manganese, Dissolved 2280 ug/L 10/06/23 08:47 7439-96-510/03/23 06:0425.0 5.5 5
Nickel, Dissolved ND ug/L 10/05/23 14:51 7440-02-010/03/23 06:045.0 1.0 1
Selenium, Dissolved ND ug/L 10/05/23 14:51 7782-49-210/03/23 06:0415.0 3.9 1
Silver, Dissolved ND ug/L 10/05/23 14:51 7440-22-410/03/23 06:045.0 1.0 1
Thallium, Dissolved ND ug/L 10/05/23 14:51 7440-28-010/03/23 06:0415.0 2.9 1
Vanadium, Dissolved ND ug/L 10/05/23 14:51 7440-62-210/03/23 06:0410.0 1.0 1
Zinc, Dissolved 61.8 ug/L 10/05/23 14:51 7440-66-610/03/23 06:0420.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 HG- 091323 Lab ID: 92688066008 Collected: 09/13/23 16:58 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 10:43 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:56 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/20/23 21:37 83-32-909/19/23 10:3110.0 2.0 1
Acenaphthylene ND ug/L 09/20/23 21:37 208-96-809/19/23 10:3110.0 2.0 1
Acetophenone ND ug/L 09/20/23 21:37 98-86-209/19/23 10:3110.0 1.5 1
Anthracene ND ug/L 09/20/23 21:37 120-12-709/19/23 10:3110.0 2.3 1
Atrazine ND ug/L 09/20/23 21:37 1912-24-909/19/23 10:3110.0 3.2 1
Benzaldehyde ND ug/L 09/20/23 21:37 100-52-709/19/23 10:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/20/23 21:37 56-55-309/19/23 10:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/20/23 21:37 50-32-809/19/23 10:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/20/23 21:37 205-99-209/19/23 10:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/20/23 21:37 191-24-209/19/23 10:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/20/23 21:37 207-08-909/19/23 10:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/20/23 21:37 92-52-409/19/23 10:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/20/23 21:37 101-55-309/19/23 10:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/20/23 21:37 85-68-709/19/23 10:3110.0 3.1 1
Caprolactam ND ug/L 09/20/23 21:37 105-60-209/19/23 10:3110.0 6.9 1
Carbazole ND ug/L 09/20/23 21:37 86-74-809/19/23 10:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/20/23 21:37 59-50-709/19/23 10:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/20/23 21:37 106-47-809/19/23 10:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/20/23 21:37 111-91-109/19/23 10:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/20/23 21:37 111-44-409/19/23 10:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/20/23 21:37 91-58-709/19/23 10:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/20/23 21:37 95-57-809/19/23 10:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/20/23 21:37 7005-72-309/19/23 10:3110.0 2.0 1
Chrysene ND ug/L 09/20/23 21:37 218-01-909/19/23 10:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/20/23 21:37 53-70-309/19/23 10:3110.0 3.0 1
Dibenzofuran ND ug/L 09/20/23 21:37 132-64-909/19/23 10:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/20/23 21:37 91-94-109/19/23 10:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/20/23 21:37 120-83-209/19/23 10:3110.0 1.4 1
Diethylphthalate ND ug/L 09/20/23 21:37 84-66-209/19/23 10:3110.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/20/23 21:37 105-67-909/19/23 10:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/20/23 21:37 131-11-309/19/23 10:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/20/23 21:37 84-74-209/19/23 10:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/20/23 21:37 534-52-109/19/23 10:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/20/23 21:37 51-28-509/19/23 10:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/20/23 21:37 121-14-209/19/23 10:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/20/23 21:37 606-20-209/19/23 10:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/20/23 21:37 117-84-009/19/23 10:3110.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 HG- 091323 Lab ID: 92688066008 Collected: 09/13/23 16:58 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate 4.4J ug/L 09/20/23 21:37 117-81-709/19/23 10:316.0 3.7 1
Fluoranthene ND ug/L 09/20/23 21:37 206-44-009/19/23 10:3110.0 2.2 1
Fluorene ND ug/L 09/20/23 21:37 86-73-709/19/23 10:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/20/23 21:37 87-68-309/19/23 10:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/20/23 21:37 118-74-109/19/23 10:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/20/23 21:37 77-47-409/19/23 10:3110.0 1.6 1
Hexachloroethane ND ug/L 09/20/23 21:37 67-72-109/19/23 10:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/20/23 21:37 193-39-509/19/23 10:3110.0 2.9 1
Isophorone ND ug/L 09/20/23 21:37 78-59-109/19/23 10:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/20/23 21:37 91-57-609/19/23 10:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/20/23 21:37 95-48-709/19/23 10:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/20/23 21:37 15831-10-409/19/23 10:3110.0 1.2 1
Naphthalene ND ug/L 09/20/23 21:37 91-20-309/19/23 10:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/20/23 21:37 88-74-409/19/23 10:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/20/23 21:37 99-09-209/19/23 10:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/20/23 21:37 100-01-609/19/23 10:3120.0 5.1 1
Nitrobenzene ND ug/L 09/20/23 21:37 98-95-309/19/23 10:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/20/23 21:37 88-75-509/19/23 10:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/20/23 21:37 100-02-709/19/23 10:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/20/23 21:37 621-64-709/19/23 10:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/20/23 21:37 86-30-609/19/23 10:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/20/23 21:37 108-60-109/19/23 10:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/20/23 21:37 87-86-509/19/23 10:3120.0 3.8 1
Phenanthrene ND ug/L 09/20/23 21:37 85-01-809/19/23 10:3110.0 2.0 1
Phenol ND ug/L 09/20/23 21:37 108-95-209/19/23 10:3110.0 1.4 1
Pyrene ND ug/L 09/20/23 21:37 129-00-009/19/23 10:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/20/23 21:37 95-95-409/19/23 10:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/20/23 21:37 88-06-209/19/23 10:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)54 %09/20/23 21:37 4165-60-009/19/23 10:3110-138 1
2-Fluorobiphenyl (S)56 %09/20/23 21:37 321-60-809/19/23 10:3110-130 1
Terphenyl-d14 (S)116 %09/20/23 21:37 1718-51-009/19/23 10:3119-191 1
Phenol-d6 (S)28 %09/20/23 21:37 13127-88-309/19/23 10:3110-130 1
2-Fluorophenol (S)39 %09/20/23 21:37 367-12-409/19/23 10:3110-130 1
2,4,6-Tribromophenol (S)97 %09/20/23 21:37 118-79-609/19/23 10:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/24/23 18:14 67-64-125.0 5.1 1
Benzene ND ug/L 09/24/23 18:14 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/24/23 18:14 75-27-41.0 0.31 1
Bromoform ND ug/L 09/24/23 18:14 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/24/23 18:14 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/24/23 18:14 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/24/23 18:14 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 HG- 091323 Lab ID: 92688066008 Collected: 09/13/23 16:58 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/24/23 18:14 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/24/23 18:14 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/24/23 18:14 75-00-31.0 0.65 1
Chloroform ND ug/L 09/24/23 18:14 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/24/23 18:14 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/24/23 18:14 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/24/23 18:14 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/24/23 18:14 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/24/23 18:14 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/24/23 18:14 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/24/23 18:14 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/24/23 18:14 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/24/23 18:14 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/24/23 18:14 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/24/23 18:14 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/24/23 18:14 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/24/23 18:14 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/24/23 18:14 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/24/23 18:14 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/24/23 18:14 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/24/23 18:14 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/24/23 18:14 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/24/23 18:14 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/24/23 18:14 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/24/23 18:14 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/24/23 18:14 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/24/23 18:14 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/24/23 18:14 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/24/23 18:14 1634-04-41.0 0.42 1
Styrene ND ug/L 09/24/23 18:14 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/24/23 18:14 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/24/23 18:14 127-18-41.0 0.29 1
Toluene ND ug/L 09/24/23 18:14 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/24/23 18:14 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/24/23 18:14 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/24/23 18:14 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/24/23 18:14 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/24/23 18:14 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/24/23 18:14 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/24/23 18:14 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/24/23 18:14 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/24/23 18:14 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %09/24/23 18:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/24/23 18:14 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: PZ17 HG- 091323 Lab ID: 92688066008 Collected: 09/13/23 16:58 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)99 %09/24/23 18:14 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 97.1 mg/L 09/21/23 13:435.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/20/23 02:55 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 52.3 mg/L 09/16/23 06:43 16887-00-61.0 0.60 1
Sulfate 66.3 mg/L 09/16/23 06:43 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: BR02 WG- 091323 Lab ID: 92688066009 Collected: 09/13/23 16:58 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 7.5 Std. Units 09/15/23 11:071
True Color 5.0 units 09/15/23 11:075.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony 7.1J ug/L 10/04/23 00:17 7440-36-010/02/23 09:4615.0 5.5 1
Arsenic ND ug/L 10/04/23 00:17 7440-38-210/02/23 09:4610.0 3.4 1
Barium 196 ug/L 10/04/23 00:17 7440-39-310/02/23 09:4610.0 0.84 1
Beryllium ND ug/L 10/04/23 00:17 7440-41-710/02/23 09:464.0 0.17 1
Boron 28.3J ug/L 10/04/23 00:17 7440-42-810/02/23 09:4650.0 12.4 1
Cadmium 0.47J ug/L 10/04/23 00:17 7440-43-910/02/23 09:461.0 0.33 1
Chromium 91.2 ug/L 10/04/23 00:17 7440-47-310/02/23 09:465.0 1.7 1
Cobalt 8.1J ug/L 10/04/23 00:17 7440-48-410/02/23 09:4610.0 0.96 1
Copper 7.2 ug/L 10/04/23 00:17 7440-50-810/02/23 09:465.0 2.6 1
Lead 7.0J ug/L 10/04/23 00:17 7439-92-110/02/23 09:4610.0 2.1 1
Manganese 216 ug/L 10/04/23 00:17 7439-96-510/02/23 09:465.0 1.1 1
Nickel 30.9 ug/L 10/04/23 00:17 7440-02-010/02/23 09:465.0 1.0 1
Selenium ND ug/L 10/04/23 00:17 7782-49-210/02/23 09:4615.0 3.9 1
Silver ND ug/L 10/04/23 00:17 7440-22-410/02/23 09:465.0 1.0 1
Thallium ND ug/L 10/04/23 00:17 7440-28-010/02/23 09:4615.0 2.9 1
Vanadium 27.3 ug/L 10/04/23 00:17 7440-62-210/02/23 09:4610.0 1.0 1
Zinc 71.0 ug/L 10/04/23 00:17 7440-66-610/02/23 09:4620.0 11.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury 0.31 ug/L 10/09/23 10:46 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/21/23 15:00 83-32-909/20/23 10:0210.0 2.0 1
Acenaphthylene ND ug/L 09/21/23 15:00 208-96-809/20/23 10:0210.0 2.0 1
Acetophenone ND ug/L 09/21/23 15:00 98-86-209/20/23 10:0210.0 1.5 1
Anthracene ND ug/L 09/21/23 15:00 120-12-709/20/23 10:0210.0 2.3 1
Atrazine ND ug/L 09/21/23 15:00 1912-24-9 L109/20/23 10:0210.0 3.2 1
Benzaldehyde ND ug/L 09/21/23 15:00 100-52-709/20/23 10:0210.0 3.6 1
Benzo(a)anthracene ND ug/L 09/21/23 15:00 56-55-309/20/23 10:0210.0 2.7 1
Benzo(a)pyrene ND ug/L 09/21/23 15:00 50-32-809/20/23 10:0210.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/21/23 15:00 205-99-209/20/23 10:0210.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/21/23 15:00 191-24-209/20/23 10:0210.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/21/23 15:00 207-08-909/20/23 10:0210.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/21/23 15:00 92-52-409/20/23 10:0210.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/21/23 15:00 101-55-309/20/23 10:0210.0 1.8 1
Butylbenzylphthalate ND ug/L 09/21/23 15:00 85-68-709/20/23 10:0210.0 3.1 1
Caprolactam ND ug/L 09/21/23 15:00 105-60-209/20/23 10:0210.0 6.9 1
Carbazole ND ug/L 09/21/23 15:00 86-74-809/20/23 10:0210.0 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: BR02 WG- 091323 Lab ID: 92688066009 Collected: 09/13/23 16:58 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
4-Chloro-3-methylphenol ND ug/L 09/21/23 15:00 59-50-709/20/23 10:0210.0 3.3 1
4-Chloroaniline ND ug/L 09/21/23 15:00 106-47-809/20/23 10:0220.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/21/23 15:00 111-91-109/20/23 10:0210.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/21/23 15:00 111-44-409/20/23 10:0210.0 1.9 1
2-Chloronaphthalene ND ug/L 09/21/23 15:00 91-58-709/20/23 10:0210.0 1.7 1
2-Chlorophenol ND ug/L 09/21/23 15:00 95-57-809/20/23 10:0210.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/21/23 15:00 7005-72-309/20/23 10:0210.0 2.0 1
Chrysene ND ug/L 09/21/23 15:00 218-01-909/20/23 10:0210.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/21/23 15:00 53-70-309/20/23 10:0210.0 3.0 1
Dibenzofuran ND ug/L 09/21/23 15:00 132-64-909/20/23 10:0210.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/21/23 15:00 91-94-109/20/23 10:0220.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/21/23 15:00 120-83-209/20/23 10:0210.0 1.4 1
Diethylphthalate ND ug/L 09/21/23 15:00 84-66-209/20/23 10:0210.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/21/23 15:00 105-67-909/20/23 10:0210.0 1.7 1
Dimethylphthalate ND ug/L 09/21/23 15:00 131-11-309/20/23 10:0210.0 2.1 1
Di-n-butylphthalate ND ug/L 09/21/23 15:00 84-74-209/20/23 10:0210.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/21/23 15:00 534-52-109/20/23 10:0220.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/21/23 15:00 51-28-509/20/23 10:0250.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/21/23 15:00 121-14-209/20/23 10:0210.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/21/23 15:00 606-20-209/20/23 10:0210.0 1.7 1
Di-n-octylphthalate ND ug/L 09/21/23 15:00 117-84-009/20/23 10:0210.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/21/23 15:00 117-81-709/20/23 10:026.0 3.7 1
Fluoranthene ND ug/L 09/21/23 15:00 206-44-009/20/23 10:0210.0 2.2 1
Fluorene ND ug/L 09/21/23 15:00 86-73-709/20/23 10:0210.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/21/23 15:00 87-68-309/20/23 10:0210.0 1.8 1
Hexachlorobenzene ND ug/L 09/21/23 15:00 118-74-109/20/23 10:0210.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/21/23 15:00 77-47-409/20/23 10:0210.0 1.6 1
Hexachloroethane ND ug/L 09/21/23 15:00 67-72-109/20/23 10:0210.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/21/23 15:00 193-39-509/20/23 10:0210.0 2.9 1
Isophorone ND ug/L 09/21/23 15:00 78-59-109/20/23 10:0210.0 1.7 1
2-Methylnaphthalene ND ug/L 09/21/23 15:00 91-57-609/20/23 10:0210.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/21/23 15:00 95-48-709/20/23 10:0210.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/21/23 15:00 15831-10-409/20/23 10:0210.0 1.2 1
Naphthalene ND ug/L 09/21/23 15:00 91-20-309/20/23 10:0210.0 2.1 1
2-Nitroaniline ND ug/L 09/21/23 15:00 88-74-409/20/23 10:0220.0 3.0 1
3-Nitroaniline ND ug/L 09/21/23 15:00 99-09-209/20/23 10:0220.0 3.8 1
4-Nitroaniline ND ug/L 09/21/23 15:00 100-01-609/20/23 10:0220.0 5.1 1
Nitrobenzene ND ug/L 09/21/23 15:00 98-95-309/20/23 10:0210.0 1.9 1
2-Nitrophenol ND ug/L 09/21/23 15:00 88-75-509/20/23 10:0210.0 1.4 1
4-Nitrophenol ND ug/L 09/21/23 15:00 100-02-709/20/23 10:0250.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/21/23 15:00 621-64-709/20/23 10:0210.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/21/23 15:00 86-30-609/20/23 10:0210.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/21/23 15:00 108-60-109/20/23 10:0210.0 1.2 1
Pentachlorophenol ND ug/L 09/21/23 15:00 87-86-509/20/23 10:0220.0 3.8 1
Phenanthrene ND ug/L 09/21/23 15:00 85-01-809/20/23 10:0210.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: BR02 WG- 091323 Lab ID: 92688066009 Collected: 09/13/23 16:58 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Phenol ND ug/L 09/21/23 15:00 108-95-209/20/23 10:0210.0 1.4 1
Pyrene ND ug/L 09/21/23 15:00 129-00-009/20/23 10:0210.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/21/23 15:00 95-95-409/20/23 10:0210.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/21/23 15:00 88-06-209/20/23 10:0210.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)108 %09/21/23 15:00 4165-60-009/20/23 10:0210-138 1
2-Fluorobiphenyl (S)105 %09/21/23 15:00 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)119 %09/21/23 15:00 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)44 %09/21/23 15:00 13127-88-309/20/23 10:0210-130 1
2-Fluorophenol (S)22 %09/21/23 15:00 367-12-409/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)36 %09/21/23 15:00 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/24/23 18:32 67-64-125.0 5.1 1
Benzene ND ug/L 09/24/23 18:32 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/24/23 18:32 75-27-41.0 0.31 1
Bromoform ND ug/L 09/24/23 18:32 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/24/23 18:32 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/24/23 18:32 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/24/23 18:32 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/24/23 18:32 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/24/23 18:32 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/24/23 18:32 75-00-31.0 0.65 1
Chloroform ND ug/L 09/24/23 18:32 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/24/23 18:32 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/24/23 18:32 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/24/23 18:32 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/24/23 18:32 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/24/23 18:32 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/24/23 18:32 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/24/23 18:32 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/24/23 18:32 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/24/23 18:32 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/24/23 18:32 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/24/23 18:32 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/24/23 18:32 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/24/23 18:32 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/24/23 18:32 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/24/23 18:32 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/24/23 18:32 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/24/23 18:32 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/24/23 18:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/24/23 18:32 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/24/23 18:32 98-82-81.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: BR02 WG- 091323 Lab ID: 92688066009 Collected: 09/13/23 16:58 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Methyl acetate ND ug/L 09/24/23 18:32 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/24/23 18:32 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/24/23 18:32 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/24/23 18:32 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/24/23 18:32 1634-04-41.0 0.42 1
Styrene ND ug/L 09/24/23 18:32 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/24/23 18:32 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/24/23 18:32 127-18-41.0 0.29 1
Toluene ND ug/L 09/24/23 18:32 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/24/23 18:32 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/24/23 18:32 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/24/23 18:32 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/24/23 18:32 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/24/23 18:32 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/24/23 18:32 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/24/23 18:32 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/24/23 18:32 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/24/23 18:32 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)96 %09/24/23 18:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/24/23 18:32 17060-07-070-130 1
Toluene-d8 (S)98 %09/24/23 18:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: Trip Blank Lab ID: 92688066010 Collected: 09/13/23 09:00 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/21/23 03:28 67-64-1 v225.0 5.1 1
Benzene ND ug/L 09/21/23 03:28 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/21/23 03:28 75-27-41.0 0.31 1
Bromoform ND ug/L 09/21/23 03:28 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/21/23 03:28 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/21/23 03:28 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/21/23 03:28 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/21/23 03:28 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/21/23 03:28 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/21/23 03:28 75-00-31.0 0.65 1
Chloroform ND ug/L 09/21/23 03:28 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/21/23 03:28 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/21/23 03:28 110-82-7 v21.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/21/23 03:28 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/21/23 03:28 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/21/23 03:28 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/21/23 03:28 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/21/23 03:28 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/21/23 03:28 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/21/23 03:28 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/21/23 03:28 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/21/23 03:28 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/21/23 03:28 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/21/23 03:28 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/21/23 03:28 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/21/23 03:28 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/21/23 03:28 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/21/23 03:28 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/21/23 03:28 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/21/23 03:28 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/21/23 03:28 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/21/23 03:28 79-20-9 v210.0 2.4 1
Methylcyclohexane ND ug/L 09/21/23 03:28 108-87-2 v210.0 1.5 1
Methylene Chloride ND ug/L 09/21/23 03:28 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/21/23 03:28 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/21/23 03:28 1634-04-41.0 0.42 1
Styrene ND ug/L 09/21/23 03:28 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/21/23 03:28 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/21/23 03:28 127-18-41.0 0.29 1
Toluene ND ug/L 09/21/23 03:28 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/21/23 03:28 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/21/23 03:28 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/21/23 03:28 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/21/23 03:28 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/21/23 03:28 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 116
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Sample: Trip Blank Lab ID: 92688066010 Collected: 09/13/23 09:00 Received: 09/14/23 07:53 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/21/23 03:28 76-13-1 v21.0 0.32 1
Vinyl chloride ND ug/L 09/21/23 03:28 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/21/23 03:28 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/21/23 03:28 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %09/21/23 03:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %09/21/23 03:28 17060-07-070-130 1
Toluene-d8 (S)100 %09/21/23 03:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
799946
SM 2120B-2011
SM 2120B-2011
2120B True Color EDEN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples:92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008, 92688066009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4143422
Associated Lab Samples: 92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008, 92688066009
Matrix: Water
AnalyzedMDL
True Color units ND 5.0 09/15/23 10:165.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4143423LABORATORY CONTROL SAMPLE:
LCSSpike
True Color units 35.035 100 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688066005
4143424SAMPLE DUPLICATE:
pH Std. Units 7.1 0 107.1
True Color units ND 10ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
955304
EPA 7470
EPA 7470
7470 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008, 92688066009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5252836
Associated Lab Samples: 92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008, 92688066009
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/09/23 09:320.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5252837LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.12 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5252838MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5252839
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 99 75-12596 3 202ND2.1 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
955306
EPA 7470
EPA 7470
7470 Mercury Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5252843
Associated Lab Samples: 92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Matrix: Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/09/23 11:080.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5252844LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.12 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5252845MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5252846
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2 100 85-11598 2 202ND2.0 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954340
EPA 3010
EPA 6010
6010 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008, 92688066009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5247760
Associated Lab Samples: 92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008, 92688066009
Matrix: Water
AnalyzedMDL
Antimony ug/L ND 15.0 10/03/23 23:265.5
Arsenic ug/L ND 10.0 10/03/23 23:263.4
Barium ug/L ND 10.0 10/03/23 23:260.84
Beryllium ug/L ND 4.0 10/03/23 23:260.17
Boron ug/L ND 50.0 10/03/23 23:2612.4
Cadmium ug/L ND 1.0 10/03/23 23:260.33
Chromium ug/L ND 5.0 10/03/23 23:261.7
Cobalt ug/L ND 10.0 10/03/23 23:260.96
Copper ug/L ND 5.0 10/03/23 23:262.6
Lead ug/L ND 10.0 10/03/23 23:262.1
Manganese ug/L ND 5.0 10/03/23 23:261.1
Nickel ug/L ND 5.0 10/03/23 23:261.0
Selenium ug/L ND 15.0 10/03/23 23:263.9
Silver ug/L ND 5.0 10/03/23 23:261.0
Thallium ug/L ND 15.0 10/03/23 23:262.9
Vanadium ug/L ND 10.0 10/03/23 23:261.0
Zinc ug/L ND 20.0 10/03/23 23:2611.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5247761LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 255250 102 80-120
Arsenic ug/L 242250 97 80-120
Barium ug/L 254250 101 80-120
Beryllium ug/L 25.125 100 80-120
Boron ug/L 12401250 100 80-120
Cadmium ug/L 25.225 101 80-120
Chromium ug/L 248250 99 80-120
Cobalt ug/L 254250 102 80-120
Copper ug/L 250250 100 80-120
Lead ug/L 259250 104 80-120
Manganese ug/L 250250 100 80-120
Nickel ug/L 257250 103 80-120
Selenium ug/L 254250 101 80-120
Silver ug/L 24.425 98 80-120
Thallium ug/L 238250 95 80-120
Vanadium ug/L 249250 100 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5247761LABORATORY CONTROL SAMPLE:
LCSSpike
Zinc ug/L 12401250 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5247762MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5247763
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 250 102 75-125101 1 20250ND256 253
Arsenic ug/L 250 98 75-12598 0 20250ND246 246
Barium ug/L 250 101 75-125101 0 2025044.7 297 297
Beryllium ug/L 25 102 75-125101 0 2025ND25.4 25.3
Boron ug/L 1250 101 75-125101 0 20125055.7 1320 1320
Cadmium ug/L 25 101 75-125100 0 2025ND25.2 25.1
Chromium ug/L 250 100 75-125100 0 20250ND251 251
Cobalt ug/L 250 102 75-125101 0 20250ND254 253
Copper ug/L 250 100 75-125100 1 20250ND250 252
Lead ug/L 250 102 75-125102 0 20250ND256 255
Manganese ug/L 250 100 75-125100 0 2025011.2 261 260
Nickel ug/L 250 103 75-125102 1 20250ND257 255
Selenium ug/L 250 103 75-125102 1 20250ND259 256
Silver ug/L 25 95 75-12597 3 2025ND23.7 24.3
Thallium ug/L 250 96 75-12597 1 20250ND240 243
Vanadium ug/L 250 101 75-125101 0 20250ND253 253
Zinc ug/L 1250 100 75-125100 0 201250ND1250 1250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954596
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5249435
Associated Lab Samples: 92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Matrix: Water
AnalyzedMDL
Antimony, Dissolved ug/L ND 15.0 10/05/23 10:345.5
Arsenic, Dissolved ug/L ND 10.0 10/05/23 10:343.4
Barium, Dissolved ug/L ND 10.0 10/05/23 10:340.84
Beryllium, Dissolved ug/L ND 4.0 10/05/23 10:340.17
Boron, Dissolved ug/L ND 50.0 10/05/23 10:3412.4
Cadmium, Dissolved ug/L ND 1.0 10/05/23 10:340.33
Chromium, Dissolved ug/L ND 5.0 10/05/23 10:341.7
Cobalt, Dissolved ug/L ND 10.0 10/05/23 10:340.96
Copper, Dissolved ug/L ND 5.0 10/05/23 10:342.6
Lead, Dissolved ug/L ND 10.0 10/05/23 10:342.1
Manganese, Dissolved ug/L ND 5.0 10/05/23 10:341.1
Nickel, Dissolved ug/L ND 5.0 10/05/23 10:341.0
Selenium, Dissolved ug/L ND 15.0 10/05/23 10:343.9
Silver, Dissolved ug/L ND 5.0 10/05/23 10:341.0
Thallium, Dissolved ug/L ND 15.0 10/05/23 10:342.9
Vanadium, Dissolved ug/L ND 10.0 10/05/23 10:341.0
Zinc, Dissolved ug/L ND 20.0 10/05/23 10:3411.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5249436LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 257250 103 80-120
Arsenic, Dissolved ug/L 245250 98 80-120
Barium, Dissolved ug/L 251250 100 80-120
Beryllium, Dissolved ug/L 24.725 99 80-120
Boron, Dissolved ug/L 12401250 99 80-120
Cadmium, Dissolved ug/L 26.025 104 80-120
Chromium, Dissolved ug/L 253250 101 80-120
Cobalt, Dissolved ug/L 256250 102 80-120
Copper, Dissolved ug/L 245250 98 80-120
Lead, Dissolved ug/L 258250 103 80-120
Manganese, Dissolved ug/L 252250 101 80-120
Nickel, Dissolved ug/L 260250 104 80-120
Selenium, Dissolved ug/L 258250 103 80-120
Silver, Dissolved ug/L 25.225 101 80-120
Thallium, Dissolved ug/L 261250 104 80-120
Vanadium, Dissolved ug/L 250250 100 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5249436LABORATORY CONTROL SAMPLE:
LCSSpike
Zinc, Dissolved ug/L 13001250 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5249437MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5249438
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 250 103 75-125103 1 20250ND259 257
Arsenic, Dissolved ug/L 250 100 75-12598 2 20250ND254 248
Barium, Dissolved ug/L 250 101 75-125101 0 2025043.0 296 295
Beryllium, Dissolved ug/L 25 99 75-12599 0 2025ND24.9 24.8
Boron, Dissolved ug/L 1250 101 75-125100 0 20125056.2 1320 1310
Cadmium, Dissolved ug/L 25 103 75-125103 0 2025ND25.8 25.8
Chromium, Dissolved ug/L 250 100 75-125100 0 20250ND250 250
Cobalt, Dissolved ug/L 250 103 75-125103 0 20250ND259 257
Copper, Dissolved ug/L 250 100 75-125100 0 20250ND252 251
Lead, Dissolved ug/L 250 102 75-125101 0 20250ND255 253
Manganese, Dissolved ug/L 250 101 75-125100 0 202502.3J 254 253
Nickel, Dissolved ug/L 250 105 75-125104 0 20250ND262 261
Selenium, Dissolved ug/L 250 101 75-125100 0 20250ND252 251
Silver, Dissolved ug/L 25 101 75-125101 0 2025ND25.7 25.6
Thallium, Dissolved ug/L 250 102 75-125101 1 20250ND256 253
Vanadium, Dissolved ug/L 250 102 75-125101 0 20250ND255 254
Zinc, Dissolved ug/L 1250 103 75-125103 0 201250ND1290 1290
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800498
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688066010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4146332
Associated Lab Samples:92688066010
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/21/23 01:580.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/21/23 01:580.22
1,1,2-Trichloroethane ug/L ND 1.0 09/21/23 01:580.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 v209/21/23 01:580.32
1,1-Dichloroethane ug/L ND 1.0 09/21/23 01:580.37
1,1-Dichloroethene ug/L ND 1.0 09/21/23 01:580.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/21/23 01:580.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/21/23 01:580.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/21/23 01:580.27
1,2-Dichlorobenzene ug/L ND 1.0 09/21/23 01:580.34
1,2-Dichloroethane ug/L ND 1.0 09/21/23 01:580.32
1,2-Dichloropropane ug/L ND 1.0 09/21/23 01:580.36
1,3-Dichlorobenzene ug/L ND 1.0 09/21/23 01:580.34
1,4-Dichlorobenzene ug/L ND 1.0 09/21/23 01:580.33
2-Butanone (MEK)ug/L ND 5.0 09/21/23 01:584.0
2-Hexanone ug/L ND 5.0 09/21/23 01:580.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/21/23 01:582.7
Acetone ug/L ND 25.0 v209/21/23 01:585.1
Benzene ug/L ND 1.0 09/21/23 01:580.34
Bromodichloromethane ug/L ND 1.0 09/21/23 01:580.31
Bromoform ug/L ND 1.0 09/21/23 01:580.34
Bromomethane ug/L ND 2.0 v209/21/23 01:581.7
Carbon disulfide ug/L ND 2.0 09/21/23 01:580.36
Carbon tetrachloride ug/L ND 1.0 09/21/23 01:580.33
Chlorobenzene ug/L ND 1.0 09/21/23 01:580.28
Chloroethane ug/L ND 1.0 09/21/23 01:580.65
Chloroform ug/L ND 1.0 09/21/23 01:580.43
Chloromethane ug/L ND 1.0 09/21/23 01:580.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/21/23 01:580.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/21/23 01:580.36
Cyclohexane ug/L ND 1.0 v209/21/23 01:580.35
Dibromochloromethane ug/L ND 1.0 09/21/23 01:580.36
Dichlorodifluoromethane ug/L ND 1.0 09/21/23 01:580.35
Ethylbenzene ug/L ND 1.0 09/21/23 01:580.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/21/23 01:580.33
m&p-Xylene ug/L ND 2.0 09/21/23 01:580.71
Methyl acetate ug/L ND 10.0 v209/21/23 01:582.4
Methyl-tert-butyl ether ug/L ND 1.0 09/21/23 01:580.42
Methylcyclohexane ug/L ND 10.0 v209/21/23 01:581.5
Methylene Chloride ug/L ND 5.0 09/21/23 01:582.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4146332
Associated Lab Samples:92688066010
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/21/23 01:580.34
Styrene ug/L ND 1.0 09/21/23 01:580.29
Tetrachloroethene ug/L ND 1.0 09/21/23 01:580.29
Toluene ug/L ND 1.0 09/21/23 01:580.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/21/23 01:580.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/21/23 01:580.36
Trichloroethene ug/L ND 1.0 09/21/23 01:580.38
Trichlorofluoromethane ug/L ND 1.0 09/21/23 01:580.30
Vinyl chloride ug/L ND 1.0 09/21/23 01:580.39
1,2-Dichloroethane-d4 (S)%91 70-130 09/21/23 01:58
4-Bromofluorobenzene (S)%99 70-130 09/21/23 01:58
Toluene-d8 (S)%101 70-130 09/21/23 01:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4146333LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 17.520 88 70-130
1,1,2,2-Tetrachloroethane ug/L 19.820 99 70-130
1,1,2-Trichloroethane ug/L 19.220 96 70-130
1,1,2-Trichlorotrifluoroethane ug/L 16.5 v32082 70-132
1,1-Dichloroethane ug/L 17.020 85 70-130
1,1-Dichloroethene ug/L 17.720 89 69-131
1,2,4-Trichlorobenzene ug/L 18.320 92 70-130
1,2-Dibromo-3-chloropropane ug/L 17.720 89 70-130
1,2-Dibromoethane (EDB)ug/L 19.320 97 70-130
1,2-Dichlorobenzene ug/L 19.320 96 70-130
1,2-Dichloroethane ug/L 17.120 86 70-130
1,2-Dichloropropane ug/L 18.420 92 70-130
1,3-Dichlorobenzene ug/L 19.320 97 70-130
1,4-Dichlorobenzene ug/L 18.720 94 70-130
2-Butanone (MEK)ug/L 33.740 84 67-133
2-Hexanone ug/L 39.440 99 70-133
4-Methyl-2-pentanone (MIBK)ug/L 37.340 93 70-130
Acetone ug/L 31.9 v34080 67-130
Benzene ug/L 18.720 93 70-130
Bromodichloromethane ug/L 17.720 88 70-130
Bromoform ug/L 18.020 90 70-133
Bromomethane ug/L 12.6 v32063 41-148
Carbon disulfide ug/L 18.220 91 70-131
Carbon tetrachloride ug/L 18.020 90 70-130
Chlorobenzene ug/L 19.320 96 70-130
Chloroethane ug/L 15.620 78 41-157
Chloroform ug/L 17.120 86 70-130
Chloromethane ug/L 14.020 70 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4146333LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 16.920 84 70-130
cis-1,3-Dichloropropene ug/L 18.020 90 70-130
Cyclohexane ug/L 18.0 v32090 63-137
Dibromochloromethane ug/L 19.020 95 70-130
Dichlorodifluoromethane ug/L 17.320 86 54-147
Ethylbenzene ug/L 19.320 97 70-130
Isopropylbenzene (Cumene)ug/L 20.020 100 70-130
m&p-Xylene ug/L 39.140 98 70-130
Methyl acetate ug/L 14.8 v32074 70-130
Methyl-tert-butyl ether ug/L 16.220 81 70-130
Methylcyclohexane ug/L 18.0 v32090 70-130
Methylene Chloride ug/L 18.020 90 62-130
o-Xylene ug/L 19.620 98 70-130
Styrene ug/L 20.120 101 70-130
Tetrachloroethene ug/L 17.720 88 70-130
Toluene ug/L 18.420 92 70-130
trans-1,2-Dichloroethene ug/L 17.420 87 70-130
trans-1,3-Dichloropropene ug/L 17.920 89 70-130
Trichloroethene ug/L 18.220 91 70-130
Trichlorofluoromethane ug/L 16.320 82 57-130
Vinyl chloride ug/L 14.120 70 66-140
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4146334MATRIX SPIKE SAMPLE:
MSSpike
Result
92688366001
1,1,1-Trichloroethane ug/L 15.720 79 70-150ND
1,1,2,2-Tetrachloroethane ug/L 16.320 81 66-144ND
1,1,2-Trichloroethane ug/L 15.420 77 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 16.5 v32082 66-168ND
1,1-Dichloroethane ug/L 15.120 75 68-150ND
1,1-Dichloroethene ug/L 16.520 83 64-162ND
1,2,4-Trichlorobenzene ug/L 16.020 80 69-147ND
1,2-Dibromo-3-chloropropane ug/L 13.820 69 62-146ND
1,2-Dibromoethane (EDB)ug/L 16.120 81 70-143ND
1,2-Dichlorobenzene ug/L 16.620 83 70-142ND
1,2-Dichloroethane ug/L 15.020 75 68-145ND
1,2-Dichloropropane ug/L 16.120 81 70-144ND
1,3-Dichlorobenzene ug/L 16.920 84 70-142ND
1,4-Dichlorobenzene ug/L 16.520 82 70-140ND
2-Butanone (MEK)ug/L 30.140 75 57-156ND
2-Hexanone ug/L 32.140 80 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 29.840 75 65-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4146334MATRIX SPIKE SAMPLE:
MSSpike
Result
92688366001
Acetone ug/L 25.240 63 49-162ND
Benzene ug/L 15.820 79 68-144ND
Bromodichloromethane ug/L 15.220 76 70-141ND
Bromoform ug/L 14.720 73 59-144ND
Bromomethane ug/L 11.5 v32057 23-190ND
Carbon disulfide ug/L 16.620 83 64-160ND
Carbon tetrachloride ug/L 16.520 82 70-147ND
Chlorobenzene ug/L 16.520 83 70-143ND
Chloroethane ug/L 15.620 78 55-190ND
Chloroform ug/L 15.820 77 67-1480.46J
Chloromethane ug/L 14.320 72 38-180ND
cis-1,2-Dichloroethene ug/L 15.320 77 67-151ND
cis-1,3-Dichloropropene ug/L 15.020 75 70-142ND
Cyclohexane ug/L 16.920 85 64-162ND
Dibromochloromethane ug/L 15.220 76 68-140ND
Dichlorodifluoromethane ug/L 16.7 v32083 15-200ND
Ethylbenzene ug/L 17.020 85 70-145ND
Isopropylbenzene (Cumene)ug/L 17.720 88 70-144ND
m&p-Xylene ug/L 34.640 86 70-148ND
Methyl acetate ug/L 12.0 M12060 62-144ND
Methyl-tert-butyl ether ug/L 13.420 67 64-146ND
Methylcyclohexane ug/L 17.5 v32087 70-155ND
Methylene Chloride ug/L 16.720 83 54-149ND
o-Xylene ug/L 16.920 84 70-145ND
Styrene ug/L 16.420 82 70-147ND
Tetrachloroethene ug/L 16.620 83 70-145ND
Toluene ug/L 16.220 78 65-1460.52J
trans-1,2-Dichloroethene ug/L 15.820 79 69-155ND
trans-1,3-Dichloropropene ug/L 14.920 75 70-142ND
Trichloroethene ug/L 15.820 79 70-152ND
Trichlorofluoromethane ug/L 16.320 81 60-158ND
Vinyl chloride ug/L 14.120 71 51-178ND
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688366002
4146335SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L ND v230ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688366002
4146335SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND v230ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND v230ND
Methylene Chloride ug/L ND 30ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 0.49J 300.45J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9292
4-Bromofluorobenzene (S)%99100
Toluene-d8 (S)%101102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801270
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150670
Associated Lab Samples:92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/23/23 02:440.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/23/23 02:440.22
1,1,2-Trichloroethane ug/L ND 1.0 09/23/23 02:440.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/23/23 02:440.32
1,1-Dichloroethane ug/L ND 1.0 09/23/23 02:440.37
1,1-Dichloroethene ug/L ND 1.0 09/23/23 02:440.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/23/23 02:440.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/23/23 02:440.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/23/23 02:440.27
1,2-Dichlorobenzene ug/L ND 1.0 09/23/23 02:440.34
1,2-Dichloroethane ug/L ND 1.0 09/23/23 02:440.32
1,2-Dichloropropane ug/L ND 1.0 09/23/23 02:440.36
1,3-Dichlorobenzene ug/L ND 1.0 09/23/23 02:440.34
1,4-Dichlorobenzene ug/L ND 1.0 09/23/23 02:440.33
2-Butanone (MEK)ug/L ND 5.0 09/23/23 02:444.0
2-Hexanone ug/L ND 5.0 09/23/23 02:440.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/23/23 02:442.7
Acetone ug/L ND 25.0 09/23/23 02:445.1
Benzene ug/L ND 1.0 09/23/23 02:440.34
Bromodichloromethane ug/L ND 1.0 09/23/23 02:440.31
Bromoform ug/L ND 1.0 09/23/23 02:440.34
Bromomethane ug/L ND 2.0 09/23/23 02:441.7
Carbon disulfide ug/L ND 2.0 09/23/23 02:440.36
Carbon tetrachloride ug/L ND 1.0 09/23/23 02:440.33
Chlorobenzene ug/L ND 1.0 09/23/23 02:440.28
Chloroethane ug/L ND 1.0 09/23/23 02:440.65
Chloroform ug/L ND 1.0 09/23/23 02:440.43
Chloromethane ug/L ND 1.0 09/23/23 02:440.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/23/23 02:440.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/23/23 02:440.36
Cyclohexane ug/L ND 1.0 09/23/23 02:440.35
Dibromochloromethane ug/L ND 1.0 09/23/23 02:440.36
Dichlorodifluoromethane ug/L ND 1.0 09/23/23 02:440.35
Ethylbenzene ug/L ND 1.0 09/23/23 02:440.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/23/23 02:440.33
m&p-Xylene ug/L ND 2.0 09/23/23 02:440.71
Methyl acetate ug/L ND 10.0 09/23/23 02:442.4
Methyl-tert-butyl ether ug/L ND 1.0 09/23/23 02:440.42
Methylcyclohexane ug/L ND 10.0 09/23/23 02:441.5
Methylene Chloride ug/L ND 5.0 09/23/23 02:442.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150670
Associated Lab Samples:92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/23/23 02:440.34
Styrene ug/L ND 1.0 09/23/23 02:440.29
Tetrachloroethene ug/L ND 1.0 09/23/23 02:440.29
Toluene ug/L ND 1.0 09/23/23 02:440.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/23/23 02:440.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/23/23 02:440.36
Trichloroethene ug/L ND 1.0 09/23/23 02:440.38
Trichlorofluoromethane ug/L ND 1.0 09/23/23 02:440.30
Vinyl chloride ug/L ND 1.0 09/23/23 02:440.39
1,2-Dichloroethane-d4 (S)%107 70-130 09/23/23 02:44
4-Bromofluorobenzene (S)%99 70-130 09/23/23 02:44
Toluene-d8 (S)%98 70-130 09/23/23 02:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150671LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.520 103 70-130
1,1,2,2-Tetrachloroethane ug/L 21.020 105 70-130
1,1,2-Trichloroethane ug/L 20.220 101 70-130
1,1,2-Trichlorotrifluoroethane ug/L 20.520 103 70-132
1,1-Dichloroethane ug/L 20.720 103 70-130
1,1-Dichloroethene ug/L 22.020 110 69-131
1,2,4-Trichlorobenzene ug/L 19.320 97 70-130
1,2-Dibromo-3-chloropropane ug/L 17.420 87 70-130
1,2-Dibromoethane (EDB)ug/L 19.920 100 70-130
1,2-Dichlorobenzene ug/L 19.820 99 70-130
1,2-Dichloroethane ug/L 20.820 104 70-130
1,2-Dichloropropane ug/L 19.720 99 70-130
1,3-Dichlorobenzene ug/L 19.320 97 70-130
1,4-Dichlorobenzene ug/L 19.520 97 70-130
2-Butanone (MEK)ug/L 41.540 104 67-133
2-Hexanone ug/L 42.240 106 70-133
4-Methyl-2-pentanone (MIBK)ug/L 41.340 103 70-130
Acetone ug/L 41.840 104 67-130
Benzene ug/L 19.720 98 70-130
Bromodichloromethane ug/L 19.620 98 70-130
Bromoform ug/L 17.320 87 70-133
Bromomethane ug/L 18.420 92 41-148
Carbon disulfide ug/L 21.620 108 70-131
Carbon tetrachloride ug/L 20.820 104 70-130
Chlorobenzene ug/L 19.420 97 70-130
Chloroethane ug/L 20.620 103 41-157
Chloroform ug/L 21.120 106 70-130
Chloromethane ug/L 19.020 95 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150671LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 20.620 103 70-130
cis-1,3-Dichloropropene ug/L 20.020 100 70-130
Cyclohexane ug/L 21.020 105 63-137
Dibromochloromethane ug/L 19.920 100 70-130
Dichlorodifluoromethane ug/L 23.620 118 54-147
Ethylbenzene ug/L 19.620 98 70-130
Isopropylbenzene (Cumene)ug/L 20.020 100 70-130
m&p-Xylene ug/L 38.740 97 70-130
Methyl acetate ug/L 18.420 92 70-130
Methyl-tert-butyl ether ug/L 19.220 96 70-130
Methylcyclohexane ug/L 21.020 105 70-130
Methylene Chloride ug/L 20.920 104 62-130
o-Xylene ug/L 19.820 99 70-130
Styrene ug/L 19.820 99 70-130
Tetrachloroethene ug/L 17.720 89 70-130
Toluene ug/L 19.520 98 70-130
trans-1,2-Dichloroethene ug/L 21.720 109 70-130
trans-1,3-Dichloropropene ug/L 20.120 101 70-130
Trichloroethene ug/L 19.420 97 70-130
Trichlorofluoromethane ug/L 20.820 104 57-130
Vinyl chloride ug/L 18.220 91 66-140
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150672MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
4150673
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 99 70-150134 30 3020ND19.9 26.8
1,1,2,2-Tetrachloroethane ug/L 20 102 66-144134 28 3020ND20.3 26.9
1,1,2-Trichloroethane ug/L 20 100 70-142133 28 3020ND20.0 26.6
1,1,2-Trichlorotrifluoroethane ug/L 20 125 66-168165 28 3020ND24.9 33.0
1,1-Dichloroethane ug/L 20 96 68-150128 29 3020ND19.2 25.7
1,1-Dichloroethene ug/L 20 103 64-162137 27 3020ND20.8 27.4
1,2,4-Trichlorobenzene ug/L R1209869-147133 31 3020ND19.6 26.7
1,2-Dibromo-3-chloropropane ug/L R1209762-146132 31 3020ND19.4 26.5
1,2-Dibromoethane (EDB) ug/L 20 102 70-143137 29 3020ND20.4 27.3
1,2-Dichlorobenzene ug/L 20 101 70-142133 27 3020ND20.1 26.5
1,2-Dichloroethane ug/L 20 97 68-145129 29 3020ND19.3 25.8
1,2-Dichloropropane ug/L 20 100 70-144132 28 3020ND20.0 26.4
1,3-Dichlorobenzene ug/L 20 103 70-142134 26 3020ND20.7 26.9
1,4-Dichlorobenzene ug/L R12010070-140136 31 3020ND19.9 27.2
2-Butanone (MEK)ug/L R1409757-156132 31 3040ND38.6 52.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150672MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
4150673
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 100 62-153136 30 3040ND40.1 54.2
4-Methyl-2-pentanone(MIBK)ug/L 40 98 65-144128 26 3040ND39.1 51.1
Acetone ug/L 40 90 49-162120 28 3040ND37.3 49.4
Benzene ug/L 20 101 68-144131 26 3020ND20.1 26.2
Bromodichloromethane ug/L 20 98 70-141129 27 3020ND19.5 25.7
Bromoform ug/L 20 102 59-144136 29 3020ND20.4 27.3
Bromomethane ug/L v12010723-190136 24 3020ND21.3 27.3
Carbon disulfide ug/L 20 108 64-160143 28 3020ND21.6 28.6
Carbon tetrachloride ug/L 20 108 70-147145 29 3020ND21.7 29.0
Chlorobenzene ug/L 20 102 70-143136 28 3020ND20.4 27.2
Chloroethane ug/L 20 97 55-190127 27 3020ND19.4 25.3
Chloroform ug/L 20 83 67-148118 14 302029.7 46.3 53.3
Chloromethane ug/L 20 89 38-180119 29 3020ND17.8 23.9
cis-1,2-Dichloroethene ug/L 20 98 67-151130 28 3020ND19.6 25.9
cis-1,3-Dichloropropene ug/L 20 99 70-142132 28 3020ND19.9 26.4
Cyclohexane ug/L 20 115 64-162152 28 3020ND23.0 30.4
Dibromochloromethane ug/L 20 101 68-140137 30 3020ND20.2 27.4
Dichlorodifluoromethane ug/L 20 121 15-200161 28 3020ND24.2 32.3
Ethylbenzene ug/L 20 101 70-145134 28 3020ND20.1 26.8
Isopropylbenzene(Cumene)ug/L 20 105 70-144140 29 3020ND20.9 27.9
m&p-Xylene ug/L 40 102 70-148135 27 3040ND40.9 54.0
Methyl acetate ug/L R1208062-144122 41 3020ND16.1 24.4
Methyl-tert-butyl ether ug/L R1209164-146124 31 3020ND18.2 24.8
Methylcyclohexane ug/L M12013370-155168 23 3020ND26.6 33.6
Methylene Chloride ug/L 20 90 54-149118 26 3020ND18.5 24.1
o-Xylene ug/L 20 101 70-145133 27 3020ND20.2 26.5
Styrene ug/L 20 100 70-147135 29 3020ND20.1 26.9
Tetrachloroethene ug/L 20 104 70-145135 26 3020ND20.8 27.0
Toluene ug/L 20 100 65-146130 26 3020ND20.0 26.0
trans-1,2-Dichloroethene ug/L 20 101 69-155133 28 3020ND20.2 26.6
trans-1,3-Dichloropropene ug/L 20 98 70-142131 29 3020ND19.7 26.3
Trichloroethene ug/L 20 104 70-152138 28 3020ND20.9 27.7
Trichlorofluoromethane ug/L 20 111 60-158147 28 3020ND22.2 29.5
Vinyl chloride ug/L 20 87 51-178116 29 3020ND17.4 23.3
1,2-Dichloroethane-d4 (S) %97 70-13097
4-Bromofluorobenzene (S) %99 70-130100
Toluene-d8 (S)%98 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801271
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688066001, 92688066008, 92688066009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150674
Associated Lab Samples:92688066001, 92688066008, 92688066009
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/24/23 14:000.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/24/23 14:000.22
1,1,2-Trichloroethane ug/L ND 1.0 09/24/23 14:000.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/24/23 14:000.32
1,1-Dichloroethane ug/L ND 1.0 09/24/23 14:000.37
1,1-Dichloroethene ug/L ND 1.0 09/24/23 14:000.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/24/23 14:000.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/24/23 14:000.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/24/23 14:000.27
1,2-Dichlorobenzene ug/L ND 1.0 09/24/23 14:000.34
1,2-Dichloroethane ug/L ND 1.0 09/24/23 14:000.32
1,2-Dichloropropane ug/L ND 1.0 09/24/23 14:000.36
1,3-Dichlorobenzene ug/L ND 1.0 09/24/23 14:000.34
1,4-Dichlorobenzene ug/L ND 1.0 09/24/23 14:000.33
2-Butanone (MEK)ug/L ND 5.0 09/24/23 14:004.0
2-Hexanone ug/L ND 5.0 09/24/23 14:000.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/24/23 14:002.7
Acetone ug/L ND 25.0 09/24/23 14:005.1
Benzene ug/L ND 1.0 09/24/23 14:000.34
Bromodichloromethane ug/L ND 1.0 09/24/23 14:000.31
Bromoform ug/L ND 1.0 09/24/23 14:000.34
Bromomethane ug/L ND 2.0 09/24/23 14:001.7
Carbon disulfide ug/L ND 2.0 09/24/23 14:000.36
Carbon tetrachloride ug/L ND 1.0 09/24/23 14:000.33
Chlorobenzene ug/L ND 1.0 09/24/23 14:000.28
Chloroethane ug/L ND 1.0 09/24/23 14:000.65
Chloroform ug/L ND 1.0 09/24/23 14:000.43
Chloromethane ug/L ND 1.0 09/24/23 14:000.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/24/23 14:000.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/24/23 14:000.36
Cyclohexane ug/L ND 1.0 09/24/23 14:000.35
Dibromochloromethane ug/L ND 1.0 09/24/23 14:000.36
Dichlorodifluoromethane ug/L ND 1.0 09/24/23 14:000.35
Ethylbenzene ug/L ND 1.0 09/24/23 14:000.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/24/23 14:000.33
m&p-Xylene ug/L ND 2.0 09/24/23 14:000.71
Methyl acetate ug/L ND 10.0 09/24/23 14:002.4
Methyl-tert-butyl ether ug/L ND 1.0 09/24/23 14:000.42
Methylcyclohexane ug/L ND 10.0 09/24/23 14:001.5
Methylene Chloride ug/L ND 5.0 09/24/23 14:002.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150674
Associated Lab Samples:92688066001, 92688066008, 92688066009
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/24/23 14:000.34
Styrene ug/L ND 1.0 09/24/23 14:000.29
Tetrachloroethene ug/L ND 1.0 09/24/23 14:000.29
Toluene ug/L ND 1.0 09/24/23 14:000.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/24/23 14:000.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/24/23 14:000.36
Trichloroethene ug/L ND 1.0 09/24/23 14:000.38
Trichlorofluoromethane ug/L ND 1.0 09/24/23 14:000.30
Vinyl chloride ug/L ND 1.0 09/24/23 14:000.39
1,2-Dichloroethane-d4 (S)%105 70-130 09/24/23 14:00
4-Bromofluorobenzene (S)%98 70-130 09/24/23 14:00
Toluene-d8 (S)%100 70-130 09/24/23 14:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150675LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 22.420 112 70-130
1,1,2,2-Tetrachloroethane ug/L 23.120 116 70-130
1,1,2-Trichloroethane ug/L 21.820 109 70-130
1,1,2-Trichlorotrifluoroethane ug/L 22.220 111 70-132
1,1-Dichloroethane ug/L 22.120 111 70-130
1,1-Dichloroethene ug/L 23.420 117 69-131
1,2,4-Trichlorobenzene ug/L 21.820 109 70-130
1,2-Dibromo-3-chloropropane ug/L 18.720 94 70-130
1,2-Dibromoethane (EDB)ug/L 22.220 111 70-130
1,2-Dichlorobenzene ug/L 21.020 105 70-130
1,2-Dichloroethane ug/L 22.320 112 70-130
1,2-Dichloropropane ug/L 21.420 107 70-130
1,3-Dichlorobenzene ug/L 21.220 106 70-130
1,4-Dichlorobenzene ug/L 20.720 103 70-130
2-Butanone (MEK)ug/L 45.340 113 67-133
2-Hexanone ug/L 46.840 117 70-133
4-Methyl-2-pentanone (MIBK)ug/L 45.340 113 70-130
Acetone ug/L 44.240 110 67-130
Benzene ug/L 21.020 105 70-130
Bromodichloromethane ug/L 21.020 105 70-130
Bromoform ug/L 19.520 98 70-133
Bromomethane ug/L 20.620 103 41-148
Carbon disulfide ug/L 23.820 119 70-131
Carbon tetrachloride ug/L 21.520 107 70-130
Chlorobenzene ug/L 21.320 106 70-130
Chloroethane ug/L 21.420 107 41-157
Chloroform ug/L 21.920 109 70-130
Chloromethane ug/L 20.420 102 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150675LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 22.120 111 70-130
cis-1,3-Dichloropropene ug/L 22.020 110 70-130
Cyclohexane ug/L 21.620 108 63-137
Dibromochloromethane ug/L 21.820 109 70-130
Dichlorodifluoromethane ug/L 24.320 121 54-147
Ethylbenzene ug/L 21.420 107 70-130
Isopropylbenzene (Cumene)ug/L 22.320 112 70-130
m&p-Xylene ug/L 44.040 110 70-130
Methyl acetate ug/L 19.720 98 70-130
Methyl-tert-butyl ether ug/L 20.520 103 70-130
Methylcyclohexane ug/L 22.420 112 70-130
Methylene Chloride ug/L 22.520 113 62-130
o-Xylene ug/L 21.720 108 70-130
Styrene ug/L 22.120 111 70-130
Tetrachloroethene ug/L 20.120 100 70-130
Toluene ug/L 20.720 103 70-130
trans-1,2-Dichloroethene ug/L 23.320 116 70-130
trans-1,3-Dichloropropene ug/L 22.220 111 70-130
Trichloroethene ug/L 21.720 108 70-130
Trichlorofluoromethane ug/L 21.520 107 57-130
Vinyl chloride ug/L 19.120 95 66-140
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150676MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689036004
4150677
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 112 70-150109 3 3020ND22.5 21.9
1,1,2,2-Tetrachloroethane ug/L 20 115 66-144110 4 3020ND22.9 22.0
1,1,2-Trichloroethane ug/L 20 112 70-142109 3 3020ND22.5 21.7
1,1,2-Trichlorotrifluoroethane ug/L 20 140 66-168136 2 3020ND27.9 27.3
1,1-Dichloroethane ug/L 20 109 68-150106 3 3020ND21.7 21.1
1,1-Dichloroethene ug/L 20 115 64-162113 2 3020ND23.1 22.6
1,2,4-Trichlorobenzene ug/L 20 115 69-147109 5 30201.5 24.5 23.3
1,2-Dibromo-3-chloropropane ug/L 20 111 62-146108 2 3020ND22.2 21.6
1,2-Dibromoethane (EDB) ug/L 20 116 70-143113 2 3020ND23.1 22.6
1,2-Dichlorobenzene ug/L 20 115 70-142108 5 30204.0 26.9 25.6
1,2-Dichloroethane ug/L 20 108 68-145106 2 3020ND21.6 21.2
1,2-Dichloropropane ug/L 20 114 70-144106 7 3020ND22.8 21.2
1,3-Dichlorobenzene ug/L 20 116 70-142111 4 30202.0 25.3 24.2
1,4-Dichlorobenzene ug/L 20 116 70-140105 7 302012.0 35.3 33.0
2-Butanone (MEK)ug/L 40 112 57-156112 1 3040ND46.9 47.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150676MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689036004
4150677
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 115 62-153112 2 3040ND45.9 44.8
4-Methyl-2-pentanone(MIBK)ug/L 40 107 65-144107 0 3040ND42.9 42.8
Acetone ug/L 40 89 49-162120 16 304034.3 70.0 82.4
Benzene ug/L 20 113 68-144110 2 3020ND22.5 22.0
Bromodichloromethane ug/L 20 110 70-141107 3 3020ND21.9 21.3
Bromoform ug/L 20 117 59-144111 5 3020ND23.3 22.3
Bromomethane ug/L v12011323-190106 6 3020ND22.6 21.2
Carbon disulfide ug/L 20 122 64-160118 3 3020ND24.4 23.7
Carbon tetrachloride ug/L 20 122 70-147118 3 3020ND24.4 23.6
Chlorobenzene ug/L 20 115 70-143111 3 30202.0 25.0 24.2
Chloroethane ug/L 20 109 55-190106 2 3020ND21.8 21.2
Chloroform ug/L 20 110 67-148104 5 3020ND21.9 20.8
Chloromethane ug/L 20 101 38-18099 2 3020ND20.2 19.8
cis-1,2-Dichloroethene ug/L 20 109 67-151106 2 3020ND21.8 21.3
cis-1,3-Dichloropropene ug/L 20 111 70-142109 2 3020ND22.3 21.8
Cyclohexane ug/L 20 128 64-162126 2 3020ND25.7 25.2
Dibromochloromethane ug/L 20 117 68-140111 5 3020ND23.4 22.2
Dichlorodifluoromethane ug/L 20 136 15-200132 2 3020ND27.1 26.4
Ethylbenzene ug/L 20 114 70-145110 3 3020ND22.8 22.0
Isopropylbenzene(Cumene)ug/L 20 118 70-144115 2 3020ND23.6 23.0
m&p-Xylene ug/L 40 115 70-148112 3 3040ND45.9 44.7
Methyl acetate ug/L 20 100 62-14495 5 3020ND20.0 19.0
Methyl-tert-butyl ether ug/L 20 102 64-14699 3 3020ND20.4 19.8
Methylcyclohexane ug/L 20 144 70-155137 5 3020ND28.8 27.4
Methylene Chloride ug/L 20 102 54-14998 4 3020ND20.4 19.6
o-Xylene ug/L 20 114 70-145110 4 3020ND22.9 22.0
Styrene ug/L 20 114 70-147110 4 3020ND22.9 22.0
Tetrachloroethene ug/L 20 116 70-145111 4 3020ND23.2 22.3
Toluene ug/L 20 112 65-146108 4 3020ND22.4 21.5
trans-1,2-Dichloroethene ug/L 20 112 69-155107 5 3020ND22.5 21.4
trans-1,3-Dichloropropene ug/L 20 111 70-142108 3 3020ND22.3 21.6
Trichloroethene ug/L 20 115 70-152113 2 3020ND23.1 22.6
Trichlorofluoromethane ug/L 20 124 60-158120 3 3020ND24.8 24.0
Vinyl chloride ug/L 20 99 51-17896 3 3020ND19.8 19.3
1,2-Dichloroethane-d4 (S) %97 70-13097
4-Bromofluorobenzene (S) %100 70-130100
Toluene-d8 (S)%97 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800409
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4145738
Associated Lab Samples: 92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/20/23 11:451.2
2,4,5-Trichlorophenol ug/L ND 10.0 09/20/23 11:451.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/20/23 11:451.6
2,4-Dichlorophenol ug/L ND 10.0 09/20/23 11:451.4
2,4-Dimethylphenol ug/L ND 10.0 09/20/23 11:451.7
2,4-Dinitrophenol ug/L ND 50.0 09/20/23 11:4526.0
2,4-Dinitrotoluene ug/L ND 10.0 09/20/23 11:451.6
2,6-Dinitrotoluene ug/L ND 10.0 09/20/23 11:451.7
2-Chloronaphthalene ug/L ND 10.0 09/20/23 11:451.7
2-Chlorophenol ug/L ND 10.0 09/20/23 11:451.2
2-Methylnaphthalene ug/L ND 10.0 09/20/23 11:451.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/20/23 11:451.9
2-Nitroaniline ug/L ND 20.0 09/20/23 11:453.0
2-Nitrophenol ug/L ND 10.0 09/20/23 11:451.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/20/23 11:451.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/20/23 11:458.1
3-Nitroaniline ug/L ND 20.0 09/20/23 11:453.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/20/23 11:457.8
4-Bromophenylphenyl ether ug/L ND 10.0 09/20/23 11:451.8
4-Chloro-3-methylphenol ug/L ND 10.0 09/20/23 11:453.3
4-Chloroaniline ug/L ND 20.0 09/20/23 11:453.6
4-Chlorophenylphenyl ether ug/L ND 10.0 09/20/23 11:452.0
4-Nitroaniline ug/L ND 20.0 09/20/23 11:455.1
4-Nitrophenol ug/L ND 50.0 09/20/23 11:456.6
Acenaphthene ug/L ND 10.0 09/20/23 11:452.0
Acenaphthylene ug/L ND 10.0 09/20/23 11:452.0
Acetophenone ug/L ND 10.0 09/20/23 11:451.5
Anthracene ug/L ND 10.0 09/20/23 11:452.3
Atrazine ug/L ND 10.0 09/20/23 11:453.2
Benzaldehyde ug/L ND 10.0 09/20/23 11:453.6
Benzo(a)anthracene ug/L ND 10.0 09/20/23 11:452.7
Benzo(a)pyrene ug/L ND 10.0 09/20/23 11:452.8
Benzo(b)fluoranthene ug/L ND 10.0 09/20/23 11:452.6
Benzo(g,h,i)perylene ug/L ND 10.0 09/20/23 11:452.8
Benzo(k)fluoranthene ug/L ND 10.0 09/20/23 11:452.7
Biphenyl (Diphenyl)ug/L ND 10.0 09/20/23 11:451.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/20/23 11:451.8
bis(2-Chloroethyl) ether ug/L ND 10.0 09/20/23 11:451.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/20/23 11:453.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4145738
Associated Lab Samples: 92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Matrix: Water
AnalyzedMDL
Butylbenzylphthalate ug/L ND 10.0 09/20/23 11:453.1
Caprolactam ug/L ND 10.0 09/20/23 11:456.9
Carbazole ug/L ND 10.0 09/20/23 11:452.4
Chrysene ug/L ND 10.0 09/20/23 11:452.8
Di-n-butylphthalate ug/L ND 10.0 09/20/23 11:452.2
Di-n-octylphthalate ug/L ND 10.0 09/20/23 11:453.9
Dibenz(a,h)anthracene ug/L ND 10.0 09/20/23 11:453.0
Dibenzofuran ug/L ND 10.0 09/20/23 11:452.1
Diethylphthalate ug/L ND 10.0 09/20/23 11:452.0
Dimethylphthalate ug/L ND 10.0 09/20/23 11:452.1
Fluoranthene ug/L ND 10.0 09/20/23 11:452.2
Fluorene ug/L ND 10.0 09/20/23 11:452.1
Hexachloro-1,3-butadiene ug/L ND 10.0 09/20/23 11:451.8
Hexachlorobenzene ug/L ND 10.0 09/20/23 11:452.2
Hexachlorocyclopentadiene ug/L ND 10.0 09/20/23 11:451.6
Hexachloroethane ug/L ND 10.0 09/20/23 11:451.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/20/23 11:452.9
Isophorone ug/L ND 10.0 09/20/23 11:451.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/20/23 11:451.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/20/23 11:453.0
Naphthalene ug/L ND 10.0 09/20/23 11:452.1
Nitrobenzene ug/L ND 10.0 09/20/23 11:451.9
Pentachlorophenol ug/L ND 20.0 09/20/23 11:453.8
Phenanthrene ug/L ND 10.0 09/20/23 11:452.0
Phenol ug/L ND 10.0 09/20/23 11:451.4
Pyrene ug/L ND 10.0 09/20/23 11:452.2
2,4,6-Tribromophenol (S)%130 10-164 09/20/23 11:45
2-Fluorobiphenyl (S)%116 10-130 09/20/23 11:45
2-Fluorophenol (S)%87 10-130 09/20/23 11:45
Nitrobenzene-d5 (S)%124 10-138 09/20/23 11:45
Phenol-d6 (S)%62 10-130 09/20/23 11:45
Terphenyl-d14 (S)%142 19-191 09/20/23 11:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4145739LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 30.650 61 21-135
2,4,5-Trichlorophenol ug/L 41.250 82 38-147
2,4,6-Trichlorophenol ug/L 38.650 77 34-142
2,4-Dichlorophenol ug/L 35.350 71 36-136
2,4-Dimethylphenol ug/L 35.050 70 38-134
2,4-Dinitrophenol ug/L 229250 92 10-169
2,4-Dinitrotoluene ug/L 50.350 101 44-154
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4145739LABORATORY CONTROL SAMPLE:
LCSSpike
2,6-Dinitrotoluene ug/L 41.450 83 44-156
2-Chloronaphthalene ug/L 34.750 69 25-130
2-Chlorophenol ug/L 36.650 73 29-130
2-Methylnaphthalene ug/L 34.150 68 23-130
2-Methylphenol(o-Cresol)ug/L 31.450 63 31-130
2-Nitroaniline ug/L 76.7100 77 39-145
2-Nitrophenol ug/L 37.850 76 29-142
3&4-Methylphenol(m&p Cresol)ug/L 32.950 66 30-130
3,3'-Dichlorobenzidine ug/L 143100 143 44-158
3-Nitroaniline ug/L 97.4100 97 45-152
4,6-Dinitro-2-methylphenol ug/L 104100 104 39-158
4-Bromophenylphenyl ether ug/L 39.350 79 47-147
4-Chloro-3-methylphenol ug/L 67.4100 67 40-138
4-Chloroaniline ug/L 72.1100 72 35-130
4-Chlorophenylphenyl ether ug/L 37.750 75 36-139
4-Nitroaniline ug/L 125100 125 46-157
4-Nitrophenol ug/L 160250 64 17-130
Acenaphthene ug/L 35.950 72 34-135
Acenaphthylene ug/L 35.950 72 35-137
Acetophenone ug/L 34.250 68 30-137
Anthracene ug/L 46.250 92 47-146
Atrazine ug/L 36.350 73 30-130
Benzaldehyde ug/L 28.650 57 17-167
Benzo(a)anthracene ug/L 62.450 125 48-160
Benzo(a)pyrene ug/L 62.050 124 47-165
Benzo(b)fluoranthene ug/L 70.250 140 49-171
Benzo(g,h,i)perylene ug/L 59.750 119 46-166
Benzo(k)fluoranthene ug/L 64.450 129 55-162
Biphenyl (Diphenyl)ug/L 34.750 69 28-130
bis(2-Chloroethoxy)methane ug/L 32.350 65 33-136
bis(2-Chloroethyl) ether ug/L 33.650 67 30-142
bis(2-Ethylhexyl)phthalate ug/L 69.750 139 46-173
Butylbenzylphthalate ug/L 65.050 130 53-169
Caprolactam ug/L 21.550 43 13-130
Carbazole ug/L 58.050 116 48-157
Chrysene ug/L 58.650 117 54-152
Di-n-butylphthalate ug/L 60.050 120 49-161
Di-n-octylphthalate ug/L 67.550 135 50-166
Dibenz(a,h)anthracene ug/L 60.250 120 46-166
Dibenzofuran ug/L 35.250 70 37-136
Diethylphthalate ug/L 49.850 100 45-149
Dimethylphthalate ug/L 39.850 80 43-145
Fluoranthene ug/L 58.050 116 50-153
Fluorene ug/L 37.150 74 42-142
Hexachloro-1,3-butadiene ug/L 27.350 55 10-130
Hexachlorobenzene ug/L 39.750 79 44-138
Hexachlorocyclopentadiene ug/L 32.850 66 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4145739LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloroethane ug/L 22.850 46 10-130
Indeno(1,2,3-cd)pyrene ug/L 58.250 116 46-166
Isophorone ug/L 33.150 66 36-135
N-Nitroso-di-n-propylamine ug/L 35.650 71 33-140
N-Nitrosodiphenylamine ug/L 41.650 83 46-144
Naphthalene ug/L 30.250 60 20-130
Nitrobenzene ug/L 31.550 63 33-133
Pentachlorophenol ug/L 103100 103 21-163
Phenanthrene ug/L 46.350 93 47-146
Phenol ug/L 21.250 42 19-130
Pyrene ug/L 57.350 115 53-155
2,4,6-Tribromophenol (S)%124 10-164
2-Fluorobiphenyl (S)%85 10-130
2-Fluorophenol (S)%66 10-130
Nitrobenzene-d5 (S)%83 10-138
Phenol-d6 (S)%53 10-130
Terphenyl-d14 (S)%143 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4145742MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
4145743
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-chloropropane)ug/L 83.3 70 11-14385 20 3083.3ND 58.0 70.6
2,4,5-Trichlorophenol ug/L R183.3 83 10-170145 54 3083.3ND 69.4 121
2,4,6-Trichlorophenol ug/L R183.3 48 10-166126 91 3083.3ND 39.6 105
2,4-Dichlorophenol ug/L R183.3 76 10-153113 39 3083.3ND 63.4 94.0
2,4-Dimethylphenol ug/L 83.3 88 20-147110 23 3083.3ND 72.9 92.0
2,4-Dinitrophenol ug/L 417 10 10-172135 30417NDND 563
2,4-Dinitrotoluene ug/L 83.3 115 30-164146 24 3083.3ND 95.7 122
2,6-Dinitrotoluene ug/L 83.3 119 31-163142 18 3083.3ND 99.6 119
2-Chloronaphthalene ug/L 83.3 86 15-134103 18 3083.3ND 71.7 86.2
2-Chlorophenol ug/L 83.3 77 10-139101 27 3083.3ND 64.4 84.3
2-Methylnaphthalene ug/L 83.3 87 12-130108 21 3083.3ND 72.6 89.9
2-Methylphenol(o-Cresol) ug/L 83.3 77 19-13294 20 3083.3ND 64.0 78.3
2-Nitroaniline ug/L 167 106 23-154140 27 30167ND177 233
2-Nitrophenol ug/L R183.3 71 10-159110 43 3083.3ND 59.4 91.8
3&4-Methylphenol(m&pCresol)ug/L 83.3 89 13-136108 19 3083.3ND 73.9 89.7
3,3'-Dichlorobenzidine ug/L 167 137 10-178166 19 30167ND229 277
3-Nitroaniline ug/L 167 127 20-166152 18 30167ND211 253
4,6-Dinitro-2-methylphenol ug/L 167 18 10-187133 30167ND29.9J 222
4-Bromophenylphenyl ether ug/L 83.3 108 31-157129 17 3083.3ND 90.1 107
4-Chloro-3-methylphenol ug/L 167 97 27-146121 22 30167ND162 202
4-Chloroaniline ug/L 167 96 13-143111 15 30167ND159 185
4-Chlorophenylphenyl ether ug/L 83.3 108 23-149133 21 3083.3ND 89.9 111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4145742MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
4145743
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Nitroaniline ug/L 167 133 24-171160 19 30167ND222 267
4-Nitrophenol ug/L M1417010-13099 30417NDND 414
Acenaphthene ug/L 83.3 94 21-147116 21 3083.3ND 78.2 97.0
Acenaphthylene ug/L 83.3 94 19-150114 19 3083.3ND 78.2 95.0
Acetophenone ug/L 83.3 79 22-14598 21 3083.3ND 65.8 81.4
Anthracene ug/L 83.3 105 36-152127 19 3083.3ND 87.9 106
Atrazine ug/L 83.3 109 18-17381 30 3083.3ND 90.9 67.3
Benzaldehyde ug/L 83.3 63 16-16381 25 3083.3ND 52.4 67.5
Benzo(a)anthracene ug/L 83.3 121 42-163147 20 3083.3ND 101 123
Benzo(a)pyrene ug/L 83.3 122 40-169147 19 3083.3ND 101 123
Benzo(b)fluoranthene ug/L 83.3 138 40-177168 19 3083.3ND 115 140
Benzo(g,h,i)perylene ug/L 83.3 121 38-174147 19 3083.3ND 101 122
Benzo(k)fluoranthene ug/L 83.3 123 41-171152 21 3083.3ND 103 126
Biphenyl (Diphenyl)ug/L 83.3 87 14-137106 20 3083.3ND 72.3 87.9bis(2-Chloroethoxy)methane ug/L 83.3 77 19-14697 22 3083.3ND 64.4 80.5
bis(2-Chloroethyl) ether ug/L 83.3 77 19-15190 16 3083.3ND 64.0 75.2
bis(2-Ethylhexyl)phthalate ug/L 83.3 138 42-168168 19 3083.3ND 115 140
Butylbenzylphthalate ug/L 83.3 130 42-177154 17 3083.3ND 108 128
Caprolactam ug/L 83.3 82 10-13068 18 3083.3ND 68.6 57.1
Carbazole ug/L 83.3 118 38-164141 18 3083.3ND 98.4 118
Chrysene ug/L 83.3 113 43-159139 20 3083.3ND 94.6 115
Di-n-butylphthalate ug/L 83.3 121 42-160143 16 3083.3ND 101 119
Di-n-octylphthalate ug/L 83.3 134 42-171163 20 3083.3ND 112 136
Dibenz(a,h)anthracene ug/L 83.3 119 40-171146 21 3083.3ND 98.9 121
Dibenzofuran ug/L 83.3 94 23-147117 21 3083.3ND 78.7 97.3
Diethylphthalate ug/L 83.3 117 33-157142 19 3083.3ND 97.8 119
Dimethylphthalate ug/L 83.3 110 27-154133 19 3083.3ND 91.7 111
Fluoranthene ug/L 83.3 117 42-157137 15 3083.3ND 97.8 114
Fluorene ug/L 83.3 105 25-155129 21 3083.3ND 87.2 107
Hexachloro-1,3-butadiene ug/L 83.3 74 10-13096 25 3083.3ND 62.0 79.8
Hexachlorobenzene ug/L 83.3 103 32-145125 19 3083.3ND 85.8 104
Hexachlorocyclopentadiene ug/L 83.3 83 10-130106 25 3083.3ND 68.9 88.6
Hexachloroethane ug/L 83.3 58 10-13073 22 3083.3ND 48.4 60.5
Indeno(1,2,3-cd)pyrene ug/L 83.3 117 39-174142 19 3083.3ND 97.2 118
Isophorone ug/L 83.3 80 19-146105 27 3083.3ND 66.3 87.1
N-Nitroso-di-n-propylamine ug/L 83.3 83 20-150107 24 3083.3ND 69.6 88.9
N-Nitrosodiphenylamine ug/L 83.3 107 33-149130 20 3083.3ND 88.9 108
Naphthalene ug/L 83.3 76 10-12894 21 3083.3ND 63.2 78.4
Nitrobenzene ug/L 83.3 73 19-14594 24 3083.3ND 61.2 78.1
Pentachlorophenol ug/L R11672710-188132 131 30167ND45.7 219
Phenanthrene ug/L 83.3 105 38-150127 19 3083.3ND 87.7 106
Phenol ug/L 83.3 61 10-13071 15 3083.3ND 50.9 59.4
Pyrene ug/L 83.3 112 42-163136 20 3083.3ND 93.4 114
2,4,6-Tribromophenol (S) %83 10-164137
2-Fluorobiphenyl (S)%78 10-13094
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4145742MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
4145743
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Fluorophenol (S)%43 10-13072
Nitrobenzene-d5 (S)%73 10-13889
Phenol-d6 (S)%57 10-13068
Terphenyl-d14 (S)%101 19-191118
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800690
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688066009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147306
Associated Lab Samples:92688066009
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/21/23 10:161.2
2,4,5-Trichlorophenol ug/L ND 10.0 09/21/23 10:161.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/21/23 10:161.6
2,4-Dichlorophenol ug/L ND 10.0 09/21/23 10:161.4
2,4-Dimethylphenol ug/L ND 10.0 09/21/23 10:161.7
2,4-Dinitrophenol ug/L ND 50.0 09/21/23 10:1626.0
2,4-Dinitrotoluene ug/L ND 10.0 09/21/23 10:161.6
2,6-Dinitrotoluene ug/L ND 10.0 09/21/23 10:161.7
2-Chloronaphthalene ug/L ND 10.0 09/21/23 10:161.7
2-Chlorophenol ug/L ND 10.0 09/21/23 10:161.2
2-Methylnaphthalene ug/L ND 10.0 09/21/23 10:161.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/21/23 10:161.9
2-Nitroaniline ug/L ND 20.0 09/21/23 10:163.0
2-Nitrophenol ug/L ND 10.0 09/21/23 10:161.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/21/23 10:161.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/21/23 10:168.1
3-Nitroaniline ug/L ND 20.0 09/21/23 10:163.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/21/23 10:167.8
4-Bromophenylphenyl ether ug/L ND 10.0 09/21/23 10:161.8
4-Chloro-3-methylphenol ug/L ND 10.0 09/21/23 10:163.3
4-Chloroaniline ug/L ND 20.0 09/21/23 10:163.6
4-Chlorophenylphenyl ether ug/L ND 10.0 09/21/23 10:162.0
4-Nitroaniline ug/L ND 20.0 09/21/23 10:165.1
4-Nitrophenol ug/L ND 50.0 09/21/23 10:166.6
Acenaphthene ug/L ND 10.0 09/21/23 10:162.0
Acenaphthylene ug/L ND 10.0 09/21/23 10:162.0
Acetophenone ug/L ND 10.0 09/21/23 10:161.5
Anthracene ug/L ND 10.0 09/21/23 10:162.3
Atrazine ug/L ND 10.0 09/21/23 10:163.2
Benzaldehyde ug/L ND 10.0 09/21/23 10:163.6
Benzo(a)anthracene ug/L ND 10.0 09/21/23 10:162.7
Benzo(a)pyrene ug/L ND 10.0 09/21/23 10:162.8
Benzo(b)fluoranthene ug/L ND 10.0 09/21/23 10:162.6
Benzo(g,h,i)perylene ug/L ND 10.0 09/21/23 10:162.8
Benzo(k)fluoranthene ug/L ND 10.0 09/21/23 10:162.7
Biphenyl (Diphenyl)ug/L ND 10.0 09/21/23 10:161.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/21/23 10:161.8
bis(2-Chloroethyl) ether ug/L ND 10.0 09/21/23 10:161.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/21/23 10:163.7
Butylbenzylphthalate ug/L ND 10.0 09/21/23 10:163.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
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Page 79 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147306
Associated Lab Samples:92688066009
Matrix: Water
AnalyzedMDL
Caprolactam ug/L ND 10.0 09/21/23 10:166.9
Carbazole ug/L ND 10.0 09/21/23 10:162.4
Chrysene ug/L ND 10.0 09/21/23 10:162.8
Di-n-butylphthalate ug/L ND 10.0 09/21/23 10:162.2
Di-n-octylphthalate ug/L ND 10.0 09/21/23 10:163.9
Dibenz(a,h)anthracene ug/L ND 10.0 09/21/23 10:163.0
Dibenzofuran ug/L ND 10.0 09/21/23 10:162.1
Diethylphthalate ug/L ND 10.0 09/21/23 10:162.0
Dimethylphthalate ug/L ND 10.0 09/21/23 10:162.1
Fluoranthene ug/L ND 10.0 09/21/23 10:162.2
Fluorene ug/L ND 10.0 09/21/23 10:162.1
Hexachloro-1,3-butadiene ug/L ND 10.0 09/21/23 10:161.8
Hexachlorobenzene ug/L ND 10.0 09/21/23 10:162.2
Hexachlorocyclopentadiene ug/L ND 10.0 09/21/23 10:161.6
Hexachloroethane ug/L ND 10.0 09/21/23 10:161.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/21/23 10:162.9
Isophorone ug/L ND 10.0 09/21/23 10:161.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/21/23 10:161.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/21/23 10:163.0
Naphthalene ug/L ND 10.0 09/21/23 10:162.1
Nitrobenzene ug/L ND 10.0 09/21/23 10:161.9
Pentachlorophenol ug/L ND 20.0 09/21/23 10:163.8
Phenanthrene ug/L ND 10.0 09/21/23 10:162.0
Phenol ug/L ND 10.0 09/21/23 10:161.4
Pyrene ug/L ND 10.0 09/21/23 10:162.2
2,4,6-Tribromophenol (S)%117 10-164 09/21/23 10:16
2-Fluorobiphenyl (S)%99 10-130 09/21/23 10:16
2-Fluorophenol (S)%77 10-130 09/21/23 10:16
Nitrobenzene-d5 (S)%102 10-138 09/21/23 10:16
Phenol-d6 (S)%57 10-130 09/21/23 10:16
Terphenyl-d14 (S)%131 19-191 09/21/23 10:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147307LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 38.2100 38 21-135
2,4,5-Trichlorophenol ug/L 58.2100 58 38-147
2,4,6-Trichlorophenol ug/L 45.6100 46 34-142
2,4-Dichlorophenol ug/L 46.8100 47 36-136
2,4-Dimethylphenol ug/L 46.7100 47 38-134
2,4-Dinitrophenol ug/L 114500 23 10-169
2,4-Dinitrotoluene ug/L 70.4100 70 44-154
2,6-Dinitrotoluene ug/L 61.7100 62 44-156
2-Chloronaphthalene ug/L 42.5100 43 25-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147307LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 46.1100 46 29-130
2-Methylnaphthalene ug/L 40.4100 40 23-130
2-Methylphenol(o-Cresol)ug/L 41.9100 42 31-130
2-Nitroaniline ug/L 115200 57 39-145
2-Nitrophenol ug/L 46.8100 47 29-142
3&4-Methylphenol(m&p Cresol)ug/L 43.5100 44 30-130
3,3'-Dichlorobenzidine ug/L 193200 96 44-158
3-Nitroaniline ug/L 145200 72 45-152
4,6-Dinitro-2-methylphenol ug/L 92.2200 46 39-158
4-Bromophenylphenyl ether ug/L 61.5100 61 47-147
4-Chloro-3-methylphenol ug/L 95.5200 48 40-138
4-Chloroaniline ug/L 97.3200 49 35-130
4-Chlorophenylphenyl ether ug/L 52.6100 53 36-139
4-Nitroaniline ug/L 169200 85 46-157
4-Nitrophenol ug/L 141500 28 17-130
Acenaphthene ug/L 46.3100 46 34-135
Acenaphthylene ug/L 45.3100 45 35-137
Acetophenone ug/L 43.2100 43 30-137
Anthracene ug/L 67.3100 67 47-146
Atrazine ug/L 77.6 L150155 30-130
Benzaldehyde ug/L 36.750 73 17-167
Benzo(a)anthracene ug/L 83.3100 83 48-160
Benzo(a)pyrene ug/L 84.2100 84 47-165
Benzo(b)fluoranthene ug/L 97.3100 97 49-171
Benzo(g,h,i)perylene ug/L 81.7100 82 46-166
Benzo(k)fluoranthene ug/L 88.2100 88 55-162
Biphenyl (Diphenyl)ug/L 42.8100 43 28-130
bis(2-Chloroethoxy)methane ug/L 41.9100 42 33-136
bis(2-Chloroethyl) ether ug/L 42.3100 42 30-142
bis(2-Ethylhexyl)phthalate ug/L 98.0100 98 46-173
Butylbenzylphthalate ug/L 90.3100 90 53-169
Caprolactam ug/L 28.350 57 13-130
Carbazole ug/L 78.9100 79 48-157
Chrysene ug/L 79.1100 79 54-152
Di-n-butylphthalate ug/L 82.0100 82 49-161
Di-n-octylphthalate ug/L 92.8100 93 50-166
Dibenz(a,h)anthracene ug/L 82.5100 82 46-166
Dibenzofuran ug/L 46.2100 46 37-136
Diethylphthalate ug/L 70.4100 70 45-149
Dimethylphthalate ug/L 58.8100 59 43-145
Fluoranthene ug/L 77.4100 77 50-153
Fluorene ug/L 52.3100 52 42-142
Hexachloro-1,3-butadiene ug/L 31.1100 31 10-130
Hexachlorobenzene ug/L 63.4100 63 44-138
Hexachlorocyclopentadiene ug/L 38.0100 38 10-130
Hexachloroethane ug/L 25.7100 26 10-130
Indeno(1,2,3-cd)pyrene ug/L 79.8100 80 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147307LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 44.9100 45 36-135
N-Nitroso-di-n-propylamine ug/L 48.8100 49 33-140
N-Nitrosodiphenylamine ug/L 64.2100 64 46-144
Naphthalene ug/L 34.1100 34 20-130
Nitrobenzene ug/L 39.6100 40 33-133
Pentachlorophenol ug/L 109200 55 21-163
Phenanthrene ug/L 66.6100 67 47-146
Phenol ug/L 30.5100 31 19-130
Pyrene ug/L 79.0100 79 53-155
2,4,6-Tribromophenol (S)%125 10-164
2-Fluorobiphenyl (S)%69 10-130
2-Fluorophenol (S)%51 10-130
Nitrobenzene-d5 (S)%69 10-138
Phenol-d6 (S)%47 10-130
Terphenyl-d14 (S)%131 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147308MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688452005
4147309
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-chloropropane)ug/L 83.3 65 11-14358 10 3083.3ND 53.8 48.5
2,4,5-Trichlorophenol ug/L M183.3 7 10-17021 3083.3ND 6.2J 17.2
2,4,6-Trichlorophenol ug/L M183.3 3 10-16610 3083.3ND 2.6J 8.7J
2,4-Dichlorophenol ug/L M183.3 9 10-15322 3083.3ND 7.1J 18.0
2,4-Dimethylphenol ug/L 83.3 71 20-14770 2 3083.3ND 58.9 58.0
2,4-Dinitrophenol ug/L M1417010-1720 30417NDND ND
2,4-Dinitrotoluene ug/L 83.3 115 30-164110 5 3083.3ND 96.2 91.5
2,6-Dinitrotoluene ug/L 83.3 104 31-16399 5 3083.3ND 86.5 82.7
2-Chloronaphthalene ug/L 83.3 78 15-13470 10 3083.3ND 64.6 58.3
2-Chlorophenol ug/L 83.3 11 10-13926 3083.3ND 9.0J 21.9
2-Methylnaphthalene ug/L 83.3 77 12-13068 12 3083.3ND 64.3 57.0
2-Methylphenol(o-Cresol) ug/L 83.3 48 19-13255 13 3083.3ND 39.7 45.4
2-Nitroaniline ug/L 167 95 23-15491 4 30167ND158 152
2-Nitrophenol ug/L M183.3 6 10-15917 3083.3ND 5.2J 14.3J3&4-Methylphenol(m&pCresol)ug/L 83.3 48 13-13655 14 3083.3ND 39.7 45.6
3,3'-Dichlorobenzidine ug/L 167 171 10-178159 7 30167ND284 266
3-Nitroaniline ug/L 167 120 20-166115 4 30167ND200 192
4,6-Dinitro-2-methylphenol ug/L 167 10 10-18714 30167ND16.7J 24.1J
4-Bromophenylphenyl ether ug/L 83.3 99 31-15793 6 3083.3ND 82.6 77.7
4-Chloro-3-methylphenol ug/L 167 46 27-14662 30 30167ND76.0 103
4-Chloroaniline ug/L 167 81 13-14374 9 30167ND134 123
4-Chlorophenylphenyl ether ug/L 83.3 89 23-14982 8 3083.3ND 74.4 68.7
4-Nitroaniline ug/L 167 146 24-171139 5 30167ND244 232
4-Nitrophenol ug/L M1417010-1300 30417NDND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147308MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688452005
4147309
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L 83.3 79 21-14772 9 3083.3ND 65.6 59.9
Acenaphthylene ug/L 83.3 79 19-15072 9 3083.3ND 65.5 60.1
Acetophenone ug/L 83.3 72 22-14564 11 3083.3ND 59.7 53.6
Anthracene ug/L 83.3 108 36-152105 3 3083.3ND 90.4 87.8
Atrazine ug/L 83.3 150 18-173143 5 3083.3ND 125 119
Benzaldehyde ug/L 83.3 71 16-16366 7 3083.3ND 59.2 55.1
Benzo(a)anthracene ug/L 83.3 148 42-163140 6 3083.3ND 123 117
Benzo(a)pyrene ug/L 83.3 145 40-169141 3 3083.3ND 121 118
Benzo(b)fluoranthene ug/L 83.3 165 40-177163 1 3083.3ND 138 136
Benzo(g,h,i)perylene ug/L 83.3 145 38-174139 4 3083.3ND 121 116
Benzo(k)fluoranthene ug/L 83.3 150 41-171141 7 3083.3ND 125 117
Biphenyl (Diphenyl)ug/L 83.3 77 14-13769 11 3083.3ND 64.3 57.8
bis(2-Chloroethoxy)methane ug/L 83.3 73 19-14665 12 3083.3ND 60.7 54.1
bis(2-Chloroethyl) ether ug/L 83.3 68 19-15161 10 3083.3ND 56.5 51.2
bis(2-Ethylhexyl)phthalate ug/L M183.3 172 42-168160 7 3083.3ND 144 133
Butylbenzylphthalate ug/L 83.3 163 42-177151 8 3083.3ND 136 126
Caprolactam ug/L 83.3 53 10-13052 3 3083.3ND 44.1 42.9
Carbazole ug/L 83.3 140 38-164132 6 3083.3ND 117 110
Chrysene ug/L 83.3 139 43-159131 6 3083.3ND 116 109
Di-n-butylphthalate ug/L 83.3 142 42-160136 4 3083.3ND 118 113
Di-n-octylphthalate ug/L 83.3 164 42-171152 7 3083.3ND 136 127
Dibenz(a,h)anthracene ug/L 83.3 144 40-171138 4 3083.3ND 120 115
Dibenzofuran ug/L 83.3 78 23-14772 8 3083.3ND 64.8 60.1
Diethylphthalate ug/L 83.3 115 33-157111 4 3083.3ND 96.0 92.3
Dimethylphthalate ug/L 83.3 94 27-15491 3 3083.3ND 78.2 75.6
Fluoranthene ug/L 83.3 136 42-157129 5 3083.3ND 113 107
Fluorene ug/L 83.3 86 25-15580 7 3083.3ND 71.6 66.8
Hexachloro-1,3-butadiene ug/L 83.3 62 10-13054 13 3083.3ND 51.5 45.2
Hexachlorobenzene ug/L 83.3 101 32-14596 5 3083.3ND 84.3 80.4
Hexachlorocyclopentadiene ug/L 83.3 70 10-13063 10 3083.3ND 58.5 52.9
Hexachloroethane ug/L 83.3 45 10-13038 18 3083.3ND 37.4 31.3
Indeno(1,2,3-cd)pyrene ug/L 83.3 139 39-174135 3 3083.3ND 116 113
Isophorone ug/L 83.3 75 19-14669 8 3083.3ND 62.4 57.5
N-Nitroso-di-n-propylamine ug/L 83.3 81 20-15071 12 3083.3ND 67.2 59.5
N-Nitrosodiphenylamine ug/L 83.3 108 33-149102 6 3083.3ND 90.0 84.6
Naphthalene ug/L 83.3 67 10-12860 11 3083.3ND 55.6 49.8
Nitrobenzene ug/L 83.3 68 19-14563 8 3083.3ND 56.9 52.7
Pentachlorophenol ug/L M1167810-18813 30167ND14.0J 21.0J
Phenanthrene ug/L 83.3 109 38-150104 5 3083.3ND 91.2 87.0
Phenol ug/L 83.3 16 10-13027 3083.3ND 13.1J 22.5
Pyrene ug/L 83.3 138 42-163130 6 3083.3ND 115 108
2,4,6-Tribromophenol (S) %S0910-16422
2-Fluorobiphenyl (S)%73 10-13062
2-Fluorophenol (S)%S0310-1309
Nitrobenzene-d5 (S)%69 10-13861
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147308MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688452005
4147309
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%12 10-13023
Terphenyl-d14 (S)%134 19-191117
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800448
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688066001, 92688066002, 92688066003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4145920
Associated Lab Samples:92688066001, 92688066002, 92688066003
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/19/23 14:105.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4145921LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 52.650 105 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4145922LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 50.650 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4145923MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92686947024
4145924
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 108 80-120109 0 25506.7 60.8 61.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4145925MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92686947025
4145926
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 84 80-12083 1 2550ND42.0 41.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800851
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688066004, 92688066005, 92688066006, 92688066007, 92688066008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4148204
Associated Lab Samples:92688066004, 92688066005, 92688066006, 92688066007, 92688066008
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/21/23 11:515.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4148205LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 52.450 105 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4149487LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 50.250 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4148206MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
4148207
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 100 80-12098 1 255085.1 135 134
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4148208MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4148209
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 113 80-120108 2 255081.0 137 135
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800665
SM 4500-S2D-2011
SM 4500-S2D-2011
4500S2D Sulfide Water
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147249
Associated Lab Samples: 92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Matrix: Water
AnalyzedMDL
Sulfide mg/L ND 0.10 09/20/23 02:400.022
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147250LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide mg/L 0.520.5 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147268MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
4147269
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 104 80-120107 3 100.5ND 0.53 0.54
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147270MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92686947023
4147271
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 103 80-120101 2 100.5ND 0.52 0.51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 116
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800065
EPA 9056A
EPA 9056A
9056 IC anions 28 Days
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4143912
Associated Lab Samples: 92688066001, 92688066002, 92688066003, 92688066004, 92688066005, 92688066006, 92688066007,92688066008
Matrix: Water
AnalyzedMDL
Chloride mg/L ND 1.0 09/15/23 20:480.60
Sulfate mg/L ND 1.0 09/15/23 20:480.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4143913LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 51.450 103 90-110
Sulfate mg/L 51.250 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4143914MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
4143915
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L M1508090-11080 0 105070.3 111 110
Sulfate mg/L 50 94 90-11092 1 1050146193 192
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 116
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Re-extraction conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.1g
Sample was received or analysis requested beyond the recognized method holding time.H3
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associatedsamples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in theassociated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 116
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92688066001 799946RW04 WG- 091323 SM 2120B-2011
92688066002 799946RW06 WG- 091323 SM 2120B-2011
92688066003 799946RW07 WG- 091323 SM 2120B-2011
92688066004 799946PZ01 WG- 091323 SM 2120B-2011
92688066005 799946PZ05 WG- 091323 SM 2120B-2011
92688066006 799946PZ03 WG- 091323 SM 2120B-2011
92688066007 799946PZ17 WG- 091323 SM 2120B-2011
92688066008 799946PZ17 HG- 091323 SM 2120B-2011
92688066009 799946BR02 WG- 091323 SM 2120B-2011
92688066001 954340 954437RW04 WG- 091323 EPA 3010 EPA 6010
92688066002 954340 954437RW06 WG- 091323 EPA 3010 EPA 6010
92688066003 954340 954437RW07 WG- 091323 EPA 3010 EPA 6010
92688066004 954340 954437PZ01 WG- 091323 EPA 3010 EPA 6010
92688066005 954340 954437PZ05 WG- 091323 EPA 3010 EPA 6010
92688066006 954340 954437PZ03 WG- 091323 EPA 3010 EPA 6010
92688066007 954340 954437PZ17 WG- 091323 EPA 3010 EPA 6010
92688066008 954340 954437PZ17 HG- 091323 EPA 3010 EPA 6010
92688066009 954340 954437BR02 WG- 091323 EPA 3010 EPA 6010
92688066001 954596 954652RW04 WG- 091323 EPA 3010 EPA 6010
92688066002 954596 954652RW06 WG- 091323 EPA 3010 EPA 6010
92688066003 954596 954652RW07 WG- 091323 EPA 3010 EPA 6010
92688066004 954596 954652PZ01 WG- 091323 EPA 3010 EPA 6010
92688066005 954596 954652PZ05 WG- 091323 EPA 3010 EPA 6010
92688066006 954596 954652PZ03 WG- 091323 EPA 3010 EPA 6010
92688066007 954596 954652PZ17 WG- 091323 EPA 3010 EPA 6010
92688066008 954596 954652PZ17 HG- 091323 EPA 3010 EPA 6010
92688066001 955304 955582RW04 WG- 091323 EPA 7470 EPA 7470
92688066002 955304 955582RW06 WG- 091323 EPA 7470 EPA 7470
92688066003 955304 955582RW07 WG- 091323 EPA 7470 EPA 7470
92688066004 955304 955582PZ01 WG- 091323 EPA 7470 EPA 7470
92688066005 955304 955582PZ05 WG- 091323 EPA 7470 EPA 7470
92688066006 955304 955582PZ03 WG- 091323 EPA 7470 EPA 7470
92688066007 955304 955582PZ17 WG- 091323 EPA 7470 EPA 7470
92688066008 955304 955582PZ17 HG- 091323 EPA 7470 EPA 7470
92688066009 955304 955582BR02 WG- 091323 EPA 7470 EPA 7470
92688066001 955306 955584RW04 WG- 091323 EPA 7470 EPA 7470
92688066002 955306 955584RW06 WG- 091323 EPA 7470 EPA 7470
92688066003 955306 955584RW07 WG- 091323 EPA 7470 EPA 7470
92688066004 955306 955584PZ01 WG- 091323 EPA 7470 EPA 7470
92688066005 955306 955584PZ05 WG- 091323 EPA 7470 EPA 7470
92688066006 955306 955584PZ03 WG- 091323 EPA 7470 EPA 7470
92688066007 955306 955584PZ17 WG- 091323 EPA 7470 EPA 7470
92688066008 955306 955584PZ17 HG- 091323 EPA 7470 EPA 7470
92688066001 800409 800733RW04 WG- 091323 EPA 3510C EPA 8270E
92688066002 800409 800733RW06 WG- 091323 EPA 3510C EPA 8270E
92688066003 800409 800733RW07 WG- 091323 EPA 3510C EPA 8270E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 116
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92688066
Pactiv Evergreen GWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92688066004 800409 800733PZ01 WG- 091323 EPA 3510C EPA 8270E
92688066005 800409 800733PZ05 WG- 091323 EPA 3510C EPA 8270E
92688066006 800409 800733PZ03 WG- 091323 EPA 3510C EPA 8270E
92688066007 800409 800733PZ17 WG- 091323 EPA 3510C EPA 8270E
92688066008 800409 800733PZ17 HG- 091323 EPA 3510C EPA 8270E
92688066009 800690 800926BR02 WG- 091323 EPA 3510C EPA 8270E
92688066001 801271RW04 WG- 091323 EPA 8260D
92688066002 801270RW06 WG- 091323 EPA 8260D
92688066003 801270RW07 WG- 091323 EPA 8260D
92688066004 801270PZ01 WG- 091323 EPA 8260D
92688066005 801270PZ05 WG- 091323 EPA 8260D
92688066006 801270PZ03 WG- 091323 EPA 8260D
92688066007 801270PZ17 WG- 091323 EPA 8260D
92688066008 801271PZ17 HG- 091323 EPA 8260D
92688066009 801271BR02 WG- 091323 EPA 8260D
92688066010 800498Trip Blank EPA 8260D
92688066001 800448RW04 WG- 091323 SM 2320B-2011
92688066002 800448RW06 WG- 091323 SM 2320B-2011
92688066003 800448RW07 WG- 091323 SM 2320B-2011
92688066004 800851PZ01 WG- 091323 SM 2320B-2011
92688066005 800851PZ05 WG- 091323 SM 2320B-2011
92688066006 800851PZ03 WG- 091323 SM 2320B-2011
92688066007 800851PZ17 WG- 091323 SM 2320B-2011
92688066008 800851PZ17 HG- 091323 SM 2320B-2011
92688066001 800665RW04 WG- 091323 SM 4500-S2D-2011
92688066002 800665RW06 WG- 091323 SM 4500-S2D-2011
92688066003 800665RW07 WG- 091323 SM 4500-S2D-2011
92688066004 800665PZ01 WG- 091323 SM 4500-S2D-2011
92688066005 800665PZ05 WG- 091323 SM 4500-S2D-2011
92688066006 800665PZ03 WG- 091323 SM 4500-S2D-2011
92688066007 800665PZ17 WG- 091323 SM 4500-S2D-2011
92688066008 800665PZ17 HG- 091323 SM 4500-S2D-2011
92688066001 800065RW04 WG- 091323 EPA 9056A
92688066002 800065RW06 WG- 091323 EPA 9056A
92688066003 800065RW07 WG- 091323 EPA 9056A
92688066004 800065PZ01 WG- 091323 EPA 9056A
92688066005 800065PZ05 WG- 091323 EPA 9056A
92688066006 800065PZ03 WG- 091323 EPA 9056A
92688066007 800065PZ17 WG- 091323 EPA 9056A
92688066008 800065PZ17 HG- 091323 EPA 9056A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 08:24 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 116
Page 92 of 116
Page 93 of 116
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Thisreportshouldnotbereproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamplesincludedinthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
Client - Charlotte
PACE Charlotte
9800 Kincey Ave.
Huntersville NC 28078
REPORT OF
LABORATORY
ANALYSIS FOR
PCDD/PCDF
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
October 5, 2023
Pace Project #: 10669217
Sample Receipt Date: 09/19/2023
Client Project #: 92688066
Client Sub PO #: N/A
The report provided has been invoiced as a Level 2
PCDD/PCDF Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questionstoIsaac Johnson,your Pace
Project Manager.
State Cert #: 530
Suite 100
Report Prepared for:
Page 1 of 22Report No.....10669217_SW8290AFC_L2_dfr
October 05, 2023
Isaac Johnson, Project Manager
[phone]
[phone] (fax)
[e-mail]
Page 95 of 116
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
This report presents the results from the analyses performed on eight samples submitted by a
representative of Pace Analytical Services, LLC. The samples were analyzed for the presence or absence
of polychlorodibenzo-p-dioxins (PCDDs) and polychlorodibenzofurans (PCDFs) using a modified version
of USEPA Method 8290A. The estimated detection limits (EDLs) were based on signal-to-noise
measurements. Estimated maximum possible concentration (EMPC) values were treated as positives inthe toxic equivalence calculations.
The isotopically-labeled PCDD/PCDF internal standards in the sample extracts were recovered at32-105%. Except for three low values, which were flagged "R" on the results table, the labeled internalstandard recoveries obtained for this project were within the 40-135% target range specified in Method8290A. Since the quantification of the native 2,3,7,8-substituted congeners was based on isotope dilution,the data were automatically corrected for recovery and accurate values were obtained.
Values were flagged "I" where incorrect isotope ratios were obtained or "P" where polychlorinateddiphenylethers were present. Concentrations below the calibration range were flagged "J" and should be
regarded as estimates.
A laboratory method blank was prepared and analyzed with the sample batch as part of our routine quality
control procedures. The results show the blank to contain trace levels of selected congeners. These
levels were below the calibration range of the method. Sample concentrations similar to the corresponding
blank levels were flagged "B" on the results tables and may be, at least partially, attributed to the
background.
Laboratory and matrix spike samples were also prepared using clean reference matrix or sample matrix
that had been fortified with native standard materials. The results show that the spiked native compounds
were recovered at 70-108% with relative percent differences of 0.1-4.2%. These results were within thetarget ranges for the method.
The response obtained for the labeled OCDD in calibration standard analysis L230924A_13 was outsidethe target range. As specified in our procedures for this method, the average of the daily response factorsfor this compound was used in the calculations for the samples from this runshift. The affected valueswere flagged "Y" on the results tables.
DISCUSSION
Page 2 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 96 of 116
REPORT OF LABORATORY ANALYSIS
This report shallnot bereproduced,except in full,
withoutthe written consentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Report No.....10668265
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 97 of 116
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 4 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 98 of 116
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Page 6 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 100 of 116
10669217
Page 7 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 101 of 116
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
A =
B = C = D = E = H2 =
I =
J = L = Nn = P = R =
S =
U = V = X = Y = * =
Reporting Limit based on signal to noise (EDL)
Less than 10x higher than method blank level Result obtained from confirmation analysis Result obtained from analysis of diluted sample Exceeds calibration range Extracted outside of holding time
Isotope ratio out of specification
Estimated value Suppressive interference, analyte may be biased low Value obtained from additional analysis PCDE Interference Recovery outside target range
Peak saturated
Analyte not detected Result verified by confirmation analysis %D Exceeds limits Calculated using average of daily RFs See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 8 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 102 of 116
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 9 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 103 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID RW04 WG-09132310669217001L230923A_07AH5
NA957 mL
NAL230816L230922B_18 & L230923A_18BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/13/2023 09:5009/19/2023 08:5009/20/2023 12:0009/23/2023 08:42
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF -----1.1 2,3,7,8-TCDF-13C 2.00 48IJ1.9Total TCDF 3.0 1.1 2,3,7,8-TCDD-13C 2.00 44J-----1,2,3,7,8-PeCDF-13C 2.00 472,3,7,8-TCDD ND 1.8 2,3,4,7,8-PeCDF-13C 2.00 45-----Total TCDD ND 1.8 1,2,3,7,8-PeCDD-13C 2.00 51-----1,2,3,4,7,8-HxCDF-13C 2.00 32 R1,2,3,7,8-PeCDF -----0.93 1,2,3,6,7,8-HxCDF-13C 2.00 54PJ3.52,3,4,7,8-PeCDF -----0.70 2,3,4,6,7,8-HxCDF-13C 2.00 54IJ1.3Total PeCDF 3.3 0.70 1,2,3,7,8,9-HxCDF-13C 2.00 48J-----1,2,3,4,7,8-HxCDD-13C 2.00 501,2,3,7,8-PeCDD 1.4 0.90 1,2,3,6,7,8-HxCDD-13C 2.00 55BJ-----Total PeCDD 3.7 0.90 1,2,3,4,6,7,8-HpCDF-13C 2.00 42BJ-----1,2,3,4,7,8,9-HpCDF-13C 2.00 36 R1,2,3,4,7,8-HxCDF ND 1.6 1,2,3,4,6,7,8-HpCDD-13C 2.00 51-----1,2,3,6,7,8-HxCDF ND 0.97 OCDD-13C 4.00 35-----R2,3,4,6,7,8-HxCDF 1.3 0.89 J-----1,2,3,7,8,9-HxCDF 1.3 1.2 1,2,3,4-TCDD-13C 2.00 NABJ-----Total HxCDF 8.3 0.89 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD -----2.4 2,3,7,8-TCDD-37Cl4 0.20 81IJ3.31,2,3,6,7,8-HxCDD ND 2.0-----1,2,3,7,8,9-HxCDD ND 2.1-----Total HxCDD 19 2.0 BJ-----
1,2,3,4,6,7,8-HpCDF ND 1.7 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 3.3 Equivalence: 2.9 pg/L-----Total HpCDF 3.1 1.7 (Lower-bound - Using 2005 WHO Factors)BJ-----
1,2,3,4,6,7,8-HpCDD 20 1.7 J-----Total HpCDD 140 1.7-----
OCDF 5.1 3.7 BJ-----OCDD 140 5.2-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelR=Recovery outside target rangeP = PCDE Interference
I=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 10 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 104 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID RW06 WG-09132310669217002L230923A_08AH5
NA819 mL
NAL230816L230922B_18 & L230923A_18BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/13/2023 10:2909/19/2023 08:5009/20/2023 12:0009/23/2023 09:25
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.44 2,3,7,8-TCDF-13C 2.00 89-----Total TCDF ND 0.44 2,3,7,8-TCDD-13C 2.00 84-----1,2,3,7,8-PeCDF-13C 2.00 832,3,7,8-TCDD ND 0.62 2,3,4,7,8-PeCDF-13C 2.00 85-----Total TCDD ND 0.62 1,2,3,7,8-PeCDD-13C 2.00 92-----1,2,3,4,7,8-HxCDF-13C 2.00 661,2,3,7,8-PeCDF ND 0.59 1,2,3,6,7,8-HxCDF-13C 2.00 104-----2,3,4,7,8-PeCDF ND 0.55 2,3,4,6,7,8-HxCDF-13C 2.00 105-----Total PeCDF ND 0.55 1,2,3,7,8,9-HxCDF-13C 2.00 96-----1,2,3,4,7,8-HxCDD-13C 2.00 1011,2,3,7,8-PeCDD ND 0.61 1,2,3,6,7,8-HxCDD-13C 2.00 102-----Total PeCDD ND 0.61 1,2,3,4,6,7,8-HpCDF-13C 2.00 81-----1,2,3,4,7,8,9-HpCDF-13C 2.00 691,2,3,4,7,8-HxCDF ND 2.0 1,2,3,4,6,7,8-HpCDD-13C 2.00 99-----1,2,3,6,7,8-HxCDF ND 0.72 OCDD-13C 4.00 68-----2,3,4,6,7,8-HxCDF ND 0.65-----1,2,3,7,8,9-HxCDF -----0.58 1,2,3,4-TCDD-13C 2.00 NAIJ1.2Total HxCDF ND 0.58 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD 2.3 0.71 2,3,7,8-TCDD-37Cl4 0.20 85BJ-----1,2,3,6,7,8-HxCDD ND 0.70-----1,2,3,7,8,9-HxCDD ND 0.69-----Total HxCDD 2.3 0.69 BJ-----
1,2,3,4,6,7,8-HpCDF ND 0.87 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 1.9 Equivalence: 0.38 pg/L-----Total HpCDF ND 0.87 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----0.99 IJ2.3Total HpCDD ND 0.99-----
OCDF -----1.7 IJ2.4OCDD25 3.2 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 11 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 105 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID RW07 WG-09132310669217003L230923A_09AH5
NA851 mL
NAL230816L230922B_18 & L230923A_18BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/13/2023 12:2709/19/2023 08:5009/20/2023 12:0009/23/2023 10:09
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.59 2,3,7,8-TCDF-13C 2.00 91-----Total TCDF ND 0.59 2,3,7,8-TCDD-13C 2.00 85-----1,2,3,7,8-PeCDF-13C 2.00 862,3,7,8-TCDD ND 0.77 2,3,4,7,8-PeCDF-13C 2.00 86-----Total TCDD ND 0.77 1,2,3,7,8-PeCDD-13C 2.00 93-----1,2,3,4,7,8-HxCDF-13C 2.00 651,2,3,7,8-PeCDF ND 0.60 1,2,3,6,7,8-HxCDF-13C 2.00 99-----2,3,4,7,8-PeCDF ND 0.43 2,3,4,6,7,8-HxCDF-13C 2.00 101-----Total PeCDF ND 0.43 1,2,3,7,8,9-HxCDF-13C 2.00 91-----1,2,3,4,7,8-HxCDD-13C 2.00 961,2,3,7,8-PeCDD ND 0.62 1,2,3,6,7,8-HxCDD-13C 2.00 101-----Total PeCDD ND 0.62 1,2,3,4,6,7,8-HpCDF-13C 2.00 77-----1,2,3,4,7,8,9-HpCDF-13C 2.00 661,2,3,4,7,8-HxCDF ND 0.80 1,2,3,4,6,7,8-HpCDD-13C 2.00 90-----1,2,3,6,7,8-HxCDF ND 0.47 OCDD-13C 4.00 58-----2,3,4,6,7,8-HxCDF ND 0.44-----1,2,3,7,8,9-HxCDF 1.2 0.64 1,2,3,4-TCDD-13C 2.00 NABJ-----Total HxCDF 1.2 0.44 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD 2.2 0.61 2,3,7,8-TCDD-37Cl4 0.20 90BJ-----1,2,3,6,7,8-HxCDD ND 0.54-----1,2,3,7,8,9-HxCDD ND 0.56-----Total HxCDD 2.2 0.54 BJ-----
1,2,3,4,6,7,8-HpCDF ND 1.2 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 2.2 Equivalence: 0.36 pg/L-----Total HpCDF ND 1.2 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----1.3 IJ2.0Total HpCDD ND 1.3-----
OCDF 3.2 2.5 BJ-----OCDD 28 3.7 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 12 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 106 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ01 WG-09132310669217004L230923A_10AH5
NA926 mL
NAL230816L230922B_18 & L230923A_18BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/13/2023 12:5409/19/2023 08:5009/20/2023 12:0009/23/2023 10:53
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.71 2,3,7,8-TCDF-13C 2.00 68-----Total TCDF ND 0.71 2,3,7,8-TCDD-13C 2.00 59-----1,2,3,7,8-PeCDF-13C 2.00 592,3,7,8-TCDD ND 1.1 2,3,4,7,8-PeCDF-13C 2.00 62-----Total TCDD ND 1.1 1,2,3,7,8-PeCDD-13C 2.00 65-----1,2,3,4,7,8-HxCDF-13C 2.00 411,2,3,7,8-PeCDF -----0.65 1,2,3,6,7,8-HxCDF-13C 2.00 68PJ112,3,4,7,8-PeCDF ND 0.45 2,3,4,6,7,8-HxCDF-13C 2.00 70-----Total PeCDF 0.82 0.45 1,2,3,7,8,9-HxCDF-13C 2.00 61J-----1,2,3,4,7,8-HxCDD-13C 2.00 681,2,3,7,8-PeCDD ND 0.51 1,2,3,6,7,8-HxCDD-13C 2.00 64-----Total PeCDD ND 0.51 1,2,3,4,6,7,8-HpCDF-13C 2.00 52-----1,2,3,4,7,8,9-HpCDF-13C 2.00 451,2,3,4,7,8-HxCDF ND 1.7 1,2,3,4,6,7,8-HpCDD-13C 2.00 62-----1,2,3,6,7,8-HxCDF ND 1.1 OCDD-13C 4.00 43-----2,3,4,6,7,8-HxCDF ND 0.98-----1,2,3,7,8,9-HxCDF ND 1.3 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF 2.0 0.98 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD ND 0.95 2,3,7,8-TCDD-37Cl4 0.20 80-----1,2,3,6,7,8-HxCDD ND 0.87-----1,2,3,7,8,9-HxCDD ND 0.89-----Total HxCDD ND 0.87-----
1,2,3,4,6,7,8-HpCDF -----1.8 Total 2,3,7,8-TCDDIJ3.11,2,3,4,7,8,9-HpCDF ND 3.3 Equivalence: 0.47 pg/L-----Total HpCDF ND 1.8 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD 7.7 1.4 BJ-----Total HpCDD 7.7 1.4 BJ-----
OCDF 11 2.9 BJ-----OCDD 83 3.6 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelP = PCDE InterferenceI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 13 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 107 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ05 WG-09132310669217005L230922B_11AH5
NA902 mL
NAL230816L230922B_01 & L230922B_18BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/13/2023 14:4609/19/2023 08:5009/20/2023 12:0009/22/2023 22:32
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.54 2,3,7,8-TCDF-13C 2.00 88-----Total TCDF ND 0.54 2,3,7,8-TCDD-13C 2.00 80-----1,2,3,7,8-PeCDF-13C 2.00 862,3,7,8-TCDD ND 0.86 2,3,4,7,8-PeCDF-13C 2.00 88-----Total TCDD ND 0.86 1,2,3,7,8-PeCDD-13C 2.00 96-----1,2,3,4,7,8-HxCDF-13C 2.00 761,2,3,7,8-PeCDF ND 0.43 1,2,3,6,7,8-HxCDF-13C 2.00 98-----2,3,4,7,8-PeCDF ND 0.30 2,3,4,6,7,8-HxCDF-13C 2.00 99-----Total PeCDF ND 0.30 1,2,3,7,8,9-HxCDF-13C 2.00 92-----1,2,3,4,7,8-HxCDD-13C 2.00 931,2,3,7,8-PeCDD ND 0.42 1,2,3,6,7,8-HxCDD-13C 2.00 96-----Total PeCDD ND 0.42 1,2,3,4,6,7,8-HpCDF-13C 2.00 74-----1,2,3,4,7,8,9-HpCDF-13C 2.00 711,2,3,4,7,8-HxCDF ND 0.89 1,2,3,4,6,7,8-HpCDD-13C 2.00 86-----1,2,3,6,7,8-HxCDF ND 0.68 OCDD-13C 4.00 73-----2,3,4,6,7,8-HxCDF ND 0.65-----1,2,3,7,8,9-HxCDF 1.6 0.91 1,2,3,4-TCDD-13C 2.00 NABJ-----Total HxCDF 1.6 0.65 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD -----1.1 2,3,7,8-TCDD-37Cl4 0.20 85IJ1.51,2,3,6,7,8-HxCDD ND 0.98-----1,2,3,7,8,9-HxCDD ND 1.00-----Total HxCDD ND 0.98-----
1,2,3,4,6,7,8-HpCDF ND 1.2 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 2.0 Equivalence: 0.34 pg/L-----Total HpCDF ND 1.2 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD 2.4 1.5 BJ-----Total HpCDD 2.4 1.5 BJ-----
OCDF 4.5 2.9 BJ-----OCDD 24 3.6 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 14 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 108 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ03 WG-09132310669217006L230923A_11AH5
NA249 mL
NAL230816L230922B_18 & L230923A_18BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/13/2023 15:2709/19/2023 08:5009/20/2023 12:0009/23/2023 11:36
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 2.4 2,3,7,8-TCDF-13C 2.00 65-----Total TCDF ND 2.4 2,3,7,8-TCDD-13C 2.00 61-----1,2,3,7,8-PeCDF-13C 2.00 622,3,7,8-TCDD ND 4.4 2,3,4,7,8-PeCDF-13C 2.00 64-----Total TCDD ND 4.4 1,2,3,7,8-PeCDD-13C 2.00 71-----1,2,3,4,7,8-HxCDF-13C 2.00 451,2,3,7,8-PeCDF ND 1.8 1,2,3,6,7,8-HxCDF-13C 2.00 74-----2,3,4,7,8-PeCDF ND 1.4 2,3,4,6,7,8-HxCDF-13C 2.00 77-----Total PeCDF ND 1.4 1,2,3,7,8,9-HxCDF-13C 2.00 68-----1,2,3,4,7,8-HxCDD-13C 2.00 741,2,3,7,8-PeCDD ND 1.7 1,2,3,6,7,8-HxCDD-13C 2.00 76-----Total PeCDD ND 1.7 1,2,3,4,6,7,8-HpCDF-13C 2.00 54-----1,2,3,4,7,8,9-HpCDF-13C 2.00 491,2,3,4,7,8-HxCDF ND 3.9 1,2,3,4,6,7,8-HpCDD-13C 2.00 71-----1,2,3,6,7,8-HxCDF ND 2.3 OCDD-13C 4.00 52-----2,3,4,6,7,8-HxCDF ND 2.2-----1,2,3,7,8,9-HxCDF ND 3.1 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 2.2 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD 8.3 3.9 2,3,7,8-TCDD-37Cl4 0.20 78BJ-----1,2,3,6,7,8-HxCDD ND 3.7-----1,2,3,7,8,9-HxCDD ND 3.7-----Total HxCDD 8.3 3.7 BJ-----
1,2,3,4,6,7,8-HpCDF ND 5.6 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 10 Equivalence: 0.97 pg/L-----Total HpCDF ND 5.6 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----5.2 IJ8.9Total HpCDD ND 5.2-----
OCDF ND 9.6-----OCDD 160 11 J-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 15 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 109 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ17 WG-09132310669217007L230923A_12AH5
NA856 mL
NAL230816L230922B_18 & L230923A_18BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/13/2023 16:5609/19/2023 08:5009/20/2023 12:0009/23/2023 12:20
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.55 2,3,7,8-TCDF-13C 2.00 94-----Total TCDF ND 0.55 2,3,7,8-TCDD-13C 2.00 81-----1,2,3,7,8-PeCDF-13C 2.00 872,3,7,8-TCDD ND 0.68 2,3,4,7,8-PeCDF-13C 2.00 85-----Total TCDD ND 0.68 1,2,3,7,8-PeCDD-13C 2.00 94-----1,2,3,4,7,8-HxCDF-13C 2.00 601,2,3,7,8-PeCDF ND 0.49 1,2,3,6,7,8-HxCDF-13C 2.00 97-----2,3,4,7,8-PeCDF ND 0.34 2,3,4,6,7,8-HxCDF-13C 2.00 102-----Total PeCDF ND 0.34 1,2,3,7,8,9-HxCDF-13C 2.00 90-----1,2,3,4,7,8-HxCDD-13C 2.00 971,2,3,7,8-PeCDD ND 0.30 1,2,3,6,7,8-HxCDD-13C 2.00 100-----Total PeCDD ND 0.30 1,2,3,4,6,7,8-HpCDF-13C 2.00 74-----1,2,3,4,7,8,9-HpCDF-13C 2.00 601,2,3,4,7,8-HxCDF ND 0.72 1,2,3,4,6,7,8-HpCDD-13C 2.00 89-----1,2,3,6,7,8-HxCDF ND 0.46 OCDD-13C 4.00 61-----2,3,4,6,7,8-HxCDF ND 0.43-----1,2,3,7,8,9-HxCDF -----0.57 1,2,3,4-TCDD-13C 2.00 NAIJ1.00Total HxCDF 0.70 0.43 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD 2.3 0.68 2,3,7,8-TCDD-37Cl4 0.20 87BJ-----1,2,3,6,7,8-HxCDD ND 0.64-----1,2,3,7,8,9-HxCDD ND 0.65-----Total HxCDD 2.3 0.64 BJ-----
1,2,3,4,6,7,8-HpCDF 1.1 1.1 Total 2,3,7,8-TCDDBJ-----1,2,3,4,7,8,9-HpCDF ND 2.2 Equivalence: 0.38 pg/L-----Total HpCDF 3.7 1.1 (Lower-bound - Using 2005 WHO Factors)BJ-----
1,2,3,4,6,7,8-HpCDD 3.0 0.97 BJ-----Total HpCDD 3.0 0.97 BJ-----
OCDF 2.5 2.3 BJ-----OCDD 25 3.4 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 16 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 110 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ17 HG-09132310669217008L230924A_09BAL
NA860 mL
NAL230816L230924A_01 & L230924A_13BLANK-108427
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/13/2023 16:5809/19/2023 08:5009/20/2023 12:0009/24/2023 21:20
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.53 2,3,7,8-TCDF-13C 2.00 70-----Total TCDF ND 0.53 2,3,7,8-TCDD-13C 2.00 62-----1,2,3,7,8-PeCDF-13C 2.00 692,3,7,8-TCDD ND 0.48 2,3,4,7,8-PeCDF-13C 2.00 71-----Total TCDD ND 0.48 1,2,3,7,8-PeCDD-13C 2.00 75-----1,2,3,4,7,8-HxCDF-13C 2.00 491,2,3,7,8-PeCDF ND 0.55 1,2,3,6,7,8-HxCDF-13C 2.00 77-----2,3,4,7,8-PeCDF ND 0.38 2,3,4,6,7,8-HxCDF-13C 2.00 77-----Total PeCDF ND 0.38 1,2,3,7,8,9-HxCDF-13C 2.00 66-----1,2,3,4,7,8-HxCDD-13C 2.00 701,2,3,7,8-PeCDD ND 0.45 1,2,3,6,7,8-HxCDD-13C 2.00 75-----Total PeCDD ND 0.45 1,2,3,4,6,7,8-HpCDF-13C 2.00 53-----1,2,3,4,7,8,9-HpCDF-13C 2.00 401,2,3,4,7,8-HxCDF ND 0.61 1,2,3,4,6,7,8-HpCDD-13C 2.00 56-----1,2,3,6,7,8-HxCDF ND 0.39 OCDD-13C 4.00 48-----Y2,3,4,6,7,8-HxCDF ND 0.37-----1,2,3,7,8,9-HxCDF 1.2 0.55 1,2,3,4-TCDD-13C 2.00 NABJ-----Total HxCDF 1.2 0.37 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD -----0.63 2,3,7,8-TCDD-37Cl4 0.20 76IJ2.11,2,3,6,7,8-HxCDD ND 0.57-----1,2,3,7,8,9-HxCDD ND 0.58-----Total HxCDD ND 0.57-----
1,2,3,4,6,7,8-HpCDF ND 1.4 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 3.1 Equivalence: 0.37 pg/L-----Total HpCDF ND 1.4 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD 2.9 1.9 BJ-----Total HpCDD 2.9 1.9 BJ-----
OCDF ND 3.6-----OCDD -----4.2 IJ20
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specificationY =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 17 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 111 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
BLANK-108427L230922B_09
AH5
983 mLL230816L230922B_01 & L230922B_18
MatrixDilutionExtractedAnalyzed
Water
09/20/2023 12:0009/22/2023 21:05
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKOY
NativeIsomers pg/LConc EMPCpg/L pg/L InternalStandards Addedng's PercentRecoveryEDL
2,3,7,8-TCDF -----0.67 0.54 IJ 2,3,7,8-TCDF-13C 2.00 97Total TCDF ND -----0.54 2,3,7,8-TCDD-13C 2.00 901,2,3,7,8-PeCDF-13C 2.00 962,3,7,8-TCDD ND -----0.74 2,3,4,7,8-PeCDF-13C 2.00 91Total TCDD ND -----0.74 1,2,3,7,8-PeCDD-13C 2.00 1081,2,3,4,7,8-HxCDF-13C 2.00 791,2,3,7,8-PeCDF -----1.1 0.54 IJ 1,2,3,6,7,8-HxCDF-13C 2.00 1062,3,4,7,8-PeCDF -----0.72 0.40 IJ 2,3,4,6,7,8-HxCDF-13C 2.00 110Total PeCDF ND -----0.40 1,2,3,7,8,9-HxCDF-13C 2.00 1031,2,3,4,7,8-HxCDD-13C 2.00 1011,2,3,7,8-PeCDD 0.93 -----0.35 J 1,2,3,6,7,8-HxCDD-13C 2.00 114Total PeCDD 0.93 -----0.35 J 1,2,3,4,6,7,8-HpCDF-13C 2.00 901,2,3,4,7,8,9-HpCDF-13C 2.00 801,2,3,4,7,8-HxCDF 1.1 -----0.33 J 1,2,3,4,6,7,8-HpCDD-13C 2.00 1061,2,3,6,7,8-HxCDF -----0.73 0.23 IJ OCDD-13C 4.00 842,3,4,6,7,8-HxCDF -----0.49 0.22 IJ1,2,3,7,8,9-HxCDF 1.7 -----0.29 J 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF 2.7 -----0.22 J 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 2.9 -----0.55 J 2,3,7,8-TCDD-37Cl4 0.20 991,2,3,6,7,8-HxCDD -----0.73 0.50 IJ1,2,3,7,8,9-HxCDD -----1.1 0.51 IJTotal HxCDD 2.9 -----0.50 J
1,2,3,4,6,7,8-HpCDF 1.4 -----0.80 J Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----1.5 Equivalence: 2.1 pg/LTotal HpCDF 1.4 -----0.80 J (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD 1.7 -----0.83 JTotal HpCDD 1.7 -----0.83 J
OCDF 2.9 -----1.5 JOCDD12-----1.9 J
Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
I =Isotope ratio out of specification
EDL=EstimatedDetection Limit
Page 18 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 112 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCS-108428L230922B_02
AH5
947 mLL230816L230922B_01 & L230922B_18
MatrixDilutionExtractedAnalyzed
Water
09/20/2023 12:0009/22/2023 16:00
NA
Method Blank ID BLANK-108427
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.21 2,3,7,8-TCDF-13C 2.0 81103Total TCDF 2,3,7,8-TCDD-13C 2.0 711,2,3,7,8-PeCDF-13C 2.0 852,3,7,8-TCDD 0.20 0.22 2,3,4,7,8-PeCDF-13C 2.0 78108Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 951,2,3,4,7,8-HxCDF-13C 2.0 781,2,3,7,8-PeCDF 1.0 0.95 1,2,3,6,7,8-HxCDF-13C 2.0 87952,3,4,7,8-PeCDF 1.0 0.99 2,3,4,6,7,8-HxCDF-13C 2.0 8599Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 861,2,3,4,7,8-HxCDD-13C 2.0 821,2,3,7,8-PeCDD 1.0 0.97 1,2,3,6,7,8-HxCDD-13C 2.0 8797Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 841,2,3,4,7,8,9-HpCDF-13C 2.0 761,2,3,4,7,8-HxCDF 1.0 0.92 1,2,3,4,6,7,8-HpCDD-13C 2.0 94921,2,3,6,7,8-HxCDF 1.0 0.98 OCDD-13C 4.0 79982,3,4,6,7,8-HxCDF 1.0 0.99 991,2,3,7,8,9-HxCDF 1.0 0.98 1,2,3,4-TCDD-13C 2.0 NA98Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.1 2,3,7,8-TCDD-37Cl4 0.20 771051,2,3,6,7,8-HxCDD 1.0 0.98 981,2,3,7,8,9-HxCDD 1.0 1.1 107Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.90 901,2,3,4,7,8,9-HpCDF 1.0 0.95 95Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.81 81Total HpCDD
OCDF 2.0 1.5 73OCDD2.0 1.4 70
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 19 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 113 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
10669217005-MSL230922B_06
AH5
864 mLL230816L230922B_01 & L230922B_18
MatrixDilutionExtractedAnalyzed
WATER
09/20/2023 12:0009/22/2023 18:54
Client - PACE Charlotte
NA
Method Blank ID BLANK-108427
Client's Sample ID PZ05 WG-091323-MS
Method 8290A Spiked Sample Report
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.20 2,3,7,8-TCDF-13C 2.00 801012,3,7,8-TCDD-13C 2.00 741,2,3,7,8-PeCDF-13C 2.00 792,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.00 831041,2,3,7,8-PeCDD-13C 2.00 891,2,3,4,7,8-HxCDF-13C 2.00 741,2,3,7,8-PeCDF 1.00 0.96 1,2,3,6,7,8-HxCDF-13C 2.00 90962,3,4,7,8-PeCDF 1.00 0.95 2,3,4,6,7,8-HxCDF-13C 2.00 89951,2,3,7,8,9-HxCDF-13C 2.00 841,2,3,4,7,8-HxCDD-13C 2.00 841,2,3,7,8-PeCDD 1.00 0.92 1,2,3,6,7,8-HxCDD-13C 2.00 90921,2,3,4,6,7,8-HpCDF-13C 2.00 751,2,3,4,7,8,9-HpCDF-13C 2.00 741,2,3,4,7,8-HxCDF 1.00 0.89 1,2,3,4,6,7,8-HpCDD-13C 2.00 82891,2,3,6,7,8-HxCDF 1.00 0.96 OCDD-13C 4.00 70962,3,4,6,7,8-HxCDF 1.00 1.00 1001,2,3,7,8,9-HxCDF 1.00 0.95 1,2,3,4-TCDD-13C 2.00 NA951,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 1.00 1.05 2,3,7,8-TCDD-37Cl4 0.20 761051,2,3,6,7,8-HxCDD 1.00 0.94 941,2,3,7,8,9-HxCDD 1.00 0.98 98
1,2,3,4,6,7,8-HpCDF 1.00 0.90 901,2,3,4,7,8,9-HpCDF 1.00 0.90 90
1,2,3,4,6,7,8-HpCDD 1.00 0.86 86
OCDF 2.00 1.84 92OCDD2.00 1.85 91
Qs = Quantity Spiked Qm = Quantity Measured Rec. = Recovery (Expressed as Percent)
Page 20 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 114 of 116
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
10669217005-MSDL230922B_07
AH5
916 mLL230816L230922B_01 & L230922B_18
MatrixDilutionExtractedAnalyzed
WATER
09/20/2023 12:0009/22/2023 19:38
Client - PACE Charlotte
NA
Method Blank ID BLANK-108427
Client's Sample ID PZ05 WG-091323-MSD
Method 8290A Spiked Sample Report
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.20 2,3,7,8-TCDF-13C 2.00 771002,3,7,8-TCDD-13C 2.00 721,2,3,7,8-PeCDF-13C 2.00 762,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.00 791041,2,3,7,8-PeCDD-13C 2.00 871,2,3,4,7,8-HxCDF-13C 2.00 691,2,3,7,8-PeCDF 1.00 0.96 1,2,3,6,7,8-HxCDF-13C 2.00 87962,3,4,7,8-PeCDF 1.00 0.96 2,3,4,6,7,8-HxCDF-13C 2.00 88961,2,3,7,8,9-HxCDF-13C 2.00 801,2,3,4,7,8-HxCDD-13C 2.00 841,2,3,7,8-PeCDD 1.00 0.93 1,2,3,6,7,8-HxCDD-13C 2.00 88931,2,3,4,6,7,8-HpCDF-13C 2.00 691,2,3,4,7,8,9-HpCDF-13C 2.00 661,2,3,4,7,8-HxCDF 1.00 0.92 1,2,3,4,6,7,8-HpCDD-13C 2.00 80921,2,3,6,7,8-HxCDF 1.00 0.98 OCDD-13C 4.00 64982,3,4,6,7,8-HxCDF 1.00 0.98 981,2,3,7,8,9-HxCDF 1.00 0.96 1,2,3,4-TCDD-13C 2.00 NA961,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 1.00 1.06 2,3,7,8-TCDD-37Cl4 0.20 741061,2,3,6,7,8-HxCDD 1.00 0.95 951,2,3,7,8,9-HxCDD 1.00 0.97 97
1,2,3,4,6,7,8-HpCDF 1.00 0.94 941,2,3,4,7,8,9-HpCDF 1.00 0.93 93
1,2,3,4,6,7,8-HpCDD 1.00 0.85 85
OCDF 2.00 1.87 93OCDD2.00 1.88 93
Qs = Quantity Spiked Qm = Quantity Measured Rec. = Recovery (Expressed as Percent)
Page 21 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 115 of 116
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]Method 8290A Spike Sample Results
Client - PACE Charlotte
Client Sample ID
Lab Sample ID
MS ID
MSD ID
PZ05 WG-091323
10669217005
10669217005-MS
10669217005-MSD
Sample Filename
MS Filename
MSD Filename
L230922B_11
L230922B_06
L230922B_07
Analyte
Quantity Unspiked Sample Contribution
to MS to MSD
Quantity Measured
MS MSD
RPD
Spiked
(ng)
Subtracted Recovery
MS MSD
(ng)(ng)(ng)(ng)(%)(%)
2,3,7,8-TCDF 0.20 ND ND 0.20 0.20 101 1001.4
2,3,7,8-TCDD 0.20 ND ND 0.21 0.21 104 1040.1
1,2,3,7,8-PeCDF 1.00 ND ND 0.96 0.96 96 960.1
2,3,4,7,8-PeCDF 1.00 ND ND 0.95 0.96 95 960.2
1,2,3,7,8-PeCDD 1.00 ND ND 0.92 0.93 92 931.8
1,2,3,4,7,8-HxCDF 1.00 ND ND 0.89 0.92 89 923.3
1,2,3,6,7,8-HxCDF 1.00 ND ND 0.96 0.98 96 982.0
2,3,4,6,7,8-HxCDF 1.00 ND ND 1.00 0.98 100 981.5
1,2,3,7,8,9-HxCDF 1.00 0.00134 0.00142 0.95 0.96 95 961.0
1,2,3,4,7,8-HxCDD 1.00 0.00149 0.00157 1.05 1.06 105 1060.5
1,2,3,6,7,8-HxCDD 1.00 ND ND 0.94 0.95 94 950.8
1,2,3,7,8,9-HxCDD 1.00 ND ND 0.98 0.97 98 971.0
1,2,3,4,6,7,8-HpCDF 1.00 ND ND 0.90 0.94 90 944.2
1,2,3,4,7,8,9-HpCDF 1.00 ND ND 0.90 0.93 90 933.5
1,2,3,4,6,7,8-HpCDD 1.00 0.00205 0.00218 0.86 0.85 86 850.7
OCDF 2.00 0.00385 0.00408 1.84 1.87 92 931.6
OCDD 2.00 0.0205 0.0217 1.85 1.88 91 931.5
Quantity Spiked - the amount of analyte spiked into the spiked samplesUnspiked Sample Contribution - calculated based on the amount found in the sample and the extracted amounts of the spiked and unspiked samplesQuantity Measured - the total amount of analyte measured in the spiked samplesRPD - the Relative Percent Difference of the spiked sample Quantity Measured valuesSubtracted Recovery - calculated after subtracting the unspiked sample contribution
Page 22 of 22Report No.....10669217_SW8290AFC_L2_dfr
Page 116 of 116
#=CL#
October 31, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92688280
92688280
Project:
Pace Project No.:
RE:
Christina AshdownENSAFE313 Wingo WayMount Pleasant, SC 29464
Pactiv Evergreen GWS
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on September 15, 2023. The results relate onlyto the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and thelaboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc: Jennings Kerr, ENSAFE Inc.
Lab, ENSAFE Inc.
David Warren, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 183
#=CP#
CERTIFICATIONS
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Project:
92688280
Pactiv Evergreen GWS
Pace Analytical Services Ormond Beach
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REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 2 of 183
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Lab ID Sample ID Matrix Date Collected Date Received
92688280001 PZ12WG-091423 Water 09/14/23 10:05 09/15/23 16:42
92688280002 PZ14WG-091423 Water 09/14/23 11:28 09/15/23 16:42
92688280003 PZ14HG-091423 Water 09/14/23 11:30 09/15/23 16:42
92688280004 BR01WG-091423 Water 09/14/23 12:00 09/15/23 16:42
92688280005 PZ11WG-091423 Water 09/14/23 12:12 09/15/23 16:42
92688280006 PZ06WG-091423 Water 09/14/23 15:40 09/15/23 16:42
92688280007 PZ02WG-091423 Water 09/14/23 14:58 09/15/23 16:42
92688280008 BR03WG-091423 Water 09/14/23 17:30 09/15/23 16:42
92688280009 EB01Q-091423 Water 09/14/23 17:20 09/15/23 16:42
92688280010 PZ13WG-091523 Water 09/15/23 10:06 09/15/23 16:42
92688280011 PZ07WG-091523 Water 09/15/23 11:00 09/15/23 16:42
92688280012 TB1-091423 Water 09/14/23 09:00 09/15/23 16:32
92688280013 TB2-091423 Water 09/14/23 09:00 09/15/23 16:32
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 183
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92688280001 PZ12WG-091423 EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CTMH
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688280002 PZ14WG-091423 EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CTMH
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688280003 PZ14HG-091423 EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CTMH
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688280004 BR01WG-091423 EPA 6010 17 PASI-OAME, KC2
EPA 6010 17 PASI-OAAM1, KC2
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688280005 PZ11WG-091423 EPA 6010 17 PASI-OAME
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 183
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688280006 PZ06WG-091423 EPA 6010 17 PASI-OAAM1, AME
EPA 6010 17 PASI-OAAM1, KC2
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688280007 PZ02WG-091423 EPA 1664B 1 PASI-CDVR
EPA 8015C 2 PASI-CHH
EPA 5030B/8015C 2 PASI-CTEG
EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-ARVS
SM 2540D-2015 1 PASI-AMAB2
SM 4500-S2D-2011 1 PASI-AJP1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
SM 5220D-2011 1 PASI-AJMH1
SM 5310B-2014 1 PASI-AMJP
EPA 9056A 2 PASI-ACDC
92688280008 BR03WG-091423 EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 183
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688280009 EB01Q-091423 EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688280010 PZ13WG-091523 EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-AYEG
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92688280011 PZ07WG-091523 EPA 1664B 1 PASI-CDVR
EPA 8015C 2 PASI-CHH
EPA 5030B/8015C 2 PASI-CTEG
EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAAM1
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-AYEG
SM 2540C-2015 1 PASI-ARVS
SM 2540D-2015 1 PASI-AMAB2
SM 4500-S2D-2011 1 PASI-AJP1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 183
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
SM 5220D-2011 1 PASI-AJMH1
SM 5310B-2014 1 PASI-AMJP
EPA 9056A 2 PASI-ACDC
92688280012 TB1-091423 EPA 8260D 52 PASI-CLMB
92688280013 TB2-091423 EPA 5030B/8015C 2 PASI-CTEG
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ12WG-091423 Lab ID: 92688280001 Collected: 09/14/23 10:05 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:20 7440-36-0 D310/02/23 09:460.030 0.011 2
Arsenic 0.042 mg/L 10/04/23 00:20 7440-38-210/02/23 09:460.020 0.0068 2
Barium 0.36 mg/L 10/04/23 00:20 7440-39-310/02/23 09:460.020 0.0017 2
Beryllium 0.0025J mg/L 10/04/23 00:20 7440-41-710/02/23 09:460.0080 0.00034 2
Boron 0.44 mg/L 10/04/23 00:20 7440-42-810/02/23 09:460.10 0.025 2
Cadmium ND mg/L 10/04/23 00:20 7440-43-9 D310/02/23 09:460.0020 0.00066 2
Chromium 0.17 mg/L 10/04/23 00:20 7440-47-310/02/23 09:460.010 0.0034 2
Cobalt 0.0035J mg/L 10/04/23 00:20 7440-48-410/02/23 09:460.020 0.0019 2
Copper ND mg/L 10/04/23 00:20 7440-50-8 D310/02/23 09:460.010 0.0052 2
Lead ND mg/L 10/04/23 00:20 7439-92-1 D310/02/23 09:460.020 0.0042 2
Manganese 0.18 mg/L 10/04/23 00:20 7439-96-510/02/23 09:460.010 0.0022 2
Nickel 0.055 mg/L 10/04/23 00:20 7440-02-010/02/23 09:460.010 0.0020 2
Selenium ND mg/L 10/04/23 00:20 7782-49-2 D310/02/23 09:460.030 0.0078 2
Silver ND mg/L 10/04/23 00:20 7440-22-4 D310/02/23 09:460.010 0.0020 2
Thallium ND mg/L 10/04/23 00:20 7440-28-0 D310/02/23 09:460.030 0.0058 2
Vanadium 0.96 mg/L 10/04/23 00:20 7440-62-210/02/23 09:460.020 0.0020 2
Zinc ND mg/L 10/04/23 00:20 7440-66-6 D310/02/23 09:460.040 0.022 2
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:08 7440-36-010/03/23 06:040.015 0.0055 1
Arsenic, Dissolved 0.042 mg/L 10/05/23 11:08 7440-38-210/03/23 06:040.010 0.0034 1
Barium, Dissolved 0.34 mg/L 10/05/23 11:08 7440-39-310/03/23 06:040.010 0.00084 1
Beryllium, Dissolved 0.0019J mg/L 10/05/23 11:08 7440-41-710/03/23 06:040.0040 0.00017 1
Boron, Dissolved 0.43 mg/L 10/05/23 11:08 7440-42-810/03/23 06:040.050 0.012 1
Cadmium, Dissolved ND mg/L 10/05/23 11:08 7440-43-910/03/23 06:040.0010 0.00033 1
Chromium, Dissolved 0.15 mg/L 10/05/23 11:08 7440-47-310/03/23 06:040.0050 0.0017 1
Cobalt, Dissolved 0.0030J mg/L 10/05/23 11:08 7440-48-410/03/23 06:040.010 0.00096 1
Copper, Dissolved ND mg/L 10/05/23 11:08 7440-50-810/03/23 06:040.0050 0.0026 1
Lead, Dissolved ND mg/L 10/05/23 11:08 7439-92-110/03/23 06:040.010 0.0021 1
Manganese, Dissolved 0.15 mg/L 10/05/23 11:08 7439-96-510/03/23 06:040.0050 0.0011 1
Nickel, Dissolved 0.046 mg/L 10/05/23 11:08 7440-02-010/03/23 06:040.0050 0.0010 1
Selenium, Dissolved ND mg/L 10/05/23 11:08 7782-49-210/03/23 06:040.015 0.0039 1
Silver, Dissolved ND mg/L 10/05/23 11:08 7440-22-410/03/23 06:040.0050 0.0010 1
Thallium, Dissolved ND mg/L 10/05/23 11:08 7440-28-010/03/23 06:040.015 0.0029 1
Vanadium, Dissolved 0.81 mg/L 10/05/23 11:08 7440-62-210/03/23 06:040.010 0.0010 1
Zinc, Dissolved ND mg/L 10/05/23 11:08 7440-66-610/03/23 06:040.020 0.011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:02 7439-97-6 D310/04/23 09:500.00080 0.00056 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 12:36 7439-97-6 D310/02/23 15:100.00040 0.00028 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ12WG-091423 Lab ID: 92688280001 Collected: 09/14/23 10:05 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene 87.7 ug/L 09/21/23 17:08 83-32-909/20/23 10:0250.0 10.0 1
Acenaphthylene ND ug/L 09/21/23 17:08 208-96-809/20/23 10:0250.0 9.8 1
Acetophenone ND ug/L 09/21/23 17:08 98-86-209/20/23 10:0250.0 7.5 1
Anthracene ND ug/L 09/21/23 17:08 120-12-709/20/23 10:0250.0 11.6 1
Atrazine ND ug/L 09/21/23 17:08 1912-24-909/20/23 10:0250.0 15.9 1
Benzaldehyde ND ug/L 09/21/23 17:08 100-52-709/20/23 10:0250.0 18.0 1
Benzo(a)anthracene ND ug/L 09/21/23 17:08 56-55-309/20/23 10:0250.0 13.4 1
Benzo(a)pyrene ND ug/L 09/21/23 17:08 50-32-809/20/23 10:0250.0 13.9 1
Benzo(b)fluoranthene ND ug/L 09/21/23 17:08 205-99-209/20/23 10:0250.0 13.0 1
Benzo(g,h,i)perylene ND ug/L 09/21/23 17:08 191-24-209/20/23 10:0250.0 14.2 1
Benzo(k)fluoranthene ND ug/L 09/21/23 17:08 207-08-909/20/23 10:0250.0 13.6 1
Biphenyl (Diphenyl)22.4J ug/L 09/21/23 17:08 92-52-409/20/23 10:0250.0 9.1 1
4-Bromophenylphenyl ether ND ug/L 09/21/23 17:08 101-55-309/20/23 10:0250.0 8.8 1
Butylbenzylphthalate ND ug/L 09/21/23 17:08 85-68-709/20/23 10:0250.0 15.7 1
Caprolactam ND ug/L 09/21/23 17:08 105-60-209/20/23 10:0250.0 34.7 1
Carbazole 16.8J ug/L 09/21/23 17:08 86-74-809/20/23 10:0250.0 11.8 1
4-Chloro-3-methylphenol ND ug/L 09/21/23 17:08 59-50-709/20/23 10:0250.0 16.7 1
4-Chloroaniline ND ug/L 09/21/23 17:08 106-47-809/20/23 10:02100 18.2 1
bis(2-Chloroethoxy)methane ND ug/L 09/21/23 17:08 111-91-109/20/23 10:0250.0 9.1 1
bis(2-Chloroethyl) ether ND ug/L 09/21/23 17:08 111-44-409/20/23 10:0250.0 9.6 1
2-Chloronaphthalene ND ug/L 09/21/23 17:08 91-58-709/20/23 10:0250.0 8.6 1
2-Chlorophenol ND ug/L 09/21/23 17:08 95-57-809/20/23 10:0250.0 6.0 1
4-Chlorophenylphenyl ether ND ug/L 09/21/23 17:08 7005-72-309/20/23 10:0250.0 10.0 1
Chrysene ND ug/L 09/21/23 17:08 218-01-909/20/23 10:0250.0 13.8 1
Dibenz(a,h)anthracene ND ug/L 09/21/23 17:08 53-70-309/20/23 10:0250.0 14.8 1
Dibenzofuran 44.5J ug/L 09/21/23 17:08 132-64-909/20/23 10:0250.0 10.5 1
3,3'-Dichlorobenzidine ND ug/L 09/21/23 17:08 91-94-109/20/23 10:02100 40.6 1
2,4-Dichlorophenol ND ug/L 09/21/23 17:08 120-83-209/20/23 10:0250.0 7.0 1
Diethylphthalate ND ug/L 09/21/23 17:08 84-66-209/20/23 10:0250.0 10.2 1
2,4-Dimethylphenol ND ug/L 09/21/23 17:08 105-67-909/20/23 10:0250.0 8.5 1
Dimethylphthalate ND ug/L 09/21/23 17:08 131-11-309/20/23 10:0250.0 10.6 1
Di-n-butylphthalate ND ug/L 09/21/23 17:08 84-74-209/20/23 10:0250.0 11.0 1
4,6-Dinitro-2-methylphenol ND ug/L 09/21/23 17:08 534-52-109/20/23 10:02100 38.9 1
2,4-Dinitrophenol ND ug/L 09/21/23 17:08 51-28-509/20/23 10:02250 130 1
2,4-Dinitrotoluene ND ug/L 09/21/23 17:08 121-14-209/20/23 10:0250.0 8.1 1
2,6-Dinitrotoluene ND ug/L 09/21/23 17:08 606-20-209/20/23 10:0250.0 8.6 1
Di-n-octylphthalate ND ug/L 09/21/23 17:08 117-84-009/20/23 10:0250.0 19.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/21/23 17:08 117-81-709/20/23 10:0230.0 18.6 1
Fluoranthene ND ug/L 09/21/23 17:08 206-44-009/20/23 10:0250.0 11.0 1
Fluorene 29.8J ug/L 09/21/23 17:08 86-73-709/20/23 10:0250.0 10.4 1
Hexachloro-1,3-butadiene ND ug/L 09/21/23 17:08 87-68-309/20/23 10:0250.0 8.8 1
Hexachlorobenzene ND ug/L 09/21/23 17:08 118-74-109/20/23 10:0250.0 10.8 1
Hexachlorocyclopentadiene ND ug/L 09/21/23 17:08 77-47-409/20/23 10:0250.0 8.0 1
Hexachloroethane ND ug/L 09/21/23 17:08 67-72-109/20/23 10:0250.0 6.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/21/23 17:08 193-39-509/20/23 10:0250.0 14.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ12WG-091423 Lab ID: 92688280001 Collected: 09/14/23 10:05 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 09/21/23 17:08 78-59-109/20/23 10:0250.0 8.3 1
2-Methylnaphthalene 23.9J ug/L 09/21/23 17:08 91-57-609/20/23 10:0250.0 9.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/21/23 17:08 95-48-709/20/23 10:0250.0 9.4 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/21/23 17:08 15831-10-409/20/23 10:0250.0 6.1 1
Naphthalene 108 ug/L 09/21/23 17:08 91-20-309/20/23 10:0250.0 10.4 1
2-Nitroaniline ND ug/L 09/21/23 17:08 88-74-409/20/23 10:02100 14.9 1
3-Nitroaniline ND ug/L 09/21/23 17:08 99-09-209/20/23 10:02100 18.8 1
4-Nitroaniline ND ug/L 09/21/23 17:08 100-01-609/20/23 10:02100 25.5 1
Nitrobenzene ND ug/L 09/21/23 17:08 98-95-309/20/23 10:0250.0 9.4 1
2-Nitrophenol ND ug/L 09/21/23 17:08 88-75-509/20/23 10:0250.0 7.0 1
4-Nitrophenol ND ug/L 09/21/23 17:08 100-02-709/20/23 10:02250 33.0 1
N-Nitroso-di-n-propylamine ND ug/L 09/21/23 17:08 621-64-709/20/23 10:0250.0 6.6 1
N-Nitrosodiphenylamine ND ug/L 09/21/23 17:08 86-30-609/20/23 10:0250.0 15.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/21/23 17:08 108-60-109/20/23 10:0250.0 5.8 1
Pentachlorophenol ND ug/L 09/21/23 17:08 87-86-509/20/23 10:02100 18.8 1
Phenanthrene 34.1J ug/L 09/21/23 17:08 85-01-809/20/23 10:0250.0 10.0 1
Phenol ND ug/L 09/21/23 17:08 108-95-209/20/23 10:0250.0 6.8 1
Pyrene ND ug/L 09/21/23 17:08 129-00-009/20/23 10:0250.0 11.0 1
2,4,5-Trichlorophenol ND ug/L 09/21/23 17:08 95-95-409/20/23 10:0250.0 7.1 1
2,4,6-Trichlorophenol ND ug/L 09/21/23 17:08 88-06-209/20/23 10:0250.0 7.8 1
SurrogatesNitrobenzene-d5 (S)112 %09/21/23 17:08 4165-60-009/20/23 10:0210-138 1
2-Fluorobiphenyl (S)111 %09/21/23 17:08 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)143 %09/21/23 17:08 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)70 %09/21/23 17:08 13127-88-309/20/23 10:0210-130 1
2-Fluorophenol (S)91 %09/21/23 17:08 367-12-409/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)132 %09/21/23 17:08 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/28/23 05:20 67-64-162.5 12.8 2.5
Benzene 1.1J ug/L 09/28/23 05:20 71-43-22.5 0.86 2.5
Bromodichloromethane ND ug/L 09/28/23 05:20 75-27-42.5 0.77 2.5
Bromoform ND ug/L 09/28/23 05:20 75-25-22.5 0.85 2.5
Bromomethane ND ug/L 09/28/23 05:20 74-83-9 v25.0 4.2 2.5
2-Butanone (MEK)ND ug/L 09/28/23 05:20 78-93-312.5 9.9 2.5
Carbon disulfide ND ug/L 09/28/23 05:20 75-15-05.0 0.89 2.5
Carbon tetrachloride ND ug/L 09/28/23 05:20 56-23-52.5 0.83 2.5
Chlorobenzene 0.83J ug/L 09/28/23 05:20 108-90-72.5 0.71 2.5
Chloroethane ND ug/L 09/28/23 05:20 75-00-32.5 1.6 2.5
Chloroform ND ug/L 09/28/23 05:20 67-66-32.5 1.1 2.5
Chloromethane ND ug/L 09/28/23 05:20 74-87-32.5 1.4 2.5
Cyclohexane ND ug/L 09/28/23 05:20 110-82-72.5 0.88 2.5
1,2-Dibromo-3-chloropropane ND ug/L 09/28/23 05:20 96-12-85.0 0.85 2.5
Dibromochloromethane ND ug/L 09/28/23 05:20 124-48-12.5 0.90 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ12WG-091423 Lab ID: 92688280001 Collected: 09/14/23 10:05 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 09/28/23 05:20 106-93-42.5 0.68 2.5
1,2-Dichlorobenzene ND ug/L 09/28/23 05:20 95-50-12.5 0.85 2.5
1,3-Dichlorobenzene ND ug/L 09/28/23 05:20 541-73-12.5 0.85 2.5
1,4-Dichlorobenzene ND ug/L 09/28/23 05:20 106-46-72.5 0.83 2.5
Dichlorodifluoromethane ND ug/L 09/28/23 05:20 75-71-82.5 0.86 2.5
1,1-Dichloroethane ND ug/L 09/28/23 05:20 75-34-32.5 0.92 2.5
1,2-Dichloroethane ND ug/L 09/28/23 05:20 107-06-22.5 0.80 2.5
1,1-Dichloroethene ND ug/L 09/28/23 05:20 75-35-42.5 0.87 2.5
cis-1,2-Dichloroethene 2.4J ug/L 09/28/23 05:20 156-59-22.5 0.96 2.5
trans-1,2-Dichloroethene ND ug/L 09/28/23 05:20 156-60-52.5 0.99 2.5
1,2-Dichloropropane ND ug/L 09/28/23 05:20 78-87-52.5 0.89 2.5
cis-1,3-Dichloropropene ND ug/L 09/28/23 05:20 10061-01-52.5 0.91 2.5
trans-1,3-Dichloropropene ND ug/L 09/28/23 05:20 10061-02-62.5 0.91 2.5
Ethylbenzene 15.9 ug/L 09/28/23 05:20 100-41-42.5 0.76 2.5
2-Hexanone ND ug/L 09/28/23 05:20 591-78-612.5 1.2 2.5
Isopropylbenzene (Cumene)1.0J ug/L 09/28/23 05:20 98-82-82.5 0.83 2.5
Methyl acetate ND ug/L 09/28/23 05:20 79-20-9 v225.0 6.0 2.5
Methylcyclohexane ND ug/L 09/28/23 05:20 108-87-225.0 3.8 2.5
Methylene Chloride ND ug/L 09/28/23 05:20 75-09-212.5 4.9 2.5
4-Methyl-2-pentanone (MIBK)ND ug/L 09/28/23 05:20 108-10-112.5 6.8 2.5
Methyl-tert-butyl ether ND ug/L 09/28/23 05:20 1634-04-42.5 1.1 2.5
Styrene ND ug/L 09/28/23 05:20 100-42-52.5 0.73 2.5
1,1,2,2-Tetrachloroethane ND ug/L 09/28/23 05:20 79-34-52.5 0.56 2.5
Tetrachloroethene ND ug/L 09/28/23 05:20 127-18-42.5 0.73 2.5
Toluene ND ug/L 09/28/23 05:20 108-88-32.5 0.60 2.5
1,2,4-Trichlorobenzene ND ug/L 09/28/23 05:20 120-82-12.5 1.6 2.5
1,1,1-Trichloroethane ND ug/L 09/28/23 05:20 71-55-62.5 0.83 2.5
1,1,2-Trichloroethane ND ug/L 09/28/23 05:20 79-00-52.5 0.81 2.5
Trichloroethene ND ug/L 09/28/23 05:20 79-01-62.5 0.96 2.5
Trichlorofluoromethane ND ug/L 09/28/23 05:20 75-69-42.5 0.74 2.5
1,1,2-Trichlorotrifluoroethane ND ug/L 09/28/23 05:20 76-13-12.5 0.79 2.5
Vinyl chloride ND ug/L 09/28/23 05:20 75-01-4 v22.5 0.96 2.5
m&p-Xylene 11.9 ug/L 09/28/23 05:20 179601-23-15.0 1.8 2.5
o-Xylene 7.9 ug/L 09/28/23 05:20 95-47-62.5 0.84 2.5
Surrogates
4-Bromofluorobenzene (S)100 %09/28/23 05:20 460-00-4 D370-130 2.5
1,2-Dichloroethane-d4 (S)97 %09/28/23 05:20 17060-07-070-130 2.5
Toluene-d8 (S)100 %09/28/23 05:20 2037-26-570-130 2.5
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 3000 mg/L 09/21/23 14:145.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
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[phone]
Page 11 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ12WG-091423 Lab ID: 92688280001 Collected: 09/14/23 10:05 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 0.30 mg/L 09/20/23 02:59 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 1530 mg/L 09/20/23 21:18 16887-00-650.0 30.0 50
Sulfate 630 mg/L 09/20/23 21:18 14808-79-850.0 25.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14WG-091423 Lab ID: 92688280002 Collected: 09/14/23 11:28 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:24 7440-36-010/02/23 09:460.015 0.0055 1
Arsenic ND mg/L 10/04/23 00:24 7440-38-210/02/23 09:460.010 0.0034 1
Barium 0.11 mg/L 10/04/23 00:24 7440-39-310/02/23 09:460.010 0.00084 1
Beryllium ND mg/L 10/04/23 00:24 7440-41-710/02/23 09:460.0040 0.00017 1
Boron 0.036J mg/L 10/04/23 00:24 7440-42-810/02/23 09:460.050 0.012 1
Cadmium ND mg/L 10/04/23 00:24 7440-43-910/02/23 09:460.0010 0.00033 1
Chromium ND mg/L 10/04/23 00:24 7440-47-310/02/23 09:460.0050 0.0017 1
Cobalt ND mg/L 10/04/23 00:24 7440-48-410/02/23 09:460.010 0.00096 1
Copper ND mg/L 10/04/23 00:24 7440-50-810/02/23 09:460.0050 0.0026 1
Lead ND mg/L 10/04/23 00:24 7439-92-110/02/23 09:460.010 0.0021 1
Manganese 0.25 mg/L 10/04/23 00:24 7439-96-510/02/23 09:460.0050 0.0011 1
Nickel ND mg/L 10/04/23 00:24 7440-02-010/02/23 09:460.0050 0.0010 1
Selenium ND mg/L 10/04/23 00:24 7782-49-210/02/23 09:460.015 0.0039 1
Silver ND mg/L 10/04/23 00:24 7440-22-410/02/23 09:460.0050 0.0010 1
Thallium ND mg/L 10/04/23 00:24 7440-28-010/02/23 09:460.015 0.0029 1
Vanadium 0.0012J mg/L 10/04/23 00:24 7440-62-210/02/23 09:460.010 0.0010 1
Zinc ND mg/L 10/04/23 00:24 7440-66-610/02/23 09:460.020 0.011 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:12 7440-36-010/03/23 06:040.015 0.0055 1
Arsenic, Dissolved ND mg/L 10/05/23 11:12 7440-38-210/03/23 06:040.010 0.0034 1
Barium, Dissolved 0.10 mg/L 10/05/23 11:12 7440-39-310/03/23 06:040.010 0.00084 1
Beryllium, Dissolved ND mg/L 10/05/23 11:12 7440-41-710/03/23 06:040.0040 0.00017 1
Boron, Dissolved 0.037J mg/L 10/05/23 11:12 7440-42-810/03/23 06:040.050 0.012 1
Cadmium, Dissolved ND mg/L 10/05/23 11:12 7440-43-910/03/23 06:040.0010 0.00033 1
Chromium, Dissolved ND mg/L 10/05/23 11:12 7440-47-310/03/23 06:040.0050 0.0017 1
Cobalt, Dissolved ND mg/L 10/05/23 11:12 7440-48-410/03/23 06:040.010 0.00096 1
Copper, Dissolved ND mg/L 10/05/23 11:12 7440-50-810/03/23 06:040.0050 0.0026 1
Lead, Dissolved ND mg/L 10/05/23 11:12 7439-92-110/03/23 06:040.010 0.0021 1
Manganese, Dissolved 0.25 mg/L 10/05/23 11:12 7439-96-510/03/23 06:040.0050 0.0011 1
Nickel, Dissolved ND mg/L 10/05/23 11:12 7440-02-010/03/23 06:040.0050 0.0010 1
Selenium, Dissolved ND mg/L 10/05/23 11:12 7782-49-210/03/23 06:040.015 0.0039 1
Silver, Dissolved ND mg/L 10/05/23 11:12 7440-22-410/03/23 06:040.0050 0.0010 1
Thallium, Dissolved ND mg/L 10/05/23 11:12 7440-28-010/03/23 06:040.015 0.0029 1
Vanadium, Dissolved 0.0015J mg/L 10/05/23 11:12 7440-62-210/03/23 06:040.010 0.0010 1
Zinc, Dissolved ND mg/L 10/05/23 11:12 7440-66-610/03/23 06:040.020 0.011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:04 7439-97-610/04/23 09:500.00020 0.00014 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 12:38 7439-97-610/02/23 15:100.00020 0.00014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14WG-091423 Lab ID: 92688280002 Collected: 09/14/23 11:28 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/21/23 17:34 83-32-909/20/23 10:028.7 1.7 1
Acenaphthylene ND ug/L 09/21/23 17:34 208-96-809/20/23 10:028.7 1.7 1
Acetophenone ND ug/L 09/21/23 17:34 98-86-209/20/23 10:028.7 1.3 1
Anthracene ND ug/L 09/21/23 17:34 120-12-709/20/23 10:028.7 2.0 1
Atrazine ND ug/L 09/21/23 17:34 1912-24-909/20/23 10:028.7 2.8 1
Benzaldehyde ND ug/L 09/21/23 17:34 100-52-709/20/23 10:028.7 3.1 1
Benzo(a)anthracene ND ug/L 09/21/23 17:34 56-55-309/20/23 10:028.7 2.3 1
Benzo(a)pyrene ND ug/L 09/21/23 17:34 50-32-809/20/23 10:028.7 2.4 1
Benzo(b)fluoranthene ND ug/L 09/21/23 17:34 205-99-209/20/23 10:028.7 2.3 1
Benzo(g,h,i)perylene ND ug/L 09/21/23 17:34 191-24-209/20/23 10:028.7 2.5 1
Benzo(k)fluoranthene ND ug/L 09/21/23 17:34 207-08-909/20/23 10:028.7 2.4 1
Biphenyl (Diphenyl)ND ug/L 09/21/23 17:34 92-52-409/20/23 10:028.7 1.6 1
4-Bromophenylphenyl ether ND ug/L 09/21/23 17:34 101-55-309/20/23 10:028.7 1.5 1
Butylbenzylphthalate ND ug/L 09/21/23 17:34 85-68-709/20/23 10:028.7 2.7 1
Caprolactam ND ug/L 09/21/23 17:34 105-60-209/20/23 10:028.7 6.0 1
Carbazole ND ug/L 09/21/23 17:34 86-74-809/20/23 10:028.7 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/21/23 17:34 59-50-709/20/23 10:028.7 2.9 1
4-Chloroaniline ND ug/L 09/21/23 17:34 106-47-809/20/23 10:0217.4 3.2 1
bis(2-Chloroethoxy)methane ND ug/L 09/21/23 17:34 111-91-109/20/23 10:028.7 1.6 1
bis(2-Chloroethyl) ether ND ug/L 09/21/23 17:34 111-44-409/20/23 10:028.7 1.7 1
2-Chloronaphthalene ND ug/L 09/21/23 17:34 91-58-709/20/23 10:028.7 1.5 1
2-Chlorophenol ND ug/L 09/21/23 17:34 95-57-809/20/23 10:028.7 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/21/23 17:34 7005-72-309/20/23 10:028.7 1.7 1
Chrysene ND ug/L 09/21/23 17:34 218-01-909/20/23 10:028.7 2.4 1
Dibenz(a,h)anthracene ND ug/L 09/21/23 17:34 53-70-309/20/23 10:028.7 2.6 1
Dibenzofuran ND ug/L 09/21/23 17:34 132-64-909/20/23 10:028.7 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/21/23 17:34 91-94-109/20/23 10:0217.4 7.1 1
2,4-Dichlorophenol ND ug/L 09/21/23 17:34 120-83-209/20/23 10:028.7 1.2 1
Diethylphthalate ND ug/L 09/21/23 17:34 84-66-209/20/23 10:028.7 1.8 1
2,4-Dimethylphenol 16.9 ug/L 09/21/23 17:34 105-67-909/20/23 10:028.7 1.5 1
Dimethylphthalate ND ug/L 09/21/23 17:34 131-11-309/20/23 10:028.7 1.9 1
Di-n-butylphthalate ND ug/L 09/21/23 17:34 84-74-209/20/23 10:028.7 1.9 1
4,6-Dinitro-2-methylphenol ND ug/L 09/21/23 17:34 534-52-109/20/23 10:0217.4 6.8 1
2,4-Dinitrophenol ND ug/L 09/21/23 17:34 51-28-509/20/23 10:0243.5 22.6 1
2,4-Dinitrotoluene ND ug/L 09/21/23 17:34 121-14-209/20/23 10:028.7 1.4 1
2,6-Dinitrotoluene ND ug/L 09/21/23 17:34 606-20-209/20/23 10:028.7 1.5 1
Di-n-octylphthalate ND ug/L 09/21/23 17:34 117-84-009/20/23 10:028.7 3.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/21/23 17:34 117-81-709/20/23 10:025.2 3.2 1
Fluoranthene ND ug/L 09/21/23 17:34 206-44-009/20/23 10:028.7 1.9 1
Fluorene ND ug/L 09/21/23 17:34 86-73-709/20/23 10:028.7 1.8 1
Hexachloro-1,3-butadiene ND ug/L 09/21/23 17:34 87-68-309/20/23 10:028.7 1.5 1
Hexachlorobenzene ND ug/L 09/21/23 17:34 118-74-109/20/23 10:028.7 1.9 1
Hexachlorocyclopentadiene ND ug/L 09/21/23 17:34 77-47-409/20/23 10:028.7 1.4 1
Hexachloroethane ND ug/L 09/21/23 17:34 67-72-109/20/23 10:028.7 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/21/23 17:34 193-39-509/20/23 10:028.7 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14WG-091423 Lab ID: 92688280002 Collected: 09/14/23 11:28 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 09/21/23 17:34 78-59-109/20/23 10:028.7 1.4 1
2-Methylnaphthalene 2.3J ug/L 09/21/23 17:34 91-57-609/20/23 10:028.7 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/21/23 17:34 95-48-709/20/23 10:028.7 1.6 1
3&4-Methylphenol(m&p Cresol)13.1 ug/L 09/21/23 17:34 15831-10-409/20/23 10:028.7 1.1 1
Naphthalene 13.2 ug/L 09/21/23 17:34 91-20-309/20/23 10:028.7 1.8 1
2-Nitroaniline ND ug/L 09/21/23 17:34 88-74-409/20/23 10:0217.4 2.6 1
3-Nitroaniline ND ug/L 09/21/23 17:34 99-09-209/20/23 10:0217.4 3.3 1
4-Nitroaniline ND ug/L 09/21/23 17:34 100-01-609/20/23 10:0217.4 4.4 1
Nitrobenzene ND ug/L 09/21/23 17:34 98-95-309/20/23 10:028.7 1.6 1
2-Nitrophenol ND ug/L 09/21/23 17:34 88-75-509/20/23 10:028.7 1.2 1
4-Nitrophenol ND ug/L 09/21/23 17:34 100-02-709/20/23 10:0243.5 5.7 1
N-Nitroso-di-n-propylamine ND ug/L 09/21/23 17:34 621-64-709/20/23 10:028.7 1.2 1
N-Nitrosodiphenylamine ND ug/L 09/21/23 17:34 86-30-609/20/23 10:028.7 2.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/21/23 17:34 108-60-109/20/23 10:028.7 1.0 1
Pentachlorophenol ND ug/L 09/21/23 17:34 87-86-509/20/23 10:0217.4 3.3 1
Phenanthrene ND ug/L 09/21/23 17:34 85-01-809/20/23 10:028.7 1.7 1
Phenol ND ug/L 09/21/23 17:34 108-95-209/20/23 10:028.7 1.2 1
Pyrene ND ug/L 09/21/23 17:34 129-00-009/20/23 10:028.7 1.9 1
2,4,5-Trichlorophenol ND ug/L 09/21/23 17:34 95-95-409/20/23 10:028.7 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/21/23 17:34 88-06-209/20/23 10:028.7 1.3 1
SurrogatesNitrobenzene-d5 (S)123 %09/21/23 17:34 4165-60-009/20/23 10:0210-138 1
2-Fluorobiphenyl (S)118 %09/21/23 17:34 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)143 %09/21/23 17:34 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)43 %09/21/23 17:34 13127-88-309/20/23 10:0210-130 1
2-Fluorophenol (S)19 %09/21/23 17:34 367-12-409/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)36 %09/21/23 17:34 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 318 ug/L 09/28/23 00:50 67-64-1100 20.4 4
Benzene 106 ug/L 09/28/23 00:50 71-43-24.0 1.4 4
Bromodichloromethane ND ug/L 09/28/23 00:50 75-27-44.0 1.2 4
Bromoform ND ug/L 09/28/23 00:50 75-25-24.0 1.4 4
Bromomethane ND ug/L 09/28/23 00:50 74-83-9 v28.0 6.6 4
2-Butanone (MEK)56.0 ug/L 09/28/23 00:50 78-93-320.0 15.8 4
Carbon disulfide ND ug/L 09/28/23 00:50 75-15-08.0 1.4 4
Carbon tetrachloride ND ug/L 09/28/23 00:50 56-23-54.0 1.3 4
Chlorobenzene ND ug/L 09/28/23 00:50 108-90-74.0 1.1 4
Chloroethane ND ug/L 09/28/23 00:50 75-00-34.0 2.6 4
Chloroform ND ug/L 09/28/23 00:50 67-66-34.0 1.7 4
Chloromethane ND ug/L 09/28/23 00:50 74-87-34.0 2.2 4
Cyclohexane 189 ug/L 09/28/23 00:50 110-82-74.0 1.4 4
1,2-Dibromo-3-chloropropane ND ug/L 09/28/23 00:50 96-12-88.0 1.4 4
Dibromochloromethane ND ug/L 09/28/23 00:50 124-48-14.0 1.4 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14WG-091423 Lab ID: 92688280002 Collected: 09/14/23 11:28 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 09/28/23 00:50 106-93-44.0 1.1 4
1,2-Dichlorobenzene ND ug/L 09/28/23 00:50 95-50-14.0 1.4 4
1,3-Dichlorobenzene ND ug/L 09/28/23 00:50 541-73-14.0 1.4 4
1,4-Dichlorobenzene ND ug/L 09/28/23 00:50 106-46-74.0 1.3 4
Dichlorodifluoromethane ND ug/L 09/28/23 00:50 75-71-84.0 1.4 4
1,1-Dichloroethane ND ug/L 09/28/23 00:50 75-34-34.0 1.5 4
1,2-Dichloroethane ND ug/L 09/28/23 00:50 107-06-24.0 1.3 4
1,1-Dichloroethene ND ug/L 09/28/23 00:50 75-35-44.0 1.4 4
cis-1,2-Dichloroethene ND ug/L 09/28/23 00:50 156-59-24.0 1.5 4
trans-1,2-Dichloroethene 26.9 ug/L 09/28/23 00:50 156-60-54.0 1.6 4
1,2-Dichloropropane ND ug/L 09/28/23 00:50 78-87-54.0 1.4 4
cis-1,3-Dichloropropene ND ug/L 09/28/23 00:50 10061-01-54.0 1.5 4
trans-1,3-Dichloropropene ND ug/L 09/28/23 00:50 10061-02-64.0 1.5 4
Ethylbenzene 187 ug/L 09/28/23 00:50 100-41-44.0 1.2 4
2-Hexanone 89.2 ug/L 09/28/23 00:50 591-78-620.0 1.9 4
Isopropylbenzene (Cumene)20.7 ug/L 09/28/23 00:50 98-82-84.0 1.3 4
Methyl acetate ND ug/L 09/28/23 00:50 79-20-9 v240.0 9.6 4
Methylcyclohexane 119 ug/L 09/28/23 00:50 108-87-240.0 6.0 4
Methylene Chloride ND ug/L 09/28/23 00:50 75-09-220.0 7.8 4
4-Methyl-2-pentanone (MIBK)16.7J ug/L 09/28/23 00:50 108-10-120.0 10.8 4
Methyl-tert-butyl ether ND ug/L 09/28/23 00:50 1634-04-44.0 1.7 4
Styrene ND ug/L 09/28/23 00:50 100-42-54.0 1.2 4
1,1,2,2-Tetrachloroethane ND ug/L 09/28/23 00:50 79-34-54.0 0.90 4
Tetrachloroethene ND ug/L 09/28/23 00:50 127-18-44.0 1.2 4
Toluene 55.9 ug/L 09/28/23 00:50 108-88-34.0 0.96 4
1,2,4-Trichlorobenzene ND ug/L 09/28/23 00:50 120-82-14.0 2.6 4
1,1,1-Trichloroethane ND ug/L 09/28/23 00:50 71-55-64.0 1.3 4
1,1,2-Trichloroethane ND ug/L 09/28/23 00:50 79-00-54.0 1.3 4
Trichloroethene ND ug/L 09/28/23 00:50 79-01-64.0 1.5 4
Trichlorofluoromethane ND ug/L 09/28/23 00:50 75-69-44.0 1.2 4
1,1,2-Trichlorotrifluoroethane ND ug/L 09/28/23 00:50 76-13-14.0 1.3 4
Vinyl chloride ND ug/L 09/28/23 00:50 75-01-4 v24.0 1.5 4
m&p-Xylene 590 ug/L 09/28/23 00:50 179601-23-18.0 2.8 4
o-Xylene 120 ug/L 09/28/23 00:50 95-47-64.0 1.4 4
Surrogates
4-Bromofluorobenzene (S)98 %09/28/23 00:50 460-00-4 D370-130 4
1,2-Dichloroethane-d4 (S)99 %09/28/23 00:50 17060-07-070-130 4
Toluene-d8 (S)96 %09/28/23 00:50 2037-26-570-130 4
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 242 mg/L 09/21/23 16:445.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14WG-091423 Lab ID: 92688280002 Collected: 09/14/23 11:28 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 0.81 mg/L 09/20/23 02:59 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 29.3 mg/L 09/20/23 21:33 16887-00-61.0 0.60 1
Sulfate 14.3 mg/L 09/20/23 21:33 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14HG-091423 Lab ID: 92688280003 Collected: 09/14/23 11:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:27 7440-36-010/02/23 09:460.015 0.0055 1
Arsenic ND mg/L 10/04/23 00:27 7440-38-210/02/23 09:460.010 0.0034 1
Barium 0.11 mg/L 10/04/23 00:27 7440-39-310/02/23 09:460.010 0.00084 1
Beryllium ND mg/L 10/04/23 00:27 7440-41-710/02/23 09:460.0040 0.00017 1
Boron 0.037J mg/L 10/04/23 00:27 7440-42-810/02/23 09:460.050 0.012 1
Cadmium ND mg/L 10/04/23 00:27 7440-43-910/02/23 09:460.0010 0.00033 1
Chromium ND mg/L 10/04/23 00:27 7440-47-310/02/23 09:460.0050 0.0017 1
Cobalt ND mg/L 10/04/23 00:27 7440-48-410/02/23 09:460.010 0.00096 1
Copper ND mg/L 10/04/23 00:27 7440-50-810/02/23 09:460.0050 0.0026 1
Lead ND mg/L 10/04/23 00:27 7439-92-110/02/23 09:460.010 0.0021 1
Manganese 0.26 mg/L 10/04/23 00:27 7439-96-510/02/23 09:460.0050 0.0011 1
Nickel ND mg/L 10/04/23 00:27 7440-02-010/02/23 09:460.0050 0.0010 1
Selenium ND mg/L 10/04/23 00:27 7782-49-210/02/23 09:460.015 0.0039 1
Silver ND mg/L 10/04/23 00:27 7440-22-410/02/23 09:460.0050 0.0010 1
Thallium ND mg/L 10/04/23 00:27 7440-28-010/02/23 09:460.015 0.0029 1
Vanadium 0.0014J mg/L 10/04/23 00:27 7440-62-210/02/23 09:460.010 0.0010 1
Zinc ND mg/L 10/04/23 00:27 7440-66-610/02/23 09:460.020 0.011 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:16 7440-36-010/03/23 06:040.015 0.0055 1
Arsenic, Dissolved ND mg/L 10/05/23 11:16 7440-38-210/03/23 06:040.010 0.0034 1
Barium, Dissolved 0.10 mg/L 10/05/23 11:16 7440-39-310/03/23 06:040.010 0.00084 1
Beryllium, Dissolved ND mg/L 10/05/23 11:16 7440-41-710/03/23 06:040.0040 0.00017 1
Boron, Dissolved 0.036J mg/L 10/05/23 11:16 7440-42-810/03/23 06:040.050 0.012 1
Cadmium, Dissolved ND mg/L 10/05/23 11:16 7440-43-910/03/23 06:040.0010 0.00033 1
Chromium, Dissolved ND mg/L 10/05/23 11:16 7440-47-310/03/23 06:040.0050 0.0017 1
Cobalt, Dissolved ND mg/L 10/05/23 11:16 7440-48-410/03/23 06:040.010 0.00096 1
Copper, Dissolved ND mg/L 10/05/23 11:16 7440-50-810/03/23 06:040.0050 0.0026 1
Lead, Dissolved ND mg/L 10/05/23 11:16 7439-92-110/03/23 06:040.010 0.0021 1
Manganese, Dissolved 0.25 mg/L 10/05/23 11:16 7439-96-510/03/23 06:040.0050 0.0011 1
Nickel, Dissolved ND mg/L 10/05/23 11:16 7440-02-010/03/23 06:040.0050 0.0010 1
Selenium, Dissolved ND mg/L 10/05/23 11:16 7782-49-210/03/23 06:040.015 0.0039 1
Silver, Dissolved ND mg/L 10/05/23 11:16 7440-22-410/03/23 06:040.0050 0.0010 1
Thallium, Dissolved ND mg/L 10/05/23 11:16 7440-28-010/03/23 06:040.015 0.0029 1
Vanadium, Dissolved 0.0016J mg/L 10/05/23 11:16 7440-62-210/03/23 06:040.010 0.0010 1
Zinc, Dissolved ND mg/L 10/05/23 11:16 7440-66-610/03/23 06:040.020 0.011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:06 7439-97-610/04/23 09:500.00020 0.00014 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 12:41 7439-97-610/02/23 15:100.00020 0.00014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14HG-091423 Lab ID: 92688280003 Collected: 09/14/23 11:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/21/23 18:00 83-32-909/20/23 10:028.3 1.7 1
Acenaphthylene ND ug/L 09/21/23 18:00 208-96-809/20/23 10:028.3 1.6 1
Acetophenone ND ug/L 09/21/23 18:00 98-86-209/20/23 10:028.3 1.2 1
Anthracene ND ug/L 09/21/23 18:00 120-12-709/20/23 10:028.3 1.9 1
Atrazine ND ug/L 09/21/23 18:00 1912-24-909/20/23 10:028.3 2.6 1
Benzaldehyde ND ug/L 09/21/23 18:00 100-52-709/20/23 10:028.3 3.0 1
Benzo(a)anthracene ND ug/L 09/21/23 18:00 56-55-309/20/23 10:028.3 2.2 1
Benzo(a)pyrene ND ug/L 09/21/23 18:00 50-32-809/20/23 10:028.3 2.3 1
Benzo(b)fluoranthene ND ug/L 09/21/23 18:00 205-99-209/20/23 10:028.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 09/21/23 18:00 191-24-209/20/23 10:028.3 2.4 1
Benzo(k)fluoranthene ND ug/L 09/21/23 18:00 207-08-909/20/23 10:028.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 09/21/23 18:00 92-52-409/20/23 10:028.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 09/21/23 18:00 101-55-309/20/23 10:028.3 1.5 1
Butylbenzylphthalate ND ug/L 09/21/23 18:00 85-68-709/20/23 10:028.3 2.6 1
Caprolactam ND ug/L 09/21/23 18:00 105-60-209/20/23 10:028.3 5.8 1
Carbazole ND ug/L 09/21/23 18:00 86-74-809/20/23 10:028.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/21/23 18:00 59-50-709/20/23 10:028.3 2.8 1
4-Chloroaniline ND ug/L 09/21/23 18:00 106-47-809/20/23 10:0216.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/21/23 18:00 111-91-109/20/23 10:028.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 09/21/23 18:00 111-44-409/20/23 10:028.3 1.6 1
2-Chloronaphthalene ND ug/L 09/21/23 18:00 91-58-709/20/23 10:028.3 1.4 1
2-Chlorophenol ND ug/L 09/21/23 18:00 95-57-809/20/23 10:028.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/21/23 18:00 7005-72-309/20/23 10:028.3 1.7 1
Chrysene ND ug/L 09/21/23 18:00 218-01-909/20/23 10:028.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 09/21/23 18:00 53-70-309/20/23 10:028.3 2.5 1
Dibenzofuran ND ug/L 09/21/23 18:00 132-64-909/20/23 10:028.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/21/23 18:00 91-94-109/20/23 10:0216.7 6.8 1
2,4-Dichlorophenol ND ug/L 09/21/23 18:00 120-83-209/20/23 10:028.3 1.2 1
Diethylphthalate ND ug/L 09/21/23 18:00 84-66-209/20/23 10:028.3 1.7 1
2,4-Dimethylphenol 11.8 ug/L 09/21/23 18:00 105-67-909/20/23 10:028.3 1.4 1
Dimethylphthalate ND ug/L 09/21/23 18:00 131-11-309/20/23 10:028.3 1.8 1
Di-n-butylphthalate ND ug/L 09/21/23 18:00 84-74-209/20/23 10:028.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/21/23 18:00 534-52-109/20/23 10:0216.7 6.5 1
2,4-Dinitrophenol ND ug/L 09/21/23 18:00 51-28-509/20/23 10:0241.7 21.7 1
2,4-Dinitrotoluene ND ug/L 09/21/23 18:00 121-14-209/20/23 10:028.3 1.4 1
2,6-Dinitrotoluene ND ug/L 09/21/23 18:00 606-20-209/20/23 10:028.3 1.4 1
Di-n-octylphthalate ND ug/L 09/21/23 18:00 117-84-009/20/23 10:028.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/21/23 18:00 117-81-709/20/23 10:025.0 3.1 1
Fluoranthene ND ug/L 09/21/23 18:00 206-44-009/20/23 10:028.3 1.8 1
Fluorene ND ug/L 09/21/23 18:00 86-73-709/20/23 10:028.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 09/21/23 18:00 87-68-309/20/23 10:028.3 1.5 1
Hexachlorobenzene ND ug/L 09/21/23 18:00 118-74-109/20/23 10:028.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 09/21/23 18:00 77-47-409/20/23 10:028.3 1.3 1
Hexachloroethane ND ug/L 09/21/23 18:00 67-72-109/20/23 10:028.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/21/23 18:00 193-39-509/20/23 10:028.3 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14HG-091423 Lab ID: 92688280003 Collected: 09/14/23 11:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 09/21/23 18:00 78-59-109/20/23 10:028.3 1.4 1
2-Methylnaphthalene 3.4J ug/L 09/21/23 18:00 91-57-609/20/23 10:028.3 1.6 1
2-Methylphenol(o-Cresol)2.1J ug/L 09/21/23 18:00 95-48-709/20/23 10:028.3 1.6 1
3&4-Methylphenol(m&p Cresol)11.2 ug/L 09/21/23 18:00 15831-10-409/20/23 10:028.3 1.0 1
Naphthalene 12.5 ug/L 09/21/23 18:00 91-20-309/20/23 10:028.3 1.7 1
2-Nitroaniline ND ug/L 09/21/23 18:00 88-74-409/20/23 10:0216.7 2.5 1
3-Nitroaniline ND ug/L 09/21/23 18:00 99-09-209/20/23 10:0216.7 3.1 1
4-Nitroaniline ND ug/L 09/21/23 18:00 100-01-609/20/23 10:0216.7 4.2 1
Nitrobenzene ND ug/L 09/21/23 18:00 98-95-309/20/23 10:028.3 1.6 1
2-Nitrophenol ND ug/L 09/21/23 18:00 88-75-509/20/23 10:028.3 1.2 1
4-Nitrophenol ND ug/L 09/21/23 18:00 100-02-709/20/23 10:0241.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 09/21/23 18:00 621-64-709/20/23 10:028.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 09/21/23 18:00 86-30-609/20/23 10:028.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/21/23 18:00 108-60-109/20/23 10:028.3 0.96 1
Pentachlorophenol ND ug/L 09/21/23 18:00 87-86-509/20/23 10:0216.7 3.1 1
Phenanthrene ND ug/L 09/21/23 18:00 85-01-809/20/23 10:028.3 1.7 1
Phenol ND ug/L 09/21/23 18:00 108-95-209/20/23 10:028.3 1.1 1
Pyrene ND ug/L 09/21/23 18:00 129-00-009/20/23 10:028.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 09/21/23 18:00 95-95-409/20/23 10:028.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/21/23 18:00 88-06-209/20/23 10:028.3 1.3 1
SurrogatesNitrobenzene-d5 (S)94 %09/21/23 18:00 4165-60-009/20/23 10:0210-138 1
2-Fluorobiphenyl (S)92 %09/21/23 18:00 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)121 %09/21/23 18:00 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)50 %09/21/23 18:00 13127-88-309/20/23 10:0210-130 1
2-Fluorophenol (S)67 %09/21/23 18:00 367-12-409/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)116 %09/21/23 18:00 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 301 ug/L 09/28/23 01:08 67-64-1100 20.4 4
Benzene 106 ug/L 09/28/23 01:08 71-43-24.0 1.4 4
Bromodichloromethane ND ug/L 09/28/23 01:08 75-27-44.0 1.2 4
Bromoform ND ug/L 09/28/23 01:08 75-25-24.0 1.4 4
Bromomethane ND ug/L 09/28/23 01:08 74-83-9 v28.0 6.6 4
2-Butanone (MEK)54.7 ug/L 09/28/23 01:08 78-93-320.0 15.8 4
Carbon disulfide ND ug/L 09/28/23 01:08 75-15-08.0 1.4 4
Carbon tetrachloride ND ug/L 09/28/23 01:08 56-23-54.0 1.3 4
Chlorobenzene ND ug/L 09/28/23 01:08 108-90-74.0 1.1 4
Chloroethane ND ug/L 09/28/23 01:08 75-00-34.0 2.6 4
Chloroform ND ug/L 09/28/23 01:08 67-66-34.0 1.7 4
Chloromethane ND ug/L 09/28/23 01:08 74-87-34.0 2.2 4
Cyclohexane 190 ug/L 09/28/23 01:08 110-82-74.0 1.4 4
1,2-Dibromo-3-chloropropane ND ug/L 09/28/23 01:08 96-12-88.0 1.4 4
Dibromochloromethane ND ug/L 09/28/23 01:08 124-48-14.0 1.4 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14HG-091423 Lab ID: 92688280003 Collected: 09/14/23 11:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 09/28/23 01:08 106-93-44.0 1.1 4
1,2-Dichlorobenzene ND ug/L 09/28/23 01:08 95-50-14.0 1.4 4
1,3-Dichlorobenzene ND ug/L 09/28/23 01:08 541-73-14.0 1.4 4
1,4-Dichlorobenzene ND ug/L 09/28/23 01:08 106-46-74.0 1.3 4
Dichlorodifluoromethane ND ug/L 09/28/23 01:08 75-71-84.0 1.4 4
1,1-Dichloroethane ND ug/L 09/28/23 01:08 75-34-34.0 1.5 4
1,2-Dichloroethane ND ug/L 09/28/23 01:08 107-06-24.0 1.3 4
1,1-Dichloroethene ND ug/L 09/28/23 01:08 75-35-44.0 1.4 4
cis-1,2-Dichloroethene ND ug/L 09/28/23 01:08 156-59-24.0 1.5 4
trans-1,2-Dichloroethene 69.5 ug/L 09/28/23 01:08 156-60-54.0 1.6 4
1,2-Dichloropropane ND ug/L 09/28/23 01:08 78-87-54.0 1.4 4
cis-1,3-Dichloropropene ND ug/L 09/28/23 01:08 10061-01-54.0 1.5 4
trans-1,3-Dichloropropene ND ug/L 09/28/23 01:08 10061-02-64.0 1.5 4
Ethylbenzene 183 ug/L 09/28/23 01:08 100-41-44.0 1.2 4
2-Hexanone 87.4 ug/L 09/28/23 01:08 591-78-620.0 1.9 4
Isopropylbenzene (Cumene)20.4 ug/L 09/28/23 01:08 98-82-84.0 1.3 4
Methyl acetate ND ug/L 09/28/23 01:08 79-20-9 v240.0 9.6 4
Methylcyclohexane 125 ug/L 09/28/23 01:08 108-87-240.0 6.0 4
Methylene Chloride ND ug/L 09/28/23 01:08 75-09-220.0 7.8 4
4-Methyl-2-pentanone (MIBK)16.7J ug/L 09/28/23 01:08 108-10-120.0 10.8 4
Methyl-tert-butyl ether ND ug/L 09/28/23 01:08 1634-04-44.0 1.7 4
Styrene ND ug/L 09/28/23 01:08 100-42-54.0 1.2 4
1,1,2,2-Tetrachloroethane ND ug/L 09/28/23 01:08 79-34-54.0 0.90 4
Tetrachloroethene ND ug/L 09/28/23 01:08 127-18-44.0 1.2 4
Toluene 53.8 ug/L 09/28/23 01:08 108-88-34.0 0.96 4
1,2,4-Trichlorobenzene ND ug/L 09/28/23 01:08 120-82-14.0 2.6 4
1,1,1-Trichloroethane ND ug/L 09/28/23 01:08 71-55-64.0 1.3 4
1,1,2-Trichloroethane ND ug/L 09/28/23 01:08 79-00-54.0 1.3 4
Trichloroethene ND ug/L 09/28/23 01:08 79-01-64.0 1.5 4
Trichlorofluoromethane ND ug/L 09/28/23 01:08 75-69-44.0 1.2 4
1,1,2-Trichlorotrifluoroethane ND ug/L 09/28/23 01:08 76-13-14.0 1.3 4
Vinyl chloride ND ug/L 09/28/23 01:08 75-01-4 v24.0 1.5 4
m&p-Xylene 576 ug/L 09/28/23 01:08 179601-23-18.0 2.8 4
o-Xylene 119 ug/L 09/28/23 01:08 95-47-64.0 1.4 4
Surrogates
4-Bromofluorobenzene (S)98 %09/28/23 01:08 460-00-4 D370-130 4
1,2-Dichloroethane-d4 (S)97 %09/28/23 01:08 17060-07-070-130 4
Toluene-d8 (S)96 %09/28/23 01:08 2037-26-570-130 4
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 236 mg/L 09/21/23 16:525.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ14HG-091423 Lab ID: 92688280003 Collected: 09/14/23 11:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 0.74 mg/L 09/20/23 03:00 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 29.3 mg/L 09/20/23 21:48 16887-00-61.0 0.60 1
Sulfate 14.2 mg/L 09/20/23 21:48 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR01WG-091423 Lab ID: 92688280004 Collected: 09/14/23 12:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:31 7440-36-0 IS10/02/23 09:460.015 0.0055 1
Arsenic ND mg/L 10/04/23 00:31 7440-38-2 IS10/02/23 09:460.010 0.0034 1
Barium 0.34 mg/L 10/06/23 06:48 7440-39-310/02/23 09:460.050 0.0042 5
Beryllium ND mg/L 10/04/23 00:31 7440-41-7 IS10/02/23 09:460.0040 0.00017 1
Boron ND mg/L 10/04/23 00:31 7440-42-8 IS10/02/23 09:460.050 0.012 1
Cadmium ND mg/L 10/04/23 00:31 7440-43-9 IS10/02/23 09:460.0010 0.00033 1
Chromium 0.32 mg/L 10/06/23 06:48 7440-47-310/02/23 09:460.025 0.0085 5
Cobalt 0.019J mg/L 10/06/23 06:48 7440-48-410/02/23 09:460.050 0.0048 5
Copper 0.018J mg/L 10/06/23 06:48 7440-50-810/02/23 09:460.025 0.013 5
Lead ND mg/L 10/06/23 06:48 7439-92-1 D310/02/23 09:460.050 0.010 5
Manganese 9.8 mg/L 10/06/23 12:14 7439-96-510/02/23 09:460.10 0.022 20
Nickel 0.55 mg/L 10/06/23 06:48 7440-02-010/02/23 09:460.025 0.0050 5
Selenium ND mg/L 10/06/23 06:48 7782-49-2 D310/02/23 09:460.075 0.020 5
Silver ND mg/L 10/04/23 00:31 7440-22-4 IS10/02/23 09:460.0050 0.0010 1
Thallium ND mg/L 10/04/23 00:31 7440-28-0 IS10/02/23 09:460.015 0.0029 1
Vanadium 0.0095J mg/L 10/06/23 06:48 7440-62-210/02/23 09:460.050 0.0050 5
Zinc ND mg/L 10/06/23 06:48 7440-66-6 D310/02/23 09:460.10 0.055 5
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:20 7440-36-0 IS10/03/23 06:040.015 0.0055 1
Arsenic, Dissolved ND mg/L 10/05/23 11:20 7440-38-2 IS10/03/23 06:040.010 0.0034 1
Barium, Dissolved 0.36 mg/L 10/05/23 11:20 7440-39-310/03/23 06:040.010 0.00084 1
Beryllium, Dissolved ND mg/L 10/06/23 08:01 7440-41-7 D310/03/23 06:040.080 0.0034 20
Boron, Dissolved ND mg/L 10/05/23 11:20 7440-42-8 IS10/03/23 06:040.050 0.012 1
Cadmium, Dissolved ND mg/L 10/06/23 07:58 7440-43-9 IS10/03/23 06:040.0020 0.00066 2
Chromium, Dissolved 0.22 mg/L 10/06/23 08:01 7440-47-310/03/23 06:040.10 0.034 20
Cobalt, Dissolved 0.021J mg/L 10/06/23 08:01 7440-48-410/03/23 06:040.20 0.019 20
Copper, Dissolved ND mg/L 10/06/23 08:01 7440-50-8 D310/03/23 06:040.10 0.052 20
Lead, Dissolved ND mg/L 10/06/23 07:58 7439-92-1 IS10/03/23 06:040.020 0.0042 2
Manganese, Dissolved 11.7 mg/L 10/06/23 08:01 7439-96-510/03/23 06:040.10 0.022 20
Nickel, Dissolved 0.40 mg/L 10/06/23 08:01 7440-02-010/03/23 06:040.10 0.020 20
Selenium, Dissolved ND mg/L 10/05/23 11:20 7782-49-2 IS10/03/23 06:040.015 0.0039 1
Silver, Dissolved ND mg/L 10/06/23 07:58 7440-22-4 IS10/03/23 06:040.010 0.0020 2
Thallium, Dissolved ND mg/L 10/06/23 07:58 7440-28-0 IS10/03/23 06:040.030 0.0058 2
Vanadium, Dissolved ND mg/L 10/06/23 08:01 7440-62-2 D310/03/23 06:040.20 0.020 20
Zinc, Dissolved 0.67 mg/L 10/06/23 08:01 7440-66-610/03/23 06:040.40 0.22 20
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:09 7439-97-610/04/23 09:500.00020 0.00014 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 12:43 7439-97-610/02/23 15:100.00020 0.00014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR01WG-091423 Lab ID: 92688280004 Collected: 09/14/23 12:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/21/23 18:25 83-32-909/20/23 10:0210.0 2.0 1
Acenaphthylene ND ug/L 09/21/23 18:25 208-96-809/20/23 10:0210.0 2.0 1
Acetophenone ND ug/L 09/21/23 18:25 98-86-209/20/23 10:0210.0 1.5 1
Anthracene ND ug/L 09/21/23 18:25 120-12-709/20/23 10:0210.0 2.3 1
Atrazine ND ug/L 09/21/23 18:25 1912-24-909/20/23 10:0210.0 3.2 1
Benzaldehyde ND ug/L 09/21/23 18:25 100-52-709/20/23 10:0210.0 3.6 1
Benzo(a)anthracene ND ug/L 09/21/23 18:25 56-55-309/20/23 10:0210.0 2.7 1
Benzo(a)pyrene ND ug/L 09/21/23 18:25 50-32-809/20/23 10:0210.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/21/23 18:25 205-99-209/20/23 10:0210.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/21/23 18:25 191-24-209/20/23 10:0210.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/21/23 18:25 207-08-909/20/23 10:0210.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/21/23 18:25 92-52-409/20/23 10:0210.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/21/23 18:25 101-55-309/20/23 10:0210.0 1.8 1
Butylbenzylphthalate ND ug/L 09/21/23 18:25 85-68-709/20/23 10:0210.0 3.1 1
Caprolactam ND ug/L 09/21/23 18:25 105-60-209/20/23 10:0210.0 6.9 1
Carbazole ND ug/L 09/21/23 18:25 86-74-809/20/23 10:0210.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/21/23 18:25 59-50-709/20/23 10:0210.0 3.3 1
4-Chloroaniline ND ug/L 09/21/23 18:25 106-47-809/20/23 10:0220.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/21/23 18:25 111-91-109/20/23 10:0210.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/21/23 18:25 111-44-409/20/23 10:0210.0 1.9 1
2-Chloronaphthalene ND ug/L 09/21/23 18:25 91-58-709/20/23 10:0210.0 1.7 1
2-Chlorophenol ND ug/L 09/21/23 18:25 95-57-809/20/23 10:0210.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/21/23 18:25 7005-72-309/20/23 10:0210.0 2.0 1
Chrysene ND ug/L 09/21/23 18:25 218-01-909/20/23 10:0210.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/21/23 18:25 53-70-309/20/23 10:0210.0 3.0 1
Dibenzofuran ND ug/L 09/21/23 18:25 132-64-909/20/23 10:0210.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/21/23 18:25 91-94-109/20/23 10:0220.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/21/23 18:25 120-83-209/20/23 10:0210.0 1.4 1
Diethylphthalate ND ug/L 09/21/23 18:25 84-66-209/20/23 10:0210.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/21/23 18:25 105-67-909/20/23 10:0210.0 1.7 1
Dimethylphthalate ND ug/L 09/21/23 18:25 131-11-309/20/23 10:0210.0 2.1 1
Di-n-butylphthalate ND ug/L 09/21/23 18:25 84-74-209/20/23 10:0210.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/21/23 18:25 534-52-109/20/23 10:0220.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/21/23 18:25 51-28-509/20/23 10:0250.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/21/23 18:25 121-14-209/20/23 10:0210.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/21/23 18:25 606-20-209/20/23 10:0210.0 1.7 1
Di-n-octylphthalate ND ug/L 09/21/23 18:25 117-84-009/20/23 10:0210.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/21/23 18:25 117-81-709/20/23 10:026.0 3.7 1
Fluoranthene ND ug/L 09/21/23 18:25 206-44-009/20/23 10:0210.0 2.2 1
Fluorene ND ug/L 09/21/23 18:25 86-73-709/20/23 10:0210.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/21/23 18:25 87-68-309/20/23 10:0210.0 1.8 1
Hexachlorobenzene ND ug/L 09/21/23 18:25 118-74-109/20/23 10:0210.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/21/23 18:25 77-47-409/20/23 10:0210.0 1.6 1
Hexachloroethane ND ug/L 09/21/23 18:25 67-72-109/20/23 10:0210.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/21/23 18:25 193-39-509/20/23 10:0210.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR01WG-091423 Lab ID: 92688280004 Collected: 09/14/23 12:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 09/21/23 18:25 78-59-109/20/23 10:0210.0 1.7 1
2-Methylnaphthalene ND ug/L 09/21/23 18:25 91-57-609/20/23 10:0210.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/21/23 18:25 95-48-709/20/23 10:0210.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/21/23 18:25 15831-10-409/20/23 10:0210.0 1.2 1
Naphthalene ND ug/L 09/21/23 18:25 91-20-309/20/23 10:0210.0 2.1 1
2-Nitroaniline ND ug/L 09/21/23 18:25 88-74-409/20/23 10:0220.0 3.0 1
3-Nitroaniline ND ug/L 09/21/23 18:25 99-09-209/20/23 10:0220.0 3.8 1
4-Nitroaniline ND ug/L 09/21/23 18:25 100-01-609/20/23 10:0220.0 5.1 1
Nitrobenzene ND ug/L 09/21/23 18:25 98-95-309/20/23 10:0210.0 1.9 1
2-Nitrophenol ND ug/L 09/21/23 18:25 88-75-509/20/23 10:0210.0 1.4 1
4-Nitrophenol ND ug/L 09/21/23 18:25 100-02-709/20/23 10:0250.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/21/23 18:25 621-64-709/20/23 10:0210.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/21/23 18:25 86-30-609/20/23 10:0210.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/21/23 18:25 108-60-109/20/23 10:0210.0 1.2 1
Pentachlorophenol ND ug/L 09/21/23 18:25 87-86-509/20/23 10:0220.0 3.8 1
Phenanthrene ND ug/L 09/21/23 18:25 85-01-809/20/23 10:0210.0 2.0 1
Phenol ND ug/L 09/21/23 18:25 108-95-209/20/23 10:0210.0 1.4 1
Pyrene ND ug/L 09/21/23 18:25 129-00-009/20/23 10:0210.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/21/23 18:25 95-95-409/20/23 10:0210.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/21/23 18:25 88-06-209/20/23 10:0210.0 1.6 1
SurrogatesNitrobenzene-d5 (S)116 %09/21/23 18:25 4165-60-0 1g09/20/23 10:0210-138 1
2-Fluorobiphenyl (S)114 %09/21/23 18:25 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)142 %09/21/23 18:25 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)7 %09/21/23 18:25 13127-88-3 S009/20/23 10:0210-130 1
2-Fluorophenol (S)1 %09/21/23 18:25 367-12-4 S009/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)2 %09/21/23 18:25 118-79-6 S009/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/26/23 15:36 67-64-125.0 5.1 1
Benzene 0.47J ug/L 09/26/23 15:36 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/26/23 15:36 75-27-41.0 0.31 1
Bromoform ND ug/L 09/26/23 15:36 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/26/23 15:36 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/26/23 15:36 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/26/23 15:36 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/26/23 15:36 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/26/23 15:36 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/26/23 15:36 75-00-31.0 0.65 1
Chloroform ND ug/L 09/26/23 15:36 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/26/23 15:36 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/26/23 15:36 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/26/23 15:36 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/26/23 15:36 124-48-11.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR01WG-091423 Lab ID: 92688280004 Collected: 09/14/23 12:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 09/26/23 15:36 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/26/23 15:36 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/26/23 15:36 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/26/23 15:36 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/26/23 15:36 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/26/23 15:36 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/26/23 15:36 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/26/23 15:36 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 0.43J ug/L 09/26/23 15:36 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/26/23 15:36 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/26/23 15:36 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/26/23 15:36 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/26/23 15:36 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/26/23 15:36 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/26/23 15:36 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/26/23 15:36 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/26/23 15:36 79-20-9 v210.0 2.4 1
Methylcyclohexane ND ug/L 09/26/23 15:36 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/26/23 15:36 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/26/23 15:36 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/26/23 15:36 1634-04-41.0 0.42 1
Styrene ND ug/L 09/26/23 15:36 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/26/23 15:36 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/26/23 15:36 127-18-41.0 0.29 1
Toluene ND ug/L 09/26/23 15:36 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/26/23 15:36 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/26/23 15:36 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/26/23 15:36 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/26/23 15:36 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/26/23 15:36 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/26/23 15:36 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/26/23 15:36 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/26/23 15:36 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/26/23 15:36 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %09/26/23 15:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %09/26/23 15:36 17060-07-070-130 1
Toluene-d8 (S)95 %09/26/23 15:36 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 768 mg/L 09/21/23 17:015.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR01WG-091423 Lab ID: 92688280004 Collected: 09/14/23 12:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/20/23 03:00 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 15900 mg/L 09/21/23 10:38 16887-00-6400 240 400
Sulfate 540 mg/L 09/20/23 23:32 14808-79-8100 50.0 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ11WG-091423 Lab ID: 92688280005 Collected: 09/14/23 12:12 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:34 7440-36-0 D310/02/23 09:460.15 0.055 10
Arsenic 0.046J mg/L 10/04/23 00:34 7440-38-210/02/23 09:460.10 0.034 10
Barium 0.72 mg/L 10/04/23 00:34 7440-39-310/02/23 09:460.10 0.0084 10
Beryllium ND mg/L 10/04/23 00:34 7440-41-7 D310/02/23 09:460.040 0.0017 10
Boron 0.34J mg/L 10/04/23 00:34 7440-42-810/02/23 09:460.50 0.12 10
Cadmium ND mg/L 10/04/23 00:34 7440-43-9 D310/02/23 09:460.010 0.0033 10
Chromium 0.17 mg/L 10/04/23 00:34 7440-47-310/02/23 09:460.050 0.017 10
Cobalt ND mg/L 10/04/23 00:34 7440-48-4 D310/02/23 09:460.10 0.0096 10
Copper 0.066 mg/L 10/04/23 00:34 7440-50-810/02/23 09:460.050 0.026 10
Lead ND mg/L 10/04/23 00:34 7439-92-1 D310/02/23 09:460.10 0.021 10
Manganese 0.23 mg/L 10/04/23 00:34 7439-96-510/02/23 09:460.050 0.011 10
Nickel 0.020J mg/L 10/04/23 00:34 7440-02-010/02/23 09:460.050 0.010 10
Selenium ND mg/L 10/04/23 00:34 7782-49-2 D310/02/23 09:460.15 0.039 10
Silver ND mg/L 10/04/23 00:34 7440-22-4 D310/02/23 09:460.050 0.010 10
Thallium ND mg/L 10/04/23 00:34 7440-28-0 D310/02/23 09:460.15 0.029 10
Vanadium 0.84 mg/L 10/04/23 00:34 7440-62-210/02/23 09:460.10 0.010 10
Zinc ND mg/L 10/04/23 00:34 7440-66-6 D310/02/23 09:460.20 0.11 10
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:31 7440-36-010/03/23 06:040.075 0.028 5
Arsenic, Dissolved 0.060 mg/L 10/05/23 11:31 7440-38-210/03/23 06:040.050 0.017 5
Barium, Dissolved 0.58 mg/L 10/05/23 11:31 7440-39-310/03/23 06:040.050 0.0042 5
Beryllium, Dissolved ND mg/L 10/05/23 11:31 7440-41-710/03/23 06:040.020 0.00085 5
Boron, Dissolved 0.32 mg/L 10/05/23 11:31 7440-42-810/03/23 06:040.25 0.062 5
Cadmium, Dissolved ND mg/L 10/05/23 11:31 7440-43-910/03/23 06:040.0050 0.0016 5
Chromium, Dissolved 0.15 mg/L 10/05/23 11:31 7440-47-310/03/23 06:040.025 0.0085 5
Cobalt, Dissolved 0.0052J mg/L 10/05/23 11:31 7440-48-410/03/23 06:040.050 0.0048 5
Copper, Dissolved 0.044 mg/L 10/05/23 11:31 7440-50-810/03/23 06:040.025 0.013 5
Lead, Dissolved ND mg/L 10/05/23 11:31 7439-92-110/03/23 06:040.050 0.010 5
Manganese, Dissolved 0.18 mg/L 10/05/23 11:31 7439-96-510/03/23 06:040.025 0.0055 5
Nickel, Dissolved 0.016J mg/L 10/05/23 11:31 7440-02-010/03/23 06:040.025 0.0050 5
Selenium, Dissolved ND mg/L 10/05/23 11:31 7782-49-210/03/23 06:040.075 0.020 5
Silver, Dissolved ND mg/L 10/05/23 11:31 7440-22-410/03/23 06:040.025 0.0050 5
Thallium, Dissolved ND mg/L 10/05/23 11:31 7440-28-010/03/23 06:040.075 0.014 5
Vanadium, Dissolved 0.73 mg/L 10/05/23 11:31 7440-62-210/03/23 06:040.050 0.0050 5
Zinc, Dissolved ND mg/L 10/05/23 11:31 7440-66-610/03/23 06:040.10 0.055 5
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:11 7439-97-6 D310/04/23 09:500.00040 0.00028 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved 0.00018J mg/L 10/03/23 12:45 7439-97-610/02/23 15:100.00020 0.00014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ11WG-091423 Lab ID: 92688280005 Collected: 09/14/23 12:12 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/21/23 18:51 83-32-909/20/23 10:0250.0 10.0 1
Acenaphthylene ND ug/L 09/21/23 18:51 208-96-809/20/23 10:0250.0 9.8 1
Acetophenone ND ug/L 09/21/23 18:51 98-86-209/20/23 10:0250.0 7.5 1
Anthracene ND ug/L 09/21/23 18:51 120-12-709/20/23 10:0250.0 11.6 1
Atrazine ND ug/L 09/21/23 18:51 1912-24-909/20/23 10:0250.0 15.9 1
Benzaldehyde ND ug/L 09/21/23 18:51 100-52-709/20/23 10:0250.0 18.0 1
Benzo(a)anthracene ND ug/L 09/21/23 18:51 56-55-309/20/23 10:0250.0 13.4 1
Benzo(a)pyrene ND ug/L 09/21/23 18:51 50-32-809/20/23 10:0250.0 13.9 1
Benzo(b)fluoranthene ND ug/L 09/21/23 18:51 205-99-209/20/23 10:0250.0 13.0 1
Benzo(g,h,i)perylene ND ug/L 09/21/23 18:51 191-24-209/20/23 10:0250.0 14.2 1
Benzo(k)fluoranthene ND ug/L 09/21/23 18:51 207-08-909/20/23 10:0250.0 13.6 1
Biphenyl (Diphenyl)ND ug/L 09/21/23 18:51 92-52-409/20/23 10:0250.0 9.1 1
4-Bromophenylphenyl ether ND ug/L 09/21/23 18:51 101-55-309/20/23 10:0250.0 8.8 1
Butylbenzylphthalate ND ug/L 09/21/23 18:51 85-68-709/20/23 10:0250.0 15.7 1
Caprolactam ND ug/L 09/21/23 18:51 105-60-209/20/23 10:0250.0 34.7 1
Carbazole ND ug/L 09/21/23 18:51 86-74-809/20/23 10:0250.0 11.8 1
4-Chloro-3-methylphenol ND ug/L 09/21/23 18:51 59-50-709/20/23 10:0250.0 16.7 1
4-Chloroaniline ND ug/L 09/21/23 18:51 106-47-809/20/23 10:02100 18.2 1
bis(2-Chloroethoxy)methane ND ug/L 09/21/23 18:51 111-91-109/20/23 10:0250.0 9.1 1
bis(2-Chloroethyl) ether ND ug/L 09/21/23 18:51 111-44-409/20/23 10:0250.0 9.6 1
2-Chloronaphthalene ND ug/L 09/21/23 18:51 91-58-709/20/23 10:0250.0 8.6 1
2-Chlorophenol ND ug/L 09/21/23 18:51 95-57-809/20/23 10:0250.0 6.0 1
4-Chlorophenylphenyl ether ND ug/L 09/21/23 18:51 7005-72-309/20/23 10:0250.0 10.0 1
Chrysene ND ug/L 09/21/23 18:51 218-01-909/20/23 10:0250.0 13.8 1
Dibenz(a,h)anthracene ND ug/L 09/21/23 18:51 53-70-309/20/23 10:0250.0 14.8 1
Dibenzofuran ND ug/L 09/21/23 18:51 132-64-909/20/23 10:0250.0 10.5 1
3,3'-Dichlorobenzidine ND ug/L 09/21/23 18:51 91-94-109/20/23 10:02100 40.6 1
2,4-Dichlorophenol ND ug/L 09/21/23 18:51 120-83-209/20/23 10:0250.0 7.0 1
Diethylphthalate ND ug/L 09/21/23 18:51 84-66-209/20/23 10:0250.0 10.2 1
2,4-Dimethylphenol ND ug/L 09/21/23 18:51 105-67-909/20/23 10:0250.0 8.5 1
Dimethylphthalate ND ug/L 09/21/23 18:51 131-11-309/20/23 10:0250.0 10.6 1
Di-n-butylphthalate ND ug/L 09/21/23 18:51 84-74-209/20/23 10:0250.0 11.0 1
4,6-Dinitro-2-methylphenol ND ug/L 09/21/23 18:51 534-52-109/20/23 10:02100 38.9 1
2,4-Dinitrophenol ND ug/L 09/21/23 18:51 51-28-509/20/23 10:02250 130 1
2,4-Dinitrotoluene ND ug/L 09/21/23 18:51 121-14-209/20/23 10:0250.0 8.1 1
2,6-Dinitrotoluene ND ug/L 09/21/23 18:51 606-20-209/20/23 10:0250.0 8.6 1
Di-n-octylphthalate ND ug/L 09/21/23 18:51 117-84-009/20/23 10:0250.0 19.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/21/23 18:51 117-81-709/20/23 10:0230.0 18.6 1
Fluoranthene ND ug/L 09/21/23 18:51 206-44-009/20/23 10:0250.0 11.0 1
Fluorene ND ug/L 09/21/23 18:51 86-73-709/20/23 10:0250.0 10.4 1
Hexachloro-1,3-butadiene ND ug/L 09/21/23 18:51 87-68-309/20/23 10:0250.0 8.8 1
Hexachlorobenzene ND ug/L 09/21/23 18:51 118-74-109/20/23 10:0250.0 10.8 1
Hexachlorocyclopentadiene ND ug/L 09/21/23 18:51 77-47-409/20/23 10:0250.0 8.0 1
Hexachloroethane ND ug/L 09/21/23 18:51 67-72-109/20/23 10:0250.0 6.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/21/23 18:51 193-39-509/20/23 10:0250.0 14.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ11WG-091423 Lab ID: 92688280005 Collected: 09/14/23 12:12 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 09/21/23 18:51 78-59-109/20/23 10:0250.0 8.3 1
2-Methylnaphthalene ND ug/L 09/21/23 18:51 91-57-609/20/23 10:0250.0 9.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/21/23 18:51 95-48-709/20/23 10:0250.0 9.4 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/21/23 18:51 15831-10-409/20/23 10:0250.0 6.1 1
Naphthalene ND ug/L 09/21/23 18:51 91-20-309/20/23 10:0250.0 10.4 1
2-Nitroaniline ND ug/L 09/21/23 18:51 88-74-409/20/23 10:02100 14.9 1
3-Nitroaniline ND ug/L 09/21/23 18:51 99-09-209/20/23 10:02100 18.8 1
4-Nitroaniline ND ug/L 09/21/23 18:51 100-01-609/20/23 10:02100 25.5 1
Nitrobenzene ND ug/L 09/21/23 18:51 98-95-309/20/23 10:0250.0 9.4 1
2-Nitrophenol ND ug/L 09/21/23 18:51 88-75-509/20/23 10:0250.0 7.0 1
4-Nitrophenol ND ug/L 09/21/23 18:51 100-02-709/20/23 10:02250 33.0 1
N-Nitroso-di-n-propylamine ND ug/L 09/21/23 18:51 621-64-709/20/23 10:0250.0 6.6 1
N-Nitrosodiphenylamine ND ug/L 09/21/23 18:51 86-30-609/20/23 10:0250.0 15.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/21/23 18:51 108-60-109/20/23 10:0250.0 5.8 1
Pentachlorophenol ND ug/L 09/21/23 18:51 87-86-509/20/23 10:02100 18.8 1
Phenanthrene ND ug/L 09/21/23 18:51 85-01-809/20/23 10:0250.0 10.0 1
Phenol ND ug/L 09/21/23 18:51 108-95-209/20/23 10:0250.0 6.8 1
Pyrene ND ug/L 09/21/23 18:51 129-00-009/20/23 10:0250.0 11.0 1
2,4,5-Trichlorophenol ND ug/L 09/21/23 18:51 95-95-409/20/23 10:0250.0 7.1 1
2,4,6-Trichlorophenol ND ug/L 09/21/23 18:51 88-06-209/20/23 10:0250.0 7.8 1
SurrogatesNitrobenzene-d5 (S)73 %09/21/23 18:51 4165-60-009/20/23 10:0210-138 1
2-Fluorobiphenyl (S)68 %09/21/23 18:51 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)84 %09/21/23 18:51 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)30 %09/21/23 18:51 13127-88-309/20/23 10:0210-130 1
2-Fluorophenol (S)39 %09/21/23 18:51 367-12-409/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)61 %09/21/23 18:51 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/22/23 17:51 67-64-125.0 5.1 1
Benzene ND ug/L 09/22/23 17:51 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/22/23 17:51 75-27-41.0 0.31 1
Bromoform ND ug/L 09/22/23 17:51 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/22/23 17:51 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/22/23 17:51 78-93-35.0 4.0 1
Carbon disulfide 1.6J ug/L 09/22/23 17:51 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/22/23 17:51 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/22/23 17:51 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/22/23 17:51 75-00-31.0 0.65 1
Chloroform ND ug/L 09/22/23 17:51 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/22/23 17:51 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/22/23 17:51 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/22/23 17:51 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/22/23 17:51 124-48-11.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ11WG-091423 Lab ID: 92688280005 Collected: 09/14/23 12:12 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 09/22/23 17:51 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/22/23 17:51 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/22/23 17:51 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/22/23 17:51 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/22/23 17:51 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/22/23 17:51 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/22/23 17:51 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/22/23 17:51 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/22/23 17:51 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/22/23 17:51 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/22/23 17:51 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/22/23 17:51 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/22/23 17:51 10061-02-61.0 0.36 1
Ethylbenzene 0.37J ug/L 09/22/23 17:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/22/23 17:51 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/22/23 17:51 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/22/23 17:51 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/22/23 17:51 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/22/23 17:51 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/22/23 17:51 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/22/23 17:51 1634-04-41.0 0.42 1
Styrene ND ug/L 09/22/23 17:51 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/22/23 17:51 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/22/23 17:51 127-18-41.0 0.29 1
Toluene 0.52J ug/L 09/22/23 17:51 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/22/23 17:51 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/22/23 17:51 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/22/23 17:51 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/22/23 17:51 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/22/23 17:51 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/22/23 17:51 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/22/23 17:51 75-01-41.0 0.39 1
m&p-Xylene 2.0J ug/L 09/22/23 17:51 179601-23-12.0 0.71 1
o-Xylene 1.0 ug/L 09/22/23 17:51 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %09/22/23 17:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %09/22/23 17:51 17060-07-070-130 1
Toluene-d8 (S)99 %09/22/23 17:51 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 1460 mg/L 09/21/23 15:105.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ11WG-091423 Lab ID: 92688280005 Collected: 09/14/23 12:12 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 0.31 mg/L 09/20/23 03:01 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 201 mg/L 09/21/23 10:53 16887-00-610.0 6.0 10
Sulfate 9.5J mg/L 09/21/23 10:53 14808-79-8 D310.0 5.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ06WG-091423 Lab ID: 92688280006 Collected: 09/14/23 15:40 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:44 7440-36-010/02/23 09:460.015 0.0055 1
Arsenic ND mg/L 10/04/23 00:44 7440-38-210/02/23 09:460.010 0.0034 1
Barium 0.12 mg/L 10/04/23 00:44 7440-39-310/02/23 09:460.010 0.00084 1
Beryllium ND mg/L 10/04/23 00:44 7440-41-710/02/23 09:460.0040 0.00017 1
Boron 0.055 mg/L 10/04/23 00:44 7440-42-810/02/23 09:460.050 0.012 1
Cadmium ND mg/L 10/04/23 00:44 7440-43-910/02/23 09:460.0010 0.00033 1
Chromium 0.0027J mg/L 10/04/23 00:44 7440-47-310/02/23 09:460.0050 0.0017 1
Cobalt 0.0019J mg/L 10/04/23 00:44 7440-48-410/02/23 09:460.010 0.00096 1
Copper ND mg/L 10/04/23 00:44 7440-50-810/02/23 09:460.0050 0.0026 1
Lead ND mg/L 10/04/23 00:44 7439-92-110/02/23 09:460.010 0.0021 1
Manganese 3.2 mg/L 10/05/23 18:05 7439-96-510/02/23 09:460.050 0.011 10
Nickel ND mg/L 10/04/23 00:44 7440-02-010/02/23 09:460.0050 0.0010 1
Selenium ND mg/L 10/04/23 00:44 7782-49-210/02/23 09:460.015 0.0039 1
Silver ND mg/L 10/04/23 00:44 7440-22-410/02/23 09:460.0050 0.0010 1
Thallium ND mg/L 10/04/23 00:44 7440-28-010/02/23 09:460.015 0.0029 1
Vanadium 0.0043J mg/L 10/04/23 00:44 7440-62-210/02/23 09:460.010 0.0010 1
Zinc ND mg/L 10/04/23 00:44 7440-66-610/02/23 09:460.020 0.011 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:35 7440-36-010/03/23 06:040.015 0.0055 1
Arsenic, Dissolved ND mg/L 10/05/23 11:35 7440-38-210/03/23 06:040.010 0.0034 1
Barium, Dissolved 0.10 mg/L 10/05/23 11:35 7440-39-310/03/23 06:040.010 0.00084 1
Beryllium, Dissolved ND mg/L 10/05/23 11:35 7440-41-710/03/23 06:040.0040 0.00017 1
Boron, Dissolved 0.057 mg/L 10/05/23 11:35 7440-42-810/03/23 06:040.050 0.012 1
Cadmium, Dissolved 0.00040J mg/L 10/05/23 11:35 7440-43-910/03/23 06:040.0010 0.00033 1
Chromium, Dissolved ND mg/L 10/05/23 11:35 7440-47-310/03/23 06:040.0050 0.0017 1
Cobalt, Dissolved 0.0018J mg/L 10/05/23 11:35 7440-48-410/03/23 06:040.010 0.00096 1
Copper, Dissolved ND mg/L 10/05/23 11:35 7440-50-810/03/23 06:040.0050 0.0026 1
Lead, Dissolved ND mg/L 10/05/23 11:35 7439-92-110/03/23 06:040.010 0.0021 1
Manganese, Dissolved 2.8 mg/L 10/06/23 08:05 7439-96-510/03/23 06:040.025 0.0055 5
Nickel, Dissolved ND mg/L 10/05/23 11:35 7440-02-010/03/23 06:040.0050 0.0010 1
Selenium, Dissolved ND mg/L 10/05/23 11:35 7782-49-210/03/23 06:040.015 0.0039 1
Silver, Dissolved ND mg/L 10/05/23 11:35 7440-22-410/03/23 06:040.0050 0.0010 1
Thallium, Dissolved ND mg/L 10/05/23 11:35 7440-28-010/03/23 06:040.015 0.0029 1
Vanadium, Dissolved 0.0012J mg/L 10/05/23 11:35 7440-62-210/03/23 06:040.010 0.0010 1
Zinc, Dissolved ND mg/L 10/05/23 11:35 7440-66-610/03/23 06:040.020 0.011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:13 7439-97-610/04/23 09:500.00020 0.00014 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 12:48 7439-97-610/02/23 15:100.00020 0.00014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ06WG-091423 Lab ID: 92688280006 Collected: 09/14/23 15:40 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/22/23 11:12 83-32-909/20/23 10:0210.0 2.0 1
Acenaphthylene ND ug/L 09/22/23 11:12 208-96-809/20/23 10:0210.0 2.0 1
Acetophenone ND ug/L 09/22/23 11:12 98-86-209/20/23 10:0210.0 1.5 1
Anthracene ND ug/L 09/22/23 11:12 120-12-709/20/23 10:0210.0 2.3 1
Atrazine ND ug/L 09/22/23 11:12 1912-24-909/20/23 10:0210.0 3.2 1
Benzaldehyde ND ug/L 09/22/23 11:12 100-52-709/20/23 10:0210.0 3.6 1
Benzo(a)anthracene ND ug/L 09/22/23 11:12 56-55-309/20/23 10:0210.0 2.7 1
Benzo(a)pyrene ND ug/L 09/22/23 11:12 50-32-809/20/23 10:0210.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/22/23 11:12 205-99-209/20/23 10:0210.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/22/23 11:12 191-24-209/20/23 10:0210.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/22/23 11:12 207-08-909/20/23 10:0210.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/22/23 11:12 92-52-409/20/23 10:0210.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/22/23 11:12 101-55-309/20/23 10:0210.0 1.8 1
Butylbenzylphthalate ND ug/L 09/22/23 11:12 85-68-709/20/23 10:0210.0 3.1 1
Caprolactam ND ug/L 09/22/23 11:12 105-60-209/20/23 10:0210.0 6.9 1
Carbazole ND ug/L 09/22/23 11:12 86-74-809/20/23 10:0210.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/22/23 11:12 59-50-709/20/23 10:0210.0 3.3 1
4-Chloroaniline ND ug/L 09/22/23 11:12 106-47-809/20/23 10:0220.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/22/23 11:12 111-91-109/20/23 10:0210.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/22/23 11:12 111-44-409/20/23 10:0210.0 1.9 1
2-Chloronaphthalene ND ug/L 09/22/23 11:12 91-58-709/20/23 10:0210.0 1.7 1
2-Chlorophenol ND ug/L 09/22/23 11:12 95-57-809/20/23 10:0210.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/22/23 11:12 7005-72-309/20/23 10:0210.0 2.0 1
Chrysene ND ug/L 09/22/23 11:12 218-01-909/20/23 10:0210.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/22/23 11:12 53-70-309/20/23 10:0210.0 3.0 1
Dibenzofuran ND ug/L 09/22/23 11:12 132-64-909/20/23 10:0210.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/22/23 11:12 91-94-109/20/23 10:0220.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/22/23 11:12 120-83-209/20/23 10:0210.0 1.4 1
Diethylphthalate ND ug/L 09/22/23 11:12 84-66-209/20/23 10:0210.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/22/23 11:12 105-67-909/20/23 10:0210.0 1.7 1
Dimethylphthalate ND ug/L 09/22/23 11:12 131-11-309/20/23 10:0210.0 2.1 1
Di-n-butylphthalate ND ug/L 09/22/23 11:12 84-74-209/20/23 10:0210.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/22/23 11:12 534-52-109/20/23 10:0220.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/22/23 11:12 51-28-509/20/23 10:0250.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/22/23 11:12 121-14-209/20/23 10:0210.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/22/23 11:12 606-20-209/20/23 10:0210.0 1.7 1
Di-n-octylphthalate ND ug/L 09/22/23 11:12 117-84-009/20/23 10:0210.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/22/23 11:12 117-81-709/20/23 10:026.0 3.7 1
Fluoranthene ND ug/L 09/22/23 11:12 206-44-009/20/23 10:0210.0 2.2 1
Fluorene ND ug/L 09/22/23 11:12 86-73-709/20/23 10:0210.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/22/23 11:12 87-68-309/20/23 10:0210.0 1.8 1
Hexachlorobenzene ND ug/L 09/22/23 11:12 118-74-109/20/23 10:0210.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/22/23 11:12 77-47-409/20/23 10:0210.0 1.6 1
Hexachloroethane ND ug/L 09/22/23 11:12 67-72-109/20/23 10:0210.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/22/23 11:12 193-39-509/20/23 10:0210.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ06WG-091423 Lab ID: 92688280006 Collected: 09/14/23 15:40 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 09/22/23 11:12 78-59-109/20/23 10:0210.0 1.7 1
2-Methylnaphthalene ND ug/L 09/22/23 11:12 91-57-609/20/23 10:0210.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/22/23 11:12 95-48-709/20/23 10:0210.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/22/23 11:12 15831-10-409/20/23 10:0210.0 1.2 1
Naphthalene ND ug/L 09/22/23 11:12 91-20-309/20/23 10:0210.0 2.1 1
2-Nitroaniline ND ug/L 09/22/23 11:12 88-74-409/20/23 10:0220.0 3.0 1
3-Nitroaniline ND ug/L 09/22/23 11:12 99-09-209/20/23 10:0220.0 3.8 1
4-Nitroaniline ND ug/L 09/22/23 11:12 100-01-609/20/23 10:0220.0 5.1 1
Nitrobenzene ND ug/L 09/22/23 11:12 98-95-309/20/23 10:0210.0 1.9 1
2-Nitrophenol ND ug/L 09/22/23 11:12 88-75-509/20/23 10:0210.0 1.4 1
4-Nitrophenol ND ug/L 09/22/23 11:12 100-02-709/20/23 10:0250.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/22/23 11:12 621-64-709/20/23 10:0210.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/22/23 11:12 86-30-609/20/23 10:0210.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/22/23 11:12 108-60-109/20/23 10:0210.0 1.2 1
Pentachlorophenol ND ug/L 09/22/23 11:12 87-86-509/20/23 10:0220.0 3.8 1
Phenanthrene ND ug/L 09/22/23 11:12 85-01-809/20/23 10:0210.0 2.0 1
Phenol ND ug/L 09/22/23 11:12 108-95-209/20/23 10:0210.0 1.4 1
Pyrene ND ug/L 09/22/23 11:12 129-00-009/20/23 10:0210.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/22/23 11:12 95-95-409/20/23 10:0210.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/22/23 11:12 88-06-209/20/23 10:0210.0 1.6 1
SurrogatesNitrobenzene-d5 (S)120 %09/22/23 11:12 4165-60-009/20/23 10:0210-138 1
2-Fluorobiphenyl (S)112 %09/22/23 11:12 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)149 %09/22/23 11:12 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)34 %09/22/23 11:12 13127-88-309/20/23 10:0210-130 1
2-Fluorophenol (S)10 %09/22/23 11:12 367-12-409/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)22 %09/22/23 11:12 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/22/23 18:10 67-64-125.0 5.1 1
Benzene ND ug/L 09/22/23 18:10 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/22/23 18:10 75-27-41.0 0.31 1
Bromoform ND ug/L 09/22/23 18:10 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/22/23 18:10 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/22/23 18:10 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/22/23 18:10 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/22/23 18:10 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/22/23 18:10 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/22/23 18:10 75-00-31.0 0.65 1
Chloroform ND ug/L 09/22/23 18:10 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/22/23 18:10 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/22/23 18:10 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/22/23 18:10 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/22/23 18:10 124-48-11.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ06WG-091423 Lab ID: 92688280006 Collected: 09/14/23 15:40 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 09/22/23 18:10 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/22/23 18:10 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/22/23 18:10 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/22/23 18:10 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/22/23 18:10 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/22/23 18:10 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/22/23 18:10 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/22/23 18:10 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 0.71J ug/L 09/22/23 18:10 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/22/23 18:10 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/22/23 18:10 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/22/23 18:10 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/22/23 18:10 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/22/23 18:10 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/22/23 18:10 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/22/23 18:10 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/22/23 18:10 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/22/23 18:10 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/22/23 18:10 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/22/23 18:10 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/22/23 18:10 1634-04-41.0 0.42 1
Styrene ND ug/L 09/22/23 18:10 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/22/23 18:10 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/22/23 18:10 127-18-41.0 0.29 1
Toluene ND ug/L 09/22/23 18:10 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/22/23 18:10 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/22/23 18:10 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/22/23 18:10 79-00-51.0 0.32 1
Trichloroethene 6.8 ug/L 09/22/23 18:10 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/22/23 18:10 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/22/23 18:10 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/22/23 18:10 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/22/23 18:10 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/22/23 18:10 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %09/22/23 18:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %09/22/23 18:10 17060-07-070-130 1
Toluene-d8 (S)98 %09/22/23 18:10 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 104 mg/L 09/21/23 15:265.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ06WG-091423 Lab ID: 92688280006 Collected: 09/14/23 15:40 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 0.032J mg/L 09/20/23 03:02 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 150 mg/L 09/21/23 08:39 16887-00-63.0 1.8 3
Sulfate 19.8 mg/L 09/21/23 01:24 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ02WG-091423 Lab ID: 92688280007 Collected: 09/14/23 14:58 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
HEM, Oil and Grease
Oil and Grease 4.7J mg/L 10/06/23 11:305.0 1.1 1
Analytical Method: EPA 8015C Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8015 Diesel Low Volume
Diesel Range Organics(C10-C28)ND mg/L 09/22/23 17:20 M109/21/23 15:555.1 1.6 1
Surrogatesn-Pentacosane (S)39 %09/22/23 17:20 629-99-209/21/23 15:5529-158 1
Analytical Method: EPA 5030B/8015C
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)0.39 mg/L 09/24/23 02:060.080 0.034 1
Surrogates
4-Bromofluorobenzene (S)89 %09/24/23 02:06 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:48 7440-36-0 D310/02/23 09:460.075 0.028 5
Arsenic 0.025J mg/L 10/04/23 00:48 7440-38-210/02/23 09:460.050 0.017 5
Barium 0.14 mg/L 10/04/23 00:48 7440-39-310/02/23 09:460.050 0.0042 5
Beryllium 0.0031J mg/L 10/04/23 00:48 7440-41-710/02/23 09:460.020 0.00085 5
Boron 0.14J mg/L 10/04/23 00:48 7440-42-810/02/23 09:460.25 0.062 5
Cadmium ND mg/L 10/04/23 00:48 7440-43-9 D310/02/23 09:460.0050 0.0016 5
Chromium 0.040 mg/L 10/04/23 00:48 7440-47-310/02/23 09:460.025 0.0085 5
Cobalt 0.0086J mg/L 10/04/23 00:48 7440-48-410/02/23 09:460.050 0.0048 5
Copper ND mg/L 10/04/23 00:48 7440-50-8 D310/02/23 09:460.025 0.013 5
Lead ND mg/L 10/04/23 00:48 7439-92-1 D310/02/23 09:460.050 0.010 5
Manganese 0.13 mg/L 10/04/23 00:48 7439-96-510/02/23 09:460.025 0.0055 5
Nickel 0.19 mg/L 10/04/23 00:48 7440-02-010/02/23 09:460.025 0.0050 5
Selenium ND mg/L 10/04/23 00:48 7782-49-2 D310/02/23 09:460.075 0.020 5
Silver ND mg/L 10/04/23 00:48 7440-22-4 D310/02/23 09:460.025 0.0050 5
Thallium ND mg/L 10/04/23 00:48 7440-28-0 D310/02/23 09:460.075 0.014 5
Vanadium 0.55 mg/L 10/04/23 00:48 7440-62-210/02/23 09:460.050 0.0050 5
Zinc ND mg/L 10/04/23 00:48 7440-66-6 D310/02/23 09:460.10 0.055 5
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:39 7440-36-010/03/23 06:040.015 0.0055 1
Arsenic, Dissolved 0.016 mg/L 10/05/23 11:39 7440-38-210/03/23 06:040.010 0.0034 1
Barium, Dissolved 0.11 mg/L 10/05/23 11:39 7440-39-310/03/23 06:040.010 0.00084 1
Beryllium, Dissolved 0.0018J mg/L 10/05/23 11:39 7440-41-710/03/23 06:040.0040 0.00017 1
Boron, Dissolved 0.095 mg/L 10/05/23 11:39 7440-42-810/03/23 06:040.050 0.012 1
Cadmium, Dissolved ND mg/L 10/05/23 11:39 7440-43-910/03/23 06:040.0010 0.00033 1
Chromium, Dissolved 0.029 mg/L 10/05/23 11:39 7440-47-310/03/23 06:040.0050 0.0017 1
Cobalt, Dissolved 0.0060J mg/L 10/05/23 11:39 7440-48-410/03/23 06:040.010 0.00096 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ02WG-091423 Lab ID: 92688280007 Collected: 09/14/23 14:58 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Copper, Dissolved ND mg/L 10/05/23 11:39 7440-50-810/03/23 06:040.0050 0.0026 1
Lead, Dissolved 0.0067J mg/L 10/05/23 11:39 7439-92-110/03/23 06:040.010 0.0021 1
Manganese, Dissolved 0.089 mg/L 10/05/23 11:39 7439-96-510/03/23 06:040.0050 0.0011 1
Nickel, Dissolved 0.14 mg/L 10/05/23 11:39 7440-02-010/03/23 06:040.0050 0.0010 1
Selenium, Dissolved ND mg/L 10/05/23 11:39 7782-49-210/03/23 06:040.015 0.0039 1
Silver, Dissolved ND mg/L 10/05/23 11:39 7440-22-410/03/23 06:040.0050 0.0010 1
Thallium, Dissolved ND mg/L 10/05/23 11:39 7440-28-010/03/23 06:040.015 0.0029 1
Vanadium, Dissolved 0.40 mg/L 10/05/23 11:39 7440-62-210/03/23 06:040.010 0.0010 1
Zinc, Dissolved 0.013J mg/L 10/05/23 11:39 7440-66-610/03/23 06:040.020 0.011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:20 7439-97-6 D310/04/23 09:500.0016 0.0011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 12:50 7439-97-6 D310/02/23 15:100.00080 0.00056 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/22/23 11:38 83-32-909/20/23 10:0250.0 10.0 1
Acenaphthylene ND ug/L 09/22/23 11:38 208-96-809/20/23 10:0250.0 9.8 1
Acetophenone ND ug/L 09/22/23 11:38 98-86-209/20/23 10:0250.0 7.5 1
Anthracene ND ug/L 09/22/23 11:38 120-12-709/20/23 10:0250.0 11.6 1
Atrazine ND ug/L 09/22/23 11:38 1912-24-909/20/23 10:0250.0 15.9 1
Benzaldehyde ND ug/L 09/22/23 11:38 100-52-709/20/23 10:0250.0 18.0 1
Benzo(a)anthracene ND ug/L 09/22/23 11:38 56-55-309/20/23 10:0250.0 13.4 1
Benzo(a)pyrene ND ug/L 09/22/23 11:38 50-32-809/20/23 10:0250.0 13.9 1
Benzo(b)fluoranthene ND ug/L 09/22/23 11:38 205-99-209/20/23 10:0250.0 13.0 1
Benzo(g,h,i)perylene ND ug/L 09/22/23 11:38 191-24-209/20/23 10:0250.0 14.2 1
Benzo(k)fluoranthene ND ug/L 09/22/23 11:38 207-08-909/20/23 10:0250.0 13.6 1
Biphenyl (Diphenyl)ND ug/L 09/22/23 11:38 92-52-409/20/23 10:0250.0 9.1 1
4-Bromophenylphenyl ether ND ug/L 09/22/23 11:38 101-55-309/20/23 10:0250.0 8.8 1
Butylbenzylphthalate ND ug/L 09/22/23 11:38 85-68-709/20/23 10:0250.0 15.7 1
Caprolactam ND ug/L 09/22/23 11:38 105-60-209/20/23 10:0250.0 34.7 1
Carbazole ND ug/L 09/22/23 11:38 86-74-809/20/23 10:0250.0 11.8 1
4-Chloro-3-methylphenol ND ug/L 09/22/23 11:38 59-50-709/20/23 10:0250.0 16.7 1
4-Chloroaniline ND ug/L 09/22/23 11:38 106-47-809/20/23 10:02100 18.2 1
bis(2-Chloroethoxy)methane ND ug/L 09/22/23 11:38 111-91-109/20/23 10:0250.0 9.1 1
bis(2-Chloroethyl) ether ND ug/L 09/22/23 11:38 111-44-409/20/23 10:0250.0 9.6 1
2-Chloronaphthalene ND ug/L 09/22/23 11:38 91-58-709/20/23 10:0250.0 8.6 1
2-Chlorophenol ND ug/L 09/22/23 11:38 95-57-809/20/23 10:0250.0 6.0 1
4-Chlorophenylphenyl ether ND ug/L 09/22/23 11:38 7005-72-309/20/23 10:0250.0 10.0 1
Chrysene ND ug/L 09/22/23 11:38 218-01-909/20/23 10:0250.0 13.8 1
Dibenz(a,h)anthracene ND ug/L 09/22/23 11:38 53-70-309/20/23 10:0250.0 14.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 39 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ02WG-091423 Lab ID: 92688280007 Collected: 09/14/23 14:58 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Dibenzofuran ND ug/L 09/22/23 11:38 132-64-909/20/23 10:0250.0 10.5 1
3,3'-Dichlorobenzidine ND ug/L 09/22/23 11:38 91-94-109/20/23 10:02100 40.6 1
2,4-Dichlorophenol ND ug/L 09/22/23 11:38 120-83-209/20/23 10:0250.0 7.0 1
Diethylphthalate ND ug/L 09/22/23 11:38 84-66-209/20/23 10:0250.0 10.2 1
2,4-Dimethylphenol ND ug/L 09/22/23 11:38 105-67-909/20/23 10:0250.0 8.5 1
Dimethylphthalate ND ug/L 09/22/23 11:38 131-11-309/20/23 10:0250.0 10.6 1
Di-n-butylphthalate ND ug/L 09/22/23 11:38 84-74-209/20/23 10:0250.0 11.0 1
4,6-Dinitro-2-methylphenol ND ug/L 09/22/23 11:38 534-52-109/20/23 10:02100 38.9 1
2,4-Dinitrophenol ND ug/L 09/22/23 11:38 51-28-509/20/23 10:02250 130 1
2,4-Dinitrotoluene ND ug/L 09/22/23 11:38 121-14-209/20/23 10:0250.0 8.1 1
2,6-Dinitrotoluene ND ug/L 09/22/23 11:38 606-20-209/20/23 10:0250.0 8.6 1
Di-n-octylphthalate ND ug/L 09/22/23 11:38 117-84-009/20/23 10:0250.0 19.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/22/23 11:38 117-81-709/20/23 10:0230.0 18.6 1
Fluoranthene ND ug/L 09/22/23 11:38 206-44-009/20/23 10:0250.0 11.0 1
Fluorene ND ug/L 09/22/23 11:38 86-73-709/20/23 10:0250.0 10.4 1
Hexachloro-1,3-butadiene ND ug/L 09/22/23 11:38 87-68-309/20/23 10:0250.0 8.8 1
Hexachlorobenzene ND ug/L 09/22/23 11:38 118-74-109/20/23 10:0250.0 10.8 1
Hexachlorocyclopentadiene ND ug/L 09/22/23 11:38 77-47-409/20/23 10:0250.0 8.0 1
Hexachloroethane ND ug/L 09/22/23 11:38 67-72-109/20/23 10:0250.0 6.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/22/23 11:38 193-39-509/20/23 10:0250.0 14.4 1
Isophorone ND ug/L 09/22/23 11:38 78-59-109/20/23 10:0250.0 8.3 1
2-Methylnaphthalene ND ug/L 09/22/23 11:38 91-57-609/20/23 10:0250.0 9.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/22/23 11:38 95-48-709/20/23 10:0250.0 9.4 1
3&4-Methylphenol(m&p Cresol)17.0J ug/L 09/22/23 11:38 15831-10-409/20/23 10:0250.0 6.1 1
Naphthalene ND ug/L 09/22/23 11:38 91-20-309/20/23 10:0250.0 10.4 1
2-Nitroaniline ND ug/L 09/22/23 11:38 88-74-409/20/23 10:02100 14.9 1
3-Nitroaniline ND ug/L 09/22/23 11:38 99-09-209/20/23 10:02100 18.8 1
4-Nitroaniline ND ug/L 09/22/23 11:38 100-01-609/20/23 10:02100 25.5 1
Nitrobenzene ND ug/L 09/22/23 11:38 98-95-309/20/23 10:0250.0 9.4 1
2-Nitrophenol ND ug/L 09/22/23 11:38 88-75-509/20/23 10:0250.0 7.0 1
4-Nitrophenol ND ug/L 09/22/23 11:38 100-02-709/20/23 10:02250 33.0 1
N-Nitroso-di-n-propylamine ND ug/L 09/22/23 11:38 621-64-709/20/23 10:0250.0 6.6 1
N-Nitrosodiphenylamine ND ug/L 09/22/23 11:38 86-30-609/20/23 10:0250.0 15.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/22/23 11:38 108-60-109/20/23 10:0250.0 5.8 1
Pentachlorophenol ND ug/L 09/22/23 11:38 87-86-509/20/23 10:02100 18.8 1
Phenanthrene ND ug/L 09/22/23 11:38 85-01-809/20/23 10:0250.0 10.0 1
Phenol 49.1J ug/L 09/22/23 11:38 108-95-209/20/23 10:0250.0 6.8 1
Pyrene ND ug/L 09/22/23 11:38 129-00-009/20/23 10:0250.0 11.0 1
2,4,5-Trichlorophenol ND ug/L 09/22/23 11:38 95-95-409/20/23 10:0250.0 7.1 1
2,4,6-Trichlorophenol ND ug/L 09/22/23 11:38 88-06-209/20/23 10:0250.0 7.8 1
SurrogatesNitrobenzene-d5 (S)112 %09/22/23 11:38 4165-60-009/20/23 10:0210-138 1
2-Fluorobiphenyl (S)106 %09/22/23 11:38 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)137 %09/22/23 11:38 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)68 %09/22/23 11:38 13127-88-309/20/23 10:0210-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ02WG-091423 Lab ID: 92688280007 Collected: 09/14/23 14:58 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Surrogates2-Fluorophenol (S)86 %09/22/23 11:38 367-12-409/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)135 %09/22/23 11:38 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 188 ug/L 09/22/23 18:28 67-64-125.0 5.1 1
Benzene 10.0 ug/L 09/22/23 18:28 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/22/23 18:28 75-27-41.0 0.31 1
Bromoform ND ug/L 09/22/23 18:28 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/22/23 18:28 74-83-92.0 1.7 1
2-Butanone (MEK)68.6 ug/L 09/22/23 18:28 78-93-35.0 4.0 1
Carbon disulfide 2.0J ug/L 09/22/23 18:28 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/22/23 18:28 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/22/23 18:28 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/22/23 18:28 75-00-31.0 0.65 1
Chloroform ND ug/L 09/22/23 18:28 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/22/23 18:28 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/22/23 18:28 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/22/23 18:28 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/22/23 18:28 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/22/23 18:28 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/22/23 18:28 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/22/23 18:28 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/22/23 18:28 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/22/23 18:28 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/22/23 18:28 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/22/23 18:28 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/22/23 18:28 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/22/23 18:28 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/22/23 18:28 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/22/23 18:28 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/22/23 18:28 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/22/23 18:28 10061-02-61.0 0.36 1
Ethylbenzene 22.1 ug/L 09/22/23 18:28 100-41-41.0 0.30 1
2-Hexanone 0.74J ug/L 09/22/23 18:28 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)0.40J ug/L 09/22/23 18:28 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/22/23 18:28 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/22/23 18:28 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/22/23 18:28 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)14.9 ug/L 09/22/23 18:28 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/22/23 18:28 1634-04-41.0 0.42 1
Styrene ND ug/L 09/22/23 18:28 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/22/23 18:28 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/22/23 18:28 127-18-41.0 0.29 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ02WG-091423 Lab ID: 92688280007 Collected: 09/14/23 14:58 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Toluene 27.5 ug/L 09/22/23 18:28 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/22/23 18:28 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/22/23 18:28 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/22/23 18:28 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/22/23 18:28 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/22/23 18:28 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/22/23 18:28 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/22/23 18:28 75-01-41.0 0.39 1
m&p-Xylene 70.9 ug/L 09/22/23 18:28 179601-23-12.0 0.71 1
o-Xylene 28.8 ug/L 09/22/23 18:28 95-47-61.0 0.34 1
Surrogates4-Bromofluorobenzene (S)101 %09/22/23 18:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %09/22/23 18:28 17060-07-070-130 1
Toluene-d8 (S)99 %09/22/23 18:28 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 5860 mg/L 09/28/23 14:385.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 9880 mg/L 09/19/23 23:20625 625 1
Analytical Method: SM 2540D-2015
Pace Analytical Services - Asheville
2540D Total Suspended Solids
Total Suspended Solids 12.6 mg/L 09/20/23 13:402.7 2.7 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 19.3 mg/L 09/20/23 03:02 18496-25-810.0 2.2 100
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 97.8 mg/L 10/04/23 04:53 7727-37-910/03/23 03:445.0 2.5 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand 1590 mg/L 09/23/23 11:2609/22/23 13:26125 62.5 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon 504 mg/L 10/03/23 22:43 7440-44-050.0 25.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ02WG-091423 Lab ID: 92688280007 Collected: 09/14/23 14:58 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 1360 mg/L 09/21/23 11:08 16887-00-650.0 30.0 50
Sulfate 89.8 mg/L 09/21/23 11:08 14808-79-850.0 25.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR03WG-091423 Lab ID: 92688280008 Collected: 09/14/23 17:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:51 7440-36-010/02/23 09:460.015 0.0055 1
Arsenic ND mg/L 10/04/23 00:51 7440-38-210/02/23 09:460.010 0.0034 1
Barium 0.21 mg/L 10/04/23 00:51 7440-39-310/02/23 09:460.010 0.00084 1
Beryllium ND mg/L 10/04/23 00:51 7440-41-710/02/23 09:460.0040 0.00017 1
Boron 0.045J mg/L 10/04/23 00:51 7440-42-810/02/23 09:460.050 0.012 1
Cadmium ND mg/L 10/04/23 00:51 7440-43-910/02/23 09:460.0010 0.00033 1
Chromium 0.0039J mg/L 10/04/23 00:51 7440-47-310/02/23 09:460.0050 0.0017 1
Cobalt 0.0017J mg/L 10/04/23 00:51 7440-48-410/02/23 09:460.010 0.00096 1
Copper 0.0043J mg/L 10/04/23 00:51 7440-50-810/02/23 09:460.0050 0.0026 1
Lead ND mg/L 10/04/23 00:51 7439-92-110/02/23 09:460.010 0.0021 1
Manganese 0.097 mg/L 10/04/23 00:51 7439-96-510/02/23 09:460.0050 0.0011 1
Nickel 0.032 mg/L 10/04/23 00:51 7440-02-010/02/23 09:460.0050 0.0010 1
Selenium ND mg/L 10/04/23 00:51 7782-49-210/02/23 09:460.015 0.0039 1
Silver ND mg/L 10/04/23 00:51 7440-22-410/02/23 09:460.0050 0.0010 1
Thallium ND mg/L 10/04/23 00:51 7440-28-0 IS10/02/23 09:460.015 0.0029 1
Vanadium 0.11 mg/L 10/04/23 00:51 7440-62-210/02/23 09:460.010 0.0010 1
Zinc ND mg/L 10/04/23 00:51 7440-66-610/02/23 09:460.020 0.011 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:42 7440-36-0 D310/03/23 06:040.015 0.0055 1
Arsenic, Dissolved 0.0062J mg/L 10/05/23 11:42 7440-38-210/03/23 06:040.010 0.0034 1
Barium, Dissolved 0.19 mg/L 10/05/23 11:42 7440-39-310/03/23 06:040.010 0.00084 1
Beryllium, Dissolved ND mg/L 10/05/23 11:42 7440-41-7 D310/03/23 06:040.0040 0.00017 1
Boron, Dissolved 0.046J mg/L 10/05/23 11:42 7440-42-810/03/23 06:040.050 0.012 1
Cadmium, Dissolved 0.00052J mg/L 10/05/23 11:42 7440-43-910/03/23 06:040.0010 0.00033 1
Chromium, Dissolved 0.0030J mg/L 10/05/23 11:42 7440-47-310/03/23 06:040.0050 0.0017 1
Cobalt, Dissolved 0.0022J mg/L 10/05/23 11:42 7440-48-410/03/23 06:040.010 0.00096 1
Copper, Dissolved ND mg/L 10/05/23 11:42 7440-50-8 D310/03/23 06:040.0050 0.0026 1
Lead, Dissolved ND mg/L 10/05/23 11:42 7439-92-1 D310/03/23 06:040.010 0.0021 1
Manganese, Dissolved 0.048 mg/L 10/05/23 11:42 7439-96-510/03/23 06:040.0050 0.0011 1
Nickel, Dissolved 0.026 mg/L 10/05/23 11:42 7440-02-010/03/23 06:040.0050 0.0010 1
Selenium, Dissolved ND mg/L 10/05/23 11:42 7782-49-2 D310/03/23 06:040.015 0.0039 1
Silver, Dissolved 0.0029J mg/L 10/05/23 11:42 7440-22-410/03/23 06:040.0050 0.0010 1
Thallium, Dissolved ND mg/L 10/05/23 11:42 7440-28-0 D310/03/23 06:040.015 0.0029 1
Vanadium, Dissolved 0.10 mg/L 10/05/23 11:42 7440-62-210/03/23 06:040.010 0.0010 1
Zinc, Dissolved ND mg/L 10/05/23 11:42 7440-66-6 D310/03/23 06:040.020 0.011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:22 7439-97-610/04/23 09:500.00020 0.00014 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 12:57 7439-97-610/02/23 15:100.00020 0.00014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 183
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR03WG-091423 Lab ID: 92688280008 Collected: 09/14/23 17:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/21/23 19:17 83-32-909/20/23 10:0210.0 2.0 1
Acenaphthylene ND ug/L 09/21/23 19:17 208-96-809/20/23 10:0210.0 2.0 1
Acetophenone ND ug/L 09/21/23 19:17 98-86-209/20/23 10:0210.0 1.5 1
Anthracene ND ug/L 09/21/23 19:17 120-12-709/20/23 10:0210.0 2.3 1
Atrazine ND ug/L 09/21/23 19:17 1912-24-909/20/23 10:0210.0 3.2 1
Benzaldehyde ND ug/L 09/21/23 19:17 100-52-709/20/23 10:0210.0 3.6 1
Benzo(a)anthracene ND ug/L 09/21/23 19:17 56-55-3 M109/20/23 10:0210.0 2.7 1
Benzo(a)pyrene ND ug/L 09/21/23 19:17 50-32-809/20/23 10:0210.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/21/23 19:17 205-99-2 M109/20/23 10:0210.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/21/23 19:17 191-24-209/20/23 10:0210.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/21/23 19:17 207-08-909/20/23 10:0210.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/21/23 19:17 92-52-409/20/23 10:0210.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/21/23 19:17 101-55-309/20/23 10:0210.0 1.8 1
Butylbenzylphthalate ND ug/L 09/21/23 19:17 85-68-709/20/23 10:0210.0 3.1 1
Caprolactam ND ug/L 09/21/23 19:17 105-60-209/20/23 10:0210.0 6.9 1
Carbazole ND ug/L 09/21/23 19:17 86-74-809/20/23 10:0210.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/21/23 19:17 59-50-7 R109/20/23 10:0210.0 3.3 1
4-Chloroaniline ND ug/L 09/21/23 19:17 106-47-809/20/23 10:0220.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/21/23 19:17 111-91-109/20/23 10:0210.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/21/23 19:17 111-44-409/20/23 10:0210.0 1.9 1
2-Chloronaphthalene ND ug/L 09/21/23 19:17 91-58-709/20/23 10:0210.0 1.7 1
2-Chlorophenol ND ug/L 09/21/23 19:17 95-57-8 M109/20/23 10:0210.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/21/23 19:17 7005-72-309/20/23 10:0210.0 2.0 1
Chrysene ND ug/L 09/21/23 19:17 218-01-909/20/23 10:0210.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/21/23 19:17 53-70-3 M109/20/23 10:0210.0 3.0 1
Dibenzofuran ND ug/L 09/21/23 19:17 132-64-909/20/23 10:0210.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/21/23 19:17 91-94-1 M109/20/23 10:0220.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/21/23 19:17 120-83-2 M109/20/23 10:0210.0 1.4 1
Diethylphthalate ND ug/L 09/21/23 19:17 84-66-209/20/23 10:0210.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/21/23 19:17 105-67-909/20/23 10:0210.0 1.7 1
Dimethylphthalate ND ug/L 09/21/23 19:17 131-11-309/20/23 10:0210.0 2.1 1
Di-n-butylphthalate ND ug/L 09/21/23 19:17 84-74-2 M109/20/23 10:0210.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/21/23 19:17 534-52-1 M109/20/23 10:0220.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/21/23 19:17 51-28-5 M109/20/23 10:0250.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/21/23 19:17 121-14-209/20/23 10:0210.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/21/23 19:17 606-20-209/20/23 10:0210.0 1.7 1
Di-n-octylphthalate ND ug/L 09/21/23 19:17 117-84-0 M109/20/23 10:0210.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/21/23 19:17 117-81-7 M109/20/23 10:026.0 3.7 1
Fluoranthene ND ug/L 09/21/23 19:17 206-44-009/20/23 10:0210.0 2.2 1
Fluorene ND ug/L 09/21/23 19:17 86-73-709/20/23 10:0210.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/21/23 19:17 87-68-309/20/23 10:0210.0 1.8 1
Hexachlorobenzene ND ug/L 09/21/23 19:17 118-74-109/20/23 10:0210.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/21/23 19:17 77-47-409/20/23 10:0210.0 1.6 1
Hexachloroethane ND ug/L 09/21/23 19:17 67-72-1 R109/20/23 10:0210.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/21/23 19:17 193-39-509/20/23 10:0210.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR03WG-091423 Lab ID: 92688280008 Collected: 09/14/23 17:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 09/21/23 19:17 78-59-109/20/23 10:0210.0 1.7 1
2-Methylnaphthalene ND ug/L 09/21/23 19:17 91-57-609/20/23 10:0210.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/21/23 19:17 95-48-7 R109/20/23 10:0210.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/21/23 19:17 15831-10-4 R109/20/23 10:0210.0 1.2 1
Naphthalene ND ug/L 09/21/23 19:17 91-20-309/20/23 10:0210.0 2.1 1
2-Nitroaniline ND ug/L 09/21/23 19:17 88-74-409/20/23 10:0220.0 3.0 1
3-Nitroaniline ND ug/L 09/21/23 19:17 99-09-209/20/23 10:0220.0 3.8 1
4-Nitroaniline ND ug/L 09/21/23 19:17 100-01-609/20/23 10:0220.0 5.1 1
Nitrobenzene ND ug/L 09/21/23 19:17 98-95-309/20/23 10:0210.0 1.9 1
2-Nitrophenol ND ug/L 09/21/23 19:17 88-75-5 M109/20/23 10:0210.0 1.4 1
4-Nitrophenol ND ug/L 09/21/23 19:17 100-02-7 M109/20/23 10:0250.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/21/23 19:17 621-64-709/20/23 10:0210.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/21/23 19:17 86-30-609/20/23 10:0210.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/21/23 19:17 108-60-109/20/23 10:0210.0 1.2 1
Pentachlorophenol ND ug/L 09/21/23 19:17 87-86-5 M109/20/23 10:0220.0 3.8 1
Phenanthrene ND ug/L 09/21/23 19:17 85-01-809/20/23 10:0210.0 2.0 1
Phenol ND ug/L 09/21/23 19:17 108-95-209/20/23 10:0210.0 1.4 1
Pyrene ND ug/L 09/21/23 19:17 129-00-009/20/23 10:0210.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/21/23 19:17 95-95-4 M109/20/23 10:0210.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/21/23 19:17 88-06-2 M109/20/23 10:0210.0 1.6 1
SurrogatesNitrobenzene-d5 (S)108 %09/21/23 19:17 4165-60-0 1g09/20/23 10:0210-138 1
2-Fluorobiphenyl (S)110 %09/21/23 19:17 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)136 %09/21/23 19:17 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)10 %09/21/23 19:17 13127-88-309/20/23 10:0210-130 1
2-Fluorophenol (S)3 %09/21/23 19:17 367-12-4 S009/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)5 %09/21/23 19:17 118-79-6 S009/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 16.0J ug/L 09/22/23 18:47 67-64-125.0 5.1 1
Benzene 0.49J ug/L 09/22/23 18:47 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/22/23 18:47 75-27-41.0 0.31 1
Bromoform ND ug/L 09/22/23 18:47 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/22/23 18:47 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/22/23 18:47 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/22/23 18:47 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/22/23 18:47 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/22/23 18:47 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/22/23 18:47 75-00-31.0 0.65 1
Chloroform ND ug/L 09/22/23 18:47 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/22/23 18:47 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/22/23 18:47 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/22/23 18:47 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/22/23 18:47 124-48-11.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR03WG-091423 Lab ID: 92688280008 Collected: 09/14/23 17:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 09/22/23 18:47 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/22/23 18:47 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/22/23 18:47 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/22/23 18:47 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/22/23 18:47 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/22/23 18:47 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/22/23 18:47 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/22/23 18:47 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/22/23 18:47 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/22/23 18:47 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/22/23 18:47 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/22/23 18:47 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/22/23 18:47 10061-02-61.0 0.36 1
Ethylbenzene 21.5 ug/L 09/22/23 18:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/22/23 18:47 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/22/23 18:47 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/22/23 18:47 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/22/23 18:47 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/22/23 18:47 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)3.3J ug/L 09/22/23 18:47 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/22/23 18:47 1634-04-41.0 0.42 1
Styrene ND ug/L 09/22/23 18:47 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/22/23 18:47 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/22/23 18:47 127-18-41.0 0.29 1
Toluene 0.45J ug/L 09/22/23 18:47 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/22/23 18:47 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/22/23 18:47 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/22/23 18:47 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/22/23 18:47 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/22/23 18:47 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/22/23 18:47 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/22/23 18:47 75-01-41.0 0.39 1
m&p-Xylene 19.6 ug/L 09/22/23 18:47 179601-23-12.0 0.71 1
o-Xylene 24.7 ug/L 09/22/23 18:47 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %09/22/23 18:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %09/22/23 18:47 17060-07-070-130 1
Toluene-d8 (S)98 %09/22/23 18:47 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 81.0 mg/L 09/21/23 16:035.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: BR03WG-091423 Lab ID: 92688280008 Collected: 09/14/23 17:30 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 0.24 mg/L 09/20/23 03:03 18496-25-8 M10.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 8910 mg/L 09/21/23 08:54 16887-00-6 M1200 120 200
Sulfate 500 mg/L 09/21/23 08:54 14808-79-8 M1200 100 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: EB01Q-091423 Lab ID: 92688280009 Collected: 09/14/23 17:20 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:54 7440-36-010/02/23 09:460.015 0.0055 1
Arsenic ND mg/L 10/04/23 00:54 7440-38-210/02/23 09:460.010 0.0034 1
Barium ND mg/L 10/04/23 00:54 7440-39-310/02/23 09:460.010 0.00084 1
Beryllium ND mg/L 10/04/23 00:54 7440-41-710/02/23 09:460.0040 0.00017 1
Boron ND mg/L 10/04/23 00:54 7440-42-810/02/23 09:460.050 0.012 1
Cadmium ND mg/L 10/04/23 00:54 7440-43-910/02/23 09:460.0010 0.00033 1
Chromium ND mg/L 10/04/23 00:54 7440-47-310/02/23 09:460.0050 0.0017 1
Cobalt ND mg/L 10/04/23 00:54 7440-48-410/02/23 09:460.010 0.00096 1
Copper ND mg/L 10/04/23 00:54 7440-50-810/02/23 09:460.0050 0.0026 1
Lead ND mg/L 10/04/23 00:54 7439-92-110/02/23 09:460.010 0.0021 1
Manganese ND mg/L 10/04/23 00:54 7439-96-510/02/23 09:460.0050 0.0011 1
Nickel ND mg/L 10/04/23 00:54 7440-02-010/02/23 09:460.0050 0.0010 1
Selenium ND mg/L 10/04/23 00:54 7782-49-210/02/23 09:460.015 0.0039 1
Silver ND mg/L 10/04/23 00:54 7440-22-410/02/23 09:460.0050 0.0010 1
Thallium ND mg/L 10/04/23 00:54 7440-28-010/02/23 09:460.015 0.0029 1
Vanadium ND mg/L 10/04/23 00:54 7440-62-210/02/23 09:460.010 0.0010 1
Zinc ND mg/L 10/04/23 00:54 7440-66-610/02/23 09:460.020 0.011 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:46 7440-36-010/03/23 06:040.015 0.0055 1
Arsenic, Dissolved ND mg/L 10/05/23 11:46 7440-38-210/03/23 06:040.010 0.0034 1
Barium, Dissolved ND mg/L 10/05/23 11:46 7440-39-310/03/23 06:040.010 0.00084 1
Beryllium, Dissolved ND mg/L 10/05/23 11:46 7440-41-710/03/23 06:040.0040 0.00017 1
Boron, Dissolved ND mg/L 10/05/23 11:46 7440-42-810/03/23 06:040.050 0.012 1
Cadmium, Dissolved ND mg/L 10/05/23 11:46 7440-43-910/03/23 06:040.0010 0.00033 1
Chromium, Dissolved ND mg/L 10/05/23 11:46 7440-47-310/03/23 06:040.0050 0.0017 1
Cobalt, Dissolved ND mg/L 10/05/23 11:46 7440-48-410/03/23 06:040.010 0.00096 1
Copper, Dissolved ND mg/L 10/05/23 11:46 7440-50-810/03/23 06:040.0050 0.0026 1
Lead, Dissolved ND mg/L 10/05/23 11:46 7439-92-110/03/23 06:040.010 0.0021 1
Manganese, Dissolved ND mg/L 10/05/23 11:46 7439-96-510/03/23 06:040.0050 0.0011 1
Nickel, Dissolved ND mg/L 10/05/23 11:46 7440-02-010/03/23 06:040.0050 0.0010 1
Selenium, Dissolved ND mg/L 10/05/23 11:46 7782-49-210/03/23 06:040.015 0.0039 1
Silver, Dissolved ND mg/L 10/05/23 11:46 7440-22-410/03/23 06:040.0050 0.0010 1
Thallium, Dissolved ND mg/L 10/05/23 11:46 7440-28-010/03/23 06:040.015 0.0029 1
Vanadium, Dissolved ND mg/L 10/05/23 11:46 7440-62-210/03/23 06:040.010 0.0010 1
Zinc, Dissolved ND mg/L 10/05/23 11:46 7440-66-610/03/23 06:040.020 0.011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:25 7439-97-610/04/23 09:500.00020 0.00014 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 12:59 7439-97-610/02/23 15:100.00020 0.00014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: EB01Q-091423 Lab ID: 92688280009 Collected: 09/14/23 17:20 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/22/23 12:04 83-32-909/20/23 10:0210.0 2.0 1
Acenaphthylene ND ug/L 09/22/23 12:04 208-96-809/20/23 10:0210.0 2.0 1
Acetophenone ND ug/L 09/22/23 12:04 98-86-209/20/23 10:0210.0 1.5 1
Anthracene ND ug/L 09/22/23 12:04 120-12-709/20/23 10:0210.0 2.3 1
Atrazine ND ug/L 09/22/23 12:04 1912-24-909/20/23 10:0210.0 3.2 1
Benzaldehyde ND ug/L 09/22/23 12:04 100-52-709/20/23 10:0210.0 3.6 1
Benzo(a)anthracene ND ug/L 09/22/23 12:04 56-55-309/20/23 10:0210.0 2.7 1
Benzo(a)pyrene ND ug/L 09/22/23 12:04 50-32-809/20/23 10:0210.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/22/23 12:04 205-99-209/20/23 10:0210.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/22/23 12:04 191-24-209/20/23 10:0210.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/22/23 12:04 207-08-909/20/23 10:0210.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/22/23 12:04 92-52-409/20/23 10:0210.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/22/23 12:04 101-55-309/20/23 10:0210.0 1.8 1
Butylbenzylphthalate ND ug/L 09/22/23 12:04 85-68-709/20/23 10:0210.0 3.1 1
Caprolactam ND ug/L 09/22/23 12:04 105-60-209/20/23 10:0210.0 6.9 1
Carbazole ND ug/L 09/22/23 12:04 86-74-809/20/23 10:0210.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/22/23 12:04 59-50-709/20/23 10:0210.0 3.3 1
4-Chloroaniline ND ug/L 09/22/23 12:04 106-47-809/20/23 10:0220.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/22/23 12:04 111-91-109/20/23 10:0210.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/22/23 12:04 111-44-409/20/23 10:0210.0 1.9 1
2-Chloronaphthalene ND ug/L 09/22/23 12:04 91-58-709/20/23 10:0210.0 1.7 1
2-Chlorophenol ND ug/L 09/22/23 12:04 95-57-809/20/23 10:0210.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/22/23 12:04 7005-72-309/20/23 10:0210.0 2.0 1
Chrysene ND ug/L 09/22/23 12:04 218-01-909/20/23 10:0210.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/22/23 12:04 53-70-309/20/23 10:0210.0 3.0 1
Dibenzofuran ND ug/L 09/22/23 12:04 132-64-909/20/23 10:0210.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/22/23 12:04 91-94-109/20/23 10:0220.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/22/23 12:04 120-83-209/20/23 10:0210.0 1.4 1
Diethylphthalate ND ug/L 09/22/23 12:04 84-66-209/20/23 10:0210.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/22/23 12:04 105-67-909/20/23 10:0210.0 1.7 1
Dimethylphthalate ND ug/L 09/22/23 12:04 131-11-309/20/23 10:0210.0 2.1 1
Di-n-butylphthalate ND ug/L 09/22/23 12:04 84-74-209/20/23 10:0210.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/22/23 12:04 534-52-109/20/23 10:0220.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/22/23 12:04 51-28-509/20/23 10:0250.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/22/23 12:04 121-14-209/20/23 10:0210.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/22/23 12:04 606-20-209/20/23 10:0210.0 1.7 1
Di-n-octylphthalate ND ug/L 09/22/23 12:04 117-84-009/20/23 10:0210.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/22/23 12:04 117-81-709/20/23 10:026.0 3.7 1
Fluoranthene ND ug/L 09/22/23 12:04 206-44-009/20/23 10:0210.0 2.2 1
Fluorene ND ug/L 09/22/23 12:04 86-73-709/20/23 10:0210.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/22/23 12:04 87-68-309/20/23 10:0210.0 1.8 1
Hexachlorobenzene ND ug/L 09/22/23 12:04 118-74-109/20/23 10:0210.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/22/23 12:04 77-47-409/20/23 10:0210.0 1.6 1
Hexachloroethane ND ug/L 09/22/23 12:04 67-72-109/20/23 10:0210.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/22/23 12:04 193-39-509/20/23 10:0210.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 50 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: EB01Q-091423 Lab ID: 92688280009 Collected: 09/14/23 17:20 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 09/22/23 12:04 78-59-109/20/23 10:0210.0 1.7 1
2-Methylnaphthalene 3.8J ug/L 09/22/23 12:04 91-57-6 C709/20/23 10:0210.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/22/23 12:04 95-48-709/20/23 10:0210.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/22/23 12:04 15831-10-409/20/23 10:0210.0 1.2 1
Naphthalene 3.5J ug/L 09/22/23 12:04 91-20-3 C709/20/23 10:0210.0 2.1 1
2-Nitroaniline ND ug/L 09/22/23 12:04 88-74-409/20/23 10:0220.0 3.0 1
3-Nitroaniline ND ug/L 09/22/23 12:04 99-09-209/20/23 10:0220.0 3.8 1
4-Nitroaniline ND ug/L 09/22/23 12:04 100-01-609/20/23 10:0220.0 5.1 1
Nitrobenzene ND ug/L 09/22/23 12:04 98-95-309/20/23 10:0210.0 1.9 1
2-Nitrophenol ND ug/L 09/22/23 12:04 88-75-509/20/23 10:0210.0 1.4 1
4-Nitrophenol ND ug/L 09/22/23 12:04 100-02-709/20/23 10:0250.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/22/23 12:04 621-64-709/20/23 10:0210.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/22/23 12:04 86-30-609/20/23 10:0210.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/22/23 12:04 108-60-109/20/23 10:0210.0 1.2 1
Pentachlorophenol ND ug/L 09/22/23 12:04 87-86-509/20/23 10:0220.0 3.8 1
Phenanthrene ND ug/L 09/22/23 12:04 85-01-809/20/23 10:0210.0 2.0 1
Phenol ND ug/L 09/22/23 12:04 108-95-209/20/23 10:0210.0 1.4 1
Pyrene ND ug/L 09/22/23 12:04 129-00-009/20/23 10:0210.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/22/23 12:04 95-95-409/20/23 10:0210.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/22/23 12:04 88-06-209/20/23 10:0210.0 1.6 1
SurrogatesNitrobenzene-d5 (S)41 %09/22/23 12:04 4165-60-0 1g09/20/23 10:0210-138 1
2-Fluorobiphenyl (S)36 %09/22/23 12:04 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)136 %09/22/23 12:04 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)6 %09/22/23 12:04 13127-88-3 S009/20/23 10:0210-130 1
2-Fluorophenol (S)1 %09/22/23 12:04 367-12-4 S009/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)10 %09/22/23 12:04 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/22/23 00:56 67-64-125.0 5.1 1
Benzene ND ug/L 09/22/23 00:56 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/22/23 00:56 75-27-41.0 0.31 1
Bromoform ND ug/L 09/22/23 00:56 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/22/23 00:56 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/22/23 00:56 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/22/23 00:56 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/22/23 00:56 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/22/23 00:56 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/22/23 00:56 75-00-31.0 0.65 1
Chloroform ND ug/L 09/22/23 00:56 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/22/23 00:56 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/22/23 00:56 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/22/23 00:56 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/22/23 00:56 124-48-11.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: EB01Q-091423 Lab ID: 92688280009 Collected: 09/14/23 17:20 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 09/22/23 00:56 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/22/23 00:56 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/22/23 00:56 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/22/23 00:56 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/22/23 00:56 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/22/23 00:56 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/22/23 00:56 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/22/23 00:56 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/22/23 00:56 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/22/23 00:56 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/22/23 00:56 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/22/23 00:56 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/22/23 00:56 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/22/23 00:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/22/23 00:56 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/22/23 00:56 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/22/23 00:56 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/22/23 00:56 108-87-210.0 1.5 1
Methylene Chloride 2.6J ug/L 09/22/23 00:56 75-09-2 C0,C95.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/22/23 00:56 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/22/23 00:56 1634-04-41.0 0.42 1
Styrene ND ug/L 09/22/23 00:56 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/22/23 00:56 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/22/23 00:56 127-18-41.0 0.29 1
Toluene ND ug/L 09/22/23 00:56 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/22/23 00:56 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/22/23 00:56 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/22/23 00:56 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/22/23 00:56 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/22/23 00:56 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/22/23 00:56 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/22/23 00:56 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/22/23 00:56 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/22/23 00:56 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %09/22/23 00:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %09/22/23 00:56 17060-07-070-130 1
Toluene-d8 (S)100 %09/22/23 00:56 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 ND mg/L 09/22/23 19:115.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: EB01Q-091423 Lab ID: 92688280009 Collected: 09/14/23 17:20 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/20/23 03:04 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride ND mg/L 09/21/23 13:51 16887-00-61.0 0.60 1
Sulfate ND mg/L 09/21/23 13:51 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ13WG-091523 Lab ID: 92688280010 Collected: 09/15/23 10:06 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 00:58 7440-36-010/02/23 09:460.015 0.0055 1
Arsenic ND mg/L 10/04/23 00:58 7440-38-210/02/23 09:460.010 0.0034 1
Barium 0.021 mg/L 10/04/23 00:58 7440-39-310/02/23 09:460.010 0.00084 1
Beryllium ND mg/L 10/04/23 00:58 7440-41-710/02/23 09:460.0040 0.00017 1
Boron 0.043J mg/L 10/04/23 00:58 7440-42-810/02/23 09:460.050 0.012 1
Cadmium ND mg/L 10/04/23 00:58 7440-43-910/02/23 09:460.0010 0.00033 1
Chromium ND mg/L 10/04/23 00:58 7440-47-310/02/23 09:460.0050 0.0017 1
Cobalt 0.010 mg/L 10/04/23 00:58 7440-48-410/02/23 09:460.010 0.00096 1
Copper 0.036 mg/L 10/04/23 00:58 7440-50-810/02/23 09:460.0050 0.0026 1
Lead ND mg/L 10/04/23 00:58 7439-92-110/02/23 09:460.010 0.0021 1
Manganese 0.26 mg/L 10/04/23 00:58 7439-96-510/02/23 09:460.0050 0.0011 1
Nickel 0.030 mg/L 10/04/23 00:58 7440-02-010/02/23 09:460.0050 0.0010 1
Selenium ND mg/L 10/04/23 00:58 7782-49-210/02/23 09:460.015 0.0039 1
Silver ND mg/L 10/04/23 00:58 7440-22-410/02/23 09:460.0050 0.0010 1
Thallium ND mg/L 10/04/23 00:58 7440-28-010/02/23 09:460.015 0.0029 1
Vanadium 0.0031J mg/L 10/04/23 00:58 7440-62-210/02/23 09:460.010 0.0010 1
Zinc 0.10 mg/L 10/04/23 00:58 7440-66-610/02/23 09:460.020 0.011 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:50 7440-36-010/03/23 06:040.015 0.0055 1
Arsenic, Dissolved ND mg/L 10/05/23 11:50 7440-38-210/03/23 06:040.010 0.0034 1
Barium, Dissolved 0.019 mg/L 10/05/23 11:50 7440-39-310/03/23 06:040.010 0.00084 1
Beryllium, Dissolved ND mg/L 10/05/23 11:50 7440-41-710/03/23 06:040.0040 0.00017 1
Boron, Dissolved 0.043J mg/L 10/05/23 11:50 7440-42-810/03/23 06:040.050 0.012 1
Cadmium, Dissolved ND mg/L 10/05/23 11:50 7440-43-910/03/23 06:040.0010 0.00033 1
Chromium, Dissolved ND mg/L 10/05/23 11:50 7440-47-310/03/23 06:040.0050 0.0017 1
Cobalt, Dissolved 0.0078J mg/L 10/05/23 11:50 7440-48-410/03/23 06:040.010 0.00096 1
Copper, Dissolved 0.0036J mg/L 10/05/23 11:50 7440-50-810/03/23 06:040.0050 0.0026 1
Lead, Dissolved ND mg/L 10/05/23 11:50 7439-92-110/03/23 06:040.010 0.0021 1
Manganese, Dissolved 0.25 mg/L 10/05/23 11:50 7439-96-510/03/23 06:040.0050 0.0011 1
Nickel, Dissolved 0.023 mg/L 10/05/23 11:50 7440-02-010/03/23 06:040.0050 0.0010 1
Selenium, Dissolved ND mg/L 10/05/23 11:50 7782-49-210/03/23 06:040.015 0.0039 1
Silver, Dissolved ND mg/L 10/05/23 11:50 7440-22-410/03/23 06:040.0050 0.0010 1
Thallium, Dissolved ND mg/L 10/05/23 11:50 7440-28-010/03/23 06:040.015 0.0029 1
Vanadium, Dissolved 0.0021J mg/L 10/05/23 11:50 7440-62-210/03/23 06:040.010 0.0010 1
Zinc, Dissolved 0.096 mg/L 10/05/23 11:50 7440-66-610/03/23 06:040.020 0.011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:27 7439-97-610/04/23 09:500.00020 0.00014 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 13:01 7439-97-610/02/23 15:100.00020 0.00014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ13WG-091523 Lab ID: 92688280010 Collected: 09/15/23 10:06 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/22/23 12:29 83-32-909/20/23 10:0210.0 2.0 1
Acenaphthylene ND ug/L 09/22/23 12:29 208-96-809/20/23 10:0210.0 2.0 1
Acetophenone ND ug/L 09/22/23 12:29 98-86-209/20/23 10:0210.0 1.5 1
Anthracene ND ug/L 09/22/23 12:29 120-12-709/20/23 10:0210.0 2.3 1
Atrazine ND ug/L 09/22/23 12:29 1912-24-909/20/23 10:0210.0 3.2 1
Benzaldehyde ND ug/L 09/22/23 12:29 100-52-709/20/23 10:0210.0 3.6 1
Benzo(a)anthracene ND ug/L 09/22/23 12:29 56-55-309/20/23 10:0210.0 2.7 1
Benzo(a)pyrene ND ug/L 09/22/23 12:29 50-32-809/20/23 10:0210.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/22/23 12:29 205-99-209/20/23 10:0210.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/22/23 12:29 191-24-209/20/23 10:0210.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/22/23 12:29 207-08-909/20/23 10:0210.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/22/23 12:29 92-52-409/20/23 10:0210.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/22/23 12:29 101-55-309/20/23 10:0210.0 1.8 1
Butylbenzylphthalate ND ug/L 09/22/23 12:29 85-68-709/20/23 10:0210.0 3.1 1
Caprolactam ND ug/L 09/22/23 12:29 105-60-209/20/23 10:0210.0 6.9 1
Carbazole ND ug/L 09/22/23 12:29 86-74-809/20/23 10:0210.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/22/23 12:29 59-50-709/20/23 10:0210.0 3.3 1
4-Chloroaniline ND ug/L 09/22/23 12:29 106-47-809/20/23 10:0220.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/22/23 12:29 111-91-109/20/23 10:0210.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/22/23 12:29 111-44-409/20/23 10:0210.0 1.9 1
2-Chloronaphthalene ND ug/L 09/22/23 12:29 91-58-709/20/23 10:0210.0 1.7 1
2-Chlorophenol ND ug/L 09/22/23 12:29 95-57-809/20/23 10:0210.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/22/23 12:29 7005-72-309/20/23 10:0210.0 2.0 1
Chrysene ND ug/L 09/22/23 12:29 218-01-909/20/23 10:0210.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/22/23 12:29 53-70-309/20/23 10:0210.0 3.0 1
Dibenzofuran ND ug/L 09/22/23 12:29 132-64-909/20/23 10:0210.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/22/23 12:29 91-94-109/20/23 10:0220.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/22/23 12:29 120-83-209/20/23 10:0210.0 1.4 1
Diethylphthalate ND ug/L 09/22/23 12:29 84-66-209/20/23 10:0210.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/22/23 12:29 105-67-909/20/23 10:0210.0 1.7 1
Dimethylphthalate ND ug/L 09/22/23 12:29 131-11-309/20/23 10:0210.0 2.1 1
Di-n-butylphthalate ND ug/L 09/22/23 12:29 84-74-209/20/23 10:0210.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/22/23 12:29 534-52-109/20/23 10:0220.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/22/23 12:29 51-28-509/20/23 10:0250.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/22/23 12:29 121-14-209/20/23 10:0210.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/22/23 12:29 606-20-209/20/23 10:0210.0 1.7 1
Di-n-octylphthalate ND ug/L 09/22/23 12:29 117-84-009/20/23 10:0210.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/22/23 12:29 117-81-709/20/23 10:026.0 3.7 1
Fluoranthene ND ug/L 09/22/23 12:29 206-44-009/20/23 10:0210.0 2.2 1
Fluorene ND ug/L 09/22/23 12:29 86-73-709/20/23 10:0210.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/22/23 12:29 87-68-309/20/23 10:0210.0 1.8 1
Hexachlorobenzene ND ug/L 09/22/23 12:29 118-74-109/20/23 10:0210.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/22/23 12:29 77-47-409/20/23 10:0210.0 1.6 1
Hexachloroethane ND ug/L 09/22/23 12:29 67-72-109/20/23 10:0210.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/22/23 12:29 193-39-509/20/23 10:0210.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ13WG-091523 Lab ID: 92688280010 Collected: 09/15/23 10:06 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Isophorone ND ug/L 09/22/23 12:29 78-59-109/20/23 10:0210.0 1.7 1
2-Methylnaphthalene ND ug/L 09/22/23 12:29 91-57-609/20/23 10:0210.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/22/23 12:29 95-48-709/20/23 10:0210.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/22/23 12:29 15831-10-409/20/23 10:0210.0 1.2 1
Naphthalene ND ug/L 09/22/23 12:29 91-20-309/20/23 10:0210.0 2.1 1
2-Nitroaniline ND ug/L 09/22/23 12:29 88-74-409/20/23 10:0220.0 3.0 1
3-Nitroaniline ND ug/L 09/22/23 12:29 99-09-209/20/23 10:0220.0 3.8 1
4-Nitroaniline ND ug/L 09/22/23 12:29 100-01-609/20/23 10:0220.0 5.1 1
Nitrobenzene ND ug/L 09/22/23 12:29 98-95-309/20/23 10:0210.0 1.9 1
2-Nitrophenol ND ug/L 09/22/23 12:29 88-75-509/20/23 10:0210.0 1.4 1
4-Nitrophenol ND ug/L 09/22/23 12:29 100-02-709/20/23 10:0250.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/22/23 12:29 621-64-709/20/23 10:0210.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/22/23 12:29 86-30-609/20/23 10:0210.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/22/23 12:29 108-60-109/20/23 10:0210.0 1.2 1
Pentachlorophenol ND ug/L 09/22/23 12:29 87-86-509/20/23 10:0220.0 3.8 1
Phenanthrene ND ug/L 09/22/23 12:29 85-01-809/20/23 10:0210.0 2.0 1
Phenol ND ug/L 09/22/23 12:29 108-95-209/20/23 10:0210.0 1.4 1
Pyrene ND ug/L 09/22/23 12:29 129-00-009/20/23 10:0210.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/22/23 12:29 95-95-409/20/23 10:0210.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/22/23 12:29 88-06-209/20/23 10:0210.0 1.6 1
SurrogatesNitrobenzene-d5 (S)81 %09/22/23 12:29 4165-60-009/20/23 10:0210-138 1
2-Fluorobiphenyl (S)71 %09/22/23 12:29 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)147 %09/22/23 12:29 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)37 %09/22/23 12:29 13127-88-309/20/23 10:0210-130 1
2-Fluorophenol (S)53 %09/22/23 12:29 367-12-409/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)144 %09/22/23 12:29 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/22/23 19:05 67-64-125.0 5.1 1
Benzene ND ug/L 09/22/23 19:05 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/22/23 19:05 75-27-41.0 0.31 1
Bromoform ND ug/L 09/22/23 19:05 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/22/23 19:05 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/22/23 19:05 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/22/23 19:05 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/22/23 19:05 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/22/23 19:05 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/22/23 19:05 75-00-31.0 0.65 1
Chloroform 2.3 ug/L 09/22/23 19:05 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/22/23 19:05 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/22/23 19:05 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/22/23 19:05 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/22/23 19:05 124-48-11.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ13WG-091523 Lab ID: 92688280010 Collected: 09/15/23 10:06 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 09/22/23 19:05 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/22/23 19:05 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/22/23 19:05 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/22/23 19:05 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/22/23 19:05 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/22/23 19:05 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/22/23 19:05 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/22/23 19:05 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/22/23 19:05 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/22/23 19:05 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/22/23 19:05 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/22/23 19:05 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/22/23 19:05 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/22/23 19:05 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/22/23 19:05 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/22/23 19:05 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/22/23 19:05 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/22/23 19:05 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/22/23 19:05 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/22/23 19:05 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/22/23 19:05 1634-04-41.0 0.42 1
Styrene ND ug/L 09/22/23 19:05 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/22/23 19:05 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/22/23 19:05 127-18-41.0 0.29 1
Toluene ND ug/L 09/22/23 19:05 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/22/23 19:05 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/22/23 19:05 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/22/23 19:05 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/22/23 19:05 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/22/23 19:05 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/22/23 19:05 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/22/23 19:05 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/22/23 19:05 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/22/23 19:05 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %09/22/23 19:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %09/22/23 19:05 17060-07-070-130 1
Toluene-d8 (S)97 %09/22/23 19:05 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 108 mg/L 09/27/23 20:245.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ13WG-091523 Lab ID: 92688280010 Collected: 09/15/23 10:06 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/20/23 03:04 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 12.2 mg/L 09/20/23 21:03 16887-00-61.0 0.60 1
Sulfate 138 mg/L 09/21/23 07:38 14808-79-83.0 1.5 3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ07WG-091523 Lab ID: 92688280011 Collected: 09/15/23 11:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
HEM, Oil and Grease
Oil and Grease 32.4 mg/L 10/06/23 11:305.0 1.1 1
Analytical Method: EPA 8015C Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8015 Diesel Low Volume
Diesel Range Organics(C10-C28)ND mg/L 09/22/23 18:1409/21/23 15:555.4 1.7 1
Surrogatesn-Pentacosane (S)33 %09/22/23 18:14 629-99-209/21/23 15:5529-158 1
Analytical Method: EPA 5030B/8015C
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/L 09/24/23 01:390.080 0.034 1
Surrogates
4-Bromofluorobenzene (S)89 %09/24/23 01:39 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND mg/L 10/04/23 01:01 7440-36-0 D310/02/23 09:460.075 0.028 5
Arsenic 0.021J mg/L 10/04/23 01:01 7440-38-210/02/23 09:460.050 0.017 5
Barium 0.13 mg/L 10/04/23 01:01 7440-39-310/02/23 09:460.050 0.0042 5
Beryllium 0.0078J mg/L 10/04/23 01:01 7440-41-710/02/23 09:460.020 0.00085 5
Boron 0.17J mg/L 10/04/23 01:01 7440-42-810/02/23 09:460.25 0.062 5
Cadmium ND mg/L 10/04/23 01:01 7440-43-9 D310/02/23 09:460.0050 0.0016 5
Chromium 0.22 mg/L 10/04/23 01:01 7440-47-310/02/23 09:460.025 0.0085 5
Cobalt 0.014J mg/L 10/04/23 01:01 7440-48-410/02/23 09:460.050 0.0048 5
Copper 0.060 mg/L 10/04/23 01:01 7440-50-810/02/23 09:460.025 0.013 5
Lead 0.039J mg/L 10/04/23 01:01 7439-92-110/02/23 09:460.050 0.010 5
Manganese 0.12 mg/L 10/04/23 01:01 7439-96-510/02/23 09:460.025 0.0055 5
Nickel 0.15 mg/L 10/04/23 01:01 7440-02-010/02/23 09:460.025 0.0050 5
Selenium ND mg/L 10/04/23 01:01 7782-49-2 D310/02/23 09:460.075 0.020 5
Silver ND mg/L 10/04/23 01:01 7440-22-4 D310/02/23 09:460.025 0.0050 5
Thallium ND mg/L 10/04/23 01:01 7440-28-0 D310/02/23 09:460.075 0.014 5
Vanadium 0.96 mg/L 10/04/23 01:01 7440-62-210/02/23 09:460.050 0.0050 5
Zinc ND mg/L 10/04/23 01:01 7440-66-6 D310/02/23 09:460.10 0.055 5
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND mg/L 10/05/23 11:54 7440-36-0 D310/03/23 06:040.030 0.011 2
Arsenic, Dissolved 0.013J mg/L 10/05/23 11:54 7440-38-210/03/23 06:040.020 0.0068 2
Barium, Dissolved 0.11 mg/L 10/05/23 11:54 7440-39-310/03/23 06:040.020 0.0017 2
Beryllium, Dissolved 0.0057J mg/L 10/05/23 11:54 7440-41-710/03/23 06:040.0080 0.00034 2
Boron, Dissolved 0.13 mg/L 10/05/23 11:54 7440-42-810/03/23 06:040.10 0.025 2
Cadmium, Dissolved 0.00072J mg/L 10/05/23 11:54 7440-43-910/03/23 06:040.0020 0.00066 2
Chromium, Dissolved 0.20 mg/L 10/05/23 11:54 7440-47-310/03/23 06:040.010 0.0034 2
Cobalt, Dissolved 0.010J mg/L 10/05/23 11:54 7440-48-410/03/23 06:040.020 0.0019 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ07WG-091523 Lab ID: 92688280011 Collected: 09/15/23 11:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Copper, Dissolved 0.049 mg/L 10/05/23 11:54 7440-50-810/03/23 06:040.010 0.0052 2
Lead, Dissolved 0.033 mg/L 10/05/23 11:54 7439-92-110/03/23 06:040.020 0.0042 2
Manganese, Dissolved 0.086 mg/L 10/05/23 11:54 7439-96-510/03/23 06:040.010 0.0022 2
Nickel, Dissolved 0.12 mg/L 10/05/23 11:54 7440-02-010/03/23 06:040.010 0.0020 2
Selenium, Dissolved ND mg/L 10/05/23 11:54 7782-49-2 D310/03/23 06:040.030 0.0078 2
Silver, Dissolved ND mg/L 10/05/23 11:54 7440-22-4 D310/03/23 06:040.010 0.0020 2
Thallium, Dissolved ND mg/L 10/05/23 11:54 7440-28-0 D310/03/23 06:040.030 0.0058 2
Vanadium, Dissolved 0.80 mg/L 10/05/23 11:54 7440-62-210/03/23 06:040.020 0.0020 2
Zinc, Dissolved 0.028J mg/L 10/05/23 11:54 7440-66-610/03/23 06:040.040 0.022 2
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND mg/L 10/05/23 11:29 7439-97-6 D310/04/23 09:500.0016 0.0011 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND mg/L 10/03/23 13:04 7439-97-6 D310/02/23 15:100.00080 0.00056 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/22/23 12:55 83-32-909/20/23 10:0250.0 10.0 1
Acenaphthylene ND ug/L 09/22/23 12:55 208-96-809/20/23 10:0250.0 9.8 1
Acetophenone ND ug/L 09/22/23 12:55 98-86-209/20/23 10:0250.0 7.5 1
Anthracene ND ug/L 09/22/23 12:55 120-12-709/20/23 10:0250.0 11.6 1
Atrazine ND ug/L 09/22/23 12:55 1912-24-909/20/23 10:0250.0 15.9 1
Benzaldehyde ND ug/L 09/22/23 12:55 100-52-709/20/23 10:0250.0 18.0 1
Benzo(a)anthracene ND ug/L 09/22/23 12:55 56-55-309/20/23 10:0250.0 13.4 1
Benzo(a)pyrene ND ug/L 09/22/23 12:55 50-32-809/20/23 10:0250.0 13.9 1
Benzo(b)fluoranthene ND ug/L 09/22/23 12:55 205-99-209/20/23 10:0250.0 13.0 1
Benzo(g,h,i)perylene ND ug/L 09/22/23 12:55 191-24-209/20/23 10:0250.0 14.2 1
Benzo(k)fluoranthene ND ug/L 09/22/23 12:55 207-08-909/20/23 10:0250.0 13.6 1
Biphenyl (Diphenyl)ND ug/L 09/22/23 12:55 92-52-409/20/23 10:0250.0 9.1 1
4-Bromophenylphenyl ether ND ug/L 09/22/23 12:55 101-55-309/20/23 10:0250.0 8.8 1
Butylbenzylphthalate ND ug/L 09/22/23 12:55 85-68-709/20/23 10:0250.0 15.7 1
Caprolactam ND ug/L 09/22/23 12:55 105-60-209/20/23 10:0250.0 34.7 1
Carbazole ND ug/L 09/22/23 12:55 86-74-809/20/23 10:0250.0 11.8 1
4-Chloro-3-methylphenol ND ug/L 09/22/23 12:55 59-50-709/20/23 10:0250.0 16.7 1
4-Chloroaniline ND ug/L 09/22/23 12:55 106-47-809/20/23 10:02100 18.2 1
bis(2-Chloroethoxy)methane ND ug/L 09/22/23 12:55 111-91-109/20/23 10:0250.0 9.1 1
bis(2-Chloroethyl) ether ND ug/L 09/22/23 12:55 111-44-409/20/23 10:0250.0 9.6 1
2-Chloronaphthalene ND ug/L 09/22/23 12:55 91-58-709/20/23 10:0250.0 8.6 1
2-Chlorophenol ND ug/L 09/22/23 12:55 95-57-809/20/23 10:0250.0 6.0 1
4-Chlorophenylphenyl ether ND ug/L 09/22/23 12:55 7005-72-309/20/23 10:0250.0 10.0 1
Chrysene ND ug/L 09/22/23 12:55 218-01-909/20/23 10:0250.0 13.8 1
Dibenz(a,h)anthracene ND ug/L 09/22/23 12:55 53-70-309/20/23 10:0250.0 14.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ07WG-091523 Lab ID: 92688280011 Collected: 09/15/23 11:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Dibenzofuran ND ug/L 09/22/23 12:55 132-64-909/20/23 10:0250.0 10.5 1
3,3'-Dichlorobenzidine ND ug/L 09/22/23 12:55 91-94-109/20/23 10:02100 40.6 1
2,4-Dichlorophenol ND ug/L 09/22/23 12:55 120-83-209/20/23 10:0250.0 7.0 1
Diethylphthalate ND ug/L 09/22/23 12:55 84-66-209/20/23 10:0250.0 10.2 1
2,4-Dimethylphenol ND ug/L 09/22/23 12:55 105-67-909/20/23 10:0250.0 8.5 1
Dimethylphthalate ND ug/L 09/22/23 12:55 131-11-309/20/23 10:0250.0 10.6 1
Di-n-butylphthalate ND ug/L 09/22/23 12:55 84-74-209/20/23 10:0250.0 11.0 1
4,6-Dinitro-2-methylphenol ND ug/L 09/22/23 12:55 534-52-109/20/23 10:02100 38.9 1
2,4-Dinitrophenol ND ug/L 09/22/23 12:55 51-28-509/20/23 10:02250 130 1
2,4-Dinitrotoluene ND ug/L 09/22/23 12:55 121-14-209/20/23 10:0250.0 8.1 1
2,6-Dinitrotoluene ND ug/L 09/22/23 12:55 606-20-209/20/23 10:0250.0 8.6 1
Di-n-octylphthalate ND ug/L 09/22/23 12:55 117-84-009/20/23 10:0250.0 19.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/22/23 12:55 117-81-709/20/23 10:0230.0 18.6 1
Fluoranthene ND ug/L 09/22/23 12:55 206-44-009/20/23 10:0250.0 11.0 1
Fluorene ND ug/L 09/22/23 12:55 86-73-709/20/23 10:0250.0 10.4 1
Hexachloro-1,3-butadiene ND ug/L 09/22/23 12:55 87-68-309/20/23 10:0250.0 8.8 1
Hexachlorobenzene ND ug/L 09/22/23 12:55 118-74-109/20/23 10:0250.0 10.8 1
Hexachlorocyclopentadiene ND ug/L 09/22/23 12:55 77-47-409/20/23 10:0250.0 8.0 1
Hexachloroethane ND ug/L 09/22/23 12:55 67-72-109/20/23 10:0250.0 6.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/22/23 12:55 193-39-509/20/23 10:0250.0 14.4 1
Isophorone ND ug/L 09/22/23 12:55 78-59-109/20/23 10:0250.0 8.3 1
2-Methylnaphthalene ND ug/L 09/22/23 12:55 91-57-609/20/23 10:0250.0 9.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/22/23 12:55 95-48-709/20/23 10:0250.0 9.4 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/22/23 12:55 15831-10-409/20/23 10:0250.0 6.1 1
Naphthalene ND ug/L 09/22/23 12:55 91-20-309/20/23 10:0250.0 10.4 1
2-Nitroaniline ND ug/L 09/22/23 12:55 88-74-409/20/23 10:02100 14.9 1
3-Nitroaniline ND ug/L 09/22/23 12:55 99-09-209/20/23 10:02100 18.8 1
4-Nitroaniline ND ug/L 09/22/23 12:55 100-01-609/20/23 10:02100 25.5 1
Nitrobenzene ND ug/L 09/22/23 12:55 98-95-309/20/23 10:0250.0 9.4 1
2-Nitrophenol ND ug/L 09/22/23 12:55 88-75-509/20/23 10:0250.0 7.0 1
4-Nitrophenol ND ug/L 09/22/23 12:55 100-02-709/20/23 10:02250 33.0 1
N-Nitroso-di-n-propylamine ND ug/L 09/22/23 12:55 621-64-709/20/23 10:0250.0 6.6 1
N-Nitrosodiphenylamine ND ug/L 09/22/23 12:55 86-30-609/20/23 10:0250.0 15.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/22/23 12:55 108-60-109/20/23 10:0250.0 5.8 1
Pentachlorophenol ND ug/L 09/22/23 12:55 87-86-509/20/23 10:02100 18.8 1
Phenanthrene ND ug/L 09/22/23 12:55 85-01-809/20/23 10:0250.0 10.0 1
Phenol ND ug/L 09/22/23 12:55 108-95-209/20/23 10:0250.0 6.8 1
Pyrene ND ug/L 09/22/23 12:55 129-00-009/20/23 10:0250.0 11.0 1
2,4,5-Trichlorophenol ND ug/L 09/22/23 12:55 95-95-409/20/23 10:0250.0 7.1 1
2,4,6-Trichlorophenol ND ug/L 09/22/23 12:55 88-06-209/20/23 10:0250.0 7.8 1
SurrogatesNitrobenzene-d5 (S)113 %09/22/23 12:55 4165-60-009/20/23 10:0210-138 1
2-Fluorobiphenyl (S)106 %09/22/23 12:55 321-60-809/20/23 10:0210-130 1
Terphenyl-d14 (S)143 %09/22/23 12:55 1718-51-009/20/23 10:0219-191 1
Phenol-d6 (S)65 %09/22/23 12:55 13127-88-309/20/23 10:0210-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ07WG-091523 Lab ID: 92688280011 Collected: 09/15/23 11:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Surrogates2-Fluorophenol (S)83 %09/22/23 12:55 367-12-409/20/23 10:0210-130 1
2,4,6-Tribromophenol (S)130 %09/22/23 12:55 118-79-609/20/23 10:0210-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 15.9J ug/L 09/22/23 19:23 67-64-125.0 5.1 1
Benzene 0.46J ug/L 09/22/23 19:23 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/22/23 19:23 75-27-41.0 0.31 1
Bromoform ND ug/L 09/22/23 19:23 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/22/23 19:23 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/22/23 19:23 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/22/23 19:23 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/22/23 19:23 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/22/23 19:23 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/22/23 19:23 75-00-31.0 0.65 1
Chloroform ND ug/L 09/22/23 19:23 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/22/23 19:23 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/22/23 19:23 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/22/23 19:23 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/22/23 19:23 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/22/23 19:23 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/22/23 19:23 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/22/23 19:23 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/22/23 19:23 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/22/23 19:23 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/22/23 19:23 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/22/23 19:23 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/22/23 19:23 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/22/23 19:23 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/22/23 19:23 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/22/23 19:23 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/22/23 19:23 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/22/23 19:23 10061-02-61.0 0.36 1
Ethylbenzene 0.36J ug/L 09/22/23 19:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/22/23 19:23 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/22/23 19:23 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/22/23 19:23 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/22/23 19:23 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/22/23 19:23 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/22/23 19:23 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/22/23 19:23 1634-04-41.0 0.42 1
Styrene ND ug/L 09/22/23 19:23 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/22/23 19:23 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/22/23 19:23 127-18-41.0 0.29 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 62 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ07WG-091523 Lab ID: 92688280011 Collected: 09/15/23 11:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Toluene 2.8 ug/L 09/22/23 19:23 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/22/23 19:23 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/22/23 19:23 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/22/23 19:23 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/22/23 19:23 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/22/23 19:23 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/22/23 19:23 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/22/23 19:23 75-01-41.0 0.39 1
m&p-Xylene 1.6J ug/L 09/22/23 19:23 179601-23-12.0 0.71 1
o-Xylene 1.7 ug/L 09/22/23 19:23 95-47-61.0 0.34 1
Surrogates4-Bromofluorobenzene (S)100 %09/22/23 19:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %09/22/23 19:23 17060-07-070-130 1
Toluene-d8 (S)98 %09/22/23 19:23 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 3220 mg/L 09/27/23 20:475.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 5810 mg/L 09/19/23 23:20333 333 1
Analytical Method: SM 2540D-2015
Pace Analytical Services - Asheville
2540D Total Suspended Solids
Total Suspended Solids 4.6 mg/L 09/20/23 13:412.5 2.5 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 0.080J mg/L 09/20/23 03:05 18496-25-80.10 0.022 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 56.9 mg/L 10/04/23 04:54 7727-37-910/03/23 03:445.0 2.5 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand 2160 mg/L 09/23/23 11:2609/22/23 13:26200 100 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon 436 mg/L 10/03/23 23:02 7440-44-050.0 25.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: PZ07WG-091523 Lab ID: 92688280011 Collected: 09/15/23 11:00 Received: 09/15/23 16:42 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 206 mg/L 09/21/23 11:22 16887-00-6 M110.0 6.0 10
Sulfate 20.1 mg/L 09/21/23 11:22 14808-79-810.0 5.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: TB1-091423 Lab ID: 92688280012 Collected: 09/14/23 09:00 Received: 09/15/23 16:32 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/19/23 18:51 67-64-125.0 5.1 1
Benzene ND ug/L 09/19/23 18:51 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/19/23 18:51 75-27-41.0 0.31 1
Bromoform ND ug/L 09/19/23 18:51 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/19/23 18:51 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/19/23 18:51 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/19/23 18:51 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/19/23 18:51 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/19/23 18:51 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/19/23 18:51 75-00-31.0 0.65 1
Chloroform ND ug/L 09/19/23 18:51 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/19/23 18:51 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/19/23 18:51 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/19/23 18:51 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/19/23 18:51 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/19/23 18:51 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/19/23 18:51 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/19/23 18:51 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/19/23 18:51 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/19/23 18:51 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/19/23 18:51 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/19/23 18:51 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/19/23 18:51 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/19/23 18:51 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/19/23 18:51 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/19/23 18:51 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/19/23 18:51 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/19/23 18:51 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/19/23 18:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/19/23 18:51 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/19/23 18:51 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/19/23 18:51 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/19/23 18:51 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/19/23 18:51 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/19/23 18:51 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/19/23 18:51 1634-04-41.0 0.42 1
Styrene ND ug/L 09/19/23 18:51 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/19/23 18:51 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/19/23 18:51 127-18-41.0 0.29 1
Toluene ND ug/L 09/19/23 18:51 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/19/23 18:51 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/19/23 18:51 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/19/23 18:51 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/19/23 18:51 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/19/23 18:51 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: TB1-091423 Lab ID: 92688280012 Collected: 09/14/23 09:00 Received: 09/15/23 16:32 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/19/23 18:51 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/19/23 18:51 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/19/23 18:51 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/19/23 18:51 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %09/19/23 18:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %09/19/23 18:51 17060-07-070-130 1
Toluene-d8 (S)99 %09/19/23 18:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 183
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Sample: TB2-091423 Lab ID: 92688280013 Collected: 09/14/23 09:00 Received: 09/15/23 16:32 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 5030B/8015C
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/L 09/23/23 19:330.080 0.034 1
Surrogates
4-Bromofluorobenzene (S)84 %09/23/23 19:33 460-00-470-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804467
EPA 1664B
EPA 1664B
1664 HEM, Oil and Grease
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688280007, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4166196
Associated Lab Samples:92688280007, 92688280011
Matrix: Water
AnalyzedMDL
Oil and Grease mg/L ND 5.0 10/06/23 11:301.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4166197LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/L 32.940 82 78-114
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4166198MATRIX SPIKE SAMPLE:
MSSpike
Result
92691492002
Oil and Grease mg/L 32.638.5 82 78-114ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
35829841003
4166199SAMPLE DUPLICATE:
Oil and Grease mg/L 192 1 30194
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801614
EPA 5030B/8015C
EPA 5030B/8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688280007, 92688280011, 92688280013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152640
Associated Lab Samples:92688280007, 92688280011, 92688280013
Matrix: Water
AnalyzedMDL
Gas Range Organics (C6-C10)mg/L ND 0.080 09/23/23 19:070.034
4-Bromofluorobenzene (S)%85 70-130 09/23/23 19:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152641LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/L 1.01 102 70-130
4-Bromofluorobenzene (S)%87 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4152643MATRIX SPIKE SAMPLE:
MSSpike
Result
92688903001
Gas Range Organics (C6-C10)mg/L 1.21 108 63-1300.15
4-Bromofluorobenzene (S)%89 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688992001
4152642SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/L ND F1,HS30ND
4-Bromofluorobenzene (S)%8685
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954846
EPA 7470
EPA 7470
7470 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5250379
Associated Lab Samples: 92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
Mercury mg/L ND 0.00020 10/05/23 10:250.00014
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5250380LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/L 0.00190.002 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5250381MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35830499001
5250382
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/L 0.002 97 75-12598 1 200.0020.14Uug/L 0.0020 0.0020
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954441
EPA 7470
EPA 7470
7470 Mercury Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5248254
Associated Lab Samples: 92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
Mercury, Dissolved mg/L ND 0.00020 10/03/23 12:130.00014
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5248255LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved mg/L 0.00190.002 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5248256MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92687719001
5248257
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved mg/L 0.002 94 85-11594 0 200.002ND 0.0019 0.0019
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954340
EPA 3010
EPA 6010
6010 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5247760
Associated Lab Samples: 92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
Antimony mg/L ND 0.015 10/03/23 23:260.0055
Arsenic mg/L ND 0.010 10/03/23 23:260.0034
Barium mg/L ND 0.010 10/03/23 23:260.00084
Beryllium mg/L ND 0.0040 10/03/23 23:260.00017
Boron mg/L ND 0.050 10/03/23 23:260.012
Cadmium mg/L ND 0.0010 10/03/23 23:260.00033
Chromium mg/L ND 0.0050 10/03/23 23:260.0017
Cobalt mg/L ND 0.010 10/03/23 23:260.00096
Copper mg/L ND 0.0050 10/03/23 23:260.0026
Lead mg/L ND 0.010 10/03/23 23:260.0021
Manganese mg/L ND 0.0050 10/03/23 23:260.0011
Nickel mg/L ND 0.0050 10/03/23 23:260.0010
Selenium mg/L ND 0.015 10/03/23 23:260.0039
Silver mg/L ND 0.0050 10/03/23 23:260.0010
Thallium mg/L ND 0.015 10/03/23 23:260.0029
Vanadium mg/L ND 0.010 10/03/23 23:260.0010
Zinc mg/L ND 0.020 10/03/23 23:260.011
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5247761LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/L 0.250.25 102 80-120
Arsenic mg/L 0.240.25 97 80-120
Barium mg/L 0.250.25 101 80-120
Beryllium mg/L 0.0250.025 100 80-120
Boron mg/L 1.21.2 100 80-120
Cadmium mg/L 0.0250.025 101 80-120
Chromium mg/L 0.250.25 99 80-120
Cobalt mg/L 0.250.25 102 80-120
Copper mg/L 0.250.25 100 80-120
Lead mg/L 0.260.25 104 80-120
Manganese mg/L 0.250.25 100 80-120
Nickel mg/L 0.260.25 103 80-120
Selenium mg/L 0.250.25 101 80-120
Silver mg/L 0.0240.025 98 80-120
Thallium mg/L 0.240.25 95 80-120
Vanadium mg/L 0.250.25 100 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5247761LABORATORY CONTROL SAMPLE:
LCSSpike
Zinc mg/L 1.21.2 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5247762MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5247763
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony mg/L 0.25 102 75-125101 1 200.25ND 0.26 0.25
Arsenic mg/L 0.25 98 75-12598 0 200.25ND 0.25 0.25
Barium mg/L 0.25 101 75-125101 0 200.2544.7 ug/L 0.30 0.30
Beryllium mg/L 0.025 102 75-125101 0 200.025ND 0.025 0.025
Boron mg/L 1.2 101 75-125101 0 201.255.7 ug/L 1.3 1.3
Cadmium mg/L 0.025 101 75-125100 0 200.025ND 0.025 0.025
Chromium mg/L 0.25 100 75-125100 0 200.25ND 0.25 0.25
Cobalt mg/L 0.25 102 75-125101 0 200.25ND 0.25 0.25
Copper mg/L 0.25 100 75-125100 1 200.25ND 0.25 0.25
Lead mg/L 0.25 102 75-125102 0 200.25ND 0.26 0.26
Manganese mg/L 0.25 100 75-125100 0 200.2511.2 ug/L 0.26 0.26
Nickel mg/L 0.25 103 75-125102 1 200.25ND 0.26 0.26
Selenium mg/L 0.25 103 75-125102 1 200.25ND 0.26 0.26
Silver mg/L 0.025 95 75-12597 3 200.025ND 0.024 0.024
Thallium mg/L 0.25 96 75-12597 1 200.25ND 0.24 0.24
Vanadium mg/L 0.25 101 75-125101 0 200.25ND 0.25 0.25
Zinc mg/L 1.2 100 75-125100 0 201.2ND 1.3 1.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954596
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5249435
Associated Lab Samples: 92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
Antimony, Dissolved mg/L ND 0.015 10/05/23 10:340.0055
Arsenic, Dissolved mg/L ND 0.010 10/05/23 10:340.0034
Barium, Dissolved mg/L ND 0.010 10/05/23 10:340.00084
Beryllium, Dissolved mg/L ND 0.0040 10/05/23 10:340.00017
Boron, Dissolved mg/L ND 0.050 10/05/23 10:340.012
Cadmium, Dissolved mg/L ND 0.0010 10/05/23 10:340.00033
Chromium, Dissolved mg/L ND 0.0050 10/05/23 10:340.0017
Cobalt, Dissolved mg/L ND 0.010 10/05/23 10:340.00096
Copper, Dissolved mg/L ND 0.0050 10/05/23 10:340.0026
Lead, Dissolved mg/L ND 0.010 10/05/23 10:340.0021
Manganese, Dissolved mg/L ND 0.0050 10/05/23 10:340.0011
Nickel, Dissolved mg/L ND 0.0050 10/05/23 10:340.0010
Selenium, Dissolved mg/L ND 0.015 10/05/23 10:340.0039
Silver, Dissolved mg/L ND 0.0050 10/05/23 10:340.0010
Thallium, Dissolved mg/L ND 0.015 10/05/23 10:340.0029
Vanadium, Dissolved mg/L ND 0.010 10/05/23 10:340.0010
Zinc, Dissolved mg/L ND 0.020 10/05/23 10:340.011
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5249436LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved mg/L 0.260.25 103 80-120
Arsenic, Dissolved mg/L 0.250.25 98 80-120
Barium, Dissolved mg/L 0.250.25 100 80-120
Beryllium, Dissolved mg/L 0.0250.025 99 80-120
Boron, Dissolved mg/L 1.21.2 99 80-120
Cadmium, Dissolved mg/L 0.0260.025 104 80-120
Chromium, Dissolved mg/L 0.250.25 101 80-120
Cobalt, Dissolved mg/L 0.260.25 102 80-120
Copper, Dissolved mg/L 0.250.25 98 80-120
Lead, Dissolved mg/L 0.260.25 103 80-120
Manganese, Dissolved mg/L 0.250.25 101 80-120
Nickel, Dissolved mg/L 0.260.25 104 80-120
Selenium, Dissolved mg/L 0.260.25 103 80-120
Silver, Dissolved mg/L 0.0250.025 101 80-120
Thallium, Dissolved mg/L 0.260.25 104 80-120
Vanadium, Dissolved mg/L 0.250.25 100 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5249436LABORATORY CONTROL SAMPLE:
LCSSpike
Zinc, Dissolved mg/L 1.31.2 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5249437MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5249438
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved mg/L 0.25 103 75-125103 1 200.25ND 0.26 0.26
Arsenic, Dissolved mg/L 0.25 100 75-12598 2 200.25ND 0.25 0.25
Barium, Dissolved mg/L 0.25 101 75-125101 0 200.2543.0 ug/L 0.30 0.29
Beryllium, Dissolved mg/L 0.025 99 75-12599 0 200.025ND 0.025 0.025
Boron, Dissolved mg/L 1.2 101 75-125100 0 201.256.2 ug/L 1.3 1.3
Cadmium, Dissolved mg/L 0.025 103 75-125103 0 200.025ND 0.026 0.026
Chromium, Dissolved mg/L 0.25 100 75-125100 0 200.25ND 0.25 0.25
Cobalt, Dissolved mg/L 0.25 103 75-125103 0 200.25ND 0.26 0.26
Copper, Dissolved mg/L 0.25 100 75-125100 0 200.25ND 0.25 0.25
Lead, Dissolved mg/L 0.25 102 75-125101 0 200.25ND 0.25 0.25
Manganese, Dissolved mg/L 0.25 101 75-125100 0 200.252.3J ug/L 0.25 0.25
Nickel, Dissolved mg/L 0.25 105 75-125104 0 200.25ND 0.26 0.26
Selenium, Dissolved mg/L 0.25 101 75-125100 0 200.25ND 0.25 0.25
Silver, Dissolved mg/L 0.025 101 75-125101 0 200.025ND 0.026 0.026
Thallium, Dissolved mg/L 0.25 102 75-125101 1 200.25ND 0.26 0.25
Vanadium, Dissolved mg/L 0.25 102 75-125101 0 200.25ND 0.25 0.25
Zinc, Dissolved mg/L 1.2 103 75-125103 0 201.2ND 1.3 1.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800499
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688280012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4146342
Associated Lab Samples:92688280012
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/19/23 17:560.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/19/23 17:560.22
1,1,2-Trichloroethane ug/L ND 1.0 09/19/23 17:560.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/19/23 17:560.32
1,1-Dichloroethane ug/L ND 1.0 09/19/23 17:560.37
1,1-Dichloroethene ug/L ND 1.0 09/19/23 17:560.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/19/23 17:560.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/19/23 17:560.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/19/23 17:560.27
1,2-Dichlorobenzene ug/L ND 1.0 09/19/23 17:560.34
1,2-Dichloroethane ug/L ND 1.0 09/19/23 17:560.32
1,2-Dichloropropane ug/L ND 1.0 09/19/23 17:560.36
1,3-Dichlorobenzene ug/L ND 1.0 09/19/23 17:560.34
1,4-Dichlorobenzene ug/L ND 1.0 09/19/23 17:560.33
2-Butanone (MEK)ug/L ND 5.0 09/19/23 17:564.0
2-Hexanone ug/L ND 5.0 09/19/23 17:560.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/19/23 17:562.7
Acetone ug/L ND 25.0 09/19/23 17:565.1
Benzene ug/L ND 1.0 09/19/23 17:560.34
Bromodichloromethane ug/L ND 1.0 09/19/23 17:560.31
Bromoform ug/L ND 1.0 09/19/23 17:560.34
Bromomethane ug/L ND 2.0 09/19/23 17:561.7
Carbon disulfide ug/L ND 2.0 09/19/23 17:560.36
Carbon tetrachloride ug/L ND 1.0 09/19/23 17:560.33
Chlorobenzene ug/L ND 1.0 09/19/23 17:560.28
Chloroethane ug/L ND 1.0 09/19/23 17:560.65
Chloroform ug/L ND 1.0 09/19/23 17:560.43
Chloromethane ug/L ND 1.0 09/19/23 17:560.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/19/23 17:560.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/19/23 17:560.36
Cyclohexane ug/L ND 1.0 09/19/23 17:560.35
Dibromochloromethane ug/L ND 1.0 09/19/23 17:560.36
Dichlorodifluoromethane ug/L ND 1.0 09/19/23 17:560.35
Ethylbenzene ug/L ND 1.0 09/19/23 17:560.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/19/23 17:560.33
m&p-Xylene ug/L ND 2.0 09/19/23 17:560.71
Methyl acetate ug/L ND 10.0 09/19/23 17:562.4
Methyl-tert-butyl ether ug/L ND 1.0 09/19/23 17:560.42
Methylcyclohexane ug/L ND 10.0 09/19/23 17:561.5
Methylene Chloride ug/L ND 5.0 09/19/23 17:562.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4146342
Associated Lab Samples:92688280012
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/19/23 17:560.34
Styrene ug/L ND 1.0 09/19/23 17:560.29
Tetrachloroethene ug/L ND 1.0 09/19/23 17:560.29
Toluene ug/L ND 1.0 09/19/23 17:560.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/19/23 17:560.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/19/23 17:560.36
Trichloroethene ug/L ND 1.0 09/19/23 17:560.38
Trichlorofluoromethane ug/L ND 1.0 09/19/23 17:560.30
Vinyl chloride ug/L ND 1.0 09/19/23 17:560.39
1,2-Dichloroethane-d4 (S)%93 70-130 09/19/23 17:56
4-Bromofluorobenzene (S)%97 70-130 09/19/23 17:56
Toluene-d8 (S)%99 70-130 09/19/23 17:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4146343LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.320 102 70-130
1,1,2,2-Tetrachloroethane ug/L 21.020 105 70-130
1,1,2-Trichloroethane ug/L 20.420 102 70-130
1,1,2-Trichlorotrifluoroethane ug/L 22.120 111 70-132
1,1-Dichloroethane ug/L 21.320 107 70-130
1,1-Dichloroethene ug/L 22.620 113 69-131
1,2,4-Trichlorobenzene ug/L 19.920 99 70-130
1,2-Dibromo-3-chloropropane ug/L 19.920 100 70-130
1,2-Dibromoethane (EDB)ug/L 20.620 103 70-130
1,2-Dichlorobenzene ug/L 20.620 103 70-130
1,2-Dichloroethane ug/L 19.820 99 70-130
1,2-Dichloropropane ug/L 21.720 109 70-130
1,3-Dichlorobenzene ug/L 21.120 105 70-130
1,4-Dichlorobenzene ug/L 20.620 103 70-130
2-Butanone (MEK)ug/L 39.840 99 67-133
2-Hexanone ug/L 41.240 103 70-133
4-Methyl-2-pentanone (MIBK)ug/L 40.440 101 70-130
Acetone ug/L 40.640 102 67-130
Benzene ug/L 21.320 106 70-130
Bromodichloromethane ug/L 20.320 102 70-130
Bromoform ug/L 18.620 93 70-133
Bromomethane ug/L 19.120 96 41-148
Carbon disulfide ug/L 22.220 111 70-131
Carbon tetrachloride ug/L 21.220 106 70-130
Chlorobenzene ug/L 20.720 104 70-130
Chloroethane ug/L 20.620 103 41-157
Chloroform ug/L 20.320 102 70-130
Chloromethane ug/L 18.420 92 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4146343LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 20.620 103 70-130
cis-1,3-Dichloropropene ug/L 20.620 103 70-130
Cyclohexane ug/L 22.520 113 63-137
Dibromochloromethane ug/L 20.020 100 70-130
Dichlorodifluoromethane ug/L 22.020 110 54-147
Ethylbenzene ug/L 20.620 103 70-130
Isopropylbenzene (Cumene)ug/L 21.020 105 70-130
m&p-Xylene ug/L 41.240 103 70-130
Methyl acetate ug/L 20.520 103 70-130
Methyl-tert-butyl ether ug/L 19.520 97 70-130
Methylcyclohexane ug/L 25.020 125 70-130
Methylene Chloride ug/L 21.520 107 62-130
o-Xylene ug/L 20.120 100 70-130
Styrene ug/L 21.120 105 70-130
Tetrachloroethene ug/L 21.120 106 70-130
Toluene ug/L 20.720 103 70-130
trans-1,2-Dichloroethene ug/L 20.920 104 70-130
trans-1,3-Dichloropropene ug/L 19.920 100 70-130
Trichloroethene ug/L 20.920 104 70-130
Trichlorofluoromethane ug/L 19.320 97 57-130
Vinyl chloride ug/L 17.320 87 66-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4146344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688511001
4146345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 117 70-150117 0 3020ND23.4 23.4
1,1,2,2-Tetrachloroethane ug/L 20 118 66-144115 2 3020ND23.6 23.1
1,1,2-Trichloroethane ug/L 20 116 70-142115 1 3020ND23.2 23.0
1,1,2-Trichlorotrifluoroethane ug/L 20 133 66-168127 5 3020ND26.7 25.4
1,1-Dichloroethane ug/L 20 122 68-150120 2 3020ND24.5 24.0
1,1-Dichloroethene ug/L 20 134 64-162131 2 3020ND26.8 26.3
1,2,4-Trichlorobenzene ug/L 20 107 69-147108 1 3020ND21.5 21.6
1,2-Dibromo-3-chloropropane ug/L 20 103 62-146100 3 3020ND20.6 19.9
1,2-Dibromoethane (EDB) ug/L 20 113 70-143113 0 3020ND22.7 22.6
1,2-Dichlorobenzene ug/L 20 113 70-142111 2 3020ND22.7 22.3
1,2-Dichloroethane ug/L 20 111 68-145110 1 3020ND22.1 21.9
1,2-Dichloropropane ug/L 20 121 70-144118 3 3020ND24.3 23.6
1,3-Dichlorobenzene ug/L 20 118 70-142113 4 3020ND23.6 22.7
1,4-Dichlorobenzene ug/L 20 116 70-140111 4 3020ND23.2 22.3
2-Butanone (MEK)ug/L 40 110 57-156116 5 3040ND44.2 46.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4146344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688511001
4146345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 116 62-153117 0 3040ND46.5 46.6
4-Methyl-2-pentanone(MIBK)ug/L 40 113 65-144112 1 3040ND45.4 44.9
Acetone ug/L 40 112 49-162117 4 3040ND44.8 46.8
Benzene ug/L 20 122 68-144119 3 3020ND24.5 23.7
Bromodichloromethane ug/L 20 110 70-141108 2 3020ND22.1 21.6
Bromoform ug/L 20 100 59-14497 3 3020ND20.0 19.3
Bromomethane ug/L 20 112 23-190118 6 3020ND22.4 23.7
Carbon disulfide ug/L 20 130 64-160127 3 3020ND26.1 25.4
Carbon tetrachloride ug/L 20 122 70-147119 2 3020ND24.5 23.9
Chlorobenzene ug/L 20 121 70-143115 6 3020ND24.3 23.0
Chloroethane ug/L 20 115 55-190114 1 3020ND23.0 22.8
Chloroform ug/L 20 110 67-148112 2 3020ND22.1 22.4
Chloromethane ug/L 20 104 38-180105 2 3020ND20.7 21.1
cis-1,2-Dichloroethene ug/L 20 118 67-151118 0 3020ND23.6 23.6
cis-1,3-Dichloropropene ug/L 20 114 70-142111 3 3020ND22.7 22.2
Cyclohexane ug/L 20 131 64-162131 0 3020ND26.3 26.2
Dibromochloromethane ug/L 20 113 68-140106 6 3020ND22.6 21.2
Dichlorodifluoromethane ug/L 20 128 15-200126 2 3020ND25.6 25.1
Ethylbenzene ug/L 20 121 70-145116 5 3020ND24.3 23.1
Isopropylbenzene(Cumene)ug/L 20 125 70-144119 5 3020ND25.0 23.9
m&p-Xylene ug/L 40 121 70-148116 4 3040ND48.4 46.4
Methyl acetate ug/L 20 111 62-144112 1 3020ND22.2 22.4
Methyl-tert-butyl ether ug/L 20 109 64-146109 0 3020ND21.8 21.8
Methylcyclohexane ug/L 20 143 70-155136 5 3020ND28.6 27.3
Methylene Chloride ug/L 20 119 54-149117 1 3020ND25.0 24.7
o-Xylene ug/L 20 116 70-145112 4 3020ND23.2 22.4
Styrene ug/L 20 119 70-147115 4 3020ND23.9 23.0
Tetrachloroethene ug/L 20 118 70-145113 4 3020ND23.5 22.6
Toluene ug/L 20 118 65-146116 2 3020ND23.6 23.1
trans-1,2-Dichloroethene ug/L 20 124 69-155124 0 3020ND24.9 24.8
trans-1,3-Dichloropropene ug/L 20 112 70-142109 3 3020ND22.4 21.7
Trichloroethene ug/L 20 119 70-152116 3 3020ND23.8 23.2
Trichlorofluoromethane ug/L 20 115 60-158113 1 3020ND22.9 22.6
Vinyl chloride ug/L v32010451-178103 0 3020ND20.7 20.7
1,2-Dichloroethane-d4 (S) %89 70-13095
4-Bromofluorobenzene (S) %101 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801146
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688280009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4149670
Associated Lab Samples:92688280009
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/22/23 00:200.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/22/23 00:200.22
1,1,2-Trichloroethane ug/L ND 1.0 09/22/23 00:200.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/22/23 00:200.32
1,1-Dichloroethane ug/L ND 1.0 09/22/23 00:200.37
1,1-Dichloroethene ug/L ND 1.0 09/22/23 00:200.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/22/23 00:200.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/22/23 00:200.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/22/23 00:200.27
1,2-Dichlorobenzene ug/L ND 1.0 09/22/23 00:200.34
1,2-Dichloroethane ug/L ND 1.0 09/22/23 00:200.32
1,2-Dichloropropane ug/L ND 1.0 09/22/23 00:200.36
1,3-Dichlorobenzene ug/L ND 1.0 09/22/23 00:200.34
1,4-Dichlorobenzene ug/L ND 1.0 09/22/23 00:200.33
2-Butanone (MEK)ug/L ND 5.0 09/22/23 00:204.0
2-Hexanone ug/L ND 5.0 09/22/23 00:200.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/22/23 00:202.7
Acetone ug/L ND 25.0 09/22/23 00:205.1
Benzene ug/L ND 1.0 09/22/23 00:200.34
Bromodichloromethane ug/L ND 1.0 09/22/23 00:200.31
Bromoform ug/L ND 1.0 09/22/23 00:200.34
Bromomethane ug/L ND 2.0 09/22/23 00:201.7
Carbon disulfide ug/L ND 2.0 09/22/23 00:200.36
Carbon tetrachloride ug/L ND 1.0 09/22/23 00:200.33
Chlorobenzene ug/L ND 1.0 09/22/23 00:200.28
Chloroethane ug/L ND 1.0 09/22/23 00:200.65
Chloroform ug/L ND 1.0 09/22/23 00:200.43
Chloromethane ug/L ND 1.0 09/22/23 00:200.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/22/23 00:200.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/22/23 00:200.36
Cyclohexane ug/L ND 1.0 09/22/23 00:200.35
Dibromochloromethane ug/L ND 1.0 09/22/23 00:200.36
Dichlorodifluoromethane ug/L ND 1.0 09/22/23 00:200.35
Ethylbenzene ug/L ND 1.0 09/22/23 00:200.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/22/23 00:200.33
m&p-Xylene ug/L ND 2.0 09/22/23 00:200.71
Methyl acetate ug/L ND 10.0 09/22/23 00:202.4
Methyl-tert-butyl ether ug/L ND 1.0 09/22/23 00:200.42
Methylcyclohexane ug/L ND 10.0 09/22/23 00:201.5
Methylene Chloride ug/L ND 5.0 09/22/23 00:202.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4149670
Associated Lab Samples:92688280009
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/22/23 00:200.34
Styrene ug/L ND 1.0 09/22/23 00:200.29
Tetrachloroethene ug/L ND 1.0 09/22/23 00:200.29
Toluene ug/L ND 1.0 09/22/23 00:200.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/22/23 00:200.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/22/23 00:200.36
Trichloroethene ug/L ND 1.0 09/22/23 00:200.38
Trichlorofluoromethane ug/L ND 1.0 09/22/23 00:200.30
Vinyl chloride ug/L ND 1.0 09/22/23 00:200.39
1,2-Dichloroethane-d4 (S)%98 70-130 09/22/23 00:20
4-Bromofluorobenzene (S)%97 70-130 09/22/23 00:20
Toluene-d8 (S)%100 70-130 09/22/23 00:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4149671LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.220 96 70-130
1,1,2,2-Tetrachloroethane ug/L 21.520 108 70-130
1,1,2-Trichloroethane ug/L 21.120 106 70-130
1,1,2-Trichlorotrifluoroethane ug/L 17.920 90 70-132
1,1-Dichloroethane ug/L 19.720 99 70-130
1,1-Dichloroethene ug/L 20.720 104 69-131
1,2,4-Trichlorobenzene ug/L 19.920 99 70-130
1,2-Dibromo-3-chloropropane ug/L 18.320 91 70-130
1,2-Dibromoethane (EDB)ug/L 21.020 105 70-130
1,2-Dichlorobenzene ug/L 20.720 104 70-130
1,2-Dichloroethane ug/L 19.520 98 70-130
1,2-Dichloropropane ug/L 20.020 100 70-130
1,3-Dichlorobenzene ug/L 20.520 103 70-130
1,4-Dichlorobenzene ug/L 20.220 101 70-130
2-Butanone (MEK)ug/L 41.540 104 67-133
2-Hexanone ug/L 43.740 109 70-133
4-Methyl-2-pentanone (MIBK)ug/L 42.940 107 70-130
Acetone ug/L 40.640 101 67-130
Benzene ug/L 19.820 99 70-130
Bromodichloromethane ug/L 19.120 95 70-130
Bromoform ug/L 17.720 89 70-133
Bromomethane ug/L 19.520 98 41-148
Carbon disulfide ug/L 21.320 106 70-131
Carbon tetrachloride ug/L 19.420 97 70-130
Chlorobenzene ug/L 20.420 102 70-130
Chloroethane ug/L 19.620 98 41-157
Chloroform ug/L 19.720 98 70-130
Chloromethane ug/L 18.220 91 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4149671LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 20.220 101 70-130
cis-1,3-Dichloropropene ug/L 20.220 101 70-130
Cyclohexane ug/L 18.520 92 63-137
Dibromochloromethane ug/L 20.620 103 70-130
Dichlorodifluoromethane ug/L 18.320 91 54-147
Ethylbenzene ug/L 20.020 100 70-130
Isopropylbenzene (Cumene)ug/L 20.820 104 70-130
m&p-Xylene ug/L 40.540 101 70-130
Methyl acetate ug/L 19.220 96 70-130
Methyl-tert-butyl ether ug/L 19.220 96 70-130
Methylcyclohexane ug/L 18.620 93 70-130
Methylene Chloride ug/L 19.920 100 62-130
o-Xylene ug/L 20.120 101 70-130
Styrene ug/L 20.920 104 70-130
Tetrachloroethene ug/L 18.320 91 70-130
Toluene ug/L 19.720 99 70-130
trans-1,2-Dichloroethene ug/L 20.620 103 70-130
trans-1,3-Dichloropropene ug/L 19.820 99 70-130
Trichloroethene ug/L 20.020 100 70-130
Trichlorofluoromethane ug/L 17.420 87 57-130
Vinyl chloride ug/L 16.820 84 66-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4149672MATRIX SPIKE SAMPLE:
MSSpike
Result
92688803001
1,1,1-Trichloroethane ug/L 20.720 103 70-150ND
1,1,2,2-Tetrachloroethane ug/L 18.720 93 66-144ND
1,1,2-Trichloroethane ug/L 18.920 94 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 23.120 111 66-168ND
1,1-Dichloroethane ug/L 44.520 104 68-15023.6
1,1-Dichloroethene ug/L 52.820 118 64-16229.3
1,2,4-Trichlorobenzene ug/L 18.920 94 69-147ND
1,2-Dibromo-3-chloropropane ug/L 16.220 81 62-146ND
1,2-Dibromoethane (EDB)ug/L 18.120 91 70-143ND
1,2-Dichlorobenzene ug/L 18.720 94 70-142ND
1,2-Dichloroethane ug/L 19.120 95 68-145ND
1,2-Dichloropropane ug/L 19.220 96 70-144ND
1,3-Dichlorobenzene ug/L 18.720 93 70-142ND
1,4-Dichlorobenzene ug/L 18.720 93 70-140ND
2-Butanone (MEK)ug/L 36.940 92 57-156ND
2-Hexanone ug/L 36.840 92 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 37.440 94 65-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4149672MATRIX SPIKE SAMPLE:
MSSpike
Result
92688803001
Acetone ug/L 34.940 87 49-162ND
Benzene ug/L 19.520 98 68-144ND
Bromodichloromethane ug/L 19.020 95 70-141ND
Bromoform ug/L 15.920 80 59-144ND
Bromomethane ug/L 19.720 98 23-190ND
Carbon disulfide ug/L 22.520 113 64-160ND
Carbon tetrachloride ug/L 20.820 104 70-147ND
Chlorobenzene ug/L 18.920 95 70-143ND
Chloroethane ug/L 19.720 98 55-190ND
Chloroform ug/L 19.720 98 67-148ND
Chloromethane ug/L 19.320 96 38-180ND
cis-1,2-Dichloroethene ug/L 96.120 111 67-15173.9
cis-1,3-Dichloropropene ug/L 18.920 95 70-142ND
Cyclohexane ug/L 21.520 108 64-162ND
Dibromochloromethane ug/L 18.620 93 68-140ND
Dichlorodifluoromethane ug/L 23.720 119 15-200ND
Ethylbenzene ug/L 18.620 93 70-145ND
Isopropylbenzene (Cumene)ug/L 19.520 98 70-144ND
m&p-Xylene ug/L 37.440 93 70-148ND
Methyl acetate ug/L 16.920 84 62-144ND
Methyl-tert-butyl ether ug/L 18.120 90 64-146ND
Methylcyclohexane ug/L 22.120 111 70-155ND
Methylene Chloride ug/L 20.220 101 54-149ND
o-Xylene ug/L 18.520 92 70-145ND
Styrene ug/L 18.920 95 70-147ND
Tetrachloroethene ug/L 28.520 94 70-1459.6
Toluene ug/L 18.820 94 65-146ND
trans-1,2-Dichloroethene ug/L 22.320 108 69-155ND
trans-1,3-Dichloropropene ug/L 19.020 95 70-142ND
Trichloroethene ug/L 10420 113 70-15281.7
Trichlorofluoromethane ug/L 20.720 103 60-158ND
Vinyl chloride ug/L 28.420 93 51-1789.8
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688803002
4149673SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L 0.99J 301.1
1,1-Dichloroethane ug/L 19.1 3 3019.6
1,1-Dichloroethene ug/L 50.0 0 3050.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688803002
4149673SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 63.0 2 3064.4
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 7.8 0 307.9
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L 1.0 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L 163 3 30167
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L 6.8 1 306.9
1,2-Dichloroethane-d4 (S)%103100
4-Bromofluorobenzene (S)%9798
Toluene-d8 (S)%9998
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801460
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688280005, 92688280006, 92688280007, 92688280008, 92688280010, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4151417
Associated Lab Samples:92688280005, 92688280006, 92688280007, 92688280008, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/22/23 12:010.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/22/23 12:010.22
1,1,2-Trichloroethane ug/L ND 1.0 09/22/23 12:010.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/22/23 12:010.32
1,1-Dichloroethane ug/L ND 1.0 09/22/23 12:010.37
1,1-Dichloroethene ug/L ND 1.0 09/22/23 12:010.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/22/23 12:010.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/22/23 12:010.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/22/23 12:010.27
1,2-Dichlorobenzene ug/L ND 1.0 09/22/23 12:010.34
1,2-Dichloroethane ug/L ND 1.0 09/22/23 12:010.32
1,2-Dichloropropane ug/L ND 1.0 09/22/23 12:010.36
1,3-Dichlorobenzene ug/L ND 1.0 09/22/23 12:010.34
1,4-Dichlorobenzene ug/L ND 1.0 09/22/23 12:010.33
2-Butanone (MEK)ug/L ND 5.0 09/22/23 12:014.0
2-Hexanone ug/L ND 5.0 09/22/23 12:010.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/22/23 12:012.7
Acetone ug/L ND 25.0 09/22/23 12:015.1
Benzene ug/L ND 1.0 09/22/23 12:010.34
Bromodichloromethane ug/L ND 1.0 09/22/23 12:010.31
Bromoform ug/L ND 1.0 09/22/23 12:010.34
Bromomethane ug/L ND 2.0 09/22/23 12:011.7
Carbon disulfide ug/L ND 2.0 09/22/23 12:010.36
Carbon tetrachloride ug/L ND 1.0 09/22/23 12:010.33
Chlorobenzene ug/L ND 1.0 09/22/23 12:010.28
Chloroethane ug/L ND 1.0 09/22/23 12:010.65
Chloroform ug/L ND 1.0 09/22/23 12:010.43
Chloromethane ug/L ND 1.0 09/22/23 12:010.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/22/23 12:010.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/22/23 12:010.36
Cyclohexane ug/L ND 1.0 09/22/23 12:010.35
Dibromochloromethane ug/L ND 1.0 09/22/23 12:010.36
Dichlorodifluoromethane ug/L ND 1.0 09/22/23 12:010.35
Ethylbenzene ug/L ND 1.0 09/22/23 12:010.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/22/23 12:010.33
m&p-Xylene ug/L ND 2.0 09/22/23 12:010.71
Methyl acetate ug/L ND 10.0 09/22/23 12:012.4
Methyl-tert-butyl ether ug/L ND 1.0 09/22/23 12:010.42
Methylcyclohexane ug/L ND 10.0 09/22/23 12:011.5
Methylene Chloride ug/L ND 5.0 09/22/23 12:012.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
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Page 85 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4151417
Associated Lab Samples:92688280005, 92688280006, 92688280007, 92688280008, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/22/23 12:010.34
Styrene ug/L ND 1.0 09/22/23 12:010.29
Tetrachloroethene ug/L ND 1.0 09/22/23 12:010.29
Toluene ug/L ND 1.0 09/22/23 12:010.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/22/23 12:010.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/22/23 12:010.36
Trichloroethene ug/L ND 1.0 09/22/23 12:010.38
Trichlorofluoromethane ug/L ND 1.0 09/22/23 12:010.30
Vinyl chloride ug/L ND 1.0 09/22/23 12:010.39
1,2-Dichloroethane-d4 (S)%95 70-130 09/22/23 12:01
4-Bromofluorobenzene (S)%96 70-130 09/22/23 12:01
Toluene-d8 (S)%98 70-130 09/22/23 12:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4151418LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.620 98 70-130
1,1,2,2-Tetrachloroethane ug/L 20.420 102 70-130
1,1,2-Trichloroethane ug/L 20.320 101 70-130
1,1,2-Trichlorotrifluoroethane ug/L 22.020 110 70-132
1,1-Dichloroethane ug/L 20.320 101 70-130
1,1-Dichloroethene ug/L 21.920 110 69-131
1,2,4-Trichlorobenzene ug/L 17.620 88 70-130
1,2-Dibromo-3-chloropropane ug/L 17.020 85 70-130
1,2-Dibromoethane (EDB)ug/L 19.920 99 70-130
1,2-Dichlorobenzene ug/L 19.520 97 70-130
1,2-Dichloroethane ug/L 19.620 98 70-130
1,2-Dichloropropane ug/L 20.520 102 70-130
1,3-Dichlorobenzene ug/L 19.820 99 70-130
1,4-Dichlorobenzene ug/L 19.620 98 70-130
2-Butanone (MEK)ug/L 38.340 96 67-133
2-Hexanone ug/L 40.140 100 70-133
4-Methyl-2-pentanone (MIBK)ug/L 39.540 99 70-130
Acetone ug/L 38.340 96 67-130
Benzene ug/L 20.420 102 70-130
Bromodichloromethane ug/L 19.020 95 70-130
Bromoform ug/L 17.120 86 70-133
Bromomethane ug/L 22.220 111 41-148
Carbon disulfide ug/L 22.120 110 70-131
Carbon tetrachloride ug/L 19.820 99 70-130
Chlorobenzene ug/L 20.420 102 70-130
Chloroethane ug/L 19.820 99 41-157
Chloroform ug/L 19.320 97 70-130
Chloromethane ug/L 17.520 88 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4151418LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 20.520 102 70-130
cis-1,3-Dichloropropene ug/L 19.320 96 70-130
Cyclohexane ug/L 21.920 109 63-137
Dibromochloromethane ug/L 19.220 96 70-130
Dichlorodifluoromethane ug/L 21.420 107 54-147
Ethylbenzene ug/L 20.020 100 70-130
Isopropylbenzene (Cumene)ug/L 20.320 102 70-130
m&p-Xylene ug/L 40.140 100 70-130
Methyl acetate ug/L 19.820 99 70-130
Methyl-tert-butyl ether ug/L 18.420 92 70-130
Methylcyclohexane ug/L 23.720 119 70-130
Methylene Chloride ug/L 20.820 104 62-130
o-Xylene ug/L 19.520 98 70-130
Styrene ug/L 20.320 102 70-130
Tetrachloroethene ug/L 19.220 96 70-130
Toluene ug/L 19.920 99 70-130
trans-1,2-Dichloroethene ug/L 20.920 105 70-130
trans-1,3-Dichloropropene ug/L 18.820 94 70-130
Trichloroethene ug/L 20.020 100 70-130
Trichlorofluoromethane ug/L 18.620 93 57-130
Vinyl chloride ug/L 16.620 83 66-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4151419MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4151420
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 115 70-150129 11 3020ND23.0 25.7
1,1,2,2-Tetrachloroethane ug/L 20 115 66-144124 7 3020ND23.0 24.7
1,1,2-Trichloroethane ug/L 20 112 70-142122 8 3020ND22.4 24.3
1,1,2-Trichlorotrifluoroethane ug/L 20 122 66-168131 7 3020ND24.3 26.2
1,1-Dichloroethane ug/L 20 118 68-150133 11 3020ND23.7 26.5
1,1-Dichloroethene ug/L 20 134 64-162149 11 3020ND26.8 29.8
1,2,4-Trichlorobenzene ug/L 20 102 69-147109 7 3020ND20.3 21.8
1,2-Dibromo-3-chloropropane ug/L 20 99 62-146111 11 3020ND19.9 22.2
1,2-Dibromoethane (EDB) ug/L 20 108 70-143119 9 3020ND21.7 23.8
1,2-Dichlorobenzene ug/L 20 104 70-142111 6 3020ND20.8 22.2
1,2-Dichloroethane ug/L 20 112 68-145124 10 3020ND22.4 24.8
1,2-Dichloropropane ug/L 20 118 70-144127 8 3020ND23.6 25.5
1,3-Dichlorobenzene ug/L 20 104 70-142112 7 3020ND20.8 22.3
1,4-Dichlorobenzene ug/L 20 102 70-140110 8 3020ND20.5 22.1
2-Butanone (MEK)ug/L 40 121 57-156136 11 3040ND51.2 57.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4151419MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4151420
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 123 62-153138 11 3040ND49.1 55.0
4-Methyl-2-pentanone(MIBK)ug/L 40 121 65-144133 9 30403.3J 51.7 56.5
Acetone ug/L 40 121 49-162133 7 304016.0J 64.6 69.3
Benzene ug/L 20 116 68-144123 6 30200.49J 23.8 25.2
Bromodichloromethane ug/L 20 110 70-141117 6 3020ND22.0 23.5
Bromoform ug/L 20 94 59-144102 8 3020ND18.8 20.4
Bromomethane ug/L 20 98 23-190113 14 3020ND19.6 22.6
Carbon disulfide ug/L 20 126 64-160145 14 3020ND25.1 28.9
Carbon tetrachloride ug/L 20 118 70-147123 4 3020ND23.7 24.6
Chlorobenzene ug/L 20 108 70-143120 10 3020ND21.7 24.0
Chloroethane ug/L 20 112 55-190121 7 3020ND22.4 24.2
Chloroform ug/L 20 111 67-148123 11 3020ND22.2 24.6
Chloromethane ug/L 20 97 38-180108 11 3020ND19.6 21.9
cis-1,2-Dichloroethene ug/L 20 120 67-151130 8 3020ND23.9 26.0
cis-1,3-Dichloropropene ug/L 20 107 70-142114 7 3020ND21.4 22.9
Cyclohexane ug/L 20 126 64-162138 9 3020ND25.3 27.6
Dibromochloromethane ug/L 20 103 68-140114 10 3020ND20.7 22.8
Dichlorodifluoromethane ug/L 20 119 15-200130 9 3020ND23.7 25.9
Ethylbenzene ug/L 20 95 70-145102 3 302021.5 40.5 41.9
Isopropylbenzene(Cumene)ug/L 20 112 70-144122 9 3020ND22.4 24.4
m&p-Xylene ug/L 40 102 70-148111 6 304019.6 60.3 64.2
Methyl acetate ug/L 20 119 62-144124 5 3020ND23.8 24.9
Methyl-tert-butyl ether ug/L 20 106 64-146117 10 3020ND21.3 23.5
Methylcyclohexane ug/L 20 134 70-155142 6 3020ND26.8 28.5
Methylene Chloride ug/L 20 121 54-149136 11 3020ND25.5 28.5
o-Xylene ug/L 20 92 70-14596 2 302024.7 43.1 44.0
Styrene ug/L 20 108 70-147118 9 3020ND21.5 23.6
Tetrachloroethene ug/L 20 104 70-145113 8 3020ND20.8 22.5
Toluene ug/L 20 109 65-146119 8 30200.45J 22.3 24.3
trans-1,2-Dichloroethene ug/L 20 121 69-155139 14 3020ND24.1 27.9
trans-1,3-Dichloropropene ug/L 20 110 70-142115 4 3020ND22.0 22.9
Trichloroethene ug/L 20 113 70-152122 7 3020ND22.6 24.3
Trichlorofluoromethane ug/L 20 111 60-158123 10 3020ND22.1 24.5
Vinyl chloride ug/L 20 97 51-178110 12 3020ND19.5 22.0
1,2-Dichloroethane-d4 (S) %99 70-130100
4-Bromofluorobenzene (S) %99 70-130100
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802052
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688280004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4154511
Associated Lab Samples:92688280004
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/26/23 12:560.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/26/23 12:560.22
1,1,2-Trichloroethane ug/L ND 1.0 09/26/23 12:560.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/26/23 12:560.32
1,1-Dichloroethane ug/L ND 1.0 09/26/23 12:560.37
1,1-Dichloroethene ug/L ND 1.0 09/26/23 12:560.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/26/23 12:560.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/26/23 12:560.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/26/23 12:560.27
1,2-Dichlorobenzene ug/L ND 1.0 09/26/23 12:560.34
1,2-Dichloroethane ug/L ND 1.0 09/26/23 12:560.32
1,2-Dichloropropane ug/L ND 1.0 09/26/23 12:560.36
1,3-Dichlorobenzene ug/L ND 1.0 09/26/23 12:560.34
1,4-Dichlorobenzene ug/L ND 1.0 09/26/23 12:560.33
2-Butanone (MEK)ug/L ND 5.0 09/26/23 12:564.0
2-Hexanone ug/L ND 5.0 09/26/23 12:560.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/26/23 12:562.7
Acetone ug/L ND 25.0 09/26/23 12:565.1
Benzene ug/L ND 1.0 09/26/23 12:560.34
Bromodichloromethane ug/L ND 1.0 09/26/23 12:560.31
Bromoform ug/L ND 1.0 09/26/23 12:560.34
Bromomethane ug/L ND 2.0 v209/26/23 12:561.7
Carbon disulfide ug/L ND 2.0 09/26/23 12:560.36
Carbon tetrachloride ug/L ND 1.0 09/26/23 12:560.33
Chlorobenzene ug/L ND 1.0 09/26/23 12:560.28
Chloroethane ug/L ND 1.0 09/26/23 12:560.65
Chloroform ug/L ND 1.0 09/26/23 12:560.43
Chloromethane ug/L ND 1.0 09/26/23 12:560.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/26/23 12:560.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/26/23 12:560.36
Cyclohexane ug/L ND 1.0 09/26/23 12:560.35
Dibromochloromethane ug/L ND 1.0 09/26/23 12:560.36
Dichlorodifluoromethane ug/L ND 1.0 09/26/23 12:560.35
Ethylbenzene ug/L ND 1.0 09/26/23 12:560.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/26/23 12:560.33
m&p-Xylene ug/L ND 2.0 09/26/23 12:560.71
Methyl acetate ug/L ND 10.0 v209/26/23 12:562.4
Methyl-tert-butyl ether ug/L ND 1.0 09/26/23 12:560.42
Methylcyclohexane ug/L ND 10.0 09/26/23 12:561.5
Methylene Chloride ug/L ND 5.0 09/26/23 12:562.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4154511
Associated Lab Samples:92688280004
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/26/23 12:560.34
Styrene ug/L ND 1.0 09/26/23 12:560.29
Tetrachloroethene ug/L ND 1.0 09/26/23 12:560.29
Toluene ug/L ND 1.0 09/26/23 12:560.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/26/23 12:560.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/26/23 12:560.36
Trichloroethene ug/L ND 1.0 09/26/23 12:560.38
Trichlorofluoromethane ug/L ND 1.0 09/26/23 12:560.30
Vinyl chloride ug/L ND 1.0 09/26/23 12:560.39
1,2-Dichloroethane-d4 (S)%96 70-130 09/26/23 12:56
4-Bromofluorobenzene (S)%101 70-130 09/26/23 12:56
Toluene-d8 (S)%95 70-130 09/26/23 12:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4154512LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.120 96 70-130
1,1,2,2-Tetrachloroethane ug/L 20.320 102 70-130
1,1,2-Trichloroethane ug/L 19.620 98 70-130
1,1,2-Trichlorotrifluoroethane ug/L 21.420 107 70-132
1,1-Dichloroethane ug/L 20.220 101 70-130
1,1-Dichloroethene ug/L 21.120 105 69-131
1,2,4-Trichlorobenzene ug/L 22.020 110 70-130
1,2-Dibromo-3-chloropropane ug/L 18.320 91 70-130
1,2-Dibromoethane (EDB)ug/L 21.520 108 70-130
1,2-Dichlorobenzene ug/L 21.420 107 70-130
1,2-Dichloroethane ug/L 19.620 98 70-130
1,2-Dichloropropane ug/L 19.920 99 70-130
1,3-Dichlorobenzene ug/L 21.620 108 70-130
1,4-Dichlorobenzene ug/L 22.120 111 70-130
2-Butanone (MEK)ug/L 37.540 94 67-133
2-Hexanone ug/L 37.940 95 70-133
4-Methyl-2-pentanone (MIBK)ug/L 37.440 94 70-130
Acetone ug/L 33.840 85 67-130
Benzene ug/L 20.220 101 70-130
Bromodichloromethane ug/L 18.020 90 70-130
Bromoform ug/L 18.720 94 70-133
Bromomethane ug/L 10.8 v32054 41-148
Carbon disulfide ug/L 21.120 105 70-131
Carbon tetrachloride ug/L 19.720 99 70-130
Chlorobenzene ug/L 21.420 107 70-130
Chloroethane ug/L 18.920 94 41-157
Chloroform ug/L 19.120 96 70-130
Chloromethane ug/L 17.220 86 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4154512LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 19.720 99 70-130
cis-1,3-Dichloropropene ug/L 19.320 96 70-130
Cyclohexane ug/L 19.720 98 63-137
Dibromochloromethane ug/L 19.520 98 70-130
Dichlorodifluoromethane ug/L 22.520 113 54-147
Ethylbenzene ug/L 21.220 106 70-130
Isopropylbenzene (Cumene)ug/L 21.620 108 70-130
m&p-Xylene ug/L 42.640 107 70-130
Methyl acetate ug/L 15.9 v32080 70-130
Methyl-tert-butyl ether ug/L 18.120 91 70-130
Methylcyclohexane ug/L 19.920 99 70-130
Methylene Chloride ug/L 18.820 94 62-130
o-Xylene ug/L 20.820 104 70-130
Styrene ug/L 20.920 105 70-130
Tetrachloroethene ug/L 21.020 105 70-130
Toluene ug/L 19.420 97 70-130
trans-1,2-Dichloroethene ug/L 20.320 101 70-130
trans-1,3-Dichloropropene ug/L 19.320 96 70-130
Trichloroethene ug/L 21.220 106 70-130
Trichlorofluoromethane ug/L 20.420 102 57-130
Vinyl chloride ug/L 16.720 84 66-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4154514MATRIX SPIKE SAMPLE:
MSSpike
Result
92689562031
1,1,1-Trichloroethane ug/L 21.720 109 70-150ND
1,1,2,2-Tetrachloroethane ug/L 21.920 110 66-144ND
1,1,2-Trichloroethane ug/L 21.320 106 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 24.5
1,1-Dichloroethane ug/L 22.720 111 68-150ND
1,1-Dichloroethene ug/L 47.420 107 64-16226.1
1,2,4-Trichlorobenzene ug/L 22.720 113 69-147ND
1,2-Dibromo-3-chloropropane ug/L 19.020 95 62-146ND
1,2-Dibromoethane (EDB)ug/L 22.720 114 70-143ND
1,2-Dichlorobenzene ug/L 23.520 118 70-142ND
1,2-Dichloroethane ug/L 21.620 108 68-145ND
1,2-Dichloropropane ug/L 22.320 111 70-144ND
1,3-Dichlorobenzene ug/L 23.720 118 70-142ND
1,4-Dichlorobenzene ug/L 23.620 118 70-140ND
2-Butanone (MEK)ug/L 37.340 93 57-156ND
2-Hexanone ug/L 39.040 97 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 39.140 98 65-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4154514MATRIX SPIKE SAMPLE:
MSSpike
Result
92689562031
Acetone ug/L 34.140 85 49-162ND
Benzene ug/L 23.020 115 68-144ND
Bromodichloromethane ug/L 20.220 101 70-141ND
Bromoform ug/L 19.120 96 59-144ND
Bromomethane ug/L 14.4 v32072 23-190ND
Carbon disulfide ug/L 23.820 119 64-160ND
Carbon tetrachloride ug/L 23.720 118 70-147ND
Chlorobenzene ug/L 24.020 120 70-143ND
Chloroethane ug/L 20.820 104 55-190ND
Chloroform ug/L 21.420 107 67-148ND
Chloromethane ug/L 18.420 92 38-180ND
cis-1,2-Dichloroethene ug/L 54.520 86 67-15137.3
cis-1,3-Dichloropropene ug/L 20.620 103 70-142ND
Cyclohexane ug/L 22.0
Dibromochloromethane ug/L 21.020 105 68-140ND
Dichlorodifluoromethane ug/L 21.820 109 15-200ND
Ethylbenzene ug/L 23.620 118 70-145ND
Isopropylbenzene (Cumene)ug/L 23.7
m&p-Xylene ug/L 47.140 118 70-148ND
Methyl acetate ug/L 16.9
Methyl-tert-butyl ether ug/L 19.220 96 64-146ND
Methylcyclohexane ug/L 21.6
Methylene Chloride ug/L 21.220 106 54-149ND
o-Xylene ug/L 22.820 114 70-145ND
Styrene ug/L 23.020 115 70-147ND
Tetrachloroethene ug/L 25.620 119 70-1451.9
Toluene ug/L 21.920 108 65-146ND
trans-1,2-Dichloroethene ug/L 23.020 115 69-155ND
trans-1,3-Dichloropropene ug/L 21.120 105 70-142ND
Trichloroethene ug/L 29.320 120 70-1525.3
Trichlorofluoromethane ug/L 22.820 114 60-158ND
Vinyl chloride ug/L 45.620 89 51-17827.8
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689562030
4154513SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689562030
4154513SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L 1.2 2 301.3
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 11.8 2 3012.1
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9696
4-Bromofluorobenzene (S)%9799
Toluene-d8 (S)%9496
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802109
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688280001, 92688280002, 92688280003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4154930
Associated Lab Samples:92688280001, 92688280002, 92688280003
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/27/23 22:440.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/27/23 22:440.22
1,1,2-Trichloroethane ug/L ND 1.0 09/27/23 22:440.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/27/23 22:440.32
1,1-Dichloroethane ug/L ND 1.0 09/27/23 22:440.37
1,1-Dichloroethene ug/L ND 1.0 09/27/23 22:440.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/27/23 22:440.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/27/23 22:440.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/27/23 22:440.27
1,2-Dichlorobenzene ug/L ND 1.0 09/27/23 22:440.34
1,2-Dichloroethane ug/L ND 1.0 09/27/23 22:440.32
1,2-Dichloropropane ug/L ND 1.0 09/27/23 22:440.36
1,3-Dichlorobenzene ug/L ND 1.0 09/27/23 22:440.34
1,4-Dichlorobenzene ug/L ND 1.0 09/27/23 22:440.33
2-Butanone (MEK)ug/L ND 5.0 09/27/23 22:444.0
2-Hexanone ug/L ND 5.0 09/27/23 22:440.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/27/23 22:442.7
Acetone ug/L ND 25.0 09/27/23 22:445.1
Benzene ug/L ND 1.0 09/27/23 22:440.34
Bromodichloromethane ug/L ND 1.0 09/27/23 22:440.31
Bromoform ug/L ND 1.0 09/27/23 22:440.34
Bromomethane ug/L ND 2.0 v209/27/23 22:441.7
Carbon disulfide ug/L ND 2.0 09/27/23 22:440.36
Carbon tetrachloride ug/L ND 1.0 09/27/23 22:440.33
Chlorobenzene ug/L ND 1.0 09/27/23 22:440.28
Chloroethane ug/L ND 1.0 09/27/23 22:440.65
Chloroform ug/L ND 1.0 09/27/23 22:440.43
Chloromethane ug/L ND 1.0 09/27/23 22:440.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/27/23 22:440.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/27/23 22:440.36
Cyclohexane ug/L ND 1.0 09/27/23 22:440.35
Dibromochloromethane ug/L ND 1.0 09/27/23 22:440.36
Dichlorodifluoromethane ug/L ND 1.0 09/27/23 22:440.35
Ethylbenzene ug/L ND 1.0 09/27/23 22:440.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/27/23 22:440.33
m&p-Xylene ug/L ND 2.0 09/27/23 22:440.71
Methyl acetate ug/L ND 10.0 v209/27/23 22:442.4
Methyl-tert-butyl ether ug/L ND 1.0 09/27/23 22:440.42
Methylcyclohexane ug/L ND 10.0 09/27/23 22:441.5
Methylene Chloride ug/L ND 5.0 09/27/23 22:442.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4154930
Associated Lab Samples:92688280001, 92688280002, 92688280003
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/27/23 22:440.34
Styrene ug/L ND 1.0 09/27/23 22:440.29
Tetrachloroethene ug/L ND 1.0 09/27/23 22:440.29
Toluene ug/L ND 1.0 09/27/23 22:440.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/27/23 22:440.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/27/23 22:440.36
Trichloroethene ug/L ND 1.0 09/27/23 22:440.38
Trichlorofluoromethane ug/L ND 1.0 09/27/23 22:440.30
Vinyl chloride ug/L ND 1.0 v209/27/23 22:440.39
1,2-Dichloroethane-d4 (S)%90 70-130 09/27/23 22:44
4-Bromofluorobenzene (S)%98 70-130 09/27/23 22:44
Toluene-d8 (S)%99 70-130 09/27/23 22:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4154931LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 17.820 89 70-130
1,1,2,2-Tetrachloroethane ug/L 20.520 102 70-130
1,1,2-Trichloroethane ug/L 19.420 97 70-130
1,1,2-Trichlorotrifluoroethane ug/L 16.620 83 70-132
1,1-Dichloroethane ug/L 18.220 91 70-130
1,1-Dichloroethene ug/L 19.120 95 69-131
1,2,4-Trichlorobenzene ug/L 19.320 97 70-130
1,2-Dibromo-3-chloropropane ug/L 18.020 90 70-130
1,2-Dibromoethane (EDB)ug/L 19.820 99 70-130
1,2-Dichlorobenzene ug/L 19.920 100 70-130
1,2-Dichloroethane ug/L 18.320 91 70-130
1,2-Dichloropropane ug/L 19.920 99 70-130
1,3-Dichlorobenzene ug/L 19.920 100 70-130
1,4-Dichlorobenzene ug/L 19.320 97 70-130
2-Butanone (MEK)ug/L 39.540 99 67-133
2-Hexanone ug/L 42.540 106 70-133
4-Methyl-2-pentanone (MIBK)ug/L 40.240 100 70-130
Acetone ug/L 38.240 96 67-130
Benzene ug/L 18.820 94 70-130
Bromodichloromethane ug/L 18.220 91 70-130
Bromoform ug/L 17.420 87 70-133
Bromomethane ug/L 11.8 v32059 41-148
Carbon disulfide ug/L 18.420 92 70-131
Carbon tetrachloride ug/L 18.920 95 70-130
Chlorobenzene ug/L 20.120 100 70-130
Chloroethane ug/L 15.720 78 41-157
Chloroform ug/L 18.020 90 70-130
Chloromethane ug/L 15.120 75 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4154931LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 17.820 89 70-130
cis-1,3-Dichloropropene ug/L 18.720 94 70-130
Cyclohexane ug/L 16.920 84 63-137
Dibromochloromethane ug/L 18.720 94 70-130
Dichlorodifluoromethane ug/L 16.320 81 54-147
Ethylbenzene ug/L 19.620 98 70-130
Isopropylbenzene (Cumene)ug/L 19.920 99 70-130
m&p-Xylene ug/L 39.240 98 70-130
Methyl acetate ug/L 15.0 v32075 70-130
Methyl-tert-butyl ether ug/L 16.720 83 70-130
Methylcyclohexane ug/L 16.720 83 70-130
Methylene Chloride ug/L 19.820 99 62-130
o-Xylene ug/L 19.220 96 70-130
Styrene ug/L 19.920 100 70-130
Tetrachloroethene ug/L 19.620 98 70-130
Toluene ug/L 19.220 96 70-130
trans-1,2-Dichloroethene ug/L 18.220 91 70-130
trans-1,3-Dichloropropene ug/L 18.520 92 70-130
Trichloroethene ug/L 19.720 98 70-130
Trichlorofluoromethane ug/L 16.520 82 57-130
Vinyl chloride ug/L 15.0 v32075 66-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4154932MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689562011
4154933
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 74 70-15071 3020NDND ND
1,1,2,2-Tetrachloroethane ug/L 20 97 66-144103 3020NDND ND
1,1,2-Trichloroethane ug/L 20 96 70-14278 3020NDND ND
1,1,2-Trichlorotrifluoroethane ug/L M1206966-16862 3020NDND ND
1,1-Dichloroethane ug/L 20 89 68-15090 3020NDND ND
1,1-Dichloroethene ug/L M12014564-162177 3020NDND 35.3J
1,2,4-Trichlorobenzene ug/L 20 78 69-14776 3020NDND ND
1,2-Dibromo-3-chloropropane ug/L M1204462-1460 3020NDND ND
1,2-Dibromoethane (EDB) ug/L M1206670-14393 3020NDND ND
1,2-Dichlorobenzene ug/L 20 93 70-142109 3020NDND ND
1,2-Dichloroethane ug/L 20 96 68-14595 3020NDND ND
1,2-Dichloropropane ug/L 20 80 70-14497 3020NDND ND
1,3-Dichlorobenzene ug/L 20 99 70-142105 3020NDND ND
1,4-Dichlorobenzene ug/L 20 131 70-140115 3020NDND ND
2-Butanone (MEK)ug/L 40 138 57-156121 3040NDND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4154932MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689562011
4154933
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 104 62-153116 3040NDND ND
4-Methyl-2-pentanone(MIBK)ug/L 40 106 65-144109 3040NDND ND
Acetone ug/L M14025649-162262 3040NDND ND
Benzene ug/L 20 107 68-14499 3020NDND ND
Bromodichloromethane ug/L 20 85 70-141124 3020NDND ND
Bromoform ug/L M1204959-14464 3020NDND ND
Bromomethane ug/L v3208523-190103 3020NDND ND
Carbon disulfide ug/L 20 97 64-160102 3020NDND ND
Carbon tetrachloride ug/L M1205270-14733 3020NDND ND
Chlorobenzene ug/L 20 128 70-143115 3020NDND ND
Chloroethane ug/L M12011755-190292 3020NDND ND
Chloroform ug/L 20 87 67-14897 3020NDND ND
Chloromethane ug/L 20 107 38-18080 3020NDND ND
cis-1,2-Dichloroethene ug/L M120-1330 67-151-909 1 302093509080 9170
cis-1,3-Dichloropropene ug/L 20 82 70-14276 3020NDND ND
Cyclohexane ug/L 20 89 64-16278 3020NDND ND
Dibromochloromethane ug/L 20 85 68-14068 3020NDND ND
Dichlorodifluoromethane ug/L 20 60 15-20055 3020NDND ND
Ethylbenzene ug/L 20 142 70-145115 3020NDND ND
Isopropylbenzene(Cumene)ug/L 20 92 70-144104 3020NDND ND
m&p-Xylene ug/L 40 121 70-148119 3040NDND ND
Methyl acetate ug/L M1,v220062-1440 3020NDND ND
Methyl-tert-butyl ether ug/L 20 80 64-14680 3020NDND ND
Methylcyclohexane ug/L M12045770-155461 3020NDND ND
Methylene Chloride ug/L M12031654-149330 3020NDND ND
o-Xylene ug/L 20 113 70-145105 3020NDND ND
Styrene ug/L 20 106 70-14791 3020NDND ND
Tetrachloroethene ug/L 20 126 70-14590 3020NDND ND
Toluene ug/L M1201065-1465 3020ND29.2J 28.2J
trans-1,2-Dichloroethene ug/L M12015169-155162 3020NDND ND
trans-1,3-Dichloropropene ug/L M1207470-14246 3020NDND ND
Trichloroethene ug/L 20 125 70-152135 3020NDND ND
Trichlorofluoromethane ug/L 20 97 60-15887 3020NDND ND
Vinyl chloride ug/L M1,v320-272 51-178-171 2 302012801230 1250
1,2-Dichloroethane-d4 (S) %95 70-13098
4-Bromofluorobenzene (S) %97 70-13097
Toluene-d8 (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801219
EPA 3511
EPA 8015C
8015 Diesel Low Volume
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688280007, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150272
Associated Lab Samples:92688280007, 92688280011
Matrix: Water
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/L ND 0.50 09/22/23 16:270.15
n-Pentacosane (S)%101 29-158 09/22/23 16:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150273LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/L 9.410 94 61-130
n-Pentacosane (S)%107 29-158
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4150274MATRIX SPIKE SAMPLE:
MSSpike
Result
92688280007
Diesel Range Organics(C10-C28)mg/L 11.1 M153.3 19 29-134ND
n-Pentacosane (S)%29 29-158
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688280011
4150275SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/L ND 30ND
n-Pentacosane (S)%6233
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800691
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147310
Associated Lab Samples: 92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/21/23 11:081.2
2,4,5-Trichlorophenol ug/L ND 10.0 09/21/23 11:081.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/21/23 11:081.6
2,4-Dichlorophenol ug/L ND 10.0 09/21/23 11:081.4
2,4-Dimethylphenol ug/L ND 10.0 09/21/23 11:081.7
2,4-Dinitrophenol ug/L ND 50.0 09/21/23 11:0826.0
2,4-Dinitrotoluene ug/L ND 10.0 09/21/23 11:081.6
2,6-Dinitrotoluene ug/L ND 10.0 09/21/23 11:081.7
2-Chloronaphthalene ug/L ND 10.0 09/21/23 11:081.7
2-Chlorophenol ug/L ND 10.0 09/21/23 11:081.2
2-Methylnaphthalene ug/L ND 10.0 09/21/23 11:081.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/21/23 11:081.9
2-Nitroaniline ug/L ND 20.0 09/21/23 11:083.0
2-Nitrophenol ug/L ND 10.0 09/21/23 11:081.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/21/23 11:081.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/21/23 11:088.1
3-Nitroaniline ug/L ND 20.0 09/21/23 11:083.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/21/23 11:087.8
4-Bromophenylphenyl ether ug/L ND 10.0 09/21/23 11:081.8
4-Chloro-3-methylphenol ug/L ND 10.0 09/21/23 11:083.3
4-Chloroaniline ug/L ND 20.0 09/21/23 11:083.6
4-Chlorophenylphenyl ether ug/L ND 10.0 09/21/23 11:082.0
4-Nitroaniline ug/L ND 20.0 09/21/23 11:085.1
4-Nitrophenol ug/L ND 50.0 09/21/23 11:086.6
Acenaphthene ug/L ND 10.0 09/21/23 11:082.0
Acenaphthylene ug/L ND 10.0 09/21/23 11:082.0
Acetophenone ug/L ND 10.0 09/21/23 11:081.5
Anthracene ug/L ND 10.0 09/21/23 11:082.3
Atrazine ug/L ND 10.0 09/21/23 11:083.2
Benzaldehyde ug/L ND 10.0 09/21/23 11:083.6
Benzo(a)anthracene ug/L ND 10.0 09/21/23 11:082.7
Benzo(a)pyrene ug/L ND 10.0 09/21/23 11:082.8
Benzo(b)fluoranthene ug/L ND 10.0 09/21/23 11:082.6
Benzo(g,h,i)perylene ug/L ND 10.0 09/21/23 11:082.8
Benzo(k)fluoranthene ug/L ND 10.0 09/21/23 11:082.7
Biphenyl (Diphenyl)ug/L ND 10.0 09/21/23 11:081.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/21/23 11:081.8
bis(2-Chloroethyl) ether ug/L ND 10.0 09/21/23 11:081.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/21/23 11:083.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147310
Associated Lab Samples: 92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
Butylbenzylphthalate ug/L ND 10.0 09/21/23 11:083.1
Caprolactam ug/L ND 10.0 09/21/23 11:086.9
Carbazole ug/L ND 10.0 09/21/23 11:082.4
Chrysene ug/L ND 10.0 09/21/23 11:082.8
Di-n-butylphthalate ug/L ND 10.0 09/21/23 11:082.2
Di-n-octylphthalate ug/L ND 10.0 09/21/23 11:083.9
Dibenz(a,h)anthracene ug/L ND 10.0 09/21/23 11:083.0
Dibenzofuran ug/L ND 10.0 09/21/23 11:082.1
Diethylphthalate ug/L ND 10.0 09/21/23 11:082.0
Dimethylphthalate ug/L ND 10.0 09/21/23 11:082.1
Fluoranthene ug/L ND 10.0 09/21/23 11:082.2
Fluorene ug/L ND 10.0 09/21/23 11:082.1
Hexachloro-1,3-butadiene ug/L ND 10.0 09/21/23 11:081.8
Hexachlorobenzene ug/L ND 10.0 09/21/23 11:082.2
Hexachlorocyclopentadiene ug/L ND 10.0 09/21/23 11:081.6
Hexachloroethane ug/L ND 10.0 09/21/23 11:081.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/21/23 11:082.9
Isophorone ug/L ND 10.0 09/21/23 11:081.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/21/23 11:081.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/21/23 11:083.0
Naphthalene ug/L ND 10.0 09/21/23 11:082.1
Nitrobenzene ug/L ND 10.0 09/21/23 11:081.9
Pentachlorophenol ug/L ND 20.0 09/21/23 11:083.8
Phenanthrene ug/L ND 10.0 09/21/23 11:082.0
Phenol ug/L ND 10.0 09/21/23 11:081.4
Pyrene ug/L ND 10.0 09/21/23 11:082.2
2,4,6-Tribromophenol (S)%38 10-164 09/21/23 11:08
2-Fluorobiphenyl (S)%88 10-130 09/21/23 11:08
2-Fluorophenol (S)%28 10-130 09/21/23 11:08
Nitrobenzene-d5 (S)%96 10-138 09/21/23 11:08
Phenol-d6 (S)%44 10-130 09/21/23 11:08
Terphenyl-d14 (S)%131 19-191 09/21/23 11:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147311LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 38.5100 38 21-135
2,4,5-Trichlorophenol ug/L 59.6100 60 38-147
2,4,6-Trichlorophenol ug/L 52.5100 53 34-142
2,4-Dichlorophenol ug/L 48.3100 48 36-136
2,4-Dimethylphenol ug/L 47.8100 48 38-134
2,4-Dinitrophenol ug/L 264500 53 10-169
2,4-Dinitrotoluene ug/L 74.7100 75 44-154
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
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Huntersville, NC 28078
[phone]
Page 100 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147311LABORATORY CONTROL SAMPLE:
LCSSpike
2,6-Dinitrotoluene ug/L 62.3100 62 44-156
2-Chloronaphthalene ug/L 44.0100 44 25-130
2-Chlorophenol ug/L 45.4100 45 29-130
2-Methylnaphthalene ug/L 43.6100 44 23-130
2-Methylphenol(o-Cresol)ug/L 41.0100 41 31-130
2-Nitroaniline ug/L 115200 58 39-145
2-Nitrophenol ug/L 49.1100 49 29-142
3&4-Methylphenol(m&p Cresol)ug/L 45.3100 45 30-130
3,3'-Dichlorobenzidine ug/L 200200 100 44-158
3-Nitroaniline ug/L 144200 72 45-152
4,6-Dinitro-2-methylphenol ug/L 147200 74 39-158
4-Bromophenylphenyl ether ug/L 59.1100 59 47-147
4-Chloro-3-methylphenol ug/L 95.0200 47 40-138
4-Chloroaniline ug/L 98.3200 49 35-130
4-Chlorophenylphenyl ether ug/L 53.2100 53 36-139
4-Nitroaniline ug/L 183200 91 46-157
4-Nitrophenol ug/L 219500 44 17-130
Acenaphthene ug/L 46.5100 47 34-135
Acenaphthylene ug/L 46.5100 47 35-137
Acetophenone ug/L 43.4100 43 30-137
Anthracene ug/L 66.2100 66 47-146
Atrazine ug/L 56.950 114 30-130
Benzaldehyde ug/L 36.250 72 17-167
Benzo(a)anthracene ug/L 86.6100 87 48-160
Benzo(a)pyrene ug/L 85.7100 86 47-165
Benzo(b)fluoranthene ug/L 100100 100 49-171
Benzo(g,h,i)perylene ug/L 82.9100 83 46-166
Benzo(k)fluoranthene ug/L 89.9100 90 55-162
Biphenyl (Diphenyl)ug/L 44.8100 45 28-130
bis(2-Chloroethoxy)methane ug/L 44.1100 44 33-136
bis(2-Chloroethyl) ether ug/L 39.8100 40 30-142
bis(2-Ethylhexyl)phthalate ug/L 101100 101 46-173
Butylbenzylphthalate ug/L 93.7100 94 53-169
Caprolactam ug/L 30.650 61 13-130
Carbazole ug/L 81.1100 81 48-157
Chrysene ug/L 80.5100 80 54-152
Di-n-butylphthalate ug/L 84.1100 84 49-161
Di-n-octylphthalate ug/L 94.9100 95 50-166
Dibenz(a,h)anthracene ug/L 82.9100 83 46-166
Dibenzofuran ug/L 46.7100 47 37-136
Diethylphthalate ug/L 72.9100 73 45-149
Dimethylphthalate ug/L 59.7100 60 43-145
Fluoranthene ug/L 80.1100 80 50-153
Fluorene ug/L 51.9100 52 42-142
Hexachloro-1,3-butadiene ug/L 28.6100 29 10-130
Hexachlorobenzene ug/L 59.9100 60 44-138
Hexachlorocyclopentadiene ug/L 42.8100 43 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 101 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147311LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloroethane ug/L 17.0100 17 10-130
Indeno(1,2,3-cd)pyrene ug/L 81.1100 81 46-166
Isophorone ug/L 45.8100 46 36-135
N-Nitroso-di-n-propylamine ug/L 49.2100 49 33-140
N-Nitrosodiphenylamine ug/L 62.2100 62 46-144
Naphthalene ug/L 36.2100 36 20-130
Nitrobenzene ug/L 41.1100 41 33-133
Pentachlorophenol ug/L 150200 75 21-163
Phenanthrene ug/L 65.4100 65 47-146
Phenol ug/L 27.0100 27 19-130
Pyrene ug/L 81.6100 82 53-155
2,4,6-Tribromophenol (S)%130 10-164
2-Fluorobiphenyl (S)%74 10-130
2-Fluorophenol (S)%53 10-130
Nitrobenzene-d5 (S)%74 10-138
Phenol-d6 (S)%45 10-130
Terphenyl-d14 (S)%138 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147312MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4147313
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-chloropropane)ug/L 100 88 11-14374 18 30100ND87.9 73.5
2,4,5-Trichlorophenol ug/L M11001110-1707 30100ND11.5J 7.3J
2,4,6-Trichlorophenol ug/L M1100410-1660 30100ND3.8J ND
2,4-Dichlorophenol ug/L M11001510-1536 30100ND14.8J 6.1J
2,4-Dimethylphenol ug/L 100 101 20-14779 24 30100ND101 78.9
2,4-Dinitrophenol ug/L M1500010-1720 30500NDND ND
2,4-Dinitrotoluene ug/L 100 134 30-164126 6 30100ND134 126
2,6-Dinitrotoluene ug/L 100 127 31-163113 12 30100ND127 113
2-Chloronaphthalene ug/L 100 102 15-13478 26 30100ND102 78.2
2-Chlorophenol ug/L M11001810-1397 30100ND17.5J 7.0J
2-Methylnaphthalene ug/L 100 103 12-13080 25 30100ND103 80.1
2-Methylphenol(o-Cresol) ug/L R11007119-13248 38 30100ND71.0 48.3
2-Nitroaniline ug/L 200 116 23-154104 10 30200ND231 208
2-Nitrophenol ug/L M1100310-1590 30100ND3.0J ND
3&4-Methylphenol(m&pCresol)ug/L R11006913-13645 43 30100ND68.9 44.6
3,3'-Dichlorobenzidine ug/L M120017910-178170 5 30200ND357 340
3-Nitroaniline ug/L 200 139 20-166132 5 30200ND277 264
4,6-Dinitro-2-methylphenol ug/L M1200810-1877 30200NDND ND
4-Bromophenylphenyl ether ug/L 100 116 31-157108 7 30100ND116 108
4-Chloro-3-methylphenol ug/L R12007427-14650 39 30200ND148 99.9
4-Chloroaniline ug/L 200 111 13-14385 27 30200ND223 170
4-Chlorophenylphenyl ether ug/L 100 113 23-14993 20 30100ND113 92.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147312MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4147313
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Nitroaniline ug/L 200 160 24-171158 1 30200ND321 316
4-Nitrophenol ug/L M1500010-1300 30500NDND ND
Acenaphthene ug/L 100 104 21-14781 24 30100ND104 81.2
Acenaphthylene ug/L 100 103 19-15082 23 30100ND103 81.8
Acetophenone ug/L 100 97 22-14582 17 30100ND97.5 82.0
Anthracene ug/L 100 126 36-152121 4 30100ND126 121
Atrazine ug/L 100 154 18-173158 3 30100ND154 158
Benzaldehyde ug/L 100 99 16-16379 23 30100ND99.4 78.6
Benzo(a)anthracene ug/L M110016542-163161 2 30100ND165 161
Benzo(a)pyrene ug/L 100 166 40-169168 1 30100ND166 168
Benzo(b)fluoranthene ug/L M110018340-177189 3 30100ND183 189
Benzo(g,h,i)perylene ug/L 100 173 38-174174 1 30100ND173 174
Benzo(k)fluoranthene ug/L 100 169 41-171164 3 30100ND169 164
Biphenyl (Diphenyl)ug/L 100 102 14-13781 23 30100ND102 81.4bis(2-Chloroethoxy)methane ug/L 100 97 19-14680 19 30100ND96.9 80.1
bis(2-Chloroethyl) ether ug/L 100 94 19-15179 17 30100ND93.6 78.7
bis(2-Ethylhexyl)phthalate ug/L M110018642-168185 1 30100ND186 185
Butylbenzylphthalate ug/L 100 171 42-177174 2 30100ND171 174
Caprolactam ug/L 100 60 10-13046 27 30100ND60.0 45.7
Carbazole ug/L 100 158 38-164157 1 30100ND158 157
Chrysene ug/L 100 154 43-159154 0 30100ND154 154
Di-n-butylphthalate ug/L M110016142-160159 2 30100ND161 159
Di-n-octylphthalate ug/L M110018342-171185 1 30100ND183 185
Dibenz(a,h)anthracene ug/L M110017440-171174 0 30100ND174 174
Dibenzofuran ug/L 100 101 23-14781 22 30100ND101 80.8
Diethylphthalate ug/L 100 136 33-157129 5 30100ND136 129
Dimethylphthalate ug/L 100 116 27-154102 13 30100ND116 102
Fluoranthene ug/L 100 156 42-157152 3 30100ND156 152
Fluorene ug/L 100 110 25-15589 22 30100ND110 88.8
Hexachloro-1,3-butadiene ug/L 100 83 10-13066 23 30100ND82.8 65.9
Hexachlorobenzene ug/L 100 117 32-145111 5 30100ND117 111
Hexachlorocyclopentadiene ug/L 100 88 10-13071 22 30100ND87.8 70.7
Hexachloroethane ug/L R11006410-13045 35 30100ND63.7 44.6
Indeno(1,2,3-cd)pyrene ug/L 100 168 39-174167 0 30100ND168 167
Isophorone ug/L 100 102 19-14684 19 30100ND102 84.4
N-Nitroso-di-n-propylamine ug/L 100 108 20-15093 15 30100ND108 93.2
N-Nitrosodiphenylamine ug/L 100 124 33-149118 5 30100ND124 118
Naphthalene ug/L 100 92 10-12873 23 30100ND93.6 74.1
Nitrobenzene ug/L 100 98 19-14577 24 30100ND97.7 77.0
Pentachlorophenol ug/L M1200610-1886 30200ND11.8J 11.5J
Phenanthrene ug/L 100 126 38-150119 5 30100ND126 119
Phenol ug/L 100 23 10-13012 30100ND23.3 12.1J
Pyrene ug/L 100 147 42-163148 1 30100ND147 148
2,4,6-Tribromophenol (S) %S01210-1645
2-Fluorobiphenyl (S)%88 10-13071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
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[phone]
Page 103 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147312MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4147313
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Fluorophenol (S)%S0410-1301
Nitrobenzene-d5 (S)%89 10-13870
Phenol-d6 (S)%S01710-1308
Terphenyl-d14 (S)%128 19-191126
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800851
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4148204
Associated Lab Samples:92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280008
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/21/23 11:515.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4148205LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 52.450 105 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4149487LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 50.250 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4148206MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
4148207
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 100 80-12098 1 255085.1 135 134
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4148208MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4148209
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 113 80-120108 2 255081.0 137 135
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801391
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688280009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150994
Associated Lab Samples:92688280009
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/22/23 17:115.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150995LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 52.650 105 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150996LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 49.350 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150997MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689016007
4150998
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M15013580-120140 1 2550301368 371
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150999MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689016008
4151000
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 106 80-120106 0 2550124177 177
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802381
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688280010, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4156302
Associated Lab Samples:92688280010, 92688280011
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/27/23 20:075.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4156303LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 46.550 93 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4156304LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 47.450 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4156305MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280010
4156306
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 116 80-120101 5 2550108165 158
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802640
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688280007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4157372
Associated Lab Samples:92688280007
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/28/23 14:025.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157373LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 48.350 97 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157374LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 48.350 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4158201MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688804004
4158202
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M15013480-120-409 8 255033203390 3110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4158976MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265001
4158977
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1505580-12047 6 255037.1 64.5 60.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 108 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800660
SM 2540C-2015
SM 2540C-2015
2540C Total Dissolved Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688280007, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147236
Associated Lab Samples:92688280007, 92688280011
Matrix: Water
AnalyzedMDL
Total Dissolved Solids mg/L ND 25.0 09/19/23 23:2025.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147237LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 242250 97 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688674001
4147238SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 160 5 25169
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800722
SM 2540D-2015
SM 2540D-2015
2540D Total Suspended Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688280007, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147435
Associated Lab Samples:92688280007, 92688280011
Matrix: Water
AnalyzedMDL
Total Suspended Solids mg/L ND 2.5 09/20/23 13:402.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147436LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 234250 94 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688690001
4147915SAMPLE DUPLICATE:
Total Suspended Solids mg/L 807 3 25786
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688442002
4147916SAMPLE DUPLICATE:
Total Suspended Solids mg/L 207 11 25186
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800666
SM 4500-S2D-2011
SM 4500-S2D-2011
4500S2D Sulfide Water
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147255
Associated Lab Samples: 92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
Sulfide mg/L ND 0.10 09/20/23 02:560.022
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147256LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide mg/L 0.500.5 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147259MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4147260
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L M10.5 76 80-12079 2 100.50.24 0.62 0.63
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147272MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688078001
4147273
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 101 80-120109 8 100.5ND 0.51 0.55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803662
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688280007, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4162331
Associated Lab Samples:92688280007, 92688280011
Matrix: Water
AnalyzedMDL
Nitrogen, Kjeldahl, Total mg/L ND 0.50 10/04/23 04:510.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4162332LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 10.710 107 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4162383MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689831002
4162384
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 105 90-110102 3 10101.3 11.8 11.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801433
SM 5220D-2011
SM 5220D-2011
5220D COD
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688280007, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4151255
Associated Lab Samples:92688280007, 92688280011
Matrix: Water
AnalyzedMDL
Chemical Oxygen Demand mg/L ND 25.0 09/23/23 11:2012.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4151256LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand mg/L 786750 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4151257MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689016007
4151258
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L M110011790-110117 0 3100ND133 133
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4151259MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689016008
4151260
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L M110011590-110115 0 3100ND138 138
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803834
SM 5310B-2014
SM 5310B-2014
5310B TOC
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688280007, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4163063
Associated Lab Samples:92688280007, 92688280011
Matrix: Water
AnalyzedMDL
Total Organic Carbon mg/L ND 1.0 10/03/23 16:500.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4163064LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon mg/L 24.525 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4163065MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689241001
4163066
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon mg/L 25 97 90-11097 0 102526600ug/L 50.9 50.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4163067MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690723004
4163068
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon mg/L P4259390-11094 1 10256.0 29.3 29.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 183
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800716
EPA 9056A
EPA 9056A
9056 IC anions 28 Days
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147423
Associated Lab Samples: 92688280001, 92688280002, 92688280003, 92688280004, 92688280005, 92688280006, 92688280007,92688280008, 92688280009, 92688280010, 92688280011
Matrix: Water
AnalyzedMDL
Chloride mg/L ND 1.0 09/20/23 20:330.60
Sulfate mg/L ND 1.0 09/20/23 20:330.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147424LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 49.750 99 90-110
Sulfate mg/L 49.550 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147425MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4147426
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L M150-270 90-110177 3 105089108770 8990
Sulfate mg/L M150-51 90-110-13 4 1050500475 494
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147427MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280011
4147428
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L M1508790-11084 1 1050206249 248
Sulfate mg/L 50 94 90-11094 0 105020.1 67.1 66.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 183
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Re-extraction conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.1g
Result confirmed by second analysis.C0
Analyte is a possible laboratory contaminant (not present in method blank).C7
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The sample was analyzed at a dilution due to foaming of the sample in the purge vessel.F1
Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).HS
The internal standard response is below criteria. Results may be biased high.IS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Sample field preservation does not meet EPA or method recommendations for this analysis.P4
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 183
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92688280007 804467PZ02WG-091423 EPA 1664B
92688280011 804467PZ07WG-091523 EPA 1664B
92688280007 801219 801397PZ02WG-091423 EPA 3511 EPA 8015C
92688280011 801219 801397PZ07WG-091523 EPA 3511 EPA 8015C
92688280007 801614PZ02WG-091423 EPA 5030B/8015C
92688280011 801614PZ07WG-091523 EPA 5030B/8015C
92688280013 801614TB2-091423 EPA 5030B/8015C
92688280001 954340 954437PZ12WG-091423 EPA 3010 EPA 6010
92688280002 954340 954437PZ14WG-091423 EPA 3010 EPA 6010
92688280003 954340 954437PZ14HG-091423 EPA 3010 EPA 6010
92688280004 954340 954437BR01WG-091423 EPA 3010 EPA 6010
92688280005 954340 954437PZ11WG-091423 EPA 3010 EPA 6010
92688280006 954340 954437PZ06WG-091423 EPA 3010 EPA 6010
92688280007 954340 954437PZ02WG-091423 EPA 3010 EPA 6010
92688280008 954340 954437BR03WG-091423 EPA 3010 EPA 6010
92688280009 954340 954437EB01Q-091423 EPA 3010 EPA 6010
92688280010 954340 954437PZ13WG-091523 EPA 3010 EPA 6010
92688280011 954340 954437PZ07WG-091523 EPA 3010 EPA 6010
92688280001 954596 954652PZ12WG-091423 EPA 3010 EPA 6010
92688280002 954596 954652PZ14WG-091423 EPA 3010 EPA 6010
92688280003 954596 954652PZ14HG-091423 EPA 3010 EPA 6010
92688280004 954596 954652BR01WG-091423 EPA 3010 EPA 6010
92688280005 954596 954652PZ11WG-091423 EPA 3010 EPA 6010
92688280006 954596 954652PZ06WG-091423 EPA 3010 EPA 6010
92688280007 954596 954652PZ02WG-091423 EPA 3010 EPA 6010
92688280008 954596 954652BR03WG-091423 EPA 3010 EPA 6010
92688280009 954596 954652EB01Q-091423 EPA 3010 EPA 6010
92688280010 954596 954652PZ13WG-091523 EPA 3010 EPA 6010
92688280011 954596 954652PZ07WG-091523 EPA 3010 EPA 6010
92688280001 954846 955151PZ12WG-091423 EPA 7470 EPA 7470
92688280002 954846 955151PZ14WG-091423 EPA 7470 EPA 7470
92688280003 954846 955151PZ14HG-091423 EPA 7470 EPA 7470
92688280004 954846 955151BR01WG-091423 EPA 7470 EPA 7470
92688280005 954846 955151PZ11WG-091423 EPA 7470 EPA 7470
92688280006 954846 955151PZ06WG-091423 EPA 7470 EPA 7470
92688280007 954846 955151PZ02WG-091423 EPA 7470 EPA 7470
92688280008 954846 955151BR03WG-091423 EPA 7470 EPA 7470
92688280009 954846 955151EB01Q-091423 EPA 7470 EPA 7470
92688280010 954846 955151PZ13WG-091523 EPA 7470 EPA 7470
92688280011 954846 955151PZ07WG-091523 EPA 7470 EPA 7470
92688280001 954441 954514PZ12WG-091423 EPA 7470 EPA 7470
92688280002 954441 954514PZ14WG-091423 EPA 7470 EPA 7470
92688280003 954441 954514PZ14HG-091423 EPA 7470 EPA 7470
92688280004 954441 954514BR01WG-091423 EPA 7470 EPA 7470
92688280005 954441 954514PZ11WG-091423 EPA 7470 EPA 7470
92688280006 954441 954514PZ06WG-091423 EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 183
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92688280007 954441 954514PZ02WG-091423 EPA 7470 EPA 7470
92688280008 954441 954514BR03WG-091423 EPA 7470 EPA 7470
92688280009 954441 954514EB01Q-091423 EPA 7470 EPA 7470
92688280010 954441 954514PZ13WG-091523 EPA 7470 EPA 7470
92688280011 954441 954514PZ07WG-091523 EPA 7470 EPA 7470
92688280001 800691 800928PZ12WG-091423 EPA 3510C EPA 8270E
92688280002 800691 800928PZ14WG-091423 EPA 3510C EPA 8270E
92688280003 800691 800928PZ14HG-091423 EPA 3510C EPA 8270E
92688280004 800691 800928BR01WG-091423 EPA 3510C EPA 8270E
92688280005 800691 800928PZ11WG-091423 EPA 3510C EPA 8270E
92688280006 800691 800928PZ06WG-091423 EPA 3510C EPA 8270E
92688280007 800691 800928PZ02WG-091423 EPA 3510C EPA 8270E
92688280008 800691 800928BR03WG-091423 EPA 3510C EPA 8270E
92688280009 800691 800928EB01Q-091423 EPA 3510C EPA 8270E
92688280010 800691 800928PZ13WG-091523 EPA 3510C EPA 8270E
92688280011 800691 800928PZ07WG-091523 EPA 3510C EPA 8270E
92688280001 802109PZ12WG-091423 EPA 8260D
92688280002 802109PZ14WG-091423 EPA 8260D
92688280003 802109PZ14HG-091423 EPA 8260D
92688280004 802052BR01WG-091423 EPA 8260D
92688280005 801460PZ11WG-091423 EPA 8260D
92688280006 801460PZ06WG-091423 EPA 8260D
92688280007 801460PZ02WG-091423 EPA 8260D
92688280008 801460BR03WG-091423 EPA 8260D
92688280009 801146EB01Q-091423 EPA 8260D
92688280010 801460PZ13WG-091523 EPA 8260D
92688280011 801460PZ07WG-091523 EPA 8260D
92688280012 800499TB1-091423 EPA 8260D
92688280001 800851PZ12WG-091423 SM 2320B-2011
92688280002 800851PZ14WG-091423 SM 2320B-2011
92688280003 800851PZ14HG-091423 SM 2320B-2011
92688280004 800851BR01WG-091423 SM 2320B-2011
92688280005 800851PZ11WG-091423 SM 2320B-2011
92688280006 800851PZ06WG-091423 SM 2320B-2011
92688280007 802640PZ02WG-091423 SM 2320B-2011
92688280008 800851BR03WG-091423 SM 2320B-2011
92688280009 801391EB01Q-091423 SM 2320B-2011
92688280010 802381PZ13WG-091523 SM 2320B-2011
92688280011 802381PZ07WG-091523 SM 2320B-2011
92688280007 800660PZ02WG-091423 SM 2540C-2015
92688280011 800660PZ07WG-091523 SM 2540C-2015
92688280007 800722PZ02WG-091423 SM 2540D-2015
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 183
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92688280
Pactiv Evergreen GWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92688280011 800722PZ07WG-091523 SM 2540D-2015
92688280001 800666PZ12WG-091423 SM 4500-S2D-2011
92688280002 800666PZ14WG-091423 SM 4500-S2D-2011
92688280003 800666PZ14HG-091423 SM 4500-S2D-2011
92688280004 800666BR01WG-091423 SM 4500-S2D-2011
92688280005 800666PZ11WG-091423 SM 4500-S2D-2011
92688280006 800666PZ06WG-091423 SM 4500-S2D-2011
92688280007 800666PZ02WG-091423 SM 4500-S2D-2011
92688280008 800666BR03WG-091423 SM 4500-S2D-2011
92688280009 800666EB01Q-091423 SM 4500-S2D-2011
92688280010 800666PZ13WG-091523 SM 4500-S2D-2011
92688280011 800666PZ07WG-091523 SM 4500-S2D-2011
92688280007 803662 803953PZ02WG-091423 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92688280011 803662 803953PZ07WG-091523 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92688280007 801433 801586PZ02WG-091423 SM 5220D-2011 SM 5220D-2011
92688280011 801433 801586PZ07WG-091523 SM 5220D-2011 SM 5220D-2011
92688280007 803834PZ02WG-091423 SM 5310B-2014
92688280011 803834PZ07WG-091523 SM 5310B-2014
92688280001 800716PZ12WG-091423 EPA 9056A
92688280002 800716PZ14WG-091423 EPA 9056A
92688280003 800716PZ14HG-091423 EPA 9056A
92688280004 800716BR01WG-091423 EPA 9056A
92688280005 800716PZ11WG-091423 EPA 9056A
92688280006 800716PZ06WG-091423 EPA 9056A
92688280007 800716PZ02WG-091423 EPA 9056A
92688280008 800716BR03WG-091423 EPA 9056A
92688280009 800716EB01Q-091423 EPA 9056A
92688280010 800716PZ13WG-091523 EPA 9056A
92688280011 800716PZ07WG-091523 EPA 9056A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2023 09:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 183
Page 120 of 183
Page 121 of 183
Pa
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e

1
2
2

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8
3
The electronic signature above is the equivalent of a handwritten signature.This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC.
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)106 Vantage Point Drive West Columbia,SC 29172Tel:[phone] Fax:[phone] www.pacelabs.com
Report of Analysis
Pace Analytical Services,LLC9800KinceyAvenueSuite100Huntersville,NC 28078
Attention:Matthew Brainard
Project Name:Pactiv Evergreen GWS
Project Number:92688280
Lot Number:YI15070
Date Completed:09/28/2023
09/28/2023 8:12 PMApprovedandreleasedby:
Project Coordinator 1:Jenna S.Holliday
Page 1 of 26
Page 123 of 183
PACE ANALYTICAL SERVICES,LLC
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.)106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.pacelabs.com
Case NarrativePaceAnalyticalServices,LLCLotNumber:YI15070
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header informationassociatedwitheachsample.
All results listed in this report relate only to the samples that are contained within this report.Where
sampling is conducted by the client,results relate to the accuracy of the information provided,and as thesamplesarereceived.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace")Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to
the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page ordiscussedbelow.
Pace is a TNI accredited laboratory;however,the following analyses are currently not listed on our TNI
scope of accreditation:Drinking Water:VOC (excluding BTEX,MTBE,Naphthalene,&1,2-dichloroethane)EPA 524.2,E.coli and Total coliforms SM 9223 B-2004,Solid Chemical Material:TOC
Walkley-Black,Biological Tissue:All,Non-Potable Water:SGT-HEM EPA 1664B,Silica EPA 200.7,Boron,Calcium,Silicon,Strontium EPA 200.8,Bicarbonate,Carbonate,and Hydroxide Alkalinity SM 2320
B-2011,SM 9221 C E-2006 &SM 9222D-2006,Strontium SW-846 6010D,VOC SM 6200 B-2011,FecalColiformColilert-18,PFAS by Isotope Dilution SOP.
If you have any questions regarding this report,please contact the Pace Project Manager listed on the
cover page.
BOD Analysis1-The GGA associated with BOD batch 84958 was out of range at 164 mg/L (valid range is 167.5 –
228.5 mg/L).The associated BOD results should be considered estimated.All other QC passedacceptancecriteria.
6 -The BOD result has been reported as less than the stated value due to oxygen depletion of less than
2.0 mg/l at each sample dilution.The sample was prepared with a standard series of dilutions based ontheCODresult.
Nitrate Analysis
The matrix spike/matrix spike duplicate (MS/MSD)for batch 85117 recovered outside of the acceptancelimits.The associated laboratory control sample (LCS)passed acceptance criteria.Therefore,the data
has been reported.
Page 2 of 26
Page 124 of 183
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical Services, LLC
Lot Number: YI15070

Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Sample Number Sample ID Matrix Date Sampled Date Received
001 09/14/2023 1005PZ12WG-091423 Aqueous 09/15/2023
002 09/14/2023 1128PZ14WG-091423 Aqueous 09/15/2023
003 09/14/2023 1130PZ14HG-091423 Aqueous 09/15/2023
004 09/14/2023 1200BR01WG-091423 Aqueous 09/15/2023
005 09/14/2023 1212PZ11WG-091423 Aqueous 09/15/2023
006 09/14/2023 1540PZ06WG-091423 Aqueous 09/15/2023
007 09/14/2023 1458PZ02WG-091423 Aqueous 09/15/2023
008 09/14/2023 1730BR03WG-091423 Aqueous 09/15/2023
009 09/14/2023 1720EB01Q-091423 Aqueous 09/15/2023
010 09/15/2023 1006PZ13WG-091523 Aqueous 09/15/2023
011 09/15/2023 1100PZ07WG-091523 Aqueous 09/15/2023
(11 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 26
Page 125 of 183
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical Services, LLC
Lot Number: YI15070

Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 PZ12WG-091423 Aqueous Platinum-Cobalt Color SM 2120B-7500 *color units 6
002 PZ14WG-091423 Aqueous Platinum-Cobalt Color SM 2120B-10 *color units 7
003 PZ14HG-091423 Aqueous Platinum-Cobalt Color SM 2120B-10 *color units 8
004 BR01WG-091423 Aqueous Platinum-Cobalt Color SM 2120B-160 *color units 9
005 PZ11WG-091423 Aqueous Platinum-Cobalt Color SM 2120B-9000 *color units 10
006 PZ06WG-091423 Aqueous Platinum-Cobalt Color SM 2120B-10 *color units 11
007 PZ02WG-091423 Aqueous BOD, 5 day SM 5210B-<66 6 mg/L 12
007 PZ02WG-091423 Aqueous Platinum-Cobalt Color SM 2120B- 16000 *color units 12
008 BR03WG-091423 Aqueous Platinum-Cobalt Color SM 2120B-200 *color units 13
010 PZ13WG-091523 Aqueous Platinum-Cobalt Color SM 2120B-15 *color units 15
011 PZ07WG-091523 Aqueous BOD, 5 day SM 5210B-<27 6 mg/L 16
011 PZ07WG-091523 Aqueous Platinum-Cobalt Color SM 2120B- 16000 *color units 16
(12 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 26
Page 126 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
PZ12WG-091423
YI15070-001
09/14/2023 1005
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 500 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 7500 *1color units25002500
Footnote(s): *Color pH = 7.76
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 26
Page 127 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
PZ14WG-091423
YI15070-002
09/14/2023 1128
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 1 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 10 *1color units5.05.0
Footnote(s): *Color pH = 6.46
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 26
Page 128 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
PZ14HG-091423
YI15070-003
09/14/2023 1130
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 1 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 10 *1color units5.05.0
Footnote(s): *Color pH = 6.39
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 26
Page 129 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
BR01WG-091423
YI15070-004
09/14/2023 1200
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 4 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 160 *1color units2020
Footnote(s): *Color pH = 6.57
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 26
Page 130 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
PZ11WG-091423
YI15070-005
09/14/2023 1212
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 300 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 9000 *1color units15001500
Footnote(s): *Color pH = 6.90
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 26
Page 131 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
PZ06WG-091423
YI15070-006
09/14/2023 1540
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 1 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 10 *1color units5.05.0
Footnote(s): *Color pH = 6.66
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 26
Page 132 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
PZ02WG-091423
YI15070-007
09/14/2023 1458
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (BOD, 5 day) SM 5210B-2016 1 09/20/2023 1812 TAD 09/15/2023 2225 84958
1 (Nitrate - N) 353.2 25 09/16/2023 1325 CLL2 85117
1 (Platinum-Cob) SM 2120B-2011 400 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
BOD, 5 day SM 5210B-2016 <66 6 1mg/L0.182.0
Nitrate - N 353.2 ND 1mg/L0.250.50
Platinum-Cobalt Color SM 2120B-2011 16000 *1color units20002000
Footnote(s): *Color pH = 9.936-D.O. depletion < 2.00 mg/L
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 26
Page 133 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
BR03WG-091423
YI15070-008
09/14/2023 1730
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 5 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 200 *1color units2525
Footnote(s): *Color pH = 8.81
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 26
Page 134 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
EB01Q-091423
YI15070-009
09/14/2023 1720
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 1 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 ND *1color units5.05.0
Footnote(s): *Color pH = 4.55
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 26
Page 135 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
PZ13WG-091523
YI15070-010
09/15/2023 1006
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Platinum-Cob) SM 2120B-2011 1 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
Platinum-Cobalt Color SM 2120B-2011 15 *1color units5.05.0
Footnote(s): *Color pH = 6.75
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 26
Page 136 of 183
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
PZ07WG-091523
YI15070-011
09/15/2023 1100
09/15/2023
Aqueous
Project Name: Pactiv Evergreen GWS
Project Number: 92688280
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (BOD, 5 day) SM 5210B-2016 1 09/20/2023 1815 TAD 09/15/2023 2230 84958
1 (Nitrate - N) 353.2 25 09/16/2023 1327 CLL2 85117
1 (Platinum-Cob) SM 2120B-2011 400 09/16/2023 0858 CLL2
AnalyticalCASParameterNumberMethod Result Q LOQ Units Run DL
BOD, 5 day SM 5210B-2016 <27 6 1mg/L0.182.0
Nitrate - N 353.2 ND S 1mg/L0.250.50
Platinum-Cobalt Color SM 2120B-2011 16000 *1color units20002000
Footnote(s): *Color pH = 8.356-D.O. depletion < 2.00 mg/L
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 26
Page 137 of 183
QC Summary
QC Data for Lot Number: YI15070
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 16 of 26
Page 138 of 183
Inorganic non-metals - BOD Blank and GGA
Batch:SCF:
SCF Range:
84958
0.6 - 1.0Analytical Method:SM 5210B-2016
Matrix:Aqueous
0.9
Sample ID Result Q Limit Analysis DateDepl Avg. Depl (mg/L)Avg. Result
(mg/L)Prep Date
YQ84958-041 (Blank)09/20/2023 16590.2 09/15/2023 20480.1
YQ84958-141 (Blank)09/20/2023 16590.2 09/15/2023 20480.04
YQ84958-241 (Blank)09/20/2023 16590.20.05 09/15/2023 20480.01
YQ84958-035 (GGA)164 09/20/2023 17051 167.5-228.5 09/15/2023 2055
YQ84958-135 (GGA)177 09/20/2023 1705167.5-228.5 09/15/2023 2055
YQ84958-235 (GGA)191.5 09/20/2023 1705167.5-228.5 09/15/2023 2055177.5
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
QC Data for Lot Number: YI15070106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 17 of 26
Page 139 of 183
Inorganic non-metals - MB
Batch:
Sample ID:YQ85117-001
85117
Analytical Method:353.2
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Nitrate - N ND 09/16/2023 13220.020 0.010 mg/L1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
QC Data for Lot Number: YI15070106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 18 of 26
Page 140 of 183
Inorganic non-metals - LCS
Batch:
Sample ID:YQ85117-002
85117
Analytical Method:353.2
Matrix:Aqueous
Parameter Result Q % Rec
Spike
Amount Analysis Date
%Rec
LimitDil(mg/L)(mg/L)
Nitrate - N 0.40 09/16/2023 13231010.40 90-1101
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
QC Data for Lot Number: YI15070106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 19 of 26
Page 141 of 183
Inorganic non-metals - MS
Batch:
Sample ID:YI15070-011MS
85117
Analytical Method:353.2
Matrix:Aqueous
Parameter Result Q % Rec
Spike
Amount Analysis Date
%Rec
Limit
Sample
Amount Dil(mg/L) (mg/L) (mg/L)
Nitrate - N 0.26 09/16/2023 1333N650.40 90-110ND25
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
QC Data for Lot Number: YI15070106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 20 of 26
Page 142 of 183
Inorganic non-metals - MSD
Batch:
Sample ID:YI15070-011MD
85117
Analytical Method:353.2
Matrix:Aqueous
Parameter Result Q % Rec
Spike
Amount Analysis Date% RPD
%Rec
Limit % RPD
Limit
Sample
Amount Dil(mg/L) (mg/L) (mg/L)
Nitrate - N 0.28 09/16/2023 1335N690.40 90-1106.6 20ND25
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
QC Data for Lot Number: YI15070106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 21 of 26
Page 143 of 183
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 22 of 26
Page 144 of 183
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PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 26 of 26
Page 148 of 183
Thisreportshouldnotbereproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamplesincludedinthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
Matthew Brainard
PACE Charlotte
9800 Kincey Ave.
Huntersville NC 28078
REPORT OF
LABORATORY
ANALYSIS FOR
PCDD/PCDF
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
October 27, 2023
Pace Project #: 10670311
Sample Receipt Date: 09/27/2023
Client Project #: 92688280
Client Sub PO #: N/A
The report provided has been invoiced as a Level 2
PCDD/PCDF Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questionstoIsaac Johnson,your Pace
Project Manager.
State Cert #: 530
Suite 100
Report Prepared for:
Page 1 of 35Report No.....10670311_SW8290AFC_L2_dfr
October 27, 2023
Isaac Johnson, Project Manager
[phone]
[phone] (fax)
[e-mail]
Page 149 of 183
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
This report presents the results from the analyses performed on eleven samples submitted by a
representative of Pace Analytical Services, LLC. The samples were analyzed for the presence or absence
of polychlorodibenzo-p-dioxins (PCDDs) and polychlorodibenzofurans (PCDFs) using a modified version
of USEPA Method 8290A. The estimated detection limits (EDLs) were based on signal-to-noise
measurements. Estimated maximum possible concentration (EMPC) values were treated as positives inthe toxic equivalence calculations.
The isotopically-labeled PCDD/PCDF internal standards in the sample extracts were recovered at20-121%. Except for thirty low values, which were flagged "R" on the results tables, the labeled internalstandard recoveries obtained for this project were within the 40-135% target range specified in Method8290A. Since the quantification of the native 2,3,7,8-substituted congeners was based on isotope dilution,the data were automatically corrected for recovery and accurate values were obtained.
Values were flagged "I" where incorrect isotope ratios were obtained. Concentrations below the calibrationrange were flagged "J" and should be regarded as estimates.
A laboratory method blank was prepared and analyzed with each sample batch as part of our routine
quality control procedures. The results show the blanks to contain trace levels of selected congeners.
These levels were below the calibration range of the method. Sample concentrations similar to the
corresponding blank levels were flagged "B" on the results tables and may be, at least partially, attributed
to the background.
Laboratory and matrix spike samples were also prepared using clean reference matrix or sample matrix
that had been fortified with native standard materials. The results show that the spiked native compounds
were recovered at 79-117% with relative percent differences of 0.0-12.6%. These results were within the
target ranges for the method. Matrix spikes were not prepared with the extraction batches extracted on10/10/2023 and 10/24/2023.
The responses obtained for selected labeled congeners in calibration standard analyses L231016A_18,L231026B_22, and U231021A_17 were outside the target range. As specified in our procedures for thismethod, the averages of the daily response factors for these compounds were used in the calculations forthe samples from these runshifts. The affected values were flagged "Y" on the results tables.
DISCUSSION
Page 2 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 150 of 183
REPORT OF LABORATORY ANALYSIS
This report shallnot bereproduced,except in full,
withoutthe written consentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Report No.....10670311
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 151 of 183
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 4 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 152 of 183
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Page 6 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 154 of 183
Page 7 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 155 of 183
Page 8 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 156 of 183
Page 9 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 157 of 183
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
A =
B = C = D = E = H2 =
I =
J = L = Nn = P = R =
S =
U = V = X = Y = * =
Reporting Limit based on signal to noise (EDL)
Less than 10x higher than method blank level Result obtained from confirmation analysis Result obtained from analysis of diluted sample Exceeds calibration range Extracted outside of holding time
Isotope ratio out of specification
Estimated value Suppressive interference, analyte may be biased low Value obtained from additional analysis PCDE Interference Recovery outside target range
Peak saturated
Analyte not detected Result verified by confirmation analysis %D Exceeds limits Calculated using average of daily RFs See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 10 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 158 of 183
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 11 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 159 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ12WG-09142392688280001-RU231027A_11JF
NA103 mL
NAU230926U231026A_23 & U231027A_16BLANK-108989
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/14/2023 10:0509/27/2023 16:4510/24/2023 10:0010/27/2023 09:51
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 21 2,3,7,8-TCDF-13C 2.00 64-----Total TCDF ND 21 2,3,7,8-TCDD-13C 2.00 60-----1,2,3,7,8-PeCDF-13C 2.00 492,3,7,8-TCDD ND 21 2,3,4,7,8-PeCDF-13C 2.00 48-----Total TCDD ND 21 1,2,3,7,8-PeCDD-13C 2.00 52-----1,2,3,4,7,8-HxCDF-13C 2.00 751,2,3,7,8-PeCDF ND 20 1,2,3,6,7,8-HxCDF-13C 2.00 73-----2,3,4,7,8-PeCDF ND 15 2,3,4,6,7,8-HxCDF-13C 2.00 68-----Total PeCDF ND 15 1,2,3,7,8,9-HxCDF-13C 2.00 58-----1,2,3,4,7,8-HxCDD-13C 2.00 651,2,3,7,8-PeCDD ND 23 1,2,3,6,7,8-HxCDD-13C 2.00 73-----Total PeCDD 780 23 1,2,3,4,6,7,8-HpCDF-13C 2.00 44-----1,2,3,4,7,8,9-HpCDF-13C 2.00 36 R1,2,3,4,7,8-HxCDF ND 32 1,2,3,4,6,7,8-HpCDD-13C 2.00 40-----1,2,3,6,7,8-HxCDF ND 31 OCDD-13C 4.00 40-----2,3,4,6,7,8-HxCDF ND 32-----1,2,3,7,8,9-HxCDF ND 49 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 31 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 35 2,3,7,8-TCDD-37Cl4 0.20 80-----1,2,3,6,7,8-HxCDD ND 26-----1,2,3,7,8,9-HxCDD ND 29-----Total HxCDD 6800 26-----
1,2,3,4,6,7,8-HpCDF 110 44 Total 2,3,7,8-TCDDJ-----1,2,3,4,7,8,9-HpCDF ND 68 Equivalence: 54 pg/L-----Total HpCDF 110 44 (Lower-bound - Using 2005 WHO Factors)BJ-----
1,2,3,4,6,7,8-HpCDD 4200 54-----Total HpCDD 17000 54-----
OCDF 570 160 J-----OCDD 39000 170-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelR=Recovery outside target range
EDL = Estimated Detection Limit
Page 12 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 160 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ14WG-09142392688280002U231021A_05AH5
NA880 mL
NAU230926U231020B_19 & U231021A_17BLANK-108749
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/14/2023 11:2809/27/2023 16:4510/10/2023 10:4110/21/2023 03:11
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.69 2,3,7,8-TCDF-13C 2.00 87-----Total TCDF ND 0.69 2,3,7,8-TCDD-13C 2.00 82-----1,2,3,7,8-PeCDF-13C 2.00 832,3,7,8-TCDD ND 1.1 2,3,4,7,8-PeCDF-13C 2.00 83-----Total TCDD ND 1.1 1,2,3,7,8-PeCDD-13C 2.00 90-----1,2,3,4,7,8-HxCDF-13C 2.00 1071,2,3,7,8-PeCDF ND 0.66 1,2,3,6,7,8-HxCDF-13C 2.00 102-----2,3,4,7,8-PeCDF ND 0.48 2,3,4,6,7,8-HxCDF-13C 2.00 100-----Total PeCDF ND 0.48 1,2,3,7,8,9-HxCDF-13C 2.00 87-----1,2,3,4,7,8-HxCDD-13C 2.00 991,2,3,7,8-PeCDD ND 0.69 1,2,3,6,7,8-HxCDD-13C 2.00 104-----Total PeCDD ND 0.69 1,2,3,4,6,7,8-HpCDF-13C 2.00 79-----1,2,3,4,7,8,9-HpCDF-13C 2.00 90 Y1,2,3,4,7,8-HxCDF ND 0.73 1,2,3,4,6,7,8-HpCDD-13C 2.00 75-----1,2,3,6,7,8-HxCDF ND 0.74 OCDD-13C 4.00 78-----Y2,3,4,6,7,8-HxCDF ND 0.68-----1,2,3,7,8,9-HxCDF -----1.0 1,2,3,4-TCDD-13C 2.00 NAIJ1.1Total HxCDF ND 0.68 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 0.90 2,3,7,8-TCDD-37Cl4 0.20 82-----1,2,3,6,7,8-HxCDD ND 0.74-----1,2,3,7,8,9-HxCDD ND 0.78-----Total HxCDD ND 0.74-----
1,2,3,4,6,7,8-HpCDF ND 1.7 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 2.7 Equivalence: 0.13 pg/L-----Total HpCDF 1.8 1.7 (Lower-bound - Using 2005 WHO Factors)BJ-----
1,2,3,4,6,7,8-HpCDD -----1.6 IJ1.6Total HpCDD 2.9 1.6 BJ-----
OCDF ND 3.4-----OCDD -----3.5 IJ17
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specificationY =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 13 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 161 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ14HG-09142392688280003U231021A_06AH5
NA957 mL
NAU230926U231020B_19 & U231021A_17BLANK-108749
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/14/2023 11:3009/27/2023 16:4510/10/2023 10:4110/21/2023 03:57
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 1.0 2,3,7,8-TCDF-13C 2.00 74-----Total TCDF ND 1.0 2,3,7,8-TCDD-13C 2.00 71-----1,2,3,7,8-PeCDF-13C 2.00 672,3,7,8-TCDD ND 1.7 2,3,4,7,8-PeCDF-13C 2.00 69-----Total TCDD ND 1.7 1,2,3,7,8-PeCDD-13C 2.00 74-----1,2,3,4,7,8-HxCDF-13C 2.00 881,2,3,7,8-PeCDF ND 0.72 1,2,3,6,7,8-HxCDF-13C 2.00 87-----2,3,4,7,8-PeCDF ND 0.50 2,3,4,6,7,8-HxCDF-13C 2.00 84-----Total PeCDF ND 0.50 1,2,3,7,8,9-HxCDF-13C 2.00 76-----1,2,3,4,7,8-HxCDD-13C 2.00 811,2,3,7,8-PeCDD ND 0.95 1,2,3,6,7,8-HxCDD-13C 2.00 86-----Total PeCDD ND 0.95 1,2,3,4,6,7,8-HpCDF-13C 2.00 64-----1,2,3,4,7,8,9-HpCDF-13C 2.00 80 Y1,2,3,4,7,8-HxCDF ND 1.1 1,2,3,4,6,7,8-HpCDD-13C 2.00 63-----1,2,3,6,7,8-HxCDF ND 1.1 OCDD-13C 4.00 65-----Y2,3,4,6,7,8-HxCDF ND 1.0-----1,2,3,7,8,9-HxCDF ND 1.5 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 1.0 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD -----0.93 2,3,7,8-TCDD-37Cl4 0.20 77IJ1.61,2,3,6,7,8-HxCDD ND 0.80-----1,2,3,7,8,9-HxCDD ND 0.83-----Total HxCDD ND 0.80-----
1,2,3,4,6,7,8-HpCDF ND 1.3 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 2.1 Equivalence: 0.19 pg/L-----Total HpCDF ND 1.3 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----0.87 IJ2.0Total HpCDD ND 0.87-----
OCDF ND 3.3-----OCDD 23 6.1 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specificationY =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 14 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 162 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID BR01WG-09142392688280004U231021A_07AH5
NA916 mL
NAU230926U231020B_19 & U231021A_17BLANK-108749
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/14/2023 12:0009/27/2023 16:4510/10/2023 10:4110/21/2023 04:44
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.96 2,3,7,8-TCDF-13C 2.00 87-----Total TCDF ND 0.96 2,3,7,8-TCDD-13C 2.00 83-----1,2,3,7,8-PeCDF-13C 2.00 822,3,7,8-TCDD ND 1.4 2,3,4,7,8-PeCDF-13C 2.00 80-----Total TCDD ND 1.4 1,2,3,7,8-PeCDD-13C 2.00 88-----1,2,3,4,7,8-HxCDF-13C 2.00 1151,2,3,7,8-PeCDF ND 0.82 1,2,3,6,7,8-HxCDF-13C 2.00 114-----2,3,4,7,8-PeCDF ND 0.61 2,3,4,6,7,8-HxCDF-13C 2.00 108-----Total PeCDF ND 0.61 1,2,3,7,8,9-HxCDF-13C 2.00 93-----1,2,3,4,7,8-HxCDD-13C 2.00 1091,2,3,7,8-PeCDD ND 0.85 1,2,3,6,7,8-HxCDD-13C 2.00 112-----Total PeCDD ND 0.85 1,2,3,4,6,7,8-HpCDF-13C 2.00 85-----1,2,3,4,7,8,9-HpCDF-13C 2.00 97 Y1,2,3,4,7,8-HxCDF ND 0.84 1,2,3,4,6,7,8-HpCDD-13C 2.00 81-----1,2,3,6,7,8-HxCDF ND 0.81 OCDD-13C 4.00 85-----Y2,3,4,6,7,8-HxCDF ND 0.83-----1,2,3,7,8,9-HxCDF ND 1.1 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 0.81 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD -----1.0 2,3,7,8-TCDD-37Cl4 0.20 78IJ2.31,2,3,6,7,8-HxCDD ND 0.86-----1,2,3,7,8,9-HxCDD ND 0.90-----Total HxCDD ND 0.86-----
1,2,3,4,6,7,8-HpCDF ND 1.4 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 2.6 Equivalence: 0.25 pg/L-----Total HpCDF ND 1.4 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----1.2 IJ1.4Total HpCDD 2.1 1.2 BJ-----
OCDF 4.5 2.9 J-----OCDD 20 5.7 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specificationY =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 15 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 163 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ11WG-09142392688280005-RU231027A_12JF
NA103 mL
NAU230926U231026A_23 & U231027A_16BLANK-108989
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/14/2023 12:1209/27/2023 16:4510/24/2023 10:0010/27/2023 10:38
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 15 2,3,7,8-TCDF-13C 2.00 80-----Total TCDF ND 15 2,3,7,8-TCDD-13C 2.00 73-----1,2,3,7,8-PeCDF-13C 2.00 632,3,7,8-TCDD ND 21 2,3,4,7,8-PeCDF-13C 2.00 61-----Total TCDD ND 21 1,2,3,7,8-PeCDD-13C 2.00 63-----1,2,3,4,7,8-HxCDF-13C 2.00 1011,2,3,7,8-PeCDF ND 23 1,2,3,6,7,8-HxCDF-13C 2.00 95-----2,3,4,7,8-PeCDF ND 16 2,3,4,6,7,8-HxCDF-13C 2.00 89-----Total PeCDF ND 16 1,2,3,7,8,9-HxCDF-13C 2.00 73-----1,2,3,4,7,8-HxCDD-13C 2.00 761,2,3,7,8-PeCDD ND 21 1,2,3,6,7,8-HxCDD-13C 2.00 90-----Total PeCDD ND 21 1,2,3,4,6,7,8-HpCDF-13C 2.00 55-----1,2,3,4,7,8,9-HpCDF-13C 2.00 451,2,3,4,7,8-HxCDF ND 41 1,2,3,4,6,7,8-HpCDD-13C 2.00 52-----1,2,3,6,7,8-HxCDF ND 42 OCDD-13C 4.00 53-----2,3,4,6,7,8-HxCDF ND 45-----1,2,3,7,8,9-HxCDF ND 66 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 41 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 57 2,3,7,8-TCDD-37Cl4 0.20 92-----1,2,3,6,7,8-HxCDD ND 41-----1,2,3,7,8,9-HxCDD ND 46-----Total HxCDD ND 41-----
1,2,3,4,6,7,8-HpCDF ND 74 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 120 Equivalence: 3.6 pg/L-----Total HpCDF 240 74 (Lower-bound - Using 2005 WHO Factors)J-----
1,2,3,4,6,7,8-HpCDD 310 38 J-----Total HpCDD 550 38-----
OCDF 490 230 J-----OCDD 1100 180-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
EDL = Estimated Detection Limit
Page 16 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 164 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ06WG-09142392688280006U231021A_09AH5
NA909 mL
NAU230926U231020B_19 & U231021A_17BLANK-108749
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/14/2023 15:4009/27/2023 16:4510/10/2023 10:4110/21/2023 06:17
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.86 2,3,7,8-TCDF-13C 2.00 79-----Total TCDF ND 0.86 2,3,7,8-TCDD-13C 2.00 78-----1,2,3,7,8-PeCDF-13C 2.00 742,3,7,8-TCDD ND 1.9 2,3,4,7,8-PeCDF-13C 2.00 74-----Total TCDD ND 1.9 1,2,3,7,8-PeCDD-13C 2.00 80-----1,2,3,4,7,8-HxCDF-13C 2.00 1031,2,3,7,8-PeCDF ND 1.3 1,2,3,6,7,8-HxCDF-13C 2.00 100-----2,3,4,7,8-PeCDF ND 0.94 2,3,4,6,7,8-HxCDF-13C 2.00 97-----Total PeCDF ND 0.94 1,2,3,7,8,9-HxCDF-13C 2.00 81-----1,2,3,4,7,8-HxCDD-13C 2.00 961,2,3,7,8-PeCDD ND 0.93 1,2,3,6,7,8-HxCDD-13C 2.00 99-----Total PeCDD ND 0.93 1,2,3,4,6,7,8-HpCDF-13C 2.00 74-----1,2,3,4,7,8,9-HpCDF-13C 2.00 85 Y1,2,3,4,7,8-HxCDF ND 0.76 1,2,3,4,6,7,8-HpCDD-13C 2.00 72-----1,2,3,6,7,8-HxCDF ND 0.72 OCDD-13C 4.00 72-----Y2,3,4,6,7,8-HxCDF ND 0.71-----1,2,3,7,8,9-HxCDF ND 1.1 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 0.71 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD -----1.1 2,3,7,8-TCDD-37Cl4 0.20 79IJ1.51,2,3,6,7,8-HxCDD ND 0.85-----1,2,3,7,8,9-HxCDD ND 0.94-----Total HxCDD ND 0.85-----
1,2,3,4,6,7,8-HpCDF ND 1.5 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 2.5 Equivalence: 0.19 pg/L-----Total HpCDF ND 1.5 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----1.8 IJ2.7Total HpCDD ND 1.8-----
OCDF ND 5.2-----OCDD -----8.8 IJ19
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
I=Isotope ratio out of specificationY =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 17 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 165 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ02WG-09142392688280007-RU231027A_13JF
NA99.3 mL
NAU230926U231026A_23 & U231027A_16BLANK-108989
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/14/2023 14:5809/27/2023 16:4510/24/2023 10:0010/27/2023 11:25
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 19 2,3,7,8-TCDF-13C 2.00 61-----Total TCDF ND 19 2,3,7,8-TCDD-13C 2.00 58-----1,2,3,7,8-PeCDF-13C 2.00 532,3,7,8-TCDD ND 28 2,3,4,7,8-PeCDF-13C 2.00 51-----Total TCDD ND 28 1,2,3,7,8-PeCDD-13C 2.00 54-----1,2,3,4,7,8-HxCDF-13C 2.00 871,2,3,7,8-PeCDF ND 19 1,2,3,6,7,8-HxCDF-13C 2.00 87-----2,3,4,7,8-PeCDF ND 14 2,3,4,6,7,8-HxCDF-13C 2.00 75-----Total PeCDF ND 14 1,2,3,7,8,9-HxCDF-13C 2.00 66-----1,2,3,4,7,8-HxCDD-13C 2.00 691,2,3,7,8-PeCDD ND 18 1,2,3,6,7,8-HxCDD-13C 2.00 82-----Total PeCDD ND 18 1,2,3,4,6,7,8-HpCDF-13C 2.00 46-----1,2,3,4,7,8,9-HpCDF-13C 2.00 411,2,3,4,7,8-HxCDF ND 45 1,2,3,4,6,7,8-HpCDD-13C 2.00 45-----1,2,3,6,7,8-HxCDF ND 45 OCDD-13C 4.00 43-----2,3,4,6,7,8-HxCDF ND 48-----1,2,3,7,8,9-HxCDF ND 72 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 45 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 60 2,3,7,8-TCDD-37Cl4 0.20 93-----1,2,3,6,7,8-HxCDD ND 46-----1,2,3,7,8,9-HxCDD ND 50-----Total HxCDD ND 46-----
1,2,3,4,6,7,8-HpCDF -----67 Total 2,3,7,8-TCDDIJ971,2,3,4,7,8,9-HpCDF ND 100 Equivalence: 4.6 pg/L-----Total HpCDF ND 67 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----57 IJ320Total HpCDD 270 57 BJ-----
OCDF 370 310 BJ-----OCDD 1100 240-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 18 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 166 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID BR03WG-09142392688280008U231021A_03AH5
NA829 mL
NAU230926U231020B_19 & U231021A_17BLANK-108749
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/14/2023 17:3009/27/2023 16:4510/06/2023 11:3110/21/2023 01:38
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 1.4 2,3,7,8-TCDF-13C 2.00 54-----Total TCDF ND 1.4 2,3,7,8-TCDD-13C 2.00 52-----1,2,3,7,8-PeCDF-13C 2.00 512,3,7,8-TCDD ND 1.6 2,3,4,7,8-PeCDF-13C 2.00 49-----Total TCDD ND 1.6 1,2,3,7,8-PeCDD-13C 2.00 56-----1,2,3,4,7,8-HxCDF-13C 2.00 801,2,3,7,8-PeCDF ND 1.1 1,2,3,6,7,8-HxCDF-13C 2.00 75-----2,3,4,7,8-PeCDF ND 0.79 2,3,4,6,7,8-HxCDF-13C 2.00 69-----Total PeCDF ND 0.79 1,2,3,7,8,9-HxCDF-13C 2.00 61-----1,2,3,4,7,8-HxCDD-13C 2.00 721,2,3,7,8-PeCDD ND 2.1 1,2,3,6,7,8-HxCDD-13C 2.00 73-----Total PeCDD ND 2.1 1,2,3,4,6,7,8-HpCDF-13C 2.00 61-----1,2,3,4,7,8,9-HpCDF-13C 2.00 71 Y1,2,3,4,7,8-HxCDF ND 1.0 1,2,3,4,6,7,8-HpCDD-13C 2.00 56-----1,2,3,6,7,8-HxCDF ND 1.0 OCDD-13C 4.00 61-----Y2,3,4,6,7,8-HxCDF ND 1.0-----1,2,3,7,8,9-HxCDF ND 1.4 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 1.0 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 1.5 2,3,7,8-TCDD-37Cl4 0.20 61-----1,2,3,6,7,8-HxCDD ND 1.3-----1,2,3,7,8,9-HxCDD ND 1.3-----Total HxCDD ND 1.3-----
1,2,3,4,6,7,8-HpCDF ND 1.9 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 3.1 Equivalence: 0.047 pg/L-----Total HpCDF ND 1.9 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD 4.0 2.1 BJ-----Total HpCDD 4.0 2.1 BJ-----
OCDF ND 5.8-----OCDD 26 7.4 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelY =Calculated using average of daily RFs
EDL = Estimated Detection Limit
Page 19 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 167 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID EB01Q-09142392688280009-RU231027A_14JF
NA945 mL
NAU230926U231026A_23 & U231027A_16BLANK-108989
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/14/2023 17:2009/27/2023 16:4510/24/2023 10:0010/27/2023 12:12
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 1.1 2,3,7,8-TCDF-13C 2.00 78-----Total TCDF ND 1.1 2,3,7,8-TCDD-13C 2.00 75-----1,2,3,7,8-PeCDF-13C 2.00 762,3,7,8-TCDD ND 1.7 2,3,4,7,8-PeCDF-13C 2.00 76-----Total TCDD ND 1.7 1,2,3,7,8-PeCDD-13C 2.00 79-----1,2,3,4,7,8-HxCDF-13C 2.00 1211,2,3,7,8-PeCDF ND 1.7 1,2,3,6,7,8-HxCDF-13C 2.00 118-----2,3,4,7,8-PeCDF ND 1.2 2,3,4,6,7,8-HxCDF-13C 2.00 107-----Total PeCDF ND 1.2 1,2,3,7,8,9-HxCDF-13C 2.00 93-----1,2,3,4,7,8-HxCDD-13C 2.00 951,2,3,7,8-PeCDD ND 1.4 1,2,3,6,7,8-HxCDD-13C 2.00 111-----Total PeCDD ND 1.4 1,2,3,4,6,7,8-HpCDF-13C 2.00 68-----1,2,3,4,7,8,9-HpCDF-13C 2.00 601,2,3,4,7,8-HxCDF ND 2.0 1,2,3,4,6,7,8-HpCDD-13C 2.00 65-----1,2,3,6,7,8-HxCDF ND 2.1 OCDD-13C 4.00 61-----2,3,4,6,7,8-HxCDF ND 2.2-----1,2,3,7,8,9-HxCDF ND 3.1 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 2.0 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 3.5 2,3,7,8-TCDD-37Cl4 0.20 85-----1,2,3,6,7,8-HxCDD ND 2.7-----1,2,3,7,8,9-HxCDD ND 2.9-----Total HxCDD ND 2.7-----
1,2,3,4,6,7,8-HpCDF ND 3.9 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 5.8 Equivalence: 0.19 pg/L-----Total HpCDF 7.1 3.9 (Lower-bound - Using 2005 WHO Factors)BJ-----
1,2,3,4,6,7,8-HpCDD 18 2.5 BJ-----Total HpCDD 18 2.5 BJ-----
OCDF ND 12-----OCDD 41 16 J-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank level
EDL = Estimated Detection Limit
Page 20 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 168 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ13WG-09152392688280010U231021B_05BAL
NA937 mL
NAU230926U231021B_02 & U231021B_18BLANK-108749
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/15/2023 10:0609/27/2023 16:4510/10/2023 10:4110/21/2023 17:07
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 1.1 2,3,7,8-TCDF-13C 2.00 70-----Total TCDF ND 1.1 2,3,7,8-TCDD-13C 2.00 69-----1,2,3,7,8-PeCDF-13C 2.00 682,3,7,8-TCDD ND 2.0 2,3,4,7,8-PeCDF-13C 2.00 68-----Total TCDD ND 2.0 1,2,3,7,8-PeCDD-13C 2.00 75-----1,2,3,4,7,8-HxCDF-13C 2.00 871,2,3,7,8-PeCDF ND 1.2 1,2,3,6,7,8-HxCDF-13C 2.00 85-----2,3,4,7,8-PeCDF ND 0.83 2,3,4,6,7,8-HxCDF-13C 2.00 85-----Total PeCDF ND 0.83 1,2,3,7,8,9-HxCDF-13C 2.00 75-----1,2,3,4,7,8-HxCDD-13C 2.00 821,2,3,7,8-PeCDD ND 1.2 1,2,3,6,7,8-HxCDD-13C 2.00 87-----Total PeCDD ND 1.2 1,2,3,4,6,7,8-HpCDF-13C 2.00 70-----1,2,3,4,7,8,9-HpCDF-13C 2.00 631,2,3,4,7,8-HxCDF ND 0.68 1,2,3,4,6,7,8-HpCDD-13C 2.00 73-----1,2,3,6,7,8-HxCDF -----0.69 OCDD-13C 4.00 55IJ0.752,3,4,6,7,8-HxCDF ND 0.66-----1,2,3,7,8,9-HxCDF -----0.91 1,2,3,4-TCDD-13C 2.00 NAIJ1.2Total HxCDF ND 0.66 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD -----1.2 2,3,7,8-TCDD-37Cl4 0.20 71IJ2.51,2,3,6,7,8-HxCDD ND 0.97-----1,2,3,7,8,9-HxCDD ND 1.0-----Total HxCDD ND 0.97-----
1,2,3,4,6,7,8-HpCDF ND 1.8 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 2.7 Equivalence: 0.49 pg/L-----Total HpCDF ND 1.8 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----1.4 IJ3.2Total HpCDD ND 1.4-----
OCDF 5.2 3.7 J-----OCDD -----4.2 IJ19
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
I=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 21 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 169 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ07WG-09152392688280011-RU231027A_15JF
NA102 mL
NAU230926U231026A_23 & U231027A_16BLANK-108989
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/15/2023 11:0009/27/2023 16:4510/24/2023 10:0010/27/2023 12:58
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 26 2,3,7,8-TCDF-13C 2.00 44-----Total TCDF ND 26 2,3,7,8-TCDD-13C 2.00 41-----1,2,3,7,8-PeCDF-13C 2.00 31 R2,3,7,8-TCDD ND 35 2,3,4,7,8-PeCDF-13C 2.00 33-----RTotal TCDD ND 35 1,2,3,7,8-PeCDD-13C 2.00 35-----R1,2,3,4,7,8-HxCDF-13C 2.00 34 R1,2,3,7,8-PeCDF ND 35 1,2,3,6,7,8-HxCDF-13C 2.00 33-----R2,3,4,7,8-PeCDF ND 24 2,3,4,6,7,8-HxCDF-13C 2.00 33-----RTotal PeCDF ND 24 1,2,3,7,8,9-HxCDF-13C 2.00 27-----R1,2,3,4,7,8-HxCDD-13C 2.00 32 R1,2,3,7,8-PeCDD ND 27 1,2,3,6,7,8-HxCDD-13C 2.00 36-----RTotal PeCDD 67 27 1,2,3,4,6,7,8-HpCDF-13C 2.00 25J-----R1,2,3,4,7,8,9-HpCDF-13C 2.00 20 R1,2,3,4,7,8-HxCDF ND 38 1,2,3,4,6,7,8-HpCDD-13C 2.00 26-----R1,2,3,6,7,8-HxCDF ND 38 OCDD-13C 4.00 24-----R2,3,4,6,7,8-HxCDF ND 37-----1,2,3,7,8,9-HxCDF ND 57 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 37 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 40 2,3,7,8-TCDD-37Cl4 0.20 85-----1,2,3,6,7,8-HxCDD -----33 IJ561,2,3,7,8,9-HxCDD ND 35-----Total HxCDD 200 33 J-----
1,2,3,4,6,7,8-HpCDF -----63 Total 2,3,7,8-TCDDIJ1201,2,3,4,7,8,9-HpCDF ND 110 Equivalence: 15 pg/L-----Total HpCDF 600 63 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD 770 58-----Total HpCDD 1300 58-----
OCDF -----140 IJ450OCDD1600200-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
R=Recovery outside target rangeI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 22 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 170 of 183
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
BLANK-108695L231011A_12
SMT
968 mLL230816L231011A_06 & L231011A_24
MatrixDilutionExtractedAnalyzed
Water
10/06/2023 11:3110/11/2023 14:08
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKSK
NativeIsomers pg/LConc EMPCpg/L pg/L InternalStandards Addedng's PercentRecoveryEDL
2,3,7,8-TCDF ND -----0.75 2,3,7,8-TCDF-13C 2.00 72Total TCDF ND -----0.75 2,3,7,8-TCDD-13C 2.00 701,2,3,7,8-PeCDF-13C 2.00 772,3,7,8-TCDD ND -----1.1 2,3,4,7,8-PeCDF-13C 2.00 73Total TCDD ND -----1.1 1,2,3,7,8-PeCDD-13C 2.00 961,2,3,4,7,8-HxCDF-13C 2.00 821,2,3,7,8-PeCDF ND -----0.49 1,2,3,6,7,8-HxCDF-13C 2.00 652,3,4,7,8-PeCDF -----0.54 0.35 IJ 2,3,4,6,7,8-HxCDF-13C 2.00 59Total PeCDF ND -----0.35 1,2,3,7,8,9-HxCDF-13C 2.00 631,2,3,4,7,8-HxCDD-13C 2.00 641,2,3,7,8-PeCDD -----1.0 0.71 IJ 1,2,3,6,7,8-HxCDD-13C 2.00 79Total PeCDD ND -----0.71 1,2,3,4,6,7,8-HpCDF-13C 2.00 761,2,3,4,7,8,9-HpCDF-13C 2.00 741,2,3,4,7,8-HxCDF 1.3 -----0.23 J 1,2,3,4,6,7,8-HpCDD-13C 2.00 811,2,3,6,7,8-HxCDF -----0.58 0.30 IJ OCDD-13C 4.00 622,3,4,6,7,8-HxCDF -----0.81 0.31 IJ1,2,3,7,8,9-HxCDF 2.0 -----0.38 J 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF 3.3 -----0.23 J 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 2.3 -----0.62 J 2,3,7,8-TCDD-37Cl4 0.20 671,2,3,6,7,8-HxCDD 1.0 -----0.47 J1,2,3,7,8,9-HxCDD -----1.4 0.52 IJTotal HxCDD 3.3 -----0.47 J
1,2,3,4,6,7,8-HpCDF -----1.2 1.1 IJ Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----1.5 Equivalence: 2.2 pg/LTotal HpCDF ND -----1.1 (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD 2.0 -----1.7 JTotal HpCDD 2.0 -----1.7 J
OCDF ND -----2.1OCDD15-----3.9 J
Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
I =Isotope ratio out of specification
EDL=EstimatedDetection Limit
Page 23 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 171 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
BLANK-108749L231014A_14
JRH
1010 mLL230816L231014A_01 & L231014A_18
MatrixDilutionExtractedAnalyzed
Water
10/10/2023 10:4110/14/2023 21:04
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKTA
NativeIsomers pg/LConc EMPCpg/L pg/L InternalStandards Addedng's PercentRecoveryEDL
2,3,7,8-TCDF ND -----0.99 2,3,7,8-TCDF-13C 2.00 73Total TCDF ND -----0.99 2,3,7,8-TCDD-13C 2.00 711,2,3,7,8-PeCDF-13C 2.00 752,3,7,8-TCDD ND -----0.97 2,3,4,7,8-PeCDF-13C 2.00 73Total TCDD ND -----0.97 1,2,3,7,8-PeCDD-13C 2.00 921,2,3,4,7,8-HxCDF-13C 2.00 631,2,3,7,8-PeCDF ND -----0.78 1,2,3,6,7,8-HxCDF-13C 2.00 782,3,4,7,8-PeCDF ND -----0.61 2,3,4,6,7,8-HxCDF-13C 2.00 68Total PeCDF ND -----0.61 1,2,3,7,8,9-HxCDF-13C 2.00 691,2,3,4,7,8-HxCDD-13C 2.00 671,2,3,7,8-PeCDD ND -----0.97 1,2,3,6,7,8-HxCDD-13C 2.00 85Total PeCDD ND -----0.97 1,2,3,4,6,7,8-HpCDF-13C 2.00 641,2,3,4,7,8,9-HpCDF-13C 2.00 611,2,3,4,7,8-HxCDF ND -----1.0 1,2,3,4,6,7,8-HpCDD-13C 2.00 651,2,3,6,7,8-HxCDF ND -----0.87 OCDD-13C 4.00 422,3,4,6,7,8-HxCDF ND -----0.881,2,3,7,8,9-HxCDF 1.7 -----1.2 J 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF 1.7 -----0.87 J 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 2.2 -----0.88 J 2,3,7,8-TCDD-37Cl4 0.20 801,2,3,6,7,8-HxCDD -----0.66 0.65 IJ1,2,3,7,8,9-HxCDD ND -----0.73Total HxCDD 2.2 -----0.65 J
1,2,3,4,6,7,8-HpCDF ND -----2.1 Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----3.5 Equivalence: 0.51 pg/LTotal HpCDF 3.5 -----2.1 J (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD 4.8 -----2.8 JTotal HpCDD 4.8 -----2.8 J
OCDF -----6.0 4.2 IJOCDD31-----7.2 J
Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
I =Isotope ratio out of specification
EDL=EstimatedDetection Limit
Page 24 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 172 of 183
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
BLANK-108989L231026B_09
SMT
955 mLL230816L231026B_03 & L231026B_22
MatrixDilutionExtractedAnalyzed
Water
10/24/2023 10:0010/26/2023 17:47
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKVM
NativeIsomers pg/LConc EMPCpg/L pg/L InternalStandards Addedng's PercentRecoveryEDL
2,3,7,8-TCDF ND -----0.89 2,3,7,8-TCDF-13C 2.00 78Total TCDF ND -----0.89 2,3,7,8-TCDD-13C 2.00 721,2,3,7,8-PeCDF-13C 2.00 742,3,7,8-TCDD ND -----1.4 2,3,4,7,8-PeCDF-13C 2.00 73Total TCDD ND -----1.4 1,2,3,7,8-PeCDD-13C 2.00 791,2,3,4,7,8-HxCDF-13C 2.00 941,2,3,7,8-PeCDF -----1.8 1.2 IJ 1,2,3,6,7,8-HxCDF-13C 2.00 912,3,4,7,8-PeCDF ND -----0.72 2,3,4,6,7,8-HxCDF-13C 2.00 84Total PeCDF ND -----0.72 1,2,3,7,8,9-HxCDF-13C 2.00 771,2,3,4,7,8-HxCDD-13C 2.00 741,2,3,7,8-PeCDD ND -----1.5 1,2,3,6,7,8-HxCDD-13C 2.00 92Total PeCDD ND -----1.5 1,2,3,4,6,7,8-HpCDF-13C 2.00 721,2,3,4,7,8,9-HpCDF-13C 2.00 591,2,3,4,7,8-HxCDF ND -----1.5 1,2,3,4,6,7,8-HpCDD-13C 2.00 701,2,3,6,7,8-HxCDF ND -----1.7 OCDD-13C 4.00 66 Y2,3,4,6,7,8-HxCDF ND -----1.71,2,3,7,8,9-HxCDF ND -----2.4 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF ND -----1.5 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD ND -----1.3 2,3,7,8-TCDD-37Cl4 0.20 851,2,3,6,7,8-HxCDD -----2.1 1.1 IJ1,2,3,7,8,9-HxCDD ND -----1.2Total HxCDD 2.2 -----1.1 J
1,2,3,4,6,7,8-HpCDF ND -----8.3 Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----14 Equivalence: 0.51 pg/LTotal HpCDF 20 -----8.3 J (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD 22 -----2.3 JTotal HpCDD 39 -----2.3 J
OCDF 39 -----6.2 JOCDD-----53 7.9 IJ
Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
I =Isotope ratio out of specification
Y=Calculated using average of daily RFs
EDL=EstimatedDetection Limit
Page 25 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 173 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCS-108696L231011A_08
SMT
973 mLL230816L231011A_06 & L231011A_24
MatrixDilutionExtractedAnalyzed
Water
10/06/2023 11:3110/11/2023 11:20
NA
Method Blank ID BLANK-108695
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.19 2,3,7,8-TCDF-13C 2.0 6294Total TCDF 2,3,7,8-TCDD-13C 2.0 601,2,3,7,8-PeCDF-13C 2.0 672,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.0 63106Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 771,2,3,4,7,8-HxCDF-13C 2.0 761,2,3,7,8-PeCDF 1.0 0.91 1,2,3,6,7,8-HxCDF-13C 2.0 61912,3,4,7,8-PeCDF 1.0 0.91 2,3,4,6,7,8-HxCDF-13C 2.0 5491Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 551,2,3,4,7,8-HxCDD-13C 2.0 571,2,3,7,8-PeCDD 1.0 0.96 1,2,3,6,7,8-HxCDD-13C 2.0 7196Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 611,2,3,4,7,8,9-HpCDF-13C 2.0 671,2,3,4,7,8-HxCDF 1.0 0.97 1,2,3,4,6,7,8-HpCDD-13C 2.0 63971,2,3,6,7,8-HxCDF 1.0 0.90 OCDD-13C 4.0 48902,3,4,6,7,8-HxCDF 1.0 0.97 971,2,3,7,8,9-HxCDF 1.0 0.95 1,2,3,4-TCDD-13C 2.0 NA95Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.1 2,3,7,8-TCDD-37Cl4 0.20 681071,2,3,6,7,8-HxCDD 1.0 0.94 941,2,3,7,8,9-HxCDD 1.0 1.0 104Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.97 971,2,3,4,7,8,9-HpCDF 1.0 0.94 94Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.88 88Total HpCDD
OCDF 2.0 1.6 82OCDD2.0 1.6 82
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 26 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 174 of 183
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCS-108750L231014A_02
JRH
1020 mLL230816L231014A_01 & L231014A_18
MatrixDilutionExtractedAnalyzed
Water
10/10/2023 10:4110/14/2023 12:40
NA
Method Blank ID BLANK-108749
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.17 2,3,7,8-TCDF-13C 2.0 4886Total TCDF 2,3,7,8-TCDD-13C 2.0 451,2,3,7,8-PeCDF-13C 2.0 482,3,7,8-TCDD 0.20 0.19 2,3,4,7,8-PeCDF-13C 2.0 4696Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 591,2,3,4,7,8-HxCDF-13C 2.0 571,2,3,7,8-PeCDF 1.0 0.84 1,2,3,6,7,8-HxCDF-13C 2.0 47842,3,4,7,8-PeCDF 1.0 0.85 2,3,4,6,7,8-HxCDF-13C 2.0 4485Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 481,2,3,4,7,8-HxCDD-13C 2.0 441,2,3,7,8-PeCDD 1.0 0.84 1,2,3,6,7,8-HxCDD-13C 2.0 5484Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 461,2,3,4,7,8,9-HpCDF-13C 2.0 431,2,3,4,7,8-HxCDF 1.0 0.88 1,2,3,4,6,7,8-HpCDD-13C 2.0 45881,2,3,6,7,8-HxCDF 1.0 0.89 OCDD-13C 4.0 3289 R2,3,4,6,7,8-HxCDF 1.0 0.89 891,2,3,7,8,9-HxCDF 1.0 0.91 1,2,3,4-TCDD-13C 2.0 NA91Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 0.98 2,3,7,8-TCDD-37Cl4 0.20 73981,2,3,6,7,8-HxCDD 1.0 0.90 901,2,3,7,8,9-HxCDD 1.0 0.96 96Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 1.00 1001,2,3,4,7,8,9-HpCDF 1.0 0.95 95Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.91 91Total HpCDD
OCDF 2.0 1.9 97OCDD2.0 2.1 104
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 27 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 175 of 183
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCS-108990L231026B_05
SMT
931 mLL230816L231026B_03 & L231026B_22
MatrixDilutionExtractedAnalyzed
Water
10/24/2023 10:0010/26/2023 15:03
NA
Method Blank ID BLANK-108989
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.17 2,3,7,8-TCDF-13C 2.0 7586Total TCDF 2,3,7,8-TCDD-13C 2.0 691,2,3,7,8-PeCDF-13C 2.0 732,3,7,8-TCDD 0.20 0.19 2,3,4,7,8-PeCDF-13C 2.0 7394Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 781,2,3,4,7,8-HxCDF-13C 2.0 921,2,3,7,8-PeCDF 1.0 0.84 1,2,3,6,7,8-HxCDF-13C 2.0 92842,3,4,7,8-PeCDF 1.0 0.84 2,3,4,6,7,8-HxCDF-13C 2.0 8684Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 761,2,3,4,7,8-HxCDD-13C 2.0 831,2,3,7,8-PeCDD 1.0 0.81 1,2,3,6,7,8-HxCDD-13C 2.0 9681Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 751,2,3,4,7,8,9-HpCDF-13C 2.0 621,2,3,4,7,8-HxCDF 1.0 0.84 1,2,3,4,6,7,8-HpCDD-13C 2.0 75841,2,3,6,7,8-HxCDF 1.0 0.88 OCDD-13C 4.0 7088 Y2,3,4,6,7,8-HxCDF 1.0 0.91 911,2,3,7,8,9-HxCDF 1.0 0.87 1,2,3,4-TCDD-13C 2.0 NA87Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 0.93 2,3,7,8-TCDD-37Cl4 0.20 72931,2,3,6,7,8-HxCDD 1.0 0.86 861,2,3,7,8,9-HxCDD 1.0 0.87 87Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.91 911,2,3,4,7,8,9-HpCDF 1.0 0.90 90Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.83 83Total HpCDD
OCDF 2.0 1.9 94OCDD2.0 1.9 97
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 28 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 176 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCSD-108751L231014A_03
JRH
1010 mLL230816L231014A_01 & L231014A_18
MatrixDilutionExtractedAnalyzed
Water
10/10/2023 10:4110/14/2023 13:22
NA
Method Blank ID BLANK-108749
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.18 2,3,7,8-TCDF-13C 2.0 3489 RTotal TCDF 2,3,7,8-TCDD-13C 2.0 33 R1,2,3,7,8-PeCDF-13C 2.0 34 R2,3,7,8-TCDD 0.20 0.20 2,3,4,7,8-PeCDF-13C 2.0 35100 RTotal TCDD 1,2,3,7,8-PeCDD-13C 2.0 431,2,3,4,7,8-HxCDF-13C 2.0 37 R1,2,3,7,8-PeCDF 1.0 0.87 1,2,3,6,7,8-HxCDF-13C 2.0 3587 R2,3,4,7,8-PeCDF 1.0 0.86 2,3,4,6,7,8-HxCDF-13C 2.0 3486 RTotal PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 34 R1,2,3,4,7,8-HxCDD-13C 2.0 33 R1,2,3,7,8-PeCDD 1.0 0.88 1,2,3,6,7,8-HxCDD-13C 2.0 3988 RTotal PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 33 R1,2,3,4,7,8,9-HpCDF-13C 2.0 32 R1,2,3,4,7,8-HxCDF 1.0 0.88 1,2,3,4,6,7,8-HpCDD-13C 2.0 3488 R1,2,3,6,7,8-HxCDF 1.0 0.91 OCDD-13C 4.0 2591 R2,3,4,6,7,8-HxCDF 1.0 0.90 901,2,3,7,8,9-HxCDF 1.0 0.91 1,2,3,4-TCDD-13C 2.0 NA91Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 0.97 2,3,7,8-TCDD-37Cl4 0.20 71971,2,3,6,7,8-HxCDD 1.0 0.98 981,2,3,7,8,9-HxCDD 1.0 0.98 98Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.99 991,2,3,4,7,8,9-HpCDF 1.0 0.96 96Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.95 95Total HpCDD
OCDF 2.0 2.0 99OCDD2.0 2.1 107
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 29 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 177 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCSD-108991L231026B_06
SMT
966 mLL230816L231026B_03 & L231026B_22
MatrixDilutionExtractedAnalyzed
Water
10/24/2023 10:0010/26/2023 15:44
NA
Method Blank ID BLANK-108989
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.17 2,3,7,8-TCDF-13C 2.0 7686Total TCDF 2,3,7,8-TCDD-13C 2.0 731,2,3,7,8-PeCDF-13C 2.0 702,3,7,8-TCDD 0.20 0.18 2,3,4,7,8-PeCDF-13C 2.0 7288Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 771,2,3,4,7,8-HxCDF-13C 2.0 771,2,3,7,8-PeCDF 1.0 0.83 1,2,3,6,7,8-HxCDF-13C 2.0 85832,3,4,7,8-PeCDF 1.0 0.82 2,3,4,6,7,8-HxCDF-13C 2.0 9282Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 791,2,3,4,7,8-HxCDD-13C 2.0 911,2,3,7,8-PeCDD 1.0 0.79 1,2,3,6,7,8-HxCDD-13C 2.0 9879Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 721,2,3,4,7,8,9-HpCDF-13C 2.0 491,2,3,4,7,8-HxCDF 1.0 0.79 1,2,3,4,6,7,8-HpCDD-13C 2.0 71791,2,3,6,7,8-HxCDF 1.0 0.90 OCDD-13C 4.0 8690 Y2,3,4,6,7,8-HxCDF 1.0 0.87 871,2,3,7,8,9-HxCDF 1.0 0.79 1,2,3,4-TCDD-13C 2.0 NA79Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 0.82 2,3,7,8-TCDD-37Cl4 0.20 82821,2,3,6,7,8-HxCDD 1.0 0.88 881,2,3,7,8,9-HxCDD 1.0 0.82 82Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.86 861,2,3,4,7,8,9-HpCDF 1.0 0.89 89Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.79 79Total HpCDD
OCDF 2.0 1.7 85OCDD2.0 1.9 94
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 30 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 178 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Client
Spike 1 IDSpike 1 Filename L231014A_02LCS-108750
PACE Charlotte
Spike Recovery Relative Percent Difference (RPD) Results
Spike 2 IDSpike 2 Filename L231014A_03LCSD-108751
Method 8290A
Spike 1 Spike 2Compound%REC %REC %RPD
2,3,7,8-TCDF 86 89 3.42,3,7,8-TCDD 96 100 4.11,2,3,7,8-PeCDF 84 87 3.52,3,4,7,8-PeCDF 85 86 1.21,2,3,7,8-PeCDD 84 88 4.71,2,3,4,7,8-HxCDF 88 88 0.01,2,3,6,7,8-HxCDF 89 91 2.22,3,4,6,7,8-HxCDF 89 90 1.11,2,3,7,8,9-HxCDF 91 91 0.01,2,3,4,7,8-HxCDD 98 97 1.01,2,3,6,7,8-HxCDD 90 98 8.51,2,3,7,8,9-HxCDD 96 98 2.11,2,3,4,6,7,8-HpCDF 100 99 1.01,2,3,4,7,8,9-HpCDF 95 96 1.01,2,3,4,6,7,8-HpCDD 91 95 4.3OCDF97992.0OCDD1041072.8
%REC = Percent RecoveredRPD=The differencebetweenthetwo valuesdivided by the mean value
Page 31 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 179 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Client
Spike 1 IDSpike 1 Filename L231026B_05LCS-108990
PACE Charlotte
Spike Recovery Relative Percent Difference (RPD) Results
Spike 2 IDSpike 2 Filename L231026B_06LCSD-108991
Method 8290A
Spike 1 Spike 2Compound%REC %REC %RPD
2,3,7,8-TCDF 86 86 0.02,3,7,8-TCDD 94 88 6.61,2,3,7,8-PeCDF 84 83 1.22,3,4,7,8-PeCDF 84 82 2.41,2,3,7,8-PeCDD 81 79 2.51,2,3,4,7,8-HxCDF 84 79 6.11,2,3,6,7,8-HxCDF 88 90 2.22,3,4,6,7,8-HxCDF 91 87 4.51,2,3,7,8,9-HxCDF 87 79 9.61,2,3,4,7,8-HxCDD 93 82 12.61,2,3,6,7,8-HxCDD 86 88 2.31,2,3,7,8,9-HxCDD 87 82 5.91,2,3,4,6,7,8-HpCDF 91 86 5.61,2,3,4,7,8,9-HpCDF 90 89 1.11,2,3,4,6,7,8-HpCDD 83 79 4.9OCDF948510.1OCDD97943.1
%REC = Percent RecoveredRPD=The differencebetweenthetwo valuesdivided by the mean value
Page 32 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 180 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
92688280008-MSL231016A_01
JRH
843 mLL230816L231015B_17 & L231016A_18
MatrixDilutionExtractedAnalyzed
WATER
10/06/2023 11:3110/16/2023 01:23
Client - PACE Charlotte
NA
Method Blank ID BLANK-108695
Client's Sample ID BR03WG-091423-MS
Method 8290A Spiked Sample Report
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.18 2,3,7,8-TCDF-13C 2.00 66902,3,7,8-TCDD-13C 2.00 681,2,3,7,8-PeCDF-13C 2.00 682,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.00 661031,2,3,7,8-PeCDD-13C 2.00 791,2,3,4,7,8-HxCDF-13C 2.00 611,2,3,7,8-PeCDF 1.00 0.82 1,2,3,6,7,8-HxCDF-13C 2.00 75822,3,4,7,8-PeCDF 1.00 0.82 2,3,4,6,7,8-HxCDF-13C 2.00 71821,2,3,7,8,9-HxCDF-13C 2.00 651,2,3,4,7,8-HxCDD-13C 2.00 771,2,3,7,8-PeCDD 1.00 0.83 1,2,3,6,7,8-HxCDD-13C 2.00 82831,2,3,4,6,7,8-HpCDF-13C 2.00 641,2,3,4,7,8,9-HpCDF-13C 2.00 76 Y1,2,3,4,7,8-HxCDF 1.00 0.88 1,2,3,4,6,7,8-HpCDD-13C 2.00 68881,2,3,6,7,8-HxCDF 1.00 0.84 OCDD-13C 4.00 7184 Y2,3,4,6,7,8-HxCDF 1.00 0.86 861,2,3,7,8,9-HxCDF 1.00 0.84 1,2,3,4-TCDD-13C 2.00 NA841,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 1.00 0.94 2,3,7,8-TCDD-37Cl4 0.20 84941,2,3,6,7,8-HxCDD 1.00 0.86 861,2,3,7,8,9-HxCDD 1.00 0.88 88
1,2,3,4,6,7,8-HpCDF 1.00 0.93 931,2,3,4,7,8,9-HpCDF 1.00 0.96 96
1,2,3,4,6,7,8-HpCDD 1.00 0.97 96
OCDF 2.00 1.90 95OCDD2.00 2.28 113
Y =Calculated using average of daily RFs
Qs = Quantity Spiked Qm = Quantity Measured Rec. = Recovery (Expressed as Percent)
Page 33 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 181 of 183
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
92688280008-MSDL231016A_02
JRH
968 mLL230816L231015B_17 & L231016A_18
MatrixDilutionExtractedAnalyzed
WATER
10/06/2023 11:3110/16/2023 02:05
Client - PACE Charlotte
NA
Method Blank ID BLANK-108695
Client's Sample ID BR03WG-091423-MSD
Method 8290A Spiked Sample Report
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.20 2,3,7,8-TCDF-13C 2.00 50992,3,7,8-TCDD-13C 2.00 501,2,3,7,8-PeCDF-13C 2.00 522,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.00 531061,2,3,7,8-PeCDD-13C 2.00 621,2,3,4,7,8-HxCDF-13C 2.00 37 R1,2,3,7,8-PeCDF 1.00 0.85 1,2,3,6,7,8-HxCDF-13C 2.00 64852,3,4,7,8-PeCDF 1.00 0.86 2,3,4,6,7,8-HxCDF-13C 2.00 57861,2,3,7,8,9-HxCDF-13C 2.00 421,2,3,4,7,8-HxCDD-13C 2.00 601,2,3,7,8-PeCDD 1.00 0.87 1,2,3,6,7,8-HxCDD-13C 2.00 72871,2,3,4,6,7,8-HpCDF-13C 2.00 541,2,3,4,7,8,9-HpCDF-13C 2.00 64 Y1,2,3,4,7,8-HxCDF 1.00 0.85 1,2,3,4,6,7,8-HpCDD-13C 2.00 57851,2,3,6,7,8-HxCDF 1.00 0.81 OCDD-13C 4.00 5581 Y2,3,4,6,7,8-HxCDF 1.00 0.90 901,2,3,7,8,9-HxCDF 1.00 0.89 1,2,3,4-TCDD-13C 2.00 NA891,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD 1.00 0.96 2,3,7,8-TCDD-37Cl4 0.20 65961,2,3,6,7,8-HxCDD 1.00 0.85 851,2,3,7,8,9-HxCDD 1.00 0.82 82
1,2,3,4,6,7,8-HpCDF 1.00 0.87 871,2,3,4,7,8,9-HpCDF 1.00 0.97 97
1,2,3,4,6,7,8-HpCDD 1.00 0.97 97
OCDF 2.00 1.99 100OCDD2.00 2.37 117
R=Recovery outside target rangeY =Calculated using average of daily RFs
Qs = Quantity Spiked Qm = Quantity Measured Rec. = Recovery (Expressed as Percent)
Page 34 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 182 of 183
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]Method 8290A Spike Sample Results
Client - PACE Charlotte
Client Sample ID
Lab Sample ID
MS ID
MSD ID
BR03WG-091423
92688280008
92688280008-MS
92688280008-MSD
Sample Filename
MS Filename
MSD Filename
U231021A_03
L231016A_01
L231016A_02
Analyte
Quantity Unspiked Sample Contribution
to MS to MSD
Quantity Measured
MS MSD
RPD
Spiked
(ng)
Subtracted Recovery
MS MSD
(ng)(ng)(ng)(ng)(%)(%)
2,3,7,8-TCDF 0.20 ND ND 0.18 0.20 90 9910.0
2,3,7,8-TCDD 0.20 ND ND 0.21 0.21 103 1063.0
1,2,3,7,8-PeCDF 1.00 ND ND 0.82 0.85 82 853.6
2,3,4,7,8-PeCDF 1.00 ND ND 0.82 0.86 82 865.0
1,2,3,7,8-PeCDD 1.00 ND ND 0.83 0.87 83 874.6
1,2,3,4,7,8-HxCDF 1.00 ND ND 0.88 0.85 88 853.6
1,2,3,6,7,8-HxCDF 1.00 ND ND 0.84 0.81 84 813.7
2,3,4,6,7,8-HxCDF 1.00 ND ND 0.86 0.90 86 904.7
1,2,3,7,8,9-HxCDF 1.00 ND ND 0.84 0.89 84 895.8
1,2,3,4,7,8-HxCDD 1.00 ND ND 0.94 0.96 94 962.6
1,2,3,6,7,8-HxCDD 1.00 ND ND 0.86 0.85 86 851.0
1,2,3,7,8,9-HxCDD 1.00 ND ND 0.88 0.82 88 826.7
1,2,3,4,6,7,8-HpCDF 1.00 ND ND 0.93 0.87 93 877.1
1,2,3,4,7,8,9-HpCDF 1.00 ND ND 0.96 0.97 96 971.1
1,2,3,4,6,7,8-HpCDD 1.00 0.00335 0.00384 0.97 0.97 96 970.4
OCDF 2.00 ND ND 1.90 1.99 95 1004.7
OCDD 2.00 0.0219 0.0251 2.28 2.37 113 1174.1
Quantity Spiked - the amount of analyte spiked into the spiked samplesUnspiked Sample Contribution - calculated based on the amount found in the sample and the extracted amounts of the spiked and unspiked samplesQuantity Measured - the total amount of analyte measured in the spiked samplesRPD - the Relative Percent Difference of the spiked sample Quantity Measured valuesSubtracted Recovery - calculated after subtracting the unspiked sample contribution
Page 35 of 35Report No.....10670311_SW8290AFC_L2_dfr
Page 183 of 183
#=CL#
October 18, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92688596
92688596
Project:
Pace Project No.:
RE:
Christina AshdownENSAFE313 Wingo WayMount Pleasant, SC 29464
Pactiv Evergreen GWS
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on September 18, 2023. The results relate onlyto the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and thelaboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc: Jennings Kerr, ENSAFE Inc.
Lab, ENSAFE Inc.
David Warren, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 48
#=CP#
CERTIFICATIONS
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Project:
92688596
Pactiv Evergreen GWS
Pace Analytical Services Ormond Beach
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Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 48
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Lab ID Sample ID Matrix Date Collected Date Received
92688596001 PZ18WG-091823 Water 09/18/23 15:30 09/18/23 17:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 48
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92688596001 PZ18WG-091823 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OKC2
EPA 6010 17 PASI-OTMA
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-AYEG
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Sample: PZ18WG-091823 Lab ID: 92688596001 Collected: 09/18/23 15:30 Received: 09/18/23 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 5.8 Std. Units 09/19/23 14:0210
True Color 500 units 09/19/23 14:0250.0 50.0 10
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/13/23 23:30 7440-36-010/13/23 00:2015.0 5.5 1
Arsenic ND ug/L 10/13/23 23:30 7440-38-210/13/23 00:2010.0 3.4 1
Barium 168 ug/L 10/13/23 23:30 7440-39-310/13/23 00:2010.0 0.84 1
Beryllium 0.81J ug/L 10/13/23 23:30 7440-41-710/13/23 00:204.0 0.17 1
Boron ND ug/L 10/13/23 23:30 7440-42-810/13/23 00:2050.0 12.4 1
Cadmium 0.89J ug/L 10/13/23 23:30 7440-43-910/13/23 00:201.0 0.33 1
Chromium ND ug/L 10/13/23 23:30 7440-47-310/13/23 00:205.0 1.7 1
Cobalt 1.6J ug/L 10/13/23 23:30 7440-48-410/13/23 00:2010.0 0.96 1
Copper ND ug/L 10/13/23 23:30 7440-50-810/13/23 00:205.0 2.6 1
Lead ND ug/L 10/13/23 23:30 7439-92-110/13/23 00:2010.0 2.1 1
Manganese 630 ug/L 10/13/23 23:30 7439-96-510/13/23 00:205.0 1.1 1
Nickel ND ug/L 10/13/23 23:30 7440-02-010/13/23 00:205.0 1.0 1
Selenium ND ug/L 10/13/23 23:30 7782-49-210/13/23 00:2015.0 3.9 1
Silver ND ug/L 10/13/23 23:30 7440-22-410/13/23 00:205.0 1.0 1
Thallium ND ug/L 10/13/23 23:30 7440-28-010/13/23 00:2015.0 2.9 1
Vanadium ND ug/L 10/13/23 23:30 7440-62-210/13/23 00:2010.0 1.0 1
Zinc ND ug/L 10/13/23 23:30 7440-66-610/13/23 00:2020.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/17/23 17:46 7440-36-010/17/23 04:2515.0 5.5 1
Arsenic, Dissolved ND ug/L 10/17/23 17:46 7440-38-210/17/23 04:2510.0 3.4 1
Barium, Dissolved 172 ug/L 10/17/23 17:46 7440-39-310/17/23 04:2510.0 0.84 1
Beryllium, Dissolved ND ug/L 10/17/23 17:46 7440-41-710/17/23 04:254.0 0.17 1
Boron, Dissolved ND ug/L 10/17/23 17:46 7440-42-810/17/23 04:2550.0 12.4 1
Cadmium, Dissolved 0.58J ug/L 10/17/23 17:46 7440-43-910/17/23 04:251.0 0.33 1
Chromium, Dissolved ND ug/L 10/17/23 17:46 7440-47-310/17/23 04:255.0 1.7 1
Cobalt, Dissolved 3.3J ug/L 10/17/23 17:46 7440-48-410/17/23 04:2510.0 0.96 1
Copper, Dissolved ND ug/L 10/17/23 17:46 7440-50-810/17/23 04:255.0 2.6 1
Lead, Dissolved ND ug/L 10/17/23 17:46 7439-92-110/17/23 04:2510.0 2.1 1
Manganese, Dissolved 610 ug/L 10/17/23 17:46 7439-96-510/17/23 04:255.0 1.1 1
Nickel, Dissolved ND ug/L 10/17/23 17:46 7440-02-010/17/23 04:255.0 1.0 1
Selenium, Dissolved ND ug/L 10/17/23 17:46 7782-49-210/17/23 04:2515.0 3.9 1
Silver, Dissolved ND ug/L 10/17/23 17:46 7440-22-410/17/23 04:255.0 1.0 1
Thallium, Dissolved ND ug/L 10/17/23 17:46 7440-28-010/17/23 04:2515.0 2.9 1
Vanadium, Dissolved 1.4J ug/L 10/17/23 17:46 7440-62-210/17/23 04:2510.0 1.0 1
Zinc, Dissolved ND ug/L 10/17/23 17:46 7440-66-610/17/23 04:2520.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Sample: PZ18WG-091823 Lab ID: 92688596001 Collected: 09/18/23 15:30 Received: 09/18/23 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/16/23 11:02 7439-97-610/16/23 07:290.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/16/23 10:25 7439-97-610/16/23 07:290.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/25/23 14:47 83-32-909/23/23 09:368.3 1.7 1
Acenaphthylene ND ug/L 09/25/23 14:47 208-96-809/23/23 09:368.3 1.6 1
Acetophenone ND ug/L 09/25/23 14:47 98-86-209/23/23 09:368.3 1.2 1
Anthracene ND ug/L 09/25/23 14:47 120-12-709/23/23 09:368.3 1.9 1
Atrazine ND ug/L 09/25/23 14:47 1912-24-909/23/23 09:368.3 2.6 1
Benzaldehyde ND ug/L 09/25/23 14:47 100-52-709/23/23 09:368.3 3.0 1
Benzo(a)anthracene ND ug/L 09/25/23 14:47 56-55-309/23/23 09:368.3 2.2 1
Benzo(a)pyrene ND ug/L 09/25/23 14:47 50-32-809/23/23 09:368.3 2.3 1
Benzo(b)fluoranthene ND ug/L 09/25/23 14:47 205-99-209/23/23 09:368.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 09/25/23 14:47 191-24-209/23/23 09:368.3 2.4 1
Benzo(k)fluoranthene ND ug/L 09/25/23 14:47 207-08-909/23/23 09:368.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 09/25/23 14:47 92-52-409/23/23 09:368.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 09/25/23 14:47 101-55-309/23/23 09:368.3 1.5 1
Butylbenzylphthalate ND ug/L 09/25/23 14:47 85-68-709/23/23 09:368.3 2.6 1
Caprolactam ND ug/L 09/25/23 14:47 105-60-209/23/23 09:368.3 5.8 1
Carbazole ND ug/L 09/25/23 14:47 86-74-809/23/23 09:368.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/25/23 14:47 59-50-709/23/23 09:368.3 2.8 1
4-Chloroaniline ND ug/L 09/25/23 14:47 106-47-809/23/23 09:3616.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/25/23 14:47 111-91-109/23/23 09:368.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 09/25/23 14:47 111-44-409/23/23 09:368.3 1.6 1
2-Chloronaphthalene ND ug/L 09/25/23 14:47 91-58-709/23/23 09:368.3 1.4 1
2-Chlorophenol ND ug/L 09/25/23 14:47 95-57-809/23/23 09:368.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/25/23 14:47 7005-72-309/23/23 09:368.3 1.7 1
Chrysene ND ug/L 09/25/23 14:47 218-01-909/23/23 09:368.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 09/25/23 14:47 53-70-309/23/23 09:368.3 2.5 1
Dibenzofuran ND ug/L 09/25/23 14:47 132-64-909/23/23 09:368.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/25/23 14:47 91-94-109/23/23 09:3616.7 6.8 1
2,4-Dichlorophenol ND ug/L 09/25/23 14:47 120-83-209/23/23 09:368.3 1.2 1
Diethylphthalate ND ug/L 09/25/23 14:47 84-66-209/23/23 09:368.3 1.7 1
2,4-Dimethylphenol ND ug/L 09/25/23 14:47 105-67-909/23/23 09:368.3 1.4 1
Dimethylphthalate ND ug/L 09/25/23 14:47 131-11-309/23/23 09:368.3 1.8 1
Di-n-butylphthalate ND ug/L 09/25/23 14:47 84-74-209/23/23 09:368.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/25/23 14:47 534-52-109/23/23 09:3616.7 6.5 1
2,4-Dinitrophenol ND ug/L 09/25/23 14:47 51-28-509/23/23 09:3641.7 21.7 1
2,4-Dinitrotoluene ND ug/L 09/25/23 14:47 121-14-209/23/23 09:368.3 1.4 1
2,6-Dinitrotoluene ND ug/L 09/25/23 14:47 606-20-209/23/23 09:368.3 1.4 1
Di-n-octylphthalate ND ug/L 09/25/23 14:47 117-84-009/23/23 09:368.3 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Sample: PZ18WG-091823 Lab ID: 92688596001 Collected: 09/18/23 15:30 Received: 09/18/23 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/25/23 14:47 117-81-709/23/23 09:365.0 3.1 1
Fluoranthene ND ug/L 09/25/23 14:47 206-44-009/23/23 09:368.3 1.8 1
Fluorene ND ug/L 09/25/23 14:47 86-73-709/23/23 09:368.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 09/25/23 14:47 87-68-309/23/23 09:368.3 1.5 1
Hexachlorobenzene ND ug/L 09/25/23 14:47 118-74-109/23/23 09:368.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 09/25/23 14:47 77-47-409/23/23 09:368.3 1.3 1
Hexachloroethane ND ug/L 09/25/23 14:47 67-72-109/23/23 09:368.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/25/23 14:47 193-39-509/23/23 09:368.3 2.4 1
Isophorone ND ug/L 09/25/23 14:47 78-59-109/23/23 09:368.3 1.4 1
2-Methylnaphthalene ND ug/L 09/25/23 14:47 91-57-609/23/23 09:368.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/25/23 14:47 95-48-709/23/23 09:368.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/25/23 14:47 15831-10-409/23/23 09:368.3 1.0 1
Naphthalene ND ug/L 09/25/23 14:47 91-20-309/23/23 09:368.3 1.7 1
2-Nitroaniline ND ug/L 09/25/23 14:47 88-74-409/23/23 09:3616.7 2.5 1
3-Nitroaniline ND ug/L 09/25/23 14:47 99-09-209/23/23 09:3616.7 3.1 1
4-Nitroaniline ND ug/L 09/25/23 14:47 100-01-609/23/23 09:3616.7 4.2 1
Nitrobenzene ND ug/L 09/25/23 14:47 98-95-309/23/23 09:368.3 1.6 1
2-Nitrophenol ND ug/L 09/25/23 14:47 88-75-509/23/23 09:368.3 1.2 1
4-Nitrophenol ND ug/L 09/25/23 14:47 100-02-709/23/23 09:3641.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 09/25/23 14:47 621-64-709/23/23 09:368.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 09/25/23 14:47 86-30-609/23/23 09:368.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/25/23 14:47 108-60-109/23/23 09:368.3 0.96 1
Pentachlorophenol ND ug/L 09/25/23 14:47 87-86-509/23/23 09:3616.7 3.1 1
Phenanthrene ND ug/L 09/25/23 14:47 85-01-809/23/23 09:368.3 1.7 1
Phenol ND ug/L 09/25/23 14:47 108-95-209/23/23 09:368.3 1.1 1
Pyrene ND ug/L 09/25/23 14:47 129-00-009/23/23 09:368.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 09/25/23 14:47 95-95-409/23/23 09:368.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/25/23 14:47 88-06-209/23/23 09:368.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)82 %09/25/23 14:47 4165-60-009/23/23 09:3610-138 1
2-Fluorobiphenyl (S)76 %09/25/23 14:47 321-60-809/23/23 09:3610-130 1
Terphenyl-d14 (S)73 %09/25/23 14:47 1718-51-009/23/23 09:3619-191 1
Phenol-d6 (S)12 %09/25/23 14:47 13127-88-309/23/23 09:3610-130 1
2-Fluorophenol (S)3 %09/25/23 14:47 367-12-4 S009/23/23 09:3610-130 1
2,4,6-Tribromophenol (S)13 %09/25/23 14:47 118-79-609/23/23 09:3610-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/22/23 19:42 67-64-125.0 5.1 1
Benzene ND ug/L 09/22/23 19:42 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/22/23 19:42 75-27-41.0 0.31 1
Bromoform ND ug/L 09/22/23 19:42 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/22/23 19:42 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 09/22/23 19:42 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/22/23 19:42 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Sample: PZ18WG-091823 Lab ID: 92688596001 Collected: 09/18/23 15:30 Received: 09/18/23 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/22/23 19:42 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/22/23 19:42 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/22/23 19:42 75-00-31.0 0.65 1
Chloroform ND ug/L 09/22/23 19:42 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/22/23 19:42 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/22/23 19:42 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/22/23 19:42 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/22/23 19:42 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/22/23 19:42 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/22/23 19:42 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/22/23 19:42 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/22/23 19:42 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/22/23 19:42 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/22/23 19:42 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/22/23 19:42 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/22/23 19:42 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/22/23 19:42 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/22/23 19:42 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/22/23 19:42 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/22/23 19:42 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/22/23 19:42 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/22/23 19:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/22/23 19:42 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/22/23 19:42 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/22/23 19:42 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/22/23 19:42 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/22/23 19:42 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/22/23 19:42 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/22/23 19:42 1634-04-41.0 0.42 1
Styrene ND ug/L 09/22/23 19:42 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/22/23 19:42 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/22/23 19:42 127-18-41.0 0.29 1
Toluene ND ug/L 09/22/23 19:42 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/22/23 19:42 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/22/23 19:42 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/22/23 19:42 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/22/23 19:42 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/22/23 19:42 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/22/23 19:42 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/22/23 19:42 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/22/23 19:42 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/22/23 19:42 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %09/22/23 19:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %09/22/23 19:42 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Sample: PZ18WG-091823 Lab ID: 92688596001 Collected: 09/18/23 15:30 Received: 09/18/23 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)98 %09/22/23 19:42 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 8.2 mg/L 09/25/23 18:325.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/20/23 03:05 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 94.1 mg/L 09/21/23 12:07 16887-00-61.0 0.60 1
Sulfate 23.8 mg/L 09/21/23 12:07 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800521
SM 2120B-2011
SM 2120B-2011
2120B True Color EDEN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4146443
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
True Color units ND 5.0 09/19/23 13:565.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4146444LABORATORY CONTROL SAMPLE:
LCSSpike
True Color units 35.035 100 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688596001
4146445SAMPLE DUPLICATE:
pH Std. Units 5.8 0 105.8
True Color units 500 0 10500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
958305
EPA 7470
EPA 7470
7470 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5270629
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/16/23 10:370.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5270630LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.02 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5270631MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35832183002
5270632
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L R1210075-12578 25 2020.14U 2.0 1.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
958303
EPA 7470
EPA 7470
7470 Mercury Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5270621
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/16/23 10:210.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5270622LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.02 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5270623MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688596001
5270624
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2 96 85-11594 2 202ND1.9 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
957722
EPA 3010
EPA 6010
6010 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5267139
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
Antimony ug/L ND 15.0 10/13/23 22:005.5
Arsenic ug/L ND 10.0 10/13/23 22:003.4
Barium ug/L ND 10.0 10/13/23 22:000.84
Beryllium ug/L ND 4.0 10/13/23 22:000.17
Boron ug/L ND 50.0 10/13/23 22:0012.4
Cadmium ug/L ND 1.0 10/13/23 22:000.33
Chromium ug/L ND 5.0 10/13/23 22:001.7
Cobalt ug/L ND 10.0 10/13/23 22:000.96
Copper ug/L ND 5.0 10/13/23 22:002.6
Lead ug/L ND 10.0 10/13/23 22:002.1
Manganese ug/L ND 5.0 10/13/23 22:001.1
Nickel ug/L ND 5.0 10/13/23 22:001.0
Selenium ug/L ND 15.0 10/13/23 22:003.9
Silver ug/L ND 5.0 10/13/23 22:001.0
Thallium ug/L ND 15.0 10/13/23 22:002.9
Vanadium ug/L ND 10.0 10/13/23 22:001.0
Zinc ug/L ND 20.0 10/13/23 22:0011.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5267140LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 252250 101 80-120
Arsenic ug/L 248250 99 80-120
Barium ug/L 253250 101 80-120
Beryllium ug/L 24.925 100 80-120
Boron ug/L 12501250 100 80-120
Cadmium ug/L 26.125 105 80-120
Chromium ug/L 254250 102 80-120
Cobalt ug/L 255250 102 80-120
Copper ug/L 245250 98 80-120
Lead ug/L 258250 103 80-120
Manganese ug/L 252250 101 80-120
Nickel ug/L 260250 104 80-120
Selenium ug/L 257250 103 80-120
Silver ug/L 24.925 100 80-120
Thallium ug/L 255250 102 80-120
Vanadium ug/L 251250 100 80-120
Zinc ug/L 13001250 104 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5267141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35833152001
5267142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 250 103 75-125104 0 202505.5U 259 259
Arsenic ug/L 250 101 75-125101 0 202503.4U 253 253
Barium ug/L 250 102 75-125103 1 2025015.2 270 272
Beryllium ug/L 25 101 75-125101 0 20250.17U 25.2 25.3
Boron ug/L 1250 102 75-125102 0 2012504361700 1710
Cadmium ug/L 25 103 75-125103 0 20250.33U 26.0 25.9
Chromium ug/L 250 102 75-125102 0 202501.7U 256 256
Cobalt ug/L 250 103 75-125103 0 202500.96U 258 258
Copper ug/L 250 102 75-125102 0 202502.6U 256 257
Lead ug/L 250 102 75-125102 0 202502.1U 254 254
Manganese ug/L 250 101 75-125101 0 202501.5J 253 253
Nickel ug/L 250 105 75-125105 0 202501.0U 262 262
Selenium ug/L M12507175-12571 0 202503.9U 178 177
Silver ug/L 25 100 75-125100 0 20251.0U 25.3 25.4
Thallium ug/L 250 100 75-125101 1 202502.9U 249 252
Vanadium ug/L 250 102 75-125102 0 202503.3J 259 259
Zinc ug/L 1250 103 75-125103 0 20125011.0U 1290 1290
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
958577
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5271822
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
Antimony, Dissolved ug/L ND 15.0 10/17/23 17:395.5
Arsenic, Dissolved ug/L ND 10.0 10/17/23 17:393.4
Barium, Dissolved ug/L ND 10.0 10/17/23 17:390.84
Beryllium, Dissolved ug/L ND 4.0 10/17/23 17:390.17
Boron, Dissolved ug/L ND 50.0 10/17/23 17:3912.4
Cadmium, Dissolved ug/L ND 1.0 10/17/23 17:390.33
Chromium, Dissolved ug/L ND 5.0 10/17/23 17:391.7
Cobalt, Dissolved ug/L ND 10.0 10/17/23 17:390.96
Copper, Dissolved ug/L ND 5.0 10/17/23 17:392.6
Lead, Dissolved ug/L ND 10.0 10/17/23 17:392.1
Manganese, Dissolved ug/L ND 5.0 10/17/23 17:391.1
Nickel, Dissolved ug/L ND 5.0 10/17/23 17:391.0
Selenium, Dissolved ug/L ND 15.0 10/17/23 17:393.9
Silver, Dissolved ug/L ND 5.0 10/17/23 17:391.0
Thallium, Dissolved ug/L ND 15.0 10/17/23 17:392.9
Vanadium, Dissolved ug/L ND 10.0 10/17/23 17:391.0
Zinc, Dissolved ug/L ND 20.0 10/17/23 17:3911.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5271823LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 247250 99 80-120
Arsenic, Dissolved ug/L 240250 96 80-120
Barium, Dissolved ug/L 258250 103 80-120
Beryllium, Dissolved ug/L 25.025 100 80-120
Boron, Dissolved ug/L 12501250 100 80-120
Cadmium, Dissolved ug/L 24.825 99 80-120
Chromium, Dissolved ug/L 247250 99 80-120
Cobalt, Dissolved ug/L 245250 98 80-120
Copper, Dissolved ug/L 251250 100 80-120
Lead, Dissolved ug/L 258250 103 80-120
Manganese, Dissolved ug/L 246250 98 80-120
Nickel, Dissolved ug/L 254250 102 80-120
Selenium, Dissolved ug/L 249250 100 80-120
Silver, Dissolved ug/L 24.725 99 80-120
Thallium, Dissolved ug/L 229250 91 80-120
Vanadium, Dissolved ug/L 253250 101 80-120
Zinc, Dissolved ug/L 12401250 99 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5271824MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35834623031
5271825
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 250 98 75-12598 0 202505.5U 245 246
Arsenic, Dissolved ug/L 250 93 75-12596 2 202504.5J 237 243
Barium, Dissolved ug/L 250 104 75-125102 2 202507.9J 268 262
Beryllium, Dissolved ug/L 25 100 75-125101 1 20250.17U 25.0 25.2
Boron, Dissolved ug/L 1250 100 75-125100 0 20125024.0J 1270 1280
Cadmium, Dissolved ug/L 25 98 75-12599 1 20250.33U 24.5 24.7
Chromium, Dissolved ug/L 250 100 75-12599 1 202504.3J 253 252
Cobalt, Dissolved ug/L 250 98 75-12598 0 202500.96U 245 245
Copper, Dissolved ug/L 250 101 75-125101 0 2025011.8 265 264
Lead, Dissolved ug/L 250 101 75-125102 1 202502.1U 254 256
Manganese, Dissolved ug/L 250 100 75-12598 1 20250234483 480
Nickel, Dissolved ug/L 250 101 75-125101 0 202501.0U 253 253
Selenium, Dissolved ug/L 250 97 75-125100 3 202503.9U 242 250
Silver, Dissolved ug/L 25 99 75-12597 2 20251.0U 25.4 25.0
Thallium, Dissolved ug/L 250 91 75-12591 1 202502.9U 226 227
Vanadium, Dissolved ug/L 250 102 75-125102 1 202506.3J 262 261
Zinc, Dissolved ug/L 1250 97 75-12598 1 20125011.0U 1210 1230
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801460
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4151417
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/22/23 12:010.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/22/23 12:010.22
1,1,2-Trichloroethane ug/L ND 1.0 09/22/23 12:010.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/22/23 12:010.32
1,1-Dichloroethane ug/L ND 1.0 09/22/23 12:010.37
1,1-Dichloroethene ug/L ND 1.0 09/22/23 12:010.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/22/23 12:010.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/22/23 12:010.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/22/23 12:010.27
1,2-Dichlorobenzene ug/L ND 1.0 09/22/23 12:010.34
1,2-Dichloroethane ug/L ND 1.0 09/22/23 12:010.32
1,2-Dichloropropane ug/L ND 1.0 09/22/23 12:010.36
1,3-Dichlorobenzene ug/L ND 1.0 09/22/23 12:010.34
1,4-Dichlorobenzene ug/L ND 1.0 09/22/23 12:010.33
2-Butanone (MEK)ug/L ND 5.0 09/22/23 12:014.0
2-Hexanone ug/L ND 5.0 09/22/23 12:010.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/22/23 12:012.7
Acetone ug/L ND 25.0 09/22/23 12:015.1
Benzene ug/L ND 1.0 09/22/23 12:010.34
Bromodichloromethane ug/L ND 1.0 09/22/23 12:010.31
Bromoform ug/L ND 1.0 09/22/23 12:010.34
Bromomethane ug/L ND 2.0 09/22/23 12:011.7
Carbon disulfide ug/L ND 2.0 09/22/23 12:010.36
Carbon tetrachloride ug/L ND 1.0 09/22/23 12:010.33
Chlorobenzene ug/L ND 1.0 09/22/23 12:010.28
Chloroethane ug/L ND 1.0 09/22/23 12:010.65
Chloroform ug/L ND 1.0 09/22/23 12:010.43
Chloromethane ug/L ND 1.0 09/22/23 12:010.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/22/23 12:010.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/22/23 12:010.36
Cyclohexane ug/L ND 1.0 09/22/23 12:010.35
Dibromochloromethane ug/L ND 1.0 09/22/23 12:010.36
Dichlorodifluoromethane ug/L ND 1.0 09/22/23 12:010.35
Ethylbenzene ug/L ND 1.0 09/22/23 12:010.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/22/23 12:010.33
m&p-Xylene ug/L ND 2.0 09/22/23 12:010.71
Methyl acetate ug/L ND 10.0 09/22/23 12:012.4
Methyl-tert-butyl ether ug/L ND 1.0 09/22/23 12:010.42
Methylcyclohexane ug/L ND 10.0 09/22/23 12:011.5
Methylene Chloride ug/L ND 5.0 09/22/23 12:012.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4151417
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/22/23 12:010.34
Styrene ug/L ND 1.0 09/22/23 12:010.29
Tetrachloroethene ug/L ND 1.0 09/22/23 12:010.29
Toluene ug/L ND 1.0 09/22/23 12:010.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/22/23 12:010.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/22/23 12:010.36
Trichloroethene ug/L ND 1.0 09/22/23 12:010.38
Trichlorofluoromethane ug/L ND 1.0 09/22/23 12:010.30
Vinyl chloride ug/L ND 1.0 09/22/23 12:010.39
1,2-Dichloroethane-d4 (S)%95 70-130 09/22/23 12:01
4-Bromofluorobenzene (S)%96 70-130 09/22/23 12:01
Toluene-d8 (S)%98 70-130 09/22/23 12:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4151418LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.620 98 70-130
1,1,2,2-Tetrachloroethane ug/L 20.420 102 70-130
1,1,2-Trichloroethane ug/L 20.320 101 70-130
1,1,2-Trichlorotrifluoroethane ug/L 22.020 110 70-132
1,1-Dichloroethane ug/L 20.320 101 70-130
1,1-Dichloroethene ug/L 21.920 110 69-131
1,2,4-Trichlorobenzene ug/L 17.620 88 70-130
1,2-Dibromo-3-chloropropane ug/L 17.020 85 70-130
1,2-Dibromoethane (EDB)ug/L 19.920 99 70-130
1,2-Dichlorobenzene ug/L 19.520 97 70-130
1,2-Dichloroethane ug/L 19.620 98 70-130
1,2-Dichloropropane ug/L 20.520 102 70-130
1,3-Dichlorobenzene ug/L 19.820 99 70-130
1,4-Dichlorobenzene ug/L 19.620 98 70-130
2-Butanone (MEK)ug/L 38.340 96 67-133
2-Hexanone ug/L 40.140 100 70-133
4-Methyl-2-pentanone (MIBK)ug/L 39.540 99 70-130
Acetone ug/L 38.340 96 67-130
Benzene ug/L 20.420 102 70-130
Bromodichloromethane ug/L 19.020 95 70-130
Bromoform ug/L 17.120 86 70-133
Bromomethane ug/L 22.220 111 41-148
Carbon disulfide ug/L 22.120 110 70-131
Carbon tetrachloride ug/L 19.820 99 70-130
Chlorobenzene ug/L 20.420 102 70-130
Chloroethane ug/L 19.820 99 41-157
Chloroform ug/L 19.320 97 70-130
Chloromethane ug/L 17.520 88 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4151418LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 20.520 102 70-130
cis-1,3-Dichloropropene ug/L 19.320 96 70-130
Cyclohexane ug/L 21.920 109 63-137
Dibromochloromethane ug/L 19.220 96 70-130
Dichlorodifluoromethane ug/L 21.420 107 54-147
Ethylbenzene ug/L 20.020 100 70-130
Isopropylbenzene (Cumene)ug/L 20.320 102 70-130
m&p-Xylene ug/L 40.140 100 70-130
Methyl acetate ug/L 19.820 99 70-130
Methyl-tert-butyl ether ug/L 18.420 92 70-130
Methylcyclohexane ug/L 23.720 119 70-130
Methylene Chloride ug/L 20.820 104 62-130
o-Xylene ug/L 19.520 98 70-130
Styrene ug/L 20.320 102 70-130
Tetrachloroethene ug/L 19.220 96 70-130
Toluene ug/L 19.920 99 70-130
trans-1,2-Dichloroethene ug/L 20.920 105 70-130
trans-1,3-Dichloropropene ug/L 18.820 94 70-130
Trichloroethene ug/L 20.020 100 70-130
Trichlorofluoromethane ug/L 18.620 93 57-130
Vinyl chloride ug/L 16.620 83 66-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4151419MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4151420
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 115 70-150129 11 3020ND23.0 25.7
1,1,2,2-Tetrachloroethane ug/L 20 115 66-144124 7 3020ND23.0 24.7
1,1,2-Trichloroethane ug/L 20 112 70-142122 8 3020ND22.4 24.3
1,1,2-Trichlorotrifluoroethane ug/L 20 122 66-168131 7 3020ND24.3 26.2
1,1-Dichloroethane ug/L 20 118 68-150133 11 3020ND23.7 26.5
1,1-Dichloroethene ug/L 20 134 64-162149 11 3020ND26.8 29.8
1,2,4-Trichlorobenzene ug/L 20 102 69-147109 7 3020ND20.3 21.8
1,2-Dibromo-3-chloropropane ug/L 20 99 62-146111 11 3020ND19.9 22.2
1,2-Dibromoethane (EDB) ug/L 20 108 70-143119 9 3020ND21.7 23.8
1,2-Dichlorobenzene ug/L 20 104 70-142111 6 3020ND20.8 22.2
1,2-Dichloroethane ug/L 20 112 68-145124 10 3020ND22.4 24.8
1,2-Dichloropropane ug/L 20 118 70-144127 8 3020ND23.6 25.5
1,3-Dichlorobenzene ug/L 20 104 70-142112 7 3020ND20.8 22.3
1,4-Dichlorobenzene ug/L 20 102 70-140110 8 3020ND20.5 22.1
2-Butanone (MEK)ug/L 40 121 57-156136 11 3040ND51.2 57.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
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[phone]
Page 19 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4151419MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4151420
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 123 62-153138 11 3040ND49.1 55.0
4-Methyl-2-pentanone(MIBK)ug/L 40 121 65-144133 9 30403.3J 51.7 56.5
Acetone ug/L 40 121 49-162133 7 304016.0J 64.6 69.3
Benzene ug/L 20 116 68-144123 6 30200.49J 23.8 25.2
Bromodichloromethane ug/L 20 110 70-141117 6 3020ND22.0 23.5
Bromoform ug/L 20 94 59-144102 8 3020ND18.8 20.4
Bromomethane ug/L 20 98 23-190113 14 3020ND19.6 22.6
Carbon disulfide ug/L 20 126 64-160145 14 3020ND25.1 28.9
Carbon tetrachloride ug/L 20 118 70-147123 4 3020ND23.7 24.6
Chlorobenzene ug/L 20 108 70-143120 10 3020ND21.7 24.0
Chloroethane ug/L 20 112 55-190121 7 3020ND22.4 24.2
Chloroform ug/L 20 111 67-148123 11 3020ND22.2 24.6
Chloromethane ug/L 20 97 38-180108 11 3020ND19.6 21.9
cis-1,2-Dichloroethene ug/L 20 120 67-151130 8 3020ND23.9 26.0
cis-1,3-Dichloropropene ug/L 20 107 70-142114 7 3020ND21.4 22.9
Cyclohexane ug/L 20 126 64-162138 9 3020ND25.3 27.6
Dibromochloromethane ug/L 20 103 68-140114 10 3020ND20.7 22.8
Dichlorodifluoromethane ug/L 20 119 15-200130 9 3020ND23.7 25.9
Ethylbenzene ug/L 20 95 70-145102 3 302021.5 40.5 41.9
Isopropylbenzene(Cumene)ug/L 20 112 70-144122 9 3020ND22.4 24.4
m&p-Xylene ug/L 40 102 70-148111 6 304019.6 60.3 64.2
Methyl acetate ug/L 20 119 62-144124 5 3020ND23.8 24.9
Methyl-tert-butyl ether ug/L 20 106 64-146117 10 3020ND21.3 23.5
Methylcyclohexane ug/L 20 134 70-155142 6 3020ND26.8 28.5
Methylene Chloride ug/L 20 121 54-149136 11 3020ND25.5 28.5
o-Xylene ug/L 20 92 70-14596 2 302024.7 43.1 44.0
Styrene ug/L 20 108 70-147118 9 3020ND21.5 23.6
Tetrachloroethene ug/L 20 104 70-145113 8 3020ND20.8 22.5
Toluene ug/L 20 109 65-146119 8 30200.45J 22.3 24.3
trans-1,2-Dichloroethene ug/L 20 121 69-155139 14 3020ND24.1 27.9
trans-1,3-Dichloropropene ug/L 20 110 70-142115 4 3020ND22.0 22.9
Trichloroethene ug/L 20 113 70-152122 7 3020ND22.6 24.3
Trichlorofluoromethane ug/L 20 111 60-158123 10 3020ND22.1 24.5
Vinyl chloride ug/L 20 97 51-178110 12 3020ND19.5 22.0
1,2-Dichloroethane-d4 (S) %99 70-130100
4-Bromofluorobenzene (S) %99 70-130100
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
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[phone]
Page 20 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801417
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4151103
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/22/23 19:331.2
2,4,5-Trichlorophenol ug/L ND 10.0 09/22/23 19:331.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/22/23 19:331.6
2,4-Dichlorophenol ug/L ND 10.0 09/22/23 19:331.4
2,4-Dimethylphenol ug/L ND 10.0 09/22/23 19:331.7
2,4-Dinitrophenol ug/L ND 50.0 09/22/23 19:3326.0
2,4-Dinitrotoluene ug/L ND 10.0 09/22/23 19:331.6
2,6-Dinitrotoluene ug/L ND 10.0 09/22/23 19:331.7
2-Chloronaphthalene ug/L ND 10.0 09/22/23 19:331.7
2-Chlorophenol ug/L ND 10.0 09/22/23 19:331.2
2-Methylnaphthalene ug/L ND 10.0 09/22/23 19:331.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/22/23 19:331.9
2-Nitroaniline ug/L ND 20.0 09/22/23 19:333.0
2-Nitrophenol ug/L ND 10.0 09/22/23 19:331.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/22/23 19:331.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/22/23 19:338.1
3-Nitroaniline ug/L ND 20.0 09/22/23 19:333.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/22/23 19:337.8
4-Bromophenylphenyl ether ug/L ND 10.0 09/22/23 19:331.8
4-Chloro-3-methylphenol ug/L ND 10.0 09/22/23 19:333.3
4-Chloroaniline ug/L ND 20.0 09/22/23 19:333.6
4-Chlorophenylphenyl ether ug/L ND 10.0 09/22/23 19:332.0
4-Nitroaniline ug/L ND 20.0 09/22/23 19:335.1
4-Nitrophenol ug/L ND 50.0 09/22/23 19:336.6
Acenaphthene ug/L ND 10.0 09/22/23 19:332.0
Acenaphthylene ug/L ND 10.0 09/22/23 19:332.0
Acetophenone ug/L ND 10.0 09/22/23 19:331.5
Anthracene ug/L ND 10.0 09/22/23 19:332.3
Atrazine ug/L ND 10.0 09/22/23 19:333.2
Benzaldehyde ug/L ND 10.0 09/22/23 19:333.6
Benzo(a)anthracene ug/L ND 10.0 09/22/23 19:332.7
Benzo(a)pyrene ug/L ND 10.0 09/22/23 19:332.8
Benzo(b)fluoranthene ug/L ND 10.0 09/22/23 19:332.6
Benzo(g,h,i)perylene ug/L ND 10.0 09/22/23 19:332.8
Benzo(k)fluoranthene ug/L ND 10.0 09/22/23 19:332.7
Biphenyl (Diphenyl)ug/L ND 10.0 09/22/23 19:331.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/22/23 19:331.8
bis(2-Chloroethyl) ether ug/L ND 10.0 09/22/23 19:331.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/22/23 19:333.7
Butylbenzylphthalate ug/L ND 10.0 09/22/23 19:333.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
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[phone]
Page 21 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4151103
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
Caprolactam ug/L ND 10.0 09/22/23 19:336.9
Carbazole ug/L ND 10.0 09/22/23 19:332.4
Chrysene ug/L ND 10.0 09/22/23 19:332.8
Di-n-butylphthalate ug/L 2.5J 10.0 09/22/23 19:332.2
Di-n-octylphthalate ug/L ND 10.0 09/22/23 19:333.9
Dibenz(a,h)anthracene ug/L ND 10.0 09/22/23 19:333.0
Dibenzofuran ug/L ND 10.0 09/22/23 19:332.1
Diethylphthalate ug/L ND 10.0 09/22/23 19:332.0
Dimethylphthalate ug/L ND 10.0 09/22/23 19:332.1
Fluoranthene ug/L ND 10.0 09/22/23 19:332.2
Fluorene ug/L ND 10.0 09/22/23 19:332.1
Hexachloro-1,3-butadiene ug/L ND 10.0 09/22/23 19:331.8
Hexachlorobenzene ug/L ND 10.0 09/22/23 19:332.2
Hexachlorocyclopentadiene ug/L ND 10.0 09/22/23 19:331.6
Hexachloroethane ug/L ND 10.0 09/22/23 19:331.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/22/23 19:332.9
Isophorone ug/L ND 10.0 09/22/23 19:331.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/22/23 19:331.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/22/23 19:333.0
Naphthalene ug/L ND 10.0 09/22/23 19:332.1
Nitrobenzene ug/L ND 10.0 09/22/23 19:331.9
Pentachlorophenol ug/L ND 20.0 09/22/23 19:333.8
Phenanthrene ug/L ND 10.0 09/22/23 19:332.0
Phenol ug/L ND 10.0 09/22/23 19:331.4
Pyrene ug/L ND 10.0 09/22/23 19:332.2
2,4,6-Tribromophenol (S)%142 10-164 09/22/23 19:33
2-Fluorobiphenyl (S)%102 10-130 09/22/23 19:33
2-Fluorophenol (S)%79 10-130 09/22/23 19:33
Nitrobenzene-d5 (S)%109 10-138 09/22/23 19:33
Phenol-d6 (S)%60 10-130 09/22/23 19:33
Terphenyl-d14 (S)%151 19-191 09/22/23 19:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4151104LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 30.350 61 21-135
2,4,5-Trichlorophenol ug/L 50.950 102 38-147
2,4,6-Trichlorophenol ug/L 46.950 94 34-142
2,4-Dichlorophenol ug/L 43.550 87 36-136
2,4-Dimethylphenol ug/L 42.150 84 38-134
2,4-Dinitrophenol ug/L 240250 96 10-169
2,4-Dinitrotoluene ug/L 49.650 99 44-154
2,6-Dinitrotoluene ug/L 49.550 99 44-156
2-Chloronaphthalene ug/L 38.850 78 25-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4151104LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 37.650 75 29-130
2-Methylnaphthalene ug/L 37.250 74 23-130
2-Methylphenol(o-Cresol)ug/L 33.450 67 31-130
2-Nitroaniline ug/L 91.9100 92 39-145
2-Nitrophenol ug/L 43.050 86 29-142
3&4-Methylphenol(m&p Cresol)ug/L 37.850 76 30-130
3,3'-Dichlorobenzidine ug/L 134100 134 44-158
3-Nitroaniline ug/L 102100 102 45-152
4,6-Dinitro-2-methylphenol ug/L 106100 106 39-158
4-Bromophenylphenyl ether ug/L 49.850 100 47-147
4-Chloro-3-methylphenol ug/L 84.7100 85 40-138
4-Chloroaniline ug/L 82.6100 83 35-130
4-Chlorophenylphenyl ether ug/L 45.250 90 36-139
4-Nitroaniline ug/L 111100 111 46-157
4-Nitrophenol ug/L 144250 58 17-130
Acenaphthene ug/L 40.750 81 34-135
Acenaphthylene ug/L 40.450 81 35-137
Acetophenone ug/L 36.150 72 30-137
Anthracene ug/L 47.050 94 47-146
Atrazine ug/L 18.450 37 30-130
Benzaldehyde ug/L 30.050 60 17-167
Benzo(a)anthracene ug/L 59.150 118 48-160
Benzo(a)pyrene ug/L 59.550 119 47-165
Benzo(b)fluoranthene ug/L 73.050 146 49-171
Benzo(g,h,i)perylene ug/L 55.650 111 46-166
Benzo(k)fluoranthene ug/L 63.950 128 55-162
Biphenyl (Diphenyl)ug/L 39.050 78 28-130
bis(2-Chloroethoxy)methane ug/L 39.450 79 33-136
bis(2-Chloroethyl) ether ug/L 32.550 65 30-142
bis(2-Ethylhexyl)phthalate ug/L 69.650 139 46-173
Butylbenzylphthalate ug/L 63.750 127 53-169
Caprolactam ug/L 24.1100 24 13-130
Carbazole ug/L 53.350 107 48-157
Chrysene ug/L 55.350 111 54-152
Di-n-butylphthalate ug/L 62.950 126 49-161
Di-n-octylphthalate ug/L 63.650 127 50-166
Dibenz(a,h)anthracene ug/L 54.850 110 46-166
Dibenzofuran ug/L 40.350 81 37-136
Diethylphthalate ug/L 49.850 100 45-149
Dimethylphthalate ug/L 46.150 92 43-145
Fluoranthene ug/L 50.550 101 50-153
Fluorene ug/L 43.250 86 42-142
Hexachloro-1,3-butadiene ug/L 31.050 62 10-130
Hexachlorobenzene ug/L 48.050 96 44-138
Hexachlorocyclopentadiene ug/L 37.750 75 10-130
Hexachloroethane ug/L 21.250 42 10-130
Indeno(1,2,3-cd)pyrene ug/L 54.750 109 46-166
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4151104LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 39.950 80 36-135
N-Nitroso-di-n-propylamine ug/L 40.850 82 33-140
N-Nitrosodiphenylamine ug/L 49.550 99 46-144
Naphthalene ug/L 32.150 64 20-130
Nitrobenzene ug/L 35.250 70 33-133
Pentachlorophenol ug/L 102100 102 21-163
Phenanthrene ug/L 47.050 94 47-146
Phenol ug/L 22.250 44 19-130
Pyrene ug/L 56.350 113 53-155
2,4,6-Tribromophenol (S)%158 10-164
2-Fluorobiphenyl (S)%105 10-130
2-Fluorophenol (S)%69 10-130
Nitrobenzene-d5 (S)%101 10-138
Phenol-d6 (S)%59 10-130
Terphenyl-d14 (S)%154 19-191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801853
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4153553
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/25/23 18:055.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4153554LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.450 103 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4153555LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.550 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4153556MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688820001
4153557
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 102 80-120107 1 2550139191 193
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800666
SM 4500-S2D-2011
SM 4500-S2D-2011
4500S2D Sulfide Water
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147255
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
Sulfide mg/L ND 0.10 09/20/23 02:560.022
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147256LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide mg/L 0.500.5 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147259MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4147260
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L M10.5 76 80-12079 2 100.50.24 0.62 0.63
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147272MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688078001
4147273
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 101 80-120109 8 100.5ND 0.51 0.55
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800716
EPA 9056A
EPA 9056A
9056 IC anions 28 Days
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92688596001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4147423
Associated Lab Samples:92688596001
Matrix: Water
AnalyzedMDL
Chloride mg/L ND 1.0 09/20/23 20:330.60
Sulfate mg/L ND 1.0 09/20/23 20:330.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4147424LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 49.750 99 90-110
Sulfate mg/L 49.550 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147425MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280008
4147426
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L M150-270 90-110177 3 105089108770 8990
Sulfate mg/L M150-51 90-110-13 4 1050500475 494
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4147427MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280011
4147428
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L M1508790-11084 1 1050206249 248
Sulfate mg/L 50 94 90-11094 0 105020.1 67.1 66.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 27 of 48
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 48
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92688596
Pactiv Evergreen GWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92688596001 800521PZ18WG-091823 SM 2120B-2011
92688596001 957722 957738PZ18WG-091823 EPA 3010 EPA 6010
92688596001 958577 958641PZ18WG-091823 EPA 3010 EPA 6010
92688596001 958305 958318PZ18WG-091823 EPA 7470 EPA 7470
92688596001 958303 958316PZ18WG-091823 EPA 7470 EPA 7470
92688596001 801417 801536PZ18WG-091823 EPA 3510C EPA 8270E
92688596001 801460PZ18WG-091823 EPA 8260D
92688596001 801853PZ18WG-091823 SM 2320B-2011
92688596001 800666PZ18WG-091823 SM 4500-S2D-2011
92688596001 800716PZ18WG-091823 EPA 9056A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2023 04:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 48
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Thisreportshouldnotbereproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamplesincludedinthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
Matthew Brainard
PACE Charlotte
9800 Kincey Ave.
Huntersville NC 28078
REPORT OF
LABORATORY
ANALYSIS FOR
PCDD/PCDF
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
October 10, 2023
Pace Project #: 10670312
Sample Receipt Date: 09/27/2023
Client Project #: 92688596
Client Sub PO #: N/A
The report provided has been invoiced as a Level 2
PCDD/PCDF Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questionstoIsaac Johnson,your Pace
Project Manager.
State Cert #: 530
Suite 100
Report Prepared for:
Page 1 of 16Report No.....10670312_SW8290AFC_L2_dfr
October 10, 2023
Isaac Johnson, Project Manager
[phone]
[phone] (fax)
[e-mail]
Page 33 of 48
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
This report presents the results from the analysis performed on one sample submitted by a representative
of Pace Analytical Services, LLC. The sample was analyzed for the presence or absence of
polychlorodibenzo-p-dioxins (PCDDs) and polychlorodibenzofurans (PCDFs) using a modified version of
USEPA Method 8290A. The estimated detection limits (EDLs) were based on signal-to-noise
measurements. Estimated maximum possible concentration (EMPC) values were treated as positives inthe toxic equivalence calculations.
The isotopically-labeled PCDD/PCDF internal standards in the sample extract were recovered at 22-72%.Except for four low values, which were flagged "R" on the results tables, the labeled internal standardrecoveries obtained for this project were within the 40-135% target range specified in Method 8290A.Since the quantification of the native 2,3,7,8-substituted congeners was based on isotope dilution, thedata were automatically corrected for recovery and accurate values were obtained.
A laboratory method blank was prepared and analyzed with the sample batch as part of our routine qualitycontrol procedures. The results show the blank to contain trace levels of one or more selected congeners.
These levels were below the calibration range of the method. Sample concentrations similar to the
corresponding blank levels were flagged "B" on the results table and may be, at least partially, attributed
to the background.
Laboratory spike samples were also prepared using clean reference matrix that had been fortified with
native standard materials. The results show that the spiked native compounds were recovered at
86-104% with relative percent differences of 0.0-6.0%. These results were within the target ranges for the
method. Matrix spikes were not prepared with the extraction batch.
DISCUSSION
Page 2 of 16Report No.....10670312_SW8290AFC_L2_dfr
Page 34 of 48
REPORT OF LABORATORY ANALYSIS
This report shallnot bereproduced,except in full,
withoutthe written consentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 16Report No.....10670312_SW8290AFC_L2_dfr
Page 35 of 48
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 4 of 16Report No.....10670312_SW8290AFC_L2_dfr
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Page 9 of 16Report No.....10670312_SW8290AFC_L2_dfr
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Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
A =
B = C = D = E = H2 =
I =
J = L = Nn = P = R =
S =
U = V = X = Y = * =
Reporting Limit based on signal to noise (EDL)
Less than 10x higher than method blank level Result obtained from confirmation analysis Result obtained from analysis of diluted sample Exceeds calibration range Extracted outside of holding time
Isotope ratio out of specification
Estimated value Suppressive interference, analyte may be biased low Value obtained from additional analysis PCDE Interference Recovery outside target range
Peak saturated
Analyte not detected Result verified by confirmation analysis %D Exceeds limits Calculated using average of daily RFs See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 10 of 16Report No.....10670312_SW8290AFC_L2_dfr
Page 42 of 48
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 11 of 16Report No.....10670312_SW8290AFC_L2_dfr
Page 43 of 48
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ18WG-09182392688596001L231009A_10JF
NA996 mL
NAL230816L231009A_01 & L231009B_01BLANK-108589
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/18/2023 15:3009/27/2023 08:5010/05/2023 09:1010/09/2023 14:27
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 0.61 2,3,7,8-TCDF-13C 2.00 62-----Total TCDF ND 0.61 2,3,7,8-TCDD-13C 2.00 22-----R1,2,3,7,8-PeCDF-13C 2.00 612,3,7,8-TCDD ND 3.0 2,3,4,7,8-PeCDF-13C 2.00 65-----Total TCDD ND 3.0 1,2,3,7,8-PeCDD-13C 2.00 67-----1,2,3,4,7,8-HxCDF-13C 2.00 521,2,3,7,8-PeCDF -----0.50 1,2,3,6,7,8-HxCDF-13C 2.00 59IJ0.692,3,4,7,8-PeCDF ND 0.35 2,3,4,6,7,8-HxCDF-13C 2.00 72-----Total PeCDF ND 0.35 1,2,3,7,8,9-HxCDF-13C 2.00 61-----1,2,3,4,7,8-HxCDD-13C 2.00 721,2,3,7,8-PeCDD ND 0.63 1,2,3,6,7,8-HxCDD-13C 2.00 64-----Total PeCDD ND 0.63 1,2,3,4,6,7,8-HpCDF-13C 2.00 53-----1,2,3,4,7,8,9-HpCDF-13C 2.00 461,2,3,4,7,8-HxCDF ND 1.2 1,2,3,4,6,7,8-HpCDD-13C 2.00 61-----1,2,3,6,7,8-HxCDF ND 0.92 OCDD-13C 4.00 46-----2,3,4,6,7,8-HxCDF ND 0.80-----1,2,3,7,8,9-HxCDF ND 1.1 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 0.80 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD -----1.00 2,3,7,8-TCDD-37Cl4 0.20 27IJ2.31,2,3,6,7,8-HxCDD ND 0.93-----1,2,3,7,8,9-HxCDD ND 0.94-----Total HxCDD ND 0.93-----
1,2,3,4,6,7,8-HpCDF ND 2.5 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 4.7 Equivalence: 0.29 pg/L-----Total HpCDF ND 2.5 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----1.8 IJ3.2Total HpCDD ND 1.8-----
OCDF ND 4.9-----OCDD 28 5.5 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelR=Recovery outside target rangeI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 12 of 16Report No.....10670312_SW8290AFC_L2_dfr
Page 44 of 48
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
BLANK-108589L231009A_07
SMT
1020 mLL230816L231009A_01 & L231009B_01
MatrixDilutionExtractedAnalyzed
Water
10/05/2023 09:1010/09/2023 12:21
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKQZ
NativeIsomers pg/LConc EMPCpg/L pg/L InternalStandards Addedng's PercentRecoveryEDL
2,3,7,8-TCDF ND -----0.96 2,3,7,8-TCDF-13C 2.00 68Total TCDF ND -----0.96 2,3,7,8-TCDD-13C 2.00 22 R1,2,3,7,8-PeCDF-13C 2.00 742,3,7,8-TCDD ND -----3.7 2,3,4,7,8-PeCDF-13C 2.00 79Total TCDD ND -----3.7 1,2,3,7,8-PeCDD-13C 2.00 821,2,3,4,7,8-HxCDF-13C 2.00 621,2,3,7,8-PeCDF -----1.9 0.78 IJ 1,2,3,6,7,8-HxCDF-13C 2.00 572,3,4,7,8-PeCDF 0.91 -----0.54 J 2,3,4,6,7,8-HxCDF-13C 2.00 83Total PeCDF 0.91 -----0.54 J 1,2,3,7,8,9-HxCDF-13C 2.00 671,2,3,4,7,8-HxCDD-13C 2.00 851,2,3,7,8-PeCDD -----0.96 0.72 IJ 1,2,3,6,7,8-HxCDD-13C 2.00 81Total PeCDD ND -----0.72 1,2,3,4,6,7,8-HpCDF-13C 2.00 651,2,3,4,7,8,9-HpCDF-13C 2.00 521,2,3,4,7,8-HxCDF ND -----0.94 1,2,3,4,6,7,8-HpCDD-13C 2.00 751,2,3,6,7,8-HxCDF ND -----0.97 OCDD-13C 4.00 592,3,4,6,7,8-HxCDF 0.92 -----0.76 J1,2,3,7,8,9-HxCDF 1.6 -----1.0 J 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF 2.5 -----0.76 J 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD -----2.1 0.71 IJ 2,3,7,8-TCDD-37Cl4 0.20 241,2,3,6,7,8-HxCDD -----0.75 0.67 IJ1,2,3,7,8,9-HxCDD -----1.0 0.67 IJTotal HxCDD ND -----0.67
1,2,3,4,6,7,8-HpCDF -----2.5 1.7 IJ Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----3.7 Equivalence: 2.0 pg/LTotal HpCDF 4.5 -----1.7 J (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD 3.2 -----1.6 JTotal HpCDD 3.2 -----1.6 J
OCDF 17 -----2.6 JOCDD40-----3.8 J
Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
R =Recovery outside target range
I =Isotope ratio out of specification
EDL=EstimatedDetection Limit
Page 13 of 16Report No.....10670312_SW8290AFC_L2_dfr
Page 45 of 48
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCS-108590L231009A_04
SMT
1020 mLL230816L231009A_01 & L231009B_01
MatrixDilutionExtractedAnalyzed
Water
10/05/2023 09:1010/09/2023 10:15
NA
Method Blank ID BLANK-108589
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.19 2,3,7,8-TCDF-13C 2.0 7296Total TCDF 2,3,7,8-TCDD-13C 2.0 36 R1,2,3,7,8-PeCDF-13C 2.0 742,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.0 76103Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 831,2,3,4,7,8-HxCDF-13C 2.0 631,2,3,7,8-PeCDF 1.0 0.95 1,2,3,6,7,8-HxCDF-13C 2.0 76952,3,4,7,8-PeCDF 1.0 0.98 2,3,4,6,7,8-HxCDF-13C 2.0 8298Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 761,2,3,4,7,8-HxCDD-13C 2.0 821,2,3,7,8-PeCDD 1.0 0.90 1,2,3,6,7,8-HxCDD-13C 2.0 8490Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 721,2,3,4,7,8,9-HpCDF-13C 2.0 651,2,3,4,7,8-HxCDF 1.0 0.88 1,2,3,4,6,7,8-HpCDD-13C 2.0 81881,2,3,6,7,8-HxCDF 1.0 0.97 OCDD-13C 4.0 68972,3,4,6,7,8-HxCDF 1.0 0.99 991,2,3,7,8,9-HxCDF 1.0 0.94 1,2,3,4-TCDD-13C 2.0 NA94Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.0 2,3,7,8-TCDD-37Cl4 0.20 391041,2,3,6,7,8-HxCDD 1.0 0.93 931,2,3,7,8,9-HxCDD 1.0 0.95 95Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.93 931,2,3,4,7,8,9-HpCDF 1.0 1.0 100Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.90 90Total HpCDD
OCDF 2.0 2.1 104OCDD2.0 2.0 102
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 14 of 16Report No.....10670312_SW8290AFC_L2_dfr
Page 46 of 48
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCSD-108591L231009A_05
SMT
1020 mLL230816L231009A_01 & L231009B_01
MatrixDilutionExtractedAnalyzed
Water
10/05/2023 09:1010/09/2023 10:57
NA
Method Blank ID BLANK-108589
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.19 2,3,7,8-TCDF-13C 2.0 5994Total TCDF 2,3,7,8-TCDD-13C 2.0 18 R1,2,3,7,8-PeCDF-13C 2.0 592,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.0 62104Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 671,2,3,4,7,8-HxCDF-13C 2.0 541,2,3,7,8-PeCDF 1.0 0.95 1,2,3,6,7,8-HxCDF-13C 2.0 40952,3,4,7,8-PeCDF 1.0 0.95 2,3,4,6,7,8-HxCDF-13C 2.0 7395Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 611,2,3,4,7,8-HxCDD-13C 2.0 721,2,3,7,8-PeCDD 1.0 0.87 1,2,3,6,7,8-HxCDD-13C 2.0 7387Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 561,2,3,4,7,8,9-HpCDF-13C 2.0 441,2,3,4,7,8-HxCDF 1.0 0.87 1,2,3,4,6,7,8-HpCDD-13C 2.0 65871,2,3,6,7,8-HxCDF 1.0 1.0 OCDD-13C 4.0 531032,3,4,6,7,8-HxCDF 1.0 0.96 961,2,3,7,8,9-HxCDF 1.0 0.93 1,2,3,4-TCDD-13C 2.0 NA93Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.0 2,3,7,8-TCDD-37Cl4 0.20 201031,2,3,6,7,8-HxCDD 1.0 0.94 941,2,3,7,8,9-HxCDD 1.0 0.92 92Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.92 921,2,3,4,7,8,9-HpCDF 1.0 0.99 99Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.86 86Total HpCDD
OCDF 2.0 2.0 101OCDD2.0 2.0 101
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 15 of 16Report No.....10670312_SW8290AFC_L2_dfr
Page 47 of 48
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Client
Spike 1 IDSpike 1 Filename L231009A_04LCS-108590
PACE Charlotte
Spike Recovery Relative Percent Difference (RPD) Results
Spike 2 IDSpike 2 Filename L231009A_05LCSD-108591
Method 8290A
Spike 1 Spike 2Compound%REC %REC %RPD
2,3,7,8-TCDF 96 94 2.12,3,7,8-TCDD 103 104 1.01,2,3,7,8-PeCDF 95 95 0.02,3,4,7,8-PeCDF 98 95 3.11,2,3,7,8-PeCDD 90 87 3.41,2,3,4,7,8-HxCDF 88 87 1.11,2,3,6,7,8-HxCDF 97 103 6.02,3,4,6,7,8-HxCDF 99 96 3.11,2,3,7,8,9-HxCDF 94 93 1.11,2,3,4,7,8-HxCDD 104 103 1.01,2,3,6,7,8-HxCDD 93 94 1.11,2,3,7,8,9-HxCDD 95 92 3.21,2,3,4,6,7,8-HpCDF 93 92 1.11,2,3,4,7,8,9-HpCDF 100 99 1.01,2,3,4,6,7,8-HpCDD 90 86 4.5OCDF1041012.9OCDD1021011.0
%REC = Percent RecoveredRPD=The differencebetweenthetwo valuesdivided by the mean value
Page 16 of 16Report No.....10670312_SW8290AFC_L2_dfr
Page 48 of 48
#=CL#
November 01, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92689056
92689056
Project:
Pace Project No.:
RE:
Christina AshdownENSAFE313 Wingo WayMount Pleasant, SC 29464
Pactiv Evergreen GWS (09/19)
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on September 20, 2023. The results relate onlyto the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and thelaboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc: Jennings Kerr, ENSAFE Inc.
Lab, ENSAFE Inc.
David Warren, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 101
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 101
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Pace Analytical Services National
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 101
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Lab ID Sample ID Matrix Date Collected Date Received
92689056001 PZ21WG-091923 Water 09/19/23 09:25 09/20/23 08:25
92689056002 RW01WG-091923 Water 09/19/23 11:55 09/20/23 08:25
92689056003 PZ20WG-091923 Water 09/19/23 17:20 09/20/23 08:25
92689056004 PZ04WG-091923 Water 09/19/23 14:15 09/20/23 08:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 101
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92689056001 PZ21WG-091923 SM 2120B-2011 2 PASI-EAED
EPA 6010 17 PASI-OAAM1
EPA 6010 17 PASI-OKC2, TMA
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-AYEG
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92689056002 RW01WG-091923 SM 2120B-2011 2 PASI-EAED
EPA 6010 17 PASI-OAAM1, KC2
EPA 6010 17 PASI-OAME, TMA
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-AYEG
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92689056003 PZ20WG-091923 SM 2120B-2011 2 PASI-EAED
EPA 6010 17 PASI-OAAM1
EPA 6010 17 PASI-OAME
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-AYEG
SM 4500-S2D-2011 1 PASI-AJP1
EPA 9056A 2 PASI-ACDC
92689056004 PZ04WG-091923 EPA 1664B 1 PASI-CDVR
EPA 8015C 2 PASI-CHH
RSK-175 4 PANCCM
EPA 5030B/8015C 2 PASI-CTEG
EPA 6010 17 PASI-OAAM1, KC2
EPA 6010 17 PASI-OAME
EPA 7470 1 PASI-OJNK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 101
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-ARVS
SM 2540D-2015 1 PASI-ARVS
SM 4500-S2D-2011 1 PASI-AJP1
SM 5210B-2016 1 PASI-AMDM
EPA 9040C 1 PASI-ASMS
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 1 PASI-AMFO
SM 5220D-2011 1 PASI-AJP1
SM 5310B-2014 1 PASI-AMJP
EPA 9056A 2 PASI-ACDC
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ21WG-091923 Lab ID: 92689056001 Collected: 09/19/23 09:25 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.4 Std. Units 09/21/23 10:37 H31
True Color 5.0 units 09/21/23 10:37 H35.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/04/23 18:01 7440-36-010/04/23 07:0415.0 5.5 1
Arsenic ND ug/L 10/04/23 18:01 7440-38-210/04/23 07:0410.0 3.4 1
Barium 91.3 ug/L 10/04/23 18:01 7440-39-310/04/23 07:0410.0 0.84 1
Beryllium ND ug/L 10/04/23 18:01 7440-41-710/04/23 07:044.0 0.17 1
Boron 32.3J ug/L 10/04/23 18:01 7440-42-810/04/23 07:0450.0 12.4 1
Cadmium ND ug/L 10/04/23 18:01 7440-43-910/04/23 07:041.0 0.33 1
Chromium ND ug/L 10/04/23 18:01 7440-47-310/04/23 07:045.0 1.7 1
Cobalt 1.2J ug/L 10/04/23 18:01 7440-48-410/04/23 07:0410.0 0.96 1
Copper ND ug/L 10/04/23 18:01 7440-50-810/04/23 07:045.0 2.6 1
Lead ND ug/L 10/04/23 18:01 7439-92-110/04/23 07:0410.0 2.1 1
Manganese 833 ug/L 10/04/23 18:01 7439-96-510/04/23 07:045.0 1.1 1
Nickel ND ug/L 10/04/23 18:01 7440-02-010/04/23 07:045.0 1.0 1
Selenium ND ug/L 10/04/23 18:01 7782-49-210/04/23 07:0415.0 3.9 1
Silver ND ug/L 10/04/23 18:01 7440-22-410/04/23 07:045.0 1.0 1
Thallium ND ug/L 10/04/23 18:01 7440-28-010/04/23 07:0415.0 2.9 1
Vanadium ND ug/L 10/04/23 18:01 7440-62-210/04/23 07:0410.0 1.0 1
Zinc ND ug/L 10/04/23 18:01 7440-66-610/04/23 07:0420.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/03/23 20:28 7440-36-010/03/23 07:4315.0 5.5 1
Arsenic, Dissolved ND ug/L 10/04/23 02:00 7440-38-210/03/23 07:4310.0 3.4 1
Barium, Dissolved 92.2 ug/L 10/04/23 02:00 7440-39-310/03/23 07:4310.0 0.84 1
Beryllium, Dissolved ND ug/L 10/04/23 02:00 7440-41-710/03/23 07:434.0 0.17 1
Boron, Dissolved 37.5J ug/L 10/04/23 02:00 7440-42-810/03/23 07:4350.0 12.4 1
Cadmium, Dissolved 0.45J ug/L 10/04/23 02:00 7440-43-910/03/23 07:431.0 0.33 1
Chromium, Dissolved ND ug/L 10/04/23 02:00 7440-47-310/03/23 07:435.0 1.7 1
Cobalt, Dissolved ND ug/L 10/04/23 02:00 7440-48-410/03/23 07:4310.0 0.96 1
Copper, Dissolved 4.0J ug/L 10/04/23 02:00 7440-50-810/03/23 07:435.0 2.6 1
Lead, Dissolved ND ug/L 10/04/23 02:00 7439-92-110/03/23 07:4310.0 2.1 1
Manganese, Dissolved 648 ug/L 10/04/23 02:00 7439-96-510/03/23 07:435.0 1.1 1
Nickel, Dissolved ND ug/L 10/04/23 02:00 7440-02-010/03/23 07:435.0 1.0 1
Selenium, Dissolved ND ug/L 10/04/23 02:00 7782-49-210/03/23 07:4315.0 3.9 1
Silver, Dissolved ND ug/L 10/04/23 02:00 7440-22-410/03/23 07:435.0 1.0 1
Thallium, Dissolved ND ug/L 10/04/23 02:00 7440-28-010/03/23 07:4315.0 2.9 1
Vanadium, Dissolved ND ug/L 10/04/23 02:00 7440-62-210/03/23 07:4310.0 1.0 1
Zinc, Dissolved ND ug/L 10/04/23 02:00 7440-66-610/03/23 07:4320.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ21WG-091923 Lab ID: 92689056001 Collected: 09/19/23 09:25 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 09:37 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:13 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/25/23 17:19 83-32-909/25/23 12:3110.0 2.0 1
Acenaphthylene ND ug/L 09/25/23 17:19 208-96-809/25/23 12:3110.0 2.0 1
Acetophenone ND ug/L 09/25/23 17:19 98-86-209/25/23 12:3110.0 1.5 1
Anthracene ND ug/L 09/25/23 17:19 120-12-709/25/23 12:3110.0 2.3 1
Atrazine ND ug/L 09/25/23 17:19 1912-24-909/25/23 12:3110.0 3.2 1
Benzaldehyde ND ug/L 09/25/23 17:19 100-52-709/25/23 12:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/25/23 17:19 56-55-309/25/23 12:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/25/23 17:19 50-32-809/25/23 12:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/25/23 17:19 205-99-209/25/23 12:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/25/23 17:19 191-24-209/25/23 12:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/25/23 17:19 207-08-909/25/23 12:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/25/23 17:19 92-52-409/25/23 12:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/25/23 17:19 101-55-309/25/23 12:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/25/23 17:19 85-68-709/25/23 12:3110.0 3.1 1
Caprolactam ND ug/L 09/25/23 17:19 105-60-209/25/23 12:3110.0 6.9 1
Carbazole ND ug/L 09/25/23 17:19 86-74-809/25/23 12:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/25/23 17:19 59-50-709/25/23 12:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/25/23 17:19 106-47-809/25/23 12:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/25/23 17:19 111-91-109/25/23 12:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/25/23 17:19 111-44-409/25/23 12:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/25/23 17:19 91-58-709/25/23 12:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/25/23 17:19 95-57-809/25/23 12:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/25/23 17:19 7005-72-309/25/23 12:3110.0 2.0 1
Chrysene ND ug/L 09/25/23 17:19 218-01-909/25/23 12:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/25/23 17:19 53-70-309/25/23 12:3110.0 3.0 1
Dibenzofuran ND ug/L 09/25/23 17:19 132-64-909/25/23 12:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/25/23 17:19 91-94-109/25/23 12:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/25/23 17:19 120-83-209/25/23 12:3110.0 1.4 1
Diethylphthalate ND ug/L 09/25/23 17:19 84-66-209/25/23 12:3110.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/25/23 17:19 105-67-909/25/23 12:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/25/23 17:19 131-11-309/25/23 12:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/25/23 17:19 84-74-209/25/23 12:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/25/23 17:19 534-52-109/25/23 12:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/25/23 17:19 51-28-509/25/23 12:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/25/23 17:19 121-14-209/25/23 12:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/25/23 17:19 606-20-209/25/23 12:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/25/23 17:19 117-84-009/25/23 12:3110.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ21WG-091923 Lab ID: 92689056001 Collected: 09/19/23 09:25 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/25/23 17:19 117-81-709/25/23 12:316.0 3.7 1
Fluoranthene ND ug/L 09/25/23 17:19 206-44-009/25/23 12:3110.0 2.2 1
Fluorene ND ug/L 09/25/23 17:19 86-73-709/25/23 12:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/25/23 17:19 87-68-309/25/23 12:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/25/23 17:19 118-74-109/25/23 12:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/25/23 17:19 77-47-409/25/23 12:3110.0 1.6 1
Hexachloroethane ND ug/L 09/25/23 17:19 67-72-109/25/23 12:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/25/23 17:19 193-39-509/25/23 12:3110.0 2.9 1
Isophorone ND ug/L 09/25/23 17:19 78-59-109/25/23 12:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/25/23 17:19 91-57-609/25/23 12:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/25/23 17:19 95-48-709/25/23 12:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/25/23 17:19 15831-10-409/25/23 12:3110.0 1.2 1
Naphthalene ND ug/L 09/25/23 17:19 91-20-309/25/23 12:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/25/23 17:19 88-74-409/25/23 12:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/25/23 17:19 99-09-209/25/23 12:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/25/23 17:19 100-01-609/25/23 12:3120.0 5.1 1
Nitrobenzene ND ug/L 09/25/23 17:19 98-95-309/25/23 12:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/25/23 17:19 88-75-509/25/23 12:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/25/23 17:19 100-02-709/25/23 12:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/25/23 17:19 621-64-709/25/23 12:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/25/23 17:19 86-30-609/25/23 12:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/25/23 17:19 108-60-109/25/23 12:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/25/23 17:19 87-86-509/25/23 12:3120.0 3.8 1
Phenanthrene ND ug/L 09/25/23 17:19 85-01-809/25/23 12:3110.0 2.0 1
Phenol ND ug/L 09/25/23 17:19 108-95-209/25/23 12:3110.0 1.4 1
Pyrene ND ug/L 09/25/23 17:19 129-00-009/25/23 12:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/25/23 17:19 95-95-409/25/23 12:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/25/23 17:19 88-06-209/25/23 12:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)116 %09/25/23 17:19 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)108 %09/25/23 17:19 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)146 %09/25/23 17:19 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)55 %09/25/23 17:19 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)80 %09/25/23 17:19 367-12-409/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)137 %09/25/23 17:19 118-79-609/25/23 12:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 07:40 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 07:40 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 07:40 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 07:40 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 07:40 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 07:40 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 07:40 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ21WG-091923 Lab ID: 92689056001 Collected: 09/19/23 09:25 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/30/23 07:40 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 07:40 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 07:40 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 07:40 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 07:40 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 07:40 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 07:40 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 07:40 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 07:40 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 07:40 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 07:40 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 07:40 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 07:40 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 07:40 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 07:40 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 07:40 75-35-4 v11.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 07:40 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 07:40 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 07:40 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 07:40 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 07:40 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 07:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 07:40 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 07:40 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 07:40 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 07:40 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 07:40 75-09-2 v15.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 07:40 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 07:40 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 07:40 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 07:40 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 07:40 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 07:40 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 07:40 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 07:40 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 07:40 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 07:40 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 07:40 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 07:40 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 07:40 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 07:40 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 07:40 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %09/30/23 07:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %09/30/23 07:40 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ21WG-091923 Lab ID: 92689056001 Collected: 09/19/23 09:25 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)98 %09/30/23 07:40 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 115 mg/L 09/27/23 21:135.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/22/23 08:05 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 93.2 mg/L 09/21/23 21:48 16887-00-62.0 1.2 2
Sulfate 100 mg/L 09/21/23 21:48 14808-79-82.0 1.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: RW01WG-091923 Lab ID: 92689056002 Collected: 09/19/23 11:55 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 7.6 Std. Units 09/21/23 10:405
True Color 100 units 09/21/23 10:4025.0 25.0 5
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/04/23 18:05 7440-36-010/04/23 07:0415.0 5.5 1
Arsenic ND ug/L 10/04/23 18:05 7440-38-210/04/23 07:0410.0 3.4 1
Barium 56.6 ug/L 10/04/23 18:05 7440-39-310/04/23 07:0410.0 0.84 1
Beryllium ND ug/L 10/04/23 18:05 7440-41-710/04/23 07:044.0 0.17 1
Boron 60.9 ug/L 10/04/23 18:05 7440-42-810/04/23 07:0450.0 12.4 1
Cadmium ND ug/L 10/04/23 18:05 7440-43-910/04/23 07:041.0 0.33 1
Chromium 3.6J ug/L 10/04/23 18:05 7440-47-310/04/23 07:045.0 1.7 1
Cobalt 0.98J ug/L 10/04/23 18:05 7440-48-410/04/23 07:0410.0 0.96 1
Copper 3.8J ug/L 10/04/23 18:05 7440-50-810/04/23 07:045.0 2.6 1
Lead ND ug/L 10/04/23 18:05 7439-92-110/04/23 07:0410.0 2.1 1
Manganese 1570 ug/L 10/05/23 12:06 7439-96-510/04/23 07:0425.0 5.5 5
Nickel 2.7J ug/L 10/04/23 18:05 7440-02-010/04/23 07:045.0 1.0 1
Selenium ND ug/L 10/04/23 18:05 7782-49-210/04/23 07:0415.0 3.9 1
Silver ND ug/L 10/04/23 18:05 7440-22-410/04/23 07:045.0 1.0 1
Thallium ND ug/L 10/04/23 18:05 7440-28-010/04/23 07:0415.0 2.9 1
Vanadium 11.5 ug/L 10/04/23 18:05 7440-62-210/04/23 07:0410.0 1.0 1
Zinc 79.6 ug/L 10/04/23 18:05 7440-66-610/04/23 07:0420.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/03/23 22:42 7440-36-010/03/23 07:4315.0 5.5 1
Arsenic, Dissolved ND ug/L 10/03/23 22:42 7440-38-210/03/23 07:4310.0 3.4 1
Barium, Dissolved 34.4 ug/L 10/03/23 22:42 7440-39-310/03/23 07:4310.0 0.84 1
Beryllium, Dissolved ND ug/L 10/03/23 22:42 7440-41-710/03/23 07:434.0 0.17 1
Boron, Dissolved 65.6 ug/L 10/03/23 22:42 7440-42-810/03/23 07:4350.0 12.4 1
Cadmium, Dissolved ND ug/L 10/03/23 22:42 7440-43-910/03/23 07:431.0 0.33 1
Chromium, Dissolved ND ug/L 10/03/23 22:42 7440-47-310/03/23 07:435.0 1.7 1
Cobalt, Dissolved ND ug/L 10/03/23 22:42 7440-48-410/03/23 07:4310.0 0.96 1
Copper, Dissolved ND ug/L 10/03/23 22:42 7440-50-810/03/23 07:435.0 2.6 1
Lead, Dissolved ND ug/L 10/03/23 22:42 7439-92-110/03/23 07:4310.0 2.1 1
Manganese, Dissolved 1320 ug/L 10/06/23 16:06 7439-96-510/03/23 07:4325.0 5.5 5
Nickel, Dissolved 1.6J ug/L 10/03/23 22:42 7440-02-010/03/23 07:435.0 1.0 1
Selenium, Dissolved ND ug/L 10/03/23 22:42 7782-49-210/03/23 07:4315.0 3.9 1
Silver, Dissolved ND ug/L 10/03/23 22:42 7440-22-410/03/23 07:435.0 1.0 1
Thallium, Dissolved ND ug/L 10/03/23 22:42 7440-28-010/03/23 07:4315.0 2.9 1
Vanadium, Dissolved 4.1J ug/L 10/03/23 22:42 7440-62-210/03/23 07:4310.0 1.0 1
Zinc, Dissolved ND ug/L 10/03/23 22:42 7440-66-610/03/23 07:4320.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: RW01WG-091923 Lab ID: 92689056002 Collected: 09/19/23 11:55 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 09:39 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:15 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/25/23 17:45 83-32-909/25/23 12:3110.0 2.0 1
Acenaphthylene ND ug/L 09/25/23 17:45 208-96-809/25/23 12:3110.0 2.0 1
Acetophenone ND ug/L 09/25/23 17:45 98-86-209/25/23 12:3110.0 1.5 1
Anthracene ND ug/L 09/25/23 17:45 120-12-709/25/23 12:3110.0 2.3 1
Atrazine ND ug/L 09/25/23 17:45 1912-24-909/25/23 12:3110.0 3.2 1
Benzaldehyde ND ug/L 09/25/23 17:45 100-52-709/25/23 12:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/25/23 17:45 56-55-309/25/23 12:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/25/23 17:45 50-32-809/25/23 12:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/25/23 17:45 205-99-209/25/23 12:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/25/23 17:45 191-24-209/25/23 12:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/25/23 17:45 207-08-909/25/23 12:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/25/23 17:45 92-52-409/25/23 12:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/25/23 17:45 101-55-309/25/23 12:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/25/23 17:45 85-68-709/25/23 12:3110.0 3.1 1
Caprolactam ND ug/L 09/25/23 17:45 105-60-209/25/23 12:3110.0 6.9 1
Carbazole ND ug/L 09/25/23 17:45 86-74-809/25/23 12:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/25/23 17:45 59-50-709/25/23 12:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/25/23 17:45 106-47-809/25/23 12:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/25/23 17:45 111-91-109/25/23 12:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/25/23 17:45 111-44-409/25/23 12:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/25/23 17:45 91-58-709/25/23 12:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/25/23 17:45 95-57-809/25/23 12:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/25/23 17:45 7005-72-309/25/23 12:3110.0 2.0 1
Chrysene ND ug/L 09/25/23 17:45 218-01-909/25/23 12:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/25/23 17:45 53-70-309/25/23 12:3110.0 3.0 1
Dibenzofuran ND ug/L 09/25/23 17:45 132-64-909/25/23 12:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/25/23 17:45 91-94-109/25/23 12:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/25/23 17:45 120-83-209/25/23 12:3110.0 1.4 1
Diethylphthalate ND ug/L 09/25/23 17:45 84-66-209/25/23 12:3110.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/25/23 17:45 105-67-909/25/23 12:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/25/23 17:45 131-11-309/25/23 12:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/25/23 17:45 84-74-209/25/23 12:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/25/23 17:45 534-52-109/25/23 12:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/25/23 17:45 51-28-509/25/23 12:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/25/23 17:45 121-14-209/25/23 12:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/25/23 17:45 606-20-209/25/23 12:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/25/23 17:45 117-84-009/25/23 12:3110.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: RW01WG-091923 Lab ID: 92689056002 Collected: 09/19/23 11:55 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/25/23 17:45 117-81-709/25/23 12:316.0 3.7 1
Fluoranthene ND ug/L 09/25/23 17:45 206-44-009/25/23 12:3110.0 2.2 1
Fluorene ND ug/L 09/25/23 17:45 86-73-709/25/23 12:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/25/23 17:45 87-68-309/25/23 12:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/25/23 17:45 118-74-109/25/23 12:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/25/23 17:45 77-47-409/25/23 12:3110.0 1.6 1
Hexachloroethane ND ug/L 09/25/23 17:45 67-72-109/25/23 12:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/25/23 17:45 193-39-509/25/23 12:3110.0 2.9 1
Isophorone ND ug/L 09/25/23 17:45 78-59-109/25/23 12:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/25/23 17:45 91-57-609/25/23 12:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/25/23 17:45 95-48-709/25/23 12:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/25/23 17:45 15831-10-409/25/23 12:3110.0 1.2 1
Naphthalene ND ug/L 09/25/23 17:45 91-20-309/25/23 12:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/25/23 17:45 88-74-409/25/23 12:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/25/23 17:45 99-09-209/25/23 12:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/25/23 17:45 100-01-609/25/23 12:3120.0 5.1 1
Nitrobenzene ND ug/L 09/25/23 17:45 98-95-309/25/23 12:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/25/23 17:45 88-75-509/25/23 12:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/25/23 17:45 100-02-709/25/23 12:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/25/23 17:45 621-64-709/25/23 12:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/25/23 17:45 86-30-609/25/23 12:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/25/23 17:45 108-60-109/25/23 12:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/25/23 17:45 87-86-509/25/23 12:3120.0 3.8 1
Phenanthrene ND ug/L 09/25/23 17:45 85-01-809/25/23 12:3110.0 2.0 1
Phenol ND ug/L 09/25/23 17:45 108-95-209/25/23 12:3110.0 1.4 1
Pyrene ND ug/L 09/25/23 17:45 129-00-009/25/23 12:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/25/23 17:45 95-95-409/25/23 12:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/25/23 17:45 88-06-209/25/23 12:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)108 %09/25/23 17:45 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)95 %09/25/23 17:45 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)140 %09/25/23 17:45 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)52 %09/25/23 17:45 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)76 %09/25/23 17:45 367-12-409/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)141 %09/25/23 17:45 118-79-609/25/23 12:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 07:58 67-64-125.0 5.1 1
Benzene 2.7 ug/L 09/30/23 07:58 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 07:58 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 07:58 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 07:58 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 07:58 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 07:58 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: RW01WG-091923 Lab ID: 92689056002 Collected: 09/19/23 11:55 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/30/23 07:58 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 07:58 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 07:58 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 07:58 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 07:58 74-87-31.0 0.54 1
Cyclohexane 0.76J ug/L 09/30/23 07:58 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 07:58 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 07:58 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 07:58 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 07:58 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 07:58 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 07:58 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 07:58 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 07:58 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 07:58 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 07:58 75-35-4 v11.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 07:58 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 07:58 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 07:58 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 07:58 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 07:58 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 07:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 07:58 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 07:58 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 07:58 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 07:58 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 07:58 75-09-2 v15.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 07:58 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 07:58 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 07:58 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 07:58 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 07:58 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 07:58 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 07:58 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 07:58 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 07:58 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 07:58 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 07:58 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 07:58 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 07:58 75-01-41.0 0.39 1
m&p-Xylene 0.71J ug/L 09/30/23 07:58 179601-23-12.0 0.71 1
o-Xylene 0.40J ug/L 09/30/23 07:58 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %09/30/23 07:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/30/23 07:58 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: RW01WG-091923 Lab ID: 92689056002 Collected: 09/19/23 11:55 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)98 %09/30/23 07:58 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 370 mg/L 09/27/23 22:415.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/22/23 08:06 18496-25-80.10 0.022 1
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 48.0 mg/L 09/21/23 20:06 16887-00-61.0 0.60 1
Sulfate 41.8 mg/L 09/21/23 20:06 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ20WG-091923 Lab ID: 92689056003 Collected: 09/19/23 17:20 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 7.9 Std. Units 09/21/23 10:4250
True Color 250 units 09/21/23 10:42250 250 50
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/04/23 18:09 7440-36-010/04/23 07:0415.0 5.5 1
Arsenic 4.9J ug/L 10/04/23 18:09 7440-38-210/04/23 07:0410.0 3.4 1
Barium 36.7 ug/L 10/04/23 18:09 7440-39-310/04/23 07:0410.0 0.84 1
Beryllium ND ug/L 10/04/23 18:09 7440-41-710/04/23 07:044.0 0.17 1
Boron 110 ug/L 10/04/23 18:09 7440-42-810/04/23 07:0450.0 12.4 1
Cadmium 0.37J ug/L 10/04/23 18:09 7440-43-910/04/23 07:041.0 0.33 1
Chromium 3.9J ug/L 10/04/23 18:09 7440-47-310/04/23 07:045.0 1.7 1
Cobalt 2.7J ug/L 10/04/23 18:09 7440-48-410/04/23 07:0410.0 0.96 1
Copper 4.6J ug/L 10/04/23 18:09 7440-50-810/04/23 07:045.0 2.6 1
Lead ND ug/L 10/04/23 18:09 7439-92-110/04/23 07:0410.0 2.1 1
Manganese 799 ug/L 10/04/23 18:09 7439-96-510/04/23 07:045.0 1.1 1
Nickel 5.8 ug/L 10/04/23 18:09 7440-02-010/04/23 07:045.0 1.0 1
Selenium ND ug/L 10/04/23 18:09 7782-49-210/04/23 07:0415.0 3.9 1
Silver ND ug/L 10/04/23 18:09 7440-22-410/04/23 07:045.0 1.0 1
Thallium ND ug/L 10/04/23 18:09 7440-28-010/04/23 07:0415.0 2.9 1
Vanadium 17.8 ug/L 10/04/23 18:09 7440-62-210/04/23 07:0410.0 1.0 1
Zinc 27.5 ug/L 10/04/23 18:09 7440-66-610/04/23 07:0420.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/03/23 22:45 7440-36-010/03/23 07:4315.0 5.5 1
Arsenic, Dissolved ND ug/L 10/03/23 22:45 7440-38-210/03/23 07:4310.0 3.4 1
Barium, Dissolved 34.3 ug/L 10/03/23 22:45 7440-39-310/03/23 07:4310.0 0.84 1
Beryllium, Dissolved ND ug/L 10/03/23 22:45 7440-41-710/03/23 07:434.0 0.17 1
Boron, Dissolved 115 ug/L 10/03/23 22:45 7440-42-810/03/23 07:4350.0 12.4 1
Cadmium, Dissolved ND ug/L 10/03/23 22:45 7440-43-910/03/23 07:431.0 0.33 1
Chromium, Dissolved 2.1J ug/L 10/03/23 22:45 7440-47-310/03/23 07:435.0 1.7 1
Cobalt, Dissolved ND ug/L 10/03/23 22:45 7440-48-410/03/23 07:4310.0 0.96 1
Copper, Dissolved ND ug/L 10/03/23 22:45 7440-50-810/03/23 07:435.0 2.6 1
Lead, Dissolved ND ug/L 10/03/23 22:45 7439-92-110/03/23 07:4310.0 2.1 1
Manganese, Dissolved 824 ug/L 10/03/23 22:45 7439-96-510/03/23 07:435.0 1.1 1
Nickel, Dissolved 1.5J ug/L 10/03/23 22:45 7440-02-010/03/23 07:435.0 1.0 1
Selenium, Dissolved ND ug/L 10/03/23 22:45 7782-49-210/03/23 07:4315.0 3.9 1
Silver, Dissolved ND ug/L 10/03/23 22:45 7440-22-410/03/23 07:435.0 1.0 1
Thallium, Dissolved ND ug/L 10/03/23 22:45 7440-28-010/03/23 07:4315.0 2.9 1
Vanadium, Dissolved 9.4J ug/L 10/03/23 22:45 7440-62-210/03/23 07:4310.0 1.0 1
Zinc, Dissolved ND ug/L 10/03/23 22:45 7440-66-610/03/23 07:4320.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ20WG-091923 Lab ID: 92689056003 Collected: 09/19/23 17:20 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 09:41 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:18 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/26/23 10:48 83-32-909/25/23 12:31100 20.1 10
Acenaphthylene ND ug/L 09/26/23 10:48 208-96-809/25/23 12:31100 19.5 10
Acetophenone ND ug/L 09/26/23 10:48 98-86-209/25/23 12:31100 15.0 10
Anthracene ND ug/L 09/26/23 10:48 120-12-709/25/23 12:31100 23.1 10
Atrazine ND ug/L 09/26/23 10:48 1912-24-909/25/23 12:31100 31.8 10
Benzaldehyde ND ug/L 09/26/23 10:48 100-52-709/25/23 12:31100 36.0 10
Benzo(a)anthracene ND ug/L 09/26/23 10:48 56-55-309/25/23 12:31100 26.9 10
Benzo(a)pyrene ND ug/L 09/26/23 10:48 50-32-809/25/23 12:31100 27.8 10
Benzo(b)fluoranthene ND ug/L 09/26/23 10:48 205-99-209/25/23 12:31100 26.0 10
Benzo(g,h,i)perylene ND ug/L 09/26/23 10:48 191-24-209/25/23 12:31100 28.4 10
Benzo(k)fluoranthene ND ug/L 09/26/23 10:48 207-08-909/25/23 12:31100 27.1 10
Biphenyl (Diphenyl)ND ug/L 09/26/23 10:48 92-52-409/25/23 12:31100 18.2 10
4-Bromophenylphenyl ether ND ug/L 09/26/23 10:48 101-55-309/25/23 12:31100 17.7 10
Butylbenzylphthalate ND ug/L 09/26/23 10:48 85-68-709/25/23 12:31100 31.4 10
Caprolactam ND ug/L 09/26/23 10:48 105-60-209/25/23 12:31100 69.4 10
Carbazole ND ug/L 09/26/23 10:48 86-74-809/25/23 12:31100 23.5 10
4-Chloro-3-methylphenol ND ug/L 09/26/23 10:48 59-50-709/25/23 12:31100 33.4 10
4-Chloroaniline ND ug/L 09/26/23 10:48 106-47-809/25/23 12:31200 36.3 10
bis(2-Chloroethoxy)methane ND ug/L 09/26/23 10:48 111-91-109/25/23 12:31100 18.2 10
bis(2-Chloroethyl) ether ND ug/L 09/26/23 10:48 111-44-409/25/23 12:31100 19.1 10
2-Chloronaphthalene ND ug/L 09/26/23 10:48 91-58-709/25/23 12:31100 17.2 10
2-Chlorophenol ND ug/L 09/26/23 10:48 95-57-809/25/23 12:31100 12.0 10
4-Chlorophenylphenyl ether ND ug/L 09/26/23 10:48 7005-72-309/25/23 12:31100 20.0 10
Chrysene ND ug/L 09/26/23 10:48 218-01-909/25/23 12:31100 27.7 10
Dibenz(a,h)anthracene ND ug/L 09/26/23 10:48 53-70-309/25/23 12:31100 29.5 10
Dibenzofuran ND ug/L 09/26/23 10:48 132-64-909/25/23 12:31100 21.0 10
3,3'-Dichlorobenzidine ND ug/L 09/26/23 10:48 91-94-109/25/23 12:31200 81.2 10
2,4-Dichlorophenol ND ug/L 09/26/23 10:48 120-83-209/25/23 12:31100 14.0 10
Diethylphthalate ND ug/L 09/26/23 10:48 84-66-209/25/23 12:31100 20.5 10
2,4-Dimethylphenol ND ug/L 09/26/23 10:48 105-67-909/25/23 12:31100 17.0 10
Dimethylphthalate ND ug/L 09/26/23 10:48 131-11-309/25/23 12:31100 21.3 10
Di-n-butylphthalate ND ug/L 09/26/23 10:48 84-74-209/25/23 12:31100 22.0 10
4,6-Dinitro-2-methylphenol ND ug/L 09/26/23 10:48 534-52-109/25/23 12:31200 77.8 10
2,4-Dinitrophenol ND ug/L 09/26/23 10:48 51-28-509/25/23 12:31500 260 10
2,4-Dinitrotoluene ND ug/L 09/26/23 10:48 121-14-209/25/23 12:31100 16.2 10
2,6-Dinitrotoluene ND ug/L 09/26/23 10:48 606-20-209/25/23 12:31100 17.2 10
Di-n-octylphthalate ND ug/L 09/26/23 10:48 117-84-009/25/23 12:31100 39.2 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ20WG-091923 Lab ID: 92689056003 Collected: 09/19/23 17:20 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/26/23 10:48 117-81-709/25/23 12:3160.0 37.3 10
Fluoranthene ND ug/L 09/26/23 10:48 206-44-009/25/23 12:31100 21.9 10
Fluorene ND ug/L 09/26/23 10:48 86-73-709/25/23 12:31100 20.9 10
Hexachloro-1,3-butadiene ND ug/L 09/26/23 10:48 87-68-309/25/23 12:31100 17.7 10
Hexachlorobenzene ND ug/L 09/26/23 10:48 118-74-109/25/23 12:31100 21.6 10
Hexachlorocyclopentadiene ND ug/L 09/26/23 10:48 77-47-409/25/23 12:31100 15.9 10
Hexachloroethane ND ug/L 09/26/23 10:48 67-72-109/25/23 12:31100 13.8 10
Indeno(1,2,3-cd)pyrene ND ug/L 09/26/23 10:48 193-39-509/25/23 12:31100 28.9 10
Isophorone ND ug/L 09/26/23 10:48 78-59-109/25/23 12:31100 16.6 10
2-Methylnaphthalene ND ug/L 09/26/23 10:48 91-57-609/25/23 12:31100 18.7 10
2-Methylphenol(o-Cresol)ND ug/L 09/26/23 10:48 95-48-709/25/23 12:31100 18.7 10
3&4-Methylphenol(m&p Cresol)ND ug/L 09/26/23 10:48 15831-10-409/25/23 12:31100 12.2 10
Naphthalene ND ug/L 09/26/23 10:48 91-20-309/25/23 12:31100 20.9 10
2-Nitroaniline ND ug/L 09/26/23 10:48 88-74-409/25/23 12:31200 29.8 10
3-Nitroaniline ND ug/L 09/26/23 10:48 99-09-209/25/23 12:31200 37.5 10
4-Nitroaniline ND ug/L 09/26/23 10:48 100-01-609/25/23 12:31200 51.0 10
Nitrobenzene ND ug/L 09/26/23 10:48 98-95-309/25/23 12:31100 18.7 10
2-Nitrophenol ND ug/L 09/26/23 10:48 88-75-509/25/23 12:31100 14.0 10
4-Nitrophenol ND ug/L 09/26/23 10:48 100-02-709/25/23 12:31500 65.9 10
N-Nitroso-di-n-propylamine ND ug/L 09/26/23 10:48 621-64-709/25/23 12:31100 13.3 10
N-Nitrosodiphenylamine ND ug/L 09/26/23 10:48 86-30-609/25/23 12:31100 30.0 10
2,2'-Oxybis(1-chloropropane)ND ug/L 09/26/23 10:48 108-60-109/25/23 12:31100 11.5 10
Pentachlorophenol ND ug/L 09/26/23 10:48 87-86-509/25/23 12:31200 37.6 10
Phenanthrene ND ug/L 09/26/23 10:48 85-01-809/25/23 12:31100 20.0 10
Phenol ND ug/L 09/26/23 10:48 108-95-209/25/23 12:31100 13.5 10
Pyrene ND ug/L 09/26/23 10:48 129-00-009/25/23 12:31100 22.0 10
2,4,5-Trichlorophenol ND ug/L 09/26/23 10:48 95-95-409/25/23 12:31100 14.2 10
2,4,6-Trichlorophenol ND ug/L 09/26/23 10:48 88-06-209/25/23 12:31100 15.5 10
Surrogates
Nitrobenzene-d5 (S)0 %09/26/23 10:48 4165-60-0 D3,S409/25/23 12:3110-138 10
2-Fluorobiphenyl (S)0 %09/26/23 10:48 321-60-8 S409/25/23 12:3110-130 10
Terphenyl-d14 (S)0 %09/26/23 10:48 1718-51-0 S409/25/23 12:3119-191 10
Phenol-d6 (S)0 %09/26/23 10:48 13127-88-3 S409/25/23 12:3110-130 10
2-Fluorophenol (S)0 %09/26/23 10:48 367-12-4 S409/25/23 12:3110-130 10
2,4,6-Tribromophenol (S)0 %09/26/23 10:48 118-79-6 S409/25/23 12:3110-164 10
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 26.5 ug/L 09/30/23 08:17 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 08:17 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 08:17 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 08:17 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 08:17 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 08:17 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 08:17 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ20WG-091923 Lab ID: 92689056003 Collected: 09/19/23 17:20 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/30/23 08:17 56-23-51.0 0.33 1
Chlorobenzene 0.44J ug/L 09/30/23 08:17 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 08:17 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 08:17 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 08:17 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 08:17 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 08:17 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 08:17 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 08:17 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 08:17 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 08:17 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 08:17 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 08:17 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 08:17 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 08:17 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 08:17 75-35-4 v11.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 08:17 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 08:17 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 08:17 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 08:17 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 08:17 10061-02-61.0 0.36 1
Ethylbenzene 4.3 ug/L 09/30/23 08:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 08:17 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 08:17 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 08:17 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 08:17 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 08:17 75-09-2 v15.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 08:17 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 08:17 1634-04-41.0 0.42 1
Styrene 0.64J ug/L 09/30/23 08:17 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 08:17 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 08:17 127-18-41.0 0.29 1
Toluene 20.5 ug/L 09/30/23 08:17 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 08:17 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 08:17 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 08:17 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 08:17 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 08:17 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 08:17 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 08:17 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 08:17 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 08:17 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)104 %09/30/23 08:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %09/30/23 08:17 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ20WG-091923 Lab ID: 92689056003 Collected: 09/19/23 17:20 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)101 %09/30/23 08:17 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 633 mg/L 09/27/23 22:505.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 11.5 mg/L 09/22/23 08:06 18496-25-85.0 1.1 50
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 16.4 mg/L 09/21/23 20:20 16887-00-61.0 0.60 1
Sulfate 19.3 mg/L 09/21/23 20:20 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ04WG-091923 Lab ID: 92689056004 Collected: 09/19/23 14:15 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
HEM, Oil and Grease
Oil and Grease ND mg/L 10/10/23 11:005.0 1.1 1
Analytical Method: EPA 8015C Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8015 Diesel Low Volume
Diesel Range Organics(C10-C28)ND mg/L 09/26/23 10:3409/25/23 13:124.2 1.3 1
Surrogatesn-Pentacosane (S)6 %09/26/23 10:34 629-99-2 P3,S209/25/23 13:1229-158 1
Analytical Method: RSK-175 Preparation Method: RSK175
Pace National - Mt. Juliet
VOA (GC) RSK175
Methane 721 ug/L 10/02/23 12:49 74-82-810/02/23 12:4910.0 2.91 1
Ethane ND ug/L 10/02/23 12:49 74-84-010/02/23 12:4913.0 4.07 1
Ethene ND ug/L 10/02/23 12:49 74-85-110/02/23 12:4913.0 4.26 1
n-Propane ND ug/L 10/02/23 12:49 74-98-610/02/23 12:4918.6 5.48 1
Analytical Method: EPA 5030B/8015C
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)0.41 mg/L 09/24/23 01:130.080 0.034 1
Surrogates4-Bromofluorobenzene (S)88 %09/24/23 01:13 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/04/23 18:12 7440-36-010/04/23 07:0415.0 5.5 1
Arsenic 254 ug/L 10/04/23 18:12 7440-38-210/04/23 07:0410.0 3.4 1
Barium 71.3 ug/L 10/04/23 18:12 7440-39-310/04/23 07:0410.0 0.84 1
Beryllium ND ug/L 10/04/23 18:12 7440-41-710/04/23 07:044.0 0.17 1
Boron 190 ug/L 10/04/23 18:12 7440-42-810/04/23 07:0450.0 12.4 1
Cadmium 0.81J ug/L 10/04/23 18:12 7440-43-910/04/23 07:041.0 0.33 1
Chromium 118 ug/L 10/04/23 18:12 7440-47-310/04/23 07:045.0 1.7 1
Cobalt 3.6J ug/L 10/04/23 18:12 7440-48-410/04/23 07:0410.0 0.96 1
Copper 22.2 ug/L 10/04/23 18:12 7440-50-810/04/23 07:045.0 2.6 1
Lead ND ug/L 10/04/23 18:12 7439-92-110/04/23 07:0410.0 2.1 1
Manganese 82.3 ug/L 10/04/23 18:12 7439-96-510/04/23 07:045.0 1.1 1
Nickel 117 ug/L 10/04/23 18:12 7440-02-010/04/23 07:045.0 1.0 1
Selenium 4.2J ug/L 10/04/23 18:12 7782-49-210/04/23 07:0415.0 3.9 1
Silver ND ug/L 10/04/23 18:12 7440-22-410/04/23 07:045.0 1.0 1
Thallium ND ug/L 10/05/23 12:10 7440-28-0 D310/04/23 07:0430.0 5.8 2
Vanadium 1320 ug/L 10/04/23 18:12 7440-62-210/04/23 07:0410.0 1.0 1
Zinc 29.8 ug/L 10/04/23 18:12 7440-66-610/04/23 07:0420.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved 17.9 ug/L 10/03/23 22:49 7440-36-010/03/23 07:4315.0 5.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ04WG-091923 Lab ID: 92689056004 Collected: 09/19/23 14:15 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Arsenic, Dissolved 297 ug/L 10/03/23 22:49 7440-38-210/03/23 07:4310.0 3.4 1
Barium, Dissolved 53.7 ug/L 10/03/23 22:49 7440-39-310/03/23 07:4310.0 0.84 1
Beryllium, Dissolved ND ug/L 10/03/23 22:49 7440-41-710/03/23 07:434.0 0.17 1
Boron, Dissolved 199 ug/L 10/03/23 22:49 7440-42-810/03/23 07:4350.0 12.4 1
Cadmium, Dissolved 0.34J ug/L 10/03/23 22:49 7440-43-910/03/23 07:431.0 0.33 1
Chromium, Dissolved 115 ug/L 10/03/23 22:49 7440-47-310/03/23 07:435.0 1.7 1
Cobalt, Dissolved 4.0J ug/L 10/03/23 22:49 7440-48-410/03/23 07:4310.0 0.96 1
Copper, Dissolved ND ug/L 10/03/23 22:49 7440-50-810/03/23 07:435.0 2.6 1
Lead, Dissolved ND ug/L 10/03/23 22:49 7439-92-110/03/23 07:4310.0 2.1 1
Manganese, Dissolved 23.0 ug/L 10/03/23 22:49 7439-96-510/03/23 07:435.0 1.1 1
Nickel, Dissolved 95.6 ug/L 10/03/23 22:49 7440-02-010/03/23 07:435.0 1.0 1
Selenium, Dissolved 6.1J ug/L 10/03/23 22:49 7782-49-210/03/23 07:4315.0 3.9 1
Silver, Dissolved ND ug/L 10/03/23 22:49 7440-22-410/03/23 07:435.0 1.0 1
Thallium, Dissolved ND ug/L 10/03/23 22:49 7440-28-0 IS10/03/23 07:4315.0 2.9 1
Vanadium, Dissolved 1340 ug/L 10/03/23 22:49 7440-62-210/03/23 07:4310.0 1.0 1
Zinc, Dissolved 15.4J ug/L 10/03/23 22:49 7440-66-610/03/23 07:4320.0 11.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury 3.2 ug/L 10/09/23 09:44 7439-97-6 D310/05/23 10:340.40 0.28 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved 3.6 ug/L 10/09/23 11:20 7439-97-6 D310/05/23 11:370.40 0.28 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/25/23 18:36 83-32-909/25/23 12:3150.0 10.0 1
Acenaphthylene ND ug/L 09/25/23 18:36 208-96-809/25/23 12:3150.0 9.8 1
Acetophenone ND ug/L 09/25/23 18:36 98-86-209/25/23 12:3150.0 7.5 1
Anthracene ND ug/L 09/25/23 18:36 120-12-709/25/23 12:3150.0 11.6 1
Atrazine ND ug/L 09/25/23 18:36 1912-24-909/25/23 12:3150.0 15.9 1
Benzaldehyde ND ug/L 09/25/23 18:36 100-52-709/25/23 12:3150.0 18.0 1
Benzo(a)anthracene ND ug/L 09/25/23 18:36 56-55-309/25/23 12:3150.0 13.4 1
Benzo(a)pyrene ND ug/L 09/25/23 18:36 50-32-809/25/23 12:3150.0 13.9 1
Benzo(b)fluoranthene ND ug/L 09/25/23 18:36 205-99-209/25/23 12:3150.0 13.0 1
Benzo(g,h,i)perylene ND ug/L 09/25/23 18:36 191-24-209/25/23 12:3150.0 14.2 1
Benzo(k)fluoranthene ND ug/L 09/25/23 18:36 207-08-909/25/23 12:3150.0 13.6 1
Biphenyl (Diphenyl)ND ug/L 09/25/23 18:36 92-52-409/25/23 12:3150.0 9.1 1
4-Bromophenylphenyl ether ND ug/L 09/25/23 18:36 101-55-309/25/23 12:3150.0 8.8 1
Butylbenzylphthalate ND ug/L 09/25/23 18:36 85-68-709/25/23 12:3150.0 15.7 1
Caprolactam ND ug/L 09/25/23 18:36 105-60-209/25/23 12:3150.0 34.7 1
Carbazole ND ug/L 09/25/23 18:36 86-74-809/25/23 12:3150.0 11.8 1
4-Chloro-3-methylphenol ND ug/L 09/25/23 18:36 59-50-709/25/23 12:3150.0 16.7 1
4-Chloroaniline ND ug/L 09/25/23 18:36 106-47-809/25/23 12:31100 18.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ04WG-091923 Lab ID: 92689056004 Collected: 09/19/23 14:15 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Chloroethoxy)methane ND ug/L 09/25/23 18:36 111-91-109/25/23 12:3150.0 9.1 1
bis(2-Chloroethyl) ether ND ug/L 09/25/23 18:36 111-44-409/25/23 12:3150.0 9.6 1
2-Chloronaphthalene ND ug/L 09/25/23 18:36 91-58-709/25/23 12:3150.0 8.6 1
2-Chlorophenol ND ug/L 09/25/23 18:36 95-57-809/25/23 12:3150.0 6.0 1
4-Chlorophenylphenyl ether ND ug/L 09/25/23 18:36 7005-72-309/25/23 12:3150.0 10.0 1
Chrysene ND ug/L 09/25/23 18:36 218-01-909/25/23 12:3150.0 13.8 1
Dibenz(a,h)anthracene ND ug/L 09/25/23 18:36 53-70-309/25/23 12:3150.0 14.8 1
Dibenzofuran ND ug/L 09/25/23 18:36 132-64-909/25/23 12:3150.0 10.5 1
3,3'-Dichlorobenzidine ND ug/L 09/25/23 18:36 91-94-109/25/23 12:31100 40.6 1
2,4-Dichlorophenol ND ug/L 09/25/23 18:36 120-83-209/25/23 12:3150.0 7.0 1
Diethylphthalate ND ug/L 09/25/23 18:36 84-66-209/25/23 12:3150.0 10.2 1
2,4-Dimethylphenol ND ug/L 09/25/23 18:36 105-67-909/25/23 12:3150.0 8.5 1
Dimethylphthalate ND ug/L 09/25/23 18:36 131-11-309/25/23 12:3150.0 10.6 1
Di-n-butylphthalate ND ug/L 09/25/23 18:36 84-74-209/25/23 12:3150.0 11.0 1
4,6-Dinitro-2-methylphenol ND ug/L 09/25/23 18:36 534-52-109/25/23 12:31100 38.9 1
2,4-Dinitrophenol ND ug/L 09/25/23 18:36 51-28-509/25/23 12:31250 130 1
2,4-Dinitrotoluene ND ug/L 09/25/23 18:36 121-14-209/25/23 12:3150.0 8.1 1
2,6-Dinitrotoluene ND ug/L 09/25/23 18:36 606-20-209/25/23 12:3150.0 8.6 1
Di-n-octylphthalate ND ug/L 09/25/23 18:36 117-84-009/25/23 12:3150.0 19.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/25/23 18:36 117-81-709/25/23 12:3130.0 18.6 1
Fluoranthene ND ug/L 09/25/23 18:36 206-44-009/25/23 12:3150.0 11.0 1
Fluorene ND ug/L 09/25/23 18:36 86-73-709/25/23 12:3150.0 10.4 1
Hexachloro-1,3-butadiene ND ug/L 09/25/23 18:36 87-68-309/25/23 12:3150.0 8.8 1
Hexachlorobenzene ND ug/L 09/25/23 18:36 118-74-109/25/23 12:3150.0 10.8 1
Hexachlorocyclopentadiene ND ug/L 09/25/23 18:36 77-47-409/25/23 12:3150.0 8.0 1
Hexachloroethane ND ug/L 09/25/23 18:36 67-72-109/25/23 12:3150.0 6.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/25/23 18:36 193-39-509/25/23 12:3150.0 14.4 1
Isophorone ND ug/L 09/25/23 18:36 78-59-109/25/23 12:3150.0 8.3 1
2-Methylnaphthalene ND ug/L 09/25/23 18:36 91-57-609/25/23 12:3150.0 9.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/25/23 18:36 95-48-709/25/23 12:3150.0 9.4 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/25/23 18:36 15831-10-409/25/23 12:3150.0 6.1 1
Naphthalene ND ug/L 09/25/23 18:36 91-20-309/25/23 12:3150.0 10.4 1
2-Nitroaniline ND ug/L 09/25/23 18:36 88-74-409/25/23 12:31100 14.9 1
3-Nitroaniline ND ug/L 09/25/23 18:36 99-09-209/25/23 12:31100 18.8 1
4-Nitroaniline ND ug/L 09/25/23 18:36 100-01-609/25/23 12:31100 25.5 1
Nitrobenzene ND ug/L 09/25/23 18:36 98-95-309/25/23 12:3150.0 9.4 1
2-Nitrophenol ND ug/L 09/25/23 18:36 88-75-509/25/23 12:3150.0 7.0 1
4-Nitrophenol ND ug/L 09/25/23 18:36 100-02-709/25/23 12:31250 33.0 1
N-Nitroso-di-n-propylamine ND ug/L 09/25/23 18:36 621-64-709/25/23 12:3150.0 6.6 1
N-Nitrosodiphenylamine ND ug/L 09/25/23 18:36 86-30-609/25/23 12:3150.0 15.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/25/23 18:36 108-60-109/25/23 12:3150.0 5.8 1
Pentachlorophenol ND ug/L 09/25/23 18:36 87-86-509/25/23 12:31100 18.8 1
Phenanthrene ND ug/L 09/25/23 18:36 85-01-809/25/23 12:3150.0 10.0 1
Phenol ND ug/L 09/25/23 18:36 108-95-209/25/23 12:3150.0 6.8 1
Pyrene ND ug/L 09/25/23 18:36 129-00-009/25/23 12:3150.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ04WG-091923 Lab ID: 92689056004 Collected: 09/19/23 14:15 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4,5-Trichlorophenol ND ug/L 09/25/23 18:36 95-95-409/25/23 12:3150.0 7.1 1
2,4,6-Trichlorophenol ND ug/L 09/25/23 18:36 88-06-209/25/23 12:3150.0 7.8 1
Surrogates
Nitrobenzene-d5 (S)110 %09/25/23 18:36 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)97 %09/25/23 18:36 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)136 %09/25/23 18:36 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)58 %09/25/23 18:36 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)79 %09/25/23 18:36 367-12-409/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)124 %09/25/23 18:36 118-79-609/25/23 12:3110-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 18.0J ug/L 09/30/23 19:16 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 19:16 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 19:16 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 19:16 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 19:16 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 19:16 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 19:16 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/30/23 19:16 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 19:16 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 19:16 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 19:16 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 19:16 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 19:16 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 19:16 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 19:16 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 19:16 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 19:16 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 19:16 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 19:16 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 19:16 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 19:16 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 19:16 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 19:16 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 19:16 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 19:16 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 19:16 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 19:16 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 19:16 10061-02-61.0 0.36 1
Ethylbenzene 72.9 ug/L 09/30/23 19:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 19:16 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)2.5 ug/L 09/30/23 19:16 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 19:16 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 19:16 108-87-210.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ04WG-091923 Lab ID: 92689056004 Collected: 09/19/23 14:15 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Methylene Chloride ND ug/L 09/30/23 19:16 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 19:16 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 19:16 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 19:16 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 19:16 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 19:16 127-18-41.0 0.29 1
Toluene 1.1 ug/L 09/30/23 19:16 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 19:16 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 19:16 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 19:16 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 19:16 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 19:16 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 19:16 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 19:16 75-01-41.0 0.39 1
m&p-Xylene 240 ug/L 09/30/23 19:16 179601-23-12.0 0.71 1
o-Xylene 119 ug/L 09/30/23 19:16 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)106 %09/30/23 19:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %09/30/23 19:16 17060-07-070-130 1
Toluene-d8 (S)100 %09/30/23 19:16 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 4180 mg/L 10/03/23 13:595.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 16200 mg/L 09/20/23 21:042500 2500 1
Analytical Method: SM 2540D-2015
Pace Analytical Services - Asheville
2540D Total Suspended Solids
Total Suspended Solids 12.3 mg/L 09/20/23 20:373.0 3.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 33.0 mg/L 09/22/23 08:06 18496-25-85.0 1.1 50
Analytical Method: SM 5210B-2016
Pace Analytical Services - Asheville
5210B BOD, 5 day
BOD, 5 day 76.8 mg/L 09/26/23 05:49 B209/21/23 07:132.0 2.0 1
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
9040 pH
pH at 25 Degrees C 11.6 Std. Units 10/05/23 15:51 H30.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 101
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Sample: PZ04WG-091923 Lab ID: 92689056004 Collected: 09/19/23 14:15 Received: 09/20/23 08:25 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 7.4 mg/L 10/06/23 04:04 7727-37-910/05/23 14:205.0 2.5 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 09/21/23 01:14 14797-55-80.040 0.010 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand 1030 mg/L 10/06/23 00:1610/05/23 01:5250.0 25.0 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon 144 mg/L 10/04/23 01:36 7440-44-050.0 25.0 50
Analytical Method: EPA 9056A
Pace Analytical Services - Asheville
9056 IC anions 28 Days
Chloride 4960 mg/L 09/21/23 23:08 16887-00-6100 60.0 100
Sulfate 824 mg/L 09/21/23 20:34 14808-79-820.0 10.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801021
SM 2120B-2011
SM 2120B-2011
2120B True Color EDEN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples: 92689056001, 92689056002, 92689056003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4149069
Associated Lab Samples:92689056001, 92689056002, 92689056003
Matrix: Water
AnalyzedMDL
True Color units ND 5.0 09/21/23 08:275.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4149070LABORATORY CONTROL SAMPLE:
LCSSpike
True Color units 35.035 100 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689056001
4149071SAMPLE DUPLICATE:
pH Std. Units 6.4 H10106.4
True Color units 5.0 H10105.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804855
EPA 1664B
EPA 1664B
1664 HEM, Oil and Grease
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4168212
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Oil and Grease mg/L ND 5.0 10/10/23 11:001.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4168213LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/L 32.140 80 78-114
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4168214MATRIX SPIKE SAMPLE:
MSSpike
Result
92689056004
Oil and Grease mg/L 31.939.6 79 78-114ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92690141001
4168215SAMPLE DUPLICATE:
Oil and Grease mg/L 1.1J 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2142504
RSK175
RSK-175
VOA (GC) RSK175
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3980567-2
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Methane ug/L ND 10.0 10/02/23 10:422.91
Ethane ug/L ND 13.0 10/02/23 10:424.07
Ethene ug/L ND 13.0 10/02/23 10:424.26
n-Propane ug/L ND 18.6 10/02/23 10:425.48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3980567-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3980567-5
Methane ug/L 67.267.8 99.1 85.0-11511175.2 11.2 20
Ethane ug/L 117129 90.7 85.0-11589.9116 0.858 20
Ethene ug/L 117127 92.1 85.0-11590.6115 1.72 20
n-Propane ug/L 172186 92.5 85.0-11591.4170 1.17 20
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1657583-04
R3980567-3SAMPLE DUPLICATE:
Methane ug/L ND 0.00 20ND
Ethane ug/L ND 0.00 20ND
Ethene ug/L ND 0.00 20ND
n-Propane ug/L ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1660867-05
R3980567-4SAMPLE DUPLICATE:
Methane ug/L 1290 0.778 201280
Ethane ug/L 10.7J J5.45 2011.3
Ethene ug/L ND 0.00 20ND
n-Propane ug/L 49.6 0.202 2049.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801614
EPA 5030B/8015C
EPA 5030B/8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152640
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Gas Range Organics (C6-C10)mg/L ND 0.080 09/23/23 19:070.034
4-Bromofluorobenzene (S)%85 70-130 09/23/23 19:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152641LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/L 1.01 102 70-130
4-Bromofluorobenzene (S)%87 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4152643MATRIX SPIKE SAMPLE:
MSSpike
Result
92688903001
Gas Range Organics (C6-C10)mg/L 1.21 108 63-1300.15
4-Bromofluorobenzene (S)%89 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688992001
4152642SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/L ND F1,HS30ND
4-Bromofluorobenzene (S)%8685
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
955304
EPA 7470
EPA 7470
7470 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92689056001, 92689056002, 92689056003, 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5252836
Associated Lab Samples:92689056001, 92689056002, 92689056003, 92689056004
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/09/23 09:320.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5252837LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.12 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5252838MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5252839
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 99 75-12596 3 202ND2.1 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
955306
EPA 7470
EPA 7470
7470 Mercury Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92689056001, 92689056002, 92689056003, 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5252843
Associated Lab Samples:92689056001, 92689056002, 92689056003, 92689056004
Matrix: Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/09/23 11:080.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5252844LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.12 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5252845MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5252846
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2 100 85-11598 2 202ND2.0 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954997
EPA 3010
EPA 6010
6010 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92689056001, 92689056002, 92689056003, 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5251493
Associated Lab Samples:92689056001, 92689056002, 92689056003, 92689056004
Matrix: Water
AnalyzedMDL
Antimony ug/L ND 15.0 10/05/23 10:225.5
Arsenic ug/L ND 10.0 10/05/23 10:223.4
Barium ug/L ND 10.0 10/05/23 10:220.84
Beryllium ug/L ND 4.0 10/05/23 10:220.17
Boron ug/L ND 50.0 10/05/23 10:2212.4
Cadmium ug/L ND 1.0 10/05/23 10:220.33
Chromium ug/L ND 5.0 10/05/23 10:221.7
Cobalt ug/L ND 10.0 10/05/23 10:220.96
Copper ug/L ND 5.0 10/05/23 10:222.6
Lead ug/L ND 10.0 10/05/23 10:222.1
Manganese ug/L ND 5.0 10/05/23 10:221.1
Nickel ug/L ND 5.0 10/05/23 10:221.0
Selenium ug/L ND 15.0 10/05/23 10:223.9
Silver ug/L ND 5.0 10/05/23 10:221.0
Thallium ug/L ND 15.0 10/05/23 10:222.9
Vanadium ug/L ND 10.0 10/05/23 10:221.0
Zinc ug/L ND 20.0 10/05/23 10:2211.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5251494LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 238250 95 80-120
Arsenic ug/L 233250 93 80-120
Barium ug/L 239250 96 80-120
Beryllium ug/L 23.425 94 80-120
Boron ug/L 11701250 94 80-120
Cadmium ug/L 24.725 99 80-120
Chromium ug/L 237250 95 80-120
Cobalt ug/L 240250 96 80-120
Copper ug/L 230250 92 80-120
Lead ug/L 243250 97 80-120
Manganese ug/L 236250 94 80-120
Nickel ug/L 246250 99 80-120
Selenium ug/L 244250 98 80-120
Silver ug/L 22.925 92 80-120
Thallium ug/L 243250 97 80-120
Vanadium ug/L 235250 94 80-120
Zinc ug/L 12301250 98 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5251495MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35831393001
5251496
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 250 96 75-12597 1 202505.5U 242 245
Arsenic ug/L 250 93 75-12595 2 202503.4U 235 239
Barium ug/L 250 95 75-12596 1 202503.0J 241 244
Beryllium ug/L 25 95 75-12596 1 20250.17U 23.8 24.0
Boron ug/L 1250 95 75-12596 1 20125016.4J 1210 1220
Cadmium ug/L 25 98 75-12599 1 20250.33U 24.7 24.9
Chromium ug/L 250 96 75-12596 1 202501.7U 241 242
Cobalt ug/L 250 98 75-12599 1 202500.96U 244 247
Copper ug/L 250 95 75-12596 1 202502.6U 239 241
Lead ug/L 250 97 75-12598 1 202502.1U 243 245
Manganese ug/L 250 95 75-12595 1 202501.1J 238 239
Nickel ug/L 250 99 75-125100 1 202501.0U 247 249
Selenium ug/L 250 84 75-12585 1 202503.9U 211 213
Silver ug/L 25 94 75-12596 1 20251.0U 23.6 23.9
Thallium ug/L 250 96 75-12597 1 202502.9U 242 244
Vanadium ug/L 250 96 75-12596 1 202502.8J 242 243
Zinc ug/L 1250 97 75-12598 1 20125011.0U 1220 1230
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954621
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92689056001, 92689056002, 92689056003, 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5249505
Associated Lab Samples:92689056001, 92689056002, 92689056003, 92689056004
Matrix: Water
AnalyzedMDL
Antimony, Dissolved ug/L ND 15.0 10/03/23 20:005.5
Arsenic, Dissolved ug/L ND 10.0 10/04/23 01:413.4
Barium, Dissolved ug/L ND 10.0 10/04/23 01:410.84
Beryllium, Dissolved ug/L ND 4.0 10/04/23 01:410.17
Boron, Dissolved ug/L ND 50.0 10/04/23 01:4112.4
Cadmium, Dissolved ug/L ND 1.0 10/04/23 01:410.33
Chromium, Dissolved ug/L ND 5.0 10/04/23 01:411.7
Cobalt, Dissolved ug/L ND 10.0 10/04/23 01:410.96
Copper, Dissolved ug/L ND 5.0 10/04/23 01:412.6
Lead, Dissolved ug/L ND 10.0 10/04/23 01:412.1
Manganese, Dissolved ug/L ND 5.0 10/04/23 01:411.1
Nickel, Dissolved ug/L ND 5.0 10/04/23 01:411.0
Selenium, Dissolved ug/L ND 15.0 10/04/23 01:413.9
Silver, Dissolved ug/L ND 5.0 10/04/23 01:411.0
Thallium, Dissolved ug/L ND 15.0 10/04/23 01:412.9
Vanadium, Dissolved ug/L ND 10.0 10/04/23 01:411.0
Zinc, Dissolved ug/L ND 20.0 10/04/23 01:4111.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5249506LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 238250 95 80-120
Arsenic, Dissolved ug/L 243250 97 80-120
Barium, Dissolved ug/L 242250 97 80-120
Beryllium, Dissolved ug/L 24.325 97 80-120
Boron, Dissolved ug/L 12101250 97 80-120
Cadmium, Dissolved ug/L 26.225 105 80-120
Chromium, Dissolved ug/L 245250 98 80-120
Cobalt, Dissolved ug/L 250250 100 80-120
Copper, Dissolved ug/L 234250 93 80-120
Lead, Dissolved ug/L 254250 102 80-120
Manganese, Dissolved ug/L 244250 97 80-120
Nickel, Dissolved ug/L 256250 102 80-120
Selenium, Dissolved ug/L 252250 101 80-120
Silver, Dissolved ug/L 24.025 96 80-120
Thallium, Dissolved ug/L 251250 100 80-120
Vanadium, Dissolved ug/L 242250 97 80-120
Zinc, Dissolved ug/L 13001250 104 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5249507MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35830912003
5249508
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 250 90 75-12591 1 202505.5U 226 229
Arsenic, Dissolved ug/L 250 96 75-12597 0 202503.4U 240 241
Barium, Dissolved ug/L 250 96 75-12595 0 2025018.5 258 257
Beryllium, Dissolved ug/L 25 96 75-12597 1 20250.17U 24.1 24.3
Boron, Dissolved ug/L 1250 97 75-12598 1 20125037.2J 1250 1260
Cadmium, Dissolved ug/L 25 99 75-125100 1 20250.48J 25.3 25.6
Chromium, Dissolved ug/L 250 96 75-12597 1 202502.1J 242 244
Cobalt, Dissolved ug/L 250 98 75-12599 1 202500.96U 246 248
Copper, Dissolved ug/L 250 95 75-12596 1 202502.6U 239 241
Lead, Dissolved ug/L 250 99 75-125100 1 202504.3J 252 256
Manganese, Dissolved ug/L 250 95 75-12596 1 2025025.8 264 265
Nickel, Dissolved ug/L 250 99 75-125100 1 202501.0U 249 251
Selenium, Dissolved ug/L 250 86 75-12586 0 202503.9U 214 215
Silver, Dissolved ug/L 25 96 75-12597 1 20251.0U 24.9 25.3
Thallium, Dissolved ug/L 250 97 75-12598 1 202502.9U 244 246
Vanadium, Dissolved ug/L 250 96 75-12597 1 202502.1J 243 245
Zinc, Dissolved ug/L 1250 99 75-125100 1 20125011.0U 1240 1250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803103
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4159661
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/30/23 13:040.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/30/23 13:040.22
1,1,2-Trichloroethane ug/L ND 1.0 09/30/23 13:040.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/30/23 13:040.32
1,1-Dichloroethane ug/L ND 1.0 09/30/23 13:040.37
1,1-Dichloroethene ug/L ND 1.0 09/30/23 13:040.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/30/23 13:040.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/30/23 13:040.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/30/23 13:040.27
1,2-Dichlorobenzene ug/L ND 1.0 09/30/23 13:040.34
1,2-Dichloroethane ug/L ND 1.0 09/30/23 13:040.32
1,2-Dichloropropane ug/L ND 1.0 09/30/23 13:040.36
1,3-Dichlorobenzene ug/L ND 1.0 09/30/23 13:040.34
1,4-Dichlorobenzene ug/L ND 1.0 09/30/23 13:040.33
2-Butanone (MEK)ug/L ND 5.0 09/30/23 13:044.0
2-Hexanone ug/L ND 5.0 09/30/23 13:040.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/30/23 13:042.7
Acetone ug/L ND 25.0 09/30/23 13:045.1
Benzene ug/L ND 1.0 09/30/23 13:040.34
Bromodichloromethane ug/L ND 1.0 09/30/23 13:040.31
Bromoform ug/L ND 1.0 09/30/23 13:040.34
Bromomethane ug/L ND 2.0 v209/30/23 13:041.7
Carbon disulfide ug/L ND 2.0 09/30/23 13:040.36
Carbon tetrachloride ug/L ND 1.0 09/30/23 13:040.33
Chlorobenzene ug/L ND 1.0 09/30/23 13:040.28
Chloroethane ug/L ND 1.0 09/30/23 13:040.65
Chloroform ug/L ND 1.0 09/30/23 13:040.43
Chloromethane ug/L ND 1.0 09/30/23 13:040.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/30/23 13:040.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/30/23 13:040.36
Cyclohexane ug/L ND 1.0 09/30/23 13:040.35
Dibromochloromethane ug/L ND 1.0 09/30/23 13:040.36
Dichlorodifluoromethane ug/L ND 1.0 09/30/23 13:040.35
Ethylbenzene ug/L ND 1.0 09/30/23 13:040.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/30/23 13:040.33
m&p-Xylene ug/L ND 2.0 09/30/23 13:040.71
Methyl acetate ug/L ND 10.0 09/30/23 13:042.4
Methyl-tert-butyl ether ug/L ND 1.0 09/30/23 13:040.42
Methylcyclohexane ug/L ND 10.0 09/30/23 13:041.5
Methylene Chloride ug/L ND 5.0 09/30/23 13:042.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4159661
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/30/23 13:040.34
Styrene ug/L ND 1.0 09/30/23 13:040.29
Tetrachloroethene ug/L ND 1.0 09/30/23 13:040.29
Toluene ug/L ND 1.0 09/30/23 13:040.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/30/23 13:040.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/30/23 13:040.36
Trichloroethene ug/L ND 1.0 09/30/23 13:040.38
Trichlorofluoromethane ug/L ND 1.0 09/30/23 13:040.30
Vinyl chloride ug/L ND 1.0 09/30/23 13:040.39
1,2-Dichloroethane-d4 (S)%102 70-130 09/30/23 13:04
4-Bromofluorobenzene (S)%100 70-130 09/30/23 13:04
Toluene-d8 (S)%100 70-130 09/30/23 13:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4159662LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.020 100 70-130
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130
1,1,2-Trichloroethane ug/L 20.120 101 70-130
1,1,2-Trichlorotrifluoroethane ug/L 21.020 105 70-132
1,1-Dichloroethane ug/L 19.420 97 70-130
1,1-Dichloroethene ug/L 19.820 99 69-131
1,2,4-Trichlorobenzene ug/L 20.420 102 70-130
1,2-Dibromo-3-chloropropane ug/L 19.820 99 70-130
1,2-Dibromoethane (EDB)ug/L 19.820 99 70-130
1,2-Dichlorobenzene ug/L 20.220 101 70-130
1,2-Dichloroethane ug/L 20.020 100 70-130
1,2-Dichloropropane ug/L 20.120 100 70-130
1,3-Dichlorobenzene ug/L 19.820 99 70-130
1,4-Dichlorobenzene ug/L 19.920 100 70-130
2-Butanone (MEK)ug/L 39.040 97 67-133
2-Hexanone ug/L 40.540 101 70-133
4-Methyl-2-pentanone (MIBK)ug/L 40.740 102 70-130
Acetone ug/L 40.540 101 67-130
Benzene ug/L 19.920 99 70-130
Bromodichloromethane ug/L 20.420 102 70-130
Bromoform ug/L 19.920 100 70-133
Bromomethane ug/L 15.1 v32076 41-148
Carbon disulfide ug/L 20.720 104 70-131
Carbon tetrachloride ug/L 22.020 110 70-130
Chlorobenzene ug/L 20.020 100 70-130
Chloroethane ug/L 18.620 93 41-157
Chloroform ug/L 20.420 102 70-130
Chloromethane ug/L 18.620 93 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4159662LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 20.020 100 70-130
cis-1,3-Dichloropropene ug/L 20.320 102 70-130
Cyclohexane ug/L 20.320 101 63-137
Dibromochloromethane ug/L 19.020 95 70-130
Dichlorodifluoromethane ug/L 24.620 123 54-147
Ethylbenzene ug/L 19.820 99 70-130
Isopropylbenzene (Cumene)ug/L 20.420 102 70-130
m&p-Xylene ug/L 40.340 101 70-130
Methyl acetate ug/L 17.620 88 70-130
Methyl-tert-butyl ether ug/L 19.220 96 70-130
Methylcyclohexane ug/L 21.020 105 70-130
Methylene Chloride ug/L 19.720 99 62-130
o-Xylene ug/L 19.920 100 70-130
Styrene ug/L 20.320 101 70-130
Tetrachloroethene ug/L 20.020 100 70-130
Toluene ug/L 19.920 100 70-130
trans-1,2-Dichloroethene ug/L 20.020 100 70-130
trans-1,3-Dichloropropene ug/L 21.420 107 70-130
Trichloroethene ug/L 20.620 103 70-130
Trichlorofluoromethane ug/L 20.220 101 57-130
Vinyl chloride ug/L 17.220 86 66-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4159663MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689895009
4159664
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 112 70-150107 5 3020ND22.5 21.4
1,1,2,2-Tetrachloroethane ug/L 20 134 66-144120 11 3020ND26.7 24.0
1,1,2-Trichloroethane ug/L 20 118 70-142113 4 3020ND23.7 22.6
1,1,2-Trichlorotrifluoroethane ug/L 20 108 66-168105 3 3020ND21.7 21.0
1,1-Dichloroethane ug/L 20 110 68-150105 5 3020ND23.7 22.6
1,1-Dichloroethene ug/L 20 110 64-162105 4 30203.6 25.6 24.5
1,2,4-Trichlorobenzene ug/L 20 132 69-147123 7 3020ND26.4 24.6
1,2-Dibromo-3-chloropropane ug/L 20 127 62-146117 8 3020ND25.4 23.5
1,2-Dibromoethane (EDB) ug/L 20 136 70-143119 14 3020ND27.2 23.7
1,2-Dichlorobenzene ug/L 20 126 70-142123 3 3020ND25.3 24.6
1,2-Dichloroethane ug/L 20 119 68-145110 8 3020ND23.8 22.0
1,2-Dichloropropane ug/L 20 118 70-144112 5 3020ND23.5 22.5
1,3-Dichlorobenzene ug/L 20 124 70-142122 1 3020ND24.8 24.4
1,4-Dichlorobenzene ug/L 20 122 70-140119 2 3020ND24.4 23.8
2-Butanone (MEK)ug/L 40 115 57-156104 10 3040ND46.0 41.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4159663MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689895009
4159664
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 131 62-153118 11 3040ND52.6 47.3
4-Methyl-2-pentanone(MIBK)ug/L 40 119 65-144110 8 3040ND47.4 43.9
Acetone ug/L 40 123 49-162109 3040ND49.2J 43.8J
Benzene ug/L 20 114 68-144110 3 3020ND22.7 21.9
Bromodichloromethane ug/L 20 118 70-141114 4 3020ND23.6 22.7
Bromoform ug/L 20 134 59-144116 15 3020ND26.9 23.1
Bromomethane ug/L v3209323-19090 3 3020ND18.6 18.0
Carbon disulfide ug/L 20 107 64-160104 3 3020ND21.4 20.8
Carbon tetrachloride ug/L 20 116 70-147114 2 3020ND23.1 22.8
Chlorobenzene ug/L 20 127 70-143116 10 3020ND25.5 23.1
Chloroethane ug/L 20 107 55-19099 8 3020ND21.5 19.8
Chloroform ug/L 20 113 67-148111 1 3020ND22.6 22.3
Chloromethane ug/L 20 95 38-18092 4 3020ND19.1 18.4
cis-1,2-Dichloroethene ug/L 20 128 67-15185 4 3020200225 216
cis-1,3-Dichloropropene ug/L 20 117 70-142110 6 3020ND23.3 22.0
Cyclohexane ug/L 20 105 64-162101 4 3020ND21.0 20.3
Dibromochloromethane ug/L 20 124 68-140115 8 3020ND24.8 23.0
Dichlorodifluoromethane ug/L 20 121 15-200116 4 3020ND24.1 23.3
Ethylbenzene ug/L 20 127 70-145116 9 3020ND25.5 23.2
Isopropylbenzene(Cumene)ug/L 20 127 70-144118 8 3020ND25.5 23.6
m&p-Xylene ug/L 40 129 70-148118 8 3040ND51.5 47.4
Methyl acetate ug/L 20 107 62-14495 3020ND21.5 19.0J
Methyl-tert-butyl ether ug/L 20 111 64-146103 8 3020ND22.3 20.5
Methylcyclohexane ug/L 20 106 70-155111 5 3020ND21.2 22.2
Methylene Chloride ug/L 20 112 54-149106 5 3020ND22.3 21.3
o-Xylene ug/L 20 126 70-145113 11 3020ND25.2 22.6
Styrene ug/L 20 124 70-147116 6 3020ND24.8 23.2
Tetrachloroethene ug/L 20 121 70-145111 9 3020ND24.1 22.2
Toluene ug/L 20 116 65-146109 6 3020ND23.2 21.8
trans-1,2-Dichloroethene ug/L 20 113 69-155108 3 302015.9 38.4 37.4
trans-1,3-Dichloropropene ug/L 20 123 70-142117 5 3020ND24.7 23.4
Trichloroethene ug/L 20 118 70-152112 5 3020ND24.9 23.7
Trichlorofluoromethane ug/L 20 108 60-158105 3 3020ND21.5 21.0
Vinyl chloride ug/L 20 87 51-17886 1 3020ND17.3 17.2
1,2-Dichloroethane-d4 (S) %102 70-130102
4-Bromofluorobenzene (S) %102 70-13099
Toluene-d8 (S)%98 70-13098
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4160037MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689624005
4160038
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 117 70-150122 4 3020ND23.4 24.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4160037MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689624005
4160038
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,2,2-Tetrachloroethane ug/L 20 108 66-144111 3 3020ND21.6 22.2
1,1,2-Trichloroethane ug/L 20 112 70-142119 6 3020ND22.5 23.8
1,1,2-Trichlorotrifluoroethane ug/L 20 116 66-168121 4 3020ND23.3 24.1
1,1-Dichloroethane ug/L 20 111 68-150116 5 3020ND22.2 23.3
1,1-Dichloroethene ug/L 20 116 64-162123 6 3020ND23.2 24.6
1,2,4-Trichlorobenzene ug/L 20 117 69-147120 2 3020ND23.5 24.11,2-Dibromo-3-chloropropane ug/L 20 105 62-146109 4 3020ND20.9 21.9
1,2-Dibromoethane (EDB) ug/L 20 112 70-143115 2 3020ND22.4 23.0
1,2-Dichlorobenzene ug/L 20 109 70-142115 5 3020ND21.7 22.9
1,2-Dichloroethane ug/L 20 113 68-145115 2 3020ND22.5 23.0
1,2-Dichloropropane ug/L 20 112 70-144116 3 3020ND22.5 23.1
1,3-Dichlorobenzene ug/L 20 109 70-142113 4 3020ND21.8 22.7
1,4-Dichlorobenzene ug/L 20 106 70-140113 6 3020ND21.1 22.5
2-Butanone (MEK)ug/L 40 106 57-156108 2 3040ND42.2 43.2
2-Hexanone ug/L 40 112 62-153111 1 3040ND44.6 44.44-Methyl-2-pentanone(MIBK)ug/L 40 109 65-144110 1 3040ND43.7 44.1
Acetone ug/L 40 100 49-162103 3 3040ND40.0 41.1
Benzene ug/L 20 111 68-144116 4 3020ND22.3 23.2
Bromodichloromethane ug/L 20 114 70-141118 3 3020ND22.8 23.6
Bromoform ug/L 20 108 59-144113 4 3020ND21.7 22.6
Bromomethane ug/L v3207923-19092 14 3020ND15.8 18.3
Carbon disulfide ug/L 20 119 64-160124 4 3020ND23.8 24.8
Carbon tetrachloride ug/L 20 127 70-147130 2 3020ND25.4 25.9
Chlorobenzene ug/L 20 107 70-143112 5 3020ND21.4 22.4
Chloroethane ug/L 20 107 55-190112 5 3020ND21.4 22.5
Chloroform ug/L 20 113 67-148120 6 3020ND22.6 24.1
Chloromethane ug/L 20 103 38-180110 7 3020ND20.6 22.1
cis-1,2-Dichloroethene ug/L 20 110 67-151114 4 3020ND21.9 22.8
cis-1,3-Dichloropropene ug/L 20 111 70-142115 3 3020ND22.1 22.9
Cyclohexane ug/L 20 114 64-162121 6 3020ND22.8 24.1
Dibromochloromethane ug/L 20 111 68-140115 4 3020ND22.1 23.0
Dichlorodifluoromethane ug/L 20 139 15-200148 6 3020ND27.8 29.5
Ethylbenzene ug/L 20 108 70-145110 2 3020ND21.6 21.9Isopropylbenzene(Cumene)ug/L 20 114 70-144117 2 3020ND22.9 23.4
m&p-Xylene ug/L 40 110 70-148113 2 3040ND44.1 45.2
Methyl acetate ug/L 20 102 62-14496 5 3020ND20.4 19.3
Methyl-tert-butyl ether ug/L 20 101 64-146108 6 3020ND20.3 21.5
Methylcyclohexane ug/L 20 125 70-155123 1 3020ND25.0 24.7
Methylene Chloride ug/L 20 105 54-149110 4 3020ND21.0 21.9
o-Xylene ug/L 20 109 70-145111 2 3020ND21.8 22.2
Styrene ug/L 20 105 70-147112 6 3020ND21.1 22.5
Tetrachloroethene ug/L 20 113 70-145114 1 3020ND22.5 22.7
Toluene ug/L 20 110 65-146112 2 3020ND21.9 22.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4160037MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689624005
4160038
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
trans-1,2-Dichloroethene ug/L 20 113 69-155121 7 3020ND22.6 24.1
trans-1,3-Dichloropropene ug/L 20 115 70-142121 6 3020ND22.9 24.2
Trichloroethene ug/L 20 114 70-152122 8 3020ND22.7 24.5
Trichlorofluoromethane ug/L 20 116 60-158127 9 3020ND23.2 25.4
Vinyl chloride ug/L 20 98 51-178102 5 3020ND19.5 20.4
1,2-Dichloroethane-d4 (S) %103 70-130101
4-Bromofluorobenzene (S) %100 70-130102
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803106
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689056001, 92689056002, 92689056003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4159708
Associated Lab Samples:92689056001, 92689056002, 92689056003
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/30/23 01:150.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/30/23 01:150.22
1,1,2-Trichloroethane ug/L ND 1.0 09/30/23 01:150.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/30/23 01:150.32
1,1-Dichloroethane ug/L ND 1.0 09/30/23 01:150.37
1,1-Dichloroethene ug/L ND 1.0 v109/30/23 01:150.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/30/23 01:150.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/30/23 01:150.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/30/23 01:150.27
1,2-Dichlorobenzene ug/L ND 1.0 09/30/23 01:150.34
1,2-Dichloroethane ug/L ND 1.0 09/30/23 01:150.32
1,2-Dichloropropane ug/L ND 1.0 09/30/23 01:150.36
1,3-Dichlorobenzene ug/L ND 1.0 09/30/23 01:150.34
1,4-Dichlorobenzene ug/L ND 1.0 09/30/23 01:150.33
2-Butanone (MEK)ug/L ND 5.0 09/30/23 01:154.0
2-Hexanone ug/L ND 5.0 09/30/23 01:150.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/30/23 01:152.7
Acetone ug/L ND 25.0 09/30/23 01:155.1
Benzene ug/L ND 1.0 09/30/23 01:150.34
Bromodichloromethane ug/L ND 1.0 09/30/23 01:150.31
Bromoform ug/L ND 1.0 09/30/23 01:150.34
Bromomethane ug/L ND 2.0 v209/30/23 01:151.7
Carbon disulfide ug/L ND 2.0 09/30/23 01:150.36
Carbon tetrachloride ug/L ND 1.0 09/30/23 01:150.33
Chlorobenzene ug/L ND 1.0 09/30/23 01:150.28
Chloroethane ug/L ND 1.0 09/30/23 01:150.65
Chloroform ug/L ND 1.0 09/30/23 01:150.43
Chloromethane ug/L ND 1.0 09/30/23 01:150.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/30/23 01:150.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/30/23 01:150.36
Cyclohexane ug/L ND 1.0 09/30/23 01:150.35
Dibromochloromethane ug/L ND 1.0 09/30/23 01:150.36
Dichlorodifluoromethane ug/L ND 1.0 09/30/23 01:150.35
Ethylbenzene ug/L ND 1.0 09/30/23 01:150.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/30/23 01:150.33
m&p-Xylene ug/L ND 2.0 09/30/23 01:150.71
Methyl acetate ug/L ND 10.0 09/30/23 01:152.4
Methyl-tert-butyl ether ug/L ND 1.0 09/30/23 01:150.42
Methylcyclohexane ug/L ND 10.0 09/30/23 01:151.5
Methylene Chloride ug/L ND 5.0 v109/30/23 01:152.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4159708
Associated Lab Samples:92689056001, 92689056002, 92689056003
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/30/23 01:150.34
Styrene ug/L ND 1.0 09/30/23 01:150.29
Tetrachloroethene ug/L ND 1.0 09/30/23 01:150.29
Toluene ug/L ND 1.0 09/30/23 01:150.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/30/23 01:150.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/30/23 01:150.36
Trichloroethene ug/L ND 1.0 09/30/23 01:150.38
Trichlorofluoromethane ug/L ND 1.0 09/30/23 01:150.30
Vinyl chloride ug/L ND 1.0 09/30/23 01:150.39
1,2-Dichloroethane-d4 (S)%105 70-130 09/30/23 01:15
4-Bromofluorobenzene (S)%97 70-130 09/30/23 01:15
Toluene-d8 (S)%99 70-130 09/30/23 01:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4159709LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 22.020 110 70-130
1,1,2,2-Tetrachloroethane ug/L 22.420 112 70-130
1,1,2-Trichloroethane ug/L 21.320 107 70-130
1,1,2-Trichlorotrifluoroethane ug/L 21.920 110 70-132
1,1-Dichloroethane ug/L 23.320 116 70-130
1,1-Dichloroethene ug/L 25.1 v120126 69-131
1,2,4-Trichlorobenzene ug/L 18.620 93 70-130
1,2-Dibromo-3-chloropropane ug/L 18.920 95 70-130
1,2-Dibromoethane (EDB)ug/L 20.720 104 70-130
1,2-Dichlorobenzene ug/L 20.220 101 70-130
1,2-Dichloroethane ug/L 21.620 108 70-130
1,2-Dichloropropane ug/L 22.520 113 70-130
1,3-Dichlorobenzene ug/L 20.620 103 70-130
1,4-Dichlorobenzene ug/L 20.520 102 70-130
2-Butanone (MEK)ug/L 45.040 113 67-133
2-Hexanone ug/L 45.240 113 70-133
4-Methyl-2-pentanone (MIBK)ug/L 44.640 112 70-130
Acetone ug/L 47.240 118 67-130
Benzene ug/L 22.220 111 70-130
Bromodichloromethane ug/L 21.120 105 70-130
Bromoform ug/L 18.620 93 70-133
Bromomethane ug/L 18.4 v32092 41-148
Carbon disulfide ug/L 24.120 120 70-131
Carbon tetrachloride ug/L 21.720 109 70-130
Chlorobenzene ug/L 21.620 108 70-130
Chloroethane ug/L 20.120 101 41-157
Chloroform ug/L 21.420 107 70-130
Chloromethane ug/L 19.420 97 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4159709LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 23.020 115 70-130
cis-1,3-Dichloropropene ug/L 21.320 106 70-130
Cyclohexane ug/L 23.820 119 63-137
Dibromochloromethane ug/L 20.120 101 70-130
Dichlorodifluoromethane ug/L 22.820 114 54-147
Ethylbenzene ug/L 21.720 108 70-130
Isopropylbenzene (Cumene)ug/L 21.620 108 70-130
m&p-Xylene ug/L 42.740 107 70-130
Methyl acetate ug/L 21.120 105 70-130
Methyl-tert-butyl ether ug/L 20.320 102 70-130
Methylcyclohexane ug/L 24.720 123 70-130
Methylene Chloride ug/L 25.2 v120126 62-130
o-Xylene ug/L 20.620 103 70-130
Styrene ug/L 21.420 107 70-130
Tetrachloroethene ug/L 19.520 98 70-130
Toluene ug/L 21.420 107 70-130
trans-1,2-Dichloroethene ug/L 23.520 117 70-130
trans-1,3-Dichloropropene ug/L 20.420 102 70-130
Trichloroethene ug/L 21.120 106 70-130
Trichlorofluoromethane ug/L 20.120 101 57-130
Vinyl chloride ug/L 18.420 92 66-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4159711MATRIX SPIKE SAMPLE:
MSSpike
Result
92689056002
1,1,1-Trichloroethane ug/L 23.520 117 70-150ND
1,1,2,2-Tetrachloroethane ug/L 24.320 121 66-144ND
1,1,2-Trichloroethane ug/L 24.020 120 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 24.420 122 66-168ND
1,1-Dichloroethane ug/L 22.420 112 68-150ND
1,1-Dichloroethene ug/L 23.220 116 64-162ND
1,2,4-Trichlorobenzene ug/L 23.720 118 69-147ND
1,2-Dibromo-3-chloropropane ug/L 23.320 116 62-146ND
1,2-Dibromoethane (EDB)ug/L 24.720 124 70-143ND
1,2-Dichlorobenzene ug/L 24.120 121 70-142ND
1,2-Dichloroethane ug/L 23.220 116 68-145ND
1,2-Dichloropropane ug/L 23.520 117 70-144ND
1,3-Dichlorobenzene ug/L 24.120 120 70-142ND
1,4-Dichlorobenzene ug/L 23.920 119 70-140ND
2-Butanone (MEK)ug/L 49.940 125 57-156ND
2-Hexanone ug/L 46.840 117 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 46.740 117 65-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4159711MATRIX SPIKE SAMPLE:
MSSpike
Result
92689056002
Acetone ug/L 41.640 104 49-162ND
Benzene ug/L 26.220 117 68-1442.7
Bromodichloromethane ug/L 22.820 114 70-141ND
Bromoform ug/L 23.020 115 59-144ND
Bromomethane ug/L 19.920 99 23-190ND
Carbon disulfide ug/L 23.820 119 64-160ND
Carbon tetrachloride ug/L 23.720 119 70-147ND
Chlorobenzene ug/L 24.120 121 70-143ND
Chloroethane ug/L 22.720 114 55-190ND
Chloroform ug/L 22.820 114 67-148ND
Chloromethane ug/L 20.920 102 38-180ND
cis-1,2-Dichloroethene ug/L 22.520 112 67-151ND
cis-1,3-Dichloropropene ug/L 23.020 115 70-142ND
Cyclohexane ug/L 23.020 111 64-1620.76J
Dibromochloromethane ug/L 23.920 119 68-140ND
Dichlorodifluoromethane ug/L 24.820 124 15-200ND
Ethylbenzene ug/L 23.920 119 70-145ND
Isopropylbenzene (Cumene)ug/L 24.320 121 70-144ND
m&p-Xylene ug/L 48.140 119 70-1480.71J
Methyl acetate ug/L 20.120 100 62-144ND
Methyl-tert-butyl ether ug/L 21.220 106 64-146ND
Methylcyclohexane ug/L 25.120 126 70-155ND
Methylene Chloride ug/L 22.020 110 54-149ND
o-Xylene ug/L 24.020 118 70-1450.40J
Styrene ug/L 23.820 119 70-147ND
Tetrachloroethene ug/L 24.020 120 70-145ND
Toluene ug/L 23.020 115 65-146ND
trans-1,2-Dichloroethene ug/L 20.720 103 69-155ND
trans-1,3-Dichloropropene ug/L 22.720 114 70-142ND
Trichloroethene ug/L 24.920 124 70-152ND
Trichlorofluoromethane ug/L 23.320 116 60-158ND
Vinyl chloride ug/L 19.820 99 51-178ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689056001
4159710SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689056001
4159710SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%95106
4-Bromofluorobenzene (S)%9697
Toluene-d8 (S)%10398
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801644
EPA 3511
EPA 8015C
8015 Diesel Low Volume
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152693
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/L ND 0.50 09/25/23 12:000.15
n-Pentacosane (S)%63 29-158 09/25/23 12:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152694LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/L 11.110 111 61-130
n-Pentacosane (S)%109 29-158
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4152695MATRIX SPIKE SAMPLE:
MSSpike
Result
92689587001
Diesel Range Organics(C10-C28)mg/L 10.710 107 29-134ND
n-Pentacosane (S)%101 29-158
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689587002
4152696SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/L ND 30ND
n-Pentacosane (S)%9698
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801703
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689056001, 92689056002, 92689056003, 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152817
Associated Lab Samples:92689056001, 92689056002, 92689056003, 92689056004
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/25/23 16:291.2
2,4,5-Trichlorophenol ug/L ND 10.0 09/25/23 16:291.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/25/23 16:291.6
2,4-Dichlorophenol ug/L ND 10.0 09/25/23 16:291.4
2,4-Dimethylphenol ug/L ND 10.0 09/25/23 16:291.7
2,4-Dinitrophenol ug/L ND 50.0 09/25/23 16:2926.0
2,4-Dinitrotoluene ug/L ND 10.0 09/25/23 16:291.6
2,6-Dinitrotoluene ug/L ND 10.0 09/25/23 16:291.7
2-Chloronaphthalene ug/L ND 10.0 09/25/23 16:291.7
2-Chlorophenol ug/L ND 10.0 09/25/23 16:291.2
2-Methylnaphthalene ug/L ND 10.0 09/25/23 16:291.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/25/23 16:291.9
2-Nitroaniline ug/L ND 20.0 09/25/23 16:293.0
2-Nitrophenol ug/L ND 10.0 09/25/23 16:291.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/25/23 16:291.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/25/23 16:298.1
3-Nitroaniline ug/L ND 20.0 09/25/23 16:293.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/25/23 16:297.8
4-Bromophenylphenyl ether ug/L ND 10.0 09/25/23 16:291.8
4-Chloro-3-methylphenol ug/L ND 10.0 09/25/23 16:293.3
4-Chloroaniline ug/L ND 20.0 09/25/23 16:293.6
4-Chlorophenylphenyl ether ug/L ND 10.0 09/25/23 16:292.0
4-Nitroaniline ug/L ND 20.0 09/25/23 16:295.1
4-Nitrophenol ug/L ND 50.0 09/25/23 16:296.6
Acenaphthene ug/L ND 10.0 09/25/23 16:292.0
Acenaphthylene ug/L ND 10.0 09/25/23 16:292.0
Acetophenone ug/L ND 10.0 09/25/23 16:291.5
Anthracene ug/L ND 10.0 09/25/23 16:292.3
Atrazine ug/L ND 10.0 09/25/23 16:293.2
Benzaldehyde ug/L ND 10.0 09/25/23 16:293.6
Benzo(a)anthracene ug/L ND 10.0 09/25/23 16:292.7
Benzo(a)pyrene ug/L ND 10.0 09/25/23 16:292.8
Benzo(b)fluoranthene ug/L ND 10.0 09/25/23 16:292.6
Benzo(g,h,i)perylene ug/L ND 10.0 09/25/23 16:292.8
Benzo(k)fluoranthene ug/L ND 10.0 09/25/23 16:292.7
Biphenyl (Diphenyl)ug/L ND 10.0 09/25/23 16:291.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/25/23 16:291.8
bis(2-Chloroethyl) ether ug/L ND 10.0 09/25/23 16:291.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/25/23 16:293.7
Butylbenzylphthalate ug/L ND 10.0 09/25/23 16:293.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152817
Associated Lab Samples:92689056001, 92689056002, 92689056003, 92689056004
Matrix: Water
AnalyzedMDL
Caprolactam ug/L ND 10.0 09/25/23 16:296.9
Carbazole ug/L ND 10.0 09/25/23 16:292.4
Chrysene ug/L ND 10.0 09/25/23 16:292.8
Di-n-butylphthalate ug/L ND 10.0 09/25/23 16:292.2
Di-n-octylphthalate ug/L ND 10.0 09/25/23 16:293.9
Dibenz(a,h)anthracene ug/L ND 10.0 09/25/23 16:293.0
Dibenzofuran ug/L ND 10.0 09/25/23 16:292.1
Diethylphthalate ug/L ND 10.0 09/25/23 16:292.0
Dimethylphthalate ug/L ND 10.0 09/25/23 16:292.1
Fluoranthene ug/L ND 10.0 09/25/23 16:292.2
Fluorene ug/L ND 10.0 09/25/23 16:292.1
Hexachloro-1,3-butadiene ug/L ND 10.0 09/25/23 16:291.8
Hexachlorobenzene ug/L ND 10.0 09/25/23 16:292.2
Hexachlorocyclopentadiene ug/L ND 10.0 09/25/23 16:291.6
Hexachloroethane ug/L ND 10.0 09/25/23 16:291.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/25/23 16:292.9
Isophorone ug/L ND 10.0 09/25/23 16:291.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/25/23 16:291.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/25/23 16:293.0
Naphthalene ug/L ND 10.0 09/25/23 16:292.1
Nitrobenzene ug/L ND 10.0 09/25/23 16:291.9
Pentachlorophenol ug/L ND 20.0 09/25/23 16:293.8
Phenanthrene ug/L ND 10.0 09/25/23 16:292.0
Phenol ug/L ND 10.0 09/25/23 16:291.4
Pyrene ug/L ND 10.0 09/25/23 16:292.2
2,4,6-Tribromophenol (S)%118 10-164 09/25/23 16:29
2-Fluorobiphenyl (S)%97 10-130 09/25/23 16:29
2-Fluorophenol (S)%66 10-130 09/25/23 16:29
Nitrobenzene-d5 (S)%108 10-138 09/25/23 16:29
Phenol-d6 (S)%56 10-130 09/25/23 16:29
Terphenyl-d14 (S)%141 19-191 09/25/23 16:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152818LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 18.650 37 21-135
2,4,5-Trichlorophenol ug/L 34.950 70 38-147
2,4,6-Trichlorophenol ug/L 24.450 49 34-142
2,4-Dichlorophenol ug/L 21.650 43 36-136
2,4-Dimethylphenol ug/L 21.250 42 38-134
2,4-Dinitrophenol ug/L 152250 61 10-169
2,4-Dinitrotoluene ug/L 35.150 70 44-154
2,6-Dinitrotoluene ug/L 29.950 60 44-156
2-Chloronaphthalene ug/L 20.250 40 25-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152818LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 22.650 45 29-130
2-Methylnaphthalene ug/L 18.450 37 23-130
2-Methylphenol(o-Cresol)ug/L 20.150 40 31-130
2-Nitroaniline ug/L 56.4100 56 39-145
2-Nitrophenol ug/L 21.850 44 29-142
3&4-Methylphenol(m&p Cresol)ug/L 19.950 40 30-130
3,3'-Dichlorobenzidine ug/L 89.0100 89 44-158
3-Nitroaniline ug/L 73.0100 73 45-152
4,6-Dinitro-2-methylphenol ug/L 69.7100 70 39-158
4-Bromophenylphenyl ether ug/L 29.550 59 47-147
4-Chloro-3-methylphenol ug/L 44.0100 44 40-138
4-Chloroaniline ug/L 41.8100 42 35-130
4-Chlorophenylphenyl ether ug/L 25.850 52 36-139
4-Nitroaniline ug/L 87.5100 87 46-157
4-Nitrophenol ug/L 113250 45 17-130
Acenaphthene ug/L 22.550 45 34-135
Acenaphthylene ug/L 21.950 44 35-137
Acetophenone ug/L 21.550 43 30-137
Anthracene ug/L 33.750 67 47-146
Atrazine ug/L 34.850 70 30-130
Benzaldehyde ug/L 23.850 48 17-167
Benzo(a)anthracene ug/L 40.350 81 48-160
Benzo(a)pyrene ug/L 42.050 84 47-165
Benzo(b)fluoranthene ug/L 47.550 95 49-171
Benzo(g,h,i)perylene ug/L 42.950 86 46-166
Benzo(k)fluoranthene ug/L 43.250 86 55-162
Biphenyl (Diphenyl)ug/L 20.250 40 28-130
bis(2-Chloroethoxy)methane ug/L 20.150 40 33-136
bis(2-Chloroethyl) ether ug/L 22.550 45 30-142
bis(2-Ethylhexyl)phthalate ug/L 41.450 83 46-173
Butylbenzylphthalate ug/L 40.150 80 53-169
Caprolactam ug/L 21.350 43 13-130
Carbazole ug/L 39.850 80 48-157
Chrysene ug/L 39.450 79 54-152
Di-n-butylphthalate ug/L 38.050 76 49-161
Di-n-octylphthalate ug/L 40.450 81 50-166
Dibenz(a,h)anthracene ug/L 41.750 83 46-166
Dibenzofuran ug/L 23.250 46 37-136
Diethylphthalate ug/L 34.050 68 45-149
Dimethylphthalate ug/L 29.250 58 43-145
Fluoranthene ug/L 39.350 79 50-153
Fluorene ug/L 25.550 51 42-142
Hexachloro-1,3-butadiene ug/L 10.350 21 10-130
Hexachlorobenzene ug/L 29.750 59 44-138
Hexachlorocyclopentadiene ug/L 15.550 31 10-130
Hexachloroethane ug/L 6.8J50 14 10-130
Indeno(1,2,3-cd)pyrene ug/L 40.950 82 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152818LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 19.950 40 36-135
N-Nitroso-di-n-propylamine ug/L 23.250 46 33-140
N-Nitrosodiphenylamine ug/L 30.950 62 46-144
Naphthalene ug/L 15.350 31 20-130
Nitrobenzene ug/L 20.050 40 33-133
Pentachlorophenol ug/L 69.5100 70 21-163
Phenanthrene ug/L 33.950 68 47-146
Phenol ug/L 13.350 27 19-130
Pyrene ug/L 38.050 76 53-155
2,4,6-Tribromophenol (S)%68 10-164
2-Fluorobiphenyl (S)%37 10-130
2-Fluorophenol (S)%29 10-130
Nitrobenzene-d5 (S)%36 10-138
Phenol-d6 (S)%24 10-130
Terphenyl-d14 (S)%67 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4152820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-chloropropane)ug/L 83.3 58 11-14352 11 3083.3ND 48.4 43.5
2,4,5-Trichlorophenol ug/L 83.3 83 10-17080 4 3083.3ND 69.3 66.9
2,4,6-Trichlorophenol ug/L 83.3 60 10-16668 12 3083.3ND 50.4 56.7
2,4-Dichlorophenol ug/L 83.3 74 10-15368 8 3083.3ND 61.7 56.9
2,4-Dimethylphenol ug/L 83.3 77 20-14765 17 3083.3ND 64.6 54.4
2,4-Dinitrophenol ug/L M1417010-17265 30417NDND 269
2,4-Dinitrotoluene ug/L 83.3 89 30-16476 16 3083.3ND 73.9 63.1
2,6-Dinitrotoluene ug/L 83.3 85 31-16373 15 3083.3ND 70.5 60.8
2-Chloronaphthalene ug/L 83.3 60 15-13449 20 3083.3ND 50.4 41.0
2-Chlorophenol ug/L 83.3 74 10-13962 17 3083.3ND 61.7 52.0
2-Methylnaphthalene ug/L 83.3 55 12-13057 2 3083.3ND 46.1 47.2
2-Methylphenol(o-Cresol) ug/L 83.3 67 19-13256 17 3083.3ND 55.5 46.9
2-Nitroaniline ug/L 167 78 23-15473 7 30167ND131 121
2-Nitrophenol ug/L 83.3 82 10-15967 20 3083.3ND 68.4 56.03&4-Methylphenol(m&pCresol)ug/L 83.3 64 13-13654 17 3083.3ND 53.6 45.4
3,3'-Dichlorobenzidine ug/L R116711210-17881 32 30167ND187 135
3-Nitroaniline ug/L 167 55 20-16645 20 30167ND92.2 75.1
4,6-Dinitro-2-methylphenol ug/L R11673210-18769 73 30167ND53.9 116
4-Bromophenylphenyl ether ug/L 83.3 81 31-15763 25 3083.3ND 67.3 52.6
4-Chloro-3-methylphenol ug/L 167 74 27-14666 10 30167ND123 111
4-Chloroaniline ug/L M11671313-1439 30167ND22.4J 15.4J
4-Chlorophenylphenyl ether ug/L 83.3 75 23-14959 24 3083.3ND 62.2 49.1
4-Nitroaniline ug/L 167 99 24-17178 24 30167ND166 130
4-Nitrophenol ug/L 417 18 10-13047 30417ND76.1J 195
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4152820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L 83.3 69 21-14754 24 3083.3ND 57.2 44.9
Acenaphthylene ug/L 83.3 68 19-15054 23 3083.3ND 56.9 45.2
Acetophenone ug/L 83.3 73 22-14562 17 3083.3ND 61.1 51.3
Anthracene ug/L 83.3 88 36-15267 27 3083.3ND 73.6 55.9
Atrazine ug/L 83.3 92 18-17388 4 3083.3ND 76.4 73.1
Benzaldehyde ug/L 83.3 75 16-16374 1 3083.3ND 62.2 61.4
Benzo(a)anthracene ug/L R183.3 105 42-16376 32 3083.3ND 87.5 63.4
Benzo(a)pyrene ug/L 83.3 108 40-16980 30 3083.3ND 90.1 66.7
Benzo(b)fluoranthene ug/L 83.3 119 40-17787 30 3083.3ND 98.9 72.7
Benzo(g,h,i)perylene ug/L 83.3 105 38-17482 25 3083.3ND 87.2 68.1
Benzo(k)fluoranthene ug/L R183.3 115 41-17180 36 3083.3ND 96.2 66.7
Biphenyl (Diphenyl)ug/L 83.3 62 14-13750 22 3083.3ND 51.7 41.5
bis(2-Chloroethoxy)methane ug/L 83.3 71 19-14661 16 3083.3ND 59.2 50.5
bis(2-Chloroethyl) ether ug/L 83.3 64 19-15155 14 3083.3ND 53.1 46.0
bis(2-Ethylhexyl)phthalate ug/L 83.3 113 42-16886 27 3083.3ND 94.5 71.9
Butylbenzylphthalate ug/L 83.3 109 42-17782 29 3083.3ND 91.0 68.1
Caprolactam ug/L 83.3 36 10-13032 11 3083.3ND 29.7 26.7
Carbazole ug/L 83.3 105 38-16479 28 3083.3ND 87.2 65.4
Chrysene ug/L 83.3 102 43-15976 30 3083.3ND 85.0 63.0
Di-n-butylphthalate ug/L 83.3 103 42-16077 29 3083.3ND 85.8 64.2
Di-n-octylphthalate ug/L 83.3 114 42-17192 22 3083.3ND 95.3 76.7
Dibenz(a,h)anthracene ug/L 83.3 105 40-17179 28 3083.3ND 87.1 66.1
Dibenzofuran ug/L 83.3 67 23-14753 23 3083.3ND 55.9 44.2
Diethylphthalate ug/L 83.3 88 33-15773 18 3083.3ND 73.1 60.9
Dimethylphthalate ug/L 83.3 77 27-15467 14 3083.3ND 64.0 55.9
Fluoranthene ug/L 83.3 103 42-15776 30 3083.3ND 85.7 63.6
Fluorene ug/L 83.3 73 25-15559 20 3083.3ND 60.5 49.3
Hexachloro-1,3-butadiene ug/L R183.3 22 10-13042 62 3083.3ND 18.7 35.4
Hexachlorobenzene ug/L 83.3 82 32-14566 21 3083.3ND 68.5 55.3
Hexachlorocyclopentadiene ug/L 83.3 42 10-13046 9 3083.3ND 35.3 38.7
Hexachloroethane ug/L 83.3 17 10-13034 3083.3ND 13.9J 28.6
Indeno(1,2,3-cd)pyrene ug/L 83.3 101 39-17477 27 3083.3ND 84.1 64.2
Isophorone ug/L 83.3 75 19-14662 18 3083.3ND 62.1 52.0
N-Nitroso-di-n-propylamine ug/L 83.3 78 20-15069 12 3083.3ND 64.6 57.2
N-Nitrosodiphenylamine ug/L 83.3 83 33-14966 23 3083.3ND 69.3 54.8
Naphthalene ug/L 83.3 44 10-12853 19 3083.3ND 36.4 44.1
Nitrobenzene ug/L 83.3 70 19-14557 21 3083.3ND 58.4 47.3
Pentachlorophenol ug/L 167 52 10-18865 22 30167ND87.3 109
Phenanthrene ug/L 83.3 87 38-15065 29 3083.3ND 72.7 54.6
Phenol ug/L 83.3 45 10-13035 26 3083.3ND 37.9 29.1
Pyrene ug/L 83.3 98 42-16374 29 3083.3ND 81.9 61.3
2,4,6-Tribromophenol (S) %82 10-16474
2-Fluorobiphenyl (S)%60 10-13051
2-Fluorophenol (S)%46 10-13044
Nitrobenzene-d5 (S)%64 10-13860
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4152820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%43 10-13035
Terphenyl-d14 (S)%85 19-19168
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802381
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056001, 92689056002, 92689056003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4156302
Associated Lab Samples:92689056001, 92689056002, 92689056003
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/27/23 20:075.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4156303LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 46.550 93 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4156304LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 47.450 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4156305MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688280010
4156306
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 116 80-120101 5 2550108165 158
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803715
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4162457
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 10/03/23 13:415.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4162458LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 50.650 101 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4162459LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.950 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4162460MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265009
4162461
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 102 80-120102 1 255010.9 62.1 61.7
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4162462MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4162463
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 103 80-120103 0 255010.1 61.5 61.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800967
SM 2540C-2015
SM 2540C-2015
2540C Total Dissolved Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4148910
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Total Dissolved Solids mg/L ND 25.0 09/20/23 21:0225.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4148911LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 256250 102 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688804001
4148912SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 20400 2 2519900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800968
SM 2540D-2015
SM 2540D-2015
2540D Total Suspended Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4148913
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Total Suspended Solids mg/L ND 2.5 09/20/23 20:332.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4148914LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 244250 97 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688854001
4148915SAMPLE DUPLICATE:
Total Suspended Solids mg/L 424 11 25380
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688887001
4148928SAMPLE DUPLICATE:
Total Suspended Solids mg/L 2910 0 252910
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801294
SM 4500-S2D-2011
SM 4500-S2D-2011
4500S2D Sulfide Water
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056001, 92689056002, 92689056003, 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150742
Associated Lab Samples:92689056001, 92689056002, 92689056003, 92689056004
Matrix: Water
AnalyzedMDL
Sulfide mg/L ND 0.10 09/22/23 07:560.022
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150743LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide mg/L 0.520.5 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150744MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689296025
4150745
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L R10.5 96 80-120109 13 100.5ND 0.48 0.54
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150746MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689296001
4150747
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 97 80-120104 7 100.5ND 0.49 0.52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800976
SM 5210B-2016
SM 5210B-2016
5210B BOD, 5 day
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4148937
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
BOD, 5 day mg/L ND 2.0 09/26/23 04:212.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4148939LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day mg/L 191198 96 84.6-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92688701002
4148940SAMPLE DUPLICATE:
BOD, 5 day mg/L 12.5 7 2511.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804463
EPA 9040C
EPA 9040C
9040 pH
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92690915003
4166183SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 8.0 H30108.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92690915004
4166184SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 7.8 H30107.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804042
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4164105
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Nitrogen, Kjeldahl, Total mg/L ND 0.50 10/06/23 04:010.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4164106LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 10.210 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4164107MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689775001
4164108
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 96 90-11094 1 101013.1 22.7 22.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4164109MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689775002
4164110
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 97 90-11097 1 10105.9 15.6 15.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800981
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres.
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4148955
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Nitrogen, Nitrate mg/L ND 0.040 09/21/23 00:530.010
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4148956LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 1.51.5 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4148957MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689016008
4148958
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 101 90-110102 1 101.5ND 1.5 1.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4148959MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689036004
4148960
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 77 90-11076 0 101.5ND 1.1 1.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804240
SM 5220D-2011
SM 5220D-2011
5220D COD
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4165189
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Chemical Oxygen Demand mg/L ND 25.0 10/06/23 00:1612.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4165190LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand mg/L 779750 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4165191MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4165192
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L 100 100 90-110102 2 3100ND106 108
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4165193MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690267001
4165194
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L M110011490-110112 2 310039.3 153 151
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803834
SM 5310B-2014
SM 5310B-2014
5310B TOC
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4163063
Associated Lab Samples:92689056004
Matrix: Water
AnalyzedMDL
Total Organic Carbon mg/L ND 1.0 10/03/23 16:500.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4163064LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon mg/L 24.525 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4163065MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689241001
4163066
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon mg/L 25 97 90-11097 0 102526600ug/L 50.9 50.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4163067MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690723004
4163068
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon mg/L P4259390-11094 1 10256.0 29.3 29.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 101
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801019
EPA 9056A
EPA 9056A
9056 IC anions 28 Days
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689056001, 92689056002, 92689056003, 92689056004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4149063
Associated Lab Samples:92689056001, 92689056002, 92689056003, 92689056004
Matrix: Water
AnalyzedMDL
Chloride mg/L ND 1.0 09/21/23 18:560.60
Sulfate mg/L ND 1.0 09/21/23 18:560.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4149064LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 51.150 102 90-110
Sulfate mg/L 51.350 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4149065MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689056001
4149066
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L 50 90 90-11091 1 105093.2 138 139
Sulfate mg/L 50 91 90-11093 1 1050100146 147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 101
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculatedfor the dilution using the most amount of sample.B2
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The sample was analyzed at a dilution due to foaming of the sample in the purge vessel.F1
Analysis conducted outside the EPA method holding time.H1
Sample was received or analysis requested beyond the recognized method holding time.H3
Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).HS
The internal standard response is below criteria. Results may be biased high.IS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.P3
Sample field preservation does not meet EPA or method recommendations for this analysis.P4
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from samplere-analysis).S2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 101
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
ANALYTE QUALIFIERS
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in theassociated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 101
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92689056001 801021PZ21WG-091923 SM 2120B-2011
92689056002 801021RW01WG-091923 SM 2120B-2011
92689056003 801021PZ20WG-091923 SM 2120B-2011
92689056004 804855PZ04WG-091923 EPA 1664B
92689056004 801644 801722PZ04WG-091923 EPA 3511 EPA 8015C
92689056004 2142504 2142504PZ04WG-091923 RSK175 RSK-175
92689056004 801614PZ04WG-091923 EPA 5030B/8015C
92689056001 954997 955101PZ21WG-091923 EPA 3010 EPA 6010
92689056002 954997 955101RW01WG-091923 EPA 3010 EPA 6010
92689056003 954997 955101PZ20WG-091923 EPA 3010 EPA 6010
92689056004 954997 955101PZ04WG-091923 EPA 3010 EPA 6010
92689056001 954621 954719PZ21WG-091923 EPA 3010 EPA 6010
92689056002 954621 954719RW01WG-091923 EPA 3010 EPA 6010
92689056003 954621 954719PZ20WG-091923 EPA 3010 EPA 6010
92689056004 954621 954719PZ04WG-091923 EPA 3010 EPA 6010
92689056001 955304 955582PZ21WG-091923 EPA 7470 EPA 7470
92689056002 955304 955582RW01WG-091923 EPA 7470 EPA 7470
92689056003 955304 955582PZ20WG-091923 EPA 7470 EPA 7470
92689056004 955304 955582PZ04WG-091923 EPA 7470 EPA 7470
92689056001 955306 955584PZ21WG-091923 EPA 7470 EPA 7470
92689056002 955306 955584RW01WG-091923 EPA 7470 EPA 7470
92689056003 955306 955584PZ20WG-091923 EPA 7470 EPA 7470
92689056004 955306 955584PZ04WG-091923 EPA 7470 EPA 7470
92689056001 801703 801890PZ21WG-091923 EPA 3510C EPA 8270E
92689056002 801703 801890RW01WG-091923 EPA 3510C EPA 8270E
92689056003 801703 801890PZ20WG-091923 EPA 3510C EPA 8270E
92689056004 801703 801890PZ04WG-091923 EPA 3510C EPA 8270E
92689056001 803106PZ21WG-091923 EPA 8260D
92689056002 803106RW01WG-091923 EPA 8260D
92689056003 803106PZ20WG-091923 EPA 8260D
92689056004 803103PZ04WG-091923 EPA 8260D
92689056001 802381PZ21WG-091923 SM 2320B-2011
92689056002 802381RW01WG-091923 SM 2320B-2011
92689056003 802381PZ20WG-091923 SM 2320B-2011
92689056004 803715PZ04WG-091923 SM 2320B-2011
92689056004 800967PZ04WG-091923 SM 2540C-2015
92689056004 800968PZ04WG-091923 SM 2540D-2015
92689056001 801294PZ21WG-091923 SM 4500-S2D-2011
92689056002 801294RW01WG-091923 SM 4500-S2D-2011
92689056003 801294PZ20WG-091923 SM 4500-S2D-2011
92689056004 801294PZ04WG-091923 SM 4500-S2D-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 101
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92689056
Pactiv Evergreen GWS (09/19)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92689056004 800976 801008PZ04WG-091923 SM 5210B-2016 SM 5210B-2016
92689056004 804463PZ04WG-091923 EPA 9040C
92689056004 804042 804549PZ04WG-091923 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689056004 800981PZ04WG-091923 EPA 353.2 Rev 2.0 1993
92689056004 804240 804541PZ04WG-091923 SM 5220D-2011 SM 5220D-2011
92689056004 803834PZ04WG-091923 SM 5310B-2014
92689056001 801019PZ21WG-091923 EPA 9056A
92689056002 801019RW01WG-091923 EPA 9056A
92689056003 801019PZ20WG-091923 EPA 9056A
92689056004 801019PZ04WG-091923 EPA 9056A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2023 08:27 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 101
Page 72 of 101
Page 73 of 101
Page 74 of 101
Page 75 of 101
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Thisreportshouldnotbereproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamplesincludedinthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,LLC.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
Matthew Brainard
PACE Charlotte
9800 Kincey Ave.
Huntersville NC 28078
REPORT OF
LABORATORY
ANALYSIS FOR
PCDD/PCDF
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
November 1, 2023
Pace Project #: 10670647
Sample Receipt Date: 09/29/2023
Client Project #: 92689056
Client Sub PO #: N/A
The report provided has been invoiced as a Level 2
PCDD/PCDF Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questionstoIsaac Johnson,your Pace
Project Manager.
State Cert #: 530
Suite 100
Report Prepared for:
Page 1 of 23Report No.....10670647_SW8290AFC_L2_dfr
November 01, 2023
Isaac Johnson, Project Manager
[phone]
[phone] (fax)
[e-mail]
Page 79 of 101
Pace Analytical Services,LLC.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
This report presents the results from the analyses performed on four samples submitted by a
representative of Pace Analytical Services, LLC. The samples were analyzed for the presence or absence
of polychlorodibenzo-p-dioxins (PCDDs) and polychlorodibenzofurans (PCDFs) using a modified version
of USEPA Method 8290A. The estimated detection limits (EDLs) were based on signal-to-noise
measurements. Estimated maximum possible concentration (EMPC) values were treated as positives inthe toxic equivalence calculations. Also, sample "PZ04WG-091923" was extracted outside of the 30-dayhold time recommended in the method, therefore, the reported values should be regarded as minimumpossible concentrations.
The isotopically-labeled PCDD/PCDF internal standards in the sample extracts were recovered at30-79%. Except for five low values, which were flagged "R" on the results tables, the labeled internalstandard recoveries obtained for this project were within the 40-135% target range specified in Method8290A. Since the quantification of the native 2,3,7,8-substituted congeners was based on isotope dilution,the data were automatically corrected for recovery and accurate values were obtained. Due to thecomplexity of the matrix, a reduced sample volume was extracted for sample PZ04WG-091923.
Values were flagged "I" where incorrect isotope ratios were obtained. Concentrations below the calibration
range were flagged "J" and should be regarded as estimates.
A laboratory method blank was prepared and analyzed with each sample batch as part of our routine
quality control procedures. The results show the blanks to contain trace levels of one or more selected
congeners. These levels were below the calibration range of the method. Sample concentrations similar
to the corresponding blank levels were flagged "B" on the results tables and may be, at least partially,
attributed to the background.
Laboratory spike samples were also prepared using clean reference matrix that had been fortified withnative standard materials. The results show that the spiked native compounds were recovered at79-110% with relative percent differences of 0.0-12.6%. These results were within the target ranges forthe method. Matrix spikes were not prepared with the extraction batch.
The response obtained for the labeled OCDD in calibration standard analysis L231026B_22 was outsidethe target range. As specified in our procedures for this method, the average of the daily response factorsfor this compound was used in the calculations for the samples from this runshift. The affected valueswere flagged "Y" on the results tables.
DISCUSSION
Page 2 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 80 of 101
REPORT OF LABORATORY ANALYSIS
This report shallnot bereproduced,except in full,
withoutthe written consentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Report No.....10673016
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 23Report No.....10670647_SW8290AFC_L2_dfr
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Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 4 of 23Report No.....10670647_SW8290AFC_L2_dfr
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Page 9 of 23Report No.....10670647_SW8290AFC_L2_dfr
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Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
A =
B = C = D = E = H2 =
I =
J = L = Nn = P = R =
S =
U = V = X = Y = * =
Reporting Limit based on signal to noise (EDL)
Less than 10x higher than method blank level Result obtained from confirmation analysis Result obtained from analysis of diluted sample Exceeds calibration range Extracted outside of holding time
Isotope ratio out of specification
Estimated value Suppressive interference, analyte may be biased low Value obtained from additional analysis PCDE Interference Recovery outside target range
Peak saturated
Analyte not detected Result verified by confirmation analysis %D Exceeds limits Calculated using average of daily RFs See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 10 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 88 of 101
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 11 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 89 of 101
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ21WG-09192392689056001U231031B_07JF
NA957 mL
NAU230926U231031B_01 & U231031B_18BLANK-108777
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/19/2023 09:2509/29/2023 08:5010/11/2023 10:3010/31/2023 19:37
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 1.2 2,3,7,8-TCDF-13C 2.00 65-----Total TCDF ND 1.2 2,3,7,8-TCDD-13C 2.00 63-----1,2,3,7,8-PeCDF-13C 2.00 632,3,7,8-TCDD ND 2.2 2,3,4,7,8-PeCDF-13C 2.00 63-----Total TCDD ND 2.2 1,2,3,7,8-PeCDD-13C 2.00 72-----1,2,3,4,7,8-HxCDF-13C 2.00 631,2,3,7,8-PeCDF ND 2.1 1,2,3,6,7,8-HxCDF-13C 2.00 60-----2,3,4,7,8-PeCDF ND 1.5 2,3,4,6,7,8-HxCDF-13C 2.00 65-----Total PeCDF ND 1.5 1,2,3,7,8,9-HxCDF-13C 2.00 66-----1,2,3,4,7,8-HxCDD-13C 2.00 681,2,3,7,8-PeCDD ND 2.0 1,2,3,6,7,8-HxCDD-13C 2.00 72-----Total PeCDD ND 2.0 1,2,3,4,6,7,8-HpCDF-13C 2.00 63-----1,2,3,4,7,8,9-HpCDF-13C 2.00 611,2,3,4,7,8-HxCDF ND 1.7 1,2,3,4,6,7,8-HpCDD-13C 2.00 64-----1,2,3,6,7,8-HxCDF ND 1.6 OCDD-13C 4.00 62-----2,3,4,6,7,8-HxCDF ND 1.6-----1,2,3,7,8,9-HxCDF ND 1.9 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 1.6 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 1.9 2,3,7,8-TCDD-37Cl4 0.20 84-----1,2,3,6,7,8-HxCDD ND 1.4-----1,2,3,7,8,9-HxCDD ND 1.6-----Total HxCDD ND 1.4-----
1,2,3,4,6,7,8-HpCDF 2.9 2.8 Total 2,3,7,8-TCDDJ-----1,2,3,4,7,8,9-HpCDF ND 4.2 Equivalence: 0.085 pg/L-----Total HpCDF 2.9 2.8 (Lower-bound - Using 2005 WHO Factors)J-----
1,2,3,4,6,7,8-HpCDD -----3.9 IJ4.1Total HpCDD ND 3.9-----
OCDF -----5.3 IJ18OCDD327.2 J-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
I=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 12 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 90 of 101
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID RW01WG-09192392689056002U231031B_08JF
NA983 mL
NAU230926U231031B_01 & U231031B_18BLANK-108777
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/19/2023 11:5509/29/2023 08:5010/11/2023 10:3010/31/2023 20:24
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF ND 1.2 2,3,7,8-TCDF-13C 2.00 72-----Total TCDF ND 1.2 2,3,7,8-TCDD-13C 2.00 69-----1,2,3,7,8-PeCDF-13C 2.00 662,3,7,8-TCDD ND 2.3 2,3,4,7,8-PeCDF-13C 2.00 68-----Total TCDD ND 2.3 1,2,3,7,8-PeCDD-13C 2.00 77-----1,2,3,4,7,8-HxCDF-13C 2.00 651,2,3,7,8-PeCDF ND 1.4 1,2,3,6,7,8-HxCDF-13C 2.00 62-----2,3,4,7,8-PeCDF ND 1.0 2,3,4,6,7,8-HxCDF-13C 2.00 64-----Total PeCDF ND 1.0 1,2,3,7,8,9-HxCDF-13C 2.00 67-----1,2,3,4,7,8-HxCDD-13C 2.00 661,2,3,7,8-PeCDD ND 2.1 1,2,3,6,7,8-HxCDD-13C 2.00 79-----Total PeCDD ND 2.1 1,2,3,4,6,7,8-HpCDF-13C 2.00 62-----1,2,3,4,7,8,9-HpCDF-13C 2.00 581,2,3,4,7,8-HxCDF ND 0.69 1,2,3,4,6,7,8-HpCDD-13C 2.00 61-----1,2,3,6,7,8-HxCDF ND 0.69 OCDD-13C 4.00 57-----2,3,4,6,7,8-HxCDF ND 0.64-----1,2,3,7,8,9-HxCDF -----0.80 1,2,3,4-TCDD-13C 2.00 NAIJ1.7Total HxCDF ND 0.64 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 2.1 2,3,7,8-TCDD-37Cl4 0.20 87-----1,2,3,6,7,8-HxCDD ND 1.9-----1,2,3,7,8,9-HxCDD ND 1.9-----Total HxCDD ND 1.9-----
1,2,3,4,6,7,8-HpCDF ND 3.1 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 4.5 Equivalence: 0.24 pg/L-----Total HpCDF ND 3.1 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD 5.4 4.1 BJ-----Total HpCDD 5.4 4.1 BJ-----
OCDF 9.2 4.4 J-----OCDD 33 8.7 J-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 13 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 91 of 101
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ20WG-09192392689056003U231031B_09JF
NA991 mL
NAU230926U231031B_01 & U231031B_18BLANK-108777
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/19/2023 17:2009/29/2023 08:5010/11/2023 10:3010/31/2023 21:10
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF -----1.2 2,3,7,8-TCDF-13C 2.00 66IJ4.1Total TCDF ND 1.2 2,3,7,8-TCDD-13C 2.00 63-----1,2,3,7,8-PeCDF-13C 2.00 572,3,7,8-TCDD ND 3.1 2,3,4,7,8-PeCDF-13C 2.00 57-----Total TCDD ND 3.1 1,2,3,7,8-PeCDD-13C 2.00 62-----1,2,3,4,7,8-HxCDF-13C 2.00 531,2,3,7,8-PeCDF ND 1.5 1,2,3,6,7,8-HxCDF-13C 2.00 50-----2,3,4,7,8-PeCDF -----0.95 2,3,4,6,7,8-HxCDF-13C 2.00 53IJ1.1Total PeCDF ND 0.95 1,2,3,7,8,9-HxCDF-13C 2.00 52-----1,2,3,4,7,8-HxCDD-13C 2.00 521,2,3,7,8-PeCDD ND 2.5 1,2,3,6,7,8-HxCDD-13C 2.00 61-----Total PeCDD ND 2.5 1,2,3,4,6,7,8-HpCDF-13C 2.00 39-----R1,2,3,4,7,8,9-HpCDF-13C 2.00 39 R1,2,3,4,7,8-HxCDF ND 2.9 1,2,3,4,6,7,8-HpCDD-13C 2.00 39-----R1,2,3,6,7,8-HxCDF ND 2.9 OCDD-13C 4.00 30-----R2,3,4,6,7,8-HxCDF ND 3.0-----1,2,3,7,8,9-HxCDF ND 3.5 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF ND 2.9 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 5.6 2,3,7,8-TCDD-37Cl4 0.20 85-----1,2,3,6,7,8-HxCDD ND 4.5-----1,2,3,7,8,9-HxCDD ND 4.8-----Total HxCDD ND 4.5-----
1,2,3,4,6,7,8-HpCDF ND 7.3 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 10 Equivalence: 0.76 pg/L-----Total HpCDF ND 7.3 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD ND 7.5-----Total HpCDD ND 7.5-----
OCDF 23 15 J-----OCDD 69 25 J-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
R=Recovery outside target rangeI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 14 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 92 of 101
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID PZ04WG-09192392689056004-RL231027B_15JF
NA105 mL
NAL230816L231027A_09 & L231027B_17BLANK-108989
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/19/2023 14:1509/29/2023 08:5010/24/2023 10:0010/28/2023 00:17
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF 42 14 2,3,7,8-TCDF-13C 2.00 65J-----Total TCDF 42 14 2,3,7,8-TCDD-13C 2.00 63J-----1,2,3,7,8-PeCDF-13C 2.00 572,3,7,8-TCDD ND 11 2,3,4,7,8-PeCDF-13C 2.00 62-----Total TCDD ND 11 1,2,3,7,8-PeCDD-13C 2.00 68-----1,2,3,4,7,8-HxCDF-13C 2.00 531,2,3,7,8-PeCDF 49 14 1,2,3,6,7,8-HxCDF-13C 2.00 76J-----2,3,4,7,8-PeCDF 16 8.3 2,3,4,6,7,8-HxCDF-13C 2.00 66J-----Total PeCDF 66 8.3 1,2,3,7,8,9-HxCDF-13C 2.00 54J-----1,2,3,4,7,8-HxCDD-13C 2.00 541,2,3,7,8-PeCDD ND 13 1,2,3,6,7,8-HxCDD-13C 2.00 61-----Total PeCDD ND 13 1,2,3,4,6,7,8-HpCDF-13C 2.00 47-----1,2,3,4,7,8,9-HpCDF-13C 2.00 411,2,3,4,7,8-HxCDF ND 47 1,2,3,4,6,7,8-HpCDD-13C 2.00 50-----1,2,3,6,7,8-HxCDF ND 34 OCDD-13C 4.00 41-----2,3,4,6,7,8-HxCDF ND 34-----1,2,3,7,8,9-HxCDF ND 51 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF 73 34 1,2,3,7,8,9-HxCDD-13C 2.00 NAJ-----
1,2,3,4,7,8-HxCDD ND 34 2,3,7,8-TCDD-37Cl4 0.20 89-----1,2,3,6,7,8-HxCDD 55 31 J-----1,2,3,7,8,9-HxCDD 35 32 J-----Total HxCDD 150 31 J-----
1,2,3,4,6,7,8-HpCDF 110 53 Total 2,3,7,8-TCDDJ-----1,2,3,4,7,8,9-HpCDF ND 86 Equivalence: 25 pg/L-----Total HpCDF 110 53 (Lower-bound - Using 2005 WHO Factors)BJ-----
1,2,3,4,6,7,8-HpCDD 380 74 J-----Total HpCDD 720 74 J-----
OCDF 670 130 J-----OCDD 880 110 J-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank level
EDL = Estimated Detection Limit
Page 15 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 93 of 101
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
BLANK-108777F231014A_10
JRH
982 mLF230720F231014A_03 & F231014A_12
MatrixDilutionExtractedAnalyzed
Water
10/11/2023 10:3010/14/2023 16:42
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKTJ
NativeIsomers pg/LConc EMPCpg/L pg/L InternalStandards Addedng's PercentRecoveryEDL
2,3,7,8-TCDF ND -----1.2 2,3,7,8-TCDF-13C 2.00 59Total TCDF ND -----1.2 2,3,7,8-TCDD-13C 2.00 571,2,3,7,8-PeCDF-13C 2.00 542,3,7,8-TCDD ND -----2.2 2,3,4,7,8-PeCDF-13C 2.00 53Total TCDD ND -----2.2 1,2,3,7,8-PeCDD-13C 2.00 591,2,3,4,7,8-HxCDF-13C 2.00 631,2,3,7,8-PeCDF -----1.3 1.2 IJ 1,2,3,6,7,8-HxCDF-13C 2.00 622,3,4,7,8-PeCDF -----1.6 0.81 IJ 2,3,4,6,7,8-HxCDF-13C 2.00 63Total PeCDF ND -----0.81 1,2,3,7,8,9-HxCDF-13C 2.00 591,2,3,4,7,8-HxCDD-13C 2.00 581,2,3,7,8-PeCDD ND -----0.91 1,2,3,6,7,8-HxCDD-13C 2.00 65Total PeCDD ND -----0.91 1,2,3,4,6,7,8-HpCDF-13C 2.00 521,2,3,4,7,8,9-HpCDF-13C 2.00 491,2,3,4,7,8-HxCDF -----1.3 1.1 IJ 1,2,3,4,6,7,8-HpCDD-13C 2.00 611,2,3,6,7,8-HxCDF -----2.2 1.1 IJ OCDD-13C 4.00 402,3,4,6,7,8-HxCDF ND -----1.21,2,3,7,8,9-HxCDF 1.8 -----1.6 J 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF 1.8 -----1.1 J 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD ND -----2.2 2,3,7,8-TCDD-37Cl4 0.20 771,2,3,6,7,8-HxCDD -----1.7 1.6 IJ1,2,3,7,8,9-HxCDD ND -----1.8Total HxCDD ND -----1.6
1,2,3,4,6,7,8-HpCDF ND -----3.1 Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----5.2 Equivalence: 1.3 pg/LTotal HpCDF ND -----3.1 (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD 5.5 -----3.0 JTotal HpCDD 9.5 -----3.0 J
OCDF -----14 3.6 IJOCDD-----28 3.7 IJ
Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
I =Isotope ratio out of specification
EDL=EstimatedDetection Limit
Page 16 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 94 of 101
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
BLANK-108989L231026B_09
SMT
955 mLL230816L231026B_03 & L231026B_22
MatrixDilutionExtractedAnalyzed
Water
10/24/2023 10:0010/26/2023 17:47
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKVM
NativeIsomers pg/LConc EMPCpg/L pg/L InternalStandards Addedng's PercentRecoveryEDL
2,3,7,8-TCDF ND -----0.89 2,3,7,8-TCDF-13C 2.00 78Total TCDF ND -----0.89 2,3,7,8-TCDD-13C 2.00 721,2,3,7,8-PeCDF-13C 2.00 742,3,7,8-TCDD ND -----1.4 2,3,4,7,8-PeCDF-13C 2.00 73Total TCDD ND -----1.4 1,2,3,7,8-PeCDD-13C 2.00 791,2,3,4,7,8-HxCDF-13C 2.00 941,2,3,7,8-PeCDF -----1.8 1.2 IJ 1,2,3,6,7,8-HxCDF-13C 2.00 912,3,4,7,8-PeCDF ND -----0.72 2,3,4,6,7,8-HxCDF-13C 2.00 84Total PeCDF ND -----0.72 1,2,3,7,8,9-HxCDF-13C 2.00 771,2,3,4,7,8-HxCDD-13C 2.00 741,2,3,7,8-PeCDD ND -----1.5 1,2,3,6,7,8-HxCDD-13C 2.00 92Total PeCDD ND -----1.5 1,2,3,4,6,7,8-HpCDF-13C 2.00 721,2,3,4,7,8,9-HpCDF-13C 2.00 591,2,3,4,7,8-HxCDF ND -----1.5 1,2,3,4,6,7,8-HpCDD-13C 2.00 701,2,3,6,7,8-HxCDF ND -----1.7 OCDD-13C 4.00 66 Y2,3,4,6,7,8-HxCDF ND -----1.71,2,3,7,8,9-HxCDF ND -----2.4 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF ND -----1.5 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD ND -----1.3 2,3,7,8-TCDD-37Cl4 0.20 851,2,3,6,7,8-HxCDD -----2.1 1.1 IJ1,2,3,7,8,9-HxCDD ND -----1.2Total HxCDD 2.2 -----1.1 J
1,2,3,4,6,7,8-HpCDF ND -----8.3 Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----14 Equivalence: 0.51 pg/LTotal HpCDF 20 -----8.3 J (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD 22 -----2.3 JTotal HpCDD 39 -----2.3 J
OCDF 39 -----6.2 JOCDD-----53 7.9 IJ
Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
I =Isotope ratio out of specification
Y=Calculated using average of daily RFs
EDL=EstimatedDetection Limit
Page 17 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 95 of 101
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCS-108778F231014A_04
JRH
1010 mLF230720F231014A_03 & F231014A_12
MatrixDilutionExtractedAnalyzed
Water
10/11/2023 10:3010/14/2023 12:07
NA
Method Blank ID BLANK-108777
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.19 2,3,7,8-TCDF-13C 2.0 6194Total TCDF 2,3,7,8-TCDD-13C 2.0 601,2,3,7,8-PeCDF-13C 2.0 582,3,7,8-TCDD 0.20 0.20 2,3,4,7,8-PeCDF-13C 2.0 5998Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 621,2,3,4,7,8-HxCDF-13C 2.0 611,2,3,7,8-PeCDF 1.0 0.90 1,2,3,6,7,8-HxCDF-13C 2.0 67902,3,4,7,8-PeCDF 1.0 0.93 2,3,4,6,7,8-HxCDF-13C 2.0 6393Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 621,2,3,4,7,8-HxCDD-13C 2.0 571,2,3,7,8-PeCDD 1.0 0.87 1,2,3,6,7,8-HxCDD-13C 2.0 6887Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 561,2,3,4,7,8,9-HpCDF-13C 2.0 541,2,3,4,7,8-HxCDF 1.0 0.96 1,2,3,4,6,7,8-HpCDD-13C 2.0 68961,2,3,6,7,8-HxCDF 1.0 0.98 OCDD-13C 4.0 46982,3,4,6,7,8-HxCDF 1.0 1.0 1021,2,3,7,8,9-HxCDF 1.0 1.0 1,2,3,4-TCDD-13C 2.0 NA101Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.1 2,3,7,8-TCDD-37Cl4 0.20 751061,2,3,6,7,8-HxCDD 1.0 0.94 941,2,3,7,8,9-HxCDD 1.0 1.0 104Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.93 931,2,3,4,7,8,9-HpCDF 1.0 0.93 93Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.88 88Total HpCDD
OCDF 2.0 1.8 92OCDD2.0 2.1 106
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 18 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 96 of 101
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCS-108990L231026B_05
SMT
931 mLL230816L231026B_03 & L231026B_22
MatrixDilutionExtractedAnalyzed
Water
10/24/2023 10:0010/26/2023 15:03
NA
Method Blank ID BLANK-108989
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.17 2,3,7,8-TCDF-13C 2.0 7586Total TCDF 2,3,7,8-TCDD-13C 2.0 691,2,3,7,8-PeCDF-13C 2.0 732,3,7,8-TCDD 0.20 0.19 2,3,4,7,8-PeCDF-13C 2.0 7394Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 781,2,3,4,7,8-HxCDF-13C 2.0 921,2,3,7,8-PeCDF 1.0 0.84 1,2,3,6,7,8-HxCDF-13C 2.0 92842,3,4,7,8-PeCDF 1.0 0.84 2,3,4,6,7,8-HxCDF-13C 2.0 8684Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 761,2,3,4,7,8-HxCDD-13C 2.0 831,2,3,7,8-PeCDD 1.0 0.81 1,2,3,6,7,8-HxCDD-13C 2.0 9681Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 751,2,3,4,7,8,9-HpCDF-13C 2.0 621,2,3,4,7,8-HxCDF 1.0 0.84 1,2,3,4,6,7,8-HpCDD-13C 2.0 75841,2,3,6,7,8-HxCDF 1.0 0.88 OCDD-13C 4.0 7088 Y2,3,4,6,7,8-HxCDF 1.0 0.91 911,2,3,7,8,9-HxCDF 1.0 0.87 1,2,3,4-TCDD-13C 2.0 NA87Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 0.93 2,3,7,8-TCDD-37Cl4 0.20 72931,2,3,6,7,8-HxCDD 1.0 0.86 861,2,3,7,8,9-HxCDD 1.0 0.87 87Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.91 911,2,3,4,7,8,9-HpCDF 1.0 0.90 90Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.83 83Total HpCDD
OCDF 2.0 1.9 94OCDD2.0 1.9 97
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 19 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 97 of 101
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCSD-108779F231014A_05
JRH
1010 mLF230720F231014A_03 & F231014A_12
MatrixDilutionExtractedAnalyzed
Water
10/11/2023 10:3010/14/2023 12:52
NA
Method Blank ID BLANK-108777
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.19 2,3,7,8-TCDF-13C 2.0 5195Total TCDF 2,3,7,8-TCDD-13C 2.0 511,2,3,7,8-PeCDF-13C 2.0 492,3,7,8-TCDD 0.20 0.19 2,3,4,7,8-PeCDF-13C 2.0 5093Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 531,2,3,4,7,8-HxCDF-13C 2.0 571,2,3,7,8-PeCDF 1.0 0.87 1,2,3,6,7,8-HxCDF-13C 2.0 59872,3,4,7,8-PeCDF 1.0 0.90 2,3,4,6,7,8-HxCDF-13C 2.0 6090Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 551,2,3,4,7,8-HxCDD-13C 2.0 531,2,3,7,8-PeCDD 1.0 0.86 1,2,3,6,7,8-HxCDD-13C 2.0 6186Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 511,2,3,4,7,8,9-HpCDF-13C 2.0 461,2,3,4,7,8-HxCDF 1.0 0.97 1,2,3,4,6,7,8-HpCDD-13C 2.0 60971,2,3,6,7,8-HxCDF 1.0 1.0 OCDD-13C 4.0 37101 R2,3,4,6,7,8-HxCDF 1.0 0.94 941,2,3,7,8,9-HxCDF 1.0 0.97 1,2,3,4-TCDD-13C 2.0 NA97Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.0 2,3,7,8-TCDD-37Cl4 0.20 861021,2,3,6,7,8-HxCDD 1.0 0.92 921,2,3,7,8,9-HxCDD 1.0 1.0 100Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.92 921,2,3,4,7,8,9-HpCDF 1.0 0.87 87Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.87 87Total HpCDD
OCDF 2.0 1.9 95OCDD2.0 2.2 110
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 20 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 98 of 101
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCSD-108991L231026B_06
SMT
966 mLL230816L231026B_03 & L231026B_22
MatrixDilutionExtractedAnalyzed
Water
10/24/2023 10:0010/26/2023 15:44
NA
Method Blank ID BLANK-108989
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.17 2,3,7,8-TCDF-13C 2.0 7686Total TCDF 2,3,7,8-TCDD-13C 2.0 731,2,3,7,8-PeCDF-13C 2.0 702,3,7,8-TCDD 0.20 0.18 2,3,4,7,8-PeCDF-13C 2.0 7288Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 771,2,3,4,7,8-HxCDF-13C 2.0 771,2,3,7,8-PeCDF 1.0 0.83 1,2,3,6,7,8-HxCDF-13C 2.0 85832,3,4,7,8-PeCDF 1.0 0.82 2,3,4,6,7,8-HxCDF-13C 2.0 9282Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 791,2,3,4,7,8-HxCDD-13C 2.0 911,2,3,7,8-PeCDD 1.0 0.79 1,2,3,6,7,8-HxCDD-13C 2.0 9879Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 721,2,3,4,7,8,9-HpCDF-13C 2.0 491,2,3,4,7,8-HxCDF 1.0 0.79 1,2,3,4,6,7,8-HpCDD-13C 2.0 71791,2,3,6,7,8-HxCDF 1.0 0.90 OCDD-13C 4.0 8690 Y2,3,4,6,7,8-HxCDF 1.0 0.87 871,2,3,7,8,9-HxCDF 1.0 0.79 1,2,3,4-TCDD-13C 2.0 NA79Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 0.82 2,3,7,8-TCDD-37Cl4 0.20 82821,2,3,6,7,8-HxCDD 1.0 0.88 881,2,3,7,8,9-HxCDD 1.0 0.82 82Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.86 861,2,3,4,7,8,9-HpCDF 1.0 0.89 89Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.79 79Total HpCDD
OCDF 2.0 1.7 85OCDD2.0 1.9 94
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 21 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 99 of 101
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Client
Spike 1 IDSpike 1 Filename F231014A_04LCS-108778
PACE Charlotte
Spike Recovery Relative Percent Difference (RPD) Results
Spike 2 IDSpike 2 Filename F231014A_05LCSD-108779
Method 8290A
Spike 1 Spike 2Compound%REC %REC %RPD
2,3,7,8-TCDF 94 95 1.12,3,7,8-TCDD 98 93 5.21,2,3,7,8-PeCDF 90 87 3.42,3,4,7,8-PeCDF 93 90 3.31,2,3,7,8-PeCDD 87 86 1.21,2,3,4,7,8-HxCDF 96 97 1.01,2,3,6,7,8-HxCDF 98 101 3.02,3,4,6,7,8-HxCDF 102 94 8.21,2,3,7,8,9-HxCDF 101 97 4.01,2,3,4,7,8-HxCDD 106 102 3.81,2,3,6,7,8-HxCDD 94 92 2.21,2,3,7,8,9-HxCDD 104 100 3.91,2,3,4,6,7,8-HpCDF 93 92 1.11,2,3,4,7,8,9-HpCDF 93 87 6.71,2,3,4,6,7,8-HpCDD 88 87 1.1OCDF92953.2OCDD1061103.7
%REC = Percent RecoveredRPD=The differencebetweenthetwo valuesdivided by the mean value
Page 22 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 100 of 101
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Client
Spike 1 IDSpike 1 Filename L231026B_05LCS-108990
PACE Charlotte
Spike Recovery Relative Percent Difference (RPD) Results
Spike 2 IDSpike 2 Filename L231026B_06LCSD-108991
Method 8290A
Spike 1 Spike 2Compound%REC %REC %RPD
2,3,7,8-TCDF 86 86 0.02,3,7,8-TCDD 94 88 6.61,2,3,7,8-PeCDF 84 83 1.22,3,4,7,8-PeCDF 84 82 2.41,2,3,7,8-PeCDD 81 79 2.51,2,3,4,7,8-HxCDF 84 79 6.11,2,3,6,7,8-HxCDF 88 90 2.22,3,4,6,7,8-HxCDF 91 87 4.51,2,3,7,8,9-HxCDF 87 79 9.61,2,3,4,7,8-HxCDD 93 82 12.61,2,3,6,7,8-HxCDD 86 88 2.31,2,3,7,8,9-HxCDD 87 82 5.91,2,3,4,6,7,8-HpCDF 91 86 5.61,2,3,4,7,8,9-HpCDF 90 89 1.11,2,3,4,6,7,8-HpCDD 83 79 4.9OCDF948510.1OCDD97943.1
%REC = Percent RecoveredRPD=The differencebetweenthetwo valuesdivided by the mean value
Page 23 of 23Report No.....10670647_SW8290AFC_L2_dfr
Page 101 of 101
#=CL#
October 19, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92689437
92689437
Project:
Pace Project No.:
RE:
Christina AshdownENSAFE313 Wingo WayMount Pleasant, SC 29464
Pactiv Energreen GWS (9/21)-Revised Report
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on September 22, 2023. The results relate onlyto the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and thelaboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Ormond Beach
This revision was issued on 10/19/23 to amend the sample IDs for -001 and -002.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc: Jennings Kerr, ENSAFE Inc.
Lab, ENSAFE Inc.
David Warren, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 73
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 73
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Lab ID Sample ID Matrix Date Collected Date Received
92689437001 PZ09WG-092123 Water 09/21/23 09:05 09/22/23 08:10
92689437002 PZ08WG-092123 Water 09/21/23 10:05 09/22/23 08:10
92689437003 EB02WQ-092123 Water 09/21/23 11:05 09/22/23 08:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 73
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92689437001 PZ09WG-092123 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAME
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 300.0 Rev 2.1 1993 4 PASI-ACDC
92689437002 PZ08WG-092123 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAME
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 300.0 Rev 2.1 1993 4 PASI-ACDC
92689437003 EB02WQ-092123 SM 2120B-2011 2 PASI-ELRB
EPA 6010 17 PASI-OAME
EPA 6010 17 PASI-OAME
EPA 7470 1 PASI-OJNK
EPA 7470 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 4500-S2D-2011 1 PASI-AJP1
EPA 300.0 Rev 2.1 1993 4 PASI-ACDC
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ09WG-092123 Lab ID: 92689437001 Collected: 09/21/23 09:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.4 Std. Units 10/18/23 14:561
True Color ND units 10/18/23 14:56 H35.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/04/23 02:37 7440-36-010/02/23 12:1915.0 5.5 1
Arsenic ND ug/L 10/04/23 02:37 7440-38-210/02/23 12:1910.0 3.4 1
Barium 353 ug/L 10/04/23 02:37 7440-39-310/02/23 12:1910.0 0.84 1
Beryllium ND ug/L 10/04/23 02:37 7440-41-710/02/23 12:194.0 0.17 1
Boron ND ug/L 10/04/23 02:37 7440-42-810/02/23 12:1950.0 12.4 1
Cadmium ND ug/L 10/04/23 02:37 7440-43-910/02/23 12:191.0 0.33 1
Chromium ND ug/L 10/04/23 02:37 7440-47-310/02/23 12:195.0 1.7 1
Cobalt 1.3J ug/L 10/04/23 02:37 7440-48-410/02/23 12:1910.0 0.96 1
Copper ND ug/L 10/04/23 02:37 7440-50-810/02/23 12:195.0 2.6 1
Lead ND ug/L 10/04/23 02:37 7439-92-110/02/23 12:1910.0 2.1 1
Manganese 6.1 ug/L 10/04/23 02:37 7439-96-510/02/23 12:195.0 1.1 1
Nickel 1.6J ug/L 10/04/23 02:37 7440-02-010/02/23 12:195.0 1.0 1
Selenium ND ug/L 10/04/23 02:37 7782-49-210/02/23 12:1915.0 3.9 1
Silver ND ug/L 10/04/23 02:37 7440-22-410/02/23 12:195.0 1.0 1
Thallium ND ug/L 10/04/23 02:37 7440-28-010/02/23 12:1915.0 2.9 1
Vanadium ND ug/L 10/04/23 02:37 7440-62-210/02/23 12:1910.0 1.0 1
Zinc ND ug/L 10/04/23 02:37 7440-66-610/02/23 12:1920.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/03/23 22:52 7440-36-010/03/23 07:4315.0 5.5 1
Arsenic, Dissolved ND ug/L 10/03/23 22:52 7440-38-210/03/23 07:4310.0 3.4 1
Barium, Dissolved 348 ug/L 10/03/23 22:52 7440-39-310/03/23 07:4310.0 0.84 1
Beryllium, Dissolved ND ug/L 10/03/23 22:52 7440-41-710/03/23 07:434.0 0.17 1
Boron, Dissolved ND ug/L 10/03/23 22:52 7440-42-810/03/23 07:4350.0 12.4 1
Cadmium, Dissolved ND ug/L 10/03/23 22:52 7440-43-910/03/23 07:431.0 0.33 1
Chromium, Dissolved ND ug/L 10/03/23 22:52 7440-47-310/03/23 07:435.0 1.7 1
Cobalt, Dissolved ND ug/L 10/03/23 22:52 7440-48-410/03/23 07:4310.0 0.96 1
Copper, Dissolved ND ug/L 10/03/23 22:52 7440-50-810/03/23 07:435.0 2.6 1
Lead, Dissolved ND ug/L 10/03/23 22:52 7439-92-110/03/23 07:4310.0 2.1 1
Manganese, Dissolved 5.0 ug/L 10/03/23 22:52 7439-96-510/03/23 07:435.0 1.1 1
Nickel, Dissolved 1.8J ug/L 10/03/23 22:52 7440-02-010/03/23 07:435.0 1.0 1
Selenium, Dissolved ND ug/L 10/03/23 22:52 7782-49-210/03/23 07:4315.0 3.9 1
Silver, Dissolved ND ug/L 10/03/23 22:52 7440-22-410/03/23 07:435.0 1.0 1
Thallium, Dissolved ND ug/L 10/03/23 22:52 7440-28-010/03/23 07:4315.0 2.9 1
Vanadium, Dissolved ND ug/L 10/03/23 22:52 7440-62-210/03/23 07:4310.0 1.0 1
Zinc, Dissolved ND ug/L 10/03/23 22:52 7440-66-610/03/23 07:4320.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ09WG-092123 Lab ID: 92689437001 Collected: 09/21/23 09:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury 0.16J ug/L 10/09/23 10:48 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 11:59 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/26/23 19:24 83-32-909/25/23 17:2610.0 2.0 1
Acenaphthylene ND ug/L 09/26/23 19:24 208-96-809/25/23 17:2610.0 2.0 1
Acetophenone ND ug/L 09/26/23 19:24 98-86-209/25/23 17:2610.0 1.5 1
Anthracene ND ug/L 09/26/23 19:24 120-12-709/25/23 17:2610.0 2.3 1
Atrazine ND ug/L 09/26/23 19:24 1912-24-909/25/23 17:2610.0 3.2 1
Benzaldehyde ND ug/L 09/26/23 19:24 100-52-709/25/23 17:2610.0 3.6 1
Benzo(a)anthracene ND ug/L 09/26/23 19:24 56-55-309/25/23 17:2610.0 2.7 1
Benzo(a)pyrene ND ug/L 09/26/23 19:24 50-32-809/25/23 17:2610.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/26/23 19:24 205-99-209/25/23 17:2610.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/26/23 19:24 191-24-209/25/23 17:2610.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/26/23 19:24 207-08-909/25/23 17:2610.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/26/23 19:24 92-52-409/25/23 17:2610.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/26/23 19:24 101-55-309/25/23 17:2610.0 1.8 1
Butylbenzylphthalate ND ug/L 09/26/23 19:24 85-68-709/25/23 17:2610.0 3.1 1
Caprolactam ND ug/L 09/26/23 19:24 105-60-209/25/23 17:2610.0 6.9 1
Carbazole ND ug/L 09/26/23 19:24 86-74-809/25/23 17:2610.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/26/23 19:24 59-50-709/25/23 17:2610.0 3.3 1
4-Chloroaniline ND ug/L 09/26/23 19:24 106-47-809/25/23 17:2620.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/26/23 19:24 111-91-109/25/23 17:2610.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/26/23 19:24 111-44-409/25/23 17:2610.0 1.9 1
2-Chloronaphthalene ND ug/L 09/26/23 19:24 91-58-709/25/23 17:2610.0 1.7 1
2-Chlorophenol ND ug/L 09/26/23 19:24 95-57-809/25/23 17:2610.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/26/23 19:24 7005-72-309/25/23 17:2610.0 2.0 1
Chrysene ND ug/L 09/26/23 19:24 218-01-909/25/23 17:2610.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/26/23 19:24 53-70-309/25/23 17:2610.0 3.0 1
Dibenzofuran ND ug/L 09/26/23 19:24 132-64-909/25/23 17:2610.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/26/23 19:24 91-94-109/25/23 17:2620.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/26/23 19:24 120-83-209/25/23 17:2610.0 1.4 1
Diethylphthalate ND ug/L 09/26/23 19:24 84-66-209/25/23 17:2610.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/26/23 19:24 105-67-909/25/23 17:2610.0 1.7 1
Dimethylphthalate ND ug/L 09/26/23 19:24 131-11-309/25/23 17:2610.0 2.1 1
Di-n-butylphthalate ND ug/L 09/26/23 19:24 84-74-209/25/23 17:2610.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/26/23 19:24 534-52-109/25/23 17:2620.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/26/23 19:24 51-28-509/25/23 17:2650.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/26/23 19:24 121-14-209/25/23 17:2610.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/26/23 19:24 606-20-209/25/23 17:2610.0 1.7 1
Di-n-octylphthalate ND ug/L 09/26/23 19:24 117-84-009/25/23 17:2610.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ09WG-092123 Lab ID: 92689437001 Collected: 09/21/23 09:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/26/23 19:24 117-81-709/25/23 17:266.0 3.7 1
Fluoranthene ND ug/L 09/26/23 19:24 206-44-009/25/23 17:2610.0 2.2 1
Fluorene ND ug/L 09/26/23 19:24 86-73-709/25/23 17:2610.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/26/23 19:24 87-68-309/25/23 17:2610.0 1.8 1
Hexachlorobenzene ND ug/L 09/26/23 19:24 118-74-109/25/23 17:2610.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/26/23 19:24 77-47-409/25/23 17:2610.0 1.6 1
Hexachloroethane ND ug/L 09/26/23 19:24 67-72-109/25/23 17:2610.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/26/23 19:24 193-39-509/25/23 17:2610.0 2.9 1
Isophorone ND ug/L 09/26/23 19:24 78-59-109/25/23 17:2610.0 1.7 1
2-Methylnaphthalene ND ug/L 09/26/23 19:24 91-57-609/25/23 17:2610.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/26/23 19:24 95-48-709/25/23 17:2610.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/26/23 19:24 15831-10-409/25/23 17:2610.0 1.2 1
Naphthalene ND ug/L 09/26/23 19:24 91-20-309/25/23 17:2610.0 2.1 1
2-Nitroaniline ND ug/L 09/26/23 19:24 88-74-409/25/23 17:2620.0 3.0 1
3-Nitroaniline ND ug/L 09/26/23 19:24 99-09-209/25/23 17:2620.0 3.8 1
4-Nitroaniline ND ug/L 09/26/23 19:24 100-01-609/25/23 17:2620.0 5.1 1
Nitrobenzene ND ug/L 09/26/23 19:24 98-95-309/25/23 17:2610.0 1.9 1
2-Nitrophenol ND ug/L 09/26/23 19:24 88-75-509/25/23 17:2610.0 1.4 1
4-Nitrophenol ND ug/L 09/26/23 19:24 100-02-709/25/23 17:2650.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/26/23 19:24 621-64-709/25/23 17:2610.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/26/23 19:24 86-30-609/25/23 17:2610.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/26/23 19:24 108-60-109/25/23 17:2610.0 1.2 1
Pentachlorophenol ND ug/L 09/26/23 19:24 87-86-509/25/23 17:2620.0 3.8 1
Phenanthrene ND ug/L 09/26/23 19:24 85-01-809/25/23 17:2610.0 2.0 1
Phenol ND ug/L 09/26/23 19:24 108-95-209/25/23 17:2610.0 1.4 1
Pyrene ND ug/L 09/26/23 19:24 129-00-009/25/23 17:2610.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/26/23 19:24 95-95-409/25/23 17:2610.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/26/23 19:24 88-06-209/25/23 17:2610.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)121 %09/26/23 19:24 4165-60-009/25/23 17:2610-138 1
2-Fluorobiphenyl (S)124 %09/26/23 19:24 321-60-809/25/23 17:2610-130 1
Terphenyl-d14 (S)154 %09/26/23 19:24 1718-51-009/25/23 17:2619-191 1
Phenol-d6 (S)61 %09/26/23 19:24 13127-88-309/25/23 17:2610-130 1
2-Fluorophenol (S)85 %09/26/23 19:24 367-12-409/25/23 17:2610-130 1
2,4,6-Tribromophenol (S)152 %09/26/23 19:24 118-79-609/25/23 17:2610-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/01/23 07:19 67-64-125.0 5.1 1
Benzene ND ug/L 10/01/23 07:19 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 10/01/23 07:19 75-27-41.0 0.31 1
Bromoform ND ug/L 10/01/23 07:19 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/01/23 07:19 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/01/23 07:19 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/01/23 07:19 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ09WG-092123 Lab ID: 92689437001 Collected: 09/21/23 09:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 10/01/23 07:19 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/01/23 07:19 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/01/23 07:19 75-00-31.0 0.65 1
Chloroform 1.1 ug/L 10/01/23 07:19 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/01/23 07:19 74-87-31.0 0.54 1
Cyclohexane ND ug/L 10/01/23 07:19 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 10/01/23 07:19 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/01/23 07:19 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/01/23 07:19 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 10/01/23 07:19 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/01/23 07:19 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/01/23 07:19 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/01/23 07:19 75-71-8 v11.0 0.35 1
1,1-Dichloroethane ND ug/L 10/01/23 07:19 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/01/23 07:19 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/01/23 07:19 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/01/23 07:19 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/01/23 07:19 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/01/23 07:19 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/01/23 07:19 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/01/23 07:19 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 10/01/23 07:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/01/23 07:19 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 10/01/23 07:19 98-82-81.0 0.33 1
Methyl acetate ND ug/L 10/01/23 07:19 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 10/01/23 07:19 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 10/01/23 07:19 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/01/23 07:19 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/01/23 07:19 1634-04-41.0 0.42 1
Styrene ND ug/L 10/01/23 07:19 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 10/01/23 07:19 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/01/23 07:19 127-18-41.0 0.29 1
Toluene ND ug/L 10/01/23 07:19 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 10/01/23 07:19 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/01/23 07:19 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/01/23 07:19 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/01/23 07:19 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/01/23 07:19 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 10/01/23 07:19 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 10/01/23 07:19 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 10/01/23 07:19 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/01/23 07:19 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %10/01/23 07:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %10/01/23 07:19 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ09WG-092123 Lab ID: 92689437001 Collected: 09/21/23 09:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)100 %10/01/23 07:19 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 40.8 mg/L 10/03/23 19:135.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/27/23 01:41 18496-25-80.10 0.022 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Bromide 0.16 mg/L 09/22/23 22:27 24959-67-90.10 0.060 1
Chloride 147 mg/L 09/22/23 23:25 16887-00-63.0 1.8 3
Fluoride 0.050J mg/L 09/22/23 22:27 16984-48-80.10 0.050 1
Sulfate 26.1 mg/L 09/22/23 22:27 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ08WG-092123 Lab ID: 92689437002 Collected: 09/21/23 10:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 10 Std. Units 10/18/23 15:0010
True Color 350 units 10/18/23 15:00 H350.0 50.0 10
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/04/23 02:40 7440-36-010/02/23 12:1915.0 5.5 1
Arsenic 4.9J ug/L 10/04/23 02:40 7440-38-210/02/23 12:1910.0 3.4 1
Barium 19.0 ug/L 10/04/23 02:40 7440-39-310/02/23 12:1910.0 0.84 1
Beryllium 0.27J ug/L 10/04/23 02:40 7440-41-710/02/23 12:194.0 0.17 1
Boron 67.4 ug/L 10/04/23 02:40 7440-42-810/02/23 12:1950.0 12.4 1
Cadmium ND ug/L 10/04/23 02:40 7440-43-910/02/23 12:191.0 0.33 1
Chromium 10.8 ug/L 10/04/23 02:40 7440-47-310/02/23 12:195.0 1.7 1
Cobalt 3.1J ug/L 10/04/23 02:40 7440-48-410/02/23 12:1910.0 0.96 1
Copper 5.3 ug/L 10/04/23 02:40 7440-50-810/02/23 12:195.0 2.6 1
Lead 7.5J ug/L 10/04/23 02:40 7439-92-110/02/23 12:1910.0 2.1 1
Manganese 48.2 ug/L 10/04/23 02:40 7439-96-510/02/23 12:195.0 1.1 1
Nickel 14.0 ug/L 10/04/23 02:40 7440-02-010/02/23 12:195.0 1.0 1
Selenium ND ug/L 10/04/23 02:40 7782-49-210/02/23 12:1915.0 3.9 1
Silver ND ug/L 10/04/23 02:40 7440-22-410/02/23 12:195.0 1.0 1
Thallium ND ug/L 10/04/23 02:40 7440-28-010/02/23 12:1915.0 2.9 1
Vanadium 38.9 ug/L 10/04/23 02:40 7440-62-210/02/23 12:1910.0 1.0 1
Zinc ND ug/L 10/04/23 02:40 7440-66-610/02/23 12:1920.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/03/23 22:56 7440-36-010/03/23 07:4315.0 5.5 1
Arsenic, Dissolved 4.6J ug/L 10/03/23 22:56 7440-38-210/03/23 07:4310.0 3.4 1
Barium, Dissolved 7.1J ug/L 10/03/23 22:56 7440-39-310/03/23 07:4310.0 0.84 1
Beryllium, Dissolved ND ug/L 10/03/23 22:56 7440-41-710/03/23 07:434.0 0.17 1
Boron, Dissolved 77.9 ug/L 10/03/23 22:56 7440-42-810/03/23 07:4350.0 12.4 1
Cadmium, Dissolved ND ug/L 10/03/23 22:56 7440-43-910/03/23 07:431.0 0.33 1
Chromium, Dissolved 4.3J ug/L 10/03/23 22:56 7440-47-310/03/23 07:435.0 1.7 1
Cobalt, Dissolved 1.2J ug/L 10/03/23 22:56 7440-48-410/03/23 07:4310.0 0.96 1
Copper, Dissolved ND ug/L 10/03/23 22:56 7440-50-810/03/23 07:435.0 2.6 1
Lead, Dissolved ND ug/L 10/03/23 22:56 7439-92-110/03/23 07:4310.0 2.1 1
Manganese, Dissolved 10.5 ug/L 10/03/23 22:56 7439-96-510/03/23 07:435.0 1.1 1
Nickel, Dissolved 6.9 ug/L 10/03/23 22:56 7440-02-010/03/23 07:435.0 1.0 1
Selenium, Dissolved ND ug/L 10/03/23 22:56 7782-49-210/03/23 07:4315.0 3.9 1
Silver, Dissolved ND ug/L 10/03/23 22:56 7440-22-410/03/23 07:435.0 1.0 1
Thallium, Dissolved ND ug/L 10/03/23 22:56 7440-28-0 IS10/03/23 07:4315.0 2.9 1
Vanadium, Dissolved 23.8 ug/L 10/03/23 22:56 7440-62-210/03/23 07:4310.0 1.0 1
Zinc, Dissolved ND ug/L 10/03/23 22:56 7440-66-610/03/23 07:4320.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ08WG-092123 Lab ID: 92689437002 Collected: 09/21/23 10:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury 0.32 ug/L 10/09/23 10:50 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved 0.35 ug/L 10/09/23 12:01 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/26/23 18:59 83-32-909/25/23 17:2610.0 2.0 1
Acenaphthylene ND ug/L 09/26/23 18:59 208-96-809/25/23 17:2610.0 2.0 1
Acetophenone ND ug/L 09/26/23 18:59 98-86-209/25/23 17:2610.0 1.5 1
Anthracene ND ug/L 09/26/23 18:59 120-12-709/25/23 17:2610.0 2.3 1
Atrazine ND ug/L 09/26/23 18:59 1912-24-909/25/23 17:2610.0 3.2 1
Benzaldehyde ND ug/L 09/26/23 18:59 100-52-709/25/23 17:2610.0 3.6 1
Benzo(a)anthracene ND ug/L 09/26/23 18:59 56-55-309/25/23 17:2610.0 2.7 1
Benzo(a)pyrene ND ug/L 09/26/23 18:59 50-32-809/25/23 17:2610.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/26/23 18:59 205-99-209/25/23 17:2610.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/26/23 18:59 191-24-209/25/23 17:2610.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/26/23 18:59 207-08-909/25/23 17:2610.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/26/23 18:59 92-52-409/25/23 17:2610.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/26/23 18:59 101-55-309/25/23 17:2610.0 1.8 1
Butylbenzylphthalate ND ug/L 09/26/23 18:59 85-68-709/25/23 17:2610.0 3.1 1
Caprolactam ND ug/L 09/26/23 18:59 105-60-209/25/23 17:2610.0 6.9 1
Carbazole ND ug/L 09/26/23 18:59 86-74-809/25/23 17:2610.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/26/23 18:59 59-50-709/25/23 17:2610.0 3.3 1
4-Chloroaniline ND ug/L 09/26/23 18:59 106-47-809/25/23 17:2620.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/26/23 18:59 111-91-109/25/23 17:2610.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/26/23 18:59 111-44-409/25/23 17:2610.0 1.9 1
2-Chloronaphthalene ND ug/L 09/26/23 18:59 91-58-709/25/23 17:2610.0 1.7 1
2-Chlorophenol ND ug/L 09/26/23 18:59 95-57-809/25/23 17:2610.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/26/23 18:59 7005-72-309/25/23 17:2610.0 2.0 1
Chrysene ND ug/L 09/26/23 18:59 218-01-909/25/23 17:2610.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/26/23 18:59 53-70-309/25/23 17:2610.0 3.0 1
Dibenzofuran ND ug/L 09/26/23 18:59 132-64-909/25/23 17:2610.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/26/23 18:59 91-94-109/25/23 17:2620.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/26/23 18:59 120-83-209/25/23 17:2610.0 1.4 1
Diethylphthalate ND ug/L 09/26/23 18:59 84-66-209/25/23 17:2610.0 2.0 1
2,4-Dimethylphenol ND ug/L 09/26/23 18:59 105-67-909/25/23 17:2610.0 1.7 1
Dimethylphthalate ND ug/L 09/26/23 18:59 131-11-309/25/23 17:2610.0 2.1 1
Di-n-butylphthalate ND ug/L 09/26/23 18:59 84-74-209/25/23 17:2610.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/26/23 18:59 534-52-109/25/23 17:2620.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/26/23 18:59 51-28-509/25/23 17:2650.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/26/23 18:59 121-14-209/25/23 17:2610.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/26/23 18:59 606-20-209/25/23 17:2610.0 1.7 1
Di-n-octylphthalate ND ug/L 09/26/23 18:59 117-84-009/25/23 17:2610.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ08WG-092123 Lab ID: 92689437002 Collected: 09/21/23 10:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/26/23 18:59 117-81-709/25/23 17:266.0 3.7 1
Fluoranthene ND ug/L 09/26/23 18:59 206-44-009/25/23 17:2610.0 2.2 1
Fluorene ND ug/L 09/26/23 18:59 86-73-709/25/23 17:2610.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/26/23 18:59 87-68-309/25/23 17:2610.0 1.8 1
Hexachlorobenzene ND ug/L 09/26/23 18:59 118-74-109/25/23 17:2610.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/26/23 18:59 77-47-409/25/23 17:2610.0 1.6 1
Hexachloroethane ND ug/L 09/26/23 18:59 67-72-109/25/23 17:2610.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/26/23 18:59 193-39-509/25/23 17:2610.0 2.9 1
Isophorone ND ug/L 09/26/23 18:59 78-59-109/25/23 17:2610.0 1.7 1
2-Methylnaphthalene ND ug/L 09/26/23 18:59 91-57-609/25/23 17:2610.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/26/23 18:59 95-48-709/25/23 17:2610.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/26/23 18:59 15831-10-409/25/23 17:2610.0 1.2 1
Naphthalene 15.1 ug/L 09/26/23 18:59 91-20-309/25/23 17:2610.0 2.1 1
2-Nitroaniline ND ug/L 09/26/23 18:59 88-74-409/25/23 17:2620.0 3.0 1
3-Nitroaniline ND ug/L 09/26/23 18:59 99-09-209/25/23 17:2620.0 3.8 1
4-Nitroaniline ND ug/L 09/26/23 18:59 100-01-609/25/23 17:2620.0 5.1 1
Nitrobenzene ND ug/L 09/26/23 18:59 98-95-309/25/23 17:2610.0 1.9 1
2-Nitrophenol ND ug/L 09/26/23 18:59 88-75-509/25/23 17:2610.0 1.4 1
4-Nitrophenol ND ug/L 09/26/23 18:59 100-02-709/25/23 17:2650.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/26/23 18:59 621-64-709/25/23 17:2610.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/26/23 18:59 86-30-609/25/23 17:2610.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/26/23 18:59 108-60-109/25/23 17:2610.0 1.2 1
Pentachlorophenol ND ug/L 09/26/23 18:59 87-86-509/25/23 17:2620.0 3.8 1
Phenanthrene 2.9J ug/L 09/26/23 18:59 85-01-809/25/23 17:2610.0 2.0 1
Phenol ND ug/L 09/26/23 18:59 108-95-209/25/23 17:2610.0 1.4 1
Pyrene ND ug/L 09/26/23 18:59 129-00-009/25/23 17:2610.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/26/23 18:59 95-95-409/25/23 17:2610.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/26/23 18:59 88-06-209/25/23 17:2610.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)114 %09/26/23 18:59 4165-60-009/25/23 17:2610-138 1
2-Fluorobiphenyl (S)118 %09/26/23 18:59 321-60-809/25/23 17:2610-130 1
Terphenyl-d14 (S)144 %09/26/23 18:59 1718-51-009/25/23 17:2619-191 1
Phenol-d6 (S)59 %09/26/23 18:59 13127-88-309/25/23 17:2610-130 1
2-Fluorophenol (S)85 %09/26/23 18:59 367-12-409/25/23 17:2610-130 1
2,4,6-Tribromophenol (S)151 %09/26/23 18:59 118-79-609/25/23 17:2610-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/01/23 10:03 67-64-125.0 5.1 1
Benzene 0.50J ug/L 10/01/23 10:03 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 10/01/23 10:03 75-27-41.0 0.31 1
Bromoform ND ug/L 10/01/23 10:03 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/01/23 10:03 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/01/23 10:03 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/01/23 10:03 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ08WG-092123 Lab ID: 92689437002 Collected: 09/21/23 10:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 10/01/23 10:03 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/01/23 10:03 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/01/23 10:03 75-00-31.0 0.65 1
Chloroform ND ug/L 10/01/23 10:03 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/01/23 10:03 74-87-31.0 0.54 1
Cyclohexane ND ug/L 10/01/23 10:03 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 10/01/23 10:03 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/01/23 10:03 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/01/23 10:03 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 10/01/23 10:03 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/01/23 10:03 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/01/23 10:03 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/01/23 10:03 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/01/23 10:03 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/01/23 10:03 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/01/23 10:03 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/01/23 10:03 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/01/23 10:03 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/01/23 10:03 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/01/23 10:03 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/01/23 10:03 10061-02-61.0 0.36 1
Ethylbenzene 87.0 ug/L 10/01/23 10:03 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/01/23 10:03 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)1.7 ug/L 10/01/23 10:03 98-82-81.0 0.33 1
Methyl acetate ND ug/L 10/01/23 10:03 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 10/01/23 10:03 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 10/01/23 10:03 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/01/23 10:03 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/01/23 10:03 1634-04-41.0 0.42 1
Styrene ND ug/L 10/01/23 10:03 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 10/01/23 10:03 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/01/23 10:03 127-18-41.0 0.29 1
Toluene 3.2 ug/L 10/01/23 10:03 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 10/01/23 10:03 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/01/23 10:03 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/01/23 10:03 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/01/23 10:03 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/01/23 10:03 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 10/01/23 10:03 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 10/01/23 10:03 75-01-41.0 0.39 1
m&p-Xylene 333 ug/L 10/01/23 10:03 179601-23-12.0 0.71 1
o-Xylene 106 ug/L 10/01/23 10:03 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %10/01/23 10:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %10/01/23 10:03 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: PZ08WG-092123 Lab ID: 92689437002 Collected: 09/21/23 10:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)98 %10/01/23 10:03 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 1550 mg/L 10/05/23 12:025.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide 5.2 mg/L 09/27/23 01:46 18496-25-81.0 0.22 10
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Bromide 0.35 mg/L 09/22/23 22:42 24959-67-90.10 0.060 1
Chloride 2670 mg/L 09/22/23 23:39 16887-00-6100 60.0 100
Fluoride 0.14 mg/L 09/22/23 22:42 16984-48-80.10 0.050 1
Sulfate 175 mg/L 09/22/23 23:39 14808-79-8100 50.0 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: EB02WQ-092123 Lab ID: 92689437003 Collected: 09/21/23 11:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 4.8 Std. Units 10/18/23 15:011
True Color ND units 10/18/23 15:01 H35.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Antimony ND ug/L 10/04/23 02:51 7440-36-010/02/23 12:1915.0 5.5 1
Arsenic ND ug/L 10/04/23 02:51 7440-38-210/02/23 12:1910.0 3.4 1
Barium ND ug/L 10/04/23 02:51 7440-39-310/02/23 12:1910.0 0.84 1
Beryllium ND ug/L 10/04/23 02:51 7440-41-710/02/23 12:194.0 0.17 1
Boron ND ug/L 10/04/23 02:51 7440-42-810/02/23 12:1950.0 12.4 1
Cadmium ND ug/L 10/04/23 02:51 7440-43-910/02/23 12:191.0 0.33 1
Chromium ND ug/L 10/04/23 02:51 7440-47-310/02/23 12:195.0 1.7 1
Cobalt ND ug/L 10/04/23 02:51 7440-48-410/02/23 12:1910.0 0.96 1
Copper ND ug/L 10/04/23 02:51 7440-50-810/02/23 12:195.0 2.6 1
Lead ND ug/L 10/04/23 02:51 7439-92-110/02/23 12:1910.0 2.1 1
Manganese ND ug/L 10/04/23 02:51 7439-96-510/02/23 12:195.0 1.1 1
Nickel ND ug/L 10/04/23 02:51 7440-02-010/02/23 12:195.0 1.0 1
Selenium ND ug/L 10/04/23 02:51 7782-49-210/02/23 12:1915.0 3.9 1
Silver ND ug/L 10/04/23 02:51 7440-22-410/02/23 12:195.0 1.0 1
Thallium ND ug/L 10/04/23 02:51 7440-28-010/02/23 12:1915.0 2.9 1
Vanadium ND ug/L 10/04/23 02:51 7440-62-210/02/23 12:1910.0 1.0 1
Zinc ND ug/L 10/04/23 02:51 7440-66-610/02/23 12:1920.0 11.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP, Dissolved
Antimony, Dissolved ND ug/L 10/03/23 22:59 7440-36-010/03/23 07:4315.0 5.5 1
Arsenic, Dissolved ND ug/L 10/03/23 22:59 7440-38-210/03/23 07:4310.0 3.4 1
Barium, Dissolved ND ug/L 10/03/23 22:59 7440-39-310/03/23 07:4310.0 0.84 1
Beryllium, Dissolved ND ug/L 10/03/23 22:59 7440-41-710/03/23 07:434.0 0.17 1
Boron, Dissolved ND ug/L 10/03/23 22:59 7440-42-810/03/23 07:4350.0 12.4 1
Cadmium, Dissolved ND ug/L 10/03/23 22:59 7440-43-910/03/23 07:431.0 0.33 1
Chromium, Dissolved ND ug/L 10/03/23 22:59 7440-47-310/03/23 07:435.0 1.7 1
Cobalt, Dissolved ND ug/L 10/03/23 22:59 7440-48-410/03/23 07:4310.0 0.96 1
Copper, Dissolved ND ug/L 10/03/23 22:59 7440-50-810/03/23 07:435.0 2.6 1
Lead, Dissolved ND ug/L 10/03/23 22:59 7439-92-110/03/23 07:4310.0 2.1 1
Manganese, Dissolved ND ug/L 10/03/23 22:59 7439-96-510/03/23 07:435.0 1.1 1
Nickel, Dissolved ND ug/L 10/03/23 22:59 7440-02-010/03/23 07:435.0 1.0 1
Selenium, Dissolved ND ug/L 10/03/23 22:59 7782-49-210/03/23 07:4315.0 3.9 1
Silver, Dissolved ND ug/L 10/03/23 22:59 7440-22-410/03/23 07:435.0 1.0 1
Thallium, Dissolved ND ug/L 10/03/23 22:59 7440-28-010/03/23 07:4315.0 2.9 1
Vanadium, Dissolved ND ug/L 10/03/23 22:59 7440-62-210/03/23 07:4310.0 1.0 1
Zinc, Dissolved ND ug/L 10/03/23 22:59 7440-66-610/03/23 07:4320.0 11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: EB02WQ-092123 Lab ID: 92689437003 Collected: 09/21/23 11:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/09/23 10:52 7439-97-610/05/23 10:340.20 0.14 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/09/23 12:03 7439-97-610/05/23 11:370.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/26/23 18:33 83-32-909/25/23 17:268.3 1.7 1
Acenaphthylene ND ug/L 09/26/23 18:33 208-96-809/25/23 17:268.3 1.6 1
Acetophenone ND ug/L 09/26/23 18:33 98-86-209/25/23 17:268.3 1.2 1
Anthracene ND ug/L 09/26/23 18:33 120-12-709/25/23 17:268.3 1.9 1
Atrazine ND ug/L 09/26/23 18:33 1912-24-909/25/23 17:268.3 2.6 1
Benzaldehyde ND ug/L 09/26/23 18:33 100-52-709/25/23 17:268.3 3.0 1
Benzo(a)anthracene ND ug/L 09/26/23 18:33 56-55-309/25/23 17:268.3 2.2 1
Benzo(a)pyrene ND ug/L 09/26/23 18:33 50-32-809/25/23 17:268.3 2.3 1
Benzo(b)fluoranthene ND ug/L 09/26/23 18:33 205-99-209/25/23 17:268.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 09/26/23 18:33 191-24-209/25/23 17:268.3 2.4 1
Benzo(k)fluoranthene ND ug/L 09/26/23 18:33 207-08-909/25/23 17:268.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 09/26/23 18:33 92-52-409/25/23 17:268.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 09/26/23 18:33 101-55-309/25/23 17:268.3 1.5 1
Butylbenzylphthalate ND ug/L 09/26/23 18:33 85-68-709/25/23 17:268.3 2.6 1
Caprolactam ND ug/L 09/26/23 18:33 105-60-209/25/23 17:268.3 5.8 1
Carbazole ND ug/L 09/26/23 18:33 86-74-809/25/23 17:268.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/26/23 18:33 59-50-709/25/23 17:268.3 2.8 1
4-Chloroaniline ND ug/L 09/26/23 18:33 106-47-809/25/23 17:2616.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/26/23 18:33 111-91-109/25/23 17:268.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 09/26/23 18:33 111-44-409/25/23 17:268.3 1.6 1
2-Chloronaphthalene ND ug/L 09/26/23 18:33 91-58-709/25/23 17:268.3 1.4 1
2-Chlorophenol ND ug/L 09/26/23 18:33 95-57-809/25/23 17:268.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/26/23 18:33 7005-72-309/25/23 17:268.3 1.7 1
Chrysene ND ug/L 09/26/23 18:33 218-01-909/25/23 17:268.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 09/26/23 18:33 53-70-309/25/23 17:268.3 2.5 1
Dibenzofuran ND ug/L 09/26/23 18:33 132-64-909/25/23 17:268.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/26/23 18:33 91-94-109/25/23 17:2616.7 6.8 1
2,4-Dichlorophenol ND ug/L 09/26/23 18:33 120-83-209/25/23 17:268.3 1.2 1
Diethylphthalate ND ug/L 09/26/23 18:33 84-66-209/25/23 17:268.3 1.7 1
2,4-Dimethylphenol ND ug/L 09/26/23 18:33 105-67-909/25/23 17:268.3 1.4 1
Dimethylphthalate ND ug/L 09/26/23 18:33 131-11-309/25/23 17:268.3 1.8 1
Di-n-butylphthalate ND ug/L 09/26/23 18:33 84-74-209/25/23 17:268.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/26/23 18:33 534-52-109/25/23 17:2616.7 6.5 1
2,4-Dinitrophenol ND ug/L 09/26/23 18:33 51-28-509/25/23 17:2641.7 21.7 1
2,4-Dinitrotoluene ND ug/L 09/26/23 18:33 121-14-209/25/23 17:268.3 1.4 1
2,6-Dinitrotoluene ND ug/L 09/26/23 18:33 606-20-209/25/23 17:268.3 1.4 1
Di-n-octylphthalate ND ug/L 09/26/23 18:33 117-84-009/25/23 17:268.3 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: EB02WQ-092123 Lab ID: 92689437003 Collected: 09/21/23 11:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
bis(2-Ethylhexyl)phthalate ND ug/L 09/26/23 18:33 117-81-709/25/23 17:265.0 3.1 1
Fluoranthene ND ug/L 09/26/23 18:33 206-44-009/25/23 17:268.3 1.8 1
Fluorene ND ug/L 09/26/23 18:33 86-73-709/25/23 17:268.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 09/26/23 18:33 87-68-309/25/23 17:268.3 1.5 1
Hexachlorobenzene ND ug/L 09/26/23 18:33 118-74-109/25/23 17:268.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 09/26/23 18:33 77-47-409/25/23 17:268.3 1.3 1
Hexachloroethane ND ug/L 09/26/23 18:33 67-72-109/25/23 17:268.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/26/23 18:33 193-39-509/25/23 17:268.3 2.4 1
Isophorone ND ug/L 09/26/23 18:33 78-59-109/25/23 17:268.3 1.4 1
2-Methylnaphthalene ND ug/L 09/26/23 18:33 91-57-609/25/23 17:268.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/26/23 18:33 95-48-709/25/23 17:268.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/26/23 18:33 15831-10-409/25/23 17:268.3 1.0 1
Naphthalene ND ug/L 09/26/23 18:33 91-20-309/25/23 17:268.3 1.7 1
2-Nitroaniline ND ug/L 09/26/23 18:33 88-74-409/25/23 17:2616.7 2.5 1
3-Nitroaniline ND ug/L 09/26/23 18:33 99-09-209/25/23 17:2616.7 3.1 1
4-Nitroaniline ND ug/L 09/26/23 18:33 100-01-609/25/23 17:2616.7 4.2 1
Nitrobenzene ND ug/L 09/26/23 18:33 98-95-309/25/23 17:268.3 1.6 1
2-Nitrophenol ND ug/L 09/26/23 18:33 88-75-509/25/23 17:268.3 1.2 1
4-Nitrophenol ND ug/L 09/26/23 18:33 100-02-709/25/23 17:2641.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 09/26/23 18:33 621-64-709/25/23 17:268.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 09/26/23 18:33 86-30-609/25/23 17:268.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/26/23 18:33 108-60-109/25/23 17:268.3 0.96 1
Pentachlorophenol ND ug/L 09/26/23 18:33 87-86-509/25/23 17:2616.7 3.1 1
Phenanthrene ND ug/L 09/26/23 18:33 85-01-809/25/23 17:268.3 1.7 1
Phenol ND ug/L 09/26/23 18:33 108-95-209/25/23 17:268.3 1.1 1
Pyrene ND ug/L 09/26/23 18:33 129-00-009/25/23 17:268.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 09/26/23 18:33 95-95-409/25/23 17:268.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/26/23 18:33 88-06-209/25/23 17:268.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)106 %09/26/23 18:33 4165-60-009/25/23 17:2610-138 1
2-Fluorobiphenyl (S)105 %09/26/23 18:33 321-60-809/25/23 17:2610-130 1
Terphenyl-d14 (S)160 %09/26/23 18:33 1718-51-009/25/23 17:2619-191 1
Phenol-d6 (S)54 %09/26/23 18:33 13127-88-309/25/23 17:2610-130 1
2-Fluorophenol (S)70 %09/26/23 18:33 367-12-409/25/23 17:2610-130 1
2,4,6-Tribromophenol (S)143 %09/26/23 18:33 118-79-609/25/23 17:2610-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/29/23 21:40 67-64-125.0 5.1 1
Benzene ND ug/L 09/29/23 21:40 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/29/23 21:40 75-27-41.0 0.31 1
Bromoform ND ug/L 09/29/23 21:40 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/29/23 21:40 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/29/23 21:40 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/29/23 21:40 75-15-02.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: EB02WQ-092123 Lab ID: 92689437003 Collected: 09/21/23 11:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 09/29/23 21:40 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/29/23 21:40 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/29/23 21:40 75-00-31.0 0.65 1
Chloroform ND ug/L 09/29/23 21:40 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/29/23 21:40 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/29/23 21:40 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/23 21:40 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/29/23 21:40 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/23 21:40 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/29/23 21:40 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/29/23 21:40 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/29/23 21:40 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/29/23 21:40 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/29/23 21:40 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/29/23 21:40 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/29/23 21:40 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/29/23 21:40 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/29/23 21:40 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/29/23 21:40 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/29/23 21:40 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/29/23 21:40 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/29/23 21:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/29/23 21:40 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/29/23 21:40 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/29/23 21:40 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/29/23 21:40 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/29/23 21:40 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/29/23 21:40 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/29/23 21:40 1634-04-41.0 0.42 1
Styrene ND ug/L 09/29/23 21:40 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/23 21:40 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/29/23 21:40 127-18-41.0 0.29 1
Toluene ND ug/L 09/29/23 21:40 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/29/23 21:40 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/29/23 21:40 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/29/23 21:40 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/29/23 21:40 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/29/23 21:40 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 09/29/23 21:40 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/29/23 21:40 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/29/23 21:40 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/29/23 21:40 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %09/29/23 21:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %09/29/23 21:40 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Sample: EB02WQ-092123 Lab ID: 92689437003 Collected: 09/21/23 11:05 Received: 09/22/23 08:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
SurrogatesToluene-d8 (S)101 %09/29/23 21:40 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 ND mg/L 10/05/23 12:175.0 5.0 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND mg/L 09/27/23 01:47 18496-25-80.10 0.022 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Bromide ND mg/L 09/22/23 22:56 24959-67-90.10 0.060 1
Chloride ND mg/L 09/22/23 22:56 16887-00-61.0 0.60 1
Fluoride ND mg/L 09/22/23 22:56 16984-48-80.10 0.050 1
Sulfate ND mg/L 09/22/23 22:56 14808-79-81.0 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807305
SM 2120B-2011
SM 2120B-2011
2120B True Color EDEN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples: 92689437001, 92689437002, 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4180390
Associated Lab Samples:92689437001, 92689437002, 92689437003
Matrix: Water
AnalyzedMDL
True Color units ND 5.0 10/18/23 14:545.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4180391LABORATORY CONTROL SAMPLE:
LCSSpike
True Color units 35.035 100 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689437001
4180392SAMPLE DUPLICATE:
pH Std. Units 6.4 0 106.4
True Color units ND H310ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
955304
EPA 7470
EPA 7470
7470 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92689437001, 92689437002, 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5252836
Associated Lab Samples:92689437001, 92689437002, 92689437003
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/09/23 09:320.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5252837LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.12 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5252838MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5252839
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 99 75-12596 3 202ND2.1 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
955306
EPA 7470
EPA 7470
7470 Mercury Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92689437001, 92689437002, 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5252843
Associated Lab Samples:92689437001, 92689437002, 92689437003
Matrix: Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/09/23 11:080.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5252844LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.12 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5252845MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688066005
5252846
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2 100 85-11598 2 202ND2.0 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954422
EPA 3010
EPA 6010
6010 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92689437001, 92689437002, 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5248196
Associated Lab Samples:92689437001, 92689437002, 92689437003
Matrix: Water
AnalyzedMDL
Antimony ug/L ND 15.0 10/04/23 01:055.5
Arsenic ug/L ND 10.0 10/04/23 01:053.4
Barium ug/L ND 10.0 10/04/23 01:050.84
Beryllium ug/L ND 4.0 10/04/23 01:050.17
Boron ug/L ND 50.0 10/04/23 01:0512.4
Cadmium ug/L ND 1.0 10/04/23 01:050.33
Chromium ug/L ND 5.0 10/04/23 01:051.7
Cobalt ug/L ND 10.0 10/04/23 01:050.96
Copper ug/L ND 5.0 10/04/23 01:052.6
Lead ug/L ND 10.0 10/04/23 01:052.1
Manganese ug/L ND 5.0 10/04/23 01:051.1
Nickel ug/L ND 5.0 10/04/23 01:051.0
Selenium ug/L ND 15.0 10/04/23 01:053.9
Silver ug/L ND 5.0 10/04/23 01:051.0
Thallium ug/L ND 15.0 10/04/23 01:052.9
Vanadium ug/L ND 10.0 10/04/23 01:051.0
Zinc ug/L ND 20.0 10/04/23 01:0511.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5248197LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 252250 101 80-120
Arsenic ug/L 240250 96 80-120
Barium ug/L 257250 103 80-120
Beryllium ug/L 25.025 100 80-120
Boron ug/L 12501250 100 80-120
Cadmium ug/L 25.125 100 80-120
Chromium ug/L 253250 101 80-120
Cobalt ug/L 254250 102 80-120
Copper ug/L 253250 101 80-120
Lead ug/L 258250 103 80-120
Manganese ug/L 251250 100 80-120
Nickel ug/L 256250 102 80-120
Selenium ug/L 253250 101 80-120
Silver ug/L 24.225 97 80-120
Thallium ug/L 238250 95 80-120
Vanadium ug/L 252250 101 80-120
Zinc ug/L 12401250 99 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5248198MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35830363001
5248199
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 250 100 75-125101 1 202505.5U 252 255
Arsenic ug/L 250 96 75-12597 1 202503.4U 241 243
Barium ug/L 250 103 75-125102 1 202500.84U 258 255
Beryllium ug/L 25 101 75-125102 1 20250.17U 25.2 25.4
Boron ug/L 1250 100 75-12599 0 20125020.4J 1270 1260
Cadmium ug/L 25 100 75-125100 1 20250.48J 25.4 25.6
Chromium ug/L 250 101 75-125100 1 202501.7U 253 252
Cobalt ug/L 250 101 75-125102 1 202500.96U 253 255
Copper ug/L 250 102 75-125101 1 202502.6U 254 252
Lead ug/L 250 102 75-125103 1 202502.1U 257 259
Manganese ug/L 250 101 75-125100 0 202502.4J 254 253
Nickel ug/L 250 102 75-125103 1 202501.0U 256 257
Selenium ug/L 250 101 75-125101 1 202503.9U 254 255
Silver ug/L 25 97 75-12598 1 20251.0U 24.1 24.4
Thallium ug/L 250 94 75-12596 1 202504.0J 240 243
Vanadium ug/L 250 101 75-125101 1 202503.4J 257 255
Zinc ug/L 1250 99 75-12599 0 20125011.0U 1230 1240
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954621
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92689437001, 92689437002, 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5249505
Associated Lab Samples:92689437001, 92689437002, 92689437003
Matrix: Water
AnalyzedMDL
Antimony, Dissolved ug/L ND 15.0 10/03/23 20:005.5
Arsenic, Dissolved ug/L ND 10.0 10/04/23 01:413.4
Barium, Dissolved ug/L ND 10.0 10/04/23 01:410.84
Beryllium, Dissolved ug/L ND 4.0 10/04/23 01:410.17
Boron, Dissolved ug/L ND 50.0 10/04/23 01:4112.4
Cadmium, Dissolved ug/L ND 1.0 10/04/23 01:410.33
Chromium, Dissolved ug/L ND 5.0 10/04/23 01:411.7
Cobalt, Dissolved ug/L ND 10.0 10/04/23 01:410.96
Copper, Dissolved ug/L ND 5.0 10/04/23 01:412.6
Lead, Dissolved ug/L ND 10.0 10/04/23 01:412.1
Manganese, Dissolved ug/L ND 5.0 10/04/23 01:411.1
Nickel, Dissolved ug/L ND 5.0 10/04/23 01:411.0
Selenium, Dissolved ug/L ND 15.0 10/04/23 01:413.9
Silver, Dissolved ug/L ND 5.0 10/04/23 01:411.0
Thallium, Dissolved ug/L ND 15.0 10/04/23 01:412.9
Vanadium, Dissolved ug/L ND 10.0 10/04/23 01:411.0
Zinc, Dissolved ug/L ND 20.0 10/04/23 01:4111.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5249506LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 238250 95 80-120
Arsenic, Dissolved ug/L 243250 97 80-120
Barium, Dissolved ug/L 242250 97 80-120
Beryllium, Dissolved ug/L 24.325 97 80-120
Boron, Dissolved ug/L 12101250 97 80-120
Cadmium, Dissolved ug/L 26.225 105 80-120
Chromium, Dissolved ug/L 245250 98 80-120
Cobalt, Dissolved ug/L 250250 100 80-120
Copper, Dissolved ug/L 234250 93 80-120
Lead, Dissolved ug/L 254250 102 80-120
Manganese, Dissolved ug/L 244250 97 80-120
Nickel, Dissolved ug/L 256250 102 80-120
Selenium, Dissolved ug/L 252250 101 80-120
Silver, Dissolved ug/L 24.025 96 80-120
Thallium, Dissolved ug/L 251250 100 80-120
Vanadium, Dissolved ug/L 242250 97 80-120
Zinc, Dissolved ug/L 13001250 104 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5249507MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35830912003
5249508
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 250 90 75-12591 1 202505.5U 226 229
Arsenic, Dissolved ug/L 250 96 75-12597 0 202503.4U 240 241
Barium, Dissolved ug/L 250 96 75-12595 0 2025018.5 258 257
Beryllium, Dissolved ug/L 25 96 75-12597 1 20250.17U 24.1 24.3
Boron, Dissolved ug/L 1250 97 75-12598 1 20125037.2J 1250 1260
Cadmium, Dissolved ug/L 25 99 75-125100 1 20250.48J 25.3 25.6
Chromium, Dissolved ug/L 250 96 75-12597 1 202502.1J 242 244
Cobalt, Dissolved ug/L 250 98 75-12599 1 202500.96U 246 248
Copper, Dissolved ug/L 250 95 75-12596 1 202502.6U 239 241
Lead, Dissolved ug/L 250 99 75-125100 1 202504.3J 252 256
Manganese, Dissolved ug/L 250 95 75-12596 1 2025025.8 264 265
Nickel, Dissolved ug/L 250 99 75-125100 1 202501.0U 249 251
Selenium, Dissolved ug/L 250 86 75-12586 0 202503.9U 214 215
Silver, Dissolved ug/L 25 96 75-12597 1 20251.0U 24.9 25.3
Thallium, Dissolved ug/L 250 97 75-12598 1 202502.9U 244 246
Vanadium, Dissolved ug/L 250 96 75-12597 1 202502.1J 243 245
Zinc, Dissolved ug/L 1250 99 75-125100 1 20125011.0U 1240 1250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802720
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689437001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4157710
Associated Lab Samples:92689437001
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 10/01/23 01:510.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/01/23 01:510.22
1,1,2-Trichloroethane ug/L ND 1.0 10/01/23 01:510.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 10/01/23 01:510.32
1,1-Dichloroethane ug/L ND 1.0 10/01/23 01:510.37
1,1-Dichloroethene ug/L ND 1.0 10/01/23 01:510.35
1,2,4-Trichlorobenzene ug/L ND 1.0 10/01/23 01:510.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/01/23 01:510.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/01/23 01:510.27
1,2-Dichlorobenzene ug/L ND 1.0 10/01/23 01:510.34
1,2-Dichloroethane ug/L ND 1.0 10/01/23 01:510.32
1,2-Dichloropropane ug/L ND 1.0 10/01/23 01:510.36
1,3-Dichlorobenzene ug/L ND 1.0 10/01/23 01:510.34
1,4-Dichlorobenzene ug/L ND 1.0 10/01/23 01:510.33
2-Butanone (MEK)ug/L ND 5.0 10/01/23 01:514.0
2-Hexanone ug/L ND 5.0 10/01/23 01:510.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/01/23 01:512.7
Acetone ug/L ND 25.0 10/01/23 01:515.1
Benzene ug/L ND 1.0 10/01/23 01:510.34
Bromodichloromethane ug/L ND 1.0 10/01/23 01:510.31
Bromoform ug/L ND 1.0 10/01/23 01:510.34
Bromomethane ug/L ND 2.0 10/01/23 01:511.7
Carbon disulfide ug/L ND 2.0 10/01/23 01:510.36
Carbon tetrachloride ug/L ND 1.0 10/01/23 01:510.33
Chlorobenzene ug/L ND 1.0 10/01/23 01:510.28
Chloroethane ug/L ND 1.0 10/01/23 01:510.65
Chloroform ug/L ND 1.0 10/01/23 01:510.43
Chloromethane ug/L ND 1.0 10/01/23 01:510.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/01/23 01:510.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/01/23 01:510.36
Cyclohexane ug/L ND 1.0 10/01/23 01:510.35
Dibromochloromethane ug/L ND 1.0 10/01/23 01:510.36
Dichlorodifluoromethane ug/L ND 1.0 v110/01/23 01:510.35
Ethylbenzene ug/L ND 1.0 10/01/23 01:510.30
Isopropylbenzene (Cumene)ug/L ND 1.0 10/01/23 01:510.33
m&p-Xylene ug/L ND 2.0 10/01/23 01:510.71
Methyl acetate ug/L ND 10.0 10/01/23 01:512.4
Methyl-tert-butyl ether ug/L ND 1.0 10/01/23 01:510.42
Methylcyclohexane ug/L ND 10.0 10/01/23 01:511.5
Methylene Chloride ug/L ND 5.0 10/01/23 01:512.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4157710
Associated Lab Samples:92689437001
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 10/01/23 01:510.34
Styrene ug/L ND 1.0 10/01/23 01:510.29
Tetrachloroethene ug/L ND 1.0 10/01/23 01:510.29
Toluene ug/L ND 1.0 10/01/23 01:510.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/01/23 01:510.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/01/23 01:510.36
Trichloroethene ug/L ND 1.0 10/01/23 01:510.38
Trichlorofluoromethane ug/L ND 1.0 10/01/23 01:510.30
Vinyl chloride ug/L ND 1.0 10/01/23 01:510.39
1,2-Dichloroethane-d4 (S)%105 70-130 10/01/23 01:51
4-Bromofluorobenzene (S)%100 70-130 10/01/23 01:51
Toluene-d8 (S)%100 70-130 10/01/23 01:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157711LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.320 102 70-130
1,1,2,2-Tetrachloroethane ug/L 20.220 101 70-130
1,1,2-Trichloroethane ug/L 20.020 100 70-130
1,1,2-Trichlorotrifluoroethane ug/L 23.120 115 70-132
1,1-Dichloroethane ug/L 22.320 111 70-130
1,1-Dichloroethene ug/L 22.920 115 69-131
1,2,4-Trichlorobenzene ug/L 21.320 107 70-130
1,2-Dibromo-3-chloropropane ug/L 19.020 95 70-130
1,2-Dibromoethane (EDB)ug/L 21.120 105 70-130
1,2-Dichlorobenzene ug/L 22.120 110 70-130
1,2-Dichloroethane ug/L 22.520 113 70-130
1,2-Dichloropropane ug/L 22.020 110 70-130
1,3-Dichlorobenzene ug/L 22.220 111 70-130
1,4-Dichlorobenzene ug/L 21.920 109 70-130
2-Butanone (MEK)ug/L 37.940 95 67-133
2-Hexanone ug/L 38.640 97 70-133
4-Methyl-2-pentanone (MIBK)ug/L 39.140 98 70-130
Acetone ug/L 40.140 100 67-130
Benzene ug/L 21.520 107 70-130
Bromodichloromethane ug/L 19.120 96 70-130
Bromoform ug/L 19.820 99 70-133
Bromomethane ug/L 19.220 96 41-148
Carbon disulfide ug/L 23.720 118 70-131
Carbon tetrachloride ug/L 21.120 106 70-130
Chlorobenzene ug/L 21.520 107 70-130
Chloroethane ug/L 20.720 103 41-157
Chloroform ug/L 21.720 108 70-130
Chloromethane ug/L 20.620 103 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157711LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 22.620 113 70-130
cis-1,3-Dichloropropene ug/L 21.120 105 70-130
Cyclohexane ug/L 22.020 110 63-137
Dibromochloromethane ug/L 21.020 105 70-130
Dichlorodifluoromethane ug/L 27.1 v120136 54-147
Ethylbenzene ug/L 21.020 105 70-130
Isopropylbenzene (Cumene)ug/L 21.920 110 70-130
m&p-Xylene ug/L 43.340 108 70-130
Methyl acetate ug/L 19.320 97 70-130
Methyl-tert-butyl ether ug/L 20.720 103 70-130
Methylcyclohexane ug/L 22.520 112 70-130
Methylene Chloride ug/L 22.220 111 62-130
o-Xylene ug/L 21.520 108 70-130
Styrene ug/L 21.720 108 70-130
Tetrachloroethene ug/L 19.420 97 70-130
Toluene ug/L 21.320 106 70-130
trans-1,2-Dichloroethene ug/L 21.420 107 70-130
trans-1,3-Dichloropropene ug/L 20.920 105 70-130
Trichloroethene ug/L 21.220 106 70-130
Trichlorofluoromethane ug/L 22.120 110 57-130
Vinyl chloride ug/L 19.820 99 66-140
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4157712MATRIX SPIKE SAMPLE:
MSSpike
Result
92689386003
1,1,1-Trichloroethane ug/L 24.420 122 70-150ND
1,1,2,2-Tetrachloroethane ug/L 22.620 113 66-144ND
1,1,2-Trichloroethane ug/L 22.420 112 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 23.120 116 66-168ND
1,1-Dichloroethane ug/L 22.620 113 68-150ND
1,1-Dichloroethene ug/L 23.120 116 64-162ND
1,2,4-Trichlorobenzene ug/L 23.920 120 69-147ND
1,2-Dibromo-3-chloropropane ug/L 23.520 117 62-146ND
1,2-Dibromoethane (EDB)ug/L 22.720 113 70-143ND
1,2-Dichlorobenzene ug/L 22.920 114 70-142ND
1,2-Dichloroethane ug/L 22.120 110 68-145ND
1,2-Dichloropropane ug/L 22.820 114 70-144ND
1,3-Dichlorobenzene ug/L 21.820 109 70-142ND
1,4-Dichlorobenzene ug/L 22.220 111 70-140ND
2-Butanone (MEK)ug/L 45.040 113 57-156ND
2-Hexanone ug/L 47.140 118 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 44.540 111 65-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4157712MATRIX SPIKE SAMPLE:
MSSpike
Result
92689386003
Acetone ug/L 42.740 107 49-162ND
Benzene ug/L 22.520 113 68-144ND
Bromodichloromethane ug/L 22.220 111 70-141ND
Bromoform ug/L 22.720 114 59-144ND
Bromomethane ug/L 19.6 v32098 23-190ND
Carbon disulfide ug/L 23.420 117 64-160ND
Carbon tetrachloride ug/L 24.820 124 70-147ND
Chlorobenzene ug/L 22.120 111 70-143ND
Chloroethane ug/L 22.020 110 55-190ND
Chloroform ug/L 22.920 115 67-148ND
Chloromethane ug/L 21.320 106 38-180ND
cis-1,2-Dichloroethene ug/L 22.220 111 67-151ND
cis-1,3-Dichloropropene ug/L 21.820 109 70-142ND
Cyclohexane ug/L 22.720 113 64-162ND
Dibromochloromethane ug/L 23.020 115 68-140ND
Dichlorodifluoromethane ug/L 28.020 140 15-200ND
Ethylbenzene ug/L 22.720 114 70-145ND
Isopropylbenzene (Cumene)ug/L 24.020 120 70-144ND
m&p-Xylene ug/L 46.240 116 70-148ND
Methyl acetate ug/L 20.320 102 62-144ND
Methyl-tert-butyl ether ug/L 21.420 107 64-146ND
Methylcyclohexane ug/L 24.420 122 70-155ND
Methylene Chloride ug/L 21.220 106 54-149ND
o-Xylene ug/L 22.620 113 70-145ND
Styrene ug/L 22.520 112 70-147ND
Tetrachloroethene ug/L 22.320 111 70-145ND
Toluene ug/L 22.420 112 65-146ND
trans-1,2-Dichloroethene ug/L 22.920 115 69-155ND
trans-1,3-Dichloropropene ug/L 22.820 114 70-142ND
Trichloroethene ug/L 23.120 115 70-152ND
Trichlorofluoromethane ug/L 23.320 117 60-158ND
Vinyl chloride ug/L 20.020 100 51-178ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689386004
4157713SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689386004
4157713SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%101106
4-Bromofluorobenzene (S)%98100
Toluene-d8 (S)%99100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802723
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4157732
Associated Lab Samples:92689437003
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/29/23 21:050.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/29/23 21:050.22
1,1,2-Trichloroethane ug/L ND 1.0 09/29/23 21:050.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/29/23 21:050.32
1,1-Dichloroethane ug/L ND 1.0 09/29/23 21:050.37
1,1-Dichloroethene ug/L ND 1.0 09/29/23 21:050.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/29/23 21:050.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/29/23 21:050.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/29/23 21:050.27
1,2-Dichlorobenzene ug/L ND 1.0 09/29/23 21:050.34
1,2-Dichloroethane ug/L ND 1.0 09/29/23 21:050.32
1,2-Dichloropropane ug/L ND 1.0 09/29/23 21:050.36
1,3-Dichlorobenzene ug/L ND 1.0 09/29/23 21:050.34
1,4-Dichlorobenzene ug/L ND 1.0 09/29/23 21:050.33
2-Butanone (MEK)ug/L ND 5.0 09/29/23 21:054.0
2-Hexanone ug/L ND 5.0 09/29/23 21:050.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/29/23 21:052.7
Acetone ug/L ND 25.0 09/29/23 21:055.1
Benzene ug/L ND 1.0 09/29/23 21:050.34
Bromodichloromethane ug/L ND 1.0 09/29/23 21:050.31
Bromoform ug/L ND 1.0 09/29/23 21:050.34
Bromomethane ug/L ND 2.0 v209/29/23 21:051.7
Carbon disulfide ug/L ND 2.0 09/29/23 21:050.36
Carbon tetrachloride ug/L ND 1.0 09/29/23 21:050.33
Chlorobenzene ug/L ND 1.0 09/29/23 21:050.28
Chloroethane ug/L ND 1.0 09/29/23 21:050.65
Chloroform ug/L ND 1.0 09/29/23 21:050.43
Chloromethane ug/L ND 1.0 09/29/23 21:050.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/29/23 21:050.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/29/23 21:050.36
Cyclohexane ug/L ND 1.0 09/29/23 21:050.35
Dibromochloromethane ug/L ND 1.0 09/29/23 21:050.36
Dichlorodifluoromethane ug/L ND 1.0 09/29/23 21:050.35
Ethylbenzene ug/L ND 1.0 09/29/23 21:050.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/29/23 21:050.33
m&p-Xylene ug/L ND 2.0 09/29/23 21:050.71
Methyl acetate ug/L ND 10.0 09/29/23 21:052.4
Methyl-tert-butyl ether ug/L ND 1.0 09/29/23 21:050.42
Methylcyclohexane ug/L ND 10.0 09/29/23 21:051.5
Methylene Chloride ug/L ND 5.0 09/29/23 21:052.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4157732
Associated Lab Samples:92689437003
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/29/23 21:050.34
Styrene ug/L ND 1.0 09/29/23 21:050.29
Tetrachloroethene ug/L ND 1.0 09/29/23 21:050.29
Toluene ug/L ND 1.0 09/29/23 21:050.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/29/23 21:050.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/29/23 21:050.36
Trichloroethene ug/L ND 1.0 09/29/23 21:050.38
Trichlorofluoromethane ug/L ND 1.0 09/29/23 21:050.30
Vinyl chloride ug/L ND 1.0 09/29/23 21:050.39
1,2-Dichloroethane-d4 (S)%100 70-130 09/29/23 21:05
4-Bromofluorobenzene (S)%99 70-130 09/29/23 21:05
Toluene-d8 (S)%99 70-130 09/29/23 21:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157733LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.820 99 70-130
1,1,2,2-Tetrachloroethane ug/L 20.720 103 70-130
1,1,2-Trichloroethane ug/L 20.920 105 70-130
1,1,2-Trichlorotrifluoroethane ug/L 19.920 100 70-132
1,1-Dichloroethane ug/L 19.320 97 70-130
1,1-Dichloroethene ug/L 19.420 97 69-131
1,2,4-Trichlorobenzene ug/L 20.220 101 70-130
1,2-Dibromo-3-chloropropane ug/L 21.020 105 70-130
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130
1,2-Dichlorobenzene ug/L 20.420 102 70-130
1,2-Dichloroethane ug/L 19.620 98 70-130
1,2-Dichloropropane ug/L 20.520 102 70-130
1,3-Dichlorobenzene ug/L 19.420 97 70-130
1,4-Dichlorobenzene ug/L 19.820 99 70-130
2-Butanone (MEK)ug/L 40.240 101 67-133
2-Hexanone ug/L 42.240 106 70-133
4-Methyl-2-pentanone (MIBK)ug/L 41.940 105 70-130
Acetone ug/L 40.240 101 67-130
Benzene ug/L 20.120 100 70-130
Bromodichloromethane ug/L 20.320 101 70-130
Bromoform ug/L 20.320 101 70-133
Bromomethane ug/L 13.0 v32065 41-148
Carbon disulfide ug/L 19.620 98 70-131
Carbon tetrachloride ug/L 21.220 106 70-130
Chlorobenzene ug/L 20.420 102 70-130
Chloroethane ug/L 17.720 89 41-157
Chloroform ug/L 20.420 102 70-130
Chloromethane ug/L 17.120 86 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157733LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 19.420 97 70-130
cis-1,3-Dichloropropene ug/L 20.420 102 70-130
Cyclohexane ug/L 19.720 98 63-137
Dibromochloromethane ug/L 20.120 101 70-130
Dichlorodifluoromethane ug/L 20.220 101 54-147
Ethylbenzene ug/L 20.120 101 70-130
Isopropylbenzene (Cumene)ug/L 20.320 101 70-130
m&p-Xylene ug/L 40.840 102 70-130
Methyl acetate ug/L 18.520 92 70-130
Methyl-tert-butyl ether ug/L 19.020 95 70-130
Methylcyclohexane ug/L 20.420 102 70-130
Methylene Chloride ug/L 19.020 95 62-130
o-Xylene ug/L 19.820 99 70-130
Styrene ug/L 20.220 101 70-130
Tetrachloroethene ug/L 19.820 99 70-130
Toluene ug/L 20.520 102 70-130
trans-1,2-Dichloroethene ug/L 19.420 97 70-130
trans-1,3-Dichloropropene ug/L 21.220 106 70-130
Trichloroethene ug/L 21.120 105 70-130
Trichlorofluoromethane ug/L 19.320 96 57-130
Vinyl chloride ug/L 15.620 78 66-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4159141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4159142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 107 70-150113 5 3020ND21.5 22.7
1,1,2,2-Tetrachloroethane ug/L 20 103 66-144109 5 3020ND20.7 21.8
1,1,2-Trichloroethane ug/L 20 102 70-142118 15 3020ND20.4 23.7
1,1,2-Trichlorotrifluoroethane ug/L 20 106 66-168112 5 3020ND21.2 22.4
1,1-Dichloroethane ug/L 20 104 68-150110 5 3020ND20.9 22.0
1,1-Dichloroethene ug/L 20 106 64-162113 6 3020ND21.1 22.5
1,2,4-Trichlorobenzene ug/L 20 106 69-147114 7 3020ND21.3 22.8
1,2-Dibromo-3-chloropropane ug/L 20 101 62-146111 9 3020ND20.3 22.1
1,2-Dibromoethane (EDB) ug/L 20 106 70-143111 4 3020ND21.3 22.1
1,2-Dichlorobenzene ug/L 20 103 70-142110 7 3020ND20.5 22.0
1,2-Dichloroethane ug/L 20 101 68-145110 8 3020ND20.2 22.0
1,2-Dichloropropane ug/L 20 103 70-144113 9 3020ND20.7 22.6
1,3-Dichlorobenzene ug/L 20 99 70-142109 10 3020ND19.7 21.7
1,4-Dichlorobenzene ug/L 20 99 70-140110 10 3020ND19.8 22.0
2-Butanone (MEK)ug/L 40 98 57-156105 7 3040ND39.0 41.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4159141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4159142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 104 62-153111 6 3040ND41.8 44.5
4-Methyl-2-pentanone(MIBK)ug/L 40 100 65-144110 10 3040ND39.9 44.0
Acetone ug/L 40 102 49-162104 1 3040ND41.0 41.4
Benzene ug/L 20 104 68-144114 9 3020ND20.7 22.7
Bromodichloromethane ug/L 20 102 70-141114 12 3020ND20.3 22.9
Bromoform ug/L 20 102 59-144109 6 3020ND20.5 21.7
Bromomethane ug/L v3209023-19093 3 3020ND17.9 18.6
Carbon disulfide ug/L 20 105 64-160112 7 3020ND21.1 22.5
Carbon tetrachloride ug/L 20 108 70-147122 13 3020ND21.6 24.5
Chlorobenzene ug/L 20 101 70-143110 9 3020ND20.2 22.1
Chloroethane ug/L 20 98 55-190102 4 3020ND19.6 20.5
Chloroform ug/L 20 102 67-148112 10 3020ND20.3 22.4
Chloromethane ug/L 20 92 38-18098 6 3020ND18.5 19.6
cis-1,2-Dichloroethene ug/L 20 100 67-151110 9 3020ND20.1 21.9
cis-1,3-Dichloropropene ug/L 20 97 70-142113 15 3020ND19.5 22.6
Cyclohexane ug/L 20 104 64-162111 6 3020ND20.9 22.3
Dibromochloromethane ug/L 20 102 68-140106 5 3020ND20.3 21.2
Dichlorodifluoromethane ug/L 20 113 15-200118 4 3020ND22.7 23.6
Ethylbenzene ug/L 20 101 70-145108 7 3020ND20.1 21.6
Isopropylbenzene(Cumene)ug/L 20 103 70-144113 9 3020ND20.7 22.6
m&p-Xylene ug/L 40 103 70-148110 7 3040ND41.3 44.2
Methyl acetate ug/L 20 92 62-14494 3 3020ND18.3 18.8
Methyl-tert-butyl ether ug/L 20 94 64-146104 9 3020ND18.9 20.8
Methylcyclohexane ug/L 20 110 70-155118 7 3020ND22.0 23.5
Methylene Chloride ug/L 20 98 54-149108 9 3020ND19.6 21.5
o-Xylene ug/L 20 100 70-145106 6 3020ND19.9 21.2
Styrene ug/L 20 101 70-147111 9 3020ND20.2 22.2
Tetrachloroethene ug/L 20 99 70-145110 11 3020ND19.8 22.0
Toluene ug/L 20 102 65-146113 11 3020ND20.3 22.7
trans-1,2-Dichloroethene ug/L 20 103 69-155110 6 3020ND20.7 22.0
trans-1,3-Dichloropropene ug/L 20 107 70-142120 12 3020ND21.3 24.1
Trichloroethene ug/L 20 106 70-152117 9 3020ND21.3 23.4
Trichlorofluoromethane ug/L 20 105 60-158114 9 3020ND20.9 22.8
Vinyl chloride ug/L 20 87 51-17893 7 3020ND17.4 18.6
1,2-Dichloroethane-d4 (S) %102 70-13098
4-Bromofluorobenzene (S) %101 70-13099
Toluene-d8 (S)%99 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803315
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689437002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4160556
Associated Lab Samples:92689437002
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 10/01/23 01:310.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/01/23 01:310.22
1,1,2-Trichloroethane ug/L ND 1.0 10/01/23 01:310.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 10/01/23 01:310.32
1,1-Dichloroethane ug/L ND 1.0 10/01/23 01:310.37
1,1-Dichloroethene ug/L ND 1.0 10/01/23 01:310.35
1,2,4-Trichlorobenzene ug/L ND 1.0 10/01/23 01:310.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/01/23 01:310.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/01/23 01:310.27
1,2-Dichlorobenzene ug/L ND 1.0 10/01/23 01:310.34
1,2-Dichloroethane ug/L ND 1.0 10/01/23 01:310.32
1,2-Dichloropropane ug/L ND 1.0 10/01/23 01:310.36
1,3-Dichlorobenzene ug/L ND 1.0 10/01/23 01:310.34
1,4-Dichlorobenzene ug/L ND 1.0 10/01/23 01:310.33
2-Butanone (MEK)ug/L ND 5.0 10/01/23 01:314.0
2-Hexanone ug/L ND 5.0 10/01/23 01:310.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/01/23 01:312.7
Acetone ug/L ND 25.0 10/01/23 01:315.1
Benzene ug/L ND 1.0 10/01/23 01:310.34
Bromodichloromethane ug/L ND 1.0 10/01/23 01:310.31
Bromoform ug/L ND 1.0 10/01/23 01:310.34
Bromomethane ug/L ND 2.0 v210/01/23 01:311.7
Carbon disulfide ug/L ND 2.0 10/01/23 01:310.36
Carbon tetrachloride ug/L ND 1.0 10/01/23 01:310.33
Chlorobenzene ug/L ND 1.0 10/01/23 01:310.28
Chloroethane ug/L ND 1.0 10/01/23 01:310.65
Chloroform ug/L ND 1.0 10/01/23 01:310.43
Chloromethane ug/L ND 1.0 10/01/23 01:310.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/01/23 01:310.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/01/23 01:310.36
Cyclohexane ug/L ND 1.0 10/01/23 01:310.35
Dibromochloromethane ug/L ND 1.0 10/01/23 01:310.36
Dichlorodifluoromethane ug/L ND 1.0 10/01/23 01:310.35
Ethylbenzene ug/L ND 1.0 10/01/23 01:310.30
Isopropylbenzene (Cumene)ug/L ND 1.0 10/01/23 01:310.33
m&p-Xylene ug/L ND 2.0 10/01/23 01:310.71
Methyl acetate ug/L ND 10.0 10/01/23 01:312.4
Methyl-tert-butyl ether ug/L ND 1.0 10/01/23 01:310.42
Methylcyclohexane ug/L ND 10.0 10/01/23 01:311.5
Methylene Chloride ug/L ND 5.0 10/01/23 01:312.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4160556
Associated Lab Samples:92689437002
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 10/01/23 01:310.34
Styrene ug/L ND 1.0 10/01/23 01:310.29
Tetrachloroethene ug/L ND 1.0 10/01/23 01:310.29
Toluene ug/L ND 1.0 10/01/23 01:310.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/01/23 01:310.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/01/23 01:310.36
Trichloroethene ug/L ND 1.0 10/01/23 01:310.38
Trichlorofluoromethane ug/L ND 1.0 10/01/23 01:310.30
Vinyl chloride ug/L ND 1.0 10/01/23 01:310.39
1,2-Dichloroethane-d4 (S)%94 70-130 10/01/23 01:31
4-Bromofluorobenzene (S)%97 70-130 10/01/23 01:31
Toluene-d8 (S)%98 70-130 10/01/23 01:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4160557LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.320 101 70-130
1,1,2,2-Tetrachloroethane ug/L 21.420 107 70-130
1,1,2-Trichloroethane ug/L 21.220 106 70-130
1,1,2-Trichlorotrifluoroethane ug/L 22.020 110 70-132
1,1-Dichloroethane ug/L 21.420 107 70-130
1,1-Dichloroethene ug/L 23.420 117 69-131
1,2,4-Trichlorobenzene ug/L 18.420 92 70-130
1,2-Dibromo-3-chloropropane ug/L 18.720 94 70-130
1,2-Dibromoethane (EDB)ug/L 20.020 100 70-130
1,2-Dichlorobenzene ug/L 20.120 101 70-130
1,2-Dichloroethane ug/L 20.320 101 70-130
1,2-Dichloropropane ug/L 21.720 109 70-130
1,3-Dichlorobenzene ug/L 20.220 101 70-130
1,4-Dichlorobenzene ug/L 20.020 100 70-130
2-Butanone (MEK)ug/L 41.540 104 67-133
2-Hexanone ug/L 41.740 104 70-133
4-Methyl-2-pentanone (MIBK)ug/L 41.440 104 70-130
Acetone ug/L 42.440 106 67-130
Benzene ug/L 21.520 108 70-130
Bromodichloromethane ug/L 19.620 98 70-130
Bromoform ug/L 18.120 90 70-133
Bromomethane ug/L 16.2 v32081 41-148
Carbon disulfide ug/L 21.920 110 70-131
Carbon tetrachloride ug/L 20.420 102 70-130
Chlorobenzene ug/L 20.720 103 70-130
Chloroethane ug/L 19.520 97 41-157
Chloroform ug/L 20.520 103 70-130
Chloromethane ug/L 17.920 90 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
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[phone]
Page 37 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4160557LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 21.420 107 70-130
cis-1,3-Dichloropropene ug/L 20.620 103 70-130
Cyclohexane ug/L 22.420 112 63-137
Dibromochloromethane ug/L 19.520 98 70-130
Dichlorodifluoromethane ug/L 23.420 117 54-147
Ethylbenzene ug/L 20.320 102 70-130
Isopropylbenzene (Cumene)ug/L 20.620 103 70-130
m&p-Xylene ug/L 40.540 101 70-130
Methyl acetate ug/L 19.920 99 70-130
Methyl-tert-butyl ether ug/L 19.520 97 70-130
Methylcyclohexane ug/L 22.820 114 70-130
Methylene Chloride ug/L 23.020 115 62-130
o-Xylene ug/L 20.220 101 70-130
Styrene ug/L 20.620 103 70-130
Tetrachloroethene ug/L 19.020 95 70-130
Toluene ug/L 20.520 103 70-130
trans-1,2-Dichloroethene ug/L 22.220 111 70-130
trans-1,3-Dichloropropene ug/L 19.220 96 70-130
Trichloroethene ug/L 20.220 101 70-130
Trichlorofluoromethane ug/L 18.820 94 57-130
Vinyl chloride ug/L 17.720 89 66-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4160558MATRIX SPIKE SAMPLE:
MSSpike
Result
92690349007
1,1,1-Trichloroethane ug/L 25.320 127 70-150ND
1,1,2,2-Tetrachloroethane ug/L 24.220 121 66-144ND
1,1,2-Trichloroethane ug/L 24.520 122 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 27.320 136 66-168ND
1,1-Dichloroethane ug/L 29.7 v120132 68-1503.2
1,1-Dichloroethene ug/L 30.9 v120148 64-1621.2
1,2,4-Trichlorobenzene ug/L 21.120 105 69-147ND
1,2-Dibromo-3-chloropropane ug/L 20.320 102 62-146ND
1,2-Dibromoethane (EDB)ug/L 23.520 118 70-143ND
1,2-Dichlorobenzene ug/L 22.920 115 70-142ND
1,2-Dichloroethane ug/L 24.520 123 68-145ND
1,2-Dichloropropane ug/L 26.220 131 70-144ND
1,3-Dichlorobenzene ug/L 23.320 116 70-142ND
1,4-Dichlorobenzene ug/L 22.620 113 70-140ND
2-Butanone (MEK)ug/L 48.840 122 57-156ND
2-Hexanone ug/L 48.240 120 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 47.640 119 65-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
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Huntersville, NC 28078
[phone]
Page 38 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4160558MATRIX SPIKE SAMPLE:
MSSpike
Result
92690349007
Acetone ug/L 46.640 117 49-162ND
Benzene ug/L 25.620 128 68-144ND
Bromodichloromethane ug/L 23.820 119 70-141ND
Bromoform ug/L 20.520 103 59-144ND
Bromomethane ug/L 25.1 v320125 23-190ND
Carbon disulfide ug/L 27.720 139 64-160ND
Carbon tetrachloride ug/L 25.020 125 70-147ND
Chlorobenzene ug/L 24.520 122 70-143ND
Chloroethane ug/L 25.120 126 55-190ND
Chloroform ug/L 22.920 114 67-148ND
Chloromethane ug/L 22.420 112 38-180ND
cis-1,2-Dichloroethene ug/L 27.220 133 67-151ND
cis-1,3-Dichloropropene ug/L 23.920 119 70-142ND
Cyclohexane ug/L 28.3 v120142 64-162ND
Dibromochloromethane ug/L 22.820 114 68-140ND
Dichlorodifluoromethane ug/L 28.820 144 15-200ND
Ethylbenzene ug/L 24.320 122 70-145ND
Isopropylbenzene (Cumene)ug/L 24.820 124 70-144ND
m&p-Xylene ug/L 48.740 122 70-148ND
Methyl acetate ug/L 23.120 116 62-144ND
Methyl-tert-butyl ether ug/L 23.420 117 64-146ND
Methylcyclohexane ug/L 29.4 v120147 70-155ND
Methylene Chloride ug/L 27.8 v120139 54-149ND
o-Xylene ug/L 23.520 117 70-145ND
Styrene ug/L 24.120 120 70-147ND
Tetrachloroethene ug/L 23.420 117 70-145ND
Toluene ug/L 24.620 123 65-146ND
trans-1,2-Dichloroethene ug/L 27.320 136 69-155ND
trans-1,3-Dichloropropene ug/L 23.220 116 70-142ND
Trichloroethene ug/L 25.120 122 70-152ND
Trichlorofluoromethane ug/L 24.020 120 60-158ND
Vinyl chloride ug/L 21.820 109 51-178ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92690406001
4160559SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND v130ND
1,1-Dichloroethene ug/L ND v130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92690406001
4160559SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND v130ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND v130ND
Methylene Chloride ug/L ND v130ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%101102
4-Bromofluorobenzene (S)%9799
Toluene-d8 (S)%9997
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801703
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689437001, 92689437002, 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152817
Associated Lab Samples:92689437001, 92689437002, 92689437003
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/25/23 16:291.2
2,4,5-Trichlorophenol ug/L ND 10.0 09/25/23 16:291.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/25/23 16:291.6
2,4-Dichlorophenol ug/L ND 10.0 09/25/23 16:291.4
2,4-Dimethylphenol ug/L ND 10.0 09/25/23 16:291.7
2,4-Dinitrophenol ug/L ND 50.0 09/25/23 16:2926.0
2,4-Dinitrotoluene ug/L ND 10.0 09/25/23 16:291.6
2,6-Dinitrotoluene ug/L ND 10.0 09/25/23 16:291.7
2-Chloronaphthalene ug/L ND 10.0 09/25/23 16:291.7
2-Chlorophenol ug/L ND 10.0 09/25/23 16:291.2
2-Methylnaphthalene ug/L ND 10.0 09/25/23 16:291.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/25/23 16:291.9
2-Nitroaniline ug/L ND 20.0 09/25/23 16:293.0
2-Nitrophenol ug/L ND 10.0 09/25/23 16:291.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/25/23 16:291.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/25/23 16:298.1
3-Nitroaniline ug/L ND 20.0 09/25/23 16:293.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/25/23 16:297.8
4-Bromophenylphenyl ether ug/L ND 10.0 09/25/23 16:291.8
4-Chloro-3-methylphenol ug/L ND 10.0 09/25/23 16:293.3
4-Chloroaniline ug/L ND 20.0 09/25/23 16:293.6
4-Chlorophenylphenyl ether ug/L ND 10.0 09/25/23 16:292.0
4-Nitroaniline ug/L ND 20.0 09/25/23 16:295.1
4-Nitrophenol ug/L ND 50.0 09/25/23 16:296.6
Acenaphthene ug/L ND 10.0 09/25/23 16:292.0
Acenaphthylene ug/L ND 10.0 09/25/23 16:292.0
Acetophenone ug/L ND 10.0 09/25/23 16:291.5
Anthracene ug/L ND 10.0 09/25/23 16:292.3
Atrazine ug/L ND 10.0 09/25/23 16:293.2
Benzaldehyde ug/L ND 10.0 09/25/23 16:293.6
Benzo(a)anthracene ug/L ND 10.0 09/25/23 16:292.7
Benzo(a)pyrene ug/L ND 10.0 09/25/23 16:292.8
Benzo(b)fluoranthene ug/L ND 10.0 09/25/23 16:292.6
Benzo(g,h,i)perylene ug/L ND 10.0 09/25/23 16:292.8
Benzo(k)fluoranthene ug/L ND 10.0 09/25/23 16:292.7
Biphenyl (Diphenyl)ug/L ND 10.0 09/25/23 16:291.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/25/23 16:291.8
bis(2-Chloroethyl) ether ug/L ND 10.0 09/25/23 16:291.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/25/23 16:293.7
Butylbenzylphthalate ug/L ND 10.0 09/25/23 16:293.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152817
Associated Lab Samples:92689437001, 92689437002, 92689437003
Matrix: Water
AnalyzedMDL
Caprolactam ug/L ND 10.0 09/25/23 16:296.9
Carbazole ug/L ND 10.0 09/25/23 16:292.4
Chrysene ug/L ND 10.0 09/25/23 16:292.8
Di-n-butylphthalate ug/L ND 10.0 09/25/23 16:292.2
Di-n-octylphthalate ug/L ND 10.0 09/25/23 16:293.9
Dibenz(a,h)anthracene ug/L ND 10.0 09/25/23 16:293.0
Dibenzofuran ug/L ND 10.0 09/25/23 16:292.1
Diethylphthalate ug/L ND 10.0 09/25/23 16:292.0
Dimethylphthalate ug/L ND 10.0 09/25/23 16:292.1
Fluoranthene ug/L ND 10.0 09/25/23 16:292.2
Fluorene ug/L ND 10.0 09/25/23 16:292.1
Hexachloro-1,3-butadiene ug/L ND 10.0 09/25/23 16:291.8
Hexachlorobenzene ug/L ND 10.0 09/25/23 16:292.2
Hexachlorocyclopentadiene ug/L ND 10.0 09/25/23 16:291.6
Hexachloroethane ug/L ND 10.0 09/25/23 16:291.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/25/23 16:292.9
Isophorone ug/L ND 10.0 09/25/23 16:291.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/25/23 16:291.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/25/23 16:293.0
Naphthalene ug/L ND 10.0 09/25/23 16:292.1
Nitrobenzene ug/L ND 10.0 09/25/23 16:291.9
Pentachlorophenol ug/L ND 20.0 09/25/23 16:293.8
Phenanthrene ug/L ND 10.0 09/25/23 16:292.0
Phenol ug/L ND 10.0 09/25/23 16:291.4
Pyrene ug/L ND 10.0 09/25/23 16:292.2
2,4,6-Tribromophenol (S)%118 10-164 09/25/23 16:29
2-Fluorobiphenyl (S)%97 10-130 09/25/23 16:29
2-Fluorophenol (S)%66 10-130 09/25/23 16:29
Nitrobenzene-d5 (S)%108 10-138 09/25/23 16:29
Phenol-d6 (S)%56 10-130 09/25/23 16:29
Terphenyl-d14 (S)%141 19-191 09/25/23 16:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152818LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 18.650 37 21-135
2,4,5-Trichlorophenol ug/L 34.950 70 38-147
2,4,6-Trichlorophenol ug/L 24.450 49 34-142
2,4-Dichlorophenol ug/L 21.650 43 36-136
2,4-Dimethylphenol ug/L 21.250 42 38-134
2,4-Dinitrophenol ug/L 152250 61 10-169
2,4-Dinitrotoluene ug/L 35.150 70 44-154
2,6-Dinitrotoluene ug/L 29.950 60 44-156
2-Chloronaphthalene ug/L 20.250 40 25-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152818LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 22.650 45 29-130
2-Methylnaphthalene ug/L 18.450 37 23-130
2-Methylphenol(o-Cresol)ug/L 20.150 40 31-130
2-Nitroaniline ug/L 56.4100 56 39-145
2-Nitrophenol ug/L 21.850 44 29-142
3&4-Methylphenol(m&p Cresol)ug/L 19.950 40 30-130
3,3'-Dichlorobenzidine ug/L 89.0100 89 44-158
3-Nitroaniline ug/L 73.0100 73 45-152
4,6-Dinitro-2-methylphenol ug/L 69.7100 70 39-158
4-Bromophenylphenyl ether ug/L 29.550 59 47-147
4-Chloro-3-methylphenol ug/L 44.0100 44 40-138
4-Chloroaniline ug/L 41.8100 42 35-130
4-Chlorophenylphenyl ether ug/L 25.850 52 36-139
4-Nitroaniline ug/L 87.5100 87 46-157
4-Nitrophenol ug/L 113250 45 17-130
Acenaphthene ug/L 22.550 45 34-135
Acenaphthylene ug/L 21.950 44 35-137
Acetophenone ug/L 21.550 43 30-137
Anthracene ug/L 33.750 67 47-146
Atrazine ug/L 34.850 70 30-130
Benzaldehyde ug/L 23.850 48 17-167
Benzo(a)anthracene ug/L 40.350 81 48-160
Benzo(a)pyrene ug/L 42.050 84 47-165
Benzo(b)fluoranthene ug/L 47.550 95 49-171
Benzo(g,h,i)perylene ug/L 42.950 86 46-166
Benzo(k)fluoranthene ug/L 43.250 86 55-162
Biphenyl (Diphenyl)ug/L 20.250 40 28-130
bis(2-Chloroethoxy)methane ug/L 20.150 40 33-136
bis(2-Chloroethyl) ether ug/L 22.550 45 30-142
bis(2-Ethylhexyl)phthalate ug/L 41.450 83 46-173
Butylbenzylphthalate ug/L 40.150 80 53-169
Caprolactam ug/L 21.350 43 13-130
Carbazole ug/L 39.850 80 48-157
Chrysene ug/L 39.450 79 54-152
Di-n-butylphthalate ug/L 38.050 76 49-161
Di-n-octylphthalate ug/L 40.450 81 50-166
Dibenz(a,h)anthracene ug/L 41.750 83 46-166
Dibenzofuran ug/L 23.250 46 37-136
Diethylphthalate ug/L 34.050 68 45-149
Dimethylphthalate ug/L 29.250 58 43-145
Fluoranthene ug/L 39.350 79 50-153
Fluorene ug/L 25.550 51 42-142
Hexachloro-1,3-butadiene ug/L 10.350 21 10-130
Hexachlorobenzene ug/L 29.750 59 44-138
Hexachlorocyclopentadiene ug/L 15.550 31 10-130
Hexachloroethane ug/L 6.8J50 14 10-130
Indeno(1,2,3-cd)pyrene ug/L 40.950 82 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152818LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 19.950 40 36-135
N-Nitroso-di-n-propylamine ug/L 23.250 46 33-140
N-Nitrosodiphenylamine ug/L 30.950 62 46-144
Naphthalene ug/L 15.350 31 20-130
Nitrobenzene ug/L 20.050 40 33-133
Pentachlorophenol ug/L 69.5100 70 21-163
Phenanthrene ug/L 33.950 68 47-146
Phenol ug/L 13.350 27 19-130
Pyrene ug/L 38.050 76 53-155
2,4,6-Tribromophenol (S)%68 10-164
2-Fluorobiphenyl (S)%37 10-130
2-Fluorophenol (S)%29 10-130
Nitrobenzene-d5 (S)%36 10-138
Phenol-d6 (S)%24 10-130
Terphenyl-d14 (S)%67 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4152820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-chloropropane)ug/L 83.3 58 11-14352 11 3083.3ND 48.4 43.5
2,4,5-Trichlorophenol ug/L 83.3 83 10-17080 4 3083.3ND 69.3 66.9
2,4,6-Trichlorophenol ug/L 83.3 60 10-16668 12 3083.3ND 50.4 56.7
2,4-Dichlorophenol ug/L 83.3 74 10-15368 8 3083.3ND 61.7 56.9
2,4-Dimethylphenol ug/L 83.3 77 20-14765 17 3083.3ND 64.6 54.4
2,4-Dinitrophenol ug/L M1417010-17265 30417NDND 269
2,4-Dinitrotoluene ug/L 83.3 89 30-16476 16 3083.3ND 73.9 63.1
2,6-Dinitrotoluene ug/L 83.3 85 31-16373 15 3083.3ND 70.5 60.8
2-Chloronaphthalene ug/L 83.3 60 15-13449 20 3083.3ND 50.4 41.0
2-Chlorophenol ug/L 83.3 74 10-13962 17 3083.3ND 61.7 52.0
2-Methylnaphthalene ug/L 83.3 55 12-13057 2 3083.3ND 46.1 47.2
2-Methylphenol(o-Cresol) ug/L 83.3 67 19-13256 17 3083.3ND 55.5 46.9
2-Nitroaniline ug/L 167 78 23-15473 7 30167ND131 121
2-Nitrophenol ug/L 83.3 82 10-15967 20 3083.3ND 68.4 56.03&4-Methylphenol(m&pCresol)ug/L 83.3 64 13-13654 17 3083.3ND 53.6 45.4
3,3'-Dichlorobenzidine ug/L R116711210-17881 32 30167ND187 135
3-Nitroaniline ug/L 167 55 20-16645 20 30167ND92.2 75.1
4,6-Dinitro-2-methylphenol ug/L R11673210-18769 73 30167ND53.9 116
4-Bromophenylphenyl ether ug/L 83.3 81 31-15763 25 3083.3ND 67.3 52.6
4-Chloro-3-methylphenol ug/L 167 74 27-14666 10 30167ND123 111
4-Chloroaniline ug/L M11671313-1439 30167ND22.4J 15.4J
4-Chlorophenylphenyl ether ug/L 83.3 75 23-14959 24 3083.3ND 62.2 49.1
4-Nitroaniline ug/L 167 99 24-17178 24 30167ND166 130
4-Nitrophenol ug/L 417 18 10-13047 30417ND76.1J 195
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
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Page 44 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4152820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L 83.3 69 21-14754 24 3083.3ND 57.2 44.9
Acenaphthylene ug/L 83.3 68 19-15054 23 3083.3ND 56.9 45.2
Acetophenone ug/L 83.3 73 22-14562 17 3083.3ND 61.1 51.3
Anthracene ug/L 83.3 88 36-15267 27 3083.3ND 73.6 55.9
Atrazine ug/L 83.3 92 18-17388 4 3083.3ND 76.4 73.1
Benzaldehyde ug/L 83.3 75 16-16374 1 3083.3ND 62.2 61.4
Benzo(a)anthracene ug/L R183.3 105 42-16376 32 3083.3ND 87.5 63.4
Benzo(a)pyrene ug/L 83.3 108 40-16980 30 3083.3ND 90.1 66.7
Benzo(b)fluoranthene ug/L 83.3 119 40-17787 30 3083.3ND 98.9 72.7
Benzo(g,h,i)perylene ug/L 83.3 105 38-17482 25 3083.3ND 87.2 68.1
Benzo(k)fluoranthene ug/L R183.3 115 41-17180 36 3083.3ND 96.2 66.7
Biphenyl (Diphenyl)ug/L 83.3 62 14-13750 22 3083.3ND 51.7 41.5
bis(2-Chloroethoxy)methane ug/L 83.3 71 19-14661 16 3083.3ND 59.2 50.5
bis(2-Chloroethyl) ether ug/L 83.3 64 19-15155 14 3083.3ND 53.1 46.0
bis(2-Ethylhexyl)phthalate ug/L 83.3 113 42-16886 27 3083.3ND 94.5 71.9
Butylbenzylphthalate ug/L 83.3 109 42-17782 29 3083.3ND 91.0 68.1
Caprolactam ug/L 83.3 36 10-13032 11 3083.3ND 29.7 26.7
Carbazole ug/L 83.3 105 38-16479 28 3083.3ND 87.2 65.4
Chrysene ug/L 83.3 102 43-15976 30 3083.3ND 85.0 63.0
Di-n-butylphthalate ug/L 83.3 103 42-16077 29 3083.3ND 85.8 64.2
Di-n-octylphthalate ug/L 83.3 114 42-17192 22 3083.3ND 95.3 76.7
Dibenz(a,h)anthracene ug/L 83.3 105 40-17179 28 3083.3ND 87.1 66.1
Dibenzofuran ug/L 83.3 67 23-14753 23 3083.3ND 55.9 44.2
Diethylphthalate ug/L 83.3 88 33-15773 18 3083.3ND 73.1 60.9
Dimethylphthalate ug/L 83.3 77 27-15467 14 3083.3ND 64.0 55.9
Fluoranthene ug/L 83.3 103 42-15776 30 3083.3ND 85.7 63.6
Fluorene ug/L 83.3 73 25-15559 20 3083.3ND 60.5 49.3
Hexachloro-1,3-butadiene ug/L R183.3 22 10-13042 62 3083.3ND 18.7 35.4
Hexachlorobenzene ug/L 83.3 82 32-14566 21 3083.3ND 68.5 55.3
Hexachlorocyclopentadiene ug/L 83.3 42 10-13046 9 3083.3ND 35.3 38.7
Hexachloroethane ug/L 83.3 17 10-13034 3083.3ND 13.9J 28.6
Indeno(1,2,3-cd)pyrene ug/L 83.3 101 39-17477 27 3083.3ND 84.1 64.2
Isophorone ug/L 83.3 75 19-14662 18 3083.3ND 62.1 52.0
N-Nitroso-di-n-propylamine ug/L 83.3 78 20-15069 12 3083.3ND 64.6 57.2
N-Nitrosodiphenylamine ug/L 83.3 83 33-14966 23 3083.3ND 69.3 54.8
Naphthalene ug/L 83.3 44 10-12853 19 3083.3ND 36.4 44.1
Nitrobenzene ug/L 83.3 70 19-14557 21 3083.3ND 58.4 47.3
Pentachlorophenol ug/L 167 52 10-18865 22 30167ND87.3 109
Phenanthrene ug/L 83.3 87 38-15065 29 3083.3ND 72.7 54.6
Phenol ug/L 83.3 45 10-13035 26 3083.3ND 37.9 29.1
Pyrene ug/L 83.3 98 42-16374 29 3083.3ND 81.9 61.3
2,4,6-Tribromophenol (S) %82 10-16474
2-Fluorobiphenyl (S)%60 10-13051
2-Fluorophenol (S)%46 10-13044
Nitrobenzene-d5 (S)%64 10-13860
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4152820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%43 10-13035
Terphenyl-d14 (S)%85 19-19168
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803715
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689437001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4162457
Associated Lab Samples:92689437001
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 10/03/23 13:415.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4162458LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 50.650 101 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4162459LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.950 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4162460MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265009
4162461
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 102 80-120102 1 255010.9 62.1 61.7
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4162462MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4162463
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 103 80-120103 0 255010.1 61.5 61.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804057
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689437002, 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4164233
Associated Lab Samples:92689437002, 92689437003
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 10/05/23 11:345.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4164234LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.150 102 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4164235LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.350 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4164236MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689881007
4164237
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 96 80-12098 1 255053.6 101 103
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4164238MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689881008
4164239
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 97 80-12099 1 255048.6 97.0 98.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802243
SM 4500-S2D-2011
SM 4500-S2D-2011
4500S2D Sulfide Water
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689437001, 92689437002, 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4155674
Associated Lab Samples:92689437001, 92689437002, 92689437003
Matrix: Water
AnalyzedMDL
Sulfide mg/L ND 0.10 09/27/23 01:350.022
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4155675LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide mg/L 0.540.5 109 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4155678MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689489018
4155679
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L M10.5 125 80-120124 0 100.5ND 0.62 0.62
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4155708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689489017
4155709
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide mg/L 0.5 108 80-120108 0 100.5ND 0.54 0.54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801381
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689437001, 92689437002, 92689437003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150965
Associated Lab Samples:92689437001, 92689437002, 92689437003
Matrix: Water
AnalyzedMDL
Bromide mg/L ND 0.10 09/22/23 16:290.060
Chloride mg/L ND 1.0 09/22/23 16:290.60
Fluoride mg/L ND 0.10 09/22/23 16:290.050
Sulfate mg/L ND 1.0 09/22/23 16:290.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150966LABORATORY CONTROL SAMPLE:
LCSSpike
Bromide mg/L 2.62.5 102 90-110
Chloride mg/L 53.150 106 90-110
Fluoride mg/L 2.72.5 106 90-110
Sulfate mg/L 53.450 107 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150967MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689410005
4150968
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromide mg/L 2.5 99 90-110101 2 102.5ND 2.5 2.5
Chloride mg/L 50 103 90-110104 1 1050ND51.3 52.0
Fluoride mg/L 2.5 106 90-110101 5 102.5ND 2.7 2.6
Sulfate mg/L 50 103 90-110104 1 1050ND51.4 52.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150969MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4150970
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromide mg/L 2.5 99 90-110101 2 102.5ND 2.5 2.5
Chloride mg/L 50 103 90-110105 2 10501.2 52.7 53.7
Fluoride mg/L 2.5 96 90-11099 2 102.5ND 2.5 2.5
Sulfate mg/L 50 103 90-110105 2 10501.4 53.1 54.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 73
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was received or analysis requested beyond the recognized method holding time.H3
The internal standard response is below criteria. Results may be biased high.IS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in theassociated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 73
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92689437
Pactiv Energreen GWS (9/21)-Revised Report
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92689437001 807305PZ09WG-092123 SM 2120B-2011
92689437002 807305PZ08WG-092123 SM 2120B-2011
92689437003 807305EB02WQ-092123 SM 2120B-2011
92689437001 954422 954504PZ09WG-092123 EPA 3010 EPA 6010
92689437002 954422 954504PZ08WG-092123 EPA 3010 EPA 6010
92689437003 954422 954504EB02WQ-092123 EPA 3010 EPA 6010
92689437001 954621 954719PZ09WG-092123 EPA 3010 EPA 6010
92689437002 954621 954719PZ08WG-092123 EPA 3010 EPA 6010
92689437003 954621 954719EB02WQ-092123 EPA 3010 EPA 6010
92689437001 955304 955582PZ09WG-092123 EPA 7470 EPA 7470
92689437002 955304 955582PZ08WG-092123 EPA 7470 EPA 7470
92689437003 955304 955582EB02WQ-092123 EPA 7470 EPA 7470
92689437001 955306 955584PZ09WG-092123 EPA 7470 EPA 7470
92689437002 955306 955584PZ08WG-092123 EPA 7470 EPA 7470
92689437003 955306 955584EB02WQ-092123 EPA 7470 EPA 7470
92689437001 801703 801890PZ09WG-092123 EPA 3510C EPA 8270E
92689437002 801703 801890PZ08WG-092123 EPA 3510C EPA 8270E
92689437003 801703 801890EB02WQ-092123 EPA 3510C EPA 8270E
92689437001 802720PZ09WG-092123 EPA 8260D
92689437002 803315PZ08WG-092123 EPA 8260D
92689437003 802723EB02WQ-092123 EPA 8260D
92689437001 803715PZ09WG-092123 SM 2320B-2011
92689437002 804057PZ08WG-092123 SM 2320B-2011
92689437003 804057EB02WQ-092123 SM 2320B-2011
92689437001 802243PZ09WG-092123 SM 4500-S2D-2011
92689437002 802243PZ08WG-092123 SM 4500-S2D-2011
92689437003 802243EB02WQ-092123 SM 4500-S2D-2011
92689437001 801381PZ09WG-092123 EPA 300.0 Rev 2.1 1993
92689437002 801381PZ08WG-092123 EPA 300.0 Rev 2.1 1993
92689437003 801381EB02WQ-092123 EPA 300.0 Rev 2.1 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 73
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Page 54 of 73
Page 55 of 73
Thisreportshouldnotbereproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamplesincludedinthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
Matthew Brainard
PACE Charlotte
9800 Kincey Ave.
Huntersville NC 28078
REPORT OF
LABORATORY
ANALYSIS FOR
PCDD/PCDF
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
October 10, 2023
Pace Project #: 10670284
Sample Receipt Date: 09/27/2023
Client Project #: 92689437
Client Sub PO #: N/A
The report provided has been invoiced as a Level 2
PCDD/PCDF Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questionstoIsaac Johnson,your Pace
Project Manager.
State Cert #: 530
Suite 100
Report Prepared for:
Page 1 of 18Report No.....10670284_SW8290AFC_L2_dfr
October 10, 2023
Isaac Johnson, Project Manager
[phone]
[phone] (fax)
[e-mail]
Page 56 of 73
Pace Analytical Services,Inc.1700 Elm StreetMinneapolis, MN 55414Phone: [phone]
Fax: [phone]
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
This report presents the results from the analyses performed on three samples submitted by a
representative of Pace Analytical Services, LLC. The samples were analyzed for the presence or absence
of polychlorodibenzo-p-dioxins (PCDDs) and polychlorodibenzofurans (PCDFs) using a modified version
of USEPA Method 8290A. The estimated detection limits (EDLs) were based on signal-to-noise
measurements. Estimated maximum possible concentration (EMPC) values were treated as positives inthe toxic equivalence calculations.
Second column confirmation analyses of 2,3,7,8-TCDF values obtained from the primary (DB5-MS)column are performed only when specifically requested for a project and only when the values are abovethe concentration of the lowest calibration standard. Typical resolution for this isomer using the DB5-MScolumn ranges from 25-30%.
The isotopically-labeled PCDD/PCDF internal standards in the sample extracts were recovered at15-65%. Except for fifteen low values, which were flagged "R" on the results tables, the labeled internalstandard recoveries obtained for this project were within the 40-135% target range specified in Method
8290A. Since the quantification of the native 2,3,7,8-substituted congeners was based on isotope dilution,
the data were automatically corrected for recovery and accurate values were obtained.
Values were flagged "I" where incorrect isotope ratios were obtained or "P" where polychlorinated diphenyl
ethers were present. Concentrations below the calibration range were flagged "J" and should be regarded
as estimates.
A laboratory method blank was prepared and analyzed with the sample batch as part of our routine quality
control procedures. The results show the blank to contain trace levels of one or more selected congeners.
These levels were below the calibration range of the method. Sample concentrations similar to the
corresponding blank levels were flagged "B" on the results tables and may be, at least partially, attributedto the background.
Laboratory spike samples were also prepared using clean reference matrix that had been fortified withnative standard materials. The results show that the spiked native compounds were recovered at86-104% with relative percent differences of 0.0-6.0%. These results were within the target ranges for themethod. Matrix spikes were not prepared with the extraction batch.
DISCUSSION
Page 2 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 57 of 73
REPORT OF LABORATORY ANALYSIS
This report shallnot bereproduced,except in full,
withoutthe written consentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 58 of 73
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 4 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 59 of 73
Pa
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9/28/23
Page 6 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 61 of 73
Page 7 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 62 of 73
Page 8 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 63 of 73
Page 9 of 18Report No.....10670284_SW8290AFC_L2_dfr
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Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
A =
B = C = D = E = H2 =
I =
J = L = Nn = P = R =
S =
U = V = X = Y = * =
Reporting Limit based on signal to noise (EDL)
Less than 10x higher than method blank level Result obtained from confirmation analysis Result obtained from analysis of diluted sample Exceeds calibration range Extracted outside of holding time
Isotope ratio out of specification
Estimated value Suppressive interference, analyte may be biased low Value obtained from additional analysis PCDE Interference Recovery outside target range
Peak saturated
Analyte not detected Result verified by confirmation analysis %D Exceeds limits Calculated using average of daily RFs See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 10 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 65 of 73
Pace Analytical Services, LLC1700 Elm Street, Suite 200Minneapolis, MN 55414Phone: [phone]Fax: [phone]www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,without the written consent of Pace Analytical Services, LLC.
Page 11 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 66 of 73
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID P209WG-09212392689437001L231009A_11JF
NA940 mL
NAL230816L231009A_01 & L231009B_01BLANK-108589
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/21/2023 09:0509/27/2023 08:5010/05/2023 09:1010/09/2023 15:09
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF -----0.71 2,3,7,8-TCDF-13C 2.00 54IJ0.79Total TCDF ND 0.71 2,3,7,8-TCDD-13C 2.00 32-----R1,2,3,7,8-PeCDF-13C 2.00 532,3,7,8-TCDD ND 1.5 2,3,4,7,8-PeCDF-13C 2.00 58-----Total TCDD ND 1.5 1,2,3,7,8-PeCDD-13C 2.00 60-----1,2,3,4,7,8-HxCDF-13C 2.00 491,2,3,7,8-PeCDF ND 0.95 1,2,3,6,7,8-HxCDF-13C 2.00 38-----R2,3,4,7,8-PeCDF ND 0.59 2,3,4,6,7,8-HxCDF-13C 2.00 65-----Total PeCDF ND 0.59 1,2,3,7,8,9-HxCDF-13C 2.00 59-----1,2,3,4,7,8-HxCDD-13C 2.00 631,2,3,7,8-PeCDD ND 0.63 1,2,3,6,7,8-HxCDD-13C 2.00 61-----Total PeCDD ND 0.63 1,2,3,4,6,7,8-HpCDF-13C 2.00 50-----1,2,3,4,7,8,9-HpCDF-13C 2.00 39 R1,2,3,4,7,8-HxCDF ND 1.0 1,2,3,4,6,7,8-HpCDD-13C 2.00 58-----1,2,3,6,7,8-HxCDF ND 1.3 OCDD-13C 4.00 46-----2,3,4,6,7,8-HxCDF ND 0.86-----1,2,3,7,8,9-HxCDF -----0.99 1,2,3,4-TCDD-13C 2.00 NAIJ1.2Total HxCDF ND 0.86 1,2,3,7,8,9-HxCDD-13C 2.00 NA-----
1,2,3,4,7,8-HxCDD ND 1.1 2,3,7,8-TCDD-37Cl4 0.20 39-----1,2,3,6,7,8-HxCDD ND 1.1-----1,2,3,7,8,9-HxCDD ND 1.1-----Total HxCDD ND 1.1-----
1,2,3,4,6,7,8-HpCDF ND 2.4 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 5.3 Equivalence: 0.23 pg/L-----Total HpCDF ND 2.4 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD -----1.5 IJ2.3Total HpCDD 6.1 1.5 BJ-----
OCDF ND 4.7-----OCDD 34 5.4 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelR=Recovery outside target rangeI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 12 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 67 of 73
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID P208WG-09212392689437002L231009A_12JF
NA948 mL
NAL230816L231009A_01 & L231009B_01BLANK-108589
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/21/2023 10:0509/27/2023 08:5010/05/2023 09:1010/09/2023 15:52
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF 27 1.1 2,3,7,8-TCDF-13C 2.00 51-----Total TCDF 60 1.1 2,3,7,8-TCDD-13C 2.00 23-----R1,2,3,7,8-PeCDF-13C 2.00 452,3,7,8-TCDD ND 3.0 2,3,4,7,8-PeCDF-13C 2.00 47-----Total TCDD ND 3.0 1,2,3,7,8-PeCDD-13C 2.00 48-----1,2,3,4,7,8-HxCDF-13C 2.00 38 R1,2,3,7,8-PeCDF -----1.5 1,2,3,6,7,8-HxCDF-13C 2.00 38PJ6.5 R2,3,4,7,8-PeCDF 5.0 1.0 2,3,4,6,7,8-HxCDF-13C 2.00 50BJ-----Total PeCDF 5.0 1.0 1,2,3,7,8,9-HxCDF-13C 2.00 42BJ-----1,2,3,4,7,8-HxCDD-13C 2.00 511,2,3,7,8-PeCDD ND 0.83 1,2,3,6,7,8-HxCDD-13C 2.00 48-----Total PeCDD ND 0.83 1,2,3,4,6,7,8-HpCDF-13C 2.00 37-----R1,2,3,4,7,8,9-HpCDF-13C 2.00 31 R1,2,3,4,7,8-HxCDF -----1.5 1,2,3,4,6,7,8-HpCDD-13C 2.00 43IJ4.61,2,3,6,7,8-HxCDF -----1.4 OCDD-13C 4.00 33IJ1.5 R2,3,4,6,7,8-HxCDF ND 1.2-----1,2,3,7,8,9-HxCDF 2.1 1.6 1,2,3,4-TCDD-13C 2.00 NABJ-----Total HxCDF 3.6 1.2 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD ND 1.8 2,3,7,8-TCDD-37Cl4 0.20 30-----1,2,3,6,7,8-HxCDD ND 1.6-----1,2,3,7,8,9-HxCDD ND 1.7-----Total HxCDD ND 1.6-----
1,2,3,4,6,7,8-HpCDF 4.0 3.5 Total 2,3,7,8-TCDDJ-----1,2,3,4,7,8,9-HpCDF ND 6.4 Equivalence: 5.3 pg/L-----Total HpCDF 4.0 3.5 (Lower-bound - Using 2005 WHO Factors)BJ-----
1,2,3,4,6,7,8-HpCDD -----3.5 IJ5.2Total HpCDD ND 3.5-----
OCDF ND 7.8-----OCDD -----9.5 IJ66
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelR=Recovery outside target rangeP = PCDE Interference
I=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 13 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 68 of 73
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected ByFilename
Total Amount Extracted% MoistureDry Weight ExtractedICAL IDCCal Filename(s)Method Blank ID
Client's Sample ID EB02WQ-09212392689437003L231009A_13JF
NA958 mL
NAL230816L231009A_01 & L231009B_01BLANK-108589
MatrixDilutionCollectedReceivedExtractedAnalyzed
WATERNA09/21/2023 11:0509/27/2023 08:5010/05/2023 09:1010/09/2023 16:34
Client - PACE Charlotte
Method 8290A Sample Analysis Results
NativeIsomers Concpg/L pg/L InternalStandards Addedng's PercentRecoveryEMPCpg/L EDL
2,3,7,8-TCDF -----0.75 2,3,7,8-TCDF-13C 2.00 49IJ1.0Total TCDF ND 0.75 2,3,7,8-TCDD-13C 2.00 15-----R1,2,3,7,8-PeCDF-13C 2.00 482,3,7,8-TCDD ND 3.9 2,3,4,7,8-PeCDF-13C 2.00 51-----Total TCDD ND 3.9 1,2,3,7,8-PeCDD-13C 2.00 54-----1,2,3,4,7,8-HxCDF-13C 2.00 431,2,3,7,8-PeCDF 1.4 0.96 1,2,3,6,7,8-HxCDF-13C 2.00 40J-----2,3,4,7,8-PeCDF ND 0.63 2,3,4,6,7,8-HxCDF-13C 2.00 58-----Total PeCDF 1.4 0.63 1,2,3,7,8,9-HxCDF-13C 2.00 48BJ-----1,2,3,4,7,8-HxCDD-13C 2.00 551,2,3,7,8-PeCDD ND 1.1 1,2,3,6,7,8-HxCDD-13C 2.00 57-----Total PeCDD ND 1.1 1,2,3,4,6,7,8-HpCDF-13C 2.00 43-----1,2,3,4,7,8,9-HpCDF-13C 2.00 34 R1,2,3,4,7,8-HxCDF ND 1.7 1,2,3,4,6,7,8-HpCDD-13C 2.00 50-----1,2,3,6,7,8-HxCDF ND 1.7 OCDD-13C 4.00 38-----R2,3,4,6,7,8-HxCDF ND 1.2-----1,2,3,7,8,9-HxCDF ND 1.7 1,2,3,4-TCDD-13C 2.00 NA-----Total HxCDF 1.3 1.2 1,2,3,7,8,9-HxCDD-13C 2.00 NABJ-----
1,2,3,4,7,8-HxCDD -----1.5 2,3,7,8-TCDD-37Cl4 0.20 23IJ2.31,2,3,6,7,8-HxCDD ND 1.4-----1,2,3,7,8,9-HxCDD ND 1.4-----Total HxCDD ND 1.4-----
1,2,3,4,6,7,8-HpCDF ND 3.1 Total 2,3,7,8-TCDD-----1,2,3,4,7,8,9-HpCDF ND 5.6 Equivalence: 0.43 pg/L-----Total HpCDF ND 3.1 (Lower-bound - Using 2005 WHO Factors)-----
1,2,3,4,6,7,8-HpCDD 4.3 3.3 BJ-----Total HpCDD 7.8 3.3 BJ-----
OCDF -----4.9 IJ6.3OCDD43 8.0 BJ-----
Conc =Concentration (Totalsinclude 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not ApplicableNC = Not Calculated
J = Estimated value
B =Less than 10x higher than method blank levelR=Recovery outside target rangeI=Isotope ratio out of specification
EDL = Estimated Detection Limit
Page 14 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 69 of 73
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
BLANK-108589L231009A_07
SMT
1020 mLL230816L231009A_01 & L231009B_01
MatrixDilutionExtractedAnalyzed
Water
10/05/2023 09:1010/09/2023 12:21
NA
Method 8290A Blank Analysis Results
Lab Sample Name DFBLKQZ
NativeIsomers pg/LConc EMPCpg/L pg/L InternalStandards Addedng's PercentRecoveryEDL
2,3,7,8-TCDF ND -----0.96 2,3,7,8-TCDF-13C 2.00 68Total TCDF ND -----0.96 2,3,7,8-TCDD-13C 2.00 22 R1,2,3,7,8-PeCDF-13C 2.00 742,3,7,8-TCDD ND -----3.7 2,3,4,7,8-PeCDF-13C 2.00 79Total TCDD ND -----3.7 1,2,3,7,8-PeCDD-13C 2.00 821,2,3,4,7,8-HxCDF-13C 2.00 621,2,3,7,8-PeCDF -----1.9 0.78 IJ 1,2,3,6,7,8-HxCDF-13C 2.00 572,3,4,7,8-PeCDF 0.91 -----0.54 J 2,3,4,6,7,8-HxCDF-13C 2.00 83Total PeCDF 0.91 -----0.54 J 1,2,3,7,8,9-HxCDF-13C 2.00 671,2,3,4,7,8-HxCDD-13C 2.00 851,2,3,7,8-PeCDD -----0.96 0.72 IJ 1,2,3,6,7,8-HxCDD-13C 2.00 81Total PeCDD ND -----0.72 1,2,3,4,6,7,8-HpCDF-13C 2.00 651,2,3,4,7,8,9-HpCDF-13C 2.00 521,2,3,4,7,8-HxCDF ND -----0.94 1,2,3,4,6,7,8-HpCDD-13C 2.00 751,2,3,6,7,8-HxCDF ND -----0.97 OCDD-13C 4.00 592,3,4,6,7,8-HxCDF 0.92 -----0.76 J1,2,3,7,8,9-HxCDF 1.6 -----1.0 J 1,2,3,4-TCDD-13C 2.00 NATotal HxCDF 2.5 -----0.76 J 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7,8-HxCDD -----2.1 0.71 IJ 2,3,7,8-TCDD-37Cl4 0.20 241,2,3,6,7,8-HxCDD -----0.75 0.67 IJ1,2,3,7,8,9-HxCDD -----1.0 0.67 IJTotal HxCDD ND -----0.67
1,2,3,4,6,7,8-HpCDF -----2.5 1.7 IJ Total 2,3,7,8-TCDD1,2,3,4,7,8,9-HpCDF ND -----3.7 Equivalence: 2.0 pg/LTotal HpCDF 4.5 -----1.7 J (Lower-bound - Using 2005 WHO Factors)
1,2,3,4,6,7,8-HpCDD 3.2 -----1.6 JTotal HpCDD 3.2 -----1.6 J
OCDF 17 -----2.6 JOCDD40-----3.8 J
Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).EMPC=EstimatedMaximumPossibleConcentration
J =Estimated value
R =Recovery outside target range
I =Isotope ratio out of specification
EDL=EstimatedDetection Limit
Page 15 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 70 of 73
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCS-108590L231009A_04
SMT
1020 mLL230816L231009A_01 & L231009B_01
MatrixDilutionExtractedAnalyzed
Water
10/05/2023 09:1010/09/2023 10:15
NA
Method Blank ID BLANK-108589
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.19 2,3,7,8-TCDF-13C 2.0 7296Total TCDF 2,3,7,8-TCDD-13C 2.0 36 R1,2,3,7,8-PeCDF-13C 2.0 742,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.0 76103Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 831,2,3,4,7,8-HxCDF-13C 2.0 631,2,3,7,8-PeCDF 1.0 0.95 1,2,3,6,7,8-HxCDF-13C 2.0 76952,3,4,7,8-PeCDF 1.0 0.98 2,3,4,6,7,8-HxCDF-13C 2.0 8298Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 761,2,3,4,7,8-HxCDD-13C 2.0 821,2,3,7,8-PeCDD 1.0 0.90 1,2,3,6,7,8-HxCDD-13C 2.0 8490Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 721,2,3,4,7,8,9-HpCDF-13C 2.0 651,2,3,4,7,8-HxCDF 1.0 0.88 1,2,3,4,6,7,8-HpCDD-13C 2.0 81881,2,3,6,7,8-HxCDF 1.0 0.97 OCDD-13C 4.0 68972,3,4,6,7,8-HxCDF 1.0 0.99 991,2,3,7,8,9-HxCDF 1.0 0.94 1,2,3,4-TCDD-13C 2.0 NA94Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.0 2,3,7,8-TCDD-37Cl4 0.20 391041,2,3,6,7,8-HxCDD 1.0 0.93 931,2,3,7,8,9-HxCDD 1.0 0.95 95Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.93 931,2,3,4,7,8,9-HpCDF 1.0 1.0 100Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.90 90Total HpCDD
OCDF 2.0 2.1 104OCDD2.0 2.0 102
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 16 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 71 of 73
REPORTOF LABORATORY ANALYSIS
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Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Lab Sample ID
Injected By
FilenameTotal Amount ExtractedICAL IDCCal Filename(s)
LCSD-108591L231009A_05
SMT
1020 mLL230816L231009A_01 & L231009B_01
MatrixDilutionExtractedAnalyzed
Water
10/05/2023 09:1010/09/2023 10:57
NA
Method Blank ID BLANK-108589
Method 8290A Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDF 0.20 0.19 2,3,7,8-TCDF-13C 2.0 5994Total TCDF 2,3,7,8-TCDD-13C 2.0 18 R1,2,3,7,8-PeCDF-13C 2.0 592,3,7,8-TCDD 0.20 0.21 2,3,4,7,8-PeCDF-13C 2.0 62104Total TCDD 1,2,3,7,8-PeCDD-13C 2.0 671,2,3,4,7,8-HxCDF-13C 2.0 541,2,3,7,8-PeCDF 1.0 0.95 1,2,3,6,7,8-HxCDF-13C 2.0 40952,3,4,7,8-PeCDF 1.0 0.95 2,3,4,6,7,8-HxCDF-13C 2.0 7395Total PeCDF 1,2,3,7,8,9-HxCDF-13C 2.0 611,2,3,4,7,8-HxCDD-13C 2.0 721,2,3,7,8-PeCDD 1.0 0.87 1,2,3,6,7,8-HxCDD-13C 2.0 7387Total PeCDD 1,2,3,4,6,7,8-HpCDF-13C 2.0 561,2,3,4,7,8,9-HpCDF-13C 2.0 441,2,3,4,7,8-HxCDF 1.0 0.87 1,2,3,4,6,7,8-HpCDD-13C 2.0 65871,2,3,6,7,8-HxCDF 1.0 1.0 OCDD-13C 4.0 531032,3,4,6,7,8-HxCDF 1.0 0.96 961,2,3,7,8,9-HxCDF 1.0 0.93 1,2,3,4-TCDD-13C 2.0 NA93Total HxCDF 1,2,3,7,8,9-HxCDD-13C 2.0 NA
1,2,3,4,7,8-HxCDD 1.0 1.0 2,3,7,8-TCDD-37Cl4 0.20 201031,2,3,6,7,8-HxCDD 1.0 0.94 941,2,3,7,8,9-HxCDD 1.0 0.92 92Total HxCDD
1,2,3,4,6,7,8-HpCDF 1.0 0.92 921,2,3,4,7,8,9-HpCDF 1.0 0.99 99Total HpCDF
1,2,3,4,6,7,8-HpCDD 1.0 0.86 86Total HpCDD
OCDF 2.0 2.0 101OCDD2.0 2.0 101
Qs = Quantity SpikedQm = Quantity Measured
Rec.=Recovery (Expressedas Percent)R=Recoveryoutsideof target range
Y =RF averaging used in calculationsNn=Value obtained from additional analysis
NA = Not Applicable* =See Discussion
Page 17 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 72 of 73
REPORTOF LABORATORY ANALYSIS
This report shall notbe reproduced,except in full,without thewrittenconsentofPaceAnalyticalServices,Inc.
Pace Analytical Services,LLC1700 Elm Street - Suite 200Minneapolis, MN 55414
Tel:[phone]Fax:[phone]
Client
Spike 1 IDSpike 1 Filename L231009A_04LCS-108590
PACE Charlotte
Spike Recovery Relative Percent Difference (RPD) Results
Spike 2 IDSpike 2 Filename L231009A_05LCSD-108591
Method 8290A
Spike 1 Spike 2Compound%REC %REC %RPD
2,3,7,8-TCDF 96 94 2.12,3,7,8-TCDD 103 104 1.01,2,3,7,8-PeCDF 95 95 0.02,3,4,7,8-PeCDF 98 95 3.11,2,3,7,8-PeCDD 90 87 3.41,2,3,4,7,8-HxCDF 88 87 1.11,2,3,6,7,8-HxCDF 97 103 6.02,3,4,6,7,8-HxCDF 99 96 3.11,2,3,7,8,9-HxCDF 94 93 1.11,2,3,4,7,8-HxCDD 104 103 1.01,2,3,6,7,8-HxCDD 93 94 1.11,2,3,7,8,9-HxCDD 95 92 3.21,2,3,4,6,7,8-HpCDF 93 92 1.11,2,3,4,7,8,9-HpCDF 100 99 1.01,2,3,4,6,7,8-HpCDD 90 86 4.5OCDF1041012.9OCDD1021011.0
%REC = Percent RecoveredRPD=The differencebetweenthetwo valuesdivided by the mean value
Page 18 of 18Report No.....10670284_SW8290AFC_L2_dfr
Page 73 of 73
#=CL#
November 07, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92693772
92693772
Project:
Pace Project No.:
RE:
Christina Ashdown
ENSAFE
313 Wingo Way
Mount Pleasant, SC 29464
Pactiv Evergreen Surface Water
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on October 17, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc:Jennings Kerr, ENSAFE Inc.
Lab, ENSAFE Inc.
David Warren, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Pace Analytical Services Ormond Beach
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Pace Analytical Services Charlotte
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9800 Kincey Ave. Ste 100, Huntersville, NC 28078
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REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 33
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Lab ID Sample ID Matrix Date Collected Date Received
92693772001 RW05WG-10172023 Water 10/17/23 12:25 10/17/23 15:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 3 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92693772001 RW05WG-10172023 EPA 200.7 5 PASI-OAAM1
EPA 200.7 5 PASI-OAAM1, AME
EPA 200.8 16 PASI-OLEC
EPA 200.8 16 PASI-OLEC
EPA 245.1 1 PASI-OLEC
EPA 245.1 1 PASI-OLEC
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Sample: RW05WG-10172023 Lab ID: 92693772001 Collected: 10/17/23 12:25 Received: 10/17/23 15:43 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Boron 2210J ug/L 10/30/23 11:05 7440-42-8 D310/28/23 00:292500 620 1
Calcium 21200J ug/L 10/30/23 11:05 7440-70-2 D310/28/23 00:2925000 9500 1
Iron 3460 ug/L 10/30/23 11:05 7439-89-6 D310/28/23 00:292000 1250 1
Magnesium ND ug/L 10/30/23 11:05 7439-95-4 D310/28/23 00:2925000 4200 1
Sodium 6570000 ug/L 10/30/23 11:05 7440-23-5 D310/28/23 00:29100000 27000 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Boron, Dissolved 4420 ug/L 10/30/23 10:24 7440-42-8 D310/28/23 00:292500 620 1
Calcium, Dissolved 11500J ug/L 10/30/23 10:24 7440-70-2 D310/28/23 00:2925000 9500 1
Iron, Dissolved 1320J ug/L 10/30/23 10:24 7439-89-6 D310/28/23 00:292000 1250 1
Magnesium, Dissolved ND ug/L 10/30/23 10:24 7439-95-4 D310/28/23 00:2925000 4200 1
Sodium, Dissolved 13500000 ug/L 10/31/23 14:25 7440-23-5 D310/28/23 00:29500000 135000 5
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS
Aluminum 2750 ug/L 10/29/23 14:52 7429-90-510/28/23 00:29500 432 1
Arsenic 322 ug/L 10/29/23 14:52 7440-38-210/28/23 00:2950.0 25.0 1
Barium 166 ug/L 10/29/23 14:52 7440-39-310/28/23 00:2950.0 25.0 1
Beryllium 2.7J ug/L 10/29/23 14:52 7440-41-710/28/23 00:295.0 1.6 1
Cadmium ND ug/L 10/29/23 14:52 7440-43-910/28/23 00:295.0 3.4 1
Chromium 151 ug/L 10/29/23 14:52 7440-47-310/28/23 00:2950.0 25.0 1
Cobalt ND ug/L 10/29/23 14:52 7440-48-410/28/23 00:2950.0 12.2 1
Copper 62.9 ug/L 10/29/23 14:52 7440-50-810/28/23 00:2950.0 21.0 1
Lead 250 ug/L 10/29/23 14:52 7439-92-110/28/23 00:2950.0 11.0 1
Manganese 129 ug/L 10/29/23 14:52 7439-96-510/28/23 00:2950.0 14.6 1
Molybdenum 126 ug/L 10/29/23 14:52 7439-98-710/28/23 00:2950.0 11.1 1
Nickel 135 ug/L 10/29/23 14:52 7440-02-010/28/23 00:2950.0 13.2 1
Selenium ND ug/L 10/29/23 14:52 7782-49-210/28/23 00:29100 10 1
Silver ND ug/L 10/29/23 14:52 7440-22-410/28/23 00:2925.0 1.4 1
Thallium ND ug/L 10/29/23 14:52 7440-28-010/28/23 00:2950.0 5.3 1
Zinc 1710 ug/L 10/29/23 14:52 7440-66-610/28/23 00:29500 336 1
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS, Dissolved
Aluminum, Dissolved 4950 ug/L 10/29/23 15:13 7429-90-510/28/23 00:29500 432 1
Arsenic, Dissolved 613 ug/L 10/29/23 15:13 7440-38-210/28/23 00:2950.0 25.0 1
Barium, Dissolved 216 ug/L 10/29/23 15:13 7440-39-310/28/23 00:2950.0 25.0 1
Beryllium, Dissolved 3.8J ug/L 10/29/23 15:13 7440-41-710/28/23 00:295.0 1.6 1
Cadmium, Dissolved ND ug/L 10/29/23 15:13 7440-43-910/28/23 00:295.0 3.4 1
Chromium, Dissolved 199 ug/L 10/29/23 15:13 7440-47-310/28/23 00:2950.0 25.0 1
Cobalt, Dissolved ND ug/L 10/29/23 15:13 7440-48-410/28/23 00:2950.0 12.2 1
Copper, Dissolved ND ug/L 10/29/23 15:13 7440-50-810/28/23 00:2950.0 21.0 1
Lead, Dissolved 30.9J ug/L 10/29/23 15:13 7439-92-110/28/23 00:2950.0 11.0 1
Manganese, Dissolved 44.9J ug/L 10/29/23 15:13 7439-96-510/28/23 00:2950.0 14.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Sample: RW05WG-10172023 Lab ID: 92693772001 Collected: 10/17/23 12:25 Received: 10/17/23 15:43 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS, Dissolved
Molybdenum, Dissolved 235 ug/L 10/29/23 15:13 7439-98-710/28/23 00:2950.0 11.1 1
Nickel, Dissolved 189 ug/L 10/29/23 15:13 7440-02-010/28/23 00:2950.0 13.2 1
Selenium, Dissolved 10J ug/L 10/29/23 15:13 7782-49-210/28/23 00:29100 10 1
Silver, Dissolved ND ug/L 10/29/23 15:13 7440-22-410/28/23 00:2925.0 1.4 1
Thallium, Dissolved ND ug/L 10/29/23 15:13 7440-28-010/28/23 00:2950.0 5.3 1
Zinc, Dissolved ND ug/L 10/29/23 15:13 7440-66-610/28/23 00:29500 336 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/30/23 16:26 7439-97-6 D310/30/23 09:148.0 5.6 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/30/23 16:38 7439-97-6 D310/30/23 09:148.0 5.6 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene 12.4 ug/L 10/24/23 19:43 83-32-910/23/23 12:398.7 1.7 1
Acenaphthylene ND ug/L 10/24/23 19:43 208-96-810/23/23 12:398.7 1.7 1
Acetophenone ND ug/L 10/24/23 19:43 98-86-210/23/23 12:398.7 1.3 1
Anthracene ND ug/L 10/24/23 19:43 120-12-710/23/23 12:398.7 2.0 1
Atrazine ND ug/L 10/24/23 19:43 1912-24-9 L110/23/23 12:398.7 2.8 1
Benzaldehyde ND ug/L 10/24/23 19:43 100-52-7 v210/23/23 12:398.7 3.1 1
Benzo(a)anthracene ND ug/L 10/24/23 19:43 56-55-310/23/23 12:398.7 2.3 1
Benzo(a)pyrene ND ug/L 10/24/23 19:43 50-32-810/23/23 12:398.7 2.4 1
Benzo(b)fluoranthene ND ug/L 10/24/23 19:43 205-99-210/23/23 12:398.7 2.3 1
Benzo(g,h,i)perylene ND ug/L 10/24/23 19:43 191-24-210/23/23 12:398.7 2.5 1
Benzo(k)fluoranthene ND ug/L 10/24/23 19:43 207-08-910/23/23 12:398.7 2.4 1
Biphenyl (Diphenyl)2.3J ug/L 10/24/23 19:43 92-52-410/23/23 12:398.7 1.6 1
4-Bromophenylphenyl ether ND ug/L 10/24/23 19:43 101-55-310/23/23 12:398.7 1.5 1
Butylbenzylphthalate ND ug/L 10/24/23 19:43 85-68-710/23/23 12:398.7 2.7 1
Caprolactam ND ug/L 10/24/23 19:43 105-60-210/23/23 12:398.7 6.0 1
Carbazole 12.0 ug/L 10/24/23 19:43 86-74-810/23/23 12:398.7 2.0 1
4-Chloro-3-methylphenol ND ug/L 10/24/23 19:43 59-50-710/23/23 12:398.7 2.9 1
4-Chloroaniline ND ug/L 10/24/23 19:43 106-47-810/23/23 12:3917.4 3.2 1
bis(2-Chloroethoxy)methane ND ug/L 10/24/23 19:43 111-91-110/23/23 12:398.7 1.6 1
bis(2-Chloroethyl) ether ND ug/L 10/24/23 19:43 111-44-410/23/23 12:398.7 1.7 1
2-Chloronaphthalene ND ug/L 10/24/23 19:43 91-58-710/23/23 12:398.7 1.5 1
2-Chlorophenol ND ug/L 10/24/23 19:43 95-57-810/23/23 12:398.7 1.0 1
4-Chlorophenylphenyl ether ND ug/L 10/24/23 19:43 7005-72-310/23/23 12:398.7 1.7 1
Chrysene ND ug/L 10/24/23 19:43 218-01-910/23/23 12:398.7 2.4 1
Dibenz(a,h)anthracene ND ug/L 10/24/23 19:43 53-70-310/23/23 12:398.7 2.6 1
Dibenzofuran 5.0J ug/L 10/24/23 19:43 132-64-910/23/23 12:398.7 1.8 1
3,3'-Dichlorobenzidine ND ug/L 10/24/23 19:43 91-94-110/23/23 12:3917.4 7.1 1
2,4-Dichlorophenol ND ug/L 10/24/23 19:43 120-83-210/23/23 12:398.7 1.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Sample: RW05WG-10172023 Lab ID: 92693772001 Collected: 10/17/23 12:25 Received: 10/17/23 15:43 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Diethylphthalate ND ug/L 10/24/23 19:43 84-66-210/23/23 12:398.7 1.8 1
2,4-Dimethylphenol 1.7J ug/L 10/24/23 19:43 105-67-910/23/23 12:398.7 1.5 1
Dimethylphthalate ND ug/L 10/24/23 19:43 131-11-310/23/23 12:398.7 1.9 1
Di-n-butylphthalate ND ug/L 10/24/23 19:43 84-74-210/23/23 12:398.7 1.9 1
4,6-Dinitro-2-methylphenol ND ug/L 10/24/23 19:43 534-52-110/23/23 12:3917.4 6.8 1
2,4-Dinitrophenol ND ug/L 10/24/23 19:43 51-28-510/23/23 12:3943.5 22.6 1
2,4-Dinitrotoluene ND ug/L 10/24/23 19:43 121-14-210/23/23 12:398.7 1.4 1
2,6-Dinitrotoluene ND ug/L 10/24/23 19:43 606-20-210/23/23 12:398.7 1.5 1
Di-n-octylphthalate ND ug/L 10/24/23 19:43 117-84-010/23/23 12:398.7 3.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/24/23 19:43 117-81-710/23/23 12:395.2 3.2 1
Fluoranthene ND ug/L 10/24/23 19:43 206-44-010/23/23 12:398.7 1.9 1
Fluorene 4.3J ug/L 10/24/23 19:43 86-73-710/23/23 12:398.7 1.8 1
Hexachloro-1,3-butadiene ND ug/L 10/24/23 19:43 87-68-310/23/23 12:398.7 1.5 1
Hexachlorobenzene ND ug/L 10/24/23 19:43 118-74-110/23/23 12:398.7 1.9 1
Hexachlorocyclopentadiene ND ug/L 10/24/23 19:43 77-47-410/23/23 12:398.7 1.4 1
Hexachloroethane ND ug/L 10/24/23 19:43 67-72-110/23/23 12:398.7 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/24/23 19:43 193-39-510/23/23 12:398.7 2.5 1
Isophorone ND ug/L 10/24/23 19:43 78-59-110/23/23 12:398.7 1.4 1
2-Methylnaphthalene 17.7 ug/L 10/24/23 19:43 91-57-610/23/23 12:398.7 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 10/24/23 19:43 95-48-710/23/23 12:398.7 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/24/23 19:43 15831-10-410/23/23 12:398.7 1.1 1
Naphthalene 225 ug/L 10/25/23 14:02 91-20-310/23/23 12:3934.8 7.3 4
2-Nitroaniline ND ug/L 10/24/23 19:43 88-74-410/23/23 12:3917.4 2.6 1
3-Nitroaniline ND ug/L 10/24/23 19:43 99-09-210/23/23 12:3917.4 3.3 1
4-Nitroaniline ND ug/L 10/24/23 19:43 100-01-610/23/23 12:3917.4 4.4 1
Nitrobenzene ND ug/L 10/24/23 19:43 98-95-310/23/23 12:398.7 1.6 1
2-Nitrophenol ND ug/L 10/24/23 19:43 88-75-510/23/23 12:398.7 1.2 1
4-Nitrophenol ND ug/L 10/24/23 19:43 100-02-710/23/23 12:3943.5 5.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/24/23 19:43 621-64-710/23/23 12:398.7 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/24/23 19:43 86-30-610/23/23 12:398.7 2.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/24/23 19:43 108-60-110/23/23 12:398.7 1.0 1
Pentachlorophenol ND ug/L 10/24/23 19:43 87-86-510/23/23 12:3917.4 3.3 1
Phenanthrene 2.4J ug/L 10/24/23 19:43 85-01-810/23/23 12:398.7 1.7 1
Phenol 6.2J ug/L 10/24/23 19:43 108-95-210/23/23 12:398.7 1.2 1
Pyrene ND ug/L 10/24/23 19:43 129-00-010/23/23 12:398.7 1.9 1
2,4,5-Trichlorophenol ND ug/L 10/24/23 19:43 95-95-4 v110/23/23 12:398.7 1.2 1
2,4,6-Trichlorophenol ND ug/L 10/24/23 19:43 88-06-2 v110/23/23 12:398.7 1.3 1
Surrogates
Nitrobenzene-d5 (S)54 %10/24/23 19:43 4165-60-0 1g10/23/23 12:3910-133 1
2-Fluorobiphenyl (S)59 %10/24/23 19:43 321-60-810/23/23 12:3910-130 1
Terphenyl-d14 (S)75 %10/24/23 19:43 1718-51-010/23/23 12:3910-193 1
Phenol-d6 (S)20 %10/24/23 19:43 13127-88-310/23/23 12:3910-130 1
2-Fluorophenol (S)2 %10/24/23 19:43 367-12-4 S210/23/23 12:3910-130 1
2,4,6-Tribromophenol (S)5 %10/24/23 19:43 118-79-6 S210/23/23 12:3910-166 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Sample: RW05WG-10172023 Lab ID: 92693772001 Collected: 10/17/23 12:25 Received: 10/17/23 15:43 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 85.5J ug/L 10/19/23 04:59 67-64-1250 51.1 10
Benzene ND ug/L 10/19/23 04:59 71-43-210.0 3.4 10
Bromodichloromethane ND ug/L 10/19/23 04:59 75-27-410.0 3.1 10
Bromoform ND ug/L 10/19/23 04:59 75-25-210.0 3.4 10
Bromomethane ND ug/L 10/19/23 04:59 74-83-920.0 16.6 10
2-Butanone (MEK)ND ug/L 10/19/23 04:59 78-93-350.0 39.6 10
Carbon disulfide ND ug/L 10/19/23 04:59 75-15-020.0 3.6 10
Carbon tetrachloride ND ug/L 10/19/23 04:59 56-23-510.0 3.3 10
Chlorobenzene ND ug/L 10/19/23 04:59 108-90-710.0 2.8 10
Chloroethane ND ug/L 10/19/23 04:59 75-00-310.0 6.5 10
Chloroform ND ug/L 10/19/23 04:59 67-66-310.0 4.3 10
Chloromethane ND ug/L 10/19/23 04:59 74-87-310.0 5.4 10
Cyclohexane ND ug/L 10/19/23 04:59 110-82-710.0 3.5 10
1,2-Dibromo-3-chloropropane ND ug/L 10/19/23 04:59 96-12-820.0 3.4 10
Dibromochloromethane ND ug/L 10/19/23 04:59 124-48-110.0 3.6 10
1,2-Dibromoethane (EDB)ND ug/L 10/19/23 04:59 106-93-410.0 2.7 10
1,2-Dichlorobenzene ND ug/L 10/19/23 04:59 95-50-110.0 3.4 10
1,3-Dichlorobenzene ND ug/L 10/19/23 04:59 541-73-110.0 3.4 10
1,4-Dichlorobenzene ND ug/L 10/19/23 04:59 106-46-710.0 3.3 10
Dichlorodifluoromethane ND ug/L 10/19/23 04:59 75-71-810.0 3.5 10
1,1-Dichloroethane ND ug/L 10/19/23 04:59 75-34-310.0 3.7 10
1,2-Dichloroethane ND ug/L 10/19/23 04:59 107-06-210.0 3.2 10
1,1-Dichloroethene ND ug/L 10/19/23 04:59 75-35-410.0 3.5 10
cis-1,2-Dichloroethene ND ug/L 10/19/23 04:59 156-59-210.0 3.8 10
trans-1,2-Dichloroethene ND ug/L 10/19/23 04:59 156-60-510.0 4.0 10
1,2-Dichloropropane ND ug/L 10/19/23 04:59 78-87-510.0 3.6 10
cis-1,3-Dichloropropene ND ug/L 10/19/23 04:59 10061-01-510.0 3.6 10
trans-1,3-Dichloropropene ND ug/L 10/19/23 04:59 10061-02-610.0 3.6 10
Ethylbenzene 4.6J ug/L 10/19/23 04:59 100-41-410.0 3.0 10
2-Hexanone ND ug/L 10/19/23 04:59 591-78-650.0 4.8 10
Isopropylbenzene (Cumene)ND ug/L 10/19/23 04:59 98-82-810.0 3.3 10
Methyl acetate ND ug/L 10/19/23 04:59 79-20-9100 23.9 10
Methylcyclohexane ND ug/L 10/19/23 04:59 108-87-2100 15.1 10
Methylene Chloride ND ug/L 10/19/23 04:59 75-09-250.0 19.5 10
4-Methyl-2-pentanone (MIBK)ND ug/L 10/19/23 04:59 108-10-150.0 27.1 10
Methyl-tert-butyl ether ND ug/L 10/19/23 04:59 1634-04-410.0 4.2 10
Styrene ND ug/L 10/19/23 04:59 100-42-510.0 2.9 10
1,1,2,2-Tetrachloroethane ND ug/L 10/19/23 04:59 79-34-510.0 2.2 10
Tetrachloroethene ND ug/L 10/19/23 04:59 127-18-410.0 2.9 10
Toluene 8.8J ug/L 10/19/23 04:59 108-88-310.0 2.4 10
1,2,4-Trichlorobenzene ND ug/L 10/19/23 04:59 120-82-110.0 6.4 10
1,1,1-Trichloroethane ND ug/L 10/19/23 04:59 71-55-610.0 3.3 10
1,1,2-Trichloroethane ND ug/L 10/19/23 04:59 79-00-510.0 3.2 10
Trichloroethene ND ug/L 10/19/23 04:59 79-01-610.0 3.8 10
Trichlorofluoromethane ND ug/L 10/19/23 04:59 75-69-410.0 3.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Sample: RW05WG-10172023 Lab ID: 92693772001 Collected: 10/17/23 12:25 Received: 10/17/23 15:43 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 10/19/23 04:59 76-13-110.0 3.2 10
Vinyl chloride ND ug/L 10/19/23 04:59 75-01-410.0 3.9 10
m&p-Xylene 9.1J ug/L 10/19/23 04:59 179601-23-120.0 7.1 10
o-Xylene 4.5J ug/L 10/19/23 04:59 95-47-610.0 3.4 10
Surrogates
4-Bromofluorobenzene (S)97 %10/19/23 04:59 460-00-4 D3,F170-130 10
1,2-Dichloroethane-d4 (S)101 %10/19/23 04:59 17060-07-070-130 10
Toluene-d8 (S)109 %10/19/23 04:59 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
962123
EPA 245.1
EPA 245.1
245.1 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92693772001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5291441
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/30/23 13:130.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5291442LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 1.82 88 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5291443MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35833416001
5291444
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 80 70-13078 3 2020.14U 1.6 1.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
962119
EPA 245.1
EPA 245.1
245.1 Mercury - Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92693772001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5291433
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/30/23 16:350.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5291434LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
5291435
Mercury, Dissolved ug/L 1.72 87 85-115891.8 2 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
961843
EPA 200.7
EPA 200.7
200.7 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92693772001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5289908
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
Boron ug/L ND 50.0 10/30/23 10:2712.4
Calcium ug/L ND 500 10/30/23 10:27190
Iron ug/L ND 40.0 10/30/23 10:2725.0
Magnesium ug/L ND 500 10/30/23 10:2784.0
Sodium ug/L ND 2000 10/30/23 10:27540
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5289909LABORATORY CONTROL SAMPLE:
LCSSpike
Boron ug/L 12901250 103 85-115
Calcium ug/L 1330012500 106 85-115
Iron ug/L 25902500 103 85-115
Magnesium ug/L 1340012500 108 85-115
Sodium ug/L 1240012500 99 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5289910MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
20294002004
5289911
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Boron ug/L 1250 106 70-130106 0 2012501031430 1430
Calcium ug/L 12500 106 70-130109 1 20125004170055000 55400
Iron ug/L 2500 104 70-130103 1 202500ND2600 2590
Magnesium ug/L 12500 108 70-130108 0 20125001160025100 25100
Sodium ug/L 12500 110 70-130113 1 20125003930053000 53500
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5289912MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35837484002
5289913
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Boron ug/L M1125010770-130110 2 2012509672300 2350
Calcium ug/L 12500 101 70-130107 2 201250037.1 mg/L 49700 50500
Iron ug/L 2500 103 70-130102 0 2025001.2 mg/L 3820 3800
Magnesium ug/L 12500 106 70-130110 2 201250014.4 mg/L 27700 28200
Sodium ug/L 12500 84 70-130104 1 2012500183 mg/L 194000 196000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
961841
EPA 200.7
EPA 200.7
200.7 MET Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92693772001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5289898
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
Boron, Dissolved ug/L ND 50.0 10/30/23 09:5712.4
Calcium, Dissolved ug/L ND 500 10/30/23 09:57190
Iron, Dissolved ug/L ND 40.0 10/30/23 09:5725.0
Magnesium, Dissolved ug/L ND 500 10/30/23 09:5784.0
Sodium, Dissolved ug/L ND 2000 10/30/23 09:57540
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5289899LABORATORY CONTROL SAMPLE:
LCSSpike
Boron, Dissolved ug/L 13101250 104 85-115
Calcium, Dissolved ug/L 1340012500 107 85-115
Iron, Dissolved ug/L 26102500 104 85-115
Magnesium, Dissolved ug/L 1360012500 109 85-115
Sodium, Dissolved ug/L 1260012500 100 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5289900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35837063003
5289901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Boron, Dissolved ug/L 1250 105 70-130106 1 20125018.1J 1330 1340
Calcium, Dissolved ug/L 12500 104 70-130105 0 20125004870061700 61900
Iron, Dissolved ug/L 2500 104 70-130105 1 20250025.0U 2600 2630
Magnesium, Dissolved ug/L 12500 107 70-130109 1 2012500908022500 22700
Sodium, Dissolved ug/L 12500 104 70-130104 1 2012500649019400 19500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
961842
EPA 200.8
EPA 200.8
200.8 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92693772001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5289902
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
Aluminum ug/L ND 10.0 10/29/23 14:278.6
Arsenic ug/L ND 1.0 10/29/23 14:270.50
Barium ug/L ND 1.0 10/29/23 14:270.50
Beryllium ug/L ND 0.10 10/29/23 14:270.033
Cadmium ug/L ND 0.10 10/29/23 14:270.067
Chromium ug/L ND 1.0 10/29/23 14:270.50
Cobalt ug/L ND 1.0 10/29/23 14:270.24
Copper ug/L ND 1.0 10/29/23 14:270.42
Lead ug/L ND 1.0 10/29/23 14:270.22
Manganese ug/L ND 1.0 10/29/23 14:270.29
Molybdenum ug/L ND 1.0 10/29/23 14:270.22
Nickel ug/L ND 1.0 10/29/23 14:270.26
Selenium ug/L ND 2.0 10/29/23 14:270.20
Silver ug/L ND 0.50 10/29/23 14:270.028
Thallium ug/L ND 1.0 10/29/23 14:270.11
Zinc ug/L ND 10.0 10/29/23 14:276.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5289903LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum ug/L 525500 105 85-115
Arsenic ug/L 51.650 103 85-115
Barium ug/L 52.350 105 85-115
Beryllium ug/L 5.45 108 85-115
Cadmium ug/L 5.35 106 85-115
Chromium ug/L 51.450 103 85-115
Cobalt ug/L 52.950 106 85-115
Copper ug/L 55.250 110 85-115
Lead ug/L 54.550 109 85-115
Manganese ug/L 52.250 104 85-115
Molybdenum ug/L 51.250 102 85-115
Nickel ug/L 54.250 108 85-115
Selenium ug/L 51.150 102 85-115
Silver ug/L 5.45 109 85-115
Thallium ug/L 53.450 107 85-115
Zinc ug/L 266250 106 85-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5289904MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
20294002001
5289905
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 500 104 70-130103 1 20500ND521 517
Arsenic ug/L 50 100 70-13099 0 2050ND50.7 50.5
Barium ug/L 50 102 70-130101 1 2050ND52.1 51.4
Beryllium ug/L 5 109 70-130105 4 205ND5.4 5.2
Cadmium ug/L 5 99 70-130102 2 205ND5.0 5.1
Chromium ug/L 50 98 70-13097 1 2050ND49.5 49.0
Cobalt ug/L 50 101 70-130101 1 2050ND50.7 50.3
Copper ug/L 50 102 70-130103 0 20501.3 52.4 52.7
Lead ug/L 50 102 70-130102 0 2050ND51.1 51.0
Manganese ug/L 50 99 70-13097 2 2050ND49.6 48.7
Molybdenum ug/L 50 103 70-130103 1 20501.5 52.8 53.1
Nickel ug/L 50 101 70-130101 0 2050ND50.3 50.4
Selenium ug/L 50 96 70-13097 2 2050ND49.1 50.0
Silver ug/L 5 100 70-130102 2 205ND5.0 5.1
Thallium ug/L 50 102 70-130102 0 2050ND50.8 51.0
Zinc ug/L 250 98 70-13099 1 20250ND247 250
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5289906MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35837381001
5289907
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 500 109 70-130108 1 2050064.9 611 605
Arsenic ug/L 50 101 70-130101 0 20500.50U 51.1 50.9
Barium ug/L 50 102 70-130102 0 205010.6 61.8 61.5
Beryllium ug/L 5 107 70-130106 1 2050.033U 5.4 5.3
Cadmium ug/L 5 102 70-130103 1 2050.067U 5.1 5.2
Chromium ug/L 50 101 70-130102 0 20501.2 51.8 52.0
Cobalt ug/L 50 104 70-130102 2 20500.24U 51.8 50.9
Copper ug/L 50 105 70-130105 1 20500.42U 52.7 52.4
Lead ug/L 50 106 70-130107 1 20500.22U 53.2 53.5
Manganese ug/L 50 101 70-130101 0 205017.3 67.6 67.8
Molybdenum ug/L 50 102 70-130102 0 20500.49J 51.3 51.5
Nickel ug/L 50 104 70-130103 1 20500.26U 51.9 51.6
Selenium ug/L 50 100 70-130100 0 20500.37J 50.2 50.2
Silver ug/L 5 104 70-130106 2 2050.028U 5.2 5.3
Thallium ug/L 50 105 70-130106 0 20500.11U 52.7 52.9
Zinc ug/L 250 101 70-130102 2 202506.7U 252 256
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
961840
EPA 200.8
EPA 200.8
200.8 MET Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92693772001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5289892
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
Aluminum, Dissolved ug/L ND 10.0 10/29/23 14:558.6
Arsenic, Dissolved ug/L ND 1.0 10/29/23 14:550.50
Barium, Dissolved ug/L ND 1.0 10/29/23 14:550.50
Beryllium, Dissolved ug/L ND 0.10 10/29/23 14:550.033
Cadmium, Dissolved ug/L ND 0.10 10/29/23 14:550.067
Chromium, Dissolved ug/L ND 1.0 10/29/23 14:550.50
Cobalt, Dissolved ug/L ND 1.0 10/29/23 14:550.24
Copper, Dissolved ug/L ND 1.0 10/29/23 14:550.42
Lead, Dissolved ug/L ND 1.0 10/29/23 14:550.22
Manganese, Dissolved ug/L ND 1.0 10/29/23 14:550.29
Molybdenum, Dissolved ug/L ND 1.0 10/29/23 14:550.22
Nickel, Dissolved ug/L ND 1.0 10/29/23 14:550.26
Selenium, Dissolved ug/L ND 2.0 10/29/23 14:550.20
Silver, Dissolved ug/L ND 0.50 10/29/23 14:550.028
Thallium, Dissolved ug/L ND 1.0 10/29/23 14:550.11
Zinc, Dissolved ug/L ND 10.0 10/29/23 14:556.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5289893LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum, Dissolved ug/L 531500 106 85-115
Arsenic, Dissolved ug/L 51.350 103 85-115
Barium, Dissolved ug/L 52.350 105 85-115
Beryllium, Dissolved ug/L 5.55 110 85-115
Cadmium, Dissolved ug/L 5.25 104 85-115
Chromium, Dissolved ug/L 50.950 102 85-115
Cobalt, Dissolved ug/L 53.150 106 85-115
Copper, Dissolved ug/L 54.850 110 85-115
Lead, Dissolved ug/L 54.750 109 85-115
Manganese, Dissolved ug/L 51.750 103 85-115
Molybdenum, Dissolved ug/L 50.750 101 85-115
Nickel, Dissolved ug/L 53.350 107 85-115
Selenium, Dissolved ug/L 51.050 102 85-115
Silver, Dissolved ug/L 5.45 107 85-115
Thallium, Dissolved ug/L 53.350 107 85-115
Zinc, Dissolved ug/L 262250 105 85-115
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
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Page 16 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5289894MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35837063001
5289895
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum, Dissolved ug/L 500 104 70-130105 1 205008.6U 521 526
Arsenic, Dissolved ug/L 50 102 70-130100 2 20500.50U 51.0 50.1
Barium, Dissolved ug/L 50 103 70-130104 0 20509.8 61.6 61.7
Beryllium, Dissolved ug/L 5 105 70-130105 0 2050.035J 5.3 5.3
Cadmium, Dissolved ug/L 5 103 70-130103 1 2050.067U 5.1 5.2
Chromium, Dissolved ug/L 50 102 70-130101 1 20500.50U 51.1 50.6
Cobalt, Dissolved ug/L 50 104 70-130100 4 20500.24U 51.9 50.1
Copper, Dissolved ug/L 50 105 70-130102 3 20500.42U 52.7 51.1
Lead, Dissolved ug/L 50 107 70-130107 0 20500.22U 53.5 53.3
Manganese, Dissolved ug/L 50 103 70-130101 1 20504.1 55.7 54.9
Molybdenum, Dissolved ug/L 50 104 70-130101 2 20502.8 54.6 53.2
Nickel, Dissolved ug/L 50 105 70-130102 3 20500.26U 52.5 51.2
Selenium, Dissolved ug/L 50 96 70-13096 1 20500.20U 48.4 48.0
Silver, Dissolved ug/L 5 104 70-130102 2 2050.028U 5.2 5.1
Thallium, Dissolved ug/L 50 105 70-130105 0 20500.11U 52.7 52.7
Zinc, Dissolved ug/L 250 101 70-13099 2 202506.7U 255 249
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807365
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92693772001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4180695
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 10/19/23 00:270.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/19/23 00:270.22
1,1,2-Trichloroethane ug/L ND 1.0 10/19/23 00:270.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 10/19/23 00:270.32
1,1-Dichloroethane ug/L ND 1.0 10/19/23 00:270.37
1,1-Dichloroethene ug/L ND 1.0 10/19/23 00:270.35
1,2,4-Trichlorobenzene ug/L ND 1.0 10/19/23 00:270.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/19/23 00:270.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/19/23 00:270.27
1,2-Dichlorobenzene ug/L ND 1.0 10/19/23 00:270.34
1,2-Dichloroethane ug/L ND 1.0 10/19/23 00:270.32
1,2-Dichloropropane ug/L ND 1.0 10/19/23 00:270.36
1,3-Dichlorobenzene ug/L ND 1.0 10/19/23 00:270.34
1,4-Dichlorobenzene ug/L ND 1.0 10/19/23 00:270.33
2-Butanone (MEK)ug/L ND 5.0 10/19/23 00:274.0
2-Hexanone ug/L ND 5.0 10/19/23 00:270.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/19/23 00:272.7
Acetone ug/L ND 25.0 10/19/23 00:275.1
Benzene ug/L ND 1.0 10/19/23 00:270.34
Bromodichloromethane ug/L ND 1.0 10/19/23 00:270.31
Bromoform ug/L ND 1.0 10/19/23 00:270.34
Bromomethane ug/L ND 2.0 10/19/23 00:271.7
Carbon disulfide ug/L ND 2.0 10/19/23 00:270.36
Carbon tetrachloride ug/L ND 1.0 10/19/23 00:270.33
Chlorobenzene ug/L ND 1.0 10/19/23 00:270.28
Chloroethane ug/L ND 1.0 10/19/23 00:270.65
Chloroform ug/L ND 1.0 10/19/23 00:270.43
Chloromethane ug/L ND 1.0 10/19/23 00:270.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/19/23 00:270.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/19/23 00:270.36
Cyclohexane ug/L ND 1.0 10/19/23 00:270.35
Dibromochloromethane ug/L ND 1.0 10/19/23 00:270.36
Dichlorodifluoromethane ug/L ND 1.0 10/19/23 00:270.35
Ethylbenzene ug/L ND 1.0 10/19/23 00:270.30
Isopropylbenzene (Cumene)ug/L ND 1.0 10/19/23 00:270.33
m&p-Xylene ug/L ND 2.0 10/19/23 00:270.71
Methyl acetate ug/L ND 10.0 10/19/23 00:272.4
Methyl-tert-butyl ether ug/L ND 1.0 10/19/23 00:270.42
Methylcyclohexane ug/L ND 10.0 10/19/23 00:271.5
Methylene Chloride ug/L ND 5.0 10/19/23 00:272.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4180695
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 10/19/23 00:270.34
Styrene ug/L ND 1.0 10/19/23 00:270.29
Tetrachloroethene ug/L ND 1.0 10/19/23 00:270.29
Toluene ug/L ND 1.0 10/19/23 00:270.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/19/23 00:270.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/19/23 00:270.36
Trichloroethene ug/L ND 1.0 10/19/23 00:270.38
Trichlorofluoromethane ug/L ND 1.0 10/19/23 00:270.30
Vinyl chloride ug/L ND 1.0 10/19/23 00:270.39
1,2-Dichloroethane-d4 (S)%100 70-130 10/19/23 00:27
4-Bromofluorobenzene (S)%100 70-130 10/19/23 00:27
Toluene-d8 (S)%106 70-130 10/19/23 00:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4180696LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.320 101 70-130
1,1,2,2-Tetrachloroethane ug/L 20.620 103 70-130
1,1,2-Trichloroethane ug/L 20.320 102 70-130
1,1,2-Trichlorotrifluoroethane ug/L 21.020 105 70-132
1,1-Dichloroethane ug/L 19.820 99 70-130
1,1-Dichloroethene ug/L 21.420 107 69-131
1,2,4-Trichlorobenzene ug/L 19.620 98 70-130
1,2-Dibromo-3-chloropropane ug/L 19.120 96 70-130
1,2-Dibromoethane (EDB)ug/L 20.020 100 70-130
1,2-Dichlorobenzene ug/L 21.020 105 70-130
1,2-Dichloroethane ug/L 20.620 103 70-130
1,2-Dichloropropane ug/L 20.920 105 70-130
1,3-Dichlorobenzene ug/L 20.920 104 70-130
1,4-Dichlorobenzene ug/L 20.720 103 70-130
2-Butanone (MEK)ug/L 32.440 81 67-133
2-Hexanone ug/L 38.540 96 70-133
4-Methyl-2-pentanone (MIBK)ug/L 37.140 93 70-130
Acetone ug/L 38.840 97 67-130
Benzene ug/L 20.820 104 70-130
Bromodichloromethane ug/L 20.420 102 70-130
Bromoform ug/L 18.420 92 70-133
Bromomethane ug/L 19.220 96 41-148
Carbon disulfide ug/L 21.020 105 70-131
Carbon tetrachloride ug/L 20.920 105 70-130
Chlorobenzene ug/L 20.320 101 70-130
Chloroethane ug/L 21.020 105 41-157
Chloroform ug/L 20.020 100 70-130
Chloromethane ug/L 18.920 94 59-141
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4180696LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 19.620 98 70-130
cis-1,3-Dichloropropene ug/L 19.920 100 70-130
Cyclohexane ug/L 19.420 97 63-137
Dibromochloromethane ug/L 19.520 97 70-130
Dichlorodifluoromethane ug/L 25.720 129 54-147
Ethylbenzene ug/L 20.020 100 70-130
Isopropylbenzene (Cumene)ug/L 20.120 101 70-130
m&p-Xylene ug/L 39.440 98 70-130
Methyl acetate ug/L 16.820 84 70-130
Methyl-tert-butyl ether ug/L 18.520 93 70-130
Methylcyclohexane ug/L 20.820 104 70-130
Methylene Chloride ug/L 20.720 103 62-130
o-Xylene ug/L 19.620 98 70-130
Styrene ug/L 19.720 99 70-130
Tetrachloroethene ug/L 19.220 96 70-130
Toluene ug/L 20.220 101 70-130
trans-1,2-Dichloroethene ug/L 19.820 99 70-130
trans-1,3-Dichloropropene ug/L 19.120 95 70-130
Trichloroethene ug/L 20.920 105 70-130
Trichlorofluoromethane ug/L 21.620 108 57-130
Vinyl chloride ug/L 17.320 87 66-140
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%104 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4180698MATRIX SPIKE SAMPLE:
MSSpike
Result
92693480007
1,1,1-Trichloroethane ug/L 23.120 116 70-150<1.0
1,1,2,2-Tetrachloroethane ug/L 21.020 105 66-144<1.0
1,1,2-Trichloroethane ug/L 21.020 105 70-142<1.0
1,1,2-Trichlorotrifluoroethane ug/L 27.420 137 66-168<1.0
1,1-Dichloroethane ug/L 21.520 107 68-150<1.0
1,1-Dichloroethene ug/L 24.720 123 64-162<1.0
1,2,4-Trichlorobenzene ug/L 21.020 105 69-147<1.0
1,2-Dibromo-3-chloropropane ug/L 20.220 101 62-146<2.0
1,2-Dibromoethane (EDB)ug/L 19.820 99 70-143<1.0
1,2-Dichlorobenzene ug/L 21.520 107 70-142<1.0
1,2-Dichloroethane ug/L 21.620 108 68-145<1.0
1,2-Dichloropropane ug/L 21.720 108 70-144<1.0
1,3-Dichlorobenzene ug/L 21.920 109 70-142<1.0
1,4-Dichlorobenzene ug/L 22.020 110 70-140<1.0
2-Butanone (MEK)ug/L 34.840 87 57-156<5.0
2-Hexanone ug/L 40.140 100 62-153<5.0
4-Methyl-2-pentanone (MIBK)ug/L 38.840 97 65-144<5.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4180698MATRIX SPIKE SAMPLE:
MSSpike
Result
92693480007
Acetone ug/L 41.240 98 49-162<25.0
Benzene ug/L 22.020 110 68-144<1.0
Bromodichloromethane ug/L 21.120 106 70-141<1.0
Bromoform ug/L 18.520 92 59-144<1.0
Bromomethane ug/L 20.3 v320102 23-190<2.0
Carbon disulfide ug/L 24.320 121 64-160<2.0
Carbon tetrachloride ug/L 23.820 119 70-147<1.0
Chlorobenzene ug/L 21.420 107 70-143<1.0
Chloroethane ug/L 23.920 120 55-190<1.0
Chloroform ug/L 22.620 113 67-148<1.0
Chloromethane ug/L 21.220 106 38-180<1.0
cis-1,2-Dichloroethene ug/L 21.020 105 67-151<1.0
cis-1,3-Dichloropropene ug/L 20.320 101 70-142<1.0
Cyclohexane ug/L 23.820 119 64-162<1.0
Dibromochloromethane ug/L 19.820 99 68-140<1.0
Dichlorodifluoromethane ug/L 34.020 170 15-200<1.0
Ethylbenzene ug/L 21.820 107 70-1450.37J
Isopropylbenzene (Cumene)ug/L 22.120 108 70-1440.46J
m&p-Xylene ug/L 41.840 104 70-148<2.0
Methyl acetate ug/L 17.420 87 62-144<10.0
Methyl-tert-butyl ether ug/L 18.520 93 64-146<1.0
Methylcyclohexane ug/L 25.820 129 70-155<10.0
Methylene Chloride ug/L 21.420 106 54-149<5.0
o-Xylene ug/L 20.220 101 70-145<1.0
Styrene ug/L 20.420 102 70-147<1.0
Tetrachloroethene ug/L 21.320 107 70-145<1.0
Toluene ug/L 21.620 108 65-146<1.0
trans-1,2-Dichloroethene ug/L 22.320 111 69-155<1.0
trans-1,3-Dichloropropene ug/L 19.720 99 70-142<1.0
Trichloroethene ug/L 23.420 117 70-152<1.0
Trichlorofluoromethane ug/L 26.920 135 60-158<1.0
Vinyl chloride ug/L 20.820 104 51-178<1.0
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%104 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693480006
4180697SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30<1.0
1,1,2,2-Tetrachloroethane ug/L ND 30<1.0
1,1,2-Trichloroethane ug/L ND 30<1.0
1,1,2-Trichlorotrifluoroethane ug/L ND 30<1.0
1,1-Dichloroethane ug/L ND 30<1.0
1,1-Dichloroethene ug/L ND 30<1.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693480006
4180697SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30<1.0
1,2-Dibromo-3-chloropropane ug/L ND 30<2.0
1,2-Dibromoethane (EDB)ug/L ND 30<1.0
1,2-Dichlorobenzene ug/L ND 30<1.0
1,2-Dichloroethane ug/L ND 30<1.0
1,2-Dichloropropane ug/L ND 30<1.0
1,3-Dichlorobenzene ug/L ND 30<1.0
1,4-Dichlorobenzene ug/L ND 30<1.0
2-Butanone (MEK)ug/L ND 30<5.0
2-Hexanone ug/L ND 30<5.0
4-Methyl-2-pentanone (MIBK)ug/L ND 30<5.0
Acetone ug/L ND 30<25.0
Benzene ug/L ND 30<1.0
Bromodichloromethane ug/L ND 30<1.0
Bromoform ug/L ND 30<1.0
Bromomethane ug/L ND v230<2.0
Carbon disulfide ug/L ND 30<2.0
Carbon tetrachloride ug/L ND 30<1.0
Chlorobenzene ug/L ND 30<1.0
Chloroethane ug/L ND 30<1.0
Chloroform ug/L ND 30<1.0
Chloromethane ug/L ND 30<1.0
cis-1,2-Dichloroethene ug/L ND 30<1.0
cis-1,3-Dichloropropene ug/L ND 30<1.0
Cyclohexane ug/L ND 30<1.0
Dibromochloromethane ug/L ND 30<1.0
Dichlorodifluoromethane ug/L ND 30<1.0
Ethylbenzene ug/L ND 30<1.0
Isopropylbenzene (Cumene)ug/L ND 30<1.0
m&p-Xylene ug/L ND 30<2.0
Methyl acetate ug/L ND 30<10.0
Methyl-tert-butyl ether ug/L ND 30<1.0
Methylcyclohexane ug/L ND 30<10.0
Methylene Chloride ug/L ND 30<5.0
o-Xylene ug/L ND 30<1.0
Styrene ug/L ND 30<1.0
Tetrachloroethene ug/L ND 30<1.0
Toluene ug/L ND 30<1.0
trans-1,2-Dichloroethene ug/L ND 30<1.0
trans-1,3-Dichloropropene ug/L ND 30<1.0
Trichloroethene ug/L ND 30<1.0
Trichlorofluoromethane ug/L ND 30<1.0
Vinyl chloride ug/L ND 30<1.0
1,2-Dichloroethane-d4 (S)%97103
4-Bromofluorobenzene (S)%9898
Toluene-d8 (S)%109106
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
808179
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92693772001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4184522
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 1.0 10/24/23 18:010.12
2,4,5-Trichlorophenol ug/L ND 1.0 v110/24/23 18:010.14
2,4,6-Trichlorophenol ug/L ND 1.0 v110/24/23 18:010.16
2,4-Dichlorophenol ug/L ND 1.0 10/24/23 18:010.14
2,4-Dimethylphenol ug/L ND 1.0 10/24/23 18:010.17
2,4-Dinitrophenol ug/L ND 5.0 10/24/23 18:012.6
2,4-Dinitrotoluene ug/L ND 1.0 10/24/23 18:010.16
2,6-Dinitrotoluene ug/L ND 1.0 10/24/23 18:010.17
2-Chloronaphthalene ug/L ND 1.0 10/24/23 18:010.17
2-Chlorophenol ug/L ND 1.0 10/24/23 18:010.12
2-Methylnaphthalene ug/L ND 1.0 10/24/23 18:010.19
2-Methylphenol(o-Cresol)ug/L ND 1.0 10/24/23 18:010.19
2-Nitroaniline ug/L ND 2.0 10/24/23 18:010.30
2-Nitrophenol ug/L ND 1.0 10/24/23 18:010.14
3&4-Methylphenol(m&p Cresol)ug/L ND 1.0 10/24/23 18:010.12
3,3'-Dichlorobenzidine ug/L ND 2.0 10/24/23 18:010.81
3-Nitroaniline ug/L ND 2.0 10/24/23 18:010.38
4,6-Dinitro-2-methylphenol ug/L ND 2.0 10/24/23 18:010.78
4-Bromophenylphenyl ether ug/L ND 1.0 10/24/23 18:010.18
4-Chloro-3-methylphenol ug/L ND 1.0 10/24/23 18:010.33
4-Chloroaniline ug/L ND 2.0 10/24/23 18:010.36
4-Chlorophenylphenyl ether ug/L ND 1.0 10/24/23 18:010.20
4-Nitroaniline ug/L ND 2.0 10/24/23 18:010.51
4-Nitrophenol ug/L ND 5.0 10/24/23 18:010.66
Acenaphthene ug/L ND 1.0 10/24/23 18:010.20
Acenaphthylene ug/L ND 1.0 10/24/23 18:010.20
Acetophenone ug/L ND 1.0 10/24/23 18:010.15
Anthracene ug/L ND 1.0 10/24/23 18:010.23
Atrazine ug/L ND 1.0 10/24/23 18:010.32
Benzaldehyde ug/L ND 1.0 v210/24/23 18:010.36
Benzo(a)anthracene ug/L ND 1.0 10/24/23 18:010.27
Benzo(a)pyrene ug/L ND 1.0 10/24/23 18:010.28
Benzo(b)fluoranthene ug/L ND 1.0 10/24/23 18:010.26
Benzo(g,h,i)perylene ug/L ND 1.0 10/24/23 18:010.28
Benzo(k)fluoranthene ug/L ND 1.0 10/24/23 18:010.27
Biphenyl (Diphenyl)ug/L ND 1.0 10/24/23 18:010.18
bis(2-Chloroethoxy)methane ug/L ND 1.0 10/24/23 18:010.18
bis(2-Chloroethyl) ether ug/L ND 1.0 10/24/23 18:010.19
bis(2-Ethylhexyl)phthalate ug/L ND 0.60 10/24/23 18:010.37
Butylbenzylphthalate ug/L ND 1.0 10/24/23 18:010.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4184522
Associated Lab Samples:92693772001
Matrix: Water
AnalyzedMDL
Caprolactam ug/L ND 1.0 10/24/23 18:010.69
Carbazole ug/L ND 1.0 10/24/23 18:010.24
Chrysene ug/L ND 1.0 10/24/23 18:010.28
Di-n-butylphthalate ug/L ND 1.0 10/24/23 18:010.22
Di-n-octylphthalate ug/L ND 1.0 10/24/23 18:010.39
Dibenz(a,h)anthracene ug/L ND 1.0 10/24/23 18:010.30
Dibenzofuran ug/L ND 1.0 10/24/23 18:010.21
Diethylphthalate ug/L ND 1.0 10/24/23 18:010.20
Dimethylphthalate ug/L ND 1.0 10/24/23 18:010.21
Fluoranthene ug/L ND 1.0 10/24/23 18:010.22
Fluorene ug/L ND 1.0 10/24/23 18:010.21
Hexachloro-1,3-butadiene ug/L ND 1.0 10/24/23 18:010.18
Hexachlorobenzene ug/L ND 1.0 10/24/23 18:010.22
Hexachlorocyclopentadiene ug/L ND 1.0 10/24/23 18:010.16
Hexachloroethane ug/L ND 1.0 10/24/23 18:010.14
Indeno(1,2,3-cd)pyrene ug/L ND 1.0 10/24/23 18:010.29
Isophorone ug/L ND 1.0 10/24/23 18:010.17
N-Nitroso-di-n-propylamine ug/L ND 1.0 10/24/23 18:010.13
N-Nitrosodiphenylamine ug/L ND 1.0 10/24/23 18:010.30
Naphthalene ug/L ND 1.0 10/24/23 18:010.21
Nitrobenzene ug/L ND 1.0 10/24/23 18:010.19
Pentachlorophenol ug/L ND 2.0 10/24/23 18:010.38
Phenanthrene ug/L ND 1.0 10/24/23 18:010.20
Phenol ug/L ND 1.0 10/24/23 18:010.14
Pyrene ug/L ND 1.0 10/24/23 18:010.22
2,4,6-Tribromophenol (S)%104 10-166 10/24/23 18:01
2-Fluorobiphenyl (S)%98 10-130 10/24/23 18:01
2-Fluorophenol (S)%64 10-130 10/24/23 18:01
Nitrobenzene-d5 (S)%120 10-133 10/24/23 18:01
Phenol-d6 (S)%37 10-130 10/24/23 18:01
Terphenyl-d14 (S)%139 10-193 10/24/23 18:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4184523LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 59.650 119 23-130
2,4,5-Trichlorophenol ug/L 31.9 v15064 36-150
2,4,6-Trichlorophenol ug/L 19.6 v15039 30-151
2,4-Dichlorophenol ug/L 43.650 87 36-140
2,4-Dimethylphenol ug/L 54.050 108 36-155
2,4-Dinitrophenol ug/L 51.6250 21 10-169
2,4-Dinitrotoluene ug/L 63.950 128 46-160
2,6-Dinitrotoluene ug/L 40.950 82 47-161
2-Chloronaphthalene ug/L 49.650 99 29-134
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
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Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4184523LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 35.050 70 29-130
2-Methylnaphthalene ug/L 49.950 100 26-130
2-Methylphenol(o-Cresol)ug/L 56.450 113 32-130
2-Nitroaniline ug/L 117100 117 41-150
2-Nitrophenol ug/L 40.450 81 31-145
3&4-Methylphenol(m&p Cresol)ug/L 46.850 94 29-130
3,3'-Dichlorobenzidine ug/L 145100 145 46-153
3-Nitroaniline ug/L 123100 123 47-156
4,6-Dinitro-2-methylphenol ug/L 30.6100 31 23-161
4-Bromophenylphenyl ether ug/L 63.250 126 45-143
4-Chloro-3-methylphenol ug/L 115100 115 42-143
4-Chloroaniline ug/L 93.6100 94 37-135
4-Chlorophenylphenyl ether ug/L 36.450 73 43-140
4-Nitroaniline ug/L 71.5100 71 47-157
4-Nitrophenol ug/L 35.0J250 14 10-130
Acenaphthene ug/L 53.750 107 38-138
Acenaphthylene ug/L 36.850 74 39-139
Acetophenone ug/L 45.450 91 34-135
Anthracene ug/L 58.350 117 45-136
Atrazine ug/L 78.4 L150157 23-145
Benzaldehyde ug/L 58.6 v350117 11-140
Benzo(a)anthracene ug/L 64.650 129 52-151
Benzo(a)pyrene ug/L 66.150 132 46-165
Benzo(b)fluoranthene ug/L 73.050 146 44-170
Benzo(g,h,i)perylene ug/L 65.650 131 39-171
Benzo(k)fluoranthene ug/L 62.650 125 43-168
Biphenyl (Diphenyl)ug/L 51.450 103 34-130
bis(2-Chloroethoxy)methane ug/L 47.550 95 37-140
bis(2-Chloroethyl) ether ug/L 34.850 70 33-136
bis(2-Ethylhexyl)phthalate ug/L 67.350 135 50-169
Butylbenzylphthalate ug/L 67.250 134 50-174
Caprolactam ug/L 33.250 66 10-130
Carbazole ug/L 63.550 127 52-151
Chrysene ug/L 63.150 126 52-148
Di-n-butylphthalate ug/L 65.850 132 51-154
Di-n-octylphthalate ug/L 78.350 157 44-170
Dibenz(a,h)anthracene ug/L 66.050 132 41-171
Dibenzofuran ug/L 54.850 110 42-157
Diethylphthalate ug/L 62.650 125 50-149
Dimethylphthalate ug/L 61.450 123 47-146
Fluoranthene ug/L 69.650 139 51-152
Fluorene ug/L 33.350 67 46-143
Hexachloro-1,3-butadiene ug/L 31.550 63 10-130
Hexachlorobenzene ug/L 63.250 126 40-139
Hexachlorocyclopentadiene ug/L 37.950 76 10-130
Hexachloroethane ug/L 22.750 45 10-130
Indeno(1,2,3-cd)pyrene ug/L 63.550 127 40-172
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
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Page 25 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4184523LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 54.150 108 37-143
N-Nitroso-di-n-propylamine ug/L 54.450 109 38-145
N-Nitrosodiphenylamine ug/L 55.850 112 46-144
Naphthalene ug/L 43.850 88 21-130
Nitrobenzene ug/L 49.850 100 33-136
Pentachlorophenol ug/L 26.8100 27 19-156
Phenanthrene ug/L 58.850 118 49-143
Phenol ug/L 24.150 48 18-130
Pyrene ug/L 61.250 122 48-156
2,4,6-Tribromophenol (S)%59 10-166
2-Fluorobiphenyl (S)%96 10-130
2-Fluorophenol (S)%33 10-130
Nitrobenzene-d5 (S)%102 10-133
Phenol-d6 (S)%53 10-130
Terphenyl-d14 (S)%121 10-193
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4184524MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92694322004
4184525
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-
chloropropane)ug/L 100 107 10-13279 30 30100ND107 79.2
2,4,5-Trichlorophenol ug/L v11001310-17481 30100ND13.1J 81.1
2,4,6-Trichlorophenol ug/L M1,v1100310-17372 30100NDND 71.8
2,4-Dichlorophenol ug/L 100 19 10-15378 30100ND19.3J 77.7
2,4-Dimethylphenol ug/L 100 86 12-15779 9 30100ND86.2 78.5
2,4-Dinitrophenol ug/L M1500010-16514 30500NDND 69.1J
2,4-Dinitrotoluene ug/L 100 75 29-16882 9 30100ND75.1 81.9
2,6-Dinitrotoluene ug/L 100 117 28-16894 22 30100ND117 94.0
2-Chloronaphthalene ug/L 100 68 11-13666 3 30100ND68.2 66.2
2-Chlorophenol ug/L R11002410-13469 98 30100ND23.7 69.4
2-Methylnaphthalene ug/L 100 60 10-13171 17 30100ND60.0 71.0
2-Methylphenol(o-Cresol) ug/L 100 95 10-13077 21 30100ND95.2 77.0
2-Nitroaniline ug/L 200 110 19-15683 29 30200ND220 165
2-Nitrophenol ug/L 100 14 10-16084 30100ND13.8J 84.3
3&4-Methylphenol(m&p
Cresol)
ug/L 100 70 10-13267 4 30100ND69.8 67.2
3,3'-Dichlorobenzidine ug/L 200 127 10-173112 13 30200ND254 223
3-Nitroaniline ug/L 200 110 19-16992 17 30200ND219 184
4,6-Dinitro-2-methylphenol ug/L M1200710-17834 30200NDND 67.9
4-Bromophenylphenyl ether ug/L M1,R110015828-14987 58 30100ND158 86.6
4-Chloro-3-methylphenol ug/L 200 84 18-14886 3 30200ND167 172
4-Chloroaniline ug/L 200 88 10-14168 27 30200ND177 135
4-Chlorophenylphenyl ether ug/L 100 107 24-14480 29 30100ND107 80.4
4-Nitroaniline ug/L R120011918-17072 50 30200ND237 143
4-Nitrophenol ug/L M1500010-13023 30500NDND 115
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 26 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4184524MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92694322004
4184525
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L 100 90 18-14273 21 30100ND90.4 72.9
Acenaphthylene ug/L 100 93 18-14374 22 30100ND92.9 74.4
Acetophenone ug/L R11009910-14271 33 30100ND98.6 70.9
Anthracene ug/L M1,R110014932-13870 72 30100ND149 70.0
Atrazine ug/L M0,R110019311-16561 104 30100ND193 61.2
Benzaldehyde ug/L v31009710-13076 24 30100ND97.1 75.9
Benzo(a)anthracene ug/L 100 114 41-155104 10 30100ND114 104
Benzo(a)pyrene ug/L 100 120 10-167102 16 30100ND120 102
Benzo(b)fluoranthene ug/L 100 116 31-172112 3 30100ND116 112
Benzo(g,h,i)perylene ug/L R110013426-17788 41 30100ND134 87.8
Benzo(k)fluoranthene ug/L 100 103 31-16883 22 30100ND103 82.7
Biphenyl (Diphenyl)ug/L 100 74 13-13769 7 30100ND74.3 69.2
bis(2-
Chloroethoxy)methane ug/L 100 86 12-14371 19 30100ND85.6 70.9
bis(2-Chloroethyl) ether ug/L R11009910-13968 37 30100ND98.9 67.9
bis(2-Ethylhexyl)phthalate ug/L 100 117 41-173106 10 30100ND117 106
Butylbenzylphthalate ug/L 100 115 38-182108 6 30100ND115 108
Caprolactam ug/L 100 53 10-13058 9 30100ND52.9 57.7
Carbazole ug/L M1,R110017351-149101 52 30100ND173 101
Chrysene ug/L R110011241-15276 39 30100ND112 76.0
Di-n-butylphthalate ug/L M1,R110017137-16267 88 30100ND171 66.6
Di-n-octylphthalate ug/L 100 134 36-176113 17 30100ND134 113
Dibenz(a,h)anthracene ug/L 100 140 29-175103 30 30100ND140 103
Dibenzofuran ug/L 100 60 23-14471 17 30100ND60.0 71.0
Diethylphthalate ug/L 100 102 33-15492 10 30100ND102 92.3
Dimethylphthalate ug/L 100 108 29-15084 24 30100ND108 84.5
Fluoranthene ug/L 100 116 40-15686 30 30100ND116 86.2
Fluorene ug/L 100 102 26-14878 27 30100ND102 77.8
Hexachloro-1,3-butadiene ug/L 100 31 10-13033 5 30100ND31.1 32.9
Hexachlorobenzene ug/L M1,R110014927-14589 50 30100ND149 89.2
Hexachlorocyclopentadiene ug/L 100 34 10-13039 12 30100ND34.4 38.9
Hexachloroethane ug/L 100 27 10-13023 17 30100ND27.0 22.7
Indeno(1,2,3-cd)pyrene ug/L 100 134 28-176102 27 30100ND134 102
Isophorone ug/L 100 61 14-14576 21 30100ND61.3 75.5
N-Nitroso-di-n-propylamine ug/L R110011112-14980 33 30100ND111 79.6
N-Nitrosodiphenylamine ug/L M1,R110015929-14972 76 30100ND159 71.6
Naphthalene ug/L 100 51 10-13054 6 30100ND50.8 54.2
Nitrobenzene ug/L 100 79 10-14570 13 30100ND79.3 69.7
Pentachlorophenol ug/L M1200010-17858 30200NDND 116
Phenanthrene ug/L 100 114 36-14691 23 30100ND114 90.8
Phenol ug/L 100 30 10-13039 24 30100ND30.5 38.7
Pyrene ug/L 100 105 42-156105 0 30100ND105 105
2,4,6-Tribromophenol (S) %29 10-166114
2-Fluorobiphenyl (S)%92 10-13079
2-Fluorophenol (S)%S0810-13078
Nitrobenzene-d5 (S)%103 10-13385
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
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[phone]
Page 27 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4184524MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92694322004
4184525
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%35 10-13051
Terphenyl-d14 (S)%134 10-193117
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Re-extraction conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.1g
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The sample was analyzed at a dilution due to foaming of the sample in the purge vessel.F1
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2023 05:10 PM
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[phone]
Page 29 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92693772
Pactiv Evergreen Surface Water
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92693772001 961843 961855RW05WG-10172023 EPA 200.7 EPA 200.7
92693772001 961841 961860RW05WG-10172023 EPA 200.7 EPA 200.7
92693772001 961842 961854RW05WG-10172023 EPA 200.8 EPA 200.8
92693772001 961840 961859RW05WG-10172023 EPA 200.8 EPA 200.8
92693772001 962123 962158RW05WG-10172023 EPA 245.1 EPA 245.1
92693772001 962119 962159RW05WG-10172023 EPA 245.1 EPA 245.1
92693772001 808179 808510RW05WG-10172023 EPA 3510C EPA 8270E
92693772001 807365RW05WG-10172023 EPA 8260D
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 30 of 33
Page 31 of 33
Page 32 of 33
Pa
g
e

3
3

o
f

3
3
#=CL#
October 10, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92689265
92689265
Project:
Pace Project No.:
RE:
Christina Ashdown
ENSAFE
313 Wingo Way
Mount Pleasant, SC 29464
Pactiv Evergreen SW/Seep
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on September 21, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc: Jennings Kerr, ENSAFE Inc.
Lab, ENSAFE Inc.
David Warren, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 1 of 120
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
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Page 2 of 120
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID Matrix Date Collected Date Received
92689265001 SWDOWNWS-092023 Water 09/20/23 13:05 09/21/23 08:15
92689265002 SWDOWNH-092023 Water 09/20/23 13:05 09/21/23 08:15
92689265003 SEEP02WG-092023 Water 09/20/23 14:15 09/21/23 08:15
92689265004 SW01-00-WS-092023 Water 09/20/23 14:35 09/21/23 08:15
92689265005 SW01-02-WS-092023 Water 09/20/23 14:50 09/21/23 08:15
92689265006 SW01-05-WS-092023 Water 09/20/23 15:10 09/21/23 08:15
92689265007 SW01-10-WS-092023 Water 09/20/23 15:20 09/21/23 08:15
92689265008 SEEP01-WG-092023 Water 09/20/23 15:30 09/21/23 08:15
92689265009 SW02-WS-092023 Water 09/20/23 15:50 09/21/23 08:15
92689265010 SWUP-WS-092023 Water 09/20/23 17:00 09/21/23 08:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 120
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92689265001 SWDOWNWS-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OKC2
EPA 200.7 21 PASI-OTMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
SM 4500-P E-2011 1 PASI-AJP1
SM 5220D-2011 1 PASI-AJP1
92689265002 SWDOWNH-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OKC2
EPA 200.7 21 PASI-OTMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
SM 4500-P E-2011 1 PASI-AJP1
SM 5220D-2011 1 PASI-AJP1
92689265003 SEEP02WG-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OAME, TMA
EPA 200.7 21 PASI-OTMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 120
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
SM 4500-P E-2011 1 PASI-AJP1
SM 5220D-2011 1 PASI-AJP1
92689265004 SW01-00-WS-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OKC2
EPA 200.7 21 PASI-OTMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
SM 4500-P E-2011 1 PASI-AJP1
SM 5220D-2011 1 PASI-AJP1
92689265005 SW01-02-WS-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OKC2
EPA 200.7 21 PASI-OTMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
SM 4500-P E-2011 1 PASI-AJP1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 120
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 5220D-2011 1 PASI-AJP1
92689265006 SW01-05-WS-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OKC2
EPA 200.7 21 PASI-OTMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
SM 4500-P E-2011 1 PASI-AJP1
SM 5220D-2011 1 PASI-AJP1
92689265007 SW01-10-WS-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OKC2
EPA 200.7 21 PASI-OTMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
SM 4500-P E-2011 1 PASI-AJP1
SM 5220D-2011 1 PASI-AJP1
92689265008 SEEP01-WG-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OKC2, TMA
EPA 200.7 21 PASI-OAME, TMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 120
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
SM 4500-P E-2011 1 PASI-AJP1
SM 5220D-2011 1 PASI-AJP1
92689265009 SW02-WS-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OKC2
EPA 200.7 21 PASI-OTMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
SM 4500-P E-2011 1 PASI-AJP1
SM 5220D-2011 1 PASI-AJP1
92689265010 SWUP-WS-092023 SM 2120B-2011 2 PASI-ELRB
EPA 200.7 21 PASI-OAAM1
EPA 200.7 21 PASI-OTMA
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AMAB2
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-ANCF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 420.4 Rev 1.0 1993 1 PASI-AARJ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 120
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-P E-2011 1 PASI-AJP1
SM 5220D-2011 1 PASI-AJP1
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNWS-092023 Lab ID: 92689265001 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.8 Std. Units 09/26/23 12:51 H31
True Color 10.0 units 09/26/23 12:51 H35.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 68.9J ug/L 10/04/23 01:19 7429-90-510/03/23 04:43100 30.7 1
Arsenic ND ug/L 10/04/23 01:19 7440-38-210/03/23 04:4310.0 3.4 1
Barium 15.3 ug/L 10/04/23 01:19 7440-39-310/03/23 04:4310.0 0.84 1
Beryllium ND ug/L 10/04/23 01:19 7440-41-710/03/23 04:434.0 0.17 1
Boron ND ug/L 10/04/23 01:19 7440-42-810/03/23 04:4350.0 12.4 1
Cadmium ND ug/L 10/04/23 01:19 7440-43-910/03/23 04:431.0 0.33 1
Calcium 3300 ug/L 10/04/23 01:19 7440-70-210/03/23 04:43500 190 1
Chromium ND ug/L 10/04/23 01:19 7440-47-310/03/23 04:435.0 1.7 1
Cobalt ND ug/L 10/04/23 01:19 7440-48-410/03/23 04:4310.0 0.96 1
Copper ND ug/L 10/04/23 01:19 7440-50-810/03/23 04:435.0 2.6 1
Iron 257 ug/L 10/04/23 01:19 7439-89-610/03/23 04:4340.0 25.0 1
Lead ND ug/L 10/04/23 01:19 7439-92-110/03/23 04:4310.0 2.1 1
Magnesium 852 ug/L 10/04/23 01:19 7439-95-410/03/23 04:43500 84.0 1
Manganese 28.4 ug/L 10/04/23 01:19 7439-96-510/03/23 04:435.0 1.1 1
Molybdenum ND ug/L 10/04/23 01:19 7439-98-710/03/23 04:4310.0 1.6 1
Nickel ND ug/L 10/04/23 01:19 7440-02-010/03/23 04:435.0 1.0 1
Selenium ND ug/L 10/04/23 01:19 7782-49-210/03/23 04:4315.0 3.9 1
Silver ND ug/L 10/04/23 01:19 7440-22-410/03/23 04:435.0 1.0 1
Sodium 5080 ug/L 10/04/23 01:19 7440-23-510/03/23 04:432000 540 1
Thallium ND ug/L 10/04/23 01:19 7440-28-010/03/23 04:4315.0 2.9 1
Zinc ND ug/L 10/04/23 01:19 7440-66-610/03/23 04:4320.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 10/06/23 13:55 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 13:55 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 15.7 ug/L 10/06/23 13:55 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 13:55 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved 12.7J ug/L 10/06/23 13:55 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 13:55 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 3210 ug/L 10/06/23 13:55 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved ND ug/L 10/06/23 13:55 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved ND ug/L 10/06/23 13:55 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved ND ug/L 10/06/23 13:55 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 110 ug/L 10/06/23 13:55 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 13:55 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 873 ug/L 10/06/23 13:55 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 25.4 ug/L 10/06/23 13:55 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved ND ug/L 10/06/23 13:55 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved ND ug/L 10/06/23 13:55 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNWS-092023 Lab ID: 92689265001 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 13:55 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 13:55 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 5900 ug/L 10/06/23 13:55 7440-23-510/03/23 23:492000 540 1
Thallium, Dissolved ND ug/L 10/06/23 13:55 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved ND ug/L 10/06/23 13:55 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 15:43 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 12:54 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/25/23 19:01 83-32-909/25/23 12:318.3 1.7 1
Acenaphthylene ND ug/L 09/25/23 19:01 208-96-809/25/23 12:318.3 1.6 1
Acetophenone ND ug/L 09/25/23 19:01 98-86-209/25/23 12:318.3 1.2 1
Anthracene ND ug/L 09/25/23 19:01 120-12-709/25/23 12:318.3 1.9 1
Atrazine ND ug/L 09/25/23 19:01 1912-24-909/25/23 12:318.3 2.6 1
Benzaldehyde ND ug/L 09/25/23 19:01 100-52-709/25/23 12:318.3 3.0 1
Benzo(a)anthracene ND ug/L 09/25/23 19:01 56-55-309/25/23 12:318.3 2.2 1
Benzo(a)pyrene ND ug/L 09/25/23 19:01 50-32-809/25/23 12:318.3 2.3 1
Benzo(b)fluoranthene ND ug/L 09/25/23 19:01 205-99-209/25/23 12:318.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 09/25/23 19:01 191-24-209/25/23 12:318.3 2.4 1
Benzo(k)fluoranthene ND ug/L 09/25/23 19:01 207-08-909/25/23 12:318.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 09/25/23 19:01 92-52-409/25/23 12:318.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 09/25/23 19:01 101-55-309/25/23 12:318.3 1.5 1
Butylbenzylphthalate ND ug/L 09/25/23 19:01 85-68-709/25/23 12:318.3 2.6 1
Caprolactam ND ug/L 09/25/23 19:01 105-60-209/25/23 12:318.3 5.8 1
Carbazole ND ug/L 09/25/23 19:01 86-74-809/25/23 12:318.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/25/23 19:01 59-50-709/25/23 12:318.3 2.8 1
4-Chloroaniline ND ug/L 09/25/23 19:01 106-47-809/25/23 12:3116.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/25/23 19:01 111-91-109/25/23 12:318.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 09/25/23 19:01 111-44-409/25/23 12:318.3 1.6 1
2-Chloronaphthalene ND ug/L 09/25/23 19:01 91-58-709/25/23 12:318.3 1.4 1
2-Chlorophenol ND ug/L 09/25/23 19:01 95-57-809/25/23 12:318.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/25/23 19:01 7005-72-309/25/23 12:318.3 1.7 1
Chrysene ND ug/L 09/25/23 19:01 218-01-909/25/23 12:318.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 09/25/23 19:01 53-70-309/25/23 12:318.3 2.5 1
Dibenzofuran ND ug/L 09/25/23 19:01 132-64-909/25/23 12:318.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/25/23 19:01 91-94-109/25/23 12:3116.7 6.8 1
2,4-Dichlorophenol ND ug/L 09/25/23 19:01 120-83-209/25/23 12:318.3 1.2 1
Diethylphthalate ND ug/L 09/25/23 19:01 84-66-209/25/23 12:318.3 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNWS-092023 Lab ID: 92689265001 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/25/23 19:01 105-67-909/25/23 12:318.3 1.4 1
Dimethylphthalate ND ug/L 09/25/23 19:01 131-11-309/25/23 12:318.3 1.8 1
Di-n-butylphthalate ND ug/L 09/25/23 19:01 84-74-209/25/23 12:318.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/25/23 19:01 534-52-109/25/23 12:3116.7 6.5 1
2,4-Dinitrophenol ND ug/L 09/25/23 19:01 51-28-509/25/23 12:3141.7 21.7 1
2,4-Dinitrotoluene ND ug/L 09/25/23 19:01 121-14-209/25/23 12:318.3 1.4 1
2,6-Dinitrotoluene ND ug/L 09/25/23 19:01 606-20-209/25/23 12:318.3 1.4 1
Di-n-octylphthalate ND ug/L 09/25/23 19:01 117-84-009/25/23 12:318.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/25/23 19:01 117-81-709/25/23 12:315.0 3.1 1
Fluoranthene ND ug/L 09/25/23 19:01 206-44-009/25/23 12:318.3 1.8 1
Fluorene ND ug/L 09/25/23 19:01 86-73-709/25/23 12:318.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 09/25/23 19:01 87-68-309/25/23 12:318.3 1.5 1
Hexachlorobenzene ND ug/L 09/25/23 19:01 118-74-109/25/23 12:318.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 09/25/23 19:01 77-47-409/25/23 12:318.3 1.3 1
Hexachloroethane ND ug/L 09/25/23 19:01 67-72-109/25/23 12:318.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/25/23 19:01 193-39-509/25/23 12:318.3 2.4 1
Isophorone ND ug/L 09/25/23 19:01 78-59-109/25/23 12:318.3 1.4 1
2-Methylnaphthalene ND ug/L 09/25/23 19:01 91-57-609/25/23 12:318.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/25/23 19:01 95-48-709/25/23 12:318.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/25/23 19:01 15831-10-409/25/23 12:318.3 1.0 1
Naphthalene ND ug/L 09/25/23 19:01 91-20-309/25/23 12:318.3 1.7 1
2-Nitroaniline ND ug/L 09/25/23 19:01 88-74-409/25/23 12:3116.7 2.5 1
3-Nitroaniline ND ug/L 09/25/23 19:01 99-09-209/25/23 12:3116.7 3.1 1
4-Nitroaniline ND ug/L 09/25/23 19:01 100-01-609/25/23 12:3116.7 4.2 1
Nitrobenzene ND ug/L 09/25/23 19:01 98-95-309/25/23 12:318.3 1.6 1
2-Nitrophenol ND ug/L 09/25/23 19:01 88-75-509/25/23 12:318.3 1.2 1
4-Nitrophenol ND ug/L 09/25/23 19:01 100-02-709/25/23 12:3141.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 09/25/23 19:01 621-64-709/25/23 12:318.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 09/25/23 19:01 86-30-609/25/23 12:318.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/25/23 19:01 108-60-109/25/23 12:318.3 0.96 1
Pentachlorophenol ND ug/L 09/25/23 19:01 87-86-509/25/23 12:3116.7 3.1 1
Phenanthrene ND ug/L 09/25/23 19:01 85-01-809/25/23 12:318.3 1.7 1
Phenol ND ug/L 09/25/23 19:01 108-95-209/25/23 12:318.3 1.1 1
Pyrene ND ug/L 09/25/23 19:01 129-00-009/25/23 12:318.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 09/25/23 19:01 95-95-409/25/23 12:318.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/25/23 19:01 88-06-209/25/23 12:318.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)104 %09/25/23 19:01 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)92 %09/25/23 19:01 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)125 %09/25/23 19:01 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)42 %09/25/23 19:01 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)38 %09/25/23 19:01 367-12-409/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)67 %09/25/23 19:01 118-79-609/25/23 12:3110-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNWS-092023 Lab ID: 92689265001 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 09:12 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 09:12 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 09:12 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 09:12 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 09:12 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 09:12 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 09:12 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/30/23 09:12 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 09:12 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 09:12 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 09:12 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 09:12 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 09:12 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 09:12 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 09:12 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 09:12 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 09:12 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 09:12 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 09:12 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 09:12 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 09:12 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 09:12 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 09:12 75-35-4 v11.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 09:12 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 09:12 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 09:12 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 09:12 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 09:12 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 09:12 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 09:12 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 09:12 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 09:12 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 09:12 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 09:12 75-09-2 v15.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 09:12 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 09:12 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 09:12 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 09:12 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 09:12 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 09:12 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 09:12 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 09:12 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 09:12 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 09:12 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 09:12 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNWS-092023 Lab ID: 92689265001 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 09:12 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 09:12 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 09:12 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 09:12 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %09/30/23 09:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/30/23 09:12 17060-07-070-130 1
Toluene-d8 (S)99 %09/30/23 09:12 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 37.1 mg/L 09/28/23 17:15 M15.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 35.0 mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 3.3 mg/L 09/22/23 17:41 16887-00-61.0 0.60 1
Sulfate 3.0 mg/L 09/22/23 17:41 14808-79-81.0 0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 10/10/23 01:22 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 10/10/23 04:17 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable ND mg/L 09/27/23 15:29 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.029J mg/L 09/22/23 04:320.050 0.012 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand ND mg/L 10/06/23 00:1710/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNH-092023 Lab ID: 92689265002 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.7 Std. Units 09/26/23 12:52 H31
True Color 10.0 units 09/26/23 12:52 H35.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 75.7J ug/L 10/04/23 01:23 7429-90-510/03/23 04:43100 30.7 1
Arsenic ND ug/L 10/04/23 01:23 7440-38-210/03/23 04:4310.0 3.4 1
Barium 15.1 ug/L 10/04/23 01:23 7440-39-310/03/23 04:4310.0 0.84 1
Beryllium ND ug/L 10/04/23 01:23 7440-41-710/03/23 04:434.0 0.17 1
Boron ND ug/L 10/04/23 01:23 7440-42-810/03/23 04:4350.0 12.4 1
Cadmium ND ug/L 10/04/23 01:23 7440-43-910/03/23 04:431.0 0.33 1
Calcium 3240 ug/L 10/04/23 01:23 7440-70-210/03/23 04:43500 190 1
Chromium ND ug/L 10/04/23 01:23 7440-47-310/03/23 04:435.0 1.7 1
Cobalt ND ug/L 10/04/23 01:23 7440-48-410/03/23 04:4310.0 0.96 1
Copper ND ug/L 10/04/23 01:23 7440-50-810/03/23 04:435.0 2.6 1
Iron 276 ug/L 10/04/23 01:23 7439-89-610/03/23 04:4340.0 25.0 1
Lead ND ug/L 10/04/23 01:23 7439-92-110/03/23 04:4310.0 2.1 1
Magnesium 840 ug/L 10/04/23 01:23 7439-95-410/03/23 04:43500 84.0 1
Manganese 28.1 ug/L 10/04/23 01:23 7439-96-510/03/23 04:435.0 1.1 1
Molybdenum ND ug/L 10/04/23 01:23 7439-98-710/03/23 04:4310.0 1.6 1
Nickel 1.4J ug/L 10/04/23 01:23 7440-02-010/03/23 04:435.0 1.0 1
Selenium ND ug/L 10/04/23 01:23 7782-49-210/03/23 04:4315.0 3.9 1
Silver ND ug/L 10/04/23 01:23 7440-22-410/03/23 04:435.0 1.0 1
Sodium 4930 ug/L 10/04/23 01:23 7440-23-510/03/23 04:432000 540 1
Thallium ND ug/L 10/04/23 01:23 7440-28-010/03/23 04:4315.0 2.9 1
Zinc ND ug/L 10/04/23 01:23 7440-66-610/03/23 04:4320.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 10/06/23 14:15 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 14:15 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 15.7 ug/L 10/06/23 14:15 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 14:15 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved ND ug/L 10/06/23 14:15 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 14:15 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 3250 ug/L 10/06/23 14:15 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved ND ug/L 10/06/23 14:15 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved ND ug/L 10/06/23 14:15 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved ND ug/L 10/06/23 14:15 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 104 ug/L 10/06/23 14:15 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 14:15 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 878 ug/L 10/06/23 14:15 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 25.7 ug/L 10/06/23 14:15 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved ND ug/L 10/06/23 14:15 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved ND ug/L 10/06/23 14:15 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNH-092023 Lab ID: 92689265002 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 14:15 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 14:15 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 5900 ug/L 10/06/23 14:15 7440-23-510/03/23 23:492000 540 1
Thallium, Dissolved ND ug/L 10/06/23 14:15 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved ND ug/L 10/06/23 14:15 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 15:45 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 12:56 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/25/23 19:26 83-32-909/25/23 12:318.3 1.7 1
Acenaphthylene ND ug/L 09/25/23 19:26 208-96-809/25/23 12:318.3 1.6 1
Acetophenone ND ug/L 09/25/23 19:26 98-86-209/25/23 12:318.3 1.2 1
Anthracene ND ug/L 09/25/23 19:26 120-12-709/25/23 12:318.3 1.9 1
Atrazine ND ug/L 09/25/23 19:26 1912-24-909/25/23 12:318.3 2.6 1
Benzaldehyde ND ug/L 09/25/23 19:26 100-52-709/25/23 12:318.3 3.0 1
Benzo(a)anthracene ND ug/L 09/25/23 19:26 56-55-309/25/23 12:318.3 2.2 1
Benzo(a)pyrene ND ug/L 09/25/23 19:26 50-32-809/25/23 12:318.3 2.3 1
Benzo(b)fluoranthene ND ug/L 09/25/23 19:26 205-99-209/25/23 12:318.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 09/25/23 19:26 191-24-209/25/23 12:318.3 2.4 1
Benzo(k)fluoranthene ND ug/L 09/25/23 19:26 207-08-909/25/23 12:318.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 09/25/23 19:26 92-52-409/25/23 12:318.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 09/25/23 19:26 101-55-309/25/23 12:318.3 1.5 1
Butylbenzylphthalate ND ug/L 09/25/23 19:26 85-68-709/25/23 12:318.3 2.6 1
Caprolactam ND ug/L 09/25/23 19:26 105-60-209/25/23 12:318.3 5.8 1
Carbazole ND ug/L 09/25/23 19:26 86-74-809/25/23 12:318.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/25/23 19:26 59-50-709/25/23 12:318.3 2.8 1
4-Chloroaniline ND ug/L 09/25/23 19:26 106-47-809/25/23 12:3116.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/25/23 19:26 111-91-109/25/23 12:318.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 09/25/23 19:26 111-44-409/25/23 12:318.3 1.6 1
2-Chloronaphthalene ND ug/L 09/25/23 19:26 91-58-709/25/23 12:318.3 1.4 1
2-Chlorophenol ND ug/L 09/25/23 19:26 95-57-809/25/23 12:318.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/25/23 19:26 7005-72-309/25/23 12:318.3 1.7 1
Chrysene ND ug/L 09/25/23 19:26 218-01-909/25/23 12:318.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 09/25/23 19:26 53-70-309/25/23 12:318.3 2.5 1
Dibenzofuran ND ug/L 09/25/23 19:26 132-64-909/25/23 12:318.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/25/23 19:26 91-94-109/25/23 12:3116.7 6.8 1
2,4-Dichlorophenol ND ug/L 09/25/23 19:26 120-83-209/25/23 12:318.3 1.2 1
Diethylphthalate ND ug/L 09/25/23 19:26 84-66-209/25/23 12:318.3 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNH-092023 Lab ID: 92689265002 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/25/23 19:26 105-67-909/25/23 12:318.3 1.4 1
Dimethylphthalate ND ug/L 09/25/23 19:26 131-11-309/25/23 12:318.3 1.8 1
Di-n-butylphthalate ND ug/L 09/25/23 19:26 84-74-209/25/23 12:318.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/25/23 19:26 534-52-109/25/23 12:3116.7 6.5 1
2,4-Dinitrophenol ND ug/L 09/25/23 19:26 51-28-509/25/23 12:3141.7 21.7 1
2,4-Dinitrotoluene ND ug/L 09/25/23 19:26 121-14-209/25/23 12:318.3 1.4 1
2,6-Dinitrotoluene ND ug/L 09/25/23 19:26 606-20-209/25/23 12:318.3 1.4 1
Di-n-octylphthalate ND ug/L 09/25/23 19:26 117-84-009/25/23 12:318.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/25/23 19:26 117-81-709/25/23 12:315.0 3.1 1
Fluoranthene ND ug/L 09/25/23 19:26 206-44-009/25/23 12:318.3 1.8 1
Fluorene ND ug/L 09/25/23 19:26 86-73-709/25/23 12:318.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 09/25/23 19:26 87-68-309/25/23 12:318.3 1.5 1
Hexachlorobenzene ND ug/L 09/25/23 19:26 118-74-109/25/23 12:318.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 09/25/23 19:26 77-47-409/25/23 12:318.3 1.3 1
Hexachloroethane ND ug/L 09/25/23 19:26 67-72-109/25/23 12:318.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/25/23 19:26 193-39-509/25/23 12:318.3 2.4 1
Isophorone ND ug/L 09/25/23 19:26 78-59-109/25/23 12:318.3 1.4 1
2-Methylnaphthalene ND ug/L 09/25/23 19:26 91-57-609/25/23 12:318.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/25/23 19:26 95-48-709/25/23 12:318.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/25/23 19:26 15831-10-409/25/23 12:318.3 1.0 1
Naphthalene ND ug/L 09/25/23 19:26 91-20-309/25/23 12:318.3 1.7 1
2-Nitroaniline ND ug/L 09/25/23 19:26 88-74-409/25/23 12:3116.7 2.5 1
3-Nitroaniline ND ug/L 09/25/23 19:26 99-09-209/25/23 12:3116.7 3.1 1
4-Nitroaniline ND ug/L 09/25/23 19:26 100-01-609/25/23 12:3116.7 4.2 1
Nitrobenzene ND ug/L 09/25/23 19:26 98-95-309/25/23 12:318.3 1.6 1
2-Nitrophenol ND ug/L 09/25/23 19:26 88-75-509/25/23 12:318.3 1.2 1
4-Nitrophenol ND ug/L 09/25/23 19:26 100-02-709/25/23 12:3141.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 09/25/23 19:26 621-64-709/25/23 12:318.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 09/25/23 19:26 86-30-609/25/23 12:318.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/25/23 19:26 108-60-109/25/23 12:318.3 0.96 1
Pentachlorophenol ND ug/L 09/25/23 19:26 87-86-509/25/23 12:3116.7 3.1 1
Phenanthrene ND ug/L 09/25/23 19:26 85-01-809/25/23 12:318.3 1.7 1
Phenol ND ug/L 09/25/23 19:26 108-95-209/25/23 12:318.3 1.1 1
Pyrene ND ug/L 09/25/23 19:26 129-00-009/25/23 12:318.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 09/25/23 19:26 95-95-409/25/23 12:318.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/25/23 19:26 88-06-209/25/23 12:318.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)89 %09/25/23 19:26 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)88 %09/25/23 19:26 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)137 %09/25/23 19:26 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)21 %09/25/23 19:26 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)9 %09/25/23 19:26 367-12-4 S009/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)21 %09/25/23 19:26 118-79-609/25/23 12:3110-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNH-092023 Lab ID: 92689265002 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 18:23 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 18:23 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 18:23 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 18:23 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 18:23 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 18:23 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 18:23 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/30/23 18:23 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 18:23 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 18:23 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 18:23 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 18:23 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 18:23 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 18:23 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 18:23 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 18:23 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 18:23 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 18:23 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 18:23 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 18:23 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 18:23 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 18:23 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 18:23 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 18:23 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 18:23 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 18:23 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 18:23 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 18:23 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 18:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 18:23 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 18:23 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 18:23 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 18:23 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 18:23 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 18:23 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 18:23 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 18:23 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 18:23 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 18:23 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 18:23 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 18:23 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 18:23 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 18:23 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 18:23 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 18:23 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWDOWNH-092023 Lab ID: 92689265002 Collected: 09/20/23 13:05 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 18:23 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 18:23 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 18:23 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 18:23 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %09/30/23 18:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %09/30/23 18:23 17060-07-070-130 1
Toluene-d8 (S)100 %09/30/23 18:23 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 15.1 mg/L 10/03/23 16:365.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 40.0 mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 3.4 mg/L 09/22/23 17:55 16887-00-61.0 0.60 1
Sulfate 3.0 mg/L 09/22/23 17:55 14808-79-81.0 0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 0.031J mg/L 10/10/23 01:24 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 10/10/23 04:18 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable ND mg/L 09/27/23 15:30 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.021J mg/L 09/22/23 04:330.050 0.012 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand ND mg/L 10/06/23 00:1710/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP02WG-092023 Lab ID: 92689265003 Collected: 09/20/23 14:15 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 9.3 Std. Units 09/26/23 12:55 H35
True Color 200 units 09/26/23 12:55 H325.0 25.0 5
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 866 ug/L 10/08/23 15:48 7429-90-510/03/23 04:43100 30.7 1
Arsenic ND ug/L 10/08/23 15:48 7440-38-210/03/23 04:4310.0 3.4 1
Barium 30.1 ug/L 10/06/23 17:23 7440-39-310/03/23 04:4310.0 0.84 1
Beryllium ND ug/L 10/08/23 15:48 7440-41-710/03/23 04:434.0 0.17 1
Boron 13.5J ug/L 10/08/23 15:48 7440-42-810/03/23 04:4350.0 12.4 1
Cadmium ND ug/L 10/08/23 15:48 7440-43-910/03/23 04:431.0 0.33 1
Calcium 4510 ug/L 10/08/23 15:48 7440-70-210/03/23 04:43500 190 1
Chromium 2.1J ug/L 10/08/23 15:48 7440-47-310/03/23 04:435.0 1.7 1
Cobalt ND ug/L 10/06/23 17:23 7440-48-410/03/23 04:4310.0 0.96 1
Copper 5.3 ug/L 10/08/23 15:48 7440-50-810/03/23 04:435.0 2.6 1
Iron 1300 ug/L 10/08/23 15:48 7439-89-610/03/23 04:4340.0 25.0 1
Lead ND ug/L 10/08/23 15:48 7439-92-110/03/23 04:4310.0 2.1 1
Magnesium 965 ug/L 10/08/23 15:48 7439-95-410/03/23 04:43500 84.0 1
Manganese 126 ug/L 10/08/23 15:48 7439-96-510/03/23 04:435.0 1.1 1
Molybdenum 2.8J ug/L 10/08/23 15:48 7439-98-710/03/23 04:4310.0 1.6 1
Nickel 3.1J ug/L 10/08/23 15:48 7440-02-010/03/23 04:435.0 1.0 1
Selenium ND ug/L 10/08/23 15:48 7782-49-210/03/23 04:4315.0 3.9 1
Silver ND ug/L 10/08/23 15:48 7440-22-410/03/23 04:435.0 1.0 1
Sodium 79000 ug/L 10/08/23 15:48 7440-23-510/03/23 04:432000 540 1
Thallium ND ug/L 10/08/23 15:48 7440-28-010/03/23 04:4315.0 2.9 1
Zinc 13.3J ug/L 10/08/23 15:48 7440-66-610/03/23 04:4320.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved 363 ug/L 10/06/23 14:19 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 14:19 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 16.0 ug/L 10/06/23 14:19 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 14:19 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved 20.5J ug/L 10/06/23 14:19 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 14:19 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 4060 ug/L 10/06/23 14:19 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved ND ug/L 10/06/23 14:19 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved ND ug/L 10/06/23 14:19 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved 4.2J ug/L 10/06/23 14:19 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 325 ug/L 10/06/23 14:19 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 14:19 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 804 ug/L 10/06/23 14:19 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 46.2 ug/L 10/06/23 14:19 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved 4.0J ug/L 10/06/23 14:19 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved 3.5J ug/L 10/06/23 14:19 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP02WG-092023 Lab ID: 92689265003 Collected: 09/20/23 14:15 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 14:19 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 14:19 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 81400 ug/L 10/06/23 14:19 7440-23-510/03/23 23:492000 540 1
Thallium, Dissolved ND ug/L 10/06/23 14:19 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved ND ug/L 10/06/23 14:19 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 15:48 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 12:58 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/25/23 19:52 83-32-909/25/23 12:3110.0 2.0 1
Acenaphthylene ND ug/L 09/25/23 19:52 208-96-809/25/23 12:3110.0 2.0 1
Acetophenone ND ug/L 09/25/23 19:52 98-86-209/25/23 12:3110.0 1.5 1
Anthracene ND ug/L 09/25/23 19:52 120-12-709/25/23 12:3110.0 2.3 1
Atrazine ND ug/L 09/25/23 19:52 1912-24-909/25/23 12:3110.0 3.2 1
Benzaldehyde ND ug/L 09/25/23 19:52 100-52-709/25/23 12:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/25/23 19:52 56-55-309/25/23 12:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/25/23 19:52 50-32-809/25/23 12:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/25/23 19:52 205-99-209/25/23 12:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/25/23 19:52 191-24-209/25/23 12:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/25/23 19:52 207-08-909/25/23 12:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/25/23 19:52 92-52-409/25/23 12:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/25/23 19:52 101-55-309/25/23 12:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/25/23 19:52 85-68-709/25/23 12:3110.0 3.1 1
Caprolactam ND ug/L 09/25/23 19:52 105-60-209/25/23 12:3110.0 6.9 1
Carbazole ND ug/L 09/25/23 19:52 86-74-809/25/23 12:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/25/23 19:52 59-50-709/25/23 12:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/25/23 19:52 106-47-809/25/23 12:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/25/23 19:52 111-91-109/25/23 12:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/25/23 19:52 111-44-409/25/23 12:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/25/23 19:52 91-58-709/25/23 12:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/25/23 19:52 95-57-809/25/23 12:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/25/23 19:52 7005-72-309/25/23 12:3110.0 2.0 1
Chrysene ND ug/L 09/25/23 19:52 218-01-909/25/23 12:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/25/23 19:52 53-70-309/25/23 12:3110.0 3.0 1
Dibenzofuran ND ug/L 09/25/23 19:52 132-64-909/25/23 12:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/25/23 19:52 91-94-109/25/23 12:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/25/23 19:52 120-83-209/25/23 12:3110.0 1.4 1
Diethylphthalate ND ug/L 09/25/23 19:52 84-66-209/25/23 12:3110.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP02WG-092023 Lab ID: 92689265003 Collected: 09/20/23 14:15 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/25/23 19:52 105-67-909/25/23 12:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/25/23 19:52 131-11-309/25/23 12:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/25/23 19:52 84-74-209/25/23 12:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/25/23 19:52 534-52-109/25/23 12:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/25/23 19:52 51-28-509/25/23 12:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/25/23 19:52 121-14-209/25/23 12:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/25/23 19:52 606-20-209/25/23 12:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/25/23 19:52 117-84-009/25/23 12:3110.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/25/23 19:52 117-81-709/25/23 12:316.0 3.7 1
Fluoranthene ND ug/L 09/25/23 19:52 206-44-009/25/23 12:3110.0 2.2 1
Fluorene ND ug/L 09/25/23 19:52 86-73-709/25/23 12:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/25/23 19:52 87-68-309/25/23 12:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/25/23 19:52 118-74-109/25/23 12:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/25/23 19:52 77-47-409/25/23 12:3110.0 1.6 1
Hexachloroethane ND ug/L 09/25/23 19:52 67-72-109/25/23 12:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/25/23 19:52 193-39-509/25/23 12:3110.0 2.9 1
Isophorone ND ug/L 09/25/23 19:52 78-59-109/25/23 12:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/25/23 19:52 91-57-609/25/23 12:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/25/23 19:52 95-48-709/25/23 12:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/25/23 19:52 15831-10-409/25/23 12:3110.0 1.2 1
Naphthalene ND ug/L 09/25/23 19:52 91-20-309/25/23 12:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/25/23 19:52 88-74-409/25/23 12:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/25/23 19:52 99-09-209/25/23 12:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/25/23 19:52 100-01-609/25/23 12:3120.0 5.1 1
Nitrobenzene ND ug/L 09/25/23 19:52 98-95-309/25/23 12:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/25/23 19:52 88-75-509/25/23 12:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/25/23 19:52 100-02-709/25/23 12:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/25/23 19:52 621-64-709/25/23 12:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/25/23 19:52 86-30-609/25/23 12:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/25/23 19:52 108-60-109/25/23 12:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/25/23 19:52 87-86-509/25/23 12:3120.0 3.8 1
Phenanthrene ND ug/L 09/25/23 19:52 85-01-809/25/23 12:3110.0 2.0 1
Phenol ND ug/L 09/25/23 19:52 108-95-209/25/23 12:3110.0 1.4 1
Pyrene ND ug/L 09/25/23 19:52 129-00-009/25/23 12:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/25/23 19:52 95-95-409/25/23 12:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/25/23 19:52 88-06-209/25/23 12:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)24 %09/25/23 19:52 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)24 %09/25/23 19:52 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)62 %09/25/23 19:52 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)14 %09/25/23 19:52 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)21 %09/25/23 19:52 367-12-409/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)49 %09/25/23 19:52 118-79-609/25/23 12:3110-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP02WG-092023 Lab ID: 92689265003 Collected: 09/20/23 14:15 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/01/23 05:46 67-64-125.0 5.1 1
Benzene ND ug/L 10/01/23 05:46 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 10/01/23 05:46 75-27-41.0 0.31 1
Bromoform ND ug/L 10/01/23 05:46 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/01/23 05:46 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/01/23 05:46 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/01/23 05:46 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/01/23 05:46 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/01/23 05:46 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/01/23 05:46 75-00-31.0 0.65 1
Chloroform ND ug/L 10/01/23 05:46 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/01/23 05:46 74-87-31.0 0.54 1
Cyclohexane ND ug/L 10/01/23 05:46 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 10/01/23 05:46 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/01/23 05:46 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/01/23 05:46 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 10/01/23 05:46 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/01/23 05:46 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/01/23 05:46 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/01/23 05:46 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/01/23 05:46 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/01/23 05:46 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/01/23 05:46 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/01/23 05:46 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/01/23 05:46 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/01/23 05:46 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/01/23 05:46 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/01/23 05:46 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 10/01/23 05:46 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/01/23 05:46 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 10/01/23 05:46 98-82-81.0 0.33 1
Methyl acetate ND ug/L 10/01/23 05:46 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 10/01/23 05:46 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 10/01/23 05:46 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/01/23 05:46 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/01/23 05:46 1634-04-41.0 0.42 1
Styrene ND ug/L 10/01/23 05:46 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 10/01/23 05:46 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/01/23 05:46 127-18-41.0 0.29 1
Toluene ND ug/L 10/01/23 05:46 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 10/01/23 05:46 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/01/23 05:46 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/01/23 05:46 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/01/23 05:46 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/01/23 05:46 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP02WG-092023 Lab ID: 92689265003 Collected: 09/20/23 14:15 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 10/01/23 05:46 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 10/01/23 05:46 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 10/01/23 05:46 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/01/23 05:46 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %10/01/23 05:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %10/01/23 05:46 17060-07-070-130 1
Toluene-d8 (S)98 %10/01/23 05:46 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 115 mg/L 10/03/23 16:435.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 235 mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 34.1 mg/L 09/22/23 18:10 16887-00-61.0 0.60 1
Sulfate 13.6 mg/L 09/22/23 18:10 14808-79-81.0 0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 0.040J mg/L 10/10/23 01:28 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 0.83 mg/L 10/10/23 04:19 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable ND mg/L 09/27/23 15:31 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P 1.6 mg/L 09/22/23 04:330.25 0.059 5
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand 32.1 mg/L 10/06/23 00:1710/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-00-WS-092023 Lab ID: 92689265004 Collected: 09/20/23 14:35 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.7 Std. Units 09/26/23 12:56 H31
True Color 5.0 units 09/26/23 12:56 H35.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 79.1J ug/L 10/04/23 01:30 7429-90-510/03/23 04:43100 30.7 1
Arsenic ND ug/L 10/04/23 01:30 7440-38-210/03/23 04:4310.0 3.4 1
Barium 14.7 ug/L 10/04/23 01:30 7440-39-310/03/23 04:4310.0 0.84 1
Beryllium ND ug/L 10/04/23 01:30 7440-41-710/03/23 04:434.0 0.17 1
Boron ND ug/L 10/04/23 01:30 7440-42-810/03/23 04:4350.0 12.4 1
Cadmium ND ug/L 10/04/23 01:30 7440-43-910/03/23 04:431.0 0.33 1
Calcium 2440 ug/L 10/04/23 01:30 7440-70-210/03/23 04:43500 190 1
Chromium ND ug/L 10/04/23 01:30 7440-47-310/03/23 04:435.0 1.7 1
Cobalt ND ug/L 10/04/23 01:30 7440-48-410/03/23 04:4310.0 0.96 1
Copper ND ug/L 10/04/23 01:30 7440-50-810/03/23 04:435.0 2.6 1
Iron 285 ug/L 10/04/23 01:30 7439-89-610/03/23 04:4340.0 25.0 1
Lead ND ug/L 10/04/23 01:30 7439-92-110/03/23 04:4310.0 2.1 1
Magnesium 751 ug/L 10/04/23 01:30 7439-95-410/03/23 04:43500 84.0 1
Manganese 19.0 ug/L 10/04/23 01:30 7439-96-510/03/23 04:435.0 1.1 1
Molybdenum ND ug/L 10/04/23 01:30 7439-98-710/03/23 04:4310.0 1.6 1
Nickel ND ug/L 10/04/23 01:30 7440-02-010/03/23 04:435.0 1.0 1
Selenium ND ug/L 10/04/23 01:30 7782-49-210/03/23 04:4315.0 3.9 1
Silver ND ug/L 10/04/23 01:30 7440-22-410/03/23 04:435.0 1.0 1
Sodium 2100 ug/L 10/04/23 01:30 7440-23-510/03/23 04:432000 540 1
Thallium ND ug/L 10/04/23 01:30 7440-28-010/03/23 04:4315.0 2.9 1
Zinc ND ug/L 10/04/23 01:30 7440-66-610/03/23 04:4320.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 10/06/23 14:22 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 14:22 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 15.2 ug/L 10/06/23 14:22 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 14:22 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved ND ug/L 10/06/23 14:22 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 14:22 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 2440 ug/L 10/06/23 14:22 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved ND ug/L 10/06/23 14:22 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved ND ug/L 10/06/23 14:22 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved ND ug/L 10/06/23 14:22 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 124 ug/L 10/06/23 14:22 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 14:22 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 791 ug/L 10/06/23 14:22 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 14.3 ug/L 10/06/23 14:22 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved ND ug/L 10/06/23 14:22 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved ND ug/L 10/06/23 14:22 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-00-WS-092023 Lab ID: 92689265004 Collected: 09/20/23 14:35 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 14:22 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 14:22 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 2420 ug/L 10/06/23 14:22 7440-23-510/03/23 23:492000 540 1
Thallium, Dissolved ND ug/L 10/06/23 14:22 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved ND ug/L 10/06/23 14:22 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 15:50 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 13:00 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/25/23 20:18 83-32-909/25/23 12:3110.0 2.0 1
Acenaphthylene ND ug/L 09/25/23 20:18 208-96-809/25/23 12:3110.0 2.0 1
Acetophenone ND ug/L 09/25/23 20:18 98-86-209/25/23 12:3110.0 1.5 1
Anthracene ND ug/L 09/25/23 20:18 120-12-709/25/23 12:3110.0 2.3 1
Atrazine ND ug/L 09/25/23 20:18 1912-24-909/25/23 12:3110.0 3.2 1
Benzaldehyde ND ug/L 09/25/23 20:18 100-52-709/25/23 12:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/25/23 20:18 56-55-309/25/23 12:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/25/23 20:18 50-32-809/25/23 12:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/25/23 20:18 205-99-209/25/23 12:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/25/23 20:18 191-24-209/25/23 12:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/25/23 20:18 207-08-909/25/23 12:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/25/23 20:18 92-52-409/25/23 12:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/25/23 20:18 101-55-309/25/23 12:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/25/23 20:18 85-68-709/25/23 12:3110.0 3.1 1
Caprolactam ND ug/L 09/25/23 20:18 105-60-209/25/23 12:3110.0 6.9 1
Carbazole ND ug/L 09/25/23 20:18 86-74-809/25/23 12:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/25/23 20:18 59-50-709/25/23 12:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/25/23 20:18 106-47-809/25/23 12:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/25/23 20:18 111-91-109/25/23 12:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/25/23 20:18 111-44-409/25/23 12:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/25/23 20:18 91-58-709/25/23 12:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/25/23 20:18 95-57-809/25/23 12:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/25/23 20:18 7005-72-309/25/23 12:3110.0 2.0 1
Chrysene ND ug/L 09/25/23 20:18 218-01-909/25/23 12:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/25/23 20:18 53-70-309/25/23 12:3110.0 3.0 1
Dibenzofuran ND ug/L 09/25/23 20:18 132-64-909/25/23 12:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/25/23 20:18 91-94-109/25/23 12:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/25/23 20:18 120-83-209/25/23 12:3110.0 1.4 1
Diethylphthalate ND ug/L 09/25/23 20:18 84-66-209/25/23 12:3110.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-00-WS-092023 Lab ID: 92689265004 Collected: 09/20/23 14:35 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/25/23 20:18 105-67-909/25/23 12:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/25/23 20:18 131-11-309/25/23 12:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/25/23 20:18 84-74-209/25/23 12:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/25/23 20:18 534-52-109/25/23 12:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/25/23 20:18 51-28-509/25/23 12:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/25/23 20:18 121-14-209/25/23 12:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/25/23 20:18 606-20-209/25/23 12:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/25/23 20:18 117-84-009/25/23 12:3110.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/25/23 20:18 117-81-709/25/23 12:316.0 3.7 1
Fluoranthene ND ug/L 09/25/23 20:18 206-44-009/25/23 12:3110.0 2.2 1
Fluorene ND ug/L 09/25/23 20:18 86-73-709/25/23 12:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/25/23 20:18 87-68-309/25/23 12:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/25/23 20:18 118-74-109/25/23 12:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/25/23 20:18 77-47-409/25/23 12:3110.0 1.6 1
Hexachloroethane ND ug/L 09/25/23 20:18 67-72-109/25/23 12:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/25/23 20:18 193-39-509/25/23 12:3110.0 2.9 1
Isophorone ND ug/L 09/25/23 20:18 78-59-109/25/23 12:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/25/23 20:18 91-57-609/25/23 12:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/25/23 20:18 95-48-709/25/23 12:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/25/23 20:18 15831-10-409/25/23 12:3110.0 1.2 1
Naphthalene ND ug/L 09/25/23 20:18 91-20-309/25/23 12:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/25/23 20:18 88-74-409/25/23 12:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/25/23 20:18 99-09-209/25/23 12:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/25/23 20:18 100-01-609/25/23 12:3120.0 5.1 1
Nitrobenzene ND ug/L 09/25/23 20:18 98-95-309/25/23 12:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/25/23 20:18 88-75-509/25/23 12:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/25/23 20:18 100-02-709/25/23 12:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/25/23 20:18 621-64-709/25/23 12:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/25/23 20:18 86-30-609/25/23 12:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/25/23 20:18 108-60-109/25/23 12:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/25/23 20:18 87-86-509/25/23 12:3120.0 3.8 1
Phenanthrene ND ug/L 09/25/23 20:18 85-01-809/25/23 12:3110.0 2.0 1
Phenol ND ug/L 09/25/23 20:18 108-95-209/25/23 12:3110.0 1.4 1
Pyrene ND ug/L 09/25/23 20:18 129-00-009/25/23 12:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/25/23 20:18 95-95-409/25/23 12:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/25/23 20:18 88-06-209/25/23 12:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)110 %09/25/23 20:18 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)102 %09/25/23 20:18 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)135 %09/25/23 20:18 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)10 %09/25/23 20:18 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)8 %09/25/23 20:18 367-12-4 S009/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)21 %09/25/23 20:18 118-79-609/25/23 12:3110-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-00-WS-092023 Lab ID: 92689265004 Collected: 09/20/23 14:35 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 18:41 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 18:41 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 18:41 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 18:41 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 18:41 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 18:41 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 18:41 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/30/23 18:41 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 18:41 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 18:41 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 18:41 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 18:41 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 18:41 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 18:41 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 18:41 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 18:41 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 18:41 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 18:41 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 18:41 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 18:41 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 18:41 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 18:41 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 18:41 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 18:41 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 18:41 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 18:41 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 18:41 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 18:41 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 18:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 18:41 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 18:41 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 18:41 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 18:41 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 18:41 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 18:41 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 18:41 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 18:41 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 18:41 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 18:41 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 18:41 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 18:41 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 18:41 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 18:41 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 18:41 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 18:41 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-00-WS-092023 Lab ID: 92689265004 Collected: 09/20/23 14:35 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 18:41 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 18:41 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 18:41 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 18:41 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %09/30/23 18:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %09/30/23 18:41 17060-07-070-130 1
Toluene-d8 (S)101 %09/30/23 18:41 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 11.5 mg/L 10/03/23 16:545.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids ND mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 1.2 mg/L 09/22/23 18:24 16887-00-61.0 0.60 1
Sulfate 1.6 mg/L 09/22/23 18:24 14808-79-81.0 0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 10/10/23 01:30 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 10/10/23 04:20 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable ND mg/L 09/27/23 15:32 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 09/22/23 04:340.050 0.012 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand ND mg/L 10/06/23 00:1710/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-02-WS-092023 Lab ID: 92689265005 Collected: 09/20/23 14:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.6 Std. Units 09/26/23 12:56 H31
True Color 5.0 units 09/26/23 12:56 H35.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 75.2J ug/L 10/04/23 03:58 7429-90-510/03/23 04:43100 30.7 1
Arsenic ND ug/L 10/04/23 03:58 7440-38-210/03/23 04:4310.0 3.4 1
Barium 14.6 ug/L 10/04/23 03:58 7440-39-310/03/23 04:4310.0 0.84 1
Beryllium ND ug/L 10/04/23 03:58 7440-41-710/03/23 04:434.0 0.17 1
Boron ND ug/L 10/04/23 03:58 7440-42-810/03/23 04:4350.0 12.4 1
Cadmium ND ug/L 10/04/23 03:58 7440-43-910/03/23 04:431.0 0.33 1
Calcium 2440 ug/L 10/04/23 03:58 7440-70-210/03/23 04:43500 190 1
Chromium ND ug/L 10/04/23 03:58 7440-47-310/03/23 04:435.0 1.7 1
Cobalt ND ug/L 10/04/23 03:58 7440-48-410/03/23 04:4310.0 0.96 1
Copper ND ug/L 10/04/23 03:58 7440-50-810/03/23 04:435.0 2.6 1
Iron 297 ug/L 10/04/23 03:58 7439-89-610/03/23 04:4340.0 25.0 1
Lead ND ug/L 10/04/23 03:58 7439-92-110/03/23 04:4310.0 2.1 1
Magnesium 748 ug/L 10/04/23 03:58 7439-95-410/03/23 04:43500 84.0 1
Manganese 18.4 ug/L 10/04/23 03:58 7439-96-510/03/23 04:435.0 1.1 1
Molybdenum ND ug/L 10/04/23 03:58 7439-98-710/03/23 04:4310.0 1.6 1
Nickel ND ug/L 10/04/23 03:58 7440-02-010/03/23 04:435.0 1.0 1
Selenium ND ug/L 10/04/23 03:58 7782-49-210/03/23 04:4315.0 3.9 1
Silver ND ug/L 10/04/23 03:58 7440-22-410/03/23 04:435.0 1.0 1
Sodium 1940J ug/L 10/04/23 03:58 7440-23-510/03/23 04:432000 540 1
Thallium ND ug/L 10/04/23 03:58 7440-28-010/03/23 04:4315.0 2.9 1
Zinc ND ug/L 10/04/23 03:58 7440-66-610/03/23 04:4320.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 10/06/23 14:26 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 14:26 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 14.8 ug/L 10/06/23 14:26 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 14:26 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved ND ug/L 10/06/23 14:26 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 14:26 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 2440 ug/L 10/06/23 14:26 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved ND ug/L 10/06/23 14:26 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved ND ug/L 10/06/23 14:26 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved ND ug/L 10/06/23 14:26 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 127 ug/L 10/06/23 14:26 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 14:26 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 783 ug/L 10/06/23 14:26 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 14.9 ug/L 10/06/23 14:26 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved ND ug/L 10/06/23 14:26 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved 1.7J ug/L 10/06/23 14:26 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-02-WS-092023 Lab ID: 92689265005 Collected: 09/20/23 14:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 14:26 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 14:26 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 2560 ug/L 10/06/23 14:26 7440-23-510/03/23 23:492000 540 1
Thallium, Dissolved ND ug/L 10/06/23 14:26 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved ND ug/L 10/06/23 14:26 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 15:52 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 13:03 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/26/23 09:57 83-32-909/25/23 12:318.3 1.7 1
Acenaphthylene ND ug/L 09/26/23 09:57 208-96-809/25/23 12:318.3 1.6 1
Acetophenone ND ug/L 09/26/23 09:57 98-86-209/25/23 12:318.3 1.2 1
Anthracene ND ug/L 09/26/23 09:57 120-12-709/25/23 12:318.3 1.9 1
Atrazine ND ug/L 09/26/23 09:57 1912-24-909/25/23 12:318.3 2.6 1
Benzaldehyde ND ug/L 09/26/23 09:57 100-52-709/25/23 12:318.3 3.0 1
Benzo(a)anthracene ND ug/L 09/26/23 09:57 56-55-309/25/23 12:318.3 2.2 1
Benzo(a)pyrene ND ug/L 09/26/23 09:57 50-32-809/25/23 12:318.3 2.3 1
Benzo(b)fluoranthene ND ug/L 09/26/23 09:57 205-99-209/25/23 12:318.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 09/26/23 09:57 191-24-209/25/23 12:318.3 2.4 1
Benzo(k)fluoranthene ND ug/L 09/26/23 09:57 207-08-909/25/23 12:318.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 09/26/23 09:57 92-52-409/25/23 12:318.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 09/26/23 09:57 101-55-309/25/23 12:318.3 1.5 1
Butylbenzylphthalate ND ug/L 09/26/23 09:57 85-68-709/25/23 12:318.3 2.6 1
Caprolactam ND ug/L 09/26/23 09:57 105-60-209/25/23 12:318.3 5.8 1
Carbazole ND ug/L 09/26/23 09:57 86-74-809/25/23 12:318.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/26/23 09:57 59-50-709/25/23 12:318.3 2.8 1
4-Chloroaniline ND ug/L 09/26/23 09:57 106-47-809/25/23 12:3116.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/26/23 09:57 111-91-109/25/23 12:318.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 09/26/23 09:57 111-44-409/25/23 12:318.3 1.6 1
2-Chloronaphthalene ND ug/L 09/26/23 09:57 91-58-709/25/23 12:318.3 1.4 1
2-Chlorophenol ND ug/L 09/26/23 09:57 95-57-809/25/23 12:318.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/26/23 09:57 7005-72-309/25/23 12:318.3 1.7 1
Chrysene ND ug/L 09/26/23 09:57 218-01-909/25/23 12:318.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 09/26/23 09:57 53-70-309/25/23 12:318.3 2.5 1
Dibenzofuran ND ug/L 09/26/23 09:57 132-64-909/25/23 12:318.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/26/23 09:57 91-94-109/25/23 12:3116.7 6.8 1
2,4-Dichlorophenol ND ug/L 09/26/23 09:57 120-83-209/25/23 12:318.3 1.2 1
Diethylphthalate ND ug/L 09/26/23 09:57 84-66-209/25/23 12:318.3 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-02-WS-092023 Lab ID: 92689265005 Collected: 09/20/23 14:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/26/23 09:57 105-67-909/25/23 12:318.3 1.4 1
Dimethylphthalate ND ug/L 09/26/23 09:57 131-11-309/25/23 12:318.3 1.8 1
Di-n-butylphthalate ND ug/L 09/26/23 09:57 84-74-209/25/23 12:318.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/26/23 09:57 534-52-109/25/23 12:3116.7 6.5 1
2,4-Dinitrophenol ND ug/L 09/26/23 09:57 51-28-509/25/23 12:3141.7 21.7 1
2,4-Dinitrotoluene ND ug/L 09/26/23 09:57 121-14-209/25/23 12:318.3 1.4 1
2,6-Dinitrotoluene ND ug/L 09/26/23 09:57 606-20-209/25/23 12:318.3 1.4 1
Di-n-octylphthalate ND ug/L 09/26/23 09:57 117-84-009/25/23 12:318.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/26/23 09:57 117-81-709/25/23 12:315.0 3.1 1
Fluoranthene ND ug/L 09/26/23 09:57 206-44-009/25/23 12:318.3 1.8 1
Fluorene ND ug/L 09/26/23 09:57 86-73-709/25/23 12:318.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 09/26/23 09:57 87-68-309/25/23 12:318.3 1.5 1
Hexachlorobenzene ND ug/L 09/26/23 09:57 118-74-109/25/23 12:318.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 09/26/23 09:57 77-47-409/25/23 12:318.3 1.3 1
Hexachloroethane ND ug/L 09/26/23 09:57 67-72-109/25/23 12:318.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/26/23 09:57 193-39-509/25/23 12:318.3 2.4 1
Isophorone ND ug/L 09/26/23 09:57 78-59-109/25/23 12:318.3 1.4 1
2-Methylnaphthalene ND ug/L 09/26/23 09:57 91-57-609/25/23 12:318.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/26/23 09:57 95-48-709/25/23 12:318.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/26/23 09:57 15831-10-409/25/23 12:318.3 1.0 1
Naphthalene ND ug/L 09/26/23 09:57 91-20-309/25/23 12:318.3 1.7 1
2-Nitroaniline ND ug/L 09/26/23 09:57 88-74-409/25/23 12:3116.7 2.5 1
3-Nitroaniline ND ug/L 09/26/23 09:57 99-09-209/25/23 12:3116.7 3.1 1
4-Nitroaniline ND ug/L 09/26/23 09:57 100-01-609/25/23 12:3116.7 4.2 1
Nitrobenzene ND ug/L 09/26/23 09:57 98-95-309/25/23 12:318.3 1.6 1
2-Nitrophenol ND ug/L 09/26/23 09:57 88-75-509/25/23 12:318.3 1.2 1
4-Nitrophenol ND ug/L 09/26/23 09:57 100-02-709/25/23 12:3141.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 09/26/23 09:57 621-64-709/25/23 12:318.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 09/26/23 09:57 86-30-609/25/23 12:318.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/26/23 09:57 108-60-109/25/23 12:318.3 0.96 1
Pentachlorophenol ND ug/L 09/26/23 09:57 87-86-509/25/23 12:3116.7 3.1 1
Phenanthrene ND ug/L 09/26/23 09:57 85-01-809/25/23 12:318.3 1.7 1
Phenol ND ug/L 09/26/23 09:57 108-95-209/25/23 12:318.3 1.1 1
Pyrene 2.4J ug/L 09/26/23 09:57 129-00-009/25/23 12:318.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 09/26/23 09:57 95-95-409/25/23 12:318.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/26/23 09:57 88-06-209/25/23 12:318.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)115 %09/26/23 09:57 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)109 %09/26/23 09:57 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)138 %09/26/23 09:57 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)52 %09/26/23 09:57 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)67 %09/26/23 09:57 367-12-409/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)107 %09/26/23 09:57 118-79-609/25/23 12:3110-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-02-WS-092023 Lab ID: 92689265005 Collected: 09/20/23 14:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 03:18 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 03:18 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 03:18 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 03:18 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 03:18 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 03:18 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 03:18 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/30/23 03:18 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 03:18 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 03:18 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 03:18 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 03:18 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 03:18 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 03:18 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 03:18 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 03:18 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 03:18 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 03:18 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 03:18 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 03:18 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 03:18 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 03:18 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 03:18 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 03:18 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 03:18 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 03:18 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 03:18 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 03:18 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 03:18 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 03:18 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 03:18 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 03:18 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 03:18 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 03:18 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 03:18 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 03:18 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 03:18 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 03:18 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 03:18 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 03:18 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 03:18 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 03:18 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 03:18 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 03:18 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 03:18 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-02-WS-092023 Lab ID: 92689265005 Collected: 09/20/23 14:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 03:18 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 03:18 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 03:18 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 03:18 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %09/30/23 03:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/30/23 03:18 17060-07-070-130 1
Toluene-d8 (S)100 %09/30/23 03:18 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 10.4 mg/L 10/03/23 17:005.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids ND mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 1.2 mg/L 09/22/23 18:38 16887-00-61.0 0.60 1
Sulfate 1.6 mg/L 09/22/23 18:38 14808-79-81.0 0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 10/10/23 01:31 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 10/10/23 04:21 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable ND mg/L 09/27/23 15:33 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 09/22/23 04:340.050 0.012 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand ND mg/L 10/06/23 00:1810/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-05-WS-092023 Lab ID: 92689265006 Collected: 09/20/23 15:10 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.6 Std. Units 09/26/23 12:57 H31
True Color 5.0 units 09/26/23 12:57 H35.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 65.1J ug/L 10/04/23 04:02 7429-90-510/03/23 04:43100 30.7 1
Arsenic ND ug/L 10/04/23 04:02 7440-38-210/03/23 04:4310.0 3.4 1
Barium 14.7 ug/L 10/04/23 04:02 7440-39-310/03/23 04:4310.0 0.84 1
Beryllium ND ug/L 10/04/23 04:02 7440-41-710/03/23 04:434.0 0.17 1
Boron ND ug/L 10/04/23 04:02 7440-42-810/03/23 04:4350.0 12.4 1
Cadmium ND ug/L 10/04/23 04:02 7440-43-910/03/23 04:431.0 0.33 1
Calcium 2450 ug/L 10/04/23 04:02 7440-70-210/03/23 04:43500 190 1
Chromium ND ug/L 10/04/23 04:02 7440-47-310/03/23 04:435.0 1.7 1
Cobalt ND ug/L 10/04/23 04:02 7440-48-410/03/23 04:4310.0 0.96 1
Copper ND ug/L 10/04/23 04:02 7440-50-810/03/23 04:435.0 2.6 1
Iron 262 ug/L 10/04/23 04:02 7439-89-610/03/23 04:4340.0 25.0 1
Lead ND ug/L 10/04/23 04:02 7439-92-110/03/23 04:4310.0 2.1 1
Magnesium 751 ug/L 10/04/23 04:02 7439-95-410/03/23 04:43500 84.0 1
Manganese 17.9 ug/L 10/04/23 04:02 7439-96-510/03/23 04:435.0 1.1 1
Molybdenum ND ug/L 10/04/23 04:02 7439-98-710/03/23 04:4310.0 1.6 1
Nickel ND ug/L 10/04/23 04:02 7440-02-010/03/23 04:435.0 1.0 1
Selenium ND ug/L 10/04/23 04:02 7782-49-210/03/23 04:4315.0 3.9 1
Silver ND ug/L 10/04/23 04:02 7440-22-410/03/23 04:435.0 1.0 1
Sodium 2260 ug/L 10/04/23 04:02 7440-23-510/03/23 04:432000 540 1
Thallium ND ug/L 10/04/23 04:02 7440-28-010/03/23 04:4315.0 2.9 1
Zinc ND ug/L 10/04/23 04:02 7440-66-610/03/23 04:4320.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 10/06/23 14:29 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 14:29 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 15.1 ug/L 10/06/23 14:29 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 14:29 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved ND ug/L 10/06/23 14:29 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 14:29 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 2450 ug/L 10/06/23 14:29 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved ND ug/L 10/06/23 14:29 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved ND ug/L 10/06/23 14:29 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved ND ug/L 10/06/23 14:29 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 130 ug/L 10/06/23 14:29 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 14:29 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 787 ug/L 10/06/23 14:29 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 14.9 ug/L 10/06/23 14:29 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved ND ug/L 10/06/23 14:29 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved ND ug/L 10/06/23 14:29 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-05-WS-092023 Lab ID: 92689265006 Collected: 09/20/23 15:10 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 14:29 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 14:29 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 2520 ug/L 10/06/23 14:29 7440-23-510/03/23 23:492000 540 1
Thallium, Dissolved ND ug/L 10/06/23 14:29 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved ND ug/L 10/06/23 14:29 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 15:54 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 13:05 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/26/23 10:23 83-32-909/25/23 12:3110.0 2.0 1
Acenaphthylene ND ug/L 09/26/23 10:23 208-96-809/25/23 12:3110.0 2.0 1
Acetophenone ND ug/L 09/26/23 10:23 98-86-209/25/23 12:3110.0 1.5 1
Anthracene ND ug/L 09/26/23 10:23 120-12-709/25/23 12:3110.0 2.3 1
Atrazine ND ug/L 09/26/23 10:23 1912-24-909/25/23 12:3110.0 3.2 1
Benzaldehyde ND ug/L 09/26/23 10:23 100-52-709/25/23 12:3110.0 3.6 1
Benzo(a)anthracene ND ug/L 09/26/23 10:23 56-55-309/25/23 12:3110.0 2.7 1
Benzo(a)pyrene ND ug/L 09/26/23 10:23 50-32-809/25/23 12:3110.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/26/23 10:23 205-99-209/25/23 12:3110.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/26/23 10:23 191-24-209/25/23 12:3110.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/26/23 10:23 207-08-909/25/23 12:3110.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/26/23 10:23 92-52-409/25/23 12:3110.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/26/23 10:23 101-55-309/25/23 12:3110.0 1.8 1
Butylbenzylphthalate ND ug/L 09/26/23 10:23 85-68-709/25/23 12:3110.0 3.1 1
Caprolactam ND ug/L 09/26/23 10:23 105-60-209/25/23 12:3110.0 6.9 1
Carbazole ND ug/L 09/26/23 10:23 86-74-809/25/23 12:3110.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/26/23 10:23 59-50-709/25/23 12:3110.0 3.3 1
4-Chloroaniline ND ug/L 09/26/23 10:23 106-47-809/25/23 12:3120.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/26/23 10:23 111-91-109/25/23 12:3110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/26/23 10:23 111-44-409/25/23 12:3110.0 1.9 1
2-Chloronaphthalene ND ug/L 09/26/23 10:23 91-58-709/25/23 12:3110.0 1.7 1
2-Chlorophenol ND ug/L 09/26/23 10:23 95-57-809/25/23 12:3110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/26/23 10:23 7005-72-309/25/23 12:3110.0 2.0 1
Chrysene ND ug/L 09/26/23 10:23 218-01-909/25/23 12:3110.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/26/23 10:23 53-70-309/25/23 12:3110.0 3.0 1
Dibenzofuran ND ug/L 09/26/23 10:23 132-64-909/25/23 12:3110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/26/23 10:23 91-94-109/25/23 12:3120.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/26/23 10:23 120-83-209/25/23 12:3110.0 1.4 1
Diethylphthalate ND ug/L 09/26/23 10:23 84-66-209/25/23 12:3110.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-05-WS-092023 Lab ID: 92689265006 Collected: 09/20/23 15:10 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/26/23 10:23 105-67-909/25/23 12:3110.0 1.7 1
Dimethylphthalate ND ug/L 09/26/23 10:23 131-11-309/25/23 12:3110.0 2.1 1
Di-n-butylphthalate ND ug/L 09/26/23 10:23 84-74-209/25/23 12:3110.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/26/23 10:23 534-52-109/25/23 12:3120.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/26/23 10:23 51-28-509/25/23 12:3150.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/26/23 10:23 121-14-209/25/23 12:3110.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/26/23 10:23 606-20-209/25/23 12:3110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/26/23 10:23 117-84-009/25/23 12:3110.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/26/23 10:23 117-81-709/25/23 12:316.0 3.7 1
Fluoranthene ND ug/L 09/26/23 10:23 206-44-009/25/23 12:3110.0 2.2 1
Fluorene ND ug/L 09/26/23 10:23 86-73-709/25/23 12:3110.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/26/23 10:23 87-68-309/25/23 12:3110.0 1.8 1
Hexachlorobenzene ND ug/L 09/26/23 10:23 118-74-109/25/23 12:3110.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/26/23 10:23 77-47-409/25/23 12:3110.0 1.6 1
Hexachloroethane ND ug/L 09/26/23 10:23 67-72-109/25/23 12:3110.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/26/23 10:23 193-39-509/25/23 12:3110.0 2.9 1
Isophorone ND ug/L 09/26/23 10:23 78-59-109/25/23 12:3110.0 1.7 1
2-Methylnaphthalene ND ug/L 09/26/23 10:23 91-57-609/25/23 12:3110.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/26/23 10:23 95-48-709/25/23 12:3110.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/26/23 10:23 15831-10-409/25/23 12:3110.0 1.2 1
Naphthalene ND ug/L 09/26/23 10:23 91-20-309/25/23 12:3110.0 2.1 1
2-Nitroaniline ND ug/L 09/26/23 10:23 88-74-409/25/23 12:3120.0 3.0 1
3-Nitroaniline ND ug/L 09/26/23 10:23 99-09-209/25/23 12:3120.0 3.8 1
4-Nitroaniline ND ug/L 09/26/23 10:23 100-01-609/25/23 12:3120.0 5.1 1
Nitrobenzene ND ug/L 09/26/23 10:23 98-95-309/25/23 12:3110.0 1.9 1
2-Nitrophenol ND ug/L 09/26/23 10:23 88-75-509/25/23 12:3110.0 1.4 1
4-Nitrophenol ND ug/L 09/26/23 10:23 100-02-709/25/23 12:3150.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/26/23 10:23 621-64-709/25/23 12:3110.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/26/23 10:23 86-30-609/25/23 12:3110.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/26/23 10:23 108-60-109/25/23 12:3110.0 1.2 1
Pentachlorophenol ND ug/L 09/26/23 10:23 87-86-509/25/23 12:3120.0 3.8 1
Phenanthrene ND ug/L 09/26/23 10:23 85-01-809/25/23 12:3110.0 2.0 1
Phenol ND ug/L 09/26/23 10:23 108-95-209/25/23 12:3110.0 1.4 1
Pyrene ND ug/L 09/26/23 10:23 129-00-009/25/23 12:3110.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/26/23 10:23 95-95-409/25/23 12:3110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/26/23 10:23 88-06-209/25/23 12:3110.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)84 %09/26/23 10:23 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)80 %09/26/23 10:23 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)92 %09/26/23 10:23 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)39 %09/26/23 10:23 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)22 %09/26/23 10:23 367-12-409/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)31 %09/26/23 10:23 118-79-609/25/23 12:3110-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-05-WS-092023 Lab ID: 92689265006 Collected: 09/20/23 15:10 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 03:35 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 03:35 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 03:35 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 03:35 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 03:35 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 03:35 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 03:35 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/30/23 03:35 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 03:35 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 03:35 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 03:35 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 03:35 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 03:35 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 03:35 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 03:35 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 03:35 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 03:35 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 03:35 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 03:35 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 03:35 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 03:35 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 03:35 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 03:35 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 03:35 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 03:35 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 03:35 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 03:35 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 03:35 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 03:35 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 03:35 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 03:35 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 03:35 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 03:35 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 03:35 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 03:35 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 03:35 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 03:35 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 03:35 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 03:35 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 03:35 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 03:35 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 03:35 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 03:35 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 03:35 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 03:35 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-05-WS-092023 Lab ID: 92689265006 Collected: 09/20/23 15:10 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 03:35 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 03:35 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 03:35 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 03:35 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %09/30/23 03:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/30/23 03:35 17060-07-070-130 1
Toluene-d8 (S)99 %09/30/23 03:35 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 10.9 mg/L 10/03/23 17:055.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids ND mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 1.2 mg/L 09/22/23 19:21 16887-00-61.0 0.60 1
Sulfate 1.8 mg/L 09/22/23 19:21 14808-79-81.0 0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 10/10/23 01:32 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 10/10/23 04:22 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable ND mg/L 09/27/23 15:33 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 09/22/23 04:350.050 0.012 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand ND mg/L 10/06/23 00:1810/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-10-WS-092023 Lab ID: 92689265007 Collected: 09/20/23 15:20 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.4 Std. Units 09/26/23 12:58 H31
True Color 10.0 units 09/26/23 12:58 H35.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 82.0J ug/L 10/04/23 04:05 7429-90-510/03/23 04:43100 30.7 1
Arsenic ND ug/L 10/04/23 04:05 7440-38-210/03/23 04:4310.0 3.4 1
Barium 15.1 ug/L 10/04/23 04:05 7440-39-310/03/23 04:4310.0 0.84 1
Beryllium ND ug/L 10/04/23 04:05 7440-41-710/03/23 04:434.0 0.17 1
Boron ND ug/L 10/04/23 04:05 7440-42-810/03/23 04:4350.0 12.4 1
Cadmium ND ug/L 10/04/23 04:05 7440-43-910/03/23 04:431.0 0.33 1
Calcium 2440 ug/L 10/04/23 04:05 7440-70-210/03/23 04:43500 190 1
Chromium ND ug/L 10/04/23 04:05 7440-47-310/03/23 04:435.0 1.7 1
Cobalt ND ug/L 10/04/23 04:05 7440-48-410/03/23 04:4310.0 0.96 1
Copper ND ug/L 10/04/23 04:05 7440-50-810/03/23 04:435.0 2.6 1
Iron 289 ug/L 10/04/23 04:05 7439-89-610/03/23 04:4340.0 25.0 1
Lead ND ug/L 10/04/23 04:05 7439-92-110/03/23 04:4310.0 2.1 1
Magnesium 759 ug/L 10/04/23 04:05 7439-95-410/03/23 04:43500 84.0 1
Manganese 19.1 ug/L 10/04/23 04:05 7439-96-510/03/23 04:435.0 1.1 1
Molybdenum ND ug/L 10/04/23 04:05 7439-98-710/03/23 04:4310.0 1.6 1
Nickel ND ug/L 10/04/23 04:05 7440-02-010/03/23 04:435.0 1.0 1
Selenium ND ug/L 10/04/23 04:05 7782-49-210/03/23 04:4315.0 3.9 1
Silver ND ug/L 10/04/23 04:05 7440-22-410/03/23 04:435.0 1.0 1
Sodium 1900J ug/L 10/04/23 04:05 7440-23-510/03/23 04:432000 540 1
Thallium ND ug/L 10/04/23 04:05 7440-28-010/03/23 04:4315.0 2.9 1
Zinc ND ug/L 10/04/23 04:05 7440-66-610/03/23 04:4320.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 10/06/23 14:32 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 14:32 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 15.2 ug/L 10/06/23 14:32 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 14:32 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved ND ug/L 10/06/23 14:32 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 14:32 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 2420 ug/L 10/06/23 14:32 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved ND ug/L 10/06/23 14:32 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved ND ug/L 10/06/23 14:32 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved ND ug/L 10/06/23 14:32 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 145 ug/L 10/06/23 14:32 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 14:32 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 780 ug/L 10/06/23 14:32 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 15.5 ug/L 10/06/23 14:32 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved ND ug/L 10/06/23 14:32 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved ND ug/L 10/06/23 14:32 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-10-WS-092023 Lab ID: 92689265007 Collected: 09/20/23 15:20 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 14:32 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 14:32 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 2250 ug/L 10/06/23 14:32 7440-23-510/03/23 23:492000 540 1
Thallium, Dissolved ND ug/L 10/06/23 14:32 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved ND ug/L 10/06/23 14:32 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 15:57 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 13:07 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/26/23 18:07 83-32-909/25/23 17:268.7 1.7 1
Acenaphthylene ND ug/L 09/26/23 18:07 208-96-809/25/23 17:268.7 1.7 1
Acetophenone ND ug/L 09/26/23 18:07 98-86-209/25/23 17:268.7 1.3 1
Anthracene ND ug/L 09/26/23 18:07 120-12-709/25/23 17:268.7 2.0 1
Atrazine ND ug/L 09/26/23 18:07 1912-24-909/25/23 17:268.7 2.8 1
Benzaldehyde ND ug/L 09/26/23 18:07 100-52-709/25/23 17:268.7 3.1 1
Benzo(a)anthracene ND ug/L 09/26/23 18:07 56-55-309/25/23 17:268.7 2.3 1
Benzo(a)pyrene ND ug/L 09/26/23 18:07 50-32-809/25/23 17:268.7 2.4 1
Benzo(b)fluoranthene ND ug/L 09/26/23 18:07 205-99-209/25/23 17:268.7 2.3 1
Benzo(g,h,i)perylene ND ug/L 09/26/23 18:07 191-24-209/25/23 17:268.7 2.5 1
Benzo(k)fluoranthene ND ug/L 09/26/23 18:07 207-08-909/25/23 17:268.7 2.4 1
Biphenyl (Diphenyl)ND ug/L 09/26/23 18:07 92-52-409/25/23 17:268.7 1.6 1
4-Bromophenylphenyl ether ND ug/L 09/26/23 18:07 101-55-309/25/23 17:268.7 1.5 1
Butylbenzylphthalate ND ug/L 09/26/23 18:07 85-68-709/25/23 17:268.7 2.7 1
Caprolactam ND ug/L 09/26/23 18:07 105-60-209/25/23 17:268.7 6.0 1
Carbazole ND ug/L 09/26/23 18:07 86-74-809/25/23 17:268.7 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/26/23 18:07 59-50-709/25/23 17:268.7 2.9 1
4-Chloroaniline ND ug/L 09/26/23 18:07 106-47-809/25/23 17:2617.4 3.2 1
bis(2-Chloroethoxy)methane ND ug/L 09/26/23 18:07 111-91-109/25/23 17:268.7 1.6 1
bis(2-Chloroethyl) ether ND ug/L 09/26/23 18:07 111-44-409/25/23 17:268.7 1.7 1
2-Chloronaphthalene ND ug/L 09/26/23 18:07 91-58-709/25/23 17:268.7 1.5 1
2-Chlorophenol ND ug/L 09/26/23 18:07 95-57-809/25/23 17:268.7 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/26/23 18:07 7005-72-309/25/23 17:268.7 1.7 1
Chrysene ND ug/L 09/26/23 18:07 218-01-909/25/23 17:268.7 2.4 1
Dibenz(a,h)anthracene ND ug/L 09/26/23 18:07 53-70-309/25/23 17:268.7 2.6 1
Dibenzofuran ND ug/L 09/26/23 18:07 132-64-909/25/23 17:268.7 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/26/23 18:07 91-94-109/25/23 17:2617.4 7.1 1
2,4-Dichlorophenol ND ug/L 09/26/23 18:07 120-83-209/25/23 17:268.7 1.2 1
Diethylphthalate ND ug/L 09/26/23 18:07 84-66-209/25/23 17:268.7 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-10-WS-092023 Lab ID: 92689265007 Collected: 09/20/23 15:20 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/26/23 18:07 105-67-909/25/23 17:268.7 1.5 1
Dimethylphthalate ND ug/L 09/26/23 18:07 131-11-309/25/23 17:268.7 1.9 1
Di-n-butylphthalate ND ug/L 09/26/23 18:07 84-74-209/25/23 17:268.7 1.9 1
4,6-Dinitro-2-methylphenol ND ug/L 09/26/23 18:07 534-52-109/25/23 17:2617.4 6.8 1
2,4-Dinitrophenol ND ug/L 09/26/23 18:07 51-28-509/25/23 17:2643.5 22.6 1
2,4-Dinitrotoluene ND ug/L 09/26/23 18:07 121-14-209/25/23 17:268.7 1.4 1
2,6-Dinitrotoluene ND ug/L 09/26/23 18:07 606-20-209/25/23 17:268.7 1.5 1
Di-n-octylphthalate ND ug/L 09/26/23 18:07 117-84-009/25/23 17:268.7 3.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/26/23 18:07 117-81-709/25/23 17:265.2 3.2 1
Fluoranthene ND ug/L 09/26/23 18:07 206-44-009/25/23 17:268.7 1.9 1
Fluorene ND ug/L 09/26/23 18:07 86-73-709/25/23 17:268.7 1.8 1
Hexachloro-1,3-butadiene ND ug/L 09/26/23 18:07 87-68-309/25/23 17:268.7 1.5 1
Hexachlorobenzene ND ug/L 09/26/23 18:07 118-74-109/25/23 17:268.7 1.9 1
Hexachlorocyclopentadiene ND ug/L 09/26/23 18:07 77-47-409/25/23 17:268.7 1.4 1
Hexachloroethane ND ug/L 09/26/23 18:07 67-72-109/25/23 17:268.7 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/26/23 18:07 193-39-509/25/23 17:268.7 2.5 1
Isophorone ND ug/L 09/26/23 18:07 78-59-109/25/23 17:268.7 1.4 1
2-Methylnaphthalene ND ug/L 09/26/23 18:07 91-57-609/25/23 17:268.7 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/26/23 18:07 95-48-709/25/23 17:268.7 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/26/23 18:07 15831-10-409/25/23 17:268.7 1.1 1
Naphthalene ND ug/L 09/26/23 18:07 91-20-309/25/23 17:268.7 1.8 1
2-Nitroaniline ND ug/L 09/26/23 18:07 88-74-409/25/23 17:2617.4 2.6 1
3-Nitroaniline ND ug/L 09/26/23 18:07 99-09-209/25/23 17:2617.4 3.3 1
4-Nitroaniline ND ug/L 09/26/23 18:07 100-01-609/25/23 17:2617.4 4.4 1
Nitrobenzene ND ug/L 09/26/23 18:07 98-95-309/25/23 17:268.7 1.6 1
2-Nitrophenol ND ug/L 09/26/23 18:07 88-75-509/25/23 17:268.7 1.2 1
4-Nitrophenol ND ug/L 09/26/23 18:07 100-02-709/25/23 17:2643.5 5.7 1
N-Nitroso-di-n-propylamine ND ug/L 09/26/23 18:07 621-64-709/25/23 17:268.7 1.2 1
N-Nitrosodiphenylamine ND ug/L 09/26/23 18:07 86-30-609/25/23 17:268.7 2.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/26/23 18:07 108-60-109/25/23 17:268.7 1.0 1
Pentachlorophenol ND ug/L 09/26/23 18:07 87-86-509/25/23 17:2617.4 3.3 1
Phenanthrene ND ug/L 09/26/23 18:07 85-01-809/25/23 17:268.7 1.7 1
Phenol ND ug/L 09/26/23 18:07 108-95-209/25/23 17:268.7 1.2 1
Pyrene ND ug/L 09/26/23 18:07 129-00-009/25/23 17:268.7 1.9 1
2,4,5-Trichlorophenol ND ug/L 09/26/23 18:07 95-95-409/25/23 17:268.7 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/26/23 18:07 88-06-209/25/23 17:268.7 1.3 1
Surrogates
Nitrobenzene-d5 (S)118 %09/26/23 18:07 4165-60-009/25/23 17:2610-138 1
2-Fluorobiphenyl (S)125 %09/26/23 18:07 321-60-809/25/23 17:2610-130 1
Terphenyl-d14 (S)161 %09/26/23 18:07 1718-51-009/25/23 17:2619-191 1
Phenol-d6 (S)22 %09/26/23 18:07 13127-88-309/25/23 17:2610-130 1
2-Fluorophenol (S)4 %09/26/23 18:07 367-12-4 S009/25/23 17:2610-130 1
2,4,6-Tribromophenol (S)12 %09/26/23 18:07 118-79-609/25/23 17:2610-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-10-WS-092023 Lab ID: 92689265007 Collected: 09/20/23 15:20 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 03:53 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 03:53 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 03:53 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 03:53 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 03:53 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 03:53 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 03:53 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/30/23 03:53 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 03:53 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 03:53 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 03:53 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 03:53 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 03:53 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 03:53 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 03:53 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 03:53 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 03:53 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 03:53 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 03:53 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 03:53 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 03:53 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 03:53 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 03:53 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 03:53 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 03:53 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 03:53 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 03:53 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 03:53 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 03:53 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 03:53 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 03:53 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 03:53 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 03:53 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 03:53 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 03:53 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 03:53 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 03:53 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 03:53 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 03:53 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 03:53 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 03:53 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 03:53 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 03:53 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 03:53 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 03:53 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW01-10-WS-092023 Lab ID: 92689265007 Collected: 09/20/23 15:20 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 03:53 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 03:53 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 03:53 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 03:53 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %09/30/23 03:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/30/23 03:53 17060-07-070-130 1
Toluene-d8 (S)100 %09/30/23 03:53 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 10.2 mg/L 10/03/23 17:115.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids ND mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 1.2 mg/L 09/22/23 19:36 16887-00-61.0 0.60 1
Sulfate 1.5 mg/L 09/22/23 19:36 14808-79-81.0 0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 10/10/23 01:34 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 10/10/23 04:24 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable ND mg/L 09/27/23 15:37 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 09/22/23 04:350.050 0.012 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand ND mg/L 10/06/23 00:1810/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP01-WG-092023 Lab ID: 92689265008 Collected: 09/20/23 15:30 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 10.2 Std. Units 09/26/23 13:00 H35
True Color 250 units 09/26/23 13:00 H325.0 25.0 5
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 1070 ug/L 10/04/23 04:09 7429-90-510/03/23 04:43100 30.7 1
Arsenic ND ug/L 10/04/23 04:09 7440-38-210/03/23 04:4310.0 3.4 1
Barium 75.6 ug/L 10/04/23 04:09 7440-39-310/03/23 04:4310.0 0.84 1
Beryllium ND ug/L 10/04/23 04:09 7440-41-710/03/23 04:434.0 0.17 1
Boron 192 ug/L 10/04/23 04:09 7440-42-810/03/23 04:4350.0 12.4 1
Cadmium 0.43J ug/L 10/04/23 04:09 7440-43-910/03/23 04:431.0 0.33 1
Calcium 10700 ug/L 10/04/23 04:09 7440-70-210/03/23 04:43500 190 1
Chromium 18.5 ug/L 10/04/23 04:09 7440-47-310/03/23 04:435.0 1.7 1
Cobalt 2.4J ug/L 10/04/23 04:09 7440-48-410/03/23 04:4310.0 0.96 1
Copper 8.2 ug/L 10/04/23 04:09 7440-50-810/03/23 04:435.0 2.6 1
Iron 2390 ug/L 10/04/23 04:09 7439-89-610/03/23 04:4340.0 25.0 1
Lead ND ug/L 10/04/23 04:09 7439-92-110/03/23 04:4310.0 2.1 1
Magnesium 1210 ug/L 10/04/23 04:09 7439-95-410/03/23 04:43500 84.0 1
Manganese 207 ug/L 10/04/23 04:09 7439-96-510/03/23 04:435.0 1.1 1
Molybdenum 11.1 ug/L 10/04/23 04:09 7439-98-710/03/23 04:4310.0 1.6 1
Nickel 7.0 ug/L 10/04/23 04:09 7440-02-010/03/23 04:435.0 1.0 1
Selenium ND ug/L 10/04/23 04:09 7782-49-210/03/23 04:4315.0 3.9 1
Silver ND ug/L 10/04/23 04:09 7440-22-410/03/23 04:435.0 1.0 1
Sodium 485000 ug/L 10/06/23 17:26 7440-23-510/03/23 04:4320000 5400 10
Thallium ND ug/L 10/04/23 04:09 7440-28-010/03/23 04:4315.0 2.9 1
Zinc 75.2 ug/L 10/04/23 04:09 7440-66-610/03/23 04:4320.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved 396 ug/L 10/06/23 14:36 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 14:36 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 44.6 ug/L 10/06/23 14:36 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 14:36 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved 143 ug/L 10/06/23 14:36 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 14:36 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 7320 ug/L 10/06/23 14:36 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved 13.7 ug/L 10/06/23 14:36 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved 1.5J ug/L 10/06/23 14:36 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved 3.7J ug/L 10/06/23 14:36 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 1160 ug/L 10/06/23 14:36 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 14:36 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 910 ug/L 10/06/23 14:36 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 114 ug/L 10/06/23 14:36 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved 7.9J ug/L 10/06/23 14:36 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved 5.9 ug/L 10/06/23 14:36 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP01-WG-092023 Lab ID: 92689265008 Collected: 09/20/23 15:30 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 14:36 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 14:36 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 372000 ug/L 10/08/23 15:41 7440-23-510/03/23 23:4910000 2700 5
Thallium, Dissolved ND ug/L 10/06/23 14:36 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved 50.7 ug/L 10/06/23 14:36 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 16:04 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 13:09 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/26/23 19:50 83-32-909/25/23 17:2610.0 2.0 1
Acenaphthylene ND ug/L 09/26/23 19:50 208-96-809/25/23 17:2610.0 2.0 1
Acetophenone ND ug/L 09/26/23 19:50 98-86-209/25/23 17:2610.0 1.5 1
Anthracene ND ug/L 09/26/23 19:50 120-12-709/25/23 17:2610.0 2.3 1
Atrazine ND ug/L 09/26/23 19:50 1912-24-909/25/23 17:2610.0 3.2 1
Benzaldehyde ND ug/L 09/26/23 19:50 100-52-709/25/23 17:2610.0 3.6 1
Benzo(a)anthracene ND ug/L 09/26/23 19:50 56-55-309/25/23 17:2610.0 2.7 1
Benzo(a)pyrene ND ug/L 09/26/23 19:50 50-32-809/25/23 17:2610.0 2.8 1
Benzo(b)fluoranthene ND ug/L 09/26/23 19:50 205-99-209/25/23 17:2610.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 09/26/23 19:50 191-24-209/25/23 17:2610.0 2.8 1
Benzo(k)fluoranthene ND ug/L 09/26/23 19:50 207-08-909/25/23 17:2610.0 2.7 1
Biphenyl (Diphenyl)ND ug/L 09/26/23 19:50 92-52-409/25/23 17:2610.0 1.8 1
4-Bromophenylphenyl ether ND ug/L 09/26/23 19:50 101-55-309/25/23 17:2610.0 1.8 1
Butylbenzylphthalate ND ug/L 09/26/23 19:50 85-68-709/25/23 17:2610.0 3.1 1
Caprolactam ND ug/L 09/26/23 19:50 105-60-209/25/23 17:2610.0 6.9 1
Carbazole ND ug/L 09/26/23 19:50 86-74-809/25/23 17:2610.0 2.4 1
4-Chloro-3-methylphenol ND ug/L 09/26/23 19:50 59-50-709/25/23 17:2610.0 3.3 1
4-Chloroaniline ND ug/L 09/26/23 19:50 106-47-809/25/23 17:2620.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 09/26/23 19:50 111-91-109/25/23 17:2610.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/26/23 19:50 111-44-409/25/23 17:2610.0 1.9 1
2-Chloronaphthalene ND ug/L 09/26/23 19:50 91-58-709/25/23 17:2610.0 1.7 1
2-Chlorophenol ND ug/L 09/26/23 19:50 95-57-809/25/23 17:2610.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/26/23 19:50 7005-72-309/25/23 17:2610.0 2.0 1
Chrysene ND ug/L 09/26/23 19:50 218-01-909/25/23 17:2610.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 09/26/23 19:50 53-70-309/25/23 17:2610.0 3.0 1
Dibenzofuran ND ug/L 09/26/23 19:50 132-64-909/25/23 17:2610.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/26/23 19:50 91-94-109/25/23 17:2620.0 8.1 1
2,4-Dichlorophenol ND ug/L 09/26/23 19:50 120-83-209/25/23 17:2610.0 1.4 1
Diethylphthalate ND ug/L 09/26/23 19:50 84-66-209/25/23 17:2610.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP01-WG-092023 Lab ID: 92689265008 Collected: 09/20/23 15:30 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/26/23 19:50 105-67-909/25/23 17:2610.0 1.7 1
Dimethylphthalate ND ug/L 09/26/23 19:50 131-11-309/25/23 17:2610.0 2.1 1
Di-n-butylphthalate ND ug/L 09/26/23 19:50 84-74-209/25/23 17:2610.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 09/26/23 19:50 534-52-109/25/23 17:2620.0 7.8 1
2,4-Dinitrophenol ND ug/L 09/26/23 19:50 51-28-509/25/23 17:2650.0 26.0 1
2,4-Dinitrotoluene ND ug/L 09/26/23 19:50 121-14-209/25/23 17:2610.0 1.6 1
2,6-Dinitrotoluene ND ug/L 09/26/23 19:50 606-20-209/25/23 17:2610.0 1.7 1
Di-n-octylphthalate ND ug/L 09/26/23 19:50 117-84-009/25/23 17:2610.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/26/23 19:50 117-81-709/25/23 17:266.0 3.7 1
Fluoranthene ND ug/L 09/26/23 19:50 206-44-009/25/23 17:2610.0 2.2 1
Fluorene ND ug/L 09/26/23 19:50 86-73-709/25/23 17:2610.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 09/26/23 19:50 87-68-309/25/23 17:2610.0 1.8 1
Hexachlorobenzene ND ug/L 09/26/23 19:50 118-74-109/25/23 17:2610.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 09/26/23 19:50 77-47-409/25/23 17:2610.0 1.6 1
Hexachloroethane ND ug/L 09/26/23 19:50 67-72-109/25/23 17:2610.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/26/23 19:50 193-39-509/25/23 17:2610.0 2.9 1
Isophorone ND ug/L 09/26/23 19:50 78-59-109/25/23 17:2610.0 1.7 1
2-Methylnaphthalene ND ug/L 09/26/23 19:50 91-57-609/25/23 17:2610.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 09/26/23 19:50 95-48-709/25/23 17:2610.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/26/23 19:50 15831-10-409/25/23 17:2610.0 1.2 1
Naphthalene ND ug/L 09/26/23 19:50 91-20-309/25/23 17:2610.0 2.1 1
2-Nitroaniline ND ug/L 09/26/23 19:50 88-74-409/25/23 17:2620.0 3.0 1
3-Nitroaniline ND ug/L 09/26/23 19:50 99-09-209/25/23 17:2620.0 3.8 1
4-Nitroaniline ND ug/L 09/26/23 19:50 100-01-609/25/23 17:2620.0 5.1 1
Nitrobenzene ND ug/L 09/26/23 19:50 98-95-309/25/23 17:2610.0 1.9 1
2-Nitrophenol ND ug/L 09/26/23 19:50 88-75-509/25/23 17:2610.0 1.4 1
4-Nitrophenol ND ug/L 09/26/23 19:50 100-02-709/25/23 17:2650.0 6.6 1
N-Nitroso-di-n-propylamine ND ug/L 09/26/23 19:50 621-64-709/25/23 17:2610.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 09/26/23 19:50 86-30-609/25/23 17:2610.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/26/23 19:50 108-60-109/25/23 17:2610.0 1.2 1
Pentachlorophenol ND ug/L 09/26/23 19:50 87-86-509/25/23 17:2620.0 3.8 1
Phenanthrene ND ug/L 09/26/23 19:50 85-01-809/25/23 17:2610.0 2.0 1
Phenol ND ug/L 09/26/23 19:50 108-95-209/25/23 17:2610.0 1.4 1
Pyrene ND ug/L 09/26/23 19:50 129-00-009/25/23 17:2610.0 2.2 1
2,4,5-Trichlorophenol ND ug/L 09/26/23 19:50 95-95-409/25/23 17:2610.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/26/23 19:50 88-06-209/25/23 17:2610.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)59 %09/26/23 19:50 4165-60-009/25/23 17:2610-138 1
2-Fluorobiphenyl (S)61 %09/26/23 19:50 321-60-809/25/23 17:2610-130 1
Terphenyl-d14 (S)149 %09/26/23 19:50 1718-51-009/25/23 17:2619-191 1
Phenol-d6 (S)35 %09/26/23 19:50 13127-88-309/25/23 17:2610-130 1
2-Fluorophenol (S)47 %09/26/23 19:50 367-12-409/25/23 17:2610-130 1
2,4,6-Tribromophenol (S)113 %09/26/23 19:50 118-79-609/25/23 17:2610-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP01-WG-092023 Lab ID: 92689265008 Collected: 09/20/23 15:30 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/01/23 06:05 67-64-125.0 5.1 1
Benzene ND ug/L 10/01/23 06:05 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 10/01/23 06:05 75-27-41.0 0.31 1
Bromoform ND ug/L 10/01/23 06:05 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/01/23 06:05 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/01/23 06:05 78-93-35.0 4.0 1
Carbon disulfide 1.8J ug/L 10/01/23 06:05 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/01/23 06:05 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/01/23 06:05 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/01/23 06:05 75-00-31.0 0.65 1
Chloroform ND ug/L 10/01/23 06:05 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/01/23 06:05 74-87-31.0 0.54 1
Cyclohexane ND ug/L 10/01/23 06:05 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 10/01/23 06:05 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/01/23 06:05 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/01/23 06:05 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 10/01/23 06:05 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/01/23 06:05 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/01/23 06:05 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/01/23 06:05 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/01/23 06:05 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/01/23 06:05 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/01/23 06:05 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/01/23 06:05 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/01/23 06:05 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/01/23 06:05 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/01/23 06:05 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/01/23 06:05 10061-02-61.0 0.36 1
Ethylbenzene 0.90J ug/L 10/01/23 06:05 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/01/23 06:05 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 10/01/23 06:05 98-82-81.0 0.33 1
Methyl acetate ND ug/L 10/01/23 06:05 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 10/01/23 06:05 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 10/01/23 06:05 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/01/23 06:05 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/01/23 06:05 1634-04-41.0 0.42 1
Styrene ND ug/L 10/01/23 06:05 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 10/01/23 06:05 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/01/23 06:05 127-18-41.0 0.29 1
Toluene ND ug/L 10/01/23 06:05 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 10/01/23 06:05 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/01/23 06:05 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/01/23 06:05 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/01/23 06:05 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/01/23 06:05 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SEEP01-WG-092023 Lab ID: 92689265008 Collected: 09/20/23 15:30 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 10/01/23 06:05 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 10/01/23 06:05 75-01-41.0 0.39 1
m&p-Xylene 2.2 ug/L 10/01/23 06:05 179601-23-12.0 0.71 1
o-Xylene 0.98J ug/L 10/01/23 06:05 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %10/01/23 06:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/01/23 06:05 17060-07-070-130 1
Toluene-d8 (S)98 %10/01/23 06:05 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 503 mg/L 10/03/23 19:195.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 1210 mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 23.4 mg/L 09/22/23 19:50 16887-00-61.0 0.60 1
Sulfate 223 mg/L 09/22/23 23:10 14808-79-85.0 2.5 5
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 0.33 mg/L 10/10/23 01:35 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 2.0 mg/L 10/10/23 04:25 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable 0.011J mg/L 09/27/23 15:38 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.95 mg/L 09/22/23 04:360.25 0.059 5
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand 146 mg/L 10/06/23 00:1910/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW02-WS-092023 Lab ID: 92689265009 Collected: 09/20/23 15:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.6 Std. Units 09/26/23 13:01 H31
True Color 5.0 units 09/26/23 13:01 H35.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 67.0J ug/L 10/04/23 04:13 7429-90-510/03/23 04:43100 30.7 1
Arsenic ND ug/L 10/04/23 04:13 7440-38-210/03/23 04:4310.0 3.4 1
Barium 14.2 ug/L 10/04/23 04:13 7440-39-310/03/23 04:4310.0 0.84 1
Beryllium ND ug/L 10/04/23 04:13 7440-41-710/03/23 04:434.0 0.17 1
Boron ND ug/L 10/04/23 04:13 7440-42-810/03/23 04:4350.0 12.4 1
Cadmium ND ug/L 10/04/23 04:13 7440-43-910/03/23 04:431.0 0.33 1
Calcium 2400 ug/L 10/04/23 04:13 7440-70-210/03/23 04:43500 190 1
Chromium ND ug/L 10/04/23 04:13 7440-47-310/03/23 04:435.0 1.7 1
Cobalt ND ug/L 10/04/23 04:13 7440-48-410/03/23 04:4310.0 0.96 1
Copper ND ug/L 10/04/23 04:13 7440-50-810/03/23 04:435.0 2.6 1
Iron 251 ug/L 10/04/23 04:13 7439-89-610/03/23 04:4340.0 25.0 1
Lead ND ug/L 10/04/23 04:13 7439-92-110/03/23 04:4310.0 2.1 1
Magnesium 746 ug/L 10/04/23 04:13 7439-95-410/03/23 04:43500 84.0 1
Manganese 16.5 ug/L 10/04/23 04:13 7439-96-510/03/23 04:435.0 1.1 1
Molybdenum ND ug/L 10/04/23 04:13 7439-98-710/03/23 04:4310.0 1.6 1
Nickel ND ug/L 10/04/23 04:13 7440-02-010/03/23 04:435.0 1.0 1
Selenium ND ug/L 10/04/23 04:13 7782-49-210/03/23 04:4315.0 3.9 1
Silver ND ug/L 10/04/23 04:13 7440-22-410/03/23 04:435.0 1.0 1
Sodium 1840J ug/L 10/04/23 04:13 7440-23-510/03/23 04:432000 540 1
Thallium ND ug/L 10/04/23 04:13 7440-28-010/03/23 04:4315.0 2.9 1
Zinc ND ug/L 10/04/23 04:13 7440-66-610/03/23 04:4320.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 10/06/23 14:39 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 14:39 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 14.8 ug/L 10/06/23 14:39 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 14:39 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved ND ug/L 10/06/23 14:39 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 14:39 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 2370 ug/L 10/06/23 14:39 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved ND ug/L 10/06/23 14:39 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved ND ug/L 10/06/23 14:39 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved ND ug/L 10/06/23 14:39 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 126 ug/L 10/06/23 14:39 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 14:39 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 782 ug/L 10/06/23 14:39 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 13.6 ug/L 10/06/23 14:39 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved ND ug/L 10/06/23 14:39 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved ND ug/L 10/06/23 14:39 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW02-WS-092023 Lab ID: 92689265009 Collected: 09/20/23 15:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 14:39 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 14:39 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 2140 ug/L 10/06/23 14:39 7440-23-510/03/23 23:492000 540 1
Thallium, Dissolved ND ug/L 10/06/23 14:39 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved ND ug/L 10/06/23 14:39 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 16:06 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 13:16 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/28/23 23:08 83-32-909/27/23 13:008.7 1.7 1
Acenaphthylene ND ug/L 09/28/23 23:08 208-96-809/27/23 13:008.7 1.7 1
Acetophenone ND ug/L 09/28/23 23:08 98-86-209/27/23 13:008.7 1.3 1
Anthracene ND ug/L 09/28/23 23:08 120-12-709/27/23 13:008.7 2.0 1
Atrazine ND ug/L 09/28/23 23:08 1912-24-909/27/23 13:008.7 2.8 1
Benzaldehyde ND ug/L 09/28/23 23:08 100-52-709/27/23 13:008.7 3.1 1
Benzo(a)anthracene ND ug/L 09/28/23 23:08 56-55-309/27/23 13:008.7 2.3 1
Benzo(a)pyrene ND ug/L 09/28/23 23:08 50-32-809/27/23 13:008.7 2.4 1
Benzo(b)fluoranthene ND ug/L 09/28/23 23:08 205-99-209/27/23 13:008.7 2.3 1
Benzo(g,h,i)perylene ND ug/L 09/28/23 23:08 191-24-209/27/23 13:008.7 2.5 1
Benzo(k)fluoranthene ND ug/L 09/28/23 23:08 207-08-909/27/23 13:008.7 2.4 1
Biphenyl (Diphenyl)ND ug/L 09/28/23 23:08 92-52-409/27/23 13:008.7 1.6 1
4-Bromophenylphenyl ether ND ug/L 09/28/23 23:08 101-55-309/27/23 13:008.7 1.5 1
Butylbenzylphthalate ND ug/L 09/28/23 23:08 85-68-709/27/23 13:008.7 2.7 1
Caprolactam ND ug/L 09/28/23 23:08 105-60-209/27/23 13:008.7 6.0 1
Carbazole ND ug/L 09/28/23 23:08 86-74-809/27/23 13:008.7 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/28/23 23:08 59-50-709/27/23 13:008.7 2.9 1
4-Chloroaniline ND ug/L 09/28/23 23:08 106-47-809/27/23 13:0017.4 3.2 1
bis(2-Chloroethoxy)methane ND ug/L 09/28/23 23:08 111-91-109/27/23 13:008.7 1.6 1
bis(2-Chloroethyl) ether ND ug/L 09/28/23 23:08 111-44-409/27/23 13:008.7 1.7 1
2-Chloronaphthalene ND ug/L 09/28/23 23:08 91-58-709/27/23 13:008.7 1.5 1
2-Chlorophenol ND ug/L 09/28/23 23:08 95-57-809/27/23 13:008.7 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/28/23 23:08 7005-72-309/27/23 13:008.7 1.7 1
Chrysene ND ug/L 09/28/23 23:08 218-01-909/27/23 13:008.7 2.4 1
Dibenz(a,h)anthracene ND ug/L 09/28/23 23:08 53-70-309/27/23 13:008.7 2.6 1
Dibenzofuran ND ug/L 09/28/23 23:08 132-64-909/27/23 13:008.7 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/28/23 23:08 91-94-109/27/23 13:0017.4 7.1 1
2,4-Dichlorophenol ND ug/L 09/28/23 23:08 120-83-209/27/23 13:008.7 1.2 1
Diethylphthalate ND ug/L 09/28/23 23:08 84-66-209/27/23 13:008.7 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW02-WS-092023 Lab ID: 92689265009 Collected: 09/20/23 15:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/28/23 23:08 105-67-909/27/23 13:008.7 1.5 1
Dimethylphthalate ND ug/L 09/28/23 23:08 131-11-309/27/23 13:008.7 1.9 1
Di-n-butylphthalate ND ug/L 09/28/23 23:08 84-74-209/27/23 13:008.7 1.9 1
4,6-Dinitro-2-methylphenol ND ug/L 09/28/23 23:08 534-52-109/27/23 13:0017.4 6.8 1
2,4-Dinitrophenol ND ug/L 09/28/23 23:08 51-28-509/27/23 13:0043.5 22.6 1
2,4-Dinitrotoluene ND ug/L 09/28/23 23:08 121-14-209/27/23 13:008.7 1.4 1
2,6-Dinitrotoluene ND ug/L 09/28/23 23:08 606-20-209/27/23 13:008.7 1.5 1
Di-n-octylphthalate ND ug/L 09/28/23 23:08 117-84-009/27/23 13:008.7 3.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/28/23 23:08 117-81-709/27/23 13:005.2 3.2 1
Fluoranthene ND ug/L 09/28/23 23:08 206-44-009/27/23 13:008.7 1.9 1
Fluorene ND ug/L 09/28/23 23:08 86-73-709/27/23 13:008.7 1.8 1
Hexachloro-1,3-butadiene ND ug/L 09/28/23 23:08 87-68-309/27/23 13:008.7 1.5 1
Hexachlorobenzene ND ug/L 09/28/23 23:08 118-74-109/27/23 13:008.7 1.9 1
Hexachlorocyclopentadiene ND ug/L 09/28/23 23:08 77-47-409/27/23 13:008.7 1.4 1
Hexachloroethane ND ug/L 09/28/23 23:08 67-72-109/27/23 13:008.7 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/28/23 23:08 193-39-509/27/23 13:008.7 2.5 1
Isophorone ND ug/L 09/28/23 23:08 78-59-109/27/23 13:008.7 1.4 1
2-Methylnaphthalene ND ug/L 09/28/23 23:08 91-57-609/27/23 13:008.7 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/28/23 23:08 95-48-709/27/23 13:008.7 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/28/23 23:08 15831-10-409/27/23 13:008.7 1.1 1
Naphthalene ND ug/L 09/28/23 23:08 91-20-309/27/23 13:008.7 1.8 1
2-Nitroaniline ND ug/L 09/28/23 23:08 88-74-409/27/23 13:0017.4 2.6 1
3-Nitroaniline ND ug/L 09/28/23 23:08 99-09-209/27/23 13:0017.4 3.3 1
4-Nitroaniline ND ug/L 09/28/23 23:08 100-01-609/27/23 13:0017.4 4.4 1
Nitrobenzene ND ug/L 09/28/23 23:08 98-95-309/27/23 13:008.7 1.6 1
2-Nitrophenol ND ug/L 09/28/23 23:08 88-75-509/27/23 13:008.7 1.2 1
4-Nitrophenol ND ug/L 09/28/23 23:08 100-02-709/27/23 13:0043.5 5.7 1
N-Nitroso-di-n-propylamine ND ug/L 09/28/23 23:08 621-64-709/27/23 13:008.7 1.2 1
N-Nitrosodiphenylamine ND ug/L 09/28/23 23:08 86-30-609/27/23 13:008.7 2.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/28/23 23:08 108-60-109/27/23 13:008.7 1.0 1
Pentachlorophenol ND ug/L 09/28/23 23:08 87-86-509/27/23 13:0017.4 3.3 1
Phenanthrene ND ug/L 09/28/23 23:08 85-01-809/27/23 13:008.7 1.7 1
Phenol ND ug/L 09/28/23 23:08 108-95-209/27/23 13:008.7 1.2 1
Pyrene ND ug/L 09/28/23 23:08 129-00-009/27/23 13:008.7 1.9 1
2,4,5-Trichlorophenol ND ug/L 09/28/23 23:08 95-95-409/27/23 13:008.7 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/28/23 23:08 88-06-209/27/23 13:008.7 1.3 1
Surrogates
Nitrobenzene-d5 (S)125 %09/28/23 23:08 4165-60-009/27/23 13:0010-138 1
2-Fluorobiphenyl (S)120 %09/28/23 23:08 321-60-809/27/23 13:0010-130 1
Terphenyl-d14 (S)133 %09/28/23 23:08 1718-51-009/27/23 13:0019-191 1
Phenol-d6 (S)59 %09/28/23 23:08 13127-88-309/27/23 13:0010-130 1
2-Fluorophenol (S)85 %09/28/23 23:08 367-12-409/27/23 13:0010-130 1
2,4,6-Tribromophenol (S)145 %09/28/23 23:08 118-79-609/27/23 13:0010-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW02-WS-092023 Lab ID: 92689265009 Collected: 09/20/23 15:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 04:11 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 04:11 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 04:11 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 04:11 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 04:11 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 04:11 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 04:11 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/30/23 04:11 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 04:11 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 04:11 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 04:11 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 04:11 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 04:11 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 04:11 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 04:11 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 04:11 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 04:11 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 04:11 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 04:11 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 04:11 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 04:11 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 04:11 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 04:11 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 04:11 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 04:11 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 04:11 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 04:11 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 04:11 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 04:11 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 04:11 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 04:11 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 04:11 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 04:11 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 04:11 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 04:11 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 04:11 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 04:11 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 04:11 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 04:11 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 04:11 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 04:11 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 04:11 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 04:11 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 04:11 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 04:11 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SW02-WS-092023 Lab ID: 92689265009 Collected: 09/20/23 15:50 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 04:11 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 04:11 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 04:11 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 04:11 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %09/30/23 04:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/30/23 04:11 17060-07-070-130 1
Toluene-d8 (S)101 %09/30/23 04:11 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 10.9 mg/L 10/03/23 17:265.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids ND mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 1.2 mg/L 09/22/23 20:04 16887-00-61.0 0.60 1
Sulfate 1.5 mg/L 09/22/23 20:04 14808-79-81.0 0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 10/10/23 02:26 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 10/10/23 04:28 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable ND mg/L 09/27/23 15:39 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 09/22/23 04:370.050 0.012 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand ND mg/L 10/06/23 00:1910/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWUP-WS-092023 Lab ID: 92689265010 Collected: 09/20/23 17:00 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.6 Std. Units 09/26/23 13:01 H31
True Color 5.0 units 09/26/23 13:01 H35.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Aluminum 84.5J ug/L 10/05/23 10:19 7429-90-510/03/23 23:49100 30.7 1
Arsenic ND ug/L 10/05/23 10:19 7440-38-210/03/23 23:4910.0 3.4 1
Barium 14.4 ug/L 10/05/23 10:19 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium ND ug/L 10/05/23 10:19 7440-41-710/03/23 23:494.0 0.17 1
Boron ND ug/L 10/05/23 10:19 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium ND ug/L 10/05/23 10:19 7440-43-910/03/23 23:491.0 0.33 1
Calcium 2400 ug/L 10/05/23 10:19 7440-70-210/03/23 23:49500 190 1
Chromium ND ug/L 10/05/23 10:19 7440-47-310/03/23 23:495.0 1.7 1
Cobalt ND ug/L 10/05/23 10:19 7440-48-410/03/23 23:4910.0 0.96 1
Copper ND ug/L 10/05/23 10:19 7440-50-810/03/23 23:495.0 2.6 1
Iron 292 ug/L 10/05/23 10:19 7439-89-610/03/23 23:4940.0 25.0 1
Lead ND ug/L 10/05/23 10:19 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium 766 ug/L 10/05/23 10:19 7439-95-410/03/23 23:49500 84.0 1
Manganese 18.1 ug/L 10/05/23 10:19 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum ND ug/L 10/05/23 10:19 7439-98-710/03/23 23:4910.0 1.6 1
Nickel ND ug/L 10/05/23 10:19 7440-02-010/03/23 23:495.0 1.0 1
Selenium ND ug/L 10/05/23 10:19 7782-49-210/03/23 23:4915.0 3.9 1
Silver ND ug/L 10/05/23 10:19 7440-22-410/03/23 23:495.0 1.0 1
Sodium 2140 ug/L 10/05/23 10:19 7440-23-510/03/23 23:492000 540 1
Thallium ND ug/L 10/05/23 10:19 7440-28-010/03/23 23:4915.0 2.9 1
Zinc ND ug/L 10/05/23 10:19 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 10/06/23 14:43 7429-90-510/03/23 23:49100 30.7 1
Arsenic, Dissolved ND ug/L 10/06/23 14:43 7440-38-210/03/23 23:4910.0 3.4 1
Barium, Dissolved 15.0 ug/L 10/06/23 14:43 7440-39-310/03/23 23:4910.0 0.84 1
Beryllium, Dissolved ND ug/L 10/06/23 14:43 7440-41-710/03/23 23:494.0 0.17 1
Boron, Dissolved ND ug/L 10/06/23 14:43 7440-42-810/03/23 23:4950.0 12.4 1
Cadmium, Dissolved ND ug/L 10/06/23 14:43 7440-43-910/03/23 23:491.0 0.33 1
Calcium, Dissolved 2380 ug/L 10/06/23 14:43 7440-70-210/03/23 23:49500 190 1
Chromium, Dissolved ND ug/L 10/06/23 14:43 7440-47-310/03/23 23:495.0 1.7 1
Cobalt, Dissolved ND ug/L 10/06/23 14:43 7440-48-410/03/23 23:4910.0 0.96 1
Copper, Dissolved ND ug/L 10/06/23 14:43 7440-50-810/03/23 23:495.0 2.6 1
Iron, Dissolved 136 ug/L 10/06/23 14:43 7439-89-610/03/23 23:4940.0 25.0 1
Lead, Dissolved ND ug/L 10/06/23 14:43 7439-92-110/03/23 23:4910.0 2.1 1
Magnesium, Dissolved 793 ug/L 10/06/23 14:43 7439-95-410/03/23 23:49500 84.0 1
Manganese, Dissolved 15.9 ug/L 10/06/23 14:43 7439-96-510/03/23 23:495.0 1.1 1
Molybdenum, Dissolved ND ug/L 10/06/23 14:43 7439-98-710/03/23 23:4910.0 1.6 1
Nickel, Dissolved ND ug/L 10/06/23 14:43 7440-02-010/03/23 23:495.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWUP-WS-092023 Lab ID: 92689265010 Collected: 09/20/23 17:00 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Selenium, Dissolved ND ug/L 10/06/23 14:43 7782-49-210/03/23 23:4915.0 3.9 1
Silver, Dissolved ND ug/L 10/06/23 14:43 7440-22-410/03/23 23:495.0 1.0 1
Sodium, Dissolved 2020 ug/L 10/06/23 14:43 7440-23-510/03/23 23:492000 540 1
Thallium, Dissolved ND ug/L 10/06/23 14:43 7440-28-010/03/23 23:4915.0 2.9 1
Zinc, Dissolved ND ug/L 10/06/23 14:43 7440-66-610/03/23 23:4920.0 11.0 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/09/23 16:08 7439-97-610/05/23 11:560.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/10/23 13:19 7439-97-610/10/23 09:510.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 09/25/23 20:44 83-32-909/25/23 12:318.3 1.7 1
Acenaphthylene ND ug/L 09/25/23 20:44 208-96-809/25/23 12:318.3 1.6 1
Acetophenone ND ug/L 09/25/23 20:44 98-86-209/25/23 12:318.3 1.2 1
Anthracene ND ug/L 09/25/23 20:44 120-12-709/25/23 12:318.3 1.9 1
Atrazine ND ug/L 09/25/23 20:44 1912-24-909/25/23 12:318.3 2.6 1
Benzaldehyde ND ug/L 09/25/23 20:44 100-52-709/25/23 12:318.3 3.0 1
Benzo(a)anthracene ND ug/L 09/25/23 20:44 56-55-3 R109/25/23 12:318.3 2.2 1
Benzo(a)pyrene ND ug/L 09/25/23 20:44 50-32-809/25/23 12:318.3 2.3 1
Benzo(b)fluoranthene ND ug/L 09/25/23 20:44 205-99-209/25/23 12:318.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 09/25/23 20:44 191-24-209/25/23 12:318.3 2.4 1
Benzo(k)fluoranthene ND ug/L 09/25/23 20:44 207-08-9 R109/25/23 12:318.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 09/25/23 20:44 92-52-409/25/23 12:318.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 09/25/23 20:44 101-55-309/25/23 12:318.3 1.5 1
Butylbenzylphthalate ND ug/L 09/25/23 20:44 85-68-709/25/23 12:318.3 2.6 1
Caprolactam ND ug/L 09/25/23 20:44 105-60-209/25/23 12:318.3 5.8 1
Carbazole ND ug/L 09/25/23 20:44 86-74-809/25/23 12:318.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 09/25/23 20:44 59-50-709/25/23 12:318.3 2.8 1
4-Chloroaniline ND ug/L 09/25/23 20:44 106-47-8 M109/25/23 12:3116.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/25/23 20:44 111-91-109/25/23 12:318.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 09/25/23 20:44 111-44-409/25/23 12:318.3 1.6 1
2-Chloronaphthalene ND ug/L 09/25/23 20:44 91-58-709/25/23 12:318.3 1.4 1
2-Chlorophenol ND ug/L 09/25/23 20:44 95-57-809/25/23 12:318.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 09/25/23 20:44 7005-72-309/25/23 12:318.3 1.7 1
Chrysene ND ug/L 09/25/23 20:44 218-01-909/25/23 12:318.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 09/25/23 20:44 53-70-309/25/23 12:318.3 2.5 1
Dibenzofuran ND ug/L 09/25/23 20:44 132-64-909/25/23 12:318.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/25/23 20:44 91-94-1 R109/25/23 12:3116.7 6.8 1
2,4-Dichlorophenol ND ug/L 09/25/23 20:44 120-83-209/25/23 12:318.3 1.2 1
Diethylphthalate ND ug/L 09/25/23 20:44 84-66-209/25/23 12:318.3 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWUP-WS-092023 Lab ID: 92689265010 Collected: 09/20/23 17:00 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2,4-Dimethylphenol ND ug/L 09/25/23 20:44 105-67-909/25/23 12:318.3 1.4 1
Dimethylphthalate ND ug/L 09/25/23 20:44 131-11-309/25/23 12:318.3 1.8 1
Di-n-butylphthalate ND ug/L 09/25/23 20:44 84-74-209/25/23 12:318.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/25/23 20:44 534-52-1 R109/25/23 12:3116.7 6.5 1
2,4-Dinitrophenol ND ug/L 09/25/23 20:44 51-28-5 M109/25/23 12:3141.7 21.7 1
2,4-Dinitrotoluene ND ug/L 09/25/23 20:44 121-14-209/25/23 12:318.3 1.4 1
2,6-Dinitrotoluene ND ug/L 09/25/23 20:44 606-20-209/25/23 12:318.3 1.4 1
Di-n-octylphthalate ND ug/L 09/25/23 20:44 117-84-009/25/23 12:318.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/25/23 20:44 117-81-709/25/23 12:315.0 3.1 1
Fluoranthene ND ug/L 09/25/23 20:44 206-44-009/25/23 12:318.3 1.8 1
Fluorene ND ug/L 09/25/23 20:44 86-73-709/25/23 12:318.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 09/25/23 20:44 87-68-3 R109/25/23 12:318.3 1.5 1
Hexachlorobenzene ND ug/L 09/25/23 20:44 118-74-109/25/23 12:318.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 09/25/23 20:44 77-47-409/25/23 12:318.3 1.3 1
Hexachloroethane ND ug/L 09/25/23 20:44 67-72-109/25/23 12:318.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/25/23 20:44 193-39-509/25/23 12:318.3 2.4 1
Isophorone ND ug/L 09/25/23 20:44 78-59-109/25/23 12:318.3 1.4 1
2-Methylnaphthalene ND ug/L 09/25/23 20:44 91-57-609/25/23 12:318.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/25/23 20:44 95-48-709/25/23 12:318.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/25/23 20:44 15831-10-409/25/23 12:318.3 1.0 1
Naphthalene ND ug/L 09/25/23 20:44 91-20-309/25/23 12:318.3 1.7 1
2-Nitroaniline ND ug/L 09/25/23 20:44 88-74-409/25/23 12:3116.7 2.5 1
3-Nitroaniline ND ug/L 09/25/23 20:44 99-09-209/25/23 12:3116.7 3.1 1
4-Nitroaniline ND ug/L 09/25/23 20:44 100-01-609/25/23 12:3116.7 4.2 1
Nitrobenzene ND ug/L 09/25/23 20:44 98-95-309/25/23 12:318.3 1.6 1
2-Nitrophenol ND ug/L 09/25/23 20:44 88-75-509/25/23 12:318.3 1.2 1
4-Nitrophenol ND ug/L 09/25/23 20:44 100-02-709/25/23 12:3141.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 09/25/23 20:44 621-64-709/25/23 12:318.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 09/25/23 20:44 86-30-609/25/23 12:318.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/25/23 20:44 108-60-109/25/23 12:318.3 0.96 1
Pentachlorophenol ND ug/L 09/25/23 20:44 87-86-509/25/23 12:3116.7 3.1 1
Phenanthrene ND ug/L 09/25/23 20:44 85-01-809/25/23 12:318.3 1.7 1
Phenol ND ug/L 09/25/23 20:44 108-95-209/25/23 12:318.3 1.1 1
Pyrene ND ug/L 09/25/23 20:44 129-00-009/25/23 12:318.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 09/25/23 20:44 95-95-409/25/23 12:318.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 09/25/23 20:44 88-06-209/25/23 12:318.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)57 %09/25/23 20:44 4165-60-009/25/23 12:3110-138 1
2-Fluorobiphenyl (S)55 %09/25/23 20:44 321-60-809/25/23 12:3110-130 1
Terphenyl-d14 (S)131 %09/25/23 20:44 1718-51-009/25/23 12:3119-191 1
Phenol-d6 (S)15 %09/25/23 20:44 13127-88-309/25/23 12:3110-130 1
2-Fluorophenol (S)6 %09/25/23 20:44 367-12-4 S009/25/23 12:3110-130 1
2,4,6-Tribromophenol (S)31 %09/25/23 20:44 118-79-609/25/23 12:3110-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWUP-WS-092023 Lab ID: 92689265010 Collected: 09/20/23 17:00 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/30/23 04:29 67-64-125.0 5.1 1
Benzene ND ug/L 09/30/23 04:29 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 09/30/23 04:29 75-27-41.0 0.31 1
Bromoform ND ug/L 09/30/23 04:29 75-25-21.0 0.34 1
Bromomethane ND ug/L 09/30/23 04:29 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 09/30/23 04:29 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 09/30/23 04:29 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 09/30/23 04:29 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 09/30/23 04:29 108-90-71.0 0.28 1
Chloroethane ND ug/L 09/30/23 04:29 75-00-31.0 0.65 1
Chloroform ND ug/L 09/30/23 04:29 67-66-31.0 0.43 1
Chloromethane ND ug/L 09/30/23 04:29 74-87-31.0 0.54 1
Cyclohexane ND ug/L 09/30/23 04:29 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 09/30/23 04:29 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 09/30/23 04:29 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 09/30/23 04:29 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 09/30/23 04:29 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 09/30/23 04:29 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 09/30/23 04:29 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/30/23 04:29 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 09/30/23 04:29 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 09/30/23 04:29 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 09/30/23 04:29 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 09/30/23 04:29 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 09/30/23 04:29 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 09/30/23 04:29 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 09/30/23 04:29 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 09/30/23 04:29 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 09/30/23 04:29 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/30/23 04:29 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 09/30/23 04:29 98-82-81.0 0.33 1
Methyl acetate ND ug/L 09/30/23 04:29 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 09/30/23 04:29 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 09/30/23 04:29 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/30/23 04:29 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 09/30/23 04:29 1634-04-41.0 0.42 1
Styrene ND ug/L 09/30/23 04:29 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 09/30/23 04:29 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 09/30/23 04:29 127-18-41.0 0.29 1
Toluene ND ug/L 09/30/23 04:29 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 09/30/23 04:29 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 09/30/23 04:29 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 09/30/23 04:29 79-00-51.0 0.32 1
Trichloroethene ND ug/L 09/30/23 04:29 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 09/30/23 04:29 75-69-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 120
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Sample: SWUP-WS-092023 Lab ID: 92689265010 Collected: 09/20/23 17:00 Received: 09/21/23 08:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2-Trichlorotrifluoroethane ND ug/L 09/30/23 04:29 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 09/30/23 04:29 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 09/30/23 04:29 179601-23-12.0 0.71 1
o-Xylene ND ug/L 09/30/23 04:29 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %09/30/23 04:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/30/23 04:29 17060-07-070-130 1
Toluene-d8 (S)100 %09/30/23 04:29 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 10.1 mg/L 10/03/23 14:005.0 5.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids ND mg/L 09/23/23 11:3725.0 25.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Chloride 1.2 mg/L 09/22/23 20:18 16887-00-61.0 0.60 1
Sulfate 1.4 mg/L 09/22/23 20:18 14808-79-81.0 0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 10/10/23 02:30 7664-41-70.10 0.031 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 10/10/23 04:31 7727-37-910/09/23 19:440.50 0.25 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable ND mg/L 09/27/23 15:39 64743-03-909/27/23 12:180.020 0.0076 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
SM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 09/22/23 04:37 M10.050 0.012 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
5220D COD
Chemical Oxygen Demand ND mg/L 10/06/23 00:1910/05/23 01:5225.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802098
SM 2120B-2011
SM 2120B-2011
2120B True Color EDEN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4154835
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
True Color units ND 5.0 09/26/23 12:485.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4154836LABORATORY CONTROL SAMPLE:
LCSSpike
True Color units 35.035 100 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689265010
4154837SAMPLE DUPLICATE:
pH Std. Units 6.6 H30106.6
True Color units 5.0 H30105.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
955302
EPA 245.1
EPA 245.1
245.1 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5252820
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/09/23 15:110.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5252821LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.02 102 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5252822MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
20290568008
5252823
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 92 70-13088 4 202ND1.9 1.8
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5252824MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
5252825
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 100 70-13095 5 202ND2.0 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
956743
EPA 245.1
EPA 245.1
245.1 Mercury - Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5261123
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/10/23 12:490.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5261124LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 1.82 92 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5261125MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
5261126
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2 95 70-13094 2 202ND1.9 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954588
EPA 200.7
EPA 200.7
200.7 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5249407
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009
Matrix: Water
AnalyzedMDL
Aluminum ug/L ND 100 10/04/23 00:1530.7
Arsenic ug/L ND 10.0 10/04/23 00:153.4
Barium ug/L ND 10.0 10/04/23 00:150.84
Beryllium ug/L ND 4.0 10/04/23 00:150.17
Boron ug/L ND 50.0 10/04/23 00:1512.4
Cadmium ug/L ND 1.0 10/04/23 00:150.33
Calcium ug/L ND 500 10/04/23 00:15190
Chromium ug/L ND 5.0 10/04/23 00:151.7
Cobalt ug/L ND 10.0 10/04/23 00:150.96
Copper ug/L ND 5.0 10/04/23 00:152.6
Iron ug/L ND 40.0 10/04/23 00:1525.0
Lead ug/L ND 10.0 10/04/23 00:152.1
Magnesium ug/L ND 500 10/04/23 00:1584.0
Manganese ug/L ND 5.0 10/04/23 00:151.1
Molybdenum ug/L ND 10.0 10/04/23 00:151.6
Nickel ug/L ND 5.0 10/04/23 00:151.0
Selenium ug/L ND 15.0 10/04/23 00:153.9
Silver ug/L ND 5.0 10/04/23 00:151.0
Sodium ug/L ND 2000 10/04/23 00:15540
Thallium ug/L ND 15.0 10/04/23 00:152.9
Zinc ug/L ND 20.0 10/04/23 00:1511.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5249408LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum ug/L 24002500 96 85-115
Arsenic ug/L 241250 97 85-115
Barium ug/L 243250 97 85-115
Beryllium ug/L 24.225 97 85-115
Boron ug/L 12101250 97 85-115
Cadmium ug/L 26.225 105 85-115
Calcium ug/L 1260012500 101 85-115
Chromium ug/L 246250 98 85-115
Cobalt ug/L 250250 100 85-115
Copper ug/L 234250 94 85-115
Iron ug/L 24402500 98 85-115
Lead ug/L 254250 102 85-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5249408LABORATORY CONTROL SAMPLE:
LCSSpike
Magnesium ug/L 1230012500 99 85-115
Manganese ug/L 244250 97 85-115
Molybdenum ug/L 241250 96 85-115
Nickel ug/L 257250 103 85-115
Selenium ug/L 253250 101 85-115
Silver ug/L 24.325 97 85-115
Sodium ug/L 1190012500 95 85-115
Thallium ug/L 253250 101 85-115
Zinc ug/L 13101250 105 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5249409MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35831106007
5249410
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 2500 108 70-130108 0 20250065.2J 2750 2760
Arsenic ug/L 250 101 70-130103 2 202503.4U 255 261
Barium ug/L 250 100 70-130100 0 2025016.4 267 267
Beryllium ug/L 25 103 70-130103 0 20250.22J 26.0 26.1
Boron ug/L 1250 100 70-130101 0 20125013502600 2610
Cadmium ug/L 25 97 70-13097 0 20250.70J 25.0 25.0
Calcium ug/L 12500 92 70-13094 0 2012500158000170000 170000
Chromium ug/L 250 97 70-13097 0 202501.7U 244 244
Cobalt ug/L 250 98 70-13098 0 202501.5J 247 247
Copper ug/L 250 108 70-130109 0 202504.3J 276 277
Iron ug/L 2500 96 70-13096 0 2025003362720 2730
Lead ug/L 250 93 70-13094 0 202502.1U 234 234
Magnesium ug/L E125009670-130117 1 2012500367000379000 381000
Manganese ug/L 250 96 70-13096 0 202508.3 248 249
Molybdenum ug/L 250 97 70-13097 0 202505.1J 248 249
Nickel ug/L 250 99 70-13099 0 202501.0U 247 248
Selenium ug/L 250 97 70-13099 2 202503.9U 241 247
Silver ug/L 25 108 70-130109 0 20252.8J 29.8 29.9
Sodium ug/L E12500-187 70-130-178 0 201250019700001940000 1940000
Thallium ug/L 250 89 70-13089 0 202502.9U 222 221
Zinc ug/L 1250 97 70-13097 0 20125017.0J 1230 1230
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5249411MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35831106008
5249412
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 2500 101 70-130102 0 20250030.7U 2550 2560
Arsenic ug/L 250 102 70-130105 3 202503.4U 255 262
Barium ug/L 250 98 70-13099 0 2025017.8 264 265
Beryllium ug/L 25 100 70-130100 0 20250.17U 25.1 25.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5249411MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35831106008
5249412
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Boron ug/L 1250 100 70-130100 0 2012506151860 1870
Cadmium ug/L 25 98 70-130100 2 20250.65J 25.2 25.6
Calcium ug/L 12500 92 70-130101 1 2012500103000115000 116000
Chromium ug/L 250 98 70-13098 0 202501.7U 244 245
Cobalt ug/L 250 99 70-13099 0 202501.7J 250 250
Copper ug/L 250 104 70-130104 0 202504.0J 263 263
Iron ug/L 2500 96 70-13096 0 2025002942680 2690
Lead ug/L 250 95 70-13095 0 202502.1U 237 239
Magnesium ug/L E125009070-13098 1 2012500154000165000 166000
Manganese ug/L 250 96 70-13096 0 2025068.4 308 309
Molybdenum ug/L 250 98 70-13099 1 202506.1J 252 253
Nickel ug/L 250 100 70-130101 1 202501.6J 252 253
Selenium ug/L 250 99 70-13098 1 202503.9U 247 246
Silver ug/L 25 103 70-130103 0 20251.8J 27.5 27.5
Sodium ug/L E125003770-13075 0 201250010200001020000 1020000
Thallium ug/L 250 90 70-13092 2 202502.9U 225 229
Zinc ug/L 1250 100 70-130100 0 20125011.0U 1260 1260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954932
EPA 200.7
EPA 200.7
200.7 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5251002
Associated Lab Samples:92689265010
Matrix: Water
AnalyzedMDL
Aluminum ug/L ND 100 10/05/23 10:0130.7
Arsenic ug/L ND 10.0 10/05/23 10:013.4
Barium ug/L ND 10.0 10/05/23 10:010.84
Beryllium ug/L ND 4.0 10/05/23 10:010.17
Boron ug/L ND 50.0 10/05/23 10:0112.4
Cadmium ug/L ND 1.0 10/05/23 10:010.33
Calcium ug/L ND 500 10/05/23 10:01190
Chromium ug/L ND 5.0 10/05/23 10:011.7
Cobalt ug/L ND 10.0 10/05/23 10:010.96
Copper ug/L ND 5.0 10/05/23 10:012.6
Iron ug/L ND 40.0 10/05/23 10:0125.0
Lead ug/L ND 10.0 10/05/23 10:012.1
Magnesium ug/L ND 500 10/05/23 10:0184.0
Manganese ug/L ND 5.0 10/05/23 10:011.1
Molybdenum ug/L ND 10.0 10/05/23 10:011.6
Nickel ug/L ND 5.0 10/05/23 10:011.0
Selenium ug/L ND 15.0 10/05/23 10:013.9
Silver ug/L ND 5.0 10/05/23 10:011.0
Sodium ug/L ND 2000 10/05/23 10:01540
Thallium ug/L ND 15.0 10/05/23 10:012.9
Zinc ug/L ND 20.0 10/05/23 10:0111.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5251003LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum ug/L 25502500 102 85-115
Arsenic ug/L 244250 98 85-115
Barium ug/L 258250 103 85-115
Beryllium ug/L 24.825 99 85-115
Boron ug/L 12501250 100 85-115
Cadmium ug/L 25.825 103 85-115
Calcium ug/L 1300012500 104 85-115
Chromium ug/L 256250 102 85-115
Cobalt ug/L 257250 103 85-115
Copper ug/L 251250 101 85-115
Iron ug/L 25502500 102 85-115
Lead ug/L 258250 103 85-115
Magnesium ug/L 1310012500 105 85-115
Manganese ug/L 255250 102 85-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5251003LABORATORY CONTROL SAMPLE:
LCSSpike
Molybdenum ug/L 250250 100 85-115
Nickel ug/L 260250 104 85-115
Selenium ug/L 253250 101 85-115
Silver ug/L 25.525 102 85-115
Sodium ug/L 1240012500 99 85-115
Thallium ug/L 262250 105 85-115
Zinc ug/L 12701250 102 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5251004MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35830943001
5251005
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 2500 119 70-130119 0 20250061.4U 3010 3020
Arsenic ug/L 250 107 70-130107 0 202503.4U 270 269
Barium ug/L 250 106 70-130106 0 2025028.1 292 292
Beryllium ug/L 25 110 70-130110 0 20250.34U 27.4 27.6
Boron ug/L 1250 104 70-130107 1 20125024403730 3770
Cadmium ug/L 25 96 70-13098 2 20250.66U 24.0 24.5
Calcium ug/L M112500-201 70-130-198 0 2012500273000248000 248000
Chromium ug/L 250 100 70-130100 0 202501.7U 251 251
Cobalt ug/L 250 98 70-13099 0 202501.9U 246 247
Copper ug/L 250 118 70-130118 0 202502.6U 297 296
Iron ug/L 2500 98 70-13099 1 20250090.2 2550 2560
Lead ug/L 250 90 70-13091 1 202504.2U 225 227
Magnesium ug/L E,M112500-252 70-130-236 0 2012500729000697000 699000
Manganese ug/L 250 98 70-13098 0 2025062.4 307 308
Molybdenum ug/L 250 100 70-130100 1 202503.8J 253 254
Nickel ug/L 250 97 70-13097 1 202501.0U 242 244
Selenium ug/L 250 99 70-13098 1 202507.8U 249 247
Silver ug/L M12513470-130134 0 20252.0U 33.6 33.5
Sodium ug/L M112500-4670 70-130-5130 1 201250061800005600000 5540000
Thallium ug/L 250 87 70-13086 0 20250290U216 216
Zinc ug/L 1250 93 70-13094 1 20125022.0U 1170 1180
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5251006MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
5251007
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 2500 101 70-130102 1 20250084.5J 2620 2640
Arsenic ug/L 250 97 70-13098 0 20250ND245 246
Barium ug/L 250 101 70-130103 1 2025014.4 268 271
Beryllium ug/L 25 99 70-130100 1 2025ND24.9 25.1
Boron ug/L 1250 100 70-130101 1 201250ND1260 1270
Cadmium ug/L 25 105 70-130105 1 2025ND26.3 26.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5251006MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
5251007
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Calcium ug/L 12500 103 70-130105 1 2012500240015300 15500
Chromium ug/L 250 102 70-130103 1 20250ND256 258
Cobalt ug/L 250 103 70-130104 1 20250ND258 260
Copper ug/L 250 98 70-13099 1 20250ND247 249
Iron ug/L 2500 101 70-130102 1 2025002922820 2850
Lead ug/L 250 104 70-130105 1 20250ND260 263
Magnesium ug/L 12500 103 70-130104 1 201250076613600 13800
Manganese ug/L 250 101 70-130102 1 2025018.1 271 273
Molybdenum ug/L 250 100 70-130100 1 20250ND249 251
Nickel ug/L 250 105 70-130106 1 20250ND263 265
Selenium ug/L 250 102 70-130102 1 20250ND255 256
Silver ug/L 25 102 70-130103 1 2025ND25.4 25.7
Sodium ug/L 12500 97 70-13098 1 2012500214014300 14400
Thallium ug/L 250 105 70-130105 0 20250ND262 263
Zinc ug/L 1250 104 70-130105 1 201250ND1300 1310
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
954936
EPA 200.7
EPA 200.7
200.7 MET Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5251016
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Aluminum, Dissolved ug/L ND 100 10/06/23 13:1430.7
Arsenic, Dissolved ug/L ND 10.0 10/06/23 13:143.4
Barium, Dissolved ug/L ND 10.0 10/06/23 13:140.84
Beryllium, Dissolved ug/L ND 4.0 10/06/23 13:140.17
Boron, Dissolved ug/L ND 50.0 10/06/23 13:1412.4
Cadmium, Dissolved ug/L ND 1.0 10/06/23 13:140.33
Calcium, Dissolved ug/L ND 500 10/06/23 13:14190
Chromium, Dissolved ug/L ND 5.0 10/06/23 13:141.7
Cobalt, Dissolved ug/L ND 10.0 10/06/23 13:140.96
Copper, Dissolved ug/L ND 5.0 10/06/23 13:142.6
Iron, Dissolved ug/L ND 40.0 10/06/23 13:1425.0
Lead, Dissolved ug/L ND 10.0 10/06/23 13:142.1
Magnesium, Dissolved ug/L ND 500 10/06/23 13:1484.0
Manganese, Dissolved ug/L ND 5.0 10/06/23 13:141.1
Molybdenum, Dissolved ug/L ND 10.0 10/06/23 13:141.6
Nickel, Dissolved ug/L ND 5.0 10/06/23 13:141.0
Selenium, Dissolved ug/L ND 15.0 10/06/23 13:143.9
Silver, Dissolved ug/L ND 5.0 10/06/23 13:141.0
Sodium, Dissolved ug/L ND 2000 10/06/23 13:14540
Thallium, Dissolved ug/L ND 15.0 10/06/23 13:142.9
Zinc, Dissolved ug/L ND 20.0 10/06/23 13:1411.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5251017LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum, Dissolved ug/L 26302500 105 85-115
Arsenic, Dissolved ug/L 245250 98 85-115
Barium, Dissolved ug/L 272250 109 85-115
Beryllium, Dissolved ug/L 26.525 106 85-115
Boron, Dissolved ug/L 13301250 106 85-115
Cadmium, Dissolved ug/L 25.925 104 85-115
Calcium, Dissolved ug/L 1300012500 104 85-115
Chromium, Dissolved ug/L 264250 106 85-115
Cobalt, Dissolved ug/L 260250 104 85-115
Copper, Dissolved ug/L 265250 106 85-115
Iron, Dissolved ug/L 25702500 103 85-115
Lead, Dissolved ug/L 270250 108 85-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5251017LABORATORY CONTROL SAMPLE:
LCSSpike
Magnesium, Dissolved ug/L 1350012500 108 85-115
Manganese, Dissolved ug/L 264250 106 85-115
Molybdenum, Dissolved ug/L 250250 100 85-115
Nickel, Dissolved ug/L 270250 108 85-115
Selenium, Dissolved ug/L 257250 103 85-115
Silver, Dissolved ug/L 25.825 103 85-115
Sodium, Dissolved ug/L 1360012500 108 85-115
Thallium, Dissolved ug/L 246250 98 85-115
Zinc, Dissolved ug/L 13001250 104 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5251018MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35830349001
5251019
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum, Dissolved ug/L 2500 115 70-130122 6 202500154U2990 3160
Arsenic, Dissolved ug/L 250 105 70-130114 8 2025017.0U 263 286
Barium, Dissolved ug/L 250 107 70-130113 5 2025025.1J 293 309
Beryllium, Dissolved ug/L 25 105 70-130113 8 20250.17U 26.3 28.3
Boron, Dissolved ug/L 1250 98 70-130119 7 20125026203840 4110
Cadmium, Dissolved ug/L 25 99 70-130106 6 20250.33U 24.8 26.4
Calcium, Dissolved ug/L M1125009870-130166 4 2012500178000191000 199000
Chromium, Dissolved ug/L 250 105 70-130109 4 202508.5U 263 273
Cobalt, Dissolved ug/L 250 99 70-130105 6 202500.96U 249 263
Copper, Dissolved ug/L 250 107 70-130113 6 202502.6U 268 284
Iron, Dissolved ug/L 2500 85 70-13086 1 2025001902320 2350
Lead, Dissolved ug/L 250 99 70-130104 5 202502.1U 248 261
Magnesium, Dissolved ug/L E,M112500-154 70-130-286 2 2012500917000897000 881000
Manganese, Dissolved ug/L 250 106 70-130113 5 2025067.0 332 348
Molybdenum, Dissolved ug/L 250 101 70-130107 6 202508.0U 253 269
Nickel, Dissolved ug/L 250 102 70-130108 6 202501.0U 255 271
Selenium, Dissolved ug/L 250 106 70-130111 5 202503.9U 266 279
Silver, Dissolved ug/L 25 105 70-130104 1 20251.0U 26.4 26.2
Sodium, Dissolved ug/L E,M112500-106 70-130-391 4 2012500917000903000 868000
Thallium, Dissolved ug/L 250 88 70-13094 6 202502.9U 221 234
Zinc, Dissolved ug/L 1250 102 70-130108 6 20125011.0U 1290 1360
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5251020MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
5251021
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum, Dissolved ug/L 2500 104 70-130105 1 202500ND2610 2630
Arsenic, Dissolved ug/L 250 98 70-13096 2 20250ND245 240
Barium, Dissolved ug/L 250 108 70-130108 0 2025015.0 284 285
Beryllium, Dissolved ug/L 25 107 70-130106 2 2025ND26.8 26.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5251020MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
5251021
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Boron, Dissolved ug/L 1250 104 70-130105 1 201250ND1310 1310
Cadmium, Dissolved ug/L 25 105 70-130103 2 2025ND26.3 25.8
Calcium, Dissolved ug/L 12500 105 70-130101 3 2012500238015500 15000
Chromium, Dissolved ug/L 250 105 70-130105 0 20250ND263 263
Cobalt, Dissolved ug/L 250 106 70-130103 2 20250ND264 258
Copper, Dissolved ug/L 250 105 70-130106 0 20250ND263 264
Iron, Dissolved ug/L 2500 103 70-130101 2 2025001362710 2650
Lead, Dissolved ug/L 250 110 70-130107 2 20250ND274 269
Magnesium, Dissolved ug/L 12500 106 70-130104 2 201250079314100 13800
Manganese, Dissolved ug/L 250 105 70-130105 1 2025015.9 277 279
Molybdenum, Dissolved ug/L 250 102 70-130100 2 20250ND255 250
Nickel, Dissolved ug/L 250 110 70-130108 2 20250ND275 271
Selenium, Dissolved ug/L 250 102 70-130100 2 20250ND254 250
Silver, Dissolved ug/L 25 102 70-130103 1 2025ND25.5 25.8
Sodium, Dissolved ug/L 12500 106 70-130105 1 2012500202015300 15200
Thallium, Dissolved ug/L 250 100 70-13098 2 20250ND250 244
Zinc, Dissolved ug/L 1250 105 70-130103 2 201250ND1320 1290
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802723
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689265005, 92689265006, 92689265007, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4157732
Associated Lab Samples:92689265005, 92689265006, 92689265007, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/29/23 21:050.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/29/23 21:050.22
1,1,2-Trichloroethane ug/L ND 1.0 09/29/23 21:050.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/29/23 21:050.32
1,1-Dichloroethane ug/L ND 1.0 09/29/23 21:050.37
1,1-Dichloroethene ug/L ND 1.0 09/29/23 21:050.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/29/23 21:050.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/29/23 21:050.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/29/23 21:050.27
1,2-Dichlorobenzene ug/L ND 1.0 09/29/23 21:050.34
1,2-Dichloroethane ug/L ND 1.0 09/29/23 21:050.32
1,2-Dichloropropane ug/L ND 1.0 09/29/23 21:050.36
1,3-Dichlorobenzene ug/L ND 1.0 09/29/23 21:050.34
1,4-Dichlorobenzene ug/L ND 1.0 09/29/23 21:050.33
2-Butanone (MEK)ug/L ND 5.0 09/29/23 21:054.0
2-Hexanone ug/L ND 5.0 09/29/23 21:050.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/29/23 21:052.7
Acetone ug/L ND 25.0 09/29/23 21:055.1
Benzene ug/L ND 1.0 09/29/23 21:050.34
Bromodichloromethane ug/L ND 1.0 09/29/23 21:050.31
Bromoform ug/L ND 1.0 09/29/23 21:050.34
Bromomethane ug/L ND 2.0 v209/29/23 21:051.7
Carbon disulfide ug/L ND 2.0 09/29/23 21:050.36
Carbon tetrachloride ug/L ND 1.0 09/29/23 21:050.33
Chlorobenzene ug/L ND 1.0 09/29/23 21:050.28
Chloroethane ug/L ND 1.0 09/29/23 21:050.65
Chloroform ug/L ND 1.0 09/29/23 21:050.43
Chloromethane ug/L ND 1.0 09/29/23 21:050.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/29/23 21:050.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/29/23 21:050.36
Cyclohexane ug/L ND 1.0 09/29/23 21:050.35
Dibromochloromethane ug/L ND 1.0 09/29/23 21:050.36
Dichlorodifluoromethane ug/L ND 1.0 09/29/23 21:050.35
Ethylbenzene ug/L ND 1.0 09/29/23 21:050.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/29/23 21:050.33
m&p-Xylene ug/L ND 2.0 09/29/23 21:050.71
Methyl acetate ug/L ND 10.0 09/29/23 21:052.4
Methyl-tert-butyl ether ug/L ND 1.0 09/29/23 21:050.42
Methylcyclohexane ug/L ND 10.0 09/29/23 21:051.5
Methylene Chloride ug/L ND 5.0 09/29/23 21:052.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4157732
Associated Lab Samples:92689265005, 92689265006, 92689265007, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/29/23 21:050.34
Styrene ug/L ND 1.0 09/29/23 21:050.29
Tetrachloroethene ug/L ND 1.0 09/29/23 21:050.29
Toluene ug/L ND 1.0 09/29/23 21:050.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/29/23 21:050.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/29/23 21:050.36
Trichloroethene ug/L ND 1.0 09/29/23 21:050.38
Trichlorofluoromethane ug/L ND 1.0 09/29/23 21:050.30
Vinyl chloride ug/L ND 1.0 09/29/23 21:050.39
1,2-Dichloroethane-d4 (S)%100 70-130 09/29/23 21:05
4-Bromofluorobenzene (S)%99 70-130 09/29/23 21:05
Toluene-d8 (S)%99 70-130 09/29/23 21:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157733LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.820 99 70-130
1,1,2,2-Tetrachloroethane ug/L 20.720 103 70-130
1,1,2-Trichloroethane ug/L 20.920 105 70-130
1,1,2-Trichlorotrifluoroethane ug/L 19.920 100 70-132
1,1-Dichloroethane ug/L 19.320 97 70-130
1,1-Dichloroethene ug/L 19.420 97 69-131
1,2,4-Trichlorobenzene ug/L 20.220 101 70-130
1,2-Dibromo-3-chloropropane ug/L 21.020 105 70-130
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130
1,2-Dichlorobenzene ug/L 20.420 102 70-130
1,2-Dichloroethane ug/L 19.620 98 70-130
1,2-Dichloropropane ug/L 20.520 102 70-130
1,3-Dichlorobenzene ug/L 19.420 97 70-130
1,4-Dichlorobenzene ug/L 19.820 99 70-130
2-Butanone (MEK)ug/L 40.240 101 67-133
2-Hexanone ug/L 42.240 106 70-133
4-Methyl-2-pentanone (MIBK)ug/L 41.940 105 70-130
Acetone ug/L 40.240 101 67-130
Benzene ug/L 20.120 100 70-130
Bromodichloromethane ug/L 20.320 101 70-130
Bromoform ug/L 20.320 101 70-133
Bromomethane ug/L 13.0 v32065 41-148
Carbon disulfide ug/L 19.620 98 70-131
Carbon tetrachloride ug/L 21.220 106 70-130
Chlorobenzene ug/L 20.420 102 70-130
Chloroethane ug/L 17.720 89 41-157
Chloroform ug/L 20.420 102 70-130
Chloromethane ug/L 17.120 86 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157733LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 19.420 97 70-130
cis-1,3-Dichloropropene ug/L 20.420 102 70-130
Cyclohexane ug/L 19.720 98 63-137
Dibromochloromethane ug/L 20.120 101 70-130
Dichlorodifluoromethane ug/L 20.220 101 54-147
Ethylbenzene ug/L 20.120 101 70-130
Isopropylbenzene (Cumene)ug/L 20.320 101 70-130
m&p-Xylene ug/L 40.840 102 70-130
Methyl acetate ug/L 18.520 92 70-130
Methyl-tert-butyl ether ug/L 19.020 95 70-130
Methylcyclohexane ug/L 20.420 102 70-130
Methylene Chloride ug/L 19.020 95 62-130
o-Xylene ug/L 19.820 99 70-130
Styrene ug/L 20.220 101 70-130
Tetrachloroethene ug/L 19.820 99 70-130
Toluene ug/L 20.520 102 70-130
trans-1,2-Dichloroethene ug/L 19.420 97 70-130
trans-1,3-Dichloropropene ug/L 21.220 106 70-130
Trichloroethene ug/L 21.120 105 70-130
Trichlorofluoromethane ug/L 19.320 96 57-130
Vinyl chloride ug/L 15.620 78 66-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4159141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4159142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 107 70-150113 5 3020ND21.5 22.7
1,1,2,2-Tetrachloroethane ug/L 20 103 66-144109 5 3020ND20.7 21.8
1,1,2-Trichloroethane ug/L 20 102 70-142118 15 3020ND20.4 23.7
1,1,2-
Trichlorotrifluoroethane ug/L 20 106 66-168112 5 3020ND21.2 22.4
1,1-Dichloroethane ug/L 20 104 68-150110 5 3020ND20.9 22.0
1,1-Dichloroethene ug/L 20 106 64-162113 6 3020ND21.1 22.5
1,2,4-Trichlorobenzene ug/L 20 106 69-147114 7 3020ND21.3 22.8
1,2-Dibromo-3-
chloropropane ug/L 20 101 62-146111 9 3020ND20.3 22.1
1,2-Dibromoethane (EDB) ug/L 20 106 70-143111 4 3020ND21.3 22.1
1,2-Dichlorobenzene ug/L 20 103 70-142110 7 3020ND20.5 22.0
1,2-Dichloroethane ug/L 20 101 68-145110 8 3020ND20.2 22.0
1,2-Dichloropropane ug/L 20 103 70-144113 9 3020ND20.7 22.6
1,3-Dichlorobenzene ug/L 20 99 70-142109 10 3020ND19.7 21.7
1,4-Dichlorobenzene ug/L 20 99 70-140110 10 3020ND19.8 22.0
2-Butanone (MEK)ug/L 40 98 57-156105 7 3040ND39.0 41.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4159141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4159142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 104 62-153111 6 3040ND41.8 44.5
4-Methyl-2-pentanone
(MIBK)ug/L 40 100 65-144110 10 3040ND39.9 44.0
Acetone ug/L 40 102 49-162104 1 3040ND41.0 41.4
Benzene ug/L 20 104 68-144114 9 3020ND20.7 22.7
Bromodichloromethane ug/L 20 102 70-141114 12 3020ND20.3 22.9
Bromoform ug/L 20 102 59-144109 6 3020ND20.5 21.7
Bromomethane ug/L v3209023-19093 3 3020ND17.9 18.6
Carbon disulfide ug/L 20 105 64-160112 7 3020ND21.1 22.5
Carbon tetrachloride ug/L 20 108 70-147122 13 3020ND21.6 24.5
Chlorobenzene ug/L 20 101 70-143110 9 3020ND20.2 22.1
Chloroethane ug/L 20 98 55-190102 4 3020ND19.6 20.5
Chloroform ug/L 20 102 67-148112 10 3020ND20.3 22.4
Chloromethane ug/L 20 92 38-18098 6 3020ND18.5 19.6
cis-1,2-Dichloroethene ug/L 20 100 67-151110 9 3020ND20.1 21.9
cis-1,3-Dichloropropene ug/L 20 97 70-142113 15 3020ND19.5 22.6
Cyclohexane ug/L 20 104 64-162111 6 3020ND20.9 22.3
Dibromochloromethane ug/L 20 102 68-140106 5 3020ND20.3 21.2
Dichlorodifluoromethane ug/L 20 113 15-200118 4 3020ND22.7 23.6
Ethylbenzene ug/L 20 101 70-145108 7 3020ND20.1 21.6
Isopropylbenzene
(Cumene)ug/L 20 103 70-144113 9 3020ND20.7 22.6
m&p-Xylene ug/L 40 103 70-148110 7 3040ND41.3 44.2
Methyl acetate ug/L 20 92 62-14494 3 3020ND18.3 18.8
Methyl-tert-butyl ether ug/L 20 94 64-146104 9 3020ND18.9 20.8
Methylcyclohexane ug/L 20 110 70-155118 7 3020ND22.0 23.5
Methylene Chloride ug/L 20 98 54-149108 9 3020ND19.6 21.5
o-Xylene ug/L 20 100 70-145106 6 3020ND19.9 21.2
Styrene ug/L 20 101 70-147111 9 3020ND20.2 22.2
Tetrachloroethene ug/L 20 99 70-145110 11 3020ND19.8 22.0
Toluene ug/L 20 102 65-146113 11 3020ND20.3 22.7
trans-1,2-Dichloroethene ug/L 20 103 69-155110 6 3020ND20.7 22.0
trans-1,3-Dichloropropene ug/L 20 107 70-142120 12 3020ND21.3 24.1
Trichloroethene ug/L 20 106 70-152117 9 3020ND21.3 23.4
Trichlorofluoromethane ug/L 20 105 60-158114 9 3020ND20.9 22.8
Vinyl chloride ug/L 20 87 51-17893 7 3020ND17.4 18.6
1,2-Dichloroethane-d4 (S) %102 70-13098
4-Bromofluorobenzene (S) %101 70-13099
Toluene-d8 (S)%99 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803103
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689265002, 92689265004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4159661
Associated Lab Samples:92689265002, 92689265004
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/30/23 13:040.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/30/23 13:040.22
1,1,2-Trichloroethane ug/L ND 1.0 09/30/23 13:040.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/30/23 13:040.32
1,1-Dichloroethane ug/L ND 1.0 09/30/23 13:040.37
1,1-Dichloroethene ug/L ND 1.0 09/30/23 13:040.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/30/23 13:040.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/30/23 13:040.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/30/23 13:040.27
1,2-Dichlorobenzene ug/L ND 1.0 09/30/23 13:040.34
1,2-Dichloroethane ug/L ND 1.0 09/30/23 13:040.32
1,2-Dichloropropane ug/L ND 1.0 09/30/23 13:040.36
1,3-Dichlorobenzene ug/L ND 1.0 09/30/23 13:040.34
1,4-Dichlorobenzene ug/L ND 1.0 09/30/23 13:040.33
2-Butanone (MEK)ug/L ND 5.0 09/30/23 13:044.0
2-Hexanone ug/L ND 5.0 09/30/23 13:040.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/30/23 13:042.7
Acetone ug/L ND 25.0 09/30/23 13:045.1
Benzene ug/L ND 1.0 09/30/23 13:040.34
Bromodichloromethane ug/L ND 1.0 09/30/23 13:040.31
Bromoform ug/L ND 1.0 09/30/23 13:040.34
Bromomethane ug/L ND 2.0 v209/30/23 13:041.7
Carbon disulfide ug/L ND 2.0 09/30/23 13:040.36
Carbon tetrachloride ug/L ND 1.0 09/30/23 13:040.33
Chlorobenzene ug/L ND 1.0 09/30/23 13:040.28
Chloroethane ug/L ND 1.0 09/30/23 13:040.65
Chloroform ug/L ND 1.0 09/30/23 13:040.43
Chloromethane ug/L ND 1.0 09/30/23 13:040.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/30/23 13:040.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/30/23 13:040.36
Cyclohexane ug/L ND 1.0 09/30/23 13:040.35
Dibromochloromethane ug/L ND 1.0 09/30/23 13:040.36
Dichlorodifluoromethane ug/L ND 1.0 09/30/23 13:040.35
Ethylbenzene ug/L ND 1.0 09/30/23 13:040.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/30/23 13:040.33
m&p-Xylene ug/L ND 2.0 09/30/23 13:040.71
Methyl acetate ug/L ND 10.0 09/30/23 13:042.4
Methyl-tert-butyl ether ug/L ND 1.0 09/30/23 13:040.42
Methylcyclohexane ug/L ND 10.0 09/30/23 13:041.5
Methylene Chloride ug/L ND 5.0 09/30/23 13:042.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4159661
Associated Lab Samples:92689265002, 92689265004
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/30/23 13:040.34
Styrene ug/L ND 1.0 09/30/23 13:040.29
Tetrachloroethene ug/L ND 1.0 09/30/23 13:040.29
Toluene ug/L ND 1.0 09/30/23 13:040.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/30/23 13:040.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/30/23 13:040.36
Trichloroethene ug/L ND 1.0 09/30/23 13:040.38
Trichlorofluoromethane ug/L ND 1.0 09/30/23 13:040.30
Vinyl chloride ug/L ND 1.0 09/30/23 13:040.39
1,2-Dichloroethane-d4 (S)%102 70-130 09/30/23 13:04
4-Bromofluorobenzene (S)%100 70-130 09/30/23 13:04
Toluene-d8 (S)%100 70-130 09/30/23 13:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4159662LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.020 100 70-130
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130
1,1,2-Trichloroethane ug/L 20.120 101 70-130
1,1,2-Trichlorotrifluoroethane ug/L 21.020 105 70-132
1,1-Dichloroethane ug/L 19.420 97 70-130
1,1-Dichloroethene ug/L 19.820 99 69-131
1,2,4-Trichlorobenzene ug/L 20.420 102 70-130
1,2-Dibromo-3-chloropropane ug/L 19.820 99 70-130
1,2-Dibromoethane (EDB)ug/L 19.820 99 70-130
1,2-Dichlorobenzene ug/L 20.220 101 70-130
1,2-Dichloroethane ug/L 20.020 100 70-130
1,2-Dichloropropane ug/L 20.120 100 70-130
1,3-Dichlorobenzene ug/L 19.820 99 70-130
1,4-Dichlorobenzene ug/L 19.920 100 70-130
2-Butanone (MEK)ug/L 39.040 97 67-133
2-Hexanone ug/L 40.540 101 70-133
4-Methyl-2-pentanone (MIBK)ug/L 40.740 102 70-130
Acetone ug/L 40.540 101 67-130
Benzene ug/L 19.920 99 70-130
Bromodichloromethane ug/L 20.420 102 70-130
Bromoform ug/L 19.920 100 70-133
Bromomethane ug/L 15.1 v32076 41-148
Carbon disulfide ug/L 20.720 104 70-131
Carbon tetrachloride ug/L 22.020 110 70-130
Chlorobenzene ug/L 20.020 100 70-130
Chloroethane ug/L 18.620 93 41-157
Chloroform ug/L 20.420 102 70-130
Chloromethane ug/L 18.620 93 59-141
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4159662LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 20.020 100 70-130
cis-1,3-Dichloropropene ug/L 20.320 102 70-130
Cyclohexane ug/L 20.320 101 63-137
Dibromochloromethane ug/L 19.020 95 70-130
Dichlorodifluoromethane ug/L 24.620 123 54-147
Ethylbenzene ug/L 19.820 99 70-130
Isopropylbenzene (Cumene)ug/L 20.420 102 70-130
m&p-Xylene ug/L 40.340 101 70-130
Methyl acetate ug/L 17.620 88 70-130
Methyl-tert-butyl ether ug/L 19.220 96 70-130
Methylcyclohexane ug/L 21.020 105 70-130
Methylene Chloride ug/L 19.720 99 62-130
o-Xylene ug/L 19.920 100 70-130
Styrene ug/L 20.320 101 70-130
Tetrachloroethene ug/L 20.020 100 70-130
Toluene ug/L 19.920 100 70-130
trans-1,2-Dichloroethene ug/L 20.020 100 70-130
trans-1,3-Dichloropropene ug/L 21.420 107 70-130
Trichloroethene ug/L 20.620 103 70-130
Trichlorofluoromethane ug/L 20.220 101 57-130
Vinyl chloride ug/L 17.220 86 66-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4159663MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689895009
4159664
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 112 70-150107 5 3020ND22.5 21.4
1,1,2,2-Tetrachloroethane ug/L 20 134 66-144120 11 3020ND26.7 24.0
1,1,2-Trichloroethane ug/L 20 118 70-142113 4 3020ND23.7 22.6
1,1,2-
Trichlorotrifluoroethane ug/L 20 108 66-168105 3 3020ND21.7 21.0
1,1-Dichloroethane ug/L 20 110 68-150105 5 3020ND23.7 22.6
1,1-Dichloroethene ug/L 20 110 64-162105 4 30203.6 25.6 24.5
1,2,4-Trichlorobenzene ug/L 20 132 69-147123 7 3020ND26.4 24.6
1,2-Dibromo-3-
chloropropane ug/L 20 127 62-146117 8 3020ND25.4 23.5
1,2-Dibromoethane (EDB) ug/L 20 136 70-143119 14 3020ND27.2 23.7
1,2-Dichlorobenzene ug/L 20 126 70-142123 3 3020ND25.3 24.6
1,2-Dichloroethane ug/L 20 119 68-145110 8 3020ND23.8 22.0
1,2-Dichloropropane ug/L 20 118 70-144112 5 3020ND23.5 22.5
1,3-Dichlorobenzene ug/L 20 124 70-142122 1 3020ND24.8 24.4
1,4-Dichlorobenzene ug/L 20 122 70-140119 2 3020ND24.4 23.8
2-Butanone (MEK)ug/L 40 115 57-156104 10 3040ND46.0 41.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4159663MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689895009
4159664
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 131 62-153118 11 3040ND52.6 47.3
4-Methyl-2-pentanone
(MIBK)ug/L 40 119 65-144110 8 3040ND47.4 43.9
Acetone ug/L 40 123 49-162109 3040ND49.2J 43.8J
Benzene ug/L 20 114 68-144110 3 3020ND22.7 21.9
Bromodichloromethane ug/L 20 118 70-141114 4 3020ND23.6 22.7
Bromoform ug/L 20 134 59-144116 15 3020ND26.9 23.1
Bromomethane ug/L v3209323-19090 3 3020ND18.6 18.0
Carbon disulfide ug/L 20 107 64-160104 3 3020ND21.4 20.8
Carbon tetrachloride ug/L 20 116 70-147114 2 3020ND23.1 22.8
Chlorobenzene ug/L 20 127 70-143116 10 3020ND25.5 23.1
Chloroethane ug/L 20 107 55-19099 8 3020ND21.5 19.8
Chloroform ug/L 20 113 67-148111 1 3020ND22.6 22.3
Chloromethane ug/L 20 95 38-18092 4 3020ND19.1 18.4
cis-1,2-Dichloroethene ug/L 20 128 67-15185 4 3020200225 216
cis-1,3-Dichloropropene ug/L 20 117 70-142110 6 3020ND23.3 22.0
Cyclohexane ug/L 20 105 64-162101 4 3020ND21.0 20.3
Dibromochloromethane ug/L 20 124 68-140115 8 3020ND24.8 23.0
Dichlorodifluoromethane ug/L 20 121 15-200116 4 3020ND24.1 23.3
Ethylbenzene ug/L 20 127 70-145116 9 3020ND25.5 23.2
Isopropylbenzene
(Cumene)ug/L 20 127 70-144118 8 3020ND25.5 23.6
m&p-Xylene ug/L 40 129 70-148118 8 3040ND51.5 47.4
Methyl acetate ug/L 20 107 62-14495 3020ND21.5 19.0J
Methyl-tert-butyl ether ug/L 20 111 64-146103 8 3020ND22.3 20.5
Methylcyclohexane ug/L 20 106 70-155111 5 3020ND21.2 22.2
Methylene Chloride ug/L 20 112 54-149106 5 3020ND22.3 21.3
o-Xylene ug/L 20 126 70-145113 11 3020ND25.2 22.6
Styrene ug/L 20 124 70-147116 6 3020ND24.8 23.2
Tetrachloroethene ug/L 20 121 70-145111 9 3020ND24.1 22.2
Toluene ug/L 20 116 65-146109 6 3020ND23.2 21.8
trans-1,2-Dichloroethene ug/L 20 113 69-155108 3 302015.9 38.4 37.4
trans-1,3-Dichloropropene ug/L 20 123 70-142117 5 3020ND24.7 23.4
Trichloroethene ug/L 20 118 70-152112 5 3020ND24.9 23.7
Trichlorofluoromethane ug/L 20 108 60-158105 3 3020ND21.5 21.0
Vinyl chloride ug/L 20 87 51-17886 1 3020ND17.3 17.2
1,2-Dichloroethane-d4 (S) %102 70-130102
4-Bromofluorobenzene (S) %102 70-13099
Toluene-d8 (S)%98 70-13098
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4160037MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689624005
4160038
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 117 70-150122 4 3020ND23.4 24.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4160037MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689624005
4160038
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,2,2-Tetrachloroethane ug/L 20 108 66-144111 3 3020ND21.6 22.2
1,1,2-Trichloroethane ug/L 20 112 70-142119 6 3020ND22.5 23.8
1,1,2-
Trichlorotrifluoroethane ug/L 20 116 66-168121 4 3020ND23.3 24.1
1,1-Dichloroethane ug/L 20 111 68-150116 5 3020ND22.2 23.3
1,1-Dichloroethene ug/L 20 116 64-162123 6 3020ND23.2 24.6
1,2,4-Trichlorobenzene ug/L 20 117 69-147120 2 3020ND23.5 24.1
1,2-Dibromo-3-
chloropropane ug/L 20 105 62-146109 4 3020ND20.9 21.9
1,2-Dibromoethane (EDB) ug/L 20 112 70-143115 2 3020ND22.4 23.0
1,2-Dichlorobenzene ug/L 20 109 70-142115 5 3020ND21.7 22.9
1,2-Dichloroethane ug/L 20 113 68-145115 2 3020ND22.5 23.0
1,2-Dichloropropane ug/L 20 112 70-144116 3 3020ND22.5 23.1
1,3-Dichlorobenzene ug/L 20 109 70-142113 4 3020ND21.8 22.7
1,4-Dichlorobenzene ug/L 20 106 70-140113 6 3020ND21.1 22.5
2-Butanone (MEK)ug/L 40 106 57-156108 2 3040ND42.2 43.2
2-Hexanone ug/L 40 112 62-153111 1 3040ND44.6 44.4
4-Methyl-2-pentanone
(MIBK)
ug/L 40 109 65-144110 1 3040ND43.7 44.1
Acetone ug/L 40 100 49-162103 3 3040ND40.0 41.1
Benzene ug/L 20 111 68-144116 4 3020ND22.3 23.2
Bromodichloromethane ug/L 20 114 70-141118 3 3020ND22.8 23.6
Bromoform ug/L 20 108 59-144113 4 3020ND21.7 22.6
Bromomethane ug/L v3207923-19092 14 3020ND15.8 18.3
Carbon disulfide ug/L 20 119 64-160124 4 3020ND23.8 24.8
Carbon tetrachloride ug/L 20 127 70-147130 2 3020ND25.4 25.9
Chlorobenzene ug/L 20 107 70-143112 5 3020ND21.4 22.4
Chloroethane ug/L 20 107 55-190112 5 3020ND21.4 22.5
Chloroform ug/L 20 113 67-148120 6 3020ND22.6 24.1
Chloromethane ug/L 20 103 38-180110 7 3020ND20.6 22.1
cis-1,2-Dichloroethene ug/L 20 110 67-151114 4 3020ND21.9 22.8
cis-1,3-Dichloropropene ug/L 20 111 70-142115 3 3020ND22.1 22.9
Cyclohexane ug/L 20 114 64-162121 6 3020ND22.8 24.1
Dibromochloromethane ug/L 20 111 68-140115 4 3020ND22.1 23.0
Dichlorodifluoromethane ug/L 20 139 15-200148 6 3020ND27.8 29.5
Ethylbenzene ug/L 20 108 70-145110 2 3020ND21.6 21.9
Isopropylbenzene
(Cumene)
ug/L 20 114 70-144117 2 3020ND22.9 23.4
m&p-Xylene ug/L 40 110 70-148113 2 3040ND44.1 45.2
Methyl acetate ug/L 20 102 62-14496 5 3020ND20.4 19.3
Methyl-tert-butyl ether ug/L 20 101 64-146108 6 3020ND20.3 21.5
Methylcyclohexane ug/L 20 125 70-155123 1 3020ND25.0 24.7
Methylene Chloride ug/L 20 105 54-149110 4 3020ND21.0 21.9
o-Xylene ug/L 20 109 70-145111 2 3020ND21.8 22.2
Styrene ug/L 20 105 70-147112 6 3020ND21.1 22.5
Tetrachloroethene ug/L 20 113 70-145114 1 3020ND22.5 22.7
Toluene ug/L 20 110 65-146112 2 3020ND21.9 22.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4160037MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689624005
4160038
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
trans-1,2-Dichloroethene ug/L 20 113 69-155121 7 3020ND22.6 24.1
trans-1,3-Dichloropropene ug/L 20 115 70-142121 6 3020ND22.9 24.2
Trichloroethene ug/L 20 114 70-152122 8 3020ND22.7 24.5
Trichlorofluoromethane ug/L 20 116 60-158127 9 3020ND23.2 25.4
Vinyl chloride ug/L 20 98 51-178102 5 3020ND19.5 20.4
1,2-Dichloroethane-d4 (S) %103 70-130101
4-Bromofluorobenzene (S) %100 70-130102
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803106
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689265001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4159708
Associated Lab Samples:92689265001
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 09/30/23 01:150.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/30/23 01:150.22
1,1,2-Trichloroethane ug/L ND 1.0 09/30/23 01:150.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/30/23 01:150.32
1,1-Dichloroethane ug/L ND 1.0 09/30/23 01:150.37
1,1-Dichloroethene ug/L ND 1.0 v109/30/23 01:150.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/30/23 01:150.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/30/23 01:150.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/30/23 01:150.27
1,2-Dichlorobenzene ug/L ND 1.0 09/30/23 01:150.34
1,2-Dichloroethane ug/L ND 1.0 09/30/23 01:150.32
1,2-Dichloropropane ug/L ND 1.0 09/30/23 01:150.36
1,3-Dichlorobenzene ug/L ND 1.0 09/30/23 01:150.34
1,4-Dichlorobenzene ug/L ND 1.0 09/30/23 01:150.33
2-Butanone (MEK)ug/L ND 5.0 09/30/23 01:154.0
2-Hexanone ug/L ND 5.0 09/30/23 01:150.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/30/23 01:152.7
Acetone ug/L ND 25.0 09/30/23 01:155.1
Benzene ug/L ND 1.0 09/30/23 01:150.34
Bromodichloromethane ug/L ND 1.0 09/30/23 01:150.31
Bromoform ug/L ND 1.0 09/30/23 01:150.34
Bromomethane ug/L ND 2.0 v209/30/23 01:151.7
Carbon disulfide ug/L ND 2.0 09/30/23 01:150.36
Carbon tetrachloride ug/L ND 1.0 09/30/23 01:150.33
Chlorobenzene ug/L ND 1.0 09/30/23 01:150.28
Chloroethane ug/L ND 1.0 09/30/23 01:150.65
Chloroform ug/L ND 1.0 09/30/23 01:150.43
Chloromethane ug/L ND 1.0 09/30/23 01:150.54
cis-1,2-Dichloroethene ug/L ND 1.0 09/30/23 01:150.38
cis-1,3-Dichloropropene ug/L ND 1.0 09/30/23 01:150.36
Cyclohexane ug/L ND 1.0 09/30/23 01:150.35
Dibromochloromethane ug/L ND 1.0 09/30/23 01:150.36
Dichlorodifluoromethane ug/L ND 1.0 09/30/23 01:150.35
Ethylbenzene ug/L ND 1.0 09/30/23 01:150.30
Isopropylbenzene (Cumene)ug/L ND 1.0 09/30/23 01:150.33
m&p-Xylene ug/L ND 2.0 09/30/23 01:150.71
Methyl acetate ug/L ND 10.0 09/30/23 01:152.4
Methyl-tert-butyl ether ug/L ND 1.0 09/30/23 01:150.42
Methylcyclohexane ug/L ND 10.0 09/30/23 01:151.5
Methylene Chloride ug/L ND 5.0 v109/30/23 01:152.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4159708
Associated Lab Samples:92689265001
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 09/30/23 01:150.34
Styrene ug/L ND 1.0 09/30/23 01:150.29
Tetrachloroethene ug/L ND 1.0 09/30/23 01:150.29
Toluene ug/L ND 1.0 09/30/23 01:150.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/30/23 01:150.40
trans-1,3-Dichloropropene ug/L ND 1.0 09/30/23 01:150.36
Trichloroethene ug/L ND 1.0 09/30/23 01:150.38
Trichlorofluoromethane ug/L ND 1.0 09/30/23 01:150.30
Vinyl chloride ug/L ND 1.0 09/30/23 01:150.39
1,2-Dichloroethane-d4 (S)%105 70-130 09/30/23 01:15
4-Bromofluorobenzene (S)%97 70-130 09/30/23 01:15
Toluene-d8 (S)%99 70-130 09/30/23 01:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4159709LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 22.020 110 70-130
1,1,2,2-Tetrachloroethane ug/L 22.420 112 70-130
1,1,2-Trichloroethane ug/L 21.320 107 70-130
1,1,2-Trichlorotrifluoroethane ug/L 21.920 110 70-132
1,1-Dichloroethane ug/L 23.320 116 70-130
1,1-Dichloroethene ug/L 25.1 v120126 69-131
1,2,4-Trichlorobenzene ug/L 18.620 93 70-130
1,2-Dibromo-3-chloropropane ug/L 18.920 95 70-130
1,2-Dibromoethane (EDB)ug/L 20.720 104 70-130
1,2-Dichlorobenzene ug/L 20.220 101 70-130
1,2-Dichloroethane ug/L 21.620 108 70-130
1,2-Dichloropropane ug/L 22.520 113 70-130
1,3-Dichlorobenzene ug/L 20.620 103 70-130
1,4-Dichlorobenzene ug/L 20.520 102 70-130
2-Butanone (MEK)ug/L 45.040 113 67-133
2-Hexanone ug/L 45.240 113 70-133
4-Methyl-2-pentanone (MIBK)ug/L 44.640 112 70-130
Acetone ug/L 47.240 118 67-130
Benzene ug/L 22.220 111 70-130
Bromodichloromethane ug/L 21.120 105 70-130
Bromoform ug/L 18.620 93 70-133
Bromomethane ug/L 18.4 v32092 41-148
Carbon disulfide ug/L 24.120 120 70-131
Carbon tetrachloride ug/L 21.720 109 70-130
Chlorobenzene ug/L 21.620 108 70-130
Chloroethane ug/L 20.120 101 41-157
Chloroform ug/L 21.420 107 70-130
Chloromethane ug/L 19.420 97 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4159709LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 23.020 115 70-130
cis-1,3-Dichloropropene ug/L 21.320 106 70-130
Cyclohexane ug/L 23.820 119 63-137
Dibromochloromethane ug/L 20.120 101 70-130
Dichlorodifluoromethane ug/L 22.820 114 54-147
Ethylbenzene ug/L 21.720 108 70-130
Isopropylbenzene (Cumene)ug/L 21.620 108 70-130
m&p-Xylene ug/L 42.740 107 70-130
Methyl acetate ug/L 21.120 105 70-130
Methyl-tert-butyl ether ug/L 20.320 102 70-130
Methylcyclohexane ug/L 24.720 123 70-130
Methylene Chloride ug/L 25.2 v120126 62-130
o-Xylene ug/L 20.620 103 70-130
Styrene ug/L 21.420 107 70-130
Tetrachloroethene ug/L 19.520 98 70-130
Toluene ug/L 21.420 107 70-130
trans-1,2-Dichloroethene ug/L 23.520 117 70-130
trans-1,3-Dichloropropene ug/L 20.420 102 70-130
Trichloroethene ug/L 21.120 106 70-130
Trichlorofluoromethane ug/L 20.120 101 57-130
Vinyl chloride ug/L 18.420 92 66-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4159711MATRIX SPIKE SAMPLE:
MSSpike
Result
92689056002
1,1,1-Trichloroethane ug/L 23.520 117 70-150ND
1,1,2,2-Tetrachloroethane ug/L 24.320 121 66-144ND
1,1,2-Trichloroethane ug/L 24.020 120 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 24.420 122 66-168ND
1,1-Dichloroethane ug/L 22.420 112 68-150ND
1,1-Dichloroethene ug/L 23.220 116 64-162ND
1,2,4-Trichlorobenzene ug/L 23.720 118 69-147ND
1,2-Dibromo-3-chloropropane ug/L 23.320 116 62-146ND
1,2-Dibromoethane (EDB)ug/L 24.720 124 70-143ND
1,2-Dichlorobenzene ug/L 24.120 121 70-142ND
1,2-Dichloroethane ug/L 23.220 116 68-145ND
1,2-Dichloropropane ug/L 23.520 117 70-144ND
1,3-Dichlorobenzene ug/L 24.120 120 70-142ND
1,4-Dichlorobenzene ug/L 23.920 119 70-140ND
2-Butanone (MEK)ug/L 49.940 125 57-156ND
2-Hexanone ug/L 46.840 117 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 46.740 117 65-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4159711MATRIX SPIKE SAMPLE:
MSSpike
Result
92689056002
Acetone ug/L 41.640 104 49-162ND
Benzene ug/L 26.220 117 68-1442.7
Bromodichloromethane ug/L 22.820 114 70-141ND
Bromoform ug/L 23.020 115 59-144ND
Bromomethane ug/L 19.920 99 23-190ND
Carbon disulfide ug/L 23.820 119 64-160ND
Carbon tetrachloride ug/L 23.720 119 70-147ND
Chlorobenzene ug/L 24.120 121 70-143ND
Chloroethane ug/L 22.720 114 55-190ND
Chloroform ug/L 22.820 114 67-148ND
Chloromethane ug/L 20.920 102 38-180ND
cis-1,2-Dichloroethene ug/L 22.520 112 67-151ND
cis-1,3-Dichloropropene ug/L 23.020 115 70-142ND
Cyclohexane ug/L 23.020 111 64-1620.76J
Dibromochloromethane ug/L 23.920 119 68-140ND
Dichlorodifluoromethane ug/L 24.820 124 15-200ND
Ethylbenzene ug/L 23.920 119 70-145ND
Isopropylbenzene (Cumene)ug/L 24.320 121 70-144ND
m&p-Xylene ug/L 48.140 119 70-1480.71J
Methyl acetate ug/L 20.120 100 62-144ND
Methyl-tert-butyl ether ug/L 21.220 106 64-146ND
Methylcyclohexane ug/L 25.120 126 70-155ND
Methylene Chloride ug/L 22.020 110 54-149ND
o-Xylene ug/L 24.020 118 70-1450.40J
Styrene ug/L 23.820 119 70-147ND
Tetrachloroethene ug/L 24.020 120 70-145ND
Toluene ug/L 23.020 115 65-146ND
trans-1,2-Dichloroethene ug/L 20.720 103 69-155ND
trans-1,3-Dichloropropene ug/L 22.720 114 70-142ND
Trichloroethene ug/L 24.920 124 70-152ND
Trichlorofluoromethane ug/L 23.320 116 60-158ND
Vinyl chloride ug/L 19.820 99 51-178ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689056001
4159710SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689056001
4159710SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%95106
4-Bromofluorobenzene (S)%9697
Toluene-d8 (S)%10398
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803314
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689265003, 92689265008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4160552
Associated Lab Samples:92689265003, 92689265008
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 10/01/23 01:120.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/01/23 01:120.22
1,1,2-Trichloroethane ug/L ND 1.0 10/01/23 01:120.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 10/01/23 01:120.32
1,1-Dichloroethane ug/L ND 1.0 10/01/23 01:120.37
1,1-Dichloroethene ug/L ND 1.0 10/01/23 01:120.35
1,2,4-Trichlorobenzene ug/L ND 1.0 10/01/23 01:120.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/01/23 01:120.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/01/23 01:120.27
1,2-Dichlorobenzene ug/L ND 1.0 10/01/23 01:120.34
1,2-Dichloroethane ug/L ND 1.0 10/01/23 01:120.32
1,2-Dichloropropane ug/L ND 1.0 10/01/23 01:120.36
1,3-Dichlorobenzene ug/L ND 1.0 10/01/23 01:120.34
1,4-Dichlorobenzene ug/L ND 1.0 10/01/23 01:120.33
2-Butanone (MEK)ug/L ND 5.0 10/01/23 01:124.0
2-Hexanone ug/L ND 5.0 10/01/23 01:120.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/01/23 01:122.7
Acetone ug/L ND 25.0 10/01/23 01:125.1
Benzene ug/L ND 1.0 10/01/23 01:120.34
Bromodichloromethane ug/L ND 1.0 10/01/23 01:120.31
Bromoform ug/L ND 1.0 10/01/23 01:120.34
Bromomethane ug/L ND 2.0 v210/01/23 01:121.7
Carbon disulfide ug/L ND 2.0 10/01/23 01:120.36
Carbon tetrachloride ug/L ND 1.0 10/01/23 01:120.33
Chlorobenzene ug/L ND 1.0 10/01/23 01:120.28
Chloroethane ug/L ND 1.0 10/01/23 01:120.65
Chloroform ug/L ND 1.0 10/01/23 01:120.43
Chloromethane ug/L ND 1.0 10/01/23 01:120.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/01/23 01:120.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/01/23 01:120.36
Cyclohexane ug/L ND 1.0 10/01/23 01:120.35
Dibromochloromethane ug/L ND 1.0 10/01/23 01:120.36
Dichlorodifluoromethane ug/L ND 1.0 10/01/23 01:120.35
Ethylbenzene ug/L ND 1.0 10/01/23 01:120.30
Isopropylbenzene (Cumene)ug/L ND 1.0 10/01/23 01:120.33
m&p-Xylene ug/L ND 2.0 10/01/23 01:120.71
Methyl acetate ug/L ND 10.0 10/01/23 01:122.4
Methyl-tert-butyl ether ug/L ND 1.0 10/01/23 01:120.42
Methylcyclohexane ug/L ND 10.0 10/01/23 01:121.5
Methylene Chloride ug/L ND 5.0 10/01/23 01:122.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4160552
Associated Lab Samples:92689265003, 92689265008
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 10/01/23 01:120.34
Styrene ug/L ND 1.0 10/01/23 01:120.29
Tetrachloroethene ug/L ND 1.0 10/01/23 01:120.29
Toluene ug/L ND 1.0 10/01/23 01:120.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/01/23 01:120.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/01/23 01:120.36
Trichloroethene ug/L ND 1.0 10/01/23 01:120.38
Trichlorofluoromethane ug/L ND 1.0 10/01/23 01:120.30
Vinyl chloride ug/L ND 1.0 10/01/23 01:120.39
1,2-Dichloroethane-d4 (S)%96 70-130 10/01/23 01:12
4-Bromofluorobenzene (S)%98 70-130 10/01/23 01:12
Toluene-d8 (S)%98 70-130 10/01/23 01:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4160553LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.920 105 70-130
1,1,2,2-Tetrachloroethane ug/L 21.720 108 70-130
1,1,2-Trichloroethane ug/L 20.920 105 70-130
1,1,2-Trichlorotrifluoroethane ug/L 21.720 108 70-132
1,1-Dichloroethane ug/L 21.420 107 70-130
1,1-Dichloroethene ug/L 23.220 116 69-131
1,2,4-Trichlorobenzene ug/L 18.720 93 70-130
1,2-Dibromo-3-chloropropane ug/L 18.120 90 70-130
1,2-Dibromoethane (EDB)ug/L 20.620 103 70-130
1,2-Dichlorobenzene ug/L 19.820 99 70-130
1,2-Dichloroethane ug/L 20.620 103 70-130
1,2-Dichloropropane ug/L 22.220 111 70-130
1,3-Dichlorobenzene ug/L 20.020 100 70-130
1,4-Dichlorobenzene ug/L 19.720 99 70-130
2-Butanone (MEK)ug/L 41.240 103 67-133
2-Hexanone ug/L 41.140 103 70-133
4-Methyl-2-pentanone (MIBK)ug/L 42.040 105 70-130
Acetone ug/L 41.540 104 67-130
Benzene ug/L 21.520 107 70-130
Bromodichloromethane ug/L 20.420 102 70-130
Bromoform ug/L 17.920 90 70-133
Bromomethane ug/L 14.1 v32070 41-148
Carbon disulfide ug/L 21.920 110 70-131
Carbon tetrachloride ug/L 20.620 103 70-130
Chlorobenzene ug/L 21.020 105 70-130
Chloroethane ug/L 22.020 110 41-157
Chloroform ug/L 20.720 104 70-130
Chloromethane ug/L 17.220 86 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4160553LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 21.520 108 70-130
cis-1,3-Dichloropropene ug/L 20.520 102 70-130
Cyclohexane ug/L 22.320 111 63-137
Dibromochloromethane ug/L 19.920 99 70-130
Dichlorodifluoromethane ug/L 23.020 115 54-147
Ethylbenzene ug/L 20.720 104 70-130
Isopropylbenzene (Cumene)ug/L 20.920 104 70-130
m&p-Xylene ug/L 41.440 103 70-130
Methyl acetate ug/L 19.820 99 70-130
Methyl-tert-butyl ether ug/L 19.820 99 70-130
Methylcyclohexane ug/L 22.720 114 70-130
Methylene Chloride ug/L 23.720 118 62-130
o-Xylene ug/L 20.720 103 70-130
Styrene ug/L 21.020 105 70-130
Tetrachloroethene ug/L 18.920 95 70-130
Toluene ug/L 20.820 104 70-130
trans-1,2-Dichloroethene ug/L 21.820 109 70-130
trans-1,3-Dichloropropene ug/L 19.820 99 70-130
Trichloroethene ug/L 20.620 103 70-130
Trichlorofluoromethane ug/L 18.920 95 57-130
Vinyl chloride ug/L 17.720 89 66-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4160554MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690349006
4160555
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1-Trichloroethane ug/L 20 113 70-150119 6 3020ND22.6 23.9
1,1,2,2-Tetrachloroethane ug/L 20 117 66-144118 1 3020ND23.4 23.6
1,1,2-Trichloroethane ug/L 20 111 70-142117 6 3020ND22.2 23.5
1,1,2-
Trichlorotrifluoroethane ug/L 20 105 66-168113 8 3020ND21.0 22.7
1,1-Dichloroethane ug/L 20 106 68-150114 7 3020ND21.3 22.7
1,1-Dichloroethene ug/L 20 110 64-162118 7 3020ND22.6 24.2
1,2,4-Trichlorobenzene ug/L 20 103 69-147117 13 3020ND20.6 23.5
1,2-Dibromo-3-
chloropropane ug/L 20 113 62-146119 6 3020ND22.5 23.9
1,2-Dibromoethane (EDB) ug/L 20 115 70-143124 8 3020ND22.9 24.9
1,2-Dichlorobenzene ug/L 20 115 70-142118 3 3020ND22.9 23.6
1,2-Dichloroethane ug/L 20 105 68-145113 7 3020ND21.0 22.5
1,2-Dichloropropane ug/L 20 110 70-144119 7 3020ND22.0 23.7
1,3-Dichlorobenzene ug/L 20 108 70-142116 7 3020ND21.7 23.2
1,4-Dichlorobenzene ug/L 20 109 70-140115 6 3020ND21.8 23.0
2-Butanone (MEK)ug/L 40 106 57-156104 1 3040ND42.3 41.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4160554MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690349006
4160555
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 114 62-153119 4 3040ND45.6 47.4
4-Methyl-2-pentanone
(MIBK)ug/L 40 105 65-144111 6 3040ND41.9 44.3
Acetone ug/L 40 101 49-16298 3 3040ND40.6 39.3
Benzene ug/L 20 110 68-144115 4 3020ND22.0 22.9
Bromodichloromethane ug/L 20 115 70-141121 6 3020ND22.9 24.3
Bromoform ug/L 20 115 59-144120 5 3020ND22.9 24.0
Bromomethane ug/L v3208523-19096 13 3020ND16.9 19.3
Carbon disulfide ug/L 20 109 64-160117 7 3020ND21.7 23.3
Carbon tetrachloride ug/L 20 119 70-147128 7 3020ND23.8 25.6
Chlorobenzene ug/L 20 112 70-143117 4 3020ND22.4 23.3
Chloroethane ug/L 20 98 55-190109 11 3020ND19.5 21.8
Chloroform ug/L 20 109 67-148121 11 3020ND21.7 24.1
Chloromethane ug/L 20 98 38-180108 10 3020ND19.6 21.6
cis-1,2-Dichloroethene ug/L 20 106 67-151114 7 3020ND21.3 22.7
cis-1,3-Dichloropropene ug/L 20 107 70-142115 8 3020ND21.3 23.1
Cyclohexane ug/L 20 105 64-162113 7 3020ND21.1 22.5
Dibromochloromethane ug/L 20 118 68-140121 2 3020ND23.7 24.2
Dichlorodifluoromethane ug/L 20 124 15-200135 8 3020ND24.9 27.0
Ethylbenzene ug/L 20 112 70-145117 4 3020ND22.4 23.4
Isopropylbenzene
(Cumene)ug/L 20 115 70-144121 6 3020ND23.0 24.3
m&p-Xylene ug/L 40 114 70-148119 5 3040ND45.5 47.8
Methyl acetate ug/L 20 85 62-14490 6 3020ND17.0 18.1
Methyl-tert-butyl ether ug/L 20 98 64-146104 6 3020ND19.6 20.9
Methylcyclohexane ug/L 20 107 70-155117 9 3020ND21.3 23.4
Methylene Chloride ug/L 20 102 54-149109 7 3020ND20.4 21.8
o-Xylene ug/L 20 111 70-145117 5 3020ND22.2 23.3
Styrene ug/L 20 112 70-147117 4 3020ND22.3 23.3
Tetrachloroethene ug/L 20 110 70-145113 3 3020ND22.0 22.7
Toluene ug/L 20 107 65-146114 6 3020ND21.4 22.8
trans-1,2-Dichloroethene ug/L 20 106 69-155114 7 3020ND21.3 22.8
trans-1,3-Dichloropropene ug/L 20 111 70-142120 7 3020ND22.3 24.0
Trichloroethene ug/L 20 115 70-152120 4 3020ND24.0 24.9
Trichlorofluoromethane ug/L 20 112 60-158119 6 3020ND22.5 23.9
Vinyl chloride ug/L 20 90 51-178100 11 3020ND18.0 20.1
1,2-Dichloroethane-d4 (S) %100 70-13099
4-Bromofluorobenzene (S) %99 70-130100
Toluene-d8 (S)%97 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801703
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152817
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265010
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/25/23 16:291.2
2,4,5-Trichlorophenol ug/L ND 10.0 09/25/23 16:291.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/25/23 16:291.6
2,4-Dichlorophenol ug/L ND 10.0 09/25/23 16:291.4
2,4-Dimethylphenol ug/L ND 10.0 09/25/23 16:291.7
2,4-Dinitrophenol ug/L ND 50.0 09/25/23 16:2926.0
2,4-Dinitrotoluene ug/L ND 10.0 09/25/23 16:291.6
2,6-Dinitrotoluene ug/L ND 10.0 09/25/23 16:291.7
2-Chloronaphthalene ug/L ND 10.0 09/25/23 16:291.7
2-Chlorophenol ug/L ND 10.0 09/25/23 16:291.2
2-Methylnaphthalene ug/L ND 10.0 09/25/23 16:291.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/25/23 16:291.9
2-Nitroaniline ug/L ND 20.0 09/25/23 16:293.0
2-Nitrophenol ug/L ND 10.0 09/25/23 16:291.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/25/23 16:291.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/25/23 16:298.1
3-Nitroaniline ug/L ND 20.0 09/25/23 16:293.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/25/23 16:297.8
4-Bromophenylphenyl ether ug/L ND 10.0 09/25/23 16:291.8
4-Chloro-3-methylphenol ug/L ND 10.0 09/25/23 16:293.3
4-Chloroaniline ug/L ND 20.0 09/25/23 16:293.6
4-Chlorophenylphenyl ether ug/L ND 10.0 09/25/23 16:292.0
4-Nitroaniline ug/L ND 20.0 09/25/23 16:295.1
4-Nitrophenol ug/L ND 50.0 09/25/23 16:296.6
Acenaphthene ug/L ND 10.0 09/25/23 16:292.0
Acenaphthylene ug/L ND 10.0 09/25/23 16:292.0
Acetophenone ug/L ND 10.0 09/25/23 16:291.5
Anthracene ug/L ND 10.0 09/25/23 16:292.3
Atrazine ug/L ND 10.0 09/25/23 16:293.2
Benzaldehyde ug/L ND 10.0 09/25/23 16:293.6
Benzo(a)anthracene ug/L ND 10.0 09/25/23 16:292.7
Benzo(a)pyrene ug/L ND 10.0 09/25/23 16:292.8
Benzo(b)fluoranthene ug/L ND 10.0 09/25/23 16:292.6
Benzo(g,h,i)perylene ug/L ND 10.0 09/25/23 16:292.8
Benzo(k)fluoranthene ug/L ND 10.0 09/25/23 16:292.7
Biphenyl (Diphenyl)ug/L ND 10.0 09/25/23 16:291.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/25/23 16:291.8
bis(2-Chloroethyl) ether ug/L ND 10.0 09/25/23 16:291.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/25/23 16:293.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152817
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265010
Matrix: Water
AnalyzedMDL
Butylbenzylphthalate ug/L ND 10.0 09/25/23 16:293.1
Caprolactam ug/L ND 10.0 09/25/23 16:296.9
Carbazole ug/L ND 10.0 09/25/23 16:292.4
Chrysene ug/L ND 10.0 09/25/23 16:292.8
Di-n-butylphthalate ug/L ND 10.0 09/25/23 16:292.2
Di-n-octylphthalate ug/L ND 10.0 09/25/23 16:293.9
Dibenz(a,h)anthracene ug/L ND 10.0 09/25/23 16:293.0
Dibenzofuran ug/L ND 10.0 09/25/23 16:292.1
Diethylphthalate ug/L ND 10.0 09/25/23 16:292.0
Dimethylphthalate ug/L ND 10.0 09/25/23 16:292.1
Fluoranthene ug/L ND 10.0 09/25/23 16:292.2
Fluorene ug/L ND 10.0 09/25/23 16:292.1
Hexachloro-1,3-butadiene ug/L ND 10.0 09/25/23 16:291.8
Hexachlorobenzene ug/L ND 10.0 09/25/23 16:292.2
Hexachlorocyclopentadiene ug/L ND 10.0 09/25/23 16:291.6
Hexachloroethane ug/L ND 10.0 09/25/23 16:291.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/25/23 16:292.9
Isophorone ug/L ND 10.0 09/25/23 16:291.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/25/23 16:291.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/25/23 16:293.0
Naphthalene ug/L ND 10.0 09/25/23 16:292.1
Nitrobenzene ug/L ND 10.0 09/25/23 16:291.9
Pentachlorophenol ug/L ND 20.0 09/25/23 16:293.8
Phenanthrene ug/L ND 10.0 09/25/23 16:292.0
Phenol ug/L ND 10.0 09/25/23 16:291.4
Pyrene ug/L ND 10.0 09/25/23 16:292.2
2,4,6-Tribromophenol (S)%118 10-164 09/25/23 16:29
2-Fluorobiphenyl (S)%97 10-130 09/25/23 16:29
2-Fluorophenol (S)%66 10-130 09/25/23 16:29
Nitrobenzene-d5 (S)%108 10-138 09/25/23 16:29
Phenol-d6 (S)%56 10-130 09/25/23 16:29
Terphenyl-d14 (S)%141 19-191 09/25/23 16:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152818LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 18.650 37 21-135
2,4,5-Trichlorophenol ug/L 34.950 70 38-147
2,4,6-Trichlorophenol ug/L 24.450 49 34-142
2,4-Dichlorophenol ug/L 21.650 43 36-136
2,4-Dimethylphenol ug/L 21.250 42 38-134
2,4-Dinitrophenol ug/L 152250 61 10-169
2,4-Dinitrotoluene ug/L 35.150 70 44-154
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152818LABORATORY CONTROL SAMPLE:
LCSSpike
2,6-Dinitrotoluene ug/L 29.950 60 44-156
2-Chloronaphthalene ug/L 20.250 40 25-130
2-Chlorophenol ug/L 22.650 45 29-130
2-Methylnaphthalene ug/L 18.450 37 23-130
2-Methylphenol(o-Cresol)ug/L 20.150 40 31-130
2-Nitroaniline ug/L 56.4100 56 39-145
2-Nitrophenol ug/L 21.850 44 29-142
3&4-Methylphenol(m&p Cresol)ug/L 19.950 40 30-130
3,3'-Dichlorobenzidine ug/L 89.0100 89 44-158
3-Nitroaniline ug/L 73.0100 73 45-152
4,6-Dinitro-2-methylphenol ug/L 69.7100 70 39-158
4-Bromophenylphenyl ether ug/L 29.550 59 47-147
4-Chloro-3-methylphenol ug/L 44.0100 44 40-138
4-Chloroaniline ug/L 41.8100 42 35-130
4-Chlorophenylphenyl ether ug/L 25.850 52 36-139
4-Nitroaniline ug/L 87.5100 87 46-157
4-Nitrophenol ug/L 113250 45 17-130
Acenaphthene ug/L 22.550 45 34-135
Acenaphthylene ug/L 21.950 44 35-137
Acetophenone ug/L 21.550 43 30-137
Anthracene ug/L 33.750 67 47-146
Atrazine ug/L 34.850 70 30-130
Benzaldehyde ug/L 23.850 48 17-167
Benzo(a)anthracene ug/L 40.350 81 48-160
Benzo(a)pyrene ug/L 42.050 84 47-165
Benzo(b)fluoranthene ug/L 47.550 95 49-171
Benzo(g,h,i)perylene ug/L 42.950 86 46-166
Benzo(k)fluoranthene ug/L 43.250 86 55-162
Biphenyl (Diphenyl)ug/L 20.250 40 28-130
bis(2-Chloroethoxy)methane ug/L 20.150 40 33-136
bis(2-Chloroethyl) ether ug/L 22.550 45 30-142
bis(2-Ethylhexyl)phthalate ug/L 41.450 83 46-173
Butylbenzylphthalate ug/L 40.150 80 53-169
Caprolactam ug/L 21.350 43 13-130
Carbazole ug/L 39.850 80 48-157
Chrysene ug/L 39.450 79 54-152
Di-n-butylphthalate ug/L 38.050 76 49-161
Di-n-octylphthalate ug/L 40.450 81 50-166
Dibenz(a,h)anthracene ug/L 41.750 83 46-166
Dibenzofuran ug/L 23.250 46 37-136
Diethylphthalate ug/L 34.050 68 45-149
Dimethylphthalate ug/L 29.250 58 43-145
Fluoranthene ug/L 39.350 79 50-153
Fluorene ug/L 25.550 51 42-142
Hexachloro-1,3-butadiene ug/L 10.350 21 10-130
Hexachlorobenzene ug/L 29.750 59 44-138
Hexachlorocyclopentadiene ug/L 15.550 31 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152818LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloroethane ug/L 6.8J50 14 10-130
Indeno(1,2,3-cd)pyrene ug/L 40.950 82 46-166
Isophorone ug/L 19.950 40 36-135
N-Nitroso-di-n-propylamine ug/L 23.250 46 33-140
N-Nitrosodiphenylamine ug/L 30.950 62 46-144
Naphthalene ug/L 15.350 31 20-130
Nitrobenzene ug/L 20.050 40 33-133
Pentachlorophenol ug/L 69.5100 70 21-163
Phenanthrene ug/L 33.950 68 47-146
Phenol ug/L 13.350 27 19-130
Pyrene ug/L 38.050 76 53-155
2,4,6-Tribromophenol (S)%68 10-164
2-Fluorobiphenyl (S)%37 10-130
2-Fluorophenol (S)%29 10-130
Nitrobenzene-d5 (S)%36 10-138
Phenol-d6 (S)%24 10-130
Terphenyl-d14 (S)%67 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4152820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-
chloropropane)ug/L 83.3 58 11-14352 11 3083.3ND 48.4 43.5
2,4,5-Trichlorophenol ug/L 83.3 83 10-17080 4 3083.3ND 69.3 66.9
2,4,6-Trichlorophenol ug/L 83.3 60 10-16668 12 3083.3ND 50.4 56.7
2,4-Dichlorophenol ug/L 83.3 74 10-15368 8 3083.3ND 61.7 56.9
2,4-Dimethylphenol ug/L 83.3 77 20-14765 17 3083.3ND 64.6 54.4
2,4-Dinitrophenol ug/L M1417010-17265 30417NDND 269
2,4-Dinitrotoluene ug/L 83.3 89 30-16476 16 3083.3ND 73.9 63.1
2,6-Dinitrotoluene ug/L 83.3 85 31-16373 15 3083.3ND 70.5 60.8
2-Chloronaphthalene ug/L 83.3 60 15-13449 20 3083.3ND 50.4 41.0
2-Chlorophenol ug/L 83.3 74 10-13962 17 3083.3ND 61.7 52.0
2-Methylnaphthalene ug/L 83.3 55 12-13057 2 3083.3ND 46.1 47.2
2-Methylphenol(o-Cresol) ug/L 83.3 67 19-13256 17 3083.3ND 55.5 46.9
2-Nitroaniline ug/L 167 78 23-15473 7 30167ND131 121
2-Nitrophenol ug/L 83.3 82 10-15967 20 3083.3ND 68.4 56.0
3&4-Methylphenol(m&p
Cresol)ug/L 83.3 64 13-13654 17 3083.3ND 53.6 45.4
3,3'-Dichlorobenzidine ug/L R116711210-17881 32 30167ND187 135
3-Nitroaniline ug/L 167 55 20-16645 20 30167ND92.2 75.1
4,6-Dinitro-2-methylphenol ug/L R11673210-18769 73 30167ND53.9 116
4-Bromophenylphenyl ether ug/L 83.3 81 31-15763 25 3083.3ND 67.3 52.6
4-Chloro-3-methylphenol ug/L 167 74 27-14666 10 30167ND123 111
4-Chloroaniline ug/L M11671313-1439 30167ND22.4J 15.4J
4-Chlorophenylphenyl ether ug/L 83.3 75 23-14959 24 3083.3ND 62.2 49.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4152820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Nitroaniline ug/L 167 99 24-17178 24 30167ND166 130
4-Nitrophenol ug/L 417 18 10-13047 30417ND76.1J 195
Acenaphthene ug/L 83.3 69 21-14754 24 3083.3ND 57.2 44.9
Acenaphthylene ug/L 83.3 68 19-15054 23 3083.3ND 56.9 45.2
Acetophenone ug/L 83.3 73 22-14562 17 3083.3ND 61.1 51.3
Anthracene ug/L 83.3 88 36-15267 27 3083.3ND 73.6 55.9
Atrazine ug/L 83.3 92 18-17388 4 3083.3ND 76.4 73.1
Benzaldehyde ug/L 83.3 75 16-16374 1 3083.3ND 62.2 61.4
Benzo(a)anthracene ug/L R183.3 105 42-16376 32 3083.3ND 87.5 63.4
Benzo(a)pyrene ug/L 83.3 108 40-16980 30 3083.3ND 90.1 66.7
Benzo(b)fluoranthene ug/L 83.3 119 40-17787 30 3083.3ND 98.9 72.7
Benzo(g,h,i)perylene ug/L 83.3 105 38-17482 25 3083.3ND 87.2 68.1
Benzo(k)fluoranthene ug/L R183.3 115 41-17180 36 3083.3ND 96.2 66.7
Biphenyl (Diphenyl)ug/L 83.3 62 14-13750 22 3083.3ND 51.7 41.5
bis(2-
Chloroethoxy)methane
ug/L 83.3 71 19-14661 16 3083.3ND 59.2 50.5
bis(2-Chloroethyl) ether ug/L 83.3 64 19-15155 14 3083.3ND 53.1 46.0
bis(2-Ethylhexyl)phthalate ug/L 83.3 113 42-16886 27 3083.3ND 94.5 71.9
Butylbenzylphthalate ug/L 83.3 109 42-17782 29 3083.3ND 91.0 68.1
Caprolactam ug/L 83.3 36 10-13032 11 3083.3ND 29.7 26.7
Carbazole ug/L 83.3 105 38-16479 28 3083.3ND 87.2 65.4
Chrysene ug/L 83.3 102 43-15976 30 3083.3ND 85.0 63.0
Di-n-butylphthalate ug/L 83.3 103 42-16077 29 3083.3ND 85.8 64.2
Di-n-octylphthalate ug/L 83.3 114 42-17192 22 3083.3ND 95.3 76.7
Dibenz(a,h)anthracene ug/L 83.3 105 40-17179 28 3083.3ND 87.1 66.1
Dibenzofuran ug/L 83.3 67 23-14753 23 3083.3ND 55.9 44.2
Diethylphthalate ug/L 83.3 88 33-15773 18 3083.3ND 73.1 60.9
Dimethylphthalate ug/L 83.3 77 27-15467 14 3083.3ND 64.0 55.9
Fluoranthene ug/L 83.3 103 42-15776 30 3083.3ND 85.7 63.6
Fluorene ug/L 83.3 73 25-15559 20 3083.3ND 60.5 49.3
Hexachloro-1,3-butadiene ug/L R183.3 22 10-13042 62 3083.3ND 18.7 35.4
Hexachlorobenzene ug/L 83.3 82 32-14566 21 3083.3ND 68.5 55.3
Hexachlorocyclopentadiene ug/L 83.3 42 10-13046 9 3083.3ND 35.3 38.7
Hexachloroethane ug/L 83.3 17 10-13034 3083.3ND 13.9J 28.6
Indeno(1,2,3-cd)pyrene ug/L 83.3 101 39-17477 27 3083.3ND 84.1 64.2
Isophorone ug/L 83.3 75 19-14662 18 3083.3ND 62.1 52.0
N-Nitroso-di-n-propylamine ug/L 83.3 78 20-15069 12 3083.3ND 64.6 57.2
N-Nitrosodiphenylamine ug/L 83.3 83 33-14966 23 3083.3ND 69.3 54.8
Naphthalene ug/L 83.3 44 10-12853 19 3083.3ND 36.4 44.1
Nitrobenzene ug/L 83.3 70 19-14557 21 3083.3ND 58.4 47.3
Pentachlorophenol ug/L 167 52 10-18865 22 30167ND87.3 109
Phenanthrene ug/L 83.3 87 38-15065 29 3083.3ND 72.7 54.6
Phenol ug/L 83.3 45 10-13035 26 3083.3ND 37.9 29.1
Pyrene ug/L 83.3 98 42-16374 29 3083.3ND 81.9 61.3
2,4,6-Tribromophenol (S) %82 10-16474
2-Fluorobiphenyl (S)%60 10-13051
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4152820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Fluorophenol (S)%46 10-13044
Nitrobenzene-d5 (S)%64 10-13860
Phenol-d6 (S)%43 10-13035
Terphenyl-d14 (S)%85 19-19168
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802402
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689265009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4156396
Associated Lab Samples:92689265009
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 10/01/23 14:221.2
2,4,5-Trichlorophenol ug/L ND 10.0 10/01/23 14:221.4
2,4,6-Trichlorophenol ug/L ND 10.0 10/01/23 14:221.6
2,4-Dichlorophenol ug/L ND 10.0 10/01/23 14:221.4
2,4-Dimethylphenol ug/L ND 10.0 10/01/23 14:221.7
2,4-Dinitrophenol ug/L ND 50.0 10/01/23 14:2226.0
2,4-Dinitrotoluene ug/L ND 10.0 10/01/23 14:221.6
2,6-Dinitrotoluene ug/L ND 10.0 10/01/23 14:221.7
2-Chloronaphthalene ug/L ND 10.0 10/01/23 14:221.7
2-Chlorophenol ug/L ND 10.0 10/01/23 14:221.2
2-Methylnaphthalene ug/L ND 10.0 10/01/23 14:221.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 10/01/23 14:221.9
2-Nitroaniline ug/L ND 20.0 10/01/23 14:223.0
2-Nitrophenol ug/L ND 10.0 10/01/23 14:221.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 10/01/23 14:221.2
3,3'-Dichlorobenzidine ug/L ND 20.0 10/01/23 14:228.1
3-Nitroaniline ug/L ND 20.0 10/01/23 14:223.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 10/01/23 14:227.8
4-Bromophenylphenyl ether ug/L ND 10.0 10/01/23 14:221.8
4-Chloro-3-methylphenol ug/L ND 10.0 10/01/23 14:223.3
4-Chloroaniline ug/L ND 20.0 10/01/23 14:223.6
4-Chlorophenylphenyl ether ug/L ND 10.0 10/01/23 14:222.0
4-Nitroaniline ug/L ND 20.0 10/01/23 14:225.1
4-Nitrophenol ug/L ND 50.0 10/01/23 14:226.6
Acenaphthene ug/L ND 10.0 10/01/23 14:222.0
Acenaphthylene ug/L ND 10.0 10/01/23 14:222.0
Acetophenone ug/L ND 10.0 10/01/23 14:221.5
Anthracene ug/L ND 10.0 10/01/23 14:222.3
Atrazine ug/L ND 10.0 10/01/23 14:223.2
Benzaldehyde ug/L ND 10.0 10/01/23 14:223.6
Benzo(a)anthracene ug/L ND 10.0 10/01/23 14:222.7
Benzo(a)pyrene ug/L ND 10.0 10/01/23 14:222.8
Benzo(b)fluoranthene ug/L ND 10.0 10/01/23 14:222.6
Benzo(g,h,i)perylene ug/L ND 10.0 10/01/23 14:222.8
Benzo(k)fluoranthene ug/L ND 10.0 10/01/23 14:222.7
Biphenyl (Diphenyl)ug/L ND 10.0 10/01/23 14:221.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 10/01/23 14:221.8
bis(2-Chloroethyl) ether ug/L ND 10.0 10/01/23 14:221.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 10/01/23 14:223.7
Butylbenzylphthalate ug/L ND 10.0 10/01/23 14:223.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4156396
Associated Lab Samples:92689265009
Matrix: Water
AnalyzedMDL
Caprolactam ug/L ND 10.0 10/01/23 14:226.9
Carbazole ug/L ND 10.0 10/01/23 14:222.4
Chrysene ug/L ND 10.0 10/01/23 14:222.8
Di-n-butylphthalate ug/L ND 10.0 10/01/23 14:222.2
Di-n-octylphthalate ug/L ND 10.0 10/01/23 14:223.9
Dibenz(a,h)anthracene ug/L ND 10.0 10/01/23 14:223.0
Dibenzofuran ug/L ND 10.0 10/01/23 14:222.1
Diethylphthalate ug/L ND 10.0 10/01/23 14:222.0
Dimethylphthalate ug/L ND 10.0 10/01/23 14:222.1
Fluoranthene ug/L ND 10.0 10/01/23 14:222.2
Fluorene ug/L ND 10.0 10/01/23 14:222.1
Hexachloro-1,3-butadiene ug/L ND 10.0 10/01/23 14:221.8
Hexachlorobenzene ug/L ND 10.0 10/01/23 14:222.2
Hexachlorocyclopentadiene ug/L ND 10.0 10/01/23 14:221.6
Hexachloroethane ug/L ND 10.0 10/01/23 14:221.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 10/01/23 14:222.9
Isophorone ug/L ND 10.0 10/01/23 14:221.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 10/01/23 14:221.3
N-Nitrosodiphenylamine ug/L ND 10.0 10/01/23 14:223.0
Naphthalene ug/L ND 10.0 10/01/23 14:222.1
Nitrobenzene ug/L ND 10.0 10/01/23 14:221.9
Pentachlorophenol ug/L ND 20.0 10/01/23 14:223.8
Phenanthrene ug/L ND 10.0 10/01/23 14:222.0
Phenol ug/L ND 10.0 10/01/23 14:221.4
Pyrene ug/L ND 10.0 10/01/23 14:222.2
2,4,6-Tribromophenol (S)%150 10-164 10/01/23 14:22
2-Fluorobiphenyl (S)%128 10-130 10/01/23 14:22
2-Fluorophenol (S)%93 10-130 10/01/23 14:22
Nitrobenzene-d5 (S)%137 10-138 10/01/23 14:22
Phenol-d6 (S)%70 10-130 10/01/23 14:22
Terphenyl-d14 (S)%138 19-191 10/01/23 14:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4156397LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 27.250 54 21-135
2,4,5-Trichlorophenol ug/L 41.350 83 38-147
2,4,6-Trichlorophenol ug/L 39.250 78 34-142
2,4-Dichlorophenol ug/L 36.850 74 36-136
2,4-Dimethylphenol ug/L 35.050 70 38-134
2,4-Dinitrophenol ug/L 210250 84 10-169
2,4-Dinitrotoluene ug/L 44.250 88 44-154
2,6-Dinitrotoluene ug/L 39.950 80 44-156
2-Chloronaphthalene ug/L 31.750 63 25-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4156397LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 32.550 65 29-130
2-Methylnaphthalene ug/L 30.650 61 23-130
2-Methylphenol(o-Cresol)ug/L 29.050 58 31-130
2-Nitroaniline ug/L 77.8100 78 39-145
2-Nitrophenol ug/L 36.050 72 29-142
3&4-Methylphenol(m&p Cresol)ug/L 31.850 64 30-130
3,3'-Dichlorobenzidine ug/L 112100 112 44-158
3-Nitroaniline ug/L 84.7100 85 45-152
4,6-Dinitro-2-methylphenol ug/L 94.1100 94 39-158
4-Bromophenylphenyl ether ug/L 39.650 79 47-147
4-Chloro-3-methylphenol ug/L 69.6100 70 40-138
4-Chloroaniline ug/L 69.2100 69 35-130
4-Chlorophenylphenyl ether ug/L 37.850 76 36-139
4-Nitroaniline ug/L 101100 101 46-157
4-Nitrophenol ug/L 140250 56 17-130
Acenaphthene ug/L 33.350 67 34-135
Acenaphthylene ug/L 33.550 67 35-137
Acetophenone ug/L 31.850 64 30-137
Anthracene ug/L 40.750 81 47-146
Atrazine ug/L 37.350 75 30-130
Benzaldehyde ug/L 31.250 62 17-167
Benzo(a)anthracene ug/L 52.050 104 48-160
Benzo(a)pyrene ug/L 52.050 104 47-165
Benzo(b)fluoranthene ug/L 60.450 121 49-171
Benzo(g,h,i)perylene ug/L 49.550 99 46-166
Benzo(k)fluoranthene ug/L 55.050 110 55-162
Biphenyl (Diphenyl)ug/L 31.750 63 28-130
bis(2-Chloroethoxy)methane ug/L 32.650 65 33-136
bis(2-Chloroethyl) ether ug/L 29.950 60 30-142
bis(2-Ethylhexyl)phthalate ug/L 62.650 125 46-173
Butylbenzylphthalate ug/L 54.950 110 53-169
Caprolactam ug/L 23.750 47 13-130
Carbazole ug/L 48.450 97 48-157
Chrysene ug/L 48.350 97 54-152
Di-n-butylphthalate ug/L 50.950 102 49-161
Di-n-octylphthalate ug/L 59.250 118 50-166
Dibenz(a,h)anthracene ug/L 50.150 100 46-166
Dibenzofuran ug/L 34.250 68 37-136
Diethylphthalate ug/L 42.750 85 45-149
Dimethylphthalate ug/L 37.450 75 43-145
Fluoranthene ug/L 47.750 95 50-153
Fluorene ug/L 35.950 72 42-142
Hexachloro-1,3-butadiene ug/L 23.150 46 10-130
Hexachlorobenzene ug/L 38.850 78 44-138
Hexachlorocyclopentadiene ug/L 30.650 61 10-130
Hexachloroethane ug/L 18.650 37 10-130
Indeno(1,2,3-cd)pyrene ug/L 49.150 98 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4156397LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 34.850 70 36-135
N-Nitroso-di-n-propylamine ug/L 37.650 75 33-140
N-Nitrosodiphenylamine ug/L 38.850 78 46-144
Naphthalene ug/L 27.050 54 20-130
Nitrobenzene ug/L 31.050 62 33-133
Pentachlorophenol ug/L 89.8100 90 21-163
Phenanthrene ug/L 40.650 81 47-146
Phenol ug/L 19.750 39 19-130
Pyrene ug/L 50.050 100 53-155
2,4,6-Tribromophenol (S)%112 10-164
2-Fluorobiphenyl (S)%76 10-130
2-Fluorophenol (S)%54 10-130
Nitrobenzene-d5 (S)%77 10-138
Phenol-d6 (S)%42 10-130
Terphenyl-d14 (S)%103 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4156398MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35829045003
4156399
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-
chloropropane)ug/L 50 64 11-14357 12 30501.2U 32.2 28.6
2,4,5-Trichlorophenol ug/L 50 94 10-17088 7 30501.4U 47.2 43.9
2,4,6-Trichlorophenol ug/L 50 89 10-16680 11 30501.6U 44.6 39.8
2,4-Dichlorophenol ug/L 50 86 10-15377 10 30501.4U 42.9 38.6
2,4-Dimethylphenol ug/L 50 85 20-14774 14 30501.7U 42.6 37.2
2,4-Dinitrophenol ug/L 250 43 10-17236 17 3025026.0U 108 90.6
2,4-Dinitrotoluene ug/L 50 87 30-16481 8 30501.6U 43.5 40.3
2,6-Dinitrotoluene ug/L 50 87 31-16376 13 30501.7U 43.3 38.2
2-Chloronaphthalene ug/L 50 75 15-13469 9 30501.7U 37.6 34.5
2-Chlorophenol ug/L 50 80 10-13970 13 30501.2U 40.2 35.2
2-Methylnaphthalene ug/L 50 75 12-13068 9 30501.9J 39.4 36.0
2-Methylphenol(o-Cresol) ug/L 50 71 19-13263 12 30501.9U 35.6 31.4
2-Nitroaniline ug/L 100 84 23-15477 9 301003.0U 83.9 77.1
2-Nitrophenol ug/L 50 88 10-15977 14 30501.4U 44.0 38.3
3&4-Methylphenol(m&p
Cresol)
ug/L 50 79 13-13669 14 30501.2U 39.6 34.4
3,3'-Dichlorobenzidine ug/L 100 103 10-178105 2 301008.1U 103 105
3-Nitroaniline ug/L 100 89 20-16682 9 301003.8U 89.2 81.8
4,6-Dinitro-2-methylphenol ug/L 100 83 10-18772 15 301007.8U 82.9 71.6
4-Bromophenylphenyl ether ug/L 50 86 31-15778 10 30501.8U 43.0 38.9
4-Chloro-3-methylphenol ug/L 100 86 27-14678 9 301003.3U 85.7 78.4
4-Chloroaniline ug/L 100 83 13-14376 9 301003.6U 83.1 75.6
4-Chlorophenylphenyl ether ug/L 50 82 23-14973 11 30502.0U 40.9 36.7
4-Nitroaniline ug/L 100 97 24-17196 0 301005.1U 96.5 96.2
4-Nitrophenol ug/L 250 49 10-13044 11 302506.6U 123 110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4156398MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35829045003
4156399
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L 50 76 21-14769 9 30502.0U 37.9 34.7
Acenaphthylene ug/L 50 76 19-15070 9 30502.0U 38.2 35.0
Acetophenone ug/L 50 74 22-14565 13 30501.5U 37.0 32.6
Anthracene ug/L 50 83 36-15279 4 30502.3U 41.3 39.5
Atrazine ug/L 50 103 18-173106 3 30503.2U 51.4 53.2
Benzaldehyde ug/L 50 65 16-16364 1 30503.6U 32.4 32.1
Benzo(a)anthracene ug/L 50 95 42-16394 1 30502.7U 47.6 47.1
Benzo(a)pyrene ug/L 50 100 40-16995 5 30502.8U 49.8 47.3
Benzo(b)fluoranthene ug/L 50 114 40-177104 9 30502.6U 57.1 52.1
Benzo(g,h,i)perylene ug/L 50 92 38-17491 1 30502.8U 46.1 45.6
Benzo(k)fluoranthene ug/L 50 102 41-17191 11 30502.7U 50.8 45.4
Biphenyl (Diphenyl)ug/L 50 76 14-13769 10 30501.8U 38.0 34.3
bis(2-
Chloroethoxy)methane ug/L 50 76 19-14668 11 30501.8U 37.9 33.9
bis(2-Chloroethyl) ether ug/L 50 72 19-15163 13 30501.9U 35.8 31.6
bis(2-Ethylhexyl)phthalate ug/L 50 113 42-168109 4 30503.7U 58.4 56.2
Butylbenzylphthalate ug/L 50 108 42-177105 3 30503.1U 53.8 52.4
Caprolactam ug/L 50 47 10-13044 7 30506.9U 23.4 21.9
Carbazole ug/L 50 92 38-16491 1 30502.4U 45.8 45.4
Chrysene ug/L 50 91 43-15990 1 30502.8U 45.6 45.0
Di-n-butylphthalate ug/L 50 96 42-16094 2 30502.2U 48.0 47.0
Di-n-octylphthalate ug/L 50 114 42-171112 2 30503.9U 57.0 56.1
Dibenz(a,h)anthracene ug/L 50 95 40-17192 3 30503.0U 47.4 46.0
Dibenzofuran ug/L 50 73 23-14766 10 30502.1U 36.7 33.2
Diethylphthalate ug/L 50 86 33-15779 8 30502.0U 43.0 39.5
Dimethylphthalate ug/L 50 78 27-15471 11 30502.1U 39.2 35.3
Fluoranthene ug/L 50 89 42-15789 0 30502.2U 44.6 44.4
Fluorene ug/L 50 77 25-15570 10 30502.1U 38.3 34.8
Hexachloro-1,3-butadiene ug/L 50 54 10-13059 9 30501.8U 27.0 29.7
Hexachlorobenzene ug/L 50 86 32-14578 10 30502.2U 42.9 38.8
Hexachlorocyclopentadiene ug/L 50 66 10-13065 1 30501.6U 33.0 32.6
Hexachloroethane ug/L R1503110-13045 38 30501.4U 15.3 22.4
Indeno(1,2,3-cd)pyrene ug/L 50 91 39-17489 2 30502.9U 45.5 44.7
Isophorone ug/L 50 82 19-14672 14 30501.7U 41.1 35.8
N-Nitroso-di-n-propylamine ug/L 50 88 20-15077 14 30501.3U 44.1 38.3
N-Nitrosodiphenylamine ug/L 50 87 33-14978 11 30503.0U 43.3 39.0
Naphthalene ug/L 50 64 10-12862 4 30502.1U 32.2 30.9
Nitrobenzene ug/L 50 75 19-14567 11 30501.9U 37.6 33.6
Pentachlorophenol ug/L 100 87 10-18882 6 301003.8U 86.9 82.0
Phenanthrene ug/L 50 83 38-15078 6 30502.0U 41.3 38.9
Phenol ug/L 50 53 10-13045 16 30501.4U 26.6 22.6
Pyrene ug/L 50 95 42-16392 3 30502.2U 47.5 46.2
2,4,6-Tribromophenol (S) %116 10-164114
2-Fluorobiphenyl (S)%81 10-13081
2-Fluorophenol (S)%64 10-13058
Nitrobenzene-d5 (S)%86 10-13879
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4156398MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35829045003
4156399
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%53 10-13048
Terphenyl-d14 (S)%90 19-19191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
802640
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689265001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4157372
Associated Lab Samples:92689265001
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 09/28/23 14:025.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157373LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 48.350 97 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4157374LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 48.350 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4158201MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92688804004
4158202
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M15013480-120-409 8 255033203390 3110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4158976MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265001
4158977
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1505580-12047 6 255037.1 64.5 60.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803715
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007, 92689265008,
92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4162457
Associated Lab Samples: 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007, 92689265008,
92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Alkalinity, Total as CaCO3 mg/L ND 5.0 10/03/23 13:415.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4162458LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 50.650 101 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4162459LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.950 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4162460MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265009
4162461
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 102 80-120102 1 255010.9 62.1 61.7
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4162462MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4162463
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 103 80-120103 0 255010.1 61.5 61.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801579
SM 2540C-2015
SM 2540C-2015
2540C Total Dissolved Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152167
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Total Dissolved Solids mg/L ND 25.0 09/23/23 11:3625.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152168LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 260250 104 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689410001
4152169SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 520 1 25514
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92689265010
4152170SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 26.0 25ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801381
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150965
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Chloride mg/L ND 1.0 09/22/23 16:290.60
Sulfate mg/L ND 1.0 09/22/23 16:290.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150966LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 53.150 106 90-110
Sulfate mg/L 53.450 107 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150967MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689410005
4150968
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L 50 103 90-110104 1 1050ND51.3 52.0
Sulfate mg/L 50 103 90-110104 1 1050ND51.4 52.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150969MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4150970
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L 50 103 90-110105 2 10501.2 52.7 53.7
Sulfate mg/L 50 103 90-110105 2 10501.4 53.1 54.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804835
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4168110
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008
Matrix: Water
AnalyzedMDL
Nitrogen, Ammonia mg/L ND 0.10 10/10/23 00:530.031
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4168111LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.15 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4168112MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92691698001
4168113
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 101 90-110101 0 1050.19 5.2 5.2
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4168114MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690872001
4168115
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 97 90-11096 1 105ND4.9 4.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804836
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4168116
Associated Lab Samples:92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Nitrogen, Ammonia mg/L ND 0.10 10/10/23 02:230.031
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4168117LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.05 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4168118MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265009
4168119
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 99 90-11099 0 105ND5.0 4.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4168120MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4168121
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 97 90-11097 0 105ND4.9 4.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
805041
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4168888
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Nitrogen, Kjeldahl, Total mg/L ND 0.50 10/10/23 04:150.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4168889LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 10.210 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4168890MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265009
4168891
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 105 90-110108 3 1010ND10.6 10.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4168892MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4168893
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 108 90-110108 0 1010ND10.9 10.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 108 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801986
EPA 420.4 Rev 1.0 1993
EPA 420.4 Rev 1.0 1993
420.4 Phenolics
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4154253
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Phenolics, Total Recoverable mg/L ND 0.020 09/27/23 14:440.0076
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4154254LABORATORY CONTROL SAMPLE:
LCSSpike
Phenolics, Total Recoverable mg/L 0.0490.05 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4154255MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35828659004
4154256
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenolics, Total
Recoverable mg/L M10.05 -55 90-110-57 1 100.050.11 0.083 0.082
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4154257MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4154258
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenolics, Total
Recoverable mg/L 0.05 98 90-11091 7 100.05ND 0.049 0.046
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801300
SM 4500-P E-2011
SM 4500-P E-2011
SM4500P-E Phosphorus, Ortho
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4150760
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Orthophosphate as P mg/L ND 0.050 09/22/23 04:300.012
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4150761LABORATORY CONTROL SAMPLE:
LCSSpike
Orthophosphate as P mg/L 0.240.25 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150762MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689224001
4150763
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Orthophosphate as P mg/L M10.25 84 90-11086 1 100.250.36 0.57 0.58
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4150764MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4150765
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Orthophosphate as P mg/L M10.25 86 90-11087 1 100.25ND 0.22 0.22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 120
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804240
SM 5220D-2011
SM 5220D-2011
5220D COD
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4165189
Associated Lab Samples: 92689265001, 92689265002, 92689265003, 92689265004, 92689265005, 92689265006, 92689265007,
92689265008, 92689265009, 92689265010
Matrix: Water
AnalyzedMDL
Chemical Oxygen Demand mg/L ND 25.0 10/06/23 00:1612.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4165190LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand mg/L 779750 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4165191MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92689265010
4165192
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L 100 100 90-110102 2 3100ND106 108
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4165193MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690267001
4165194
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L M110011490-110112 2 310039.3 153 151
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 120
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 120
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92689265001 802098SWDOWNWS-092023 SM 2120B-2011
92689265002 802098SWDOWNH-092023 SM 2120B-2011
92689265003 802098SEEP02WG-092023 SM 2120B-2011
92689265004 802098SW01-00-WS-092023 SM 2120B-2011
92689265005 802098SW01-02-WS-092023 SM 2120B-2011
92689265006 802098SW01-05-WS-092023 SM 2120B-2011
92689265007 802098SW01-10-WS-092023 SM 2120B-2011
92689265008 802098SEEP01-WG-092023 SM 2120B-2011
92689265009 802098SW02-WS-092023 SM 2120B-2011
92689265010 802098SWUP-WS-092023 SM 2120B-2011
92689265001 954588 954644SWDOWNWS-092023 EPA 200.7 EPA 200.7
92689265002 954588 954644SWDOWNH-092023 EPA 200.7 EPA 200.7
92689265003 954588 954644SEEP02WG-092023 EPA 200.7 EPA 200.7
92689265004 954588 954644SW01-00-WS-092023 EPA 200.7 EPA 200.7
92689265005 954588 954644SW01-02-WS-092023 EPA 200.7 EPA 200.7
92689265006 954588 954644SW01-05-WS-092023 EPA 200.7 EPA 200.7
92689265007 954588 954644SW01-10-WS-092023 EPA 200.7 EPA 200.7
92689265008 954588 954644SEEP01-WG-092023 EPA 200.7 EPA 200.7
92689265009 954588 954644SW02-WS-092023 EPA 200.7 EPA 200.7
92689265010 954932 954967SWUP-WS-092023 EPA 200.7 EPA 200.7
92689265001 954936 954968SWDOWNWS-092023 EPA 200.7 EPA 200.7
92689265002 954936 954968SWDOWNH-092023 EPA 200.7 EPA 200.7
92689265003 954936 954968SEEP02WG-092023 EPA 200.7 EPA 200.7
92689265004 954936 954968SW01-00-WS-092023 EPA 200.7 EPA 200.7
92689265005 954936 954968SW01-02-WS-092023 EPA 200.7 EPA 200.7
92689265006 954936 954968SW01-05-WS-092023 EPA 200.7 EPA 200.7
92689265007 954936 954968SW01-10-WS-092023 EPA 200.7 EPA 200.7
92689265008 954936 954968SEEP01-WG-092023 EPA 200.7 EPA 200.7
92689265009 954936 954968SW02-WS-092023 EPA 200.7 EPA 200.7
92689265010 954936 954968SWUP-WS-092023 EPA 200.7 EPA 200.7
92689265001 955302 955685SWDOWNWS-092023 EPA 245.1 EPA 245.1
92689265002 955302 955685SWDOWNH-092023 EPA 245.1 EPA 245.1
92689265003 955302 955685SEEP02WG-092023 EPA 245.1 EPA 245.1
92689265004 955302 955685SW01-00-WS-092023 EPA 245.1 EPA 245.1
92689265005 955302 955685SW01-02-WS-092023 EPA 245.1 EPA 245.1
92689265006 955302 955685SW01-05-WS-092023 EPA 245.1 EPA 245.1
92689265007 955302 955685SW01-10-WS-092023 EPA 245.1 EPA 245.1
92689265008 955302 955685SEEP01-WG-092023 EPA 245.1 EPA 245.1
92689265009 955302 955685SW02-WS-092023 EPA 245.1 EPA 245.1
92689265010 955302 955685SWUP-WS-092023 EPA 245.1 EPA 245.1
92689265001 956743 956746SWDOWNWS-092023 EPA 245.1 EPA 245.1
92689265002 956743 956746SWDOWNH-092023 EPA 245.1 EPA 245.1
92689265003 956743 956746SEEP02WG-092023 EPA 245.1 EPA 245.1
92689265004 956743 956746SW01-00-WS-092023 EPA 245.1 EPA 245.1
92689265005 956743 956746SW01-02-WS-092023 EPA 245.1 EPA 245.1
92689265006 956743 956746SW01-05-WS-092023 EPA 245.1 EPA 245.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 120
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92689265007 956743 956746SW01-10-WS-092023 EPA 245.1 EPA 245.1
92689265008 956743 956746SEEP01-WG-092023 EPA 245.1 EPA 245.1
92689265009 956743 956746SW02-WS-092023 EPA 245.1 EPA 245.1
92689265010 956743 956746SWUP-WS-092023 EPA 245.1 EPA 245.1
92689265001 801703 801890SWDOWNWS-092023 EPA 3510C EPA 8270E
92689265002 801703 801890SWDOWNH-092023 EPA 3510C EPA 8270E
92689265003 801703 801890SEEP02WG-092023 EPA 3510C EPA 8270E
92689265004 801703 801890SW01-00-WS-092023 EPA 3510C EPA 8270E
92689265005 801703 801890SW01-02-WS-092023 EPA 3510C EPA 8270E
92689265006 801703 801890SW01-05-WS-092023 EPA 3510C EPA 8270E
92689265007 801703 801890SW01-10-WS-092023 EPA 3510C EPA 8270E
92689265008 801703 801890SEEP01-WG-092023 EPA 3510C EPA 8270E
92689265009 802402 802554SW02-WS-092023 EPA 3510C EPA 8270E
92689265010 801703 801890SWUP-WS-092023 EPA 3510C EPA 8270E
92689265001 803106SWDOWNWS-092023 EPA 8260D
92689265002 803103SWDOWNH-092023 EPA 8260D
92689265003 803314SEEP02WG-092023 EPA 8260D
92689265004 803103SW01-00-WS-092023 EPA 8260D
92689265005 802723SW01-02-WS-092023 EPA 8260D
92689265006 802723SW01-05-WS-092023 EPA 8260D
92689265007 802723SW01-10-WS-092023 EPA 8260D
92689265008 803314SEEP01-WG-092023 EPA 8260D
92689265009 802723SW02-WS-092023 EPA 8260D
92689265010 802723SWUP-WS-092023 EPA 8260D
92689265001 802640SWDOWNWS-092023 SM 2320B-2011
92689265002 803715SWDOWNH-092023 SM 2320B-2011
92689265003 803715SEEP02WG-092023 SM 2320B-2011
92689265004 803715SW01-00-WS-092023 SM 2320B-2011
92689265005 803715SW01-02-WS-092023 SM 2320B-2011
92689265006 803715SW01-05-WS-092023 SM 2320B-2011
92689265007 803715SW01-10-WS-092023 SM 2320B-2011
92689265008 803715SEEP01-WG-092023 SM 2320B-2011
92689265009 803715SW02-WS-092023 SM 2320B-2011
92689265010 803715SWUP-WS-092023 SM 2320B-2011
92689265001 801579SWDOWNWS-092023 SM 2540C-2015
92689265002 801579SWDOWNH-092023 SM 2540C-2015
92689265003 801579SEEP02WG-092023 SM 2540C-2015
92689265004 801579SW01-00-WS-092023 SM 2540C-2015
92689265005 801579SW01-02-WS-092023 SM 2540C-2015
92689265006 801579SW01-05-WS-092023 SM 2540C-2015
92689265007 801579SW01-10-WS-092023 SM 2540C-2015
92689265008 801579SEEP01-WG-092023 SM 2540C-2015
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 120
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92689265009 801579SW02-WS-092023 SM 2540C-2015
92689265010 801579SWUP-WS-092023 SM 2540C-2015
92689265001 801381SWDOWNWS-092023 EPA 300.0 Rev 2.1 1993
92689265002 801381SWDOWNH-092023 EPA 300.0 Rev 2.1 1993
92689265003 801381SEEP02WG-092023 EPA 300.0 Rev 2.1 1993
92689265004 801381SW01-00-WS-092023 EPA 300.0 Rev 2.1 1993
92689265005 801381SW01-02-WS-092023 EPA 300.0 Rev 2.1 1993
92689265006 801381SW01-05-WS-092023 EPA 300.0 Rev 2.1 1993
92689265007 801381SW01-10-WS-092023 EPA 300.0 Rev 2.1 1993
92689265008 801381SEEP01-WG-092023 EPA 300.0 Rev 2.1 1993
92689265009 801381SW02-WS-092023 EPA 300.0 Rev 2.1 1993
92689265010 801381SWUP-WS-092023 EPA 300.0 Rev 2.1 1993
92689265001 804835SWDOWNWS-092023 EPA 350.1 Rev 2.0 1993
92689265002 804835SWDOWNH-092023 EPA 350.1 Rev 2.0 1993
92689265003 804835SEEP02WG-092023 EPA 350.1 Rev 2.0 1993
92689265004 804835SW01-00-WS-092023 EPA 350.1 Rev 2.0 1993
92689265005 804835SW01-02-WS-092023 EPA 350.1 Rev 2.0 1993
92689265006 804835SW01-05-WS-092023 EPA 350.1 Rev 2.0 1993
92689265007 804835SW01-10-WS-092023 EPA 350.1 Rev 2.0 1993
92689265008 804835SEEP01-WG-092023 EPA 350.1 Rev 2.0 1993
92689265009 804836SW02-WS-092023 EPA 350.1 Rev 2.0 1993
92689265010 804836SWUP-WS-092023 EPA 350.1 Rev 2.0 1993
92689265001 805041 805141SWDOWNWS-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265002 805041 805141SWDOWNH-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265003 805041 805141SEEP02WG-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265004 805041 805141SW01-00-WS-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265005 805041 805141SW01-02-WS-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265006 805041 805141SW01-05-WS-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265007 805041 805141SW01-10-WS-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265008 805041 805141SEEP01-WG-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265009 805041 805141SW02-WS-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265010 805041 805141SWUP-WS-092023 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92689265001 801986 802387SWDOWNWS-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265002 801986 802387SWDOWNH-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265003 801986 802387SEEP02WG-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265004 801986 802387SW01-00-WS-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265005 801986 802387SW01-02-WS-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265006 801986 802387SW01-05-WS-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265007 801986 802387SW01-10-WS-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265008 801986 802387SEEP01-WG-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265009 801986 802387SW02-WS-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265010 801986 802387SWUP-WS-092023 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92689265001 801300SWDOWNWS-092023 SM 4500-P E-2011
92689265002 801300SWDOWNH-092023 SM 4500-P E-2011
92689265003 801300SEEP02WG-092023 SM 4500-P E-2011
92689265004 801300SW01-00-WS-092023 SM 4500-P E-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 120
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92689265
Pactiv Evergreen SW/Seep
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92689265005 801300SW01-02-WS-092023 SM 4500-P E-2011
92689265006 801300SW01-05-WS-092023 SM 4500-P E-2011
92689265007 801300SW01-10-WS-092023 SM 4500-P E-2011
92689265008 801300SEEP01-WG-092023 SM 4500-P E-2011
92689265009 801300SW02-WS-092023 SM 4500-P E-2011
92689265010 801300SWUP-WS-092023 SM 4500-P E-2011
92689265001 804240 804541SWDOWNWS-092023 SM 5220D-2011 SM 5220D-2011
92689265002 804240 804541SWDOWNH-092023 SM 5220D-2011 SM 5220D-2011
92689265003 804240 804541SEEP02WG-092023 SM 5220D-2011 SM 5220D-2011
92689265004 804240 804541SW01-00-WS-092023 SM 5220D-2011 SM 5220D-2011
92689265005 804240 804541SW01-02-WS-092023 SM 5220D-2011 SM 5220D-2011
92689265006 804240 804541SW01-05-WS-092023 SM 5220D-2011 SM 5220D-2011
92689265007 804240 804541SW01-10-WS-092023 SM 5220D-2011 SM 5220D-2011
92689265008 804240 804541SEEP01-WG-092023 SM 5220D-2011 SM 5220D-2011
92689265009 804240 804541SW02-WS-092023 SM 5220D-2011 SM 5220D-2011
92689265010 804240 804541SWUP-WS-092023 SM 5220D-2011 SM 5220D-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/10/2023 05:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 116 of 120
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Page 120 of 120
#=CL#
October 19, 2023
LIMS USE: FR - CHRISTINA
LIMS OBJECT ID: 92690981
92690981
Project:
Pace Project No.:
RE:
Christina Ashdown
ENSAFE
313 Wingo Way
Mount Pleasant, SC 29464
PACTIV EVERGREEN ADDITIONAL S.
Dear Christina Ashdown:
Enclosed are the analytical results for sample(s) received by the laboratory on October 02, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc: Jennings Kerr, ENSAFE Inc.
Lab, ENSAFE Inc.
David Warren, ENSAFE Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 57
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 57
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Lab ID Sample ID Matrix Date Collected Date Received
92690981001 CBOF-10022023 Water 10/02/23 12:37 10/02/23 15:55
92690981002 CBOF-10022023 DUP Water 10/02/23 12:40 10/02/23 15:55
92690981003 CBUS-10022023 Water 10/02/23 13:35 10/02/23 15:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 57
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92690981001 CBOF-10022023 SM 2120B-2011 2 PASI-EVLG
EPA 200.7 5 PASI-OTMA
EPA 200.7 5 PASI-OTMA
EPA 200.8 16 PASI-OLEC
EPA 200.8 16 PASI-OBSL
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
EPA 9040C 1 PASI-ASMS
ASTM D4239-05 1 PASI-AKQB
92690981002 CBOF-10022023 DUP SM 2120B-2011 2 PASI-EVLG
EPA 200.7 5 PASI-OTMA
EPA 200.7 5 PASI-OTMA
EPA 200.8 16 PASI-OLEC
EPA 200.8 16 PASI-OBSL
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
EPA 9040C 1 PASI-ASMS
ASTM D4239-05 1 PASI-AKQB
92690981003 CBUS-10022023 SM 2120B-2011 2 PASI-EVLG
EPA 200.7 5 PASI-OTMA
EPA 200.7 5 PASI-OTMA
EPA 200.8 16 PASI-OLEC
EPA 200.8 16 PASI-OBSL
EPA 245.1 1 PASI-OJNK
EPA 245.1 1 PASI-OJNK
EPA 8270E 71 PASI-CPKS
EPA 8260D 52 PASI-CJJK
EPA 9040C 1 PASI-ASMS
ASTM D4239-05 1 PASI-AKQB
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 Lab ID: 92690981001 Collected: 10/02/23 12:37 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.1 Std. Units 10/03/23 14:261
True Color 5.0 units 10/03/23 14:265.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Boron 12.9J ug/L 10/09/23 16:19 7440-42-810/09/23 05:4350.0 12.4 1
Calcium 13500 ug/L 10/09/23 16:19 7440-70-210/09/23 05:43500 190 1
Iron 151 ug/L 10/09/23 16:19 7439-89-610/09/23 05:4340.0 25.0 1
Magnesium 4350 ug/L 10/09/23 16:19 7439-95-410/09/23 05:43500 84.0 1
Sodium 24300 ug/L 10/09/23 16:19 7440-23-510/09/23 05:432000 540 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Boron, Dissolved 16.6J ug/L 10/13/23 15:28 7440-42-810/11/23 11:3850.0 12.4 1
Calcium, Dissolved 14200 ug/L 10/13/23 15:28 7440-70-210/11/23 11:38500 190 1
Iron, Dissolved 160 ug/L 10/13/23 15:28 7439-89-610/11/23 11:3840.0 25.0 1
Magnesium, Dissolved 4350 ug/L 10/13/23 15:28 7439-95-410/11/23 11:38500 84.0 1
Sodium, Dissolved 21900 ug/L 10/13/23 15:28 7440-23-510/11/23 11:382000 540 1
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS
Aluminum 41.6 ug/L 10/10/23 00:11 7429-90-510/09/23 05:4310.0 8.6 1
Arsenic ND ug/L 10/10/23 00:11 7440-38-210/09/23 05:431.0 0.50 1
Barium 53.5 ug/L 10/10/23 00:11 7440-39-310/09/23 05:431.0 0.50 1
Beryllium ND ug/L 10/10/23 14:56 7440-41-710/09/23 05:430.10 0.033 1
Cadmium ND ug/L 10/10/23 00:11 7440-43-910/09/23 05:430.10 0.067 1
Chromium ND ug/L 10/10/23 00:11 7440-47-310/09/23 05:431.0 0.50 1
Cobalt ND ug/L 10/10/23 00:11 7440-48-410/09/23 05:431.0 0.24 1
Copper 1.0 ug/L 10/10/23 00:11 7440-50-810/09/23 05:431.0 0.42 1
Lead 2.4 ug/L 10/10/23 00:11 7439-92-110/09/23 05:431.0 0.22 1
Manganese 18.0 ug/L 10/10/23 00:11 7439-96-510/09/23 05:431.0 0.29 1
Molybdenum ND ug/L 10/10/23 00:11 7439-98-710/09/23 05:431.0 0.22 1
Nickel 0.50J ug/L 10/10/23 00:11 7440-02-010/09/23 05:431.0 0.26 1
Selenium 0.29J ug/L 10/10/23 00:11 7782-49-210/09/23 05:432.0 0.20 1
Silver ND ug/L 10/10/23 00:11 7440-22-410/09/23 05:430.50 0.028 1
Thallium ND ug/L 10/10/23 00:11 7440-28-010/09/23 05:431.0 0.11 1
Zinc ND ug/L 10/10/23 00:11 7440-66-610/09/23 05:4310.0 6.7 1
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS, Dissolved
Aluminum, Dissolved 34.9 ug/L 10/13/23 10:29 7429-90-510/11/23 11:3810.0 8.6 1
Arsenic, Dissolved ND ug/L 10/13/23 10:29 7440-38-210/11/23 11:381.0 0.50 1
Barium, Dissolved 50.9 ug/L 10/13/23 10:29 7440-39-310/11/23 11:381.0 0.50 1
Beryllium, Dissolved ND ug/L 10/13/23 10:29 7440-41-710/11/23 11:380.10 0.033 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 Lab ID: 92690981001 Collected: 10/02/23 12:37 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS, Dissolved
Cadmium, Dissolved ND ug/L 10/13/23 10:29 7440-43-910/11/23 11:380.10 0.067 1
Chromium, Dissolved ND ug/L 10/13/23 10:29 7440-47-310/11/23 11:381.0 0.50 1
Cobalt, Dissolved ND ug/L 10/13/23 10:29 7440-48-410/11/23 11:381.0 0.24 1
Copper, Dissolved 1.4 ug/L 10/13/23 10:29 7440-50-810/11/23 11:381.0 0.42 1
Lead, Dissolved 2.2 ug/L 10/13/23 10:29 7439-92-110/11/23 11:381.0 0.22 1
Manganese, Dissolved 16.8 ug/L 10/13/23 10:29 7439-96-510/11/23 11:381.0 0.29 1
Molybdenum, Dissolved ND ug/L 10/13/23 10:29 7439-98-710/11/23 11:381.0 0.22 1
Nickel, Dissolved 0.41J ug/L 10/13/23 10:29 7440-02-010/11/23 11:381.0 0.26 1
Selenium, Dissolved 0.20J ug/L 10/13/23 10:29 7782-49-210/11/23 11:382.0 0.20 1
Silver, Dissolved ND ug/L 10/13/23 10:29 7440-22-410/11/23 11:380.50 0.028 1
Thallium, Dissolved ND ug/L 10/13/23 10:29 7440-28-010/11/23 11:381.0 0.11 1
Zinc, Dissolved ND ug/L 10/13/23 10:29 7440-66-610/11/23 11:3810.0 6.7 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/12/23 10:03 7439-97-610/11/23 10:230.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/16/23 12:33 7439-97-610/12/23 07:120.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 10/06/23 14:09 83-32-910/05/23 12:588.3 1.7 1
Acenaphthylene ND ug/L 10/06/23 14:09 208-96-810/05/23 12:588.3 1.6 1
Acetophenone ND ug/L 10/06/23 14:09 98-86-210/05/23 12:588.3 1.2 1
Anthracene ND ug/L 10/06/23 14:09 120-12-710/05/23 12:588.3 1.9 1
Atrazine ND ug/L 10/06/23 14:09 1912-24-910/05/23 12:588.3 2.6 1
Benzaldehyde ND ug/L 10/06/23 14:09 100-52-710/05/23 12:588.3 3.0 1
Benzo(a)anthracene ND ug/L 10/06/23 14:09 56-55-310/05/23 12:588.3 2.2 1
Benzo(a)pyrene ND ug/L 10/06/23 14:09 50-32-810/05/23 12:588.3 2.3 1
Benzo(b)fluoranthene ND ug/L 10/06/23 14:09 205-99-210/05/23 12:588.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 10/06/23 14:09 191-24-210/05/23 12:588.3 2.4 1
Benzo(k)fluoranthene ND ug/L 10/06/23 14:09 207-08-910/05/23 12:588.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 10/06/23 14:09 92-52-410/05/23 12:588.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 10/06/23 14:09 101-55-310/05/23 12:588.3 1.5 1
Butylbenzylphthalate ND ug/L 10/06/23 14:09 85-68-710/05/23 12:588.3 2.6 1
Caprolactam ND ug/L 10/06/23 14:09 105-60-210/05/23 12:588.3 5.8 1
Carbazole ND ug/L 10/06/23 14:09 86-74-810/05/23 12:588.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 10/06/23 14:09 59-50-710/05/23 12:588.3 2.8 1
4-Chloroaniline ND ug/L 10/06/23 14:09 106-47-810/05/23 12:5816.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 10/06/23 14:09 111-91-110/05/23 12:588.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 10/06/23 14:09 111-44-410/05/23 12:588.3 1.6 1
2-Chloronaphthalene ND ug/L 10/06/23 14:09 91-58-710/05/23 12:588.3 1.4 1
2-Chlorophenol ND ug/L 10/06/23 14:09 95-57-810/05/23 12:588.3 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 Lab ID: 92690981001 Collected: 10/02/23 12:37 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
4-Chlorophenylphenyl ether ND ug/L 10/06/23 14:09 7005-72-310/05/23 12:588.3 1.7 1
Chrysene ND ug/L 10/06/23 14:09 218-01-910/05/23 12:588.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 10/06/23 14:09 53-70-310/05/23 12:588.3 2.5 1
Dibenzofuran ND ug/L 10/06/23 14:09 132-64-910/05/23 12:588.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 10/06/23 14:09 91-94-110/05/23 12:5816.7 6.8 1
2,4-Dichlorophenol ND ug/L 10/06/23 14:09 120-83-210/05/23 12:588.3 1.2 1
Diethylphthalate ND ug/L 10/06/23 14:09 84-66-210/05/23 12:588.3 1.7 1
2,4-Dimethylphenol ND ug/L 10/06/23 14:09 105-67-910/05/23 12:588.3 1.4 1
Dimethylphthalate ND ug/L 10/06/23 14:09 131-11-310/05/23 12:588.3 1.8 1
Di-n-butylphthalate ND ug/L 10/06/23 14:09 84-74-210/05/23 12:588.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 10/06/23 14:09 534-52-110/05/23 12:5816.7 6.5 1
2,4-Dinitrophenol ND ug/L 10/06/23 14:09 51-28-510/05/23 12:5841.7 21.7 1
2,4-Dinitrotoluene ND ug/L 10/06/23 14:09 121-14-210/05/23 12:588.3 1.4 1
2,6-Dinitrotoluene ND ug/L 10/06/23 14:09 606-20-210/05/23 12:588.3 1.4 1
Di-n-octylphthalate ND ug/L 10/06/23 14:09 117-84-010/05/23 12:588.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/06/23 14:09 117-81-710/05/23 12:585.0 3.1 1
Fluoranthene ND ug/L 10/06/23 14:09 206-44-010/05/23 12:588.3 1.8 1
Fluorene ND ug/L 10/06/23 14:09 86-73-710/05/23 12:588.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 10/06/23 14:09 87-68-310/05/23 12:588.3 1.5 1
Hexachlorobenzene ND ug/L 10/06/23 14:09 118-74-110/05/23 12:588.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 10/06/23 14:09 77-47-410/05/23 12:588.3 1.3 1
Hexachloroethane ND ug/L 10/06/23 14:09 67-72-110/05/23 12:588.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/06/23 14:09 193-39-510/05/23 12:588.3 2.4 1
Isophorone ND ug/L 10/06/23 14:09 78-59-110/05/23 12:588.3 1.4 1
2-Methylnaphthalene ND ug/L 10/06/23 14:09 91-57-610/05/23 12:588.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 10/06/23 14:09 95-48-710/05/23 12:588.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/06/23 14:09 15831-10-410/05/23 12:588.3 1.0 1
Naphthalene ND ug/L 10/06/23 14:09 91-20-310/05/23 12:588.3 1.7 1
2-Nitroaniline ND ug/L 10/06/23 14:09 88-74-410/05/23 12:5816.7 2.5 1
3-Nitroaniline ND ug/L 10/06/23 14:09 99-09-210/05/23 12:5816.7 3.1 1
4-Nitroaniline ND ug/L 10/06/23 14:09 100-01-610/05/23 12:5816.7 4.2 1
Nitrobenzene ND ug/L 10/06/23 14:09 98-95-310/05/23 12:588.3 1.6 1
2-Nitrophenol ND ug/L 10/06/23 14:09 88-75-510/05/23 12:588.3 1.2 1
4-Nitrophenol ND ug/L 10/06/23 14:09 100-02-710/05/23 12:5841.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 10/06/23 14:09 621-64-710/05/23 12:588.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 10/06/23 14:09 86-30-610/05/23 12:588.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/06/23 14:09 108-60-110/05/23 12:588.3 0.96 1
Pentachlorophenol ND ug/L 10/06/23 14:09 87-86-510/05/23 12:5816.7 3.1 1
Phenanthrene ND ug/L 10/06/23 14:09 85-01-810/05/23 12:588.3 1.7 1
Phenol ND ug/L 10/06/23 14:09 108-95-210/05/23 12:588.3 1.1 1
Pyrene ND ug/L 10/06/23 14:09 129-00-010/05/23 12:588.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 10/06/23 14:09 95-95-410/05/23 12:588.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 10/06/23 14:09 88-06-210/05/23 12:588.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)90 %10/06/23 14:09 4165-60-010/05/23 12:5810-138 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 Lab ID: 92690981001 Collected: 10/02/23 12:37 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Surrogates
2-Fluorobiphenyl (S)83 %10/06/23 14:09 321-60-810/05/23 12:5810-130 1
Terphenyl-d14 (S)92 %10/06/23 14:09 1718-51-010/05/23 12:5819-191 1
Phenol-d6 (S)43 %10/06/23 14:09 13127-88-310/05/23 12:5810-130 1
2-Fluorophenol (S)62 %10/06/23 14:09 367-12-410/05/23 12:5810-130 1
2,4,6-Tribromophenol (S)103 %10/06/23 14:09 118-79-610/05/23 12:5810-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/09/23 08:49 67-64-125.0 5.1 1
Benzene ND ug/L 10/09/23 08:49 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 10/09/23 08:49 75-27-41.0 0.31 1
Bromoform ND ug/L 10/09/23 08:49 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/09/23 08:49 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/09/23 08:49 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/09/23 08:49 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/09/23 08:49 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/09/23 08:49 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/09/23 08:49 75-00-31.0 0.65 1
Chloroform 0.62J ug/L 10/09/23 08:49 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/09/23 08:49 74-87-31.0 0.54 1
Cyclohexane ND ug/L 10/09/23 08:49 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/23 08:49 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/09/23 08:49 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/23 08:49 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 10/09/23 08:49 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/09/23 08:49 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/09/23 08:49 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/09/23 08:49 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/09/23 08:49 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/09/23 08:49 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/09/23 08:49 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/09/23 08:49 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/09/23 08:49 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/09/23 08:49 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/09/23 08:49 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/09/23 08:49 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 10/09/23 08:49 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/09/23 08:49 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 10/09/23 08:49 98-82-81.0 0.33 1
Methyl acetate ND ug/L 10/09/23 08:49 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 10/09/23 08:49 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 10/09/23 08:49 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/23 08:49 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/09/23 08:49 1634-04-41.0 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 Lab ID: 92690981001 Collected: 10/02/23 12:37 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Styrene ND ug/L 10/09/23 08:49 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/23 08:49 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/09/23 08:49 127-18-41.0 0.29 1
Toluene ND ug/L 10/09/23 08:49 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 10/09/23 08:49 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/09/23 08:49 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/09/23 08:49 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/09/23 08:49 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/09/23 08:49 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 10/09/23 08:49 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 10/09/23 08:49 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 10/09/23 08:49 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/09/23 08:49 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %10/09/23 08:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %10/09/23 08:49 17060-07-070-130 1
Toluene-d8 (S)104 %10/09/23 08:49 2037-26-570-130 1
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
9040 pH
pH at 25 Degrees C 7.7 Std. Units 10/11/23 17:17 H30.10 0.10 1
Analytical Method: ASTM D4239-05
Pace Analytical Services - Asheville
ASTM D4239-05 Sulfur
Sulfur 0.0535 % (w/w)10/18/23 01:39 N20.020 0.020 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 DUP Lab ID: 92690981002 Collected: 10/02/23 12:40 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.2 Std. Units 10/03/23 14:271
True Color 10.0 units 10/03/23 14:275.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Boron 12.8J ug/L 10/09/23 16:22 7440-42-810/09/23 05:4350.0 12.4 1
Calcium 13200 ug/L 10/09/23 16:22 7440-70-210/09/23 05:43500 190 1
Iron 149 ug/L 10/09/23 16:22 7439-89-610/09/23 05:4340.0 25.0 1
Magnesium 4280 ug/L 10/09/23 16:22 7439-95-410/09/23 05:43500 84.0 1
Sodium 24000 ug/L 10/09/23 16:22 7440-23-510/09/23 05:432000 540 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Boron, Dissolved 14.9J ug/L 10/13/23 15:32 7440-42-810/11/23 11:3850.0 12.4 1
Calcium, Dissolved 14200 ug/L 10/13/23 15:32 7440-70-210/11/23 11:38500 190 1
Iron, Dissolved 163 ug/L 10/13/23 15:32 7439-89-610/11/23 11:3840.0 25.0 1
Magnesium, Dissolved 4340 ug/L 10/13/23 15:32 7439-95-410/11/23 11:38500 84.0 1
Sodium, Dissolved 21900 ug/L 10/13/23 15:32 7440-23-510/11/23 11:382000 540 1
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS
Aluminum 34.7 ug/L 10/10/23 00:15 7429-90-510/09/23 05:4310.0 8.6 1
Arsenic ND ug/L 10/10/23 00:15 7440-38-210/09/23 05:431.0 0.50 1
Barium 52.6 ug/L 10/10/23 00:15 7440-39-310/09/23 05:431.0 0.50 1
Beryllium ND ug/L 10/10/23 14:58 7440-41-710/09/23 05:430.10 0.033 1
Cadmium ND ug/L 10/10/23 00:15 7440-43-910/09/23 05:430.10 0.067 1
Chromium ND ug/L 10/10/23 00:15 7440-47-310/09/23 05:431.0 0.50 1
Cobalt ND ug/L 10/10/23 00:15 7440-48-410/09/23 05:431.0 0.24 1
Copper 1.4 ug/L 10/10/23 00:15 7440-50-810/09/23 05:431.0 0.42 1
Lead 2.4 ug/L 10/10/23 00:15 7439-92-110/09/23 05:431.0 0.22 1
Manganese 17.2 ug/L 10/10/23 00:15 7439-96-510/09/23 05:431.0 0.29 1
Molybdenum ND ug/L 10/10/23 00:15 7439-98-710/09/23 05:431.0 0.22 1
Nickel 0.45J ug/L 10/10/23 00:15 7440-02-010/09/23 05:431.0 0.26 1
Selenium 0.26J ug/L 10/10/23 00:15 7782-49-210/09/23 05:432.0 0.20 1
Silver ND ug/L 10/10/23 00:15 7440-22-410/09/23 05:430.50 0.028 1
Thallium ND ug/L 10/10/23 00:15 7440-28-010/09/23 05:431.0 0.11 1
Zinc ND ug/L 10/10/23 00:15 7440-66-610/09/23 05:4310.0 6.7 1
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS, Dissolved
Aluminum, Dissolved 38.9 ug/L 10/13/23 10:31 7429-90-510/11/23 11:3810.0 8.6 1
Arsenic, Dissolved ND ug/L 10/13/23 10:31 7440-38-210/11/23 11:381.0 0.50 1
Barium, Dissolved 50.2 ug/L 10/13/23 10:31 7440-39-310/11/23 11:381.0 0.50 1
Beryllium, Dissolved ND ug/L 10/13/23 10:31 7440-41-710/11/23 11:380.10 0.033 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 DUP Lab ID: 92690981002 Collected: 10/02/23 12:40 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS, Dissolved
Cadmium, Dissolved ND ug/L 10/13/23 10:31 7440-43-910/11/23 11:380.10 0.067 1
Chromium, Dissolved ND ug/L 10/13/23 10:31 7440-47-310/11/23 11:381.0 0.50 1
Cobalt, Dissolved ND ug/L 10/13/23 10:31 7440-48-410/11/23 11:381.0 0.24 1
Copper, Dissolved 1.4 ug/L 10/13/23 10:31 7440-50-810/11/23 11:381.0 0.42 1
Lead, Dissolved 2.2 ug/L 10/13/23 10:31 7439-92-110/11/23 11:381.0 0.22 1
Manganese, Dissolved 17.0 ug/L 10/13/23 10:31 7439-96-510/11/23 11:381.0 0.29 1
Molybdenum, Dissolved ND ug/L 10/13/23 10:31 7439-98-710/11/23 11:381.0 0.22 1
Nickel, Dissolved 0.35J ug/L 10/13/23 10:31 7440-02-010/11/23 11:381.0 0.26 1
Selenium, Dissolved ND ug/L 10/13/23 10:31 7782-49-210/11/23 11:382.0 0.20 1
Silver, Dissolved ND ug/L 10/13/23 10:31 7440-22-410/11/23 11:380.50 0.028 1
Thallium, Dissolved ND ug/L 10/13/23 10:31 7440-28-010/11/23 11:381.0 0.11 1
Zinc, Dissolved ND ug/L 10/13/23 10:31 7440-66-610/11/23 11:3810.0 6.7 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/12/23 10:05 7439-97-610/11/23 10:230.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/16/23 12:40 7439-97-610/12/23 07:120.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 10/06/23 14:34 83-32-910/05/23 12:588.3 1.7 1
Acenaphthylene ND ug/L 10/06/23 14:34 208-96-810/05/23 12:588.3 1.6 1
Acetophenone ND ug/L 10/06/23 14:34 98-86-210/05/23 12:588.3 1.2 1
Anthracene ND ug/L 10/06/23 14:34 120-12-710/05/23 12:588.3 1.9 1
Atrazine ND ug/L 10/06/23 14:34 1912-24-910/05/23 12:588.3 2.6 1
Benzaldehyde ND ug/L 10/06/23 14:34 100-52-710/05/23 12:588.3 3.0 1
Benzo(a)anthracene ND ug/L 10/06/23 14:34 56-55-310/05/23 12:588.3 2.2 1
Benzo(a)pyrene ND ug/L 10/06/23 14:34 50-32-810/05/23 12:588.3 2.3 1
Benzo(b)fluoranthene ND ug/L 10/06/23 14:34 205-99-210/05/23 12:588.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 10/06/23 14:34 191-24-210/05/23 12:588.3 2.4 1
Benzo(k)fluoranthene ND ug/L 10/06/23 14:34 207-08-910/05/23 12:588.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 10/06/23 14:34 92-52-410/05/23 12:588.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 10/06/23 14:34 101-55-310/05/23 12:588.3 1.5 1
Butylbenzylphthalate ND ug/L 10/06/23 14:34 85-68-710/05/23 12:588.3 2.6 1
Caprolactam ND ug/L 10/06/23 14:34 105-60-210/05/23 12:588.3 5.8 1
Carbazole ND ug/L 10/06/23 14:34 86-74-810/05/23 12:588.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 10/06/23 14:34 59-50-710/05/23 12:588.3 2.8 1
4-Chloroaniline ND ug/L 10/06/23 14:34 106-47-810/05/23 12:5816.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 10/06/23 14:34 111-91-110/05/23 12:588.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 10/06/23 14:34 111-44-410/05/23 12:588.3 1.6 1
2-Chloronaphthalene ND ug/L 10/06/23 14:34 91-58-710/05/23 12:588.3 1.4 1
2-Chlorophenol ND ug/L 10/06/23 14:34 95-57-810/05/23 12:588.3 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 DUP Lab ID: 92690981002 Collected: 10/02/23 12:40 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
4-Chlorophenylphenyl ether ND ug/L 10/06/23 14:34 7005-72-310/05/23 12:588.3 1.7 1
Chrysene ND ug/L 10/06/23 14:34 218-01-910/05/23 12:588.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 10/06/23 14:34 53-70-310/05/23 12:588.3 2.5 1
Dibenzofuran ND ug/L 10/06/23 14:34 132-64-910/05/23 12:588.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 10/06/23 14:34 91-94-110/05/23 12:5816.7 6.8 1
2,4-Dichlorophenol ND ug/L 10/06/23 14:34 120-83-210/05/23 12:588.3 1.2 1
Diethylphthalate ND ug/L 10/06/23 14:34 84-66-210/05/23 12:588.3 1.7 1
2,4-Dimethylphenol ND ug/L 10/06/23 14:34 105-67-910/05/23 12:588.3 1.4 1
Dimethylphthalate ND ug/L 10/06/23 14:34 131-11-310/05/23 12:588.3 1.8 1
Di-n-butylphthalate ND ug/L 10/06/23 14:34 84-74-210/05/23 12:588.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 10/06/23 14:34 534-52-110/05/23 12:5816.7 6.5 1
2,4-Dinitrophenol ND ug/L 10/06/23 14:34 51-28-510/05/23 12:5841.7 21.7 1
2,4-Dinitrotoluene ND ug/L 10/06/23 14:34 121-14-210/05/23 12:588.3 1.4 1
2,6-Dinitrotoluene ND ug/L 10/06/23 14:34 606-20-210/05/23 12:588.3 1.4 1
Di-n-octylphthalate ND ug/L 10/06/23 14:34 117-84-010/05/23 12:588.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/06/23 14:34 117-81-710/05/23 12:585.0 3.1 1
Fluoranthene ND ug/L 10/06/23 14:34 206-44-010/05/23 12:588.3 1.8 1
Fluorene ND ug/L 10/06/23 14:34 86-73-710/05/23 12:588.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 10/06/23 14:34 87-68-310/05/23 12:588.3 1.5 1
Hexachlorobenzene ND ug/L 10/06/23 14:34 118-74-110/05/23 12:588.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 10/06/23 14:34 77-47-410/05/23 12:588.3 1.3 1
Hexachloroethane ND ug/L 10/06/23 14:34 67-72-110/05/23 12:588.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/06/23 14:34 193-39-510/05/23 12:588.3 2.4 1
Isophorone ND ug/L 10/06/23 14:34 78-59-110/05/23 12:588.3 1.4 1
2-Methylnaphthalene ND ug/L 10/06/23 14:34 91-57-610/05/23 12:588.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 10/06/23 14:34 95-48-710/05/23 12:588.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/06/23 14:34 15831-10-410/05/23 12:588.3 1.0 1
Naphthalene ND ug/L 10/06/23 14:34 91-20-310/05/23 12:588.3 1.7 1
2-Nitroaniline ND ug/L 10/06/23 14:34 88-74-410/05/23 12:5816.7 2.5 1
3-Nitroaniline ND ug/L 10/06/23 14:34 99-09-210/05/23 12:5816.7 3.1 1
4-Nitroaniline ND ug/L 10/06/23 14:34 100-01-610/05/23 12:5816.7 4.2 1
Nitrobenzene ND ug/L 10/06/23 14:34 98-95-310/05/23 12:588.3 1.6 1
2-Nitrophenol ND ug/L 10/06/23 14:34 88-75-510/05/23 12:588.3 1.2 1
4-Nitrophenol ND ug/L 10/06/23 14:34 100-02-710/05/23 12:5841.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 10/06/23 14:34 621-64-710/05/23 12:588.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 10/06/23 14:34 86-30-610/05/23 12:588.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/06/23 14:34 108-60-110/05/23 12:588.3 0.96 1
Pentachlorophenol ND ug/L 10/06/23 14:34 87-86-510/05/23 12:5816.7 3.1 1
Phenanthrene ND ug/L 10/06/23 14:34 85-01-810/05/23 12:588.3 1.7 1
Phenol ND ug/L 10/06/23 14:34 108-95-210/05/23 12:588.3 1.1 1
Pyrene ND ug/L 10/06/23 14:34 129-00-010/05/23 12:588.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 10/06/23 14:34 95-95-410/05/23 12:588.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 10/06/23 14:34 88-06-210/05/23 12:588.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)108 %10/06/23 14:34 4165-60-010/05/23 12:5810-138 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 DUP Lab ID: 92690981002 Collected: 10/02/23 12:40 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Surrogates
2-Fluorobiphenyl (S)106 %10/06/23 14:34 321-60-810/05/23 12:5810-130 1
Terphenyl-d14 (S)106 %10/06/23 14:34 1718-51-010/05/23 12:5819-191 1
Phenol-d6 (S)50 %10/06/23 14:34 13127-88-310/05/23 12:5810-130 1
2-Fluorophenol (S)73 %10/06/23 14:34 367-12-410/05/23 12:5810-130 1
2,4,6-Tribromophenol (S)122 %10/06/23 14:34 118-79-610/05/23 12:5810-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/09/23 22:03 67-64-125.0 5.1 1
Benzene ND ug/L 10/09/23 22:03 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 10/09/23 22:03 75-27-41.0 0.31 1
Bromoform ND ug/L 10/09/23 22:03 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/09/23 22:03 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/09/23 22:03 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/09/23 22:03 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/09/23 22:03 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/09/23 22:03 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/09/23 22:03 75-00-31.0 0.65 1
Chloroform 0.63J ug/L 10/09/23 22:03 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/09/23 22:03 74-87-31.0 0.54 1
Cyclohexane ND ug/L 10/09/23 22:03 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/23 22:03 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/09/23 22:03 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/23 22:03 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 10/09/23 22:03 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/09/23 22:03 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/09/23 22:03 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/09/23 22:03 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/09/23 22:03 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/09/23 22:03 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/09/23 22:03 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/09/23 22:03 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/09/23 22:03 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/09/23 22:03 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/09/23 22:03 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/09/23 22:03 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 10/09/23 22:03 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/09/23 22:03 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 10/09/23 22:03 98-82-81.0 0.33 1
Methyl acetate ND ug/L 10/09/23 22:03 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 10/09/23 22:03 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 10/09/23 22:03 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/23 22:03 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/09/23 22:03 1634-04-41.0 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
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Page 13 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBOF-10022023 DUP Lab ID: 92690981002 Collected: 10/02/23 12:40 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Styrene ND ug/L 10/09/23 22:03 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/23 22:03 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/09/23 22:03 127-18-41.0 0.29 1
Toluene ND ug/L 10/09/23 22:03 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 10/09/23 22:03 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/09/23 22:03 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/09/23 22:03 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/09/23 22:03 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/09/23 22:03 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 10/09/23 22:03 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 10/09/23 22:03 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 10/09/23 22:03 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/09/23 22:03 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %10/09/23 22:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/09/23 22:03 17060-07-070-130 1
Toluene-d8 (S)100 %10/09/23 22:03 2037-26-570-130 1
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
9040 pH
pH at 25 Degrees C 7.6 Std. Units 10/11/23 17:20 H30.10 0.10 1
Analytical Method: ASTM D4239-05
Pace Analytical Services - Asheville
ASTM D4239-05 Sulfur
Sulfur 0.0510 % (w/w)10/18/23 01:44 N20.020 0.020 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBUS-10022023 Lab ID: 92690981003 Collected: 10/02/23 13:35 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2120B-2011
Pace Analytical Services - Eden
2120B W True Color EDEN
pH 6.2 Std. Units 10/03/23 14:291
True Color 10.0 units 10/03/23 14:295.0 5.0 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP
Boron ND ug/L 10/09/23 16:25 7440-42-810/09/23 05:4350.0 12.4 1
Calcium 10100 ug/L 10/09/23 16:25 7440-70-210/09/23 05:43500 190 1
Iron 225 ug/L 10/09/23 16:25 7439-89-610/09/23 05:4340.0 25.0 1
Magnesium 4080 ug/L 10/09/23 16:25 7439-95-410/09/23 05:43500 84.0 1
Sodium 10900 ug/L 10/09/23 16:25 7440-23-510/09/23 05:432000 540 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Ormond Beach
200.7 MET ICP, Dissolved
Boron, Dissolved ND ug/L 10/13/23 15:40 7440-42-810/11/23 11:3850.0 12.4 1
Calcium, Dissolved 11000 ug/L 10/13/23 15:40 7440-70-210/11/23 11:38500 190 1
Iron, Dissolved 195 ug/L 10/13/23 15:40 7439-89-610/11/23 11:3840.0 25.0 1
Magnesium, Dissolved 4150 ug/L 10/13/23 15:40 7439-95-410/11/23 11:38500 84.0 1
Sodium, Dissolved 9710 ug/L 10/13/23 15:40 7440-23-510/11/23 11:382000 540 1
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS
Aluminum 111 ug/L 10/10/23 00:19 7429-90-510/09/23 05:4310.0 8.6 1
Arsenic ND ug/L 10/10/23 00:19 7440-38-210/09/23 05:431.0 0.50 1
Barium 53.1 ug/L 10/10/23 00:19 7440-39-310/09/23 05:431.0 0.50 1
Beryllium ND ug/L 10/10/23 15:03 7440-41-710/09/23 05:430.10 0.033 1
Cadmium ND ug/L 10/10/23 00:19 7440-43-910/09/23 05:430.10 0.067 1
Chromium ND ug/L 10/10/23 00:19 7440-47-310/09/23 05:431.0 0.50 1
Cobalt ND ug/L 10/10/23 00:19 7440-48-410/09/23 05:431.0 0.24 1
Copper 1.1 ug/L 10/10/23 00:19 7440-50-810/09/23 05:431.0 0.42 1
Lead 0.58J ug/L 10/10/23 00:19 7439-92-110/09/23 05:431.0 0.22 1
Manganese 13.2 ug/L 10/10/23 00:19 7439-96-510/09/23 05:431.0 0.29 1
Molybdenum ND ug/L 10/10/23 00:19 7439-98-710/09/23 05:431.0 0.22 1
Nickel 0.50J ug/L 10/10/23 00:19 7440-02-010/09/23 05:431.0 0.26 1
Selenium ND ug/L 10/10/23 00:19 7782-49-210/09/23 05:432.0 0.20 1
Silver ND ug/L 10/10/23 00:19 7440-22-410/09/23 05:430.50 0.028 1
Thallium ND ug/L 10/10/23 00:19 7440-28-010/09/23 05:431.0 0.11 1
Zinc ND ug/L 10/10/23 00:19 7440-66-610/09/23 05:4310.0 6.7 1
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS, Dissolved
Aluminum, Dissolved 101 ug/L 10/13/23 10:34 7429-90-510/11/23 11:3810.0 8.6 1
Arsenic, Dissolved ND ug/L 10/13/23 10:34 7440-38-210/11/23 11:381.0 0.50 1
Barium, Dissolved 51.0 ug/L 10/13/23 10:34 7440-39-310/11/23 11:381.0 0.50 1
Beryllium, Dissolved ND ug/L 10/13/23 10:34 7440-41-710/11/23 11:380.10 0.033 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBUS-10022023 Lab ID: 92690981003 Collected: 10/02/23 13:35 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Pace Analytical Services - Ormond Beach
200.8 MET ICPMS, Dissolved
Cadmium, Dissolved ND ug/L 10/13/23 10:34 7440-43-910/11/23 11:380.10 0.067 1
Chromium, Dissolved ND ug/L 10/13/23 10:34 7440-47-310/11/23 11:381.0 0.50 1
Cobalt, Dissolved ND ug/L 10/13/23 10:34 7440-48-410/11/23 11:381.0 0.24 1
Copper, Dissolved 1.3 ug/L 10/13/23 10:34 7440-50-810/11/23 11:381.0 0.42 1
Lead, Dissolved 0.49J ug/L 10/13/23 10:34 7439-92-110/11/23 11:381.0 0.22 1
Manganese, Dissolved 11.1 ug/L 10/13/23 10:34 7439-96-510/11/23 11:381.0 0.29 1
Molybdenum, Dissolved ND ug/L 10/13/23 10:34 7439-98-710/11/23 11:381.0 0.22 1
Nickel, Dissolved ND ug/L 10/13/23 10:34 7440-02-010/11/23 11:381.0 0.26 1
Selenium, Dissolved ND ug/L 10/13/23 10:34 7782-49-210/11/23 11:382.0 0.20 1
Silver, Dissolved ND ug/L 10/13/23 10:34 7440-22-410/11/23 11:380.50 0.028 1
Thallium, Dissolved ND ug/L 10/13/23 10:34 7440-28-010/11/23 11:381.0 0.11 1
Zinc, Dissolved 7.2J ug/L 10/13/23 10:34 7440-66-610/11/23 11:3810.0 6.7 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury
Mercury ND ug/L 10/12/23 10:08 7439-97-610/11/23 10:230.20 0.14 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Ormond Beach
245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/16/23 12:42 7439-97-610/12/23 07:120.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 10/10/23 17:21 83-32-910/08/23 11:198.3 1.7 1
Acenaphthylene ND ug/L 10/10/23 17:21 208-96-810/08/23 11:198.3 1.6 1
Acetophenone ND ug/L 10/10/23 17:21 98-86-210/08/23 11:198.3 1.2 1
Anthracene ND ug/L 10/10/23 17:21 120-12-710/08/23 11:198.3 1.9 1
Atrazine ND ug/L 10/10/23 17:21 1912-24-910/08/23 11:198.3 2.6 1
Benzaldehyde ND ug/L 10/10/23 17:21 100-52-710/08/23 11:198.3 3.0 1
Benzo(a)anthracene ND ug/L 10/10/23 17:21 56-55-310/08/23 11:198.3 2.2 1
Benzo(a)pyrene ND ug/L 10/10/23 17:21 50-32-810/08/23 11:198.3 2.3 1
Benzo(b)fluoranthene ND ug/L 10/10/23 17:21 205-99-210/08/23 11:198.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 10/10/23 17:21 191-24-210/08/23 11:198.3 2.4 1
Benzo(k)fluoranthene ND ug/L 10/10/23 17:21 207-08-910/08/23 11:198.3 2.3 1
Biphenyl (Diphenyl)ND ug/L 10/10/23 17:21 92-52-410/08/23 11:198.3 1.5 1
4-Bromophenylphenyl ether ND ug/L 10/10/23 17:21 101-55-310/08/23 11:198.3 1.5 1
Butylbenzylphthalate ND ug/L 10/10/23 17:21 85-68-710/08/23 11:198.3 2.6 1
Caprolactam ND ug/L 10/10/23 17:21 105-60-210/08/23 11:198.3 5.8 1
Carbazole ND ug/L 10/10/23 17:21 86-74-810/08/23 11:198.3 2.0 1
4-Chloro-3-methylphenol ND ug/L 10/10/23 17:21 59-50-710/08/23 11:198.3 2.8 1
4-Chloroaniline ND ug/L 10/10/23 17:21 106-47-810/08/23 11:1916.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 10/10/23 17:21 111-91-110/08/23 11:198.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 10/10/23 17:21 111-44-410/08/23 11:198.3 1.6 1
2-Chloronaphthalene ND ug/L 10/10/23 17:21 91-58-710/08/23 11:198.3 1.4 1
2-Chlorophenol ND ug/L 10/10/23 17:21 95-57-810/08/23 11:198.3 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 16 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBUS-10022023 Lab ID: 92690981003 Collected: 10/02/23 13:35 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
4-Chlorophenylphenyl ether ND ug/L 10/10/23 17:21 7005-72-310/08/23 11:198.3 1.7 1
Chrysene ND ug/L 10/10/23 17:21 218-01-910/08/23 11:198.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 10/10/23 17:21 53-70-310/08/23 11:198.3 2.5 1
Dibenzofuran ND ug/L 10/10/23 17:21 132-64-910/08/23 11:198.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 10/10/23 17:21 91-94-110/08/23 11:1916.7 6.8 1
2,4-Dichlorophenol ND ug/L 10/10/23 17:21 120-83-210/08/23 11:198.3 1.2 1
Diethylphthalate ND ug/L 10/10/23 17:21 84-66-210/08/23 11:198.3 1.7 1
2,4-Dimethylphenol ND ug/L 10/10/23 17:21 105-67-910/08/23 11:198.3 1.4 1
Dimethylphthalate ND ug/L 10/10/23 17:21 131-11-310/08/23 11:198.3 1.8 1
Di-n-butylphthalate ND ug/L 10/10/23 17:21 84-74-210/08/23 11:198.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 10/10/23 17:21 534-52-110/08/23 11:1916.7 6.5 1
2,4-Dinitrophenol ND ug/L 10/10/23 17:21 51-28-510/08/23 11:1941.7 21.7 1
2,4-Dinitrotoluene ND ug/L 10/10/23 17:21 121-14-210/08/23 11:198.3 1.4 1
2,6-Dinitrotoluene ND ug/L 10/10/23 17:21 606-20-210/08/23 11:198.3 1.4 1
Di-n-octylphthalate ND ug/L 10/10/23 17:21 117-84-0 v110/08/23 11:198.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/10/23 17:21 117-81-710/08/23 11:195.0 3.1 1
Fluoranthene ND ug/L 10/10/23 17:21 206-44-010/08/23 11:198.3 1.8 1
Fluorene ND ug/L 10/10/23 17:21 86-73-710/08/23 11:198.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 10/10/23 17:21 87-68-310/08/23 11:198.3 1.5 1
Hexachlorobenzene ND ug/L 10/10/23 17:21 118-74-110/08/23 11:198.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 10/10/23 17:21 77-47-410/08/23 11:198.3 1.3 1
Hexachloroethane ND ug/L 10/10/23 17:21 67-72-110/08/23 11:198.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/10/23 17:21 193-39-510/08/23 11:198.3 2.4 1
Isophorone ND ug/L 10/10/23 17:21 78-59-110/08/23 11:198.3 1.4 1
2-Methylnaphthalene ND ug/L 10/10/23 17:21 91-57-610/08/23 11:198.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 10/10/23 17:21 95-48-710/08/23 11:198.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/10/23 17:21 15831-10-410/08/23 11:198.3 1.0 1
Naphthalene ND ug/L 10/10/23 17:21 91-20-310/08/23 11:198.3 1.7 1
2-Nitroaniline ND ug/L 10/10/23 17:21 88-74-410/08/23 11:1916.7 2.5 1
3-Nitroaniline ND ug/L 10/10/23 17:21 99-09-210/08/23 11:1916.7 3.1 1
4-Nitroaniline ND ug/L 10/10/23 17:21 100-01-610/08/23 11:1916.7 4.2 1
Nitrobenzene ND ug/L 10/10/23 17:21 98-95-310/08/23 11:198.3 1.6 1
2-Nitrophenol ND ug/L 10/10/23 17:21 88-75-510/08/23 11:198.3 1.2 1
4-Nitrophenol ND ug/L 10/10/23 17:21 100-02-7 v210/08/23 11:1941.7 5.5 1
N-Nitroso-di-n-propylamine ND ug/L 10/10/23 17:21 621-64-710/08/23 11:198.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 10/10/23 17:21 86-30-610/08/23 11:198.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/10/23 17:21 108-60-110/08/23 11:198.3 0.96 1
Pentachlorophenol ND ug/L 10/10/23 17:21 87-86-510/08/23 11:1916.7 3.1 1
Phenanthrene ND ug/L 10/10/23 17:21 85-01-810/08/23 11:198.3 1.7 1
Phenol ND ug/L 10/10/23 17:21 108-95-210/08/23 11:198.3 1.1 1
Pyrene ND ug/L 10/10/23 17:21 129-00-010/08/23 11:198.3 1.8 1
2,4,5-Trichlorophenol ND ug/L 10/10/23 17:21 95-95-410/08/23 11:198.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 10/10/23 17:21 88-06-210/08/23 11:198.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)107 %10/10/23 17:21 4165-60-010/08/23 11:1910-138 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 17 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBUS-10022023 Lab ID: 92690981003 Collected: 10/02/23 13:35 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Surrogates
2-Fluorobiphenyl (S)105 %10/10/23 17:21 321-60-810/08/23 11:1910-130 1
Terphenyl-d14 (S)110 %10/10/23 17:21 1718-51-010/08/23 11:1919-191 1
Phenol-d6 (S)53 %10/10/23 17:21 13127-88-310/08/23 11:1910-130 1
2-Fluorophenol (S)77 %10/10/23 17:21 367-12-410/08/23 11:1910-130 1
2,4,6-Tribromophenol (S)133 %10/10/23 17:21 118-79-610/08/23 11:1910-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 5.6J ug/L 10/09/23 22:21 67-64-125.0 5.1 1
Benzene ND ug/L 10/09/23 22:21 71-43-21.0 0.34 1
Bromodichloromethane ND ug/L 10/09/23 22:21 75-27-41.0 0.31 1
Bromoform ND ug/L 10/09/23 22:21 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/09/23 22:21 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/09/23 22:21 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/09/23 22:21 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/09/23 22:21 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/09/23 22:21 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/09/23 22:21 75-00-31.0 0.65 1
Chloroform ND ug/L 10/09/23 22:21 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/09/23 22:21 74-87-31.0 0.54 1
Cyclohexane ND ug/L 10/09/23 22:21 110-82-71.0 0.35 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/23 22:21 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/09/23 22:21 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/23 22:21 106-93-41.0 0.27 1
1,2-Dichlorobenzene ND ug/L 10/09/23 22:21 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/09/23 22:21 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/09/23 22:21 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/09/23 22:21 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/09/23 22:21 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/09/23 22:21 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/09/23 22:21 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/09/23 22:21 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/09/23 22:21 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/09/23 22:21 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/09/23 22:21 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/09/23 22:21 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 10/09/23 22:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/09/23 22:21 591-78-65.0 0.48 1
Isopropylbenzene (Cumene)ND ug/L 10/09/23 22:21 98-82-81.0 0.33 1
Methyl acetate ND ug/L 10/09/23 22:21 79-20-910.0 2.4 1
Methylcyclohexane ND ug/L 10/09/23 22:21 108-87-210.0 1.5 1
Methylene Chloride ND ug/L 10/09/23 22:21 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/23 22:21 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/09/23 22:21 1634-04-41.0 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Sample: CBUS-10022023 Lab ID: 92690981003 Collected: 10/02/23 13:35 Received: 10/02/23 15:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Styrene ND ug/L 10/09/23 22:21 100-42-51.0 0.29 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/23 22:21 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/09/23 22:21 127-18-41.0 0.29 1
Toluene ND ug/L 10/09/23 22:21 108-88-31.0 0.24 1
1,2,4-Trichlorobenzene ND ug/L 10/09/23 22:21 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/09/23 22:21 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/09/23 22:21 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/09/23 22:21 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/09/23 22:21 75-69-41.0 0.30 1
1,1,2-Trichlorotrifluoroethane ND ug/L 10/09/23 22:21 76-13-11.0 0.32 1
Vinyl chloride ND ug/L 10/09/23 22:21 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 10/09/23 22:21 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/09/23 22:21 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %10/09/23 22:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/09/23 22:21 17060-07-070-130 1
Toluene-d8 (S)100 %10/09/23 22:21 2037-26-570-130 1
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
9040 pH
pH at 25 Degrees C 7.3 Std. Units 10/11/23 17:24 H30.10 0.10 1
Analytical Method: ASTM D4239-05
Pace Analytical Services - Asheville
ASTM D4239-05 Sulfur
Sulfur 0.0508 % (w/w)10/18/23 01:56 N20.020 0.020 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
803823
SM 2120B-2011
SM 2120B-2011
2120B True Color EDEN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples: 92690981001, 92690981002, 92690981003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4163004
Associated Lab Samples:92690981001, 92690981002, 92690981003
Matrix: Water
AnalyzedMDL
True Color units ND 5.0 10/03/23 14:255.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4163005LABORATORY CONTROL SAMPLE:
LCSSpike
True Color units 35.035 100 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92690981001
4163006SAMPLE DUPLICATE:
pH Std. Units 6.1 0 106.1
True Color units 5.0 0 105.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
957049
EPA 245.1
EPA 245.1
245.1 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92690981001, 92690981002, 92690981003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5263175
Associated Lab Samples:92690981001, 92690981002, 92690981003
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/12/23 09:360.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5263176LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 1.92 96 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5263177MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
20291110001
5263178
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 100 70-13098 2 202ND2.1 2.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5263179MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35833501001
5263180
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 97 70-13098 0 2020.14U 2.0 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
957393
EPA 245.1
EPA 245.1
245.1 Mercury - Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92690981001, 92690981002, 92690981003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5265295
Associated Lab Samples:92690981001, 92690981002, 92690981003
Matrix: Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/16/23 12:240.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5265296LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.02 100 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5265297MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690981001
5265298
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2 100 70-13098 2 202ND2.1 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
956313
EPA 200.7
EPA 200.7
200.7 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92690981001, 92690981002, 92690981003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5259600
Associated Lab Samples:92690981001, 92690981002, 92690981003
Matrix: Water
AnalyzedMDL
Boron ug/L ND 50.0 10/09/23 15:3112.4
Calcium ug/L ND 500 10/09/23 15:31190
Iron ug/L ND 40.0 10/09/23 15:3125.0
Magnesium ug/L ND 500 10/09/23 15:3184.0
Sodium ug/L ND 2000 10/09/23 15:31540
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5259601LABORATORY CONTROL SAMPLE:
LCSSpike
Boron ug/L 12501250 100 85-115
Calcium ug/L 1230012500 98 85-115
Iron ug/L 24402500 97 85-115
Magnesium ug/L 1270012500 102 85-115
Sodium ug/L 1270012500 102 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5259602MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35832870001
5259603
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Boron ug/L 1250 100 70-130101 1 20125015.9J 1260 1270
Calcium ug/L 12500 97 70-13098 1 2012500107013200 13300
Iron ug/L 2500 96 70-13098 1 20250012503660 3700
Magnesium ug/L 12500 103 70-130104 1 201250075013600 13700
Sodium ug/L 12500 102 70-130104 2 20125001760J14500 14800
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5259604MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92691175001
5259605
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Boron ug/L 1250 102 70-130102 0 201250ND1300 1300
Calcium ug/L 12500 99 70-13090 3 20125003560048000 46800
Iron ug/L 2500 98 70-13097 2 202500ND2470 2430
Magnesium ug/L 12500 105 70-130103 1 20125001150024700 24400
Sodium ug/L E,M11250011670-13061 3 2012500261000276000 269000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
957167
EPA 200.7
EPA 200.7
200.7 MET Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92690981001, 92690981002, 92690981003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5263563
Associated Lab Samples:92690981001, 92690981002, 92690981003
Matrix: Water
AnalyzedMDL
Boron, Dissolved ug/L ND 50.0 10/13/23 15:2112.4
Calcium, Dissolved ug/L ND 500 10/13/23 15:21190
Iron, Dissolved ug/L ND 40.0 10/13/23 15:2125.0
Magnesium, Dissolved ug/L ND 500 10/13/23 15:2184.0
Sodium, Dissolved ug/L ND 2000 10/13/23 15:21540
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5263564LABORATORY CONTROL SAMPLE:
LCSSpike
Boron, Dissolved ug/L 12801250 103 85-115
Calcium, Dissolved ug/L 1330012500 107 85-115
Iron, Dissolved ug/L 26202500 105 85-115
Magnesium, Dissolved ug/L 1330012500 106 85-115
Sodium, Dissolved ug/L 1260012500 101 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5263565MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690981003
5263566
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Boron, Dissolved ug/L 1250 103 70-130102 0 201250ND1290 1290
Calcium, Dissolved ug/L 12500 106 70-130105 1 20125001100024200 24100
Iron, Dissolved ug/L 2500 104 70-130104 0 2025001952800 2780
Magnesium, Dissolved ug/L 12500 106 70-130106 0 2012500415017400 17400
Sodium, Dissolved ug/L 12500 106 70-130106 0 2012500971023000 22900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
956312
EPA 200.8
EPA 200.8
200.8 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92690981001, 92690981002, 92690981003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5259594
Associated Lab Samples:92690981001, 92690981002, 92690981003
Matrix: Water
AnalyzedMDL
Aluminum ug/L ND 10.0 10/09/23 23:098.6
Arsenic ug/L ND 1.0 10/09/23 23:090.50
Barium ug/L ND 1.0 10/09/23 23:090.50
Beryllium ug/L ND 0.10 10/10/23 14:430.033
Cadmium ug/L ND 0.10 10/09/23 23:090.067
Chromium ug/L ND 1.0 10/09/23 23:090.50
Cobalt ug/L ND 1.0 10/09/23 23:090.24
Copper ug/L ND 1.0 10/09/23 23:090.42
Lead ug/L ND 1.0 10/09/23 23:090.22
Manganese ug/L ND 1.0 10/09/23 23:090.29
Molybdenum ug/L ND 1.0 10/09/23 23:090.22
Nickel ug/L ND 1.0 10/09/23 23:090.26
Selenium ug/L ND 2.0 10/09/23 23:090.20
Silver ug/L ND 0.50 10/09/23 23:090.028
Thallium ug/L ND 1.0 10/09/23 23:090.11
Zinc ug/L ND 10.0 10/09/23 23:096.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5259595LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum ug/L 485500 97 85-115
Arsenic ug/L 49.050 98 85-115
Barium ug/L 48.550 97 85-115
Beryllium ug/L 4.95 99 85-115
Cadmium ug/L 4.95 98 85-115
Chromium ug/L 50.050 100 85-115
Cobalt ug/L 49.350 99 85-115
Copper ug/L 48.350 97 85-115
Lead ug/L 50.950 102 85-115
Manganese ug/L 49.750 99 85-115
Molybdenum ug/L 47.650 95 85-115
Nickel ug/L 49.350 99 85-115
Selenium ug/L 51.850 104 85-115
Silver ug/L 4.75 94 85-115
Thallium ug/L 50.650 101 85-115
Zinc ug/L 248250 99 85-115
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5259596MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35832870002
5259597
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 500 118 70-130116 1 205004881080 1070
Arsenic ug/L 50 98 70-13096 1 20501.0 49.8 49.1
Barium ug/L 50 95 70-13095 0 205020.6 68.3 68.0
Beryllium ug/L 5 99 70-13099 0 2050.035J 5.0 5.0
Cadmium ug/L 5 94 70-13098 3 205<0.067 4.7 4.9
Chromium ug/L 50 99 70-13098 1 20500.99J 50.7 50.2
Cobalt ug/L 50 98 70-13097 1 20500.52J 49.5 49.0
Copper ug/L 50 97 70-13096 1 20501.8 49.5 49.0
Lead ug/L 50 102 70-130101 0 20500.70J 51.7 51.5
Manganese ug/L 50 97 70-13096 1 205034.6 83.0 82.4
Molybdenum ug/L 50 95 70-13094 0 2050<0.22 47.5 47.3
Nickel ug/L 50 99 70-13096 3 20500.89J 50.4 49.1
Selenium ug/L 50 102 70-130103 2 20500.25J 51.0 51.9
Silver ug/L 5 96 70-13094 1 205<0.028 4.8 4.7
Thallium ug/L 50 102 70-130100 1 2050<0.11 50.8 50.1
Zinc ug/L 250 99 70-13098 1 2025019.2 255 252
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5259598MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92691731001
5259599
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 500 99 70-13096 2 205000.099
mg/L 592 581
Arsenic ug/L 50 98 70-13098 0 2050ND49.4 49.3
Barium ug/L 50 98 70-13098 0 20500.019mg/L 68.4 68.4
Beryllium ug/L 5 100 70-130100 0 205ND5.0 5.0
Cadmium ug/L 5 96 70-13094 2 205ND4.8 4.7
Chromium ug/L 50 99 70-13098 1 2050ND50.2 49.7
Cobalt ug/L 50 99 70-13098 1 2050ND49.7 49.2
Copper ug/L 50 97 70-13095 2 20500.010
mg/L 58.6 57.5
Lead ug/L 50 104 70-130104 0 2050ND52.3 52.1
Manganese ug/L 50 99 70-13098 1 20500.0067
mg/L 56.0 55.4
Molybdenum ug/L 50 96 70-13097 1 2050ND48.7 49.3
Nickel ug/L 50 98 70-13099 1 20500.0031
mg/L
52.1 52.5
Selenium ug/L 50 103 70-130101 2 2050ND51.4 50.5
Silver ug/L 5 96 70-13094 2 205ND4.8 4.7
Thallium ug/L 50 103 70-130103 0 2050ND51.5 51.3
Zinc ug/L 250 100 70-13097 2 202500.050
mg/L 299 293
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
957169
EPA 200.8
EPA 200.8
200.8 MET Dissolved
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92690981001, 92690981002, 92690981003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 5263569
Associated Lab Samples:92690981001, 92690981002, 92690981003
Matrix: Water
AnalyzedMDL
Aluminum, Dissolved ug/L ND 10.0 10/13/23 15:358.6
Arsenic, Dissolved ug/L ND 1.0 10/13/23 15:350.50
Barium, Dissolved ug/L ND 1.0 10/13/23 15:350.50
Beryllium, Dissolved ug/L ND 0.10 10/13/23 10:110.033
Cadmium, Dissolved ug/L ND 0.10 10/13/23 15:350.067
Chromium, Dissolved ug/L ND 1.0 10/13/23 15:350.50
Cobalt, Dissolved ug/L ND 1.0 10/13/23 15:350.24
Copper, Dissolved ug/L ND 1.0 10/13/23 15:350.42
Lead, Dissolved ug/L ND 1.0 10/13/23 15:350.22
Manganese, Dissolved ug/L ND 1.0 10/13/23 15:350.29
Molybdenum, Dissolved ug/L ND 1.0 10/13/23 15:350.22
Nickel, Dissolved ug/L ND 1.0 10/13/23 15:350.26
Selenium, Dissolved ug/L ND 2.0 10/13/23 15:350.20
Silver, Dissolved ug/L ND 0.50 10/13/23 15:350.028
Thallium, Dissolved ug/L ND 1.0 10/13/23 15:350.11
Zinc, Dissolved ug/L ND 10.0 10/13/23 15:356.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5263570LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum, Dissolved ug/L 480500 96 85-115
Arsenic, Dissolved ug/L 48.650 97 85-115
Barium, Dissolved ug/L 47.450 95 85-115
Beryllium, Dissolved ug/L 4.65 93 85-115
Cadmium, Dissolved ug/L 5.05 100 85-115
Chromium, Dissolved ug/L 48.450 97 85-115
Cobalt, Dissolved ug/L 48.750 97 85-115
Copper, Dissolved ug/L 49.450 99 85-115
Lead, Dissolved ug/L 49.950 100 85-115
Manganese, Dissolved ug/L 48.050 96 85-115
Molybdenum, Dissolved ug/L 45.950 92 85-115
Nickel, Dissolved ug/L 48.150 96 85-115
Selenium, Dissolved ug/L 52.150 104 85-115
Silver, Dissolved ug/L 4.85 96 85-115
Thallium, Dissolved ug/L 48.550 97 85-115
Zinc, Dissolved ug/L 248250 99 85-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5263571MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35832870001
5263572
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum, Dissolved ug/L 500 104 70-130102 1 20500380900 891
Arsenic, Dissolved ug/L 50 96 70-13095 1 20500.57J 48.7 48.3
Barium, Dissolved ug/L 50 95 70-13095 0 205013.8 61.2 61.3
Beryllium, Dissolved ug/L 5 94 70-13095 1 205<0.033 4.7 4.8
Cadmium, Dissolved ug/L 5 100 70-13099 1 205<0.067 5.0 5.0
Chromium, Dissolved ug/L 50 96 70-13097 1 20500.93J 48.8 49.5
Cobalt, Dissolved ug/L 50 98 70-13097 1 20500.34J 49.1 48.6
Copper, Dissolved ug/L 50 103 70-130100 3 20500.57J 51.9 50.6
Lead, Dissolved ug/L 50 100 70-130100 0 20500.40J 50.4 50.5
Manganese, Dissolved ug/L 50 96 70-13093 2 205030.3 78.5 76.7
Molybdenum, Dissolved ug/L 50 93 70-13091 2 2050<0.22 46.6 45.8
Nickel, Dissolved ug/L 50 96 70-13095 2 20500.59J 48.7 47.9
Selenium, Dissolved ug/L 50 101 70-130100 1 20500.20J 50.8 50.4
Silver, Dissolved ug/L 5 98 70-13098 0 205<0.028 4.9 4.9
Thallium, Dissolved ug/L 50 98 70-13097 1 2050<0.11 49.2 48.6
Zinc, Dissolved ug/L 250 100 70-13097 3 20250<6.7 256 249
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804906
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92690981001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4168315
Associated Lab Samples:92690981001
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 10/09/23 00:550.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/09/23 00:550.22
1,1,2-Trichloroethane ug/L ND 1.0 10/09/23 00:550.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 10/09/23 00:550.32
1,1-Dichloroethane ug/L ND 1.0 10/09/23 00:550.37
1,1-Dichloroethene ug/L ND 1.0 10/09/23 00:550.35
1,2,4-Trichlorobenzene ug/L ND 1.0 10/09/23 00:550.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/09/23 00:550.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/09/23 00:550.27
1,2-Dichlorobenzene ug/L ND 1.0 10/09/23 00:550.34
1,2-Dichloroethane ug/L ND 1.0 10/09/23 00:550.32
1,2-Dichloropropane ug/L ND 1.0 10/09/23 00:550.36
1,3-Dichlorobenzene ug/L ND 1.0 10/09/23 00:550.34
1,4-Dichlorobenzene ug/L ND 1.0 10/09/23 00:550.33
2-Butanone (MEK)ug/L ND 5.0 10/09/23 00:554.0
2-Hexanone ug/L ND 5.0 10/09/23 00:550.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/09/23 00:552.7
Acetone ug/L ND 25.0 10/09/23 00:555.1
Benzene ug/L ND 1.0 10/09/23 00:550.34
Bromodichloromethane ug/L ND 1.0 10/09/23 00:550.31
Bromoform ug/L ND 1.0 10/09/23 00:550.34
Bromomethane ug/L ND 2.0 10/09/23 00:551.7
Carbon disulfide ug/L ND 2.0 10/09/23 00:550.36
Carbon tetrachloride ug/L ND 1.0 10/09/23 00:550.33
Chlorobenzene ug/L ND 1.0 10/09/23 00:550.28
Chloroethane ug/L ND 1.0 10/09/23 00:550.65
Chloroform ug/L ND 1.0 10/09/23 00:550.43
Chloromethane ug/L ND 1.0 10/09/23 00:550.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/09/23 00:550.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/09/23 00:550.36
Cyclohexane ug/L ND 1.0 10/09/23 00:550.35
Dibromochloromethane ug/L ND 1.0 10/09/23 00:550.36
Dichlorodifluoromethane ug/L ND 1.0 10/09/23 00:550.35
Ethylbenzene ug/L ND 1.0 10/09/23 00:550.30
Isopropylbenzene (Cumene)ug/L ND 1.0 10/09/23 00:550.33
m&p-Xylene ug/L ND 2.0 10/09/23 00:550.71
Methyl acetate ug/L ND 10.0 10/09/23 00:552.4
Methyl-tert-butyl ether ug/L ND 1.0 10/09/23 00:550.42
Methylcyclohexane ug/L ND 10.0 10/09/23 00:551.5
Methylene Chloride ug/L ND 5.0 10/09/23 00:552.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4168315
Associated Lab Samples:92690981001
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 10/09/23 00:550.34
Styrene ug/L ND 1.0 10/09/23 00:550.29
Tetrachloroethene ug/L ND 1.0 10/09/23 00:550.29
Toluene ug/L ND 1.0 10/09/23 00:550.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/09/23 00:550.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/09/23 00:550.36
Trichloroethene ug/L ND 1.0 10/09/23 00:550.38
Trichlorofluoromethane ug/L ND 1.0 10/09/23 00:550.30
Vinyl chloride ug/L ND 1.0 10/09/23 00:550.39
1,2-Dichloroethane-d4 (S)%98 70-130 10/09/23 00:55
4-Bromofluorobenzene (S)%99 70-130 10/09/23 00:55
Toluene-d8 (S)%101 70-130 10/09/23 00:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4168316LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 20.120 100 70-130
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130
1,1,2-Trichloroethane ug/L 20.320 102 70-130
1,1,2-Trichlorotrifluoroethane ug/L 21.120 105 70-132
1,1-Dichloroethane ug/L 18.720 93 70-130
1,1-Dichloroethene ug/L 20.120 101 69-131
1,2,4-Trichlorobenzene ug/L 19.520 97 70-130
1,2-Dibromo-3-chloropropane ug/L 19.420 97 70-130
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130
1,2-Dichlorobenzene ug/L 20.220 101 70-130
1,2-Dichloroethane ug/L 20.320 102 70-130
1,2-Dichloropropane ug/L 20.420 102 70-130
1,3-Dichlorobenzene ug/L 19.920 99 70-130
1,4-Dichlorobenzene ug/L 19.620 98 70-130
2-Butanone (MEK)ug/L 34.740 87 67-133
2-Hexanone ug/L 39.940 100 70-133
4-Methyl-2-pentanone (MIBK)ug/L 38.440 96 70-130
Acetone ug/L 39.640 99 67-130
Benzene ug/L 19.620 98 70-130
Bromodichloromethane ug/L 19.020 95 70-130
Bromoform ug/L 18.820 94 70-133
Bromomethane ug/L 17.320 87 41-148
Carbon disulfide ug/L 19.420 97 70-131
Carbon tetrachloride ug/L 20.520 102 70-130
Chlorobenzene ug/L 20.020 100 70-130
Chloroethane ug/L 19.020 95 41-157
Chloroform ug/L 18.520 93 70-130
Chloromethane ug/L 16.820 84 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4168316LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 18.820 94 70-130
cis-1,3-Dichloropropene ug/L 19.620 98 70-130
Cyclohexane ug/L 19.920 100 63-137
Dibromochloromethane ug/L 19.620 98 70-130
Dichlorodifluoromethane ug/L 21.120 106 54-147
Ethylbenzene ug/L 19.720 99 70-130
Isopropylbenzene (Cumene)ug/L 19.720 99 70-130
m&p-Xylene ug/L 38.640 96 70-130
Methyl acetate ug/L 17.420 87 70-130
Methyl-tert-butyl ether ug/L 19.520 97 70-130
Methylcyclohexane ug/L 21.820 109 70-130
Methylene Chloride ug/L 19.220 96 62-130
o-Xylene ug/L 19.220 96 70-130
Styrene ug/L 19.120 95 70-130
Tetrachloroethene ug/L 19.220 96 70-130
Toluene ug/L 18.820 94 70-130
trans-1,2-Dichloroethene ug/L 18.820 94 70-130
trans-1,3-Dichloropropene ug/L 18.920 95 70-130
Trichloroethene ug/L 21.020 105 70-130
Trichlorofluoromethane ug/L 20.620 103 57-130
Vinyl chloride ug/L 15.520 77 66-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4168318MATRIX SPIKE SAMPLE:
MSSpike
Result
92691088004
1,1,1-Trichloroethane ug/L 21.120 105 70-150ND
1,1,2,2-Tetrachloroethane ug/L 22.220 111 66-144ND
1,1,2-Trichloroethane ug/L 20.620 103 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 23.620 118 66-168ND
1,1-Dichloroethane ug/L 20.620 103 68-150ND
1,1-Dichloroethene ug/L 21.720 109 64-162ND
1,2,4-Trichlorobenzene ug/L 20.120 101 69-147ND
1,2-Dibromo-3-chloropropane ug/L 21.120 106 62-146ND
1,2-Dibromoethane (EDB)ug/L 21.220 106 70-143ND
1,2-Dichlorobenzene ug/L 21.120 105 70-142ND
1,2-Dichloroethane ug/L 20.320 101 68-145ND
1,2-Dichloropropane ug/L 21.420 107 70-144ND
1,3-Dichlorobenzene ug/L 21.220 106 70-142ND
1,4-Dichlorobenzene ug/L 21.020 105 70-140ND
2-Butanone (MEK)ug/L 44.240 111 57-156ND
2-Hexanone ug/L 43.840 109 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 42.740 107 65-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4168318MATRIX SPIKE SAMPLE:
MSSpike
Result
92691088004
Acetone ug/L 39.840 97 49-162ND
Benzene ug/L 20.920 104 68-144ND
Bromodichloromethane ug/L 20.120 101 70-141ND
Bromoform ug/L 20.120 101 59-144ND
Bromomethane ug/L 16.0 v32080 23-190ND
Carbon disulfide ug/L 21.420 107 64-160ND
Carbon tetrachloride ug/L 21.520 108 70-147ND
Chlorobenzene ug/L 21.120 105 70-143ND
Chloroethane ug/L 20.020 100 55-190ND
Chloroform ug/L 20.720 104 67-148ND
Chloromethane ug/L 18.020 90 38-180ND
cis-1,2-Dichloroethene ug/L 20.620 103 67-151ND
cis-1,3-Dichloropropene ug/L 20.520 102 70-142ND
Cyclohexane ug/L 23.720 118 64-162ND
Dibromochloromethane ug/L 20.320 102 68-140ND
Dichlorodifluoromethane ug/L 24.220 121 15-200ND
Ethylbenzene ug/L 21.020 105 70-145ND
Isopropylbenzene (Cumene)ug/L 21.720 108 70-144ND
m&p-Xylene ug/L 41.540 104 70-148ND
Methyl acetate ug/L 19.320 96 62-144ND
Methyl-tert-butyl ether ug/L 18.720 94 64-146ND
Methylcyclohexane ug/L 25.620 128 70-155ND
Methylene Chloride ug/L 20.920 103 54-149ND
o-Xylene ug/L 20.720 103 70-145ND
Styrene ug/L 20.820 104 70-147ND
Tetrachloroethene ug/L 21.420 107 70-145ND
Toluene ug/L 20.620 103 65-146ND
trans-1,2-Dichloroethene ug/L 21.020 105 69-155ND
trans-1,3-Dichloropropene ug/L 20.220 101 70-142ND
Trichloroethene ug/L 21.320 106 70-152ND
Trichlorofluoromethane ug/L 21.120 106 60-158ND
Vinyl chloride ug/L 17.620 88 51-178ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92691088003
4168317SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92691088003
4168317SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L 3.1 2 303.1
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9897
4-Bromofluorobenzene (S)%9799
Toluene-d8 (S)%100104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
805089
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92690981002, 92690981003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4169165
Associated Lab Samples:92690981002, 92690981003
Matrix: Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 1.0 10/09/23 13:530.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/09/23 13:530.22
1,1,2-Trichloroethane ug/L ND 1.0 10/09/23 13:530.32
1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 10/09/23 13:530.32
1,1-Dichloroethane ug/L ND 1.0 10/09/23 13:530.37
1,1-Dichloroethene ug/L ND 1.0 10/09/23 13:530.35
1,2,4-Trichlorobenzene ug/L ND 1.0 10/09/23 13:530.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/09/23 13:530.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/09/23 13:530.27
1,2-Dichlorobenzene ug/L ND 1.0 10/09/23 13:530.34
1,2-Dichloroethane ug/L ND 1.0 10/09/23 13:530.32
1,2-Dichloropropane ug/L ND 1.0 10/09/23 13:530.36
1,3-Dichlorobenzene ug/L ND 1.0 10/09/23 13:530.34
1,4-Dichlorobenzene ug/L ND 1.0 10/09/23 13:530.33
2-Butanone (MEK)ug/L ND 5.0 10/09/23 13:534.0
2-Hexanone ug/L ND 5.0 10/09/23 13:530.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/09/23 13:532.7
Acetone ug/L ND 25.0 10/09/23 13:535.1
Benzene ug/L ND 1.0 10/09/23 13:530.34
Bromodichloromethane ug/L ND 1.0 10/09/23 13:530.31
Bromoform ug/L ND 1.0 10/09/23 13:530.34
Bromomethane ug/L ND 2.0 v210/09/23 13:531.7
Carbon disulfide ug/L ND 2.0 10/09/23 13:530.36
Carbon tetrachloride ug/L ND 1.0 10/09/23 13:530.33
Chlorobenzene ug/L ND 1.0 10/09/23 13:530.28
Chloroethane ug/L ND 1.0 10/09/23 13:530.65
Chloroform ug/L ND 1.0 10/09/23 13:530.43
Chloromethane ug/L ND 1.0 10/09/23 13:530.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/09/23 13:530.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/09/23 13:530.36
Cyclohexane ug/L ND 1.0 10/09/23 13:530.35
Dibromochloromethane ug/L ND 1.0 10/09/23 13:530.36
Dichlorodifluoromethane ug/L ND 1.0 10/09/23 13:530.35
Ethylbenzene ug/L ND 1.0 10/09/23 13:530.30
Isopropylbenzene (Cumene)ug/L ND 1.0 10/09/23 13:530.33
m&p-Xylene ug/L ND 2.0 10/09/23 13:530.71
Methyl acetate ug/L ND 10.0 10/09/23 13:532.4
Methyl-tert-butyl ether ug/L ND 1.0 10/09/23 13:530.42
Methylcyclohexane ug/L ND 10.0 10/09/23 13:531.5
Methylene Chloride ug/L ND 5.0 10/09/23 13:532.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4169165
Associated Lab Samples:92690981002, 92690981003
Matrix: Water
AnalyzedMDL
o-Xylene ug/L ND 1.0 10/09/23 13:530.34
Styrene ug/L ND 1.0 10/09/23 13:530.29
Tetrachloroethene ug/L ND 1.0 10/09/23 13:530.29
Toluene ug/L ND 1.0 10/09/23 13:530.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/09/23 13:530.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/09/23 13:530.36
Trichloroethene ug/L ND 1.0 10/09/23 13:530.38
Trichlorofluoromethane ug/L ND 1.0 10/09/23 13:530.30
Vinyl chloride ug/L ND 1.0 10/09/23 13:530.39
1,2-Dichloroethane-d4 (S)%98 70-130 10/09/23 13:53
4-Bromofluorobenzene (S)%99 70-130 10/09/23 13:53
Toluene-d8 (S)%101 70-130 10/09/23 13:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4169166LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 19.020 95 70-130
1,1,2,2-Tetrachloroethane ug/L 20.820 104 70-130
1,1,2-Trichloroethane ug/L 19.720 99 70-130
1,1,2-Trichlorotrifluoroethane ug/L 19.720 99 70-132
1,1-Dichloroethane ug/L 19.320 96 70-130
1,1-Dichloroethene ug/L 19.520 97 69-131
1,2,4-Trichlorobenzene ug/L 19.720 99 70-130
1,2-Dibromo-3-chloropropane ug/L 20.820 104 70-130
1,2-Dibromoethane (EDB)ug/L 19.820 99 70-130
1,2-Dichlorobenzene ug/L 20.120 100 70-130
1,2-Dichloroethane ug/L 19.020 95 70-130
1,2-Dichloropropane ug/L 19.620 98 70-130
1,3-Dichlorobenzene ug/L 20.020 100 70-130
1,4-Dichlorobenzene ug/L 19.720 98 70-130
2-Butanone (MEK)ug/L 41.740 104 67-133
2-Hexanone ug/L 42.940 107 70-133
4-Methyl-2-pentanone (MIBK)ug/L 42.040 105 70-130
Acetone ug/L 40.840 102 67-130
Benzene ug/L 19.420 97 70-130
Bromodichloromethane ug/L 18.720 93 70-130
Bromoform ug/L 19.520 98 70-133
Bromomethane ug/L 12.0 v32060 41-148
Carbon disulfide ug/L 19.120 96 70-131
Carbon tetrachloride ug/L 19.220 96 70-130
Chlorobenzene ug/L 19.420 97 70-130
Chloroethane ug/L 18.720 93 41-157
Chloroform ug/L 18.520 93 70-130
Chloromethane ug/L 16.420 82 59-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4169166LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 19.620 98 70-130
cis-1,3-Dichloropropene ug/L 19.520 97 70-130
Cyclohexane ug/L 20.120 100 63-137
Dibromochloromethane ug/L 19.120 95 70-130
Dichlorodifluoromethane ug/L 20.320 101 54-147
Ethylbenzene ug/L 19.120 95 70-130
Isopropylbenzene (Cumene)ug/L 19.620 98 70-130
m&p-Xylene ug/L 37.940 95 70-130
Methyl acetate ug/L 18.820 94 70-130
Methyl-tert-butyl ether ug/L 17.920 90 70-130
Methylcyclohexane ug/L 21.320 107 70-130
Methylene Chloride ug/L 20.120 101 62-130
o-Xylene ug/L 19.320 96 70-130
Styrene ug/L 19.420 97 70-130
Tetrachloroethene ug/L 19.020 95 70-130
Toluene ug/L 19.020 95 70-130
trans-1,2-Dichloroethene ug/L 19.320 96 70-130
trans-1,3-Dichloropropene ug/L 19.220 96 70-130
Trichloroethene ug/L 19.720 99 70-130
Trichlorofluoromethane ug/L 18.020 90 57-130
Vinyl chloride ug/L 15.820 79 66-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4169167MATRIX SPIKE SAMPLE:
MSSpike
Result
92692091001
1,1,1-Trichloroethane ug/L 21.920 109 70-150ND
1,1,2,2-Tetrachloroethane ug/L 22.020 110 66-144ND
1,1,2-Trichloroethane ug/L 21.320 106 70-142ND
1,1,2-Trichlorotrifluoroethane ug/L 24.020 120 66-168ND
1,1-Dichloroethane ug/L 21.620 108 68-150ND
1,1-Dichloroethene ug/L 22.420 112 64-162ND
1,2,4-Trichlorobenzene ug/L 20.420 102 69-147ND
1,2-Dibromo-3-chloropropane ug/L 21.720 109 62-146ND
1,2-Dibromoethane (EDB)ug/L 21.420 107 70-143ND
1,2-Dichlorobenzene ug/L 21.520 107 70-142ND
1,2-Dichloroethane ug/L 20.520 102 68-145ND
1,2-Dichloropropane ug/L 21.920 110 70-144ND
1,3-Dichlorobenzene ug/L 21.420 107 70-142ND
1,4-Dichlorobenzene ug/L 21.220 106 70-140ND
2-Butanone (MEK)ug/L 43.740 109 57-156ND
2-Hexanone ug/L 44.040 110 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 42.640 107 65-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4169167MATRIX SPIKE SAMPLE:
MSSpike
Result
92692091001
Acetone ug/L 41.040 100 49-162ND
Benzene ug/L 21.720 108 68-144ND
Bromodichloromethane ug/L 20.920 105 70-141ND
Bromoform ug/L 21.020 105 59-144ND
Bromomethane ug/L 16.220 71 23-1902.0
Carbon disulfide ug/L 21.3 v320106 64-160ND
Carbon tetrachloride ug/L 23.220 116 70-147ND
Chlorobenzene ug/L 22.020 110 70-143ND
Chloroethane ug/L 21.020 105 55-190ND
Chloroform ug/L 20.920 104 67-148ND
Chloromethane ug/L 21.220 104 38-180ND
cis-1,2-Dichloroethene ug/L 21.520 107 67-151ND
cis-1,3-Dichloropropene ug/L 20.720 104 70-142ND
Cyclohexane ug/L 23.620 118 64-162ND
Dibromochloromethane ug/L 21.620 108 68-140ND
Dichlorodifluoromethane ug/L 26.220 131 15-200ND
Ethylbenzene ug/L 21.520 107 70-145ND
Isopropylbenzene (Cumene)ug/L 21.920 110 70-144ND
m&p-Xylene ug/L 42.340 106 70-148ND
Methyl acetate ug/L 19.020 95 62-144ND
Methyl-tert-butyl ether ug/L 18.820 94 64-146ND
Methylcyclohexane ug/L 25.320 127 70-155ND
Methylene Chloride ug/L 21.320 106 54-149ND
o-Xylene ug/L 21.220 106 70-145ND
Styrene ug/L 15.420 77 70-147ND
Tetrachloroethene ug/L 21.820 109 70-145ND
Toluene ug/L 21.020 105 65-146ND
trans-1,2-Dichloroethene ug/L 21.720 108 69-155ND
trans-1,3-Dichloropropene ug/L 20.720 103 70-142ND
Trichloroethene ug/L 22.220 111 70-152ND
Trichlorofluoromethane ug/L 22.220 111 60-158ND
Vinyl chloride ug/L 19.520 98 51-178ND
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92692091002
4169168SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1,2-Trichlorotrifluoroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92692091002
4169168SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 302.1
Carbon disulfide ug/L ND v230ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Cyclohexane ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Isopropylbenzene (Cumene)ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl acetate ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylcyclohexane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
o-Xylene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%95100
4-Bromofluorobenzene (S)%9699
Toluene-d8 (S)%100100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804310
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92690981001, 92690981002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4165394
Associated Lab Samples:92690981001, 92690981002
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 10/06/23 11:591.2
2,4,5-Trichlorophenol ug/L ND 10.0 10/06/23 11:591.4
2,4,6-Trichlorophenol ug/L ND 10.0 10/06/23 11:591.6
2,4-Dichlorophenol ug/L ND 10.0 10/06/23 11:591.4
2,4-Dimethylphenol ug/L ND 10.0 10/06/23 11:591.7
2,4-Dinitrophenol ug/L ND 50.0 10/06/23 11:5926.0
2,4-Dinitrotoluene ug/L ND 10.0 10/06/23 11:591.6
2,6-Dinitrotoluene ug/L ND 10.0 10/06/23 11:591.7
2-Chloronaphthalene ug/L ND 10.0 10/06/23 11:591.7
2-Chlorophenol ug/L ND 10.0 10/06/23 11:591.2
2-Methylnaphthalene ug/L ND 10.0 10/06/23 11:591.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 10/06/23 11:591.9
2-Nitroaniline ug/L ND 20.0 10/06/23 11:593.0
2-Nitrophenol ug/L ND 10.0 10/06/23 11:591.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 10/06/23 11:591.2
3,3'-Dichlorobenzidine ug/L ND 20.0 10/06/23 11:598.1
3-Nitroaniline ug/L ND 20.0 10/06/23 11:593.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 10/06/23 11:597.8
4-Bromophenylphenyl ether ug/L ND 10.0 10/06/23 11:591.8
4-Chloro-3-methylphenol ug/L ND 10.0 10/06/23 11:593.3
4-Chloroaniline ug/L ND 20.0 10/06/23 11:593.6
4-Chlorophenylphenyl ether ug/L ND 10.0 10/06/23 11:592.0
4-Nitroaniline ug/L ND 20.0 10/06/23 11:595.1
4-Nitrophenol ug/L ND 50.0 10/06/23 11:596.6
Acenaphthene ug/L ND 10.0 10/06/23 11:592.0
Acenaphthylene ug/L ND 10.0 10/06/23 11:592.0
Acetophenone ug/L ND 10.0 10/06/23 11:591.5
Anthracene ug/L ND 10.0 10/06/23 11:592.3
Atrazine ug/L ND 10.0 10/06/23 11:593.2
Benzaldehyde ug/L ND 10.0 10/06/23 11:593.6
Benzo(a)anthracene ug/L ND 10.0 10/06/23 11:592.7
Benzo(a)pyrene ug/L ND 10.0 10/06/23 11:592.8
Benzo(b)fluoranthene ug/L ND 10.0 10/06/23 11:592.6
Benzo(g,h,i)perylene ug/L ND 10.0 10/06/23 11:592.8
Benzo(k)fluoranthene ug/L ND 10.0 10/06/23 11:592.7
Biphenyl (Diphenyl)ug/L ND 10.0 10/06/23 11:591.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 10/06/23 11:591.8
bis(2-Chloroethyl) ether ug/L ND 10.0 10/06/23 11:591.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 10/06/23 11:593.7
Butylbenzylphthalate ug/L ND 10.0 10/06/23 11:593.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4165394
Associated Lab Samples:92690981001, 92690981002
Matrix: Water
AnalyzedMDL
Caprolactam ug/L ND 10.0 10/06/23 11:596.9
Carbazole ug/L ND 10.0 10/06/23 11:592.4
Chrysene ug/L ND 10.0 10/06/23 11:592.8
Di-n-butylphthalate ug/L ND 10.0 10/06/23 11:592.2
Di-n-octylphthalate ug/L ND 10.0 10/06/23 11:593.9
Dibenz(a,h)anthracene ug/L ND 10.0 10/06/23 11:593.0
Dibenzofuran ug/L ND 10.0 10/06/23 11:592.1
Diethylphthalate ug/L ND 10.0 10/06/23 11:592.0
Dimethylphthalate ug/L ND 10.0 10/06/23 11:592.1
Fluoranthene ug/L ND 10.0 10/06/23 11:592.2
Fluorene ug/L ND 10.0 10/06/23 11:592.1
Hexachloro-1,3-butadiene ug/L ND 10.0 10/06/23 11:591.8
Hexachlorobenzene ug/L ND 10.0 10/06/23 11:592.2
Hexachlorocyclopentadiene ug/L ND 10.0 10/06/23 11:591.6
Hexachloroethane ug/L ND 10.0 10/06/23 11:591.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 10/06/23 11:592.9
Isophorone ug/L ND 10.0 10/06/23 11:591.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 10/06/23 11:591.3
N-Nitrosodiphenylamine ug/L ND 10.0 10/06/23 11:593.0
Naphthalene ug/L ND 10.0 10/06/23 11:592.1
Nitrobenzene ug/L ND 10.0 10/06/23 11:591.9
Pentachlorophenol ug/L ND 20.0 10/06/23 11:593.8
Phenanthrene ug/L ND 10.0 10/06/23 11:592.0
Phenol ug/L ND 10.0 10/06/23 11:591.4
Pyrene ug/L ND 10.0 10/06/23 11:592.2
2,4,6-Tribromophenol (S)%72 10-164 10/06/23 11:59
2-Fluorobiphenyl (S)%58 10-130 10/06/23 11:59
2-Fluorophenol (S)%47 10-130 10/06/23 11:59
Nitrobenzene-d5 (S)%68 10-138 10/06/23 11:59
Phenol-d6 (S)%32 10-130 10/06/23 11:59
Terphenyl-d14 (S)%78 19-191 10/06/23 11:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4165395LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 38.950 78 21-135
2,4,5-Trichlorophenol ug/L 55.950 112 38-147
2,4,6-Trichlorophenol ug/L 53.750 107 34-142
2,4-Dichlorophenol ug/L 48.050 96 36-136
2,4-Dimethylphenol ug/L 47.250 94 38-134
2,4-Dinitrophenol ug/L 258250 103 10-169
2,4-Dinitrotoluene ug/L 55.850 112 44-154
2,6-Dinitrotoluene ug/L 55.650 111 44-156
2-Chloronaphthalene ug/L 45.550 91 25-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4165395LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 47.750 95 29-130
2-Methylnaphthalene ug/L 45.350 91 23-130
2-Methylphenol(o-Cresol)ug/L 41.150 82 31-130
2-Nitroaniline ug/L 108100 108 39-145
2-Nitrophenol ug/L 49.250 98 29-142
3&4-Methylphenol(m&p Cresol)ug/L 40.950 82 30-130
3,3'-Dichlorobenzidine ug/L 128100 128 44-158
3-Nitroaniline ug/L 111100 111 45-152
4,6-Dinitro-2-methylphenol ug/L 106100 106 39-158
4-Bromophenylphenyl ether ug/L 53.550 107 47-147
4-Chloro-3-methylphenol ug/L 94.7100 95 40-138
4-Chloroaniline ug/L 88.6100 89 35-130
4-Chlorophenylphenyl ether ug/L 51.850 104 36-139
4-Nitroaniline ug/L 115100 115 46-157
4-Nitrophenol ug/L 156250 62 17-130
Acenaphthene ug/L 47.350 95 34-135
Acenaphthylene ug/L 47.950 96 35-137
Acetophenone ug/L 43.750 87 30-137
Anthracene ug/L 51.250 102 47-146
Atrazine ug/L 49.450 99 30-130
Benzaldehyde ug/L 48.850 98 17-167
Benzo(a)anthracene ug/L 54.750 109 48-160
Benzo(a)pyrene ug/L 56.550 113 47-165
Benzo(b)fluoranthene ug/L 64.550 129 49-171
Benzo(g,h,i)perylene ug/L 55.550 111 46-166
Benzo(k)fluoranthene ug/L 56.750 113 55-162
Biphenyl (Diphenyl)ug/L 45.850 92 28-130
bis(2-Chloroethoxy)methane ug/L 46.150 92 33-136
bis(2-Chloroethyl) ether ug/L 44.950 90 30-142
bis(2-Ethylhexyl)phthalate ug/L 58.350 117 46-173
Butylbenzylphthalate ug/L 56.350 113 53-169
Caprolactam ug/L 27.850 56 13-130
Carbazole ug/L 55.250 110 48-157
Chrysene ug/L 54.950 110 54-152
Di-n-butylphthalate ug/L 53.750 107 49-161
Di-n-octylphthalate ug/L 60.850 122 50-166
Dibenz(a,h)anthracene ug/L 55.850 112 46-166
Dibenzofuran ug/L 47.950 96 37-136
Diethylphthalate ug/L 52.350 105 45-149
Dimethylphthalate ug/L 51.150 102 43-145
Fluoranthene ug/L 56.050 112 50-153
Fluorene ug/L 50.050 100 42-142
Hexachloro-1,3-butadiene ug/L 38.150 76 10-130
Hexachlorobenzene ug/L 53.150 106 44-138
Hexachlorocyclopentadiene ug/L 47.350 95 10-130
Hexachloroethane ug/L 30.850 62 10-130
Indeno(1,2,3-cd)pyrene ug/L 53.550 107 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4165395LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 47.250 94 36-135
N-Nitroso-di-n-propylamine ug/L 51.350 103 33-140
N-Nitrosodiphenylamine ug/L 51.750 103 46-144
Naphthalene ug/L 40.650 81 20-130
Nitrobenzene ug/L 45.250 90 33-133
Pentachlorophenol ug/L 103100 103 21-163
Phenanthrene ug/L 50.850 102 47-146
Phenol ug/L 29.550 59 19-130
Pyrene ug/L 53.950 108 53-155
2,4,6-Tribromophenol (S)%133 10-164
2-Fluorobiphenyl (S)%99 10-130
2-Fluorophenol (S)%77 10-130
Nitrobenzene-d5 (S)%104 10-138
Phenol-d6 (S)%62 10-130
Terphenyl-d14 (S)%102 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4165396MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690988001
4165397
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-
chloropropane)ug/L 83.3 72 11-14384 16 3083.3ND 60.1 70.3
2,4,5-Trichlorophenol ug/L R183.3 51 10-170125 83 3083.3ND 42.8 104
2,4,6-Trichlorophenol ug/L R183.3 27 10-166117 124 3083.3ND 22.8 97.6
2,4-Dichlorophenol ug/L R183.3 49 10-153114 79 3083.3ND 40.9 94.6
2,4-Dimethylphenol ug/L 83.3 86 20-147111 26 3083.3ND 71.3 92.7
2,4-Dinitrophenol ug/L M1417010-172111 30417NDND 461
2,4-Dinitrotoluene ug/L 83.3 109 30-164118 8 3083.3ND 91.0 98.3
2,6-Dinitrotoluene ug/L 83.3 114 31-163124 8 3083.3ND 95.0 103
2-Chloronaphthalene ug/L 83.3 82 15-134102 22 3083.3ND 68.5 85.1
2-Chlorophenol ug/L R183.3 56 10-139106 61 3083.3ND 46.8 88.1
2-Methylnaphthalene ug/L 83.3 83 12-130109 28 3083.3ND 68.8 90.8
2-Methylphenol(o-Cresol) ug/L 83.3 70 19-13291 26 3083.3ND 58.7 76.1
2-Nitroaniline ug/L 167 105 23-154118 11 30167ND176 197
2-Nitrophenol ug/L R183.3 54 10-159117 73 3083.3ND 45.0 97.2
3&4-Methylphenol(m&p
Cresol)
ug/L 83.3 71 13-13694 27 3083.3ND 59.4 78.3
3,3'-Dichlorobenzidine ug/L 167 141 10-178136 4 30167ND235 226
3-Nitroaniline ug/L 167 120 20-166121 1 30167ND200 201
4,6-Dinitro-2-methylphenol ug/L 167 10 10-187115 30167ND17.4J 192
4-Bromophenylphenyl ether ug/L 83.3 108 31-157119 10 3083.3ND 89.6 99.3
4-Chloro-3-methylphenol ug/L 167 87 27-146112 25 30167ND146 187
4-Chloroaniline ug/L 167 90 13-143109 19 30167ND150 181
4-Chlorophenylphenyl ether ug/L 83.3 101 23-149118 15 3083.3ND 84.1 97.9
4-Nitroaniline ug/L 167 122 24-171125 2 30167ND204 208
4-Nitrophenol ug/L M1417010-13065 30417NDND 273
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
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[phone]
Page 42 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4165396MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690988001
4165397
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L 83.3 86 21-147104 19 3083.3ND 71.7 86.5
Acenaphthylene ug/L 83.3 89 19-150106 18 3083.3ND 73.9 88.4
Acetophenone ug/L 83.3 82 22-14598 17 3083.3ND 68.6 81.5
Anthracene ug/L 83.3 108 36-152111 3 3083.3ND 90.1 92.4
Atrazine ug/L 83.3 128 18-17398 26 3083.3ND 106 81.8
Benzaldehyde ug/L 83.3 97 16-16395 2 3083.3ND 81.0 79.3
Benzo(a)anthracene ug/L 83.3 122 42-163117 4 3083.3ND 101 97.6
Benzo(a)pyrene ug/L 83.3 127 40-169123 3 3083.3ND 105 103
Benzo(b)fluoranthene ug/L 83.3 141 40-177137 3 3083.3ND 117 114
Benzo(g,h,i)perylene ug/L 83.3 121 38-174120 1 3083.3ND 101 99.7
Benzo(k)fluoranthene ug/L 83.3 124 41-171127 2 3083.3ND 103 105
Biphenyl (Diphenyl)ug/L 83.3 84 14-137102 19 3083.3ND 70.0 85.0
bis(2-
Chloroethoxy)methane ug/L 83.3 85 19-146106 22 3083.3ND 70.9 88.2
bis(2-Chloroethyl) ether ug/L 83.3 86 19-151101 16 3083.3ND 71.8 84.3
bis(2-Ethylhexyl)phthalate ug/L 83.3 129 42-168123 4 3083.3ND 107 102
Butylbenzylphthalate ug/L 83.3 126 42-177122 3 3083.3ND 105 102
Caprolactam ug/L R183.3 31 10-13049 34 3083.311.5 37.2 52.3
Carbazole ug/L 83.3 121 38-164119 1 3083.3ND 100 99.1
Chrysene ug/L 83.3 118 43-159114 4 3083.3ND 98.7 95.1
Di-n-butylphthalate ug/L 83.3 117 42-160114 2 3083.3ND 98.4 96.2
Di-n-octylphthalate ug/L 83.3 135 42-171129 5 3083.3ND 112 107
Dibenz(a,h)anthracene ug/L 83.3 124 40-171121 2 3083.3ND 103 101
Dibenzofuran ug/L 83.3 88 23-147106 19 3083.3ND 73.6 88.6
Diethylphthalate ug/L 83.3 102 33-157105 3 3083.36.2J 91.2 94.1
Dimethylphthalate ug/L 83.3 102 27-154113 11 3083.3ND 84.8 94.4
Fluoranthene ug/L 83.3 124 42-157121 2 3083.3ND 103 101
Fluorene ug/L 83.3 96 25-155110 13 3083.3ND 80.4 92.0
Hexachloro-1,3-butadiene ug/L R183.3 65 10-130100 43 3083.3ND 54.1 83.6
Hexachlorobenzene ug/L 83.3 110 32-145116 5 3083.3ND 91.6 96.5
Hexachlorocyclopentadiene ug/L R183.3 78 10-130111 35 3083.3ND 64.8 92.3
Hexachloroethane ug/L R183.3 54 10-13076 33 3083.3ND 45.3 63.4
Indeno(1,2,3-cd)pyrene ug/L 83.3 117 39-174117 0 3083.3ND 97.6 97.2
Isophorone ug/L 83.3 88 19-146110 22 3083.3ND 73.6 92.0
N-Nitroso-di-n-propylamine ug/L 83.3 96 20-150115 18 3083.3ND 79.8 96.0
N-Nitrosodiphenylamine ug/L 83.3 108 33-149112 4 3083.3ND 89.9 93.7
Naphthalene ug/L 83.3 75 10-12897 26 3083.3ND 62.2 80.4
Nitrobenzene ug/L 83.3 85 19-145103 20 3083.3ND 70.7 86.0
Pentachlorophenol ug/L 167 13 10-188109 30167ND21.3J 181
Phenanthrene ug/L 83.3 108 38-150111 2 3083.3ND 90.0 92.2
Phenol ug/L R183.3 44 10-13068 42 3083.3ND 36.8 56.5
Pyrene ug/L 83.3 118 42-163115 2 3083.3ND 98.0 95.6
2,4,6-Tribromophenol (S) %63 10-164133
2-Fluorobiphenyl (S)%92 10-130103
2-Fluorophenol (S)%30 10-13079
Nitrobenzene-d5 (S)%97 10-138109
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4165396MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92690988001
4165397
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%40 10-13062
Terphenyl-d14 (S)%108 19-19198
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804890
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92690981003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4168267
Associated Lab Samples:92690981003
Matrix: Water
AnalyzedMDL
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 10/09/23 18:091.2
2,4,5-Trichlorophenol ug/L ND 10.0 10/09/23 18:091.4
2,4,6-Trichlorophenol ug/L ND 10.0 10/09/23 18:091.6
2,4-Dichlorophenol ug/L ND 10.0 10/09/23 18:091.4
2,4-Dimethylphenol ug/L ND 10.0 10/09/23 18:091.7
2,4-Dinitrophenol ug/L ND 50.0 10/09/23 18:0926.0
2,4-Dinitrotoluene ug/L ND 10.0 10/09/23 18:091.6
2,6-Dinitrotoluene ug/L ND 10.0 10/09/23 18:091.7
2-Chloronaphthalene ug/L ND 10.0 10/09/23 18:091.7
2-Chlorophenol ug/L ND 10.0 10/09/23 18:091.2
2-Methylnaphthalene ug/L ND 10.0 10/09/23 18:091.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 10/09/23 18:091.9
2-Nitroaniline ug/L ND 20.0 10/09/23 18:093.0
2-Nitrophenol ug/L ND 10.0 10/09/23 18:091.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 10/09/23 18:091.2
3,3'-Dichlorobenzidine ug/L ND 20.0 10/09/23 18:098.1
3-Nitroaniline ug/L ND 20.0 10/09/23 18:093.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 10/09/23 18:097.8
4-Bromophenylphenyl ether ug/L ND 10.0 10/09/23 18:091.8
4-Chloro-3-methylphenol ug/L ND 10.0 10/09/23 18:093.3
4-Chloroaniline ug/L ND 20.0 10/09/23 18:093.6
4-Chlorophenylphenyl ether ug/L ND 10.0 10/09/23 18:092.0
4-Nitroaniline ug/L ND 20.0 10/09/23 18:095.1
4-Nitrophenol ug/L ND 50.0 10/09/23 18:096.6
Acenaphthene ug/L ND 10.0 10/09/23 18:092.0
Acenaphthylene ug/L ND 10.0 10/09/23 18:092.0
Acetophenone ug/L ND 10.0 10/09/23 18:091.5
Anthracene ug/L ND 10.0 10/09/23 18:092.3
Atrazine ug/L ND 10.0 10/09/23 18:093.2
Benzaldehyde ug/L ND 10.0 10/09/23 18:093.6
Benzo(a)anthracene ug/L ND 10.0 10/09/23 18:092.7
Benzo(a)pyrene ug/L ND 10.0 10/09/23 18:092.8
Benzo(b)fluoranthene ug/L ND 10.0 10/09/23 18:092.6
Benzo(g,h,i)perylene ug/L ND 10.0 10/09/23 18:092.8
Benzo(k)fluoranthene ug/L ND 10.0 10/09/23 18:092.7
Biphenyl (Diphenyl)ug/L ND 10.0 10/09/23 18:091.8
bis(2-Chloroethoxy)methane ug/L ND 10.0 10/09/23 18:091.8
bis(2-Chloroethyl) ether ug/L ND 10.0 10/09/23 18:091.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 10/09/23 18:093.7
Butylbenzylphthalate ug/L ND 10.0 10/09/23 18:093.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4168267
Associated Lab Samples:92690981003
Matrix: Water
AnalyzedMDL
Caprolactam ug/L ND 10.0 10/09/23 18:096.9
Carbazole ug/L ND 10.0 10/09/23 18:092.4
Chrysene ug/L ND 10.0 10/09/23 18:092.8
Di-n-butylphthalate ug/L ND 10.0 10/09/23 18:092.2
Di-n-octylphthalate ug/L ND 10.0 10/09/23 18:093.9
Dibenz(a,h)anthracene ug/L ND 10.0 10/09/23 18:093.0
Dibenzofuran ug/L ND 10.0 10/09/23 18:092.1
Diethylphthalate ug/L ND 10.0 10/09/23 18:092.0
Dimethylphthalate ug/L ND 10.0 10/09/23 18:092.1
Fluoranthene ug/L ND 10.0 10/09/23 18:092.2
Fluorene ug/L ND 10.0 10/09/23 18:092.1
Hexachloro-1,3-butadiene ug/L ND 10.0 10/09/23 18:091.8
Hexachlorobenzene ug/L ND 10.0 10/09/23 18:092.2
Hexachlorocyclopentadiene ug/L ND 10.0 v110/09/23 18:091.6
Hexachloroethane ug/L ND 10.0 10/09/23 18:091.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 10/09/23 18:092.9
Isophorone ug/L ND 10.0 10/09/23 18:091.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 10/09/23 18:091.3
N-Nitrosodiphenylamine ug/L ND 10.0 10/09/23 18:093.0
Naphthalene ug/L ND 10.0 10/09/23 18:092.1
Nitrobenzene ug/L ND 10.0 10/09/23 18:091.9
Pentachlorophenol ug/L ND 20.0 10/09/23 18:093.8
Phenanthrene ug/L ND 10.0 10/09/23 18:092.0
Phenol ug/L ND 10.0 10/09/23 18:091.4
Pyrene ug/L ND 10.0 10/09/23 18:092.2
2,4,6-Tribromophenol (S)%131 10-164 10/09/23 18:09
2-Fluorobiphenyl (S)%95 10-130 10/09/23 18:09
2-Fluorophenol (S)%83 10-130 10/09/23 18:09
Nitrobenzene-d5 (S)%116 10-138 10/09/23 18:09
Phenol-d6 (S)%61 10-130 10/09/23 18:09
Terphenyl-d14 (S)%104 19-191 10/09/23 18:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4168268LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 36.550 73 21-135
2,4,5-Trichlorophenol ug/L 56.950 114 38-147
2,4,6-Trichlorophenol ug/L 53.250 106 34-142
2,4-Dichlorophenol ug/L 51.150 102 36-136
2,4-Dimethylphenol ug/L 49.650 99 38-134
2,4-Dinitrophenol ug/L 252250 101 10-169
2,4-Dinitrotoluene ug/L 51.250 102 44-154
2,6-Dinitrotoluene ug/L 54.350 109 44-156
2-Chloronaphthalene ug/L 42.850 86 25-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4168268LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorophenol ug/L 46.850 94 29-130
2-Methylnaphthalene ug/L 44.150 88 23-130
2-Methylphenol(o-Cresol)ug/L 41.450 83 31-130
2-Nitroaniline ug/L 104100 104 39-145
2-Nitrophenol ug/L 52.550 105 29-142
3&4-Methylphenol(m&p Cresol)ug/L 42.550 85 30-130
3,3'-Dichlorobenzidine ug/L 113100 113 44-158
3-Nitroaniline ug/L 106100 106 45-152
4,6-Dinitro-2-methylphenol ug/L 99.0100 99 39-158
4-Bromophenylphenyl ether ug/L 50.350 101 47-147
4-Chloro-3-methylphenol ug/L 100100 100 40-138
4-Chloroaniline ug/L 95.3100 95 35-130
4-Chlorophenylphenyl ether ug/L 51.550 103 36-139
4-Nitroaniline ug/L 107100 107 46-157
4-Nitrophenol ug/L 134250 54 17-130
Acenaphthene ug/L 45.550 91 34-135
Acenaphthylene ug/L 47.350 95 35-137
Acetophenone ug/L 43.150 86 30-137
Anthracene ug/L 46.450 93 47-146
Atrazine ug/L 34.350 69 30-130
Benzaldehyde ug/L 38.950 78 17-167
Benzo(a)anthracene ug/L 48.450 97 48-160
Benzo(a)pyrene ug/L 50.050 100 47-165
Benzo(b)fluoranthene ug/L 54.450 109 49-171
Benzo(g,h,i)perylene ug/L 47.250 94 46-166
Benzo(k)fluoranthene ug/L 50.850 102 55-162
Biphenyl (Diphenyl)ug/L 44.250 88 28-130
bis(2-Chloroethoxy)methane ug/L 47.650 95 33-136
bis(2-Chloroethyl) ether ug/L 45.350 91 30-142
bis(2-Ethylhexyl)phthalate ug/L 53.850 108 46-173
Butylbenzylphthalate ug/L 51.550 103 53-169
Caprolactam ug/L 26.050 52 13-130
Carbazole ug/L 49.950 100 48-157
Chrysene ug/L 47.050 94 54-152
Di-n-butylphthalate ug/L 50.050 100 49-161
Di-n-octylphthalate ug/L 56.350 113 50-166
Dibenz(a,h)anthracene ug/L 48.350 97 46-166
Dibenzofuran ug/L 46.850 94 37-136
Diethylphthalate ug/L 48.450 97 45-149
Dimethylphthalate ug/L 49.050 98 43-145
Fluoranthene ug/L 50.850 102 50-153
Fluorene ug/L 48.250 96 42-142
Hexachloro-1,3-butadiene ug/L 34.450 69 10-130
Hexachlorobenzene ug/L 48.250 96 44-138
Hexachlorocyclopentadiene ug/L 44.6 v15089 10-130
Hexachloroethane ug/L 27.150 54 10-130
Indeno(1,2,3-cd)pyrene ug/L 46.550 93 46-166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4168268LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 50.250 100 36-135
N-Nitroso-di-n-propylamine ug/L 51.550 103 33-140
N-Nitrosodiphenylamine ug/L 47.450 95 46-144
Naphthalene ug/L 38.950 78 20-130
Nitrobenzene ug/L 46.650 93 33-133
Pentachlorophenol ug/L 96.5100 97 21-163
Phenanthrene ug/L 46.650 93 47-146
Phenol ug/L 29.850 60 19-130
Pyrene ug/L 48.950 98 53-155
2,4,6-Tribromophenol (S)%152 10-164
2-Fluorobiphenyl (S)%120 10-130
2-Fluorophenol (S)%96 10-130
Nitrobenzene-d5 (S)%133 10-138
Phenol-d6 (S)%76 10-130
Terphenyl-d14 (S)%113 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4168277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35829241003
4168278
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,2'-Oxybis(1-
chloropropane)ug/L H3504811-14361 24 30501.2U 24.0 30.6
2,4,5-Trichlorophenol ug/L H3508210-170100 20 30501.4U 41.1 50.2
2,4,6-Trichlorophenol ug/L H3507310-16697 28 30501.6U 36.5 48.5
2,4-Dichlorophenol ug/L H3506610-15386 27 30501.4U 32.9 43.2
2,4-Dimethylphenol ug/L H3506620-14785 25 30501.7U 32.9 42.4
2,4-Dinitrophenol ug/L H32508310-17298 17 3025026.0U 207 244
2,4-Dinitrotoluene ug/L H3508830-16496 8 30501.6U 44.2 48.2
2,6-Dinitrotoluene ug/L H3508331-163100 19 30501.7U 41.6 50.2
2-Chloronaphthalene ug/L H3505915-13479 29 30501.7U 29.4 39.3
2-Chlorophenol ug/L H3506010-13978 26 30501.2U 30.1 39.0
2-Methylnaphthalene ug/L H3506412-13080 22 30501.9U 32.0 39.9
2-Methylphenol(o-Cresol) ug/L H3505519-13269 21 30501.9U 27.7 34.3
2-Nitroaniline ug/L H31007923-15498 21 301003.0U 79.1 97.5
2-Nitrophenol ug/L H3506610-15988 29 30501.4U 32.8 44.0
3&4-Methylphenol(m&p
Cresol)
ug/L H3505413-13673 30 30501.2U 26.9 36.5
3,3'-Dichlorobenzidine ug/L H31007210-17879 9 301008.1U 71.9 79.0
3-Nitroaniline ug/L H31008320-16695 13 301003.8U 83.2 95.1
4,6-Dinitro-2-methylphenol ug/L H31008510-18795 11 301007.8U 85.2 95.5
4-Bromophenylphenyl ether ug/L H3507531-15791 19 30501.8U 37.7 45.5
4-Chloro-3-methylphenol ug/L H31007327-14690 20 301003.3U 73.4 90.2
4-Chloroaniline ug/L H31006113-14378 25 301003.6U 60.7 78.2
4-Chlorophenylphenyl ether ug/L H3507423-14992 22 30502.0U 36.8 46.0
4-Nitroaniline ug/L H31009624-171100 3 301005.1U 96.4 99.7
4-Nitrophenol ug/L H32505410-13058 7 302506.6U 134 144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4168277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35829241003
4168278
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acenaphthene ug/L H3506321-14782 26 30502.0U 31.3 40.8
Acenaphthylene ug/L H3506519-15086 27 30502.0U 32.5 42.8
Acetophenone ug/L H3505722-14573 25 30501.5U 28.4 36.5
Anthracene ug/L H3507736-15286 11 30502.3U 38.5 43.0
Atrazine ug/L H3507818-17382 5 30503.2U 39.2 41.0
Benzaldehyde ug/L H3505016-16360 17 30503.6U 25.2 29.9
Benzo(a)anthracene ug/L H3508942-16394 6 30502.7U 44.3 47.1
Benzo(a)pyrene ug/L H3508940-16996 7 30502.8U 44.7 48.1
Benzo(b)fluoranthene ug/L H3509940-177105 7 30502.6U 49.3 52.6
Benzo(g,h,i)perylene ug/L H3508538-17489 5 30502.8U 42.5 44.6
Benzo(k)fluoranthene ug/L H3509441-17196 2 30502.7U 47.0 48.1
Biphenyl (Diphenyl)ug/L H3506014-13779 28 30501.8U 29.8 39.5
bis(2-
Chloroethoxy)methane ug/L H3506119-14678 24 30501.8U 30.7 39.2
bis(2-Chloroethyl) ether ug/L H3505719-15173 25 30501.9U 28.7 36.7
bis(2-Ethylhexyl)phthalate ug/L H3509442-168101 7 30503.7U 48.2 51.7
Butylbenzylphthalate ug/L H3509442-177100 7 30503.1U 46.8 50.1
Caprolactam ug/L H3505110-13058 12 30506.9U 25.5 28.8
Carbazole ug/L H3508938-16495 6 30502.4U 44.6 47.5
Chrysene ug/L H3508643-15993 7 30502.8U 43.2 46.4
Di-n-butylphthalate ug/L H3508942-16093 5 30502.2U 44.3 46.6
Di-n-octylphthalate ug/L H35010342-171110 6 30503.9U 51.6 55.1
Dibenz(a,h)anthracene ug/L H3508640-17191 5 30503.0U 43.0 45.4
Dibenzofuran ug/L H3506423-14785 27 30502.1U 32.2 42.4
Diethylphthalate ug/L H3508333-15791 10 30502.0U 41.3 45.7
Dimethylphthalate ug/L H3507727-15492 17 30502.1U 38.7 45.8
Fluoranthene ug/L H3509042-15796 7 30502.2U 45.0 48.1
Fluorene ug/L H3507025-15588 22 30502.1U 35.1 43.8
Hexachloro-1,3-butadiene ug/L H3505710-13070 20 30501.8U 28.6 34.8
Hexachlorobenzene ug/L H3507532-14591 19 30502.2U 37.7 45.7
Hexachlorocyclopentadiene ug/L H3,v1506410-13087 30 30501.6U 32.1 43.5
Hexachloroethane ug/L H3504510-13055 21 30501.4U 22.5 27.7
Indeno(1,2,3-cd)pyrene ug/L H3508339-17487 5 30502.9U 41.5 43.7
Isophorone ug/L H3506719-14685 24 30501.7U 33.6 42.7
N-Nitroso-di-n-propylamine ug/L H3506820-15088 25 30501.3U 34.2 44.1
N-Nitrosodiphenylamine ug/L H3507733-14990 15 30503.0U 38.4 44.8
Naphthalene ug/L H3505810-12872 21 30502.1U 29.1 35.8
Nitrobenzene ug/L H3506019-14578 26 30501.9U 30.0 39.0
Pentachlorophenol ug/L H31008210-18890 9 301003.8U 82.4 89.9
Phenanthrene ug/L H3507838-15086 11 30502.0U 38.8 43.2
Phenol ug/L H3504010-13053 28 30501.4U 19.9 26.3
Pyrene ug/L H3508942-16395 6 30502.2U 44.5 47.4
2,4,6-Tribromophenol (S) %116 10-164139
2-Fluorobiphenyl (S)%75 10-130104
2-Fluorophenol (S)%60 10-13080
Nitrobenzene-d5 (S)%83 10-138108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4168277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35829241003
4168278
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%48 10-13066
Terphenyl-d14 (S)%91 19-191100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
805525
EPA 9040C
EPA 9040C
9040 pH
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92690981001, 92690981002, 92690981003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92691964003
4171122SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 7.2 H31107.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92690714001
4171933SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 6.0 H30106.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807131
ASTM D4239-05
ASTM D4239-05
ASTM D4239-05 Sulfur
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92690981001, 92690981002, 92690981003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693692001
4179453SAMPLE DUPLICATE:
Sulfur % (w/w)0.214 N24100.205
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693717002
4179454SAMPLE DUPLICATE:
Sulfur % (w/w)0.310 N24100.321
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 57
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
BATCH QUALIFIERS
Batch: 956378
[1]
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 57
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92690981
PACTIV EVERGREEN ADDITIONAL S.
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92690981001 803823CBOF-10022023 SM 2120B-2011
92690981002 803823CBOF-10022023 DUP SM 2120B-2011
92690981003 803823CBUS-10022023 SM 2120B-2011
92690981001 956313 956378CBOF-10022023 EPA 200.7 EPA 200.7
92690981002 956313 956378CBOF-10022023 DUP EPA 200.7 EPA 200.7
92690981003 956313 956378CBUS-10022023 EPA 200.7 EPA 200.7
92690981001 957167 957275CBOF-10022023 EPA 200.7 EPA 200.7
92690981002 957167 957275CBOF-10022023 DUP EPA 200.7 EPA 200.7
92690981003 957167 957275CBUS-10022023 EPA 200.7 EPA 200.7
92690981001 956312 956377CBOF-10022023 EPA 200.8 EPA 200.8
92690981002 956312 956377CBOF-10022023 DUP EPA 200.8 EPA 200.8
92690981003 956312 956377CBUS-10022023 EPA 200.8 EPA 200.8
92690981001 957169 957274CBOF-10022023 EPA 200.8 EPA 200.8
92690981002 957169 957274CBOF-10022023 DUP EPA 200.8 EPA 200.8
92690981003 957169 957274CBUS-10022023 EPA 200.8 EPA 200.8
92690981001 957049 957244CBOF-10022023 EPA 245.1 EPA 245.1
92690981002 957049 957244CBOF-10022023 DUP EPA 245.1 EPA 245.1
92690981003 957049 957244CBUS-10022023 EPA 245.1 EPA 245.1
92690981001 957393 957479CBOF-10022023 EPA 245.1 EPA 245.1
92690981002 957393 957479CBOF-10022023 DUP EPA 245.1 EPA 245.1
92690981003 957393 957479CBUS-10022023 EPA 245.1 EPA 245.1
92690981001 804310 804613CBOF-10022023 EPA 3510C EPA 8270E
92690981002 804310 804613CBOF-10022023 DUP EPA 3510C EPA 8270E
92690981003 804890 805110CBUS-10022023 EPA 3510C EPA 8270E
92690981001 804906CBOF-10022023 EPA 8260D
92690981002 805089CBOF-10022023 DUP EPA 8260D
92690981003 805089CBUS-10022023 EPA 8260D
92690981001 805525CBOF-10022023 EPA 9040C
92690981002 805525CBOF-10022023 DUP EPA 9040C
92690981003 805525CBUS-10022023 EPA 9040C
92690981001 807131CBOF-10022023 ASTM D4239-05
92690981002 807131CBOF-10022023 DUP ASTM D4239-05
92690981003 807131CBUS-10022023 ASTM D4239-05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/19/2023 04:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 57
Page 55 of 57
Page 56 of 57
Pa
g
e

5
7

o
f

5
7

Appendix D
Additional Voluntary PFAS Sampling and Analysis
Documentation

Comparison Summary of Split Groundwater and Surface Water Sample Results for PFAS
Canton Mill, Canton, North Carolina
PZ04 PZ04 PZ21 PZ21 RW01 RW01 RW05 RW05
PZ-4 PZ04WG-091923-20230919 PZ-21 PZ21WG-091923-20230919 RW-1 RW01WG-091923-20230919 RW-5 RW05WG-092023-20230920
9/19/2023 9/19/2023 9/19/2023 9/19/2023 9/19/2023 9/19/2023 9/20/2023 9/20/2023
Normal Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
Sample Description:NCDEQ Split PTVE Split NCDEQ Split PTVE Split NCDEQ Split PTVE Split NCDEQ Split PTVE Split
CAS No. Analyte Units
USEPA Method for PFAS1
801209-99-4 1,1,2,2-Tetrafluoro-2-(1,2,2,2-tetrafluoroethoxy)ethane sulfonic acid (NVHO) ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
801212-59-9 4-(Heptafluoroisopropoxy)hexafluorobutanoic acid (PFECA-G) ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
2416366-18-0 Byproduct 4 (BP4)ng/L 25 U 40 U 0.326 J 3.78 U 0.444 U 3.79 U 25 U 40 U
2416366-19-1 Byproduct 5 (BP5)ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
2416366-21-5 Byproduct 6 (BP6)ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
69087-46-3 EVE Acid ng/L 25 U NA 0.434 U NA 0.444 U NA 25 U NA
13252-13-6 Hexafluoropropylene oxide dimer acid (HFPO-DA, GenX) ng/L 25 U 20 U 0.434 U 1.89 U 0.444 U 1.89 U 25 U 20 U
773804-62-9 Hydro-EVE ng/L 25 U NA 0.434 U NA 0.444 U NA 25 U NA
4151-50-2 N-ETHYL PERFLUOROOCTANE SULFONAMIDE (ETFOSA) ng/L 200 U 40 U 3.47 U 3.78 U 3.55 U 3.79 U 200 U 40 U
1691-99-2 N-ETHYL PERFLUOROOCTANE SULFONAMIDOETHANOL (EtFOSE) ng/L 200 U 40 U 3.47 U 3.78 U 3.55 U 3.79 U 200 U 40 U
2991-50-6 N-ethyl perfluorooctanesulfonamidoacetic acid (NEtFOSAA) ng/L 200 U 40 U 3.47 U 3.78 U 3.55 U 3.79 U 200 U 40 U
31506-32-8 N-METHYL PERFLUOROOCTANE SULFONAMIDE (MEFOSA) ng/L 200 U 40 U 3.47 U 3.78 U 3.55 U 3.79 U 200 U 40 U
24448-09-7 N-METHYL PERFLUOROOCTANE SULFONAMIDOETHANOL (MeFOSE) ng/L 200 U 40 U 3.47 U 3.78 U 3.55 U 3.79 U 200 U 40 U
2355-31-9 N-methyl perfluorooctanesulfonamidoacetic acid (NMeFOSAA) ng/L 200 U 40 U 3.47 U 3.78 U 3.55 U 3.79 U 200 U 40 U
29311-67-9 Nafion Byproduct 1 ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
749836-20-2 Nafion Byproduct 2 ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
151772-58-6 Nonafluoro-3,6-dioxaheptanoic acid (NFDHA) ng/L 25 U NA 0.434 U NA 0.444 U NA 25 U NA
113507-82-7 Perfluoro(2-ethoxyethane)sulphonic acid (PFEESA) ng/L 25 U NA 0.434 U NA 0.444 U NA 25 U NA
39492-91-6 Perfluoro(3,5,7,9,11-pentaoxadodecanoic) acid (PFO5DA) (TAF) ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
39492-90-5 Perfluoro(3,5,7,9-tetraoxadecanoic) acid (PFO4DA) ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
39492-89-2 Perfluoro(3,5,7-trioxaoctanoic) acid (PFO3OA) ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
39492-88-1 Perfluoro(3,5-dioxahexanoic) acid (PFO2HxA) ng/L 23.4 J 33.5 J 0.434 U 3.78 U 0.444 U 3.79 U 38.9 101
863090-89-5 Perfluoro(4-methoxybutanoic) acid (PFMBA) ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
13140-29-9 Perfluoro-2-(perfluoromethoxy)propanoic acid (PMPA) ng/L 23.1 40 U 0.347 U 3.78 U 0.355 U 3.79 U 273 40 U
674-13-5 Perfluoro-2-methoxyacetic acid (PFMOAA) ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
377-73-1 Perfluoro-3-methoxypropanoic acid (PFMPA) ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
375-73-5 Perfluorobutanesulfonic acid (PFBS) ng/L 89 U 17.8 U 3.26 2.25 1.58 U 1.69 U 89 U 17.8 U
375-22-4 Perfluorobutanoic acid (PFBA) ng/L 100 U 20.1 2.42 2.66 1.78 U 4.04 100 U 20 U
335-77-3 Perfluorodecanesulfonic acid (PFDCS) ng/L 97 U 19.4 U 1.68 U 1.83 U 1.72 U 1.84 U 97 U 19.4 U
335-76-2 Perfluorodecanoic Acid (PFDA) ng/L 100 U 20 U 1.73 U 1.89 U 1.78 U 1.89 U 100 U 20 U
79780-39-5 Perfluorododecanesulfonic acid (PFDoS) ng/L 200 U 19.4 U 3.47 U 1.83 U 3.55 U 1.83 U 200 U 19.4 U
307-55-1 Perfluorododecanoic Acid (PFDoA) ng/L 100 U 20 U 1.73 U 1.89 U 1.78 U 1.89 U 100 U 20 U
267239-61-2 Perfluoroethoxypropyl carboxylic acid (PEPA) ng/L 25 U 40 U 0.434 U 3.78 U 0.444 U 3.79 U 25 U 40 U
375-92-8 Perfluoroheptanesulfonic acid (PFHpS) ng/L 95 U 19 U 1.65 U 1.79 U 1.69 U 1.8 U 95 U 19 U
375-85-9 Perfluoroheptanoic Acid (PFHpA) ng/L 100 U 8.74 J 1.67 J 1.38 J 2.14 1.86 J 100 U 20 U
355-46-4 Perfluorohexanesulfonic acid (PFHXS) ng/L 91 U 18.2 U 0.675 J 1.29 J 1.62 U 1.72 U 91 U 18.2 U
307-24-4 Perfluorohexanoic Acid (PFHxA) ng/L 40.7 J 65.1 2 2.14 4.1 3.95 100 U 8.23 J
68259-12-1 Perfluorononanesulfonic acid (PFNS) ng/L 96 U 19.2 U 1.67 U 1.81 U 1.7 U 1.82 U 96 U 19.2 U
375-95-1 Perfluorononanoic Acid (PFNA) ng/L 100 U 20 U 1.73 U 1.89 U 0.596 J 1.89 U 100 U 20 U
16517-11-6 Perfluorooctadecanoic acid (PFODA) ng/L 200 U 40 U 3.47 U 3.78 U 17.8 U 3.79 U 200 U 40 U
754-91-6 Perfluorooctane sulfonamide (PFOSA) ng/L 100 U 20 U 1.73 U 1.89 U 1.78 U 1.89 U 100 U 20 U
1763-23-1 Perfluorooctane sulfonic acid (PFOS) ng/L 100 U 20 U 5.15 4.81 3.62 2.78 100 U 15.5 J
335-67-1 Perfluorooctanoic Acid (PFOA) ng/L 100 U 23.2 12.2 10.1 2.64 2.47 100 U 20 U
2706-91-4 Perfluoropentanesulfonic acid (PFPeS) ng/L 94 U 18.8 U 1.63 U 1.77 U 1.67 U 1.78 U 94 U 18.8 U
2706-90-3 Perfluoropentanoic Acid (PFPeA) ng/L 124 96 1.82 2.92 6.07 5.39 100 U 20 U
422-64-0 Perfluoropropanoic acid (PPF Acid) ng/L 1000 U 200 U 17.3 U 18.9 U 17.8 U 18.9 U 1000 U 200 U
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
Page 1 of 4
Comparison Summary of Split Groundwater and Surface Water Sample Results for PFAS
Canton Mill, Canton, North Carolina
PZ04 PZ04 PZ21 PZ21 RW01 RW01 RW05 RW05
PZ-4 PZ04WG-091923-20230919 PZ-21 PZ21WG-091923-20230919 RW-1 RW01WG-091923-20230919 RW-5 RW05WG-092023-20230920
9/19/2023 9/19/2023 9/19/2023 9/19/2023 9/19/2023 9/19/2023 9/20/2023 9/20/2023
Normal Normal Normal Normal Normal Normal Normal Normal
Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater
Sample Description:NCDEQ Split PTVE Split NCDEQ Split PTVE Split NCDEQ Split PTVE Split NCDEQ Split PTVE Split
CAS No. Analyte Units
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
376-06-7 Perfluorotetradecanoic acid (PFTEDA) ng/L 100 U 20 U 1.73 U 1.89 U 1.78 U 1.89 U 100 U 20 U
72629-94-8 Perfluorotridecanoic acid (PFTrDA) ng/L 100 U 20 U 1.73 U 1.89 U 1.78 U 1.89 U 100 U 20 U
2058-94-8 Perfluoroundecanoic Acid (PFUnA) ng/L 100 U 20 U 1.73 U 1.89 U 1.78 U 1.89 U 100 U 20 U
67905-19-5 PFHxDA ng/L 200 U 40 U 3.47 U 3.78 U 17.8 U 3.79 U 200 U 40 U
2416366-22-6 R-EVE ng/L 200 U NA 3.47 U NA 3.55 U NA 200 U NA
763051-92-9 11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11Cl-PF3OUdS, F-53B Minor) ng/L 100 U 18.8 U 1.73 U 1.78 U 1.78 U 1.78 U 100 U 18.8 U
919005-14-4 4,8-Dioxa-3H-perfluorononanoic acid (ADONA) ng/L 100 U 20 U 1.73 U 1.89 U 1.78 U 1.89 U 100 U 20 U
757124-72-4 4:2 Fluorotelomer sulfonate (4:2 FTS) ng/L 188 U 188 U 81.5 U 3.55 U 83.4 U 17.8 U 188 U 37.6 U
27619-97-2 6:2 Fluorotelomer sulfonate (6:2 FTS) ng/L 750 U 750 U 65.1 U 70.8 U 333 U 71 U 750 U 750 U
39108-34-4 8:2 Fluorotelomer sulfonate (8:2 FTS) ng/L 192 U 192 U 3.33 U 3.62 U 17 U 3.64 U 192 U 38.4 U
756426-58-1 9-Chlorohexadecafluoro-3-oxanone-1-sulfonic acid (9Cl-PF3ONS, F-53B Major) ng/L 196 U 18.6 U 3.41 U 1.76 U 3.49 U 1.77 U 196 U 18.6 U
Notes:
ng/L = Nanograms per liter
USEPA = United States Environmental Protection Agency
PFAS = Per- and polyfluoroalkyl Substances
NA = Not analyzed
U = Not detected, shown with reporting limit
J = Estimated value
bold = Detected value
= NCDEQ split sample results
1 All samples were collected by EnSafe for split analyses by PTVE and NCDEQ contract laboratory, GEL Laboratories LLC. All samples were analyzed using Method "EPA 537Mod PFCs by LC-MS/MS As Received." The NCDEQ and PTVE sample laboratory reports have different reporting limits (RLs) and method detection limits (DLs), and different lists of
reported PFAS. Any results between the RL and DL should be flagged as estimated.
Page 2 of 4
Comparison Summary of Split Groundwater and Surface Water Sample Results for PFAS
Canton Mill, Canton, North Carolina
Sample Description:
CAS No. Analyte Units
USEPA Method for PFAS1
801209-99-4 1,1,2,2-Tetrafluoro-2-(1,2,2,2-tetrafluoroethoxy)ethane sulfonic acid (NVHO) ng/L
801212-59-9 4-(Heptafluoroisopropoxy)hexafluorobutanoic acid (PFECA-G) ng/L
2416366-18-0 Byproduct 4 (BP4)ng/L
2416366-19-1 Byproduct 5 (BP5)ng/L
2416366-21-5 Byproduct 6 (BP6)ng/L
69087-46-3 EVE Acid ng/L
13252-13-6 Hexafluoropropylene oxide dimer acid (HFPO-DA, GenX) ng/L
773804-62-9 Hydro-EVE ng/L
4151-50-2 N-ETHYL PERFLUOROOCTANE SULFONAMIDE (ETFOSA) ng/L
1691-99-2 N-ETHYL PERFLUOROOCTANE SULFONAMIDOETHANOL (EtFOSE) ng/L
2991-50-6 N-ethyl perfluorooctanesulfonamidoacetic acid (NEtFOSAA) ng/L
31506-32-8 N-METHYL PERFLUOROOCTANE SULFONAMIDE (MEFOSA) ng/L
24448-09-7 N-METHYL PERFLUOROOCTANE SULFONAMIDOETHANOL (MeFOSE) ng/L
2355-31-9 N-methyl perfluorooctanesulfonamidoacetic acid (NMeFOSAA) ng/L
29311-67-9 Nafion Byproduct 1 ng/L
749836-20-2 Nafion Byproduct 2 ng/L
151772-58-6 Nonafluoro-3,6-dioxaheptanoic acid (NFDHA) ng/L
113507-82-7 Perfluoro(2-ethoxyethane)sulphonic acid (PFEESA) ng/L
39492-91-6 Perfluoro(3,5,7,9,11-pentaoxadodecanoic) acid (PFO5DA) (TAF) ng/L
39492-90-5 Perfluoro(3,5,7,9-tetraoxadecanoic) acid (PFO4DA) ng/L
39492-89-2 Perfluoro(3,5,7-trioxaoctanoic) acid (PFO3OA) ng/L
39492-88-1 Perfluoro(3,5-dioxahexanoic) acid (PFO2HxA) ng/L
863090-89-5 Perfluoro(4-methoxybutanoic) acid (PFMBA) ng/L
13140-29-9 Perfluoro-2-(perfluoromethoxy)propanoic acid (PMPA) ng/L
674-13-5 Perfluoro-2-methoxyacetic acid (PFMOAA) ng/L
377-73-1 Perfluoro-3-methoxypropanoic acid (PFMPA) ng/L
375-73-5 Perfluorobutanesulfonic acid (PFBS) ng/L
375-22-4 Perfluorobutanoic acid (PFBA) ng/L
335-77-3 Perfluorodecanesulfonic acid (PFDCS) ng/L
335-76-2 Perfluorodecanoic Acid (PFDA) ng/L
79780-39-5 Perfluorododecanesulfonic acid (PFDoS) ng/L
307-55-1 Perfluorododecanoic Acid (PFDoA) ng/L
267239-61-2 Perfluoroethoxypropyl carboxylic acid (PEPA) ng/L
375-92-8 Perfluoroheptanesulfonic acid (PFHpS) ng/L
375-85-9 Perfluoroheptanoic Acid (PFHpA) ng/L
355-46-4 Perfluorohexanesulfonic acid (PFHXS) ng/L
307-24-4 Perfluorohexanoic Acid (PFHxA) ng/L
68259-12-1 Perfluorononanesulfonic acid (PFNS) ng/L
375-95-1 Perfluorononanoic Acid (PFNA) ng/L
16517-11-6 Perfluorooctadecanoic acid (PFODA) ng/L
754-91-6 Perfluorooctane sulfonamide (PFOSA) ng/L
1763-23-1 Perfluorooctane sulfonic acid (PFOS) ng/L
335-67-1 Perfluorooctanoic Acid (PFOA) ng/L
2706-91-4 Perfluoropentanesulfonic acid (PFPeS) ng/L
2706-90-3 Perfluoropentanoic Acid (PFPeA) ng/L
422-64-0 Perfluoropropanoic acid (PPF Acid) ng/L
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
SWDOWN SWDOWN SWUP CANTON INTAKE CANTON INTAKE
SW- DOWNSTREAM SWDOWNWS-092023-20230920 SW- UPSTREAM CANTON INTAKEWS-09202320230920 CANTON INTAKEH-092023-20230920
9/20/2023 9/20/2023 9/20/2023 9/20/2023 9/20/2023
Normal Normal Normal Normal Field Duplicate
Surface Water Surface Water Surface Water Surface Water Surface Water
NCDEQ Split PTVE Split NCDEQ Split PTVE Split PTVE Split (duplicate)
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U NA 0.477 U NA NA
0.432 U 1.84 U 0.477 U 1.82 U 2.01 U
0.432 U NA 0.477 U NA NA
3.46 U 3.68 U 3.82 U 3.64 U 4.02 U
3.46 U 3.68 U 3.82 U 3.64 U 4.02 U
3.46 U 3.68 U 3.82 U 3.64 U 4.02 U
3.46 U 3.68 U 3.82 U 3.64 U 4.02 U
3.46 U 3.68 U 3.82 U 3.64 U 4.02 U
3.46 U 3.68 U 3.82 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U NA 0.477 U NA NA
0.432 U NA 0.477 U NA NA
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.346 U 3.68 U 0.382 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
1.54 U 1.64 U 1.7 U 1.62 U 1.79 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
1.68 U 1.78 U 1.85 U 1.76 U 1.95 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
3.46 U 1.78 U 3.82 U 1.76 U 1.95 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
0.432 U 3.68 U 0.477 U 3.64 U 4.02 U
1.64 U 1.75 U 1.81 U 1.73 U 1.91 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
1.57 U 1.67 U 1.74 U 1.66 U 1.83 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
1.66 U 1.77 U 1.83 U 1.75 U 1.93 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
3.46 U 3.68 U 3.82 U 3.64 U 4.02 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
1.73 U 0.779 J 1.91 U 1.82 U 2.01 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
1.63 U 1.73 U 1.79 U 1.71 U 1.89 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
17.3 U 18.4 U 19.1 U 18.2 U 20.1 U
Page 3 of 4
Comparison Summary of Split Groundwater and Surface Water Sample Results for PFAS
Canton Mill, Canton, North Carolina
Sample Description:
CAS No. Analyte Units
Sample Location:
Sample ID:
Sample Date:
Sample Type:
Matrix:
376-06-7 Perfluorotetradecanoic acid (PFTEDA) ng/L
72629-94-8 Perfluorotridecanoic acid (PFTrDA) ng/L
2058-94-8 Perfluoroundecanoic Acid (PFUnA) ng/L
67905-19-5 PFHxDA ng/L
2416366-22-6 R-EVE ng/L
763051-92-9 11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11Cl-PF3OUdS, F-53B Minor) ng/L
919005-14-4 4,8-Dioxa-3H-perfluorononanoic acid (ADONA) ng/L
757124-72-4 4:2 Fluorotelomer sulfonate (4:2 FTS) ng/L
27619-97-2 6:2 Fluorotelomer sulfonate (6:2 FTS) ng/L
39108-34-4 8:2 Fluorotelomer sulfonate (8:2 FTS) ng/L
756426-58-1 9-Chlorohexadecafluoro-3-oxanone-1-sulfonic acid (9Cl-PF3ONS, F-53B Major) ng/L
Notes:
ng/L = Nanograms per liter
USEPA = United States Environmental Protection Agency
PFAS = Per- and polyfluoroalkyl Substances
NA = Not analyzed
U = Not detected, shown with reporting limit
J = Estimated value
bold = Detected value
= NCDEQ split sample results
1 All samples were collected by EnSafe for split analyses by PTVE and NCDEQ contract laboratory, GEL Laboratories LLC. All samples were analyzed using Method "EPA 537Mod PFCs by LC-MS/MS As Received." The NCDEQ and PTVE sample laboratory reports have different reporting limits (RLs) and method detection limits (DLs), and different lists of
reported PFAS. Any results between the RL and DL should be flagged as estimated.
SWDOWN SWDOWN SWUP CANTON INTAKE CANTON INTAKE
SW- DOWNSTREAM SWDOWNWS-092023-20230920 SW- UPSTREAM CANTON INTAKEWS-09202320230920 CANTON INTAKEH-092023-20230920
9/20/2023 9/20/2023 9/20/2023 9/20/2023 9/20/2023
Normal Normal Normal Normal Field Duplicate
Surface Water Surface Water Surface Water Surface Water Surface Water
NCDEQ Split PTVE Split NCDEQ Split PTVE Split PTVE Split (duplicate)
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
3.46 U 3.68 U 3.82 U 3.64 U 4.02 U
3.46 U NA 3.82 U NA NA
1.73 U 1.73 U 1.91 U 1.71 U 1.9 U
1.73 U 1.84 U 1.91 U 1.82 U 2.01 U
3.25 U 3.46 U 3.59 U 3.42 U 3.78 U
13 U 13.8 U 14.3 U 13.6 U 15.1 U
3.32 U 3.53 U 3.66 U 3.49 U 3.86 U
3.4 U 1.71 U 3.75 U 1.7 U 1.87 U
Page 4 of 4

October 19, 2023

Christina Ashdown
EnSafe
313 Wingo Way
Mt. Pleasant, South Carolina 29464

Re: PFAS Analysis
Work Order: 638199

Dear Christina Ashdown:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on September 21, 2023. This original data report has been prepared and reviewed in
accordance with GEL's standard operating procedures.

The samples were delivered with proper chain of custody documentation and signatures. All sample containers
arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample
receipt.
Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards,
with any exceptions noted. The results reported relate only to the items tested and to the sample as received by
the laboratory. These results may not be reproduced except as full reports without approval by the laboratory.
Copies of GEL's accreditations and certifications can be found on our website at www.gel.com.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 1614.

Sincerely,

PM_SIGN_HERE
Delaney Stone
Project Manager

Purchase Order: PO0000035146
Enclosures
Page 1 of 48 SDG: 638199
Reviewed by USER_SIGN_HERE
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis Report
ENFE003 EnSafe Inc.
Client SDG: 638199 GEL Work Order: 638199
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above
the limit as defined in the 'U' qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures. Please direct any questions to your Project Manager, Delaney Stone.
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound
J Value is estimated
U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
for
Page 2 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
2500162
2500162
2500162
0452
1313
1705
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/17/23
09/29/23
09/28/23
DK2
MB2
MB2
3.78
1.89
3.78
3.78
3.78
3.78
3.78
3.78
3.78
3.78
3.78
3.78
3.78
3.78
18.9
3.78
3.78
3.78
70.8
1.78
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
5
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199001
WG
19-SEP-23 09:25
21-SEP-23
PZ21WG-091923 ENFE00223Project:
ENFE003Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
1.25
0.623
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
7.55
1.25
1.25
1.25
25.4
0.623
1
2
3
UX
U
UX
UX
UX
UX
UX
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
U
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluoropropanoic acid (PPF Acid)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
Page 3 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
3.78
3.78
1.76
3.55
3.62
3.78
3.78
3.78
3.78
1.83
1.68
1.89
1.83
1.89
1.89
1.79
1.89
3.78
1.72
1.89
1.81
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199001
PZ21WG-091923 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
1.25
1.25
0.623
1.25
1.25
1.25
1.25
1.25
1.25
0.623
0.623
0.755
0.623
0.736
0.623
0.623
0.623
1.25
0.623
0.755
0.661
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
J
U
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.25
2.66
ND
ND
ND
ND
1.38
ND
1.29
2.14
ND
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
Page 4 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
1.89
3.78
1.89
1.89
1.89
1.77
1.89
1.89
1.89
1.89
1.89
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199001
PZ21WG-091923 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
0.623
1.25
0.623
0.755
0.755
0.623
0.623
0.755
0.623
0.623
0.623
U
U
U
U
U
U
U
U
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
4.81
10.1
ND
2.92
ND
ND
ND
ND
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
The following Prep Methods were performed:
EPA 537.1 Mod, Compliant witPFCs Extraction in Liquid 09/28/23 25001601016SR2
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
3
Method Description
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 5 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
2500162
2500162
0522
1713
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/17/23
09/28/23
DK2
MB2
3.79
1.89
3.79
3.79
3.79
3.79
3.79
3.79
3.79
3.79
3.79
3.79
3.79
3.79
18.9
3.79
3.79
3.79
1.78
3.79
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199002
WG
19-SEP-23 11:55
21-SEP-23
RW01WG-091923 ENFE00223Project:
ENFE003Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
1.25
0.625
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
1.25
7.58
1.25
1.25
1.25
0.625
1.25
1
2
UX
U
UX
UX
UX
UX
UX
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
U
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluoropropanoic acid (PPF Acid)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
Page 6 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
3.79
1.77
3.64
3.79
3.79
3.79
3.79
1.83
1.69
1.89
1.84
1.89
1.89
1.80
1.89
3.79
1.72
1.89
1.82
1.89
3.79
1.89
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199002
RW01WG-091923 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
1.25
0.625
1.25
1.25
1.25
1.25
1.25
0.625
0.625
0.758
0.625
0.739
0.625
0.625
0.625
1.25
0.625
0.758
0.663
0.625
1.25
0.625
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.04
ND
ND
ND
ND
1.86
ND
ND
3.95
ND
ND
ND
ND
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
Page 7 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25001621321
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/29/23MB2
1.89
1.89
1.78
1.89
1.89
1.89
1.89
1.89
17.8
71.0
1
1
1
1
1
1
1
1
5
5
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199002
RW01WG-091923 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
0.758
0.758
0.625
0.625
0.758
0.625
0.625
0.625
6.25
25.5
3
U
U
U
U
U
U
U
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
EPA 537Mod PFCs by LC-MS/MS "As Received"
2.78
2.47
ND
5.39
ND
ND
ND
ND
ND
ND
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
0.0189
The following Prep Methods were performed:
EPA 537.1 Mod, Compliant witPFCs Extraction in Liquid 09/28/23 25001601016SR2
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
3
Method Description
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 8 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25001621722ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/28/23MB22.07
4.40
4.40
2.05
4.13
16.5
4.22
4.40
4.40
4.40
4.40
2.13
1.96
2.20
2.13
2.20
2.20
2.09
2.20
4.40
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199003
WQ
19-SEP-23 12:20
21-SEP-23
FB01WQ-091923 ENFE00223Project:
ENFE003Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.726
1.45
1.45
0.726
1.45
5.91
1.45
1.45
1.45
1.45
1.45
0.726
0.726
0.880
0.726
0.858
0.726
0.726
0.726
1.45
1U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
Page 9 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25001620538
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/17/23DK2
2.00
2.20
2.11
2.20
4.40
2.20
2.20
2.20
2.07
2.20
2.20
2.20
2.20
2.20
4.40
2.20
4.40
4.40
4.40
4.40
4.40
4.40
4.40
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199003
FB01WQ-091923 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
0.726
0.880
0.770
0.726
1.45
0.726
0.880
0.880
0.726
0.726
0.880
0.726
0.726
0.726
1.45
0.726
1.45
1.45
1.45
1.45
1.45
1.45
1.45
2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
Page 10 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
4.40
4.40
4.40
4.40
4.40
22.0
4.40
4.40
4.40
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199003
FB01WQ-091923 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
1.45
1.45
1.45
1.45
1.45
8.80
1.45
1.45
1.45
UX
UX
UX
U
U
UX
UX
UX
UX
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluoropropanoic acid (PPF Acid)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
0.0220
The following Prep Methods were performed:
EPA 537.1 Mod, Compliant witPFCs Extraction in Liquid 09/28/23 25001601016SR2
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 11 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
2500162
2500162
1330
1731
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/29/23
09/28/23
MB2
MB2
188
750
192
18.8
40.0
40.0
18.6
40.0
40.0
40.0
40.0
19.4
17.8
20.0
19.4
20.0
20.0
19.0
20.0
40.0
5
5
5
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199004
WG
19-SEP-23 14:15
21-SEP-23
PZ04WG-091923 ENFE00223Project:
ENFE003Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
66.0
269
66.0
6.60
13.2
13.2
6.60
13.2
13.2
13.2
13.2
6.60
6.60
8.00
6.60
7.80
6.60
6.60
6.60
13.2
1
2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20.1
ND
ND
ND
ND
8.74
ND
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
Page 12 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25001620553
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/17/23DK2
18.2
20.0
19.2
20.0
40.0
20.0
20.0
20.0
18.8
20.0
20.0
20.0
20.0
20.0
40.0
20.0
40.0
40.0
40.0
40.0
40.0
40.0
40.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199004
PZ04WG-091923 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
6.60
8.00
7.00
6.60
13.2
6.60
8.00
8.00
6.60
6.60
8.00
6.60
6.60
6.60
13.2
6.60
13.2
13.2
13.2
13.2
13.2
13.2
13.2
3
U
U
U
U
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
65.1
ND
ND
ND
ND
ND
23.2
ND
96.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
Page 13 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
40.0
40.0
40.0
40.0
40.0
200
40.0
40.0
40.0
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199004
PZ04WG-091923 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
13.2
13.2
13.2
13.2
13.2
80.0
13.2
13.2
13.2
UX
JX
UX
U
U
UX
UX
UX
UX
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluoropropanoic acid (PPF Acid)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
33.5
ND
ND
ND
ND
ND
ND
ND
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
The following Prep Methods were performed:
EPA 537.1 Mod, Compliant witPFCs Extraction in Liquid 09/28/23 25001601016SR2
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
3
Method Description
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Page 14 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199004
PZ04WG-091923 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 15 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25001621739ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/28/23MB218.8
40.0
40.0
18.6
37.6
38.4
40.0
40.0
40.0
40.0
19.4
17.8
20.0
19.4
20.0
20.0
19.0
20.0
40.0
18.2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199005
WG
20-SEP-23 09:05
21-SEP-23
RW05WG-092023 ENFE00223Project:
ENFE003Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
6.60
13.2
13.2
6.60
13.2
13.2
13.2
13.2
13.2
13.2
6.60
6.60
8.00
6.60
7.80
6.60
6.60
6.60
13.2
6.60
1U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexane sulfonic acid
(PFHxS)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
Page 16 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
2500162
2500162
1339
0608
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/29/23
10/17/23
MB2
DK2
20.0
19.2
20.0
40.0
20.0
20.0
20.0
18.8
20.0
20.0
20.0
20.0
20.0
750
40.0
20.0
40.0
40.0
40.0
40.0
40.0
40.0
40.0
1
1
1
1
1
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199005
RW05WG-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
8.00
7.00
6.60
13.2
6.60
8.00
8.00
6.60
6.60
8.00
6.60
6.60
6.60
269
13.2
6.60
13.2
13.2
13.2
13.2
13.2
13.2
13.2
2
3
J
U
U
U
U
J
U
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
8.23
ND
ND
ND
ND
15.5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
Page 17 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
40.0
40.0
40.0
40.0
40.0
200
40.0
40.0
40.0
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199005
RW05WG-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
13.2
13.2
13.2
13.2
13.2
80.0
13.2
13.2
13.2
UX
X
UX
U
U
UX
UX
UX
UX
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluoropropanoic acid (PPF Acid)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
101
ND
ND
ND
ND
ND
ND
ND
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
The following Prep Methods were performed:
EPA 537.1 Mod, Compliant witPFCs Extraction in Liquid 09/28/23 25001601016SR2
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
3
Method Description
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Page 18 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199005
RW05WG-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 19 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25001621748ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/28/23MB21.73
3.68
3.68
1.71
3.46
13.8
3.53
3.68
3.68
3.68
3.68
1.78
1.64
1.84
1.78
1.84
1.84
1.75
1.84
3.68
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199006
WS
20-SEP-23 13:05
21-SEP-23
SWDownWS-092023 ENFE00223Project:
ENFE003Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.607
1.21
1.21
0.607
1.21
4.95
1.21
1.21
1.21
1.21
1.21
0.607
0.607
0.736
0.607
0.717
0.607
0.607
0.607
1.21
1U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
Page 20 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25001620623
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/17/23DK2
1.67
1.84
1.77
1.84
3.68
1.84
1.84
1.84
1.73
1.84
1.84
1.84
1.84
1.84
3.68
1.84
3.68
3.68
3.68
3.68
3.68
3.68
3.68
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199006
SWDownWS-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
0.607
0.736
0.644
0.607
1.21
0.607
0.736
0.736
0.607
0.607
0.736
0.607
0.607
0.607
1.21
0.607
1.21
1.21
1.21
1.21
1.21
1.21
1.21
2
U
U
U
U
U
U
J
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
0.779
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
Page 21 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
3.68
3.68
3.68
3.68
3.68
18.4
3.68
3.68
3.68
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199006
SWDownWS-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
1.21
1.21
1.21
1.21
1.21
7.36
1.21
1.21
1.21
UX
UX
UX
U
U
UX
UX
UX
UX
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluoropropanoic acid (PPF Acid)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
0.0184
The following Prep Methods were performed:
EPA 537.1 Mod, Compliant witPFCs Extraction in Liquid 09/28/23 25001601016SR2
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 22 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25001621756ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/28/23MB21.71
3.64
3.64
1.70
3.42
13.6
3.49
3.64
3.64
3.64
3.64
1.76
1.62
1.82
1.76
1.82
1.82
1.73
1.82
3.64
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199007
WS
20-SEP-23 17:55
21-SEP-23
Canton IntakeWS-092023 ENFE00223Project:
ENFE003Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.600
1.20
1.20
0.600
1.20
4.89
1.20
1.20
1.20
1.20
1.20
0.600
0.600
0.728
0.600
0.710
0.600
0.600
0.600
1.20
1U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
Page 23 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25001620638
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/17/23DK2
1.66
1.82
1.75
1.82
3.64
1.82
1.82
1.82
1.71
1.82
1.82
1.82
1.82
1.82
3.64
1.82
3.64
3.64
3.64
3.64
3.64
3.64
3.64
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199007
Canton IntakeWS-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
0.600
0.728
0.637
0.600
1.20
0.600
0.728
0.728
0.600
0.600
0.728
0.600
0.600
0.600
1.20
0.600
1.20
1.20
1.20
1.20
1.20
1.20
1.20
2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
Page 24 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
3.64
3.64
3.64
3.64
3.64
18.2
3.64
3.64
3.64
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199007
Canton IntakeWS-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
1.20
1.20
1.20
1.20
1.20
7.28
1.20
1.20
1.20
UX
UX
UX
U
U
UX
UX
UX
UX
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluoropropanoic acid (PPF Acid)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
The following Prep Methods were performed:
EPA 537.1 Mod, Compliant witPFCs Extraction in Liquid 09/28/23 25001601016SR2
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 25 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
2500162
2500162
0653
1805
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/17/23
09/28/23
DK2
MB2
4.02
2.01
4.02
4.02
4.02
4.02
4.02
4.02
4.02
4.02
4.02
4.02
4.02
4.02
20.1
4.02
4.02
4.02
1.90
4.02
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199008
WQ
20-SEP-23 17:55
21-SEP-23
Canton IntakeH-092023 ENFE00223Project:
ENFE003Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
1.33
0.664
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33
8.05
1.33
1.33
1.33
0.664
1.33
1
2
UX
U
UX
UX
UX
UX
UX
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
U
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluoropropanoic acid (PPF Acid)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
Page 26 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
4.02
1.87
3.78
15.1
3.86
4.02
4.02
4.02
4.02
1.95
1.79
2.01
1.95
2.01
2.01
1.91
2.01
4.02
1.83
2.01
1.93
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199008
Canton IntakeH-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
1.33
0.664
1.33
5.41
1.33
1.33
1.33
1.33
1.33
0.664
0.664
0.805
0.664
0.785
0.664
0.664
0.664
1.33
0.664
0.805
0.704
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
Page 27 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
2.01
4.02
2.01
2.01
2.01
1.89
2.01
2.01
2.01
2.01
2.01
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199008
Canton IntakeH-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
0.664
1.33
0.664
0.805
0.805
0.664
0.664
0.805
0.664
0.664
0.664
U
U
U
U
U
U
U
U
U
U
U
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
0.0201
The following Prep Methods were performed:
EPA 537.1 Mod, Compliant witPFCs Extraction in Liquid 09/28/23 25001601016SR2
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 28 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
2500162
2500162
0708
1814
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/17/23
09/28/23
DK2
MB2
4.33
2.17
4.33
4.33
4.33
4.33
4.33
4.33
4.33
4.33
4.33
4.33
4.33
4.33
21.7
4.33
4.33
4.33
2.04
4.33
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199009
WQ
20-SEP-23 18:00
21-SEP-23
Canton Intake FBWQ-092023 ENFE00223Project:
ENFE003Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
1.43
0.715
1.43
1.43
1.43
1.43
1.43
1.43
1.43
1.43
1.43
1.43
1.43
1.43
8.67
1.43
1.43
1.43
0.715
1.43
1
2
UX
U
UX
UX
UX
UX
UX
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
U
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluoropropanoic acid (PPF Acid)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
Page 29 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
4.33
2.02
4.07
16.3
4.16
4.33
4.33
4.33
4.33
2.10
1.93
2.17
2.10
2.17
2.17
2.06
2.17
4.33
1.97
2.17
2.08
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199009
Canton Intake FBWQ-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
1.43
0.715
1.43
5.83
1.43
1.43
1.43
1.43
1.43
0.715
0.715
0.867
0.715
0.845
0.715
0.715
0.715
1.43
0.715
0.867
0.758
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
Page 30 of 48 SDG: 638199
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 19, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
2.17
4.33
2.17
2.17
2.17
2.04
2.17
2.17
2.17
2.17
2.17
1
1
1
1
1
1
1
1
1
1
1
Christina AshdownContact:
EnSafeCompany :
313 Wingo Way
Mt. Pleasant, South Carolina 29464
Address :
PFAS AnalysisProject:
638199009
Canton Intake FBWQ-092023 ENFE00223Project:
ENFE003Client ID:Sample ID:
Client Sample ID:
0.715
1.43
0.715
0.867
0.867
0.715
0.715
0.867
0.715
0.715
0.715
U
U
U
U
U
U
U
U
U
U
U
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
0.0217
The following Prep Methods were performed:
EPA 537.1 Mod, Compliant witPFCs Extraction in Liquid 09/28/23 25001601016SR2
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 31 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
Parmname
Christina AshdownContact:
EnSafe
313 Wingo Way
Mt. Pleasant, South Carolina
October 19, 2023Report Date:
Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
MB2
DK2
MB2
DK2
MB2
10/17/23 04:22
09/28/23 16:22
10/17/23 04:22
09/28/23 16:22
10/17/23 04:22
09/28/23 16:22
QC
18.8
17.1
18.0
17.6
16.4
17.8
20.0
18.8
20.4
23.5
20.6
19.3
18.9
19.0
NOM Sample Range
(60%-158%)
(59%-144%)
(60%-141%)
(56%-151%)
(60%-153%)
(67%-154%)
(73%-141%)
(68%-135%)
(5%-158%)
(5%-149%)
(59%-145%)
(67%-144%)
(23%-155%)
(57%-139%)
Qual
X
X
X
X
X
QC1205531243
REC%
92
88
91
92
84
87
98
98
99
114
100
94
92
93
20.5
19.4
19.7
19.2
19.5
20.5
20.5
19.2
20.5
20.5
20.5
20.5
20.5
20.5
LCS
638199Workorder:
RPD/D%
Page 1 of 12
Page 32 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluorobutane sulfonic acid
(PFBS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
DK2
MB2
09/28/23 16:22
10/17/23 04:22
09/28/23 16:22
QC
18.5
17.5
19.2
18.4
17.5
18.0
16.0
23.0
18.3
19.8
20.7
19.8
21.3
20.2
16.7
NOM Sample Range
(54%-128%)
(20%-154%)
(59%-145%)
(52%-141%)
(35%-138%)
(63%-143%)
(58%-147%)
(60%-151%)
(62%-148%)
(60%-144%)
(50%-150%)
(52%-144%)
(60%-149%)
(58%-142%)
(70%-144%)
Qual
X
X
X
X
X
X
X
X
REC%
90
85
94
90
85
88
78
112
89
96
101
96
104
98
92
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
18.2
638199Workorder:
RPD/D%
Page 2 of 12
Page 33 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
DK2
MB2
09/28/23 16:22
10/17/23 04:22
09/28/23 16:22
QC
18.9
19.1
19.2
16.9
19.5
19.6
19.8
19.2
17.7
16.1
19.2
19.1
20.1
10.6
19.1
NOM Sample Range
(73%-151%)
(58%-134%)
(65%-145%)
(57%-134%)
(65%-137%)
(58%-144%)
(68%-138%)
(71%-133%)
(69%-144%)
(67%-145%)
(70%-138%)
(64%-133%)
(69%-133%)
(35%-165%)
(64%-134%)
Qual
X
REC%
92
97
93
85
95
95
101
93
86
86
94
97
98
51
93
20.5
19.8
20.5
19.9
20.5
20.5
19.5
20.5
20.5
18.7
20.5
19.7
20.5
20.5
20.5
638199Workorder:
RPD/D%
Page 3 of 12
Page 34 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PPF Acid)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid
(PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
DK2
MB2
DK2
MB2
DK2
09/28/23 16:22
10/17/23 04:22
09/28/23 16:22
10/17/23 04:37
09/28/23 16:30
10/17/23 04:37
QC
19.1
21.2
14.5
19.0
20.2
18.4
18.7
18.4
18.5
16.9
19.8
17.8
19.8
17.8
19.6
NOM Sample Range
(65%-145%)
(66%-139%)
(67%-136%)
(72%-143%)
(49%-153%)
(66%-138%)
(58%-140%)
(63%-135%)
(0%-30%)
(0%-27%)
(0%-36%)
(0%-32%)
(0%-32%)
(0%-26%)
(0%-24%)
Qual
JX
X
X
QC1205531244
2
1
10
1
19
0
2
REC%
93
103
75
92
98
90
91
90
91
89
102
94
103
88
97
20.5
20.5
19.3
20.5
20.5
20.5
20.5
20.5
20.2
19.0
19.4
18.9
19.2
20.2
20.2
LCSD
638199Workorder:
RPD/D%
Page 4 of 12
Page 35 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
DK2
MB2
DK2
09/28/23 16:30
10/17/23 04:37
09/28/23 16:30
10/17/23 04:37
QC
18.9
18.6
20.6
21.2
19.0
20.1
20.8
19.0
20.2
18.6
18.4
17.7
18.4
17.0
21.6
NOM Sample Range
(0%-26%)
(0%-45%)
(0%-40%)
(0%-26%)
(0%-30%)
(0%-27%)
(0%-27%)
(0%-28%)
(0%-36%)
(0%-27%)
(0%-30%)
(0%-28%)
(0%-23%)
(0%-40%)
(0%-39%)
Qual
X
X
X
X
X
X
X
0
9
13
3
1
6
9
3
14
3
0
1
2
6
6
REC%
100
92
102
105
94
99
103
94
100
92
91
88
91
84
107
18.8
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
638199Workorder:
RPD/D%
Page 5 of 12
Page 36 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
MB2
DK2
MB2
10/17/23 04:37
09/28/23 16:30
10/17/23 04:37
09/28/23 16:30
QC
17.2
18.9
20.3
18.9
18.9
20.9
15.5
18.3
18.4
18.3
17.4
19.9
18.4
21.8
20.3
NOM Sample Range
(0%-36%)
(0%-27%)
(0%-30%)
(0%-31%)
(0%-25%)
(0%-29%)
(0%-35%)
(0%-20%)
(0%-30%)
(0%-31%)
(0%-32%)
(0%-26%)
(0%-27%)
(0%-40%)
(0%-23%)
Qual
X
X
X
X
X
6
5
2
5
12
3
8
3
4
5
3
2
6
10
6
REC%
85
93
101
94
94
103
87
91
94
90
89
98
91
114
100
20.2
20.2
20.2
20.2
20.2
20.2
17.9
20.2
19.5
20.2
19.6
20.2
20.2
19.2
20.2
638199Workorder:
RPD/D%
Page 6 of 12
Page 37 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PPF Acid)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid
(PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
DK2
MB2
09/28/23 16:30
10/17/23 04:37
09/28/23 16:30
QC
18.0
17.9
19.2
19.9
20.1
8.06
18.6
20.7
18.6
18.2
17.5
19.7
20.2
18.9
19.2
NOM Sample Range
(0%-26%)
(0%-27%)
(0%-27%)
(0%-27%)
(0%-25%)
(0%-39%)
(0%-26%)
(0%-25%)
(0%-27%)
(0%-40%)
(0%-25%)
(0%-26%)
(0%-26%)
(0%-31%)
(0%-30%)
Qual
JX
2
10
0
4
0
27
2
8
13
23
8
3
9
1
4
REC%
89
97
95
102
99
40
92
102
92
96
87
97
100
93
95
20.2
18.4
20.2
19.4
20.2
20.2
20.2
20.2
20.2
19.0
20.2
20.2
20.2
20.2
20.2
638199Workorder:
RPD/D%
Page 7 of 12
Page 38 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
1H, 1H, 2H, 2H-Perfluorodecane
sulfonic acid (8:2 FTS)
1H, 1H, 2H, 2H-Perfluorohexane
sulfonic acid (4:2 FTS)
1H, 1H, 2H, 2H-Perfluorooctane
sulfonic acid (6:2 FTS)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
Byproduct 4 (BP4)
Byproduct 5
Byproduct 6 (BP6)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-
X)(PFPrOPrA)
N-Ethylperfluorooctane
sulfonamide (EtFOSAm)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Ethylperfluorooctane
sulfonamido ethanol (NEtFOSE)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
MB2
DK2
MB2
DK2
MB2
10/17/23 04:07
09/28/23 16:13
10/17/23 04:07
09/28/23 16:13
10/17/23 04:07
09/28/23 16:13
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
UX
U
U
U
U
U
UX
U
UX
UX
UX
U
U
U
U
QC1205531242
REC%
MB
638199Workorder:
RPD/D%
Page 8 of 12
Page 39 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
N-Methylperfluorooctane
sulfonamide (NMeFOSA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
N-Methylperfluorooctane
sulfonamido ethanol (NMeFOSE)
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA) (TAF)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMPA)
Perfluoro-4-methoxybutanoic acid
(PFMBA)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
DK2
MB2
09/28/23 16:13
10/17/23 04:07
09/28/23 16:13
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
U
UX
UX
UX
UX
UX
UX
UX
UX
U
U
U
U
REC%
638199Workorder:
RPD/D%
Page 9 of 12
Page 40 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
Perfluorodecane sulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecane sulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropyl carboxylic
acid (PEPA)
Perfluoroheptane sulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononane sulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctane sulfonamide
(PFOSAm)
Perfluorooctane sulfonic acid
(PFOS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
DK2
MB2
09/28/23 16:13
10/17/23 04:07
09/28/23 16:13
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
U
U
UX
U
U
U
U
U
U
U
U
U
U
REC%
638199Workorder:
RPD/D%
Page 10 of 12
Page 41 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500162Batch
Perfluorooctanoic acid (PFOA)
Perfluoropentane sulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PPF Acid)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid
(PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
DK2
MB2
09/28/23 16:13
10/17/23 04:07
09/28/23 16:13
QC
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
U
UX
U
U
U
The Qualifiers in this report are defined as follows:
REC%
638199Workorder:
U
J
P
C
B
E
A
X
N
H
**
<
>
h
R
^
Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
Value is estimated
Organics--The concentrations between the primary and confirmation columns/detectors is >40% different. For HPLC, the difference is >70%.
Analyte has been confirmed by GC/MS analysis
The target analyte was detected in the associated blank.
Concentration of the target analyte exceeds the instrument calibration range
The TIC is a suspected aldol-condensation product
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Organics--Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based
on nearest internal standard response factor
Analytical holding time was exceeded
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
Preparation or preservation holding time was exceeded
Sample results are rejected
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
RPD/D%
Notes:
Page 11 of 12
Page 42 of 48 SDG: 638199
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Parmname
Page 12 of 12
Units Anlst Date TimeQCNOMSampleRangeQualREC%
638199Workorder:
D
N/A
ND
NJ
JNX
UJ
Q
N1
Y
N
J
Results are reported from a diluted aliquot of the sample
RPD or %Recovery limits do not apply.
Analyte concentration is not detected above the detection limit
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Non Calibrated Compound
Compound cannot be extracted
One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
See case narrative
QC Samples were not spiked with this compound
Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based on nearest
internal standard response factor
See case narrative for an explanation
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
RPD/D%
Page 43 of 48 SDG: 638199
Page 44 of 48 SDG: 638199
Page 45 of 48 SDG: 638199
State Certification
Alabama
Alaska
Alaska Drinking Water
Arkansas
CLIA
California
Colorado
Connecticut
DoD ELAP/ ISO17025 A2LA
Florida NELAP
Foreign Soils Permit
Georgia
Georgia SDWA
Hawaii
Idaho
Illinois NELAP
Indiana
Kansas NELAP
Kentucky SDWA
Kentucky Wastewater
Louisiana Drinking Water
Louisiana NELAP
Maine
Maryland
Massachusetts
Massachusetts PFAS Approv
Michigan
Mississippi
Nebraska
Nevada
New Hampshire NELAP
New Jersey NELAP
New Mexico
New York NELAP
North Carolina
North Carolina SDWA
North Dakota
Oklahoma
Pennsylvania NELAP
Puerto Rico
S. Carolina Radiochem
Sanitation Districts of L
South Carolina Chemistry
Tennessee
Texas NELAP
Utah NELAP
Vermont
Virginia NELAP
Washington
42200
17-018
SC00012
88-00651
42D0904046
2940
SC00012
PH-0169
2567.01
E87156
P330-15-00283, P330-15-00253
SC00012
967
SC00012
SC00012
200029
C-SC-01
E-10332
KY90129
KY90129
LA024
03046 (AI33904)
2023019
270
M-SC012
Letter
9976
SC00012
NE-OS-26-13
SC000122024-04
2054
SC002
SC00012
11501
233
45709
R-158
2022-160
68-00485
SC00012
10120002
9255651
10120001
TN 02934
T104704235-23-21
SC000122022-37
VT87156
460202
C780
List of current GEL Certifications as of 19 October 2023
Page 46 of 48 SDG: 638199
LCMSMS-PFC
Technical Case Narrative
EnSafe Inc.
SDG #: 638199

Product: The Extraction and Analysis of Per- and Polyfluoroalkyl Substances Using LCMSMS
Analytical Method: EPA 537.1 Mod, PFAS, Compliant with QSM Table B-15
Analytical Procedure: GL-OA-E-076 REV# 14
Analytical Batch: 2500162

Preparation Method: EPA 537.1 Mod, Compliant with QSM Table B-1 Prep
Preparation Procedure: GL-OA-E-076 REV# 14
Preparation Batch: 2500160
The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification
638199001 PZ21WG-091923
638199002 RW01WG-091923
638199003 FB01WQ-091923
638199004 PZ04WG-091923
638199005 RW05WG-092023
638199006 SWDownWS-092023
638199007 Canton IntakeWS-092023
638199008 Canton IntakeH-092023
638199009 Canton Intake FBWQ-092023
1205531242 Method Blank (MB)
1205531243 Laboratory Control Sample (LCS)
1205531244 Laboratory Control Sample Duplicate (LCSD)

The samples in this SDG were analyzed on an "as received" basis.
Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.

Calibration Information

CCV Requirements
Calibration verification standards (ICV or CCV) requirements have not been met for samples in this batch in this
SDG. One or more target analytes failed acceptance criteria with a positive bias in the standards bracketing the
samples in this SDG. These target analytes were not detected in the associated environmental samples; therefore,
the non-compliance had no adverse effect on the data.

Quality Control (QC) Information

Laboratory Control Sample Duplicate (LCSD)
An LCSD was used in place of matrix QC due to limited sample volume.

Technical Information
Page 47 of 48 SDG: 638199

Sample Dilutions
The following samples and/or QC were diluted due to the Internal Standard Recovery not within the limits in the
undiluted analysis. 638199001 (PZ21WG-091923), 638199002 (RW01WG-091923), 638199004
(PZ04WG-091923) and 638199005 (RW05WG-092023).
Analyte
638199
001 002 004 005
1H, 1H, 2H, 2H-Perfluorohexane sulfonic acid (4:2 FTS)1X 5X 5X 1X
1H, 1H, 2H, 2H-Perfluorooctane sulfonic acid (6:2 FTS)5X 5X 5X 5X
1H, 1H, 2H, 2H-Perfluorodecane sulfonic acid (8:2 FTS)1X 1X 5X 1X

Miscellaneous Information

Additional Comments
Some analytes are X qualified because the standards used to make the initial calibration curve did not meet the
ISO 17025 criterion. These are the only standards available for these analytes.

Certification Statement

Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 48 of 48 SDG: 638199

October 11, 2023

Amy Delinsky
NC Dept Environmental Quality
1646 Mail Service Center
Raleigh, North Carolina 27699

Re: Routine Analysis
Work Order: 638295

Dear Amy Delinsky:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on September 22, 2023. This original data report has been prepared and reviewed in
accordance with GEL's standard operating procedures.

The samples were delivered with proper chain of custody documentation and signatures. All sample containers
arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample
receipt.
Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards,
with any exceptions noted. The results reported relate only to the items tested and to the sample as received by
the laboratory. These results may not be reproduced except as full reports without approval by the laboratory.
Copies of GEL's accreditations and certifications can be found on our website at www.gel.com.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 1614.

Sincerely,

PM_SIGN_HERE
Delaney Stone
Project Manager

Purchase Order: SIGNED QUOTE
Enclosures
Page 1 of 105 SDG: 638295
Reviewed by USER_SIGN_HERE
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis Report
NCDQ001 NC Dept Environmental Quality
Client SDG: 638295 GEL Work Order: 638295
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above
the limit as defined in the 'U' qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures. Please direct any questions to your Project Manager, Delaney Stone.
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound
J Value is estimated
U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
h Preparation or preservation holding time was exceeded
for
Page 2 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
24999921910ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/04/23JMB30.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
0.471
18.8
3.77
0.471
0.471
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295001
Water
19-SEP-23 10:07
22-SEP-23
PZ-21-FB NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
0.188
7.54
1.24
0.188
0.188
1UX
U
UX
UX
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
U
UX
UX
UX
UX
UX
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
Page 3 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
24999921721
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/28/23JMB3
0.377
1.88
3.77
3.77
3.70
3.54
14.1
3.62
3.77
3.77
3.77
3.77
3.77
1.68
1.88
1.83
1.88
1.88
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295001
PZ-21-FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.188
0.622
1.24
1.24
1.24
1.24
5.07
1.24
1.24
1.24
1.24
1.24
0.622
0.622
0.754
0.622
0.735
0.622
2
UX
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
Page 4 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
1.79
1.88
3.77
1.72
1.88
1.81
1.88
3.77
1.88
1.88
1.88
1.77
1.88
1.88
1.88
1.88
1.88
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295001
PZ-21-FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.622
0.622
1.24
0.622
0.754
0.660
0.622
1.24
0.622
0.754
0.754
0.622
0.622
0.754
0.622
0.622
0.622
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
0.0188
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Liquid 09/28/23 24999910826EF
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Notes:
Page 5 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295001
PZ-21-FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 6 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25010260612ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/05/23JMB30.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
0.434
17.3
3.47
0.434
0.434
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295002
Ground Water
19-SEP-23 10:05
22-SEP-23
PZ-21 NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
6.94
1.15
0.173
0.173
1UX
U
UX
JX
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
U
UX
UX
UX
UX
UX
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
0.326
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
Page 7 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25010261741
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/29/23JMB3
0.347
1.73
3.47
3.47
3.41
3.33
3.47
3.47
3.47
3.47
3.47
1.54
1.73
1.68
1.73
1.73
1.65
1.73
3.47
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295002
PZ-21 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.173
0.573
1.15
1.15
1.15
1.15
1.15
1.15
1.15
1.15
0.573
0.573
0.694
0.573
0.677
0.573
0.573
0.573
1.15
2
UX
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.26
2.42
ND
ND
ND
ND
1.67
ND
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
Page 8 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
2501026
2501026
0957
1123
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/02/23
10/02/23
JMB3
JMB3
1.58
1.73
1.67
1.73
3.47
1.73
1.73
1.73
1.63
1.73
1.73
1.73
1.73
1.73
65.1
81.5
1
1
1
1
1
1
1
1
1
1
1
1
1
1
5
25
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295002
PZ-21 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.573
0.694
0.607
0.573
1.15
0.573
0.694
0.694
0.573
0.573
0.694
0.573
0.573
0.573
23.3
28.6
3
4
J
U
U
U
U
U
U
U
U
U
U
U
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
EPA 537Mod PFCs by LC-MS/MS "As Received"
0.675
2.00
ND
ND
ND
ND
5.15
12.2
ND
1.82
ND
ND
ND
ND
ND
ND
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Liquid 09/29/23 25010191158EF
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
3
4
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Notes:
Page 9 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295002
PZ-21 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 10 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25010261815ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/29/23JMB3100
200
200
196
188
750
192
200
200
200
200
200
89.0
100
97.0
100
100
95.0
100
200
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295003
Ground Water
19-SEP-23 14:33
22-SEP-23
PZ-4 NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
33.0
66.0
66.0
66.0
66.0
269
66.0
66.0
66.0
66.0
66.0
33.0
33.0
40.0
33.0
39.0
33.0
33.0
33.0
66.0
1U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Page 11 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25010260702
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/05/23JMB3
91.0
100
96.0
100
200
100
100
100
94.0
100
100
100
100
100
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295003
PZ-4 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
33.0
40.0
35.0
33.0
66.0
33.0
40.0
40.0
33.0
33.0
40.0
33.0
33.0
33.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
2
U
J
U
U
U
U
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
U
U
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
40.7
ND
ND
ND
ND
ND
ND
ND
124
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Page 12 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
200
25.0
25.0
20.0
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295003
PZ-4 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
10.0
10.0
10.0
10.0
10.0
10.0
10.0
400
66.0
10.0
10.0
10.0
UX
UX
JX
UX
U
U
UX
UX
UX
UX
UX
X
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
23.4
ND
ND
ND
ND
ND
ND
ND
ND
23.1
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Liquid 09/29/23 25010191158EF
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Notes:
Page 13 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295003
PZ-4 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 14 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25010261824ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/29/23JMB31.78
3.55
3.55
3.49
3.55
3.55
3.55
3.55
3.55
1.58
1.78
1.72
1.78
1.78
1.69
1.78
1.62
1.78
1.70
1.78
1.78
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295004
Ground Water
19-SEP-23 12:28
22-SEP-23
RW-1 NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.586
1.17
1.17
1.17
1.17
1.17
1.17
1.17
0.586
0.586
0.710
0.586
0.692
0.586
0.586
0.586
0.586
0.710
0.621
0.586
0.586
1U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctanesulfonamide
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.14
ND
4.10
ND
0.596
ND
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
Page 15 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
2501026
2501026
2501026
1023
1149
0718
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/02/23
10/02/23
10/05/23
JMB3
JMB3
JMB3
1.78
1.78
1.67
1.78
1.78
1.78
1.78
1.78
17.0
17.8
17.8
83.4
333
0.444
0.444
0.444
0.444
0.444
0.444
0.444
0.444
0.444
0.444
0.444
1
1
1
1
1
1
1
1
5
5
5
25
25
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295004
RW-1 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.710
0.710
0.586
0.586
0.710
0.586
0.586
0.586
5.86
5.86
5.86
29.3
119
0.178
0.178
0.178
0.178
0.178
0.178
0.178
0.178
0.178
0.178
0.178
2
3
4
U
U
U
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
U
U
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorooctadecanoic acid
(PFODA)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
EPA 537Mod PFCs by LC-MS/MS "As Received"
3.62
2.64
ND
6.07
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
Page 16 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
0.444
0.444
0.444
0.444
0.444
0.444
0.444
17.8
3.55
0.444
0.444
0.355
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295004
RW-1 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.178
0.178
0.178
0.178
0.178
0.178
0.178
7.10
1.17
0.178
0.178
0.178
UX
UX
UX
UX
U
U
UX
UX
UX
UX
UX
UX
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
0.0178
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Liquid 09/29/23 25010191158EF
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
3
4
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Notes:
Page 17 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295004
RW-1 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 18 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25019641508ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/03/23MB2100
200
200
196
188
750
192
200
200
200
200
200
89.0
100
97.0
100
100
95.0
100
200
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295005
Ground Water
20-SEP-23 10:28
22-SEP-23
RW-5 NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
33.0
66.0
66.0
66.0
66.0
269
66.0
66.0
66.0
66.0
66.0
33.0
33.0
40.0
33.0
39.0
33.0
33.0
33.0
66.0
1U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Page 19 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25019640221
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/05/23JMB3
91.0
100
96.0
100
200
100
100
100
94.0
100
100
100
100
100
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295005
RW-5 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
33.0
40.0
35.0
33.0
66.0
33.0
40.0
40.0
33.0
33.0
40.0
33.0
33.0
33.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
U
U
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Page 20 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25047941902
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L 10/10/23JMB3
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
200
25.0
25.0
20.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295005
RW-5 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
10.0
10.0
10.0
10.0
10.0
10.0
10.0
400
66.0
10.0
10.0
10.0
10.0 3
UX
UX
X
UX
U
U
UX
UX
UX
UX
UX
X
Xh
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
34.1
ND
ND
ND
ND
ND
ND
ND
ND
273
38.9
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
The following Prep Methods were performed:
EPA 537.1 Modified
EPA 537.1 Modified
PFCs Extraction in Liquid
PFCs Extraction in Liquid
10/06/23
10/02/23
2504793
2501960
1457
1149
DK2
RR4
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
3
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Page 21 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295005
RW-5 NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 22 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
24999921927ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/04/23JMB30.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
0.456
18.2
3.65
0.456
0.456
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295006
Water
19-SEP-23 14:35
22-SEP-23
PZ-4-FB NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
0.182
7.29
1.20
0.182
0.182
1UX
U
UX
UX
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
U
UX
UX
UX
UX
UX
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
Page 23 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
24999921730
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/28/23JMB3
0.365
1.82
3.65
3.65
3.58
3.43
13.7
3.50
3.65
3.65
3.65
3.65
3.65
1.62
1.82
1.77
1.82
1.82
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295006
PZ-4-FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.182
0.602
1.20
1.20
1.20
1.20
4.90
1.20
1.20
1.20
1.20
1.20
0.602
0.602
0.729
0.602
0.711
0.602
2
UX
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
Page 24 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
1.73
1.82
3.65
1.66
1.82
1.75
1.82
3.65
1.82
1.82
1.82
1.71
1.82
1.82
1.82
1.82
1.82
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295006
PZ-4-FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.602
0.602
1.20
0.602
0.729
0.638
0.602
1.20
0.602
0.729
0.729
0.602
0.602
0.729
0.602
0.602
0.602
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
0.0182
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Liquid 09/28/23 24999910826EF
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Notes:
Page 25 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295006
PZ-4-FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 26 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
24999921739ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/28/23JMB31.90
3.80
3.80
3.73
3.57
14.2
3.64
3.80
3.80
3.80
3.80
3.80
1.69
1.90
1.84
1.90
1.90
1.80
1.90
3.80
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295007
Water
20-SEP-23 10:17
22-SEP-23
RW-5-FB NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.626
1.25
1.25
1.25
1.25
5.10
1.25
1.25
1.25
1.25
1.25
0.626
0.626
0.759
0.626
0.740
0.626
0.626
0.626
1.25
1U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
Page 27 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
24999922106
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/04/23JMB3
1.73
1.90
1.82
1.90
3.80
1.90
1.90
1.90
1.78
1.90
1.90
1.90
1.90
1.90
0.474
0.474
0.474
0.474
0.474
0.474
0.474
0.474
0.474
0.474
0.474
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295007
RW-5-FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.626
0.759
0.664
0.626
1.25
0.626
0.759
0.759
0.626
0.626
0.759
0.626
0.626
0.626
0.190
0.190
0.190
0.190
0.190
0.190
0.190
0.190
0.190
0.190
0.190
2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
U
U
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
Page 28 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
0.474
0.474
0.474
0.474
0.474
0.474
0.474
19.0
3.80
0.474
0.474
0.380
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295007
RW-5-FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.190
0.190
0.190
0.190
0.190
0.190
0.190
7.59
1.25
0.190
0.190
0.190
UX
UX
UX
UX
U
U
UX
UX
UX
UX
UX
UX
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
0.0190
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Liquid 09/28/23 24999910826EF
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Notes:
Page 29 of 105 SDG: 638295
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 11, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638295007
RW-5-FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 30 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
Parmname
Amy DelinskyContact:
NC Dept Environmental Quality
1646 Mail Service Center
Raleigh, North Carolina
October 11, 2023Report Date:
Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
DK2
JMB3
DK2
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
QC
19.2
19.5
21.8
19.7
19.4
20.3
20.3
20.0
20.8
19.3
17.4
15.6
20.0
NOM Sample Range
(60%-158%)
(59%-144%)
(67%-144%)
(58%-144%)
(54%-128%)
(52%-141%)
(67%-154%)
(73%-141%)
(68%-135%)
(56%-151%)
(60%-153%)
(60%-141%)
(61%-148%)
Qual
X
X
X
X
QC1205530789
REC%
93
100
106
96
94
99
99
97
108
100
89
79
97
20.6
19.4
20.6
20.6
20.6
20.6
20.6
20.6
19.2
19.3
19.6
19.8
20.6
LCS
638295Workorder:
RPD%
Page 1 of 63
Page 31 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
09/28/23 14:29
09/29/23 01:06
QC
20.8
22.6
20.0
21.9
16.0
17.3
21.4
21.9
19.0
18.7
19.4
20.3
20.6
23.1
22.4
NOM Sample Range
(23%-155%)
(57%-139%)
(20%-154%)
(59%-145%)
(35%-138%)
(63%-143%)
(5%-158%)
(5%-149%)
(59%-145%)
(48%-149%)
(52%-148%)
(58%-147%)
(60%-151%)
(62%-148%)
(60%-144%)
Qual
X
X
X
X
X
X
X
X
X
REC%
101
109
97
106
78
84
104
106
92
91
94
99
100
112
109
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
638295Workorder:
RPD%
Page 2 of 63
Page 32 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
09/28/23 14:29
QC
21.1
20.1
19.5
20.2
15.6
19.2
18.7
21.1
17.0
20.0
16.8
22.6
19.0
20.6
18.0
NOM Sample Range
(58%-142%)
(50%-150%)
(52%-144%)
(60%-149%)
(70%-144%)
(73%-151%)
(58%-134%)
(65%-145%)
(57%-134%)
(65%-137%)
(20%-160%)
(68%-138%)
(71%-133%)
(69%-144%)
(67%-145%)
Qual
X
X
X
REC%
103
97
95
98
85
93
94
102
85
97
81
115
92
100
96
20.6
20.6
20.6
20.6
18.2
20.6
19.9
20.6
19.9
20.6
20.6
19.6
20.6
20.6
18.8
638295Workorder:
RPD%
Page 3 of 63
Page 33 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
09/28/23 14:29
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
09/29/23 00:51
QC
20.5
18.3
20.5
10.7
20.1
21.6
20.2
19.9
19.7
18.5
19.6
21.2
20.0
29.4
ND
NOM Sample Range
(70%-138%)
(64%-133%)
(69%-133%)
(35%-165%)
(64%-134%)
(65%-145%)
(66%-139%)
(67%-136%)
(72%-143%)
(49%-153%)
(66%-138%)
(58%-140%)
(63%-135%)
(5%-158%)
Qual
JX
X
UX
QC1205530788
REC%
100
92
100
52
97
105
98
103
95
90
95
103
97
143
20.6
19.8
20.6
20.6
20.6
20.6
20.6
19.4
20.6
20.6
20.6
20.6
20.6
20.6
MB
638295Workorder:
RPD%
Page 4 of 63
Page 34 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
JMB3
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
UX
U
U
U
UX
U
U
U
U
UX
U
U
U
REC%
638295Workorder:
RPD%
Page 5 of 63
Page 35 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
09/28/23 14:21
09/29/23 00:51
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
UX
UX
REC%
638295Workorder:
RPD%
Page 6 of 63
Page 36 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
09/29/23 00:51
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
U
U
U
U
U
UX
U
U
U
U
U
U
U
REC%
638295Workorder:
RPD%
Page 7 of 63
Page 37 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
09/29/23 00:51
09/29/23 01:36
09/28/23 14:04
09/29/23 01:36
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
212
157
221
200
NOM Sample
10.5
ND
ND
ND
Range
(50%-145%)
(42%-138%)
(51%-159%)
(50%-148%)
Qual
U
U
U
U
U
U
UX
U
U
U
UX
X
X
QC1205530790 637450004
REC%
101
84
110
100
200
188
200
200
MS
638295Workorder:
X
U
U
UX
RPD%
Page 8 of 63
Page 38 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
09/28/23 14:04
09/29/23 01:36
09/28/23 14:04
09/29/23 01:36
09/28/23 14:04
09/29/23 01:36
QC
190
178
191
214
173
197
175
200
218
199
209
214
208
182
187
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(44%-127%)
(39%-138%)
(62%-132%)
(58%-157%)
(54%-139%)
(53%-151%)
(50%-154%)
(40%-152%)
(61%-142%)
(26%-138%)
(38%-148%)
(26%-139%)
(40%-144%)
(38%-133%)
(40%-155%)
Qual
X
X
X
X
REC%
95
89
96
107
93
105
92
104
109
100
105
107
104
91
94
200
200
200
200
186
187
190
192
200
200
200
200
200
200
200
638295Workorder:
U
U
U
UX
U
U
U
U
UX
U
U
U
U
UX
UX
RPD%
Page 9 of 63
Page 39 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
09/29/23 01:36
09/28/23 14:04
QC
274
252
213
180
202
225
219
234
206
211
214
206
220
154
191
NOM Sample
8.74
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.34
ND
ND
ND
Range
(45%-160%)
(50%-150%)
(61%-141%)
(43%-156%)
(50%-148%)
(43%-160%)
(45%-163%)
(40%-162%)
(38%-165%)
(31%-150%)
(50%-150%)
(40%-182%)
(19%-167%)
(52%-147%)
(57%-149%)
Qual
X
X
X
X
X
X
X
X
X
REC%
133
126
107
90
101
113
110
117
103
105
107
102
110
87
95
200
200
200
200
200
200
200
200
200
200
200
200
200
177
200
638295Workorder:
X
UX
UX
U
U
UX
UX
UX
UX
U
UX
JX
U
U
U
RPD%
Page 10 of 63
Page 40 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
09/28/23 14:04
09/29/23 01:36
09/28/23 14:04
QC
154
216
126
199
208
175
198
195
177
178
169
189
109
193
180
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(45%-136%)
(44%-143%)
(47%-138%)
(45%-142%)
(50%-150%)
(56%-149%)
(51%-149%)
(32%-151%)
(50%-148%)
(50%-150%)
(48%-138%)
(54%-146%)
(18%-140%)
(49%-143%)
(42%-150%)
Qual
X
REC%
80
108
65
99
104
92
99
97
97
89
88
95
54
97
90
193
200
194
200
200
190
200
200
182
200
192
200
200
200
200
638295Workorder:
U
U
U
U
UX
U
U
U
U
U
U
U
U
U
U
RPD%
Page 11 of 63
Page 41 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
JMB3
09/28/23 14:04
09/29/23 01:36
09/28/23 14:04
09/29/23 01:36
09/29/23 01:52
09/28/23 14:12
09/29/23 01:52
09/28/23 14:12
QC
203
187
204
208
198
207
184
382
215
201
221
199
203
178
214
NOM Sample
ND
ND
7.08
ND
ND
ND
ND
ND
10.5
ND
ND
ND
ND
ND
ND
Range
(50%-151%)
(55%-151%)
(51%-146%)
(32%-155%)
(41%-148%)
(41%-142%)
(44%-141%)
(45%-164%)
(0%-30%)
(0%-36%)
(0%-28%)
(0%-34%)
(0%-39%)
(0%-40%)
(0%-28%)
Qual
X
X
X
X
QC1205530791 637450004
1
24
0
1
7
0
11
REC%
101
100
99
91
99
104
92
191
102
107
110
100
101
89
107
200
188
200
200
200
200
200
200
200
188
200
200
200
200
200
MSD
638295Workorder:
*
U
U
J
UX
U
U
U
UX
X
U
U
UX
U
U
U
RPD%
Page 12 of 63
Page 42 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
DK2
09/29/23 01:52
09/28/23 14:12
09/29/23 01:52
09/28/23 14:12
09/29/23 01:52
QC
198
202
192
166
181
196
219
188
184
202
181
191
248
246
203
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.74
ND
ND
Range
(0%-31%)
(0%-33%)
(0%-39%)
(0%-40%)
(0%-44%)
(0%-29%)
(0%-42%)
(0%-36%)
(0%-40%)
(0%-36%)
(0%-33%)
(0%-26%)
(0%-32%)
(0%-34%)
(0%-30%)
Qual
X
X
X
X
X
X
X
8
16
2
5
10
11
9
11
15
3
1
2
10
3
5
REC%
99
108
103
87
94
98
109
94
92
101
91
95
120
123
102
200
186
187
190
192
200
200
200
200
200
200
200
200
200
200
638295Workorder:
UX
U
U
U
U
UX
U
U
U
U
UX
UX
X
UX
UX
RPD%
Page 13 of 63
Page 43 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
09/29/23 01:52
09/28/23 14:12
QC
185
190
200
195
220
209
200
205
187
212
173
191
171
210
139
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
2.34
ND
ND
ND
ND
ND
ND
Range
(0%-33%)
(0%-28%)
(0%-44%)
(0%-38%)
(0%-41%)
(0%-31%)
(0%-46%)
(0%-30%)
(0%-41%)
(0%-35%)
(0%-27%)
(0%-23%)
(0%-36%)
(0%-35%)
(0%-35%)
Qual
X
X
X
X
X
X
3
6
12
12
6
2
5
5
9
4
12
0
10
3
10
REC%
92
95
100
98
110
105
100
102
92
106
98
96
89
105
72
200
200
200
200
200
200
200
200
200
200
177
200
193
200
194
638295Workorder:
U
U
UX
UX
UX
UX
U
UX
JX
U
U
U
U
U
U
RPD%
Page 14 of 63
Page 44 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
09/28/23 14:12
09/29/23 01:52
09/28/23 14:12
QC
195
187
215
209
206
166
206
199
208
115
190
223
219
155
198
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.08
Range
(0%-30%)
(0%-30%)
(0%-30%)
(0%-26%)
(0%-33%)
(0%-31%)
(0%-26%)
(0%-35%)
(0%-30%)
(0%-44%)
(0%-28%)
(0%-31%)
(0%-28%)
(0%-31%)
(0%-24%)
Qual
X
2
11
21
5
6
6
15
16
10
6
2
22
8
19
3
REC%
98
94
113
104
103
91
103
103
104
58
95
112
109
83
95
200
200
190
200
200
182
200
192
200
200
200
200
200
188
200
638295Workorder:
U
UX
U
U
U
U
U
U
U
U
U
U
U
U
J
RPD%
Page 15 of 63
Page 45 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992
2501026
Batch
Batch
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
09/29/23 01:52
09/28/23 14:12
09/29/23 01:52
10/05/23 04:16
09/29/23 16:49
10/05/23 04:16
09/29/23 16:49
10/05/23 04:16
09/29/23 16:49
QC
192
192
209
197
346
22.8
21.6
23.1
25.2
23.6
20.8
21.1
25.5
22.6
NOM Sample
ND
ND
ND
ND
ND
Range
(0%-34%)
(0%-32%)
(0%-35%)
(0%-34%)
(0%-35%)
(60%-158%)
(59%-144%)
(67%-144%)
(58%-144%)
(54%-128%)
(52%-141%)
(67%-154%)
(73%-141%)
(68%-135%)
Qual
JX
X
X
X
X
QC1205532674
8
3
1
7
10
REC%
82
96
104
98
173
109
109
110
120
112
99
101
122
115
200
200
200
200
200
21.0
19.8
21.0
21.0
21.0
21.0
21.0
21.0
19.6
LCS
638295Workorder:
*
UX
U
U
U
UX
RPD%
Page 16 of 63
Page 46 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 09/29/23 16:49
10/05/23 04:16
09/29/23 16:49
10/05/23 04:16
QC
20.7
20.5
22.2
23.8
21.5
20.6
23.8
24.8
20.1
22.0
24.1
24.7
23.9
29.7
25.5
NOM Sample Range
(56%-151%)
(60%-153%)
(60%-141%)
(61%-148%)
(23%-155%)
(57%-139%)
(20%-154%)
(59%-145%)
(35%-138%)
(63%-143%)
(5%-158%)
(5%-149%)
(59%-145%)
(48%-149%)
(52%-148%)
Qual
X
X
X
X
X
X
REC%
105
103
110
113
102
98
114
118
96
105
115
118
114
142
122
19.6
19.9
20.1
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
638295Workorder:
RPD%
Page 17 of 63
Page 47 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/05/23 04:16
09/29/23 16:49
10/05/23 04:16
QC
26.4
24.4
28.6
28.0
24.4
23.7
23.4
23.2
17.0
19.7
21.1
22.5
18.3
19.4
22.5
NOM Sample Range
(58%-147%)
(60%-151%)
(62%-148%)
(60%-144%)
(58%-142%)
(50%-150%)
(52%-144%)
(60%-149%)
(70%-144%)
(73%-151%)
(58%-134%)
(65%-145%)
(57%-134%)
(65%-137%)
(20%-160%)
Qual
X
X
X
X
X
X
X
REC%
126
116
137
134
116
113
111
111
92
94
104
107
90
92
107
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
18.6
21.0
20.3
21.0
20.3
21.0
21.0
638295Workorder:
RPD%
Page 18 of 63
Page 48 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 09/29/23 16:49
10/05/23 04:16
09/29/23 16:49
QC
21.8
19.6
23.5
20.2
20.1
21.0
21.5
11.6
21.9
20.9
20.7
20.0
21.3
24.5
22.1
NOM Sample Range
(68%-138%)
(71%-133%)
(69%-144%)
(67%-145%)
(70%-138%)
(64%-133%)
(69%-133%)
(35%-165%)
(64%-134%)
(65%-145%)
(66%-139%)
(67%-136%)
(72%-143%)
(49%-153%)
(66%-138%)
Qual
X
REC%
109
93
112
105
96
104
103
55
104
100
99
101
101
117
105
19.9
21.0
21.0
19.1
21.0
20.1
21.0
21.0
21.0
21.0
21.0
19.7
21.0
21.0
21.0
638295Workorder:
RPD%
Page 19 of 63
Page 49 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 09/29/23 16:49
10/05/23 04:16
10/05/23 04:00
09/29/23 16:41
10/05/23 04:00
09/29/23 16:41
10/05/23 04:00
09/29/23 16:41
QC
21.1
19.9
26.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample Range
(58%-140%)
(63%-135%)
(5%-158%)
Qual
X
UX
U
U
UX
U
U
U
UX
U
U
U
U
QC1205532673
REC%
100
95
124
21.0
21.0
21.0
MB
638295Workorder:
RPD%
Page 20 of 63
Page 50 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/05/23 04:00
09/29/23 16:41
10/05/23 04:00
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
UX
U
U
U
U
UX
UX
UX
UX
UX
U
U
UX
UX
UX
REC%
638295Workorder:
RPD%
Page 21 of 63
Page 51 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/05/23 04:00
09/29/23 16:41
10/05/23 04:00
09/29/23 16:41
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
UX
U
UX
UX
U
U
U
U
U
U
U
UX
U
U
U
REC%
638295Workorder:
RPD%
Page 22 of 63
Page 52 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 09/29/23 16:41
10/05/23 04:00
09/29/23 16:41
10/05/23 04:00
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
U
U
U
U
U
U
U
U
UX
U
U
U
UX
REC%
638295Workorder:
RPD%
Page 23 of 63
Page 53 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/05/23 06:29
09/29/23 17:58
10/05/23 06:29
09/29/23 17:58
10/05/23 06:29
09/29/23 17:58
10/02/23 11:32
10/02/23 10:06
09/29/23 17:58
10/05/23 06:29
09/29/23 17:58
QC
22.1
13.4
20.3
16.9
19.9
17.2
20.1
19.5
15.1
ND
22.9
18.0
21.4
19.6
17.1
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(50%-145%)
(42%-138%)
(51%-159%)
(50%-148%)
(44%-127%)
(39%-138%)
(62%-132%)
(58%-157%)
(54%-139%)
(53%-151%)
(50%-154%)
(40%-152%)
(61%-142%)
(26%-138%)
(38%-148%)
Qual
X
X
X
U
J
X
QC1205532675 638295002
REC%
136
88
125
104
123
106
124
120
100
0
148
115
132
121
105
16.2
15.3
16.2
16.2
16.2
16.2
16.2
16.2
15.1
15.2
15.4
15.6
16.2
16.2
16.2
MS
638295Workorder:
*
UX
U
U
UX
U
U
U
UX
U
U
U
U
UX
U
U
RPD%
Page 24 of 63
Page 54 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 09/29/23 17:58
10/05/23 06:29
QC
19.3
17.2
22.4
22.6
258
77.1
21.2
15.6
23.4
18.7
20.2
21.0
13.3
19.0
17.7
NOM Sample
ND
ND
ND
ND
0.326
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(26%-139%)
(40%-144%)
(38%-133%)
(40%-155%)
(45%-160%)
(50%-150%)
(61%-141%)
(43%-156%)
(50%-148%)
(43%-160%)
(45%-163%)
(40%-162%)
(38%-165%)
(31%-150%)
(50%-150%)
Qual
X
X
X
X
X
X
X
X
X
X
REC%
119
106
138
139
1580
474
130
96
144
115
124
129
82
117
109
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
638295Workorder:
*
*
*
U
U
UX
UX
JX
UX
UX
U
U
UX
UX
UX
UX
U
UX
RPD%
Page 25 of 63
Page 55 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/05/23 06:29
09/29/23 17:58
10/05/23 06:29
09/29/23 17:58
QC
4.96
31.4
17.7
20.8
11.3
17.9
10.5
15.4
20.6
15.6
16.4
18.9
16.7
15.0
15.0
NOM Sample
ND
ND
3.26
2.42
ND
ND
ND
ND
ND
ND
1.67
ND
0.675
2.00
ND
Range
(40%-182%)
(19%-167%)
(52%-147%)
(57%-149%)
(45%-136%)
(44%-143%)
(47%-138%)
(45%-142%)
(50%-150%)
(56%-149%)
(51%-149%)
(32%-151%)
(50%-148%)
(50%-150%)
(48%-138%)
Qual
X
X
REC%
31
193
101
113
72
110
66
94
127
101
91
117
108
80
96
16.2
16.2
14.4
16.2
15.7
16.2
15.7
16.2
16.2
15.4
16.2
16.2
14.8
16.2
15.6
638295Workorder:
*
*
UX
U
U
U
U
U
UX
U
J
U
J
U
RPD%
Page 26 of 63
Page 56 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 09/29/23 17:58
10/05/23 06:29
09/29/23 17:58
10/05/23 06:29
10/05/23 06:45
09/29/23 18:07
10/05/23 06:45
QC
16.3
13.8
17.0
19.4
28.1
15.0
17.2
6.85
18.3
19.5
18.3
124
26.2
15.3
21.1
NOM Sample
ND
ND
ND
5.15
12.2
ND
1.82
ND
ND
ND
ND
ND
ND
ND
ND
Range
(54%-146%)
(18%-140%)
(49%-143%)
(42%-150%)
(50%-151%)
(55%-151%)
(51%-146%)
(32%-155%)
(41%-148%)
(41%-142%)
(44%-141%)
(45%-164%)
(0%-30%)
(0%-36%)
(0%-28%)
Qual
JX
X
X
QC1205532676 638295002
17
14
4
REC%
101
85
105
88
98
95
95
24
113
120
113
762
155
97
125
16.2
16.2
16.2
16.2
16.2
15.3
16.2
16.2
16.2
16.2
16.2
16.2
16.8
15.9
16.8
MSD
638295Workorder:
*
*
*
U
U
U
U
UX
U
U
U
UX
UX
U
U
RPD%
Page 27 of 63
Page 57 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/05/23 06:45
09/29/23 18:07
10/05/23 06:45
09/29/23 18:07
10/02/23 11:40
10/02/23 10:14
09/29/23 18:07
10/05/23 06:45
09/29/23 18:07
10/05/23 06:45
QC
18.7
20.9
18.5
18.7
21.8
18.6
ND
27.1
17.7
23.5
18.7
16.8
18.1
16.3
24.4
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(0%-34%)
(0%-39%)
(0%-40%)
(0%-28%)
(0%-31%)
(0%-33%)
(0%-39%)
(0%-40%)
(0%-44%)
(0%-29%)
(0%-42%)
(0%-36%)
(0%-40%)
(0%-36%)
(0%-33%)
Qual
X
X
U
J
X
X
10
5
7
7
11
20
N/A
17
1
9
5
2
6
5
9
REC%
111
124
110
111
129
118
0
169
110
139
111
100
108
97
145
16.8
16.8
16.8
16.8
16.8
15.7
15.7
16.0
16.2
16.8
16.8
16.8
16.8
16.8
16.8
638295Workorder:
*
*
*
UX
U
U
U
UX
U
U
U
U
UX
U
U
U
U
UX
RPD%
Page 28 of 63
Page 58 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/05/23 06:45
09/29/23 18:07
QC
24.9
290
84.9
25.4
13.7
25.6
20.5
22.6
13.8
17.5
21.1
18.6
5.73
35.5
16.8
NOM Sample
ND
0.326
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.26
Range
(0%-26%)
(0%-32%)
(0%-34%)
(0%-30%)
(0%-33%)
(0%-28%)
(0%-44%)
(0%-38%)
(0%-41%)
(0%-31%)
(0%-46%)
(0%-30%)
(0%-41%)
(0%-35%)
(0%-27%)
Qual
X
X
X
X
X
X
X
X
X
X
10
12
10
18
13
9
9
11
42
28
10
5
14
12
6
REC%
148
1720
504
151
81
152
122
134
82
104
125
110
34
211
91
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
14.9
638295Workorder:
*
*
*
*
*
*
UX
JX
UX
UX
U
U
UX
UX
UX
UX
U
UX
UX
U
*
RPD%
Page 29 of 63
Page 59 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026Batch
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 09/29/23 18:07
10/05/23 06:45
09/29/23 18:07
QC
22.4
15.2
21.8
11.1
18.5
21.5
17.0
18.6
21.7
19.5
16.0
16.8
18.1
14.1
20.5
NOM Sample
2.42
ND
ND
ND
ND
ND
ND
1.67
ND
0.675
2.00
ND
ND
ND
ND
Range
(0%-23%)
(0%-36%)
(0%-35%)
(0%-35%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-26%)
(0%-33%)
(0%-31%)
(0%-26%)
(0%-35%)
(0%-30%)
(0%-44%)
(0%-28%)
Qual
X
7
29
20
6
18
4
8
12
13
16
6
12
10
2
18
REC%
118
94
130
68
110
128
106
100
129
123
83
104
108
83
122
16.8
16.3
16.8
16.3
16.8
16.8
16.0
16.8
16.8
15.4
16.8
16.2
16.8
16.8
16.8
638295Workorder:
U
U
U
U
UX
U
J
U
J
U
U
U
U
RPD%
Page 30 of 63
Page 60 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501026
2501964
Batch
Batch
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
JMB3
MB2
JMB3
MB2
09/29/23 18:07
10/05/23 06:45
09/29/23 18:07
10/05/23 06:45
10/05/23 02:04
10/03/23 15:00
10/05/23 02:04
10/03/23 15:00
QC
22.8
26.1
19.3
18.2
7.25
18.2
21.7
16.7
136
22.8
19.5
23.0
25.1
22.6
NOM Sample
5.15
12.2
ND
1.82
ND
ND
ND
ND
ND
Range
(0%-31%)
(0%-28%)
(0%-31%)
(0%-24%)
(0%-34%)
(0%-32%)
(0%-35%)
(0%-34%)
(0%-35%)
(60%-158%)
(59%-144%)
(67%-144%)
(58%-144%)
(54%-128%)
Qual
JX
X
X
X
QC1205534486
16
8
25
6
6
1
11
10
9
REC%
105
82
119
98
25
108
129
99
805
108
99
109
119
107
16.8
16.8
15.8
16.8
16.8
16.8
16.8
16.8
16.8
21.1
19.8
21.1
21.1
21.1
LCS
638295Workorder:
*
*
U
UX
U
U
U
UX
RPD%
Page 31 of 63
Page 61 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
JMB3
MB2
JMB3
MB2
JMB3
10/03/23 15:00
10/05/23 02:04
10/03/23 15:00
10/05/23 02:04
10/03/23 15:00
10/05/23 02:04
QC
24.0
21.7
25.8
21.8
20.2
15.9
21.8
23.9
20.8
19.7
21.8
24.7
20.0
23.9
27.6
NOM Sample Range
(52%-141%)
(67%-154%)
(73%-141%)
(68%-135%)
(56%-151%)
(60%-153%)
(60%-141%)
(61%-148%)
(23%-155%)
(57%-139%)
(20%-154%)
(59%-145%)
(35%-138%)
(63%-143%)
(5%-158%)
Qual
X
X
X
X
X
REC%
114
103
122
111
103
79
108
113
99
94
104
117
95
113
131
21.1
21.1
21.1
19.6
19.7
20.0
20.2
21.1
21.1
21.1
21.1
21.1
21.1
21.1
21.1
638295Workorder:
RPD%
Page 32 of 63
Page 62 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
MB2
10/05/23 02:04
10/03/23 15:00
QC
29.4
24.6
25.9
25.4
27.4
22.0
39.8
38.5
24.1
23.2
25.0
26.4
16.7
21.7
21.0
NOM Sample Range
(5%-149%)
(59%-145%)
(48%-149%)
(52%-148%)
(58%-147%)
(60%-151%)
(62%-148%)
(60%-144%)
(58%-142%)
(50%-150%)
(52%-144%)
(60%-149%)
(70%-144%)
(73%-151%)
(58%-134%)
Qual
X
X
X
X
X
X
X
X
REC%
139
117
123
121
130
104
189
183
114
110
119
125
90
103
103
21.1
21.1
21.1
21.1
21.1
21.1
21.1
21.1
21.1
21.1
21.1
21.1
18.6
21.1
20.3
638295Workorder:
*
*
RPD%
Page 33 of 63
Page 63 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
JMB3
MB2
10/03/23 15:00
10/05/23 02:04
10/03/23 15:00
QC
19.2
17.7
21.8
21.2
22.2
22.7
19.2
22.2
23.5
21.4
20.8
12.5
21.5
21.2
20.8
NOM Sample Range
(65%-145%)
(57%-134%)
(65%-137%)
(20%-160%)
(68%-138%)
(71%-133%)
(69%-144%)
(67%-145%)
(70%-138%)
(64%-133%)
(69%-133%)
(35%-165%)
(64%-134%)
(65%-145%)
(66%-139%)
Qual
X
REC%
91
87
104
101
111
108
91
115
112
106
99
59
102
101
99
21.1
20.4
21.1
21.1
20.0
21.1
21.1
19.2
21.1
20.2
21.1
21.1
21.1
21.1
21.1
638295Workorder:
RPD%
Page 34 of 63
Page 64 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
JMB3
MB2
JMB3
MB2
JMB3
MB2
JMB3
10/03/23 15:00
10/05/23 02:04
10/03/23 15:00
10/05/23 02:04
10/05/23 01:47
10/03/23 14:51
10/05/23 01:47
10/03/23 14:51
10/05/23 01:47
QC
21.4
21.0
24.7
21.3
21.2
23.6
29.2
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample Range
(67%-136%)
(72%-143%)
(49%-153%)
(66%-138%)
(58%-140%)
(63%-135%)
(5%-158%)
Qual
X
X
UX
U
U
UX
U
U
U
UX
QC1205534485
REC%
108
100
117
101
101
112
139
19.8
21.1
21.1
21.1
21.1
21.1
21.1
MB
638295Workorder:
RPD%
Page 35 of 63
Page 65 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
JMB3
MB2
JMB3
10/03/23 14:51
10/05/23 01:47
10/03/23 14:51
10/05/23 01:47
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
U
U
UX
U
U
U
U
UX
UX
UX
UX
UX
U
REC%
638295Workorder:
RPD%
Page 36 of 63
Page 66 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
MB2
10/05/23 01:47
10/03/23 14:51
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
UX
UX
UX
UX
U
UX
UX
U
U
U
U
U
U
U
REC%
638295Workorder:
RPD%
Page 37 of 63
Page 67 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
MB2
JMB3
10/05/23 01:47
10/03/23 14:51
10/05/23 01:47
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
UX
U
U
U
U
U
U
U
U
U
U
U
U
U
UX
REC%
638295Workorder:
RPD%
Page 38 of 63
Page 68 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
JMB3
MB2
JMB3
MB2
JMB3
MB2
10/03/23 14:51
10/05/23 01:47
10/05/23 02:54
10/03/23 16:26
10/05/23 02:54
10/03/23 16:26
10/05/23 02:54
10/03/23 16:26
QC
ND
ND
ND
ND
26.1
14.3
21.1
16.1
17.0
16.2
15.5
21.8
15.9
19.2
12.6
NOM Sample
ND
ND
0.520
ND
ND
ND
ND
ND
ND
ND
ND
Range
(50%-145%)
(42%-138%)
(51%-159%)
(50%-148%)
(44%-127%)
(39%-138%)
(62%-132%)
(58%-157%)
(54%-139%)
(53%-151%)
(50%-154%)
Qual
U
U
U
UX
X
X
X
QC1205534487 638421009
REC%
160
93
126
99
104
99
95
133
105
126
81
16.3
15.4
16.3
16.3
16.3
16.3
16.3
16.3
15.2
15.3
15.5
MS
638295Workorder:
*UX
U
UX
U
U
U
UX
U
U
U
RPD%
Page 39 of 63
Page 69 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
JMB3
MB2
JMB3
10/03/23 16:26
10/05/23 02:54
10/03/23 16:26
10/05/23 02:54
QC
16.7
24.1
18.0
17.9
19.0
26.9
26.3
26.6
254
77.6
29.1
12.7
24.7
25.4
21.6
NOM Sample
ND
ND
ND
ND
ND
11.3
ND
0.275
2.55
ND
ND
ND
ND
ND
ND
Range
(40%-152%)
(61%-142%)
(26%-138%)
(38%-148%)
(26%-139%)
(40%-144%)
(38%-133%)
(40%-155%)
(45%-160%)
(50%-150%)
(61%-141%)
(43%-156%)
(50%-148%)
(43%-160%)
(45%-163%)
Qual
X
X
X
X
X
X
X
X
REC%
106
147
110
110
116
95
161
161
1540
475
178
78
151
155
132
15.7
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
638295Workorder:
*
*
*
*
*
*
*
U
UX
U
U
U
UX
JX
X
UX
UX
U
U
UX
UX
RPD%
Page 40 of 63
Page 70 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
MB2
JMB3
MB2
10/05/23 02:54
10/03/23 16:26
10/05/23 02:54
10/03/23 16:26
QC
12.7
10.5
16.6
14.6
2.43
23.5
16.7
24.7
15.7
20.8
12.6
16.8
21.9
17.2
21.4
NOM Sample
ND
0.777
ND
1.12
ND
ND
1.93
6.79
ND
2.21
ND
ND
ND
ND
4.37
Range
(40%-162%)
(38%-165%)
(31%-150%)
(50%-150%)
(40%-182%)
(19%-167%)
(52%-147%)
(57%-149%)
(45%-136%)
(44%-143%)
(47%-138%)
(45%-142%)
(50%-150%)
(56%-149%)
(51%-149%)
Qual
X
X
X
X
X
REC%
78
59
102
82
15
144
102
110
100
114
80
100
134
108
104
16.3
16.3
16.3
16.3
16.3
16.3
14.4
16.3
15.8
16.3
15.8
16.3
16.3
15.5
16.3
638295Workorder:
*
UX
X
U
X
UX
U
U
U
U
UX
U
RPD%
Page 41 of 63
Page 71 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
JMB3
MB2
10/04/23 11:47
10/03/23 16:26
10/04/23 11:47
10/03/23 16:26
10/05/23 02:54
10/03/23 16:26
QC
11.2
17.4
26.2
17.9
17.9
8.03
18.2
35.0
31.0
16.3
25.8
ND
17.4
21.1
20.6
NOM Sample
ND
3.78
9.21
ND
1.87
ND
ND
16.4
15.9
0.846
8.95
ND
ND
ND
0.725
Range
(32%-151%)
(50%-148%)
(50%-150%)
(48%-138%)
(54%-146%)
(18%-140%)
(49%-143%)
(42%-150%)
(50%-151%)
(55%-151%)
(51%-146%)
(32%-155%)
(41%-148%)
(41%-142%)
(44%-141%)
Qual
J
J
UX
REC%
69
92
104
114
98
49
109
114
92
100
103
0
106
129
122
16.3
14.9
16.3
15.7
16.3
16.3
16.3
16.3
16.3
15.3
16.3
16.3
16.3
16.3
16.3
638295Workorder:
*
U
U
U
U
J
UX
U
U
J
RPD%
Page 42 of 63
Page 72 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
MB2
JMB3
MB2
JMB3
MB2
JMB3
10/05/23 02:54
10/05/23 03:10
10/03/23 16:35
10/05/23 03:10
10/03/23 16:35
10/05/23 03:10
10/03/23 16:35
10/05/23 03:10
QC
87.2
25.9
14.1
20.6
15.9
17.3
17.1
14.9
21.4
16.1
17.2
15.7
16.2
23.8
NOM Sample
ND
ND
ND
0.520
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(45%-164%)
(0%-30%)
(0%-36%)
(0%-28%)
(0%-34%)
(0%-39%)
(0%-40%)
(0%-28%)
(0%-31%)
(0%-33%)
(0%-39%)
(0%-40%)
(0%-44%)
(0%-29%)
Qual
X
X
X
X
X
QC1205534488 638421009
1
2
2
2
2
6
4
2
1
11
22
3
1
REC%
532
159
92
123
97
106
105
91
131
106
113
101
102
145
16.3
16.3
15.4
16.3
16.3
16.3
16.3
16.3
16.3
15.2
15.3
15.5
15.7
16.3
MSD
638295Workorder:
*
*
*
UX
UX
U
UX
U
U
U
UX
U
U
U
U
UX
RPD%
Page 43 of 63
Page 73 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
JMB3
10/03/23 16:35
10/05/23 03:10
QC
17.7
17.6
18.5
24.7
24.8
26.9
232
70.2
27.1
9.41
25.5
18.8
21.5
13.7
9.64
NOM Sample
ND
ND
ND
11.3
ND
0.275
2.55
ND
ND
ND
ND
ND
ND
ND
0.777
Range
(0%-42%)
(0%-36%)
(0%-40%)
(0%-36%)
(0%-33%)
(0%-26%)
(0%-32%)
(0%-34%)
(0%-30%)
(0%-33%)
(0%-28%)
(0%-44%)
(0%-38%)
(0%-41%)
(0%-31%)
Qual
X
X
X
X
X
X
X
X
X
2
2
2
8
6
1
9
10
7
30
3
30
1
7
8
REC%
108
108
114
82
152
163
1410
430
166
58
156
115
132
84
54
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
638295Workorder:
*
*
*
*
*
*
U
U
U
UX
JX
X
UX
UX
U
U
UX
UX
UX
X
RPD%
Page 44 of 63
Page 74 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
MB2
JMB3
MB2
10/05/23 03:10
10/03/23 16:35
10/05/23 03:10
10/03/23 16:35
10/04/23 11:56
10/03/23 16:35
QC
16.8
13.3
2.38
22.3
15.5
26.2
14.9
19.3
14.2
16.9
20.7
16.9
20.5
11.2
16.8
NOM Sample
ND
1.12
ND
ND
1.93
6.79
ND
2.21
ND
ND
ND
ND
4.37
ND
3.78
Range
(0%-46%)
(0%-30%)
(0%-41%)
(0%-35%)
(0%-27%)
(0%-23%)
(0%-36%)
(0%-35%)
(0%-35%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-26%)
(0%-33%)
(0%-31%)
Qual
X
X
X
J
1
9
2
5
7
6
5
8
12
1
5
2
4
1
4
REC%
103
74
15
137
94
119
95
105
90
101
127
106
99
68
87
16.3
16.3
16.3
16.3
14.4
16.3
15.8
16.3
15.8
16.3
16.3
15.5
16.3
16.3
14.9
638295Workorder:
*
U
X
UX
U
U
U
U
UX
U
U
RPD%
Page 45 of 63
Page 75 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2501964Batch
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
MB2
JMB3
MB2
JMB3
10/03/23 16:35
10/04/23 11:56
10/03/23 16:35
10/05/23 03:10
10/03/23 16:35
10/05/23 03:10
QC
26.9
16.8
17.7
9.39
17.7
33.3
30.0
14.2
23.2
ND
16.4
18.5
16.8
85.0
NOM Sample
9.21
ND
1.87
ND
ND
16.4
15.9
0.846
8.95
ND
ND
ND
0.725
ND
Range
(0%-26%)
(0%-35%)
(0%-30%)
(0%-44%)
(0%-28%)
(0%-31%)
(0%-28%)
(0%-31%)
(0%-24%)
(0%-34%)
(0%-32%)
(0%-35%)
(0%-34%)
(0%-35%)
Qual
J
UX
X
2
7
1
16
3
5
3
14
11
N/A
6
13
20
2
REC%
108
107
97
58
106
104
87
87
87
0
100
113
99
518
16.3
15.7
16.3
16.3
16.3
16.3
16.3
15.3
16.3
16.3
16.3
16.3
16.3
16.3
638295Workorder:
*
*
U
U
U
J
UX
U
U
J
UX
RPD%
Page 46 of 63
Page 76 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/10/23 19:35
10/09/23 16:04
10/10/23 19:35
10/09/23 16:04
10/10/23 19:35
10/09/23 16:04
10/10/23 19:35
10/09/23 16:04
QC
23.2
17.0
23.8
23.1
21.7
22.6
20.3
23.1
17.5
18.8
16.8
20.6
22.8
20.9
22.2
NOM Sample Range
(60%-158%)
(59%-144%)
(67%-144%)
(58%-144%)
(54%-128%)
(52%-141%)
(67%-154%)
(73%-141%)
(68%-135%)
(56%-151%)
(60%-153%)
(60%-141%)
(61%-148%)
(23%-155%)
(57%-139%)
Qual
X
X
X
X
QC1205539361
REC%
110
86
113
110
103
108
97
110
89
96
84
102
108
99
105
21.0
19.8
21.0
21.0
21.0
21.0
21.0
21.0
19.6
19.7
20.0
20.2
21.0
21.0
21.0
LCS
638295Workorder:
RPD%
Page 47 of 63
Page 77 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/09/23 16:04
10/10/23 19:35
QC
21.7
21.3
20.8
21.3
19.5
23.9
22.7
18.8
23.9
16.6
21.6
34.1
18.7
24.5
21.5
NOM Sample Range
(20%-154%)
(59%-145%)
(35%-138%)
(63%-143%)
(5%-158%)
(5%-149%)
(59%-145%)
(48%-149%)
(52%-148%)
(58%-147%)
(60%-151%)
(62%-148%)
(60%-144%)
(58%-142%)
(50%-150%)
Qual
X
X
X
X
X
X
X
X
X
X
REC%
103
101
99
101
93
114
108
89
114
79
103
162
89
116
102
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
638295Workorder:
*
RPD%
Page 48 of 63
Page 78 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/10/23 19:35
10/09/23 16:04
10/10/23 19:35
10/09/23 16:04
QC
23.1
20.4
16.1
18.9
17.6
19.7
16.4
20.9
21.9
20.7
22.6
20.9
16.1
20.0
18.8
NOM Sample Range
(52%-144%)
(60%-149%)
(70%-144%)
(73%-151%)
(58%-134%)
(65%-145%)
(57%-134%)
(65%-137%)
(20%-160%)
(68%-138%)
(71%-133%)
(69%-144%)
(67%-145%)
(70%-138%)
(64%-133%)
Qual
X
X
REC%
110
97
86
90
87
94
80
99
104
104
107
99
84
95
93
21.0
21.0
18.6
21.0
20.3
21.0
20.4
21.0
21.0
20.0
21.0
21.0
19.2
21.0
20.2
638295Workorder:
RPD%
Page 49 of 63
Page 79 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/09/23 16:04
10/10/23 19:35
10/09/23 16:04
10/10/23 19:35
10/10/23 19:19
10/09/23 15:56
10/10/23 19:19
QC
20.6
11.9
19.3
20.0
21.3
18.8
19.9
24.3
20.0
21.1
19.2
20.4
ND
ND
ND
NOM Sample Range
(69%-133%)
(35%-165%)
(64%-134%)
(65%-145%)
(66%-139%)
(67%-136%)
(72%-143%)
(49%-153%)
(66%-138%)
(58%-140%)
(63%-135%)
(5%-158%)
Qual
X
X
UX
U
U
QC1205539360
REC%
98
57
92
95
101
95
95
116
95
100
91
97
21.0
21.0
21.0
21.0
21.0
19.8
21.0
21.0
21.0
21.0
21.0
21.0
MB
638295Workorder:
RPD%
Page 50 of 63
Page 80 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/10/23 19:19
10/09/23 15:56
10/10/23 19:19
10/09/23 15:56
10/10/23 19:19
10/09/23 15:56
10/10/23 19:19
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
UX
U
U
U
UX
U
U
U
U
UX
U
U
U
U
UX
REC%
638295Workorder:
RPD%
Page 51 of 63
Page 81 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/10/23 19:19
10/09/23 15:56
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
UX
UX
U
U
REC%
638295Workorder:
RPD%
Page 52 of 63
Page 82 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/09/23 15:56
10/10/23 19:19
10/09/23 15:56
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
U
U
U
UX
U
U
U
U
U
U
U
U
U
REC%
638295Workorder:
RPD%
Page 53 of 63
Page 83 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/09/23 15:56
10/10/23 19:19
10/09/23 15:56
10/10/23 19:19
10/10/23 17:56
10/09/23 16:30
10/10/23 17:56
10/09/23 16:30
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
25.5
14.2
21.8
15.6
18.9
18.7
NOM Sample
ND
ND
0.611
ND
ND
ND
Range
(50%-145%)
(42%-138%)
(51%-159%)
(50%-148%)
(44%-127%)
(39%-138%)
Qual
U
U
U
U
UX
U
U
U
UX
hX
h
h
Xh
h
h
QC1205539362 638421009
REC%
157
93
131
95
116
115
16.3
15.3
16.3
16.3
16.3
16.3
MS
638295Workorder:
*hUX
Uh
h
UXh
Uh
Uh
RPD%
Page 54 of 63
Page 84 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/09/23 16:30
10/10/23 17:56
10/09/23 16:30
10/10/23 10:14
10/09/23 18:47
10/09/23 16:30
10/10/23 17:56
10/09/23 16:30
10/10/23 17:56
QC
16.8
21.8
15.9
ND
23.9
14.1
26.3
16.8
17.2
20.2
25.7
28.9
29.4
166
77.8
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
11.8
ND
0.301
5.04
ND
Range
(62%-132%)
(58%-157%)
(54%-139%)
(53%-151%)
(50%-154%)
(40%-152%)
(61%-142%)
(26%-138%)
(38%-148%)
(26%-139%)
(40%-144%)
(38%-133%)
(40%-155%)
(45%-160%)
(50%-150%)
Qual
h
hX
h
Uh
hJ
h
hX
h
h
h
h
hX
hX
hX
hX
REC%
104
134
105
0
154
91
162
103
106
124
85
178
179
987
478
16.3
16.3
15.2
15.2
15.5
15.6
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
638295Workorder:
*
*
*
*
*
*
hU
hUX
Uh
Uh
hU
Uh
hUX
Uh
Uh
Uh
h
hUX
hJX
hX
hUX
RPD%
Page 55 of 63
Page 85 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/10/23 17:56
10/09/23 16:30
10/09/23 18:47
10/09/23 16:30
QC
28.6
8.84
25.6
18.0
21.5
18.0
12.1
17.4
12.7
2.52
17.1
15.3
38.9
13.8
19.5
NOM Sample
ND
ND
ND
0.384
ND
0.657
0.914
ND
1.15
ND
ND
2.43
10.9
ND
2.33
Range
(61%-141%)
(43%-156%)
(50%-148%)
(43%-160%)
(45%-163%)
(40%-162%)
(38%-165%)
(31%-150%)
(50%-150%)
(40%-182%)
(19%-167%)
(52%-147%)
(57%-149%)
(45%-136%)
(44%-143%)
Qual
hX
h
h
Xh
hX
hX
hX
h
Xh
hX
h
h
h
h
h
REC%
176
54
157
108
132
107
69
107
71
16
105
90
172
88
106
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
16.3
14.4
16.3
15.7
16.3
638295Workorder:
*
*
*
*
hUX
hU
hU
JXh
hXU
hX
hX
hU
Xh
hXU
hU
h
h
Uh
h
RPD%
Page 56 of 63
Page 86 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/09/23 16:30
10/10/23 17:56
10/09/23 16:30
10/09/23 18:47
10/09/23 16:30
10/09/23 18:47
10/09/23 16:30
QC
10.9
16.7
22.4
17.8
21.5
15.1
18.6
21.9
14.1
18.3
9.81
19.1
34.7
31.3
14.7
NOM Sample
ND
ND
ND
ND
5.20
ND
3.36
9.52
ND
1.91
ND
ND
19.2
15.5
0.718
Range
(47%-138%)
(45%-142%)
(50%-150%)
(56%-149%)
(51%-149%)
(32%-151%)
(50%-148%)
(50%-150%)
(48%-138%)
(54%-146%)
(18%-140%)
(49%-143%)
(42%-150%)
(50%-151%)
(55%-151%)
Qual
h
h
hX
h
h
hJ
h
h
h
h
hJ
h
h
h
h
REC%
69
103
137
112
100
93
103
76
90
101
60
114
95
97
91
15.7
16.3
16.3
15.5
16.3
16.3
14.8
16.3
15.6
16.3
16.3
16.3
16.3
16.3
15.3
638295Workorder:
Uh
Uh
hUX
Uh
h
hU
h
h
Uh
h
hU
Uh
h
h
hJ
RPD%
Page 57 of 63
Page 87 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/09/23 16:30
10/10/23 17:56
10/09/23 16:30
10/10/23 17:56
10/10/23 18:12
10/09/23 16:39
10/10/23 18:12
10/09/23 16:39
10/10/23 18:12
10/09/23 16:39
QC
26.5
ND
17.2
20.7
17.0
73.4
23.3
14.9
22.9
15.3
19.1
19.2
17.6
20.9
17.4
NOM Sample
9.38
ND
ND
ND
0.572
ND
ND
ND
0.611
ND
ND
ND
ND
ND
ND
Range
(51%-146%)
(32%-155%)
(41%-148%)
(41%-142%)
(44%-141%)
(45%-164%)
(0%-30%)
(0%-36%)
(0%-28%)
(0%-34%)
(0%-39%)
(0%-40%)
(0%-28%)
(0%-31%)
(0%-33%)
Qual
h
hUX
h
h
h
hX
hX
h
h
Xh
h
h
h
hX
h
QC1205539363 638421009
9
5
5
2
1
2
4
4
9
REC%
105
0
106
127
101
451
144
98
138
94
118
118
108
129
115
16.3
16.3
16.3
16.3
16.3
16.3
16.2
15.3
16.2
16.2
16.2
16.2
16.2
16.2
15.1
MSD
638295Workorder:
*
*
h
hUX
hU
hU
hJ
hUX
hUX
Uh
h
UXh
Uh
Uh
hU
hUX
Uh
RPD%
Page 58 of 63
Page 88 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/10/23 10:23
10/09/23 18:56
10/09/23 16:39
10/10/23 18:12
10/09/23 16:39
10/10/23 18:12
QC
ND
38.0
17.8
29.0
17.6
17.5
18.7
27.7
28.8
31.5
252
81.2
31.1
12.1
26.7
NOM Sample
ND
ND
ND
ND
ND
ND
ND
11.8
ND
0.301
5.04
ND
ND
ND
ND
Range
(0%-39%)
(0%-40%)
(0%-44%)
(0%-29%)
(0%-42%)
(0%-36%)
(0%-40%)
(0%-36%)
(0%-33%)
(0%-26%)
(0%-32%)
(0%-34%)
(0%-30%)
(0%-33%)
(0%-28%)
Qual
hU
Jh
h
hX
h
h
h
h
hX
hX
hX
hX
hX
h
h
N/A
46
23
10
5
2
8
8
0
7
41
4
8
31
4
REC%
0
246
114
179
108
108
115
98
178
193
1530
501
192
75
165
15.2
15.4
15.6
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
638295Workorder:
*
*
*
*
*
*
*
*
*
Uh
hU
Uh
hUX
Uh
Uh
Uh
h
hUX
hJX
hX
hUX
hUX
hU
hU
*
*
RPD%
Page 59 of 63
Page 89 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/10/23 18:12
10/09/23 16:39
10/09/23 18:56
10/09/23 16:39
10/10/23 18:12
QC
22.0
23.7
8.57
6.88
16.8
13.4
2.44
20.8
16.4
31.4
15.7
19.5
11.7
16.6
23.3
NOM Sample
0.384
ND
0.657
0.914
ND
1.15
ND
ND
2.43
10.9
ND
2.33
ND
ND
ND
Range
(0%-44%)
(0%-38%)
(0%-41%)
(0%-31%)
(0%-46%)
(0%-30%)
(0%-41%)
(0%-35%)
(0%-27%)
(0%-23%)
(0%-36%)
(0%-35%)
(0%-35%)
(0%-30%)
(0%-30%)
Qual
hX
hX
hX
hX
h
Xh
hX
h
h
h
h
h
h
h
hX
20
10
71
55
4
5
4
20
7
22
12
0
7
1
4
REC%
133
146
49
37
103
76
15
129
97
126
100
106
75
102
144
16.2
16.2
16.2
16.2
16.2
16.2
16.2
16.2
14.3
16.2
15.6
16.2
15.7
16.2
16.2
638295Workorder:
*
*
JXh
hXU
hX
hX
hU
Xh
hXU
hU
h
h
Uh
h
Uh
Uh
hUX
*
*
RPD%
Page 60 of 63
Page 90 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/09/23 16:39
10/09/23 18:56
10/09/23 16:39
10/09/23 18:56
10/09/23 16:39
10/10/23 18:12
10/09/23 16:39
QC
19.3
20.3
13.9
17.1
22.4
17.2
17.6
8.60
19.4
35.9
32.9
15.4
26.2
ND
17.5
NOM Sample
ND
5.20
ND
3.36
9.52
ND
1.91
ND
ND
19.2
15.5
0.718
9.38
ND
ND
Range
(0%-30%)
(0%-26%)
(0%-33%)
(0%-31%)
(0%-26%)
(0%-35%)
(0%-30%)
(0%-44%)
(0%-28%)
(0%-31%)
(0%-28%)
(0%-31%)
(0%-24%)
(0%-34%)
(0%-32%)
Qual
h
h
Jh
h
h
h
h
hJ
h
h
h
h
h
hUX
h
8
6
8
8
2
20
4
13
2
3
5
5
1
N/A
2
REC%
122
93
86
93
80
111
97
53
116
103
107
97
104
0
108
15.4
16.2
16.2
14.8
16.2
15.6
16.2
16.2
16.2
16.2
16.2
15.2
16.2
16.2
16.2
638295Workorder:
*
Uh
h
hU
h
h
Uh
h
hU
Uh
h
h
hJ
h
hUX
hU
RPD%
Page 61 of 63
Page 91 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2504794Batch
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
Parmname Units
ng/L
ng/L
ng/L
Anlst Date Time
JMB3 10/09/23 16:39
10/10/23 18:12
QC
22.5
18.0
80.6
NOM Sample
ND
0.572
ND
Range
(0%-35%)
(0%-34%)
(0%-35%)
Qual
h
h
hX
The Qualifiers in this report are defined as follows:
8
6
9
REC%
139
107
497
16.2
16.2
16.2
638295Workorder:
*
U
J
P
C
B
E
A
X
N
H
**
<
>
h
R
^
D
N/A
ND
NJ
JNX
UJ
Q
N1
Y
Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
Value is estimated
Organics--The concentrations between the primary and confirmation columns/detectors is >40% different. For HPLC, the difference is >70%.
Analyte has been confirmed by GC/MS analysis
The target analyte was detected in the associated blank.
Concentration of the target analyte exceeds the instrument calibration range
The TIC is a suspected aldol-condensation product
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Organics--Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based
on nearest internal standard response factor
Analytical holding time was exceeded
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
Preparation or preservation holding time was exceeded
Sample results are rejected
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
Results are reported from a diluted aliquot of the sample
RPD or %Recovery limits do not apply.
Analyte concentration is not detected above the detection limit
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Non Calibrated Compound
Compound cannot be extracted
One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
See case narrative
QC Samples were not spiked with this compound
hU
hJ
hUX
RPD%
Notes:
Page 62 of 63
Page 92 of 105 SDG: 638295
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Parmname
Page 63 of 63
Units Anlst Date TimeQCNOMSampleRangeQualREC%
638295Workorder:
N
J
Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based on nearest
internal standard response factor
See case narrative for an explanation
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
RPD%
Page 93 of 105 SDG: 638295
LCMSMS-PFC
Technical Case Narrative
NC Dept Environmental Quality
SDG #: 638295

Product: The Extraction and Analysis of Per- and Polyfluoroalkyl Substances Using LCMSMS
Analytical Method: EPA 537.1 Modified
Analytical Procedure: GL-OA-E-076 REV# 14
Analytical Batches: 2499992 and 2499991
The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification
638295001 PZ-21-FB
638295006 PZ-4-FB
638295007 RW-5-FB
1205530788 Method Blank (MB)
1205530789 Laboratory Control Sample (LCS)
1205530790 637450004(NonSDG) Matrix Spike (MS)
1205530791 637450004(NonSDG) Matrix Spike Duplicate (MSD)

The samples in this SDG were analyzed on an "as received" basis.
Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.

Calibration Information

CCV Requirements
Calibration verification standards (ICV or CCV) requirements have not been met for samples 1205530788 (MB),
1205530789 (LCS), 1205530790 (Non SDG 637450004MS), 1205530791 (Non SDG 637450004MSD) and All
in this batch in this SDG. One or more target analytes failed acceptance criteria with a positive bias in the
standards bracketing the samples in this SDG. These target analytes were not detected in the associated
environmental samples; therefore, the non-compliance had no adverse effect on the data.

Quality Control (QC) Information

Laboratory Control Sample Duplicate (LCSD)
An LCSD was used in place of matrix QC due to limited sample volume.

Matrix Spike (MS) Recovery Statement
The MS or MSD (See Below) recovered spiked analytes outside of the established acceptance limits. As similar
recoveries were displayed in the MS and MSD, the failures were attributed to sample matrix interference and the
data were reported.
Sample Analyte Value
1205530790 (Non SDG 637450004MS)R-EVE 191* (45%-164%)
1205530791 (Non SDG 637450004MSD)R-EVE 173* (45%-164%)
Page 94 of 105 SDG: 638295

Technical Information

Sample Dilutions
Samples 1205530790 (Non SDG 637450004MS) and 1205530791 (Non SDG 637450004MSD) were extracted
at reduced volumes due to sample matrix and the potential for clogging the SPE column.

Miscellaneous Information

Additional Comments
Some analytes are X qualified because the standards used to make the initial calibration curve did not meet the
ISO 17025 criterion. These are the only standards available for these analytes.

Product: The Extraction and Analysis of Per- and Polyfluoroalkyl Substances Using LCMSMS
Analytical Method: EPA 537.1 Modified
Analytical Procedure: GL-OA-E-076 REV# 14
Analytical Batches: 2501026 and 2501019
The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification
638295002 PZ-21
638295003 PZ-4
638295004 RW-1
1205532673 Method Blank (MB)
1205532674 Laboratory Control Sample (LCS)
1205532675 638295002(PZ-21) Matrix Spike (MS)
1205532676 638295002(PZ-21) Matrix Spike Duplicate (MSD)

The samples in this SDG were analyzed on an "as received" basis.
Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.

Quality Control (QC) Information

Matrix Spike (MS) Recovery Statement
The MS or MSD (See Below) recovered spiked analytes outside of the established acceptance limits. As similar
recoveries were displayed in the MS and MSD, the failures were attributed to sample matrix interference and the
data were reported.
Sample Analyte Value
1205532675
(PZ-21MS)Nafion Byproduct 1 (PFESA BP1)138*
(38%-133%)
Nafion Byproduct 4 (PFESA BP4)1580*
(45%-160%)
Nafion Byproduct 5 (PFESA BP5)474*
(50%-150%)
Perfluoro-2-methoxyacetic acid (PFMOAA)31* (40%-182%)
Page 95 of 105 SDG: 638295
Perfluoro-3-methoxypropanoic acid (PFMOPrA)193*
(19%-167%)
Perfluoropropanoic acid (PFPrA)24* (32%-155%)
R-EVE 762*
(45%-164%)
1205532676
(PZ-21MSD)
1, 1, 2, 2-Tetrafluoro-2-(1, 2, 2, 2-tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
155*
(50%-145%)
Fluorotelomer sulfonic acid 6:2 (6:2 FTS)169*
(50%-154%)
Nafion Byproduct 1 (PFESA BP1)145*
(38%-133%)
Nafion Byproduct 4 (PFESA BP4)1720*
(45%-160%)
Nafion Byproduct 5 (PFESA BP5)504*
(50%-150%)
Nafion Byproduct 6 (PFESA BP6)151*
(61%-141%)
Perfluoro(2-ethoxyethane)sulfonic acid (PFEESA or PES)152*
(50%-148%)
Perfluoro-2-methoxyacetic acid (PFMOAA)34* (40%-182%)
Perfluoro-3-methoxypropanoic acid (PFMOPrA)211*
(19%-167%)
Perfluoropropanoic acid (PFPrA)25* (32%-155%)
R-EVE 805*
(45%-164%)

MS/MSD Relative Percent Difference (RPD) Statement
The RPD values between the MS and MSD (See Below) were not within the acceptance limits. Since all other
RPD values met acceptance criteria, the noted exceptions are attributed to vagaries in the extraction process. The
data are reported.
Sample Analyte Value
1205532675MS and 1205532676MSD
(PZ-21)
Perfluoro(3, 5, 7-trioxaoctanoic) acid
(PFO3OA)
RPD 42*
(0%-41%)

Internal Standard (ISTD) Acceptance
Samples 1205532675 (PZ-21MS), 1205532676 (PZ-21MSD), 638295002 (PZ-21) and 638295004 (RW-1) did
not meet acceptance criteria for one or more internal standards. The samples were diluted in order to bring
internal standards within acceptance criteria. The results for these samples were reported from the undiluted and
diluted analyses.

Technical Information

Sample Dilutions
The following samples and/or QC were diluted due to the Internal Standard Recovery not within the limits in the
undiluted analysis. 1205532675 (PZ-21MS), 1205532676 (PZ-21MSD), 638295002 (PZ-21) and 638295004
Page 96 of 105 SDG: 638295
(RW-1).
Analyte
638295
002 004
Fluorotelomer sulfonic acid 4:2 (4:2 FTS)25X 25X
Fluorotelomer sulfonic acid 6:2 (6:2 FTS)5X 25X
Fluorotelomer sulfonic acid 8:2 (8:2 FTS)1X 5X
Perfluorohexadecanoic acid (PFHxDA)1X 5X
Perfluorooctadecanoic acid (PFODA)1X 5X

Miscellaneous Information

Additional Comments
Some analytes are X qualified because the standards used to make the initial calibration curve did not meet the
ISO 17025 criterion. These are the only standards available for these analytes.

Product: The Extraction and Analysis of Per- and Polyfluoroalkyl Substances Using LCMSMS
Analytical Method: EPA 537.1 Modified
Analytical Procedure: GL-OA-E-076 REV# 14
Analytical Batches: 2501964 and 2501960
The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification
638295005 RW-5
1205534485 Method Blank (MB)
1205534486 Laboratory Control Sample (LCS)
1205534487 638421009(NonSDG) Matrix Spike (MS)
1205534488 638421009(NonSDG) Matrix Spike Duplicate (MSD)

The samples in this SDG were analyzed on an "as received" basis.
Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.

Calibration Information

CCV Requirements
Calibration verification standards (ICV or CCV) requirements have not been met for samples in this batch in this
SDG. One or more target analytes failed acceptance criteria with a positive bias in the standards bracketing the
samples in this SDG. These target analytes were not detected in the associated environmental samples; therefore,
the non-compliance had no adverse effect on the data.

Quality Control (QC) Information

Laboratory Control Sample (LCS) Recovery
The LCS and/or LCSD (See Below) did not meet the spike recovery acceptance limits with a positive bias. As
target analytes were not detected in the associated samples, the data were not adversely impacted.
Page 97 of 105 SDG: 638295
Sample Analyte Value
1205534486 (LCS)Perfluoro(3, 5, 7-trioxaoctanoic) acid (PFO3OA)189* (62%-148%)

LCS (See Below) exceeded spike recovery limits for PFO2HxA. This analyte was not detected in the client
samples with the exception of 638295005, 638421007, 638421009, 638421010, 638421011. The extraction hold
dates have passed. The data were reported as is.
Sample Analyte Value
1205534486 (LCS)Perfluoro(3, 5-dioxahexanoic) acid (PFO2HxA)183* (60%-144%)

Matrix Spike (MS) Recovery Statement
The MS or MSD (See Below) recovered spiked analytes outside of the established acceptance limits. As similar
recoveries were displayed in the MS and MSD, the failures were attributed to sample matrix interference and the
data were reported.
Sample Analyte Value
1205534487 (Non SDG
638421009MS)
1, 1, 2, 2-Tetrafluoro-2-(1, 2, 2, 2-tetrafluoroethoxy)ethane
sulfonic acid (NVHOS)
160*
(50%-145%)
Hydro-EVE 147*
(61%-142%)
Nafion Byproduct 1 (PFESA BP1)161*
(38%-133%)
Nafion Byproduct 2 (PFESA BP2)161*
(40%-155%)
Nafion Byproduct 4 (PFESA BP4)1540*
(45%-160%)
Nafion Byproduct 5 (PFESA BP5)475*
(50%-150%)
Nafion Byproduct 6 (PFESA BP6)178*
(61%-141%)
Perfluoro(2-ethoxyethane)sulfonic acid (PFEESA or PES)151*
(50%-148%)
Perfluoro-2-methoxyacetic acid (PFMOAA)15*
(40%-182%)
Perfluoropropanoic acid (PFPrA)12*
(32%-155%)
R-EVE 532*
(45%-164%)
1205534488 (Non SDG
638421009MSD)
1, 1, 2, 2-Tetrafluoro-2-(1, 2, 2, 2-tetrafluoroethoxy)ethane
sulfonic acid (NVHOS)
159*
(50%-145%)
Hydro-EVE 145*
(61%-142%)
Nafion Byproduct 1 (PFESA BP1)152*
(38%-133%)
Page 98 of 105 SDG: 638295
Nafion Byproduct 2 (PFESA BP2)163*
(40%-155%)
Nafion Byproduct 4 (PFESA BP4)1410*
(45%-160%)
Nafion Byproduct 5 (PFESA BP5)430*
(50%-150%)
Nafion Byproduct 6 (PFESA BP6)166*
(61%-141%)
Perfluoro(2-ethoxyethane)sulfonic acid (PFEESA or PES)156*
(50%-148%)
Perfluoro-2-methoxyacetic acid (PFMOAA)15*
(40%-182%)
Perfluoropropanoic acid (PFPrA)11*
(32%-155%)
R-EVE 518*
(45%-164%)

Technical Information

Sample Re-extraction/Re-analysis
Samples 638295005 (RW-5) were scheduled for re-extraction due to elevated recovery for PFO2HxA in the LCS
and positive detections in the samples. The client was notified the re-extractions would be performed out of
holding. Results for PFO2HxA will be reported from both sets of extractions.

Miscellaneous Information

Additional Comments
Some analytes are X qualified because the standards used to make the initial calibration curve did not meet the
ISO 17025 criterion. These are the only standards available for these analytes.

Product: The Extraction and Analysis of Per- and Polyfluoroalkyl Substances Using LCMSMS
Analytical Method: EPA 537.1 Modified
Analytical Procedure: GL-OA-E-076 REV# 14
Analytical Batches: 2504794 and 2504793
The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification
638295005 RW-5
1205539360 Method Blank (MB)
1205539361 Laboratory Control Sample (LCS)
1205539362 638421009(NonSDG) Matrix Spike (MS)
1205539363 638421009(NonSDG) Matrix Spike Duplicate (MSD)

The samples in this SDG were analyzed on an "as received" basis.
Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
Page 99 of 105 SDG: 638295
applicable, with the following exceptions.

Quality Control (QC) Information

Laboratory Control Sample (LCS) Recovery
The LCS and/or LCSD (See Below) did not meet the spike recovery acceptance limits with a positive bias. As
target analytes were not detected in the associated samples, the data were not adversely impacted.
Sample Analyte Value
1205539361 (LCS)Perfluoro(3, 5, 7-trioxaoctanoic) acid (PFO3OA)162* (62%-148%)

Matrix Spike (MS) Recovery Statement
The MS or MSD (See Below) recovered spiked analytes outside of the established acceptance limits. As similar
recoveries were displayed in the MS and MSD, the failures were attributed to sample matrix interference and the
data were reported.
Sample Analyte Value
1205539362 (Non SDG
638421009MS)
1, 1, 2, 2-Tetrafluoro-2-(1, 2, 2, 2-tetrafluoroethoxy)ethane
sulfonic acid (NVHOS)
157*
(50%-145%)
Hydro-EVE 162*
(61%-142%)
Nafion Byproduct 1 (PFESA BP1)178*
(38%-133%)
Nafion Byproduct 2 (PFESA BP2)179*
(40%-155%)
Nafion Byproduct 4 (PFESA BP4)987*
(45%-160%)
Nafion Byproduct 5 (PFESA BP5)478*
(50%-150%)
Nafion Byproduct 6 (PFESA BP6)176*
(61%-141%)
Perfluoro(2-ethoxyethane)sulfonic acid (PFEESA or PES)157*
(50%-148%)
Perfluoro-2-methoxyacetic acid (PFMOAA)16*
(40%-182%)
Perfluorobutanoic acid (PFBA)172*
(57%-149%)
Perfluoropropanoic acid (PFPrA)10*
(32%-155%)
R-EVE 451*
(45%-164%)
1205539363 (Non SDG
638421009MSD)Fluorotelomer sulfonic acid 6:2 (6:2 FTS)246*
(50%-154%)
Hydro-EVE 179*
(61%-142%)
Page 100 of 105 SDG: 638295
Nafion Byproduct 1 (PFESA BP1)178*
(38%-133%)
Nafion Byproduct 2 (PFESA BP2)193*
(40%-155%)
Nafion Byproduct 4 (PFESA BP4)1530*
(45%-160%)
Nafion Byproduct 5 (PFESA BP5)501*
(50%-150%)
Nafion Byproduct 6 (PFESA BP6)192*
(61%-141%)
Perfluoro(2-ethoxyethane)sulfonic acid (PFEESA or PES)165*
(50%-148%)
Perfluoro(3, 5-dioxahexanoic) acid (PFO2HxA)37*
(38%-165%)
Perfluoro-2-methoxyacetic acid (PFMOAA)15*
(40%-182%)
Perfluoropropanoic acid (PFPrA)9* (32%-155%)
R-EVE 497*
(45%-164%)

MS/MSD Relative Percent Difference (RPD) Statement
The RPD values between the MS and MSD (See Below) were not within the acceptance limits. Since all other
RPD values met acceptance criteria, the noted exceptions are attributed to vagaries in the extraction process. The
data are reported.
Sample Analyte Value
1205539362MS and 1205539363MSD (Non SDG
638421009)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
RPD 46*
(0%-40%)
Nafion Byproduct 4 (PFESA BP4)RPD 41*
(0%-32%)
Perfluoro(3, 5, 7-trioxaoctanoic) acid
(PFO3OA)
RPD 71*
(0%-41%)
Perfluoro(3, 5-dioxahexanoic) acid
(PFO2HxA)
RPD 55*
(0%-31%)

Internal Standard (ISTD) Acceptance
Samples 1205539362 (Non SDG 638421009MS) and 1205539363 (Non SDG 638421009MSD) did not meet
acceptance criteria for one or more internal standards. The samples were diluted in order to bring internal
standards within acceptance criteria. The results for these samples were reported from the undiluted and diluted
analyses.

Technical Information

Holding Time Specifications
Samples (See Below) were re-extracted out of holding for PFO2HxA results. Results for PFO2HxA were
reported from both sets of extractions.
Page 101 of 105 SDG: 638295
Sample Analyte Value
1205539362 (Non SDG
638421009MS)
Received 21-SEP-23, within holding, prepped 06-OCT-23, out of
holding 04-OCT-23
1205539363 (Non SDG
638421009MSD)
Received 21-SEP-23, within holding, prepped 06-OCT-23, out of
holding 04-OCT-23
638295005 (RW-5)Received 22-SEP-23, within holding, prepped 06-OCT-23, out of
holding 04-OCT-23

Sample Dilutions
The following samples and/or QC were diluted due to the Internal Standard Recovery not within the limits in the
undiluted analysis. 1205539362 (Non SDG 638421009MS) and 1205539363 (Non SDG 638421009MSD).

Miscellaneous Information

Additional Comments
Some analytes are X qualified because the standards used to make the initial calibration curve did not meet the
ISO 17025 criterion. These are the only standards available for these analytes.

Certification Statement

Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 102 of 105 SDG: 638295
Page 103 of 105 SDG: 638295
Page 104 of 105 SDG: 638295
State Certification
Alabama
Alaska
Alaska Drinking Water
Arkansas
CLIA
California
Colorado
Connecticut
DoD ELAP/ ISO17025 A2LA
Florida NELAP
Foreign Soils Permit
Georgia
Georgia SDWA
Hawaii
Idaho
Illinois NELAP
Indiana
Kansas NELAP
Kentucky SDWA
Kentucky Wastewater
Louisiana Drinking Water
Louisiana NELAP
Maine
Maryland
Massachusetts
Massachusetts PFAS Approv
Michigan
Mississippi
Nebraska
Nevada
New Hampshire NELAP
New Jersey NELAP
New Mexico
New York NELAP
North Carolina
North Carolina SDWA
North Dakota
Oklahoma
Pennsylvania NELAP
Puerto Rico
S. Carolina Radiochem
Sanitation Districts of L
South Carolina Chemistry
Tennessee
Texas NELAP
Utah NELAP
Vermont
Virginia NELAP
Washington
42200
17-018
SC00012
88-00651
42D0904046
2940
SC00012
PH-0169
2567.01
E87156
P330-15-00283, P330-15-00253
SC00012
967
SC00012
SC00012
200029
C-SC-01
E-10332
KY90129
KY90129
LA024
03046 (AI33904)
2023019
270
M-SC012
Letter
9976
SC00012
NE-OS-26-13
SC000122024-04
2054
SC002
SC00012
11501
233
45709
R-158
2022-160
68-00485
SC00012
10120002
9255651
10120001
TN 02934
T104704235-23-21
SC000122022-37
VT87156
460202
C780
List of current GEL Certifications as of 11 October 2023
Page 105 of 105 SDG: 638295

October 05, 2023

Amy Delinsky
NC Dept Environmental Quality
1646 Mail Service Center
Raleigh, North Carolina 27699

Re: Routine Analysis
Work Order: 638302

Dear Amy Delinsky:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on September 22, 2023. This original data report has been prepared and reviewed in
accordance with GEL's standard operating procedures.

The samples were delivered with proper chain of custody documentation and signatures. All sample containers
arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample
receipt.
Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards,
with any exceptions noted. The results reported relate only to the items tested and to the sample as received by
the laboratory. These results may not be reproduced except as full reports without approval by the laboratory.
Copies of GEL's accreditations and certifications can be found on our website at www.gel.com.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 1614.

Sincerely,

PM_SIGN_HERE
Delaney Stone
Project Manager

Purchase Order: SIGNED QUOTE
Enclosures
Page 1 of 52 SDG: 638302
Olivia Olsen for
Reviewed by USER_SIGN_HERE
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis Report
NCDQ001 NC Dept Environmental Quality
Client SDG: 638302 GEL Work Order: 638302
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above
the limit as defined in the 'U' qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures. Please direct any questions to your Project Manager, Delaney Stone.
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound
J Value is estimated
U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
for
Page 2 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25007541644ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/01/23DK20.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
0.477
19.1
3.82
0.477
0.477
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302001
Surface Water
20-SEP-23 17:37
22-SEP-23
SW- Upstream NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
0.191
7.63
1.26
0.191
0.191
1UX
U
UX
UX
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
U
UX
UX
UX
UX
UX
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
Page 3 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25007541549
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/29/23JMB3
0.382
1.91
3.82
3.82
3.75
3.59
14.3
3.66
3.82
3.82
3.82
3.82
3.82
1.70
1.91
1.85
1.91
1.91
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302001
SW- Upstream NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.191
0.630
1.26
1.26
1.26
1.26
5.13
1.26
1.26
1.26
1.26
1.26
0.630
0.630
0.763
0.630
0.744
0.630
2
UX
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
Page 4 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
1.81
1.91
3.82
1.74
1.91
1.83
1.91
3.82
1.91
1.91
1.91
1.79
1.91
1.91
1.91
1.91
1.91
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302001
SW- Upstream NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.630
0.630
1.26
0.630
0.763
0.668
0.630
1.26
0.630
0.763
0.763
0.630
0.630
0.763
0.630
0.630
0.630
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
0.0191
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Liquid 09/29/23 25007520916RR4
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Notes:
Page 5 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302001
SW- Upstream NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 6 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25007541730ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/01/23DK20.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
0.432
17.3
3.46
0.432
0.432
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302002
Surface Water
20-SEP-23 13:05
22-SEP-23
SW- Downstream NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
0.173
6.92
1.14
0.173
0.173
1UX
U
UX
UX
UX
UX
UX
XU
UX
U
U
UX
UX
UX
UX
U
U
UX
UX
UX
UX
UX
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
Page 7 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
25007541623
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/29/23JMB3
0.346
1.73
3.46
3.46
3.40
3.25
13.0
3.32
3.46
3.46
3.46
3.46
3.46
1.54
1.73
1.68
1.73
1.73
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302002
SW- Downstream NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.173
0.571
1.14
1.14
1.14
1.14
4.65
1.14
1.14
1.14
1.14
1.14
0.571
0.571
0.692
0.571
0.674
0.571
2
UX
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
Page 8 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
1.64
1.73
3.46
1.57
1.73
1.66
1.73
3.46
1.73
1.73
1.73
1.63
1.73
1.73
1.73
1.73
1.73
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302002
SW- Downstream NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.571
0.571
1.14
0.571
0.692
0.605
0.571
1.14
0.571
0.692
0.692
0.571
0.571
0.692
0.571
0.571
0.571
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
0.0173
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Liquid 09/29/23 25007520916RR4
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Notes:
Page 9 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302002
SW- Downstream NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 10 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
24999921747ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
09/28/23JMB31.86
3.73
3.73
3.66
3.51
14.0
3.58
3.73
3.73
3.73
3.73
3.73
1.66
1.86
1.81
1.86
1.86
1.77
1.86
3.73
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302003
Water
20-SEP-23 13:10
22-SEP-23
SW- Downstream- FB NCDQ00117Project:
NCDQ001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
0.615
1.23
1.23
1.23
1.23
5.02
1.23
1.23
1.23
1.23
1.23
0.615
0.615
0.746
0.615
0.727
0.615
0.615
0.615
1.23
1U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorobutanesulfonic acid (PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
Page 11 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
24999922123
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
10/04/23JMB3
1.70
1.86
1.79
1.86
3.73
1.86
1.86
1.86
1.75
1.86
1.86
1.86
1.86
1.86
0.466
0.466
0.466
0.466
0.466
0.466
0.466
0.466
0.466
0.466
0.466
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302003
SW- Downstream- FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.615
0.746
0.653
0.615
1.23
0.615
0.746
0.746
0.615
0.615
0.746
0.615
0.615
0.615
0.186
0.186
0.186
0.186
0.186
0.186
0.186
0.186
0.186
0.186
0.186
2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UX
U
UX
UX
UX
UX
UX
UX
UX
U
U
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid (PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-heptafluoropropoxy)-
propanoic acid (Gen-X)
4-
(Heptafluoroisopropoxy)hexafluorob
utanoic acid (PFECA-G)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Hydro-EVE
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
Page 12 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
LCMSMS PFCs
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
0.466
0.466
0.466
0.466
0.466
0.466
0.466
18.6
3.73
0.466
0.466
0.373
1
1
1
1
1
1
1
1
1
1
1
1
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302003
SW- Downstream- FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:
0.186
0.186
0.186
0.186
0.186
0.186
0.186
7.46
1.23
0.186
0.186
0.186
UX
UX
UX
UX
U
U
UX
UX
UX
UX
UX
UX
acid (PFEESA or PES)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic) acid
(PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic acid
(PFMOPrA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoropropanoic acid (PFPrA)
R-EVE
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid (PFO5DA
or TAFN4)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
EPA 537Mod PFCs by LC-MS/MS "As Received"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
0.0186
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Liquid 09/28/23 24999910826EF
Method Description Analyst Date Time Prep Batch
The following Analytical Methods were performed:
1
2
Method Description
EPA 537.1 Modified
EPA 537.1 Modified
Analyst Comments
Notes:
Page 13 of 52 SDG: 638302
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 5, 2023
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDLPF
Amy DelinskyContact:
NC Dept Environmental QualityCompany :
1646 Mail Service Center
Raleigh, North Carolina 27699
Address :
Routine AnalysisProject:
638302003
SW- Downstream- FB NCDQ00117Project:
NCDQ001Client ID:Sample ID:
Client Sample ID:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 14 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
Parmname
Amy DelinskyContact:
NC Dept Environmental Quality
1646 Mail Service Center
Raleigh, North Carolina
October 5, 2023Report Date:
Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
DK2
JMB3
DK2
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
QC
19.2
19.5
21.8
19.7
19.4
20.3
20.3
20.0
20.8
19.3
17.4
15.6
20.0
NOM Sample Range
(60%-158%)
(59%-144%)
(67%-144%)
(58%-144%)
(54%-128%)
(52%-141%)
(67%-154%)
(73%-141%)
(68%-135%)
(56%-151%)
(60%-153%)
(60%-141%)
(61%-148%)
Qual
X
X
X
X
QC1205530789
REC%
93
100
106
96
94
99
99
97
108
100
89
79
97
20.6
19.4
20.6
20.6
20.6
20.6
20.6
20.6
19.2
19.3
19.6
19.8
20.6
LCS
638302Workorder:
RPD%
Page 1 of 32
Page 15 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
09/28/23 14:29
09/29/23 01:06
QC
20.8
22.6
20.0
21.9
16.0
17.3
21.4
21.9
19.0
18.7
19.4
20.3
20.6
23.1
22.4
NOM Sample Range
(23%-155%)
(57%-139%)
(20%-154%)
(59%-145%)
(35%-138%)
(63%-143%)
(5%-158%)
(5%-149%)
(59%-145%)
(48%-149%)
(52%-148%)
(58%-147%)
(60%-151%)
(62%-148%)
(60%-144%)
Qual
X
X
X
X
X
X
X
X
X
REC%
101
109
97
106
78
84
104
106
92
91
94
99
100
112
109
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
638302Workorder:
RPD%
Page 2 of 32
Page 16 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
09/28/23 14:29
QC
21.1
20.1
19.5
20.2
15.6
19.2
18.7
21.1
17.0
20.0
16.8
22.6
19.0
20.6
18.0
NOM Sample Range
(58%-142%)
(50%-150%)
(52%-144%)
(60%-149%)
(70%-144%)
(73%-151%)
(58%-134%)
(65%-145%)
(57%-134%)
(65%-137%)
(20%-160%)
(68%-138%)
(71%-133%)
(69%-144%)
(67%-145%)
Qual
X
X
X
REC%
103
97
95
98
85
93
94
102
85
97
81
115
92
100
96
20.6
20.6
20.6
20.6
18.2
20.6
19.9
20.6
19.9
20.6
20.6
19.6
20.6
20.6
18.8
638302Workorder:
RPD%
Page 3 of 32
Page 17 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
09/28/23 14:29
09/29/23 01:06
09/28/23 14:29
09/29/23 01:06
09/29/23 00:51
QC
20.5
18.3
20.5
10.7
20.1
21.6
20.2
19.9
19.7
18.5
19.6
21.2
20.0
29.4
ND
NOM Sample Range
(70%-138%)
(64%-133%)
(69%-133%)
(35%-165%)
(64%-134%)
(65%-145%)
(66%-139%)
(67%-136%)
(72%-143%)
(49%-153%)
(66%-138%)
(58%-140%)
(63%-135%)
(5%-158%)
Qual
JX
X
UX
QC1205530788
REC%
100
92
100
52
97
105
98
103
95
90
95
103
97
143
20.6
19.8
20.6
20.6
20.6
20.6
20.6
19.4
20.6
20.6
20.6
20.6
20.6
20.6
MB
638302Workorder:
RPD%
Page 4 of 32
Page 18 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
JMB3
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
UX
U
U
U
UX
U
U
U
U
UX
U
U
U
REC%
638302Workorder:
RPD%
Page 5 of 32
Page 19 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
09/28/23 14:21
09/29/23 00:51
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
UX
UX
REC%
638302Workorder:
RPD%
Page 6 of 32
Page 20 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
09/29/23 00:51
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
U
U
U
U
U
UX
U
U
U
U
U
U
U
REC%
638302Workorder:
RPD%
Page 7 of 32
Page 21 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
09/28/23 14:21
09/29/23 00:51
09/28/23 14:21
09/29/23 00:51
09/29/23 01:36
09/28/23 14:04
09/29/23 01:36
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
212
157
221
200
NOM Sample
10.5
ND
ND
ND
Range
(50%-145%)
(42%-138%)
(51%-159%)
(50%-148%)
Qual
U
U
U
U
U
U
UX
U
U
U
UX
X
X
QC1205530790 637450004
REC%
101
84
110
100
200
188
200
200
MS
638302Workorder:
X
U
U
UX
RPD%
Page 8 of 32
Page 22 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
09/28/23 14:04
09/29/23 01:36
09/28/23 14:04
09/29/23 01:36
09/28/23 14:04
09/29/23 01:36
QC
190
178
191
214
173
197
175
200
218
199
209
214
208
182
187
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(44%-127%)
(39%-138%)
(62%-132%)
(58%-157%)
(54%-139%)
(53%-151%)
(50%-154%)
(40%-152%)
(61%-142%)
(26%-138%)
(38%-148%)
(26%-139%)
(40%-144%)
(38%-133%)
(40%-155%)
Qual
X
X
X
X
REC%
95
89
96
107
93
105
92
104
109
100
105
107
104
91
94
200
200
200
200
186
187
190
192
200
200
200
200
200
200
200
638302Workorder:
U
U
U
UX
U
U
U
U
UX
U
U
U
U
UX
UX
RPD%
Page 9 of 32
Page 23 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
09/29/23 01:36
09/28/23 14:04
QC
274
252
213
180
202
225
219
234
206
211
214
206
220
154
191
NOM Sample
8.74
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.34
ND
ND
ND
Range
(45%-160%)
(50%-150%)
(61%-141%)
(43%-156%)
(50%-148%)
(43%-160%)
(45%-163%)
(40%-162%)
(38%-165%)
(31%-150%)
(50%-150%)
(40%-182%)
(19%-167%)
(52%-147%)
(57%-149%)
Qual
X
X
X
X
X
X
X
X
X
REC%
133
126
107
90
101
113
110
117
103
105
107
102
110
87
95
200
200
200
200
200
200
200
200
200
200
200
200
200
177
200
638302Workorder:
X
UX
UX
U
U
UX
UX
UX
UX
U
UX
JX
U
U
U
RPD%
Page 10 of 32
Page 24 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
09/28/23 14:04
09/29/23 01:36
09/28/23 14:04
QC
154
216
126
199
208
175
198
195
177
178
169
189
109
193
180
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(45%-136%)
(44%-143%)
(47%-138%)
(45%-142%)
(50%-150%)
(56%-149%)
(51%-149%)
(32%-151%)
(50%-148%)
(50%-150%)
(48%-138%)
(54%-146%)
(18%-140%)
(49%-143%)
(42%-150%)
Qual
X
REC%
80
108
65
99
104
92
99
97
97
89
88
95
54
97
90
193
200
194
200
200
190
200
200
182
200
192
200
200
200
200
638302Workorder:
U
U
U
U
UX
U
U
U
U
U
U
U
U
U
U
RPD%
Page 11 of 32
Page 25 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
JMB3
09/28/23 14:04
09/29/23 01:36
09/28/23 14:04
09/29/23 01:36
09/29/23 01:52
09/28/23 14:12
09/29/23 01:52
09/28/23 14:12
QC
203
187
204
208
198
207
184
382
215
201
221
199
203
178
214
NOM Sample
ND
ND
7.08
ND
ND
ND
ND
ND
10.5
ND
ND
ND
ND
ND
ND
Range
(50%-151%)
(55%-151%)
(51%-146%)
(32%-155%)
(41%-148%)
(41%-142%)
(44%-141%)
(45%-164%)
(0%-30%)
(0%-36%)
(0%-28%)
(0%-34%)
(0%-39%)
(0%-40%)
(0%-28%)
Qual
X
X
X
X
QC1205530791 637450004
1
24
0
1
7
0
11
REC%
101
100
99
91
99
104
92
191
102
107
110
100
101
89
107
200
188
200
200
200
200
200
200
200
188
200
200
200
200
200
MSD
638302Workorder:
*
U
U
J
UX
U
U
U
UX
X
U
U
UX
U
U
U
RPD%
Page 12 of 32
Page 26 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
DK2
09/29/23 01:52
09/28/23 14:12
09/29/23 01:52
09/28/23 14:12
09/29/23 01:52
QC
198
202
192
166
181
196
219
188
184
202
181
191
248
246
203
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.74
ND
ND
Range
(0%-31%)
(0%-33%)
(0%-39%)
(0%-40%)
(0%-44%)
(0%-29%)
(0%-42%)
(0%-36%)
(0%-40%)
(0%-36%)
(0%-33%)
(0%-26%)
(0%-32%)
(0%-34%)
(0%-30%)
Qual
X
X
X
X
X
X
X
8
16
2
5
10
11
9
11
15
3
1
2
10
3
5
REC%
99
108
103
87
94
98
109
94
92
101
91
95
120
123
102
200
186
187
190
192
200
200
200
200
200
200
200
200
200
200
638302Workorder:
UX
U
U
U
U
UX
U
U
U
U
UX
UX
X
UX
UX
RPD%
Page 13 of 32
Page 27 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
09/29/23 01:52
09/28/23 14:12
QC
185
190
200
195
220
209
200
205
187
212
173
191
171
210
139
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
2.34
ND
ND
ND
ND
ND
ND
Range
(0%-33%)
(0%-28%)
(0%-44%)
(0%-38%)
(0%-41%)
(0%-31%)
(0%-46%)
(0%-30%)
(0%-41%)
(0%-35%)
(0%-27%)
(0%-23%)
(0%-36%)
(0%-35%)
(0%-35%)
Qual
X
X
X
X
X
X
3
6
12
12
6
2
5
5
9
4
12
0
10
3
10
REC%
92
95
100
98
110
105
100
102
92
106
98
96
89
105
72
200
200
200
200
200
200
200
200
200
200
177
200
193
200
194
638302Workorder:
U
U
UX
UX
UX
UX
U
UX
JX
U
U
U
U
U
U
RPD%
Page 14 of 32
Page 28 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992Batch
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
09/28/23 14:12
09/29/23 01:52
09/28/23 14:12
QC
195
187
215
209
206
166
206
199
208
115
190
223
219
155
198
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.08
Range
(0%-30%)
(0%-30%)
(0%-30%)
(0%-26%)
(0%-33%)
(0%-31%)
(0%-26%)
(0%-35%)
(0%-30%)
(0%-44%)
(0%-28%)
(0%-31%)
(0%-28%)
(0%-31%)
(0%-24%)
Qual
X
2
11
21
5
6
6
15
16
10
6
2
22
8
19
3
REC%
98
94
113
104
103
91
103
103
104
58
95
112
109
83
95
200
200
190
200
200
182
200
192
200
200
200
200
200
188
200
638302Workorder:
U
UX
U
U
U
U
U
U
U
U
U
U
U
U
J
RPD%
Page 15 of 32
Page 29 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2499992
2500754
Batch
Batch
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
DK2
JMB3
DK2
JMB3
DK2
JMB3
09/29/23 01:52
09/28/23 14:12
09/29/23 01:52
10/01/23 14:58
09/29/23 16:32
10/01/23 14:58
09/29/23 16:32
10/01/23 14:58
09/29/23 16:32
QC
192
192
209
197
346
28.7
19.7
29.6
29.6
22.0
19.9
20.7
27.6
20.9
NOM Sample
ND
ND
ND
ND
ND
Range
(0%-34%)
(0%-32%)
(0%-35%)
(0%-34%)
(0%-35%)
(60%-158%)
(59%-144%)
(67%-144%)
(58%-144%)
(54%-128%)
(52%-141%)
(67%-154%)
(73%-141%)
(68%-135%)
Qual
JX
X
X
X
X
QC1205532191
8
3
1
7
10
REC%
82
96
104
98
173
137
99
141
141
105
95
99
132
107
200
200
200
200
200
21.0
19.8
21.0
21.0
21.0
21.0
21.0
21.0
19.5
LCS
638302Workorder:
*
UX
U
U
U
UX
RPD%
Page 16 of 32
Page 30 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
09/29/23 16:32
10/01/23 14:58
09/29/23 16:32
10/01/23 14:58
QC
21.1
17.2
15.9
27.4
23.1
20.0
19.4
21.4
23.1
28.6
35.0
35.4
29.9
32.1
27.1
NOM Sample Range
(56%-151%)
(60%-153%)
(60%-141%)
(61%-148%)
(23%-155%)
(57%-139%)
(20%-154%)
(59%-145%)
(35%-138%)
(63%-143%)
(5%-158%)
(5%-149%)
(59%-145%)
(48%-149%)
(52%-148%)
Qual
X
X
X
X
X
X
REC%
108
86
79
131
110
95
92
102
110
137
167
169
143
153
129
19.6
19.9
20.1
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
638302Workorder:
*
*
*
RPD%
Page 17 of 32
Page 31 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
10/01/23 14:58
09/29/23 16:32
10/01/23 14:58
QC
27.2
26.9
30.4
26.5
27.5
31.0
30.4
31.4
18.5
19.9
20.2
21.4
17.9
21.0
25.4
NOM Sample Range
(58%-147%)
(60%-151%)
(62%-148%)
(60%-144%)
(58%-142%)
(50%-150%)
(52%-144%)
(60%-149%)
(70%-144%)
(73%-151%)
(58%-134%)
(65%-145%)
(57%-134%)
(65%-137%)
(20%-160%)
Qual
X
X
X
X
X
X
X
REC%
130
128
145
126
131
148
145
150
100
95
100
102
88
100
121
21.0
21.0
21.0
21.0
21.0
21.0
21.0
21.0
18.6
21.0
20.2
21.0
20.3
21.0
21.0
638302Workorder:
*
*
RPD%
Page 18 of 32
Page 32 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
09/29/23 16:32
10/01/23 14:58
09/29/23 16:32
QC
20.2
19.4
22.7
19.6
22.0
20.2
20.2
12.3
20.3
22.0
21.5
17.8
20.9
30.2
21.0
NOM Sample Range
(68%-138%)
(71%-133%)
(69%-144%)
(67%-145%)
(70%-138%)
(64%-133%)
(69%-133%)
(35%-165%)
(64%-134%)
(65%-145%)
(66%-139%)
(67%-136%)
(72%-143%)
(49%-153%)
(66%-138%)
Qual
X
REC%
101
93
108
103
105
100
96
59
97
105
103
90
100
144
100
19.9
21.0
21.0
19.1
21.0
20.1
21.0
21.0
21.0
21.0
21.0
19.7
21.0
21.0
21.0
638302Workorder:
RPD%
Page 19 of 32
Page 33 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
JMB3
09/29/23 16:32
10/01/23 14:58
10/01/23 14:43
09/29/23 14:40
10/01/23 14:43
09/29/23 14:40
10/01/23 14:43
09/29/23 14:40
QC
21.6
23.9
63.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample Range
(58%-140%)
(63%-135%)
(5%-158%)
Qual
X
UX
U
U
UX
U
U
U
UX
U
U
U
U
QC1205532190
REC%
103
114
304
21.0
21.0
21.0
MB
638302Workorder:
*
RPD%
Page 20 of 32
Page 34 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
10/01/23 14:43
09/29/23 14:40
10/01/23 14:43
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
UX
U
U
U
U
UX
UX
UX
UX
UX
U
U
UX
UX
UX
REC%
638302Workorder:
RPD%
Page 21 of 32
Page 35 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
10/01/23 14:43
09/29/23 14:40
10/01/23 14:43
09/29/23 14:40
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
UX
U
UX
UX
U
U
U
U
U
U
U
UX
U
U
U
REC%
638302Workorder:
RPD%
Page 22 of 32
Page 36 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
09/29/23 14:40
10/01/23 14:43
09/29/23 14:40
10/01/23 14:43
QC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample RangeQual
U
U
U
U
U
U
U
U
U
U
UX
U
U
U
UX
REC%
638302Workorder:
RPD%
Page 23 of 32
Page 37 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
DK2
JMB3
DK2
JMB3
10/01/23 16:59
09/29/23 15:58
10/01/23 16:59
09/29/23 15:58
10/01/23 16:59
09/29/23 15:58
10/01/23 16:59
09/29/23 15:58
QC
21.3
16.0
19.7
20.2
19.5
20.8
18.7
19.4
16.6
17.9
14.3
16.2
18.4
19.0
20.9
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(50%-145%)
(42%-138%)
(51%-159%)
(50%-148%)
(44%-127%)
(39%-138%)
(62%-132%)
(58%-157%)
(54%-139%)
(53%-151%)
(50%-154%)
(40%-152%)
(61%-142%)
(26%-138%)
(38%-148%)
Qual
X
X
X
X
QC1205532192 638302001
REC%
125
100
115
118
114
122
110
114
104
112
88
99
108
111
123
17.0
16.1
17.0
17.0
17.0
17.0
17.0
17.0
15.9
15.9
16.2
16.4
17.0
17.0
17.0
MS
638302Workorder:
UX
U
U
UX
U
U
U
UX
U
U
U
U
UX
U
U
RPD%
Page 24 of 32
Page 38 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
09/29/23 15:58
10/01/23 16:59
QC
16.8
17.8
16.8
15.9
33.4
27.1
18.0
23.6
21.4
15.6
18.3
19.3
20.2
19.9
20.1
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(26%-139%)
(40%-144%)
(38%-133%)
(40%-155%)
(45%-160%)
(50%-150%)
(61%-141%)
(43%-156%)
(50%-148%)
(43%-160%)
(45%-163%)
(40%-162%)
(38%-165%)
(31%-150%)
(50%-150%)
Qual
X
X
X
X
X
X
X
X
X
X
REC%
99
105
98
93
196
159
105
139
126
91
107
113
119
117
118
17.0
17.0
17.0
17.0
17.0
17.0
17.0
17.0
17.0
17.0
17.0
17.0
17.0
17.0
17.0
638302Workorder:
*
*
U
U
UX
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
UX
RPD%
Page 25 of 32
Page 39 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
10/01/23 16:59
09/29/23 15:58
10/01/23 16:59
09/29/23 15:58
QC
17.0
21.0
15.8
18.1
13.8
21.7
11.2
18.6
19.3
18.0
18.5
20.1
15.9
17.4
16.4
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(40%-182%)
(19%-167%)
(52%-147%)
(57%-149%)
(45%-136%)
(44%-143%)
(47%-138%)
(45%-142%)
(50%-150%)
(56%-149%)
(51%-149%)
(32%-151%)
(50%-148%)
(50%-150%)
(48%-138%)
Qual
X
X
REC%
100
123
105
106
84
127
68
109
113
111
108
118
103
102
100
17.0
17.0
15.1
17.0
16.5
17.0
16.5
17.0
17.0
16.2
17.0
17.0
15.5
17.0
16.4
638302Workorder:
UX
U
U
U
U
U
U
U
UX
U
U
U
U
U
U
RPD%
Page 26 of 32
Page 40 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
1,1,2,2-Tetrafluoro-2-(1,2,2,2-
tetrafluoroethoxy)ethane sulfonic
acid (NVHOS)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (F-
53B Minor)
2,3,3,3-Tetrafluoro-2-
(1,1,2,2,3,3,3-
heptafluoropropoxy)-propanoic
acid (Gen-X)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
JMB3
DK2
09/29/23 15:58
10/01/23 16:59
09/29/23 15:58
10/01/23 16:59
10/01/23 17:14
09/29/23 16:06
10/01/23 17:14
QC
17.6
14.4
17.6
17.4
17.5
17.5
17.4
12.6
20.4
23.0
17.3
64.7
23.2
14.4
22.5
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(54%-146%)
(18%-140%)
(49%-143%)
(42%-150%)
(50%-151%)
(55%-151%)
(51%-146%)
(32%-155%)
(41%-148%)
(41%-142%)
(44%-141%)
(45%-164%)
(0%-30%)
(0%-36%)
(0%-28%)
Qual
JX
X
X
QC1205532193 638302001
9
11
13
REC%
103
84
103
99
103
109
102
71
120
135
101
379
127
84
124
17.0
17.0
17.0
17.0
17.0
16.0
17.0
17.0
17.0
17.0
17.0
17.0
18.2
17.1
18.2
MSD
638302Workorder:
*
U
U
U
U
U
U
U
UX
U
U
U
UX
UX
U
U
RPD%
Page 27 of 32
Page 41 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
2,3,3,3-Tetrafluoro-2-
(pentafluoroethoxy)propanoic acid
(PEPA)
2-(N-ethylperfluoro-1-
octanesulfonamido)-ethanol (N-
EtFOSE)
2-(N-methylperfluoro-1-
octanesulfonamido)-ethanol (N-
MeFOSE)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA,ADONA)
4-
(Heptafluoroisopropoxy)hexafluoro
butanoic acid (PFECA-G)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (F-53B
Major)
Fluorotelomer sulfonic acid 4:2 (4:2
FTS)
Fluorotelomer sulfonic acid 6:2 (6:2
FTS)
Fluorotelomer sulfonic acid 8:2 (8:2
FTS)
Hydro-EVE
N-ethylperfluoro-1-
octanesulfonamide (N-EtFOSA)
N-ethylperfluoro-1-
octanesulfonamidoacetic acid (N-
EtFOSAA)
N-methylperfluoro-1-
octanesulfonamide (N-MeFOSA)
N-methylperfluoro-1-
octanesulfonamidoacetic acid (N-
MeFOSAA)
Nafion Byproduct 1 (PFESA BP1)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
DK2
JMB3
DK2
JMB3
DK2
10/01/23 17:14
09/29/23 16:06
10/01/23 17:14
09/29/23 16:06
10/01/23 17:14
09/29/23 16:06
10/01/23 17:14
QC
22.5
20.8
18.9
17.1
24.4
17.6
17.9
17.0
16.4
21.1
20.1
18.3
20.2
24.8
18.9
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(0%-34%)
(0%-39%)
(0%-40%)
(0%-28%)
(0%-31%)
(0%-33%)
(0%-39%)
(0%-40%)
(0%-44%)
(0%-29%)
(0%-42%)
(0%-36%)
(0%-40%)
(0%-36%)
(0%-33%)
Qual
X
X
X
X
11
7
10
9
23
6
0
17
2
14
6
13
18
33
12
REC%
124
114
104
94
134
104
105
98
94
116
110
101
111
137
104
18.2
18.2
18.2
18.2
18.2
16.9
17.0
17.3
17.4
18.2
18.2
18.2
18.2
18.2
18.2
638302Workorder:
UX
U
U
U
UX
U
U
U
U
UX
U
U
U
U
UX
RPD%
Page 28 of 32
Page 42 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Nafion Byproduct 2 (PFESA BP2)
Nafion Byproduct 4 (PFESA BP4)
Nafion Byproduct 5 (PFESA BP5)
Nafion Byproduct 6 (PFESA BP6)
Nonafluoro-3,6-dioxaheptanoic
acid (NFDHA or PFECA B)
Perfluoro(2-ethoxyethane)sulfonic
acid (PFEESA or PES)
Perfluoro(3,5,7,9,11-
pentaoxadodecanoic) acid
(PFO5DA or TAFN4)
Perfluoro(3,5,7,9-tetraoxadecanoic)
acid (PFO4DA)
Perfluoro(3,5,7-trioxaoctanoic)
acid (PFO3OA)
Perfluoro(3,5-dioxahexanoic) acid
(PFO2HxA)
Perfluoro(4-methoxybutanoic) acid
(PFMOBA)
Perfluoro-2-
(perfluoromethoxy)propanoic acid
(PMPA)
Perfluoro-2-methoxyacetic acid
(PFMOAA)
Perfluoro-3-methoxypropanoic
acid (PFMOPrA)
Perfluorobutanesulfonic acid
(PFBS)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
DK2
JMB3
10/01/23 17:14
09/29/23 16:06
QC
19.7
36.3
33.2
22.9
23.2
22.3
19.2
20.9
22.2
22.0
22.7
22.3
18.3
23.5
15.9
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(0%-26%)
(0%-32%)
(0%-34%)
(0%-30%)
(0%-33%)
(0%-28%)
(0%-44%)
(0%-38%)
(0%-41%)
(0%-31%)
(0%-46%)
(0%-30%)
(0%-41%)
(0%-35%)
(0%-27%)
Qual
X
X
X
X
X
X
X
X
X
X
21
8
21
24
2
4
21
13
14
8
13
11
7
11
1
REC%
108
200
183
126
128
123
106
115
122
121
125
123
101
129
99
18.2
18.2
18.2
18.2
18.2
18.2
18.2
18.2
18.2
18.2
18.2
18.2
18.2
18.2
16.1
638302Workorder:
*
*
UX
UX
UX
UX
U
U
UX
UX
UX
UX
U
UX
UX
U
U
RPD%
Page 29 of 32
Page 43 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Perfluorobutanoic acid (PFBA)
Perfluorodecanesulfonic acid
(PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanesulfonic acid
(PFDoS)
Perfluorododecanoic acid (PFDOA)
Perfluoroethoxypropionic acid
(EVE)
Perfluoroheptanesulfonic acid
(PFHpS)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexadecanoic acid
(PFHxDA)
Perfluorohexanesulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanesulfonic acid
(PFNS)
Perfluorononanoic acid (PFNA)
Perfluorooctadecanoic acid
(PFODA)
Perfluorooctanesulfonamide
(PFOSA)
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
09/29/23 16:06
10/01/23 17:14
09/29/23 16:06
QC
20.2
15.5
16.7
11.1
18.7
20.5
20.7
18.7
19.7
17.4
18.9
17.0
19.3
14.1
20.2
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(0%-23%)
(0%-36%)
(0%-35%)
(0%-35%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-26%)
(0%-33%)
(0%-31%)
(0%-26%)
(0%-35%)
(0%-30%)
(0%-44%)
(0%-28%)
Qual
X
11
12
26
1
0
6
14
1
2
9
8
3
9
2
14
REC%
111
88
92
63
103
113
120
103
109
105
104
97
106
78
111
18.2
17.5
18.2
17.6
18.2
18.2
17.3
18.2
18.2
16.6
18.2
17.4
18.2
18.2
18.2
638302Workorder:
U
U
U
U
U
UX
U
U
U
U
U
U
U
U
U
RPD%
Page 30 of 32
Page 44 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2500754Batch
Perfluorooctanesulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluoropentanesulfonic acid
(PFPeS)
Perfluoropentanoic acid (PFPeA)
Perfluoropropanoic acid (PFPrA)
Perfluorotetradecanoic acid (PFTA)
Perfluorotridecanoic Acid (PFTriA)
Perfluoroundecanoic acid (PFUnA)
R-EVE
Parmname Units
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
ng/L
Anlst Date Time
JMB3
DK2
JMB3
DK2
09/29/23 16:06
10/01/23 17:14
09/29/23 16:06
10/01/23 17:14
QC
20.0
17.7
18.3
17.7
14.5
19.2
21.4
17.1
77.6
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(0%-31%)
(0%-28%)
(0%-31%)
(0%-24%)
(0%-34%)
(0%-32%)
(0%-35%)
(0%-34%)
(0%-35%)
Qual
JX
X
The Qualifiers in this report are defined as follows:
14
1
4
2
14
6
7
1
18
REC%
107
97
107
98
77
105
118
94
427
18.2
18.2
17.1
18.2
18.2
18.2
18.2
18.2
18.2
638302Workorder:
*
U
J
P
C
B
E
A
X
N
H
**
Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
Value is estimated
Organics--The concentrations between the primary and confirmation columns/detectors is >40% different. For HPLC, the difference is >70%.
Analyte has been confirmed by GC/MS analysis
The target analyte was detected in the associated blank.
Concentration of the target analyte exceeds the instrument calibration range
The TIC is a suspected aldol-condensation product
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Organics--Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based
on nearest internal standard response factor
Analytical holding time was exceeded
Analyte is a surrogate compound
U
U
U
U
UX
U
U
U
UX
RPD%
Notes:
Page 31 of 32
Page 45 of 52 SDG: 638302
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Parmname
Page 32 of 32
Units Anlst Date TimeQCNOMSampleRangeQualREC%
638302Workorder:
<
>
h
R
^
D
N/A
ND
NJ
JNX
UJ
Q
N1
Y
N
J
Result is less than value reported
Result is greater than value reported
Preparation or preservation holding time was exceeded
Sample results are rejected
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
Results are reported from a diluted aliquot of the sample
RPD or %Recovery limits do not apply.
Analyte concentration is not detected above the detection limit
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Non Calibrated Compound
Compound cannot be extracted
One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
See case narrative
QC Samples were not spiked with this compound
Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based on nearest
internal standard response factor
See case narrative for an explanation
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
RPD%
Page 46 of 52 SDG: 638302
LCMSMS-PFC
Technical Case Narrative
NC Dept Environmental Quality
SDG #: 638302

Product: The Extraction and Analysis of Per- and Polyfluoroalkyl Substances Using LCMSMS
Analytical Method: EPA 537.1 Modified
Analytical Procedure: GL-OA-E-076 REV# 14
Analytical Batches: 2499992 and 2499991
The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification
638302003 SW- Downstream- FB
1205530788 Method Blank (MB)
1205530789 Laboratory Control Sample (LCS)
1205530790 637450004(NonSDG) Matrix Spike (MS)
1205530791 637450004(NonSDG) Matrix Spike Duplicate (MSD)

The samples in this SDG were analyzed on an "as received" basis.
Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.

Calibration Information

CCV Requirements
Calibration verification standards (ICV or CCV) requirements have not been met for samples 1205530788 (MB),
1205530789 (LCS), 1205530790 (Non SDG 637450004MS), 1205530791 (Non SDG 637450004MSD) and All
in this batch in this SDG. One or more target analytes failed acceptance criteria with a positive bias in the
standards bracketing the samples in this SDG. These target analytes were not detected in the associated
environmental samples; therefore, the non-compliance had no adverse effect on the data.

Quality Control (QC) Information

Laboratory Control Sample Duplicate (LCSD)
An LCSD was used in place of matrix QC due to limited sample volume.

Matrix Spike (MS) Recovery Statement
The MS or MSD (See Below) recovered spiked analytes outside of the established acceptance limits. As similar
recoveries were displayed in the MS and MSD, the failures were attributed to sample matrix interference and the
data were reported.
Sample Analyte Value
1205530790 (Non SDG 637450004MS)R-EVE 191* (45%-164%)
1205530791 (Non SDG 637450004MSD)R-EVE 173* (45%-164%)
Page 47 of 52 SDG: 638302

Technical Information

Sample Dilutions
Samples 1205530790 (Non SDG 637450004MS) and 1205530791 (Non SDG 637450004MSD) were extracted
at reduced volumes due to sample matrix and the potential for clogging the SPE column.

Miscellaneous Information

Additional Comments
Some analytes are X qualified because the standards used to make the initial calibration curve did not meet the
ISO 17025 criterion. These are the only standards available for these analytes.

Product: The Extraction and Analysis of Per- and Polyfluoroalkyl Substances Using LCMSMS
Analytical Method: EPA 537.1 Modified
Analytical Procedure: GL-OA-E-076 REV# 14
Analytical Batches: 2500754 and 2500752
The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification
638302001 SW- Upstream
638302002 SW- Downstream
1205532190 Method Blank (MB)
1205532191 Laboratory Control Sample (LCS)
1205532192 638302001(SW- Upstream) Matrix Spike (MS)
1205532193 638302001(SW- Upstream) Matrix Spike Duplicate (MSD)

The samples in this SDG were analyzed on an "as received" basis.
Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.

Quality Control (QC) Information

Laboratory Control Sample (LCS) Recovery
The LCS and/or LCSD (See Below) did not meet the spike recovery acceptance limits with a positive bias. As
target analytes were not detected in the associated samples, the data were not adversely impacted.
Sample Analyte Value
1205532191 (LCS)Nafion Byproduct 5 (PFESA BP5)169* (5%-149%)
Nonafluoro-3, 6-dioxaheptanoic acid (NFDHA or PFECA B)153* (48%-149%)
Perfluoro-2-methoxyacetic acid (PFMOAA)145* (52%-144%)
Perfluoro-3-methoxypropanoic acid (PFMOPrA)150* (60%-149%)
R-EVE 304* (5%-158%)

The LCS and/or LCSD did not meet the spike recovery acceptance limits with a marginally positive bias for
Byproduct 4 (BP4). The target analyte was not detected in the associated samples with the exception of sample
Page 48 of 52 SDG: 638302
637904007, which had a detection just above the quantitation limit. The hold date for extraction had now past.
The data for the sample were reported as is. The sample had detections for several other target analytes.
Sample Analyte Value
1205532191 (LCS)Nafion Byproduct 4 (PFESA BP4)167* (5%-158%)

Matrix Spike (MS) Recovery Statement
The MS or MSD (See Below) recovered spiked analytes outside of the established acceptance limits. As similar
recoveries were displayed in the MS and MSD, the failures were attributed to sample matrix interference and the
data were reported.
Sample Analyte Value
1205532192 (SW- UpstreamMS)Nafion Byproduct 4 (PFESA BP4)196* (45%-160%)
Nafion Byproduct 5 (PFESA BP5)159* (50%-150%)
R-EVE 379* (45%-164%)
1205532193 (SW- UpstreamMSD)Nafion Byproduct 4 (PFESA BP4)200* (45%-160%)
Nafion Byproduct 5 (PFESA BP5)183* (50%-150%)
R-EVE 427* (45%-164%)

Miscellaneous Information

Additional Comments
Some analytes are X qualified because the standards used to make the initial calibration curve did not meet the
ISO 17025 criterion. These are the only standards available for these analytes.

Certification Statement

Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 49 of 52 SDG: 638302
Page 50 of 52 SDG: 638302
Page 51 of 52 SDG: 638302
State Certification
Alabama
Alaska
Alaska Drinking Water
Arkansas
CLIA
California
Colorado
Connecticut
DoD ELAP/ ISO17025 A2LA
Florida NELAP
Foreign Soils Permit
Georgia
Georgia SDWA
Hawaii
Idaho
Illinois NELAP
Indiana
Kansas NELAP
Kentucky SDWA
Kentucky Wastewater
Louisiana Drinking Water
Louisiana NELAP
Maine
Maryland
Massachusetts
Massachusetts PFAS Approv
Michigan
Mississippi
Nebraska
Nevada
New Hampshire NELAP
New Jersey NELAP
New Mexico
New York NELAP
North Carolina
North Carolina SDWA
North Dakota
Oklahoma
Pennsylvania NELAP
Puerto Rico
S. Carolina Radiochem
Sanitation Districts of L
South Carolina Chemistry
Tennessee
Texas NELAP
Utah NELAP
Vermont
Virginia NELAP
Washington
42200
17-018
SC00012
88-0651
42D0904046
2940
SC00012
PH-0169
2567.01
E87156
P330-15-00283, P330-15-00253
SC00012
967
SC00012
SC00012
200029
C-SC-01
E-10332
90129
90129
LA024
03046 (AI33904)
2019020
270
M-SC012
Letter
9976
SC00012
NE-OS-26-13
SC000122023-4
2054
SC002
SC00012
11501
233
45709
R-158
2022-160
68-00485
SC00012
10120002
9255651
10120001
TN 02934
T104704235-23-21
SC000122022-37
VT87156
460202
C780
List of current GEL Certifications as of 05 October 2023
Page 52 of 52 SDG: 638302