Loading...
HomeMy WebLinkAbout7407_Pitt_C&DLandfillInc_CDLF_Phase3_BaselineHydroLFG_FID1791669_20230419• % eurofins Environment Testing I ANALYTICAL REPORT C PREPARED FOR Attn: David Norris ELM Site Solutions Inc PO BOX 97607 C Raleigh, North Carolina 27624 Generated 3/30/2023 7:28:20 AM JOB DESCRIPTION C&D Landfill NC JOB NUMBER 410-119189-1 Analytical test results meet all requirements of the associated regulatory program (i.e., NELAC (TNI), DoD, and ISO 17025) unless otherwise noted under the individual analysis. 14 Lei I L Generated Lr/t.{7 W 3/30/2023 7:28:20 AM Authorized for release by Barbara Weyandt, Project Manager Barbara.WeyandtCcDet.eurofinsus.com (717)556-7264 Eurofins Lancaster Laboratories is a laboratory within Eurofins Lancaster Laboratories Environment Testing, LLC, a company within Eurofins Environment Testing Group of Companies Page 2 of 63 3/30/2023 Analytical test results meet all requirements of the associated regulatory program (e.g., NELAC (TNI), DoD, and ISO 17025) unless otherwise noted under the individual analysis. Data qualifiers are applied to note exceptions. Noncompliant quality control (QC) is further explained in narrative comments. • QC results that exceed the upper limits and are associated with non -detect samples are qualified but further narration is not required since the bias is high and does not change a non -detect result. Further narration is also not required with QC blank detection when the associated sample concentration is non -detect or more than ten times the level in the blank. Matrix QC may not be reported if insufficient sample or site -specific QC samples were not submitted. In these situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD is performed, unless otherwise specified in the method. Surrogate and/or isotope dilution analyte recoveries (if applicable) which are outside of the QC window are confirmed unless attributed to a dilution or otherwise noted in the narrative. E: Regulated compliance samples (e.g. SDWA, NPDES) must comply with the associated agency requirements/permits. Measurement uncertainty values, as applicable, are available upon request Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our staff. Times are local to the area of activity. Parameters listed in the 40 CFR Part 136 Table II as "analyze immediately" and tested in the laboratory are not performed within 15 minutes of collection. This report shall not be reproduced except in full, without the written approval of the laboratory. WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. The foregoing express warranty is exclusive and is given in lieu of all other warranties, expressed or implied, except as otherwise agreed. We disclaim any other warranties, expressed or implied, including a warranty of fitness for particular purpose and warranty of merchantability. In no event shall Eurofins Lancaster Laboratories Environmental, LLC be liable for indirect, special, consequential, or incidental damages including, but not limited to, damages for loss of profit or goodwill regardless of (A) the negligence (either sole or concurrent) of Eurofins Lancaster Laboratories Environmental and (B) whether Eurofins Lancaster Laboratories Environmental has been informed of the possibility of such damages. We accept no legal responsibility for the purposes for which the client uses the test results. Except as otherwise agreed, no purchase order or other order for work shall be accepted by Eurofins Lancaster Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster Laboratories Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by client. a�6 Page 3 of 63 3/30/2023 Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Table of Contents Laboratory Job ID: 410-119189-1 Cover Page .............................................. 1 Table of Contents ......................................... 4 Definitions/Glossary....................................... 5 L Case Narrative ........................................... 7 Detection Summary ........................................ 9 Client Sample Results ...................................... 10 Surrogate Summary ....................................... 23 QC Sample Results ........................................ 26 QC Association Summary ................................... 47 C Lab Chronicle ............................................ 52 Certification Summary ...................................... 54 Method Summary ......................................... 55 Sample Summary ......................................... 56 Chain of Custody .......................................... 57 Receipt Checklists ......................................... 62 Eurofins Lancaster Laboratories Environment Testing LLC Page 4 of 63 3/30/2023 Definitions/Glossary Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Qualifiers GC/MS VOA Qualifier Qualifier Description cn Refer to Case Narrative for further detail J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. GC/MS Semi VOA Qualifier Qualifier Description LCS and/or LCSD is outside acceptance limits, low biased. '+ LCS and/or LCSD is outside acceptance limits, high biased. 1 LCS/LCSD RPD exceeds control limits. cn Refer to Case Narrative for further detail E Result exceeded calibration range. J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. GC Semi VOA Qualifier cn HPLC/IC Qualifier J Metals Qualifier J Qualifier Description Refer to Case Narrative for further detail Qualifier Description Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Qualifier Description Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. General Chemistry Qualifier Qualifier Description cn Refer to Case Narrative for further detail Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. n Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Lever' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRIES Presumptive Job ID: 410-119189-1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 5 of 63 3/30/2023 Definitions/Glossary Client: ELM Site Solutions Inc Project/Site: C&D Landfill INC Job ID: 410-119189-1 Glossary (Continued) Abbreviation These commonly used abbreviations may or may not be present in this report. QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Lancaster Laboratories Environment Testing, LLC Page 6 of 63 3/30/2023 Case Narrative Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Job ID: 410-119189-1 Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC Narrative Job Narrative 410-119189-1 Job ID: 410-119189-1 Receipt The samples were received on 3/17/2023 10:24 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 1.3°C and 1.3°C GC/MS VOA Method 8260D_LL: The preservative used in the sample containers provided is not compatible with one of the Method 8260 analytes requested. The following samples were received preserved with hydrochloric acid: MW-18 (410-119189-1), MW-19 (410-119189-2) and TB-1 (410-119189-3). The requested target analyte list includes Acrylonitrile , an acid -labile compound that degrades in an acidic medium. Method 8260D_LL: The continuing calibration verification (CCV) associated with batch 410-354854 recovered outside acceptance criteria, low biased, for 1, 1 -Dichloroethene and Bromomethane. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Non -detections of the affected analytes are reported. Any detections are considered estimated. Method 8260D_LL: The continuing calibration verification (CCV) associated with batch 410-354854 recovered above the upper control limit for 1,1,1,2-Tetrachloroethane, Bromoform, Ethyl methacrylate, trans-1,3-Dichloropropene, trans- 1,4-Dichloro-2-butene and Vinyl acetate. Non -detections of the affected analytes are reported. Any detections are considered estimated. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC/MS Semi VOA Method 8270E: The continuing calibration verification (CCV) associated with batch 410-356887 recovered above the upper control limit for 2,4-Dinitrophenol, 2-Nitroaniline, 2-Nitrophenol, 4,6-Dinitro-2-methyl phenol, Bis(2-ethylhexyl) phthalate, Butylbenzylphthalate, Chlorobenzi late, Di-n-octyl phthalate, Pentachloronitrobenzene, Phenacetin and Kepone. The samples associated with this CCV were non -detects for the affected analytes; therefore, the data have been reported. Method 8270E: The laboratory control sample and/or the laboratory control sample duplicate (LCS/LCSD) for preparation batch 410-356549 and analytical batch 410-356887 recovered outside control limits for the following analyte(s): 1,4-Naphthoquinone and 1,4-phenylenediamine. These analytes have been identified as poor performers when analyzed using this method; therefore, re-extraction/re-analysis was not performed. Method 8270E: The following analyte(s) recovered outside control limits for the LCSD associated with preparation batch 410-356549 and analytical batch 410-356887: o,o',o"-Triethylphosphorothioate. This is not indicative of a systematic control problem because these were random marginal exceedances. Qualified results have been reported. Method 8270E: The continuing calibration verification (CCV) analyzed in batch 410-356887 was outside the method criteria for the following analyte(s): 1,4-phenylenediamine. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC Semi VOA Method 8141 B: The continuing calibration verification (CCV) associated with batch 180-430015 recovered above the upper control limit for Dimethoate. The samples associated with this CCV were non -detects for the affected analytes; therefore, the data have been reported. The associated samples are impacted: MW-18 (410-119189-1), MW-19 (410-119189-2) and (CCV 180-430015/12). Method 8141 B: The continuing calibration verification (CCV) associated with batch 180-430015 recovered above the upper control limit for Dimethoate and Phorate. The samples associated with this CCV were non -detects for the affected analytes; therefore, the data have been reported. The associated samples are impacted: MW-18 (410-119189-1), MW-19 (410-119189-2) and (CCV 180-430015/12). Eurofins Lancaster Laboratories Environment Testing LLC Page 7 of 63 3/3072023 Case Narrative Client: ELM Site Solutions Inc Project/Site: C&D Landfill NIC Job ID: 410-119189-1 (Continued) Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC (Continued) No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Herbicides No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. F Job ID: 410-119189-1 PCBs No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Pesticides F No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. F HPLC/IC No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Metals No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. General Chemistry Method 353.2_Pres: samples were not available preservedMW-18 (410-119189-1), MW-19 (410-119189-2), (410-119189-F-1 DU) and (410-119189-F-1 MS) No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins Lancaster Laboratories Environment Testing LLC Page 8 of 63 3/3072023 Detection Summary Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-18 Analyte Result Qualifier RL MDL Unit Sulfate 3.5 J 7.5 2.5 mg/L Chloride 6.6 J 7.5 3.0 mg/L Barium 34 2.0 0.75 ug/L Beryllium 0.20 J 0.50 0.12 ug/L Chromium 0.68 J 2.0 0.33 ug/L Cobalt 0.28 J 0.50 0.16 ug/L Iron 1400 50 20 ug/L Lead 0.25 J 0.50 0.071 ug/L Manganese 27 2.0 0.95 ug/L Vanadium 3.0 J 4.0 0.79 ug/L Total Alkalinity as CaCO3 to pH 4.5 21 8.0 2.6 mg/L Total Dissolved Solids 60 30 12 mg/L Client Sample ID: MW-19 Analyte Result Qualifier RL MDL Unit Acetone 1.1 J 5.0 1.0 ug/L Sulfate 76 15 5.0 mg/L Chloride 3.7 J 7.5 3.0 mg/L Arsenic 0.86 J 2.0 0.68 ug/L Barium 45 2.0 0.75 ug/L Beryllium 0.50 0.50 0.12 ug/L Chromium 0.50 J 2.0 0.33 ug/L Cobalt 1.7 0.50 0.16 ug/L Copper 0.40 J 1.0 0.36 ug/L Iron 4100 50 20 ug/L Lead 0.20 J 0.50 0.071 ug/L Manganese 83 2.0 0.95 ug/L Nickel 2.1 1.0 0.40 ug/L Vanadium 1.5 J 4.0 0.79 ug/L Zinc 16 10 4.0 ug/L Total Alkalinity as CaCO3 to pH 4.5 8.9 8.0 2.6 mg/L Total Dissolved Solids 130 30 12 mg/L Client Sample ID: TB-1 [ No Detections. This Detection Summary does not include radiochemical test results. F Job ID: 410-119189-1 Lab Sample ID: 410-119189-1 Dil Fac D Method Prep Type 5 EPA 300.0 R2.1 Total/NA 5 EPA 300.0 R2.1 Total/NA 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 2320B-2011 Total/NA 1 SM 2540C Total/NA Lab Sample ID: 410-119189-2 Dil Fac D Method Prep Type 1 8260D Total/NA 10 EPA 300.0 R2.1 Total/NA 5 EPA 300.0 R2.1 Total/NA 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 6020B Total Recoverable 1 2320B-2011 Total/NA 1 SM 2540C Total/NA Lab Sample ID: 410-119189-3 Eurofins Lancaster Laboratories Environment Testing, LLC Page 9 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Client Sample ID: MW-18 Lab Sample ID: 410-119189-1 Date Collected: 03/16/23 12:30 Matrix: Water Date Received: 03/17/23 10:24 Method: SW846 8260D SIM 14D - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane ND 0.40 0.17 ug/L 03/20/23 20:30 1 • Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac Toluene-d8 (Surr) 104 80 - 120 03120123 20:30 1 Method: SW846 8260D - Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND cn 0.50 0.070 ug/L - 03/18/23 05:31 1 1,1,1-Trichloroethane ND 0.50 0.080 ug/L 03/18/23 05:31 1 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/L 03/18/23 05:31 1 1,1,2-Trichloroethane ND 0.50 0.080 ug/L 03/18/23 05:31 1 1,1-Dichloroethane ND 0.50 0.10 ug/L 03/18/23 05:31 1 1,1-Dichloroethene ND cn 0.50 0.10 ug/L 03/18/23 05:31 1 1,2,3-Trichloropropane ND 1.0 0.10 ug/L 03/18/23 05:31 1 1,2,4-Trichlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:31 1 1,2-Dibromo-3-Chloropropane ND 0.50 0.10 ug/L 03/18/23 05:31 1 1,2-Dibromoethane ND 0.50 0.080 ug/L 03/18/23 05:31 1 1,2-Dichlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:31 1 1,2-Dichloroethane ND 0.50 0.070 ug/L 03/18/23 05:31 1 1,2-Dichloropropane ND 0.50 0.10 ug/L 03/18/23 05:31 1 1,3-Dichlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:31 1 1,4-Dichlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:31 1 2-Butanone ND 5.0 1.0 ug/L 03/18/23 05:31 1 2-Hexanone ND 5.0 0.10 ug/L 03/18/23 05:31 1 4-Methyl-2-pentanone ND 5.0 1.0 ug/L 03/18/23 05:31 1 Acetone ND 5.0 1.0 ug/L 03/18/23 05:31 1 Acrylonitrile ND cn 5.0 0.40 ug/L 03/18/23 05:31 1 Benzene ND 0.50 0.10 ug/L 03/18/23 05:31 1 Bromochloromethane ND 0.50 0.080 ug/L 03/18/23 05:31 1 Bromodichloromethane ND 0.50 0.080 ug/L 03/18/23 05:31 1 Bromoform ND cn 1.0 0.30 ug/L 03/18/23 05:31 1 Bromomethane ND cn 0.50 0.10 ug/L 03/18/23 05:31 1 Carbon disulfide ND 1.0 0.10 ug/L 03/18/23 05:31 1 Carbon tetrachloride ND 0.50 0.10 ug/L 03/18/23 05:31 1 Chlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:31 1 Chloroethane ND 0.50 0.10 ug/L 03/18/23 05:31 1 Chloroform ND 0.50 0.090 ug/L 03/18/23 05:31 1 Chloromethane ND 0.50 0.10 ug/L 03/18/23 05:31 1 cis-1,2-Dichloroethene ND 0.50 0.080 ug/L 03/18/23 05:31 1 cis- 1,3-Dichloropropene ND 0.50 0.10 ug/L 03/18/23 05:31 1 Dibromochloromethane ND 0.50 0.080 ug/L 03/18/23 05:31 1 Dibromomethane ND 0.50 0.080 ug/L 03/18/23 05:31 1 Ethyl methacrylate ND cn 0.50 0.10 ug/L 03/18/23 05:31 1 Ethylbenzene ND 0.50 0.080 ug/L 03/18/23 05:31 1 Methyl iodide ND 0.50 0.080 ug/L 03/18/23 05:31 1 Methylene Chloride ND 0.50 0.10 ug/L 03/18/23 05:31 1 Styrene ND 0.50 0.070 ug/L 03/18/23 05:31 1 Tetrachloroethene ND 0.50 0.20 ug/L 03/18/23 05:31 1 Tetrahydrofuran ND 5.0 0.80 ug/L 03/18/23 05:31 1 Toluene ND 0.50 0.080 ug/L 03/18/23 05:31 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 10 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-18 Date Collected: 03/16/23 12:30 Date Received: 03/17/23 10:24 Job ID: 410-119189-1 Lab Sample ID: 410-119189-1 Matrix: Water Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac trans-1,2-Dichloroethene ND 0.50 0.10 ug/L 03/18/23 05:31 1 trans-1,3-Dichloropropene ND cn 0.50 0.080 ug/L 03/18/23 05:31 1 trans-1,4-Dichloro-2-butene ND cn 5.0 2.0 ug/L 03/18/23 05:31 1 Trichloroethene ND 0.50 0.080 ug/L 03/18/23 05:31 1 Trichlorofluoromethane ND 0.50 0.10 ug/L 03/18/23 05:31 1 Vinyl acetate ND cn 1.0 0.30 ug/L 03/18/23 05:31 1 Vinyl chloride ND 0.50 0.10 ug/L 03/18/23 05:31 1 Xylenes, Total ND 1.0 0.070 ug/L 03/18/23 05:31 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dfl Fac 1, 2-Dichloroethane-d4 (Surr) 100 80 - 120 03/18/23 05:31 1 Dibromofluoromethane (Surr) 96 80 - 120 03/18/23 05:31 1 4-Bromofluorobenzene (Surr) 88 80 - 120 03/18/23 05:31 1 Toluene-d8 (Surr) 101 80 - 120 03/18/23 05:31 1 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2,4,5-Tetrachlorobenzene ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 1,2,4-Trichlorobenzene ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 sym-Trinitrobenzene ND *1 200 99 ug/L 03/23/23 08:00 03/23/23 20:33 1 1,3-Dinitrobenzene ND 5.1 1.0 ug/L 03/23/23 08:00 03/23/23 20:33 1 1,4-Naphthoquinone ND *- *1 cn 100 25 ug/L 03/23/23 08:00 03/23/23 20:33 1 1,4-phenylenediamine ND *- cn 310 76 ug/L 03/23/23 08:00 03/23/23 20:33 1 1-Naphthylamine ND 21 8.1 ug/L 03/23/23 08:00 03/23/23 20:33 1 2,3,4,6-Tetrachlorophenol ND 5.1 1.0 ug/L 03/23/23 08:00 03/23/23 20:33 1 2,4,5-Trichlorophenol ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 2,4,6-Trichlorophenol ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 2,4-Dichlorophenol ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 2,4-Dimethylphenol ND 10 3.1 ug/L 03/23/23 08:00 03/23/23 20:33 1 2,4-Dinitrophenol ND *+ cn 31 14 ug/L 03/23/23 08:00 03/23/23 20:33 1 2,4-Dinitrotoluene ND 5.1 1.0 ug/L 03/23/23 08:00 03/23/23 20:33 1 2,6-Dichlorophenol ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 2,6-Dinitrotoluene ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 2-Acetylaminofluorene ND 21 10 ug/L 03/23/23 08:00 03/23/23 20:33 1 2-Chloronaphthalene ND 1.0 0.41 ug/L 03/23/23 08:00 03/23/23 20:33 1 2-Chlorophenol ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 2-Methylnaphthalene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 1 2-Methylphenol ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 2-Naphthylamine ND *1 21 7.1 ug/L 03/23/23 08:00 03/23/23 20:33 1 2-Nitroaniline ND cn 5.1 1.0 ug/L 03/23/23 08:00 03/23/23 20:33 1 2-Nitrophenol ND cn 5.1 1.0 ug/L 03/23/23 08:00 03/23/23 20:33 1 3,3'-Dichlorobenzidine ND 10 4.1 ug/L 03/23/23 08:00 03/23/23 20:33 1 3,3'-Dimethylbenzidine ND *1 76 25 ug/L 03/23/23 08:00 03/23/23 20:33 1 3-Methylcholanthrene ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 1 3-Nitroaniline ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 1 4,6-Dinitro-2-methylphenol ND cn 21 8.1 ug/L 03/23/23 08:00 03/23/23 20:33 1 4-Aminobiphenyl ND 11 5.1 ug/L 03/23/23 08:00 03/23/23 20:33 1 4-Bromophenyl-phenylether ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 1 4-Chloro-3-methylphenol ND 5.1 1.0 ug/L 03/23/23 08:00 03/23/23 20:33 1 4-Chloroaniline ND 10 4.1 ug/L 03/23/23 08:00 03/23/23 20:33 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 11 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-18 Date Collected: 03/16/23 12:30 Date Received: 03/17/23 10:24 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Job ID: 410-119189-1 Lab Sample ID: 410-119189-1 Matrix: Water Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 4-Chlorophenyl-phenyl ether ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 4-Methylphenol ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 4-Nitroaniline ND 3.1 0.92 ug/L 03/23/23 08:00 03/23/23 20:33 4-Nitrophenol ND 31 10 ug/L 03/23/23 08:00 03/23/23 20:33 5-Nitro-o-toluidine ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 7,12-Dimethylbenz(a)anthracene ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 Acenaphthene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Acenaphthylene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Acetophenone ND 5.1 1.0 ug/L 03/23/23 08:00 03/23/23 20:33 Anthracene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Benzo[a]anthracene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Benzo[a]pyrene ND 0.51 0.11 ug/L 03/23/23 08:00 03/23/23 20:33 Benzo[b]fuoranthene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Benzo[g,h,i]perylene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Benzo[k]fluoranthene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Benzyl alcohol ND 10 4.1 ug/L 03/23/23 08:00 03/23/23 20:33 Bis(2-chloroethoxy)methane ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Bis(2-chloroethyl)ether ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Bis(2-ethylhexyl) phthalate ND cn 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 bis(2 chloro-1-methylethyl) ether ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Butylbenzylphthalate ND cn 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 Chlorobenzilate ND "1 cn 10 3.1 ug/L 03/23/23 08:00 03/23/23 20:33 Chrysene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Di-n-butyl phthalate ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 Di-n-octyl phthalate ND cn 11 5.1 ug/L 03/23/23 08:00 03/23/23 20:33 Diallate (Trans/Cis) ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 Dibenz(a,h)anthracene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Dibenzofuran ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Diethyl phthalate ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 Dimethyl phthalate ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 Ethyl methanesulfonate ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Fluoranthene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:33 Fluorene ND 0.51 0.12 ug/L 03/23/23 08:00 03/23/23 20:33 Hexachlorobenzene ND 0.51 0.11 ug/L 03/23/23 08:00 03/23/23 20:33 Hexachlorobutadiene ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Hexachlorocyclopentadiene ND 11 5.1 ug/L 03/23/23 08:00 03/23/23 20:33 Hexachloroethane ND 5.1 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Hexachloropropene ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 Indeno[1,2,3-cd]pyrene ND 0.51 0.11 ug/L 03/23/23 08:00 03/23/23 20:33 Isodrin ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Isophorone ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Isosafrole ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 Methapyrilene ND 51 15 ug/L 03/23/23 08:00 03/23/23 20:33 Methyl methanesulfonate ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 N-Nitrosodi-n-propylamine ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 N-Nitrosodi-n-butylamine ND 11 5.1 ug/L 03/23/23 08:00 03/23/23 20:33 N-Nitrosodimethylamine ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:33 N-Nitrosodiethylamine ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 N-Nitrosodiphenylamine ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:33 Dil Fac 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 12 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-18 Date Collected: 03/16/23 12:30 Date Received: 03/17/23 10:24 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit N-Nitrosomethylethylamine ND 5.1 2.0 ug/L Famphur ND 51 25 ug/L N-Nitrosopiperidine ND 2.0 0.51 ug/L N-Nitrosopyrrolidine ND 2.0 0.51 ug/L Naphthalene ND 0.51 0.10 ug/L Nitrobenzene ND 2.0 0.51 ug/L o,o',o"-Triethylphosphorothioate ND `- cn 5.1 2.0 ug/L o-Toluidine ND 10 4.1 ug/L p-Dimethylamino azobenzene ND 12 5.5 ug/L Pentachlorobenzene ND 2.0 0.51 ug/L Pentachloronitrobenzene ND cn 5.1 2.0 ug/L Pentachlorophenol ND 5.1 1.0 ug/L Phenacetin ND cn 5.1 0.51 ug/L Phenanthrene ND 0.51 0.11 ug/L Phenol ND 2.0 0.51 ug/L Kepone ND cn 51 25 ug/L Pronamide ND 5.1 2.0 ug/L Pyrene ND 0.51 0.10 ug/L Safrole, Total ND 5.1 2.0 ug/L Surrogate 2,4,6-Tribromophenol (Surf) 2-Fluorobiphenyl (Surr) 2-Fluorophenol (Surr) Nitrobenzene-d5 (Surr) p-Terphenyl-d14 (Surr) Phenol-d5 (Surr) Job ID: 410-119189-1 Lab Sample ID: 410-119189-1 Matrix: Water D Prepared 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 Analyzed 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 03/23/23 20:33 Dil Fac 1 1 1 1 1 1 1 1 1 1 %Recovery Qualifier Limits Prepared Analyzed Dil Fac 84 13 - 138 03123123 08:00 03/23/23 20:33 1 kh- 84 44 - 120 03/23/23 08:00 03/23/23 20:33 1 40 10 - 120 03/23/23 08:00 03/23/23 20:33 1 69 31 - 120 03/23/23 08:00 03/23/23 20:33 1 81 30 - 125 03/23/23 08:00 03/23/23 20:33 1 28 10 - 120 03/23/23 08:00 03/23/23 20:33 1 Method: SW846 8081 B - Organochlorine Pesticides (GC) Analyte Result Qualifier Aldrin (1C) ND alpha-BHC (1C) ND beta-BHC (1C) ND delta-BHC (1C) ND Dieldrin (1C) ND Endosulfan I (1C) ND Endosulfan II (1C) ND Endosulfan sulfate (1C) ND Endrin (1C) ND Endrin aldehyde (1C) ND gamma-BHC (Lindane) (1C) ND Heptachlor (1C) ND Heptachlor epoxide (1C) ND p,p'-DDD (1C) ND p,p'-DDE (1C) ND p,p'-DDT (1C) ND Toxaphene (1C) ND Chlordane (n.o.s.) (1C) ND Methoxychlor (1C) ND RL MDL Unit D Prepared Analyzed Dil Fac 0.020 0.0020 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.020 0.0030 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.030 0.011 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.020 0.0034 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.030 0.0053 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.020 0.0043 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.040 0.015 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.030 0.0058 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.030 0.0081 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.10 0.020 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.020 0.0020 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.020 0.0020 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.020 0.0023 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.030 0.0050 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.030 0.0050 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.030 0.0052 ug/L 03/23/23 16:25 03/24/23 06:56 1 1.0 0.30 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.50 0.16 ug/L 03/23/23 16:25 03/24/23 06:56 1 0.11 0.030 ug/L 03/23/23 16:25 03/24/23 06:56 1 Page 13 of 63 Eurofins Lancaster Laboratories Environment Testing, LLC 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-18 Date Collected: 03/16/23 12:30 Date Received: 03/17/23 10:24 Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl (Surr) (1C) 37 20 - 149 DCB Decachlorobiphenyl (Surr) (2C) 48 20 - 149 Tetrachloro-m-xylene (Surr) (1 C) 57 20 - 129 Tetrachloro-m-xylene (Surr) (2C) 59 20 - 129 Method: SW846 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Analyte Result Qualifier RL MDL Unit PCB-1016 (1C) ND 0.25 0.10 ug/L PCB-1221 (1C) ND 0.25 0.10 ug/L PCB-1232 (1C) ND 0.25 0.10 ug/L PCB-1242 (1C) ND 0.25 0.10 ug/L PCB-1248 (1C) ND 0.25 0.078 ug/L PCB-1254 (1C) ND 0.25 0.078 ug/L PCB-1260 (1C) ND 0.25 0.078 ug/L F Job ID: 410-119189-1 Lab Sample ID: 410-119189-1 Matrix: Water Prepared Analyzed 03/23/23 16:25 03/24/23 06:56 03123123 16:25 03/24/23 06:56 03123123 16:25 03/24/23 06:56 03/23/23 16:25 03/24/23 06:56 D Prepared Analyzed 03/23/2316:28 03/24/2310:40 03/23/2316:28 03/24/2310:40 03/23/2316:28 03/24/2310:40 03/23/2316:28 03/24/2310:40 03/23/2316:28 03/24/2310:40 03/23/2316:28 03/24/2310:40 03/23/2316:28 03/24/2310:40 Surrogate %Recovery Qualifier Limits Prepared Analyzed DCB Decachlorobiphenyl (Surr) (1C) 35 10 - 148 03/23/23 16:28 03/24/23 10:40 DCB Decachlorobiphenyl (Surr) (2C) 36 10 - 148 03/23/23 16:28 03/24/23 10:40 Tetrachloro-m-xylene (1C) 58 33. 137 03/23/23 16:28 03/24/23 10:40 Tetrachloro-m-xylene (2C) 60 33 - 137 03123123 16:28 03/24/23 10:40 Method: SW846 8151A - Herbicides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 2,4,5-T (1C) ND 0.15 0.066 ug/L 03/21/23 20:22 03/22/23 12:30 Silvex (2,4,5-TP) (1C) ND 0.051 0.022 ug/L 03/21/23 20:22 03/22/23 12:30 2,4-Dichlorophenoxyacetic acid (1C) ND 0.61 0.25 ug/L 03/21/23 20:22 03/22/23 12:30 Dinoseb (1C) ND 0.61 0.28 ug/L 03/21/23 20:22 03/22/23 12:30 Method: SW846 EPA 8141 B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Lab: Eurofins Pittsburgh Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dimethoate (1C) ND cn 0.98 0.26 ug/L 03/20/23 18:11 03/22/23 14:44 Disulfoton (1C) ND cn 0.98 0.40 ug/L 03/20/23 18:11 03/22/23 14:44 Parathion (1C) ND cn 0.98 0.36 ug/L 03/20/23 18:11 03/22/23 14:44 Methyl parathion (1C) ND cn 0.98 0.34 ug/L 03/20/23 18:11 03/22/23 14:44 Phorate (1C) ND cn 0.98 0.37 ug/L 03/20/23 18:11 03/22/23 14:44 Diethyl-O-pyrazinyl phosphorothioate, ND cn 0.98 0.32 ug/L 03/20/23 18:11 03/22/23 14:44 O,O- (1C) Surrogate %Recovery Qualifier Limits Prepared Analyzed Tiibutyl phosphate (2C) 107 cn 25 - 127 03120123 18:11 03/22/23 14:44 Triphenylphosphate (1C) 111 cn 70- 155 03/20/23 18:11 03/22/23 14:44 Method: EPA300.0 R2.1 -Anions, Ion Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Sulfate 3.5 J 7.5 2.5 mg/L 03/20/2314:34 Chloride 6.6 J 7.5 3.0 mg/L 03/20/2314:34 Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Antimony ND 1.0 0.20 ug/L 03/22/23 07:13 03/22/23 18:07 Arsenic ND 2.0 0.68 ug/L 03/22/23 07:13 03/22/23 18:07 Eurofins Lancaster Laboratories Environment Testing, LLC Page 14 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-18 Date Collected: 03/16/23 12:30 Date Received: 03/17/23 10:24 Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable (Continued) Analyte Result Qualifier RL Barium 34 2.0 Beryllium 0.20 J 0.50 Cadmium ND 0.50 Chromium 0.68 J 2.0 Cobalt 0.28 J 0.50 Copper ND 1.0 Iron 1400 50 Lead _ 0.25 J 0.50 Manganese 27 2.0 Nickel ND 1.0 Selenium ND 1.0 Silver ND 0.50 Thallium ND 0.50 Tin ND 2.0 Vanadium 3.0 J 4.0 Zinc ND 10 Method: SW846 7470A - Mercury (CVAA) Analyte Result Qualifier RL Mercury ND 0.20 General Chemistry Analyte Result Qualifier RL Total Alkalinity as CaCO3 to pH 4.5 21 8.0 (SM 232013-2011) Nitrate as N (EPA 353.2) ND 0.10 Nitrate Nitrite as N (EPA 353.2) ND cn 0.10 Nitrite as N (EPA 353.2) ND 0.050 Sulfide (SM 4500 S2 D-2011) ND 0.30 Cyanide, Total (SW846 9012B) ND 0.010 Total Dissolved Solids (SM 2540C) 60 30 Job ID: 410-119189-1 Lab Sample ID: 410-119189-1 Matrix: Water MDL Unit D Prepared Analyzed Dil Fac 0.75 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.12 ug/L 03/22/23 07:13 03/24/23 09:25 1 0.15 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.33 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.16 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.36 ug/L 03/22/23 07:13 03/22/23 18:07 1 20 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.071 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.95 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.40 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.28 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.10 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.13 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.60 ug/L 03/22/23 07:13 03/22/23 18:07 1 0.79 ug/L 03/22/23 07:13 03/22/23 18:07 1 4.0 ug/L 03/22/23 07:13 03/22/23 18:07 1 MDL Unit D Prepared Analyzed Dil Fac 0.079 ug/L 03/22/23 08:17 03/22/23 15:24 1 MDL Unit D Prepared Analyzed Dil Fac 2.6 mg/L 03/23/23 03:41 1 0.040 mg/L 03/20/23 07:33 1 0.040 mg/L 03/25/2313:53 1 0.015 mg/L 03/18/23 08:31 1 0.10 mg/L 03/20/2313:32 1 0.0050 mg/L 03/24/2312:00 03/27/2312:07 1 12 mg/L 03/22/23 06:15 1 Client Sample ID: MW-19 Lab Sample ID: 410-119189-2 Date Collected: 03/16/23 15:00 Matrix: Water Date Received: 03/17/23 10:24 Method: SW846 8260D SIM 14D - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL 1,4-Dioxane ND 0.40 Surrogate %Recovery Qualifier Limits Toluene-d8 (Surr) 105 80 - 120 Method: SW846 8260D - Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL 1,1,1,2-Tetrachloroethane ND cn 0.50 1,1,1-Trichloroethane ND 0.50 1,1,2,2-Tetrachloroethane ND 0.50 1,1,2-Trichloroethane ND 0.50 1,1-Dichloroethane ND 0.50 1,1-Dichloroethene ND cn 0.50 MDL Unit D Prepared Analyzed DII Fac 0.17 ug/L 03/20/23 20:50 1 Prepared Analyzed DH Fac 03/20/23 20:50 1 MDL Unit D Prepared Analyzed Dil Fac 0.070 ug/L 03/18/23 05:53 1 0.080 ug/L 03/18/23 05:53 1 0.10 ug/L 03/18/23 05:53 1 0.080 ug/L 03/18/23 05:53 1 0.10 ug/L 03/18/23 05:53 1 0.10 ug/L 03/18/23 05:53 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 15 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-19 Date Collected: 03/16/23 15:00 Date Received: 03/17/23 10:24 Job ID: 410-119189-1 Lab Sample ID: 410-119189-2 Matrix: Water Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2,3-Trichloropropane ND 1.0 0.10 ug/L 03/18/23 05:53 1 1,2,4-Trichlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:53 1 1,2-Dibromo-3-Chloropropane ND 0.50 0.10 ug/L 03/18/23 05:53 1 1,2-Dibromoethane ND 0.50 0.080 ug/L 03/18/23 05:53 1 1,2-Dichlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:53 1 1,2-Dichloroethane ND 0.50 0.070 ug/L 03/18/23 05:53 1 1,2-Dichloropropane ND 0.50 0.10 ug/L 03/18/23 05:53 1 1,3-Dichlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:53 1 1,4-Dichlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:53 1 2-Butanone ND 5.0 1.0 ug/L 03/18/23 05:53 1 2-Hexanone ND 5.0 0.10 ug/L 03/18/23 05:53 1 4-Methyl-2-pentanone ND 5.0 1.0 ug/L 03/18/23 05:53 1 Acetone 1.1 J 5.0 1.0 ug/L 03/18/23 05:53 1 Acrylonitrile ND cn 5.0 0.40 ug/L 03/18/23 05:53 1 Benzene ND 0.50 0.10 ug/L 03/18/23 05:53 1 Bromochloromethane ND 0.50 0.080 ug/L 03/18/23 05:53 1 Bromodichloromethane ND 0.50 0.080 ug/L 03/18/23 05:53 1 Bromoform ND cn 1.0 0.30 ug/L 03/18/23 05:53 1 Bromomethane ND cn 0.50 0.10 ug/L 03/18/23 05:53 1 Carbon disulfide ND 1.0 0.10 ug/L 03/18/23 05:53 1 Carbon tetrachloride ND 0.50 0.10 ug/L 03/18/23 05:53 1 Chlorobenzene ND 0.50 0.070 ug/L 03/18/23 05:53 1 Chloroethane ND 0.50 0.10 ug/L 03/18/23 05:53 1 Chloroform ND 0.50 0.090 ug/L 03/18/23 05:53 1 Chloromethane ND 0.50 0.10 ug/L 03/18/23 05:53 1 cis-1,2-Dichloroethene ND 0.50 0.080 ug/L 03/18/23 05:53 1 cis-1,3-Dichloropropene ND 0.50 0.10 ug/L 03/18/23 05:53 1 Dibromochloromethane ND 0.50 0.080 ug/L 03/18/23 05:53 1 Dibromomethane ND 0.50 0.080 ug/L 03/18/23 05:53 1 Ethyl methacrylate ND cn 0.50 0.10 ug/L 03/18/23 05:53 1 Ethylbenzene ND 0.50 0.080 ug/L 03/18/23 05:53 1 Methyl iodide ND 0.50 0.080 ug/L 03/18/23 05:53 1 Methylene Chloride ND 0.50 0.10 ug/L 03/18/23 05:53 1 Styrene ND 0.50 0.070 ug/L 03/18/23 05:53 1 Tetrachloroethene ND 0.50 0.20 ug/L 03/18/23 05:53 1 Tetrahydrofuran ND 5.0 0.80 ug/L 03/18/23 05:53 1 Toluene ND 0.50 0.080 ug/L 03/18/23 05:53 1 trans-1,2-Dichloroethene ND 0.50 0.10 ug/L 03/18/23 05:53 1 trans-1,3-Dichloropropene ND cn 0.50 0.080 ug/L 03/18/23 05:53 1 trans-1,4-Dichloro-2-butene ND cn 5.0 2.0 ug/L 03/18/23 05:53 1 Trichooroethene ND 0.50 0.080 ug/L 03/18/23 05:53 1 Trichlorofluoromethane ND 0.50 0.10 ug/L 03/18/23 05:53 1 Vinyl acetate ND cn 1.0 0.30 ug/L 03/18/23 05:53 1 Vinyl chloride ND 0.50 0.10 ug/L 03/18/23 05:53 1 Xylenes, Total ND 1.0 0.070 ug/L 03/18/23 05:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1, 2-Dichloroethane-d4 (Surr) 101 80 - 120 03118123 05:53 1 Dibromocuoromethane (Surr) 99 80 - 120 03/18/23 05:53 1 4-Bromofluorobenzene (Surr) 88 80 - 120 03/18/23 05:53 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 16 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-19 Date Collected: 03/16/23 15:00 Date Received: 03/17/23 10:24 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) Surrogate %Recovery Qualifier Limits Toluene-d8 (Surr) 101 80 - 120 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL 1,2,4, 5-Tetrachlorobenzene ND 2.0 1,2,4-Trich lorobenzene ND 2.0 sym-Trinitrobenzene ND *1 200 1,3-Dinitrobenzene ND 5.1 1,4-Naphthoquinone ND *- *1 cn 100 1,4-phenylenediamine ND *- cn 310 1-Naphthylamine ND 21 2,3,4,6-Tetrachlorophenol ND 5.1 2,4,5-Trichlorophenol ND 2.0 2,4,6-Trichlorophenol ND 2.0 2,4-Dichlorophenol ND 2.0 2,4-Dimethylphenol ND 10 2,4-Dinitrophenol ND *+ cn 31 2,4-Dinitrotol uene ND 5.1 2,6-Dichlorophenol ND 2.0 2,6-Dinitrotol uene ND 2.0 2-Acetylami nofl uorene ND 21 2-Chloronaphthalene ND 1.0 2-Chlorophenol ND 2.0 2-Methylnaphthalene ND 0.51 2-Methylphenol ND 2.0 2-Naphthylamine ND *1 21 2-Nitroaniline ND cn 5.1 2-Nitrophenol ND cn 5.1 3,3'-Dichlorobenzidine ND 10 3,3'-Dimethylbenzidine ND *1 76 3-Methylcholanthrene ND 5.1 3-Nitroaniline ND 5.1 4,6-Dinitro-2-methylphenol ND cn 21 4-Aminobi phenyl ND 11 4-Bromophenyl-phenylether ND 2.0 4-Chloro-3-methyl phenol ND 5.1 4-Chloroan it ine ND 10 4-Chlorophenyl-phenyl ether ND 2.0 4-Methylphenol ND 2.0 4-Nitroaniline ND 3.1 4-Nitrophenol ND 31 5-Nitro-o-toluidine ND 5.1 7,12-Dimethylbenz(a)anthracene ND 5.1 Acenaphthene ND 0.51 Acenaphthylene ND 0.51 Acetophenone ND 5.1 Anthracene ND 0.51 Benzo[a]anthracene ND 0.51 Benzo[a]pyrene ND 0.51 MDL Unit 0.51 ug/L 0.51 ug/L 99 ug/L 1.0 ug/L 25 ug/L 76 ug/L 8.1 ug/L 1.0 ug/L 0.51 ug/L 0.51 ug/L 0.51 ug/L 3.1 ug/L 14 ug/L 1.0 ug/L 0.51 ug/L 0.51 ug/L 10 ug/L 0.41 ug/L 0.51 ug/L 0.10 ug/L 0.51 ug/L 7.1 ug/L 1.0 ug/L 1.0 ug/L 4.1 ug/L 25 ug/L 2.0 ug/L 2.0 ug/L 8.1 ug/L 5.1 ug/L 0.51 ug/L 1.0 ug/L 4.1 ug/L 0.51 ug/L 0.51 ug/L 0.92 ug/L 10 ug/L 2.0 ug/L 2.0 ug/L 0.10 ug/L 0.10 ug/L 1.0 ug/L 0.10 ug/L 0.10 ug/L 0.11 ug/L Job ID: 410-119189-1 Lab Sample ID: 410-119189-2 Matrix: Water Prepared D Prepared 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 03/23/23 08:00 Analyzed Dil Fac 03/18/23 05:53 1 Analyzed 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 03/23/23 20:53 1 1 1 1 L 0 Eurofins Lancaster Laboratories Environment Testing, LLC Page 17 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-19 Date Collected: 03/16/23 15:00 Date Received: 03/17/23 10:24 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Job ID: 410-119189-1 Lab Sample ID: 410-119189-2 Matrix: Water Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Benzo[b]fuoranthene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:53 Benzo[g,h,i]perylene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:53 Benzo[k]fluoranthene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:53 Benzyl alcohol ND 10 4.1 ug/L 03/23/23 08:00 03/23/23 20:53 Bis(2-chloroethoxy)methane ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Bis(2-chloroethyl)ether ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Bis(2-ethylhexyl) phthalate ND cn 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 bis(2 chloro-1-methylethyl) ether ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Butylbenzylphthalate ND cn 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 Chlorobenzilate ND "1 cn 10 3.1 ug/L 03/23/23 08:00 03/23/23 20:53 Chrysene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:53 Di-n-butyl phthalate ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 Di-n-octyl phthalate ND cn 11 5.1 ug/L 03/23/23 08:00 03/23/23 20:53 Diallate (Trans/Cis) ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 Dibenz(a,h)anthracene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:53 Dibenzofuran ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Diethyl phthalate ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 Dimethyl phthalate ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 Ethyl methanesulfonate ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Fluoranthene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:53 Fluorene ND 0.51 0.12 ug/L 03/23/23 08:00 03/23/23 20:53 Hexachlorobenzene ND 0.51 0.11 ug/L 03/23/23 08:00 03/23/23 20:53 Hexachlorobutadiene ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Hexachlorocyclopentadiene ND 11 5.1 ug/L 03/23/23 08:00 03/23/23 20:53 Hexachloroethane ND 5.1 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Hexachloropropene ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 Indeno[1,2,3-cd]pyrene ND 0.51 0.11 ug/L 03/23/23 08:00 03/23/23 20:53 Isodrin ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Isophorone ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Isosafrole ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 Methapyrilene ND 51 15 ug/L 03/23/23 08:00 03/23/23 20:53 Methyl methanesulfonate ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 N-Nitrosodi-n-propylamine ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 N-Nitrosodi-n-butylamine ND 11 5.1 ug/L 03/23/23 08:00 03/23/23 20:53 N-Nitrosodimethylamine ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 N-Nitrosodiethylamine ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 N-Nitrosodiphenylamine ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 N-Nitrosomethylethylamine ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 Famphur ND 51 25 ug/L 03/23/23 08:00 03/23/23 20:53 N-Nitrosopiperidine ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 N-Nitrosopyrrolidine ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Naphthalene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:53 Nitrobenzene ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 o,o',o"-Triethylphosphorothioate ND `- cn 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 o-Toluidine ND 10 4.1 ug/L 03/23/23 08:00 03/23/23 20:53 p-Dimethylamino azobenzene ND 12 5.5 ug/L 03/23/23 08:00 03/23/23 20:53 Pentachlorobenzene ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 Pentachloronitrobenzene ND cn 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 Pentachlorophenol ND 5.1 1.0 ug/L 03/23/23 08:00 03/23/23 20:53 Dil Fac 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 18 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-19 Date Collected: 03/16/23 15:00 Date Received: 03/17/23 10:24 Job ID: 410-119189-1 Lab Sample ID: 410-119189-2 Matrix: Water Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Phenacetin ND cn 5.1 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 1 Phenanthrene ND 0.51 0.11 ug/L 03/23/23 08:00 03/23/23 20:53 1 Phenol ND 2.0 0.51 ug/L 03/23/23 08:00 03/23/23 20:53 1 Kepone ND cn 51 25 ug/L 03/23/23 08:00 03/23/23 20:53 1 Pronamide ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 1 Pyrene ND 0.51 0.10 ug/L 03/23/23 08:00 03/23/23 20:53 1 Safrole, Total ND 5.1 2.0 ug/L 03/23/23 08:00 03/23/23 20:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac C 2,4,6-Tribromophenol (Surf) 83 13 - 138 03/23/23 08.00 03/23/23 20.53 1 2-Fluorobiphenyl (Surr) 75 44 - 120 03/23/23 08:00 03/23/23 20:53 1 2-Fluorophenol (Surr) 39 10 - 120 03/23/23 08:00 03/23/23 20:53 1 Nitrobenzene-d5 (Surr) 71 31 - 120 03/23/23 08:00 03/23/23 20:53 1 p-Terphenyl-d14 (Surr) 66 30 - 125 03/23/23 08:00 03/23/23 20:53 1 Phenol-d5 (Surr) 28 10 - 120 03/23/23 08:00 03/23/23 20:53 1 Method: SW846 8081 B - Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin(1C) ND 0.020 0.0020 ug/L 03/23/23 16:25 03/24/23 07:07 1 alpha-BHC (1C) ND 0.020 0.0030 ug/L 03/23/23 16:25 03/24/23 07:07 1 beta-BHC (1C) ND 0.030 0.011 ug/L 03/23/23 16:25 03/24/23 07:07 1 delta-BHC (1C) ND 0.020 0.0034 ug/L 03/23/23 16:25 03/24/23 07:07 1 Dieldrin (1C) ND 0.030 0.0053 ug/L 03/23/23 16:25 03/24/23 07:07 1 Endosulfan I (1C) ND 0.020 0.0043 ug/L 03/23/23 16:25 03/24/23 07:07 1 Endosulfan II (1C) ND 0.040 0.015 ug/L 03/23/23 16:25 03/24/23 07:07 1 Endosulfan sulfate (1C) ND 0.030 0.0059 ug/L 03/23/23 16:25 03/24/23 07:07 1 Endrin(1C) ND 0.030 0.0082 ug/L 03/23/23 16:25 03/24/23 07:07 1 Endrin aldehyde (1C) ND 0.10 0.020 ug/L 03/23/23 16:25 03/24/23 07:07 1 gamma-BHC (Lindane) (1C) ND 0.020 0.0020 ug/L 03/23/23 16:25 03/24/23 07:07 1 Heptachlor (1C) ND 0.020 0.0020 ug/L 03/23/23 16:25 03/24/23 07:07 1 Heptachlor epoxide (1C) ND 0.020 0.0023 ug/L 03/23/23 16:25 03/24/23 07:07 1 p,p'-DDD (1C) ND 0.030 0.0050 ug/L 03/23/23 16:25 03/24/23 07:07 1 p,p'-DDE (1C) ND 0.030 0.0050 ug/L 03/23/23 16:25 03/24/23 07:07 1 p,p'-DDT (1C) ND 0.030 0.0052 ug/L 03/23/23 16:25 03/24/23 07:07 1 Toxaphene (1C) ND 1.0 0.30 ug/L 03/23/23 16:25 03/24/23 07:07 1 Chlordane (n.o.s.) (1C) ND 0.50 0.16 ug/L 03/23/23 16:25 03/24/23 07:07 1 Methoxychlor (1C) ND 0.11 0.030 ug/L 03/23/23 16:25 03/24/23 07:07 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl (Surr) (1 C) 58 20 - 149 03/23/23 16:25 03/24/23 07:07 1 DCB Decachlorobiphenyl (Surr) (2C) 69 20 - 149 03/23/23 16:25 03/24/23 07:07 1 Tetrachloro-m-xylene (Surr) (1 C) 74 20 - 129 03/23/23 16:25 03/24/23 07:07 1 Tetrachloro-m-xylene (Surr) (2C) 75 20 - 129 03123123 16:25 03/24/23 07:07 1 Method: SW846 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac PCB-1016 (1C) ND 0.25 0.10 ug/L 03/23/23 16:28 03/24/23 10:50 1 PCB-1221 (1C) ND 0.25 0.10 ug/L 03/2312316:28 03/2412310:50 1 PCB-1232 (1C) ND 0.25 0.10 ug/L 03/23/23 16:28 03/24/23 10:50 1 PCB-1242 (1C) ND 0.25 0.10 ug/L 03/23/23 16:28 03/24/23 10:50 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 19 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-19 Date Collected: 03/16/23 15:00 Date Received: 03/17/23 10:24 Method: SW846 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) Analyte Result Qualifier RL MDL Unit D PCB-1248 (1C) ND 0.25 0.079 ug/L PC13-1254 (1C) ND 0.25 0.079 ug/L PCB-1260 (1C) ND 0.25 0.079 ug/L Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl (Surr) (1C) 47 10 - 148 DCB Decachlorobiphenyl (Surr) (2C) 52 10 - 148 Tetrachloro-m-xylene (1C) 71 33- 137 Tetrachloro-m-xylene (2C) 72 33 - 137 Method: SW846 8151A - Herbicides (GC) Analyte Result Qualifier RL MDL Unit D 2,4,5-T(1C) ND 0.15 0.064 ug/L Silvex (2,4,5-TP) (1C) ND 0.049 0.022 ug/L 2,4-Dichlorophenoxyacetic acid (1 C) ND 0.59 0.25 ug/L Dinoseb (1C) ND 0.59 0.28 ug/L Job ID: 410-119189-1 Lab Sample ID: 410-119189-2 Matrix: Water Prepared Analyzed Dil Fac 03/23/2316:28 03/24/2310:50 1 03/23/2316:28 03/24/2310:50 1 03/23/2316:28 03/24/2310:50 1 Prepared Analyzed Dil Fac 0312312316:28 0312412310:50 1 0312312316:28 0312412310:50 1 0312312316:28 0312412310:50 1 0312312316:28 0312412310:50 1 Prepared Analyzed Dil Fac 03/21/23 20:22 03/22/23 12:58 1 03/21 /23 20:22 03/22/23 12:58 1 03/21 /23 20:22 03/22/23 12:58 1 03/21 /23 20:22 03/22/23 12:58 1 Method: SW846 EPA 8141 B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Lab: Eurofins Pittsburgh Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dimethoate (1C) ND on 0.98 0.26 ug/L 03/20/23 18:11 03/22/23 15:15 Disulfoton (1C) ND on 0.98 0.40 ug/L 03/20/23 18:11 03/22/23 15:15 Parathion (1C) ND on 0.98 0.36 ug/L 03/20/23 18:11 03/22/23 15:15 Methyl parathion (1C) ND on 0.98 0.34 ug/L 03/20/23 18:11 03/22/23 15:15 Phorate (1C) ND on 0.98 0.37 ug/L 03/20/23 18:11 03/22/23 15:15 Diethyl-O-pyrazinyl phosphorothioate, ND on 0.98 0.32 ug/L 03/20/23 18:11 03/22/23 15:15 O,O- (1C) Surrogate Tributyl phosphate (1 C) Triphenylphosphate (1C) %Recovery Qualifier 107 on 110 on Method: EPA300.0 R2.1 -Anions, Ion Chromatography Analyte Result Qualifier Sulfate 76 Chloride 3.7 J Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier Antimony ND Arsenic 0.86 J Barium 45 Beryllium 0.50 Cadmium ND Chromium 0.50 J Cobalt 1.7 Copper 0.40 J Iron 4100 Lead 0.20 J Manganese 83 Nickel 2.1 1 1 1 1 1 1 Limits Prepared Analyzed DU Fac 25 - 127 03/20/23 18:11 03/22/23 15:15 1 70 - 155 03/20/23 18:11 03/22/23 15:15 1 RL MDL Unit D Prepared Analyzed Dil Fac 15 5.0 mg/L 03/21/2315:07 10 7.5 3.0 mg/L 03/20/2314:43 5 RL MDL Unit D Prepared Analyzed Dil Fac 1.0 0.20 ug/L 03/22/23 07:17 03/22/23 19:11 1 2.0 0.68 ug/L 03/22/23 07:17 03/22/23 19:11 1 2.0 0.75 ug/L 03/22/23 07:17 03/22/23 19:11 1 0.50 0.12 ug/L 03/22/23 07:17 03/22/23 19:11 1 0.50 0.15 ug/L 03/22/23 07:17 03/22/23 19:11 1 2.0 0.33 ug/L 03/22/23 07:17 03/22/23 19:11 1 0.50 0.16 ug/L 03/22/23 07:17 03/22/23 19:11 1 1.0 0.36 ug/L 03/22/23 07:17 03/22/23 19:11 1 50 20 ug/L 03/22/23 07:17 03/22/23 19:11 1 0.50 0.071 ug/L 03/22/23 07:17 03/22/23 19:11 1 2.0 0.95 ug/L 03/22/23 07:17 03/22/23 19:11 1 1.0 0.40 ug/L 03/22/23 07:17 03/22/23 19:11 1 Page 20 of 63 Eurofins Lancaster Laboratories Environment Testing, LLC 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: MW-19 Date Collected: 03/16/23 15:00 Date Received: 03/17/23 10:24 Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable (Continued) Analyte Result Qualifier RL Selenium ND 1.0 Silver ND 0.50 Thallium ND 0.50 Tin ND 2.0 Vanadium 1.5 J 4.0 Zinc 16 10 Method: SW846 7470A - Mercury (CVAA) Analyte Result Qualifier RL Mercury ND 0.20 General Chemistry Analyte Result Qualifier RL Total Alkalinity as CaCO3 to pH 4.5 8.9 8.0 (SM 2320B-2011) Nitrate as N (EPA 353.2) ND 0.10 Nitrate Nitrite as N (EPA 353.2) ND cn 0.10 Nitrite as N (EPA 353.2) ND 0.050 Sulfide (SM 4500 S2 D-2011) ND 0.30 Cyanide, Total (SW846 9012B) ND 0.010 Total Dissolved Solids (SM 2540C) 130 30 Job ID: 410-119189-1 Lab Sample ID: 410-119189-2 Matrix: Water MDL Unit D Prepared Analyzed Dil Fac 0.28 ug/L 03/22/23 07:17 03/22/23 19:11 1 0.10 ug/L 03/22/23 07:17 03/22/23 19:11 1 0.13 ug/L 03/22/23 07:17 03/22/23 19:11 1 0.60 ug/L 03/22/23 07:17 03/22/23 19:11 1 0.79 ug/L 03/22/23 07:17 03/22/23 19:11 1 4.0 ug/L 03/22/23 07:17 03/22/23 19:11 1 MDL Unit D Prepared Analyzed Dil Fac 0.079 ug/L 03/22/23 08:17 03/22/23 14:58 1 MDL Unit D Prepared Analyzed Dil Fac 2.6 mg/L 03/23/23 03:35 1 0.040 mg/L 03/20/23 07:33 1 0.040 mg/L 03/25/2313:59 1 0.015 mg/L 03/18/23 08:31 1 0.10 mg/L 03/20/2313:32 1 0.0050 mg/L 03/24/2312:00 03/27/2312:07 1 12 mg/L 03/22/23 06:15 1 Client Sample ID: TB-1 Lab Sample ID: 410-119189-3 Date Collected: 03/16/23 00:00 Matrix: Water Date Received: 03/17/23 10:24 Method: SW846 8260D - Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND cn 0.50 0.070 ug/L 03/17/23 23:58 1 1,1,1-Trichloroethane ND 0.50 0.080 ug/L 03/17/23 23:58 1 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/L 03/17/23 23:58 1 1,1,2-Trichloroethane ND 0.50 0.080 ug/L 03/17/23 23:58 1 1,1-Dichloroethane ND 0.50 0.10 ug/L 03/17/23 23:58 1 1,1-Dichloroethene ND cn 0.50 0.10 ug/L 03/17/23 23:58 1 1,2,3-Trichloropropane ND 1.0 0.10 ug/L 03/17/23 23:58 1 1,2,4-Trichlorobenzene ND 0.50 0.070 ug/L 03/17/23 23:58 1 1,2-Dibromo-3-Chloropropane ND 0.50 0.10 ug/L 03/17/23 23:58 1 1,2-Dibromoethane ND 0.50 0.080 ug/L 03/17/23 23:58 1 1,2-Dichlorobenzene ND 0.50 0.070 ug/L 03/17/23 23:58 1 1,2-Dichloroethane ND 0.50 0.070 ug/L 03/17/23 23:58 1 1,2-Dichloropropane ND 0.50 0.10 ug/L 03/17/23 23:58 1 1,3-Dichlorobenzene ND 0.50 0.070 ug/L 03/17/23 23:58 1 1,4-Dichlorobenzene ND 0.50 0.070 ug/L 03/17/23 23:58 1 2-Butanone ND 5.0 1.0 ug/L 03/17/23 23:58 1 2-Hexanone ND 5.0 0.10 ug/L 03/17/23 23:58 1 4-Methyl-2-pentanone ND 5.0 1.0 ug/L 03/17/23 23:58 1 Acetone ND 5.0 1.0 ug/L 03/17/23 23:58 1 Acrylonitrile ND cn 5.0 0.40 ug/L 03/17/23 23:58 1 Benzene ND 0.50 0.10 ug/L 03/17/23 23:58 1 Bromochloromethane ND 0.50 0.080 ug/L 03/17/23 23:58 1 Bromodichloromethane ND 0.50 0.080 ug/L 03/17/23 23:58 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 21 of 63 3/30/2023 Client Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Client Sample ID: TB-1 Date Collected: 03/16/23 00:00 Date Received: 03/17/23 10:24 Job ID: 410-119189-1 Lab Sample ID: 410-119189-3 Matrix: Water Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Bromoform ND cn 1.0 0.30 ug/L 03/17/23 23:58 1 Bromomethane ND cn 0.50 0.10 ug/L 03/17/23 23:58 1 Carbon disulfide ND 1.0 0.10 ug/L 03/17/23 23:58 1 Carbon tetrachloride ND 0.50 0.10 ug/L 03/17/23 23:58 1 Chlorobenzene ND 0.50 0.070 ug/L 03/17/23 23:58 1 Chloroethane ND 0.50 0.10 ug/L 03/17/23 23:58 1 Chloroform ND 0.50 0.090 ug/L 03/17/23 23:58 1 Chloromethane ND 0.50 0.10 ug/L 03/17/23 23:58 1 cis-1,2-Dichloroethene ND 0.50 0.080 ug/L 03/17/23 23:58 1 cis-1,3-Dichloropropene ND 0.50 0.10 ug/L 03/17/23 23:58 1 Dibromochloromethane ND 0.50 0.080 ug/L 03/17/23 23:58 1 Dibromomethane ND 0.50 0.080 ug/L 03/17/23 23:58 1 Ethyl methacrylate ND cn 0.50 0.10 ug/L 03/17/23 23:58 1 Ethylbenzene ND 0.50 0.080 ug/L 03/17/23 23:58 1 Methyl iodide ND 0.50 0.080 ug/L 03/17/23 23:58 1 Methylene Chloride ND 0.50 0.10 ug/L 03/17/23 23:58 1 Styrene ND 0.50 0.070 ug/L 03/17/23 23:58 1 Tetrachloroethene ND 0.50 0.20 ug/L 03/17/23 23:58 1 Tetrahydrofuran ND 5.0 0.80 ug/L 03/17/23 23:58 1 Toluene ND 0.50 0.080 ug/L 03/17/23 23:58 1 trans-1,2-Dichloroethene ND 0.50 0.10 ug/L 03/1712323:58 1 trans-1,3-Dichloropropene ND cn 0.50 0.080 ug/L 03/1712323:58 1 trans-1,4-Dichloro-2-butene ND cn 5.0 2.0 ug/L 03/17/23 23:58 1 Trichooroethene ND 0.50 0.080 ug/L 03/17/23 23:58 1 Trichlorofluoromethane ND 0.50 0.10 ug/L 03/17/23 23:58 1 Vinyl acetate ND cn 1.0 0.30 ug/L 03/17/23 23:58 1 Vinyl chloride ND 0.50 0.10 ug/L 03/17/23 23:58 1 Xylenes, Total ND 1.0 0.070 ug/L 03/17/23 23:58 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1, 2-Dichloroethane-d4 (Surr) 106 80 - 120 03/17/23 23:58 1 Dibromofluoromethane (Surr) 102 80 - 120 03/17/23 23:58 1 4-Bromofluorobenzene (Surr) 83 80 - 120 03/17/23 23:58 1 Toluene-d8 (Surr) 101 80 - 120 03117123 23:58 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 22 of 63 3/30/2023 Surrogate Summary Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Method: 8260D - Volatile Organic Compounds by GC/MS Matrix: Water Prep Type: Total/NA Percent Surrogate Recovery (Acceptance Limits) DCA DBFM BFB TOL Lab Sample ID Client Sample ID (80-120) (80-120) (80-120) (80-120) 410-119189-1 MW-18 100 96 88 101 410-119189-2 MW-19 101 99 88 101 410-119189-3 TB-1 106 102 83 101 LCS 410-354854/5 Lab Control Sample 110 100 97 103 LCS 410-354854/6 Lab Control Sample 105 100 87 101 LCSD 410-354854/7 Lab Control Sample Dup 104 100 86 102 MB 410-354854/10 Method Blank 105 103 90 104 Surrogate Legend DCA= 1,2-Dichloroethane-d4 (Surr) DBFM = Dibromofluoromethane (Surr) BFB = 4-Bromofluorobenzene (Surr) TOL = Toluene-d8 (Surr) Method: 8260D SIM 14D - Volatile Organic Compounds (GC/MS) Matrix: Water Prep Type: Total/NA Percent Surrogate Recovery (Acceptance Limits) TOL Lab Sample ID Client Sample ID (80-120) 410-119189-1 MW-18 104 410-119189-2 MW-19 105 LCS 410-355251/4 Lab Control Sample 104 MB 410-355251/6 Method Blank 104 Surrogate Legend TOL = Toluene-d8 (Surr) Method: 8270E - Semivolatile Organic Compounds (GC/MS) Matrix: Water Prep Type: Total/NA Lab Sample ID Client Sample ID TBP (13-138) FBP ("-120) Percent Surrogate Recovery (Acceptance Limits) 2FP NBZ TPHd14 PHL (10-120) (31-120) (30-125) (10-120) 410-119189-1 MW-18 84 84 40 69 81 28 410-119189-2 MW-19 83 75 39 71 66 28 LCS 410-356549/2-A Lab Control Sample 87 85 53 69 83 38 LCS 410-356549/3-A Lab Control Sample 86 79 48 78 89 35 LCSD 410-356549/4-A Lab Control Sample Dup 77 69 48 62 88 37 MB 410-356549/1-A Method Blank 78 73 40 66 84 29 Surrogate Legend TBP = 2,4,6-Tribromophenol (Surr) FBP = 2-Fluorobiphenyl (Surr) 2FP = 2-Fluorophenol (Surr) NBZ = Nitrobenzene-d5 (Surr) TPHd14 = p-Terphenyl-d14 (Surr) PHL = Phenol-d5 (Surr) Eurofins Lancaster Laboratories Environment Testing, LLC Page 23 of 63 3/30/2023 Surrogate Summary Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Method: 8081 B - Organochlorine Pesticides (GC) Matrix: Water F Job ID: 410-119189-1 Prep Type: Total/NA Lab Sample ID Client Sample ID DCB1 (20-149) DCB2 (20-149) Percent Surrogate Recovery (Acceptance Limits) TCX1 TCX2 (20-129) (20-129) 410-119189-1 MW-18 37 48 57 59 410-119189-2 MW-19 58 69 74 75 LCS 410-356826/2-A Lab Control Sample 92 110 81 76 LCSD 410-356826/3-A Lab Control Sample Dup 94 116 74 73 MB 410-356826/1-A Method Blank 94 107 74 73 Surrogate Legend DCB = DCB Decachlorobiphenyl (Surr) TCX = Tetrachloro-m-xylene (Surr) Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Matrix: Water Prep Type: Total/NA Percent Surrogate Recovery (Acceptance Limits) DCB1 DC132 TCX1 TCX2 Lab Sample ID Client Sample ID (10-148) (10-148) (33-137) (33-137) 410-119189-1 MW-18 35 36 58 60 410-119189-2 MW-19 47 52 71 72 LCS 410-356828/2-A Lab Control Sample 32 34 63 64 LCSD 410-356828/3-A Lab Control Sample Dup 27 28 53 52 MB 410-356828/1-A Method Blank 69 73 63 63 Surrogate Legend DCB = DCB Decachlorobiphenyl (Surr) TCX = Tetrachloro-m-xylene Method: EPA 8141 B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Matrix: Water Prep Type: Total/NA Percent Surrogate Recovery (Acceptance Limits) Lab Sample ID Client Sample ID TBPH2 (25-127) TPP1 (70-155) 410-119189-1 MW-18 107 cn 111 cn LCS 180-429800/2-A Lab Control Sample 115 111 Surrogate Legend TBPH = Tributyl phosphate TPP = Triphenyl phosphate Method: EPA 8141 B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Matrix: Water Prep Type: Total/NA TBPH1 TPP1 Lab Sample ID Client Sample ID (25-127) (70-155) 410-119189-2 MW-19 107 cn 110 cn MB 180-429800/1-A Method Blank 84 109 Surrogate Legend TBPH = Tributyl phosphate TPP = Triphenyl phosphate Percent Surrogate Recovery (Acceptance Limits) Eurofins Lancaster Laboratories Environment Testing, LLC Page 24 of 63 3/30/2023 Surrogate Summary Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Method: EPA 8141 B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Matrix: Water Prep Type: Total/NA Percent Surrogate Recovery (Acceptance Limits) TBPH2 TPP2 Lab Sample ID Client Sample ID (25-127) (70.155) LCSD 180-429800/3-A Lab Control Sample Dup 114 110 Surrogate Legend TBPH = Tributyl phosphate TPP = Triphenyl phosphate Eurofins Lancaster Laboratories Environment Testing, LLC Page 25 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Method: 8260D - Volatile Organic Compounds by GUMS Lab Sample ID: MB 410-354854/10 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 354854 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 0.50 0.070 ug/L 03/17/23 22:07 1 1,1,1-Trichloroethane ND 0.50 0.080 ug/L 03/17/23 22:07 1 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/L 03/17/23 22:07 1 1,1,2-Trichloroethane ND 0.50 0.080 ug/L 03/17/23 22:07 1 1,1-Dichloroethane ND 0.50 0.10 ug/L 03/17/23 22:07 1 • 1,1-Dichloroethene ND 0.50 0.10 ug/L 03/17/23 22:07 1 1,2,3-Trichloropropane ND 1.0 0.10 ug/L 03/17/23 22:07 1 1,2,4-Trichlorobenzene ND 0.50 0.070 ug/L 03/17/23 22:07 1 1,2-Dibromo-3-Chloropropane ND 0.50 0.10 ug/L 03/17/23 22:07 1 1,2-Dibromoethane ND 0.50 0.080 ug/L 03/17/23 22:07 1 1,2-Dichlorobenzene ND 0.50 0.070 ug/L 03/17/23 22:07 1 1,2-Dichloroethane ND 0.50 0.070 ug/L 03/17/23 22:07 1 1,2-Dichloropropane ND 0.50 0.10 ug/L 03/17/23 22:07 1 1,3-Dichlorobenzene ND 0.50 0.070 ug/L 03/17/23 22:07 1 1,4-Dichlorobenzene ND 0.50 0.070 ug/L 03/17/23 22:07 1 2-Butanone ND 5.0 1.0 ug/L 03/17/23 22:07 1 2-Hexanone ND 5.0 0.10 ug/L 03/17/23 22:07 1 4-Methyl-2-pentanone ND 5.0 1.0 ug/L 03/17/23 22:07 1 Acetone ND 5.0 1.0 ug/L 03/17/23 22:07 1 Acrylonitrile ND 5.0 0.40 ug/L 03/17/23 22:07 1 Benzene ND 0.50 0.10 ug/L 03/17/23 22:07 1 Bromochloromethane ND 0.50 0.080 ug/L 03/17/23 22:07 1 Bromodichloromethane ND 0.50 0.080 ug/L 03/17/23 22:07 1 Bromoform ND 1.0 0.30 ug/L 03/17/23 22:07 1 Bromomethane ND 0.50 0.10 ug/L 03/17/23 22:07 1 Carbon disulfide ND 1.0 0.10 ug/L 03/17/23 22:07 1 Carbon tetrachloride ND 0.50 0.10 ug/L 03/17/23 22:07 1 Chlorobenzene ND 0.50 0.070 ug/L 03/17/23 22:07 1 Chloroethane ND 0.50 0.10 ug/L 03/17/23 22:07 1 Chloroform ND 0.50 0.090 ug/L 03/17/23 22:07 1 Chloromethane ND 0.50 0.10 ug/L 03/17/23 22:07 1 cis-1,2-Dichloroethene ND 0.50 0.080 ug/L 03/17/23 22:07 1 cis- 1,3-Dichloropropene ND 0.50 0.10 ug/L 03/17/23 22:07 1 Dibromochloromethane ND 0.50 0.080 ug/L 03/17/23 22:07 1 Dibromomethane ND 0.50 0.080 ug/L 03/17/23 22:07 1 Ethyl methacrylate ND 0.50 0.10 ug/L 03/17/23 22:07 1 Ethylbenzene ND 0.50 0.080 ug/L 03/17/23 22:07 1 Methyl iodide ND 0.50 0.080 ug/L 03/17/23 22:07 1 Methylene Chloride ND 0.50 0.10 ug/L 03/17/23 22:07 1 Styrene ND 0.50 0.070 ug/L 03/17/23 22:07 1 Tetrachloroethene ND 0.50 0.20 ug/L 03/17/23 22:07 1 Tetrahydrofuran ND 5.0 0.80 ug/L 03/17/23 22:07 1 Toluene ND 0.50 0.080 ug/L 03/17/23 22:07 1 trans- 1,2-Dichloroethene ND 0.50 0.10 ug/L 03/17/23 22:07 1 trans- 1,3-Dichloropropene ND 0.50 0.080 ug/L 03/17/23 22:07 1 trans- 1,4-Dichloro-2-butene ND 5.0 2.0 ug/L 03/17/23 22:07 1 Trichloroethene ND 0.50 0.080 ug/L 03/17/23 22:07 1 Trichlorofluoromethane ND 0.50 0.10 ug/L 03/17/23 22:07 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 26 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Job ID: 410-119189-1 Method: 8260D - Volatile Organic Compounds by GUMS (Continued) Lab Sample ID: MB 410-354854/10 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 354854 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac Vinyl acetate ND 1.0 0.30 ug/L 03/17/23 22:07 1 Vinyl chloride ND 0.50 0.10 ug/L 03/17/23 22:07 1 Xylenes, Total ND 1.0 0.070 ug/L 03/17/23 22:07 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 105 80- 120 03/17/23 22:07 1 Dibromofluoromethane (Surr) 103 80 - 120 03/17/23 22:07 1 4-Bromofluorobenzene (Surr) 90 80 - 120 03/17/23 22:07 1 Toluene-d8 (Surr) 104 80 - 120 03117123 22:07 1 Lab Sample ID: LCS 410-354854/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 354854 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits 1,1,1,2-Tetrachloroethane 5.20 5.45 ug/L 105 71 - 134 1,1,1-Trichloroethane 5.20 5.06 ug/L 97 78-126 1,1,2,2-Tetrachloroethane 5.20 6.37 ug/L 122 75-123 1,1,2-Trichloroethane 5.20 5.84 ug/L 112 80-120 1,1-Dichloroethane 5.20 5.57 ug/L 107 74-120 1,1-Dichloroethene 5.20 4.28 ug/L 82 80-131 1,2,3-Trichloropropane 5.20 5.92 ug/L 114 80 - 125 1,2,4-Trichlorobenzene 5.20 4.48 ug/L 86 68-122 1,2-Dibromo-3-Chloropropane 5.20 5.04 ug/L 97 56 - 148 1,2-Dibromoethane 5.20 5.86 ug/L 113 80 - 120 1,2-Dichlorobenzene 5.20 5.17 ug/L 99 80 - 120 1,2-Dichloroethane 5.20 6.29 ug/L 121 69-122 1,2-Dichloropropane 5.20 6.00 ug/L 115 80 - 120 1,3-Dichlorobenzene 5.20 4.92 ug/L 95 80 - 120 1,4-Dichlorobenzene 5.20 5.02 ug/L 97 80 - 120 2-Butanone 65.0 66.8 ug/L 103 59 - 141 2-Hexanone 65.0 63.0 ug/L 97 52 - 140 4-Methyl-2-pentanone 65.0 65.1 ug/L 100 55 - 140 Acetone 65.0 66.4 ug/L 102 60 - 146 Acrylonitrile 26.0 24.0 ug/L 92 64 - 139 Benzene 5.20 5.47 ug/L 105 80 - 120 Bromochloromethane 5.20 5.25 ug/L 101 80 - 120 Bromodichloromethane 5.20 5.90 ug/L 113 73 - 124 Bromoform 5.20 5.69 ug/L 109 49 - 144 Bromomethane 5.20 4.51 ug/L 87 60 - 136 Carbon disulfide 5.20 5.66 ug/L 109 67 - 130 Carbon tetrachloride 5.20 5.04 ug/L 97 64 - 141 Chlorobenzene 5.20 5.32 ug/L 102 80 - 120 Chloroethane 5.20 5.05 ug/L 97 63 - 120 Chloroform 5.20 5.49 ug/L 106 80 - 120 Chloromethane 5.20 5.10 ug/L 98 56 - 124 cis-1,2-Dichloroethene 5.20 5.24 ug/L 101 80 - 122 cis- 1,3-Dichloropropene 5.20 5.54 ug/L 107 67-121 Eurofins Lancaster Laboratories Environment Testing, LLC Page 27 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Method: 8260D - Volatile Organic Compounds by GUMS (Continued) Lab Sample ID: LCS 410-354854/5 Matrix: Water Analysis Batch: 354854 Spike LCS LCS Analyte Added Result Qualifier Unit Dibromochloromethane 5.20 5.68 ug/L Dibromomethane 5.20 5.85 ug/L Ethyl methacrylate 5.20 5.92 ug/L Ethylbenzene 5.20 5.48 ug/L Methyl iodide 5.20 4.66 ug/L Methylene Chloride 5.20 5.28 ug/L Styrene 5.20 5.19 ug/L Tetrachloroethene 5.20 4.78 ug/L Tetrahydrofuran 26.0 21.7 ug/L Toluene 5.20 5.38 ug/L trans- 1,2-Dichloroethene 5.20 4.85 ug/L trans- 1,3-Dichloropropene 5.20 6.02 ug/L trans- 1,4-Dichloro-2-butene 26.0 24.7 ug/L Trichloroethene 5.20 5.12 ug/L Trichlorofluoromethane 5.20 3.76 ug/L Vinyl chloride 5.20 4.67 ug/L Xylenes, Total 15.6 15.7 ug/L LCS LCS surrogate %Recovery Qualifier Limits ',2-Dichloroethane-d4 (Surr) 110 80 - 120 Xbromofluoromethane (Surr) 100 80 - 120 I-Bromofluorobenzene (Surr) 97 80 - 120 oluene-d8 (Surr) 103 80 - 120 -ab Sample ID: LCS 410-354854/6 Matrix: Water 4nalysis Batch: 354854 \nalyte /inyl acetate LCS LCS Surrogate %Recovery Qualifier 1,2-Dichloroethane-d4 (Surr) 105 Dibromofluoromethane (Surr) 100 4-Bromofluorobenzene (Surr) 87 Toluene-d8 (Surr) 101 Spike Added 12.5 Limits 80. 120 80. 120 80. 120 80 - 120 LCS LCS Result Qualifier Unit 16.8 ug/L F Job ID: 410-119189-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA D %Rec %Rec Limits 109 64-138 113 80 _ 122 114 55.133 105 80.120 90 77.120 102 80 _ 120 100 80 _ 120 92 80 _ 120 83 67.137 103 80 - 120 93 80 - 122 116 61 - 129 95 10. 172 98 80. 120 72 62. 136 90 60 _ 125 101 80 _ 120 Client Sample ID: Lab Control Sample Prep Type: Total/NA %Rec D %Rec Limits 135 38-145 Lab Sample ID: LCSD 410-354854/7 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 354854 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Vinyl acetate 12.5 16.6 ug/L 132 38 - 145 2 30 LCSD LCSD Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Surr) 104 80. 120 Dibromofluoromethane (Surr) 100 80. 120 4-Bromofluorobenzene (Surr) 86 80. 120 Eurofins Lancaster Laboratories Environment Testing, LLC Page 28 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Job ID: 410-119189-1 Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: LCSD 410-354854/7 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 354854 LCSD LCSD Surrogate %Recovery Qualifier Limits Toluene-d8 (Surr) 102 80 - 120 Method: 8260D SIM 14D - Volatile Organic Compounds (GC/MS) Lab Sample ID: MB 410-355251/6 Matrix: Water Analysis Batch: 355251 Analyte 1,4-Dioxane Surrogate Toluene-d8 (Surr) Lab Sample ID: LCS 410-355251/4 Matrix: Water Analysis Batch: 355251 Analyte 1,4-Dioxane Client Sample ID: Method Blank Prep Type: Total/NA MB Result MB Qualifier RL MDL Unit D Prepared Analyzed Dil Fac ND 0.40 0.17 ug/L 03/20/2311:48 1 MB MB %Recovery Qualifier Limits Prepared Analyzed Dil Fac 104 80 - 120 03120123 11:48 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec Added Result Qualifier Unit D %Rec Limits 5.06 5.63 ug/L ill 74 - 133 LCS LCS Surrogate %Recovery Qualifier Limits Toluene-d8 (Surr) 104 80 - 120 Method: 8270E - Semivolatile Organic Compounds (GC/MS) Lab Sample ID: MB 410-356549/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 356887 Prep Batch: 356549 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2,4,5-Tetrachlorobenzene ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 sym-Trinitrobenzene ND 200 97 ug/L 03/23/23 08:00 03/23/23 19:13 1 1,3-Dinitrobenzene ND 5.0 1.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 1,4-Naphthoquinone ND 100 25 ug/L 03/23/23 08:00 03/23/23 19:13 1 1,4-phenylenediamine ND 300 75 ug/L 03/23/23 08:00 03/23/23 19:13 1 1-Naphthylamine ND 21 8.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 2,3,4,6-Tetrachlorophenol ND 5.0 1.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 2,4,5-Trichlorophenol ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 2,4,6-Trichlorophenol ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 2,4-Dichlorophenol ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 2,4-Dimethyl phenol ND 10 3.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 2,4-Dinitrophenol ND 30 14 ug/L 03/23/23 08:00 03/23/23 19:13 1 2,4-Dinitrotoluene ND 5.0 1.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 2,6-Dichlorophenol ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 2,6-Dinitrotoluene ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 2-Acetylaminofluorene ND 21 10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 29 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Job ID: 410-119189-1 Lab Sample ID: MB 410-356549/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 356887 Prep Batch: 356549 MB MB Analyte Result Qualifier RL MDL unit D Prepared Analyzed Dil Fac 2-Chloronaphthalene ND 1.0 0.40 ug/L 03/23/23 08:00 03/23/23 19:13 1 2-Chlorophenol ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 2-Methylnaphthalene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 2-Methylphenol ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 2-Naphthylamine ND 21 7.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 2-Nitroaniline ND 5.0 1.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 2-Nitrophenol ND 5.0 1.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 3,3'-Dichlorobenzidine ND 10 4.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 3,3'-Dimethylbenzidine ND 75 25 ug/L 03/23/23 08:00 03/23/23 19:13 1 3-Methylcholanthrene ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 3-Nitroaniline ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 4,6-Dinitro-2-methylphenol ND 21 8.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 4-Aminobiphenyl ND 11 5.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 4-Bromophenyl-phenylether ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 4-Chloro-3-methylphenol ND 5.0 1.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 4-Chloroaniline ND 10 4.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 4-Chlorophenyl-phenyl ether ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 4-Methylphenol ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 4-Nitroaniline ND 3.0 0.90 ug/L 03/23/23 08:00 03/23/23 19:13 1 4-Nitrophenol ND 30 10 ug/L 03/23/23 08:00 03/23/23 19:13 1 5-Nitro-o-toluidine ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 7,12-Dimethylbenz(a)anthracene ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Acenaphthene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Acenaphthylene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Acetophenone ND 5.0 1.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Anthracene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Benzo[a]anthracene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Benzo[a]pyrene ND 0.50 0.11 ug/L 03/23/23 08:00 03/23/23 19:13 1 Benzo[b]fuoranthene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Benzo[g,h,i]perylene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Benzo[k]fluoranthene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Benzyl alcohol ND 10 4.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Bis(2-chloroethoxy)methane ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Bis(2-chloroethyl)ether ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Bis(2-ethylhexyl) phthalate ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 bis(2 chloro-1-methylethyl) ether ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Butylbenzylphthalate ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Chlorobenzilate ND 10 3.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Chrysene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Di-n-butyl phthalate ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Di-n-octyl phthalate ND 11 5.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Diallate (Trans/Cis) ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Dibenz(a,h)anthracene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Dibenzofuran ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Diethyl phthalate ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Dimethyl phthalate ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Ethyl methanesulfonate ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Fluoranthene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Fluorene ND 0.50 0.12 ug/L 03/23/23 08:00 03/23/23 19:13 1 0 Eurofins Lancaster Laboratories Environment Testing, LLC Page 30 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Job ID: 410-119189-1 Lab Sample ID: MB 410-356549/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 356887 Prep Batch: 356549 MB MB Analyte Result Qualifier RL MDL unit D Prepared Analyzed Dil Fac Hexachlorobenzene ND 0.50 0.11 ug/L 03/23/23 08:00 03/23/23 19:13 1 Hexachlorobutadiene ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Hexachlorocyclopentadiene ND 11 5.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Hexachloroethane ND 5.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Hexachloropropene ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Indeno[1,2,3-cd]pyrene ND 0.50 0.11 ug/L 03/23/23 08:00 03/23/23 19:13 1 Isodrin ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Isophorone ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Isosafrole ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Methapyrilene ND 50 15 ug/L 03/23/23 08:00 03/23/23 19:13 1 Methyl methanesulfonate ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 N-Nitrosodi-n-propylamine ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 N-Nitrosodi-n-butylamine ND 11 5.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 N-Nitrosodimethylamine ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 N-Nitrosodiethylamine ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 N-Nitrosodiphenylamine ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 N-Nitrosomethylethylamine ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Famphur ND 50 25 ug/L 03/23/23 08:00 03/23/23 19:13 1 N-Nitrosopiperidine ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 N-Nitrosopyrrolidine ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Naphthalene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Nitrobenzene ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 o,o',o"-Triethylphosphorothioate ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 o-Toluidine ND 10 4.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 p-Dimethylamino azobenzene ND 12 5.4 ug/L 03/23/23 08:00 03/23/23 19:13 1 Pentachlorobenzene ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Pentachloronitrobenzene ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Pentachlorophenol ND 5.0 1.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Phenacetin ND 5.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Phenanthrene ND 0.50 0.11 ug/L 03/23/23 08:00 03/23/23 19:13 1 Phenol ND 2.0 0.50 ug/L 03/23/23 08:00 03/23/23 19:13 1 Kepone ND 50 25 ug/L 03/23/23 08:00 03/23/23 19:13 1 Pronamide ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 Pyrene ND 0.50 0.10 ug/L 03/23/23 08:00 03/23/23 19:13 1 Safrole, Total ND 5.0 2.0 ug/L 03/23/23 08:00 03/23/23 19:13 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 2,4,6-Tribromophenol(Surr) 78 13-138 0312312308:00 0312312319:13 1 2-Fluorobiphenyl (Surr) 73 44 - 120 03/23/23 08:00 03/23/23 19:13 1 2-Fluorophenol (Surr) 40 10 - 120 03/23/23 08:00 03/23/23 19:13 1 Nitrobenzene-d5 (Surr) 66 31 - 120 03/23/23 08:00 03/23/23 19:13 1 p-Terphenyl-04 (Surr) 84 30 - 125 03/23/23 08:00 03/23/23 19:13 1 Phenol-d5 (Surr) 29 10 - 120 03/23/23 08:00 03/23/23 19:13 1 0 Eurofins Lancaster Laboratories Environment Testing, LLC Page 31 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 410-356549/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 356887 Prep Batch: 356549 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits 1,2,4,5-Tetrachlorobenzene 50.0 40.1 ug/L 80 34 - 120 1,2,4-Trichlorobenzene 50.0 38.0 ug/L 76 34 - 120 1,3-Dinitrobenzene 50.0 52.5 ug/L 105 61 - 125 2,3,4,6-Tetrachlorophenol 50.0 45.3 ug/L 91 60 - 126 2,4,5-Trichlorophenol 50.0 48.3 ug/L 97 60 - 136 2,4,6-Trichlorophenol 50.0 46.5 ug/L 93 63 - 133 2,4-Dichlorophenol 50.0 42.9 ug/L 86 60 - 127 2,4-Dimethyl phenol 50.0 39.8 ug/L 80 62 _ 120 2,4-Dinitrophenol 100 151 *+ ug/L 151 36 - 147 2,4-Dinitrotoluene 50.0 53.4 ug/L 107 66 - 131 2,6-Dichlorophenol 50.0 44.8 ug/L 90 65 - 120 2,6-Dinitrotoluene 50.0 51.5 ug/L 103 66 - 129 2-Chloronaphthalene 50.0 45.7 ug/L 91 51 - 120 2-Chlorophenol 50.0 43.5 ug/L 87 57 - 120 2-Methylnaphthalene 50.0 44.1 ug/L 88 53 - 120 2-Methylphenol 50.0 42.5 ug/L 85 58 - 120 2-Nitroaniline 50.0 58.5 ug/L 117 63 - 134 2-Nitrophenol 50.0 54.8 ug/L 110 57 - 127 3,3'-Dichlorobenzidine 100 66.0 ug/L 66 31 - 120 3-Nitroaniline 50.0 49.9 ug/L 100 44 - 125 4,6-Dinitro-2-methyl phenol 100 148 ug/L 148 54 - 148 4-Bromophenyl-phenylether 50.0 40.6 ug/L 81 66 - 120 4-Chloro-3-methyl phenol 50.0 41.0 ug/L 82 57. 129 4-Chloroaniline 50.0 30.9 ug/L 62 33 - 120 4-Chlorophenyl-phenyl ether 50.0 42.1 ug/L 84 59 - 120 4-Methylphenol 50.0 37.7 ug/L 75 49 - 120 4-Nitroaniline 50.0 47.8 ug/L 96 55 - 126 4-Nitrophenol 100 72.5 ug/L 72 17 - 120 Acenaphthene 50.0 47.1 ug/L 94 59 - 120 Acenaphthylene 50.0 47.6 ug/L 95 61 - 121 Acetophenone 50.0 40.4 ug/L 81 60 - 120 Anthracene 50.0 45.8 ug/L 92 67 - 123 Benzo[a]anthracene 50.0 44.9 ug/L 90 66 - 133 Benzo[a]pyrene 50.0 45.7 ug/L 91 64 - 131 Benzo[b]fluoranthene 50.0 45.5 ug/L 91 64 - 124 Benzo[g,h,i]perylene 50.0 51.7 ug/L 103 60 - 136 Benzo[k]fluoranthene 50.0 49.3 ug/L 99 67. 132 Benzyl alcohol 50.0 35.0 ug/L 70 33 - 136 Bis(2-chloroethoxy)methane 50.0 37.1 ug/L 74 61 _ 123 Bis(2-chloroethyl)ether 50.0 36.4 ug/L 73 62 - 120 Bis(2-ethylhexyl) phthalate 50.0 61.8 ug/L 124 60 - 133 bis(2 chloro-1-methylethyl) ether 50.0 38.8 ug/L 78 43 - 121 Butylbenzylphthalate 50.0 61.9 ug/L 124 30 - 128 Chrysene 50.0 46.5 ug/L 93 70 - 128 Di-n-butyl phthalate 50.0 53.5 ug/L 107 58 - 132 Di-n-octyl phthalate 50.0 68.8 E ug/L 138 52 - 146 Dibenz(a,h)anthracene 50.0 51.0 ug/L 102 59 - 135 Dibenzofuran 50.0 45.3 ug/L 91 63 - 120 0 Eurofins Lancaster Laboratories Environment Testing, LLC Page 32 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill INC Job ID: 410-119189-1 Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 410-356549/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 356887 Prep Batch: 356549 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Diethyl phthalate 50.0 49.7 ug/L 99 46 - 123 Dimethyl phthalate 50.0 44.2 ug/L 88 10 - 135 Fluoranthene 50.0 44.4 ug/L 89 70 - 128 Fluorene 50.0 46.6 ug/L 93 66 - 120 Hexachlorobenzene 50.0 45.9 ug/L 92 61 - 126 Hexachlorobutadiene 50.0 32.8 ug/L 66 10 - 120 Hexachlorocyclopentadiene 50.0 32.0 ug/L 64 10 - 120 Hexachloroethane 50.0 37.2 ug/L 74 16 - 120 Indeno[1,2,3-cd]pyrene 50.0 48.7 ug/L 97 55-134 Isophorone 50.0 36.1 ug/L 72 63 - 124 N-Nitrosodi-n-propylamine 50.0 36.7 ug/L 73 57 - 120 N-Nitrosodimethylamine 50.0 23.7 ug/L 47 26 - 120 N-Nitrosodiphenylamine 42.5 42.0 ug/L 99 64 - 130 Naphthalene 50.0 39.4 ug/L 79 55 - 120 Nitrobenzene 50.0 37.0 ug/L 74 59 - 120 Pentachlorophenol 100 102 ug/L 102 51 - 138 Phenanthrene 50.0 45.4 ug/L 91 66 - 120 Phenol 50.0 24.9 ug/L 50 22 - 120 Pyrene 50.0 51.1 ug/L 102 67 - 126 Surrogate LCS LCS %Recovery Qualifier Limits 2, 4, 6-Tribromophenol (Surr) 87 13 - 138 2-Fluorobiphenyl (Surr) 85 44 - 120 2-Fluorophenol (Surr) 53 10 - 120 Nitrobenzene-d5 (Surr) 69 31 - 120 p-Terphenyl-d14 (Surr) 83 30 - 125 Phenol-d5 (Surr) 38 10 - 120 Lab Sample ID: LCS 410-356549/3-A Matrix: Water Analysis Batch: 356887 Analyte Spike Added LCS LCS Result Qualifier Unit sym-Trinitrobenzene 50.0 ND ug/L 1,4-Naphthoquinone 100 ND *- ug/L 1,4-phenylenediamine 1100 ND *- ug/L 1-Naphthylamine 50.0 27.5 ug/L 2-Acetylaminofluorene 50.0 57.0 ug/L 2-Naphthylamine 50.0 32.5 ug/L 3,3'-Dimethylbenzidine 50.0 ND ug/L 3-Methylcholanthrene 50.0 43.6 ug/L 4-Aminobiphenyl 50.0 25.9 ug/L 5-Nitro-o-toluidine 50.0 44.8 ug/L 7,12-Dimethylbenz(a)anth racene 50.0 41.7 ug/L Chlorobenzilate 50.0 60.1 ug/L Diallate (Trans/Cis) 50.0 41.7 ug/L Ethyl methanesulfonate 50.0 33.7 ug/L Hexachloropropene 50.0 24.5 ug/L Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 356549 %Rec D %Rec Limits 83 10 - 120 5 10 - 120 2 10 - 120 55 10 - 120 114 63 - 130 65 30 - 120 44 10 - 120 87 61 - 121 52 10 - 120 90 51 - 120 83 71 - 120 120 10-120 83 60 - 120 67 61 - 120 49 10 - 120 Eurofins Lancaster Laboratories Environment Testing, LLC Page 33 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 410-356549/3-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 356887 Prep Batch: 356549 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Isodrin 50.0 42.4 ug/L 85 58 - 120 Isosafrole 50.0 41.6 ug/L 83 66 - 120 Methapyrilene 100 67.9 ug/L 68 10 - 120 Methyl methanesulfonate 50.0 28.1 ug/L 56 38 - 120 N-Nitrosodi-n-butylamine 50.0 32.6 ug/L 65 48 - 120 N-Nitrosodiethylamine 50.0 35.9 ug/L 72 61 - 120 N-Nitrosomethylethylamine 50.0 34.9 ug/L 70 51 - 120 Famphur 50.0 53.0 ug/L 106 70 - 130 N-Nitrosopiperidine 50.0 37.3 ug/L 75 67 - 120 N-Nitrosopyrrolidine 50.0 36.2 ug/L 72 60 - 120 o,o',o"-Triethylphosphorothioate 50.0 36.2 ug/L 72 63- 120 o-Toluidine 50.0 34.6 ug/L 69 47. 120 p-Dimethylamino azobenzene 50.0 44.1 ug/L 88 60 - 121 Pentachlorobenzene 50.0 38.1 ug/L 76 26 - 120 Pentachloronitrobenzene 50.0 44.7 ug/L 89 50 - 120 Phenacetin 50.0 53.8 ug/L 108 59 - 126 Kepone 50.2 45.4 J ug/L 91 70 - 130 Pronamide 50.0 49.2 ug/L 98 67 - 126 Safrole, Total 50.0 34.8 ug/L 70 62 - 120 LCS LCS Surrogate %Recovery Qualifier Limits 2, 4, 6-Tribromophenol (Surr) 86 13 - 138 2-Fluorobiphenyl (Surr) 79 44. 120 2-Fluorophenol (Surr) 48 10 - 120 Nitrobenzene-d5 (Surr) 78 31 - 120 p-Terphenyl-d14 (Surr) 89 30 - 125 Phenol-d5 (Surr) 35 10 - 120 Lab Sample ID: LCSD 410-356549/4-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 356887 Prep Batch: 356549 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit sym-Trinitrobenzene 50.0 ND *1 ug/L 45 10 - 120 60 30 1,4-Naphthoquinone 100 ND *- *1 ug/L 0.5 10 - 120 160 30 1,4-phenylenediamine 1100 ND *- ug/L 2 10 - 120 14 30 1-Naphthylamine 50.0 20.4 J ug/L 41 10 - 120 30 30 2-Acetylaminofluorene 50.0 47.7 ug/L 95 63 - 130 18 30 2-Naphthylamine 50.0 21.7 *1 ug/L 43 30-120 40 30 3,3'-Dimethylbenzidine 50.0 ND *1 ug/L 29 10 - 120 43 30 3-Methylcholanthrene 50.0 39.6 ug/L 79 61 - 121 10 30 4-Aminobiphenyl 50.0 19.8 ug/L 40 10 - 120 26 30 5-Nitro-o-toluidine 50.0 36.4 ug/L 73 51 _ 120 21 30 7,12-Dimethylbenz(a)anth racene 50.0 39.4 ug/L 79 71 -120 5 30 Chlorobenzilate 50.0 31.0 *1 ug/L 62 10 - 120 64 30 Diallate (Trans/Cis) 50.0 36.6 ug/L 73 60 - 120 13 30 Ethyl methanesulfonate 50.0 31.3 ug/L 63 61 - 120 8 30 Hexachloropropene 50.0 29.7 ug/L 59 10 - 120 19 30 Eurofins Lancaster Laboratories Environment Testing, LLC Page 34 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 410-35654914-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 356887 Prep Batch: 356549 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Isodrin 50.0 40.1 ug/L 80 58 - 120 6 30 Isosafrole 50.0 36.3 ug/L 73 66 - 120 13 30 Methapyrilene 100 67.8 ug/L 68 10 - 120 0 30 Methyl methanesulfonate 50.0 27.8 ug/L 56 38 - 120 1 30 N-Nitrosodi-n-butylamine 50.0 28.6 ug/L 57 48 - 120 13 30 N-Nitrosodiethylamine 50.0 31.6 ug/L 63 61 - 120 13 30 N-Nitrosomethylethylamine 50.0 34.4 ug/L 69 51 - 120 1 30 Famphur 50.0 45.9 J ug/L 92 70 - 130 14 30 N-Nitrosopiperidine 50.0 33.4 ug/L 67 67 - 120 11 30 N-Nitrosopyrrolidine 50.0 34.6 ug/L 69 60 - 120 5 30 o,o',o"-Triethylphosphorothioate 50.0 30.5 `- ug/L 61 63- 120 17 30 o-Toluidine 50.0 28.1 ug/L 56 47. 120 21 30 p-Dimethylamino azobenzene 50.0 36.2 ug/L 72 60 - 121 20 30 Pentachlorobenzene 50.0 35.0 ug/L 70 26 - 120 9 30 Pentachloronitrobenzene 50.0 42.8 ug/L 86 50 - 120 4 30 Phenacetin 50.0 46.6 ug/L 93 59 - 126 14 30 Kepone 50.2 36.3 J ug/L 72 70 - 130 22 30 Pronamide 50.0 43.2 ug/L 86 67 - 126 13 30 Safrole, Total 50.0 32.5 ug/L 65 62 - 120 7 30 LCSD LCSD Surrogate %Recovery Qualifier Limits 2, 4, 6-Tribromophenol (Surr) 77 13 - 138 2-Fluorobiphenyl (Surr) 69 44. 120 2-Fluorophenol (Surr) 48 10 - 120 Nitrobenzene-d5 (Surr) 62 31 - 120 p-Terphenyl-d14 (Surr) 88 30 - 125 Phenol-d5 (Surr) 37 10 - 120 Method: 8081 B - Organochlorine Pesticides (GC) Lab Sample ID: MB 410-356826/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 356978 Prep Batch: 356826 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin (1C) ND 0.020 0.0020 ug/L 03/23/23 16:25 03/24/23 06:25 1 alpha-BHC (1C) ND 0.020 0.0030 ug/L 03/23/23 16:25 03/24/23 06:25 1 beta-BHC (1C) ND 0.030 0.011 ug/L 03/23/23 16:25 03/24/23 06:25 1 delta-BHC (1C) ND 0.020 0.0034 ug/L 03/23/23 16:25 03/24/23 06:25 1 Dieldrin (1C) ND 0.030 0.0053 ug/L 03/23/23 16:25 03/24/23 06:25 1 Endosulfan I (1C) ND 0.020 0.0043 ug/L 03/23/23 16:25 03/24/23 06:25 1 Endosulfan 11 (1C) ND 0.040 0.015 ug/L 03/23/23 16:25 03/24/23 06:25 1 Endosulfan sulfate (1C) ND 0.030 0.0058 ug/L 03/23/23 16:25 03/24/23 06:25 1 Endrin (1C) ND 0.030 0.0081 ug/L 03/23/23 16:25 03/24/23 06:25 1 Endrin aldehyde (1C) ND 0.10 0.020 ug/L 03/23/23 16:25 03/24/23 06:25 1 gamma-BHC (Lindane) (1C) ND 0.020 0.0020 ug/L 03/23/23 16:25 03/24/23 06:25 1 Heptachlor (1C) ND 0.020 0.0020 ug/L 03/23/23 16:25 03/24/23 06:25 1 Heptachlor epoxide (1 C) ND 0.020 0.0023 ug/L 03/23/23 16:25 03/24/23 06:25 1 p,p'-DDD (1C) ND 0.030 0.0050 ug/L 03/23/23 16:25 03/24/23 06:25 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 35 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Method: 8081 B - Organochlorine Pesticides (GC) (Continued) Lab Sample ID: MB 410-35682611-A Matrix: Water Analysis Batch: 356978 MB MB Analyte Result Qualifier RL MDL Unit p,p'-DDE (1C) ND 0.030 0.0050 ug/L p,p'-DDT (1C) ND 0.030 0.0052 ug/L Toxaphene (1C) ND 1.0 0.30 ug/L Chlordane (n.o.s.) (1C) ND 0.50 0.16 ug/L Methoxychlor (1 C) ND 0.11 0.030 ug/L Surrogate DCB Decachlorobiphenyl (Surr) (1C) DCB Decachlorobiphenyl (Surr) (2C) Tetrachloro-m-xylene (Surr) (1 C) Tetrachloro-m-xylene (Surr) (2C) Lab Sample ID: LCS 410-35682612-A Matrix: Water Analysis Batch: 356978 MB MB %Recovery Qualifier Limits 94 20 - 149 107 20 - 149 74 20 - 129 73 20 - 129 Spike LCS LCS knalyte Added Result Qualifier Unit %ldrin (1C) 0.100 0.0854 ug/L alpha-BHC (1C) 0.100 0.0954 ug/L )eta-BHC (1C) 0.100 0.108 ug/L lelta-BHC (1C) 0.100 0.101 ug/L Dieldrin (1C) 0.200 0.204 ug/L ndosulfan I (1C) 0.100 0.104 ug/L ndosulfan II (1C) 0.200 0.219 ug/L ndosulfan sulfate (1C) 0.200 0.238 ug/L =ndrin (1C) 0.200 0.217 ug/L =ndrin aldehyde (1C) 0.200 0.188 ug/L Gamma-BHC (Lindane) (1C) 0.100 0.0987 ug/L ieptachlor(1C) 0.100 0.0969 ug/L ieptachlor epoxide (1C) 0.100 0.102 ug/L >,p'-DDD (1C) 0.200 0.224 ug/L >,p'-DDE (1C) 0.200 0.190 ug/L >,p'-DDT (1C) 0.200 0.211 ug/L Oethoxychlor (1 C) 1.00 1.16 ug/L LCS LCS Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl (Surr) 92 20 - 149 '1C) DCB Decachlorobiphenyl (Surr) 110 20 - 149 '2C) Tetrachloro-m-xylene (Surr) 81 20 - 129 '1C) Tetrachloro-m-xylene (Surr) 76 20 - 129 F Job ID: 410-119189-1 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 356826 L D Prepared Analyzed Dil Fac 03/23/23 16:25 03/24/23 06:25 1 03/23/23 16:25 03/24/23 06:25 1 03/23/23 16:25 03/24/23 06:25 1 03/23/23 16:25 03/24/23 06:25 1 03/23/23 16:25 03/24/23 06:25 1 • Prepared Analyzed DU Fac ILA 03/23/23 16:25 03/24/23 06:25 1 03/23/23 16:25 03/24/23 06:25 1 03/23/23 16:25 03/24/23 06:25 1 03/23/23 16:25 03/24/23 06:25 1 Client Sample ID: Lab Control Sample D %Rec Prep Type: Total/NA Prep Batch: 356826 %Rec Limits 85 10 - 148 95 47-132 108 65-139 101 56 - 141 102 58-145 104 63-138 110 61 - 138 119 63-129 109 63-131 94 57 - 135 99 61 - 139 97 35-136 102 59-146 112 42 - 148 95 20-140 106 40-145 116 66 - 148 Eurofins Lancaster Laboratories Environment Testing, LLC Page 36 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Method: 8081 B - Organochlorine Pesticides (GC) (Continued) Job ID: 410-119189-1 Lab Sample ID: LCSD 410-35682613-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 356978 Prep Batch: 356826 Spike LCSD LCSD °/Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Aldrin (1C) 0.100 0.0787 ug/L 79 10 - 148 6 30 alpha-BHC (1 C) 0.100 0.0920 ug/L 92 47 - 132 4 30 beta-BHC (1C) 0.100 0.104 ug/L 104 65 - 139 1 30 delta-BHC (1C) 0.100 0.0974 ug/L 97 56 - 141 4 30 Dieldrin (1 C) 0.200 0.202 ug/L 101 58 - 145 1 30 • Endosulfan I (1C) 0.100 0.101 ug/L 101 63 - 138 3 30 Endosulfan II (1C) 0.200 0.212 ug/L 106 61 - 138 3 30 Endosulfan sulfate (1C) 0.200 0.223 ug/L 112 63 - 129 6 30 Endrin (1C) 0.200 0.214 ug/L 107 63 - 131 1 30 Endrin aldehyde (1C) 0.200 0.179 ug/L 89 57 - 135 5 20 gamma-BHC (Lindane) (1C) 0.100 0.0977 ug/L 98 61 - 139 1 30 Heptachlor (1 C) 0.100 0.0895 ug/L 89 35 - 136 8 30 Heptachlor epoxide (1C) 0.100 0.0984 ug/L 98 59 - 146 4 30 p,p'-DDD (1C) 0.200 0.226 ug/L 113 42 - 148 1 30 p,p'-DDE (1C) 0.200 0.186 ug/L 93 20 - 140 2 30 p,p'-DDT (1C) 0.200 0.211 ug/L 106 40 - 145 0 30 Methoxychlor (1 C) 1.00 1.17 ug/L 117 66 - 148 1 30 LCSD LCSD Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl (Surr) 94 20 - 149 (lC) DCB Decachlorobiphenyl (Surr) 116 20 - 149 (2C) Tetrachloro-m-xylene (Surr) 74 20 - 129 (1C) Tetrachloro-m-xylene (Surr) 73 20 - 129 (2C) Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Lab Sample ID: MB 410-356828/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 357093 Prep Batch: 356828 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac PCB-1016 (1C) ND 0.25 0.10 ug/L 03/23/23 16:28 03/24/23 10:08 1 PCB-1221 (1C) ND 0.25 0.10 ug/L 03/23/23 16:28 03/24/23 10:08 1 PCB-1232 (1C) ND 0.25 0.10 ug/L 03/23/23 16:28 03/24/23 10:08 1 PCB-1242 (1C) ND 0.25 0.10 ug/L 03/23/23 16:28 03/24/23 10:08 1 PCB-1248 (1C) ND 0.25 0.078 ug/L 03/23/23 16:28 03/24/23 10:08 1 PCB-1254 (1C) ND 0.25 0.078 ug/L 03/23/23 16:28 03/24/23 10:08 1 PCB-1260 (1C) ND 0.25 0.078 ug/L 03/23/23 16:28 03/24/23 10:08 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl (Surr) (1C) 69 10 - 148 03/23/23 16:28 03/24/23 10:08 1 DCB Decachlorobiphenyl (Surr) (2C) 73 10 - 148 03/23/23 16:28 03/24/23 10:08 1 Tetrachloro-m-xylene (1C) 63 33- 137 03/23/23 16:28 03/24/23 10:08 1 Tetrachloro-m-xylene (2C) 63 33 - 137 03/23/23 16:28 03/24/23 10:08 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 37 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC F Job ID: 410-119189-1 Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) Lab Sample ID: LCS 410-356828/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 357093 Prep Batch: 356828 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits PCB-1016 (1C) 5.03 3.95 ug/L 78 60 - 117 PCB-1260 (1 C) 5.03 3.15 ug/L 63 57 - 134 LCS LCS Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl (Surr) 32 10 - 148 • 0 C) DCB Decachlorobiphenyl (Surr) 34 10 - 148 (2C) Tetrachloro-m-xylene (1C) 63 33 - 137 Tetrachloro-m-xylene (2C) 64 33 - 137 Lab Sample ID: LCSD 410-356828/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 357093 Prep Batch: 356828 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit PCB-1016 (1C) 5.03 3.62 ug/L 72 60 - 117 9 30 PCB-1260 (1 C) 5.03 2.84 ug/L 57 57. 134 10 30 LCSD LCSD Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl (Surr) 27 10 - 148 0 C) DCB Decachlorobiphenyl (Surr) 28 10 - 148 (2C) Tetrachloro-m-xylene (1C) 53 33 - 137 Tetrachloro-m-xylene (2C) 52 33 - 137 Method: 8151A - Herbicides (GC) Lab Sample ID: MB 410-355964/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 355987 Prep Batch: 355964 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 2,4,5-T (1C) ND 0.15 0.065 ug/L 03/21/23 20:22 03/22/23 05:03 1 Silvex (2,4,5-TP) (1C) ND 0.050 0.022 ug/L 03/21/23 20:22 03/22/23 05:03 1 2,4-Dichlorophenoxyacetic acid (1C) ND 0.60 0.25 ug/L 03/21/23 20:22 03/22/23 05:03 1 Dinoseb (1C) ND 0.60 0.28 ug/L 03/21/23 20:22 03/22/23 05:03 1 Lab Sample ID: LCS 410-355964/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 355987 Prep Batch: 355964 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits 2,4,5-T(1C) 0.250 0.186 ug/L 74 57-171 Silvex (2,4,5-TP) (1C) 0.250 0.178 ug/L 71 62 - 170 2,4-Dichlorophenoxyacetic acid 2.51 1.63 ug/L 65 53 - 159 (1C) Dinoseb (1C) 1.25 0.883 ug/L 71 10 - 169 Eurofins Lancaster Laboratories Environment Testing, LLC Page 38 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC F Job ID: 410-119189-1 Method: 8151A - Herbicides (GC) (Continued) Lab Sample ID: LCSD 410-355964/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 355987 Prep Batch: 355964 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit 2,4,5-T (1C) 0.250 0.198 ug/L 79 57- 171 6 30 Silvex (2,4,5-TP) (1C) 0.250 0.189 ug/L 76 62 - 170 6 30 2,4-Dichlorophenoxyacetic acid 2.51 1.73 ug/L 69 53 - 159 6 30 (1C) (1C) 1.25 0.944 ug/L 75 10 - 169 7 30 • —Dinoseb Method: EPA 8141 B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Lab Sample ID: MB 180-429800/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 430015 Prep Batch: 429800 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Dimethoate (1C) ND 1.0 0.26 ug/L 03/20/23 18:11 03/22/23 15:47 1 Disulfoton (1C) ND 1.0 0.41 ug/L 03/20/23 18:11 03/22/23 15:47 1 Parathion (1C) ND 1.0 0.37 ug/L 03/20/23 18:11 03/22/23 15:47 1 Methyl parathion (1C) ND 1.0 0.34 ug/L 03/20/23 18:11 03/22/23 15:47 1 Phorate (1C) ND 1.0 0.38 ug/L 03/20/23 18:11 03/22/23 15:47 1 Diethyl-O-pyrazinyl phosphorothioate, ND 1.0 0.32 ug/L 03/20/23 18:11 03/22/23 15:47 1 O,O- (1C) MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Tributyl phosphate (1C) 84 25- 127 03120123 18:11 03122123 15:47 1 Triphenylphosphate (1C) 109 70- 155 03120123 18:11 03122123 15:47 1 Lab Sample ID: LCS 180-429800/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 430015 Prep Batch: 429800 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Dimethoate (2C) 10.0 11.9 ug/L 119 50 - 148 Disulfoton (2C) 10.0 10.8 ug/L 108 61 - 125 Parathion (2C) 10.0 11.4 ug/L 114 57 - 140 Methyl parathion (1C) 10.0 10.7 ug/L 107 62 - 137 Phorate (2C) 10.0 12.5 ug/L 125 30 - 137 Diethyl-O-pyrazinyl 10.0 11.1 ug/L ill 54 - 132 phosphorothioate, 0,0- (1C) LCS LCS Surrogate %Recovery Qualifier Limits Tributyl phosphate (2C) 115 25 - 127 Triphenylphosphate (1C) 111 70 - 155 Lab Sample ID: LCSD 180-429800/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 430015 Prep Batch: 429800 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Dimethoate (2C) 10.0 11.8 ug/L 118 50 - 148 1 15 Eurofins Lancaster Laboratories Environment Testing, LLC Page 39 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Method: EPA 8141 B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique (Continued) Lab Sample ID: LCSD 180-429800/3-A Matrix: Water Analysis Batch: 430015 Spike LCSD LCSD Analyte Added Result Qualifier Unit Disulfoton (2C) 10.0 10.7 ug/L Parathion (2C) 10.0 11.4 ug/L Methyl parathion (2C) 10.0 10.6 ug/L Phorate (2C) 10.0 12.4 ug/L Diethyl-O-pyrazinyl 10.0 11.0 ug/L phosphorothioate, 0,0- (2C) LCSD LCSD Surrogate %Recovery Qualifier Limits Tributyl phosphate (2C) 114 25 - 127 Triphenylphosphate (2C) 110 70 - 155 Method: EPA 300.0 R2.1 - Anions, Ion Chromato Lab Sample ID: MB 410-355421/5 Matrix: Water Analysis Batch: 355421 MB MB Analyte Result Qualifier Sulfate ND Chloride ND Lab Sample ID: LCS 410-355421/3 Matrix: Water Analysis Batch: 355421 Analyte Sulfate Chloride Lab Sample ID: LCSD 410-35542114 Matrix: Water Analysis Batch: 355421 Analyte Sulfate Chloride Lab Sample ID: MB 410-355859/5 Matrix: Water Analysis Batch: 355859 MB MB Analyte Result Qualifier Sulfate ND Chloride ND F Job ID: 410-119189-1 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 429800 %Rec RPD D %Rec Limits RPD Limit 107 61-125 1 15 114 57-140 0 20 106 62-137 1 21 124 30-137 1 20 • 110 54-132 1 15 Client Sample ID: Method Blank Prep Type: Total/NA RL MDL Unit D Prepared Analyzed Dil Fac 1.5 0.50 mg/L 03/20/2314:08 1 1.5 0.60 mg/L 03/20/2314:08 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec Added Result Qualifier Unit D %Rec Limits 7.50 7.92 mg/L 106 90 - 110 3.00 3.14 mg/L 105 90 - 110 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike LCSD LCSD %Rec RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 7.50 7.89 mg/L 105 90 - 110 0 20 3.00 3.15 mg/L 105 90 - 110 0 20 Client Sample ID: Method Blank Prep Type: Total/NA RL MDL Unit D Prepared Analyzed Dil Fac 1.5 0.50 mg/L 03/21/2312:59 1 1.5 0.60 mg/L 03/21/2312:59 1 Page 40 of 63 Eurofins Lancaster Laboratories Environment Testing, LLC 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Method: EPA 300.0 R2.1 - Anions, Ion Chromatography (Continued) Lab Sample ID: LCS 410-355859/3 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 355859 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Sulfate 7.50 7.51 mg/L 100 90 - 110 Chloride 3.00 3.12 mg/L 104 90 - 110 Lab Sample ID: LCSD 410-355859/4 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 355859 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Sulfate 7.50 7.46 mg/L 99 90 - 110 1 20 Chloride 3.00 3.10 mg/L 103 90 - 110 1 20 Method: 6020B - Metals (ICP/MS) Lab Sample ID: MB 410-356019/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total Recoverable Analysis Batch: 356447 Prep Batch: 356019 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony ND 1.0 0.20 ug/L 03/22/23 07:13 03/22/23 17:29 1 Arsenic ND 2.0 0.68 ug/L 03/22/23 07:13 03/22/23 17:29 1 Barium ND 2.0 0.75 ug/L 03/22/23 07:13 03/22/23 17:29 1 Beryllium ND 0.50 0.12 ug/L 03/22/23 07:13 03/22/23 17:29 1 Cadmium ND 0.50 0.15 ug/L 03/22/23 07:13 03/22/23 17:29 1 Chromium ND 2.0 0.33 ug/L 03/22/23 07:13 03/22/23 17:29 1 Cobalt ND 0.50 0.16 ug/L 03/22/23 07:13 03/22/23 17:29 1 Copper ND 1.0 0.36 ug/L 03/22/23 07:13 03/22/23 17:29 1 Iron ND 50 20 ug/L 03/22/23 07:13 03/22/23 17:29 1 Lead ND 0.50 0.071 ug/L 03/22/23 07:13 03/22/23 17:29 1 Manganese ND 2.0 0.95 ug/L 03/22/23 07:13 03/22/23 17:29 1 Nickel ND 1.0 0.40 ug/L 03/22/23 07:13 03/22/23 17:29 1 Selenium ND 1.0 0.28 ug/L 03/22/23 07:13 03/22/23 17:29 1 Silver ND 0.50 0.10 ug/L 03/22/23 07:13 03/22/23 17:29 1 Thallium ND 0.50 0.13 ug/L 03/22/23 07:13 03/22/23 17:29 1 Tin ND 2.0 0.60 ug/L 03/22/23 07:13 03/22/23 17:29 1 Vanadium ND 4.0 0.79 ug/L 03/22/23 07:13 03/22/23 17:29 1 Zinc ND 10 4.0 ug/L 03/22/23 07:13 03/22/23 17:29 1 Lab Sample ID: LCS 410-356019/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total Recoverable Analysis Batch: 356447 Prep Batch: 356019 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Antimony 100 107 ug/L 107 80 - 120 Arsenic 500 500 ug/L 100 85 - 120 Barium 500 519 ug/L 104 80 - 120 Cadmium 50.0 53.2 ug/L 106 86 - 113 Chromium 500 516 ug/L 103 90 - 115 Cobalt 500 515 ug/L 103 90 - 113 Copper 500 508 ug/L 102 80-120 Eurofins Lancaster Laboratories Environment Testing, LLC Page 41 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Method: 6020B - Metals (ICP/MS) (Continued) Lab Sample ID: LCS 410-356019/2-A Matrix: Water Analysis Batch: 356447 Analyte Iron Lead Manganese Nickel Selenium Silver Thallium Tin Vanadium Zinc Lab Sample ID: LCS 410-356019/2-A Matrix: Water Analysis Batch: 357134 Analyte Beryllium Lab Sample ID: MB 410-356022/1-A Matrix: Water Analysis Batch: 356438 Spike Added LCS LCS Result Qualifier Unit 5000 5270 ug/L 50.0 52.4 ug/L 500 514 ug/L 500 515 ug/L 100 99.8 ug/L 50.0 53.2 ug/L 100 104 ug/L 100 107 ug/L 500 517 ug/L 500 507 ug/L Job ID: 410-119189-1 Client Sample ID: Lab Control Sample Prep Type: Total Recoverable Prep Batch: 356019 %Rec D %Rec Limits 105 88-119 105 90. 115 103 89.120 103 90 _ 114 100 80 _ 120 106 88.113 104 80 _ 120 107 90 _ 113 103 90 _ 115 101 90 _ 115 Client Sample ID: Lab Control Sample Prep Type: Total Recoverable Prep Batch: 356019 Spike LCS LCS %Rec Added Result Qualifier Unit D %Rec Limits 50.0 53.6 ug/L 107 90 - 112 Client Sample ID: Method Blank Prep Type: Total Recoverable Prep Batch: 356022 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony ND 1.0 0.20 ug/L 03/22/23 07:17 03/22/23 18:42 1 Arsenic ND 2.0 0.68 ug/L 03/22/23 07:17 03/22/23 18:42 1 Barium ND 2.0 0.75 ug/L 03/22/23 07:17 03/22/23 18:42 1 Beryllium ND 0.50 0.12 ug/L 03/22/23 07:17 03/22/23 18:42 1 Cadmium ND 0.50 0.15 ug/L 03/22/23 07:17 03/22/23 18:42 1 Chromium ND 2.0 0.33 ug/L 03/22/23 07:17 03/22/23 18:42 1 Cobalt ND 0.50 0.16 ug/L 03/22/23 07:17 03/22/23 18:42 1 Copper ND 1.0 0.36 ug/L 03/22/23 07:17 03/22/23 18:42 1 Iron ND 50 20 ug/L 03/22/23 07:17 03/22/23 18:42 1 Lead ND 0.50 0.071 ug/L 03/22/23 07:17 03/22/23 18:42 1 Manganese ND 2.0 0.95 ug/L 03/22/23 07:17 03/22/23 18:42 1 Nickel ND 1.0 0.40 ug/L 03/22/23 07:17 03/22/23 18:42 1 Selenium ND 1.0 0.28 ug/L 03/22/23 07:17 03/22/23 18:42 1 Silver ND 0.50 0.10 ug/L 03/22/23 07:17 03/22/23 18:42 1 Thallium ND 0.50 0.13 ug/L 03/22/23 07:17 03/22/23 18:42 1 Tin ND 2.0 0.60 ug/L 03/22/23 07:17 03/22/23 18:42 1 Vanadium ND 4.0 0.79 ug/L 03/22/23 07:17 03/22/23 18:42 1 Zinc ND 10 4.0 ug/L 03/22/23 07:17 03/22/23 18:42 1 Lab Sample ID: LCS 410-356022/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total Recoverable Analysis Batch: 356438 Prep Batch: 356022 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Antimony 100 99.8 ug/L 100 80 - 120 Arsenic 500 493 ug/L 99 85. 120 Page 42 of 63 Eurofins Lancaster Laboratories Environment Testing, LLC 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill INC Method: 6020B - Metals (ICP/MS) (Continued) Lab Sample ID: LCS 410-356022/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total Recoverable Analysis Batch: 356438 Prep Batch: 356022 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Barium 500 517 ug/L 103 80 - 120 Beryllium 50.0 52.6 ug/L 105 90 - 112 Cadmium 50.0 49.9 ug/L 100 86 - 113 Chromium 500 496 ug/L 99 90 - 115 Cobalt 500 496 ug/L 99 90 - 113 Copper 500 482 ug/L 96 80-120 Iron 5000 5020 ug/L 100 88 - 119 Lead 50.0 53.5 ug/L 107 90 - 115 Manganese 500 504 ug/L 101 89-120 Nickel 500 495 ug/L 99 90 - 114 Selenium 100 96.6 ug/L 97 80 - 120 Silver 50.0 50.1 ug/L 100 88 - 113 Thallium 100 106 ug/L 106 80 - 120 Tin 100 101 ug/L 101 90 - 113 Vanadium 500 505 ug/L 101 90 - 115 Zinc 500 496 ug/L 99 90 - 115 Method: 7470A - Mercury (CVAA) Lab Sample ID: MB 410-356074/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 356396 Prep Batch: 356074 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.20 0.079 ug/L 03/22/23 08:17 03/22/23 14:22 1 Lab Sample ID: LCS 410-356074/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 356396 Prep Batch: 356074 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Mercury 1.00 0.840 ug/L 84 80 - 118 Method: 2320B-2011 - Alkalinity, Total Lab Sample ID: MB 410-356734/95 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 356734 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Total Alkalinity as CaCO3 to pH 4.5 ND 8.0 2.6 mg/L 03/23/23 02:08 1 Lab Sample ID: LCS 410-356734/96 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 356734 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Total Alkalinity as CaCO3 to pH 189 180 mg/L 95 66 - 110 4.5 Eurofins Lancaster Laboratories Environment Testing, LLC Page 43 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Method: 2320B-2011 - Alkalinity, Total (Continued) Lab Sample ID: LCSD 410-356734/97 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 356734 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Alkalinity as CaCO3 to pH 189 181 mg/L 96 66 - 110 0 10 4.5 Method: 353.2 - Nitrogen, Nitrite Lab Sample ID: MB 410-354981/13 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 354981 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Nitrite as N ND 0.050 0.015 mg/L 03/18/23 08:30 1 Lab Sample ID: LCS 410-354981/14 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 354981 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Nitrite as N 0.699 0.657 mg/L 94 90 - 110 Lab Sample ID: LCSD 410-354981/15 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 354981 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Nitrite as N 0.699 0.660 mg/L 94 90 - 110 0 20 Method: 353.2 - Nitrogen, Nitrate -Nitrite Lab Sample ID: MB 410-357442/55 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 357442 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Nitrate Nitrite as N ND 0.10 0.040 mg/L 03/25/23 12:17 1 Lab Sample ID: MB 410-357442/88 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 357442 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Nitrate Nitrite as N ND 0.10 0.040 mg/L 03/25/23 13:23 1 Lab Sample ID: LCS 410-357442/87 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 357442 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Nitrate Nitrite as N 2.50 2.54 mg/L 102 90 - 110 Eurofins Lancaster Laboratories Environment Testing, LLC Page 44 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill INC Method: 353.2 - Nitrogen, Nitrate -Nitrite (Continued) Lab Sample ID: 410-119189-1 MS Client Sample ID: MW-18 Matrix: Water Prep Type: Total/NA Analysis Batch: 357442 Sample Sample Spike MS MS %Rec Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Nitrate Nitrite as N ND cn 1.00 1.10 cn mg/L 110 90 - 110 Lab Sample ID: 410-119189-1 DU Client Sample ID: MW-18 Matrix: Water Prep Type: Total/NA Analysis Batch: 357442 Sample Sample DU DU RPD Analyte Result Qualifier Result Qualifier Unit D RPD Limit Nitrate Nitrite as N ND cn ND cn mg/L NC 10 Method: 4500 S2 D-2011 - Sulfide, Total Lab Sample ID: MB 410-355333/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 355333 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Sulfide ND 0.30 0.10 mg/L 03/20/2313:32 1 Lab Sample ID: LCS 410-355333/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 355333 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Sulfide 0.999 0.906 mg/L 91 84 - 116 Method: 9012B - Cyanide, Total andor Amenable Lab Sample ID: MB 410-357188/2-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 357778 Prep Batch: 357188 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Cyanide, Total ND 0.010 0.0050 mg/L 03/24/23 12:00 03/27/23 12:05 1 Lab Sample ID: LCS 410-357188/1-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 357778 Prep Batch: 357188 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Cyanide, Total 0.200 0.201 mg/L 100 90 - 110 Method: SM 2540C - Solids, Total Dissolved (TDS) Lab Sample ID: MB 410-355865/1 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 355865 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Total Dissolved Solids ND 30 12 mg/L 03/22/23 06:15 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 45 of 63 3/30/2023 QC Sample Results Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Method: SM 2540C - Solids, Total Dissolved (TDS) (Continued) Lab Sample ID: LCS 410-355865/2 Matrix: Water Analysis Batch: 355865 Spike LCS LCS Analyte Added Result Qualifier Unit Total Dissolved Solids 200 208 mg/L Lab Sample ID: LCSD 410-355865/3 Matrix: Water Analysis Batch: 355865 Spike LCSD LCSD Analyte Added Result Qualifier Unit Total Dissolved Solids 200 196 mg/L F Job ID: 410-119189-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA %Rec D %Rec Limits 104 90 - 110 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA %Rec RPD D %Rec Limits RPD Limit 98 90 - 110 6 10 Eurofins Lancaster Laboratories Environment Testing, LLC Page 46 of 63 3/30/2023 QC Association Summary Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC GC/MS VOA Analysis Batch: 354854 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total/NA Water 8260D 410-119189-2 MW-19 Total/NA Water 8260D 410-119189-3 TB-1 Total/NA Water 8260D MB 410-354854/10 Method Blank Total/NA Water 8260D LCS 410-354854/5 Lab Control Sample Total/NA Water 8260D LCS 410-354854/6 Lab Control Sample Total/NA Water 8260D LCSD 410-354854/7 Lab Control Sample Dup Total/NA Water 8260D Analysis Batch: 355251 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total/NA Water 8260D SIM 14D 410-119189-2 MW-19 Total/NA Water 8260D SIM 14D MB 410-355251/6 Method Blank Total/NA Water 8260D SIM 14D LCS 410-355251/4 Lab Control Sample Total/NA Water 8260D SIM 14D GC/MS Semi VOA Prep Batch: 356549 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total/NA Water 3510C 410-119189-2 MW-19 Total/NA Water 3510C m MB 410-356549/1-A Method Blank Total/NA Water 3510C LCS 410-356549/2-A Lab Control Sample Total/NA Water 3510C LCS 410-356549/3-A Lab Control Sample Total/NA Water 3510C LCSD 410-356549/4-A Lab Control Sample Dup Total/NA Water 3510C Analysis Batch: 356887 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total/NA Water 8270E 356549 410-119189-2 MW-19 Total/NA Water 8270E 356549 MB 410-356549/1-A Method Blank Total/NA Water 8270E 356549 LCS 410-356549/2-A Lab Control Sample Total/NA Water 8270E 356549 LCS 410-356549/3-A Lab Control Sample Total/NA Water 8270E 356549 LCSD 410-356549/4-A Lab Control Sample Dup Total/NA Water 8270E 356549 GC Semi VOA Prep Batch: 355964 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total/NA Water 8151A 410-119189-2 MW-19 Total/NA Water 8151A MB 410-355964/1-A Method Blank Total/NA Water 8151A LCS 410-355964/2-A Lab Control Sample Total/NA Water 8151A LCSD 410-355964/3-A Lab Control Sample Dup Total/NA Water 8151A Analysis Batch: 355987 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total/NA Water 8151A 355964 410-119189-2 MW-19 Total/NA Water 8151A 355964 MB 410-355964/1-A Method Blank Total/NA Water 8151A 355964 LCS 410-355964/2-A Lab Control Sample Total/NA Water 8151A 355964 LCSD 410-355964/3-A Lab Control Sample Dup Total/NA Water 8151A 355964 Eurofins Lancaster Laboratories Environment Testing, LLC Page 47 of 63 3/30/2023 QC Association Summary Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC GC Semi VOA Prep Batch: 356826 Lab Sample ID Client Sample ID 410-119189-1 M W-18 410-119189-2 M W-19 MB 410-356826/1-A Method Blank LCS 410-356826/2-A Lab Control Sample LCSD 410-356826/3-A Lab Control Sample Dup Prep Batch: 356828 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 410-356828/1-A Method Blank LCS 410-356828/2-A Lab Control Sample LCSD 410-356828/3-A Lab Control Sample Dup Analysis Batch: 356978 Lab Sample ID Client Sample ID 410-119189-1 VW-18 410-119189-2 MW-19 MB 410-356826/1-A Method Blank LCS 410-356826/2-A Lab Control Sample LCSD 410-356826/3-A Lab Control Sample Dup Analysis Batch: 357093 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 410-356828/1-A Method Blank LCS 410-356828/2-A Lab Control Sample LCSD 410-356828/3-A Lab Control Sample Dup Prep Batch: 429800 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 180-429800/1-A Method Blank LCS 180-429800/2-A Lab Control Sample LCSD 180-429800/3-A Lab Control Sample Dup Analysis Batch: 430015 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 180-429800/1-A Method Blank LCS 180-429800/2-A Lab Control Sample LCSD 180-429800/3-A Lab Control Sample Dup HPLVIC Job ID: 410-119189-1 Prep Type Matrix Method Prep Batch Total/NA Water 3510C Total/NA Water 3510C Total/NA Water 3510C Total/NA Water 3510C Total/NA Water 3510C Prep Type Matrix Method Prep Batch Total/NA Water 3510C Total/NA Water 3510C Total/NA Water 3510C Total/NA Water 3510C Total/NA Water 3510C Prep Type Matrix Method Prep Batch Total/NA Water 8081 B 356826 Total/NA Water 8081 B 356826 Total/NA Water 8081 B 356826 Total/NA Water 8081 B 356826 Total/NA Water 8081 B 356826 Prep Type Matrix Method Prep Batch Total/NA Water 8082A 356828 Total/NA Water 8082A 356828 Total/NA Water 8082A 356828 Total/NA Water 8082A 356828 Total/NA Water 8082A 356828 Prep Type Matrix Method Prep Batch Total/NA Water 3510C Total/NA Water 3510C Total/NA Water 3510C Total/NA Water 3510C Total/NA Water 3510C Prep Type Matrix Method Prep Batch Total/NA Water EPA 8141 B 429800 Total/NA Water EPA 8141 B 429800 Total/NA Water EPA 8141 B 429800 Total/NA Water EPA 8141 B 429800 Total/NA Water EPA 8141 B 429800 Analysis Batch: 355421 Lab Sample ID Client Sample ID Prep Type 410-119189-1 MW-18 Total/NA Page 48 of 63 Matrix Method _ Prep Batch Water EPA 300.0 R2.1 Eurofins Lancaster Laboratories Environment Testing, LLC 3/30/2023 QC Association Summary Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC HPLC/IC (Continued) Analysis Batch: 355421 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-2 MW-19 Total/NA Water EPA 300.0 R2.1 MB 410-355421/5 Method Blank Total/NA Water EPA 300.0 R2.1 LCS 410-355421/3 Lab Control Sample Total/NA Water EPA 300.0 R2.1 LCSD 410-355421/4 Lab Control Sample Dup Total/NA Water EPA 300.0 R2.1 Analysis Batch: 355859 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-2 MW-19 Total/NA Water EPA 300.0 R2.1 MB 410-355859/5 Method Blank Total/NA Water EPA 300.0 R2.1 LCS 410-355859/3 Lab Control Sample Total/NA Water EPA 300.0 R2.1 LCSD 410-355859/4 Lab Control Sample Dup Total/NA Water EPA 300.0 R2.1 Metals Prep Batch: 356019 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total Recoverable Water 3005A MB 410-356019/1-A Method Blank Total Recoverable Water 3005A LCS 410-356019/2-A Lab Control Sample Total Recoverable Water 3005A Prep Batch: 356022 m Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-2 MW-19 Total Recoverable Water 3005A MB 410-356022/1-A Method Blank Total Recoverable Water 3005A LCS 410-356022/2-A Lab Control Sample Total Recoverable Water 3005A Prep Batch: 356074 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total/NA Water 7470A 410-119189-2 MW-19 Total/NA Water 7470A MB 410-356074/1-A Method Blank Total/NA Water 7470A LCS 410-356074/2-A Lab Control Sample Total/NA Water 7470A Analysis Batch: 356396 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total/NA Water 7470A 356074 410-119189-2 MW-19 Total/NA Water 7470A 356074 MB 410-356074/1-A Method Blank Total/NA Water 7470A 356074 LCS 410-356074/2-A Lab Control Sample Total/NA Water 7470A 356074 Analysis Batch: 356438 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-2 MW-19 Total Recoverable Water 6020E 356022 MB 410-356022/1-A Method Blank Total Recoverable Water 6020B 356022 LCS 410-356022/2-A Lab Control Sample Total Recoverable Water 6020B 356022 Analysis Batch: 356447 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-119189-1 MW-18 Total Recoverable Water 6020B 356019 MB 410-356019/1-A Method Blank Total Recoverable Water 6020B 356019 LCS 410-356019/2-A Lab Control Sample Total Recoverable Water 6020B 356019 Eurofins Lancaster Laboratories Environment Testing, LLC Page 49 of 63 3/30/2023 QC Association Summary Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Metals Analysis Batch: 357134 Lab Sample ID Client Sample ID 410-119189-1 M W-18 LCS 410-356019/2-A Lab Control Sample General Chemistry Analysis Batch: 354981 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 410-354981/13 Method Blank LCS 410-354981/14 Lab Control Sample LCSD 410-354981/15 Lab Control Sample Dup Analysis Batch: 355162 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 Analysis Batch: 355333 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 410-355333/4 Method Blank LCS 410-355333/5 Lab Control Sample Analysis Batch: 355865 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 410-355865/1 Method Blank LCS 410-355865/2 Lab Control Sample LCSD 410-355865/3 Lab Control Sample Dup Analysis Batch: 356734 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 410-356734/95 Method Blank LCS 410-356734/96 Lab Control Sample LCSD 410-356734/97 Lab Control Sample Dup Prep Batch: 357188 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 410-357188/2-A Method Blank LCS 410-357188/1-A Lab Control Sample Analysis Batch: 357442 Lab Sample ID Client Sample ID 410-119189-1 MW-18 F Job ID: 410-119189-1 Prep Type Matrix Method Prep Batch Total Recoverable Total Recoverable Water Water 6020B 6020B 356019 356019 Prep Type Matrix Method Total/NA Water 353.2 Total/NA Water 353.2 Total/NA Water 353.2 Total/NA Water 353.2 Total/NA Water 353.2 Prep Type Matrix Method Total/NA Water 353.2 Total/NA Water 353.2 Prep Type Matrix Method Total/NA Water 4500 S2 D-2011 Total/NA Water 4500 S2 D-2011 Total/NA Water 4500 S2 D-2011 Total/NA Water 4500 S2 D-2011 Prep Type Matrix Method Total/NA Water SM 2540C Total/NA Water SM 2540C Total/NA Water SM 2540C Total/NA Water SM 2540C Total/NA Water SM 2540C Prep Type Total/NA Total/NA Total/NA Total/NA Total/NA Prep Type Total/NA Total/NA Total/NA Total/NA Prep Type Total/NA Page 50 of 63 Matrix Water Water Water Water Water Matrix Water Water Water Water Method 2320B-2011 2320B-2011 2320B-2011 2320E-2011 2320B-2011 Method 9012E 9012E 9012E 9012B Prep Batch 0 Prep Batch F Prep Batch Prep Batch Prep Batch Prep Batch Matrix Method Prep Batch Water 353.2 Eurofins Lancaster Laboratories Environment Testing, LLC 3/30/2023 QC Association Summary Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC General Chemistry (Continued) Analysis Batch: 357442 (Continued) Lab Sample ID Client Sample ID 410-119189-2 MW-19 MB 410-357442/55 Method Blank MB 410-357442/88 Method Blank LCS 410-357442/87 Lab Control Sample 410-119189-1 MS MW-18 410-119189-1 DU MW-18 Analysis Batch: 357778 Lab Sample ID Client Sample ID 410-119189-1 MW-18 410-119189-2 MW-19 MB 410-357188/2-A Method Blank LCS 410-35718811-A Lab Control Sample F Job ID: 410-119189-1 Prep Type Matrix Method Prep Batch Total/NA Water 353.2 Total/NA Water 353.2 Total/NA Water 353.2 Total/NA Water 353.2 Total/NA Water 353.2 Total/NA Water 353.2 Prep Type Matrix Method Prep Batch Total/NA Water 9012B 357188 Total/NA Water 9012B 357188 Total/NA Water 9012B 357188 Total/NA Water 9012B 357188 Eurofins Lancaster Laboratories Environment Testing, LLC Page 51 of 63 3/30/2023 Lab Chronicle Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC F Job ID: 410-119189-1 Client Sample ID: MW-18 Lab Sample ID: 410-119189-1 Date Collected: 03/16/23 12:30 Matrix: Water Date Received: 03/17/23 10:24 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number Analyst Lab or Analyzed Total/NA Analysis 8260D 1 354854 TQ4J ELLE 03/18/23 05:31 Total/NA Analysis 8260D SIM 14D 1 355251 UJML ELLE 03/20/23 20:30 Total/NA Prep 3510C 356549 YDF5 ELLE 03/23/23 08:00 Total/NA Analysis 8270E 1 356887 AH7C ELLE 03/23/23 20:33 Total/NA Prep 3510C 356826 QJZ6 ELLE 03/23/2316:25 Total/NA Analysis 8081E 1 356978 UAMZ ELLE 03/24/2306:56 Total/NA Prep 3510C 356828 QJZ6 ELLE 03/23/2316:28 Total/NA Analysis 8082A 1 357093 JC94 ELLE 03/24/2310:40 Total/NA Prep 8151A 355964 UKL2 ELLE 03/21/23 20:22 Total/NA Analysis 8151A 1 355987 UAMZ ELLE 03/22/2312:30 Total/NA Prep 3510C 429800 VJC EET PIT 03/20/23 18:11 Total/NA Analysis EPA 8141B 1 430015 C1F EET PIT 03/22/2314:44 Total/NA Analysis EPA 300.0 R2.1 5 355421 L4QM ELLE 03/20/23 14:34 Total Recoverable Prep 3005A 356019 HUH3 ELLE 03/22/23 07:13 Total Recoverable Analysis 6020B 1 356447 UCIG ELLE 03/22/23 18:07 Total Recoverable Prep 3005A 356019 HUH3 ELLE 03/22/23 07:13 Total Recoverable Analysis 6020B 1 357134 F7JF ELLE 03/24/23 09:25 Total/NA Prep 7470A 356074 HUH3 ELLE 03/22/23 08:17 Total/NA Analysis 7470A 1 356396 UEFS ELLE 03/22/2315:24 Total/NA Analysis 2320B-2011 1 356734 D19Q ELLE 03/23/23 03:41 Total/NA Analysis 353.2 1 357442 Q3HN ELLE 03/25/2313:53 Total/NA Analysis 353.2 1 354981 Q3HN ELLE 03/18/23 08:31 Total/NA Analysis 353.2 1 355162 UKJF ELLE 03/20/23 07:33 Total/NA Analysis 4500 S2 D-2011 1 355333 USAE ELLE 03/20/23 13:32 Total/NA Prep 9012B 357188 NLE3 ELLE 03/24/23 12:00 - 03/24/23 13:45' Total/NA Analysis 9012B 1 357778 JCG7 ELLE 03/27/2312:07 Total/NA Analysis SM 2540C 1 355865 UOCA ELLE 03/22/23 06:15 - 03/22/23 20:08' Client Sample ID: MW-19 Lab Sample ID: 410-119189-2 Date Collected: 03/16/23 15:00 Matrix: Water Date Received: 03/17/23 10:24 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number Analyst Lab or Analyzed Total/NA Analysis 8260D 1 354854 TQ4J ELLE 03/18/23 05:53 Total/NA Analysis 8260D SIM 14D 1 355251 UJML ELLE 03/20/23 20:50 Total/NA Prep 3510C 356549 YDF5 ELLE 03/23/23 08:00 Total/NA Analysis 8270E 1 356887 AH7C ELLE 03/23/23 20:53 Total/NA Prep 3510C 356826 QJZ6 ELLE 03/23/2316:25 Total/NA Analysis 8081B 1 356978 UAMZ ELLE 03/24/2307:07 Total/NA Prep 3510C 356828 QJZ6 ELLE 03/23/2316:28 Total/NA Analysis 8082A 1 357093 JC94 ELLE 03/24/2310:50 Total/NA Prep 8151A 355964 UKL2 ELLE 03/21/23 20:22 Total/NA Analysis 8151A 1 355987 UAMZ ELLE 03/22/2312:58 Page 52 of 63 Eurofins Lancaster Laboratories Environment Testing, LLC 3/30/2023 Lab Chronicle Client: ELM Site Solutions Inc Job ID: 410-119189-1 Project/Site: C&D Landfill NC Client Sample ID: MW-19 Lab Sample ID: 410-119189-2 Date Collected: 03/16/23 15:00 Matrix: Water Date Received: 03/17/23 10:24 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number Analyst Lab or Analyzed Total/NA Prep 3510C 429800 VJC EET PIT 03/20/23 18:11 Total/NA Analysis EPA 8141 B 1 430015 C1 F EET PIT 03/22/23 15:15 Total/NA Analysis EPA300.0 R2.1 5 355421 L4QM ELLE 03/20/23 14:43 Total/NA Analysis EPA300.0 R2.1 10 355859 L4QM ELLE 03/21/23 15:07 Total Recoverable Prep 3005A 356022 HUH3 ELLE 03/22/23 07:17 Total Recoverable Analysis 6020B 1 356438 UCIG ELLE 03/22/23 19:11 Total/NA Prep 7470A 356074 HUH3 ELLE 03/22/23 08:17 Total/NA Analysis 7470A 1 356396 UEFS ELLE 03/22/2314:58 Total/NA Analysis 2320B-2011 1 356734 D19Q ELLE 03/23/23 03:35 m Total/NA Analysis 353.2 1 357442 Q3HN ELLE 03/25/2313:59 Total/NA Analysis 353.2 1 354981 Q3HN ELLE 03/18/23 08:31 Total/NA Analysis 353.2 1 355162 UKJF ELLE 03/20/23 07:33 Total/NA Analysis 4500 S2 D-2011 1 355333 USAE ELLE 03/20/23 13:32 Total/NA Prep 9012B 357188 NLE3 ELLE 03/24/23 12:00 - 03/24/23 13:45' Total/NA Analysis 9012B 1 357778 JCG7 ELLE 03/27/2312:07 Total/NA Analysis SM 2540C 1 355865 UOCA ELLE 03/22/23 06:15 - 03/22/23 20:08' Client Sample ID: T13-1 Lab Sample ID: 410-119189-3 Date Collected: 03/16/23 00:00 Matrix: Water Date Received: 03/17/23 10:24 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number Analyst Lab or Analyzed Total/NA Analysis 8260D 1 354854 TQ4J ELLE 03/17/23 23:58 Completion dates and times are reported or not reported per method requirements or individual lab discretion. Laboratory References: EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL (412)963-7058 ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL (717)656-2300 Eurofins Lancaster Laboratories Environment Testing, LLC Page 53 of 63 3/30/2023 Accreditation/Certification Summary Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Progi North Carolina (WW/SW) State Identification Number Expiration Date 521 12-31-23 F Job ID: 410-119189-1 The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte 353.2 Water Nitrate as N 8260D Water Tetrahydrofuran Laboratory: Eurofins Pittsburgh All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report. Authority Program Identification Number Expiration Date Arkansas DEQ State 19-033-0 06-27-23 California State 2891 04-30-23 Connecticut State PH-0688 09-30-24 Florida NELAP E871008 06-30-23 Georgia State PA 02-00416 04-30-23 Illinois NELAP 004375 06-30-23 Kansas NELAP E-10350 01-31-24 Kentucky (UST) State 162013 04-30-23 Kentucky (WW) State KY98043 12-31-23 Louisiana NELAP 04041 06-30-22 Louisiana (All) NELAP 04041 06-30-23 Maine State PA00164 03-06-24 Minnesota NELAP 042-999482 12-31-23 New Hampshire NELAP 2030 04-04-23 New Jersey NELAP PA005 06-30-23 New York NELAP 11182 04-01-23 North Carolina (WW/SW) State 434 12-31-23 North Dakota State R-227 04-30-23 Oregon NELAP PA-2151 02-06-24 Pennsylvania NELAP 02-00416 04-30-24 Rhode Island State LA000362 12-31-22 South Carolina State 89014 04-30-23 Texas NELAP T104704528 03-31-23 US Fish & Wildlife US Federal Programs 058448 03-31-23 USDA US Federal Programs P330-16-00211 06-21-24 Utah NELAP PA001462019-8 05-31-23 Virginia NELAP 10043 09-14-23 West Virginia DEP State 142 03-31-23 Wisconsin State 998027800 08-31-23 * Accreditation/Certification renewal pending - accreditation/certification considered valid. Eurofins Lancaster Laboratories Environment Testing, LLC Page 54 of 63 3/30/2023 Method Summary Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Job ID: 410-119189-1 Method Method Description Protocol Laboratory 8260D Volatile Organic Compounds by GC/MS SW846 ELLE 8260D SIM 14D Volatile Organic Compounds (GC/MS) SW846 ELLE 8270E Semivolatile Organic Compounds (GC/MS) SW846 ELLE 8081B Organochlorine Pesticides (GC) SW846 ELLE 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography SW846 ELLE 8151A Herbicides (GC) SW846 ELLE EPA 8141 B Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique SW846 EET PIT EPA 300.0 R2.1 Anions, Ion Chromatography EPA ELLE 6020E Metals (ICP/MS) SW846 ELLE 7470A Mercury (CVAA) SW846 ELLE 2320B-2011 Alkalinity, Total SM ELLE 353.2 Nitrate by Calculation EPA ELLE 353.2 Nitrogen, Nitrate -Nitrite EPA ELLE 353.2 Nitrogen, Nitrite EPA ELLE 4500 S2 D-2011 Sulfide, Total SM ELLE 9012B Cyanide, Total andor Amenable SW846 ELLE SM 2540C Solids, Total Dissolved (TDS) SM ELLE 3005A Preparation, Total Recoverable or Dissolved Metals SW846 ELLE 3510C Liquid -Liquid Extraction (Separatory Funnel) SW846 EET PIT 3510C Liquid -Liquid Extraction (Separatory Funnel) SW846 ELLE 5030E Purge and Trap SW846 ELLE 5030C Purge and Trap SW846 ELLE 7470A Preparation, Mercury SW846 ELLE 8151A Extraction (Herbicides) SW846 ELLE 9012B Cyanide, Total and/orAmenable, Distillation SW846 ELLE Protocol References: EPA = US Environmental Protection Agency SM = "Standard Methods For The Examination Of Water And Wastewater' SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL (412)963-7058 ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL (717)656-2300 Eurofins Lancaster Laboratories Environment Testing, LLC Page 55 of 63 3/30/2023 Sample Summary Client: ELM Site Solutions Inc Project/Site: C&D Landfill NC Job ID: 410-119189-1 Lab Sample ID Client Sample ID Matrix Collected Received 410-119189-1 MW-18 Water 03/16/2312:30 03/17/2310:24 410-119189-2 MW-19 Water 03/16/2315:00 03/17/2310:24 410-119189-3 TB-1 Water 03/16/23 00:00 03/17/23 10:24 L Eurofins Lancaster Laboratories Environment Testing LLC Page 56 of 63 3/3072023 �IIIIIIIIIIIIIII�IVWIIII��YIIIIVIIIIINIII'Chain °f Custody Record 410-119189ChainofCustody Sampler T^ Lab PM Weyandt, Barbara A CamerTradungNo(s): CDC No: 410-83363-23061.1 (7iU Phone: E-Mail: q �9 3�2 3�SZ _ Barbara. Weyandt@et.eurofinsus.com State of Origin: NC Page. Page 1 of 1 Company PWSID. ,lob #. ELM Site Solutions Inc Analysis Requested Address Due Date Requested: Preservation Codes: PO BOX 97607 A - HCL M - Hexane 6 - NaOH N -None City: TAT Requested (days): Raleigh C 2nAcelale 0-ZNa02 D Nitric Acid P - Na2O4S - O - Na2S03 State, Zip: Compliance Prolec .' Yes t No NC, 27624 rn n E - NeHSO4 R - Na2S203 F McOH S - H2SO4 G-Amrhlor Phone. PO # o o a o = L n v LL T-TSPDodecah tlrate y H - Ascorbic Add -Acetone I -Ice v MCAA J- Water EFtail. t S fl.�' Ic�.MS WOE '#- norris@elmsitesolutions com TfA�W t� co t a ry� . �I - y Y Z o U 's u o , v 0 c A 0 o — � 9 r x ~ m Ln m � W H 4 K - EDTA P 5 E Y- TrlZrtla L-EDA Project Name ( Project # I C&D Landfill NC 41004947 m a m v m m r rOp v m a w n m rn 0 f LL' = f m a y T c s a A o o d m o q x v e a^ o o v 19 c, H a o ? a_ c a o C O s 2- other (spedty) Other. Site SSOW# Sample Matrix Z.v Z 3 Type (w- --,, E€ o m Z t� N x of �I Sample (C=comp, o-s. cow m m v m of rit o 3 Sample Identification SampleG= rab aT-Th. A -a, a a $ n n H z �, .; H N m H Special Instructions/Note: Preservation Code. N N N N N D N A N N CB .N HB 1Aw —18 Water YL !� X X X !� X X xl G Water X X X X X X X Y. x X X X Water X ?) Water Water Pos le Hazard Identification Sample Disposal (A fee may"sessed if samples are retained longer than i month) Non -Hazard Flammable Skin Irritant Poison B Unknown Radiological Retum To Client EV Disposal By Lab L Archive For Months Deliverable Requested: I, II, III, IV, Other (specify) Special InstructionslOC Requirements: Empty Kit Relinquished by Date Time: Method or Shipment Relinquished by Datefrim : Company 31/3 ?3 30 Receiv d by. Daterrime 3—t-23 Company .MSS Relinquished by Dalerrime: �� Company 3-16 Z3 �v S� Recciyed by DaterTime: -3-110- 2-3 Company Relinquished by QMP ime: Company Received by Date !,us w Compa Cu5 ody Seals Intact: Custody Seal No.: Cooler Temperature(s) °C and Other Remarks Yes n No 7 r Page 57 of 63 vdr Dole/ 3130120 .Q co II co ORIGdy,ID-LNSA (717) 656-2300 I Su -SHIPPING / RECEIVING r A - EUROFINS LANCASTER LABS 2425 NEW HOLLAND PIKE v II LANCAST R, PA 17601 UNITED STATES US �� �Z� •� TO SAMPLE RECEIVING \, �0 n Art }; EUROFINS ENVIRONMENTS Idu NE t 301 ALPHA DRIVE v , RIDC PARK OITTSBURGH PA 15238 (412) 963-7058 H 449 DEPT:4031 _ 11111111111111111111111111111111illllllllllllllfllllllflll �, Ill �11«'�I�ti iN I Su�JJIL,Ju11■,ul�uvi.�u�uu ��n�� � i ncorrec>`ec��temp aS'3 L �'� FedEx Thermometer ID b Express CIF 4 1 Initials R I PT-WI-SR-001 effective 1118118 # ^ ^ 1 ' SATURDAY 12:OOP r TRK# I oz�1i 5'tA 35 6268 2895 PRIORITY OVERNIGHT 15238 0 AGCA' PA —US PIT a x w v ! � i I22 v i 1 a t `I Page 58 of 63 3/30/2023 * r _ r ' 1 h: y 1 - l0 ORIG M ID=LNSA (717) 656-2300 SN- SHIPPING /RECEIVING I i j EUROFINS LANCASTER LABS 2425 NEW HOLLAND PIKE " f o c� LANCAST R. PA 17601 V I l UNITEDTATES US \ �(� TO SAMPLE RECEIVING \, EUROFINS ENVIRONMENT 5 ,u NE F `F ■ ' 301 ALPHA DRIVE w RIDC PARK " PITTSBURGH PA 15238 (412) 963-7050 X 449 DEPT:4031 _ - ` III IIIIIIIIIIIIIIIIIilllllllllllllllllllllllllllllllllllll rt 114'[7n�correc e femp'ue■ru�lw, iQ Q11 � Y � Fe pE Thermometer ID_ Express CF Q� © Initials or N p 1 PT-WI-SR-001 effective 1178/18 a n> TRKN_ SATURDAY 12.00P F � 0201i 5435 6268 2895 ' �� PRIORITY OVERNIGHT r = �O AGCA' 1523$ _ n PA- _PITI I a x w I v i r m '- _.--- 'a^�._R ------------ -- --- -- --- '— - - ---' ) ! it z 1 Page 59 of 63 3/30/2023 N N LL Y C a C -o N cn °¢� o a co 2 � � N h Z N N ca N C c N J a v � a�� oQ.00 m n Z` w oZ m m m N y $US �t 2Z�ZZZSFQ�o'h-o i+.. oa m O u a a E MZOCLOW nF»3>N ` in a' ; �J G £ ELE E 0 m age o m o �� i •m y s o `ul Z o mmoN -.0 = U 2 LA Q y U m c :gym Om EmO p mmcmi m E, o n UO C #� 0' ..-gym ` 2Z NZZ2Q Q-opww s �O U V a d c V d Q mUp W LLU' 2_ Y� O m o a L m u �y . Ya siawe�uoa�o�egwnN le;oy , c+i N, *. m E > o o F a E S 01 t Z m c c EU ..3 O 'C t-a0 •Q �, I.. ry 'O= (Q U, m � `w N W a � O � C m m r«° O� a c m d � U coZ 7 N E m N o N (0W N W (D� I Er a � •T Ir c c `cc" a) - U CA J O C E a c d Q C Om m N C c o g v ¢ i V p W Q m v�j m N a a a d o C m C > > i C C U Z M 5, a: u 02 I SOOSO � X X c0 m w _° a � VI lq �y pl QSWISMI j a i' vQ$f"n co m v E ` i CO O 'e m E m m J W t0 N E:' n a n m N_ EwE E m ;F` 3 v- U U U ,N.} m a O, o E > 0 En w i. E A F n n (/! U a A c E (J J = c J N a m .A i,M m o ° ° x c E E a ac` � a 5 U 10 y~ �� W m W 9 T « 0 E m w m 12 > d C"N w as N CO N CO d w m E d w m ai o c M c)how iu w o E E E E m o o mM r # O d .0o C) E 10: m C E d m w in a Ar� ra- a 3 w v w to c a m C J 0 J � N CO m m U Q O (n J w m c a .1 a V p o o z aL+ N X d 0 0 ii m rn t cc N U-J U-CO ? o O U) (� p (D 0 wcv > — v Z N C a yC, O— O w (% d A A).. o E t V = U O c C •� rn N o) $o'^U a �. rn a� co m m o o m z L '(D O > Z r 0 g m '' N cr N •- N O a: > w m s co LL7 CD — E •.i O v O a a d mood �0 'O w E R� n N i. i.00 m to v� N P7 c z w d '` ao v W c E .p k L t C d U•O_ d mw: a0 wQ d .O w N� m cN '� J w0 � � S G> N cUi V m L U� Eo 7 U W 00 Qc+) .t• Ud Q old r a� E w o O EC) :: !0 ch o mt c z� ow O c R , N 0 E w v � v d Page 60 of 63 3/30/2023 0 d O r+ m L N O co m J� L � Y N N d W lC Y O v a m� C N l6 N <0 0 a C -r 3 � � R O N or- L W N J d v c 10 v` o Q o 'l G ID m Nye 0 'mO m yy o '° U) N OZ N N NNtl] U �x "L xz<zzzxf-Q�nFo ! -mo3� G E E E in i z O a O K to r» >- N d Y ; ..k t c -' U� U U `- C f.1 a C .,. '2 �+ o lL C l0 O 07 °' o `w 3rQ-Q y; % q orn -Z ° JxOQ�2xOuo U-m-c--A`-m m-E. 19-m 0 0--c_ Z Z Q _- - -E _m G- O UL - - - _-- - U_p d_O) ik O N x N Z i Q_. O W W 0 E o a co O V ¢m. o'Q p. QmUO W W U' 2_�YJ 00 8 o..00 '° C • ,.' ,. � "%. T SJ8UIE}I10a_40=J8QWnN lLnOl:, . N,, t N + E ga., _ . m U 06,9 d E J C d \ ` ' o F o a a z co c ode E m m CO 0 c U c O .0 � EO m w r N •- °o w U y�N�I 10++ � � O y 1 U in Z} m«m m 21 m o m N y M O d N E ' c u ' EO N a Q m d <>o c r c o� c si E y U • a'i cn C wo O W t 14 C) to— O d H 3 n m y a a ccm_Ow"WWiONA,6sMyiW om U OvZ:, sapsld0 DOEIB LLS X X aai-s�a•d a wvz mA'N0a1 iEn cdn E . cd F- " ° �jk uc`U) a�P E> E ` a`o9 a • - 40' � O. w N o w 0. N_ C C T ss ling F ?i 2i �Ew as ��n n OW O U O U T a $ao ��E E��t m 11 a�� O L �o d } E E J s z a kJ ) 0)O $,j O N H{ 4'% N. j (0 m E J F d d m D OE cc m —1 m� �. N m a ❑ m fh N co Cl) N co > N W c W m ❑ Z` E! E E o O oo S rc # d# ?! m �0 3 0.. E ;- in n y o > E w d m L J Q O ` fn N q O W a W f A fQ (A 0. 0 c+) F- a ILV OC/1 �_. a m a� J y O ❑' J❑ 0 }g � y N O a _ o c m o m � (Q W a $ 2 U J � c Q o u d U) w1 0 tj lC - 8«4« d Z ` O LL J _. _ Doo O (A (.% U to m > 0 Z Y N m n �v C O — 0 n fA 0)dcmo c0 o E t v _ = U aNi OCP O H O{ 'M ti r i I; N I n m d b N a)N W+ ld m c d E ^ m 00 yt co rn o f z2• 7 N C Z Z u o, c 4 C .. d C C W O f0 t M co � — y• O O as �F I~0 � D a a a fA N d c m _a 2) _a N N r A = m J 160 W , c0 0) 5 `� `� E (0 p a )i CO N Y m .P m .a a .� 0} <7 ` Q .a w ai y c N _ d❑ E , d '' ` °= `' y) o G > .N d E E c c U Uc�CD 01 t o 7 U W O Qm Ud ind av Eo W `U y fq y. m> z1 uLu a ❑ W n� it Page 61 of 63 3/30/2023 Client: ELM Site Solutions Inc Login Number: 119189 List Number: 1 Creator: McBeth, Jessica Question Login Sample Receipt Checklist Job Number: 410-119189-1 List Source: Eurofins Lancaster Laboratories Environment Testing, LLC L Answer Comment The cooler's custody seal is intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable (</=6C, not frozen). True Cooler Temperature is recorded. True WV: Container Temperature is acceptable (</=6C, not frozen). N/A WV: Container Temperature is recorded. N/A COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True There are no discrepancies between the containers received and the COC. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True There is sufficient vol. for all requested analyses. True Is the Field Sampler's name present on COC? True Sample custody seals are intact. True VOA sample vials do not have headspace >6mm in diameter (none, if from True WV)? Eurofins Lancaster Laboratories Environment Testing, LLC Page 62 of 63 3/30/2023 Login Sample Receipt Checklist Client: ELM Site Solutions Inc Job Number: 410-119189-1 Login Number: 119189 List Number: 2 Creator: Kovitch, Christina M Question List Source: Eurofins Pittsburgh List Creation: 03/18/23 05:47 PM Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins Lancaster Laboratories Environment Testing, LLC Page 63 of 63 3/30/2023 Ground Water Sample Collection Record Well/Piezo ID: Client: C&D Landfill, Inc. Date: A _ 23 Project Name: C&D Landfill Phase 3 Project Number: Site Location: Greenville. NC Start Time: Weather Conditions: Finish Time: WELLIWATER LEVEL DATA: (measured from top of casing) a. Total Well Depth: b. Casing Material: PVC c. Casing Diameter: 2' d. Screen Length: 1 b a a Depth to Water: �. 11.i f. Pump Intake In Screen Depth: g. Water Column: h. Well Volume: WELL PURGING DATA: a. Purge Method: Low -flow b. Acceptance Criteria: Minimum Required Purge Volume (@ well volumes) NA C. Field Testing Equipment Used: Make: YSi Model: Pro Plus Serial Number: d_ Feld Testing Equipment Calibration Docum ntati �n {\ ?U' Volume Removed �I) ( pH (units) Specific Conductivity Turbidity (NTUs) DO (mg(L) ORP (mV) Color Pumping Rate (ml/min) WdteF Level (fit) ®. t• Cam- 3 'L c) I.1,5 % .1 5IL t q e Z� I 1t 0 S.i.3 isA i f5.C) o .V s. & U, I I.- 2.0 I I to. i,•Iv i. .16 1- k.- 2.z5 G-S 5-6 (0(0.16 ®. t ©.`L k -- e. Stabilization Criteria: 3% +/-0.1 3% f. Acceptance criteria pass/fail Has required volume been removed? Has required turbidity been reached (10%)? Have parameters stabilized? If No or N/A — Explain below 10% 10% +/-10mv Yes No N/A ElE3 E❑ [ ❑ ❑ SAMPLE COLLECTION: Method: Peristaltic PunnD w/Pohtethylene Tubing Sample ID Container Type No. of Containers Preservation Analysis Time —14s Various 23 Various Landfill Parameters v7,3 o Additional Comments - Signature: Date: Ground Water Sample Collection Record Well/Piezn iC1: M Ins—t Client: C&D Landfill Inc. Date: Project Name: C&D Landfill Phase 3 Project Number: Site Location: Gr enville NC Start Time: _ Weather Conditions: . Finish Time: WELLIWATER LEVEL DATA: (measured from top of casing) a. Total Well Depth: Z3 b. Casing Material: PVC c. Casing Diameter: 2" t � d. Screen Length: d e. Depth to Water: 4-Q f_ Pump Intake In Screen Depth: g. Water Column: h. Well Volume: WELL PURGING DATA: a. Purge Method: Low -flow b. Acceptance Criteria: Minimum Required Purge Volume (@ well volumes) NA c. Field Testing Equipment Used: Make: YSI Model: Pro Plus Serial Number: d. Field Testing Equipment Calibration Docum ntati n I, ,--,- C, .A •� . Turbidity , i ®lSkil � � W lam DIM ffui� Sim� k ©. e. Stabilization Criteria: 3% +/-0.1 3°% f. Acceptance criteria pass/fail Has required volume been removed? Has required turbidity been reached (10%)? Have parameters stabilized? If No or N/A— Explain below 100A 100A +/-10mV Yes No N/A ❑ ❑l i�e' ❑y LJ El iJ ❑ ❑ SAMPLE COLLECTION: Method: Peristaltic Pump w/Polyethylene Tubin>i Sample ID Container Type No. of Containers Preservation Analysis Time — kci various 23 Various Landfill Parameters Additional Comments. Signature: ---.• Date:-� �- WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: DAVID HALL Well Contractor Name (or well owner personally abandoning well on his/her property) A - 4459 NC Well Contractor Certification Number GEOLOGIC EXPLORATION Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. County, State, Variance, etc) ifknown 3. Well use (check well use): Water Supply Well: ❑Agricultural ❑Municipal/Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑hidustrial/Commercial El Residential Water Supply (shared) ❑Irrigation Non -Water Supply Well: El Aquifer Recharge ❑Aquifer Storage and Recovery El Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling 4. Date well(s) abandoned- 5a. Well location: C&D LANDFILL El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑ Subsidence Control ❑Tracer El Other (explain under 7g) 03/09/23 Facility/Owner Name Facility ID# (if applicable) 802 RECYCLING LANE GREENVILLE 27834 Physical Address, City, and Zip PITT County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 350 37' 15.19" N 770 10' 54.20" W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction records) if available. For multiple injection or non -water supply wells ONLY with the same construction abandonment, you can submit one form. 6a. Well ID#: PZ-6 6b. Total well depth: 5.0 (ft.) 6c. Borehole diameter: 8.0 (in.) 6d. Water level below ground surface: 3.0 (ft.) 6e. Outer casing length (if known): (ft.) 6f. Inner casing/tubing length (if known): (ft.) For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: 1 For multiple injection or non -water supply wells ONLY with the same construction/abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): 5.0 (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d. Amount of disinfectant used: 7e. Sealing materials used (check all that apply): El Neat Cement Grout ❑ Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑ Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑ Bentonite Slurry ❑ Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: 13.0 GALLONS 7g. Provide a brief description of the abandonment procedure: OVERDRILLED WITH 4 1/4" ID AUGERS AND TREMIE GROUTED FROM BOTTOM 8. Certification: 03/31/23 Signature of Certified Well Contractor or Well Owner Date By signing this form, I hereby certify that the well(s) was (were) abandoned in accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Submit this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Iniection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. 6g. Screen length (if known): (ft.) Form GW-30 North Carolina Department of Environment and Natural Resources - Division of Water Quality Revised March 2013 WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: DAVID HALL Well Contractor Name (or well owner personally abandoning well on his/her property) A - 4459 NC Well Contractor Certification Number GEOLOGIC EXPLORATION Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. County, State, Variance, etc) ifknown 3. Well use (check well use): Water Supply Well: ❑Agricultural ❑Municipal/Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑hidustrial/Commercial El Residential Water Supply (shared) ❑Irrigation Non -Water Supply Well: El Aquifer Recharge ❑Aquifer Storage and Recovery El Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling 4. Date well(s) abandoned- 5a. Well location: C&D LANDFILL El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑ Subsidence Control ❑Tracer El Other (explain under 7g) 03/09/23 Facility/Owner Name Facility ID# (if applicable) 802 RECYCLING LANE GREENVILLE 27834 Physical Address, City, and Zip PITT County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 350 37' 15.19" N 770 10' 54.20" W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction records) if available. For multiple injection or non -water supply wells ONLY with the same construction abandonment, you can submit one form. 6a. Well ID#: PZ-6 6b. Total well depth: 5.0 (ft.) 6c. Borehole diameter: 8.0 (in.) 6d. Water level below ground surface: 3.0 (ft.) 6e. Outer casing length (if known): (ft.) 6f. Inner casing/tubing length (if known): (ft.) For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: 1 For multiple injection or non -water supply wells ONLY with the same construction/abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): 5.0 (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d. Amount of disinfectant used: 7e. Sealing materials used (check all that apply): El Neat Cement Grout ❑ Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑ Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑ Bentonite Slurry ❑ Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: 13.0 GALLONS 7g. Provide a brief description of the abandonment procedure: OVERDRILLED WITH 4 1/4" ID AUGERS AND TREMIE GROUTED FROM BOTTOM 8. Certification: 03/31/23 Signature of Certified Well Contractor or Well Owner Date By signing this form, I hereby certify that the well(s) was (were) abandoned in accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Submit this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Iniection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. 6g. Screen length (if known): (ft.) Form GW-30 North Carolina Department of Environment and Natural Resources - Division of Water Quality Revised March 2013 WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: DAVID HALL Well Contractor Name (or well owner personally abandoning well on his/her property) A - 4459 NC Well Contractor Certification Number GEOLOGIC EXPLORATION Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. County, State, Variance, etc) ifknown 3. Well use (check well use): Water Supply Well: ❑Agricultural ❑Municipal/Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑hidustrial/Commercial El Residential Water Supply (shared) ❑Irrigation Non -Water Supply Well: El Aquifer Recharge ❑Aquifer Storage and Recovery El Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling 4. Date well(s) abandoned- 5a. Well location: C&D LANDFILL El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑ Subsidence Control ❑Tracer El Other (explain under 7g) 03/09/23 Facility/Owner Name Facility ID# (if applicable) 802 RECYCLING LANE GREENVILLE 27834 Physical Address, City, and Zip PITT County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 350 37' 15.19" N 770 10' 54.20" W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction records) if available. For multiple injection or non -water supply wells ONLY with the same construction abandonment, you can submit one form. 6a. Well ID#: PZ-6 6b. Total well depth: 5.0 (ft.) 6c. Borehole diameter: 8.0 (in.) 6d. Water level below ground surface: 3.0 (ft.) 6e. Outer casing length (if known): (ft.) 6f. Inner casing/tubing length (if known): (ft.) For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: 1 For multiple injection or non -water supply wells ONLY with the same construction/abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): 5.0 (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d. Amount of disinfectant used: 7e. Sealing materials used (check all that apply): El Neat Cement Grout ❑ Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑ Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑ Bentonite Slurry ❑ Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: 13.0 GALLONS 7g. Provide a brief description of the abandonment procedure: OVERDRILLED WITH 4 1/4" ID AUGERS AND TREMIE GROUTED FROM BOTTOM 8. Certification: 03/31/23 Signature of Certified Well Contractor or Well Owner Date By signing this form, I hereby certify that the well(s) was (were) abandoned in accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Submit this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Iniection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. 6g. Screen length (if known): (ft.) Form GW-30 North Carolina Department of Environment and Natural Resources - Division of Water Quality Revised March 2013 WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: DAVID HALL Well Contractor Name (or well owner personally abandoning well on his/her property) A - 4459 NC Well Contractor Certification Number GEOLOGIC EXPLORATION Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. County, State, Variance, etc) ifknown 3. Well use (check well use): Water Supply Well: ❑Agricultural ❑Municipal/Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑hidustrial/Commercial El Residential Water Supply (shared) ❑Irrigation Non -Water Supply Well: El Aquifer Recharge ❑Aquifer Storage and Recovery El Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling 4. Date well(s) abandoned- 5a. Well location: C&D LANDFILL El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑ Subsidence Control ❑Tracer El Other (explain under 7g) 03/09/23 Facility/Owner Name Facility ID# (if applicable) 802 RECYCLING LANE GREENVILLE 27834 Physical Address, City, and Zip PITT County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 350 37' 15.19" N 770 10' 54.20" W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction records) if available. For multiple injection or non -water supply wells ONLY with the same construction abandonment, you can submit one form. 6a. Well ID#: PZ-6 6b. Total well depth: 5.0 (ft.) 6c. Borehole diameter: 8.0 (in.) 6d. Water level below ground surface: 3.0 (ft.) 6e. Outer casing length (if known): (ft.) 6f. Inner casing/tubing length (if known): (ft.) For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: 1 For multiple injection or non -water supply wells ONLY with the same construction/abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): 5.0 (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d. Amount of disinfectant used: 7e. Sealing materials used (check all that apply): El Neat Cement Grout ❑ Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑ Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑ Bentonite Slurry ❑ Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: 13.0 GALLONS 7g. Provide a brief description of the abandonment procedure: OVERDRILLED WITH 4 1/4" ID AUGERS AND TREMIE GROUTED FROM BOTTOM 8. Certification: 03/31/23 Signature of Certified Well Contractor or Well Owner Date By signing this form, I hereby certify that the well(s) was (were) abandoned in accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Submit this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Iniection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. 6g. Screen length (if known): (ft.) Form GW-30 North Carolina Department of Environment and Natural Resources - Division of Water Quality Revised March 2013 WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: DAVID HALL Well Contractor Name (or well owner personally abandoning well on his/her property) A - 4459 NC Well Contractor Certification Number GEOLOGIC EXPLORATION Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. County, State, Variance, etc) ifknown 3. Well use (check well use): Water Supply Well: ❑Agricultural ❑Municipal/Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑hidustrial/Commercial El Residential Water Supply (shared) ❑Irrigation Non -Water Supply Well: El Aquifer Recharge ❑Aquifer Storage and Recovery El Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling 4. Date well(s) abandoned- 5a. Well location: C&D LANDFILL El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑ Subsidence Control ❑Tracer El Other (explain under 7g) 03/09/23 Facility/Owner Name Facility ID# (if applicable) 802 RECYCLING LANE GREENVILLE 27834 Physical Address, City, and Zip PITT County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 350 37' 15.19" N 770 10' 54.20" W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction records) if available. For multiple injection or non -water supply wells ONLY with the same construction abandonment, you can submit one form. 6a. Well ID#: PZ-6 6b. Total well depth: 5.0 (ft.) 6c. Borehole diameter: 8.0 (in.) 6d. Water level below ground surface: 3.0 (ft.) 6e. Outer casing length (if known): (ft.) 6f. Inner casing/tubing length (if known): (ft.) For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: 1 For multiple injection or non -water supply wells ONLY with the same construction/abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): 5.0 (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d. Amount of disinfectant used: 7e. Sealing materials used (check all that apply): El Neat Cement Grout ❑ Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑ Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑ Bentonite Slurry ❑ Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: 13.0 GALLONS 7g. Provide a brief description of the abandonment procedure: OVERDRILLED WITH 4 1/4" ID AUGERS AND TREMIE GROUTED FROM BOTTOM 8. Certification: 03/31/23 Signature of Certified Well Contractor or Well Owner Date By signing this form, I hereby certify that the well(s) was (were) abandoned in accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Submit this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Iniection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. 6g. Screen length (if known): (ft.) Form GW-30 North Carolina Department of Environment and Natural Resources - Division of Water Quality Revised March 2013 WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: DAVID HALL Well Contractor Name (or well owner personally abandoning well on his/her property) A - 4459 NC Well Contractor Certification Number GEOLOGIC EXPLORATION Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. County, State, Variance, etc) ifknown 3. Well use (check well use): Water Supply Well: ❑Agricultural ❑Municipal/Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑hidustrial/Commercial El Residential Water Supply (shared) ❑Irrigation Non -Water Supply Well: El Aquifer Recharge ❑Aquifer Storage and Recovery El Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling 4. Date well(s) abandoned- 5a. Well location: C&D LANDFILL El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑ Subsidence Control ❑Tracer El Other (explain under 7g) 03/09/23 Facility/Owner Name Facility ID# (if applicable) 802 RECYCLING LANE GREENVILLE 27834 Physical Address, City, and Zip PITT County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 350 37' 15.19" N 770 10' 54.20" W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction records) if available. For multiple injection or non -water supply wells ONLY with the same construction abandonment, you can submit one form. 6a. Well ID#: PZ-6 6b. Total well depth: 5.0 (ft.) 6c. Borehole diameter: 8.0 (in.) 6d. Water level below ground surface: 3.0 (ft.) 6e. Outer casing length (if known): (ft.) 6f. Inner casing/tubing length (if known): (ft.) For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: 1 For multiple injection or non -water supply wells ONLY with the same construction/abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): 5.0 (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d. Amount of disinfectant used: 7e. Sealing materials used (check all that apply): El Neat Cement Grout ❑ Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑ Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑ Bentonite Slurry ❑ Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: 13.0 GALLONS 7g. Provide a brief description of the abandonment procedure: OVERDRILLED WITH 4 1/4" ID AUGERS AND TREMIE GROUTED FROM BOTTOM 8. Certification: 03/31/23 Signature of Certified Well Contractor or Well Owner Date By signing this form, I hereby certify that the well(s) was (were) abandoned in accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Submit this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Iniection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. 6g. Screen length (if known): (ft.) Form GW-30 North Carolina Department of Environment and Natural Resources - Division of Water Quality Revised March 2013 1/4" POLY TUBING SILICONE SEAL STOPCOCK VALVE INVERTED 5-GALLON BUCKET GROUND SURFACE II COMPACTED SOIL BACKFILL - U 1.0' GROUND SURFACE i SEASONAL HIGH WATER TABLE Detail- Landfill Gas Probe Schematic for LFG-3-1 and LFG-3-2 SITE NAME: C&D Landfill, Inc. Greenville, North Carolina SCALE:NTS WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only: 1. Well Contractor Information: DAVID HALL Well Contractor Name A - 4459 NC Well Contractor Certification Number GEOLOGIC EXPLORATION Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc) 3. Well Use (check well use): Water Supply Well: ❑Agricultural ❑Geotherral (Heating/Cooling Supply) ❑ Industrial/Commercial ❑ Irrigation Non -Water Supply Well: ❑Aquifer Recharge El Aquifer Storage and Recovery El Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cool 4. Date Well(s) Completed: 5a. Well Location: C&D LANDFILL ❑Municipal/Public El Residential Water Supply (single) ❑Residential Water Supply (shared) ❑ Wells > 100,000 GPD ❑Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑Subsidence Control ❑Tracer El Other (explain under #21 F 03/09/23 Well ID# MW-18 Facility/Owner Name Facility ID# (if applicable) 802 RECYCLING LANE GREENVILLE 27834 Physical Address, City, and Zip PITT County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 770 10' 54.20" N 770 10' 54.20" W 6. Is(are) the well(s): [EPermanent or ❑Temporary 7. Is this a repair to an existing well: ❑Yes or ONo If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this farm. 8. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells drilled: 9. Total well depth below land surface: 20.0 (ft.) For multiple wells list all depths if different (example- 3@200' and 2@100) 14. WATER ZONES FROM TO DESCRIPTION rt. rt. ft. ft. 15. OUTER CASING for multi -cased wells OR LINER if a licable FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING eother at closed -loop) FROM TO DIAMETER THICKNESS MATERIAL 0.0 tt• 10.0 tt• 2.0 in. SCH 40 PVC fL fL in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL 10.0 ft' 20.0 ft' 2.0 in. .010 SCH 40 PVC ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT 0.0 ft. 5.0 ft. PORTLANDBENTONrrE SLURRY ft. ft. rL rt. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD 8.0 tt• 20.0 tt• 20-40 FINE SILICA SAND rt. rt. 20. DRILLING LOG attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) 0.0 It. 5.0 ft' BROWN SAND 5.0 ft' 20.0 ft' TAN SAND rt. et. rt. et. ft. tt. rt. et. 21. REMARKS BENTONITE SEAL - 5.0 - 8.0 FEET 22. Certification: Signature of Certified Well Contractor 03/31/23 Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 1 SA NCAC 02C .0100 or 1 SA NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well construction info (add'See Over' in Remarks Box). You may also attach additional pages if necessary. 24. SUBMITTAL INSTRUCTIONS Submit this GW-1 within 30 days of well completion per the following: 10. Static water level below top of casing: 3.0 (ft.) 24a. For All Wells: Original form to Division of Water Resources (DWR), If water level is above casing, use "+ " 11. Borehole diameter: 80 (in.) AUGER 12. Well construction method: _ (i.e. auger, rotary, cable, direct push, etc.) Information Processing Unit, 1617 MSC, Raleigh, NC 27699-1617 24b. For Igiection Wells: Copy to DWR, Underground Injection Control (NC) Program, 1636 MSC, Raleigh, NC 27699-1636 24c. For Water Supply and Open -Loop Geothermal Return Wells: Copy to the county environmental health department of the county where installed FOR WATER SUPPLY WELLS ONLY: 24d. For Water Wells producing over 100,000 GPD: Copy to DWR, CCPCUA 13a. Yield (gpm) Method of test: Permit Program, 1611 MSC, Raleigh, NC 27699-1611 13b. Disinfection type: Amount: Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 6-6-2018 WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only: 1. Well Contractor Information: DAVID HALL Well Contractor Name A - 4459 NC Well Contractor Certification Number GEOLOGIC EXPLORATION Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc) 3. Well Use (check well use): Water Supply Well: ❑Agricultural ❑Geotherral (Heating/Cooling Supply) ❑ Industrial/Commercial ❑ Irrigation Non -Water Supply Well: ❑Aquifer Recharge El Aquifer Storage and Recovery El Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cool 4. Date Well(s) Completed: 5a. Well Location: C&D LANDFILL ❑Municipal/Public El Residential Water Supply (single) ❑Residential Water Supply (shared) ❑ Wells > 100,000 GPD ❑Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑Subsidence Control ❑Tracer El Other (explain under #21 F 03/09/23 Well ID# MW-18 Facility/Owner Name Facility ID# (if applicable) 802 RECYCLING LANE GREENVILLE 27834 Physical Address, City, and Zip PITT County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 770 10' 54.20" N 770 10' 54.20" W 6. Is(are) the well(s): [EPermanent or ❑Temporary 7. Is this a repair to an existing well: ❑Yes or ❑No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this farm. 8. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells drilled: 9. Total well depth below land surface: 20.0 (ft.) For multiple wells list all depths if different (example- 3@200' and 2@100) 14. WATER ZONES FROM TO DESCRIPTION rt. rt. ft. ft. 15. OUTER CASING for multi -cased wells OR LINER if a licable FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING eother at closed -loop) FROM TO DIAMETER THICKNESS MATERIAL 0.0 tt• 10.0 tt• 2.0 in. SCH 40 PVC fL fL in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL 10.0 ft' 20.0 ft' 2.0 in. .010 SCH 40 PVC ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT 0.0 ft. 5.0 ft. PORTLANDBENTONITE SLURRY ft. ft. rL rt. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD 8.0 tt• 20.0 tt• 20-40 FINE SILICA SAND rt. rt. 20. DRILLING LOG attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) 0.0 It. 5.0 ft' BROWN SAND 5.0 ft' 20.0 ft' TAN SAND rt. et. rt. et. ft. tt. rt. et. 21. REMARKS BENTONITE SEAL - 5.0 - 8.0 FEET 22. Certification: Signature of Certified Well Contractor 03/31/23 Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 1 SA NCAC 02C .0100 or 1 SA NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well construction info (add'See Over' in Remarks Box). You may also attach additional pages if necessary. 24. SUBMITTAL INSTRUCTIONS Submit this GW-1 within 30 days of well completion per the following: 10. Static water level below top of casing: 3.0 (ft.) 24a. For All Wells: Original form to Division of Water Resources (DWR), If water level is above casing, use "+ " 11. Borehole diameter: 80 (in.) AUGER 12. Well construction method: _ (i.e. auger, rotary, cable, direct push, etc.) Information Processing Unit, 1617 MSC, Raleigh, NC 27699-1617 24b. For Igiection Wells: Copy to DWR, Underground Injection Control (NC) Program, 1636 MSC, Raleigh, NC 27699-1636 24c. For Water Supply and Open -Loop Geothermal Return Wells: Copy to the county environmental health department of the county where installed FOR WATER SUPPLY WELLS ONLY: 24d. For Water Wells producing over 100,000 GPD: Copy to DWR, CCPCUA 13a. Yield (gpm) Method of test: Permit Program, 1611 MSC, Raleigh, NC 27699-1611 13b. Disinfection type: Amount: Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 6-6-2018 WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only: 1. Well Contractor Information: DAVID HALL Well Contractor Name A - 4459 NC Well Contractor Certification Number GEOLOGIC EXPLORATION Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc) 3. Well Use (check well use): Water Supply Well: ❑Agricultural ❑Geotherral (Heating/Cooling Supply) ❑ Industrial/Commercial ❑ Irrigation Non -Water Supply Well: ❑Aquifer Recharge El Aquifer Storage and Recovery El Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cool 4. Date Well(s) Completed: 5a. Well Location: C&D LANDFILL ❑Municipal/Public El Residential Water Supply (single) ❑Residential Water Supply (shared) ❑ Wells > 100,000 GPD ❑Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑Subsidence Control ❑Tracer El Other (explain under #21 F 03/09/23 Well ID# MW-18 Facility/Owner Name Facility ID# (if applicable) 802 RECYCLING LANE GREENVILLE 27834 Physical Address, City, and Zip PITT County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 770 10' 54.20" N 770 10' 54.20" W 6. Is(are) the well(s): [EPermanent or ❑Temporary 7. Is this a repair to an existing well: ❑Yes or ❑No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this farm. 8. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells drilled: 9. Total well depth below land surface: 20.0 (ft.) For multiple wells list all depths if different (example- 3@200' and 2@100) 14. WATER ZONES FROM TO DESCRIPTION rt. rt. ft. ft. 15. OUTER CASING for multi -cased wells OR LINER if a licable FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING eother at closed -loop) FROM TO DIAMETER THICKNESS MATERIAL 0.0 tt• 10.0 tt• 2.0 in. SCH 40 PVC fL fL in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL 10.0 ft' 20.0 ft' 2.0 in. .010 SCH 40 PVC ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT 0.0 ft. 5.0 ft. PORTLANDBENTONITE SLURRY ft. ft. rL rt. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD 8.0 tt• 20.0 tt• 20-40 FINE SILICA SAND rt. rt. 20. DRILLING LOG attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) 0.0 It. 5.0 ft' BROWN SAND 5.0 ft' 20.0 ft' TAN SAND rt. et. rt. et. ft. tt. rt. et. 21. REMARKS BENTONITE SEAL - 5.0 - 8.0 FEET 22. Certification: Signature of Certified Well Contractor 03/31/23 Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 1 SA NCAC 02C .0100 or 1 SA NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well construction info (add'See Over' in Remarks Box). You may also attach additional pages if necessary. 24. SUBMITTAL INSTRUCTIONS Submit this GW-1 within 30 days of well completion per the following: 10. Static water level below top of casing: 3.0 (ft.) 24a. For All Wells: Original form to Division of Water Resources (DWR), If water level is above casing, use "+ " 11. Borehole diameter: 80 (in.) AUGER 12. Well construction method: _ (i.e. auger, rotary, cable, direct push, etc.) Information Processing Unit, 1617 MSC, Raleigh, NC 27699-1617 24b. For Igiection Wells: Copy to DWR, Underground Injection Control (NC) Program, 1636 MSC, Raleigh, NC 27699-1636 24c. For Water Supply and Open -Loop Geothermal Return Wells: Copy to the county environmental health department of the county where installed FOR WATER SUPPLY WELLS ONLY: 24d. For Water Wells producing over 100,000 GPD: Copy to DWR, CCPCUA 13a. Yield (gpm) Method of test: Permit Program, 1611 MSC, Raleigh, NC 27699-1611 13b. Disinfection type: Amount: Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 6-6-2018