Loading...
HomeMy WebLinkAbout5002_JacksonCounty_MSWLF_Oct22GW_FID1776935_20230315DENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event#: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reoortina Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Anchor QEA of North Carolina, PLLC Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Chuck Pippin Phone: 828-281-3350 E-mail: cpippin@anchorgea.com NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006) Jackson County Municipal Solid US Highway 441 50-02 .1600 October 3 & 4, 2022 Waste Landfill Dillsboro, North Carolina 28725 Environmental Status: (Check all that apply) Initial/Background Monitoring 0 Detection Monitoring Assessment Monitoring Corrective Action T e of data submitted: (Check all that apply) X Groundwater monitoring data from monitoring wells Methane gas monitoring data X Groundwater monitoring data from private water supply wells Corrective action data (specify) X Leachate monitoring data ❑ X Surface water monitoring data Other(specify) No. No groundwater or surface water standards were exceeded. Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Chuck Pippin, P.G. Project Manager 828-281-3350 Facility Represent —t!:�'_itle (Area Code) Telephone Number Affix NC Licensed/ Professional Geologist Seal Signature j // / { / Date 231 Haywood Street Asheville, North Carolina 28801 Facility Representative Address P-1649 NC PE Firm License Number (if applicable effective May 1, 2009) I. \A C A R o •.,,, GEN 1587 2? ��ykcFOLOG�S�`Q� . S G. ­00 Revised 6/2009 F r l l i March 2023 ANCHOR Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 ISz QEA Fall 2022 Semiannual Water Quality Monitoring Report Prepared for Jackson County Solid Waste Department March 2023 Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 Fall 2022 Semiannual Water Quality Monitoring Report Prepared for Jackson County Solid Waste Department 401 Grindstaff Cove Road Sylva, North Carolina 28779 -, �' m�Ww-' A�� ProjectChuck Pipp -... Prepared by Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Jessica Mayer St;ef Professional Project Number: C01480-01.02 \\Wcl-fs1\asheville\Projects\Jackson County\ -Reports - Groundwater\2022\02_Fall 2022\Text\Jackson County -Semiannual Water Quality Report_Fa I I_2022.docx Table of Contents Table of Contents Abbreviations 1 Introduction iv 1 2 Semiannual Monitoring...........................................................................................................3 2.1 Groundwater, Surface Water, Domestic Well, and Leachate Sampling..........................................3 2.1.1 Monitoring Well Purging and Sampling Methods.................................................................3 2.1.2 Surface Water Sampling Methods................................................................................................4 2.1.3 Leachate Sampling Methods..........................................................................................................5 2.1.4 Domestic Well Sampling Methods...............................................................................................5 2.2 Sample Handling, Documentation, and Analysis....................................................................................5 2.2.1 Sampling Schedule.............................................................................................................................5 2.2.2 Fall 2022 Sampling..............................................................................................................................6 3 Findings........................................................................................................................................8 3.1 Groundwater.........................................................................................................................................................8 3.1.1 Field Parameters..................................................................................................................................9 3.1.2 Appendix II Metals (Total)................................................................................................................9 3.1.3 Appendix II Metals (Dissolved).................................................................................................... 10 3.1.4 Appendix II VOCs and 1,4-Dioxane........................................................................................... 10 3.2 Surface Water.................................................................................................................................................... 11 3.2.1 Field Parameters............................................................................................................................... 11 3.2.2 Appendix II Metals........................................................................................................................... 12 3.2.3 Appendix II VOCs and 1,4-Dioxane........................................................................................... 12 3.3 Leachate...............................................................................................................................................................12 3.4 Domestic Well.................................................................................................................................................... 13 3.4.1 Field Parameters............................................................................................................................... 13 3.4.2 VOCs...................................................................................................................................................... 13 3.5 Groundwater Flow Directions...................................................................................................................... 13 4 Summary....................................................................................................................................15 4.1 Groundwater Quality...................................................................................................................................... 15 4.1.1 Appendix II Metals........................................................................................................................... 15 4.1.2 Appendix II Volatile Organic Compounds and 1,4-Dioxane............................................ 15 Fall 2022 Semiannual Water Quality Monitoring Report i March 2023 4.1.3 Field Parameters and Other Constituents............................................................................... 15 4.2 Surface Water Quality..................................................................................................................................... 16 4.2.1 Appendix II Metals........................................................................................................................... 16 4.2.2 Appendix II Volatile Organic Compounds and 1,4-Dioxane............................................ 16 4.2.3 Field Parameters and Other Constituents............................................................................... 16 4.3 Leachate Quality............................................................................................................................................... 16 4.4 Domestic Well Water Quality...................................................................................................................... 17 5 Future Activities 6 References TABLES Table 1 Summary of Laboratory Analyses Performed on Samples Table 2 Well Construction Details and Corresponding Elevations Table 3 Analytical Summary Table 4 Mass Removal Calculations for VOCs Detected in the Leachate Sample (LT-01) FIGURES Figure 1 Site Location Map Figure 2 Site Layout Map Figure 3 Generalized Groundwater Flow Direction Figure 4 Hydrograph and Constituents of Concern Versus Time — MW-01 Figure 5 Hydrograph and Constituents of Concern Versus Time — MW-02 Figure 6 Hydrograph and Constituents of Concern Versus Time — MW-03 Figure 7 Hydrograph and Constituents of Concern Versus Time — MW-04 Figure 8 Hydrograph and Constituents of Concern Versus Time — MW-05R Figure 9 Hydrograph and Constituents of Concern Versus Time — MW-06 Figure 10 Hydrograph and Constituents of Concern Versus Time — MW-07 im 19 APPENDICES Appendix A Well Sampling Logs, and Equipment Documentation and Instrument Calibration Data Sheets Appendix B Reports of Laboratory Analysis, Chain -of -Custody Documentation, and Certificates of Analysis Fall 2022 Semiannual Water Quality Monitoring Report ii March 2023 Abbreviations pg/L micrograms per liter pmhos/cm micromhos per centimeter 2L standard 15A NCAC 2L.0202 Groundwater Standard CAER Five -Year Corrective Action Evaluation Report CAP Corrective Action Plan DEQ North Carolina Department of Environmental Quality DO dissolved oxygen EPA U.S. Environmental Protection Agency IMAC interim maximum allowable concentration J joule MDL method detection limit mg/L milligrams per liter MNA monitored natural attenuation mV millivolts NCAC North Carolina Administrative Code NTU nephelometric turbidity unit ORP oxidation reduction potential PWR partially weathered rock SC specific conductivity Site closed Municipal Solid Waste Landfill SM Standard Method SU standard unit SWS Solid Waste Section TWSA Tuckasegee Water & Sewer Authority VOC volatile organic compound Fall 2022 Semiannual Water Quality Monitoring Report iii March 2023 1 Introduction The Jackson County Solid Waste Department maintains a closed Municipal Solid Waste Landfill (Site) approximately 0.75 mile west of Dillsboro, North Carolina, on the northeast side of Old Dillsboro Road (Old U.S. Highway 74; Figure 1). Water quality monitoring at the landfill is governed by the North Carolina Department of Environmental Quality (DEQ), Division of Waste Management, Solid Waste Section (SWS), under Permit No. 50-02 issued to Jackson County. The landfill permit requires semiannual monitoring of groundwater and surface water quality. Since October 2007, when Anchor QEA of North Carolina, PLLC began performing water quality monitoring events at the Site, groundwater quality monitoring has indicated persistent low-level concentrations of constituents that exceeded groundwater quality standards. In response to the continued exceedances of the analyzed constituents, an Assessment of Corrective Measures was submitted to the North Carolina Department of Environment and Natural Resources (now DEQ) on September 7, 2010 (Altamont 2010). A Corrective Action Plan (CAP; Altamont 2011) was implemented upon approval by the North Carolina Department of Environmental and Natural Resources, as recorded in the September 1, 2011, letter regarding "Approval of the County's Corrective Action Plan" (DENR 2011). The implemented remedy includes the extraction of leachate through dedicated submersible pumps installed within landfill gas extraction wells and disposal of the leachate into the Tuckasegee Water & Sewer Authority (TWSA) collection system. In addition to the leachate extraction, groundwater natural attenuation parameters are monitored, and natural attenuation processes are evaluated. As discussed in the CAP, a corrective action evaluation report is prepared every 5 years. The evaluation report analyzes the progress of the approved corrective action remedy based on semiannual water quality monitoring data. The remedy was implemented in a phased approach, with full implementation occurring on September 6, 2013. The first Five -Year Corrective Action Evaluation Report (CAER), submitted by Altamont on October 31, 2016 (Altamont 2016), concluded that the current conditions of the monitored natural attenuation (MNA) parameters and Site geochemical parameters allow for the slow degradation of the select contaminants identified in the CAER. The second CAER was submitted by Anchor QEA on January 13, 2022, and concluded that the leachate extraction system has improved but still does not align with the anticipated performance as modeled in the CAP. This report serves as the second semiannual water quality monitoring report for 2022. The report provides an evaluation of groundwater and surface water quality. The water quality monitoring network is presented in Figure 2. The generalized groundwater flow direction in the upper parts of the underlying aquifer system is provided in Figure 3. In addition to groundwater and surface water monitoring, this report includes analysis of the extracted leachate and two domestic water wells. The water samples collected from selected monitoring points during the fall sampling event were analyzed for a range of parameters, as presented in Section 2.2 and Table 1. The fall 2022 sampling Fall 2022 Semiannual Water Quality Monitoring Report 1 March 2023 event was performed on October 3 and 4, 2022. Due to laboratory error, a resampling event for pesticide analysis was performed on January 9 and 10, 2023. These sampling efforts are being reported in accordance with requirements stipulated in the DEQ Solid Waste Management Rules codified under Title 15A, Subchapter 13B of the North Carolina Administrative Code (NCAC). Fall 2022 Semiannual Water Quality Monitoring Report 2 March 2023 2 Semiannual Monitoring 2.1 Groundwater, Surface Water, Domestic Well, and Leachate Sampling The Site monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06, and MW-07), surface water sample locations (SW-01 and SW-02), leachate sample location (LT-01), and domestic wells (DW-01 and DW-02) were sampled on October 3 and 4, 2022, and resampled January 9 and 10, 2023, by Anchor QEA. Static groundwater level measurements and field parameter data are included on the sampling logs presented in Appendix A. Field equipment calibration logs for the YSI Professional Plus Multiparameter Water Quality Meter and the Hach 2100Q Turbidimeter are also provided in Appendix A. The full suite of groundwater and surface water laboratory analytical results is presented in the laboratory analysis reports in Appendix B. Monitoring wells MW-01 and MW-06 are considered to be the Site's upgradient monitoring wells; MW-03 and MW-05R are located in the mid -gradient portion of the Site; and MW-02, MW-04, and MW-07 monitor downgradient portions of the Site. As summarized in Table 2, the total depths of the monitoring wells range from 40 to 110 feet below ground surface. The geology of the screened intervals of the monitoring wells is as follows: • Saprolite': MW-04 and MW-05R • Partially weathered rock (PWR)z: MW-03 • Bedrock3: MW-01, MW-02, MW-06, and MW-07 The locations of the monitoring wells, surface water samples, leachate, and domestic well sample locations are shown in Figure 2. 2.1. 7 Monitoring Well Purging and Sampling Methods Before the monitoring wells were sampled, the static water level was gauged in each well, and an initial round of field parameters was measured (consisting of pH, specific conductivity [SC], dissolved oxygen [DO], turbidity, temperature, and oxidation reduction potential [ORP]). Anchor QEA personnel used either low -flow techniques or disposable bailers to purge the monitoring wells and collect groundwater samples. The total depth, condition of the casing, and groundwater recharge rate determined the purging and sample collection method employed at each monitoring well. Saprolite is the result of in -place weathering that produces soil -like material that retains relict features of the parent rock. z PWR is generally found above the bedrock and is softer than bedrock, but not as soft as saprolite. 3 Bedrock is solid competent rock that underlies Saprolite and partially weathered rock. Fall 2022 Semiannual Water Quality Monitoring Report 3 March 2023 Four of the monitoring wells (MW-03, MW-04, MW-06, and MW-07) were purged using low -flow techniques in accordance with the procedures described by the U.S. Environmental Protection Agency (EPA) in Low -Flow (Minimal Drawdown) Ground -Water Sampling Procedures (EPA 1996). During purging, the field parameters (pH, SC, DO, ORP, turbidity, and temperature) were measured and recorded approximately every 3 minutes. Well purging continued until these parameters had generally stabilized for three consecutive readings. The required stabilization criteria are determined by the EPA Region 4 Science and Ecosystem Support Division in Operating Procedure: Groundwater Sampling (EPA 2017) and are summarized as follows: • pH values within ±0.1 standard unit (SU) • SC values within ±5% • Temperature, DO, and turbidity values within ±10% • ORP values within ±10 millivolts (mV) Once the parameters had stabilized, a groundwater sample was collected by field personnel wearing a new pair of nitrile gloves, using laboratory -supplied sample containers. Because of their slow recharge rates, monitoring wells MW-01, MW-02, and MW-05R were purged and sampled using disposable bailers. The wells were purged of three successive well volumes or purged dry, whichever occurred first, during each sampling event. Monitoring well MW-02 was purged dry and sampled on October 3, 2022, and again on January 10, 2023, after the well had sufficient time to recharge. Monitoring well MW-05R was purged dry in the morning on October 3, 2022, and again on January 9, 2023, and sampled later in the day after the well had sufficient time to recharge. Monitoring well MW-01 was purged and sampled on October 4, 2022, and again on January 9, 2023. A round of field parameters was measured and recorded at the start of purging and after each consecutive well volume had been purged. Field parameter data are shown in the well sampling logs included in Appendix A. 2.1.2 Surface Water Sampling Methods Surface water samples SW-01, SW-02, and SW-03 were collected on October 3 and 4, 2022, and again on January 9 or 10, 2023, at their designated locations along the Tuckasegee River, which is adjacent to and southwest of the landfill (Figure 2). Sampling location SW-01 is represents surface water quality upstream of the landfill, sampling location SW-02 represents surface water quality downstream of the landfill, and sampling location SW-03 represents surface water quality midstream of the landfill. One round of field parameters was measured and recorded at each surface water sampling location immediately prior to collecting the sample (Appendix A). The surface water samples were collected in laboratory -provided sample containers by a technician wearing a new pair of nitrile gloves. Fall 2022 Semiannual Water Quality Monitoring Report 4 March 2023 2.1.3 Leachate Sampling Methods Dedicated bottom -loading air -powered pumps, air pressure lines, and a leachate force main collection system are installed at the landfill. Pumps are installed in landfill gas extraction wells EW-1 R, EW-2R, EW-3R, EW-4, EW-5, EW-6, EW-7, EW-8, EW-9, and EW-10. The gas extraction well locations are presented in Figure 2. The leachate is pumped from the wells into a flow equalization tank, which is connected to the TWSA wastewater collection system. The flow equalization tank is east of the landfill, adjacent to the existing landfill gas flare. A grab sample of leachate (LT-01) was acquired on October 3, 2022, by collecting a sample as the leachate entered the flow equalization tank. One round of field parameters was measured and recorded after the sample was collected (Appendix A). 2. 7.4 Domestic Well Sampling Methods The domestic well water samples (DW-01 and DW-02) were collected on October 3, 2022, from an outside spigot at the residence located at 318 Joe Wilkey Road (DW-01) and 138 Joe Wilkey Road (DW-02), bordering the northern boundary of the landfill (Figure 2). The wells were purged of 30 gallons prior to sample collection. One round of field parameters was measured and recorded after the 30 gallons had been purged. The domestic well water samples were collected in laboratory -provided sample containers by field personnel wearing new nitrile gloves. 2.2 Sample Handling, Documentation, and Analysis 2.2. 7 Sampling Schedule The sampling schedule for semiannual sampling events at the Jackson County Landfill is presented in the following table: Fall 2022 Semiannual Water Quality Monitoring Report 5 March 2023 Parameter Groundwater Surface Water Leachate Domestic Well Groundwater Appendix I VOCs Annual Spring Annual Spring Annual Spring Not Applicable Appendix I Metals Annual Spring Annual Spring Annual Spring Not Applicable Appendix II VOC Annual Fall Annual Fall Annual Fall Not Applicable Appendix 11 SVOC Annual Fall Annual Fall Annual Fall Not Applicable Appendix II Metals Annual Fall Annual Fall Annual Fall Not Applicable Mercury Annual Fall Annual Fall Annual Fall Not Applicable Sulfide Semiannual Semiannual Semiannual Not Applicable 1,4-Dioxane Semiannual Semiannual Semiannual Not Applicable Herbicides and Pesticides Biennial — Fall Even Years Biennial — Fall Even Years Not Applicable Not Applicable MNA Parameters Biennial Spring and Fall Odd Years Not Applicable Not Applicable Not Applicable Hardness Not Applicable Semiannual Not Applicable Not Applicable VOC by 524.2 Not Applicable Not Applicable Not Applicable Semiannual 2.2.2 Fall 2022 Sampling Field parameters and additional observations pertaining to the Site sampling locations are provided in the sampling logs (Appendix A). Following sample collection, each groundwater, surface water, leachate, and domestic well water sample was immediately placed on ice in a sample cooler for transport to Waypoint Analytical Laboratories, a North Carolina -certified laboratory in Charlotte, North Carolina. The collected samples were analyzed for the following parameters (Table 1): • Groundwater — Appendix II metals, including mercury, using EPA Methods 6020B and 7470A — Appendix II volatile organic compounds (VC)Cs) using EPA Method 8260D — Appendix II semivolatile organic compounds (SVOCs) using EPA Method 8270D — 1,4-dioxane using EPA Method 8260DSIM — Herbicides using EPA Method 8151A — Pesticides using EPA Method 8081 B — Sulfide • Surface water — Appendix II metals, including mercury, using EPA Methods 6020B and 7470A — Appendix II volatile organic compounds (VC)Cs) using EPA Method 8260D — Appendix II semivolatile organic compounds (SVOCs) using EPA Method 8270D — 1,4-dioxane using EPA Method 8260DSIM — Hardness Fall 2022 Semiannual Water Quality Monitoring Report 6 March 2023 • Leachate - Appendix II VOCs, using EPA Method 8260D - 1,4-dioxane, using EPA Method 8260DSIM - Appendix II metals using EPA Method 6020B • Groundwater from domestic wells - VOCs using EPA Method 524.2 Proper chain -of -custody documentation procedures were followed during collection and transportation of each sample (Appendix B). Six trip blank samples for quality control/quality assurance purposes were included in the sample coolers and analyzed for Appendix II VOCs when applicable. The reports of the laboratory analyses are provided in Appendix B. Laboratory analyses performed on the samples are summarized in Table 1. Fall 2022 Semiannual Water Quality Monitoring Report 7 March 2023 3 Findings The field parameter data and laboratory analytical results for the groundwater samples (from monitoring wells MW-01 through MW-07), surface water samples (SW-01 and SW-02), leachate sample (LT-01), and domestic well samples (DW-01 and DW-02) collected at the landfill are included in Appendices A and B. The results are also submitted separately to the DEQ Division of Waste Management SWS in the Electronic Data Deliverable format (DEQ 2020). The laboratory analytical results were reported and appropriately qualified as follows: • Non -Detections: Non -detections are values reported by the laboratory as less than the method detection limits (MDLs). They are tabulated in Table 3 and flagged with a "U" qualifier. The MDL is the minimum concentration of a substance that can be measured and reported by a laboratory with 99% confidence that the constituent concentration is greater than zero. • Estimated or "J" Qualified: A "J" qualifier is used by the laboratory for parameters that are detected at estimated concentrations greater than the MDL but less than the laboratory's method reporting limit. The method reporting limit is the minimum concentration of a target analyte that can be accurately determined by the referenced method. • Groundwater Quality Standard: Detected concentrations of constituents in groundwater samples were compared to applicable North Carolina groundwater quality standards. For most constituents, this standard is defined in the 15A NCAC 2L.0202 Groundwater Standard 15A NCAC 2L.0202 (2L standard). Detected concentrations of analytes in groundwater with no established 2L standard were compared to the interim maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in accordance with 15A NCAC 02L.0202). • 2B Standard: Detections of analytes in surface water samples were compared to the surface water quality standards defined in 15A NCAC 2B (213 standards). Hardness -dependent 2B surface water standards were calculated using the average analyzed hardness value (calculated from the upstream and downstream surface water sampling location results) via the most stringent hardness -dependent metal calculation. Table 3 summarizes detected concentrations of analytes that exceeded their respective 2L standard, IMAC, or 2B standard. 3.1 Groundwater Measured field parameters and analytical results for groundwater samples collected from the monitoring wells during the fall 2022 sampling event are discussed in the following sections and summarized in Table 3. Fall 2022 Semiannual Water Quality Monitoring Report 8 March 2023 3.1.7 Field Parameters Field parameter measurements were obtained from all Site monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06, and MW-07). Field parameters are presented in Table 3 and summarized below: • pH: The pH readings ranged from 5.4 SU in MW-02 to 7.0 SU in MW-04 and MW-06. Of these monitoring wells, the pH values for MW-01, MW-02, MW-03, and MW-07 were less than the 2L standard pH range of 6.5 to 8.5 SU. • Turbidity: Turbidity ranged from 2.20 nephelometric turbidity units (NTUs) in MW-06 to 243 NTU in MW-02. Generally, higher values were measured at the monitoring wells (MW-01, MW-02, and MW-05R) that were purged and sampled using the bailer method (Section 2.1.1). The bailers were lowered gently to minimize water column disturbance when the samples were collected. • Dissolved Oxygen (DO): DO concentrations at the Site ranged from 0.58 milligram per liter (mg/L) in monitoring well MW-06 to 9.37 mg/L in monitoring well MW-04. • SC: SC concentrations at the Site ranged from 60.3 micromhos per centimeter (pmhos/cm) in monitoring well MW-06 to 820 pmhos/cm in monitoring well MW-07. • Oxidation/Reduction Potential: ORP concentrations at the Site ranged from -56.5 mV in monitoring well MW-05R to 184.7 mV in monitoring well MW-02. 3.1.2 Appendix 11 Metals (Total) Fifteen metals were detected in one or more of the monitoring well samples. Five of these metals (arsenic, chromium, cobalt, selenium, and vanadium) were detected at concentrations above their respective NC21- and/or IMAC water quality standards in one or more of the groundwater samples. A summary of the detections is provided below. • Arsenic (21L standard of 10 micrograms per liter [pg/L]): Arsenic was detected in MW-02 at a concentration of 10.1 pg/L. • Chromium (21L standard of 10 pg/L): Chromium was detected in MW-02 at a concentration of 42.2 pg/L. • Cobalt (21L standard of 1 pg/L): Cobalt was detected in MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06, and MW-07. Cobalt concentrations in these samples ranged from 2.12 pg/L (MW-07) to 105 pg/L (MW-01). As noted in Section 2.1, monitoring well MW-01 is considered to represent upgradient conditions. The second upgradient well (MW-06) also showed an exceedance of cobalt (8.07 pg/L). Historically, cobalt has been present at concentrations that exceeded its applicable water quality standard in groundwater samples from each of the seven monitoring wells. • Selenium (21- standard of 20 pg/L): Selenium was detected in MW-02 at a concentration of 36.2 pg/L. Fall 2022 Semiannual Water Quality Monitoring Report 9 March 2023 • Vanadium (2L standard of 7 pg/L): Vanadium was detected in MW-02 at a concentration of 52.3 pg/L. These metals have historically been present at concentrations exceeding their water quality standard in samples collected from multiple groundwater monitoring wells at the Site. However, the elevated turbidity value (243 NTU) measured in the MW-02 sample may have affected the reported selenium and arsenic concentrations. The dissolved metals result for MW-02 showed selenium and arsenic to be non -detect at <3.52 pg/L and <1.49 pg/L, respectively. 3.1.3 Appendix 11 Metals (Dissolved) Laboratory -filtered analysis of Appendix II metals was performed for monitoring well samples MW-02 and MW-05R because of their elevated turbidity readings (243 and 95.5 NTU, respectively) during sample collection. The reported concentrations for the dissolved metals were consistently lower than the total unfiltered metal analytical results in both monitoring wells. The total metals analysis identified arsenic, chromium, copper, selenium, and vanadium at concentrations greater than their 2L groundwater standard. However, the dissolved metals analysis only identified three metals, chromium, cobalt, and vanadium, at concentrations above their 2L standards. The MW-02 sample had dissolved metal concentrations for chromium (37.0 pg/L), cobalt (41.0 pg/L), and vanadium (42.1 pg/L) that were generally the same as the total metals concentrations observed for MW-02; however, the dissolved metal concentration for arsenic and selenium were non -detect. The dissolved metal concentration for cobalt from MW-05R was 10.5 pg/L, which is above its 2L standard and is slightly less than the total metal concentration of cobalt for MW-05R (Table 3). 3.1.4 Appendix 11 VOCs and 1,4-Dioxane Fourteen VOCs were detected in one or more of the monitoring wells (Table 3). Four of these VOCs (1,4-dichlorobenzene, 1,4-dioxane, benzene, and vinyl chloride) were detected at concentrations that exceeded their respective 2L standards in the groundwater samples collected from one or more monitoring wells. Concentration -versus -time graphs (trend plots) were created for the monitoring wells that have historically exhibited the following VOC concentrations in excess of their 2L standards (Figures 4 through 10): • 1-4-dichlorobenzene (2L standard of 6 pg/L): The detected concentration of 1,4-dichlorobenzene exceeded its 2L standard in monitoring well MW-05R (7.29 pg/L). The historical 1,4-dichlorobenzene concentrations in MW-05R have consistently fluctuated above and below the 2L standard (Figure 8). • 1,4-dioxane (2L standard of 3 pg/L): The detected concentrations of 1,4-dioxane exceeded its 2L standard in MW-03 (5.58 pg/L), MW-04 (11.0 pg/L), and MW-07 (17.6 pg/L). 1,4-dioxane was not detected in monitoring wells MW-01, MW-02, MW-05R, or MW-06. Trend plots of 1,4-dioxane concentrations in MW-04 and MW-07 show declining concentrations from 2018 Fall 2022 Semiannual Water Quality Monitoring Report 10 March 2023 into 2021; however, in the fall of 2021 and spring of 2022, respectively, concentrations began to increase (Figure 10). The trend plot for MW-3 shows 1,4-dioxane fluctuating above and below the 2L standard, but generally in a declining trend. • Benzene (21L standard of 1 pg/L): Benzene was detected at concentrations that exceeded its 2L standard in MW-05R (1.63 pg/L) and MW-07 (1.56 pg/L). Benzene concentrations at MW-5R have fluctuated consistently since 2012 (Figure 8). Benzene concentrations at MW-07 have been relatively stable since 2011 (Figure 10). • Vinyl chloride (21L standard of 0.03 pg/L): The concentration of vinyl chloride in the sample collected from one monitoring well, MW-05R (0.563 pg/L), exceeded its 2L standard. A trend plot for vinyl chloride concentrations in MW-05R shows fluctuating concentrations over time; however, the fall 2020 event concentrations have been in decline (Figure 8). A review of historical groundwater data indicates the VOCs (1,4-dichIorobenzene; 1,4-dioxane; benzene; and vinyl chloride) exhibiting concentrations that exceeded the 2L standards during the fall 2022 sampling event have been detected at relatively consistent concentrations for the past several years. As described in Section 3.2.3, historical surface water samples from the Tuckasegee River, which may receive discharge from the saprolite groundwater -bearing zone, have consistently shown no detections of these compounds, or other VOCs. 3.2 Surface Water The following sections summarize the measured field parameters and analytical results associated with the three surface water samples collected during the fall 2022 sampling event. 3.2. 7 Field Parameters Field parameters are presented in Table 3 and summarized below: • pH: The pH readings for the upstream (SW-01), downstream (SW-02), and midstream (SW-03) surface water samples collected during the fall 2022 sampling event were 6.7, 7.1, and 7.4 SU, respectively. The pH readings for all surface water samples were within than the 2B standard range of 6.0 to 9.0 SU. • Turbidity: The turbidity values measured in SW-01 (1.72 NTU), SW-02 (1.87 NTU), and SW-03 (2.01 NTU) were less than the 2B standard, which is established at less than or equal to 50 NTU for the receiving water in streams not designated as trout waters. • DO: DO was measured at a concentration of 10.53 mg/L in SW-01, 9.35 mg/L in SW-02, and 9.57 mg/L in SW-03. The 2B standard is established as greater than or equal to 6 mg/L; thus, each sample is within the acceptable DO range. • SC: SC concentrations in surface water samples SW-01, SW-02, and SW-03 were recorded at 30, 27.9 and 38.7 pmhos/cm, respectively. These concentrations of SC are consistent with historical data for surface water samples SW-01 and SW-02. Fall 2022 Semiannual Water Quality Monitoring Report 11 March 2023 • ORP: ORP values for SW-01, SW-02, and SW-03 were 86, 64, and 189.8 mV, respectively. Compared to historical surface water samples, the concentrations of ORP in surface water samples SW-01 and SW-02 are significantly less by approximately 200 mV. 3.2.2 Appendix 11 Metals Eight metals were detected in one, both or all surface water sampling locations. Of these metals, two (copper and zinc) exceeded the established 2B standards, and two additional metals (lead and nickel) had estimated concentrations (J-valued) that exceeded the 2B standards. A summary of the detections that exceed the 2B standards is provided below. • Copper (213 hardness -dependent calculated standard of 1.00 pg/L): Copper was detected in SW-01, SW-02, and SW-03. Copper concentrations in these samples ranged from 2.37 pg/L (SW-01) to 19.2 pg/L (SW-03). As noted in Section 2.1, surface water sample location SW-01 represents surface water quality upstream of the landfill, SW-02 represents the downstream water quality, and SW-03 represents surface water quality midstream of SW-01 and SW-02. SW-03 is a new monitoring location having only been sampled in spring and fall of 2022. In spring 2022, SW-03 copper was non -detect and at the upstream (SW-01) and downstream (SW-02) locations, copper was detected at J-valued concentrations of 1.22 J pg/L and 1.00 J pg/L, respectively. • Lead (213 hardness -dependent calculated standard of 0.14 pg/L): Lead was detected at an estimated concentration of 0.266 J pg/L in SW-02. • Nickel (213 hardness -dependent calculated standard of 5.94 pg/L): Nickel was detected at an estimated concentration of 0.552 J pg/L in SW-02. • Zinc (213 hardness -dependent calculated standard of 13.35 pg/L): Zinc was detected at a concentration of 13.9 pg/L in SW-02 and at an estimated concentration of 80.5 J pg/L in SW-03. There were no zinc detections reported during spring 2022 at any of the surface water sample locations. 3.2.3 Appendix 11 VOCs and 7,4-Dioxane No VOCs were detected at surface water locations SW-01, SW-02, and SW-03 above the 2B standards. 3.3 Leachate Table 3 identifies the VOCs, SVOCs, and metals identified in the leachate sample. In general, 13 metals, 11 VOCs, and 2 SVOCs were detected. The number and concentration of the constituents detected in the leachate varies each sampling event. Table 4 provides the historical concentrations of VOCs and SVOCs removed by the leachate extraction system and provides a calculation of the total mass removed. Fall 2022 Semiannual Water Quality Monitoring Report 12 March 2023 On September 1, 2012, leachate extraction was initiated following installation of leachate extraction pumps in the 10 landfill gas extraction wells at the Site (Figure 2). Based on readings taken from the leachate totalizer during the October 2022 monitoring events, approximately 24,407 gallons of leachate were discharged through a permanent connection to the TWSA between March 3, 2022, and October 4, 2022. In fall 2013, the active portion of the approved corrective action remedy was initiated. Based on the leachate analytical results for the sample collected on October 4, 2022, Anchor QEA estimates that approximately 0.033 pounds of VOCs were removed with the extracted leachate between the March 2022 and October 2022 sampling events. Mass removal calculations through October 2022 are included in Table 4 3.4 Domestic Well The following sections summarize measured field parameters and analytical results associated with the domestic well water sample collected during the fall 2022 sampling event. 3.4.7 Field Parameters The pH reading for the domestic well samples for DW-01 and DW-02 were 6.7 and 7.0 SU, respectively, which are within the 2L standard range of 6.5 to 8.5 SU. Turbidity measured in DW-01 and DW-02 were 4.95 and 2.31 NTU, respectively. DO was measured at a concentration of 4.00 mg/L in DW-01 and 10.49 mg/L in DW-02. SC measured in DW-01 and DW-02 was 68.5 and 146.5 pmhos/cm, respectively. ORP measured in DW-01 and DW-02 was 70.0 and 66.7 mV, respectively. These parameters do not have established water quality standards. 3.4.2 VOCs No VOCs were detected at concentrations that exceeded their respective MDLs in the domestic well water samples. 3.5 Groundwater Flow Directions Groundwater levels in the saprolite, PWR, and bedrock are monitored at the Site. Three of the bedrock monitoring wells (MW-01, MW-02, and MW-06) are located in the northern and northwestern portions of the Site (Figure 3; Table 2). The fourth bedrock monitoring well (MW-07) is located southwest of the landfill (Figure 3). PWR monitoring well MW-03 and saprolite monitoring wells MW-04 and MW-05R (Figure 3) are located in the south-central and southern parts of the landfill, respectively. The fall 2022 water level data collected from all of the Site monitoring wells is presented in Table 2 and on Figure 3. Generalized groundwater elevation contours are presented in Fall 2022 Semiannual Water Quality Monitoring Report 13 March 2023 Figure 3 and indicate that groundwater flow direction in the combined aquifer system (saprolite, PWR, and bedrock) is generally to the south-southwest, toward the Tuckasegee River (Figure 3). Fall 2022 Semiannual Water Quality Monitoring Report 14 March 2023 4 Summary The second semiannual water quality monitoring event of 2022 for the Site was performed on October 3 and 4, 2022, and resampled for pesticides on January 9 and 10, 2023, due to laboratory error. Appendices A and B and Table 3 provide detailed analytical results and field data summarizing the groundwater, surface water, and leachate quality at the landfill. 4.1 Groundwater Quality 4.7. 7 Appendix/1 Metals Five metals (arsenic, chromium, cobalt, selenium, and vanadium) were detected at concentrations that exceeded their associated groundwater quality standards in one or more of the monitoring wells (Table 3). Arsenic, chromium, cobalt, selenium, and vanadium concentrations exceeded 2L standards in MW-02. Cobalt concentrations exceeded the 2L standard in all the collected groundwater samples. The results for groundwater samples from MW-02, submitted for dissolved metals, show lower metals concentrations for arsenic and selenium than the total metals samples, indicating turbidity may have affected metal concentrations in this well. 4. 7.2 Appendix 11 Volatile Organic Compounds and 7,4-Dioxone Four VOCs (1,4-dichlorobenzene, 1,4-dioxane, benzene, and vinyl chloride) were detected at concentrations that exceeded their respective 2L standards (Table 3) in one or more monitoring wells, including 1,4-dichlorobenzene and benzene, in the mid -gradient monitoring well MW-05R and the downgradient well MW-07. Trend plots for samples from monitoring wells that had VOC concentrations that exceeded their 2L standards (Figures 4 through 10) show relatively consistent trends with time; however, 1,4-dioxane is generally showing higher concentrations in MW-04 and MW-07. 4.7.3 Field Parameters and Other Constituents Four of the seven samples collected from the monitoring wells had pH readings outside of the 2L standard range (6.5 to 8.5 SU). These results are consistent with historical data and are characteristic of the natural groundwater quality of the region. Turbidity readings ranged from 2.20 NTU (MW-06) to 243 NTU (MW-02). Fall 2022 Semiannual Water Quality Monitoring Report 15 March 2023 4.2 Surface Water Quality 4.2. 7 Appendix // Metals Four metals were detected at or estimated to have exceeded their associated surface water standards in one or more of the surface water sampling locations (Table 3). Zinc was detected at a concentration above 2B surface water standards in SW-02 and detected with an estimated concentration above the same applicable surface water standard in SW-03. Lead and nickel were detected at estimated concentrations above 2B standards in SW-02. Copper concentrations exceeded their 2B standard in all the collected surface water sample locations. Both the upstream and downstream surface water locations have historically reported exceedances of the 2B standards for copper, lead, and zinc. This is the second sampling event for SW-03. Constituent concentrations in spring 2022 sample for SW-03 were all below the 2B standards. 4.2.2 Appendix // Volatile Organic Compounds and 7,4-Dioxane No concentrations for VOCs exceeded 2B standards for surface water during this monitoring event. 4.2.3 Field Parameters and Other Constituents Field parameters measured in both surface water samples, including DO, pH, and turbidity were within the 2B standards established for these parameters. Based on the data presented above, the groundwater migrating from the landfill toward the Tuckasegee River does not appear to be impacting surface water quality with regards to VOCs, and 1,4-Dioxane; however, downgradient surface water sample location SW-02 had a greater number of metal constituents detected at concentrations that exceed their 2B surface water standards, which were not detected in the upstream sample location SW-01. Metal concentrations can fluctuate from one sampling to the next. Anchor QEA recommends continued monitoring to determine if a trend is developing. 4.3 Leachate Quality The leachate sample (LT-01) was collected from the flow equalization tank and analyzed for Appendix I VOCs and 1,4-dioxane. Thirteen VOCs were detected in the leachate sample (Table 3). There are no established water quality standards for leachate. 1,4-dioxane was detected at 80.0 pg/L, which is higher than the detected concentrations of the compound in the monitoring well groundwater samples. Since monitoring of 1,4-dioxane began in Fall of 2020, the 1,4-dioxane concentrations have ranged from 106 pg/L in spring of 2022 to 48.8 pg/L in Fall 2021. Fall 2022 Semiannual Water Quality Monitoring Report 16 March 2023 4.4 Domestic Well Water Quality No VOCs were detected at concentrations that exceeded their respective MDLs in the domestic well water samples. Fall 2022 Semiannual Water Quality Monitoring Report 17 March 2023 5 Future Activities Anchor QEA will continue to monitor the water quality on a semiannual basis at the Site. During spring 2023, domestic well owners will be contacted, and groundwater samples will be collected from domestic wells if permitted by the well owner, and if possible, based on well pump operability. Domestic well samples will be analyzed for VOCs only. Samples will be collected from the monitoring wells, surface water monitoring points, and leachate flow equalization tank during spring 2023 and fall 2023. In addition to the MNA parameters that were added to the monitoring requirements as part of the CAP, the analytical suites associated with the current and future sampling events are outlined in the 2011 CAP (Altamont 2011), the first CAER (Altamont 2016), and the second CAER (Anchor QEA 2022). The upcoming sampling event parameters are as follows: Sampling Event Analytical Suite Appendix I VOCs (including 1,4-dioxane) Appendix I Metals Spring 2023 Sulfide MNA Parameters Hardness Appendix II VOCs (including 1,4-dioxane) Appendix 11 Metals Appendix II SVOCs Fall 2023 Mercury MNA Parameters Hardness Sulfide Fall 2022 Semiannual Water Quality Monitoring Report 18 March 2023 6 References Altamont (Altamont Environmental, Inc.), 2010. Assessment of Corrective Measures. Prepared for North Carolina Department of Environment and Natural Resources. September 7, 2010. Altamont, 2011. Corrective Action Plan. Prepared for North Carolina Department of Environment and Natural Resources. June 30, 2011. Altamont, 2016. Five -Year Corrective Action Evaluation Report. Prepared for North Carolina Department of Environmental Quality. October 31, 2016. Anchor QEA (Anchor QEA of North Carolina, PLLC), 2020. Spring 2020 Semiannual Water Quality Monitoring Report. Prepared for Jackson County Solid Waste Department. June 2020. Anchor QEA, 2022. Five -Year Corrective Action Evaluation Report. Prepared for North Carolina Department of Environmental Quality. January 13, 2022. DENR (North Carolina Department of Environmental and Natural Resources), 2011. Letter to: Altamont Environmental, Inc. Regarding: Approval of the County's Corrective Action Plan. September 1, 2011. DEQ, 2018. "Groundwater Protection Compliance Standards — Constituents List." Last modified October 15, 2018. Available at: https://edocs.deq.nc.gov/WasteManagement/0/edoc/12571811SWS_EnviroMonitoring_Const ituents_List.pdf?searchid=13f8efbl -eel l-485a-b03f-718f2287b271. DEQ, 2020. Memorandum to: Solid Waste Directors, Landfill Owners/Operators, and North Carolina Certified Laboratories. Regarding: New Electronic Data Deliverable (EDD) Format. July 20, 2020. EPA (U.S. Environmental Protection Agency), 1996. Low -Flow (Minimal Drawdown) Ground -Water Sampling Procedures. Office of Land and Emergency Management, EPA/540/5-95/504. EPA, 2017. Science and Ecosystem Support Division. Operating Procedure: Groundwater Sampling. April 26, 2017. Fall 2022 Semiannual Water Quality Monitoring Report 19 March 2023 Tables Table 1 Summary of Laboratory Analyses Performed on Samples Groundwater Samples Location ID Date Collected Sample ID Appendix II VOCs 1,4-Dioxane Appendix II Metals Mercury Appendix II SVOCs Herbicides and Pesticides Sulfide EPA 8260D EPA 8260D SIM EPA 6020E EPA 7470A EPA 8270D EPA 8151A and 8081 B EPA 4500S2F- 2011 MW-01 10/4/2022 MW-01-20221004 X X X X X X X MW-02 10/3/2022 MW-02-20221003 X X X' X X X X MW-03 10/4/2022 MW-03-20221004 X X X X X X X MW-04 10/4/2022 MW-04-20221004 X X X X X X X MW-05R 10/3/2022 MW-05R-20221003 X X X1 X X X X MW-06 10/4/2022 MW-06-20221004 X X X X X X X MW-07 10/3/2022 MW-07-20221003 X X X X X X X Surface Water, Leachate, Domestic Well, and Quality Control Samples Location ID Date Collected Sample ID Appendix II VOCs 1,4-Dioxane Appendix II Metals Mercury Hardness Appendix II SVOCs VOCs Herbicides and Pesticides Sulfide EPA 8260D EPA 8260D SIM EPA 6020B EPA 7470A EPA 2340C- 2011 EPA 8270D EPA 524.2 EPA 8151A and 8081 B EPA 4500S21'- 2011 DW-01 10/3/2022 DW-01-20221003 X DW-02 10/3/2022 DW-02-20221003 X LT-01 10/3/2022 LT-01-20221003 X X X' SW-01 10/3/2022 SW-01-20221003 X X X X X X X X SW-02 10/3/2022 SW-02-20221003 X X X X X X X X SW-03 10/4/2022 SW-03-20221004 X X X X X X X X TB-20221003-1 10/3/2022 TB-20221003-1 X TB-20221003-2 10/3/2022 TB-20221003-2 X TB-20221003-3 10/3/2022 TB-20221003-3 X TB-20221003-4 10/3/2022 TB-20221003-4 X TB-20221004-1 10/4/2022 TB-20221004-1 X TB-20221004-2 10/4/2022 TB-20221004-2 X Notes: 1: An additional sample was collected for a laboratory -filtered dissolved metals analysis. Appendix II constituents were analyzed per Title 40 Code of Federal Regulations, Part 258. Blank cell: Analysis was not performed on that sample. BOD: biochemical oxygen demand COD: chemical oxygen demand EPA: U.S. Environmental Protection Agency (method) SIM: selective ion monitoring SM: Standard Method SVOC: semivolatile organic compound TB: trip blank TOC: total organic carbon VOC: volatile organic compound Fall 2022 Semiannual Water Quality Monitoring Report Page 1 of 1 Jackson County Closed Municipal Solid Waste Landfill March 2023 Table 2 Well Construction Details and Corresponding Elevations Stick Up Depth to Depth to Elevation of Ground (feet Depth to Approximate Approximate Top of Bottom of Top Elevation Bottom of Surface TOC above Total Well Water Depth to Top of Bedrock Screened Screened of Screened Screened Geology of Source of Well Elevation Elevation ground Depth (feet below Groundwater Bedrock Elevation Interval Interval Interval Interval Screened Construction Facility Permit Well ID Date Drilled (feet) (feet) surface) (feet bgs) TOC) Elevation (feet) (feet bgs) (feet) (feet bgs) (feet bgs) (feet) (feet) Interval Information MW-01 4/23/1992 2,169.40 2,171.42 12.0 110.5 98.90 2,072.52 83.0 2,086.40 95.0 110.0 2,074.40 2,059.40 Bedrock MW-02 4/22/1992 2,013.15 2,015.38 2.3 60.7 43.83 1,971.55 13.0 2,000.15 45.0 60.0 1,968.15 1,953.15 Bedrock Partially S&ME, Inc. MW-03 4/21/1992 2,044.16 2,045.53 1.3 65.5 50.54 1,994.99 57.0 1,987.16 48.5 63.5 1,995.66 1,980.66 weathered rock 50-02 MW-04 4/21/1992 1,978.68 1,980.77 2.0 43.0 27.56 1,953.21 NA NA 25.0 40.0 1,953.68 1,938.68 Saprolite MW-05R 1/26/2012 2,027.98 2,030.95 2.8 54.0 49.37 1,981.58 NA NA 44.0 54.0 1,983.98 1,973.98 Saprolite MW-06 3/23/2004 2,136.58 2,139.57 3.0 94.0 83.30 2,056.27 47.6 2,088.98 84.6 94.6 2,051.98 2,041.98 Bedrock Altamont Environmental, Inc. MW-07 7/30/2010 1,978.71 1,981.29 2.6 95.0 32.40 1,948.89 44.0 1,935.00 70.0 95.0 1,908.71 1,883.71 Bedrock Notes: Elevations associated with wells MW-01, MW-02, MW-03, MW-04, and MW-06 are measured relative to mean sea level and are based on surveying completed by Davenport & Associates, Inc. Elevations associated with wells MW-05R and MW-07 are measured relative to horizontal North American Datum 83 and are based on surveying completed by Wes Cole Land Surveying, PA. Depth to water was measured on October 3 and 4, 2022 (Appendix A). Depth to bedrock and screened interval for MW-01 through MW-04 was taken from S&ME, Inc., with boring logs completed on April 21 through 23, 1992. Depth to bedrock and screened interval for MW-06 was taken from an Altamont Environmental, Inc., with boring log completed on March 23, 2004. Depth to bedrock and screened interval for MW-07 was taken from an Altamont Environmental, Inc., with boring log completed on July 30, 2010. Depth to bedrock and screened interval for MW-05R was taken from an Altamont Environmental, Inc., with boring log completed on January 26, 2012. Monitoring well MW-05 was abandoned on January 26, 2012, by NYEG Drilling, LLC. Monitoring well MW-05R was installed by NYEG Drilling, LLC, on January 26, 2012, as a replacement to MW-05. Monitoring well MW-05R was surveyed by Wes Cole Land Surveying, PA, on September 28, 2012. bgs: below ground surface NA: not applicable TOC: top of casing Fall 2022 Semiannual Water Quality Monitoring Report Page 1 of 1 Jackson County Closed Municipal Solid Waste Landfill March 2023 Table 3 Analytical Summary Chemical Conventional Parameters Water level depth (feet) Temperature (°C) Dissolved oxygen (mg/L) Specific conductivity (pmhos/cm) pH (SU) ORP (mV) Turbidity (NTU) Hardness as Ca and Mg (mg/L) MNA Parameters (mg/L) Sulfide Metals (Ng/L) Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Mercury Nickel Selenium Silver Thallium Tin Vanadium Zinc Metals, Dissolved (Ng/L) Arsenic Barium Cadmium Chromium Cobalt Copper Lead Mercury Nickel Selenium Silver Thallium Vanadium Zinc Location ID DW-01 DW-02 LT-01 MW-01 MW-02 MW-03 MW-04 MW-05R MW-06 MW-07 SW-01 SW-02 SW-03 FieldQC I FieIdQC FieIdQC FieIdQC FieIdQC FieIdQC Sample ID DW-01- 20221003 DW-02- 20221003 LT-01- 20221003 MW-01- 20221004 MW-02- 20221003 MW-03- 20221004 MW-04- 20221004 MW-05R- 20221003 MW-06- 20221004 MW-07- 20221003 SW-01- 20221003 SW-02- 20221003 SW-03- 20221004 TB- 20221003-1 TB- 20221003-2 TB- 20221003-3 TB- 20221003-4 TB- 20221004-1 TB- 20221004-2 Sample Date 10/3/2022 10/3/2022 10/3/2022 10/4/2022 10/3/2021 10/4/2022 10/4/2022 10/3/2022 10/4/2022 10/3/2022 10/3/2022 10/3/2022 10/4/2022 10/3/2022 10/3/2022 10/3/2022 10/3/2022 10/4/2022 10/4/2022 Sample Type N N N N N N N N N N N N N TB TB TB TB TB TB Matrix WG WG WG WG WG WG WG WG WG WG WS WS WS WQ WQ WQ WQ WQ WQ NC2L Method NC2L IMAC NC 213 Field -- -- Field -- < 6 Field -- -- Field 6.5-8.5 6.0-9.0 Field -- -- Field <50 S M 2340C 100 SM4500S2FI -- I I -- SW6020 10 10 SW6020 700 21000 SW6020 4 6.5 SW6020 2 *0.06 SW6020 10 *9.08 SW6020 1 1.6 SW6020 1000 *1.00 SW6020 15 *0.14 SW7470 1 0.012 SW6020 100 *5.94 SW6020 20 5 SW6020 20 *0.04 SW6020 2 2 SW6020 2000 770 SW6020 7 -- SW6020 1000 *13.35 SW6020 10 10 SW6020 700 21000 SW6020 2 *0.04 SW6020 10 *5.31 SW6020 1 1.6 SW6020 1000 *0.57 SW6020 15 *0.07 SW7470 1 0.012 SW6020 100 *3.42 SW6020 20 5 SW6020 20 *0.04 SW6020 2 2 SW6020 7 -- SW6020 1000 *7.66 -- -- -- 98.90 43.83 50.54 27.56 49.37 83.30 32.40 -- -- -- 15.3 16.6 22.2 16.2 14.4 15.0 15.8 17.9 16.3 15.8 16.5 17.9 14.2 -- -- -- -- 4.00 10.49 0.09 1.05 2.73 1.45 9.37 2.08 0.58 7.33 10.53 9.35 9.57 -- -- -- -- 68.5 146.5 4967 212.0 212.1 353.7 734 677 60.3 820 30 27.9 38.7 -- -- -- -- 6.7 7.0 7.7 5.8 5.4 5.8 7.0 6.6 7.0 6.0 6.7 7.1 7.4 -- -- -- -- 70.0 66.7 -138.4 29.6 184.7 54.6 137.9 -56.5 90.4 51.1 86.0 64.0 189.8 -- -- -- -- 4.95 2.31 1000 5.94 243 4.42 2.33 95.5 2.20 5.48 1.72 1.87 2.01 -- -- -- -- -- -- -- -- -- -- -- -- -- -- 10 9.09 4 -- -- -- 1 0.830 U I 0.830 U 0.830 U 0.830 U I 1.66 U I 1.10 J I 0.830 U I 0.83 U I 0.90 J I 0.83 U -- 85.7 0.490 U 10.1 0.490 U 0.490 U 0.590 J 0.490 U 0.490 U 0.490 U 0.416 J 2.45 U -- -- -- -- -- 4460 106 224 221 151 246 48.2 422 14.1 15.2 17.0 U -- -- -- -- -- 10.6 0.240 U 1.20 U 0.240 U 0.240 U 0.240 U 0.240 U 0.240 U 0.240 U 0.102 U 1.20 U -- -- -- -- -- 0.750 U 0.327 J 0.750 U 0.442 J 0.291 J 0.150 U 0.150 U 0.150 U 0.150 U 0.350 U 0.750 U -- -- -- -- -- -- 476 1.00 U 42.2 1.66 J 1.00 U 2.76 1.00 U 1.00 U 1.90 J 0.638 J 5.00 U -- -- -- -- -- -- 151 105 40.7 7.49 3.09 15.9 8.07 2.12 0.224 J 0.248 J 0.400 U -- -- -- -- -- -- 238 5.94 41.8 5.00 2.27 4.19 2.38 2.72 2.37 1.47 19.2 -- -- -- -- -- -- 86.4 0.500 U 9.82 0.500 U 0.500 U 0.993 J 0.500 U 0.500 U 0.500 U 0.266 J 2.50 U -- -- -- -- -- -- 0.300 U 0.0700 U 0.0700 U 0.0700 U 0.400 0.0700 U 0.0700 U 0.0700 U 0.0700 U 0.0700 U 0.0700 U -- -- -- -- -- -- 232 14.7 32.0 6.84 1.47 J 4.66 3.93 7.41 0.720 U 0.552 J 3.60 U -- -- -- -- -- 125 2.30 U 36.2 2.30 U 2.30 U 2.30 U 2.30 U 2.30 U 2.30 U 0.703 U 11.5 U -- -- -- -- -- 0.650 U 0.130 U 0.650 U 0.130 U 0.168 J 0.130 U 0.130 U 0.130 U 0.130 U 0.0570 U 0.650 U -- -- -- -- -- 2.98 J 0.734 J 1.40 U 0.280 U 0.280 U 0.280 U 0.311 J 0.280 U 0.280 U 0.0610 U 1.40 U -- -- -- -- -- 18.7 J 1.50 U 7.50 U 1.50 U 1.50 U 1.50 U 1.50 U 2.09 J 1.50 U 1.44 U 7.50 U -- -- -- -- -- 581 2.10 U 52.3 2.10 U 2.10 U 3.31 J 2.10 U 2.10 U 2.10 U 0.767 U 10.5 U -- -- -- -- -- -- 764 22.8 103 13.2 J 4.69 J 12.6 J 14.3 J 14.9 J 4.85 J 13.9 80.5 J -- -- -- -- -- 12.3 -- 1.49 U -- -- 3.36 -- -- -- -- - -- -- -- -- -- 410 204 -- -- 153 - -- -- -- -- -- -- -- -- 3.50 U 1.75 U -- -- 0.350 U -- -- -- -- -- -- -- 6.09 J 37.0 -- -- 0.346 U -- -- -- -- -- -- -- 9.56 J 41.0 -- -- 10.5 -- -- -- -- -- -- -- 4.89 U 30.7 -- -- 0.690 J -- -- -- -- -- -- -- 2.64 U 8.37 -- -- 0.264 U -- -- -- -- -- -- -- 0.0700 U 0.0700 U -- -- 0.0700 U -- -- -- -- -- -- -- -- 33.4 29.7 -- -- 2.69 -- -- -- -- -- -- -- 7.03 U 3.52 U -- -- 0.703 U -- -- -- -- -- -- -- 0.570 U 0.285 U -- 0.0570 U -- -- -- -- -- -- -- 0.610 U 0.850 J -- -- 0.0874 J -- -- -- -- -- -- -- 7.67 U 42.1 -- -- 0.767 U -- -- -- -- -- -- -- -- 46.7 U 175 -- -- 5.17 J -- -- -- -- -- -- Fall 2022 Semiannual Water Quality Monitoring Report Page 1 of 3 Jackson County Closed Municipal Solid Waste Landfill March 2023 Table 3 Analytical Summary Location ID DW-01 DW-02 LT-01 MW-01 MW-02 MW-03 MW-04 MW-05R MW-06 MW-07 SW-01 SW-02 SW-03 FieldQC FieIdQC FieIdQC FieIdQC FieIdQC FieIdQC Sample ID DW-01- 20221003 DW-02- 20221003 LT-01- 20221003 MW-01- 20221004 MW-02- 20221003 MW-03- 20221004 MW-04- 20221004 MW-05R- 20221003 MW-06- 20221004 MW-07- 20221003 SW-01- 20221003 SW-02- 20221003 SW-03- 20221004 TB- 20221003-1 TB- 20221003-2 TB- 20221003-3 TB- 20221003-4 TB- 20221004-1 TB- 20221004-2 Sample Date 10/3/2022 10/3/2022 10/3/2022 10/4/2022 10/3/2021 10/4/2022 10/4/2022 10/3/2022 10/4/2022 10/3/2022 10/3/2022 10/3/2022 10/4/2022 10/3/2022 10/3/2022 10/3/2022 10/3/2022 10/4/2022 10/4/2022 Sample Type N N N N N N N N N N N N N TB TB TB TB TB TB Matrix WG WG WG WG WG WG WG WG WG WG WS WS WS WQ WQ WQ WQ WQ WQ NC2L Chemical Method NC2L IMAC NC 213 Volatile Organics (Ng/L) 1,1-dichloroethane SW8260 6 6 0.16U 0.16U 0.240 U 1.56 0.386 J 0.516 0.240 U 0.240 U 0.858 0.240 U 0.240 U 0.240 U 0.240 U 0.240 U 0.240 U 0.240 U 0.240 U 0.240 U 0.240 U 1,2-dichloroethene, cis- SW8260 70 60 -- -- 0.200 U 1.48 0.223 J 1.14 0.816 2.18 0.622 2.01 0.200 U 0.200 U 0.200 U 0.200 U 0.200 U 0.200 U 0.200 U 0.200 U 0.200 U 1,4-dioxane SW8260SIM 3 0.35 -- -- 80.0 0.139 U 0.139 U 5.58 11.0 0.139 U 0.139 U 17.6 0.139 U 0.139 U 0.139 U -- -- -- -- -- -- 4-Methyl-2-pentanone (Methyl iso SW8260 100 2800 -- -- 1.12 J 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U Benzene SW8260 1 1.19 0.21 U 0.21 U 0.568 0.550 0.180 U 0.553 0.376 J 1.63 0.180 U 1.56 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U Carbon disulfide SW8260 700 100 -- -- 0.683 J 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U 0.150 U Chlorobenzene SW8260 50 140 0.26 U 0.26 U 1.39 0.692 0.190 U 6.60 1.60 7.09 0.190 U 4.46 0.190 U 0.190 U 0.190 U 0.190 U 0.190 U 0.190 U 0.190 U 0.190 U 0.190 U Ethylbenzene SW8260 600 97 0.22U 0.22U 0.267 J 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U m,p-xylene SW8260 500 420 0.39U 0.39U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U 0.420 U Methyl ethyl ketone (2-butanone) SW8260 4000 20000 -- -- 2.36 J 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U 0.710 U o-xylene SW8260 500 600 0.22U 0.22U 0.465J 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U 0.210U Tetrachloroethene (PCE) SW8260 0.7 0.7 -- -- 0.220 U 0.342 J 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U Tetrahydrofuran SW8260 -- 2000 3100 -- -- 67.8 1.50 U 1.50 U 1.50 U 1.50 U 2.76 J 1.50 U 1.50 U 1.50 U 1.50 U 1.50 U 1.50 U 1.50 U 1.50 U 1.50 U 1.50 U 1.50 U Toluene SW8260 600 -- 0.36 0.20U 0.20U 0.240 J 0.220 U 0.220 U 0.220 U 0.220 U 0.237 J 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U 0.220 U Total xylene SW8260 500 670 0.22U 0.22U 0.465 J 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U Trichloroethene (TCE) SW8260 3 2.5 -- -- 0.180 U 0.241 J 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U 0.180 U Vinyl chloride SW8260 0.03 0.025 -- -- 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.563 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U 0.170 U Semivolatile Organics (Ng/L) 1,2-dichlorobenzene SW8260 20 79 0.220 U 0.220 U 0.220 U 0.243 J 0.220 U 0.286 J 0.220 U 0.319 J 0.220 U 0.220 U 0.220 U -- -- -- -- -- -- 1,4-dichlorobenzene SW8260 6 488 -- -- 1.82 5.72 0.210 U 4.31 2.57 7.29 0.728 4.58 0.210 U 0.210 U 0.210 U -- -- -- -- -- 1,4-dichlorobenzene SW8270 6 488 - -- -- 4.16 J 0.682 U 2.80 J 1.81 J 3.47 J 0.725 U 2.44 J -- -- 0.682 U -- -- -- -- -- Diethyl phthalate SW8270 6000 600 - -- -- 0.713 U 0.687 U 0.780 U 0.952 J 0.650 U 0.731 U 0.585 U -- -- 0.687 U -- -- -- -- Naphthalene SW8260 6 12 0.35U 0.35U 3.66 0.470 U 0.470 U 0.470 U 0.470 U 0.470 U 0.470 U 0.470 U 0.470 U 0.470 U 0.470 U -- -- -- -- Herbicides (Ng/L) 2,4,5-TP (Silvex) SW8151A 50 10 -- -- 0.01867 U 0.01650 U 0,01921 U 0.01815 U 0.02419 J 0.01815 U 0.01815 U 0.01921 U 0.01867 U 0.01815 U -- -- -- -- Pesticides (Ng/L) alpha-BHC SW8081 B 0.006 4E-04 -- -- 0.0404 J 0.0063U 0.0063U 0.0063U 0.0301 0.0063U 0.0937 0.0063U 0.0063U 0.0063U -- -- -- -- beta-BHC SW8081 B 0.02 0.008 -- -- 0.0111 U 0.0111 U 0.0111 U 0.0203 JQ 0.0402 0.0782 0.0520 0.0111 U 0.0111 U 0.0111 U -- -- -- -- delta-BHC SW8081 B -- 40 -- -- 0.0082U 0.0082U 0.0082U 0.0082U 0.0082U 0.0082U 0.0104 0.0082U 0.0082U 0.0082U -- -- -- -- gamma-BHC SW8081 B 0.03 4.2 -- -- 0.0303 J 0.0061 U 0.0061 U 0.0061 U 0.0201 0.0061 U 0.0937 0.0061 U 0.0061 U 0.0061 U -- -- -- -- Endosolfan I SW8081 B 40 0.05 -- -- 0.0160U 0.0160U 0.0160U 0.142 Q 0.0160U 0.0160U 0.0160U 0.0160U 0.0160U 0.0160U -- -- -- -- Endosulfan sulfate SW8081 B 40 20 -- -- 0.0165U 0.0165U 0.0165U 0.0507 0.0165U 0.0165U 0.0165U 0.0165U 0.0165U 0.0165U -- -- -- -- Endrin aldehyde SW8081 B 2 1 -- -- 0.0158U 0.0158U 0.0158U 0.0812 0.0158U 0.0158U 0.0158U 0.0158U 0.0158U 0.0158U -- -- -- -- Fall 2022 Semiannual Water Quality Monitoring Report Page 2 of 3 Jackson County Closed Municipal Solid Waste Landfill March 2023 Table 3 Analytical Summary Notes: indicates the detected concentration is greater than the NC2L (2022) or NC2L IMAC (2022) screening level. indicates the detected concentration is greater than the NC213 screening level. Bold indicates a detected result. Italicized indicates non -detected concentration is above one or more identified screening levels *: 213 surface water standard calculated using average analyzed hardness value (calculated from the upstream and downstream sampling location results) via the most stringent hardness -dependent metal calculation per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 213 - Surface Water and Wetland Standards (last amended September 2022). All nondetect results are reported at the method detection limit. Horizontal coordinate datum is North American Datum of 1983 State Plane North Carolina FIPS 3200 (US Survey Feet). --: compound not analyzed for the sample pg/L: micrograms per liter 213: surface water standard per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 213 — Surface Water and Wetland Standards (last amended in September 2022) or the standard obtained from the U.S. Environmental Protection Agency Nationally Recommended Water Quality Criteria for Aquatic Life and Human Health 2L: Subchapter 2L — Groundwater Classifications and Standards, Department of Environmental Quality (Amended April 1, 2022); groundwater standard from North Carolina Administrative Code, Title 15A Appendix I: indicates volatile organic compounds and metals per 40 Code of Federal Regulations Part 258 IMAC: interim maximum allowable concentration (listed in 2L Appendix 1) J: estimated value between the method detection limit and reporting limit established by the analytical laboratory. Q: RPD >40% dual column results mg/L: milligrams per liter mv: millivolts N: normal environmental sample NTU: nephelometric turbidity unit PCE: perch loroethylene SM: Standard Method SU: standard units TB: trip blank U: compound analyzed for but not detected above detection limit pmhos/cm: microsiemens per centimeter Fall 2022 Semiannual Water Quality Monitoring Report Page 3 of 3 Jackson County Closed Municipal Solid Waste Landfill March 2023 Table 4 Mass Removal Calculations for VOCs Detected in the Leachate Sample (LT-01) Sample Dates Detected VOCs Concen- tration in LT-01 (mg/L) Cumulative Flow at Gauge (gal) Differential Flow (gal) Mass Removed (lb) Estimated Cumulative Mass Removed (lb) Beginning Ending 9/1/2012 10/25/2012 1,4-dichlorobenzene 0.0034 11,500 J J J J 11,500 0.00033 4-meth I-2- entanone (MIBK) 0.0021 0.00020 Acetone 0.0292 0.00280 Benzene 0.0021 0.00020 Chlorobenzene 0.0029 0.00028 cis- 1,2-dichloroethene 0.00063 0.00006 Dichlorodifluoro-methane 0.00093 0.00009 Eth (benzene 0.0102 0.00098 Naphthalene 0.0069 0.00066 Styrene 10.00033 0.00003 Toluene 10.003 0.00029 Total x lenes 0.0094H 0.00090 Total: 0.00681 0.00681 10/26/2012 4/11/2013 1,4-dichlorobenzene 0.006 65,500 J J J J J 54,000 0.00270 Acetone 0.012 0.00540 Benzene 0.0011 0.00049 Carbon disulfide 0.0067 0.00301 Chlorobenzene 0.0024 0.00108 cis- 1,2-dichloroethene 0.00058 0.00026 Eth (benzene 0.0083 0.00373 Toluene 0.00059 0.00027 Total x lenes 0.0078 0.00351 Total: 0.02045 0.02726 4/12/2013 10/8/2013 1,4-dichlorobenzene 0.0055 114,737 J J 49,237 0.00226 4-meth I-2- entanone (MIBK) 0.0012 0.00049 Benzene 0.0020 0.00082 Chlorobenzene 0.0039 0.00160 cis- 1,2-dichloroethene 0.00080 0.00033 Eth (benzene 0.0151 0.00619 Naphthalene 0.0184 0.00754 Toluene 0.0012 0.00049 Total x lenes 0.0090 0.00369 Total: 0.02341 0.05067 10/9/2013 4/8/2014' 1,4-dichlorobenzene 0.0056 164,437 J J 49,700 0.00232 Benzene 0.0018 0.00075 Chlorobenzene 0.0051 0.00211 cis- 1,2-dichloroethene 0.00049 0.00020 Eth (benzene 0.0047 0.00195 Toluene 10.00041 0.00017 Total x lenes 10.0021 IJI 0.00087 Total: 0.00836 0.05903 4/8/2014 10/23/2014' 1,4-dichlorobenzene 0.0053 200,148 J 35,710 0.00158 Benzene 0.0014 0.00042 Chlorobenzene 0.003 0.00089 cis- 1,2-dichloroethene 0.00049 0.00015 Eth (benzene 0.0027 0.00080 Toluene 10.00051 Hi 0.00015 Total x lenes 0.0014 0.00042 Total: 0.00440 0.06343 10/23/2014 4/21/2015 1,2,3-trimethyl benzene 0.00062 241,700 41,552 0.00021 1,2,4-trimethyl benzene 0.00076 2-chlorotoluene 0.00067 1,4-dichlorobenzene 0.0059 Acetone 0.00790 Benzene 0.0022 0.000/6 Chlorobenzene 0.003 Eth (benzene 0.0056 I sopropylbenzene 0.0013 Methy tert-butyl -ether 0.0013 Na thalene 0.024 0.00831 n-propylbenzene 0.00088 Tetrah drofuran 0.089 0.03080 Toluene 0.00054 Vin I chloride 10.00038 Total x lenes 10.0030 Total: 4/21/2015 10/13/2015 1,4-dichlorobenzene 0.00600 278,420 J J J 36,720 0.00183 2-butanone 0.00960 0.00294 Benzene 0.00210 0.00064 Chlorobenzene 0.0040 0.00122 Eth (benzene 0.00710 0.00217 Naphthalene 0.021 0.00642 Tetrah drofuran 0.062 0.01896 Toluene 0.00058 0.00018 Total x lenes 0.0031 0.00095 Total: 0.03531 0.14963 10/13/2015 4/5/2016 1,4-dichlorobenzene 0.00590 337,398 J 58,978 0.00290 Benzene 0.00170 0.00083 Chlorobenzene 0.0038 0.00187 Eth (benzene 0.00500 0.00246 Toluene 0.00063 0.00031 Total x lenes 10.0025 IJI 0.00123 Total: 0.00959 0.15922 Fall 2022 Semiannual Water Quality Monitoring Report Page 1 of 3 Jackson County Closed Municipal Solid Waste Landfill March 2023 Table 4 Mass Removal Calculations for VOCs Detected in the Leachate Sample (LT-01) Sample Dates Detected VOCs Concen- tration in LT-01 (mg/L) Cumulative Flow at Gauge (gal) Differential Flow (gal) Mass Removed (lb) Estimated Cumulative Mass Removed (lb) Beginning Ending 4/5/2016 10/11/20162 No detected compounds 352,745 15,347 0.00000 Total: 0.00000 0.15922 10/11/2016 3/21/2017 1,4-dichlorobenzene 0.0046 355,947 3,202 0.00012 Acetone 0.0094 J 0.00025 Benzene 0.0015 0.00004 Chlorobenzene 0.0043 0.00011 Eth (benzene 0.0014 0.00004 Tetrah drofuran 10.066 Hi 0.00176 Total x lene 10.0015 0.00004 Total: 0.00237 0.16159 3/21/2017 10/11/2017 1,4-dichlorobenzene 0.0041 386,495 30,548 Acetone 0.0067 J J 1 UoM Acetonitrile 0.008 0.00204 Benzene 0.00061 Chlorobenzene 0.0012 Eth (benzene 10.00087 0.00022 Naphthalene 10.0012 Tetrah drofuran 10.12 Total: 0.03630 0.19789 10/12/2017 10/18/20183 1,4-dichlorobenzene 0.0028 398,872 12,377 0.00029 Acetone 0.017 J 0.00175 Benzene 0.0012 0.00012 Chlorobenzene 0.0024 0.00025 Eth (benzene 0.0018 0.00019 Methylene chloride 10.00034 111 0.00004 Total x lene 10.00098 0.00010 Total: 0.0027 0.20062 10/18/2018 10/22/20193 1,4-dichlorobenzene 0.0037 407,807 8,936 0.00028 Acetone 0.006 0.00045 Benzene 0.0017 0.00013 Chlorobenzene 0.0038 0.00028 Eth (benzene 0.0016 0.00012 Toluene 10.00039 Pi 0.00003 Total x lenes 0.0017 0.00013 Total: 0.0014 0.20203 10/22/2019 3/18/20203 1,4-dichlorobenzene 0.0056 539,644 131,836 0.00615 1,4-dioxane 0.06 J J 0.06585 Acetone 0.0064 0.00702 Benzene 0.0013 0.00143 Chlorobenzene 0.0032 0.00351 Eth (benzene 0.0027 0.00296 Methyl isobutyl ketone 0.00079 0.00087 Toluene 0.00070 0.00077 Total x lenes 0.00209 0.00229 Total: 0.0886 0.29058 3/18/2020 10/14/20203 1,2-dichloroethene, cis- 0.00029 J 639,343 99,699 0.00024 1,3-dichlorobenzene 0.00027 J il J J 0.00022 1,4-dichlorobenzene 0.0048 0.00398 1,4-dioxane 0.058 0.04814 Acetone 0.011 0.00913 cetonitri a et anenitri e 0.0047 0.00390 Benzene 0.0024 0.00199 Chlorobenzene 0.0044 0.00365 Chloroethane 0.00047 0.00039 Eth (benzene 0.0018 0.00149 Naphthalene 0.013 0.01079 Tetrah drofuran 0.094 0.07802 Toluene 0.00079 0.00066 Total x lenes 0.0037 0.00307 Vin I chloride 0.00022 0.00018 Total: 0.1659 0.45645 10/14/20204 10/20/2021 1,4-dichlorobenzene 0.00385 701,994 62,651 1,4-dioxane Acetone Benzene Chlorobenzene Eth (benzene Na hthalene Tetrah drofuran Total x lenes Total: 0.1501 0.60659 10/20/2021 3/7/2022 1,4-dichlorobenzene 0.00168 710,029 8,035 1,4-dioxane • Acetone Benzene • Chlorobenzene Tetra h drofuran 10.168 Total: 0.0585 0.66508 Fall 2022 Semiannual Water Quality Monitoring Report Page 2 of 3 Jackson County Closed Municipal Solid Waste Landfill March 2023 Table 4 Mass Removal Calculations for VOCs Detected in the Leachate Sample (LT-01) Sample Dates Detected VOCs Concen- tration in LT-01 (mg/L) Cumulative Flow at Gauge (gal) Differential Flow (gal) Mass Removed (lb) Estimated Cumulative Mass Removed (lb) Beginning Ending 3/7/2022 10/4/2022 1,4-dioxane 0.08 734,436 24,407 Benzene 5 Chlorobenzene Tetra hyd rofu ra n 0.0678 0.01378 4-Methyl-2-pentanone 0.00112 0.00023 Carbon disulfide 0.000683 0.00014 Ethylbenzene 0.000267 0.00005 Methyl ethyl ketone 0.00236 0.00048 Naphthalene 0.00366 0.00074 o-xylene 0.000465 0.00009 Toluene 0.00024 0.00005 Total xylene 0.000465 0.00009 1,4-dichlorobenzene 0.00182 0.00037 Total: 0.0327 0.69777 Notes: Total xylenes represent the sum of m,p-xylenes and o-xylenes. Only detected VOCs in leachate sample LT-01 are included in the mass removal calculation. Leachate extraction at the landfill was initiated on September 1, 2012. Connection to the TWSA sewer was completed on September 6, 2013. Up until the connection to the TWSA sewer, leachate was pumped into a temporary collection tank and then hauled off site. Extraction volume measurements for leachate hauled off site were recorded and provided by Jackson County staff. Anchor QEA bases mass removal calculations on the assumption that the VOCs concentration in one sampling event is representative of leachate quality until the next sampling event occurs and that the leachate removal system has a 100% removal and treatment efficiency. Differential flow represents the total flow between the LT-01 sample dates. Estimated cumulative mass removed and treated is estimated based upon a conversion of milligrams to pounds and liters to gallons and the multiplication of the concentration 1. Totalizer readings were not recorded during the sampling event, and the differential flow was calculated based on an interpolated totalizer reading using monthly readings taken by TWSA for 3 months before and after the sample date. 2. No VOCs were detected in the leachate sample collected during the October 2016 sampling event. 3. In March 2018, the totalizer at the TWSA connection was replaced. During the March 2018 sampling event, Anchor QEA began reading an incorrect totalizer for the volume of extracted the leachate. Differential flow was calculated for the sample dates in the same manner as Note 1. This table has been updated to reflect the updated totalizer readings from previous groundwater monitoring reports. 4. Totalizer buried during March 2021 monitoring event, due to on -Site construction. Therefore a totalizer reading was not obtained. gal: gallon J: indicates laboratory estimated concentration is above the adjusted method detection limit and below the adjusted reporting limit lb: pound mg/L: milligrams per liter TWSA: Tuckaseigee Water and Sewer Authority VOC: volatile organic compound Fall 2022 Semiannual Water Quality Monitoring Report Page 3 of 3 Jackson County Closed Municipal Solid Waste Landfill March 2023 Figures Publish Date: 2023/01/17, 2:05 PM I User: alesueur Filepath:\\orcas\gis\Jobs\JacksonCounty_NC_1480\Maps\)acksonCoLF_SemiAnnualReportsVacksonCoLF_SemiAnnualReports.aprx kZANCHOR QEA Anchor QEA of North Carolina, PLLC Figure 1 Site Location Map Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landfill SW-02 11<1j O0 0 \ O� DW-02 MW-06 (9 ®DW-01 Z ®MW-01 Q' �'• • •' .... �•1*� o ; EW -8 EW-6*'�• .♦ ♦ � EW-7 � ' �♦, ♦ EW-5 ®MW-02 1 EW-3R+ EW-1 R :•�♦ ,♦ EW-9 EW 2R+ EW-10 ♦� : .• SW 03 ¢ MW-03,' EW_4 LT-01% ��` ♦ QP ♦ �G� 4* oo ♦♦ MW-05R ♦♦ MW-07A,MW-04 '♦ i� SSW-01 l Publish Date: 2023/02/01, 8:48 AM I User: alesueur Filepath:\\orcas\gis\Jobs\JacksonCounty_NC_1480\Maps\)acksonCoLF_SemiAnnualReportsVacksonCoLF_SemiAnnualReports.aprx ANCHOR QEA Anchor QEA of North Carolina, PLLC LEGEND: Q Saprolite Monitoring Well ® PWR Monitoring Well ® Bedrock Monitoring Well Domestic Well Sampling Location Leachate Sample Location and Flow Equalization Tank Surface Water Sample Location Leachate/Landfill Gas Extraction Well • Compliance Boundary ... Edge of Waste Stream O Property Boundary Road Elevation Contour (20-Foot Interval) NOTES: 1. Contours, roads, and parcel boundaries are from Jackson County GIS. 2. Monitoring well locations are approximate. 3. Basemap provided by Esri. 4. PWR: Partially Weathered Rock 0 0 300 Feet Figure 2 Site Layout Map Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landfill CONNOR WILKEY 2060" ,(2,072.$2)� WILKEY 4p70. 2 27zp . �• • _ ♦ .... . 70 ® ♦ . 1 ♦♦ ♦` v ♦ ♦ c�0 `. ♦ O O ♦♦ 20 `` �• :• ` ♦ `♦ `. ♦♦ OO ♦♦ O O �� O ♦' 2so •• ♦♦ �� 2�8 ♦♦ 0a vO ,, ♦ • ,, ,, •••• ♦♦♦ ��r♦` �'MW-03r1. LT-01 `. (1, 994.99) •. ♦♦ Oq0 ♦♦ o ♦ ,; ��. 9 0 QPR 960. MW-07 (1^948!89) 19s0 nnw_na Publish Date: 2023/02/13, 9:06 AM I User: alesueur Filepath: \\orcas\gis\Jobs\JacksonCounty_NC_1480\Maps\JacksonCoLF_SemiAnnualReports\JacksonCoLF_SemiAnnualReports.aprx LEGEND: ® Saprolite Monitoring Well PWR Monitoring Well \ Bedrock Monitoring Well Generalized Groundwater Elevation �y Contour (10-Foot Interval) Leachate Sample Location and Flow Equalization Tank 1'o� 0 •••• Edge of waste Stream 0 Property Boundary Road Elevation Contour (20-Foot Interval) WILKEY 0 NOTES: 1. Contours, roads, and parcel boundaries are from Jackson County GIS. 2. Monitoring well locations are approximate. 3. Groundwater elevations and flow direction 2220 are updated on a semiannual basis every April and October following the sample collection events. 4. Groundwater flow direction is based on groundwater elevations in feet in monitoring wells MW-01, MW-02, MW-03, MW-04, MW-05R, and MW-06. Direction is calculated based on depth to water measured on October 3 and 4, 2022. 5. Last names of property owners are shown in parcels that border the landfill property. 6. GW: Groundwater 7. PWR: Partially Weathered Rock 0 �0 0 200 ry� � Feet kZANCHOR Figure 3 QEA Generalized Groundwater Flow Direction Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landfill Tetrachloroethene (PCE) 5 4 �3 c 0 M c 2 c 0 v 1 0 I q Date 14 12 10 c 0 8 M c 6 c 0 V 4 2 0 z11r�; 2077 2075 $ c 0 2073 a'>i w 2071 3 2069 0 ti� 2067 2065 Trichloroethene (TCE) 6 5 J 4 \ c 0 3 c v o 2 V 1 0 2�6$ Date 2079 20.0 2077 17.5 15.0 2075 � o .2 J \ 0) 12.5 2073 T LU 2 10.0 2071 c 7.5 2069 0 v �7 5.0 2067 2.5 2065 0.0 Date Pate Benzene 1,4-Dich orobenzene Notes: 1. Dashed horizontal lines represent the 2L groundwater standard. 2. Dashed vertical lines represent the start of leachate extraction. 3. Non -detects are plotted as an open symbol at the method detection limit. 4. Data presented are from semiannual sampling events from 2007 to Fall 2022. µg/L: micrograms per liter ft:feet Publish Date: 02/02/2023 10:48 AM I User: SYR-SCOL2 File Path:\\Wcl-fs1\asheville\Projects\Jackson County\ -Reports - Groundwater\python\JacksonCounty_GW_Evaluation.py kZANCHOR QEA Cis- 1,2-Dichloroethene 2079 102 2077 2075 J 101 o \ 2073 v w 0 v � 1-22071 � 3 100 2069 0 2067 10-1 2065 2079 20.0 2077 17.5 2075 o 15.0 0) i 2073 v c 12.5 w 0 2071 c 10.0 3 v 2069 c 0 U 7.5 , i 5.0 ; 2067 2.5 2065 0.0 Date 1,4-Dioxane 2079 101 2077 2075 $ � 0 J \ 2073 T 100 w � 0 2071 c U � 0 2069 0 10-1 2067 2065 79 77 75 c 0 73 rO v LL, 71 3 69 0 y 67 65 Vinyl Chloride `7 v ----- ------- ------------------------- 2dd$ 2p1' 2p1$ 2p") 2p" Date Constituent Key with 2L Standards f Tetrachloroethene (PCE) (0.70 µg/L) Trichloroethene (TCE) (3 µg/L) cis-1,2-Dichloroethene (70 µg/L) f Vinyl Chloride (0.03 µg/L) f Benzene (1 µg/L) f 1,4-Dichlorobenzene (6 µg/L) 1,4-Dioxane (3 µg/L) Groundwater Elevation (ft) -- Leachate Extraction Start Date 2079 2077 2075 $ c 0 2073 w 2071 3 2069 0 0 2067 2065 Figure 4 Hydrograph and Constituents of Concern Versus Time - MW-01 Fall 2022 Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landifll Tetrachloroethene (PCE) 5 4 �3 c O M c 2 U c O U 1 a 14 12 10 c O 8 c 6 c O U 4 2 0 Date Benzene Notes: 1. Dashed horizontal lines represent the 2L groundwater standard. 2. Dashed vertical lines represent the start of leachate extraction. 3. Non -detects are plotted as an open symbol at the method detection limit. 4. Data presented are from semiannual sampling events from 2007 to Fall 2022. µg/L: micrograms per liter ft:feet 1990 1988 1986 1984 1982 .o 1980 > LU 1978 1976 1974 0 O 1972 1970 1968 1966 c O qj U U c O U 6 5 1 0 2�6$ Date 90 ZU.0 88 17.5 86 84 15.0 82 .0 M 12.5 80 a', LU 78 — 10.0 76 0 74 0 7.5 O U 72 17 5.0 70 68 2.5 66 0.0 Publish Date: 02/02/2023 10:48 AM I User: SYR-SCOL2 File Path:\\Wcl-fs1\asheville\Projects\Jackson County\ -Reports - Groundwater\python\JacksonCounty_GW_Evaluation.py kZANCHOR QEA 2zC3$ ;)11) ;)12 ;)111 Pate 1,4-Dich orobenzene 190 11 188 186 184 )82 .0 180 > v w !78 v 12 176 3 1( 174 0 O U 172 170 168 10 166 IW 2`1 2`1 2`1 2`1 2`1 2`1 V 2`1 V n �+o 1990 1988 20.0 1986 17.5 ' 1984 ' 1982 .o 0)15.0 1980 v c 12.5 w g 1978 10.0 1976 3 v 1974 0 7.5 O U i 1972 ' 5.0 1970 1968 2.5 ---- - - -I 1966 0.0 Date 1,4-Dioxane 190 1( 188 186 184 � J 182 .o 180 v 1( w O 178 176 U 174 0 O U 172 10 170 168 166 184 182 0 M 180 v LL, 178 176 174 O 172 170 168 166 Date Constituent Key with 2L Standards f Tetrachloroethene (PCE) (0.70 µg/L) Trichloroethene (TCE) (3 µg/L) cis-1,2-Dichloroethene (70 µg/L) f Vinyl Chloride (0.03 µg/L) f Benzene (1 µg/L) f 1,4-Dichlorobenzene (6 µg/L) 1,4-Dioxane (3 µg/L) Groundwater Elevation (ft) -- Leachate Extraction Start Date 190 188 186 184 182 .o 180 178 176 174 O 172 � 170 168 166 Figure 5 Hydrograph and Constituents of Concern Versus Time - MW-02 Fall 2022 Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landifll 5 4 �3 c 0 M c 2 rZ 0 v 1 H 14 12 10 c 0 8 M c 0 6 c 0 V 4 2 0 Tetrachloroethene (PCE) 2009 2007 2005 $ 2003 0 2001 > 1999 a5 1997 1995 0 6 1993 1991 1989 Trichloroethene (TCE) 6 5 J 4 c 0 3 c v rZ Vo 2 1 0 2,,Q�, 2Q�1l 2CJNI- 2Q�10 2Q�1l 2d" 2Q22 2�6$ Date Date 20.0 2009 2007 17.5 2005 15.0 2003 0 .2 12.5 2001 > > 0) � LL, o 1999 a5 a 10.0 1997 � c c 7.5 1995 0 0 v �7 5.0 1993 1991 2.5 1989 0.0 Date Pate Benzene 1,4-Dich orobenzene Notes: 1. Dashed horizontal lines represent the 2L groundwater standard. 2. Dashed vertical lines represent the start of leachate extraction. 3. Non -detects are plotted as an open symbol at the method detection limit. 4. Data presented are from semiannual sampling events from 2007 to Fall 2022. µg/L: micrograms per liter ft:feet Publish Date: 02/02/2023 10:48 AM I User: SYR-SCOL2 File Path:\\Wcl-fs1\asheville\Projects\Jackson County\ -Reports - Groundwater\python\JacksonCounty_GW_Evaluation.py kZANCHOR QEA Cis- 1,2-Dichloroethene 2009 102 2007 2005 $ 2003 0 1 10 2001 v C LU 1999 v 12 1997 10° 1995 0 1993 1991 10-1 1989 2009 20.0 2007 2005 , 17.5 2003 0 15.0 2001 > c 12.5 ' w g 1999 10.0 1997 3: v 0 7.5 1995 0 U 5.0 1993 1991 2.5 -- i --- -- i 1989 0.0 2�1, 231, 2'32" 2'322 Date 1,4-Dioxane 2009 101 2007 2005 $ 2003 0 10° 2001 > LU 1999 a, 2 � 1997 c c 1995 0 v 10-1 1993 1991 1989 09 07 05 03 0 01 > v LL, 99 }, 97 c 95 0 0 0% 91 89 Vinyl Chloride --- ---------T------------------------- r- 2dd$ 261126122�1,o Date Constituent Key with 2L Standards f Tetrachloroethene (PCE) (0.70 µg/L) Trichloroethene (TCE) (3 µg/L) cis-1,2-Dichloroethene (70 µg/L) f Vinyl Chloride (0.03 µg/L) f Benzene (1 µg/L) f 1,4-Dichlorobenzene (6 µg/L) 1,4-Dioxane (3 µg/L) Groundwater Elevation (ft) -- Leachate Extraction Start Date 2009 2007 2005 $ 2003 0 2001 LU 1999 1997 1995 0 1993 1991 1989 Figure 6 Hydrograph and Constituents of Concern Versus Time - MW-03 Fall 2022 Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landifll Tetrachloroethene (PCE) Trichloroethene (TCE) 5 4 �3 c O M c 2 c O U I 14 12 10 c O 8 M c 6 c O U 4 2 0 1958 6 5 1956 $ o J 4 a>i � 1954LU 3 nz 3 c v 0 U o 2 0 U 1952 1 1950 0 2,,Q�, 2Q�1l 2CJ122Ci1I 2Q�10 2Q�1l 2d" 2Q22 2�6$ Date Date 1958 20.0 17.5 1956_ 15.0 � o J \ 0) 12.5 a>i � 1954 — 10.0 � c U 7.5 O o U 1952 5.0 2.5 1950 0.0 2z6$ 2cj1' 2cj16 2�1$ 2�212�22 Date Pate Benzene 1,4-Dich orobenzene Notes: 1. Dashed horizontal lines represent the 2L groundwater standard. 2. Dashed vertical lines represent the start of leachate extraction. 3. Non -detects are plotted as an open symbol at the method detection limit. 4. Data presented are from semiannual sampling events from 2007 to Fall 2022. µg/L: micrograms per liter ft:feet Publish Date: 02/02/2023 10:48 AM I User: SYR-SCOL2 File Path:\\Wcl-fs1\asheville\Projects\Jackson County\ -Reports - Groundwater\python\JacksonCounty_GW_Evaluation.py kZANCHOR QEA 1958 102 1956 $ c O 101 1954 3 100 C 0 O 0 1952 6 V IM 1950 1958 Cis- 1,2-Dichloroethene 1 1 I 1 I 1 I 1 1 1 I 1 1 I 1 I 1 1 1 1 1 1 1 ,ZpO�,Zp'\�,Lp12,1p1�,Lp1�,Lp1� 2p2� 2p2 20.0 17.5 1956 o 15.0 v c 12.5 1954 Z- ' 1 v 10.0 fu 3: c v o 7.5 O U i 1952 ' 5.0 1 I 2.5 1 I 1950 0.0 Date 1,4-Dioxane 1958 10, 1956 $_ � O J \ > 100 v � 1954 U .0 U � C U 0 O 1952 6 U 10-1 1950 c O 2 0 0 N Vinyl Chloride 2d3002p1' 2p122p112"1, 2�100 �)113 2�22 Date Constituent Key with 2L Standards f Tetrachloroethene (PCE) (0.70 µg/L) Trichloroethene (TCE) (3 µg/L) cis-1,2-Dichloroethene (70 µg/L) f Vinyl Chloride (0.03 µg/L) f Benzene (1 µg/L) f 1,4-Dichlorobenzene (6 µg/L) 1,4-Dioxane (3 µg/L) Groundwater Elevation (ft) -- Leachate Extraction Start Date 1958 1956_ c O a� 1954 3 C Z) O 1952 6 1950 Figure 7 Hydrograph and Constituents of Concern Versus Time - MW-04 Fall 2022 Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landifll 5 0 Date 14 12 10 c O 8 M c 6 c O U 4 2 0 B9 57 B5 0 a� w B3 3 B1 CS O 79 77 1 0 2�6$ Date I yjbj LU.0 17.5 1987 15.0 1985 0 .2 12.5 a>i 0) � LL, o 1983 — 10.0 � c 1981 c o 7.5 O U �7 5.0 1979 2.5 1977 0.0 2310 2�1" 2�2� 2�22 2��$ 2�1� 2�122�1� 2j16 2�1$ �3113 2�22 Date Pate Benzene 1,4-Dich orobenzene Notes: 1. Dashed horizontal lines represent the 2L groundwater standard. 2. Dashed vertical lines represent the start of leachate extraction. 3. Non -detects are plotted as an open symbol at the method detection limit. 4. Data presented are from semiannual sampling events from 2007 to Fall 2022. µg/L: micrograms per liter ft:feet Publish Date: 02/02/2023 10:48 AM I User: SYR-SCOL2 File Path:\\Wcl-fs1\asheville\Projects\Jackson County\ -Reports - Groundwater\python\JacksonCounty_GW_Evaluation.py kZANCHOR QEA 89 1 87 85 0 ' 1 D (U w O 83 v 12 3 � 1 81 O O U C7 79 1c 77 •�• 20.0 1987 17.5 1985 0 15.0 0 v c 12.5 w g 1983 10.0 3 v 1981 0 7.5 O 5.0 ; 1979 ; 2.5 1977 0.0 Date 1,4-Dioxane 89 1 87 85 o J w O 83 U rZ c 81 S o O U 1C 79 77 87 85 c O v 83 w 79 Date Constituent Key with 2L Standards f Tetrachloroethene (PCE) (0.70 µg/L) Trichloroethene (TCE) (3 µg/L) cis-1,2-Dichloroethene (70 µg/L) f Vinyl Chloride (0.03 µg/L) f Benzene (1 µg/L) f 1,4-Dichlorobenzene (6 µg/L) 1,4-Dioxane (3 µg/L) Groundwater Elevation (ft) -- Leachate Extraction Start Date 89 87 85 0 a� w 83 81 ZS O 79 77 Figure 8 Hydrograph and Constituents of Concern Versus Time - MW-05R Fall 2022 Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landifll 5 4 >s �3 c O M 1 H 14 12 10 c 0 8 c 6 c 0 V 4 2 0 Date Benzene Tetrachloroethene (PCE) i -- - -------L------------------- 2��� Notes: 1. Dashed horizontal lines represent the 2L groundwater standard. 2. Dashed vertical lines represent the start of leachate extraction. 3. Non -detects are plotted as an open symbol at the method detection limit. 4. Data presented are from semiannual sampling events from 2007 to Fall 2022. µg/L: micrograms per liter ft:feet 2066 2064 2062 2060 O 2058 a� 2056 Lu a� 2054 2052 D O 2050 2048 2046 Trichloroethene (TCE) 6 A 5 J 4 c 0 3 c v V rZ O 2 V 1 0 2�6$ Date 56 20.0 64 17.5 ' 52 15.0 60 58 a 12.5 1 a>i i LL, 56 o10.0 nz c 54 c 7.5 52 0 v 50 5.0 48 2.5 46 0.0 2zdco, Pate 1,4-Dich orobenzene Publish Date: 02/02/2023 10:48 AM I User: SYR-SCOL2 File Path:\\Wcl-fs1\asheville\Projects\Jackson County\ -Reports - Groundwater\python\JacksonCounty_GW_Evaluation.py kZANCHOR QEA Cis- 1,2-Dichloroethene 2066 102 2064 2062 2060 J 101 o 2058 ,U 2056 "' .° v � 2054 3 v 100 -6 2052 0 V c 0 2050 2048 10-1 2046 2066 2064 20.0 2062 17.5 ' 2060 0 15.0 2058 E v c 12.5 2056 Lu 10.0 2054 'u � 2052 0 v 7.5 2050 5.0 2048-------- 2.5 --- 2046 0.0 3,\" 2Q00 231" 2�12 231, 2Q;1' 2Q212Q22 Date 1,4-Dioxane 2066 101 2064 2062 2060 J o as 2058 > 100 v � 2056 "' .° 2054 2052 o V C 0 2050 10-1 2048 2046 64 62 60 58 56 w 54 52 O 50 48 46 Vinyl Chloride ::_7 m ----- ------------------ -------------- 2dd$ 2p1' 2p1$ 2p") 2p" Date Constituent Key with 2L Standards f Tetrachloroethene (PCE) (0.70 µg/L) Trichloroethene (TCE) (3 µg/L) cis-1,2-Dichloroethene (70 µg/L) f Vinyl Chloride (0.03 µg/L) f Benzene (1 µg/L) f 1,4-Dichlorobenzene (6 µg/L) 1,4-Dioxane (3 µg/L) Groundwater Elevation (ft) -- Leachate Extraction Start Date 2066 2064 2062 2060 0 2058 a� 2056 a� 2054 3 2052 0 2050 2048 2046 Figure 9 Hydrograph and Constituents of Concern Versus Time - MW-06 Fall 2022 Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landifll Tetrachloroethene (PCE) Trichloroethene (TCE) 5 4 M c 2 c O U 1 0 14 12 10 c O 8 M c 6 c O U 4 2 0 1954 6 5 1952 0 4 a>i � w O 3 nz 3 c a, 1950 � rZ 2 O t� 1 1948 0 2CJQ�, 2c31I 2CJ122Ci1I 2c310 2Q�1l 2d" 2Q22 2�6$ 2��2;)111 ;),\6 Date Date 1954 20.0 17.5 15.0 1952 0 .2 12.5 a>i 0) � 10.0 1950 u o 7.5 O U �7 5.0 2.5 1948 0.0 1954 102 F 1952 0 101 w O v `a 3 100 1950 O O U 6 10-1 1948 1954 20.0 17.5 1952 0 15.0 v c 12.5 w .0 v � 10.0 3 a, 1950 � u a 7.5 O U 5.0 2.5 1948 0.0 Cis- 1,2-Dichloroethene Date 2cj,, 231,3 3NI, 23No 3,\" 2Q2V 2Q22 2z6$ 2316 2�1$ 3113 2�22 2Q00 231" 3,\" 2Q�1, 2Q;1' 2Q212'322 Date Pate Date Benzene 1,4-Dich orobenzene 1,4-Dioxane Notes: 1. Dashed horizontal lines represent the 2L groundwater standard. 2. Dashed vertical lines represent the start of leachate extraction. 3. Non -detects are plotted as an open symbol at the method detection limit. 4. Data presented are from semiannual sampling events from 2007 to Fall 2022. µg/L: micrograms per liter ft:feet Publish Date: 02/02/2023 10:48 AM I User: SYR-SCOL2 File Path:\\Wcl-fs1\asheville\Projects\Jackson County\ -Reports - Groundwater\python\JacksonCounty_GW_Evaluation.py kZANCHOR QEA 1954 10, 1952 0 > 10° a, w rZ O U 1950 � u 0 0 O U 0 10-1 1948 1952 c O Y 1948 Vinyl Chloride 2�d$ Date Constituent Key with 2L Standards f Tetrachloroethene (PCE) (0.70 µg/L) Trichloroethene (TCE) (3 µg/L) cis-1,2-Dichloroethene (70 µg/L) f Vinyl Chloride (0.03 µg/L) f Benzene (1 µg/L) f 1,4-Dichlorobenzene (6 µg/L) 1,4-Dioxane (3 µg/L) Groundwater Elevation (ft) -- Leachate Extraction Start Date 1954 F_ 1952 0 1948 a� w Me Figure 10 Hydrograph and Constituents of Concern Versus Time - MW-07 Fall 2022 Semiannual Water Quality Monitoring Report Jackson County Closed Municipal Solid Waste Landifll Appendix A Well Sampling Logs, and Equipment Documentation and Instrument Calibration Data Sheets ANCHOR OEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Equipment Documentation and Instrument Calibration Data Sheet Project Name: Jackson COun Landfill Analyst Conducting Calibration: Project Number: C73"Q4: AP Z ,b Date of Calibration: _ Project Location: Dillsboro, NC Date of Field Measurements: j Facility ID or Permit # (if applicable): 50-02 EQUIPMENT DOCUMENTATION Rental sample analysis equipment or meters used to take measurements: Equipment Type Brand Serial Number Date of Use Rental Company Select Turbidimeter. Hach 21000 (s/n 151006045207) HF Scientific MicroTPW (s/n 200601045) Asheville, North Carolina 28801 Instrument Readings Instrument Readings (Hach 2100 (HF Scientific MicroTPW) Cal Std Information 10 NTU 20 NTU 100 NTU 800 NTU 1,000 NTU 10.0 NTU 0.02 Lot #: Expiration Date: Cal (NTU): 3 q a `v1 Cal (NTU):. s/ Cal (NTU : Cal (NTU): Cal (NTU): gal (NTU): Time: /n �(/ Time:h�J Time: Time: Time: Time: Calibration *Pre -Analysis Result (NTU): Time: t *Pre -Analysis Ra t (NTU): Time: Verification-_ Check (10 NTU): f - t-{L Check (10 NTU *Post -Analysis Resu NTU): Time: -'7._(�} n SS *Post -A sis Result (NTU): Time: Check (10 NTU): to I v Che (10 NTU): YSI Professional Plus Multiparameter Mete n 188101802) Cal Std Information Instrument Readings Date ° Lot# ❑ ened p• Date Dissolved Oxygen Initial (% : i Cal (%): mmHg: Temperature CC): Time: (% saturation) , L S . rioq DO (Site #2, Initial I%): Cal (%.: mmHg: Temperature (°C): Time: if applicable)* QC** Check DO Time: Res It %): Time: Result I%): Time: Result (%): PH 7 S.U. Initial: //'� pHmV:, Cal (S.U.: rl N pHmV: (J�a ;'mr-' �G l� l via t report to0.7S.U. V °v i)L11' PH 4 S.U. Initial: pHmV: Cal (S.U.): pHmV: ii � Time: } 01V� ICI f fD50 Ica report toais.U. +0 • l PH 10 S.U. Initia:^ pHmV: �o Cal (S.U.):: pHmV: 4,9 Time: j . j iL1 ( I ©� report to 0.1 S.U. (J ' i r l ( QC** pH 7 S.U. Time:�n Result (S.U.): Time: Result .U.): Time: Result (S.U.): jG IQ In1`1v report to 0. 1 S.U. 1�I0 li Spec. Cond. Initial: Cal (pmhos/cm): Time: I �I ad 1,000 mhos/cm Vl1/ Recove = QC** Spec. Cond. Time: Result (pmhos/cm): Time: Result (ppmhhos/cm): Time: Result (pmhos/cm): �G1 � ( 5 '' 1,000 mhos/cm 5 vJib V v % Recovery= ORP ;'Oq mV IniLial: 'Cal.: pS�J0 0 To It rc): Time: iU U P i Anatyst Signature: yst Name: Date: tots Notes: Revision 6, 12/20/20, MAK 1. Instruments shall be calibrated in accordance with the manufacturer's operation manual. 2. Specific Conductivity should be calibrated according to values representative of historic range. 3. Order of Calibration is as follows: Specific Conductivity, pH 7, PH 4, pH 10, DO, ORP, QC checks. 4. *When performing DO analyses at multiple sample sites (i.e. project/facility locations), the DO probe must be calibrated at each sample site prior to analysis. S. QC Acceptable Ranges: PH +/- 0.1 S.U. and Specific Conductivity 10%of the true value. If QC readings are out of range, the instrument needs to be recalibrated. 6. ** QC check must be performed prior to sampling and following completion of sampling, at a minimum. QC checks must be performed with calibration standard from a separate lot # as the initial QC. 7. % Recovery = (Value Obtained, pmhos/cm + True Value, pmhos/cm) x 100 8. NC Field Laboratory Certificate Number 5445 9. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 10. Unless otherwise noted, all DO calibrations and measurements are performed at 0 ppt Salinity. 11. 1 pmho/cm = 1 pS/cm Abbreviations: Method Reference: pmhos/cm: micromhos per centimeter NTU: nephelometric turbidity units Temperature: SM 2550 B-2010 'C: degrees Celsius ORP: oxidation reduction potential Specific conductivity: EPA Method 120.1, Rev. 1982 DO: dissolved oxygen s/n: serial number DO: SM 4500 O G-2011 mg/L: milligrams per liter S.U.: standard units pH: SM 4500-H' B-2011 mv: millivolt Spec. Cond.: Specific Conductivity Turbidity: SM 2130 B-2011 ac(cid i��( cUvdte 1nt, c age 1 of 1 ,n�C/� � ��(�� (�/�C �Gt-{ -- /�' C a cc �/ CI `(W►� ` 6 � V J,U y�Ai�1CHOR ,�, z QEA Equipment Documentation and Instrument Calibration Data Sheet Project Name: Jackson County Landfll Analyst Conducting Calibratio Project Number: S3a489-B492 C Date of Calibratio Project Location: Dillsboro, NC _ Date of Field Measuremen Facility ID or Permit # (if applicable): 50-02 EQUIPMENT DOCUMENTATION Rental sample analysis equipment or meters used to take measurements: E ui ment Type Brand Serial Number Date of Use Rental Com an V Select Turbidimeter.� Hach 2100Q (s/n 151006045207) HF Scientific MIcroTPW (s/n 200601045) Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Instrument Readings (Hach 2100Q) Instrument Readings (HF Scientific MicroTP Cal Std Information 10 NTU 20 NTU 100 NTU 800 NTU 1,000 NTU 10.0 NTU pratu Lot #: Expiration Date Cal (N U l Cal L4T' r Cal [ al (NTU): Cal (NTU): Cal (NTU): Time: Tim Time: Time: . Time Time: Calibration Verification: *Pre -Analysis Check (10 NTU): Result (NTU): 1 • Time: 5-;L *Pre -Analysis Check TU): Result (NTU): Time: *Post -Analysis Check (10 NTU): Result (NTU): Time: 'I°j *P -Analysis Check (10 NTU): Result (NTU): Time: YSI Professional Plus Multiparameter Meter s/n 18B101802) Instrument Readings Cal Std Information Lot# Date Opened P Date Dissolved Oxygen 0/6saturation) Initial (%): lo 1 .01 Cal M: 10 mm r Temperature (°C): (la1009 Time: DO (Site #2, if applicable)* Initial (%): Cal (%): mmHg: Temperature (°C): Time: QC** Check: DO Tim :� Result (: (J'1 Time: Result (%): Time: Result (%): PH 7 S.U. report toO.IS.U. Initial: ''`` , U pHmV n /n s��Y'4� Cal (S.U.): rV � pHmV: Time: �� i (�1 ® d+ PH 4 S.U. report to 0.1 S.U. Initial; 1_ll pHmV: Cal (S U.): pH Vt t4 1 Time: I&IT PH 10 S.U. report to 0.1 S.U. Initial: .0 pHmV: Cal (S.U.): pHmV, O Time: j(-gl �"/ C t/lJt 22 r V {I QC** pH 7 S.U. report to 0.7 S.U. Time Rest ( �.� t Time: I q0 f 1 UZI Result (S.U.): Time: Result (S.U.): /� r "i 7 Spec. Cond. 1,000 mhos/cm niti 1 A Cal (ymhos/cm): Timee- (� V W� I i / ��` zZ f i 0r ?. Recove = QC** Spec. Cond. 1,000 p mhos/cm Time: V--1 �� Result (pmhos/cm): to 2-1 Time: Result (plmhos/cm): ' I v :�+ Time: Result (pmhos/cm): �Q v-e Recove = ORP 200 mV In', I ' Cal: A /Vlfl Jl Temn 'ture (°C): Time: Analyst Signature: Analyst Name: Ifi Date: i3 Notes: Revision 6, MAK /� R „ 1 / 1 1. Instruments shall be calibrated in accordance with the manufacturer's operation manual. nts shall Vl (�', 111 lJ 2. Specific Conductivity should be calibrated according to values representative of historic range. 3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks. A ^ flJU�fl/ G 2 4. *When performing DO analyses at multiple sample sites (i.e. project/facility locations), the DO probe must be calibrated at each sample site prior to analysis. 1 J 5. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out ofrange, the instrument needs to be recalibrated. 6. ** QC check must be performed prior to sampling and following completion of sampling, at a minimum. QC checks must be performed with calibration standard from a separate lot # as the initial QC. 7. % Recovery = (Value Obtained, pmhos/cm a True Value, pmhos/cm) x 100 8. NC Field Laboratory Certificate Number 5445 9. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 10. Unless otherwise noted, all DO calibrations and measurements are performed at 0 ppt Salinity. 11. 1 pmho/cm = 1 pS/cm Abbreviations: Method Reference: pmhos/cm: micromhos per centimeter NTU: nephelometric turbidity units Temperature: SM 2550 B-2010 'C: degrees Celsius ORP: oxidation reduction potential Specific conductivity: EPA Method 120.1, Rev. 1982 DO: dissolved oxygen s/n: serial number DO: SM 4500 O G-2011 mg/L: milligrams per liter S.U.: standard units pH: SM 4500-H' B-2011 mv: millivolt Spec. Cond.: Specific Conductivity Turbidity: SM 2130 B-2011 Page 1 of 1 Anchor QEA of North Carolina, PLLC +SZANCHOR �'C �► ra 6Poff .� �arCi:�"� �..i�i.d1r uioment Documentation and Instrument Calibration Data Sheet Project Name: 30LC kSO P 1 {naytd' (� Analyst Conducting Calibration: —T(Y1 Project Number: iv 2 IUg d — O k- 01 Date of Calibration: 1 a Z3 Project Location: %JJ6c>v-n , V,4 C., _ Date of Field Measurements: Facility ID or Permit # (if applicable): SO — o 2.. EQUIPMENT DOCUMENTATION Rental sample analysis equipment or meters used to take measurements: 231 Haywood Street Asheville, North Carolina 28801 Equipment Type Brand Serial Number Date of Use Rental Company Select Turbidimeter, Hach 2100Q (s/n 151006045207) Rental Hach 2100Q (s/n Instrument Readings (Hach 2100Q) Cal Std Information 10 NTU 20 NTU 100 NTU 800 NTU Lot #: R 2 'L i°ti % J'sI TI M LI 10 E!ggiration Date: I Cal (NTU):2� ' Cal (NTU): D Cal (NTU): Q,L Timer Time: Time: Calibration Verification: *Pre -Analysis Check (10 NTU): Result � (NTU): '!l - 10 Time: On .Post -Analysis Check (10 NTU): Result (NTU): Tim�erp YSI Professional Plus Multiparameter Meter (s/n 118111111011802) Instrument Readings Cal Std Information Lot # Date ened Exp. Date Dissolved Oxygen (% saturation) Initial (%): t{ ,� Cal (%): i<l/ U- a mmH rp�j , 5 Temperature CC). I,& 4 Time://�j ! (l 0 DO (Site #2, if a licable)* Initial (%): Cal (%): mmHg: Temperature CQ: Time: QC** Check: DO Time,.,0 32 tVi L Result (%):/0 ! Time: Result (%): 7-K" Ime: I Result (%): r 3 PH7S.U. report to0.1S.U. Initi I: (p.Q(p pHmV: 25 Cal (S.U.): O1 pHmV: — 2 5 - Time: .5G uhr ® 4113 PH 4 S.U. report to0.1S.U. Ini`tial:• `"l•C> pHmV: {ti• Cal (S.U.): t0.1 ct-Jl7 pHmV: c� b�i�• V Time: 096'.0 1011 Lt lC7(22 �2 PH 10 S.U. report to0.1S.0 Initial: �l%•OrJ pHmV: �� (P Cal (S.U.): t{�'13, pHmV: Time: J '.OL itT Z QC** pH 7 S.U. report to 0.1 S.U.I%2 Time: Result (S.U.):2 . J J Time: L56 • Result (S.U.): Time: Result (S.U.): li Ito l�2 ( .` 1L.`i Spec. Cond. 1,000 mhos/cm Initial: `` to() 5 Cal (pmhos/cm): 10U0 Time: VT t 6 Z Ih (045 1112� �i�3 % Recovery= QC** Spec. Cond. 1.000 pmhos/cm Time: ' 2, 7-��� Result (Nmhos/cm): Timte�: v Result�(pmmhos/cm): lt6 [3 Time: Result (Nmhos/cm): ,&o iI / b'gL22 6 7,�/ /23 % Recovery= ORP 200 mV Initial: Lo • Cal: 2a� Temperature CC): Time: y to Analyst Signature: Analyst Name: lessic., m Date: 01 t 0 2 Notes: r Revision 8, 1/11/22, CAP 1. Instruments shall be calibrated in accordance with the manufacturer's operation manual. 2. Specific Conductivity should be calibrated according to values representative of historic range. 3.Order of Calibration is as follows; Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks. 4. 'When performing DO analyses at multiple sample sites (i.e. project/facility locations), the DO probe must be calibrated at each sample site prior to analysis. 5. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 1091 of the true value. If QC readings are out of range, the instrument needs to be recalibrated. 6. "* QC check must be performed prior to sampling and following completion of sampling, at a minimum. QC checks must be performed with calibration standard from a separate lot # as the initial QC. 7. % Recovery = (Value Obtained, pmhos/cm . True Value, pmhos/cm) x 100 8. NC Field laboratory Certificate Number 544S 9. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 10. Unless otherwise noted, all DO calibrations and measurements are performed at 0 ppt Salinity. 11. 1 pmho/cm = 1 pS/cm Abbreviations: Method Reference: pmhos/cm: micromhos per centimeter NTU: nephelometric turbidity units Temperature: SM 2550 B-2010 °C: degrees Celsius ORP: oxidation reduction potential Specific conductivity: EPA Method 120.1, Rev. 1982 DO: dissolved oxygen s/n: serial number DO: SM 4500 O G-2011 mg/L: milligrams per liter S.U.: standard units pH: SM 4500-H* B-2011 mV: millivolt Spec. Cord.: Specific Conductivity Turbidity: SM 2130 B-2011 Page 1 of 1 liiz ANCHOR CIEA iri-rvI Equipment Documentation and Instrument Calibration Data Sheet Project Name:SdLCtSoyt_(.0 hn�� tjW tjE!!2e\ Analyst Conducting Calibration: Project Number. C 2 ) y ra O - OL . 01 Date of Calibration: 0 ( 1 1 O f 2� Project Location: n i kkS lrs c x'o. t%M Date of Field Measurements: [} (! 10 / 7, Facility ID or Permit # (if applicable): _ s O - l EQUIPMENT DOCUMENTATION Rental sample analysis equipment or meters used to take measurements: Equipment Type Brand Serial Number Date of Use Rental Company Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Select Turbidimeter. Hach 2100Q (s/n 151006045207) Rental Hach 2100Q (s/n i Instrument Readings 10 NTU 21 22 d L (Hach 20 NTU IA2.1ZS 0 el 7. 3 Cal (NTU): 21000) 100 NTU As123 V Cal (NTU): q $00 NTU A2(10 U-+ I Cal (NTU): S� Cal Std Information Lot#: Expiration Date: *Pre -Analysis Time: to , Result (NTU): Time: O Time: Time: r� - 1 Calibration Verification: Check (10NTU): *Post -Analysis Check (10 NTU): q • 1'2 Result (NTU): 0� 1O Time: C✓ �d YSI Professional Plus Multiparameter Meter (s/n 1BB101802) Cal Still Information Instrument Readings Date Lot If O enact Ex. Date P Dissolved Oxygen Initial (*A): Cal (%): mmHg: Temperature CQ: Time: (% saturation) b9:3. 2.ci 1-1. S az2 o DO (Site #2, Initial (%): Cal (%): mmHg: Temperature CC): Time: if a licable)* QC** Check DO Time: 1�:32 Result (%): too.a Time: Result (%): Time: Result PH 7 S.U. Initial: pHmV: - �, Cal (S.U.): � pHmV: Z-�"'• � Time: o`I52 1 Cst F 1O1�� 0(0123 report to 0.1 S.U. . (� � . • C1 — CD �- PH 4 S.U. Initial: pHmV: Cal (S.LQ: pHmV: Time: 16tL report to0.1S.U. y.Ob 14 0. .00 Jq0.H og S5 014q 10IL2, 0112.3 PH 10 S.U. report to0.1S.U. Initial: 10-v-4 pHmV: ' "2C�2•L' Cal (S.U.): 0•C) pHmV: -101- I Time: ldU-�> LG1S. 5%(P 65122 M12.3 QC** pH 7 S.U. Time: 10 1 5 Result (S.U.): -4.0Qic Time: l Z-1 lb.�( Result (S.U.): Time: Result (S.U.): 2f3tA 1012-2, 0112_q report to0.1S.U. 6 -02- 610 Spec. Cond. Initial:: Cal (pmhos/cm): Time: 2. R 1,000 mhos/cm ( 5 3 1 000 �` q J q m 081�3 % Recovery= QC** Spec. Cond. Time: Result (pmhos/cm): Time: Result Time: Result (pmhos/c n 1 1 ` 00 2- (U -Z2 �(p(m�,hos/cm): "1 tS OV1Z2. f�23 1.000 pmhos/cm ( 1 % Recovery= ORP 200 mV InitialQQ: 1.-1.'3'.Lt Cal:+ Temperature (°C): 1c.� Time: 0'�23 �c�123 -oa Analyst Signature: Analyst Name: 5mccc, ("CULA,rs Date: 6 I I I ol 7- Notes: If IF t Revision 8, 1/11/22, CAP 1. Instruments shall be calibrated in accordance with the manufacturer's operation manual. 2. Specific Conductivity should be calibrated according to values representative of historic range. 3.Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks. 4. When performing DO analyses at multiple sample sites (i.e. project/facility locations), the DO probe must be calibrated at each sample site prior to analysis. 5. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated. 6. - QC check must be performed prior to sampling and following completion of sampling, at a minimum. QC checks must be performed with calibration standard from a separate lot # as the initial QC. 7. % Recovery = (Value Obtained, pmhos/cm _ True Value, pmhos/cm) x 100 8. NC Field Laboratory Certificate Number 5445 9. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 10. Unless otherwise noted, all DO calibrations and measurements are performed at 0 ppt Salinity. 11. 1 pmho/cm = 1 pS/cm Abbreviations: Method Reference: pmhos/cm: micromhos per centimeter NTU: nephelometric turbidity units Temperature: SM 2550 B-2010 'C: degrees Celsius ORP: oxidation reduction potential Specific conductivity EPA Method 120.1, Rev. 1982 DO: dissolved oxygen s/n: serial number DO: SM 4500 O G-2011 mg/L: milligrams per liter S.U.: standard units pH: SM 4500-H' B-2011 mV: millivolt Spec. Cond.: Specific Conductivity Turbidity: SM 2130 B-2011 Page 1 of 1 ANCHOR V QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Well Sampling Log Well ID: -MN - © 1 Project Name: 10LLksbyl CXA6" (.AyLdit Date: 011 oq IZ Project Number. C 21'480 — O(- O 1 Weather: w t] S . Project Location: n %XCO&oM , I'G Facility ID or Permit # (if applicable): Sample Collector(s):-7Zm , C,14-p Sample ID (on COC): cLOZ?) ollool — mHQ - O I Well Diameter: 2 in Sample Time: 12,30 Screen Interval: NIA ft bgs Measuring Point: 70C Well Depth (WD): //0- J ft TOC Well Type: kStick Up ❑Flush Mount Water Level in Feet (WL): 1 � � ft TOC Comments: Length of Water Column (LWQ: `Q o ft; (WD - WL) One Casing Volume: gallons; (LWC x WCV) Three Casing Volumes: o $! gallons Actual Volume Purged: gallons Tagged Bottom: at (time): Three Casing Volumes: gallons Well Casing Volumes (WCV) 1" = 0.04 Gal 2" = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft Purge Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Sample Method: Bailer-Disp. ailer-Teflon Dedicated Pump Whale Pump Grundfos Other. Oxidation Dissolved Specific pH (S.U.) Reduction Gallons Temperature Oxygen Conductivity report to 0.1 Potential Turbidity Reading Time Purged VQ (mg/L) (pmhos/cm) S.U. (m1) (NTU) Comments 3 4 5 6 7 8 9 10 Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass 1 L Glass 'Z Other Protective Casing: Pad: Lock: Vegetation: Access: Sample Analysts Sample Signature: Analysts Name: BSSi C.0 Dater Notes: IJ ' 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity, +/- 3% Conductivity, +/- 0.7 pH unit; +/- 70 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field Laboratory Certificate Number 5445 Abbreviations: Method Reference: °C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet Specific conductivity. EPA Method 120.1, Rev. 1982 mg/L milligrams per liter in: inches DO: SM 4500 O G-2011 mv: millivolt bgs: below ground surface pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 Page 1 of 1 ANCHOR �L QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Well Sampling Log Well ID: _ 0 2 Project Name: 14ksoh CaAn7fr A L,et;AaN L I Date: 01 10i Z j Project Number. C 1_1 'I is 0 — 0I , p I Weather. Suu5 1 su"Yv�!36�[ C Project Location: '0 m SIx`N 1 NC Facility ID or Permit * (if applicable): 50 - OZ Sample Collector(s): 'I-m ' C pcp Sample ID (on COQ: 2 U23n, l rV - 01MV - 01— Well Diameter. 'L in Sample Time: Screen Interval: 1N j ft bgs Measuring Point: i . Well Depth (WD): �� ft TOC Well Type: Stick Up oFlush Mount Water Level in Feet (WL): ft TOC Comments: Length of Water Column (LWQ: � ft; (WD - WL) One Casing volume: gallons; (LWC x WCV) Three Casing Volumes: -L •� gallons Actual Volume Purged: gallons Tagged Bottom: j ft at (time): Three Casing Volumes: gallons Well Casing Volumes (WCV) 1" = 0.04 Gal/Ft 2" = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft Purge Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Sample Method: Say er- isp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Oxidation Dissolved Specific pH (S.U.) Reduction Gallons Temperature Oxygen Conductivity report to 0.1 Potential Turbidity Reading Time Purged (°C) (mg/L) (pmhos/cm) S.U. (mv) (NTU) Comments 1 lulss i 0 l3 '; i 34 `3u Sr 3 2 3 4 5 6 7 8 9 10 Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plasticd' 40 mL Glass 1 L Glass Other Protective Casing: __N/ Pad: Lock: _J Vegetation: Access: Sample Analysts Sample Signature: Analysts �CG� Date: 0 0 Name• Notes: u ' 1: Stabilization -( successive readings, 3 minutes apart): within +/- 70% DO and turbidity,' +/- 3% Conductivity, +/- 0.1 pH unit +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field Laboratory Certificate Number 5445 Abbreviations: °C: degrees Celsius S.U.: standard units pmhos/cm: micromhos per centimeter ft: feet mg/L- milligrams per liter in: inches mv: millivolt bgs: below ground surface NTU: nephelometric turbidity units TOC: top of casing Method Reference: Temperature: SM 2550 B-2010 Specific conductivity: EPA Method 120.1, Rev. 1982 DO: SM 4500 O G-2011 PH: SM 4500-H' B-2011 Turbidity: SM 2130 B-2011 13 0 i-r/C-// df), PAI �*f\ 0 4 y� Page 1 of 1 ANCHOR �CEA 6.C..Li Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Low -Flow Sampling Log Well ID: fAN/—{Q_?, Project Name: )OtC1L�h �u ldC,�� Project Number. G 21 ti to — 0 % • 01 Project Location: 1Dms1oD ypKc Sample Collector(s): r 1nn , c IMP Well Diameter. 2. Screen Interval: Lila • S ^ (e3 , 5 Well Depth (as constructed): (OS-5 Depth to Water. i 0 s61"1 Measuring Point: -TAG Depth of Pump Intake: 60 Pump Used (circle): Peristaltic Bladder Comments: �t�ytiti r, , l� :�� ►ins} Date: Weather. Facility ID or Permit # (if applicable): Sample ID (on COC): in Arrive at Well: ft bgs StartTime: ft bgs Sample Time: ft Leave Well: Well Type: ft Tagged Bottom: Other (describe): b1 JOWt Z3 o Lzf (,(c7 A S 0— C>2. 20'y 10t of l ^ 03 .Stick Up ❑Flush Mount ft at (time): Purge Rate: Total Volume Purged: Pump Speed: Time DTW (feet) Temperature (°C) Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) PH (S.U.) report to 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) ZLi S fD 130 ,2• 1i S- i6 5 C E t -+0 l"2.1 � 2 Via r 9 3 L 5.Z K9=L CIO .lac (J.2 1-9 IK .O 11-3 t �¢ = �- 2, 1 Co - (� l� U l 1 �- -�{ 2•© �" U• l9 �®off Sample Analyst Signature: Sample Analyst Name: ca, r0a:��Date: 011Oc( �Z3 s Notes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity,, +/- 3% Conductivity,, +/- 0.7 pH unit +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017; 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff member's initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field laboratory Certificate Number 5445 5.1 pmho/cm = 1 VS/cm Abbreviations: Method Reference: 'C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter in: inches DO: SM 4500 O G-2016 mv: millivolt bgs: below ground surface pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 Page 1 of 1 ANCHOR Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Low -Flow Sampling Log Project Name:�df (C.SO✓t /• G __2avtv�ttAf Project Number. Project Location: 13,%1t3100,r0 r KC Sample Collector(s):�r Well Diameter. Screen Interval: 2S Well Depth (as constructed): Depth to Water. 2 5 6 Measuring Point: fdC Depth of Pump Intake: 3 rj Pump Used (circle): Peristaltic Bladder Comments: P�&fp Ori 132 JI0t�-� � — C,f�l�� �prvli�t�A. Date: Q Weather: Facility ID or Permit # (if applicable): Sample ID (on COC): in Arrive at Well: ft bgs StartTime: ft bgs Sample Time: ft Leave Well: Well Type: ft Tagged Bottom: Other (describe): I Well ID: (,f/-0 If 0 0/20 23 50 "S , 6w-L G 50- 02 LO2,-& OA VC> - rA\N —O T l312 1'St..l S L t .10 Cl Zck Up ❑Flush Mount ft at (time): Purge Rate: Total Volume Purged: Pump Speed: :15 F '.2S Time DTW (feet) Temperature (°C) Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) pH (S.U.) report to 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) %--645 2 . C1 1 a0 _+ 5•f0q Sa -6 . t.29 l 2 -tS 4 5•1-1 SoR- to o. =- 2 IS W • 9 10• 3 l0 S• 510 . Z •41 t :�-• Z - 08 5• 514• f 0.3 14,00 I(DAS IS- 5•fi 512-2 ly : o 2t0. 10 I S. 'L 5 -96 s 1L p --65 SIZ•9 - 2b -1 S 4.114 5 • + S1 • 0.-6 2-10.15 IS•1 S12.9 .2 Sample Analyst Signature: Sample Analyst Name: �e5b►4 Date: p1 Notes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity,' +/- 3% Conductivity,' +/- 0.1 pH unit' +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017: 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff member's initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field Laboratory Certificate Number 5445 5. 1 pimho/cm = 1 pS/cm Abbreviations: Method Reference: °C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter in: inches DO: SM 4500 O G-2016 mv: millivolt bgs: below ground surface pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 Page 1 of 1 ANCHOR kZQEA u Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Well Sampling Log 1 MOM: _ W,05(L Project Name: C 1GlCkSL"I Co. e_',Y1iGv1JX�-Lal cY�wl�%1t ✓(y} Date:l01 1129 12, Project Number. cza y60 — r>1 , C>J O Weather-,..,-, c k ov_A , - O 's Project Location: 1:);115 boro I Kr— Facility ID or Permit # (if applicable): — O Sample Collector(s): G�P sample ID (on COC): Zd 03 0 / 0 %— MW"OS Well Diameter: 2 in Sample Time: / I S' Screen Interval: N t Pit ft bgs 54 Measuring Point: T- Well Depth (WD): — ft TOC Well Type: tick Up ❑Flush Mount Water Level in Feet (WL): o. ft TOC Comments: L' 11 o cv. S 0 Length of Water Column (LWQ: 3 c 2 7 ft; (WD - WL) r One Casing Volume: . 51i4 gallons; (LWC x WCV) Three Casing Volumes: ' S gallons Actual Volume Purged: gallons Tagged Bottom: X ft at (time): X� Three Casing Volumes: gallons Well Casing Volumes (WCV) 1" = 0.04 Gal/Ft C27= 0.16 Gal/F 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1A7 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft Purge Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other. Sample Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Oxidation Dissolved Specific pH (S.U.) Reduction Gallons Temperature Oxygen Conductivity reportto 0.1 Potential Turbidity Reading Time Purged CQ (mg/L) (pmhos/cm) S.U. (mv) (NTU) Comments 2 3 4 5 6 7 8 9 10 Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass 1 LGlass Other Protective Casing: Pad: Lock �L Vegetation: Access: ✓ Sample Analysts amp e Signature: Analysts Date: L O� �9 �%3 Name: Notes: I 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity, +/- 3% Conductivity; +/- 0.1 pH unit; +/- 70 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. ��� �� j/1' 4. NC Field laboratory Certificate Number 5445 / ed Abbreviations: Method Reference: °C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter in: inches DO: SM 4500 O G-2011 mV: millivolt bgs: below ground surface PH: SM 4500-H' B-2011 NTU: nephelometnc turbidity units TOC: top of casing Turbidity. SM 2130 B-2011 Page 1 of 1 ANCHOR Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Low -Flow Sampling Log well ID: W— ff '. Project Name: S&r k� Co. CPNit+Q Y1VIA1 FA 1 Project Number: C2��-t$O ^ 01 • (a l Project Location: ;NWID00) , N� Sample Collector(s): �� (,i'1� Well Diameter. ;_ Screen Interval: u y ^ �� Well Depth (as constructed): C� _ Depth to Water: �, �'�ry Measuring Point: J oc Depth of Pump Intake: Pump Used (circle): Peristaltic Bladder Comments: t 1` yht7 on CO) l !!"�: p'2, [T'1`lill%C �'i 00 ScatM�i vt n1 _ Date: 0 Q 2 J Weather. 0 rS Facility ID or Permit # (if applicable): ^ OZ Sample ID (on COC):2O23C1 f0J W— in Arrive at Well: ft bgs StartTime:�Ct ft bgs Sample Time: ft Leave Well: Lng� Well Type: UStick Up ❑Flush Mount ft Tagged Bottom: ft at (time): Other (describe): Purge Rate: Total Volume Purged: Pump Speed: — Time DTw (feet) Temperature ('C) Dissolved Oxygen (mg/L) Specific Conductivity (Nmhos/cm) pH (S.U.) report to 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) �0,1 IL• S,05 -U -b4 2Lt0,0 • l y .-5 5 -�7- 2JOc� z. z z- -�-1 r I c'�r. /quo L- CU 1; 2 2. . S S. 5�-E2 2g5--- 2. `L -4_0 S _0 iu 5 - sZ O S Sample Analyst Signature: ULName: Sample Analyst '�Se&S Vc, Date: c 1 W 9 IZZ Notes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity,, +/- 3% Conductivity,, +/- 0.1 pH unit; +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017; 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff member's initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field Laboratory Certificate Number 5445 5. 1 pmho/cm = 1 pS/cm - Abbreviations: Method Reference: °C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter in: inches DO: SM 4500 O G-2016 mV: millivolt bgs: below ground surface pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 9 Page 1 of 1 Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Low -Flow Sampling Log Well ID: yvk W —O.} Project Name' j,CtSph �0 • iGt111/ =iI Project Number. C2%4150—o, 01 i Project Location: I ` -S f) � TNC, Sample Collector(s): 'M, Criy Well Diameter. Screen Interval: — Well Depth (as constructed): 15 Depth to Water: 31 L4b Measuring Point: T)L Depth of Pump Intake: _ Pump Used (circle): Peristaltic Bladder Comments:�n l� �.4'c b �3 E1 11� Date: Weather. Facility ID or Permit # (if applicable): Sample ID (on CDC): in Arrive at Well: ft bgs Start Time: ft bgs Sample Time: ft Leave Well: Well Type: ft Tagged Bottom: Other (describe): _ Dc '2.717 W S y3L�-lti.s+td.. S8 — OZ 2.C>" ,Ai — tLl i y 52 flStick Up oFlush Mount x ft at (time): Purge Rate: Total Volume Purged: Pump Speed: Time DTW (feet) Temperature (°C) Dissolved Oxygen (mg/L) Specific Conductivity (Nmhos/cm) pH (S.U.) report to 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) 0 17DI . t �`-� • ``�TiL la - 22 i O ILA s 3Z-t13 ty. - ss Z - llb . o S : 01 ;Z. b- ICIO S. `30 i i l 25 S a iS°o )2,12 1L .10 2 o �.►L 52-. 2-0 14 9 1 C to t -0 LA, Sample Analyst Signature: Sample Analyst Name: _55,55 (f tL Date: 0 —ILa Notes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity, +/- 3% Conductivity,- +/- 0.1 pH unit +/- 10 MV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017: 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff member's initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field Laboratory Certificate Number 5445 5.1 pmho/cm = 1 pS/cm Abbreviations: Method Reference: °C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft feet Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter in: inches DO: SM 4500 O G-2016 mV: millivolt bgs: below ground surface pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 Page 1 of 1 ANCHOR QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Surface Water Sampling Log Location 1D: Project Name: 3 KScrn COV-ntj I.-o YWU:: I I Date: oM-Ito I 2-3 Project Number: G21WB0^ Ol. CA Weather: so., 6wnKvr w[ [leeiclS Project Location: pi ��SlooYb N-C, Facility ID or Permit # (if applicable): 15 Q — C52 Sample Collector(s): C var Sample ID (on COQ: Comments: u1"yk1 a l��td%ll Sample Method (circle Grab Syringe Pump Bailer-Disp. Other: one): Specific Oxidation Temperature Dissolved Conductivity pH (S.U.) Reduction Turbidity Time CC) Oxygen (mg/L) (pmhos/cm) reportto 0.1 S.U. Potential (mV) (NTU) Comments .--7. 0 12 a4 1 Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass 1 L Glass 2 p • Cct Other Vegetation: ram. Access: 5cty 4bw. *Z V,-� Sample Analyst Sample Analyst Signature: Name: —kSeSSi C.C. Date: 'M�.c c� to [ 3 Notes: 1. Documentation errors are to be crossed out with a single line, so the oriainal text is still leoible, followed by the staff members initials and date 2. Samples are analyzed immediately upon collection. 3. NC Field Laboratory Certificate Number 5445 Abbreviations: Method Reference: °C: degrees Celsius Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter DO: SM 4500 O G-2011 mv: millivolt pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units Turbiditv: SM 2130 B-2011 S.U: standard units Page 1 of 1 ANCHOR QEA �" Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Surface Water Sampling Log Location ID: 5vV-a-L Project Name:, Project Number: Project Location: Sample Collector(s):^Syyl Comments: akr—kSOr1 C Lwnaau C21 H �s0 — O 1. O l 4 r ftborra, df C , C y4? ni Date: OI O 2 Weather: 50.5 Facility ID or Permit # (if applicable): 0- 02 Sample ID (on COC): 202 ,01 Sample Method (circle one): Gr Syringe Pump Bailer-Disp. Other: Time Temperature VC) Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) pH (S.U.) report to 0.1 S.U. Oxidation Reduction Potential (m1) Turbidity (NTU) Comments lb:35 ,o i�-.3'f 2'i,'3 2L42--5 4.30 Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass 1LGlass 2 'aoe( Other Vegetation: 150 yv..R. Access: 5}lep Sto M ino %9.e & c In Sample Analyst Sample Analyst Signature: Name: 'SebSi Cs, VYiw l e rs Date: pi Ip j Z Notes: 1. Documentation errors are to be crossed out with a single line, so the oriainal text is still leaible. followed by the staff members initials and date 2. Samples are analyzed immediately upon collection. 3. NC Field Laboratory Certificate Number 5445 Abbreviations: Method Reference: °C: degrees Celsius Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter DO: SM 4500 O G-2011 mv: millivolt pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units Turbiditv: SM 2130 B-2011 S.U: standard units Page 1 of 1 ,� ANCHOR QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Surface Water Sampling Log Location ID:V�J'- l� Project Name: k%y% Cownj:. A jN Date: 0 Z Project Number: LL4BO O1. Oj Weather: rop•a Project Location: ���Sbo,ro r `[�f G Facility ID or Permit # (if applicable): So- D Sample Collector(s): Sample ID (on COC): 2 07- It CA i Comments: Sample Method (circle Grab Syringe Pump Bailer-Disp. Other: one) Specific Oxidation Temperature Dissolved Conductivity pH (S.U.) Reduction Turbidity Time VQ Oxygen (mg/L) (Nmhos/cm) report to 0.1 S.U. Potential (mV) (NTU) Comments AM I 1 iDrr3 12.53 ELI -LI Ct � Z,►� Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass 1 L Glass $p h t Other Vegetation: IFT" fol-L Access: 0 Lc!y J Sample Analyst Sample Analyst Signature: Name: -&S Date: ip (Z3 Notes: 1. Documentation errors are to be crossed out with a single line, so the original text is still leoible, followed by the staff members initials and date 2. Samples are analyzed immediately upon collection. 3. NC Field Laboratory Certificate Number 5445 Abbreviations: Method Reference: °C: degrees Celsius Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter DO: SM 4500 O G-2011 mv: millivolt pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units Turbidity: SM 2130 B-2011 S.U.: standard units Page 1 of 1 ANCHOR .. QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Well Sampling Log Well ID: MW-01 Project Name: Jackson County Landfill Date: IN Z?. Project Number: C_�. —� Weather: Project Location: Dillsboro, NC Facility ID or Permit # (if applicable): 50-02 Sample Collector(s):Sample ID (on COC: MW-01- Z 2 L l Do Well Diameter: 2 in Sample Time: 7435 Screen Interval: N/A ft bgs Measuring Point: TOC Well Depth (WD): 110.5 ft TOC Well Type: KStick Up ❑Flush Mount Water Level in Feet (WL): q 10 ft TOC Comments: v ) to V q C �0 �1 Length of Water Column (LWQ: >{ Q ft; (WD - WL) /} C. One Casing Volume: gallons; (LWC x WCV) ' r Three Casing Volumes: S T gallons Actual Volume Purged: C � ID �— gallons L Tagged Bottom:, ft at (time): Three Casing Volumes: gallons✓l Well Casing Volumes (WCV) 1" = 0.04 Gal/Ft 2" = 4.1f; Gal/F 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft Purge Method: I Bailer-Dis Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Sample Method: Bailer-Dis Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Oxidation Dissolved Specific pH (S.U.) Reduction Gallons Temperature Oxygen Conductivity report to 0.1 Potential Turbidity Reading Time Purged (°C) (mg/L) (pmhos/cm) S.U. (mv) (NTU) Comments 1 21 2 b a 4 5 `Z .2, r 6 I {{ S 2 12: 0 Q r >d L i , c 7 8 9 10 Sampling Container Number of Containers Requested Analysis 500 mL Plastic (; + l 250 mL Plastic 125 mL Plastic 40 mL Glass 1 L Glass V Other Protective Casing: Pad:_"" Lock: V Vegetation: Access: Sample Analysts Sample Analysts " D /� Signature: /1! 'tc}e 1 • Z Date: �f� �� Z i.J�1��.+Lr Name: RA"k Notes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity,, +/- 3% Conductivity,' +/- 0.1 pH unit; +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. i ` I S y 4. NC Field Laboratory Certificate Number 5445 Abbreviations: Method Reference: �t� °C: degrees Celsius S.0 : standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter in: inches DO: SM 4500 0 G-2011 mV: millivolt bgs: below ground surface pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 �00 tt� 6.ko � a V - _ ' Page 1 of 1 J SD-0i iJO iM II�' ' V\z ZANCHOR v QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Well Sampling Log Well ID: MW-02 Project Name: Jackson County Landfill Date: Project Number: 013SU OM 2 Weather: L P Project Location: Dillsboro, NC Facility ID or Permit # (if applicable): 50-02 Sample Collector(s): F s �• Sample ID (on COC): MW-02- 1011003 Well Diameter: 2 in Sample Time: 10 00 Screen Interval: N/A ft bgs Measuring Point: TOC Well Depth (WD): 60.7 ft TOC Well Type: KStick Up ❑Flush Mount Water Level in Feet (WL): 3 1% ft TOC Comments: L 0U2.CA-C& , c ygkf Length of Water Column (LWQ: I ►� � - ft; (WD - WL) One Casing Volume: C gallons Three Casing Volumes: I gallons Actual Volume Purged: a .I gallons ` t Tagged Bottom: (e, J P `y ft at (time): « l Three Casing Volumes: gallons ,. Well Casing Volumes (WCV) 1" = 0.04 Gal/Ft 2" = 0.16 Gal/F1 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft Purge Method: Bailer-Disp. Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Other: Sample Method: Oxidation Dissolved Specific pH (S.U.) Reduction Gallons Temperature Oxygen Conductivity report to 0.1 Potential Turbidity Reading Time Purged CQ (mg/L) (pmhos/cm) S.U. (mv) (NTU) Comments 1 S0 0 tL4.L} '2­ :1 5.q i`814, 1 2_4 2 3 4 5 6 7 8 9 10 Sampling Container Number of Containers Requested Analysis 500 mL Plastic S '• 250 mL Plastic 125 mL Plastic vocs1 - 4 IQ X All e 40 mL Glass 1 L Glass Other Protective Casing: Pad: Lock: Vegetation: Access: Sample Analysts Sample Signature: � t Analysts Name: Sst Date:— Notes: V 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity; +/- 3% Conductivity,' +/- 0.7 pH unit; +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field Laboratory Certificate Number 5445 C'J Abbreviations: 'C: degrees Celsius pmhos/cm: micromhos per centimeter mg/L: milligrams per liter mV: millivolt NTU: nephelometric turbidity units L-jL 10'i Method Reference: S.U.: standard units Temperature: SM 2550 B-2010 ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982 in: inches DO: SM 4500 O G-2011 bgs: below ground surfs pH: SM 4500-H' B-2011 fTOC: top of casing (\ C /y� ` �` I ` Turbidity: SM 2130 B-2011 =,6A Page 1 of 1 ANCHOR •a QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 -1-Flow Sampling Log Well ID: MW-03 Project Name: Jackson County Landfill Date: Project Number. GH4dC'BtQr J l , Wea er: WWI - Project Location: Dillsboro, INC Facility ID or Permit # (if applicable): 50-02 Sample Collector(s):T _ _ Sample ID (on COC): MW-03- 22 00 Well Diameter: 2 in Arrive at Well: Screen Interval: 48.5-63.5 ft bgs Start Time: 1-1061 Well Depth (as constructed): 65.5 ft bgs Sample Time: Depth to Water.50.5 T ft Leave Well: ' Measuring Point: TOC N.1 , Well Type: XStick Up oFlush Mount Depth of Pump Intake: `T ft Tagged Bottom: UA- . rj 1 ft at (time): 1 b0 iw j 1 fW� �1 Pump Used (circle): Peristaltic Bladder Other (describe): Purge Rate: Comments: 7CrOS@ S L n V1 1--•A� l o u, Total Volume Purged: Pump Speed: Time DTW Yeet)a Ttipperature CQ Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) pH (S.U.) report to 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) W.6 a3.'5 -5,01 -3 $ 1 0. l , 5. 18 1 5 b r S 2 Sample Analyst Signature: I Sample Analyst Name: le&t Date:_w 1 Notes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity* +/- 3% Conductivity,'- +/- 0.7 pH unit +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original tent is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. / 4. NC Field Laboratory Certificate Number 5445 A { n i -to � TWO O D Qi � � r / 5. 1 pmho/cm = 1 pS/cm Q �/ W C. 1C Abbreviations: Method Reference: 'C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet 4 ` Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter in: inches DO: SM 4500 0 G-2011 mv: millivolt bgs: below ground surface pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 � nyAA0 deco nvleGl wGi&p csvv" f ul'd n-f I'iDm dS W W I en d w l t k1ui V10 Q sam P 1,t Page 1 of 1 ANCHOP, ..�, QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 v-Flow Sampling Log lWell ID: MW-04 Project Name: Project Number: Project Location: Sample Collector(s): Well Diameter: Screen Interval: Well Depth (as constructed): Depth to Water: Measuring Point: Depth of Pump Intake: Pump Used (circle): Comments: Pt,tMp OnG IZ't Jackson County Landfill G - 1.02 G % Dillsboro, NC ` In 'M 2 25 - 40 43 - , TOC 35 Peristaltic S }@POS£8{}' Date: 0 . j'LZ. .. Weather: S �° r 0.V S K-t o— Facility ID or Permit # (if applicable): 50-02 Sample ID (on COC): MW-04- 7 62I JO (34 in Arrive at Well: ft bgs Start Time: 1215 ft bgs Sample Time: G ft Leave Well: Well Type: NStick Up ❑Flush Mount ft Tagged Bottom: ft at (time): Bladder Other (describe): Purge Rate: DJ0 -L j� r v,� Sp e O W� 5r Total Volume Purged: T�(.y 'p)Z' __OTwncn o'n[a� 17't3UiUtr�li`C)SPump Speed: ,Is; F"_2 Time DTW (feet) Temperature ('C) Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) pH (S.U.) report to 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) 2 6 5 ' 5 0 �1-1 ®L t Is 2- 2A 213. 17, 1-5-5 q (1, 1Z 1>014 2-,5 2-3: itS. y� Z Z z i i's 9.12 -32 3 9 Z_ 3 Sample Analyst Signature: Sample Analyst Name: J Date: e✓' Cy j Z2 V ' Notes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity, +/- 3% Conductivity, +/- 0.1 pH unit; +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field Laboratory Certificate Number 5445 5. 1 pmho/cm = 1 PS/cm Abbreviations: Method Reference: °C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter in: inches DO: SM 4500 O G-2011 mV: millivolt bgs: below ground surface PH: SM 4500-H' B-2011 NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 ets l fpie .- bi Page 1 of 1 %l6 ANCHOR QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Well Sampling Log Well ID: MW-05R Project Name: Jackson County Landfill Date: j ❑ 1 f)R f2 -1 Project Number: VV0,MWeather. 1� l OF, Project Location: Dillsboro, NC Facility ID or Permit # (if applicable): 50-02 Sample Collector(s):� Sample ID (on COC): MW-05R- Well Diameter: 2 in Sample Time: IG 3D ��a �" Screen Interval: N/A ft bgs Measuring Point: TOC Well Depth (WD): 54 ft TOC Well Type: KStick Up ❑Flush Mount Water Level in Feet (WL): 'I - I --- ft TOC Comments: Length of Water Column (LWQ: ft; (WD - WL) One Casing Volume: Q G gallons; (LWC x WCV) Three Casing Volumes: a gallons oq (T_g Actual Volume Purged: "� gallons Tagged Bottom: SID; (� ft at (time): (�1 Three Casing Volumes: gallons Well Casing Volumes (WCV) 1" = 0.04 Gal/F 2' = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft Purge Method: I Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Sample Method: IL Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Oxidation Dissolved Specific pH (S.U.) Reduction Gallons Temperature Oxygen Conductivity report to 0.1 Potential Turbidity Reading Time Purged (°C) (mg/L) (pmhos/cm) S.U. (mv) (NTU) C_ -e s 2 0 3 4 5 6 7 8 9 10 Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass 1 L Glass Other Protective Casing: "_ Pad: .ILock: Vegetation: :� Access: p I�G1 Sample Analysts Sample Signatur nalyse: Date: Notes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity,' +/- 3% Conductivity, +/- 0.7 pH unit +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. p �/y` %�rJt/ll 4. NC Field Laboratory Certificate Number 5445 4 /' n f I Pried Cx �l a Abbreviations: 'C: degrees Celsius pmhos/cm: micromhos per centimeter mg/L: milligrams per liter mv: millivolt NTU: nephelometric turbidity units %� /� , ���-✓ Method Reference: �C Oct (� `� %f%bLa S.U.: standard units " ' Q, Temperature: SM 2550 B-2010 `- r � — tv ft: feet i 9 I/t p �y v in: inches lh� °)) Specific conductivity: EPA Method 120.1, Rev. 1982 DO: SM 4500 0 G-2011 G�,, ll�. c.7cu' �� bgs: below ground surface,# D pH: SM 4500-H' B-2011 t _ �`- TOO top of casing (1- 1 "!� 0 G U ed Turbidity: SM 2130 B-2011 m as � Page 1 of 1 ANCHOR, QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 v-Flow Sampling Log WeII ID: MW-06 Project Name: Project Number: Project Location: Sample Collector(s): Well Diameter: Screen Interval: Well Depth (as constructed): Depth to Water: Measuring Point: Depth of Pump Intake: Pump Used (circle): Comments: Jackson County Landfill L— Dillsboro, NC 2 84-94 94 5� c� TOC d' 91 Peristaltic rgtact lmoccoseap;--0v,\Q Atop ui;�- Bladder T � dw Ct� Date: t, 0 ®-f { 1 2— r Weather: (p Facility ID or Permit # (if applicable): 50-02 Sample ID (on COQ: MW-06- in Arrive at Well: fro ft bgs Start Time: ft bgs Sample Time: ft Leave Well: Well Type: XStick Up ❑Flush Mount ft Tagged Bottom: -4 , t at (time): Other (describe): Purge Rate: 1-+td Total Volume Purged: � L� � � _ Pump Speed: I �L4 bc� So ml_ ,0, C\ Time DTW (feet) Temperature (*Q Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) pH (S.U.) report to 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) -6F Iso (1-5 Z 3 (o '3 (0 B Z,' r6- S - Y3 Da ..y ,© 4.. Ca •6-ib C9 e o - 2 < 2�,9 tip: tlq 90. 2. D n 3 '10 Z�ZD Sample Analyst Signature: Sample Analyst Name: Date: l(j Notes: J 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity,- +/- 3% Conductivity,, +/- 0.7 PH unit; +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field Laboratory Certificate Number 5445 S. 1 pmho/cm = 1 pS/cm Abbreviations: 'C: degrees Celsius pmhos/cm: micromhos per centimeter mg/L: milligrams per liter mv: millivolt NTU: nephelometric turbidity units S.U.: standard units ft: feet in: inches bgs: below ground surface TOC: top of casing NacV�5,2 �)SU ���M- W4 C�Cf�� 6n Lid Method Reference: Temperature: SM 2550 B-2010 Specific conductivity: EPA Method 120.1, Rev. 1982 DO: SM 4500 O G-2011 PH: SM 4500-H' B-2011 Turbidity: SM 2130 B-2011 Page 1 of 1 ZANCHOR v QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 v-Flow Sampling Log Well ID: MW-07 Project Name: Jackson County Landfill Date: i r, I?,J, Project Number: "^AO^ 9 klA Weather. 0 Project Location: Dillsboro, INC Facility ID or Permit # (if applicable): 50-02 Sample Collector(s): Sample ID (on COC): MW-07-.20"aa. 100 3 Well Diameter: 2 in Arrive at Well: Screen Interval: 70 - 95 ft bgs Start Time: 1L Well Depth (as constructed): 95 ft bgs Sample Time: Depth to Water: ft Leave Well: I too Measuring Point: TOC Well Type: tick Up ❑Flush Mount Depth of Pump Intake: ft Tagged Bottom: ft at (time): Pump Used (circle): Peristaltic Bladder I Other (describe): Purge Rate: �ti®.rsl vy�i Comments: S'f�OS'E'E ---knaliy rd y (Z - �� Total Volume Purged: Sip-FlilffASE212" ' —�p�� (� Pump Speed: �T Time DTW (feet) Temperature (°C) Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) pH (S.U.) repot to 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) m U iP Co y CQyf� a,+ I 7-15 o j;,. 2.qo 1S< —+E Sq- 19 0 tZv m9 Q IS, Sample Analyst Signature: Sample Analyst Name: Date: ��?� 2Z Notes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity +/- 3% Conductivity, +/- 0.1 pH unit, +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3. Samples are analyzed immediately upon collection. 4. NC Field Laboratory Certificate Number 5445 5. 1 pmho/cm = 1 pS/cm Abbreviations: Method Reference: 'C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter in: inches DO: SM 4500 O G-2011 mv: millivolt bgs: below ground surface pH: SM 4500-H' 8-2011 NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 40ud 6011 CJVLVC� d1'c'sci(ved VW"0J9 'SAVt Page 1 of 1 ANCHOR Z-7 QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Surface Water Sampling Log Location ID: SW-01 Project Name: Project Number: Project Location: Sample Collector(s): Comments: Jackson County Landfill C489-99�2 ICU, Dillsboro, NC �L$4 M Upstream of landfill Date: D Weather: Facility ID or Permit # (if applicable): Sample ID (on COC): i'u Q OF 50-02 SW-01- 2(32-2 100 "' Sample Method (circle one): Grab Syringe Pump Bailer-Disp. Other: Time Temperature VC) Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) pH (S.U.) report to 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) Comments Sampling Container Number of Containers Requested Analysis 500 mL Plastic t ` 250 mL Plastic 125 mL Plastic i p + Q ([ a S' �� 40 mL Glass 1 L Glass Y IV Other Vegetation: %Vme Access: Sample Analyst Sample Analyst Signature: `- L�IJ�r �/y bu Name: Va-� (�,� j/(f� Date: (� Notes: S�4 1. Documentation errors are to be crossed out with a sinole line, so the orioinal text is still leoible, followed by the staff members initials and date 2. Samples are analyzed immediately upon collection. 3. NC Field Laboratory Certificate Number 5445 Abbreviations: 'C: degrees Celsius pmhos/cm: micromhos per centimeter mg/L: milligrams per liter mv: millivolt NTU: nephelometric turbidity units S.U.: standard units Method Reference: Temperature: SM 2550 B-2010 Specific conductivity: EPA Method 120.1, Rev. 1982 DO: SM 4500 O G-2011 pH: SM 4500-H' B-2011 Turbiditv: SM 2130 B-2011 '100[eW serve ��5 Page 1 of 1 I-AANCHOR .—v QEA u Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville. North Carolina 28801 Surface Water Sampling Log Location ID: SW-02 Project Name: Jackson County Landfill Date: 10 Project Number: C44409,0j.02 G� .D Weather: • Project Location: Dillsboro, NC Facility ID or Permit # (if applicable): 50-02 Sample Collector(s): KE - -1 i l Sample ID (on COC): SW-02- ZOZZ 10 03 Comments: Downstream of landfill Sample Method (circle Grab Syringe Pump Bailer-Disp. Other: one,. Specific Oxidation Temperature Dissolved Conductivity pH (S.U.) Reduction Turbidity Time VQ Oxygen (mg/L) (pmhos/cm) report to 0.1 S.U. Potential (mV) (NTU) Comments ��-9 q-�s 24-q -4. f 0. o 1.8?, Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass by uvcS. L4 ( p 1 L Glass Other Vegetation: Access: �{� 1 tJ _ Sample Analyst Sample Analyst Signature: a Name: Date: t� Notes: 1. Documentation errors are to be crossed out with a sinale line, so the oriainal text is still legible, followed by the staff members initials and date 2. Samples are analyzed immediately upon collection. 3. NC Field Laboratory Certificate Number 5445 Abbreviations: Method Reference: 'C: degrees Celsius Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter DO: SM 4500 O G-2011 mv: millivolt pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units Turbiditv: SM 2130 B-2011 S.U.: standard units � Page 1 of 1 ANCHOR !_... -.,.art... .\ Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Well Sampling Log ('J-.)�' v, t •pan t1 - 0;) • C.W -r .J Well ID: ,- Project Name: � � V '+(SO(AAADate: Project Number: Weather: vlp Project Location:-h ` 111616 OvEh �J Facility ID or Permit # (if applicable): —in Q Collector(s): Sample ID (on COC): Well Diameter: in Sample Time: 40 Screen Interval: ft bgs Measuring Po Well Depth (WD): OC Cc ell Type: ❑Stick Up .Flush Mount Water Level in Feet (WL): ft TO Comments: oyn I.renjOA Length of Water Column (LWQ: ft; (WD - WL) `7 +� One Casing Volume: gallons; (LWC x WCV) 0 r Three Casing Volumes: gallons RAA Actual Volume Pu gallons Tagged Bottom: ft at (time): Three Casing umes: gallons Well Casing Volu " CV) 1" = 0.04 Gal/Ft 2" = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft Purge Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Sample Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other: Oxidation Dissolved Specific pH (S.U.) Reduction Gallons Temperature Oxygen Conductivity reportto 0.1 Potential Turbidity Reading Time Purged VQ (mg/L) (pmhos/cm) S.U. (mV) (NTU) Comments 1 00 t 2 f� f 2 3 4 5 6 7 8 9 10 Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass 1 L Glass Other Protective Casing: Pad: Lock: Vegetation: Access: Sample Analyst ature: Sample Analysts C„ 2SignV� Date: (2 Name (Votes: 1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity, +/- 3% Conductivity,, +/- 0.7 pH unit +/- 10 mV for ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017) 2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 3 SamP les are anal zed immediately upon collection • Y 4. NC Field Laboratory Certificate Number 5445 Q 0-f '. 0 V1, y' FM ti 5 , g, Abbreviations: Method Reference: r' �( l -r—„ f (r1 'C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982 1/ Q F--• 1i mg/L: milligrams per liter mv: millivolt in: inches bgs: below ground surface DO: SM 4500 O G-2011 pH: SM 4500-H' B-2011 , •p NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011 Page 1 of 1 ANCHOR , v QEA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 •npling Log - Grab Location ID: DW-01 Project Name: Project Number: Project Location: Sample Collector(s):� Comments: Jackson County Landfill Date: 100S 1 2.1 ,�.1�480'>T1'dt L' Weather: 68. Dillsboro, INC Facility ID or Permit # (if applicable): 50-02 Sample ID (on COC): DW-01- 02 (00 Purged 30 gallons prior to sampling. Wilkey residence. Sample Method (circle one): Grab Syringe Pump Bailer-Disp. Other: Time Temperature CC) Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) pH (S.U.), reportto 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) Comments Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glas T• c2 VO .$ MLOe Glass -,ter Vegetation: Sample Analyst Access: Analyst �� Name: �~ "+ Date: ' Notes: 1. Documentation errors are to be crossed out with a single line, so the original tent is still legible, followed by the staff members initials and date 2. Samples are analyzed immediately upon collection. 3. NC Field Laboratory Certificate Number 5445 Abbreviations: °C: degrees Celsius pmhos/cm: micromhos per centimeter mg/L: milligrams per liter mv: millivolt NTU: nephelometric turbidity units S.U.: standard units Method Reference: Temperature: SM 2550 B-2010 Specific conductivity: EPA Method 120.1, Rev. 1982 DO: SM 4500 O G-2011 PH: SM 4500-H` B-2011 Turbidity: SM 2130 B-2011 %vc-t&S 0Up f-rD4 Page 1 of 1 ANCHOR ,.�► Q EA Anchor QEA of North Carolina, PLLC 231 Haywood Street Asheville, North Carolina 28801 Surface Water Sampling Log Location ID: Project Name: la(S�III Date: ^ a a, Project Number: CA 0 - 01 Weather: • � Project Location: tt `' /��I DI I I �VJD t�0. OC Facility ID or Permit # (if applicable): 5 0 - ba Sample Collector(s): �0 Sample ID (on COC): n i' -ID 04 a 0 3 Comments: v r SJE ' 4 Sample Method (circle Grab Syringe Pump Bailer-Disp. Other: one): Specific Oxidation Temperature Dissolved Conductivity pH (S.U.) Reduction Turbidity Time VQ Oxygen (mg/L) (Nmhos/cm) report to 0.1 S.U. Potential (mV) (NTU) Comments 14TS -"�61) (11 Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass a 1 L Glass Other Vegetation: Access: Sa le Analyst Sample Analyst Signature G rV v� Name: \ct+ P ate: Notes: 1. Documentation errors are to be crossed out with a single line. so the oriainal text is still legible, followed by the staff members initials and date 2. Samples are analyzed immediately upon collection. 3. NC Field Laboratory Certificate Number 5445 Abbreviations: Method Reference: °C: degrees Celsius Temperature: SM 2550 B-2010 Nmhos/cm: micromhos per centimeter Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter DO: SM 4500 O G-2011 mv: millivolt pH: SM 4500-H'B-2011 NTU: nephelometric turbidity units Turbidity: SM 2130 B-2011 S.U.: standard units '* doh =F dAAAu� uDa-� i h TOL� S -a Page 1 of 1 ANCHOR OEA Anchor QEA of North Carolina, PLLC 231 Haywood Street npling Log - Grab Location ID: LT-01 Asheville, North Carolina 28801 Project Name: Project Number: Project Location: Sample Collector(s): Comments: Jackson County Landfill C C21 Dillsboro, NC IAf Y* Date: — Weather. Facility ID or Permit # (if applicable): Sample ID (on COC): V 3 do Q-A GFr S u IA h U 50-02 LT-01- Sample Method (circle one): Grab Syringe Pump Bailer-Disp. Other: Time Temperature VC) Dissolved Oxygen (mg/L) Specific Conductivity (pmhos/cm) pH (S.U.) reportto 0.1 S.U. Oxidation Reduction Potential (mV) Turbidity (NTU) Comments II�D as .a n,D'� ��0 'I J �3tA 00l . Sampling Container Number of Containers Requested Analysis 500 mL Plastic 250 mL Plastic 125 mL Plastic 40 mL Glass Glass er Vegetation: 0 1 �f Access: L eO C, I a �l 1" t Sample Analyst Sample Analyst Signature: K am- C_ Name: 14(A+) e ( Date: (Q 103122, 2, Notes: 1. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date 2. Samples are analyzed immediately upon collection. 3. NC Field Laboratory Certificate Number 5445 Abbreviations: Method Reference: 'C: degrees Celsius Temperature: SM 2550 B-2010 pmhos/cm: micromhos per centimeter Specific conductivity: EPA Method 120.1, Rev. 1982 mg/L: milligrams per liter DO: SM 4500 O G-2011 mv: millivolt pH: SM 4500-H' B-2011 NTU: nephelometric turbidity units Turbidity: SM 2130 B-2011 S.U.: standard units � prt,l °{ Y � Cott eoj-ed d��ss-owed Melwf � I�.ac1A� Page 1 of 1 Appendix B Reports of Laboratory Analysis, Chain -of -Custody Documentation, and Certificates of Analysis Waypointo ANALYTICAL 1 /23/2023 Anchor QEA of North Carolina, PLLC Jessica Mayers 231 Haywood Street Asheville, NC, 28801 Ref: Analytical Testing Lab Report Number: 23-012-0004 Client Project Description: Jackson County Site: 58-02 Project Number: 58-02 Dear Jessica Mayers: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/12/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, a,j Angela D Overcash Senior Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 30 Waypoint.0 ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12/31/2023 South Carolina State Program 99012 07/31/2023 South Carolina State Program 99012 12/31/2022 Page 1 of 1 00016/23-012-0004 Page 2 of 30 Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointana lyti ca I som Sample Summary Table Report Number: 23-012-0004 Client Project Description: Jackson County Lab No Client Sample ID Matrix Date Collected Date Received 97369 20230109-MW-01 Aqueous 01/09/2023 12:30 01/12/2023 09:30 97370 20230110-MW-02 Aqueous 01/10/2023 16:52 01/12/2023 09:30 97371 20230109-MW-03 Aqueous 01/09/2023 16:34 01/12/2023 09:30 97372 20230110-MW-04 Aqueous 01/10/2023 14:09 01/12/2023 09:30 97373 20230109-MW-05R Aqueous 01/09/2023 15:15 01/12/2023 09:30 97374 20230109-MW-06 Aqueous 01/09/2023 14:30 01/12/2023 09:30 97375 20230110-MW-07 Aqueous 01/10/2023 15:10 01/12/2023 09:30 97376 20230110-SW-01 Aqueous 01/10/2023 15:45 01/12/2023 09:30 97377 20230110-SW-02 Aqueous 01/10/2023 16:35 01/12/2023 09:30 97378 20230110-SW-03 Aqueous 01/10/2023 16:00 01/12/2023 09:30 Page 3 of 30 Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointana lyti ca I som Summary of Detected Analytes Project: Jackson County Report Number: 23-012-0004 Client Sample ID Lab Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 20230109-MW-01 V 97369 8081 B alpha-BHC 8081 B gamma-BHC 20230110-MW-04 V 97372 8081 B beta-BHC 8081 B Endosulfan I 8081 B Endosulfan Sulfate 8081 B Endrin Aldehyde 20230109-MW-05R V 97373 8081 B alpha-BHC 8081 B beta-BHC 8081 B gamma-BHC 20230109-MW-06 V 97374 8081 B beta-BHC 20230110-MW-07 V 97375 8081 B alpha-BHC 8081 B beta-BHC 8081 B delta-BHC 8081 B gamma-BHC 0.0404 pq/L 0.0063 01/18/202313:33 J 0.0303 Ng/L 0.0061 01/18/202313:33 J 0.0203 pg/L 0.0111 01/18/202314:27 JQ 0.142 Ng/L 0.0160 01/18/202314:27 Q 0.0507 pq/L 0.0165 01/18/202314:27 0.0812 Ng/L 0.0158 01/18/202314:27 0.0301 pq/L 0.0063 01/18/202314:00 J 0.0402 Ng/L 0.0111 01/18/202314:00 J 0.0201 pq/L 0.0061 01/18/202314:00 J 0.0782 Ng/L 0.0937 pq/L 0.0520 Ng/L 0.0104 pq/L 0.0937 Ng/L 0.0111 01 /18/2023 13:46 0.0063 01/18/202314:41 0.0111 01 /18/2023 14:41 0.0082 01/18/202314:41 0.0061 01 /18/2023 14:41 0 Page 4 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97369 Matrix: Aqueous Sample ID: 20230109-MW-01 Sampled: 1/9/2023 12:30 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 13:33 JMV V29053 alpha-BHC 0.0404 J ug/L 0.0063 0.0500 1 01/18/23 13:33 JMV V29053 beta-BHC <0.0111 Ng/L 0.0111 0.0500 1 01/18/23 13:33 JMV V29053 delta-BHC <0.0082 ug/L 0.0082 0.0500 1 01/18/23 13:33 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 13:33 JMV V29053 alpha -Chlordane <0.0186 ug/L 0.0186 0.100 1 01/18/23 13:33 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 13:33 JMV V29053 4,4'-DDD <0.0265 ug/L 0.0265 0.100 1 01/18/23 13:33 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 13:33 JMV V29053 4,4'-DDT <0.0176 ug/L 0.0176 0.100 1 01/18/23 13:33 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 13:33 JMV V29053 EndosulfanI <0.0160 ug/L 0.0160 0.0500 1 01/18/23 13:33 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 13:33 JMV V29053 Endosulfan Sulfate <0.0165 ug/L 0.0165 0.0500 1 01/18/23 13:33 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 13:33 JMV V29053 Endrin Aldehyde <0.0158 ug/L 0.0158 0.0500 1 01/18/23 13:33 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 13:33 JMV V29053 gamma-BHC 0.0303 J ug/L 0.0061 0.0500 1 01/18/23 13:33 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 13:33 JMV V29053 Heptachlor Epoxide <0.0224 ug/L 0.0224 0.100 1 01/18/23 13:33 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 13:33 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 5 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97369 Matrix: Aqueous Sample ID: 20230109-MW-01 Sampled: 1/9/2023 12:30 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 13:33 JMV V29053 94.0 Limits:13-186% 1 01/18/2313:33 JMV V29053 100 Limits:40-134% 1 01/18/2313:33 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 6 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97370 Matrix: Aqueous Sample ID: 20230110-MW-02 Sampled: 1/10/2023 16:52 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 15:35 JMV V29053 alpha-BHC <0.0063 ug/L 0.0063 0.0500 1 01/18/23 15:35 JMV V29053 beta-BHC <0.0111 Ng/L 0.0111 0.0500 1 01/18/23 15:35 JMV V29053 delta-BHC <0.0082 ug/L 0.0082 0.0500 1 01/18/23 15:35 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 15:35 JMV V29053 alpha -Chlordane <0.0186 ug/L 0.0186 0.100 1 01/18/23 15:35 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 15:35 JMV V29053 4,4'-DDD <0.0265 ug/L 0.0265 0.100 1 01/18/23 15:35 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 15:35 JMV V29053 4,4'-DDT <0.0176 ug/L 0.0176 0.100 1 01/18/23 15:35 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 15:35 JMV V29053 EndosulfanI <0.0160 ug/L 0.0160 0.0500 1 01/18/23 15:35 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 15:35 JMV V29053 Endosulfan Sulfate <0.0165 ug/L 0.0165 0.0500 1 01/18/23 15:35 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 15:35 JMV V29053 Endrin Aldehyde <0.0158 ug/L 0.0158 0.0500 1 01/18/23 15:35 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 15:35 JMV V29053 gamma-BHC <0.0061 ug/L 0.0061 0.0500 1 01/18/23 15:35 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 15:35 JMV V29053 Heptachlor Epoxide <0.0224 ug/L 0.0224 0.100 1 01/18/23 15:35 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 15:35 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 7 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97370 Matrix: Aqueous Sample ID: 20230110-MW-02 Sampled: 1/10/2023 16:52 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 15:35 JMV V29053 87.4 Limits:13-186% 1 01/18/2315:35 JMV V29053 84.4 Limits:40-134% 1 01/18/2315:35 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 8 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97371 Matrix: Aqueous Sample ID: 20230109-MW-03 Sampled: 1/9/2023 16:34 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 14:14 JMV V29053 alpha-BHC <0.0063 pg/L 0.0063 0.0500 1 01/18/23 14:14 JMV V29053 beta-BHC <0.0111 Ng/L 0.0111 0.0500 1 01/18/23 14:14 JMV V29053 delta-BHC <0.0082 pg/L 0.0082 0.0500 1 01/18/23 14:14 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 14:14 JMV V29053 alpha -Chlordane <0.0186 pg/L 0.0186 0.100 1 01/18/23 14:14 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 14:14 JMV V29053 4,4'-DDD <0.0265 pg/L 0.0265 0.100 1 01/18/23 14:14 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 14:14 JMV V29053 4,4'-DDT <0.0176 pg/L 0.0176 0.100 1 01/18/23 14:14 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 14:14 JMV V29053 Endosulfan I <0.0160 pg/L 0.0160 0.0500 1 01/18/23 14:14 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 14:14 JMV V29053 Endosulfan Sulfate <0.0165 pg/L 0.0165 0.0500 1 01/18/23 14:14 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 14:14 JMV V29053 Endrin Aldehyde <0.0158 pg/L 0.0158 0.0500 1 01/18/23 14:14 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 14:14 JMV V29053 gamma-BHC <0.0061 pg/L 0.0061 0.0500 1 01/18/23 14:14 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 14:14 JMV V29053 Heptachlor Epoxide <0.0224 pg/L 0.0224 0.100 1 01/18/23 14:14 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 14:14 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 9 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97371 Matrix: Aqueous Sample ID: 20230109-MW-03 Sampled: 1/9/2023 16:34 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 14:14 JMV V29053 91.0 Limits:13-186% 1 01/18/2314:14 JMV V29053 82.1 Limits:40-134% 1 01/18/2314:14 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 10 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97372 Matrix: Aqueous Sample ID: 20230110-MW-04 Sampled: 1/10/2023 14:09 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 14:27 JMV V29053 alpha-BHC <0.0063 ug/L 0.0063 0.0500 1 01/18/23 14:27 JMV V29053 beta-BHC 0.0203 IQ Ng/L 0.0111 0.0500 1 01/18/23 14:27 JMV V29053 delta-BHC <0.0082 ug/L 0.0082 0.0500 1 01/18/23 14:27 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 14:27 JMV V29053 alpha -Chlordane <0.0186 ug/L 0.0186 0.100 1 01/18/23 14:27 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 14:27 JMV V29053 4,4'-DDD <0.0265 ug/L 0.0265 0.100 1 01/18/23 14:27 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 14:27 JMV V29053 4,4'-DDT <0.0176 ug/L 0.0176 0.100 1 01/18/23 14:27 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 14:27 JMV V29053 Endosulfan I 0.142 Q ug/L 0.0160 0.0500 1 01/18/23 14:27 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 14:27 JMV V29053 Endosulfan Sulfate 0.0507 ug/L 0.0165 0.0500 1 01/18/23 14:27 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 14:27 JMV V29053 Endrin Aldehyde 0.0812 ug/L 0.0158 0.0500 1 01/18/23 14:27 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 14:27 JMV V29053 gamma-BHC <0.0061 ug/L 0.0061 0.0500 1 01/18/23 14:27 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 14:27 JMV V29053 Heptachlor Epoxide <0.0224 ug/L 0.0224 0.100 1 01/18/23 14:27 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 14:27 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 11 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97372 Matrix: Aqueous Sample ID: 20230110-MW-04 Sampled: 1/10/2023 14:09 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 14:27 JMV V29053 87.5 Limits:13-186% 1 01/18/2314:27 JMV V29053 93.5 Limits:40-134% 1 01/18/2314:27 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 12 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97373 Matrix: Aqueous Sample ID: 20230109-MW-05R Sampled: 1/9/2023 15:15 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 14:00 JMV V29053 alpha-BHC 0.03013 ug/L 0.0063 0.0500 1 01/18/23 14:00 JMV V29053 beta-BHC 0.04023 Ng/L 0.0111 0.0500 1 01/18/23 14:00 JMV V29053 delta-BHC <0.0082 ug/L 0.0082 0.0500 1 01/18/23 14:00 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 14:00 JMV V29053 alpha -Chlordane <0.0186 ug/L 0.0186 0.100 1 01/18/23 14:00 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 14:00 JMV V29053 4,4'-DDD <0.0265 ug/L 0.0265 0.100 1 01/18/23 14:00 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 14:00 JMV V29053 4,4'-DDT <0.0176 ug/L 0.0176 0.100 1 01/18/23 14:00 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 14:00 JMV V29053 EndosulfanI <0.0160 ug/L 0.0160 0.0500 1 01/18/23 14:00 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 14:00 JMV V29053 Endosulfan Sulfate <0.0165 ug/L 0.0165 0.0500 1 01/18/23 14:00 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 14:00 JMV V29053 Endrin Aldehyde <0.0158 ug/L 0.0158 0.0500 1 01/18/23 14:00 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 14:00 JMV V29053 gamma-BHC 0.0201 J ug/L 0.0061 0.0500 1 01/18/23 14:00 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 14:00 JMV V29053 Heptachlor Epoxide <0.0224 ug/L 0.0224 0.100 1 01/18/23 14:00 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 14:00 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 13 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97373 Matrix: Aqueous Sample ID: 20230109-MW-05R Sampled: 1/9/2023 15:15 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 14:00 JMV V29053 82.6 Limits:13-186% 1 01/18/2314:00 JMV V29053 77.6 Limits:40-134% 1 01/18/2314:00 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 14 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97374 Matrix: Aqueous Sample ID: 20230109-MW-06 Sampled: 1/9/2023 14:30 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 13:46 JMV V29053 alpha-BHC <0.0063 ug/L 0.0063 0.0500 1 01/18/23 13:46 JMV V29053 beta-BHC 0.0782 Ng/L 0.0111 0.0500 1 01/18/23 13:46 JMV V29053 delta-BHC <0.0082 ug/L 0.0082 0.0500 1 01/18/23 13:46 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 13:46 JMV V29053 alpha -Chlordane <0.0186 ug/L 0.0186 0.100 1 01/18/23 13:46 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 13:46 JMV V29053 4,4'-DDD <0.0265 ug/L 0.0265 0.100 1 01/18/23 13:46 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 13:46 JMV V29053 4,4'-DDT <0.0176 ug/L 0.0176 0.100 1 01/18/23 13:46 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 13:46 JMV V29053 EndosulfanI <0.0160 ug/L 0.0160 0.0500 1 01/18/23 13:46 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 13:46 JMV V29053 Endosulfan Sulfate <0.0165 ug/L 0.0165 0.0500 1 01/18/23 13:46 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 13:46 JMV V29053 Endrin Aldehyde <0.0158 ug/L 0.0158 0.0500 1 01/18/23 13:46 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 13:46 JMV V29053 gamma-BHC <0.0061 ug/L 0.0061 0.0500 1 01/18/23 13:46 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 13:46 JMV V29053 Heptachlor Epoxide <0.0224 ug/L 0.0224 0.100 1 01/18/23 13:46 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 13:46 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 15 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97374 Matrix: Aqueous Sample ID: 20230109-MW-06 Sampled: 1/9/2023 14:30 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 13:46 JMV V29053 92.0 Limits:13-186% 1 01/18/2313:46 JMV V29053 92.9 Limits:40-134% 1 01/18/2313:46 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 16 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97375 Matrix: Aqueous Sample ID: 20230110-MW-07 Sampled: 1/10/2023 15:10 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 14:41 JMV V29053 alpha-BHC 0.0937 ug/L 0.0063 0.0500 1 01/18/23 14:41 JMV V29053 beta-BHC 0.0520 Ng/L 0.0111 0.0500 1 01/18/23 14:41 JMV V29053 delta-BHC 0.0104 J ug/L 0.0082 0.0500 1 01/18/23 14:41 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 14:41 JMV V29053 alpha -Chlordane <0.0186 ug/L 0.0186 0.100 1 01/18/23 14:41 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 14:41 JMV V29053 4,4'-DDD <0.0265 ug/L 0.0265 0.100 1 01/18/23 14:41 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 14:41 JMV V29053 4,4'-DDT <0.0176 ug/L 0.0176 0.100 1 01/18/23 14:41 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 14:41 JMV V29053 EndosulfanI <0.0160 ug/L 0.0160 0.0500 1 01/18/23 14:41 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 14:41 JMV V29053 Endosulfan Sulfate <0.0165 ug/L 0.0165 0.0500 1 01/18/23 14:41 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 14:41 JMV V29053 Endrin Aldehyde <0.0158 ug/L 0.0158 0.0500 1 01/18/23 14:41 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 14:41 JMV V29053 gamma-BHC 0.0937 ug/L 0.0061 0.0500 1 01/18/23 14:41 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 14:41 JMV V29053 Heptachlor Epoxide <0.0224 ug/L 0.0224 0.100 1 01/18/23 14:41 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 14:41 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 17 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97375 Matrix: Aqueous Sample ID: 20230110-MW-07 Sampled: 1/10/2023 15:10 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 14:41 JMV V29053 88.2 Limits:13-186% 1 01/18/2314:41 JMV V29053 102 Limits:40-134% 1 01/18/2314:41 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 18 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97376 Matrix: Aqueous Sample ID: 20230110-SW-01 Sampled: 1/10/2023 15:45 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 14:54 JMV V29053 alpha-BHC <0.0063 ug/L 0.0063 0.0500 1 01/18/23 14:54 JMV V29053 beta-BHC <0.0111 Ng/L 0.0111 0.0500 1 01/18/23 14:54 JMV V29053 delta-BHC <0.0082 ug/L 0.0082 0.0500 1 01/18/23 14:54 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 14:54 JMV V29053 alpha -Chlordane <0.0186 ug/L 0.0186 0.100 1 01/18/23 14:54 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 14:54 JMV V29053 4,4'-DDD <0.0265 ug/L 0.0265 0.100 1 01/18/23 14:54 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 14:54 JMV V29053 4,4'-DDT <0.0176 ug/L 0.0176 0.100 1 01/18/23 14:54 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 14:54 JMV V29053 EndosulfanI <0.0160 ug/L 0.0160 0.0500 1 01/18/23 14:54 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 14:54 JMV V29053 Endosulfan Sulfate <0.0165 ug/L 0.0165 0.0500 1 01/18/23 14:54 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 14:54 JMV V29053 Endrin Aldehyde <0.0158 ug/L 0.0158 0.0500 1 01/18/23 14:54 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 14:54 JMV V29053 gamma-BHC <0.0061 ug/L 0.0061 0.0500 1 01/18/23 14:54 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 14:54 JMV V29053 Heptachlor Epoxide <0.0224 ug/L 0.0224 0.100 1 01/18/23 14:54 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 14:54 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 19 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97376 Matrix: Aqueous Sample ID: 20230110-SW-01 Sampled: 1/10/2023 15:45 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 14:54 JMV V29053 93.5 Limits:13-186% 1 01/18/2314:54 JMV V29053 83.1 Limits:40-134% 1 01/18/2314:54 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 20 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97377 Matrix: Aqueous Sample ID: 20230110-SW-02 Sampled: 1/10/2023 16:35 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 15:22 JMV V29053 alpha-BHC <0.0063 ug/L 0.0063 0.0500 1 01/18/23 15:22 JMV V29053 beta-BHC <0.0111 Ng/L 0.0111 0.0500 1 01/18/23 15:22 JMV V29053 delta-BHC <0.0082 ug/L 0.0082 0.0500 1 01/18/23 15:22 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 15:22 JMV V29053 alpha -Chlordane <0.0186 ug/L 0.0186 0.100 1 01/18/23 15:22 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 15:22 JMV V29053 4,4'-DDD <0.0265 ug/L 0.0265 0.100 1 01/18/23 15:22 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 15:22 JMV V29053 4,4'-DDT <0.0176 ug/L 0.0176 0.100 1 01/18/23 15:22 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 15:22 JMV V29053 EndosulfanI <0.0160 ug/L 0.0160 0.0500 1 01/18/23 15:22 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 15:22 JMV V29053 Endosulfan Sulfate <0.0165 ug/L 0.0165 0.0500 1 01/18/23 15:22 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 15:22 JMV V29053 Endrin Aldehyde <0.0158 ug/L 0.0158 0.0500 1 01/18/23 15:22 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 15:22 JMV V29053 gamma-BHC <0.0061 ug/L 0.0061 0.0500 1 01/18/23 15:22 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 15:22 JMV V29053 Heptachlor Epoxide <0.0224 ug/L 0.0224 0.100 1 01/18/23 15:22 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 15:22 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 21 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97377 Matrix: Aqueous Sample ID: 20230110-SW-02 Sampled: 1/10/2023 16:35 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 15:22 JMV V29053 90.4 Limits:13-186% 1 01/18/2315:22 JMV V29053 87.4 Limits:40-134% 1 01/18/2315:22 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 22 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97378 Matrix: Aqueous Sample ID: 20230110-SW-03 Sampled: 1/10/2023 16:00 Analytical Method: 8081B Prep Batch(es): V28889 01/16/23 08:47 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0152 Ng/L 0.0152 0.0500 1 01/18/23 15:08 JMV V29053 alpha-BHC <0.0063 ug/L 0.0063 0.0500 1 01/18/23 15:08 JMV V29053 beta-BHC <0.0111 Ng/L 0.0111 0.0500 1 01/18/23 15:08 JMV V29053 delta-BHC <0.0082 ug/L 0.0082 0.0500 1 01/18/23 15:08 JMV V29053 Chlordane <0.180 Ng/L 0.180 0.500 1 01/18/23 15:08 JMV V29053 alpha -Chlordane <0.0186 ug/L 0.0186 0.100 1 01/18/23 15:08 JMV V29053 gamma -Chlordane <0.0231 Ng/L 0.0231 0.100 1 01/18/23 15:08 JMV V29053 4,4'-DDD <0.0265 ug/L 0.0265 0.100 1 01/18/23 15:08 JMV V29053 4,4'-DDE <0.0218 Ng/L 0.0218 0.100 1 01/18/23 15:08 JMV V29053 4,4'-DDT <0.0176 ug/L 0.0176 0.100 1 01/18/23 15:08 JMV V29053 Dieldrin <0.0137 Ng/L 0.0137 0.0500 1 01/18/23 15:08 JMV V29053 EndosulfanI <0.0160 ug/L 0.0160 0.0500 1 01/18/23 15:08 JMV V29053 Endosulfan II <0.0121 Ng/L 0.0121 0.0500 1 01/18/23 15:08 JMV V29053 Endosulfan Sulfate <0.0165 ug/L 0.0165 0.0500 1 01/18/23 15:08 JMV V29053 Endrin <0.0136 Ng/L 0.0136 0.0500 1 01/18/23 15:08 JMV V29053 Endrin Aldehyde <0.0158 ug/L 0.0158 0.0500 1 01/18/23 15:08 JMV V29053 Endrin Ketone <0.0181 Ng/L 0.0181 0.100 1 01/18/23 15:08 JMV V29053 gamma-BHC <0.0061 ug/L 0.0061 0.0500 1 01/18/23 15:08 JMV V29053 Heptachlor <0.0130 Ng/L 0.0130 0.0500 1 01/18/23 15:08 JMV V29053 Heptachlor Epoxide <0.0224 ug/L 0.0224 0.100 1 01/18/23 15:08 JMV V29053 Methoxychlor <0.0179 Ng/L 0.0179 0.100 1 01/18/23 15:08 JMV V29053 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 23 of 30 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Jessica Mayers Report Date : 01/23/2023 231 Haywood Street Information : Received : 01/12/2023 Asheville , NC 28801 Report Number : 23-012-0004 REPOR T OF A NA L YSIS Lab No : 97378 Matrix: Aqueous Sample ID: 20230110-SW-03 Sampled: 1/10/2023 16:00 Analytical Method: 8081B Prep Method: 3510C Test Toxaphene Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Prep Batch(es): V28889 01/16/23 08:47 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.421 Ng/L 0.421 1.00 1 01/18/23 15:08 JMV V29053 95.6 Limits:13-186% 1 01/18/2315:08 JMV V29053 94.5 Limits:40-134% 1 01/18/2315:08 JMV V29053 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Q RPD >40% dual column results Page 24 of 30 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 23-012-0004 QC Prep: V28889 QC Prep Batch Method: 3510C QC Analytical Batch(es): V29053 Analysis Method: 8081B Analysis Description: Organochlorine Pesticides by GC Lab Reagent Blank LRB-V28889 Matrix: AQU Associated Lab Samples: 97369, 97370, 97371, 97372, 97373, 97374, 97375, 97376, 97377, 97378 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Aldrin alpha-BHC beta-BHC delta-BHC Chlordane alpha -Chlordane gamma -Chlordane 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Endrin Ketone gamma-BHC Heptachlor Heptachlor Epoxide M ethoxychlor Toxaphene Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) pg/L <0.0152 pg/L <0.0063 pg/L <0.0111 pg/L <0.0082 pg/L <0.180 pg/L <0.0186 pg/L <0.0231 pg/L <0.0265 pg/L <0.0218 pg/L <0.0176 pg/L <0.0137 pg/L <0.0160 pg/L <0.0121 pg/L <0.0165 pg/L <0.0136 pg/L <0.0158 pg/L <0.0181 pg/L <0.0061 pg/L <0.0130 pg/L <0.0224 pg/L <0.0179 pg/L <0.421 0.0152 0.0063 0.0111 0.0082 0.180 0.0186 0.0231 0.0265 0.0218 0.0176 0.0137 0.0160 0.0121 0.0165 0.0136 0.0158 0.0181 0.0061 0.0130 0.0224 0.0179 0.421 0.0500 0.0500 0.0500 0.0500 0.500 0.100 0.100 0.100 0.100 0.100 0.0500 0.0500 0.0500 0.0500 0.0500 0.0500 0.100 0.0500 0.0500 0.100 0.100 1.00 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 01/18/23 12:25 100 84.0 13-186 40-134 Date: 01/23/2023 01:50 PM Page 25 of 30 Page 1 of 3 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 23-012-0004 QC Prep: V28889 QC Prep Batch Method: 3510C Laboratory Control Sample LCS-V28889 QC Analytical Batch(es): V29053 Analysis Method: 8081B Analysis Description: Organochlorine Pesticides by GC Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Chlordane pg/L 10.0 10.3 103 62-140 Toxaphene pg/L 10.0 10.2 102 33-134 Laboratory Control Sample & LCSD Parameter Units LCS-V28889 Spike Conc. LCSD-V28889 LCS Result LCSD Result LCS %Rec LCSD a/o Rec % Rec Limits RPD Max RPD Aldrin pg/L 1.00 0.960 0.920 96.0 92.0 45-134 4.2 30.0 alpha-BHC pg/L 1.00 1.03 0.980 103 98.0 54-138 4.9 30.0 beta-BHC pg/L 1.00 0.960 0.920 96.0 92.0 56-136 4.2 30.0 delta-BHC pg/L 1.00 0.770 0.720 77.0 72.0 52-142 6.7 30.0 alpha -Chlordane pg/L 1.00 1.02 0.980 102 98.0 60-129 4.0 30.0 gamma -Chlordane pg/L 1.00 1.01 0.970 101 97.0 56-136 4.0 30.0 4,4'-DDD pg/L 1.00 1.10 1.05 110 105 56-143 4.6 30.0 4,4'-DDE pg/L 1.00 1.12 1.08 112 108 57-135 3.6 30.0 4,4'-DDT pg/L 1.00 1.20 1.15 120 115 51-143 4.2 30.0 Dieldrin pg/L 1.00 1.08 1.03 108 103 60-136 4.7 30.0 EndosulfanI pg/L 1.00 1.06 1.01 106 101 62-126 4.8 30.0 EndosulfanII pg/L 1.00 1.10 1.06 110 106 52-135 3.7 30.0 Endosulfan Sulfate pg/L 1.00 1.05 1.01 105 101 62-133 3.8 30.0 Endrin pg/L 1.00 1.14 1.09 114 109 60-138 4.4 30.0 Endrin Aldehyde pg/L 1.00 1.01 0.980 101 98.0 51-132 3.0 30.0 Endrin Ketone pg/L 1.00 1.10 1.06 110 106 58-134 3.7 30.0 gamma-BHC pg/L 1.00 1.02 0.970 102 97.0 59-134 5.0 30.0 Heptachlor pg/L 1.00 0.970 0.920 97.0 92.0 54-130 5.2 30.0 Heptachlor Epoxide pg/L 1.00 1.03 0.980 103 98.0 61-133 4.9 30.0 Methoxychlor pg/L 1.00 1.10 1.06 110 106 54-145 3.7 30.0 Date: 01/23/2023 01:50 PM Page 2 of 3 Page 26 of 30 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 23-012-0004 QC Prep: V28889 QC Analytical Batch(es): V29053 QC Prep Batch Method: 3510C Analysis Method: 8081B Analysis Description: Organochlorine Pesticides by GC Laboratory Control Sample & LCSD LCS-V28889 LCSD-V28889 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Decachlorobiphenyl (S) 103 98.0 13-186 Tetrachloro-m-xylene (S) 83.0 78.0 40-134 Date: 01/23/2023 01:50 PM Page 3 of 3 Page 27 of 30 WayPAoint. NALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: 01015 Customer Name: Anchor QEA of North Carolina, PLLC Report Number: 23-012-0004 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client # Courier 0 Other: Thermometer ID: IRT15 1.6C Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F Custody seals intact on shipping container/cooler? (*� Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample Iabel(s)? (0) Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? U Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? U Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. U Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) Special precautions or instructions included? Comments: 0 Yes 0 No U N/A F Low concentration EnCore samplers (48 hr) Low conc pre -weighed vials (Sod Bis -14 d) 0Yes ONo Signature: ngelo Norvell Date & Time: 01/12/2023 11:03:37 Page 28 of 30 N Q O V Vi R n r 3 CD 7 IT V. 0 u, r LN w n � 3 m n r ❑r 7 -r CAm 7 n � A � v rn t L� v m cnu)mm-u n 3 m m 0 0 3 v o !° y n m a ❑ �(y^• ^ w - 3 0 (A> 0 3 3 Vi O. r�* w U Z uv m� @ m r v� .,, �, 00 hi��y W iJ 3 'y+ g� y Q ❑ H. � h y Z a - LA W > a C =, - r _ t 5 .�=r, NZ 1 N s'1 N w rrp a 6 wn+ ■ 10 y > 5 mO x 0 m m 3 ti m H a N {p maoa� a c am i Q a r. m 0 z � In (DID0 0 d p m `�❑LA m me QmII p o ❑ '� d — ma 3 N 4 z¢H Cx a :V z Yri a m n❑w 5 a � uzi m L a m mm nr a ui z rm C% V w m� �o L M C q W a � 4 - = C 0 9, a ❑ c N [nC M = m N o yy n ° m R m❑ Z _ c i� N p m mn z C [7 �]-- m Fw H/ m "D � Fm m n N m r y OC T. 'In Q 3 m V a n n ?4 _ m 0 m� M, �zz = d M 3 z mr"�'rn y z m m m O Z Z - y x ;lu v [7 2. m CA xC = U6)rmn d m a I in CD m m G C 0 x 0 ci o Q r n Al�Ili! Page 29 of 30 L L L Mm � 171 m � y x C7 � ❑ N C L 70 8- n CL Li ❑i3, 0 z ❑z9 ❑L x n G to n ❑o Z n L n ❑ ❑ x 0 L w n LL Z n L N n Em 0 C N v -0 m 3a 3 v m � 2 _ 0.a m e Vi r—L. E W 3 x7 � nVa� @n 5 O Mc 0 m n C: 4 s m T n •• 0 G a N a 1.0 v G G G r m ❑ r WZ 0 � �` t,j Yr a t z r m W o 7 (A xgo G W un 1 U) H m ❑ m c>�a m0Qx m m m ❑ ❑ m 0 ID v CD r r 4 D 0 �n 03 y0 c -0 z T !/ - D. a � mC Y N K 0(A 4} s w -4 - r to 3 a CL ad r a 5 F PI) 2 + •C n c eu • g m C 3 a � 7 m S r--c 'PAm�� �z n m j m z Cv ❑ 3 mr^m m p ❑ o mo m Z x�LLp m A Ow ❑ 7 $ m J a n W _ I � m N Z O x oyn a U) .p Fz m L m C y , mrn tn� 0_ U U. u m � w a ❑ ❑ 0 ai Sl it N n 0 cx� v m_ m v�rn' 3 M n ° m n w n❑ m p i -t r m nvs N 2� S 7 3 z n m M C7 [n7 m a mw i W O C m 2. m X r c sri a G) 0 10 ` m � .a Y a G .n. Z ~y � Q m co x a • O x m a M C 4O ° I m I,` a ri Page 30 of 30 Waypointo ANALYTICAL 11 /1 /2022 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville, NC, 28801 Ref: Analytical Testing Lab Report Number: 22-279-0018 Client Project Description: Jackson County C21480-01.01, WA-1 Site: 58-02 Project Number: 58-02 Dear Chuck Pippin: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/6/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, a,j Angela D Overcash Senior Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 108 0 Waypoint. ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12/31/2022 South Carolina State Program 99012 07/31/2023 South Carolina State Program 99012 12/31/2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00016/22-279-0018 Page 2 of 108 Waypoint. (2) ANALYTICAL Sample Report Number: 22-279-0018 Client Project Description: Jackson County C21480-01.01, WA-1 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca I som Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 90039 MW-01-20221004 Aqueous 10/04/2022 16:32 10/06/2022 12:30 90039 MW-01-20221004 Aqueous 10/04/2022 16:32 10/06/2022 12:30 8151A WP MTN 90039 MW-01-20221004 Aqueous 10/04/2022 16:32 10/06/2022 12:30 8081E WP MTN 90039 MW-01-20221004 Aqueous 10/04/2022 16:32 10/06/2022 12:30 8270D WP MTN 90039 MW-01-20221004 Aqueous 10/04/2022 16:32 10/06/2022 12:30 8270D WP MTN 90039 MW-01-20221004 Aqueous 10/04/2022 16:32 10/06/2022 12:30 8270C WP MTN 90040 MW-03-20221004 Aqueous 10/04/2022 17:42 10/06/2022 12:30 90040 MW-03-20221004 Aqueous 10/04/2022 17:42 10/06/2022 12:30 8270C WP MTN 90040 MW-03-20221004 Aqueous 10/04/2022 17:42 10/06/2022 12:30 8270D WP MTN 90040 MW-03-20221004 Aqueous 10/04/2022 17:42 10/06/2022 12:30 8270D WP MTN 90040 MW-03-20221004 Aqueous 10/04/2022 17:42 10/06/2022 12:30 8151A WP MTN 90040 MW-03-20221004 Aqueous 10/04/2022 17:42 10/06/2022 12:30 8081E WP MTN 90041 MW-04-20221004 Aqueous 10/04/2022 12:30 10/06/2022 12:30 90041 MW-04-20221004 Aqueous 10/04/2022 12:30 10/06/2022 12:30 8081E WP MTN 90041 MW-04-20221004 Aqueous 10/04/2022 12:30 10/06/2022 12:30 8151A WP MTN 90041 MW-04-20221004 Aqueous 10/04/2022 12:30 10/06/2022 12:30 8270C WP MTN 90041 MW-04-20221004 Aqueous 10/04/2022 12:30 10/06/2022 12:30 8270D WP MTN 90041 MW-04-20221004 Aqueous 10/04/2022 12:30 10/06/2022 12:30 8270D WP MTN 90042 MW-06-20221004 Aqueous 10/04/2022 14:36 10/06/2022 12:30 90042 MW-06-20221004 Aqueous 10/04/2022 14:36 10/06/2022 12:30 8270C WP MTN 90042 MW-06-20221004 Aqueous 10/04/2022 14:36 10/06/2022 12:30 8270D WP MTN 90042 MW-06-20221004 Aqueous 10/04/2022 14:36 10/06/2022 12:30 8270D WP MTN 90042 MW-06-20221004 Aqueous 10/04/2022 14:36 10/06/2022 12:30 8151A WP MTN 90042 MW-06-20221004 Aqueous 10/04/2022 14:36 10/06/2022 12:30 8081E WP MTN 90043 SW-03-20221004 Aqueous 10/04/2022 10:40 10/06/2022 12:30 90043 SW-03-20221004 Aqueous 10/04/2022 10:40 10/06/2022 12:30 8270C WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 108 Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointana lyti ca I som Sample Summary Table Report Number: 22-279-0018 Client Project Description: Jackson County C21480-01.01, WA-1 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 90043 SW-03-20221004 Aqueous 10/04/2022 10:40 10/06/2022 12:30 8270D WP MTN 90043 SW-03-20221004 Aqueous 10/04/2022 10:40 10/06/2022 12:30 8270D WP MTN 90043 SW-03-20221004 Aqueous 10/04/2022 10:40 10/06/2022 12:30 8151A WP MTN 90043 SW-03-20221004 Aqueous 10/04/2022 10:40 10/06/2022 12:30 8081E WP MTN 90044 TripBlank-20221004-1 Aqueous 10/04/2022 10/06/2022 12:30 90045 TripBlank-20221004-2 Aqueous 10/04/2022 10/06/2022 12:30 WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 4 of 108 Waypoint.(2) ANALYTICAL Project: Jackson County Report Number: 22-279-0018 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Summary of Detected Client Sample ID Lab Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers MW-01-20221004 V 90039 6020B Barium 106 pq/L 3.40 101101202219:18 6020B Cadmium 0.327 Ng/L 0.150 10/10/202219:18 6020B Cobalt 105 uq/L 0.080 10/10/202219:18 6020B Copper 5.94 Ng/L 0.890 10/11/202216:35 6020B Nickel 14.7 uq/L 0.720 10/10/202219:18 6020B Thallium 0.734 Ng/L 0.280 10/10/202219:18 6020B Zinc 22.8 uq/L 3.90 10/10/202219:18 8260D Benzene 0.550 pg/L 0.180 10/11/2022 05:54 8260D Chlorobenzene 0.692 uq/L 0.190 10/11/2022 05:54 8260D 1,4-Dichlorobenzene 5.72 pg/L 0.210 10/11/2022 05:54 8260D 1,1-Dichloroethane 1.56 pq/L 0.240 10/11/2022 05:54 8260D cis- 1,2-Dichloroethene 1.48 Ng/L 0.200 10/11/2022 05:54 8260D Tetrachloroethene 0.342 pq/L 0.220 10/11/2022 05:54 8260D Trichloroethene 0.241 Ng/L 0.180 10/11/2022 05:54 8270D 1,4-Dichlorobenzene 4.16 pg/L 0.707 10/20/2022 21:06 MW-03-20221004 V 90040 6020B Barium 221 Ng/L 34.0 10/17/2022 22:20 6020B Cadmium 0.442 uq/L 0.150 10/10/202219:25 6020B Chromium 1.66 Ng/L 1.00 10/10/202219:25 6020B Cobalt 7.49 uq/L 0.080 10/10/202219:25 6020B Copper 5.00 Ng/L 0.890 10/11/202216:42 6020B Nickel 6.84 uq/L 0.720 10/10/202219:25 6020B Zinc 13.2 Ng/L 3.90 10/10/202219:25 8260D Benzene 0.553 uq/L 0.180 10/11/2022 05:27 8260D Chlorobenzene 6.60 Ng/L 0.190 10/11/2022 05:27 8260D 1,2-Dichlorobenzene 0.243 uq/L 0.220 10/11/2022 05:27 8260D 1,4-Dichlorobenzene 4.31 Ng/L 0.210 10/11/2022 05:27 8260D 1,1-Dichloroethane 0.516 uq/L 0.240 10/11/2022 05:27 8260D cis- 1,2-Dichloroethene 1.14 Ng/L 0.200 10/11/2022 05:27 8260D SIM 1,4-Dioxane 5.58 uq/L 0.139 10/07/2022 12:58 8270D 1,4-Dichlorobenzene 2.80 Ng/L 0.773 10/20/2022 21:27 MW-04-20221004 V 90041 6020B Barium 151 pg/L 3.40 101101202219:32 6020B Cadmium 0.291 Ng/L 0.150 10/10/202219:32 6020B Cobalt 3.09 uq/L 0.080 101101202219:32 6020B Copper 2.27 Ng/L 0.890 10/11/202216:49 0 J I I 0 0 0 0 Page 5 of 108 Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointana lyti ca I som Summary of Detected Analytes Project: Jackson County Report Number: 22-279-0018 Client Sample ID Lab Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers MW-04-20221004 V 90041 6020B Nickel 1.47 pq/L 0.720 101101202219:32 1 6020B Silver 0.168 pg/L 0.130 10/10/202219:32 1 6020B Zinc 4.69 pq/L 3.90 10/10/202219:32 1 7470A Mercury (Total) 0.400 pg/L 0.0700 10/11/2022 16:22 8260D Benzene 0.376 pq/L 0.180 10/11/2022 04:06 1 8260D Chlorobenzene 1.60 pg/L 0.190 10/11/2022 04:06 8260D 1,4-Dichlorobenzene 2.57 pq/L 0.210 10/11/2022 04:06 8260D cis- 1,2-Dichloroethene 0.816 pg/L 0.200 10/11/2022 04:06 8260D SIM 1,4-Dioxane 11.0 pq/L 0.139 10/07/2022 13:23 8270D 1,4-Dichlorobenzene 1.81 pg/L 0.725 10/20/2022 21:47 1 8270D Diethyl phthalate 0.952 pg/L 0.731 10/20/2022 21:47 1 MW-06-20221004 V 90042 4500S2F-2011 Sulfide 1.10 mg/L 0.83 10/10/202211:00 1 6020B Barium 48.2 pq/L 3.40 10/10/202219:38 6020B Cobalt 8.07 pg/L 0.080 10/10/202219:38 6020B Copper 2.38 pq/L 0.890 10/11/202216:55 6020B Nickel 3.93 pg/L 0.720 10/10/202219:38 6020B Thallium 0.311 pq/L 0.280 10/10/202219:38 1 6020B Zinc 14.3 pg/L 3.90 10/10/202219:38 1 8260D 1,4-Dichlorobenzene 0.728 pq/L 0.210 10/11/2022 04:33 8260D 1,1-Dichloroethane 0.858 pg/L 0.240 10/11/2022 04:33 8260D cis- 1,2-Dichloroethene 0.622 pq/L 0.200 10/11/2022 04:33 SW-03-20221004 V 90043 2340C-2011 Hardness 4000 pg/L 1140 10/24/202211:30 1 6020B Copper 19.2 pg/L 4.45 10/11/202217:09 6020B Zinc 80.5 pg/L 19.5 10/10/202219:52 1 TripBlank-2022100, V 90044 8260D Acetone 4.84 pq/L 1.80 101101202214:09 1 8260D 2,2-Dichloropropane 0.313 pg/L 0.210 10/10/202214:09 1 8260D Ethylbenzene 0.352 pq/L 0.170 10/10/202214:09 1 8260D 2-Hexanone 0.480 pg/L 0.380 10/10/202214:09 1 8260D Naphthalene 1.12 pq/L 0.470 10/10/202214:09 8260D Styrene 0.283 pg/L 0.220 10/10/202214:09 1 8260D Toluene 0.304 pq/L 0.220 10/10/202214:09 1 8260D Trichloroethene 0.378 pg/L 0.180 10/10/202214:09 1 Page 6 of 108 Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointana lyti ca I som Summary of Detected Analytes Project: Jackson County Report Number: 22-279-0018 Client Sample ID Lab Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers TripBlank-2022100, V 90044 8260D o-Xylene 8260D m,p-Xylene 8260D Xylene (Total) TripBlank-2022100, V 90045 8260D Ethylbenzene 8260D Naphthalene 8260D Styrene 8260D Toluene 8260D Trichloroethene 8260D o-Xylene 8260D m,p-Xylene 8260D Xylene (Total) 0.889 pq/L 0.210 10/10/202214:09 1.10 Ng/L 0.420 10/10/202214:09 1.99 pq/L 0.210 10/10/202214:09 0.341 Ng/L 0.170 10/10/202214:36 1 1.01 pq/L 0.470 101101202214:36 0.287 Ng/L 0.220 10/10/202214:36 1 0.368 pq/L 0.220 101101202214:36 1 0.373 Ng/L 0.180 10/10/202214:36 1 0.814 pq/L 0.210 101101202214:36 1.05 Ng/L 0.420 10/10/202214:36 1.86 pq/L 0.210 101101202214:36 Page 7 of 108 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-279-0018 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/01/2022 Received : 10/06/2022 Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane <0.139 Ng/L 0.139 2.00 1 10/07/22 12:33 TBL 8260D SIM 1,4-Naphthoquinone <12.2 pg/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D 1-Naphthylamine <12.2 Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D 2-Acetylaminofluorene <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D 2-Naphthylamine <12.2 Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D 3-Methylcholanthrene <12.2 pg/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D 4-Aminobiphenyl <12.2 Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D 5-Nitro-o-toluidine <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D 7,12-Di methylbenz(a)a nthracene <12.2 Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D Diallate <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D Hexachloropropene <12.2 Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D Isosafrole <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D Methapyrilene <12.2 Ng/L 12.2 24.4 1 10/20/22 21:06 VBW 8270D N-Nitrosomethylethylamine <12.2 pg/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D N-Nitrosomorpholine <12.2 Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D N-Nitrosopyrrolidine <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D N-Nitrosopiperidine <12.2 Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D 0,0,0-Triethyl Phosphorothioate <0.402 pg/L 0.402 1.22 1 10/24/22 15:26 VBW 8270C o-Toluidine <12.2 Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D p-Dimethylaminoazobenzene <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D p-Phenylenediamine <12.2 M Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D Pronamide <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D Safrole <12.2 Ng/L 12.2 12.2 1 10/20/22 21:06 VBW 8270D Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 8 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90039 Sample ID: MW-01-20221004 Matrix: Aqueous Sampled: 10/4/2022 16:32 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Thionazine <0.402 Ng/L 0.402 1.22 1 10/24/2215:26 VBW 8270C Sulfide <0.83 mg/L 0.83 2.00 1 10/10/2211:00 SLO 4500S2F-2011 Antimony <0.680 Ng/L 0.680 2.00 1 10/10/22 19:18 EDV 6020B Arsenic <0.490 ug/L 0.490 1.00 1 10/10/22 19:18 EDV 6020B Barium 106 Ng/L 3.40 10.0 1 10/10/22 19:18 EDV 6020B Beryllium <0.240 ug/L 0.240 1.00 1 10/10/22 19:18 EDV 6020B Cadmium 0.3273 Ng/L 0.150 1.00 1 10/10/22 19:18 EDV 6020B Chromium <1.00 ug/L 1.00 2.00 1 10/10/22 19:18 EDV 6020B Cobalt 105 Ng/L 0.080 1.00 1 10/10/22 19:18 EDV 6020B Copper 5.94 ug/L 0.890 2.00 1 10/11/2216:35 EDV 6020B Lead <0.500 Ng/L 0.500 1.00 1 10/10/22 19:18 EDV 6020B Mercury (Total) <0.0700 ug/L 0.0700 0.200 1 10/11/22 16:17 EDV 7470A Nickel 14.7 Ng/L 0.720 2.00 1 10/10/22 19:18 EDV 6020B Selenium <2.30 ug/L 2.30 5.00 1 10/10/22 19:18 EDV 6020B Silver <0.130 Ng/L 0.130 1.00 1 10/10/22 19:18 EDV 6020B Tin <1.50 ug/L 1.50 5.00 1 10/10/22 19:18 EDV 6020B Thallium 0.7343 Ng/L 0.280 2.00 1 10/10/22 19:18 EDV 6020B Vanadium <2.10 ug/L 2.10 5.00 1 10/10/22 19:18 EDV 6020B Zinc 22.8 Ng/L 3.90 20.0 1 10/10/22 19:18 EDV 6020B Qualifiers/ DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit H Beyond holding time M Minimum value Page 9 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0025 H Ng/L 0.0025 0.0470 10 10/21/22 05:00 VIC L644618 alpha-BHC <0.0024 H ug/L 0.0024 0.0470 10 10/21/22 05:00 VIC L644618 beta-BHC <0.0024 H Ng/L 0.0024 0.0470 10 10/21/22 05:00 VIC L644618 delta-BHC <0.0018 H ug/L 0.0018 0.0470 10 10/21/22 05:00 VIC L644618 Chlordane <0.0259 H Ng/L 0.0259 0.235 10 10/21/22 05:00 VIC L644618 alpha -Chlordane <0.0024 H ug/L 0.0024 0.0470 10 10/21/22 05:00 VIC L644618 gamma -Chlordane <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:00 VIC L644618 4,4'-DDD <0.0025 H ug/L 0.0025 0.0470 10 10/21/22 05:00 VIC L644618 4,4'-DDE <0.0025 H Ng/L 0.0025 0.0470 10 10/21/22 05:00 VIC L644618 4,4'-DDT <0.0041 H ug/L 0.0041 0.0470 10 10/21/22 05:00 VIC L644618 Dieldrin <0.0018 H Ng/L 0.0018 0.0470 10 10/21/22 05:00 VIC L644618 EndosulfanI <0.0018 H ug/L 0.0018 0.0470 10 10/21/22 05:00 VIC L644618 EndosulfanII <0.0033 H Ng/L 0.0033 0.0470 10 10/21/22 05:00 VIC L644618 Endosulfan Sulfate <0.0017 H ug/L 0.0017 0.0470 10 10/21/22 05:00 VIC L644618 Endrin <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:00 VIC L644618 Endrin Aldehyde <0.0017 H ug/L 0.0017 0.0470 10 10/21/22 05:00 VIC L644618 Endrin Ketone <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:00 VIC L644618 gamma-BHC <0.0021 H ug/L 0.0021 0.0470 10 10/21/22 05:00 VIC L644618 Heptachlor <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:00 VIC L644618 Heptachlor Epoxide <0.0017 H ug/L 0.0017 0.0470 10 10/21/22 05:00 VIC L644618 Methoxychlor <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:00 VIC L644618 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 10 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 Lab No : 90039 Sample ID: MW-01-20221004 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/4/2022 16:32 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0236 H Ng/L 0.0236 0.353 10 10/21/22 05:00 VIC L644618 Surrogate: Decachlorobiphenyl 97.5 Limits: 36-116% 10 10/21/22 05:00 L644618 Surrogate: Tetrachloro-m-xylene 74.4 Limits: 25-123% 10 10/21/22 05:00 L644618 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2375 Pg/L 0.2375 0.2857 1 10/14/22 23:12 VIC L643610 Dalapon <0.5885 Ng/L 0.5885 0.6286 1 10/14/22 23:12 VIC L643610 2,4-DB <0.1559 ug/L 0.1559 0.2857 1 10/14/22 23:12 VIC L643610 Dicamba <0.06509 Ng/L 0.06509 0.01142 1 10/14/22 23:12 VIC L643610 Dichlorprop <0.09097 ug/L 0.09097 0.1143 1 10/14/22 23:12 VIC L643610 Dinoseb <0.03083 Ng/L 0.03083 0.1143 1 10/14/22 23:12 VIC L643610 MCPA <21.69 ug/L 21.69 57.14 1 10/14/22 23:12 VIC L643610 MCPP <13.43 Ng/L 13.43 57.14 1 10/14/22 23:12 VIC L643610 Picloram <0.05175 ug/L 0.05175 0.1143 1 10/14/22 23:12 VIC L643610 2,4,5-T <0.01144 Ng/L 0.01144 0.03428 1 10/14/22 23:12 VIC L643610 2,4,5-TP(Silvex) <0.01867 ug/L 0.01867 0.1143 1 10/14/22 23:12 VIC L643610 Surrogate: DCAA 124.2 Limits: 20-150% 1 10/14/22 23:12 L643610 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 11 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/11/22 05:54 MSA V24952 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/18/22 11:57 ANG V25258 Acrolein <2.00 Ng/L 2.00 5.00 1 10/11/22 05:54 MSA V24952 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/11/22 05:54 MSA V24952 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/18/22 11:57 ANG V25258 Benzene 0.550 ug/L 0.180 0.500 1 10/11/22 05:54 MSA V24952 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/11/22 05:54 MSA V24952 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/11/22 05:54 MSA V24952 Bromoform <1.50 Ng/L 1.50 5.00 1 10/11/22 05:54 MSA V24952 Bromomethane <0.280 ug/L 0.280 1.00 1 10/11/22 05:54 MSA V24952 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/11/22 05:54 MSA V24952 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/11/22 05:54 MSA V24952 Chlorobenzene 0.692 Ng/L 0.190 0.500 1 10/11/22 05:54 MSA V24952 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/11/22 05:54 MSA V24952 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/11/22 05:54 MSA V24952 Chloroform <0.220 ug/L 0.220 0.500 1 10/11/22 05:54 MSA V24952 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/11/22 05:54 MSA V24952 Chloroprene <0.450 ug/L 0.450 10.0 1 10/18/22 11:57 ANG V25258 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/11/22 05:54 MSA V24952 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/11/22 05:54 MSA V24952 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/11/22 05:54 MSA V24952 trans-1,4-Dichloro-2-butene <1.30 ug/L 1.30 10.0 1 10/11/22 05:54 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 12 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene <0.220 Ng/L 0.220 0.500 1 10/11/22 05:54 MSA V24952 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/11/22 05:54 MSA V24952 1,4-Dichlorobenzene 5.72 Ng/L 0.210 0.500 1 10/11/22 05:54 MSA V24952 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/11/22 05:54 MSA V24952 1,1-Dichloroethane 1.56 Ng/L 0.240 0.500 1 10/11/22 05:54 MSA V24952 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/11/22 05:54 MSA V24952 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/11/22 05:54 MSA V24952 cis- 1,2-Dich loroethene 1.48 ug/L 0.200 0.500 1 10/11/22 05:54 MSA V24952 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/11/22 05:54 MSA V24952 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/11/22 05:54 MSA V24952 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/11/22 05:54 MSA V24952 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/11/22 05:54 MSA V24952 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/11/22 05:54 MSA V24952 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/11/22 05:54 MSA V24952 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/11/22 05:54 MSA V24952 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/18/22 11:57 ANG V25258 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/11/22 05:54 MSA V24952 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/11/22 05:54 MSA V24952 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/11/22 05:54 MSA V24952 Iodomethane <0.054 ug/L 0.054 0.500 1 10/11/22 05:54 MSA V24952 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/11/22 05:54 MSA V24952 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/18/2211:57 ANG V25258 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 13 of 108 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-279-0018 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/01/2022 Received : 10/06/2022 Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/11/22 05:54 MSA V24952 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/11/22 05:54 MSA V24952 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/11/22 05:54 MSA V24952 Propionitrile <23.7 ug/L 23.7 10.0 1 10/18/2211:57 ANG V25258 Styrene <0.220 Ng/L 0.220 0.500 1 10/11/22 05:54 MSA V24952 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 05:54 MSA V24952 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/11/22 05:54 MSA V24952 Tetrachloroethene 0.3421 ug/L 0.220 0.500 1 10/11/22 05:54 MSA V24952 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/11/22 05:54 MSA V24952 Toluene <0.220 ug/L 0.220 0.500 1 10/11/22 05:54 MSA V24952 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/11/22 05:54 MSA V24952 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 05:54 MSA V24952 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/11/22 05:54 MSA V24952 Trichloroethene 0.241 J ug/L 0.180 0.500 1 10/11/22 05:54 MSA V24952 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/11/22 05:54 MSA V24952 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/11/22 05:54 MSA V24952 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/11/22 05:54 MSA V24952 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/11/22 05:54 MSA V24952 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/11/22 05:54 MSA V24952 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/11/22 05:54 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 14 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Analytical Method: 8270C Prep Method: 3510C Test <0.21 Ng/L 0.210 0.500 1 10/11/22 05:54 V24952 100 Limits: 80-124% 1 10/11/22 05:54 MSA V24952 97.8 Limits: 75-129% 1 10/11/22 05:54 MSA V24952 93.0 Limits: 63-136% 1 10/11/22 05:54 MSA V24952 95.6 Limits: 77-123% 1 10/11/22 05:54 MSA V24952 99.4 Limits:80-124% 1 10/18/2211:57 ANG V25258 99.6 Limits:75-129% 1 10/18/2211:57 ANG V25258 101 Limits:63-136% 1 10/18/2211:57 ANG V25258 101 Limits:77-123% 1 10/18/2211:57 ANG V25258 Prep Batch(es): L642252 10/10/22 15:46 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dimethoate <0.869 Disulfoton <0.568 Ethyl Parathion <0.692 Famphur <0.624 Methyl Parathion <0.982 Phorate <0.803 Surrogate: Tributyl phosphate Surrogate: Triphenyl phosphate Qualifiers/ DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit Pg/L 0.869 1.22 Ng/L 0.568 1.22 ug/L 0.692 1.22 Ng/L 0.624 1.22 ug/L 0.982 1.22 Ng/L 0.803 1.22 72.5 Limits: 50-150% 73.8 Limits: 50-150% 1 10/24/22 15:26 VBW L644472 1 10/24/22 15:26 VBW L644472 1 10/24/22 15:26 VBW L644472 1 10/24/22 15:26 VBW L644472 1 10/24/22 15:26 VBW L644472 1 10/24/22 15:26 VBW L644472 1 10/24/22 15:26 VBW 8270C 1 10/24/22 15:26 VBW 8270C H Beyond holding time M Minimum value Page 15 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,3-Dinitrobenzene <1.10 Ng/L 1.10 12.2 1 10/20/22 21:06 VBW L644470 1,3,5-Trinitrobenzene <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW L644471 Acenaphthene <0.514 Ng/L 0.514 2.44 1 10/20/22 21:06 VBW L644470 Acenaphthylene <0.523 ug/L 0.523 2.44 1 10/20/22 21:06 VBW L644470 Acetophenone <0.836 Ng/L 0.836 6.10 1 10/20/22 21:06 VBW L644470 Anthracene <0.569 ug/L 0.569 2.44 1 10/20/22 21:06 VBW L644470 Benzo(a)anthracene <0.520 Ng/L 0.520 2.44 1 10/20/22 21:06 VBW L644470 Benzo(a)pyrene <1.22 ug/L 1.22 2.44 1 10/20/22 21:06 VBW L644470 Benzo(b)fluoranthene <1.15 Ng/L 1.15 2.44 1 10/20/22 21:06 VBW L644470 Benzo(g,h,i)perylene <1.66 ug/L 1.66 2.44 1 10/20/22 21:06 VBW L644470 Benzo(k)fluoranthene <0.917 Ng/L 0.917 2.44 1 10/20/22 21:06 VBW L644470 Benzyl alcohol <3.67 ug/L 3.67 12.2 1 10/20/22 21:06 VBW L644470 Bis(2-Chloroethoxy)methane <0.528 Ng/L 0.528 6.10 1 10/20/22 21:06 VBW L644470 Bis(2-Chloroethyl)ether <0.545 ug/L 0.545 6.10 1 10/20/22 21:06 VBW L644470 Bis(2-Chloroisopropyl)ether <0.666 Ng/L 0.666 6.10 1 10/20/22 21:06 VBW L644470 Bis(2-ethylhexyl)phthalate <4.47 ug/L 4.47 6.10 1 10/20/22 21:06 VBW L644470 4-Bromophenyl phenyl ether <0.610 Ng/L 0.610 6.10 1 10/20/22 21:06 VBW L644470 Butyl benzyl phthalate <5.60 ug/L 5.60 6.10 1 10/20/22 21:06 VBW L644470 4-Chloro-3-methylphenol <0.613 Ng/L 0.613 6.10 1 10/20/22 21:06 VBW L644470 4-Chloroaniline <0.641 ug/L 0.641 6.10 1 10/20/22 21:06 VBW L644470 Chlorobenzilate <2.32 Ng/L 2.32 6.10 1 10/20/22 21:06 VBW L644470 2-Chloronaphthalene <0.580 ug/L 0.580 6.10 1 10/20/22 21:06 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 16 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2-Chlorophenol <0.897 Ng/L 0.897 6.10 1 10/20/22 21:06 VBW L644470 4-Chlorophenyl phenyl ether <0.584 ug/L 0.584 6.10 1 10/20/22 21:06 VBW L644470 Chrysene <0.891 Ng/L 0.891 2.44 1 10/20/22 21:06 VBW L644470 Dibenz(a,h)anthracene <0.307 ug/L 0.307 2.44 1 10/20/22 21:06 VBW L644470 Dibenzofuran <0.516 Ng/L 0.516 6.10 1 10/20/22 21:06 VBW L644470 1,2-Dichlorobenzene <0.767 ug/L 0.767 6.10 1 10/20/22 21:06 VBW L644470 1,3-Dichlorobenzene <0.599 Ng/L 0.599 6.10 1 10/20/22 21:06 VBW L644470 1,4-Dichlorobenzene 4.163 ug/L 0.707 6.10 1 10/20/22 21:06 VBW L644470 3,3'-Dichlorobenzidine <4.56 Ng/L 4.56 12.2 1 10/20/22 21:06 VBW L644470 2,4-Dichlorophenol <1.85 ug/L 1.85 6.10 1 10/20/22 21:06 VBW L644470 2,6-Dichlorophenol <0.857 Ng/L 0.857 6.10 1 10/20/22 21:06 VBW L644470 Diethyl phthalate <0.713 ug/L 0.713 6.10 1 10/20/22 21:06 VBW L644470 Dimethyl phthalate <0.622 Ng/L 0.622 6.10 1 10/20/22 21:06 VBW L644470 3,3' Dimethylbenzidine <2.29 u9/L 2.29 12.2 1 10/20/22 21:06 VBW L644470 2,4-Dimethyl phenol <0.822 M Ng/L 0.822 6.10 1 10/20/22 21:06 VBW L644470 Di-n-butyl phthalate <1.92 ug/L 1.92 6.10 1 10/20/22 21:06 VBW L644470 4,6- Din itro-2- methyl phenol <4.23 Ng/L 4.23 12.2 1 10/20/22 21:06 VBW L644470 2,4-Dinitrophenol <5.92 ug/L 5.92 12.2 1 10/20/22 21:06 VBW L644470 2,4-Dinitrotoluene <0.491 Ng/L 0.491 6.10 1 10/20/22 21:06 VBW L644470 2,6-Dinitrotoluene <0.503 ug/L 0.503 6.10 1 10/20/22 21:06 VBW L644470 Di-n-Octyl Phthalate <2.10 Ng/L 2.10 6.10 1 10/20/22 21:06 VBW L644470 Ethyl methanesulfonate <0.871 ug/L 0.871 6.10 1 10/20/22 21:06 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 17 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Fluoranthene <0.495 Ng/L 0.495 2.44 1 10/20/22 21:06 VBW L644470 Fluorene <0.541 ug/L 0.541 2.44 1 10/20/22 21:06 VBW L644470 Hexachlorobenzene <3.14 Ng/L 3.14 6.10 1 10/20/22 21:06 VBW L644470 Hexachlorobutadiene <0.494 ug/L 0.494 6.10 1 10/20/22 21:06 VBW L644470 Hexachlorocyclopentadiene <2.85 Ng/L 2.85 6.10 1 10/20/22 21:06 VBW L644470 Hexachloroethane <0.337 ug/L 0.337 6.10 1 10/20/22 21:06 VBW L644470 Indeno(1,2,3-cd)pyrene <1.23 Ng/L 1.23 2.44 1 10/20/22 21:06 VBW L644470 Isodrin <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW L644471 Isophorone <0.439 Ng/L 0.439 6.10 1 10/20/22 21:06 VBW L644470 Kepone <12.2 ug/L 12.2 12.2 1 10/20/22 21:06 VBW L644471 Methyl methanesulfonate <0.753 Ng/L 0.753 6.10 1 10/20/22 21:06 VBW L644470 2-Methylnaphthalene <0.591 ug/L 0.591 2.44 1 10/20/22 21:06 VBW L644470 2-Methylphenol <0.879 Ng/L 0.879 6.10 1 10/20/22 21:06 VBW L644470 3&4 Methylphenol <0.843 ug/L 0.843 6.10 1 10/20/22 21:06 VBW L644470 Naphthalene <0.590 Ng/L 0.590 2.44 1 10/20/22 21:06 VBW L644470 2-Nitroaniline <0.700 ug/L 0.700 6.10 1 10/20/22 21:06 VBW L644470 3-Nitroaniline <1.87 Ng/L 1.87 12.2 1 10/20/22 21:06 VBW L644470 4-Nitroaniline <0.902 ug/L 0.902 6.10 1 10/20/22 21:06 VBW L644470 Nitrobenzene <0.647 Ng/L 0.647 6.10 1 10/20/22 21:06 VBW L644470 2-Nitrophenol <0.739 ug/L 0.739 6.10 1 10/20/22 21:06 VBW L644470 4-Nitrophenol <1.70 Ng/L 1.70 12.2 1 10/20/22 21:06 VBW L644470 N-Nitrosodimethylamine <0.303 ug/L 0.303 6.10 1 10/20/22 21:06 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 18 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPORT OF ANAL YSIS Lab No : 90039 Matrix: Aqueous Sample ID: MW-01-20221004 Sampled: 10/4/2022 16:32 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch N-Nitrosodiphenylamine <0.955 Ng/L 0.955 12.2 1 10/20/22 21:06 VBW L644470 N-Nitrosodiethylamine <0.488 ug/L 0.488 6.10 1 10/20/22 21:06 VBW L644470 N-Nitroso-di-n-butylamine <0.917 Ng/L 0.917 6.10 1 10/20/22 21:06 VBW L644470 N-Nitroso-di-n-propylamine <0.407 ug/L 0.407 6.10 1 10/20/22 21:06 VBW L644470 Pentachlorobenzene <0.559 Ng/L 0.559 12.2 1 10/20/22 21:06 VBW L644470 Pentachloronitrobenzene <1.40 ug/L 1.40 6.10 1 10/20/22 21:06 VBW L644470 Pentachlorophenol <2.99 Ng/L 2.99 12.2 1 10/20/22 21:06 VBW L644470 Phenacetin <1.56 ug/L 1.56 6.10 1 10/20/22 21:06 VBW L644470 Phenanthrene <0.566 Ng/L 0.566 2.44 1 10/20/22 21:06 VBW L644470 Phenol <0.474 ug/L 0.474 6.10 1 10/20/22 21:06 VBW L644470 Pyrene <1.27 Ng/L 1.27 2.44 1 10/20/22 21:06 VBW L644470 1,2,4,5-Tetrachlorobenzene <0.386 ug/L 0.386 6.10 1 10/20/22 21:06 VBW L644470 2,3,4,6-Tetrachlorophenol <0.433 Ng/L 0.433 6.10 1 10/20/22 21:06 VBW L644470 1,2,4-Trichlorobenzene <0.588 ug/L 0.588 6.10 1 10/20/22 21:06 VBW L644470 2,4,5-Trichlorophenol <0.427 Ng/L 0.427 6.10 1 10/20/22 21:06 VBW L644470 2,4,6-Trichlorophenol <0.419 ug/L 0.419 6.10 1 10/20/22 21:06 VBW L644470 Surrogate: 2-Fluorobiphenyl 56.0 Limits: 24-93% 1 10/20/22 21:06 VBW L644470 Surrogate: 2-Fluorophenol 37.0 Limits: 10-44% 1 10/20/22 21:06 VBW L644470 Surrogate: Nitrobenzene-d5 56.4 Limits: 20-91% 1 10/20/22 21:06 VBW L644470 Surrogate: Phenol-d6 29.0 Limits: 7-32% 1 10/20/22 21:06 VBW L644470 Surrogate: 4-Terphenyl-d14 66.5 Limits: 35-126% 1 10/20/22 21:06 VBW L644470 Surrogate: 2,4,6-Tribromophenol 72.0 Limits: 39-110% 1 10/20/22 21:06 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 19 of 108 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-279-0018 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/01/2022 Received : 10/06/2022 Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane 5.58 Ng/L 0.139 2.00 1 10/07/22 12:58 TBL 8260D SIM 1,4-Naphthoquinone <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D 1-Naphthylamine <13.3 Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D 2-Acetylaminofluorene <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D 2-Naphthylamine <13.3 Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D 3-Methylcholanthrene <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D 4-Aminobiphenyl <13.3 Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D 5-Nitro-o-toluidine <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D 7,12-Di methylbenz(a)a nthracene <13.3 Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D Diallate <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D Hexachloropropene <13.3 Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D Isosafrole <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D Methapyrilene <13.4 Ng/L 13.4 26.7 1 10/20/22 21:27 VBW 8270D N-Nitrosomethylethylamine <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D N-Nitrosomorpholine <13.3 Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D N-Nitrosopyrrolidine <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D N-Nitrosopiperidine <13.3 Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D 0,0,0-Triethyl Phosphorothioate <0.438 ug/L 0.438 1.33 1 10/24/22 15:40 VBW 8270C o-Toluidine <13.3 Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D p-Dimethylaminoazobenzene <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D p-Phenylenediamine <13.3 M Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D Pronamide <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D Safrole <13.3 Ng/L 13.3 13.3 1 10/20/22 21:27 VBW 8270D Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 20 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90040 Sample ID: MW-03-20221004 Matrix: Aqueous Sampled: 10/4/2022 17:42 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Thionazine <0.438 Ng/L 0.438 1.33 1 10/24/2215:40 VBW 8270C Sulfide <0.83 mg/L 0.83 2.00 1 10/10/2211:00 SLO 4500S2F-2011 Antimony <0.680 Ng/L 0.680 2.00 1 10/10/22 19:25 EDV 6020B Arsenic <0.490 ug/L 0.490 1.00 1 10/10/22 19:25 EDV 6020B Barium 221 Ng/L 34.0 100 10 10/17/22 22:20 EDV 6020B Beryllium <0.240 ug/L 0.240 1.00 1 10/10/22 19:25 EDV 6020B Cadmium 0.4423 Ng/L 0.150 1.00 1 10/10/22 19:25 EDV 6020B Chromium 1.663 ug/L 1.00 2.00 1 10/10/22 19:25 EDV 6020B Cobalt 7.49 Ng/L 0.080 1.00 1 10/10/22 19:25 EDV 6020B Copper 5.00 ug/L 0.890 2.00 1 10/11/2216:42 EDV 6020B Lead <0.500 Ng/L 0.500 1.00 1 10/10/22 19:25 EDV 6020B Mercury (Total) <0.0700 ug/L 0.0700 0.200 1 10/11/22 16:19 EDV 7470A Nickel 6.84 Ng/L 0.720 2.00 1 10/10/22 19:25 EDV 6020B Selenium <2.30 ug/L 2.30 5.00 1 10/10/22 19:25 EDV 6020B Silver <0.130 Ng/L 0.130 1.00 1 10/10/22 19:25 EDV 6020B Tin <1.50 ug/L 1.50 5.00 1 10/10/22 19:25 EDV 6020B Thallium <0.280 Ng/L 0.280 2.00 1 10/10/22 19:25 EDV 6020B Vanadium <2.10 ug/L 2.10 5.00 1 10/10/22 19:25 EDV 6020B Zinc 13.23 Ng/L 3.90 20.0 1 10/10/22 19:25 EDV 6020B Qualifiers/ DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit H Beyond holding time M Minimum value Page 21 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0026 H Ng/L 0.0026 0.0500 10 10/21/22 05:28 VIC L644618 alpha-BHC <0.0026 H ug/L 0.0026 0.0500 10 10/21/22 05:28 VIC L644618 beta-BHC <0.0026 H Ng/L 0.0026 0.0500 10 10/21/22 05:28 VIC L644618 delta-BHC <0.0019 H ug/L 0.0019 0.0500 10 10/21/22 05:28 VIC L644618 Chlordane <0.0276 H Ng/L 0.0276 0.250 10 10/21/22 05:28 VIC L644618 alpha -Chlordane <0.0026 H ug/L 0.0026 0.0500 10 10/21/22 05:28 VIC L644618 gamma -Chlordane <0.0018 H Ng/L 0.0018 0.0500 10 10/21/22 05:28 VIC L644618 4,4'-DDD <0.0027 H ug/L 0.0027 0.0500 10 10/21/22 05:28 VIC L644618 4,4'-DDE <0.0026 H Ng/L 0.0026 0.0500 10 10/21/22 05:28 VIC L644618 4,4'-DDT <0.0043 H ug/L 0.0043 0.0500 10 10/21/22 05:28 VIC L644618 Dieldrin <0.0019 H Ng/L 0.0019 0.0500 10 10/21/22 05:28 VIC L644618 EndosulfanI <0.0019 H ug/L 0.0019 0.0500 10 10/21/22 05:28 VIC L644618 EndosulfanII <0.0035 H Ng/L 0.0035 0.0500 10 10/21/22 05:28 VIC L644618 Endosulfan Sulfate <0.0019 H ug/L 0.0019 0.0500 10 10/21/22 05:28 VIC L644618 Endrin <0.0019 H Ng/L 0.0019 0.0500 10 10/21/22 05:28 VIC L644618 Endrin Aldehyde <0.0019 H ug/L 0.0019 0.0500 10 10/21/22 05:28 VIC L644618 Endrin Ketone <0.0018 H Ng/L 0.0018 0.0500 10 10/21/22 05:28 VIC L644618 gamma-BHC <0.0022 H ug/L 0.0022 0.0500 10 10/21/22 05:28 VIC L644618 Heptachlor <0.0018 H Ng/L 0.0018 0.0500 10 10/21/22 05:28 VIC L644618 Heptachlor Epoxide <0.0018 H ug/L 0.0018 0.0500 10 10/21/22 05:28 VIC L644618 Methoxychlor <0.0018 H Ng/L 0.0018 0.0500 10 10/21/22 05:28 VIC L644618 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 22 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 Lab No : 90040 Sample ID: MW-03-20221004 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/4/2022 17:42 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0251 H Ng/L 0.0251 0.375 10 10/21/22 05:28 VIC L644618 Surrogate: Decachlorobiphenyl 107 Limits: 36-116% 10 10/21/22 05:28 L644618 Surrogate: Tetrachloro-m-xylene 106 Limits: 25-123% 10 10/21/22 05:28 L644618 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2445 Pg/L 0.2445 0.2941 1 10/14/22 23:37 VIC L643610 Dalapon <0.6058 Ng/L 0.6058 0.6471 1 10/14/22 23:37 VIC L643610 2,4-DB <0.1605 ug/L 0.1605 0.2941 1 10/14/22 23:37 VIC L643610 Dicam ba <0.06703 Ng/L 0.06703 0.01176 1 10/14/22 23:37 VIC L643610 Dichlorprop <0.09359 ug/L 0.09359 0.1176 1 10/14/22 23:37 VIC L643610 Dinoseb <0.03172 Ng/L 0.03172 0.1176 1 10/14/22 23:37 VIC L643610 MCPA <22.33 ug/L 22.33 58.82 1 10/14/22 23:37 VIC L643610 MCPP <13.82 Ng/L 13.82 58.82 1 10/14/22 23:37 VIC L643610 Picloram <0.05324 ug/L 0.05324 0.1176 1 10/14/22 23:37 VIC L643610 2,4,5-T <0.01178 Ng/L 0.01178 0.03529 1 10/14/22 23:37 VIC L643610 2,4,5-TP(Silvex) <0.01921 ug/L 0.01921 0.1176 1 10/14/22 23:37 VIC L643610 Surrogate: DCAA 73.24 Limits: 20-150% 1 10/14/22 23:37 L643610 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 23 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/11/22 05:27 MSA V24952 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/18/22 12:24 ANG V25258 Acrolein <2.00 Ng/L 2.00 5.00 1 10/11/22 05:27 MSA V24952 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/11/22 05:27 MSA V24952 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/18/22 12:24 ANG V25258 Benzene 0.553 ug/L 0.180 0.500 1 10/11/22 05:27 MSA V24952 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/11/22 05:27 MSA V24952 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/11/22 05:27 MSA V24952 Bromoform <1.50 Ng/L 1.50 5.00 1 10/11/22 05:27 MSA V24952 Bromomethane <0.280 ug/L 0.280 1.00 1 10/11/22 05:27 MSA V24952 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/11/22 05:27 MSA V24952 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/11/22 05:27 MSA V24952 Chlorobenzene 6.60 Ng/L 0.190 0.500 1 10/11/22 05:27 MSA V24952 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/11/22 05:27 MSA V24952 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/11/22 05:27 MSA V24952 Chloroform <0.220 ug/L 0.220 0.500 1 10/11/22 05:27 MSA V24952 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/11/22 05:27 MSA V24952 Chloroprene <0.450 ug/L 0.450 10.0 1 10/18/22 12:24 ANG V25258 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/11/22 05:27 MSA V24952 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/11/22 05:27 MSA V24952 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/11/22 05:27 MSA V24952 trans-1,4-Dichloro-2-butene <1.30 ug/L 1.30 10.0 1 10/11/22 05:27 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 24 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPORT OF ANAL YSIS Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene 0.2433 Ng/L 0.220 0.500 1 10/11/22 05:27 MSA V24952 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/11/22 05:27 MSA V24952 1,4-Dichlorobenzene 4.31 Ng/L 0.210 0.500 1 10/11/22 05:27 MSA V24952 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/11/22 05:27 MSA V24952 1,1-Dichloroethane 0.516 Ng/L 0.240 0.500 1 10/11/22 05:27 MSA V24952 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/11/22 05:27 MSA V24952 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/11/22 05:27 MSA V24952 cis- 1,2-Dich loroethene 1.14 ug/L 0.200 0.500 1 10/11/22 05:27 MSA V24952 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/11/22 05:27 MSA V24952 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/11/22 05:27 MSA V24952 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/11/22 05:27 MSA V24952 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/11/22 05:27 MSA V24952 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/11/22 05:27 MSA V24952 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/11/22 05:27 MSA V24952 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/11/22 05:27 MSA V24952 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/18/22 12:24 ANG V25258 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/11/22 05:27 MSA V24952 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/11/22 05:27 MSA V24952 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/11/22 05:27 MSA V24952 Iodomethane <0.054 ug/L 0.054 0.500 1 10/11/22 05:27 MSA V24952 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/11/22 05:27 MSA V24952 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/18/2212:24 ANG V25258 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 25 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/11/22 05:27 MSA V24952 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/11/22 05:27 MSA V24952 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/11/22 05:27 MSA V24952 Propionitrile <23.7 ug/L 23.7 10.0 1 10/18/2212:24 ANG V25258 Styrene <0.220 Ng/L 0.220 0.500 1 10/11/22 05:27 MSA V24952 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 05:27 MSA V24952 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/11/22 05:27 MSA V24952 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/11/22 05:27 MSA V24952 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/11/22 05:27 MSA V24952 Toluene <0.220 ug/L 0.220 0.500 1 10/11/22 05:27 MSA V24952 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/11/22 05:27 MSA V24952 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 05:27 MSA V24952 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/11/22 05:27 MSA V24952 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/11/22 05:27 MSA V24952 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/11/22 05:27 MSA V24952 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/11/22 05:27 MSA V24952 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/11/22 05:27 MSA V24952 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/11/22 05:27 MSA V24952 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/11/22 05:27 MSA V24952 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/11/22 05:27 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 26 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Analytical Method: 8270C Prep Method: 3510C Test <0.21 Ng/L 0.210 0.500 1 10/11/22 05:27 V24952 100 Limits: 80-124% 1 10/11/22 05:27 MSA V24952 97.8 Limits: 75-129% 1 10/11/22 05:27 MSA V24952 94.6 Limits: 63-136% 1 10/11/22 05:27 MSA V24952 96.6 Limits: 77-123% 1 10/11/22 05:27 MSA V24952 99.0 Limits:80-124% 1 10/18/2212:24 ANG V25258 101 Limits:75-129% 1 10/18/2212:24 ANG V25258 102 Limits:63-136% 1 10/18/2212:24 ANG V25258 101 Limits:77-123% 1 10/18/2212:24 ANG V25258 Prep Batch(es): L642252 10/10/22 15:46 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dimethoate <0.948 Disulfoton <0.619 Ethyl Parathion <0.755 Famphur <0.680 Methyl Parathion <1.07 Phorate <0.876 Surrogate: Tributyl phosphate Surrogate: Triphenyl phosphate Qualifiers/ DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit Pg/L 0.948 1.33 Ng/L 0.619 1.33 ug/L 0.755 1.33 Ng/L 0.680 1.33 ug/L 1.07 1.33 Ng/L 0.876 1.33 71.9 Limits: 50-150% 74.9 Limits: 50-150% 1 10/24/22 15:40 VBW L644472 1 10/24/22 15:40 VBW L644472 1 10/24/22 15:40 VBW L644472 1 10/24/22 15:40 VBW L644472 1 10/24/22 15:40 VBW L644472 1 10/24/22 15:40 VBW L644472 1 10/24/22 15:40 VBW 8270C 1 10/24/22 15:40 VBW 8270C H Beyond holding time M Minimum value Page 27 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,3-Dinitrobenzene <1.20 Ng/L 1.20 13.3 1 10/20/22 21:27 VBW L644470 1,3,5-Trinitrobenzene <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW L644471 Acenaphthene <0.563 Ng/L 0.563 2.67 1 10/20/22 21:27 VBW L644470 Acenaphthylene <0.572 ug/L 0.572 2.67 1 10/20/22 21:27 VBW L644470 Acetophenone <0.915 Ng/L 0.915 6.67 1 10/20/22 21:27 VBW L644470 Anthracene <0.623 ug/L 0.623 2.67 1 10/20/22 21:27 VBW L644470 Benzo(a)anthracene <0.570 Ng/L 0.570 2.67 1 10/20/22 21:27 VBW L644470 Benzo(a)pyrene <1.34 ug/L 1.34 2.67 1 10/20/22 21:27 VBW L644470 Benzo(b)fluoranthene <1.26 Ng/L 1.26 2.67 1 10/20/22 21:27 VBW L644470 Benzo(g,h,i)perylene <1.81 ug/L 1.81 2.67 1 10/20/22 21:27 VBW L644470 Benzo(k)fluoranthene <1.00 Ng/L 1.00 2.67 1 10/20/22 21:27 VBW L644470 Benzyl alcohol <4.00 ug/L 4.00 13.3 1 10/20/22 21:27 VBW L644470 Bis(2-Chloroethoxy)methane <0.577 Ng/L 0.577 6.67 1 10/20/22 21:27 VBW L644470 Bis(2-Chloroethyl)ether <0.596 ug/L 0.596 6.67 1 10/20/22 21:27 VBW L644470 Bis(2-Chloroisopropyl)ether <0.728 Ng/L 0.728 6.67 1 10/20/22 21:27 VBW L644470 Bis(2-ethylhexyl)phthalate <4.88 ug/L 4.88 6.67 1 10/20/22 21:27 VBW L644470 4-Bromophenyl phenyl ether <0.667 Ng/L 0.667 6.67 1 10/20/22 21:27 VBW L644470 Butyl benzyl phthalate <6.13 ug/L 6.13 6.67 1 10/20/22 21:27 VBW L644470 4-Chloro-3-methylphenol <0.671 Ng/L 0.671 6.67 1 10/20/22 21:27 VBW L644470 4-Chloroaniline <0.701 ug/L 0.701 6.67 1 10/20/22 21:27 VBW L644470 Chlorobenzilate <2.53 Ng/L 2.53 6.67 1 10/20/22 21:27 VBW L644470 2-Chloronaphthalene <0.634 ug/L 0.634 6.67 1 10/20/22 21:27 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 28 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2-Chlorophenol <0.981 Ng/L 0.981 6.67 1 10/20/22 21:27 VBW L644470 4-Chlorophenyl phenyl ether <0.638 ug/L 0.638 6.67 1 10/20/22 21:27 VBW L644470 Chrysene <0.975 Ng/L 0.975 2.67 1 10/20/22 21:27 VBW L644470 Dibenz(a,h)anthracene <0.336 ug/L 0.336 2.67 1 10/20/22 21:27 VBW L644470 Dibenzofuran <0.564 Ng/L 0.564 6.67 1 10/20/22 21:27 VBW L644470 1,2-Dichlorobenzene <0.839 ug/L 0.839 6.67 1 10/20/22 21:27 VBW L644470 1,3-Dichlorobenzene <0.654 Ng/L 0.654 6.67 1 10/20/22 21:27 VBW L644470 1,4-Dichlorobenzene 2.803 ug/L 0.773 6.67 1 10/20/22 21:27 VBW L644470 3,3'-Dichlorobenzidine <4.97 Ng/L 4.97 13.3 1 10/20/22 21:27 VBW L644470 2,4-Dichlorophenol <2.03 ug/L 2.03 6.67 1 10/20/22 21:27 VBW L644470 2,6-Dichlorophenol <0.937 Ng/L 0.937 6.67 1 10/20/22 21:27 VBW L644470 Diethyl phthalate <0.780 ug/L 0.780 6.67 1 10/20/22 21:27 VBW L644470 Dimethyl phthalate <0.680 Ng/L 0.680 6.67 1 10/20/22 21:27 VBW L644470 3,3' Dimethylbenzidine <2.50 ug/L 2.50 13.3 1 10/20/22 21:27 VBW L644470 2,4-Dimethyl phenol <0.899 M Ng/L 0.899 6.67 1 10/20/22 21:27 VBW L644470 Di-n-butyl phthalate <2.10 ug/L 2.10 6.67 1 10/20/22 21:27 VBW L644470 4,6- Din itro-2- methyl phenol <4.62 Ng/L 4.62 13.3 1 10/20/22 21:27 VBW L644470 2,4-Dinitrophenol <6.45 ug/L 6.45 13.3 1 10/20/22 21:27 VBW L644470 2,4-Dinitrotoluene <0.537 Ng/L 0.537 6.67 1 10/20/22 21:27 VBW L644470 2,6-Dinitrotoluene <0.550 ug/L 0.550 6.67 1 10/20/22 21:27 VBW L644470 Di-n-Octyl Phthalate <2.30 Ng/L 2.30 6.67 1 10/20/22 21:27 VBW L644470 Ethyl methanesulfonate <0.952 ug/L 0.952 6.67 1 10/20/22 21:27 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 29 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Fluoranthene <0.542 Ng/L 0.542 2.67 1 10/20/22 21:27 VBW L644470 Fluorene <0.592 ug/L 0.592 2.67 1 10/20/22 21:27 VBW L644470 Hexachlorobenzene <3.43 Ng/L 3.43 6.67 1 10/20/22 21:27 VBW L644470 Hexachlorobutadiene <0.540 ug/L 0.540 6.67 1 10/20/22 21:27 VBW L644470 Hexachlorocyclopentadiene <3.12 Ng/L 3.12 6.67 1 10/20/22 21:27 VBW L644470 Hexachloroethane <0.369 ug/L 0.369 6.67 1 10/20/22 21:27 VBW L644470 Indeno(1,2,3-cd)pyrene <1.35 Ng/L 1.35 2.67 1 10/20/22 21:27 VBW L644470 Isodrin <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW L644471 Isophorone <0.480 Ng/L 0.480 6.67 1 10/20/22 21:27 VBW L644470 Kepone <13.3 ug/L 13.3 13.3 1 10/20/22 21:27 VBW L644471 Methyl methanesulfonate <0.824 Ng/L 0.824 6.67 1 10/20/22 21:27 VBW L644470 2-Methylnaphthalene <0.647 ug/L 0.647 2.67 1 10/20/22 21:27 VBW L644470 2-Methylphenol <0.961 Ng/L 0.961 6.67 1 10/20/22 21:27 VBW L644470 3&4 Methylphenol <0.921 ug/L 0.921 6.67 1 10/20/22 21:27 VBW L644470 Naphthalene <0.646 Ng/L 0.646 2.67 1 10/20/22 21:27 VBW L644470 2-Nitroaniline <0.765 ug/L 0.765 6.67 1 10/20/22 21:27 VBW L644470 3-Nitroaniline <2.03 Ng/L 2.03 13.3 1 10/20/22 21:27 VBW L644470 4-Nitroaniline <0.987 ug/L 0.987 6.67 1 10/20/22 21:27 VBW L644470 Nitrobenzene <0.708 Ng/L 0.708 6.67 1 10/20/22 21:27 VBW L644470 2-Nitrophenol <0.808 ug/L 0.808 6.67 1 10/20/22 21:27 VBW L644470 4-Nitrophenol <1.85 Ng/L 1.85 13.3 1 10/20/22 21:27 VBW L644470 N-Nitrosodimethylamine <0.332 ug/L 0.332 6.67 1 10/20/22 21:27 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 30 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPORT OF ANAL YSIS Lab No : 90040 Matrix: Aqueous Sample ID: MW-03-20221004 Sampled: 10/4/2022 17:42 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch N-Nitrosodiphenylamine <1.04 Ng/L 1.04 13.3 1 10/20/22 21:27 VBW L644470 N-Nitrosodiethylamine <0.533 ug/L 0.533 6.67 1 10/20/22 21:27 VBW L644470 N-Nitroso-di-n-butylamine <1.00 Ng/L 1.00 6.67 1 10/20/22 21:27 VBW L644470 N-Nitroso-di-n-propylamine <0.445 ug/L 0.445 6.67 1 10/20/22 21:27 VBW L644470 Pentachlorobenzene <0.610 Ng/L 0.610 13.3 1 10/20/22 21:27 VBW L644470 Pentachloronitrobenzene <1.53 ug/L 1.53 6.67 1 10/20/22 21:27 VBW L644470 Pentachlorophenol <3.26 Ng/L 3.26 13.3 1 10/20/22 21:27 VBW L644470 Phenacetin <1.71 ug/L 1.71 6.67 1 10/20/22 21:27 VBW L644470 Phenanthrene <0.619 Ng/L 0.619 2.67 1 10/20/22 21:27 VBW L644470 Phenol <0.518 ug/L 0.518 6.67 1 10/20/22 21:27 VBW L644470 Pyrene <1.39 Ng/L 1.39 2.67 1 10/20/22 21:27 VBW L644470 1,2,4,5-Tetrachlorobenzene <0.422 ug/L 0.422 6.67 1 10/20/22 21:27 VBW L644470 2,3,4,6-Tetrachlorophenol <0.473 Ng/L 0.473 6.67 1 10/20/22 21:27 VBW L644470 1,2,4-Trichlorobenzene <0.642 ug/L 0.642 6.67 1 10/20/22 21:27 VBW L644470 2,4,5-Trichlorophenol <0.466 Ng/L 0.466 6.67 1 10/20/22 21:27 VBW L644470 2,4,6-Trichlorophenol <0.458 ug/L 0.458 6.67 1 10/20/22 21:27 VBW L644470 Surrogate: 2-Fluorobiphenyl 57.0 Limits: 24-93% 1 10/20/22 21:27 VBW L644470 Surrogate: 2-Fluorophenol 33.5 Limits: 10-44% 1 10/20/22 21:27 VBW L644470 Surrogate: Nitrobenzene-d5 57.6 Limits: 20-91% 1 10/20/22 21:27 VBW L644470 Surrogate: Phenol-d6 29.0 Limits: 7-32% 1 10/20/22 21:27 VBW L644470 Surrogate: 4-Terphenyl-d14 66.9 Limits: 35-126% 1 10/20/22 21:27 VBW L644470 Surrogate: 2,4,6-Tribromophenol 61.3 Limits: 39-110% 1 10/20/22 21:27 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 31 of 108 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-279-0018 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/01/2022 Received : 10/06/2022 Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane 11.0 Ng/L 0.139 2.00 1 10/07/22 13:23 TBL 8260D SIM 1,4-Naphthoquinone <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D 1-Naphthylamine <12.5 Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D 2-Acetylaminofluorene <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D 2-Naphthylamine <12.5 Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D 3-Methylcholanthrene <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D 4-Aminobiphenyl <12.5 Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D 5-Nitro-o-toluidine <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D 7,12-Di methylbenz(a)a nthracene <12.5 Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D Diallate <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D Hexachloropropene <12.5 Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D Isosafrole <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D Methapyrilene <12.5 Ng/L 12.5 25.0 1 10/20/22 21:47 VBW 8270D N-Nitrosomethylethylamine <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D N-Nitrosomorpholine <12.5 Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D N-Nitrosopyrrolidine <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D N-Nitrosopiperidine <12.5 Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D 0,0,0-Triethyl Phosphorothioate <0.412 ug/L 0.412 1.25 1 10/24/22 15:53 VBW 8270C o-Toluidine <12.5 Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D p-Dimethylaminoazobenzene <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D p-Phenylenediamine <12.5 M Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D Pronamide <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D Safrole <12.5 Ng/L 12.5 12.5 1 10/20/22 21:47 VBW 8270D Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 32 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90041 Sample ID: MW-04-20221004 Matrix: Aqueous Sampled: 10/4/2022 12:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Thionazine <0.412 Ng/L 0.412 1.25 1 10/24/2215:53 VBW 8270C Sulfide <0.83 mg/L 0.83 2.00 1 10/10/2211:00 SLO 4500S2F-2011 Antimony <0.680 Ng/L 0.680 2.00 1 10/10/22 19:32 EDV 6020B Arsenic <0.490 ug/L 0.490 1.00 1 10/10/22 19:32 EDV 6020B Barium 151 Ng/L 3.40 10.0 1 10/10/22 19:32 EDV 6020B Beryllium <0.240 ug/L 0.240 1.00 1 10/10/22 19:32 EDV 6020B Cadmium 0.2913 Ng/L 0.150 1.00 1 10/10/22 19:32 EDV 6020B Chromium <1.00 ug/L 1.00 2.00 1 10/10/22 19:32 EDV 6020B Cobalt 3.09 Ng/L 0.080 1.00 1 10/10/22 19:32 EDV 6020B Copper 2.27 ug/L 0.890 2.00 1 10/11/2216:49 EDV 6020B Lead <0.500 Ng/L 0.500 1.00 1 10/10/22 19:32 EDV 6020B Mercury (Total) 0.400 ug/L 0.0700 0.200 1 10/11/22 16:22 EDV 7470A Nickel 1.473 Ng/L 0.720 2.00 1 10/10/22 19:32 EDV 6020B Selenium <2.30 ug/L 2.30 5.00 1 10/10/22 19:32 EDV 6020B Silver 0.1683 Ng/L 0.130 1.00 1 10/10/22 19:32 EDV 6020B Tin <1.50 ug/L 1.50 5.00 1 10/10/22 19:32 EDV 6020B Thallium <0.280 Ng/L 0.280 2.00 1 10/10/22 19:32 EDV 6020B Vanadium <2.10 ug/L 2.10 5.00 1 10/10/22 19:32 EDV 6020B Zinc 4.693 Ng/L 3.90 20.0 1 10/10/22 19:32 EDV 6020B Qualifiers/ DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit H Beyond holding time M Minimum value Page 33 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0025 H Ng/L 0.0025 0.0470 10 10/21/22 05:55 VIC L644618 alpha-BHC <0.0024 H ug/L 0.0024 0.0470 10 10/21/22 05:55 VIC L644618 beta-BHC <0.0024 H Ng/L 0.0024 0.0470 10 10/21/22 05:55 VIC L644618 delta-BHC <0.0018 H ug/L 0.0018 0.0470 10 10/21/22 05:55 VIC L644618 Chlordane <0.0259 H Ng/L 0.0259 0.235 10 10/21/22 05:55 VIC L644618 alpha -Chlordane <0.0024 H ug/L 0.0024 0.0470 10 10/21/22 05:55 VIC L644618 gamma -Chlordane <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:55 VIC L644618 4,4'-DDD <0.0025 H ug/L 0.0025 0.0470 10 10/21/22 05:55 VIC L644618 4,4'-DDE <0.0025 H Ng/L 0.0025 0.0470 10 10/21/22 05:55 VIC L644618 4,4'-DDT <0.0041 H ug/L 0.0041 0.0470 10 10/21/22 05:55 VIC L644618 Dieldrin <0.0018 H Ng/L 0.0018 0.0470 10 10/21/22 05:55 VIC L644618 EndosulfanI <0.0018 H ug/L 0.0018 0.0470 10 10/21/22 05:55 VIC L644618 EndosulfanII <0.0033 H Ng/L 0.0033 0.0470 10 10/21/22 05:55 VIC L644618 Endosulfan Sulfate <0.0017 H ug/L 0.0017 0.0470 10 10/21/22 05:55 VIC L644618 Endrin <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:55 VIC L644618 Endrin Aldehyde <0.0017 H ug/L 0.0017 0.0470 10 10/21/22 05:55 VIC L644618 Endrin Ketone <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:55 VIC L644618 gamma-BHC <0.0021 H ug/L 0.0021 0.0470 10 10/21/22 05:55 VIC L644618 Heptachlor <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:55 VIC L644618 Heptachlor Epoxide <0.0017 H ug/L 0.0017 0.0470 10 10/21/22 05:55 VIC L644618 Methoxychlor <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 05:55 VIC L644618 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 34 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 Lab No : 90041 Sample ID: MW-04-20221004 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/4/2022 12:30 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0236 H N9/L 0.0236 0.353 10 10/21/22 05:55 VIC L644618 Surrogate: Decachlorobiphenyl 109 Limits: 36-116% 10 10/21/22 05:55 L644618 Surrogate: Tetrachloro-m-xylene 77.3 Limits: 25-123% 10 10/21/22 05:55 L644618 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2309 Pg/L 0.2309 0.2778 1 10/15/22 00:02 VIC L643610 Dalapon <0.5721 N9/L 0.5721 0.6111 1 10/15/22 00:02 VIC L643610 2,4-DB <0.1516 ug/L 0.1516 0.2778 1 10/15/22 00:02 VIC L643610 Dicam ba <0.06332 N9/L 0.06332 0.01111 1 10/15/22 00:02 VIC L643610 Dichlorprop <0.08842 ug/L 0.08842 0.1111 1 10/15/22 00:02 VIC L643610 Dinoseb <0.02997 N9/L 0.02997 0.1111 1 10/15/22 00:02 VIC L643610 MCPA <21.09 ug/L 21.09 55.56 1 10/15/22 00:02 VIC L643610 MCPP <13.06 N9/L 13.06 55.56 1 10/15/22 00:02 VIC L643610 Picloram <0.05030 ug/L 0.05030 0.1111 1 10/15/22 00:02 VIC L643610 2,4,5-T <0.01113 N9/L 0.01113 0.03333 1 10/15/22 00:02 VIC L643610 2,4,5-TP(Silvex) <0.01815 ug/L 0.01815 0.1111 1 10/15/22 00:02 VIC L643610 Surrogate: DCAA 74.05 Limits: 20-150% 1 10/15/22 00:02 L643610 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 35 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/11/22 04:06 MSA V24952 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/18/22 12:51 ANG V25258 Acrolein <2.00 Ng/L 2.00 5.00 1 10/11/22 04:06 MSA V24952 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/11/22 04:06 MSA V24952 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/18/22 12:51 ANG V25258 Benzene 0.3761 ug/L 0.180 0.500 1 10/11/22 04:06 MSA V24952 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/11/22 04:06 MSA V24952 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/11/22 04:06 MSA V24952 Bromoform <1.50 Ng/L 1.50 5.00 1 10/11/22 04:06 MSA V24952 Bromomethane <0.280 ug/L 0.280 1.00 1 10/11/22 04:06 MSA V24952 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/11/22 04:06 MSA V24952 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/11/22 04:06 MSA V24952 Chlorobenzene 1.60 Ng/L 0.190 0.500 1 10/11/22 04:06 MSA V24952 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/11/22 04:06 MSA V24952 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/11/22 04:06 MSA V24952 Chloroform <0.220 ug/L 0.220 0.500 1 10/11/22 04:06 MSA V24952 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/11/22 04:06 MSA V24952 Chloroprene <0.450 ug/L 0.450 10.0 1 10/18/22 12:51 ANG V25258 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/11/22 04:06 MSA V24952 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/11/22 04:06 MSA V24952 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/11/22 04:06 MSA V24952 trans-1,4-Dichloro-2-butene <1.30 ug/L 1.30 10.0 1 10/11/22 04:06 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 36 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene <0.220 Ng/L 0.220 0.500 1 10/11/22 04:06 MSA V24952 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/11/22 04:06 MSA V24952 1,4-Dichlorobenzene 2.57 Ng/L 0.210 0.500 1 10/11/22 04:06 MSA V24952 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/11/22 04:06 MSA V24952 1,1-Dichloroethane <0.240 Ng/L 0.240 0.500 1 10/11/22 04:06 MSA V24952 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/11/22 04:06 MSA V24952 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/11/22 04:06 MSA V24952 cis- 1,2-Dich loroethene 0.816 ug/L 0.200 0.500 1 10/11/22 04:06 MSA V24952 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/11/22 04:06 MSA V24952 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/11/22 04:06 MSA V24952 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/11/22 04:06 MSA V24952 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/11/22 04:06 MSA V24952 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/11/22 04:06 MSA V24952 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/11/22 04:06 MSA V24952 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/11/22 04:06 MSA V24952 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/18/22 12:51 ANG V25258 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/11/22 04:06 MSA V24952 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/11/22 04:06 MSA V24952 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/11/22 04:06 MSA V24952 Iodomethane <0.054 ug/L 0.054 0.500 1 10/11/22 04:06 MSA V24952 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/11/22 04:06 MSA V24952 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/18/2212:51 ANG V25258 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 37 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/11/22 04:06 MSA V24952 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/11/22 04:06 MSA V24952 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/11/22 04:06 MSA V24952 Propionitrile <23.7 ug/L 23.7 10.0 1 10/18/2212:51 ANG V25258 Styrene <0.220 Ng/L 0.220 0.500 1 10/11/22 04:06 MSA V24952 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 04:06 MSA V24952 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/11/22 04:06 MSA V24952 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/11/22 04:06 MSA V24952 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/11/22 04:06 MSA V24952 Toluene <0.220 ug/L 0.220 0.500 1 10/11/22 04:06 MSA V24952 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/11/22 04:06 MSA V24952 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 04:06 MSA V24952 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/11/22 04:06 MSA V24952 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/11/22 04:06 MSA V24952 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/11/22 04:06 MSA V24952 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/11/22 04:06 MSA V24952 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/11/22 04:06 MSA V24952 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/11/22 04:06 MSA V24952 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/11/22 04:06 MSA V24952 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/11/22 04:06 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 38 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Analytical Method: 8270C Prep Method: 3510C Test <0.21 N9/L 0.210 0.500 1 10/11/22 04:06 V24952 99.4 Limits: 80-124% 1 10/11/22 04:06 MSA V24952 96.8 Limits: 75-129% 1 10/11/22 04:06 MSA V24952 92.0 Limits: 63-136% 1 10/11/22 04:06 MSA V24952 96.8 Limits: 77-123% 1 10/11/22 04:06 MSA V24952 100 Limits:80-124% 1 10/18/2212:51 ANG V25258 99.0 Limits:75-129% 1 10/18/2212:51 ANG V25258 98.8 Limits:63-136% 1 10/18/2212:51 ANG V25258 102 Limits:77-123% 1 10/18/2212:51 ANG V25258 Prep Batch(es): L642252 10/10/22 15:46 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dimethoate <0.891 Disulfoton <0.582 Ethyl Parathion <0.710 Famphur <0.640 Methyl Parathion <1.01 Phorate <0.823 Surrogate: Tributyl phosphate Surrogate: Triphenyl phosphate Qualifiers/ DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit u9/L 0.891 1.25 N9/L 0.582 1.25 u9/L 0.710 1.25 N9/L 0.640 1.25 u9/L 1.01 1.25 N9/L 0.823 1.25 69.2 Limits: 50-150% 75.6 Limits: 50-150% 1 10/24/22 15:53 VBW L644472 1 10/24/22 15:53 VBW L644472 1 10/24/22 15:53 VBW L644472 1 10/24/22 15:53 VBW L644472 1 10/24/22 15:53 VBW L644472 1 10/24/22 15:53 VBW L644472 1 10/24/22 15:53 VBW 8270C 1 10/24/22 15:53 VBW 8270C H Beyond holding time M Minimum value Page 39 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,3-Dinitrobenzene <1.13 Ng/L 1.13 12.5 1 10/20/22 21:47 VBW L644470 1,3,5-Trinitrobenzene <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW L644471 Acenaphthene <0.527 Ng/L 0.527 2.50 1 10/20/22 21:47 VBW L644470 Acenaphthylene <0.536 ug/L 0.536 2.50 1 10/20/22 21:47 VBW L644470 Acetophenone <0.857 Ng/L 0.857 6.25 1 10/20/22 21:47 VBW L644470 Anthracene <0.583 ug/L 0.583 2.50 1 10/20/22 21:47 VBW L644470 Benzo(a)anthracene <0.533 Ng/L 0.533 2.50 1 10/20/22 21:47 VBW L644470 Benzo(a)pyrene <1.25 ug/L 1.25 2.50 1 10/20/22 21:47 VBW L644470 Benzo(b)fluoranthene <1.18 Ng/L 1.18 2.50 1 10/20/22 21:47 VBW L644470 Benzo(g,h,i)perylene <1.70 ug/L 1.70 2.50 1 10/20/22 21:47 VBW L644470 Benzo(k)fluoranthene <0.940 Ng/L 0.940 2.50 1 10/20/22 21:47 VBW L644470 Benzyl alcohol <3.76 ug/L 3.76 12.5 1 10/20/22 21:47 VBW L644470 Bis(2-Chloroethoxy)methane <0.541 Ng/L 0.541 6.25 1 10/20/22 21:47 VBW L644470 Bis(2-Chloroethyl)ether <0.558 ug/L 0.558 6.25 1 10/20/22 21:47 VBW L644470 Bis(2-Chloroisopropyl)ether <0.682 Ng/L 0.682 6.25 1 10/20/22 21:47 VBW L644470 Bis(2-ethylhexyl)phthalate <4.58 ug/L 4.58 6.25 1 10/20/22 21:47 VBW L644470 4-Bromophenyl phenyl ether <0.625 Ng/L 0.625 6.25 1 10/20/22 21:47 VBW L644470 Butyl benzyl phthalate <5.74 ug/L 5.74 6.25 1 10/20/22 21:47 VBW L644470 4-Chloro-3- methyl phenol <0.628 Ng/L 0.628 6.25 1 10/20/22 21:47 VBW L644470 4-Chloroaniline <0.657 ug/L 0.657 6.25 1 10/20/22 21:47 VBW L644470 Chlorobenzilate <2.38 Ng/L 2.38 6.25 1 10/20/22 21:47 VBW L644470 2-Chloronaphthalene <0.595 ug/L 0.595 6.25 1 10/20/22 21:47 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 40 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2-Chlorophenol <0.920 Ng/L 0.920 6.25 1 10/20/22 21:47 VBW L644470 4-Chlorophenyl phenyl ether <0.598 ug/L 0.598 6.25 1 10/20/22 21:47 VBW L644470 Chrysene <0.913 Ng/L 0.913 2.50 1 10/20/22 21:47 VBW L644470 Dibenz(a,h)anthracene <0.315 ug/L 0.315 2.50 1 10/20/22 21:47 VBW L644470 Dibenzofuran <0.528 Ng/L 0.528 6.25 1 10/20/22 21:47 VBW L644470 1,2-Dichlorobenzene <0.786 ug/L 0.786 6.25 1 10/20/22 21:47 VBW L644470 1,3-Dichlorobenzene <0.613 Ng/L 0.613 6.25 1 10/20/22 21:47 VBW L644470 1,4-Dichlorobenzene 1.81 J ug/L 0.725 6.25 1 10/20/22 21:47 VBW L644470 3,3'-Dichlorobenzidine <4.68 Ng/L 4.68 12.5 1 10/20/22 21:47 VBW L644470 2,4-Dichlorophenol <1.90 ug/L 1.90 6.25 1 10/20/22 21:47 VBW L644470 2,6-Dichlorophenol <0.878 Ng/L 0.878 6.25 1 10/20/22 21:47 VBW L644470 Diethyl phthalate 0.952 J ug/L 0.731 6.25 1 10/20/22 21:47 VBW L644470 Dimethyl phthalate <0.637 Ng/L 0.637 6.25 1 10/20/22 21:47 VBW L644470 3,3' Dimethylbenzidine <2.35 ug/L 2.35 12.5 1 10/20/22 21:47 VBW L644470 2,4-Dimethyl phenol <0.842 M Ng/L 0.842 6.25 1 10/20/22 21:47 VBW L644470 Di-n-butyl phthalate <1.97 ug/L 1.97 6.25 1 10/20/22 21:47 VBW L644470 4,6-Dinitro-2-methylphenol <4.34 Ng/L 4.34 12.5 1 10/20/22 21:47 VBW L644470 2,4-Dinitrophenol <6.06 ug/L 6.06 12.5 1 10/20/22 21:47 VBW L644470 2,4-Dinitrotoluene <0.503 Ng/L 0.503 6.25 1 10/20/22 21:47 VBW L644470 2,6-Dinitrotoluene <0.516 ug/L 0.516 6.25 1 10/20/22 21:47 VBW L644470 Di-n-Octyl Phthalate <2.15 Ng/L 2.15 6.25 1 10/20/22 21:47 VBW L644470 Ethyl methanesulfonate <0.892 ug/L 0.892 6.25 1 10/20/22 21:47 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 41 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Fluoranthene <0.507 Ng/L 0.507 2.50 1 10/20/22 21:47 VBW L644470 Fluorene <0.555 ug/L 0.555 2.50 1 10/20/22 21:47 VBW L644470 Hexachlorobenzene <3.21 Ng/L 3.21 6.25 1 10/20/22 21:47 VBW L644470 Hexachlorobutadiene <0.506 ug/L 0.506 6.25 1 10/20/22 21:47 VBW L644470 Hexachlorocyclopentadiene <2.93 Ng/L 2.93 6.25 1 10/20/22 21:47 VBW L644470 Hexachloroethane <0.346 ug/L 0.346 6.25 1 10/20/22 21:47 VBW L644470 Indeno(1,2,3-cd)pyrene <1.27 Ng/L 1.27 2.50 1 10/20/22 21:47 VBW L644470 Isodrin <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW L644471 Isophorone <0.450 Ng/L 0.450 6.25 1 10/20/22 21:47 VBW L644470 Kepone <12.5 ug/L 12.5 12.5 1 10/20/22 21:47 VBW L644471 Methyl methanesulfonate <0.772 Ng/L 0.772 6.25 1 10/20/22 21:47 VBW L644470 2-Methylnaphthalene <0.606 ug/L 0.606 2.50 1 10/20/22 21:47 VBW L644470 2-Methylphenol <0.901 Ng/L 0.901 6.25 1 10/20/22 21:47 VBW L644470 3&4 Methylphenol <0.863 ug/L 0.863 6.25 1 10/20/22 21:47 VBW L644470 Naphthalene <0.605 Ng/L 0.605 2.50 1 10/20/22 21:47 VBW L644470 2-Nitroaniline <0.717 ug/L 0.717 6.25 1 10/20/22 21:47 VBW L644470 3-Nitroaniline <1.91 Ng/L 1.91 12.5 1 10/20/22 21:47 VBW L644470 4-Nitroaniline <0.925 ug/L 0.925 6.25 1 10/20/22 21:47 VBW L644470 Nitrobenzene <0.663 Ng/L 0.663 6.25 1 10/20/22 21:47 VBW L644470 2-Nitrophenol <0.757 ug/L 0.757 6.25 1 10/20/22 21:47 VBW L644470 4-Nitrophenol <1.74 Ng/L 1.74 12.5 1 10/20/22 21:47 VBW L644470 N-Nitrosodimethylamine <0.311 ug/L 0.311 6.25 1 10/20/22 21:47 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 42 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPORT OF ANAL YSIS Lab No : 90041 Matrix: Aqueous Sample ID: MW-04-20221004 Sampled: 10/4/2022 12:30 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch N-Nitrosodiphenylamine <0.978 Ng/L 0.978 12.5 1 10/20/22 21:47 VBW L644470 N-Nitrosodiethylamine <0.500 ug/L 0.500 6.25 1 10/20/22 21:47 VBW L644470 N-Nitroso-di-n-butylamine <0.940 Ng/L 0.940 6.25 1 10/20/22 21:47 VBW L644470 N-Nitroso-di-n-propylamine <0.417 ug/L 0.417 6.25 1 10/20/22 21:47 VBW L644470 Pentachlorobenzene <0.573 Ng/L 0.573 12.5 1 10/20/22 21:47 VBW L644470 Pentachloronitrobenzene <1.44 ug/L 1.44 6.25 1 10/20/22 21:47 VBW L644470 Pentachlorophenol <3.06 Ng/L 3.06 12.5 1 10/20/22 21:47 VBW L644470 Phenacetin <1.60 ug/L 1.60 6.25 1 10/20/22 21:47 VBW L644470 Phenanthrene <0.580 Ng/L 0.580 2.50 1 10/20/22 21:47 VBW L644470 Phenol <0.486 ug/L 0.486 6.25 1 10/20/22 21:47 VBW L644470 Pyrene <1.30 Ng/L 1.30 2.50 1 10/20/22 21:47 VBW L644470 1,2,4,5-Tetrachlorobenzene <0.396 ug/L 0.396 6.25 1 10/20/22 21:47 VBW L644470 2,3,4,6-Tetrachlorophenol <0.443 Ng/L 0.443 6.25 1 10/20/22 21:47 VBW L644470 1,2,4-Trichlorobenzene <0.602 ug/L 0.602 6.25 1 10/20/22 21:47 VBW L644470 2,4,5-Trichlorophenol <0.437 Ng/L 0.437 6.25 1 10/20/22 21:47 VBW L644470 2,4,6-Trichlorophenol <0.430 ug/L 0.430 6.25 1 10/20/22 21:47 VBW L644470 Surrogate: 2-Fluorobiphenyl 55.2 Limits: 24-93% 1 10/20/22 21:47 VBW L644470 Surrogate: 2-Fluorophenol 37.8 Limits: 10-44% 1 10/20/22 21:47 VBW L644470 Surrogate: Nitrobenzene-d5 59.1 Limits: 20-91% 1 10/20/22 21:47 VBW L644470 Surrogate: Phenol-d6 30.5 Limits: 7-32% 1 10/20/22 21:47 VBW L644470 Surrogate: 4-Terphenyl-d14 65.0 Limits: 35-126% 1 10/20/22 21:47 VBW L644470 Surrogate: 2,4,6-Tribromophenol 72.8 Limits: 39-110% 1 10/20/22 21:47 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 43 of 108 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-279-0018 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/01/2022 Received : 10/06/2022 Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane <0.139 Ng/L 0.139 2.00 1 10/07/22 13:48 TBL 8260D SIM 1,4-Naphthoquinone <12.5 pg/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D 1-Naphthylamine <12.5 Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D 2-Acetylaminofluorene <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D 2-Naphthylamine <12.5 Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D 3-Methylcholanthrene <12.5 pg/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D 4-Aminobiphenyl <12.5 Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D 5-Nitro-o-toluidine <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D 7,12-Di methylbenz(a)a nthracene <12.5 Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D Diallate <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D Hexachloropropene <12.5 Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D Isosafrole <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D Methapyrilene <12.5 Ng/L 12.5 25.0 1 10/20/22 22:08 VBW 8270D N-Nitrosomethylethylamine <12.5 pg/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D N-Nitrosomorpholine <12.5 Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D N-Nitrosopyrrolidine <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D N-Nitrosopiperidine <12.5 Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D 0,0,0-Triethyl Phosphorothioate <0.412 pg/L 0.412 1.25 1 10/24/22 16:07 VBW 8270C o-Toluidine <12.5 Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D p-Dimethylaminoazobenzene <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D p-Phenylenediamine <12.5 M Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D Pronamide <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D Safrole <12.5 Ng/L 12.5 12.5 1 10/20/22 22:08 VBW 8270D Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 44 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90042 Sample ID: MW-06-20221004 Matrix: Aqueous Sampled: 10/4/2022 14:36 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Thionazine <0.412 Ng/L 0.412 1.25 1 10/24/2216:07 VBW 8270C Sulfide 1.10 J mg/L 0.83 2.00 1 10/10/22 11:00 SLO 4500S2F-2011 Antimony <0.680 Ng/L 0.680 2.00 1 10/10/22 19:38 EDV 6020B Arsenic <0.490 ug/L 0.490 1.00 1 10/10/22 19:38 EDV 6020B Barium 48.2 Ng/L 3.40 10.0 1 10/10/22 19:38 EDV 6020B Beryllium <0.240 ug/L 0.240 1.00 1 10/10/22 19:38 EDV 6020B Cadmium <0.150 Ng/L 0.150 1.00 1 10/10/22 19:38 EDV 6020B Chromium <1.00 ug/L 1.00 2.00 1 10/10/22 19:38 EDV 6020B Cobalt 8.07 Ng/L 0.080 1.00 1 10/10/22 19:38 EDV 6020B Copper 2.38 ug/L 0.890 2.00 1 10/11/2216:55 EDV 6020B Lead <0.500 Ng/L 0.500 1.00 1 10/10/22 19:38 EDV 6020B Mercury (Total) <0.0700 ug/L 0.0700 0.200 1 10/11/22 16:24 EDV 7470A Nickel 3.93 Ng/L 0.720 2.00 1 10/10/22 19:38 EDV 6020B Selenium <2.30 ug/L 2.30 5.00 1 10/10/22 19:38 EDV 6020B Silver <0.130 Ng/L 0.130 1.00 1 10/10/22 19:38 EDV 6020B Tin <1.50 ug/L 1.50 5.00 1 10/10/22 19:38 EDV 6020B Thallium 0.311 J Ng/L 0.280 2.00 1 10/10/22 19:38 EDV 6020B Vanadium <2.10 ug/L 2.10 5.00 1 10/10/22 19:38 EDV 6020B Zinc 14.3 J Ng/L 3.90 20.0 1 10/10/22 19:38 EDV 6020B Qualifiers/ DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit H Beyond holding time M Minimum value Page 45 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0025 H Ng/L 0.0025 0.0470 10 10/21/22 06:23 VIC L644618 alpha-BHC <0.0024 H ug/L 0.0024 0.0470 10 10/21/22 06:23 VIC L644618 beta-BHC <0.0024 H Ng/L 0.0024 0.0470 10 10/21/22 06:23 VIC L644618 delta-BHC <0.0018 H ug/L 0.0018 0.0470 10 10/21/22 06:23 VIC L644618 Chlordane <0.0259 H Ng/L 0.0259 0.235 10 10/21/22 06:23 VIC L644618 alpha -Chlordane <0.0024 H ug/L 0.0024 0.0470 10 10/21/22 06:23 VIC L644618 gamma -Chlordane <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 06:23 VIC L644618 4,4'-DDD <0.0025 H ug/L 0.0025 0.0470 10 10/21/22 06:23 VIC L644618 4,4'-DDE <0.0025 H Ng/L 0.0025 0.0470 10 10/21/22 06:23 VIC L644618 4,4'-DDT <0.0041 H ug/L 0.0041 0.0470 10 10/21/22 06:23 VIC L644618 Dieldrin <0.0018 H Ng/L 0.0018 0.0470 10 10/21/22 06:23 VIC L644618 EndosulfanI <0.0018 H ug/L 0.0018 0.0470 10 10/21/22 06:23 VIC L644618 EndosulfanII <0.0033 H Ng/L 0.0033 0.0470 10 10/21/22 06:23 VIC L644618 Endosulfan Sulfate <0.0017 H ug/L 0.0017 0.0470 10 10/21/22 06:23 VIC L644618 Endrin <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 06:23 VIC L644618 Endrin Aldehyde <0.0017 H ug/L 0.0017 0.0470 10 10/21/22 06:23 VIC L644618 Endrin Ketone <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 06:23 VIC L644618 gamma-BHC <0.0021 H ug/L 0.0021 0.0470 10 10/21/22 06:23 VIC L644618 Heptachlor <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 06:23 VIC L644618 Heptachlor Epoxide <0.0017 H ug/L 0.0017 0.0470 10 10/21/22 06:23 VIC L644618 Methoxychlor <0.0017 H Ng/L 0.0017 0.0470 10 10/21/22 06:23 VIC L644618 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 46 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 Lab No : 90042 Sample ID: MW-06-20221004 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/4/2022 14:36 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0236 H N9/L 0.0236 0.353 10 10/21/22 06:23 VIC L644618 Surrogate: Decachlorobiphenyl 108 Limits: 36-116% 10 10/21/22 06:23 L644618 Surrogate: Tetrachloro-m-xylene 78.9 Limits: 25-123% 10 10/21/22 06:23 L644618 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2309 Pg/L 0.2309 0.2778 1 10/15/22 00:27 VIC L643610 Dalapon <0.5721 N9/L 0.5721 0.6111 1 10/15/22 00:27 VIC L643610 2,4-DB <0.1516 ug/L 0.1516 0.2778 1 10/15/22 00:27 VIC L643610 Dicam ba <0.06332 N9/L 0.06332 0.01111 1 10/15/22 00:27 VIC L643610 Dichlorprop <0.08842 ug/L 0.08842 0.1111 1 10/15/22 00:27 VIC L643610 Dinoseb <0.02997 N9/L 0.02997 0.1111 1 10/15/22 00:27 VIC L643610 MCPA <21.09 ug/L 21.09 55.56 1 10/15/22 00:27 VIC L643610 MCPP <13.06 N9/L 13.06 55.56 1 10/15/22 00:27 VIC L643610 Picloram <0.05030 ug/L 0.05030 0.1111 1 10/15/22 00:27 VIC L643610 2,4,5-T <0.01113 N9/L 0.01113 0.03333 1 10/15/22 00:27 VIC L643610 2,4,5-TP(Silvex) <0.01815 ug/L 0.01815 0.1111 1 10/15/22 00:27 VIC L643610 Surrogate: DCAA 58.32 Limits: 20-150% 1 10/15/22 00:27 L643610 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 47 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/11/22 04:33 MSA V24952 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/18/2213:18 ANG V25258 Acrolein <2.00 Ng/L 2.00 5.00 1 10/11/22 04:33 MSA V24952 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/11/22 04:33 MSA V24952 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/18/22 13:18 ANG V25258 Benzene <0.180 ug/L 0.180 0.500 1 10/11/22 04:33 MSA V24952 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/11/22 04:33 MSA V24952 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/11/22 04:33 MSA V24952 Bromoform <1.50 Ng/L 1.50 5.00 1 10/11/22 04:33 MSA V24952 Bromomethane <0.280 ug/L 0.280 1.00 1 10/11/22 04:33 MSA V24952 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/11/22 04:33 MSA V24952 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/11/22 04:33 MSA V24952 Chlorobenzene <0.190 Ng/L 0.190 0.500 1 10/11/22 04:33 MSA V24952 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/11/22 04:33 MSA V24952 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/11/22 04:33 MSA V24952 Chloroform <0.220 ug/L 0.220 0.500 1 10/11/22 04:33 MSA V24952 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/11/22 04:33 MSA V24952 Chloroprene <0.450 ug/L 0.450 10.0 1 10/18/2213:18 ANG V25258 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/11/22 04:33 MSA V24952 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/11/22 04:33 MSA V24952 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/11/22 04:33 MSA V24952 trans-1,4-Dichloro-2-butene <1.30 pg/L 1.30 10.0 1 10/11/22 04:33 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 48 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPORT OF ANAL YSIS Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene <0.220 Ng/L 0.220 0.500 1 10/11/22 04:33 MSA V24952 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/11/22 04:33 MSA V24952 1,4-Dichlorobenzene 0.728 Ng/L 0.210 0.500 1 10/11/22 04:33 MSA V24952 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/11/22 04:33 MSA V24952 1,1-Dichloroethane 0.858 Ng/L 0.240 0.500 1 10/11/22 04:33 MSA V24952 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/11/22 04:33 MSA V24952 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/11/22 04:33 MSA V24952 cis- 1,2-Dich loroethene 0.622 ug/L 0.200 0.500 1 10/11/22 04:33 MSA V24952 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/11/22 04:33 MSA V24952 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/11/22 04:33 MSA V24952 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/11/22 04:33 MSA V24952 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/11/22 04:33 MSA V24952 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/11/22 04:33 MSA V24952 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/11/22 04:33 MSA V24952 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/11/22 04:33 MSA V24952 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/18/22 13:18 ANG V25258 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/11/22 04:33 MSA V24952 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/11/22 04:33 MSA V24952 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/11/22 04:33 MSA V24952 Iodomethane <0.054 ug/L 0.054 0.500 1 10/11/22 04:33 MSA V24952 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/11/22 04:33 MSA V24952 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/18/2213:18 ANG V25258 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 49 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/11/22 04:33 MSA V24952 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/11/22 04:33 MSA V24952 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/11/22 04:33 MSA V24952 Propionitrile <23.7 ug/L 23.7 10.0 1 10/18/2213:18 ANG V25258 Styrene <0.220 Ng/L 0.220 0.500 1 10/11/22 04:33 MSA V24952 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 04:33 MSA V24952 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/11/22 04:33 MSA V24952 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/11/22 04:33 MSA V24952 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/11/22 04:33 MSA V24952 Toluene <0.220 ug/L 0.220 0.500 1 10/11/22 04:33 MSA V24952 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/11/22 04:33 MSA V24952 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 04:33 MSA V24952 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/11/22 04:33 MSA V24952 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/11/22 04:33 MSA V24952 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/11/22 04:33 MSA V24952 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/11/22 04:33 MSA V24952 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/11/22 04:33 MSA V24952 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/11/22 04:33 MSA V24952 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/11/22 04:33 MSA V24952 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/11/22 04:33 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 50 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Analytical Method: 8270C Prep Method: 3510C Test <0.21 N9/L 0.210 0.500 1 10/11/22 04:33 V24952 100 Limits: 80-124% 1 10/11/22 04:33 MSA V24952 98.2 Limits: 75-129% 1 10/11/22 04:33 MSA V24952 94.0 Limits: 63-136% 1 10/11/22 04:33 MSA V24952 96.0 Limits: 77-123% 1 10/11/22 04:33 MSA V24952 119 Limits:80-124% 1 10/18/2213:18 ANG V25258 95.4 Limits:75-129% 1 10/18/2213:18 ANG V25258 93.4 Limits:63-136% 1 10/18/2213:18 ANG V25258 105 Limits:77-123% 1 10/18/2213:18 ANG V25258 Prep Batch(es): L642252 10/10/22 15:46 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dimethoate <0.891 Disulfoton <0.582 Ethyl Parathion <0.710 Famphur <0.640 Methyl Parathion <1.01 Phorate <0.823 Surrogate: Tributyl phosphate Surrogate: Triphenyl phosphate Qualifiers/ DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit u9/L 0.891 1.25 N9/L 0.582 1.25 u9/L 0.710 1.25 N9/L 0.640 1.25 u9/L 1.01 1.25 N9/L 0.823 1.25 64.8 Limits: 50-150% 69.6 Limits: 50-150% 1 10/24/22 16:07 VBW L644472 1 10/24/22 16:07 VBW L644472 1 10/24/22 16:07 VBW L644472 1 10/24/22 16:07 VBW L644472 1 10/24/22 16:07 VBW L644472 1 10/24/22 16:07 VBW L644472 1 10/24/22 16:07 VBW 8270C 1 10/24/22 16:07 VBW 8270C H Beyond holding time M Minimum value Page 51 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,3-Dinitrobenzene <1.13 Ng/L 1.13 12.5 1 10/20/22 22:08 VBW L644470 1,3,5-Trinitrobenzene <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW L644471 Acenaphthene <0.527 Ng/L 0.527 2.50 1 10/20/22 22:08 VBW L644470 Acenaphthylene <0.536 ug/L 0.536 2.50 1 10/20/22 22:08 VBW L644470 Acetophenone <0.857 Ng/L 0.857 6.25 1 10/20/22 22:08 VBW L644470 Anthracene <0.583 ug/L 0.583 2.50 1 10/20/22 22:08 VBW L644470 Benzo(a)anthracene <0.533 Ng/L 0.533 2.50 1 10/20/22 22:08 VBW L644470 Benzo(a)pyrene <1.25 ug/L 1.25 2.50 1 10/20/22 22:08 VBW L644470 Benzo(b)fluoranthene <1.18 Ng/L 1.18 2.50 1 10/20/22 22:08 VBW L644470 Benzo(g,h,i)perylene <1.70 ug/L 1.70 2.50 1 10/20/22 22:08 VBW L644470 Benzo(k)fluoranthene <0.940 Ng/L 0.940 2.50 1 10/20/22 22:08 VBW L644470 Benzyl alcohol <3.76 ug/L 3.76 12.5 1 10/20/22 22:08 VBW L644470 Bis(2-Chloroethoxy)methane <0.541 Ng/L 0.541 6.25 1 10/20/22 22:08 VBW L644470 Bis(2-Chloroethyl)ether <0.558 ug/L 0.558 6.25 1 10/20/22 22:08 VBW L644470 Bis(2-Chloroisopropyl)ether <0.682 Ng/L 0.682 6.25 1 10/20/22 22:08 VBW L644470 Bis(2-ethylhexyl)phthalate <4.58 ug/L 4.58 6.25 1 10/20/22 22:08 VBW L644470 4-Bromophenyl phenyl ether <0.625 Ng/L 0.625 6.25 1 10/20/22 22:08 VBW L644470 Butyl benzyl phthalate <5.74 ug/L 5.74 6.25 1 10/20/22 22:08 VBW L644470 4-Chloro-3- methyl phenol <0.628 Ng/L 0.628 6.25 1 10/20/22 22:08 VBW L644470 4-Chloroaniline <0.657 ug/L 0.657 6.25 1 10/20/22 22:08 VBW L644470 Chlorobenzilate <2.38 Ng/L 2.38 6.25 1 10/20/22 22:08 VBW L644470 2-Chloronaphthalene <0.595 ug/L 0.595 6.25 1 10/20/22 22:08 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 52 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2-Chlorophenol <0.920 Ng/L 0.920 6.25 1 10/20/22 22:08 VBW L644470 4-Chlorophenyl phenyl ether <0.598 ug/L 0.598 6.25 1 10/20/22 22:08 VBW L644470 Chrysene <0.913 Ng/L 0.913 2.50 1 10/20/22 22:08 VBW L644470 Dibenz(a,h)anthracene <0.315 ug/L 0.315 2.50 1 10/20/22 22:08 VBW L644470 Dibenzofuran <0.528 Ng/L 0.528 6.25 1 10/20/22 22:08 VBW L644470 1,2-Dichlorobenzene <0.786 ug/L 0.786 6.25 1 10/20/22 22:08 VBW L644470 1,3-Dichlorobenzene <0.613 Ng/L 0.613 6.25 1 10/20/22 22:08 VBW L644470 1,4-Dichlorobenzene <0.725 ug/L 0.725 6.25 1 10/20/22 22:08 VBW L644470 3,3'-Dichlorobenzidine <4.68 Ng/L 4.68 12.5 1 10/20/22 22:08 VBW L644470 2,4-Dichlorophenol <1.90 ug/L 1.90 6.25 1 10/20/22 22:08 VBW L644470 2,6-Dichlorophenol <0.878 Ng/L 0.878 6.25 1 10/20/22 22:08 VBW L644470 Diethyl phthalate <0.731 ug/L 0.731 6.25 1 10/20/22 22:08 VBW L644470 Dimethyl phthalate <0.637 Ng/L 0.637 6.25 1 10/20/22 22:08 VBW L644470 3,3' Dimethylbenzidine <2.35 ug/L 2.35 12.5 1 10/20/22 22:08 VBW L644470 2,4-Dimethyl phenol <0.842 M Ng/L 0.842 6.25 1 10/20/22 22:08 VBW L644470 Di-n-butyl phthalate <1.97 ug/L 1.97 6.25 1 10/20/22 22:08 VBW L644470 4,6- Din itro-2- methyl phenol <4.34 Ng/L 4.34 12.5 1 10/20/22 22:08 VBW L644470 2,4-Dinitrophenol <6.06 ug/L 6.06 12.5 1 10/20/22 22:08 VBW L644470 2,4-Dinitrotoluene <0.503 Ng/L 0.503 6.25 1 10/20/22 22:08 VBW L644470 2,6-Dinitrotoluene <0.516 ug/L 0.516 6.25 1 10/20/22 22:08 VBW L644470 Di-n-Octyl Phthalate <2.15 Ng/L 2.15 6.25 1 10/20/22 22:08 VBW L644470 Ethyl methanesulfonate <0.892 ug/L 0.892 6.25 1 10/20/22 22:08 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 53 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Fluoranthene <0.507 Ng/L 0.507 2.50 1 10/20/22 22:08 VBW L644470 Fluorene <0.555 ug/L 0.555 2.50 1 10/20/22 22:08 VBW L644470 Hexachlorobenzene <3.21 Ng/L 3.21 6.25 1 10/20/22 22:08 VBW L644470 Hexachlorobutadiene <0.506 ug/L 0.506 6.25 1 10/20/22 22:08 VBW L644470 Hexachlorocyclopentadiene <2.93 Ng/L 2.93 6.25 1 10/20/22 22:08 VBW L644470 Hexachloroethane <0.346 ug/L 0.346 6.25 1 10/20/22 22:08 VBW L644470 Indeno(1,2,3-cd)pyrene <1.27 Ng/L 1.27 2.50 1 10/20/22 22:08 VBW L644470 Isodrin <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW L644471 Isophorone <0.450 Ng/L 0.450 6.25 1 10/20/22 22:08 VBW L644470 Kepone <12.5 ug/L 12.5 12.5 1 10/20/22 22:08 VBW L644471 Methyl methanesulfonate <0.772 Ng/L 0.772 6.25 1 10/20/22 22:08 VBW L644470 2-Methylnaphthalene <0.606 ug/L 0.606 2.50 1 10/20/22 22:08 VBW L644470 2-Methylphenol <0.901 Ng/L 0.901 6.25 1 10/20/22 22:08 VBW L644470 3&4 Methylphenol <0.863 ug/L 0.863 6.25 1 10/20/22 22:08 VBW L644470 Naphthalene <0.605 Ng/L 0.605 2.50 1 10/20/22 22:08 VBW L644470 2-Nitroaniline <0.717 ug/L 0.717 6.25 1 10/20/22 22:08 VBW L644470 3-Nitroaniline <1.91 Ng/L 1.91 12.5 1 10/20/22 22:08 VBW L644470 4-Nitroaniline <0.925 ug/L 0.925 6.25 1 10/20/22 22:08 VBW L644470 Nitrobenzene <0.663 Ng/L 0.663 6.25 1 10/20/22 22:08 VBW L644470 2-Nitrophenol <0.757 ug/L 0.757 6.25 1 10/20/22 22:08 VBW L644470 4-Nitrophenol <1.74 Ng/L 1.74 12.5 1 10/20/22 22:08 VBW L644470 N-Nitrosodimethylamine <0.311 ug/L 0.311 6.25 1 10/20/22 22:08 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 54 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPORT OF ANAL YSIS Lab No : 90042 Matrix: Aqueous Sample ID: MW-06-20221004 Sampled: 10/4/2022 14:36 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch N-Nitrosodiphenylamine <0.978 Ng/L 0.978 12.5 1 10/20/22 22:08 VBW L644470 N-Nitrosodiethylamine <0.500 ug/L 0.500 6.25 1 10/20/22 22:08 VBW L644470 N-Nitroso-di-n-butylamine <0.940 Ng/L 0.940 6.25 1 10/20/22 22:08 VBW L644470 N-Nitroso-di-n-propylamine <0.417 ug/L 0.417 6.25 1 10/20/22 22:08 VBW L644470 Pentachlorobenzene <0.573 Ng/L 0.573 12.5 1 10/20/22 22:08 VBW L644470 Pentachloronitrobenzene <1.44 ug/L 1.44 6.25 1 10/20/22 22:08 VBW L644470 Pentachlorophenol <3.06 Ng/L 3.06 12.5 1 10/20/22 22:08 VBW L644470 Phenacetin <1.60 ug/L 1.60 6.25 1 10/20/22 22:08 VBW L644470 Phenanthrene <0.580 Ng/L 0.580 2.50 1 10/20/22 22:08 VBW L644470 Phenol <0.486 ug/L 0.486 6.25 1 10/20/22 22:08 VBW L644470 Pyrene <1.30 Ng/L 1.30 2.50 1 10/20/22 22:08 VBW L644470 1,2,4,5-Tetrachlorobenzene <0.396 ug/L 0.396 6.25 1 10/20/22 22:08 VBW L644470 2,3,4,6-Tetrachlorophenol <0.443 Ng/L 0.443 6.25 1 10/20/22 22:08 VBW L644470 1,2,4-Trichlorobenzene <0.602 ug/L 0.602 6.25 1 10/20/22 22:08 VBW L644470 2,4,5-Trichlorophenol <0.437 Ng/L 0.437 6.25 1 10/20/22 22:08 VBW L644470 2,4,6-Trichlorophenol <0.430 ug/L 0.430 6.25 1 10/20/22 22:08 VBW L644470 Surrogate: 2-Fluorobiphenyl 51.8 Limits: 24-93% 1 10/20/22 22:08 VBW L644470 Surrogate: 2-Fluorophenol 32.2 Limits: 10-44% 1 10/20/22 22:08 VBW L644470 Surrogate: Nitrobenzene-d5 52.3 Limits: 20-91% 1 10/20/22 22:08 VBW L644470 Surrogate: Phenol-d6 25.4 Limits: 7-32% 1 10/20/22 22:08 VBW L644470 Surrogate: 4-Terphenyl-d14 55.7 Limits: 35-126% 1 10/20/22 22:08 VBW L644470 Surrogate: 2,4,6-Tribromophenol 63.1 Limits: 39-110% 1 10/20/22 22:08 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 55 of 108 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-279-0018 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/01/2022 Received : 10/06/2022 Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Hardness 40003 Ng/L 1140 10000 1 10/24/22 11:30 CLB 2340C-2011 1,4-Dioxane <0.139 ug/L 0.139 2.00 1 10/07/22 14:13 TBL 8260D SIM 1,4-Naphthoquinone <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D 1-Naphthylamine <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D 2-Acetylaminofluorene <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D 2-Naphthylamine <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D 3-Methylcholanthrene <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D 4-Aminobiphenyl <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D 5-Nitro-o-toluidine <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D 7,12-Dimethyl benz(a)anth racene <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D Diallate <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D Hexachloropropene <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D Isosafrole <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D Methapyrilene <10.0 ug/L 10.0 20.0 1 10/20/22 22:28 VBW 8270D N-Nitrosomethylethylamine <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D N-Nitrosomorpholine <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D N-Nitrosopyrrolidine <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D N-Nitrosopiperidine <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D 0,0,0-Triethyl Phosphorothioate <0.389 Ng/L 0.389 1.18 1 10/24/22 16:20 VBW 8270C o-Toluidine <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D p-Dimethylaminoazobenzene <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D p-Phenylenediamine <10.0 M ug/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D Pronamide <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 56 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Safrole <10.0 Ng/L 10.0 10.0 1 10/20/22 22:28 VBW 8270D Thionazine <0.389 ug/L 0.389 1.18 1 10/24/2216:20 VBW 8270C Sulfide <0.83 mg/L 0.83 2.00 1 10/10/2211:00 SLO 4500S2F-2011 Antimony <3.40 ug/L 3.40 10.0 5 10/10/22 19:52 EDV 6020B Arsenic <2.45 Ng/L 2.45 5.00 5 10/10/22 19:52 EDV 6020B Barium <17.0 ug/L 17.0 50.0 5 10/10/22 19:52 EDV 6020B Beryllium <1.20 Ng/L 1.20 5.00 5 10/10/22 19:52 EDV 6020B Cadmium <0.750 ug/L 0.750 5.00 5 10/10/22 19:52 EDV 6020B Chromium <5.00 Ng/L 5.00 10.0 5 10/10/22 19:52 EDV 6020B Cobalt <0.400 ug/L 0.400 5.00 5 10/10/22 19:52 EDV 6020B Copper 19.2 Ng/L 4.45 10.0 5 10/11/22 17:09 EDV 6020B Lead <2.50 ug/L 2.50 5.00 5 10/10/22 19:52 EDV 6020B Mercury (Total) <0.0700 Ng/L 0.0700 0.200 1 10/24/22 15:09 EDV 7470A Nickel <3.60 ug/L 3.60 10.0 5 10/10/22 19:52 EDV 6020B Selenium <11.5 Ng/L 11.5 25.0 5 10/10/22 19:52 EDV 6020B Silver <0.650 ug/L 0.650 5.00 5 10/10/22 19:52 EDV 6020B Tin <7.50 Ng/L 7.50 25.0 5 10/10/22 19:52 EDV 6020B Thallium <1.40 ug/L 1.40 10.0 5 10/10/22 19:52 EDV 6020B Vanadium <10.5 Ng/L 10.5 25.0 5 10/10/22 19:52 EDV 6020B Zinc 80.53 ug/L 19.5 100 5 10/10/22 19:52 EDV 6020B Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 57 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0023 H Ng/L 0.0023 0.0444 10 10/21/22 06:50 VIC L644618 alpha-BHC <0.0023 H ug/L 0.0023 0.0444 10 10/21/22 06:50 VIC L644618 beta-BHC <0.0023 H Ng/L 0.0023 0.0444 10 10/21/22 06:50 VIC L644618 delta-BHC <0.0017 H ug/L 0.0017 0.0444 10 10/21/22 06:50 VIC L644618 Chlordane <0.0245 H Ng/L 0.0245 0.222 10 10/21/22 06:50 VIC L644618 alpha -Chlordane <0.0023 H ug/L 0.0023 0.0444 10 10/21/22 06:50 VIC L644618 gamma -Chlordane <0.0016 H Ng/L 0.0016 0.0444 10 10/21/22 06:50 VIC L644618 4,4'-DDD <0.0023 H ug/L 0.0023 0.0444 10 10/21/22 06:50 VIC L644618 4,4'-DDE <0.0023 H Ng/L 0.0023 0.0444 10 10/21/22 06:50 VIC L644618 4,4'-DDT <0.0038 H ug/L 0.0038 0.0444 10 10/21/22 06:50 VIC L644618 Dieldrin <0.0017 H Ng/L 0.0017 0.0444 10 10/21/22 06:50 VIC L644618 EndosulfanI <0.0017 H ug/L 0.0017 0.0444 10 10/21/22 06:50 VIC L644618 EndosulfanII <0.0031 H Ng/L 0.0031 0.0444 10 10/21/22 06:50 VIC L644618 Endosulfan Sulfate <0.0016 H ug/L 0.0016 0.0444 10 10/21/22 06:50 VIC L644618 Endrin <0.0016 H Ng/L 0.0016 0.0444 10 10/21/22 06:50 VIC L644618 Endrin Aldehyde <0.0016 H ug/L 0.0016 0.0444 10 10/21/22 06:50 VIC L644618 Endrin Ketone <0.0016 H Ng/L 0.0016 0.0444 10 10/21/22 06:50 VIC L644618 gamma-BHC <0.0020 H ug/L 0.0020 0.0444 10 10/21/22 06:50 VIC L644618 Heptachlor <0.0016 H Ng/L 0.0016 0.0444 10 10/21/22 06:50 VIC L644618 Heptachlor Epoxide <0.0016 H ug/L 0.0016 0.0444 10 10/21/22 06:50 VIC L644618 Methoxychlor <0.0016 H Ng/L 0.0016 0.0444 10 10/21/22 06:50 VIC L644618 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 58 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 Lab No : 90043 Sample ID: SW-03-20221004 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/4/2022 10:40 Analytical Method: 8081B Prep Batch(es): L644399 10/20/22 15:01 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0223 H Ng/L 0.0223 0.333 10 10/21/22 06:50 VIC L644618 Surrogate: Decachlorobiphenyl 104 Limits: 36-116% 10 10/21/22 06:50 L644618 Surrogate: Tetrachloro-m-xylene 82.2 Limits: 25-123% 10 10/21/22 06:50 L644618 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2309 Pg/L 0.2309 0.2778 1 10/15/22 00:52 VIC L643610 Dalapon <0.5721 Ng/L 0.5721 0.6111 1 10/15/22 00:52 VIC L643610 2,4-DB <0.1516 ug/L 0.1516 0.2778 1 10/15/22 00:52 VIC L643610 Dicam ba <0.06332 Ng/L 0.06332 0.01111 1 10/15/22 00:52 VIC L643610 Dichlorprop <0.08842 ug/L 0.08842 0.1111 1 10/15/22 00:52 VIC L643610 Dinoseb <0.02997 Ng/L 0.02997 0.1111 1 10/15/22 00:52 VIC L643610 MCPA <21.09 ug/L 21.09 55.56 1 10/15/22 00:52 VIC L643610 MCPP <13.06 Ng/L 13.06 55.56 1 10/15/22 00:52 VIC L643610 Picloram <0.05030 ug/L 0.05030 0.1111 1 10/15/22 00:52 VIC L643610 2,4,5-T <0.01113 Ng/L 0.01113 0.03333 1 10/15/22 00:52 VIC L643610 2,4,5-TP(Silvex) <0.01815 ug/L 0.01815 0.1111 1 10/15/22 00:52 VIC L643610 Surrogate: DCAA 60.62 Limits: 20-150% 1 10/15/22 00:52 L643610 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 59 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/11/22 05:00 MSA V24952 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/18/2213:45 ANG V25258 Acrolein <2.00 Ng/L 2.00 5.00 1 10/11/22 05:00 MSA V24952 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/11/22 05:00 MSA V24952 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/18/22 13:45 ANG V25258 Benzene <0.180 ug/L 0.180 0.500 1 10/11/22 05:00 MSA V24952 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/11/22 05:00 MSA V24952 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/11/22 05:00 MSA V24952 Bromoform <1.50 Ng/L 1.50 5.00 1 10/11/22 05:00 MSA V24952 Bromomethane <0.280 ug/L 0.280 1.00 1 10/11/22 05:00 MSA V24952 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/11/22 05:00 MSA V24952 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/11/22 05:00 MSA V24952 Chlorobenzene <0.190 Ng/L 0.190 0.500 1 10/11/22 05:00 MSA V24952 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/11/22 05:00 MSA V24952 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/11/22 05:00 MSA V24952 Chloroform <0.220 ug/L 0.220 0.500 1 10/11/22 05:00 MSA V24952 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/11/22 05:00 MSA V24952 Chloroprene <0.450 ug/L 0.450 10.0 1 10/18/2213:45 ANG V25258 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/11/22 05:00 MSA V24952 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/11/22 05:00 MSA V24952 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/11/22 05:00 MSA V24952 trans-1,4-Dichloro-2-butene <1.30 pg/L 1.30 10.0 1 10/11/22 05:00 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 60 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene <0.220 Ng/L 0.220 0.500 1 10/11/22 05:00 MSA V24952 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/11/22 05:00 MSA V24952 1,4-Dichlorobenzene <0.210 Ng/L 0.210 0.500 1 10/11/22 05:00 MSA V24952 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/11/22 05:00 MSA V24952 1,1-Dichloroethane <0.240 Ng/L 0.240 0.500 1 10/11/22 05:00 MSA V24952 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/11/22 05:00 MSA V24952 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/11/22 05:00 MSA V24952 cis- 1,2-Dich loroethene <0.200 ug/L 0.200 0.500 1 10/11/22 05:00 MSA V24952 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/11/22 05:00 MSA V24952 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/11/22 05:00 MSA V24952 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/11/22 05:00 MSA V24952 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/11/22 05:00 MSA V24952 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/11/22 05:00 MSA V24952 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/11/22 05:00 MSA V24952 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/11/22 05:00 MSA V24952 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/18/22 13:45 ANG V25258 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/11/22 05:00 MSA V24952 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/11/22 05:00 MSA V24952 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/11/22 05:00 MSA V24952 Iodomethane <0.054 ug/L 0.054 0.500 1 10/11/22 05:00 MSA V24952 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/11/22 05:00 MSA V24952 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/18/2213:45 ANG V25258 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 61 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/11/22 05:00 MSA V24952 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/11/22 05:00 MSA V24952 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/11/22 05:00 MSA V24952 Propionitrile <23.7 ug/L 23.7 10.0 1 10/18/2213:45 ANG V25258 Styrene <0.220 Ng/L 0.220 0.500 1 10/11/22 05:00 MSA V24952 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 05:00 MSA V24952 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/11/22 05:00 MSA V24952 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/11/22 05:00 MSA V24952 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/11/22 05:00 MSA V24952 Toluene <0.220 ug/L 0.220 0.500 1 10/11/22 05:00 MSA V24952 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/11/22 05:00 MSA V24952 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 05:00 MSA V24952 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/11/22 05:00 MSA V24952 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/11/22 05:00 MSA V24952 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/11/22 05:00 MSA V24952 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/11/22 05:00 MSA V24952 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/11/22 05:00 MSA V24952 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/11/22 05:00 MSA V24952 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/11/22 05:00 MSA V24952 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/11/22 05:00 MSA V24952 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 62 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25257 10/17/22 14:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Analytical Method: 8270C Prep Method: 3510C Test <0.21 N9/L 0.210 0.500 1 10/11/22 05:00 V24952 99.4 Limits: 80-124% 1 10/11/22 05:00 MSA V24952 96.2 Limits: 75-129% 1 10/11/22 05:00 MSA V24952 92.4 Limits: 63-136% 1 10/11/22 05:00 MSA V24952 95.4 Limits: 77-123% 1 10/11/22 05:00 MSA V24952 100 Limits:80-124% 1 10/18/2213:45 ANG V25258 101 Limits:75-129% 1 10/18/2213:45 ANG V25258 102 Limits:63-136% 1 10/18/2213:45 ANG V25258 101 Limits:77-123% 1 10/18/2213:45 ANG V25258 Prep Batch(es): L642252 10/10/22 15:46 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dimethoate <0.841 Disulfoton <0.549 Ethyl Parathion <0.670 Famphur <0.604 Methyl Parathion <0.949 Phorate <0.777 Surrogate: Tributyl phosphate Surrogate: Triphenyl phosphate Qualifiers/ DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit u9/L 0.841 1.18 N9/L 0.549 1.18 u9/L 0.670 1.18 N9/L 0.604 1.18 u9/L 0.949 1.18 N9/L 0.777 1.18 67.2 Limits: 50-150% 74.5 Limits: 50-150% 1 10/24/22 16:20 VBW L644472 1 10/24/22 16:20 VBW L644472 1 10/24/22 16:20 VBW L644472 1 10/24/22 16:20 VBW L644472 1 10/24/22 16:20 VBW L644472 1 10/24/22 16:20 VBW L644472 1 10/24/22 16:20 VBW 8270C 1 10/24/22 16:20 VBW 8270C H Beyond holding time M Minimum value Page 63 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,3-Dinitrobenzene <1.07 Ng/L 1.07 11.8 1 10/20/22 22:28 VBW L644470 1,3,5-Trinitrobenzene <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW L644471 Acenaphthene <0.495 Ng/L 0.495 2.35 1 10/20/22 22:28 VBW L644470 Acenaphthylene <0.504 ug/L 0.504 2.35 1 10/20/22 22:28 VBW L644470 Acetophenone <0.806 Ng/L 0.806 5.88 1 10/20/22 22:28 VBW L644470 Anthracene <0.548 ug/L 0.548 2.35 1 10/20/22 22:28 VBW L644470 Benzo(a)anthracene <0.501 Ng/L 0.501 2.35 1 10/20/22 22:28 VBW L644470 Benzo(a)pyrene <1.18 ug/L 1.18 2.35 1 10/20/22 22:28 VBW L644470 Benzo(b)fluoranthene <1.11 Ng/L 1.11 2.35 1 10/20/22 22:28 VBW L644470 Benzo(g,h,i)perylene <1.59 ug/L 1.59 2.35 1 10/20/22 22:28 VBW L644470 Benzo(k)fluoranthene <0.883 Ng/L 0.883 2.35 1 10/20/22 22:28 VBW L644470 Benzyl alcohol <3.55 ug/L 3.55 11.8 1 10/20/22 22:28 VBW L644470 Bis(2-Chloroethoxy)methane <0.509 Ng/L 0.509 5.88 1 10/20/22 22:28 VBW L644470 Bis(2-Chloroethyl)ether <0.525 ug/L 0.525 5.88 1 10/20/22 22:28 VBW L644470 Bis(2-Chloroisopropyl)ether <0.642 Ng/L 0.642 5.88 1 10/20/22 22:28 VBW L644470 Bis(2-ethylhexyl)phthalate <4.31 ug/L 4.31 5.88 1 10/20/22 22:28 VBW L644470 4-Bromophenyl phenyl ether <0.588 Ng/L 0.588 5.88 1 10/20/22 22:28 VBW L644470 Butyl benzyl phthalate <5.40 ug/L 5.40 5.88 1 10/20/22 22:28 VBW L644470 4-Chloro-3- methyl phenol <0.591 Ng/L 0.591 5.88 1 10/20/22 22:28 VBW L644470 4-Chloroaniline <0.618 ug/L 0.618 5.88 1 10/20/22 22:28 VBW L644470 Chlorobenzilate <2.23 Ng/L 2.23 5.88 1 10/20/22 22:28 VBW L644470 2-Chloronaphthalene <0.559 ug/L 0.559 5.88 1 10/20/22 22:28 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 64 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2-Chlorophenol <0.865 Ng/L 0.865 5.88 1 10/20/22 22:28 VBW L644470 4-Chlorophenyl phenyl ether <0.563 ug/L 0.563 5.88 1 10/20/22 22:28 VBW L644470 Chrysene <0.858 Ng/L 0.858 2.35 1 10/20/22 22:28 VBW L644470 Dibenz(a,h)anthracene <0.296 ug/L 0.296 2.35 1 10/20/22 22:28 VBW L644470 Dibenzofuran <0.497 Ng/L 0.497 5.88 1 10/20/22 22:28 VBW L644470 1,2-Dichlorobenzene <0.739 ug/L 0.739 5.88 1 10/20/22 22:28 VBW L644470 1,3-Dichlorobenzene <0.577 Ng/L 0.577 5.88 1 10/20/22 22:28 VBW L644470 1,4-Dichlorobenzene <0.682 ug/L 0.682 5.88 1 10/20/22 22:28 VBW L644470 3,3'-Dichlorobenzidine <4.41 Ng/L 4.41 11.8 1 10/20/22 22:28 VBW L644470 2,4-Dichlorophenol <1.79 ug/L 1.79 5.88 1 10/20/22 22:28 VBW L644470 2,6-Dichlorophenol <0.826 Ng/L 0.826 5.88 1 10/20/22 22:28 VBW L644470 Diethyl phthalate <0.687 ug/L 0.687 5.88 1 10/20/22 22:28 VBW L644470 Dimethyl phthalate <0.599 Ng/L 0.599 5.88 1 10/20/22 22:28 VBW L644470 3,3' Dimethylbenzidine <2.22 u9/L 2.22 11.8 1 10/20/22 22:28 VBW L644470 2,4-Dimethyl phenol <0.792 M Ng/L 0.792 5.88 1 10/20/22 22:28 VBW L644470 Di-n-butyl phthalate <1.85 ug/L 1.85 5.88 1 10/20/22 22:28 VBW L644470 4,6- Din itro-2- methyl phenol <4.09 Ng/L 4.09 11.8 1 10/20/22 22:28 VBW L644470 2,4-Dinitrophenol <5.72 ug/L 5.72 11.8 1 10/20/22 22:28 VBW L644470 2,4-Dinitrotoluene <0.473 Ng/L 0.473 5.88 1 10/20/22 22:28 VBW L644470 2,6-Dinitrotoluene <0.485 ug/L 0.485 5.88 1 10/20/22 22:28 VBW L644470 Di-n-Octyl Phthalate <2.02 Ng/L 2.02 5.88 1 10/20/22 22:28 VBW L644470 Ethyl methanesulfonate <0.839 ug/L 0.839 5.88 1 10/20/22 22:28 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 65 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Fluoranthene <0.477 Ng/L 0.477 2.35 1 10/20/22 22:28 VBW L644470 Fluorene <0.521 ug/L 0.521 2.35 1 10/20/22 22:28 VBW L644470 Hexachlorobenzene <3.02 Ng/L 3.02 5.88 1 10/20/22 22:28 VBW L644470 Hexachlorobutadiene <0.476 ug/L 0.476 5.88 1 10/20/22 22:28 VBW L644470 Hexachlorocyclopentadiene <2.75 Ng/L 2.75 5.88 1 10/20/22 22:28 VBW L644470 Hexachloroethane <0.325 ug/L 0.325 5.88 1 10/20/22 22:28 VBW L644470 Indeno(1,2,3-cd)pyrene <1.19 Ng/L 1.19 2.35 1 10/20/22 22:28 VBW L644470 Isodrin <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW L644471 Isophorone <0.423 Ng/L 0.423 5.88 1 10/20/22 22:28 VBW L644470 Kepone <10.0 ug/L 10.0 10.0 1 10/20/22 22:28 VBW L644471 Methyl methanesulfonate <0.726 Ng/L 0.726 5.88 1 10/20/22 22:28 VBW L644470 2-Methylnaphthalene <0.569 ug/L 0.569 2.35 1 10/20/22 22:28 VBW L644470 2-Methylphenol <0.847 Ng/L 0.847 5.88 1 10/20/22 22:28 VBW L644470 3&4 Methylphenol <0.812 ug/L 0.812 5.88 1 10/20/22 22:28 VBW L644470 Naphthalene <0.568 Ng/L 0.568 2.35 1 10/20/22 22:28 VBW L644470 2-Nitroaniline <0.675 ug/L 0.675 5.88 1 10/20/22 22:28 VBW L644470 3-Nitroaniline <1.81 Ng/L 1.81 11.8 1 10/20/22 22:28 VBW L644470 4-Nitroaniline <0.870 ug/L 0.870 5.88 1 10/20/22 22:28 VBW L644470 Nitrobenzene <0.624 Ng/L 0.624 5.88 1 10/20/22 22:28 VBW L644470 2-Nitrophenol <0.712 ug/L 0.712 5.88 1 10/20/22 22:28 VBW L644470 4-Nitrophenol <1.64 Ng/L 1.64 11.8 1 10/20/22 22:28 VBW L644470 N-Nitrosodimethylamine <0.292 ug/L 0.292 5.88 1 10/20/22 22:28 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 66 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPORT OF ANAL YSIS Lab No : 90043 Matrix: Aqueous Sample ID: SW-03-20221004 Sampled: 10/4/2022 10:40 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch N-Nitrosodiphenylamine <0.923 Ng/L 0.923 11.8 1 10/20/22 22:28 VBW L644470 N-Nitrosodiethylamine <0.470 ug/L 0.470 5.88 1 10/20/22 22:28 VBW L644470 N-Nitroso-di-n-butylamine <0.884 Ng/L 0.884 5.88 1 10/20/22 22:28 VBW L644470 N-Nitroso-di-n-propylamine <0.392 ug/L 0.392 5.88 1 10/20/22 22:28 VBW L644470 Pentachlorobenzene <0.541 Ng/L 0.541 11.8 1 10/20/22 22:28 VBW L644470 Pentachloronitrobenzene <1.35 ug/L 1.35 5.88 1 10/20/22 22:28 VBW L644470 Pentachlorophenol <2.89 Ng/L 2.89 11.8 1 10/20/22 22:28 VBW L644470 Phenacetin <1.51 ug/L 1.51 5.88 1 10/20/22 22:28 VBW L644470 Phenanthrene <0.545 Ng/L 0.545 2.35 1 10/20/22 22:28 VBW L644470 Phenol <0.457 ug/L 0.457 5.88 1 10/20/22 22:28 VBW L644470 Pyrene <1.22 Ng/L 1.22 2.35 1 10/20/22 22:28 VBW L644470 1,2,4,5-Tetrachlorobenzene <0.372 u9/L 0.372 5.88 1 10/20/22 22:28 VBW L644470 2,3,4,6-Tetrachlorophenol <0.417 Ng/L 0.417 5.88 1 10/20/22 22:28 VBW L644470 1,2,4-Trichlorobenzene <0.566 ug/L 0.566 5.88 1 10/20/22 22:28 VBW L644470 2,4,5-Trichlorophenol <0.411 Ng/L 0.411 5.88 1 10/20/22 22:28 VBW L644470 2,4,6-Trichlorophenol <0.404 ug/L 0.404 5.88 1 10/20/22 22:28 VBW L644470 Surrogate: 2-Fluorobiphenyl 51.4 Limits: 24-93% 1 10/20/22 22:28 VBW L644470 Surrogate: 2-Fluorophenol 31.6 Limits: 10-44% 1 10/20/22 22:28 VBW L644470 Surrogate: Nitrobenzene-d5 54.4 Limits: 20-91% 1 10/20/22 22:28 VBW L644470 Surrogate: Phenol-d6 26.0 Limits: 7-32% 1 10/20/22 22:28 VBW L644470 Surrogate: 4-Terphenyl-d14 71.2 Limits: 35-126% 1 10/20/22 22:28 VBW L644470 Surrogate: 2,4,6-Tribromophenol 63.6 Limits: 39-110% 1 10/20/22 22:28 VBW L644470 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 67 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPORT OF ANAL YSIS Lab No : 90044 Matrix: Aqueous Sample ID : TripBlank-20221004-1 Sampled: 10/4/2022 0:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone 4.843 Ng/L 1.80 5.00 1 10/10/22 14:09 ANG V24950 Acrolein <2.00 ug/L 2.00 5.00 1 10/10/22 14:09 ANG V24950 Acrylonitrile <0.230 Ng/L 0.230 5.00 1 10/10/22 14:09 ANG V24950 Benzene <0.180 ug/L 0.180 0.500 1 10/10/22 14:09 ANG V24950 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/10/22 14:09 ANG V24950 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/10/22 14:09 ANG V24950 Bromoform <1.50 Ng/L 1.50 5.00 1 10/10/22 14:09 ANG V24950 Bromomethane <0.280 ug/L 0.280 1.00 1 10/10/22 14:09 ANG V24950 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/10/22 14:09 ANG V24950 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/10/22 14:09 ANG V24950 Chlorobenzene <0.190 Ng/L 0.190 0.500 1 10/10/22 14:09 ANG V24950 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/10/22 14:09 ANG V24950 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/10/22 14:09 ANG V24950 Chloroform <0.220 ug/L 0.220 0.500 1 10/10/22 14:09 ANG V24950 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/10/22 14:09 ANG V24950 1,2-Dibromo-3-Chloropropane <1.10 ug/L 1.10 2.00 1 10/10/22 14:09 ANG V24950 1,2-Dibromoethane <0.200 Ng/L 0.200 0.500 1 10/10/22 14:09 ANG V24950 Dibromomethane <0.230 ug/L 0.230 0.500 1 10/10/22 14:09 ANG V24950 trans-1,4-Dichloro-2-butene <1.30 Ng/L 1.30 10.0 1 10/10/22 14:09 ANG V24950 1,2-Dichlorobenzene <0.220 ug/L 0.220 0.500 1 10/10/22 14:09 ANG V24950 1,3-Dichlorobenzene <0.190 Ng/L 0.190 0.500 1 10/10/22 14:09 ANG V24950 1,4-Dichlorobenzene <0.210 ug/L 0.210 0.500 1 10/10/22 14:09 ANG V24950 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 68 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90044 Matrix: Aqueous Sample ID : TripBlank-20221004-1 Sampled: 10/4/2022 0:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dichlorodifluoromethane <1.20 Ng/L 1.20 5.00 1 10/10/22 14:09 ANG V24950 1,1-Dichloroethane <0.240 ug/L 0.240 0.500 1 10/10/22 14:09 ANG V24950 1,2-Dichloroethane <0.150 Ng/L 0.150 0.500 1 10/10/22 14:09 ANG V24950 1,1-Dichloroethene <0.150 ug/L 0.150 0.500 1 10/10/22 14:09 ANG V24950 cis- 1,2-Dich loroethene <0.200 Ng/L 0.200 0.500 1 10/10/22 14:09 ANG V24950 trans- 1.2-Dichloroethene <0.180 ug/L 0.180 0.500 1 10/10/22 14:09 ANG V24950 1,2-Dichloropropane <0.190 Ng/L 0.190 0.500 1 10/10/22 14:09 ANG V24950 1,3-Dichloropropane <0.130 ug/L 0.130 0.500 1 10/10/22 14:09 ANG V24950 2,2-Dichloropropane 0.3133 Ng/L 0.210 2.00 1 10/10/22 14:09 ANG V24950 1,1-Dichloropropene <0.200 ug/L 0.200 0.500 1 10/10/22 14:09 ANG V24950 cis- 1,3-Dich loropropene <0.210 Ng/L 0.210 0.500 1 10/10/22 14:09 ANG V24950 trans-1,3-Dichloropropene <0.150 ug/L 0.150 0.500 1 10/10/22 14:09 ANG V24950 Ethylbenzene 0.3523 Ng/L 0.170 0.500 1 10/10/22 14:09 ANG V24950 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/10/22 14:09 ANG V24950 2-Hexanone 0.4803 Ng/L 0.380 5.00 1 10/10/22 14:09 ANG V24950 Iodomethane <0.054 ug/L 0.054 0.500 1 10/10/22 14:09 ANG V24950 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/10/22 14:09 ANG V24950 4-Methyl-2-Pentanone <1.00 ug/L 1.00 5.00 1 10/10/22 14:09 ANG V24950 Methylene Chloride <0.330 Ng/L 0.330 1.00 1 10/10/22 14:09 ANG V24950 Naphthalene 1.12 ug/L 0.470 1.00 1 10/10/22 14:09 ANG V24950 Styrene 0.2833 Ng/L 0.220 0.500 1 10/10/22 14:09 ANG V24950 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 14:09 ANG V24950 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 69 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90044 Matrix: Aqueous Sample ID : TripBlank-20221004-1 Sampled: 10/4/2022 0:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/10/22 14:09 ANG V24950 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/10/22 14:09 ANG V24950 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/10/22 14:09 ANG V24950 Toluene 0.3043 ug/L 0.220 0.500 1 10/10/22 14:09 ANG V24950 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/10/22 14:09 ANG V24950 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 14:09 ANG V24950 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/10/22 14:09 ANG V24950 Trichloroethene 0.3783 ug/L 0.180 0.500 1 10/10/22 14:09 ANG V24950 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/10/22 14:09 ANG V24950 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/10/22 14:09 ANG V24950 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/10/22 14:09 ANG V24950 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/10/22 14:09 ANG V24950 o-Xylene 0.889 Ng/L 0.210 0.500 1 10/10/22 14:09 ANG V24950 m,p-Xylene 1.10 ug/L 0.420 1.00 1 10/10/22 14:09 ANG V24950 Xylene (Total) 1.99 Ng/L 0.210 0.500 1 10/10/22 14:09 V24950 Surrogate:4-Bromofluorobenzene 98.6 Limits:80-124% 1 10/10/22 14:09 ANG V24950 Surrogate: Dibromofluoromethane 95.2 Limits: 75-129% 1 10/10/22 14:09 ANG V24950 Surrogate: 1,2-Dichloroethane - d4 94.0 Limits: 63-136% 1 10/10/22 14:09 ANG V24950 Surrogate: Toluene-d8 95.2 Limits: 77-123% 1 10/10/22 14:09 ANG V24950 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 70 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90045 Matrix: Aqueous Sample ID : TripBlank-20221004-2 Sampled: 10/4/2022 0:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/10/22 14:36 ANG V24950 Acrolein <2.00 ug/L 2.00 5.00 1 10/10/22 14:36 ANG V24950 Acrylonitrile <0.230 Ng/L 0.230 5.00 1 10/10/22 14:36 ANG V24950 Benzene <0.180 ug/L 0.180 0.500 1 10/10/22 14:36 ANG V24950 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/10/22 14:36 ANG V24950 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/10/22 14:36 ANG V24950 Bromoform <1.50 Ng/L 1.50 5.00 1 10/10/22 14:36 ANG V24950 Bromomethane <0.280 ug/L 0.280 1.00 1 10/10/22 14:36 ANG V24950 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/10/22 14:36 ANG V24950 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/10/22 14:36 ANG V24950 Chlorobenzene <0.190 Ng/L 0.190 0.500 1 10/10/22 14:36 ANG V24950 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/10/22 14:36 ANG V24950 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/10/22 14:36 ANG V24950 Chloroform <0.220 ug/L 0.220 0.500 1 10/10/22 14:36 ANG V24950 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/10/22 14:36 ANG V24950 1,2-Dibromo-3-Chloropropane <1.10 ug/L 1.10 2.00 1 10/10/22 14:36 ANG V24950 1,2-Dibromoethane <0.200 Ng/L 0.200 0.500 1 10/10/22 14:36 ANG V24950 Dibromomethane <0.230 ug/L 0.230 0.500 1 10/10/22 14:36 ANG V24950 trans-1,4-Dichloro-2-butene <1.30 Ng/L 1.30 10.0 1 10/10/22 14:36 ANG V24950 1,2-Dichlorobenzene <0.220 ug/L 0.220 0.500 1 10/10/22 14:36 ANG V24950 1,3-Dichlorobenzene <0.190 Ng/L 0.190 0.500 1 10/10/22 14:36 ANG V24950 1,4-Dichlorobenzene <0.210 ug/L 0.210 0.500 1 10/10/22 14:36 ANG V24950 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 71 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90045 Matrix: Aqueous Sample ID : TripBlank-20221004-2 Sampled: 10/4/2022 0:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dichlorodifluoromethane <1.20 Ng/L 1.20 5.00 1 10/10/22 14:36 ANG V24950 1,1-Dichloroethane <0.240 ug/L 0.240 0.500 1 10/10/22 14:36 ANG V24950 1,2-Dichloroethane <0.150 Ng/L 0.150 0.500 1 10/10/22 14:36 ANG V24950 1,1-Dichloroethene <0.150 ug/L 0.150 0.500 1 10/10/22 14:36 ANG V24950 cis- 1,2-Dich loroethene <0.200 Ng/L 0.200 0.500 1 10/10/22 14:36 ANG V24950 trans- 1.2-Dichloroethene <0.180 ug/L 0.180 0.500 1 10/10/22 14:36 ANG V24950 1,2-Dichloropropane <0.190 Ng/L 0.190 0.500 1 10/10/22 14:36 ANG V24950 1,3-Dichloropropane <0.130 ug/L 0.130 0.500 1 10/10/22 14:36 ANG V24950 2,2-Dichloropropane <0.210 Ng/L 0.210 2.00 1 10/10/22 14:36 ANG V24950 1,1-Dichloropropene <0.200 ug/L 0.200 0.500 1 10/10/22 14:36 ANG V24950 cis- 1,3-Dich loropropene <0.210 Ng/L 0.210 0.500 1 10/10/22 14:36 ANG V24950 trans-1,3-Dichloropropene <0.150 ug/L 0.150 0.500 1 10/10/22 14:36 ANG V24950 Ethylbenzene 0.3413 Ng/L 0.170 0.500 1 10/10/22 14:36 ANG V24950 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/10/22 14:36 ANG V24950 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/10/22 14:36 ANG V24950 Iodomethane <0.054 ug/L 0.054 0.500 1 10/10/22 14:36 ANG V24950 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/10/22 14:36 ANG V24950 4-Methyl-2-Pentanone <1.00 ug/L 1.00 5.00 1 10/10/22 14:36 ANG V24950 Methylene Chloride <0.330 Ng/L 0.330 1.00 1 10/10/22 14:36 ANG V24950 Naphthalene 1.01 ug/L 0.470 1.00 1 10/10/22 14:36 ANG V24950 Styrene 0.2873 Ng/L 0.220 0.500 1 10/10/22 14:36 ANG V24950 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 14:36 ANG V24950 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 72 of 108 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/01/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/06/2022 Asheville , NC 28801 Report Number : 22-279-0018 REPOR T OF A NA L YSIS Lab No : 90045 Matrix: Aqueous Sample ID : TripBlank-20221004-2 Sampled: 10/4/2022 0:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/10/22 14:36 ANG V24950 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/10/22 14:36 ANG V24950 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/10/22 14:36 ANG V24950 Toluene 0.3683 ug/L 0.220 0.500 1 10/10/22 14:36 ANG V24950 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/10/22 14:36 ANG V24950 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 14:36 ANG V24950 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/10/22 14:36 ANG V24950 Trichloroethene 0.373 J ug/L 0.180 0.500 1 10/10/22 14:36 ANG V24950 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/10/22 14:36 ANG V24950 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/10/22 14:36 ANG V24950 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/10/22 14:36 ANG V24950 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/10/22 14:36 ANG V24950 o-Xylene 0.814 Ng/L 0.210 0.500 1 10/10/22 14:36 ANG V24950 m,p-Xylene 1.05 ug/L 0.420 1.00 1 10/10/22 14:36 ANG V24950 Xylene (Total) 1.86 Ng/L 0.210 0.500 1 10/10/22 14:36 V24950 Surrogate:4-Bromofluorobenzene 99.2 Limits:80-124% 1 10/10/22 14:36 ANG V24950 Surrogate: Dibromofluoromethane 95.6 Limits: 75-129% 1 10/10/22 14:36 ANG V24950 Surrogate: 1,2-Dichloroethane - d4 94.0 Limits: 63-136% 1 10/10/22 14:36 ANG V24950 Surrogate: Toluene-d8 97.0 Limits: 77-123% 1 10/10/22 14:36 ANG V24950 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions J Estimated value M Minimum value MQL Method Quantitation Limit Page 73 of 108 • Waypoint, 449 Springbrook Charlotte, NC 28217 Rd, Ch Main 704.529.6364 ANALYTICAL www.waypoi ntana lytica l.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Analytical Batch: V25446 Analysis Method: 2340C-2011 Analysis Description: Total Hardness Lab Reagent Blank LRB Matrix: AQU Associated Lab Samples: 90043 Blank MDL MQL Analyzed Parameter Units Result Hardness pg/L <570 570 5000 10/24/22 11:30 Laboratory Control Sample LCS Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Hardness pg/L 50000 50500 101 90-110 Duplicate V 91107-DUP Result DUP RPD Max RPD Analyzed Parameter Units Result Hardness pg/L 80000 80000 0.0 20 10/24/22 11:30 Matrix Spike & Matrix Spike Duplicate V 91108-MS V 91108-MSD MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD Conc. Hardness pg/L 70000 20000 20000 92000 92000 110 110 80-120 0.0 20 Date: 11/01/2022 02:04 PM Page 1 of 33 Page 74 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Analytical Batch: V24885 Analysis Method: 4500S2F-2011 Analysis Description: Sulfide Lab Reagent Blank LRB Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL MQL Analyzed Parameter Units Result Sulfide mg/L <0.83 0.83 2.00 10/10/2211:00 Laboratory Control Sample LCS Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Sulfide mg/L 10.0 11.0 110 70-122 Date: 11/01/2022 02:04 PM Page 75 of 108 Page 2 of 33 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24878 QC Prep Batch Method: 3005A QC Analytical Batch(es): V24932,V25023 Analysis Method: 6020B Analysis Description: Metals Analyses Lab Reagent Blank LRB-V24878 Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL MQL Analyzed Parameter Units Result Antimony pg/L <0.680 0.680 2.00 10/10/22 18:31 Arsenic pg/L <0.490 0.490 1.00 10/10/22 18:31 Barium pg/L <3.40 3.40 10.0 10/10/22 18:31 Beryllium pg/L <0.240 0.240 1.00 10/10/22 18:31 Cadmium pg/L <0.150 0.150 1.00 10/10/22 18:31 Chromium pg/L <1.00 1.00 2.00 10/10/22 18:31 Cobalt pg/L <0.080 0.080 1.00 10/10/22 18:31 Copper pg/L <0.890 0.890 2.00 10/11/22 15:48 Lead pg/L <0.500 0.500 1.00 10/10/22 18:31 Nickel pg/L <0.720 0.720 2.00 10/10/22 18:31 Selenium pg/L <2.30 2.30 5.00 10/10/22 18:31 Silver pg/L <0.130 0.130 1.00 10/10/22 18:31 Tin pg/L <1.50 1.50 5.00 10/10/22 18:31 Thallium pg/L <0.280 0.280 2.00 10/10/22 18:31 Vanadium pg/L <2.10 2.10 5.00 10/10/22 18:31 Zinc pg/L <3.90 3.90 20.0 10/10/22 18:31 Laboratory Control Sample LCS-V24878 Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Antimony pg/L 100 99.7 100 80-120 Arsenic pg/L 100 93.7 94.0 80-120 Barium pg/L 100 96.5 97.0 80-120 Beryllium pg/L 100 94.1 94.0 80-120 Cadmium pg/L 100 94.0 94.0 80-120 Chromium pg/L 100 97.0 97.0 80-120 Cobalt pg/L 100 99.4 99.0 80-120 Date: 11/01/2022 02:04 PM Page 3 of 33 Page 76 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24878 QC Analytical Batch(es): V24932,V25023 QC Prep Batch Method: 3005A Analysis Method: 6020B Analysis Description: Metals Analyses Laboratory Control Sample LCS-V24878 Parameter Units Spike Conc. LCS Result LCS %Rec % Rec Limits Copper pg/L 100 98.0 98.0 80-120 Lead pg/L 100 99.6 100 80-120 Nickel pg/L 100 96.4 96.0 80-120 Selenium pg/L 100 97.6 98.0 80-120 Silver pg/L 100 98.7 99.0 80-120 Tin pg/L 100 99.2 99.0 80-120 Thallium pg/L 100 98.8 99.0 80-120 Vanadium pg/L 100 98.2 98.0 80-120 Zinc pg/L 100 98.2 98.0 80-120 Matrix Spike & Matrix Spike Duplicate Parameter Units V 89898-MS-V24878 MS Spike Result Conc. V 89898-MSD-V24878 MSD MS Result Spike Conc. MSD Result MS %Rec MSD %Rec %Rec Limits RPD Max RPD Antimony pg/L < 3.40 100 100 75.4 75.6 75.0 76.0 75-125 0.2 20.0 Arsenic pg/L 10.1 100 100 102 102 92.0 92.0 75-125 0.0 20.0 Barium pg/L 224 100 100 315 313 91.0 89.0 75-125 0.6 20.0 Beryllium pg/L < 1.20 100 100 92.9 95.0 93.0 95.0 75-125 2.2 20.0 Cadmium pg/L < 0.750 100 100 93.2 93.2 93.0 93.0 75-125 0.0 20.0 Chromium pg/L 42.2 100 100 140 141 98.0 99.0 75-125 0.7 20.0 Cobalt pg/L 40.7 100 100 141 142 100 101 75-125 0.7 20.0 Lead pg/L 9.82 100 100 110 111 100 101 75-125 0.9 20.0 Nickel pg/L 32.0 100 100 128 129 96.0 97.0 75-125 0.7 20.0 Selenium pg/L 36.2 100 100 131 124 95.0 88.0 75-125 5.4 20.0 Silver pg/L < 0.650 100 100 100 100 100 100 75-125 0.0 20.0 Tin pg/L < 7.50 100 100 98.4 101 98.0 101 75-125 2.6 20.0 Thallium pg/L < 1.40 100 100 101 102 101 102 75-125 0.9 20.0 Date: 11/01/2022 02:04 PM Page 4 of 33 Page 77 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24878 QC Analytical Batch(es): V24932,V25023 QC Prep Batch Method: 3005A Analysis Method: 6020B Analysis Description: Metals Analyses Matrix Spike & Matrix Spike Duplicate V 89898-MS-V24878 V 89898-MSD-V24878 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD Conc. Vanadium ug/L 52.3 100 100 150 152 98.0 100 75-125 1.3 20.0 Zinc ug/L 103 100 100 200 210 97.0 107 75-125 4.8 20.0 Post Digestion Spike V 89898-PDS-V24878 PDS % Analyzed Parameter Units Result Recovery Antimony ug/L 242 97.0 10/10/22 20:32 Arsenic ug/L 251 99.0 10/10/22 20:32 Barium ug/L 353 98.0 10/10/22 20:32 Beryllium ug/L 235 94.0 10/10/22 20:32 Cadmium ug/L 239 96.0 10/10/22 20:32 Chromium ug/L 267 98.0 10/10/22 20:32 Cobalt ug/L 272 101 10/10/22 20:32 Lead ug/L 256 101 10/10/22 20:32 Nickel ug/L 260 98.0 10/10/22 20:32 Selenium ug/L 266 99.0 10/10/22 20:32 Silver ug/L 251 100 10/10/22 20:32 Tin ug/L 250 100 10/10/22 20:32 Thallium ug/L 261 105 10/10/22 20:32 Vanadium ug/L 273 99.0 10/10/22 20:32 Zinc ug/L 293 97.0 10/10/22 20:32 Date: 11/01/2022 02:04 PM Page 5 of 33 Page 78 of 108 • Waypoint, 449 Springbrook Rd, Ch Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypoi ntana lytica l.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24941 QC Analytical Batch(es): V24994 QC Prep Batch Method: 7470A Analysis Method: 7470A Analysis Description: Total Aqueous Mercury Analysis - CVAA Lab Reagent Blank LRB-V24941 Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042 Blank MDL MQL Analyzed Parameter Units Result Mercury (Total) pg/L <0.0700 0.0700 0.200 10/11/22 15:15 Laboratory Control Sample LCS-V24941 Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Mercury (Total) pg/L 9.38 9.61 103 80-120 Matrix Spike & Matrix Spike Duplicate V 89834-MS-V24941 V 89834-MSD-V24941 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD Conc. Mercury (Total) pg/L <0.0700 9.38 9.38 8.39 8.74 89.0 93.0 80-120 4.0 20 Post Digestion Spike V 89834-PDS-V24941 PDS % Analyzed Parameter Units Result Recovery Mercury (Total) pg/L 4.53 97.0 10/11/22 15:39 Date: 11/01/2022 02:04 PM Page 6 of 33 Page 79 of 108 • Waypoint, 449 Springbrook Rd, Ch Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypoi ntana lytica l.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V25435 QC Analytical Batch(es): V25488 QC Prep Batch Method: 7470A Analysis Method: 7470A Analysis Description: Total Aqueous Mercury Analysis - CVAA Lab Reagent Blank LRB-V25435 Matrix: AQU Associated Lab Samples: 90043 Blank MDL MQL Analyzed Parameter Units Result Mercury (Total) pg/L <0.0700 0.0700 0.200 10/24/22 14:53 Laboratory Control Sample LCS-V25435 Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Mercury (Total) pg/L 9.38 9.32 99.0 80-120 Matrix Spike & Matrix Spike Duplicate V 90781-MS-V25435 V 90781-MSD-V25435 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD Conc. Mercury (Total) pg/L <0.0700 9.38 9.38 9.60 10.0 102 107 80-120 4.0 20 Post Digestion Spike V 90781-PDS-V25435 PDS % Analyzed Parameter Units Result Recovery Mercury (Total) pg/L 4.85 104 10/24/22 15:11 Date: 11/01/2022 02:04 PM Page 7 of 33 Page 80 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L644399 QC Analytical Batch(es): L644618 QC Prep Batch Method: 3510C Analysis Method: 8081B Analysis Description: Organochlorine Pesticides by GC Lab Reagent Blank LRB-L644399 Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Aldrin alpha-BHC beta-BHC delta-BHC Chlordane alpha -Chlordane gamma -Chlordane 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Endrin Ketone gamma-BHC Heptachlor Heptachlor Epoxide Methoxychlor Toxaphene Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) pg/L <0.0021 pg/L <0.0021 pg/L <0.0020 pg/L <0.0015 pg/L <0.0221 pg/L <0.0021 pg/L <0.0014 pg/L <0.0021 pg/L <0.0021 pg/L <0.0035 pg/L <0.0015 pg/L <0.0015 pg/L <0.0028 pg/L <0.0015 pg/L <0.0015 pg/L <0.0015 pg/L <0.0015 pg/L <0.0018 pg/L <0.0014 pg/L <0.0014 pg/L <0.0014 pg/L <0.0201 0.0021 0.0021 0.0020 0.0015 0.0221 0.0021 0.0014 0.0021 0.0021 0.0035 0.0015 0.0015 0.0028 0.0015 0.0015 0.0015 0.0015 0.0018 0.0014 0.0014 0.0014 0.0201 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.200 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.0400 10/21/22 01:47 0.300 10/21/22 01:47 10/21/22 01:47 10/21/22 01:47 87.0 51.8 36-116 25-123 Date: 11/01/2022 02:04 PM Page 81 of 108 Page 8 of 33 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L644399 QC Analytical Batch(es): L644618 QC Prep Batch Method: 3510C Analysis Method: 8081B Analysis Description: Organochlorine Pesticides by GC Laboratory Control Sample & LCSD LCS-L644399 LCSD-L644399 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Aldrin pg/L 2.00 1.43 1.80 71.5 90.0 34-105 22.9* 20.0 alpha-BHC pg/L 2.00 1.53 1.87 76.5 93.5 41-102 20.0 20.0 beta-BHC pg/L 2.00 1.62 2.05 81.0 103 26-151 23.4* 20.0 delta-BHC pg/L 2.00 1.38 1.78 69.0 89.0 40-110 25.3* 20.0 alpha -Chlordane pg/L 2.00 1.61 1.92 80.5 96.0 48-117 17.5 20.0 gamma -Chlordane pg/L 2.00 1.81 2.13 90.5 107 51-108 16.2 20.0 4,4'-DDD pg/L 2.00 1.64 2.13 82.0 107 30-110 25.9* 20.0 4,4'-DDE pg/L 2.00 1.47 1.84 73.5 92.0 41-111 22.3* 20.0 4,4'-DDT pg/L 2.00 1.82 2.10 91.0 105 39-123 14.2 20.0 Dieldrin pg/L 2.00 1.63 1.97 81.5 98.5 42-111 18.8 20.0 Endosulfan I pg/L 2.00 1.50 1.88 75.0 94.0 41-111 22.4* 20.0 Endosulfan II pg/L 2.00 1.75 2.15 87.5 108 30-110 20.5* 20.0 Endosulfan Sulfate pg/L 2.00 1.73 2.12 86.5 106 46-111 20.2* 20.0 Endrin pg/L 2.00 1.38 1.71 69.0 85.5 45-117 21.3* 20.0 Endrin Aldehyde pg/L 2.00 1.66 2.02 83.0 101 48-125 19.5 20.0 Endrin Ketone pg/L 2.00 1.56 2.01 78.0 101 51-112 25.2* 20.0 gamma-BHC pg/L 2.00 1.56 1.93 78.0 96.5 41-102 21.2* 20.0 Heptachlor pg/L 2.00 1.55 1.93 77.5 96.5 40-110 21.8* 20.0 Heptachlor Epoxide pg/L 2.00 1.60 1.98 80.0 99.0 42-115 21.2* 20.0 Methoxychlor pg/L 2.00 1.76 2.12 88.0 106 39-140 18.5 20.0 Decachlorobiphenyl (S) 101 109 36-116 Tetrachloro-m-xylene (S) 66.8 77.1 25-123 * QC Fail Date: 11/01/2022 02:04 PM Page 9 of 33 Page 82 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642283 QC Analytical Batch(es): L643610 QC Prep Batch Method: 8151A Analysis Method: 8151A Analysis Description: Phenoxy Acid Herbicides - GC/ECD Lab Reagent Blank LRB-L642283 Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 2,4-D pg/L <0.2078 0.2078 0.2500 10/14/22 19:54 Dalapon pg/L <0.5149 0.5149 0.5500 10/14/22 19:54 2,4-DB pg/L <0.1364 0.1364 0.2500 10/14/22 19:54 Dicamba pg/L <0.05700 0.05700 0.01000 10/14/22 19:54 Dichlorprop pg/L <0.07959 0.07959 0.1000 10/14/22 19:54 Dinoseb pg/L <0.02698 0.02698 0.1000 10/14/22 19:54 MCPA pg/L <18.98 18.98 50.00 10/14/22 19:54 MCPP pg/L <11.75 11.75 50.00 10/14/22 19:54 Picloram pg/L <0.04528 0.04528 0.1000 10/14/22 19:54 2,4,5-T pg/L <0.01002 0.01002 0.03000 10/14/22 19:54 2,4,5-TP (Silvex) pg/L <0.01634 0.01634 0.1000 10/14/22 19:54 DCAA (S) 10/14/22 19:54 67.9 20-150 Laboratory Control Sample & LCSD LCS-L642283 LCSD-L642283 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD a/o Rec % Rec Limits RPD Max RPD 2,4-D pg/L 5.000 3.215 3.229 64.3 64.5 20-120 0.4 20.00 Dalapon pg/L 12.50 4.245 7.396 33.9 59.1 20-120 54.1* 20.00 2,4-DB pg/L 5.000 3.419 3.464 68.3 69.2 20-120 1.3 20.00 Dicamba pg/L 0.5000 0.3689 0.3626 73.7 72.5 20-120 1.7 20.00 Dichlorprop pg/L 5.000 3.582 3.547 71.6 70.9 20-120 0.9 20.00 Dinoseb pg/L 2.500 1.734 1.756 69.3 70.2 20-120 1.2 20.00 MCPA pg/L 500.0 350.4 351.3 70.0 70.2 20-120 0.2 20.00 MCPP pg/L 500.0 345.3 355.6 69.0 71.1 20-120 2.9 20.00 Picloram pg/L 1.250 0.5693 0.5792 45.5 46.3 20-120 1.7 20.00 2,4,5-T pg/L 0.5000 0.3792 0.3818 75.8 76.3 20-120 0.6 20.00 * QC Fail Date: 11/01/2022 02:04 PM Page 10 of 33 Page 83 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642283 QC Analytical Batch(es): L643610 QC Prep Batch Method: 8151A Analysis Method: 8151A Analysis Description: Phenoxy Acid Herbicides - GC/ECD Laboratory Control Sample & LCSD LCS-L642283 LCSD-L642283 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD 2,4,5-TP (Silvex) pg/L 0.5000 0.3748 0.3676 74.9 73.5 20-120 1.9 20.00 DCAA (S) 65.8 67.9 20-150 Date: 11/01/2022 02:04 PM Page 11 of 33 Page 84 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24851 QC Analytical Batch(es): V24852 QC Prep Batch Method: 5030B Analysis Method: 8260D SIM Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V24851 Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 1,4-Dioxane pg/L <0.139 0.139 2.00 10/07/2212:08 4-Bromofluorobenzene (S) 10/07/22 12:08 119 70-130 Laboratory Control Sample LCS-V24851 Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits 1,4-Dioxane pg/L 50.0 45.6 91.2 70-130 4-Bromofluorobenzene (S) 120 70-130 Matrix Spike & Matrix Spike Duplicate V 90043-MS-V24851 V 90043-MSD-V24851 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD Conc. 1,4-Dioxane pg/L < 0.139 50.0 50.0 48.7 49.6 97.4 99.2 70-130 4-Bromofluorobenzene (S) 113 125 70-130 Date: 11/01/2022 02:04 PM Page 12 of 33 Page 85 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24949 QC Prep Batch Method: 5030B QC Analytical Batch(es): V24950 Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V24949 Matrix: AQU Associated Lab Samples: 90044, 90045 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Acetone pg/L <1.80 1.80 5.00 10/10/22 13:15 Acrolein pg/L <2.00 2.00 5.00 10/10/22 13:15 Acrylonitrile pg/L <0.230 0.230 5.00 10/10/22 13:15 Benzene pg/L <0.180 0.180 0.500 10/10/22 13:15 Bromochloromethane pg/L <0.420 0.420 1.00 10/10/22 13:15 Bromodichloromethane pg/L <0.160 0.160 0.500 10/10/22 13:15 Bromoform pg/L <1.50 1.50 5.00 10/10/22 13:15 Bromomethane pg/L <0.280 0.280 1.00 10/10/22 13:15 Carbon Disulfide pg/L <0.150 0.150 5.00 10/10/22 13:15 Carbon Tetrachloride pg/L <0.180 0.180 0.500 10/10/22 13:15 Chlorobenzene pg/L <0.190 0.190 0.500 10/10/22 13:15 Chlorodibromomethane pg/L <0.190 0.190 0.500 10/10/22 13:15 Chloroethane pg/L <0.430 0.430 1.00 10/10/22 13:15 Chloroform pg/L <0.220 0.220 0.500 10/10/22 13:15 Chloromethane pg/L <0.220 0.220 0.500 10/10/22 13:15 1,2-Dibromo-3-Chloropropane pg/L <1.10 1.10 2.00 10/10/22 13:15 1,2-Dibromoethane pg/L <0.200 0.200 0.500 10/10/22 13:15 Dibromomethane pg/L <0.230 0.230 0.500 10/10/22 13:15 trans-1,4-Dichloro-2-butene pg/L < 1.30 1.30 10.0 10/10/22 13:15 1,2-Dichlorobenzene pg/L <0.220 0.220 0.500 10/10/22 13:15 1,3-Dichlorobenzene pg/L <0.190 0.190 0.500 10/10/22 13:15 1,4-Dichlorobenzene pg/L <0.210 0.210 0.500 10/10/22 13:15 Dichlorodifluoromethane pg/L <1.20 1.20 5.00 10/10/22 13:15 1,1-Dichloroethane pg/L <0.240 0.240 0.500 10/10/22 13:15 1,2-Dichloroethane pg/L <0.150 0.150 0.500 10/10/22 13:15 1,1-Dichloroethene pg/L <0.150 0.150 0.500 10/10/22 13:15 cis-1,2-Dichloroethene pg/L <0.200 0.200 0.500 10/10/22 13:15 Date: 11/01/2022 02:04 PM Page 13 of 33 Page 86 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24949 QC Prep Batch Method: 5030B QC Analytical Batch(es): V24950 Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V24949 Matrix: AQU Associated Lab Samples: 90044, 90045 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits trans-1,2-Dichloroethene pg/L <0.180 0.180 0.500 10/10/22 13:15 1,2-Dichloropropane pg/L <0.190 0.190 0.500 10/10/22 13:15 1,3-Dichloropropane pg/L <0.130 0.130 0.500 10/10/22 13:15 2,2-Dichloropropane pg/L <0.210 0.210 2.00 10/10/22 13:15 1,1-Dichloropropene pg/L <0.200 0.200 0.500 10/10/22 13:15 cis-1,3-Dichloropropene pg/L <0.210 0.210 0.500 10/10/22 13:15 trans-1,3-Dichloropropene pg/L <0.150 0.150 0.500 10/10/22 13:15 Ethylbenzene pg/L <0.170 0.170 0.500 10/10/22 13:15 Hexachlorobutadiene pg/L <0.350 0.350 2.00 10/10/22 13:15 2-Hexanone pg/L <0.380 0.380 5.00 10/10/22 13:15 Iodomethane pg/L <0.054 0.054 0.500 10/10/22 13:15 Methyl Ethyl Ketone (MEK) pg/L <0.710 0.710 5.00 10/10/22 13:15 4-Methyl-2-Pentanone pg/L <1.00 1.00 5.00 10/10/22 13:15 Methylene Chloride pg/L <0.330 0.330 1.00 10/10/22 13:15 Naphthalene pg/L <0.470 0.470 1.00 10/10/22 13:15 Styrene pg/L <0.220 0.220 0.500 10/10/22 13:15 1,1,1,2-Tetrachloroethane pg/L <0.160 0.160 0.500 10/10/22 13:15 1,1,2,2-Tetrachloroethane pg/L <0.160 0.160 0.500 10/10/22 13:15 Tetrachloroethene pg/L <0.220 0.220 0.500 10/10/22 13:15 Tetrahydrofuran pg/L <1.50 1.50 10.0 10/10/22 13:15 Toluene pg/L <0.220 0.220 0.500 10/10/22 13:15 1,2,4-Trichlorobenzene pg/L <0.310 0.310 1.00 10/10/22 13:15 1,1,1-Trichloroethane pg/L <0.160 0.160 0.500 10/10/22 13:15 1,1,2-Trichloroethane pg/L <0.096 0.096 0.500 10/10/22 13:15 Trichloroethene pg/L <0.180 0.180 0.500 10/10/22 13:15 Trichlorofluoromethane pg/L <0.180 0.180 0.500 10/10/22 13:15 1,2,3-Trichloropropane pg/L <0.270 0.270 1.00 10/10/22 13:15 Date: 11/01/2022 02:04 PM Page 14 of 33 Page 87 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24949 QC Analytical Batch(es): V24950 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V24949 Matrix: AQU Associated Lab Samples: 90044, 90045 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Vinyl Acetate pg/L <1.00 1.00 2.00 10/10/22 13:15 Vinyl Chloride pg/L <0.170 0.170 0.500 10/10/22 13:15 o-Xylene pg/L <0.210 0.210 0.500 10/10/22 13:15 m,p-Xylene pg/L <0.420 0.420 1.00 10/10/22 13:15 4-Bromofluorobenzene (S) 10/10/22 13:15 99.0 80-124 Dibromofluoromethane (S) 10/10/22 13:15 95.0 75-129 1,2-Dichloroethane - d4 (S) 10/10/22 13:15 92.8 63-136 Toluene-d8 (S) 10/10/22 13:15 96.0 77-123 Laboratory Control Sample & LCSD LCS-V24949 LCSD-V24949 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec a/o Rec Limits RPD Max RPD Acetone pg/L 40.0 40.4 40.7 101 102 40-166 0.7 20.0 Acrolein pg/L 40.0 45.9 46.7 115 117 70-130 1.7 20.0 Acrylonitrile pg/L 40.0 46.0 47.1 115 118 81-127 2.3 20.0 Benzene pg/L 20.0 20.8 20.3 104 102 77-128 2.4 20.0 Bromochloromethane pg/L 20.0 21.3 20.7 107 104 78-135 2.8 20.0 Bromodichloromethane pg/L 20.0 19.5 19.8 97.5 99.0 76-138 1.5 20.0 Bromoform pg/L 20.0 19.5 19.9 97.5 99.5 71-135 2.0 20.0 Bromomethane pg/L 20.0 17.0 16.4 85.0 82.0 41-168 3.5 20.0 Carbon Disulfide pg/L 20.0 21.7 20.9 109 105 59-135 3.7 20.0 Carbon Tetrachloride pg/L 20.0 23.3 19.1 117 95.5 72-142 19.8 20.0 Chlorobenzene pg/L 20.0 20.3 20.2 102 101 78-119 0.4 20.0 Chlorodibromomethane pg/L 20.0 20.5 20.7 103 104 75-134 0.9 20.0 Chloroethane pg/L 20.0 17.0 16.4 85.0 82.0 57-142 3.5 20.0 Chloroform pg/L 20.0 21.2 20.2 106 101 77-130 4.8 20.0 Date: 11/01/2022 02:04 PM Page 15 of 33 Page 88 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24949 QC Analytical Batch(es): V24950 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-V24949 LCSD-V24949 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Chloromethane pg/L 20.0 15.6 15.1 78.0 75.5 47-145 3.2 20.0 1,2-Dibromo-3-Chloropropane pg/L 20.0 16.6 17.7 83.0 88.5 63-134 6.4 20.0 1,2-Dibromoethane pg/L 20.0 21.3 21.5 107 108 77-135 0.9 20.0 Dibromomethane pg/L 20.0 20.8 20.8 104 104 76-138 0.0 20.0 trans-1,4-Dichloro-2-butene pg/L 20.0 19.3 19.2 96.5 96.0 70-130 0.5 20.0 1,2-Dichlorobenzene pg/L 20.0 20.0 19.7 100 98.5 78-128 1.5 20.0 1,3-Dichlorobenzene pg/L 20.0 20.7 20.8 104 104 77-125 0.4 20.0 1,4-Dichlorobenzene pg/L 20.0 20.5 20.1 103 101 75-126 1.9 20.0 Dichlorodifluoromethane pg/L 20.0 18.1 17.1 90.5 85.5 28-163 5.6 20.0 1,1-Dichloroethane pg/L 20.0 20.7 20.8 104 104 70-130 0.4 20.0 1,2-Dichloroethane pg/L 20.0 18.8 18.5 94.0 92.5 68-131 1.6 20.0 1,1-Dichloroethene pg/L 20.0 19.6 18.8 98.0 94.0 70-154 4.1 20.0 cis-1,2-Dichloroethene pg/L 20.0 20.0 19.8 100 99.0 76-141 1.0 20.0 trans-1,2-Dichloroethene pg/L 20.0 20.6 20.0 103 100 76-135 2.9 20.0 1,2-Dichloropropane pg/L 20.0 20.8 20.1 104 101 77-130 3.4 20.0 1,3-Dichloropropane pg/L 20.0 20.1 20.9 101 105 76-132 3.9 20.0 2,2-Dichloropropane pg/L 20.0 19.2 19.4 96.0 97.0 29-149 1.0 20.0 1,1-Dichloropropene pg/L 20.0 22.3 21.5 112 108 71-136 3.6 20.0 cis-1,3-Dichloropropene pg/L 20.0 21.1 20.7 106 104 65-140 1.9 20.0 trans-1,3-Dichloropropene pg/L 20.0 21.1 20.7 106 104 67-140 1.9 20.0 Ethylbenzene pg/L 20.0 19.0 19.0 95.0 95.0 80-127 0.0 20.0 Hexachlorobutadiene pg/L 20.0 19.2 19.5 96.0 97.5 61-134 1.5 20.0 2-Hexanone pg/L 20.0 18.6 18.4 93.0 92.0 64-137 1.0 20.0 Iodomethane pg/L 20.0 14.7 14.1 73.5 70.5 70-130 4.1 20.0 Methyl Ethyl Ketone (MEK) pg/L 20.0 19.3 19.3 96.5 96.5 71-134 0.0 20.0 4-Methyl-2-Pentanone pg/L 20.0 19.4 19.9 97.0 99.5 69-134 2.5 20.0 Date: 11/01/2022 02:04 PM Page 16 of 33 Page 89 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24949 QC Analytical Batch(es): V24950 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-V24949 LCSD-V24949 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Methylene Chloride pg/L 20.0 20.1 19.4 101 97.0 73-131 3.5 20.0 Naphthalene pg/L 20.0 17.4 18.1 87.0 90.5 64-136 3.9 20.0 Styrene pg/L 20.0 20.3 19.7 102 98.5 78-129 3.0 20.0 1,1,1,2-Tetrachloroethane pg/L 20.0 19.8 19.1 99.0 95.5 79-134 3.5 20.0 1,1,2,2-Tetrachloroethane pg/L 20.0 19.2 20.1 96.0 101 62-127 4.5 20.0 Tetrachloroethene pg/L 20.0 20.4 19.8 102 99.0 80-129 2.9 20.0 Tetrahydrofuran pg/L 20.0 20.8 20.8 104 104 70-130 0.0 20.0 Toluene pg/L 20.0 20.4 19.6 102 98.0 76-131 4.0 20.0 1,2,4-Trichlorobenzene pg/L 20.0 19.5 19.7 97.5 98.5 66-139 1.0 20.0 1,1,1-Trichloroethane pg/L 20.0 20.2 19.7 101 98.5 75-135 2.5 20.0 1,1,2-Trichloroethane pg/L 20.0 21.7 21.4 109 107 70-140 1.3 20.0 Trichloroethene pg/L 20.0 21.1 20.4 106 102 77-133 3.3 20.0 Trichlorofluoromethane pg/L 20.0 18.9 17.5 94.5 87.5 62-148 7.6 20.0 1,2,3-Trichloropropane pg/L 20.0 18.9 19.2 94.5 96.0 71-127 1.5 20.0 Vinyl Acetate pg/L 20.0 21.6 22.0 108 110 34-167 1.8 20.0 Vinyl Chloride pg/L 20.0 19.3 18.2 96.5 91.0 57-141 5.8 20.0 o-Xylene pg/L 20.0 19.2 18.8 96.0 94.0 78-128 2.1 20.0 m,p-Xylene pg/L 40.0 40.0 39.7 100 99.2 77-133 0.7 20.0 4-Bromofluorobenzene (S) 97.8 99.8 80-124 Dibromofluoromethane (S) 100 98.0 75-129 1,2-Dichloroethane - d4 (S) 93.6 93.6 63-136 Toluene-d8 (S) 96.2 96.6 77-123 Date: 11/01/2022 02:04 PM Page 17 of 33 Page 90 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24951 QC Prep Batch Method: 5030B Lab Reagent Blank LRB-V24951 Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 QC Analytical Batch(es): V24952 Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Acetone pg/L <1.80 1.80 5.00 10/11/22 00:30 Acrolein pg/L <2.00 2.00 5.00 10/11/22 00:30 Acrylonitrile pg/L <0.230 0.230 5.00 10/11/22 00:30 Benzene pg/L <0.180 0.180 0.500 10/11/22 00:30 Bromochloromethane pg/L <0.420 0.420 1.00 10/11/22 00:30 Bromodichloromethane pg/L <0.160 0.160 0.500 10/11/22 00:30 Bromoform pg/L <1.50 1.50 5.00 10/11/22 00:30 Bromomethane pg/L <0.280 0.280 1.00 10/11/22 00:30 Carbon Disulfide pg/L <0.150 0.150 5.00 10/11/22 00:30 Carbon Tetrachloride pg/L <0.180 0.180 0.500 10/11/22 00:30 Chlorobenzene pg/L <0.190 0.190 0.500 10/11/22 00:30 Chlorodibromomethane pg/L <0.190 0.190 0.500 10/11/22 00:30 Chloroethane pg/L <0.430 0.430 1.00 10/11/22 00:30 Chloroform pg/L <0.220 0.220 0.500 10/11/22 00:30 Chloromethane pg/L <0.220 0.220 0.500 10/11/22 00:30 1,2-Dibromo-3-Chloropropane pg/L <1.10 1.10 2.00 10/11/22 00:30 1,2-Dibromoethane pg/L <0.200 0.200 0.500 10/11/22 00:30 Dibromomethane pg/L <0.230 0.230 0.500 10/11/22 00:30 trans-1,4-Dichloro-2-butene pg/L < 1.30 1.30 10.0 10/11/22 00:30 1,2-Dichlorobenzene pg/L <0.220 0.220 0.500 10/11/22 00:30 1,3-Dichlorobenzene pg/L <0.190 0.190 0.500 10/11/22 00:30 1,4-Dichlorobenzene pg/L <0.210 0.210 0.500 10/11/22 00:30 Dichlorodifluoromethane pg/L <1.20 1.20 5.00 10/11/22 00:30 1,1-Dichloroethane pg/L <0.240 0.240 0.500 10/11/22 00:30 1,2-Dichloroethane pg/L <0.150 0.150 0.500 10/11/22 00:30 1,1-Dichloroethene pg/L <0.150 0.150 0.500 10/11/22 00:30 cis-1,2-Dichloroethene pg/L <0.200 0.200 0.500 10/11/22 00:30 Date: 11/01/2022 02:04 PM Page 18 of 33 Page 91 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24951 QC Prep Batch Method: 5030B Lab Reagent Blank LRB-V24951 Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 QC Analytical Batch(es): V24952 Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits trans-1,2-Dichloroethene pg/L <0.180 0.180 0.500 10/11/22 00:30 1,2-Dichloropropane pg/L <0.190 0.190 0.500 10/11/22 00:30 1,3-Dichloropropane pg/L <0.130 0.130 0.500 10/11/22 00:30 2,2-Dichloropropane pg/L <0.210 0.210 2.00 10/11/22 00:30 1,1-Dichloropropene pg/L <0.200 0.200 0.500 10/11/22 00:30 cis-1,3-Dichloropropene pg/L <0.210 0.210 0.500 10/11/22 00:30 trans-1,3-Dichloropropene pg/L <0.150 0.150 0.500 10/11/22 00:30 Ethylbenzene pg/L <0.170 0.170 0.500 10/11/22 00:30 Hexachlorobutadiene pg/L <0.350 0.350 2.00 10/11/22 00:30 2-Hexanone pg/L <0.380 0.380 5.00 10/11/22 00:30 Iodomethane pg/L <0.054 0.054 0.500 10/11/22 00:30 Methyl Ethyl Ketone (MEK) pg/L <0.710 0.710 5.00 10/11/22 00:30 4-Methyl-2-Pentanone pg/L <1.00 1.00 5.00 10/11/22 00:30 Methylene Chloride pg/L <0.330 0.330 1.00 10/11/22 00:30 Naphthalene pg/L <0.470 0.470 1.00 10/11/22 00:30 Styrene pg/L <0.220 0.220 0.500 10/11/22 00:30 1,1,1,2-Tetrachloroethane pg/L <0.160 0.160 0.500 10/11/22 00:30 1,1,2,2-Tetrachloroethane pg/L <0.160 0.160 0.500 10/11/22 00:30 Tetrachloroethene pg/L <0.220 0.220 0.500 10/11/22 00:30 Tetrahydrofuran pg/L <1.50 1.50 10.0 10/11/22 00:30 Toluene pg/L <0.220 0.220 0.500 10/11/22 00:30 1,2,4-Trichlorobenzene pg/L <0.310 0.310 1.00 10/11/22 00:30 1,1,1-Trichloroethane pg/L <0.160 0.160 0.500 10/11/22 00:30 1,1,2-Trichloroethane pg/L <0.096 0.096 0.500 10/11/22 00:30 Trichloroethene pg/L <0.180 0.180 0.500 10/11/22 00:30 Trichlorofluoromethane pg/L <0.180 0.180 0.500 10/11/22 00:30 1,2,3-Trichloropropane pg/L <0.270 0.270 1.00 10/11/22 00:30 Date: 11/01/2022 02:04 PM Page 19 of 33 Page 92 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24951 QC Analytical Batch(es): V24952 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V24951 Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Vinyl Acetate pg/L <1.00 1.00 2.00 10/11/22 00:30 Vinyl Chloride pg/L <0.170 0.170 0.500 10/11/22 00:30 o-Xylene pg/L <0.210 0.210 0.500 10/11/22 00:30 m,p-Xylene pg/L <0.420 0.420 1.00 10/11/22 00:30 4-Bromofluorobenzene (S) 10/11/22 00:30 99.6 80-124 Dibromofluoromethane (S) 10/11/22 00:30 96.4 75-129 1,2-Dichloroethane - d4 (S) 10/11/22 00:30 93.4 63-136 Toluene-d8(S) 10/11/22 00:30 96.0 77-123 Laboratory Control Sample & LCSD LCS-V24951 LCSD-V24951 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD a/o Rec % Rec Limits RPD Max RPD Acetone pg/L 40.0 42.1 40.8 105 102 40-166 3.1 20.0 Acrolein pg/L 40.0 42.4 43.7 106 109 70-130 3.0 20.0 Acrylonitrile pg/L 40.0 44.6 47.5 112 119 81-127 6.2 20.0 Benzene pg/L 20.0 21.2 21.0 106 105 77-128 0.9 20.0 Bromochloromethane pg/L 20.0 20.7 19.9 104 99.5 78-135 3.9 20.0 Bromodichloromethane pg/L 20.0 19.8 19.5 99.0 97.5 76-138 1.5 20.0 Bromoform pg/L 20.0 20.3 20.8 102 104 71-135 2.4 20.0 Bromomethane pg/L 20.0 18.2 16.1 91.0 80.5 41-168 12.2 20.0 Carbon Disulfide pg/L 20.0 21.5 20.8 108 104 59-135 3.3 20.0 Carbon Tetrachloride pg/L 20.0 21.0 23.8 105 119 72-142 12.5 20.0 Chlorobenzene pg/L 20.0 20.3 19.7 102 98.5 78-119 3.0 20.0 Chlorodibromomethane pg/L 20.0 20.3 20.1 102 101 75-134 0.9 20.0 Chloroethane pg/L 20.0 17.6 16.9 88.0 84.5 57-142 4.0 20.0 Chloroform pg/L 20.0 21.1 21.2 106 106 77-130 0.4 20.0 Date: 11/01/2022 02:04 PM Page 20 of 33 Page 93 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24951 QC Analytical Batch(es): V24952 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-V24951 LCSD-V24951 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Chloromethane pg/L 20.0 16.8 16.6 84.0 83.0 47-145 1.1 20.0 1,2-Dibromo-3-Chloropropane pg/L 20.0 17.4 17.2 87.0 86.0 63-134 1.1 20.0 1,2-Dibromoethane pg/L 20.0 21.2 21.5 106 108 77-135 1.4 20.0 Dibromomethane pg/L 20.0 20.5 21.0 103 105 76-138 2.4 20.0 trans-1,4-Dichloro-2-butene pg/L 20.0 18.3 18.9 91.5 94.5 70-130 3.2 20.0 1,2-Dichlorobenzene pg/L 20.0 19.0 18.7 95.0 93.5 78-128 1.5 20.0 1,3-Dichlorobenzene pg/L 20.0 19.4 18.9 97.0 94.5 77-125 2.6 20.0 1,4-Dichlorobenzene pg/L 20.0 19.1 18.9 95.5 94.5 75-126 1.0 20.0 Dichlorodifluoromethane pg/L 20.0 18.5 18.3 92.5 91.5 28-163 1.0 20.0 1,1-Dichloroethane pg/L 20.0 21.6 21.4 108 107 70-130 0.9 20.0 1,2-Dichloroethane pg/L 20.0 18.4 18.5 92.0 92.5 68-131 0.5 20.0 1,1-Dichloroethene pg/L 20.0 20.7 19.7 104 98.5 70-154 4.9 20.0 cis-1,2-Dichloroethene pg/L 20.0 21.0 20.5 105 103 76-141 2.4 20.0 trans-1,2-Dichloroethene pg/L 20.0 21.5 20.4 108 102 76-135 5.2 20.0 1,2-Dichloropropane pg/L 20.0 21.0 20.2 105 101 77-130 3.8 20.0 1,3-Dichloropropane pg/L 20.0 19.6 19.9 98.0 99.5 76-132 1.5 20.0 2,2-Dichloropropane pg/L 20.0 18.5 17.8 92.5 89.0 29-149 3.8 20.0 1,1-Dichloropropene pg/L 20.0 23.0 22.7 115 114 71-136 1.3 20.0 cis-1,3-Dichloropropene pg/L 20.0 20.3 20.9 102 105 65-140 2.9 20.0 trans-1,3-Dichloropropene pg/L 20.0 20.3 20.9 102 105 67-140 2.9 20.0 Ethylbenzene pg/L 20.0 19.3 19.1 96.5 95.5 80-127 1.0 20.0 Hexachlorobutadiene pg/L 20.0 16.9 16.8 84.5 84.0 61-134 0.5 20.0 2-Hexanone pg/L 20.0 17.9 17.3 89.5 86.5 64-137 3.4 20.0 Iodomethane pg/L 20.0 15.7 15.6 78.5 78.0 70-130 0.6 20.0 Methyl Ethyl Ketone (MEK) pg/L 20.0 19.8 19.5 99.0 97.5 71-134 1.5 20.0 4-Methyl-2-Pentanone pg/L 20.0 19.3 19.8 96.5 99.0 69-134 2.5 20.0 Date: 11/01/2022 02:04 PM Page 21 of 33 Page 94 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V24951 QC Analytical Batch(es): V24952 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-V24951 LCSD-V24951 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits Methylene Chloride pg/L 20.0 20.3 20.2 102 101 73-131 Naphthalene pg/L 20.0 17.0 17.3 85.0 86.5 64-136 Styrene pg/L 20.0 19.9 20.3 99.5 102 78-129 1,1,1,2-Tetrachloroethane pg/L 20.0 19.7 19.3 98.5 96.5 79-134 1,1,2,2-Tetrachloroethane pg/L 20.0 18.9 19.8 94.5 99.0 62-127 Tetrachloroethene pg/L 20.0 20.9 19.8 105 99.0 80-129 Tetrahydrofuran pg/L 20.0 20.1 21.5 101 108 70-130 Toluene pg/L 20.0 20.9 20.2 105 101 76-131 1,2,4-Trichlorobenzene pg/L 20.0 17.8 16.9 89.0 84.5 66-139 1,1,1-Trichloroethane pg/L 20.0 20.9 21.0 105 105 75-135 1,1,2-Trichloroethane pg/L 20.0 22.0 21.7 110 109 70-140 Trichloroethene pg/L 20.0 22.1 20.8 111 104 77-133 Trichlorofluoromethane pg/L 20.0 19.7 18.4 98.5 92.0 62-148 1,2,3-Trichloropropane pg/L 20.0 18.9 19.9 94.5 99.5 71-127 Vinyl Acetate pg/L 20.0 17.7 20.7 88.5 104 34-167 Vinyl Chloride pg/L 20.0 19.8 19.2 99.0 96.0 57-141 o-Xylene pg/L 20.0 19.3 18.4 96.5 92.0 78-128 m,p-Xylene pg/L 40.0 40.3 39.1 101 97.7 77-133 4-Bromofluorobenzene (S) 99.8 101 80-124 Dibromofluoromethane (S) 100 101 75-129 1,2-Dichloroethane - d4 (S) 93.4 94.0 63-136 Toluene-d8 (S) 96.2 95.4 77-123 RPD 0.4 1.7 1.9 2.0 4.6 5.4 6.7 3.4 5.1 0.4 1.3 6.0 6.8 5.1 15.6 3.0 4.7 3.0 Max RPD 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 Date: 11/01/2022 02:04 PM Page 22 of 33 Page 95 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: V25257 QC Analytical Batch(es): V25258 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V25257 Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Acetonitrile pg/L <20.3 20.3 10.0 10/18/22 06:59 Allyl Chloride pg/L <0.579 0.579 10.0 10/18/22 06:59 Chloroprene pg/L <0.450 0.450 10.0 10/18/22 06:59 Ethyl Methacrylate pg/L < 1.62 1.62 10.0 10/18/22 06:59 Methacrylonitrile pg/L <12.6 12.6 10.0 10/18/22 06:59 Propionitrile pg/L <23.7 23.7 10.0 10/18/22 06:59 4-Bromofluorobenzene (S) 10/18/22 06:59 98.4 80-124 Dibromofluoromethane (S) 10/18/22 06:59 99.4 75-129 1,2-Dichloroethane - d4 (S) 10/18/22 06:59 98.2 63-136 Toluene-d8(S) 10/18/22 06:59 101 77-123 Laboratory Control Sample & LCSD LCS-V25257 LCSD-V25257 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD Acetonitrile pg/L 20.0 20.7 <20.3 104 0.0* 40-160 1.9 20.0 Allyl Chloride pg/L 20.0 18.0 17.6 90.0 88.0 40-160 2.2 20.0 Chloroprene pg/L 20.0 20.5 18.8 103 94.0 40-160 8.6 20.0 Ethyl Methacrylate pg/L 20.0 18.0 18.7 90.0 93.5 40-160 3.8 20.0 Methacrylonitrile pg/L 20.0 17.1 17.4 85.5 87.0 40-160 1.7 20.0 Propionitrile pg/L 20.0 <23.7 <23.7 0.0* 0.0* 40-160 0.0 20.0 4-Bromofluorobenzene (S) 99.6 101 80-124 Dibromofluoromethane (S) 104 101 75-129 1,2-Dichloroethane - d4 (S) 97.4 97.4 63-136 Toluene-d8(S) 100 100 77-123 * QC Fail Date: 11/01/2022 02:04 PM Page 23 of 33 Page 96 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642252 QC Prep Batch Method: 3510C Lab Reagent Blank LRB-L642252 Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL Parameter Units Result Dimethoate pg/L <0.713 0.713 Disulfoton pg/L <0.466 0.466 Ethyl Parathion pg/L <0.568 0.568 Famphur pg/L <0.512 0.512 Methyl Parathion pg/L <0.805 0.805 Phorate pg/L <0.659 0.659 0,0,0-Triethyl Phosphorothioate pg/L <0.330 0.330 Tributyl phosphate (S) Triphenyl phosphate (S) QC Analytical Batch(es): L644472 Analysis Method: 8270C Analysis Description: Organophosphorus Pesticides by GC/MS Matrix: AQU MQL Analyzed 0/0 Recovery 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 10/24/22 13:52 68.5 10/24/22 13:52 72.5 Laboratory Control Sample & LCSD LCS-L642252 LCSD-L642252 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits Dimethoate pg/L 20.0 11.1 8.79 55.5 43.9 40-140 Disulfoton pg/L 20.0 12.4 10.2 62.0 51.0 40-140 Ethyl Parathion pg/L 20.0 12.4 9.83 62.0 49.1 40-140 Famphur pg/L 20.0 13.6 11.1 68.0 55.5 40-140 Methyl Parathion pg/L 20.0 14.0 11.1 70.0 55.5 40-140 Phorate pg/L 20.0 12.1 10.0 60.5 50.0 40-140 0,0,0-Triethyl Phosphorothioate pg/L 20.0 12.6 10.8 63.0 54.0 40-140 Tributyl phosphate (S) 64.0 60.5 50-150 Triphenyl phosphate (S) 68.0 63.5 50-150 Rec Limits 50-150 50-150 RPD Max RPD 23.2* 20.0 19.4 20.0 23.1* 20.0 20.2* 20.0 23.1* 20.0 19.0 20.0 15.3 20.0 * QC Fail Date: 11/01/2022 02:04 PM Page 97 of 108 Page 24 of 33 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642250 QC Prep Batch Method: 3510C Lab Reagent Blank LRB-L642250 Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 QC Analytical Batch(es): L644470 Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 1,3-Dinitrobenzene pg/L <0.904 0.904 10.0 10/20/22 19:45 Acenaphthene pg/L <0.422 0.422 2.00 10/20/22 19:45 Acenaphthylene pg/L <0.429 0.429 2.00 10/20/22 19:45 Acetophenone pg/L <0.686 0.686 5.00 10/20/22 19:45 Anthracene pg/L <0.467 0.467 2.00 10/20/22 19:45 Benzo(a)anthracene pg/L <0.427 0.427 2.00 10/20/22 19:45 Benzo(a)pyrene pg/L <1.00 1.00 2.00 10/20/22 19:45 Benzo(b)fluoranthene pg/L <0.941 0.941 2.00 10/20/22 19:45 Benzo(g,h,i)perylene pg/L <1.36 1.36 2.00 10/20/22 19:45 Benzo(k)fluoranthene pg/L <0.752 0.752 2.00 10/20/22 19:45 Benzyl alcohol pg/L <3.01 3.01 10.0 10/20/22 19:45 Bis(2-Chloroethoxy)methane pg/L <0.433 0.433 5.00 10/20/22 19:45 Bis(2-Chloroethyl)ether pg/L <0.447 0.447 5.00 10/20/22 19:45 Bis(2-Chloroisopropyl)ether pg/L <0.546 0.546 5.00 10/20/22 19:45 Bis(2-ethylhexyl)phthalate pg/L <3.66 3.66 5.00 10/20/22 19:45 4-Bromophenyl phenyl ether pg/L <0.500 0.500 5.00 10/20/22 19:45 Butyl benzyl phthalate pg/L <4.59 4.59 5.00 10/20/22 19:45 4-Chloro-3-methylphenol pg/L <0.503 0.503 5.00 10/20/22 19:45 4-Chloroaniline pg/L <0.526 0.526 5.00 10/20/22 19:45 Chlorobenzilate pg/L <1.90 1.90 5.00 10/20/22 19:45 2-Chloronaphthalene pg/L <0.476 0.476 5.00 10/20/22 19:45 2-Chlorophenol pg/L <0.736 0.736 5.00 10/20/22 19:45 4-Chlorophenyl phenyl ether pg/L <0.479 0.479 5.00 10/20/22 19:45 Chrysene pg/L <0.731 0.731 2.00 10/20/22 19:45 Dibenz(a,h)anthracene pg/L <0.252 0.252 2.00 10/20/22 19:45 Dibenzofuran pg/L <0.423 0.423 5.00 10/20/22 19:45 1,2-Dichlorobenzene pg/L <0.629 0.629 5.00 10/20/22 19:45 Date: 11/01/2022 02:04 PM Page 25 of 33 Page 98 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642250 QC Prep Batch Method: 3510C Lab Reagent Blank LRB-L642250 Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 QC Analytical Batch(es): L644470 Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 1,3-Dichlorobenzene pg/L <0.491 0.491 5.00 10/20/22 19:45 1,4-Dichlorobenzene pg/L <0.580 0.580 5.00 10/20/22 19:45 3,3'-Dichlorobenzidine pg/L <3.74 3.74 10.0 10/20/22 19:45 2,4-Dichlorophenol pg/L <1.52 1.52 5.00 10/20/22 19:45 2,6-Dichlorophenol pg/L <0.703 0.703 5.00 10/20/22 19:45 Diethyl phthalate pg/L <0.585 0.585 5.00 10/20/22 19:45 Dimethyl phthalate pg/L <0.510 0.510 5.00 10/20/22 19:45 3,3' Dimethylbenzidine pg/L <1.88 1.88 10.0 10/20/22 19:45 2,4-Dimethylphenol pg/L <0.674 0.674 5.00 10/20/22 19:45 Di-n-butyl phthalate pg/L <1.58 1.58 5.00 10/20/22 19:45 4,6- Din itro-2-methylphenol pg/L <3.47 3.47 10.0 10/20/22 19:45 2,4-Dinitrophenol pg/L <4.85 4.85 10.0 10/20/22 19:45 2,4-Dinitrotoluene pg/L <0.403 0.403 5.00 10/20/22 19:45 2,6-Dinitrotoluene pg/L <0.413 0.413 5.00 10/20/22 19:45 Di-n-Octyl Phthalate pg/L <1.72 1.72 5.00 10/20/22 19:45 Ethyl methanesulfonate pg/L <0.714 0.714 5.00 10/20/22 19:45 Fluoranthene pg/L <0.406 0.406 2.00 10/20/22 19:45 Fluorene pg/L <0.444 0.444 2.00 10/20/22 19:45 Hexachlorobenzene pg/L <2.57 2.57 5.00 10/20/22 19:45 Hexachlorobutadiene pg/L <0.405 0.405 5.00 10/20/22 19:45 Hexachlorocyclopentadiene pg/L <2.34 2.34 5.00 10/20/22 19:45 Hexachloroethane pg/L <0.277 0.277 5.00 10/20/22 19:45 Indeno(1,2,3-cd)pyrene pg/L <1.01 1.01 2.00 10/20/22 19:45 Isophorone pg/L <0.360 0.360 5.00 10/20/22 19:45 Methyl methanesulfonate pg/L <0.618 0.618 5.00 10/20/22 19:45 2-Methylnaphthalene pg/L <0.485 0.485 2.00 10/20/22 19:45 2-Methylphenol pg/L <0.721 0.721 5.00 10/20/22 19:45 Date: 11/01/2022 02:04 PM Page 26 of 33 Page 99 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642250 QC Prep Batch Method: 3510C Lab Reagent Blank LRB-L642250 Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 QC Analytical Batch(es): L644470 Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 3&4 Methylphenol pg/L <0.691 0.691 5.00 10/20/22 19:45 Naphthalene pg/L <0.484 0.484 2.00 10/20/22 19:45 2-Nitroaniline pg/L <0.574 0.574 5.00 10/20/22 19:45 3-Nitroaniline pg/L <1.53 1.53 10.0 10/20/22 19:45 4-Nitroaniline pg/L <0.740 0.740 5.00 10/20/22 19:45 Nitrobenzene pg/L <0.531 0.531 5.00 10/20/22 19:45 2-Nitrophenol pg/L <0.606 0.606 5.00 10/20/22 19:45 4-Nitrophenol pg/L <1.39 1.39 10.0 10/20/22 19:45 N-Nitrosodimethylamine pg/L <0.249 0.249 5.00 10/20/22 19:45 N-Nitrosodiphenylamine pg/L <0.783 0.783 10.0 10/20/22 19:45 N-Nitrosodiethylamine pg/L <0.400 0.400 5.00 10/20/22 19:45 N-Nitroso-di-n-butylamine pg/L <0.752 0.752 5.00 10/20/22 19:45 N-Nitroso-di-n-propylamine pg/L <0.334 0.334 5.00 10/20/22 19:45 Pentachloronitrobenzene pg/L <1.15 1.15 5.00 10/20/22 19:45 Pentachlorophenol pg/L <2.45 2.45 10.0 10/20/22 19:45 Phenacetin pg/L <1.28 1.28 5.00 10/20/22 19:45 Phenanthrene pg/L <0.464 0.464 2.00 10/20/22 19:45 Phenol pg/L <0.389 0.389 5.00 10/20/22 19:45 Pyrene pg/L <1.04 1.04 2.00 10/20/22 19:45 1,2,4,5-Tetrachlorobenzene pg/L <0.317 0.317 5.00 10/20/22 19:45 2,3,4,6-Tetrachlorophenol pg/L <0.355 0.355 5.00 10/20/22 19:45 1,2,4-Trichlorobenzene pg/L <0.482 0.482 5.00 10/20/22 19:45 2,4,5-Trichlorophenol pg/L <0.350 0.350 5.00 10/20/22 19:45 2,4,6-Trichlorophenol pg/L <0.344 0.344 5.00 10/20/22 19:45 2-Fluorobiphenyl(S) 10/20/22 19:45 54.3 24-93 2-Fluorophenol(S) 10/20/22 19:45 21.2 10-44 Nitrobenzene-d5 (S) 10/20/22 19:45 54.4 20-91 Date: 11/01/2022 02:04 PM Page 27 of 33 Page 100 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642250 QC Analytical Batch(es): L644470 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Lab Reagent Blank LRB-L642250 Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Phenol-d6 (S) 10/20/22 19:45 13.6 7-32 4-Terphenyl-d14 (S) 10/20/22 19:45 63.6 35-126 2,4,6-Tribromophenol(S) 10/20/22 19:45 62.4 39-110 Laboratory Control Sample & LCSD LCS-L642250 LCSD-L642250 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD 1,3-Dinitrobenzene pg/L 50.0 48.6 43.3 97.2 86.6 45-135 11.5 20.0 Acenaphthene pg/L 50.0 30.2 26.1 60.4 52.2 38-117 14.5 20.0 Acenaphthylene pg/L 50.0 25.3 22.1 50.6 44.2 37-114 13.5 20.0 Acetophenone pg/L 50.0 29.1 25.1 58.2 50.2 25-108 14.7 20.0 Anthracene pg/L 50.0 29.2 25.7 58.4 51.4 34-128 12.7 20.0 Benzo(a)anthracene pg/L 50.0 31.7 27.4 63.4 54.8 36-127 14.5 20.0 Benzo(a)pyrene pg/L 50.0 30.1 26.2 60.2 52.4 34-131 13.8 20.0 Benzo(b)fluoranthene pg/L 50.0 32.2 26.4 64.4 52.8 36-131 19.7 20.0 Benzo(g,h,i)perylene pg/L 50.0 27.5 25.9 55.0 51.8 26-123 5.9 20.0 Benzo(k)fluoranthene pg/L 50.0 35.1 31.5 70.2 63.0 32-132 10.8 20.0 Benzyl alcohol pg/L 50.0 19.6 17.3 39.2 34.6 20-109 12.4 20.0 Bis(2-Chloroethoxy)methane pg/L 50.0 29.1 25.1 58.2 50.2 20-126 14.7 20.0 Bis(2-Chloroethyl)ether pg/L 50.0 26.0 22.3 52.0 44.6 16-122 15.3 20.0 Bis(2-Chloroisopropyl)ether pg/L 50.0 23.0 19.7 46.0 39.4 28-108 15.4 20.0 Bis(2-ethylhexyl)phthalate pg/L 50.0 33.0 29.6 66.0 59.2 21-162 10.8 20.0 4-Bromophenyl phenyl ether pg/L 50.0 32.8 28.6 65.6 57.2 31-124 13.6 20.0 Butyl benzyl phthalate pg/L 50.0 34.1 30.9 68.2 61.8 33-142 9.8 20.0 4-Chloro-3-methyl phenol pg/L 50.0 27.0 24.6 54.0 49.2 35-117 9.3 20.0 4-Chloroaniline pg/L 50.0 21.6 18.2 43.2 36.4 24-127 17.0 20.0 Date: 11/01/2022 02:04 PM Page 28 of 33 Page 101 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642250 QC Analytical Batch(es): L644470 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-L642250 LCSD-L642250 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Chlorobenzilate pg/L 50.0 35.1 31.7 70.2 63.4 35-118 10.1 20.0 2-Chloronaphthalene pg/L 50.0 28.4 24.3 56.8 48.6 29-137 15.5 20.0 2-Chlorophenol pg/L 50.0 22.9 20.2 45.8 40.4 27-102 12.5 20.0 4-Chlorophenyl phenyl ether pg/L 50.0 31.9 27.9 63.8 55.8 39-110 13.3 20.0 Chrysene pg/L 50.0 28.7 25.0 57.4 50.0 30-124 13.7 20.0 Dibenz(a,h)anthracene pg/L 50.0 30.5 28.4 61.0 56.8 27-124 7.1 20.0 Dibenzofuran pg/L 50.0 32.0 28.2 64.0 56.4 40-108 12.6 20.0 1,2-Dichlorobenzene pg/L 50.0 25.4 22.0 50.8 44.0 26-100 14.3 20.0 1,3-Dichlorobenzene pg/L 50.0 24.1 21.3 48.2 42.6 21-102 12.3 20.0 1,4-Dichlorobenzene pg/L 50.0 24.1 21.0 48.2 42.0 24-99 13.7 20.0 3,3'-Dichlorobenzidine pg/L 150 86.9 78.6 57.9 52.4 6-192 10.0 20.0 2,4-Dichlorophenol pg/L 50.0 30.6 27.6 61.2 55.2 32-110 10.3 20.0 2,6-Dichlorophenol pg/L 50.0 31.8 27.7 63.6 55.4 25-112 13.7 20.0 Diethyl phthalate pg/L 50.0 31.6 28.9 63.2 57.8 36-130 8.9 20.0 Dimethyl phthalate pg/L 50.0 29.8 27.8 59.6 55.6 34-123 6.9 20.0 3,3' Dimethylbenzidine pg/L 200 36.4 30.6 18.2 15.3 6-192 17.3 20.0 2,4-Dimethylphenol pg/L 50.0 9.67 10.4 19.3* 20.8* 34-105 7.2 20.0 Di-n-butyl phthalate pg/L 50.0 31.0 27.2 62.0 54.4 19-158 13.0 20.0 4,6- Din itro-2-methylphenol pg/L 50.0 38.0 33.5 76.0 67.0 27-128 12.5 20.0 2,4-Dinitrophenol pg/L 150 88.6 78.7 59.0 52.4 10-132 11.8 20.0 2,4-Dinitrotoluene pg/L 50.0 31.0 28.0 62.0 56.0 24-147 10.1 20.0 2,6-Dinitrotoluene pg/L 50.0 31.7 28.1 63.4 56.2 36-125 12.0 20.0 Di-n-Octyl Phthalate pg/L 50.0 34.4 31.6 68.8 63.2 29-136 8.4 20.0 Ethyl methanesulfonate pg/L 50.0 26.9 22.8 53.8 45.6 20-121 16.4 20.0 Fluoranthene pg/L 50.0 30.6 27.1 61.2 54.2 28-127 12.1 20.0 Fluorene pg/L 50.0 31.7 28.2 63.4 56.4 41-116 11.6 20.0 * QC Fail Date: 11/01/2022 02:04 PM Page 29 of 33 Page 102 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642250 QC Analytical Batch(es): L644470 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-L642250 LCSD-L642250 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Hexachlorobenzene pg/L 50.0 32.9 29.0 65.8 58.0 18-136 12.6 20.0 Hexachlorobutadiene pg/L 50.0 28.0 23.9 56.0 47.8 22-109 15.7 20.0 Hexachlorocyclopentadiene pg/L 50.0 26.5 23.9 53.0 47.8 10-102 10.3 20.0 Hexachloroethane pg/L 50.0 24.5 21.6 49.0 43.2 16-107 12.5 20.0 Indeno(1,2,3-cd)pyrene pg/L 50.0 30.4 28.7 60.8 57.4 22-126 5.7 20.0 Isophorone pg/L 50.0 15.5 13.3 31.0 26.6* 31-116 15.2 20.0 Methyl methanesulfonate pg/L 50.0 18.2 15.5 36.4 31.0 15-82 16.0 20.0 2-Methylnaphthalene pg/L 50.0 30.4 26.5 60.8 53.0 34-108 13.7 20.0 2-Methylphenol pg/L 50.0 16.4 15.0 32.8 30.0 22-97 8.9 20.0 3&4 Methylphenol pg/L 50.0 17.0 15.8 34.0 31.6 21-96 7.3 20.0 Naphthalene pg/L 50.0 27.1 23.2 54.2 46.4 33-108 15.5 20.0 2-Nitroaniline pg/L 50.0 32.8 29.0 65.6 58.0 32-127 12.2 20.0 3-Nitroaniline pg/L 50.0 27.3 24.5 54.6 49.0 28-142 10.8 20.0 4-Nitroaniline pg/L 50.0 36.6 33.5 73.2 67.0 23-139 8.8 20.0 Nitrobenzene pg/L 50.0 27.2 23.4 54.4 46.8 27-117 15.0 20.0 2-Nitrophenol pg/L 50.0 30.6 26.0 61.2 52.0 25-114 16.2 20.0 4-Nitrophenol pg/L 50.0 7.40 6.71 14.8 13.4 1-76 9.7 20.0 N-Nitrosodimethylamine pg/L 50.0 13.5 11.4 27.0 22.8 14-84 16.8 20.0 N-Nitrosodiphenylamine pg/L 50.0 26.7 23.7 53.4 47.4 45-135 11.9 20.0 N-Nitrosodiethylamine pg/L 50.0 28.3 23.9 56.6 47.8 25-107 16.8 20.0 N-Nitroso-di-n-butylamine pg/L 50.0 29.8 26.1 59.6 52.2 25-126 13.2 20.0 N-Nitroso-di-n-propylamine pg/L 50.0 26.2 22.6 52.4 45.2 29-114 14.7 20.0 Pentachloronitrobenzene pg/L 50.0 36.2 32.9 72.4 65.8 34-135 9.5 20.0 Pentachlorophenol pg/L 50.0 16.7 11.7 33.4 23.4 17-142 35.2* 20.0 Phenacetin pg/L 50.0 30.1 27.3 60.2 54.6 29-141 9.7 20.0 Phenanthrene pg/L 50.0 28.2 24.9 56.4 49.8 40-120 12.4 20.0 * QC Fail Date: 11/01/2022 02:04 PM Page 30 of 33 Page 103 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642250 QC Analytical Batch(es): L644470 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-L642250 LCSD-L642250 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD Phenol pg/L 50.0 7.87 7.37 15.7 14.7 11-55 6.5 20.0 Pyrene pg/L 50.0 33.5 30.4 67.0 60.8 20-154 9.7 20.0 1,2,4,5-Tetrachlorobenzene pg/L 50.0 29.9 25.7 59.8 51.4 28-110 15.1 20.0 2,3,4,6-Tetrachlorophenol pg/L 50.0 29.6 26.1 59.2 52.2 28-118 12.5 20.0 1,2,4-Trichlorobenzene pg/L 50.0 27.9 23.9 55.8 47.8 23-106 15.4 20.0 2,4,5-Trichlorophenol pg/L 50.0 31.3 27.0 62.6 54.0 26-118 14.7 20.0 2,4,6-Trichlorophenol pg/L 50.0 31.7 27.4 63.4 54.8 26-115 14.5 20.0 2-Fluorobiphenyl (S) 54.0 50.2 24-93 2-Fluorophenol (S) 20.6 19.8 10-44 Nitrobenzene-d5 (S) 54.0 49.4 20-91 Phenol-d6 (S) 13.7 13.1 7-32 4-Terphenyl-d14 (S) 65.3 63.3 35-126 2,4,6-Tribromophenol(S) 64.9 60.2 39-110 Date: 11/01/2022 02:04 PM Page 31 of 33 Page 104 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642251 QC Analytical Batch(es): L644471 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: 8270 Extended List Lab Reagent Blank LRB-L642251 Matrix: AQU Associated Lab Samples: 90039, 90040, 90041, 90042, 90043 Blank MDL MQL Analyzed Parameter Units Result 1,3,5-Trinitrobenzene pg/L <10.0 10.0 10.0 10/20/2219:45 Isodrin pg/L <10.0 10.0 10.0 10/20/2219:45 Kepone pg/L <10.0 10.0 10.0 10/20/22 19:45 1,4-Naphthoquinone pg/L <10.0 10.0 10.0 10/20/2219:45 1-Naphthylamine pg/L <10.0 10.0 10.0 10/20/2219:45 2-Acetylaminofluorene pg/L <10.0 10.0 10.0 10/20/2219:45 2-Naphthylamine pg/L <10.0 10.0 10.0 10/20/2219:45 3-Methylcholanthrene pg/L <10.0 10.0 10.0 10/20/2219:45 4-Aminobiphenyl pg/L <10.0 10.0 10.0 10/20/2219:45 5-Nitro-o-toluidine pg/L <10.0 10.0 10.0 10/20/2219:45 7,12-Di methyl benz(a)anth racene pg/L <10.0 10.0 10.0 10/20/2219:45 Diallate pg/L <10.0 10.0 10.0 10/20/2219:45 Hexachloropropene pg/L <10.0 10.0 10.0 10/20/2219:45 Isosafrole pg/L <10.0 10.0 10.0 10/20/2219:45 Methapyrilene pg/L <10.0 10.0 20.0 10/20/2219:45 N-Nitrosomethylethylamine pg/L <10.0 10.0 10.0 10/20/2219:45 N-Nitrosomorpholine pg/L <10.0 10.0 10.0 10/20/2219:45 N-Nitrosopiperidine pg/L <10.0 10.0 10.0 10/20/2219:45 N-Nitrosopyrrolidine pg/L <10.0 10.0 10.0 10/20/2219:45 o-Toluidine pg/L <10.0 10.0 10.0 10/20/2219:45 p-Dimethylaminoazobenzene pg/L <10.0 10.0 10.0 10/20/2219:45 p-Phenylenediamine pg/L <10.0 10.0 10.0 10/20/2219:45 Pronamide pg/L <10.0 10.0 10.0 10/20/2219:45 Safrole pg/L <10.0 10.0 10.0 10/20/2219:45 Date: 11/01/2022 02:04 PM Page 32 of 33 Page 105 of 108 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-279-0018 QC Prep: L642251 QC Analytical Batch(es): L644471 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: 8270 Extended List Laboratory Control Sample & LCSD LCS-L642251 LCSD-L642251 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD 1,3,5-Trinitrobenzene pg/L 50.0 29.8 33.8 59.6 67.6 20-120 12.5 20.0 Isodrin pg/L 50.0 28.9 28.7 57.8 57.4 20-120 0.6 20.0 Kepone pg/L 50.0 27.4 30.3 54.8 60.6 20-120 10.0 20.0 1,4-Naphthoquinone pg/L 50.0 13.9 14.7 27.8 29.4 20-120 5.5 20.0 1-Naphthylamine pg/L 50.0 10.3 <10.0 20.6 0.0* 20-120 2.9 20.0 2-Acetylaminofluorene pg/L 50.0 29.7 31.5 59.4 63.0 20-120 5.8 20.0 2-Naphthylamine pg/L 50.0 23.8 20.1 47.6 40.2 20-120 16.8 20.0 3-Methylcholanthrene pg/L 50.0 24.7 23.8 49.4 47.6 20-120 3.7 20.0 4-Aminobiphenyl pg/L 50.0 25.7 21.8 51.4 43.6 20-120 16.4 20.0 5-Nitro-o-toluidine pg/L 50.0 28.6 30.7 57.2 61.4 20-120 7.0 20.0 7,12-Di methyl benz(a)anth racene pg/L 50.0 20.5 19.7 41.0 39.4 20-120 3.9 20.0 Diallate pg/L 50.0 27.7 27.2 55.4 54.4 20-120 1.8 20.0 Hexachloropropene pg/L 50.0 18.2 18.8 36.4 37.6 20-120 3.2 20.0 Isosafrole pg/L 50.0 20.5 22.7 41.0 45.4 20-120 10.1 20.0 Methapyrilene pg/L 50.0 27.6 20.5 55.2 41.0 20-120 29.5* 20.0 N-Nitrosomethylethylamine pg/L 50.0 21.0 20.1 42.0 40.2 20-120 4.3 20.0 N-Nitrosomorpholine pg/L 50.0 20.4 19.8 40.8 39.6 20-120 2.9 20.0 N-Nitrosopiperidine pg/L 50.0 23.2 24.0 46.4 48.0 20-120 3.3 20.0 N-Nitrosopyrrolidine pg/L 50.0 22.7 21.8 45.4 43.6 20-120 4.0 20.0 o-Toluidine pg/L 50.0 25.2 19.4 50.4 38.8 20-120 26.0* 20.0 p-Dimethylaminoazobenzene pg/L 50.0 28.9 28.0 57.8 56.0 20-120 3.1 20.0 p-Phenylenediamine pg/L 50.0 <10.0 <10.0 0.0* 0.0* 20-120 0.0 20.0 Pronamide pg/L 50.0 29.5 30.7 59.0 61.4 20-120 3.9 20.0 Safrole pg/L 50.0 24.1 24.8 48.2 49.6 20-120 2.8 20.0 * QC Fail Date: 11/01/2022 02:04 PM Page 33 of 33 Page 106 of 108 WayPAoint. NALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: 01015 Customer Name: Anchor QEA of North Carolina, PLLC Report Number: 22-279-0018 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client # Courier 0 Other: Thermometer ID: IRT-15 2.7C Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F Custody seals intact on shipping container/cooler? (*� Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample Iabel(s)? (0) Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? U Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? U Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. U Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No U N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F Low concentration EnCore samplers (48 hr) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: ngelo Norvell Date & Time: 10/06/2022 12:50:51 Page 107 of 108 N { G7 V1 mi1 9 9 — J L� z m w e m - m m 3 O � v m' Q d to a H '• v CMo �? a rfl ° L. L. C d5 1 ? `N A -a v -n N , c n 3 D • '�pp sl � S Y S CA (A Zr to W !�� Q V O N. Sp 51 -4 1 Y� Z n �1 C o Y w w Vie' n ay N W v a C) n--yy� i 'm ❑ TF L LLGf� x a Q ma y °wr- n0L ern es �m ❑ x ,a��f z0 g >e a +� Lj n a v w :5.r [� `� 3 0 O a p �� mo �JL1 c� nv S"n wac�m g • L L Va 21 ad ¢� GN N myOZ. r� D fA 3.0 � � N C L C., � a mp �c g 7b0 Zo rL L L CD © n m $ z m ((pp m .,,5 > d Z N m x=n� D Q r n 3 x ^+ --m. o❑ rA CL m v m L: ar m Yta m r m a OX U m Z (0)n =A �. z o m°"- g 6 x ° 0 0= S LL7v �❑ 3 ca ,Zi i•+Ha m : A x n j a m >0m C.) m F [1 Z2�n� p -3 -�i L W 0 N m Q' LZX �� Mcn M CCL O x W� n nOka N , m N n•� L7 Zy n ❑ a� p U / Q 0FL �C L� Ng a N m _ N n ANC �a �o v ❑ G 0 N fA to m •, f �� n v� N m �Q�rcn�_ �m 3 r Q, N [] ! TI x "= a m [mod �C v p 1^' m a V7 N z a � p oyaTs�"A'n o a Q 7 p c $ 7 [; 7 ui O� a p a m '$ o m Q C) N y :. Anchor ❑EA of North Caro;ma, PLLC 12'27:34 a• "' "J ❑ a Jackson County C Z h a � a � m a . y m a a ►� z,t m ri zrf III�I n o � x lf+ LL— o r l l l i n Page 108 of 108 Waypointo ANALYTICAL 11 /9/2022 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville, NC, 28801 Ref: Analytical Testing Lab Report Number: 22-277-0040 Client Project Description: Jackson County C21480-01.01, WA-1 Site: 58-02 Project Number: 58-02 Dear Chuck Pippin: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/4/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, a,j Angela D Overcash Senior Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 123 0 Waypoint. ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12/31/2022 South Carolina State Program 99012 07/31/2023 South Carolina State Program 99012 12/31/2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00016/22-277-0040 Page 2 of 123 Waypoint. (2) ANALYTICAL Sample Report Number: 22-277-0040 Client Project Description: Jackson County C2148O-01.01, WA-1 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca I som Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 89898 MW-02-20221003 Aqueous 10/03/2022 10:00 10/04/2022 14:06 89898 MW-02-20221003 Aqueous 10/03/2022 10:00 10/04/2022 14:06 8270D WP MTN 89898 MW-02-20221003 Aqueous 10/03/2022 10:00 10/04/2022 14:06 8151A WP MTN 89898 MW-02-20221003 Aqueous 10/03/2022 10:00 10/04/2022 14:06 8081E WP MTN 89898 MW-02-20221003 Aqueous 10/03/2022 10:00 10/04/2022 14:06 6020E WP MTN 89898 MW-02-20221003 Aqueous 10/03/2022 10:00 10/04/2022 14:06 8270C WP MTN 89898 MW-02-20221003 Aqueous 10/03/2022 10:00 10/04/2022 14:06 8270D WP MTN 89901 MW-05R-20221003 Aqueous 10/03/2022 15:30 10/04/2022 14:06 89901 MW-05R-20221003 Aqueous 10/03/2022 15:30 10/04/2022 14:06 8270C WP MTN 89901 MW-05R-20221003 Aqueous 10/03/2022 15:30 10/04/2022 14:06 8270D WP MTN 89901 MW-05R-20221003 Aqueous 10/03/2022 15:30 10/04/2022 14:06 8270D WP MTN 89901 MW-05R-20221003 Aqueous 10/03/2022 15:30 10/04/2022 14:06 8151A WP MTN 89901 MW-05R-20221003 Aqueous 10/03/2022 15:30 10/04/2022 14:06 8081E WP MTN 89901 MW-05R-20221003 Aqueous 10/03/2022 15:30 10/04/2022 14:06 6020E WP MTN 89902 MW-07-20221003 Aqueous 10/03/2022 12:40 10/04/2022 14:06 89902 MW-07-20221003 Aqueous 10/03/2022 12:40 10/04/2022 14:06 8270C WP MTN 89902 MW-07-20221003 Aqueous 10/03/2022 12:40 10/04/2022 14:06 8270D WP MTN 89902 MW-07-20221003 Aqueous 10/03/2022 12:40 10/04/2022 14:06 8270D WP MTN 89902 MW-07-20221003 Aqueous 10/03/2022 12:40 10/04/2022 14:06 8151A WP MTN 89902 MW-07-20221003 Aqueous 10/03/2022 12:40 10/04/2022 14:06 8081E WP MTN 89903 SW-01-20221003 Aqueous 10/03/2022 13:15 10/04/2022 14:06 89903 SW-01-20221003 Aqueous 10/03/2022 13:15 10/04/2022 14:06 8151A WP MTN 89903 SW-01-20221003 Aqueous 10/03/2022 13:15 10/04/2022 14:06 8081E WP MTN 89904 SW-02-20221003 Aqueous 10/03/2022 14:40 10/04/2022 14:06 89904 SW-02-20221003 Aqueous 10/03/2022 14:40 10/04/2022 14:06 8151A WP MTN 89904 SW-02-20221003 Aqueous 10/03/2022 14:40 10/04/2022 14:06 8081E WP MTN : Pace Analytical - Huntersville, NC, Huntersville, NC WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 123 Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointana lyti ca I som Sample Summary Table Report Number: 22-277-0040 Client Project Description: Jackson County C21480-01.01, WA-1 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 89904 SW-02-20221003 Aqueous 10/03/2022 14:40 10/04/2022 14:06 6020B WP MTN 89905 LT-01-20221003 Aqueous 10/03/2022 16:00 10/04/2022 14:06 89905 LT-01-20221003 Aqueous 10/03/2022 16:00 10/04/2022 14:06 6020E WP MTN 89906 DW-01-20221003 Aqueous 10/03/2022 17:45 10/04/2022 14:06 524.2 89907 DW-02-20221003 Aqueous 10/03/2022 17:05 10/04/2022 14:06 524.2 89908 TB-20221003-1 Aqueous 10/03/2022 10/04/2022 14:06 524.2 89909 TB-20221003-2 Aqueous 10/03/2022 10/04/2022 14:06 : Pace Analytical - Huntersville, NC, Huntersville, NC WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 4 of 123 Waypoint (D 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytica Isom Summary of Detected Analytes Project: Jackson County Report Number: 22-277-0040 Client Sample ID Lab Sample ID Method Parameters MW-02-20221003 V 89898 Result Units Report Limit Analyzed 6020B Arsenic 10.1 pg/L 2.45 10/10/2022 20:12 6020E Barium 224 Ng/L 17.0 10/10/2022 20:12 6020E Dissolved Barium 204 pg/L 2.27 10/29/2022 14:08 6020E Dissolved Beryllium 0.908 Ng/L 0.510 10/29/2022 14:08 6020E Chromium 42.2 pg/L 5.00 10/10/2022 20:12 6020E Dissolved Chromium 37.0 Ng/L 1.73 10/29/2022 14:08 6020E Cobalt 40.7 pg/L 0.400 10/10/2022 20:12 6020E Dissolved Cobalt 41.0 Ng/L 0.300 10/29/2022 14:08 6020E Copper 41.8 pg/L 4.45 10/11/202217:15 6020E Dissolved Copper 30.7 Ng/L 2.45 10/29/2022 14:08 6020E Lead 9.82 pg/L 2.50 10/10/2022 20:12 6020E Dissolved Lead 8.37 Ng/L 1.32 10/29/2022 14:08 6020E Dissolved Nickel 29.7 pg/L 0.910 10/29/2022 14:08 6020E Nickel 32.0 pg/L 3.60 10/10/2022 20:12 6020E Selenium 36.2 pg/L 11.5 10/10/2022 20:12 6020E Dissolved Thallium 0.850 Ng/L 0.305 10/29/2022 14:08 6020E Vanadium 52.3 pg/L 10.5 10/10/2022 20:12 6020E Dissolved Vanadium 42.1 Ng/L 3.84 10/29/2022 14:08 6020E Zinc 103 pg/L 19.5 10/10/2022 20:12 6020E Dissolved Zinc 175 Ng/L 23.4 10/29/2022 14:08 8260D 1,1-Dichloroethane 0.386 pg/L 0.240 10/10/202218:12 8260D cis- 1,2-Dichloroethene 0.223 Ng/L 0.200 10/10/202218:12 MW-OSR-20221003 V 89901 6020B Arsenic 0.590 pg/L 0.490 10/10/202218:58 6020B Dissolved Arsenic 3.36 Ng/L 0.297 10/29/2022 14:22 6020B Barium 246 pg/L 34.0 10/17/2022 22:00 6020E Dissolved Barium 153 Ng/L 0.453 10/29/2022 14:22 6020E Chromium 2.76 pg/L 1.00 10/10/202218:58 6020E Cobalt 15.9 Ng/L 0.080 10/10/202218:58 6020E Dissolved Cobalt 10.5 pg/L 0.060 10/29/2022 14:22 6020E Copper 4.19 Ng/L 0.890 10/11/202216:02 6020E Dissolved Copper 0.690 pg/L 0.489 10/29/2022 14:22 6020E Lead 0.993 Ng/L 0.500 10/10/202218:58 6020E Dissolved Nickel 2.69 pg/L 0.182 10/29/2022 14:22 6020E Nickel 4.66 Ng/L 0.720 10/10/202218:58 6020B Dissolved Thallium 0.0874 pg/L 0.0610 10/29/2022 14:22 Qualifiers 0 0 I IJ I I Page 5 of 123 Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointana lyti ca I som Summary of Detected Analytes Project: Jackson County Report Number: 22-277-0040 Client Sample ID Lab Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers MW-OSR-20221003 V 89901 6020B Vanadium 3.31 pq/L 2.10 10/10/202218:58 J 6020B Zinc 12.6 Ng/L 3.90 10/10/202218:58 J 6020B Dissolved Zinc 5.17 uq/L 4.67 10/29/2022 14:22 JB 8151A 2,4,5-TP (Silvex) 0.02419 Ng/L 0.01634 10/14/2022 21:33 J 8260D Benzene 1.63 uq/L 0.180 10/10/202218:39 8260D Chlorobenzene 7.09 Ng/L 0.190 10/10/202218:39 8260D 1,2-Dichlorobenzene 0.286 uq/L 0.220 10/10/202218:39 J 8260D 1,4-Dichlorobenzene 7.29 pg/L 0.210 10/10/202218:39 8260D cis- 1,2-Dichloroethene 2.18 uq/L 0.200 10/10/202218:39 8260D Tetrahydrofuran 2.76 pg/L 1.50 10/10/202218:39 J 8260D Toluene 0.237 pq/L 0.220 10/10/202218:39 J 8260D Vinyl Chloride 0.563 Ng/L 0.170 10/10/2022 18:39 8270D 1,4-Dichlorobenzene 3.47 pq/L 0.644 10/20/2022 20:26 J MW-07-20221003 V 89902 6020B Barium 422 Ng/L 34.0 10/17/2022 22:07 6020B Cobalt 2.12 uq/L 0.080 10/10/202219:05 6020B Copper 2.72 Ng/L 0.890 10/11/202216:08 6020B Nickel 7.41 uq/L 0.720 10/10/202219:05 6020B Tin 2.09 Ng/L 1.50 10/10/202219:05 J 6020B Zinc 14.9 uq/L 3.90 10/10/202219:05 J 8260D Benzene 1.56 Ng/L 0.180 10/10/202219:06 8260D Chlorobenzene 4.46 uq/L 0.190 10/10/202219:06 8260D 1,2-Dichlorobenzene 0.319 Ng/L 0.220 10/10/202219:06 J 8260D 1,4-Dichlorobenzene 4.58 uq/L 0.210 10/10/202219:06 8260D cis- 1,2-Dichloroethene 2.01 Ng/L 0.200 10/10/202219:06 8260D SIM 1,4-Dioxane 17.6 uq/L 0.139 10/06/2022 12:25 8270D 1,4-Dichlorobenzene 2.44 Ng/L 0.580 10/20/2022 20:46 J SW-01-20221003 V 89903 6020B Barium 14.1 pg/L 3.40 10/10/202219:11 6020B Chromium 1.90 pg/L 1.00 10/10/202219:11 J 6020B Cobalt 0.224 uq/L 0.080 101101202219:11 J 6020B Copper 2.37 Ng/L 0.890 10/11/202216:29 6020B Zinc 4.85 pg/L 3.90 101101202219:11 J SW-02-20221003 V 89904 4500S2F-2011 Sulfide 0.90 mg/L 0.83 10/10/202211:00 J Page 6 of 123 Waypoint (D 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 AN LYT I CAL www.waypointanalytica Isom Summary of Detected Analytes Project: Jackson County Report Number: 22-277-0040 Client Sample ID Lab Sample ID Method Parameters Result Units Report Limit Analyzed SW-02-20221003 V 89904 6020B Arsenic 0.416 pg/L 0.297 11/01/202217:01 6020E Barium 15.2 pg/L 0.453 10/28/2022 23:01 6020E Chromium 0.638 pg/L 0.346 10/28/2022 23:01 6020E Cobalt 0.248 pg/L 0.060 10/28/2022 23:01 6020E Copper 1.47 pg/L 0.489 10/28/2022 23:01 6020E Lead 0.266 pg/L 0.264 10/28/2022 23:01 6020B Nickel 0.552 pg/L 0.182 10/28/2022 23:01 6020B Zinc 13.9 pg/L 4.67 10/28/2022 23:01 LT-01-20221003 V 89905 6020B Arsenic 85.7 pg/L 2.45 10/10/202219:45 6020E Dissolved Arsenic 12.3 pg/L 2.97 10/29/2022 14:26 6020E Barium 4460 pg/L 4.53 10/28/202211:05 6020E Dissolved Barium 410 pg/L 4.53 10/29/2022 14:26 6020E Beryllium 10.6 pg/L 1.20 10/10/202219:45 6020E Chromium 476 pg/L 5.00 10/10/202219:45 6020E Dissolved Chromium 6.09 pg/L 3.46 10/29/2022 14:26 6020E Cobalt 151 pg/L 0.400 10/10/202219:45 6020E Dissolved Cobalt 9.56 pg/L 0.600 10/29/2022 14:26 6020E Copper 238 pg/L 4.45 10/11/202217:02 6020E Lead 86.4 pg/L 2.50 10/10/202219:45 6020E Dissolved Nickel 33.4 pg/L 1.82 10/29/2022 14:26 6020E Nickel 232 pg/L 3.60 10/10/202219:45 6020E Selenium 125 pg/L 11.5 10/10/202219:45 6020E Tin 18.7 pg/L 7.50 10/10/202219:45 6020E Thallium 2.98 pg/L 1.40 10/10/202219:45 6020E Vanadium 581 pg/L 10.5 10/10/202219:45 6020E Zinc 764 pg/L 19.5 10/10/202219:45 8260D Benzene 0.568 pg/L 0.180 10/11/2022 02:18 8260D Carbon Disulfide 0.683 pg/L 0.150 10/11/2022 02:18 8260D Chlorobenzene 1.39 pg/L 0.190 10/11/2022 02:18 8260D 1,4-Dichlorobenzene 1.82 pg/L 0.210 10/11/2022 02:18 8260D Ethylbenzene 0.267 pg/L 0.170 10/11/2022 02:18 8260D Methyl Ethyl Ketone (MEK) 2.36 pg/L 0.710 10/11/2022 02:18 8260D 4-Methyl-2-Pentanone 1.12 pg/L 1.00 10/11/2022 02:18 8260D Naphthalene 3.66 pg/L 0.470 10/11/2022 02:18 8260D Tetrahydrofuran 67.8 pg/L 1.50 10/11/2022 02:18 Qualifiers 0 0 I 0 I Page 7 of 123 Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointana lyti ca I som Summary of Detected Analytes Project: Jackson County Report Number: 22-277-0040 Client Sample ID Lab Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers LT-01-20221003 V 89905 8260D Toluene 8260D o-Xylene 8260D Xylene (Total) 8260D SIM 1,4-Dioxane TB-20221003-2 V 89909 8260D Methylene Chloride 0.240 0.465 0.465 80.0 0.411 pq/L 0.220 10/11/2022 02:18 1 Ng/L 0.210 10/11/2022 02:18 1 uq/L 0.210 10/11/2022 02:18 1 pg/L 0.139 10/06/202213:40 pq/L 0.330 101101202213:42 1 Page 8 of 123 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-277-0040 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/09/2022 Received : 10/04/2022 Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane <0.139 Ng/L 0.139 2.00 1 10/06/22 11:35 TBL 8260D SIM 1,4-Naphthoquinone <11.8 pg/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D 1-Naphthylamine <11.8 Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D 2-Acetylaminofluorene <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D 2-Naphthylamine <11.8 Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D 3-Methylcholanthrene <11.8 pg/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D 4-Aminobiphenyl <11.8 Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D 5-Nitro-o-toluidine <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D 7,12-Dimethyl benz(a)anth racene <11.8 Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D Diallate <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D Hexachloropropene <11.8 Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D Isosafrole <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D Methapyrilene <11.8 Ng/L 11.8 23.5 1 10/20/22 20:06 VBW 8270D N-Nitrosomethylethylamine <11.8 pg/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D N-Nitrosomorpholine <11.8 Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D N-Nitrosopyrrolidine <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D N-Nitrosopiperidine <11.8 Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D 0,0,0-Triethyl Phosphorothioate <0.389 pg/L 0.389 1.18 1 10/24/22 14:46 VBW 8270C o-Toluidine <11.8 Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D p-Dimethylaminoazobenzene <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D p-Phenylenediamine <11.8 M Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D Pronamide <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D Safrole <11.8 Ng/L 11.8 11.8 1 10/20/22 20:06 VBW 8270D Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 9 of 123 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-277-0040 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/09/2022 Received : 10/04/2022 Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Thionazine <0.389 Ng/L 0.389 1.18 1 10/24/2214:46 VBW 8270C Sulfide <0.83 mg/L 0.83 2.00 1 10/10/2211:00 SLO 4500S2F-2011 Antimony <3.40 Ng/L 3.40 10.0 5 10/10/22 20:12 EDV 6020B Dissolved Antimony <3.09 ug/L 3.09 5.00 1 10/29/22 14:08 BKN 6020B Arsenic 10.1 Ng/L 2.45 5.00 5 10/10/22 20:12 EDV 6020B Dissolved Arsenic <1.49 ug/L 1.49 5.00 1 10/29/22 14:08 BKN 6020B Barium 224 Ng/L 17.0 50.0 5 10/10/22 20:12 EDV 6020B Dissolved Barium 204 ug/L 2.27 5.00 1 10/29/22 14:08 BKN 6020B Beryllium <1.20 Ng/L 1.20 5.00 5 10/10/22 20:12 EDV 6020B Dissolved Beryllium 0.9083 ug/L 0.510 5.00 1 10/29/22 14:08 BKN 6020B Cadmium <0.750 Ng/L 0.750 5.00 5 10/10/22 20:12 EDV 6020B Dissolved Cadmium <1.75 ug/L 1.75 5.00 1 10/29/22 14:08 BKN 6020B Chromium 42.2 Ng/L 5.00 10.0 5 10/10/22 20:12 EDV 6020B Dissolved Chromium 37.0 ug/L 1.73 5.00 1 10/29/22 14:08 BKN 6020B Cobalt 40.7 Ng/L 0.400 5.00 5 10/10/22 20:12 EDV 6020B Dissolved Cobalt 41.0 ug/L 0.300 5.00 1 10/29/22 14:08 BKN 6020B Copper 41.8 Ng/L 4.45 10.0 5 10/11/2217:15 EDV 6020B Dissolved Copper 30.7 ug/L 2.45 5.00 1 10/29/22 14:08 BKN 6020B Lead 9.82 Ng/L 2.50 5.00 5 10/10/22 20:12 EDV 6020B Dissolved Lead 8.37 ug/L 1.32 5.00 1 10/29/22 14:08 BKN 6020B Mercury (Total) <0.0700 Ng/L 0.0700 0.200 1 10/11/22 15:55 EDV 7470A Dissolved Mercury <0.0700 ug/L 0.0700 0.200 1 10/24/22 15:30 EDV 7470A Dissolved Nickel 29.7 Ng/L 0.910 5.00 1 10/29/22 14:08 BKN 6020B Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 10 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89898 Sample ID: MW-02-20221003 Matrix: Aqueous Sampled: 10/3/2022 10:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Nickel 32.0 Ng/L 3.60 10.0 5 10/10/22 20:12 EDV 6020B Selenium 36.2 ug/L 11.5 25.0 5 10/10/22 20:12 EDV 6020B Dissolved Selenium <3.52 Ng/L 3.52 5.00 1 10/29/22 14:08 BKN 6020E Silver <0.650 ug/L 0.650 5.00 5 10/10/22 20:12 EDV 6020B Dissolved Silver <0.285 Ng/L 0.285 5.00 1 10/29/22 14:08 BKN 6020E Tin <7.50 ug/L 7.50 25.0 5 10/10/22 20:12 EDV 6020B Dissolved Tin <7.20 Ng/L 7.20 25.0 1 10/29/22 14:08 BKN 6020B Thallium <1.40 ug/L 1.40 10.0 5 10/10/22 20:12 EDV 6020B Dissolved Thallium 0.8503 Ng/L 0.305 5.00 1 10/29/22 14:08 BKN 6020B Vanadium 52.3 ug/L 10.5 25.0 5 10/10/22 20:12 EDV 6020B Dissolved Vanadium 42.1 Ng/L 3.84 25.0 1 10/29/22 14:08 BKN 6020B Zinc 103 ug/L 19.5 100 5 10/10/22 20:12 EDV 6020B Dissolved Zinc 175 Ng/L 23.4 50.0 1 10/29/22 14:08 BKN 6020B Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 11 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0025 H Ng/L 0.0025 0.0470 10 10/20/22 08:35 VIC L644344 alpha-BHC <0.0024 H ug/L 0.0024 0.0470 10 10/20/22 08:35 VIC L644344 beta-BHC <0.0024 H Ng/L 0.0024 0.0470 10 10/20/22 08:35 VIC L644344 delta-BHC <0.0018 H ug/L 0.0018 0.0470 10 10/20/22 08:35 VIC L644344 Chlordane <0.0259 H Ng/L 0.0259 0.235 10 10/20/22 08:35 VIC L644344 alpha -Chlordane <0.0024 H ug/L 0.0024 0.0470 10 10/20/22 08:35 VIC L644344 gamma -Chlordane <0.0017 H Ng/L 0.0017 0.0470 10 10/20/22 08:35 VIC L644344 4,4'-DDD <0.0025 H ug/L 0.0025 0.0470 10 10/20/22 08:35 VIC L644344 4,4'-DDE <0.0025 H Ng/L 0.0025 0.0470 10 10/20/22 08:35 VIC L644344 4,4'-DDT <0.0041 H ug/L 0.0041 0.0470 10 10/20/22 08:35 VIC L644344 Dieldrin <0.0018 H Ng/L 0.0018 0.0470 10 10/20/22 08:35 VIC L644344 EndosulfanI <0.0018 H ug/L 0.0018 0.0470 10 10/20/22 08:35 VIC L644344 EndosulfanII <0.0033 H Ng/L 0.0033 0.0470 10 10/20/22 08:35 VIC L644344 Endosulfan Sulfate <0.0017 H ug/L 0.0017 0.0470 10 10/20/22 08:35 VIC L644344 Endrin <0.0017 H Ng/L 0.0017 0.0470 10 10/20/22 08:35 VIC L644344 Endrin Aldehyde <0.0017 H ug/L 0.0017 0.0470 10 10/20/22 08:35 VIC L644344 Endrin Ketone <0.0017 H Ng/L 0.0017 0.0470 10 10/20/22 08:35 VIC L644344 gamma-BHC <0.0021 H ug/L 0.0021 0.0470 10 10/20/22 08:35 VIC L644344 Heptachlor <0.0017 H Ng/L 0.0017 0.0470 10 10/20/22 08:35 VIC L644344 Heptachlor Epoxide <0.0017 H ug/L 0.0017 0.0470 10 10/20/22 08:35 VIC L644344 Methoxychlor <0.0017 H Ng/L 0.0017 0.0470 10 10/20/22 08:35 VIC L644344 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 12 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 Lab No : 89898 Sample ID: MW-02-20221003 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/3/2022 10:00 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0236 H Ng/L 0.0236 0.353 10 10/20/22 08:35 VIC L644344 Surrogate: Decachlorobiphenyl 77.8 Limits: 36-116% 10 10/20/22 08:35 L644344 Surrogate: Tetrachloro-m-xylene 69.7 Limits: 25-123% 10 10/20/22 08:35 L644344 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2099 Pg/L 0.2099 0.2525 1 10/14/22 21:08 VIC L643610 Dalapon <0.5201 Ng/L 0.5201 0.5556 1 10/14/22 21:08 VIC L643610 2,4-DB <0.1378 ug/L 0.1378 0.2525 1 10/14/22 21:08 VIC L643610 Dicam ba <0.05757 Ng/L 0.05757 0.01010 1 10/14/22 21:08 VIC L643610 Dichlorprop <0.08038 ug/L 0.08038 0.1010 1 10/14/22 21:08 VIC L643610 Dinoseb <0.02724 Ng/L 0.02724 0.1010 1 10/14/22 21:08 VIC L643610 MCPA <19.17 ug/L 19.17 50.51 1 10/14/22 21:08 VIC L643610 MCPP <11.87 Ng/L 11.87 50.51 1 10/14/22 21:08 VIC L643610 Picloram <0.04573 ug/L 0.04573 0.1010 1 10/14/22 21:08 VIC L643610 2,4,5-T <0.01012 Ng/L 0.01012 0.03030 1 10/14/22 21:08 VIC L643610 2,4,5-TP(Silvex) <0.01650 ug/L 0.01650 0.1010 1 10/14/22 21:08 VIC L643610 Surrogate: DCAA 58.22 Limits: 20-150% 1 10/14/22 21:08 L643610 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 13 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25068 10/12/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/10/22 18:12 ANG V24950 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/13/22 08:33 ANG V25069 Acrolein <2.00 Ng/L 2.00 5.00 1 10/10/22 18:12 ANG V24950 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/10/22 18:12 ANG V24950 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/13/22 08:33 ANG V25069 Benzene <0.180 ug/L 0.180 0.500 1 10/10/22 18:12 ANG V24950 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/10/22 18:12 ANG V24950 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/10/22 18:12 ANG V24950 Bromoform <1.50 Ng/L 1.50 5.00 1 10/10/22 18:12 ANG V24950 Bromomethane <0.280 ug/L 0.280 1.00 1 10/10/22 18:12 ANG V24950 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/10/22 18:12 ANG V24950 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/10/22 18:12 ANG V24950 Chlorobenzene <0.190 Ng/L 0.190 0.500 1 10/10/22 18:12 ANG V24950 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/10/22 18:12 ANG V24950 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/10/22 18:12 ANG V24950 Chloroform <0.220 ug/L 0.220 0.500 1 10/10/22 18:12 ANG V24950 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/10/22 18:12 ANG V24950 Chloroprene <0.450 ug/L 0.450 10.0 1 10/13/22 08:33 ANG V25069 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/10/22 18:12 ANG V24950 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/10/22 18:12 ANG V24950 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/10/22 18:12 ANG V24950 trans-1,4-Dichloro-2-butene <1.30 ug/L 1.30 10.0 1 10/10/22 18:12 ANG V24950 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 14 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25068 10/12/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene <0.220 Ng/L 0.220 0.500 1 10/10/22 18:12 ANG V24950 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/10/22 18:12 ANG V24950 1,4-Dichlorobenzene <0.210 Ng/L 0.210 0.500 1 10/10/22 18:12 ANG V24950 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/10/22 18:12 ANG V24950 1,1-Dichloroethane 0.3863 Ng/L 0.240 0.500 1 10/10/22 18:12 ANG V24950 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/10/22 18:12 ANG V24950 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/10/22 18:12 ANG V24950 cis- 1,2-Dich loroethene 0.2233 ug/L 0.200 0.500 1 10/10/22 18:12 ANG V24950 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/10/22 18:12 ANG V24950 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/10/22 18:12 ANG V24950 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/10/22 18:12 ANG V24950 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/10/22 18:12 ANG V24950 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/10/22 18:12 ANG V24950 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/10/22 18:12 ANG V24950 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/10/22 18:12 ANG V24950 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/13/22 08:33 ANG V25069 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/10/22 18:12 ANG V24950 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/10/22 18:12 ANG V24950 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/10/22 18:12 ANG V24950 Iodomethane <0.054 ug/L 0.054 0.500 1 10/10/22 18:12 ANG V24950 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/10/22 18:12 ANG V24950 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/13/22 08:33 ANG V25069 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 15 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25068 10/12/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/10/22 18:12 ANG V24950 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/10/22 18:12 ANG V24950 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/10/22 18:12 ANG V24950 Propionitrile <23.7 ug/L 23.7 10.0 1 10/13/22 08:33 ANG V25069 Styrene <0.220 Ng/L 0.220 0.500 1 10/10/22 18:12 ANG V24950 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 18:12 ANG V24950 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/10/22 18:12 ANG V24950 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/10/22 18:12 ANG V24950 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/10/22 18:12 ANG V24950 Toluene <0.220 ug/L 0.220 0.500 1 10/10/22 18:12 ANG V24950 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/10/22 18:12 ANG V24950 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 18:12 ANG V24950 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/10/22 18:12 ANG V24950 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/10/22 18:12 ANG V24950 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/10/22 18:12 ANG V24950 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/10/22 18:12 ANG V24950 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/10/22 18:12 ANG V24950 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/10/22 18:12 ANG V24950 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/10/22 18:12 ANG V24950 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/10/22 18:12 ANG V24950 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 16 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25068 10/12/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Analytical Method: 8270C Prep Method: 3510C Test <0.21 N9/L 0.210 0.500 1 10/10/22 18:12 V24950 98.6 Limits:80-124% 1 10/10/2218:12 ANG V24950 96.0 Limits:75-129% 1 10/10/2218:12 ANG V24950 94.2 Limits:63-136% 1 10/10/2218:12 ANG V24950 97.0 Limits:77-123% 1 10/10/2218:12 ANG V24950 99.0 Limits: 80-124% 1 10/13/22 08:33 ANG V25069 103 Limits: 75-129% 1 10/13/22 08:33 ANG V25069 105 Limits: 63-136% 1 10/13/22 08:33 ANG V25069 112 Limits: 77-123% 1 10/13/22 08:33 ANG V25069 Prep Batch(es): L642252 10/10/22 15:46 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dimethoate <0.841 Disulfoton <0.549 Ethyl Parathion <0.670 Famphur <0.604 Methyl Parathion <0.949 Phorate <0.777 Surrogate: Tributyl phosphate Surrogate: Triphenyl phosphate u9/L 0.841 1.18 N9/L 0.549 1.18 u9/L 0.670 1.18 N9/L 0.604 1.18 u9/L 0.949 1.18 N9/L 0.777 1.18 54.9 Limits: 50-150% 56.2 Limits: 50-150% 1 10/24/22 14:46 VBW L644472 1 10/24/22 14:46 VBW L644472 1 10/24/22 14:46 VBW L644472 1 10/24/22 14:46 VBW L644472 1 10/24/22 14:46 VBW L644472 1 10/24/22 14:46 VBW L644472 1 10/24/22 14:46 VBW 8270C 1 10/24/22 14:46 VBW 8270C Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 17 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,3-Dinitrobenzene <1.07 Ng/L 1.07 11.8 1 10/20/22 20:06 VBW L644470 1,3,5-Trinitrobenzene <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW L644471 Acenaphthene <0.495 Ng/L 0.495 2.35 1 10/20/22 20:06 VBW L644470 Acenaphthylene <0.504 ug/L 0.504 2.35 1 10/20/22 20:06 VBW L644470 Acetophenone <0.806 Ng/L 0.806 5.88 1 10/20/22 20:06 VBW L644470 Anthracene <0.548 ug/L 0.548 2.35 1 10/20/22 20:06 VBW L644470 Benzo(a)anthracene <0.501 Ng/L 0.501 2.35 1 10/20/22 20:06 VBW L644470 Benzo(a)pyrene <1.18 ug/L 1.18 2.35 1 10/20/22 20:06 VBW L644470 Benzo(b)fluoranthene <1.11 Ng/L 1.11 2.35 1 10/20/22 20:06 VBW L644470 Benzo(g,h,i)perylene <1.59 ug/L 1.59 2.35 1 10/20/22 20:06 VBW L644470 Benzo(k)fluoranthene <0.883 Ng/L 0.883 2.35 1 10/20/22 20:06 VBW L644470 Benzyl alcohol <3.55 ug/L 3.55 11.8 1 10/20/22 20:06 VBW L644470 Bis(2-Chloroethoxy)methane <0.509 Ng/L 0.509 5.88 1 10/20/22 20:06 VBW L644470 Bis(2-Chloroethyl)ether <0.525 ug/L 0.525 5.88 1 10/20/22 20:06 VBW L644470 Bis(2-Chloroisopropyl)ether <0.642 Ng/L 0.642 5.88 1 10/20/22 20:06 VBW L644470 Bis(2-ethylhexyl)phthalate <4.31 ug/L 4.31 5.88 1 10/20/22 20:06 VBW L644470 4-Bromophenyl phenyl ether <0.588 Ng/L 0.588 5.88 1 10/20/22 20:06 VBW L644470 Butyl benzyl phthalate <5.40 ug/L 5.40 5.88 1 10/20/22 20:06 VBW L644470 4-Chloro-3- methyl phenol <0.591 Ng/L 0.591 5.88 1 10/20/22 20:06 VBW L644470 4-Chloroaniline <0.618 ug/L 0.618 5.88 1 10/20/22 20:06 VBW L644470 Chlorobenzilate <2.23 Ng/L 2.23 5.88 1 10/20/22 20:06 VBW L644470 2-Chloronaphthalene <0.559 ug/L 0.559 5.88 1 10/20/22 20:06 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 18 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2-Chlorophenol <0.865 Ng/L 0.865 5.88 1 10/20/22 20:06 VBW L644470 4-Chlorophenyl phenyl ether <0.563 ug/L 0.563 5.88 1 10/20/22 20:06 VBW L644470 Chrysene <0.858 Ng/L 0.858 2.35 1 10/20/22 20:06 VBW L644470 Dibenz(a,h)anthracene <0.296 ug/L 0.296 2.35 1 10/20/22 20:06 VBW L644470 Dibenzofuran <0.497 Ng/L 0.497 5.88 1 10/20/22 20:06 VBW L644470 1,2-Dichlorobenzene <0.739 ug/L 0.739 5.88 1 10/20/22 20:06 VBW L644470 1,3-Dichlorobenzene <0.577 Ng/L 0.577 5.88 1 10/20/22 20:06 VBW L644470 1,4-Dichlorobenzene <0.682 ug/L 0.682 5.88 1 10/20/22 20:06 VBW L644470 3,3'-Dichlorobenzidine <4.41 Ng/L 4.41 11.8 1 10/20/22 20:06 VBW L644470 2,4-Dichlorophenol <1.79 ug/L 1.79 5.88 1 10/20/22 20:06 VBW L644470 2,6-Dichlorophenol <0.826 Ng/L 0.826 5.88 1 10/20/22 20:06 VBW L644470 Diethyl phthalate <0.687 ug/L 0.687 5.88 1 10/20/22 20:06 VBW L644470 Dimethyl phthalate <0.599 Ng/L 0.599 5.88 1 10/20/22 20:06 VBW L644470 3,3' Dimethylbenzidine <2.22 u9/L 2.22 11.8 1 10/20/22 20:06 VBW L644470 2,4-Dimethyl phenol <0.792 M Ng/L 0.792 5.88 1 10/20/22 20:06 VBW L644470 Di-n-butyl phthalate <1.85 ug/L 1.85 5.88 1 10/20/22 20:06 VBW L644470 4,6- Din itro-2- methyl phenol <4.09 Ng/L 4.09 11.8 1 10/20/22 20:06 VBW L644470 2,4-Dinitrophenol <5.72 ug/L 5.72 11.8 1 10/20/22 20:06 VBW L644470 2,4-Dinitrotoluene <0.473 Ng/L 0.473 5.88 1 10/20/22 20:06 VBW L644470 2,6-Dinitrotoluene <0.485 ug/L 0.485 5.88 1 10/20/22 20:06 VBW L644470 Di-n-Octyl Phthalate <2.02 Ng/L 2.02 5.88 1 10/20/22 20:06 VBW L644470 Ethyl methanesulfonate <0.839 ug/L 0.839 5.88 1 10/20/22 20:06 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 19 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Fluoranthene <0.477 Ng/L 0.477 2.35 1 10/20/22 20:06 VBW L644470 Fluorene <0.521 ug/L 0.521 2.35 1 10/20/22 20:06 VBW L644470 Hexachlorobenzene <3.02 Ng/L 3.02 5.88 1 10/20/22 20:06 VBW L644470 Hexachlorobutadiene <0.476 ug/L 0.476 5.88 1 10/20/22 20:06 VBW L644470 Hexachlorocyclopentadiene <2.75 Ng/L 2.75 5.88 1 10/20/22 20:06 VBW L644470 Hexachloroethane <0.325 ug/L 0.325 5.88 1 10/20/22 20:06 VBW L644470 Indeno(1,2,3-cd)pyrene <1.19 Ng/L 1.19 2.35 1 10/20/22 20:06 VBW L644470 Isodrin <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW L644471 Isophorone <0.423 Ng/L 0.423 5.88 1 10/20/22 20:06 VBW L644470 Kepone <11.8 ug/L 11.8 11.8 1 10/20/22 20:06 VBW L644471 Methyl methanesulfonate <0.726 Ng/L 0.726 5.88 1 10/20/22 20:06 VBW L644470 2-Methylnaphthalene <0.569 ug/L 0.569 2.35 1 10/20/22 20:06 VBW L644470 2-Methylphenol <0.847 Ng/L 0.847 5.88 1 10/20/22 20:06 VBW L644470 3&4 Methylphenol <0.812 ug/L 0.812 5.88 1 10/20/22 20:06 VBW L644470 Naphthalene <0.568 Ng/L 0.568 2.35 1 10/20/22 20:06 VBW L644470 2-Nitroaniline <0.675 ug/L 0.675 5.88 1 10/20/22 20:06 VBW L644470 3-Nitroaniline <1.81 Ng/L 1.81 11.8 1 10/20/22 20:06 VBW L644470 4-Nitroaniline <0.870 ug/L 0.870 5.88 1 10/20/22 20:06 VBW L644470 Nitrobenzene <0.624 Ng/L 0.624 5.88 1 10/20/22 20:06 VBW L644470 2-Nitrophenol <0.712 ug/L 0.712 5.88 1 10/20/22 20:06 VBW L644470 4-Nitrophenol <1.64 Ng/L 1.64 11.8 1 10/20/22 20:06 VBW L644470 N-Nitrosodimethylamine <0.292 ug/L 0.292 5.88 1 10/20/22 20:06 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 20 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPORT OF ANAL YSIS Lab No : 89898 Matrix: Aqueous Sample ID: MW-02-20221003 Sampled: 10/3/2022 10:00 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch N-Nitrosodiphenylamine <0.923 Ng/L 0.923 11.8 1 10/20/22 20:06 VBW L644470 N-Nitrosodiethylamine <0.470 ug/L 0.470 5.88 1 10/20/22 20:06 VBW L644470 N-Nitroso-di-n-butylamine <0.884 Ng/L 0.884 5.88 1 10/20/22 20:06 VBW L644470 N-Nitroso-di-n-propylamine <0.392 ug/L 0.392 5.88 1 10/20/22 20:06 VBW L644470 Pentachlorobenzene <0.541 Ng/L 0.541 11.8 1 10/20/22 20:06 VBW L644470 Pentachloronitrobenzene <1.35 ug/L 1.35 5.88 1 10/20/22 20:06 VBW L644470 Pentachlorophenol <2.89 Ng/L 2.89 11.8 1 10/20/22 20:06 VBW L644470 Phenacetin <1.51 ug/L 1.51 5.88 1 10/20/22 20:06 VBW L644470 Phenanthrene <0.545 Ng/L 0.545 2.35 1 10/20/22 20:06 VBW L644470 Phenol <0.457 ug/L 0.457 5.88 1 10/20/22 20:06 VBW L644470 Pyrene <1.22 Ng/L 1.22 2.35 1 10/20/22 20:06 VBW L644470 1,2,4,5-Tetrachlorobenzene <0.372 ug/L 0.372 5.88 1 10/20/22 20:06 VBW L644470 2,3,4,6-Tetrachlorophenol <0.417 Ng/L 0.417 5.88 1 10/20/22 20:06 VBW L644470 1,2,4-Trichlorobenzene <0.566 ug/L 0.566 5.88 1 10/20/22 20:06 VBW L644470 2,4,5-Trichlorophenol <0.411 Ng/L 0.411 5.88 1 10/20/22 20:06 VBW L644470 2,4,6-Trichlorophenol <0.404 ug/L 0.404 5.88 1 10/20/22 20:06 VBW L644470 Surrogate: 2-Fluorobiphenyl 48.3 Limits: 24-93% 1 10/20/22 20:06 VBW L644470 Surrogate: 2-Fluorophenol 28.6 Limits: 10-44% 1 10/20/22 20:06 VBW L644470 Surrogate: Nitrobenzene-d5 45.1 Limits: 20-91% 1 10/20/22 20:06 VBW L644470 Surrogate: Phenol-d6 22.0 Limits: 7-32% 1 10/20/22 20:06 VBW L644470 Surrogate: 4-Terphenyl-d14 55.7 Limits: 35-126% 1 10/20/22 20:06 VBW L644470 Surrogate: 2,4,6-Tribromophenol 56.4 Limits: 39-110% 1 10/20/22 20:06 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 21 of 123 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-277-0040 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/09/2022 Received : 10/04/2022 Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane <0.139 Ng/L 0.139 2.00 1 10/06/22 12:00 TBL 8260D SIM 1,4-Naphthoquinone <11.1 pg/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D 1-Naphthylamine <11.1 Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D 2-Acetylaminofluorene <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D 2-Naphthylamine <11.1 Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D 3-Methylcholanthrene <11.1 pg/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D 4-Aminobiphenyl <11.1 Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D 5-Nitro-o-toluidine <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D 7,12-Dimethyl benz(a)anth racene <11.1 Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D Diallate <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D Hexachloropropene <11.1 Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D Isosafrole <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D Methapyrilene <11.1 Ng/L 11.1 22.2 1 10/20/22 20:26 VBW 8270D N-Nitrosomethylethylamine <11.1 pg/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D N-Nitrosomorpholine <11.1 Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D N-Nitrosopyrrolidine <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D N-Nitrosopiperidine <11.1 Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D 0,0,0-Triethyl Phosphorothioate <0.366 pg/L 0.366 1.11 1 10/24/22 14:59 VBW 8270C o-Toluidine <11.1 Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D p-Dimethylaminoazobenzene <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D p-Phenylenediamine <11.1 M Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D Pronamide <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D Safrole <11.1 Ng/L 11.1 11.1 1 10/20/22 20:26 VBW 8270D Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 22 of 123 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-277-0040 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/09/2022 Received : 10/04/2022 Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Thionazine <0.366 Ng/L 0.366 1.11 1 10/24/2214:59 VBW 8270C Sulfide <1.66 mg/L 1.66 4.00 1 10/10/2211:00 SLO 4500S2F-2011 Antimony <0.680 Ng/L 0.680 2.00 1 10/10/22 18:58 EDV 6020B Dissolved Antimony <0.618 ug/L 0.618 1.00 1 10/29/22 14:22 BKN 6020B Arsenic 0.5903 Ng/L 0.490 1.00 1 10/10/22 18:58 EDV 6020B Dissolved Arsenic 3.36 ug/L 0.297 1.00 1 10/29/22 14:22 BKN 6020B Barium 246 Ng/L 34.0 100 10 10/17/22 22:00 EDV 6020B Dissolved Barium 153 ug/L 0.453 1.00 1 10/29/22 14:22 BKN 6020B Beryllium <0.240 Ng/L 0.240 1.00 1 10/10/22 18:58 EDV 6020B Dissolved Beryllium <0.102 ug/L 0.102 1.00 1 10/29/22 14:22 BKN 6020B Cadmium <0.150 Ng/L 0.150 1.00 1 10/10/22 18:58 EDV 6020B Dissolved Cadmium <0.350 ug/L 0.350 1.00 1 10/29/22 14:22 BKN 6020B Chromium 2.76 Ng/L 1.00 2.00 1 10/10/22 18:58 EDV 6020B Dissolved Chromium <0.346 ug/L 0.346 1.00 1 10/29/22 14:22 BKN 6020B Cobalt 15.9 Ng/L 0.080 1.00 1 10/10/22 18:58 EDV 6020B Dissolved Cobalt 10.5 ug/L 0.060 1.00 1 10/29/22 14:22 BKN 6020B Copper 4.19 Ng/L 0.890 2.00 1 10/11/2216:02 EDV 6020B Dissolved Copper 0.6903 ug/L 0.489 1.00 1 10/29/22 14:22 BKN 6020B Lead 0.9933 Ng/L 0.500 1.00 1 10/10/22 18:58 EDV 6020B Dissolved Lead <0.264 ug/L 0.264 1.00 1 10/29/22 14:22 BKN 6020B Mercury (Total) <0.0700 Ng/L 0.0700 0.200 1 10/11/22 15:58 EDV 7470A Dissolved Mercury <0.0700 ug/L 0.0700 0.200 1 10/24/22 15:32 EDV 7470A Dissolved Nickel 2.69 Ng/L 0.182 1.00 1 10/29/22 14:22 BKN 6020B Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 23 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89901 Sample ID: MW-05R-20221003 Matrix: Aqueous Sampled: 10/3/2022 15:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Nickel 4.66 Ng/L 0.720 2.00 1 10/10/2218:58 EDV 6020B Selenium <2.30 ug/L 2.30 5.00 1 10/10/2218:58 EDV 6020B Dissolved Selenium <0.703 Ng/L 0.703 1.00 1 10/29/22 14:22 BKN 6020E Silver <0.130 ug/L 0.130 1.00 1 10/10/2218:58 EDV 6020B Dissolved Silver <0.0570 Ng/L 0.0570 1.00 1 10/29/22 14:22 BKN 6020E Tin <1.50 ug/L 1.50 5.00 1 10/10/2218:58 EDV 6020B Dissolved Tin <1.44 Ng/L 1.44 5.00 1 10/29/22 14:22 BKN 6020B Thallium <0.280 ug/L 0.280 2.00 1 10/10/2218:58 EDV 6020B Dissolved Thallium 0.08743 Ng/L 0.0610 1.00 1 10/29/22 14:22 BKN 6020B Vanadium 3.313 ug/L 2.10 5.00 1 10/10/2218:58 EDV 6020B Dissolved Vanadium <0.767 Ng/L 0.767 5.00 1 10/29/22 14:22 BKN 6020B Zinc 12.63 ug/L 3.90 20.0 1 10/10/22 18:58 EDV 6020B Dissolved Zinc 5.17 3113 Ng/L 4.67 10.0 1 10/29/22 14:22 BKN 6020B Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 24 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0023 H Ng/L 0.0023 0.0444 10 10/20/22 09:02 VIC L644344 alpha-BHC <0.0023 H ug/L 0.0023 0.0444 10 10/20/22 09:02 VIC L644344 beta-BHC <0.0023 H Ng/L 0.0023 0.0444 10 10/20/22 09:02 VIC L644344 delta-BHC <0.0017 H ug/L 0.0017 0.0444 10 10/20/22 09:02 VIC L644344 Chlordane <0.0245 H Ng/L 0.0245 0.222 10 10/20/22 09:02 VIC L644344 alpha -Chlordane <0.0023 H ug/L 0.0023 0.0444 10 10/20/22 09:02 VIC L644344 gamma -Chlordane <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 09:02 VIC L644344 4,4'-DDD <0.0023 H ug/L 0.0023 0.0444 10 10/20/22 09:02 VIC L644344 4,4'-DDE <0.0023 H Ng/L 0.0023 0.0444 10 10/20/22 09:02 VIC L644344 4,4'-DDT <0.0038 H ug/L 0.0038 0.0444 10 10/20/22 09:02 VIC L644344 Dieldrin <0.0017 H Ng/L 0.0017 0.0444 10 10/20/22 09:02 VIC L644344 EndosulfanI <0.0017 H ug/L 0.0017 0.0444 10 10/20/22 09:02 VIC L644344 EndosulfanII <0.0031 H Ng/L 0.0031 0.0444 10 10/20/22 09:02 VIC L644344 Endosulfan Sulfate <0.0016 H ug/L 0.0016 0.0444 10 10/20/22 09:02 VIC L644344 Endrin <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 09:02 VIC L644344 Endrin Aldehyde <0.0016 H ug/L 0.0016 0.0444 10 10/20/22 09:02 VIC L644344 Endrin Ketone <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 09:02 VIC L644344 gamma-BHC <0.0020 H ug/L 0.0020 0.0444 10 10/20/22 09:02 VIC L644344 Heptachlor <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 09:02 VIC L644344 Heptachlor Epoxide <0.0016 H ug/L 0.0016 0.0444 10 10/20/22 09:02 VIC L644344 Methoxychlor <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 09:02 VIC L644344 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 25 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 Lab No : 89901 Sample ID: MW-05R-20221003 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/3/2022 15:30 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0223 H Ng/L 0.0223 0.333 10 10/20/22 09:02 VIC L644344 Surrogate: Decachlorobiphenyl 60.4 Limits: 36-116% 10 10/20/22 09:02 L644344 Surrogate: Tetrachloro-m-xylene 54.3 Limits: 25-123% 10 10/20/22 09:02 L644344 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2078 Pg/L 0.2078 0.2500 1 10/14/22 21:33 VIC L643610 Dalapon <0.5149 Ng/L 0.5149 0.5500 1 10/14/22 21:33 VIC L643610 2,4-DB <0.1364 ug/L 0.1364 0.2500 1 10/14/22 21:33 VIC L643610 Dicamba <0.05700 Ng/L 0.05700 0.01000 1 10/14/22 21:33 VIC L643610 Dichlorprop <0.07959 ug/L 0.07959 0.1000 1 10/14/22 21:33 VIC L643610 Dinoseb <0.02698 Ng/L 0.02698 0.1000 1 10/14/22 21:33 VIC L643610 MCPA <18.98 ug/L 18.98 50.00 1 10/14/22 21:33 VIC L643610 MCPP <11.75 Ng/L 11.75 50.00 1 10/14/22 21:33 VIC L643610 Picloram <0.04528 ug/L 0.04528 0.1000 1 10/14/22 21:33 VIC L643610 2,4,5-T <0.01002 Ng/L 0.01002 0.03000 1 10/14/22 21:33 VIC L643610 2,4,5-TP (Silvex) 0.02419 J ug/L 0.01634 0.1000 1 10/14/22 21:33 VIC L643610 Surrogate: DCAA 77.60 Limits: 20-150% 1 10/14/22 21:33 L643610 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 26 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/10/22 18:39 ANG V24950 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/17/22 19:16 ANG V25249 Acrolein <2.00 Ng/L 2.00 5.00 1 10/10/22 18:39 ANG V24950 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/10/22 18:39 ANG V24950 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/17/22 19:16 ANG V25249 Benzene 1.63 ug/L 0.180 0.500 1 10/10/22 18:39 ANG V24950 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/10/22 18:39 ANG V24950 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/10/22 18:39 ANG V24950 Bromoform <1.50 Ng/L 1.50 5.00 1 10/10/22 18:39 ANG V24950 Bromomethane <0.280 ug/L 0.280 1.00 1 10/10/22 18:39 ANG V24950 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/10/22 18:39 ANG V24950 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/10/22 18:39 ANG V24950 Chlorobenzene 7.09 Ng/L 0.190 0.500 1 10/10/22 18:39 ANG V24950 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/10/22 18:39 ANG V24950 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/10/22 18:39 ANG V24950 Chloroform <0.220 ug/L 0.220 0.500 1 10/10/22 18:39 ANG V24950 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/10/22 18:39 ANG V24950 Chloroprene <0.450 ug/L 0.450 10.0 1 10/17/22 19:16 ANG V25249 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/10/22 18:39 ANG V24950 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/10/22 18:39 ANG V24950 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/10/22 18:39 ANG V24950 trans-1,4-Dichloro-2-butene <1.30 ug/L 1.30 10.0 1 10/10/22 18:39 ANG V24950 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 27 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene 0.2863 Ng/L 0.220 0.500 1 10/10/22 18:39 ANG V24950 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/10/22 18:39 ANG V24950 1,4-Dichlorobenzene 7.29 Ng/L 0.210 0.500 1 10/10/22 18:39 ANG V24950 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/10/22 18:39 ANG V24950 1,1-Dichloroethane <0.240 Ng/L 0.240 0.500 1 10/10/22 18:39 ANG V24950 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/10/22 18:39 ANG V24950 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/10/22 18:39 ANG V24950 cis- 1,2-Dich loroethene 2.18 ug/L 0.200 0.500 1 10/10/22 18:39 ANG V24950 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/10/22 18:39 ANG V24950 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/10/22 18:39 ANG V24950 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/10/22 18:39 ANG V24950 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/10/22 18:39 ANG V24950 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/10/22 18:39 ANG V24950 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/10/22 18:39 ANG V24950 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/10/22 18:39 ANG V24950 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/17/22 19:16 ANG V25249 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/10/22 18:39 ANG V24950 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/10/22 18:39 ANG V24950 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/10/22 18:39 ANG V24950 Iodomethane <0.054 ug/L 0.054 0.500 1 10/10/22 18:39 ANG V24950 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/10/22 18:39 ANG V24950 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/17/2219:16 ANG V25249 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 28 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/10/22 18:39 ANG V24950 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/10/22 18:39 ANG V24950 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/10/22 18:39 ANG V24950 Propionitrile <23.7 ug/L 23.7 10.0 1 10/17/2219:16 ANG V25249 Styrene <0.220 Ng/L 0.220 0.500 1 10/10/22 18:39 ANG V24950 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 18:39 ANG V24950 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/10/22 18:39 ANG V24950 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/10/22 18:39 ANG V24950 Tetrahydrofuran 2.763 Ng/L 1.50 10.0 1 10/10/22 18:39 ANG V24950 Toluene 0.2373 ug/L 0.220 0.500 1 10/10/22 18:39 ANG V24950 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/10/22 18:39 ANG V24950 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 18:39 ANG V24950 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/10/22 18:39 ANG V24950 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/10/22 18:39 ANG V24950 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/10/22 18:39 ANG V24950 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/10/22 18:39 ANG V24950 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/10/22 18:39 ANG V24950 Vinyl Chloride 0.563 ug/L 0.170 0.500 1 10/10/22 18:39 ANG V24950 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/10/22 18:39 ANG V24950 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/10/22 18:39 ANG V24950 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 29 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Analytical Method: 8270C Prep Method: 3510C Test <0.21 Ng/L 0.210 0.500 1 10/10/22 18:39 V24950 100 Limits:80-124% 1 10/10/2218:39 ANG V24950 96.4 Limits:75-129% 1 10/10/2218:39 ANG V24950 93.6 Limits:63-136% 1 10/10/2218:39 ANG V24950 95.6 Limits:77-123% 1 10/10/2218:39 ANG V24950 98.8 Limits:80-124% 1 10/17/2219:16 ANG V25249 98.0 Limits:75-129% 1 10/17/2219:16 ANG V25249 97.8 Limits:63-136% 1 10/17/2219:16 ANG V25249 100 Limits:77-123% 1 10/17/2219:16 ANG V25249 Prep Batch(es): L642252 10/10/22 15:46 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dimethoate <0.791 Disulfoton <0.517 Ethyl Parathion <0.630 Famphur <0.568 Methyl Parathion <0.893 Phorate <0.731 Surrogate: Tributyl phosphate Surrogate: Triphenyl phosphate u9/L 0.791 1.11 Ng/L 0.517 1.11 u9/L 0.630 1.11 Ng/L 0.568 1.11 u9/L 0.893 1.11 Ng/L 0.731 1.11 74.3 Limits: 50-150% 62.2 Limits: 50-150% 1 10/24/22 14:59 VBW L644472 1 10/24/22 14:59 VBW L644472 1 10/24/22 14:59 VBW L644472 1 10/24/22 14:59 VBW L644472 1 10/24/22 14:59 VBW L644472 1 10/24/22 14:59 VBW L644472 1 10/24/22 14:59 VBW 8270C 1 10/24/22 14:59 VBW 8270C Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 30 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,3-Dinitrobenzene <1.00 Ng/L 1.00 11.1 1 10/20/22 20:26 VBW L644470 1,3,5-Trinitrobenzene <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW L644471 Acenaphthene <0.468 Ng/L 0.468 2.22 1 10/20/22 20:26 VBW L644470 Acenaphthylene <0.476 ug/L 0.476 2.22 1 10/20/22 20:26 VBW L644470 Acetophenone <0.762 Ng/L 0.762 5.56 1 10/20/22 20:26 VBW L644470 Anthracene <0.518 ug/L 0.518 2.22 1 10/20/22 20:26 VBW L644470 Benzo(a)anthracene <0.473 Ng/L 0.473 2.22 1 10/20/22 20:26 VBW L644470 Benzo(a)pyrene <1.11 ug/L 1.11 2.22 1 10/20/22 20:26 VBW L644470 Benzo(b)fluoranthene <1.04 Ng/L 1.04 2.22 1 10/20/22 20:26 VBW L644470 Benzo(g,h,i)perylene <1.51 ug/L 1.51 2.22 1 10/20/22 20:26 VBW L644470 Benzo(k)fluoranthene <0.834 Ng/L 0.834 2.22 1 10/20/22 20:26 VBW L644470 Benzyl alcohol <3.34 ug/L 3.34 11.1 1 10/20/22 20:26 VBW L644470 Bis(2-Chloroethoxy)methane <0.481 Ng/L 0.481 5.56 1 10/20/22 20:26 VBW L644470 Bis(2-Chloroethyl)ether <0.497 ug/L 0.497 5.56 1 10/20/22 20:26 VBW L644470 Bis(2-Chloroisopropyl)ether <0.607 Ng/L 0.607 5.56 1 10/20/22 20:26 VBW L644470 Bis(2-ethylhexyl)phthalate <4.07 ug/L 4.07 5.56 1 10/20/22 20:26 VBW L644470 4-Bromophenyl phenyl ether <0.556 Ng/L 0.556 5.56 1 10/20/22 20:26 VBW L644470 Butyl benzyl phthalate <5.11 ug/L 5.11 5.56 1 10/20/22 20:26 VBW L644470 4-Chloro-3-methylphenol <0.559 Ng/L 0.559 5.56 1 10/20/22 20:26 VBW L644470 4-Chloroaniline <0.584 ug/L 0.584 5.56 1 10/20/22 20:26 VBW L644470 Chlorobenzilate <2.11 Ng/L 2.11 5.56 1 10/20/22 20:26 VBW L644470 2-Chloronaphthalene <0.529 ug/L 0.529 5.56 1 10/20/22 20:26 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 31 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2-Chlorophenol <0.818 Ng/L 0.818 5.56 1 10/20/22 20:26 VBW L644470 4-Chlorophenyl phenyl ether <0.532 ug/L 0.532 5.56 1 10/20/22 20:26 VBW L644470 Chrysene <0.811 Ng/L 0.811 2.22 1 10/20/22 20:26 VBW L644470 Dibenz(a,h)anthracene <0.279 ug/L 0.279 2.22 1 10/20/22 20:26 VBW L644470 Dibenzofuran <0.470 Ng/L 0.470 5.56 1 10/20/22 20:26 VBW L644470 1,2-Dichlorobenzene <0.699 ug/L 0.699 5.56 1 10/20/22 20:26 VBW L644470 1,3-Dichlorobenzene <0.545 Ng/L 0.545 5.56 1 10/20/22 20:26 VBW L644470 1,4-Dichlorobenzene 3.47 J ug/L 0.644 5.56 1 10/20/22 20:26 VBW L644470 3,3'-Dichlorobenzidine <4.15 Ng/L 4.15 11.1 1 10/20/22 20:26 VBW L644470 2,4-Dichlorophenol <1.69 ug/L 1.69 5.56 1 10/20/22 20:26 VBW L644470 2,6-Dichlorophenol <0.781 Ng/L 0.781 5.56 1 10/20/22 20:26 VBW L644470 Diethyl phthalate <0.650 ug/L 0.650 5.56 1 10/20/22 20:26 VBW L644470 Dimethyl phthalate <0.567 Ng/L 0.567 5.56 1 10/20/22 20:26 VBW L644470 3,3' Dimethylbenzidine <2.09 ug/L 2.09 11.1 1 10/20/22 20:26 VBW L644470 2,4-Dimethyl phenol <0.749 M Ng/L 0.749 5.56 1 10/20/22 20:26 VBW L644470 Di-n-butyl phthalate <1.75 ug/L 1.75 5.56 1 10/20/22 20:26 VBW L644470 4,6- Din itro-2- methyl phenol <3.85 Ng/L 3.85 11.1 1 10/20/22 20:26 VBW L644470 2,4-Dinitrophenol <5.38 ug/L 5.38 11.1 1 10/20/22 20:26 VBW L644470 2,4-Dinitrotoluene <0.448 Ng/L 0.448 5.56 1 10/20/22 20:26 VBW L644470 2,6-Dinitrotoluene <0.459 ug/L 0.459 5.56 1 10/20/22 20:26 VBW L644470 Di-n-Octyl Phthalate <1.91 Ng/L 1.91 5.56 1 10/20/22 20:26 VBW L644470 Ethyl methanesulfonate <0.793 ug/L 0.793 5.56 1 10/20/22 20:26 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 32 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Fluoranthene <0.450 Ng/L 0.450 2.22 1 10/20/22 20:26 VBW L644470 Fluorene <0.492 ug/L 0.492 2.22 1 10/20/22 20:26 VBW L644470 Hexachlorobenzene <2.86 Ng/L 2.86 5.56 1 10/20/22 20:26 VBW L644470 Hexachlorobutadiene <0.450 ug/L 0.450 5.56 1 10/20/22 20:26 VBW L644470 Hexachlorocyclopentadiene <2.60 Ng/L 2.60 5.56 1 10/20/22 20:26 VBW L644470 Hexachloroethane <0.308 ug/L 0.308 5.56 1 10/20/22 20:26 VBW L644470 Indeno(1,2,3-cd)pyrene <1.12 Ng/L 1.12 2.22 1 10/20/22 20:26 VBW L644470 Isodrin <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW L644471 Isophorone <0.400 Ng/L 0.400 5.56 1 10/20/22 20:26 VBW L644470 Kepone <11.1 ug/L 11.1 11.1 1 10/20/22 20:26 VBW L644471 Methyl methanesulfonate <0.687 Ng/L 0.687 5.56 1 10/20/22 20:26 VBW L644470 2-Methylnaphthalene <0.538 ug/L 0.538 2.22 1 10/20/22 20:26 VBW L644470 2-Methylphenol <0.801 Ng/L 0.801 5.56 1 10/20/22 20:26 VBW L644470 3&4 Methylphenol <0.768 ug/L 0.768 5.56 1 10/20/22 20:26 VBW L644470 Naphthalene <0.537 Ng/L 0.537 2.22 1 10/20/22 20:26 VBW L644470 2-Nitroaniline <0.638 ug/L 0.638 5.56 1 10/20/22 20:26 VBW L644470 3-Nitroaniline <1.70 Ng/L 1.70 11.1 1 10/20/22 20:26 VBW L644470 4-Nitroaniline <0.822 ug/L 0.822 5.56 1 10/20/22 20:26 VBW L644470 Nitrobenzene <0.590 Ng/L 0.590 5.56 1 10/20/22 20:26 VBW L644470 2-Nitrophenol <0.673 ug/L 0.673 5.56 1 10/20/22 20:26 VBW L644470 4-Nitrophenol <1.54 Ng/L 1.54 11.1 1 10/20/22 20:26 VBW L644470 N-Nitrosodimethylamine <0.276 ug/L 0.276 5.56 1 10/20/22 20:26 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 33 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPORT OF ANAL YSIS Lab No : 89901 Matrix: Aqueous Sample ID: MW-05R-20221003 Sampled: 10/3/2022 15:30 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch N-Nitrosodiphenylamine <0.869 Ng/L 0.869 11.1 1 10/20/22 20:26 VBW L644470 N-Nitrosodiethylamine <0.444 ug/L 0.444 5.56 1 10/20/22 20:26 VBW L644470 N-Nitroso-di-n-butylamine <0.836 Ng/L 0.836 5.56 1 10/20/22 20:26 VBW L644470 N-Nitroso-di-n-propylamine <0.371 ug/L 0.371 5.56 1 10/20/22 20:26 VBW L644470 Pentachlorobenzene <0.509 Ng/L 0.509 11.1 1 10/20/22 20:26 VBW L644470 Pentachloronitrobenzene <1.28 ug/L 1.28 5.56 1 10/20/22 20:26 VBW L644470 Pentachlorophenol <2.72 Ng/L 2.72 11.1 1 10/20/22 20:26 VBW L644470 Phenacetin <1.42 ug/L 1.42 5.56 1 10/20/22 20:26 VBW L644470 Phenanthrene <0.515 Ng/L 0.515 2.22 1 10/20/22 20:26 VBW L644470 Phenol <0.432 ug/L 0.432 5.56 1 10/20/22 20:26 VBW L644470 Pyrene <1.15 Ng/L 1.15 2.22 1 10/20/22 20:26 VBW L644470 1,2,4,5-Tetrachlorobenzene <0.352 ug/L 0.352 5.56 1 10/20/22 20:26 VBW L644470 2,3,4,6-Tetrachlorophenol <0.394 Ng/L 0.394 5.56 1 10/20/22 20:26 VBW L644470 1,2,4-Trichlorobenzene <0.535 ug/L 0.535 5.56 1 10/20/22 20:26 VBW L644470 2,4,5-Trichlorophenol <0.389 Ng/L 0.389 5.56 1 10/20/22 20:26 VBW L644470 2,4,6-Trichlorophenol <0.382 ug/L 0.382 5.56 1 10/20/22 20:26 VBW L644470 Surrogate: 2-Fluorobiphenyl 50.6 Limits: 24-93% 1 10/20/22 20:26 VBW L644470 Surrogate: 2-Fluorophenol 31.6 Limits: 10-44% 1 10/20/22 20:26 VBW L644470 Surrogate: Nitrobenzene-d5 48.5 Limits: 20-91% 1 10/20/22 20:26 VBW L644470 Surrogate: Phenol-d6 25.8 Limits: 7-32% 1 10/20/22 20:26 VBW L644470 Surrogate: 4-Terphenyl-d14 55.4 Limits: 35-126% 1 10/20/22 20:26 VBW L644470 Surrogate: 2,4,6-Tribromophenol 65.0 Limits: 39-110% 1 10/20/22 20:26 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 34 of 123 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-277-0040 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/09/2022 Received : 10/04/2022 Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane 17.6 Ng/L 0.139 2.00 1 10/06/22 12:25 TBL 8260D SIM 1,4-Naphthoquinone <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D 1-Naphthylamine <10.0 Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D 2-Acetylaminofluorene <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D 2-Naphthylamine <10.0 Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D 3-Methylcholanthrene <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D 4-Aminobiphenyl <10.0 Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D 5-Nitro-o-toluidine <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D 7,12-Dimethyl benz(a)anth racene <10.0 Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D Diallate <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D Hexachloropropene <10.0 Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D Isosafrole <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D Methapyrilene <10.0 Ng/L 10.0 20.0 1 10/20/22 20:46 VBW 8270D N-Nitrosomethylethylamine <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D N-Nitrosomorpholine <10.0 Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D N-Nitrosopyrrolidine <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D N-Nitrosopiperidine <10.0 Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D 0,0,0-Triethyl Phosphorothioate <0.330 ug/L 0.330 1.00 1 10/24/22 15:13 VBW 8270C o-Toluidine <10.0 Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D p-Dimethylaminoazobenzene <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D p-Phenylenediamine <10.0 M Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D Pronamide <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D Safrole <10.0 Ng/L 10.0 10.0 1 10/20/22 20:46 VBW 8270D Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 35 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89902 Sample ID: MW-07-20221003 Matrix: Aqueous Sampled: 10/3/2022 12:40 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Thionazine <0.330 Ng/L 0.330 1.00 1 10/24/2215:13 VBW 8270C Sulfide <0.83 mg/L 0.83 2.00 1 10/10/2211:00 SLO 4500S2F-2011 Antimony <0.680 Ng/L 0.680 2.00 1 10/10/22 19:05 EDV 6020B Arsenic <0.490 ug/L 0.490 1.00 1 10/10/22 19:05 EDV 6020B Barium 422 Ng/L 34.0 100 10 10/17/22 22:07 EDV 6020B Beryllium <0.240 ug/L 0.240 1.00 1 10/10/22 19:05 EDV 6020B Cadmium <0.150 Ng/L 0.150 1.00 1 10/10/22 19:05 EDV 6020B Chromium <1.00 ug/L 1.00 2.00 1 10/10/22 19:05 EDV 6020B Cobalt 2.12 Ng/L 0.080 1.00 1 10/10/22 19:05 EDV 6020B Copper 2.72 ug/L 0.890 2.00 1 10/11/2216:08 EDV 6020B Lead <0.500 Ng/L 0.500 1.00 1 10/10/22 19:05 EDV 6020B Mercury (Total) <0.0700 ug/L 0.0700 0.200 1 10/11/22 16:06 EDV 7470A Nickel 7.41 Ng/L 0.720 2.00 1 10/10/22 19:05 EDV 6020B Selenium <2.30 ug/L 2.30 5.00 1 10/10/22 19:05 EDV 6020B Silver <0.130 Ng/L 0.130 1.00 1 10/10/22 19:05 EDV 6020B Tin 2.093 ug/L 1.50 5.00 1 10/10/22 19:05 EDV 6020B Thallium <0.280 Ng/L 0.280 2.00 1 10/10/22 19:05 EDV 6020B Vanadium <2.10 ug/L 2.10 5.00 1 10/10/22 19:05 EDV 6020B Zinc 14.93 Ng/L 3.90 20.0 1 10/10/22 19:05 EDV 6020B Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 36 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0021 H Ng/L 0.0021 0.0408 10 10/20/22 09:30 VIC L644344 alpha-BHC <0.0021 H ug/L 0.0021 0.0408 10 10/20/22 09:30 VIC L644344 beta-BHC <0.0021 H Ng/L 0.0021 0.0408 10 10/20/22 09:30 VIC L644344 delta-BHC <0.0016 H ug/L 0.0016 0.0408 10 10/20/22 09:30 VIC L644344 Chlordane <0.0225 H Ng/L 0.0225 0.204 10 10/20/22 09:30 VIC L644344 alpha -Chlordane <0.0021 H ug/L 0.0021 0.0408 10 10/20/22 09:30 VIC L644344 gamma -Chlordane <0.0015 H Ng/L 0.0015 0.0408 10 10/20/22 09:30 VIC L644344 4,4'-DDD <0.0022 H ug/L 0.0022 0.0408 10 10/20/22 09:30 VIC L644344 4,4'-DDE <0.0021 H Ng/L 0.0021 0.0408 10 10/20/22 09:30 VIC L644344 4,4'-DDT <0.0035 H ug/L 0.0035 0.0408 10 10/20/22 09:30 VIC L644344 Dieldrin <0.0015 H Ng/L 0.0015 0.0408 10 10/20/22 09:30 VIC L644344 EndosulfanI <0.0015 H ug/L 0.0015 0.0408 10 10/20/22 09:30 VIC L644344 EndosulfanII <0.0029 H Ng/L 0.0029 0.0408 10 10/20/22 09:30 VIC L644344 Endosulfan Sulfate <0.0015 H ug/L 0.0015 0.0408 10 10/20/22 09:30 VIC L644344 Endrin <0.0015 H Ng/L 0.0015 0.0408 10 10/20/22 09:30 VIC L644344 Endrin Aldehyde <0.0015 H ug/L 0.0015 0.0408 10 10/20/22 09:30 VIC L644344 Endrin Ketone <0.0015 H Ng/L 0.0015 0.0408 10 10/20/22 09:30 VIC L644344 gamma-BHC <0.0018 H ug/L 0.0018 0.0408 10 10/20/22 09:30 VIC L644344 Heptachlor <0.0015 H Ng/L 0.0015 0.0408 10 10/20/22 09:30 VIC L644344 Heptachlor Epoxide <0.0015 H ug/L 0.0015 0.0408 10 10/20/22 09:30 VIC L644344 Methoxychlor <0.0014 H Ng/L 0.0014 0.0408 10 10/20/22 09:30 VIC L644344 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 37 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 Lab No : 89902 Sample ID: MW-07-20221003 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/3/2022 12:40 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0205 H Ng/L 0.0205 0.306 10 10/20/22 09:30 VIC L644344 Surrogate: Decachlorobiphenyl 93.1 Limits: 36-116% 10 10/20/22 09:30 L644344 Surrogate: Tetrachloro-m-xylene 71.2 Limits: 25-123% 10 10/20/22 09:30 L644344 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2309 Pg/L 0.2309 0.2778 1 10/14/22 21:58 VIC L643610 Dalapon <0.5721 Ng/L 0.5721 0.6111 1 10/14/22 21:58 VIC L643610 2,4-DB <0.1516 ug/L 0.1516 0.2778 1 10/14/22 21:58 VIC L643610 Dicam ba <0.06332 Ng/L 0.06332 0.01111 1 10/14/22 21:58 VIC L643610 Dichlorprop <0.08842 ug/L 0.08842 0.1111 1 10/14/22 21:58 VIC L643610 Dinoseb <0.02997 Ng/L 0.02997 0.1111 1 10/14/22 21:58 VIC L643610 MCPA <21.09 ug/L 21.09 55.56 1 10/14/22 21:58 VIC L643610 MCPP <13.06 Ng/L 13.06 55.56 1 10/14/22 21:58 VIC L643610 Picloram <0.05030 ug/L 0.05030 0.1111 1 10/14/22 21:58 VIC L643610 2,4,5-T <0.01113 Ng/L 0.01113 0.03333 1 10/14/22 21:58 VIC L643610 2,4,5-TP(Silvex) <0.01815 ug/L 0.01815 0.1111 1 10/14/22 21:58 VIC L643610 Surrogate: DCAA 100.0 Limits: 20-150% 1 10/14/22 21:58 L643610 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 38 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25068 10/12/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/10/22 19:06 ANG V24950 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/13/22 08:58 ANG V25069 Acrolein <2.00 Ng/L 2.00 5.00 1 10/10/22 19:06 ANG V24950 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/10/22 19:06 ANG V24950 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/13/22 08:58 ANG V25069 Benzene 1.56 ug/L 0.180 0.500 1 10/10/22 19:06 ANG V24950 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/10/22 19:06 ANG V24950 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/10/22 19:06 ANG V24950 Bromoform <1.50 Ng/L 1.50 5.00 1 10/10/22 19:06 ANG V24950 Bromomethane <0.280 ug/L 0.280 1.00 1 10/10/22 19:06 ANG V24950 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/10/22 19:06 ANG V24950 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/10/22 19:06 ANG V24950 Chlorobenzene 4.46 Ng/L 0.190 0.500 1 10/10/22 19:06 ANG V24950 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/10/22 19:06 ANG V24950 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/10/22 19:06 ANG V24950 Chloroform <0.220 ug/L 0.220 0.500 1 10/10/22 19:06 ANG V24950 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/10/22 19:06 ANG V24950 Chloroprene <0.450 ug/L 0.450 10.0 1 10/13/22 08:58 ANG V25069 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/10/22 19:06 ANG V24950 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/10/22 19:06 ANG V24950 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/10/22 19:06 ANG V24950 trans-1,4-Dichloro-2-butene <1.30 ug/L 1.30 10.0 1 10/10/22 19:06 ANG V24950 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 39 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25068 10/12/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene 0.3193 Ng/L 0.220 0.500 1 10/10/22 19:06 ANG V24950 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/10/22 19:06 ANG V24950 1,4-Dichlorobenzene 4.58 Ng/L 0.210 0.500 1 10/10/22 19:06 ANG V24950 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/10/22 19:06 ANG V24950 1,1-Dichloroethane <0.240 Ng/L 0.240 0.500 1 10/10/22 19:06 ANG V24950 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/10/22 19:06 ANG V24950 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/10/22 19:06 ANG V24950 cis- 1,2-Dich loroethene 2.01 ug/L 0.200 0.500 1 10/10/22 19:06 ANG V24950 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/10/22 19:06 ANG V24950 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/10/22 19:06 ANG V24950 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/10/22 19:06 ANG V24950 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/10/22 19:06 ANG V24950 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/10/22 19:06 ANG V24950 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/10/22 19:06 ANG V24950 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/10/22 19:06 ANG V24950 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/13/22 08:58 ANG V25069 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/10/22 19:06 ANG V24950 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/10/22 19:06 ANG V24950 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/10/22 19:06 ANG V24950 Iodomethane <0.054 ug/L 0.054 0.500 1 10/10/22 19:06 ANG V24950 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/10/22 19:06 ANG V24950 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/13/22 08:58 ANG V25069 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 40 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 V25068 10/12/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/10/22 19:06 ANG V24950 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/10/22 19:06 ANG V24950 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/10/22 19:06 ANG V24950 Propionitrile <23.7 ug/L 23.7 10.0 1 10/13/22 08:58 ANG V25069 Styrene <0.220 Ng/L 0.220 0.500 1 10/10/22 19:06 ANG V24950 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 19:06 ANG V24950 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/10/22 19:06 ANG V24950 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/10/22 19:06 ANG V24950 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/10/22 19:06 ANG V24950 Toluene <0.220 ug/L 0.220 0.500 1 10/10/22 19:06 ANG V24950 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/10/22 19:06 ANG V24950 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 19:06 ANG V24950 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/10/22 19:06 ANG V24950 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/10/22 19:06 ANG V24950 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/10/22 19:06 ANG V24950 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/10/22 19:06 ANG V24950 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/10/22 19:06 ANG V24950 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/10/22 19:06 ANG V24950 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/10/22 19:06 ANG V24950 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/10/22 19:06 ANG V24950 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 41 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Analytical Method: 8260D Prep Method: 5030E Test Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Analytical Method: 8270C Prep Method: 3510C Test Prep Batch(es): V24949 10/10/22 09:00 V25068 10/12/22 09:00 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.21 N9/L 0.210 0.500 1 10/10/22 19:06 V24950 98.6 Limits:80-124% 1 10/10/2219:06 ANG V24950 97.0 Limits:75-129% 1 10/10/2219:06 ANG V24950 93.6 Limits:63-136% 1 10/10/2219:06 ANG V24950 96.0 Limits:77-123% 1 10/10/2219:06 ANG V24950 104 Limits: 80-124% 1 10/13/22 08:58 ANG V25069 103 Limits: 75-129% 1 10/13/22 08:58 ANG V25069 108 Limits: 63-136% 1 10/13/22 08:58 ANG V25069 112 Limits: 77-123% 1 10/13/22 08:58 ANG V25069 Prep Batch(es): L642252 10/10/22 15:46 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dimethoate <0.713 Disulfoton <0.466 Ethyl Parathion <0.568 Famphur <0.512 Methyl Parathion <0.805 Phorate <0.659 Surrogate: Tributyl phosphate Surrogate: Triphenyl phosphate u9/L 0.713 1.00 N9/L 0.466 1.00 u9/L 0.568 1.00 N9/L 0.512 1.00 u9/L 0.805 1.00 N9/L 0.659 1.00 63.5 Limits: 50-150% 67.0 Limits: 50-150% 1 10/24/22 15:13 VBW L644472 1 10/24/22 15:13 VBW L644472 1 10/24/22 15:13 VBW L644472 1 10/24/22 15:13 VBW L644472 1 10/24/22 15:13 VBW L644472 1 10/24/22 15:13 VBW L644472 1 10/24/22 15:13 VBW 8270C 1 10/24/22 15:13 VBW 8270C Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 42 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,3-Dinitrobenzene <0.904 Ng/L 0.904 10.0 1 10/20/22 20:46 VBW L644470 1,3,5-Trinitrobenzene <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW L644471 Acenaphthene <0.422 Ng/L 0.422 2.00 1 10/20/22 20:46 VBW L644470 Acenaphthylene <0.429 ug/L 0.429 2.00 1 10/20/22 20:46 VBW L644470 Acetophenone <0.686 Ng/L 0.686 5.00 1 10/20/22 20:46 VBW L644470 Anthracene <0.467 ug/L 0.467 2.00 1 10/20/22 20:46 VBW L644470 Benzo(a)anthracene <0.427 Ng/L 0.427 2.00 1 10/20/22 20:46 VBW L644470 Benzo(a)pyrene <1.00 ug/L 1.00 2.00 1 10/20/22 20:46 VBW L644470 Benzo(b)fluoranthene <0.941 Ng/L 0.941 2.00 1 10/20/22 20:46 VBW L644470 Benzo(g,h,i)perylene <1.36 ug/L 1.36 2.00 1 10/20/22 20:46 VBW L644470 Benzo(k)fluoranthene <0.752 Ng/L 0.752 2.00 1 10/20/22 20:46 VBW L644470 Benzyl alcohol <3.01 ug/L 3.01 10.0 1 10/20/22 20:46 VBW L644470 Bis(2-Chloroethoxy)methane <0.433 Ng/L 0.433 5.00 1 10/20/22 20:46 VBW L644470 Bis(2-Chloroethyl)ether <0.447 ug/L 0.447 5.00 1 10/20/22 20:46 VBW L644470 Bis(2-Chloroisopropyl)ether <0.546 Ng/L 0.546 5.00 1 10/20/22 20:46 VBW L644470 Bis(2-ethylhexyl)phthalate <3.66 ug/L 3.66 5.00 1 10/20/22 20:46 VBW L644470 4-Bromophenyl phenyl ether <0.500 Ng/L 0.500 5.00 1 10/20/22 20:46 VBW L644470 Butyl benzyl phthalate <4.59 ug/L 4.59 5.00 1 10/20/22 20:46 VBW L644470 4-Chloro-3-methylphenol <0.503 Ng/L 0.503 5.00 1 10/20/22 20:46 VBW L644470 4-Chloroaniline <0.526 ug/L 0.526 5.00 1 10/20/22 20:46 VBW L644470 Chlorobenzilate <1.90 Ng/L 1.90 5.00 1 10/20/22 20:46 VBW L644470 2-Chloronaphthalene <0.476 ug/L 0.476 5.00 1 10/20/22 20:46 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 43 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2-Chlorophenol <0.736 Ng/L 0.736 5.00 1 10/20/22 20:46 VBW L644470 4-Chlorophenyl phenyl ether <0.479 ug/L 0.479 5.00 1 10/20/22 20:46 VBW L644470 Chrysene <0.731 Ng/L 0.731 2.00 1 10/20/22 20:46 VBW L644470 Dibenz(a,h)anthracene <0.252 ug/L 0.252 2.00 1 10/20/22 20:46 VBW L644470 Dibenzofuran <0.423 Ng/L 0.423 5.00 1 10/20/22 20:46 VBW L644470 1,2-Dichlorobenzene <0.629 ug/L 0.629 5.00 1 10/20/22 20:46 VBW L644470 1,3-Dichlorobenzene <0.491 Ng/L 0.491 5.00 1 10/20/22 20:46 VBW L644470 1,4-Dichlorobenzene 2.44 J ug/L 0.580 5.00 1 10/20/22 20:46 VBW L644470 3,3'-Dichlorobenzidine <3.74 Ng/L 3.74 10.0 1 10/20/22 20:46 VBW L644470 2,4-Dichlorophenol <1.52 ug/L 1.52 5.00 1 10/20/22 20:46 VBW L644470 2,6-Dichlorophenol <0.703 Ng/L 0.703 5.00 1 10/20/22 20:46 VBW L644470 Diethyl phthalate <0.585 ug/L 0.585 5.00 1 10/20/22 20:46 VBW L644470 Dimethyl phthalate <0.510 Ng/L 0.510 5.00 1 10/20/22 20:46 VBW L644470 3,3' Dimethylbenzidine <1.88 ug/L 1.88 10.0 1 10/20/22 20:46 VBW L644470 2,4-Dimethyl phenol <0.674 M Ng/L 0.674 5.00 1 10/20/22 20:46 VBW L644470 Di-n-butyl phthalate <1.58 ug/L 1.58 5.00 1 10/20/22 20:46 VBW L644470 4,6- Din itro-2- methyl phenol <3.47 Ng/L 3.47 10.0 1 10/20/22 20:46 VBW L644470 2,4-Dinitrophenol <4.85 ug/L 4.85 10.0 1 10/20/22 20:46 VBW L644470 2,4-Dinitrotoluene <0.403 Ng/L 0.403 5.00 1 10/20/22 20:46 VBW L644470 2,6-Dinitrotoluene <0.413 ug/L 0.413 5.00 1 10/20/22 20:46 VBW L644470 Di-n-Octyl Phthalate <1.72 Ng/L 1.72 5.00 1 10/20/22 20:46 VBW L644470 Ethyl methanesulfonate <0.714 ug/L 0.714 5.00 1 10/20/22 20:46 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 44 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPORT OF ANAL YSIS Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Fluoranthene <0.406 Ng/L 0.406 2.00 1 10/20/22 20:46 VBW L644470 Fluorene <0.444 ug/L 0.444 2.00 1 10/20/22 20:46 VBW L644470 Hexachlorobenzene <2.57 Ng/L 2.57 5.00 1 10/20/22 20:46 VBW L644470 Hexachlorobutadiene <0.405 ug/L 0.405 5.00 1 10/20/22 20:46 VBW L644470 Hexachlorocyclopentadiene <2.34 Ng/L 2.34 5.00 1 10/20/22 20:46 VBW L644470 Hexachloroethane <0.277 ug/L 0.277 5.00 1 10/20/22 20:46 VBW L644470 Indeno(1,2,3-cd)pyrene <1.01 Ng/L 1.01 2.00 1 10/20/22 20:46 VBW L644470 Isodrin <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW L644471 Isophorone <0.360 Ng/L 0.360 5.00 1 10/20/22 20:46 VBW L644470 Kepone <10.0 ug/L 10.0 10.0 1 10/20/22 20:46 VBW L644471 Methyl methanesulfonate <0.618 Ng/L 0.618 5.00 1 10/20/22 20:46 VBW L644470 2-Methylnaphthalene <0.485 ug/L 0.485 2.00 1 10/20/22 20:46 VBW L644470 2-Methylphenol <0.721 Ng/L 0.721 5.00 1 10/20/22 20:46 VBW L644470 3&4 Methylphenol <0.691 ug/L 0.691 5.00 1 10/20/22 20:46 VBW L644470 Naphthalene <0.484 Ng/L 0.484 2.00 1 10/20/22 20:46 VBW L644470 2-Nitroaniline <0.574 ug/L 0.574 5.00 1 10/20/22 20:46 VBW L644470 3-Nitroaniline <1.53 Ng/L 1.53 10.0 1 10/20/22 20:46 VBW L644470 4-Nitroaniline <0.740 ug/L 0.740 5.00 1 10/20/22 20:46 VBW L644470 Nitrobenzene <0.531 Ng/L 0.531 5.00 1 10/20/22 20:46 VBW L644470 2-Nitrophenol <0.606 ug/L 0.606 5.00 1 10/20/22 20:46 VBW L644470 4-Nitrophenol <1.39 Ng/L 1.39 10.0 1 10/20/22 20:46 VBW L644470 N-Nitrosodimethylamine <0.249 ug/L 0.249 5.00 1 10/20/22 20:46 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 45 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPORT OF ANAL YSIS Lab No : 89902 Matrix: Aqueous Sample ID: MW-07-20221003 Sampled: 10/3/2022 12:40 Analytical Method: 8270D Prep Batch(es): L642250 10/10/22 15:44 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch N-Nitrosodiphenylamine <0.783 Ng/L 0.783 10.0 1 10/20/22 20:46 VBW L644470 N-Nitrosodiethylamine <0.400 ug/L 0.400 5.00 1 10/20/22 20:46 VBW L644470 N-Nitroso-di-n-butylamine <0.752 Ng/L 0.752 5.00 1 10/20/22 20:46 VBW L644470 N-Nitroso-di-n-propylamine <0.334 ug/L 0.334 5.00 1 10/20/22 20:46 VBW L644470 Pentachlorobenzene <0.459 Ng/L 0.459 10.0 1 10/20/22 20:46 VBW L644470 Pentachloronitrobenzene <1.15 ug/L 1.15 5.00 1 10/20/22 20:46 VBW L644470 Pentachlorophenol <2.45 Ng/L 2.45 10.0 1 10/20/22 20:46 VBW L644470 Phenacetin <1.28 ug/L 1.28 5.00 1 10/20/22 20:46 VBW L644470 Phenanthrene <0.464 Ng/L 0.464 2.00 1 10/20/22 20:46 VBW L644470 Phenol <0.389 ug/L 0.389 5.00 1 10/20/22 20:46 VBW L644470 Pyrene <1.04 Ng/L 1.04 2.00 1 10/20/22 20:46 VBW L644470 1,2,4,5-Tetrachlorobenzene <0.317 ug/L 0.317 5.00 1 10/20/22 20:46 VBW L644470 2,3,4,6-Tetrachlorophenol <0.355 Ng/L 0.355 5.00 1 10/20/22 20:46 VBW L644470 1,2,4-Trichlorobenzene <0.482 ug/L 0.482 5.00 1 10/20/22 20:46 VBW L644470 2,4,5-Trichlorophenol <0.350 Ng/L 0.350 5.00 1 10/20/22 20:46 VBW L644470 2,4,6-Trichlorophenol <0.344 ug/L 0.344 5.00 1 10/20/22 20:46 VBW L644470 Surrogate: 2-Fluorobiphenyl 51.4 Limits: 24-93% 1 10/20/22 20:46 VBW L644470 Surrogate: 2-Fluorophenol 28.0 Limits: 10-44% 1 10/20/22 20:46 VBW L644470 Surrogate: Nitrobenzene-d5 49.3 Limits: 20-91% 1 10/20/22 20:46 VBW L644470 Surrogate: Phenol-d6 22.7 Limits: 7-32% 1 10/20/22 20:46 VBW L644470 Surrogate: 4-Terphenyl-d14 59.2 Limits: 35-126% 1 10/20/22 20:46 VBW L644470 Surrogate: 2,4,6-Tribromophenol 62.5 Limits: 39-110% 1 10/20/22 20:46 VBW L644470 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 46 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89903 Sample ID: SW-01-20221003 Matrix: Aqueous Sampled: 10/3/2022 13:15 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane <0.139 Ng/L 0.139 2.00 1 10/06/22 12:50 TBL 8260D SIM Sulfide <0.83 mg/L 0.83 2.00 1 10/10/2211:00 SLO 4500S2F-2011 Antimony <0.680 Ng/L 0.680 2.00 1 10/10/22 19:11 EDV 6020E Arsenic <0.490 ug/L 0.490 1.00 1 10/10/22 19:11 EDV 6020B Barium 14.1 Ng/L 3.40 10.0 1 10/10/22 19:11 EDV 6020E Beryllium <0.240 ug/L 0.240 1.00 1 10/10/22 19:11 EDV 6020B Cadmium <0.150 Ng/L 0.150 1.00 1 10/10/22 19:11 EDV 6020E Chromium 1.90 J ug/L 1.00 2.00 1 10/10/22 19:11 EDV 6020B Cobalt 0.224 J Ng/L 0.080 1.00 1 10/10/22 19:11 EDV 6020E Copper 2.37 ug/L 0.890 2.00 1 10/11/22 16:29 EDV 6020B Lead <0.500 Ng/L 0.500 1.00 1 10/10/22 19:11 EDV 6020E Mercury (Total) <0.0700 ug/L 0.0700 0.200 1 10/11/22 16:09 EDV 7470A Nickel <0.720 Ng/L 0.720 2.00 1 10/10/22 19:11 EDV 6020E Selenium <2.30 ug/L 2.30 5.00 1 10/10/22 19:11 EDV 6020B Silver <0.130 Ng/L 0.130 1.00 1 10/10/22 19:11 EDV 6020E Tin <1.50 ug/L 1.50 5.00 1 10/10/22 19:11 EDV 6020B Thallium <0.280 Ng/L 0.280 2.00 1 10/10/22 19:11 EDV 6020B Vanadium <2.10 ug/L 2.10 5.00 1 10/10/22 19:11 EDV 6020B Zinc 4.85 J Ng/L 3.90 20.0 1 10/10/22 19:11 EDV 6020B Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 47 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89903 Matrix: Aqueous Sample ID: SW-01-20221003 Sampled: 10/3/2022 13:15 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0024 H Ng/L 0.0024 0.0459 10 10/20/22 09:57 VIC L644344 alpha-BHC <0.0024 H ug/L 0.0024 0.0459 10 10/20/22 09:57 VIC L644344 beta-BHC <0.0023 H Ng/L 0.0023 0.0459 10 10/20/22 09:57 VIC L644344 delta-BHC <0.0018 H ug/L 0.0018 0.0459 10 10/20/22 09:57 VIC L644344 Chlordane <0.0254 H Ng/L 0.0254 0.230 10 10/20/22 09:57 VIC L644344 alpha -Chlordane <0.0024 H ug/L 0.0024 0.0459 10 10/20/22 09:57 VIC L644344 gamma -Chlordane <0.0017 H Ng/L 0.0017 0.0459 10 10/20/22 09:57 VIC L644344 4,4'-DDD <0.0024 H ug/L 0.0024 0.0459 10 10/20/22 09:57 VIC L644344 4,4'-DDE <0.0024 H Ng/L 0.0024 0.0459 10 10/20/22 09:57 VIC L644344 4,4'-DDT <0.0040 H ug/L 0.0040 0.0459 10 10/20/22 09:57 VIC L644344 Dieldrin <0.0017 H Ng/L 0.0017 0.0459 10 10/20/22 09:57 VIC L644344 EndosulfanI <0.0017 H ug/L 0.0017 0.0459 10 10/20/22 09:57 VIC L644344 EndosulfanII <0.0032 H Ng/L 0.0032 0.0459 10 10/20/22 09:57 VIC L644344 Endosulfan Sulfate <0.0017 H ug/L 0.0017 0.0459 10 10/20/22 09:57 VIC L644344 Endrin <0.0017 H Ng/L 0.0017 0.0459 10 10/20/22 09:57 VIC L644344 Endrin Aldehyde <0.0017 H ug/L 0.0017 0.0459 10 10/20/22 09:57 VIC L644344 Endrin Ketone <0.0017 H Ng/L 0.0017 0.0459 10 10/20/22 09:57 VIC L644344 gamma-BHC <0.0020 H ug/L 0.0020 0.0459 10 10/20/22 09:57 VIC L644344 Heptachlor <0.0017 H Ng/L 0.0017 0.0459 10 10/20/22 09:57 VIC L644344 Heptachlor Epoxide <0.0016 H ug/L 0.0016 0.0459 10 10/20/22 09:57 VIC L644344 Methoxychlor <0.0016 H Ng/L 0.0016 0.0459 10 10/20/22 09:57 VIC L644344 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 48 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 Lab No : 89903 Sample ID: SW-01-20221003 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/3/2022 13:15 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0231 H Ng/L 0.0231 0.345 10 10/20/22 09:57 VIC L644344 Surrogate: Decachlorobiphenyl 77.7 Limits: 36-116% 10 10/20/22 09:57 L644344 Surrogate: Tetrachloro-m-xylene 58.8 Limits: 25-123% 10 10/20/22 09:57 L644344 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2445 Pg/L 0.2445 0.2941 1 10/14/22 22:23 VIC L643610 Dalapon <0.6058 Ng/L 0.6058 0.6471 1 10/14/22 22:23 VIC L643610 2,4-DB <0.1605 ug/L 0.1605 0.2941 1 10/14/22 22:23 VIC L643610 Dicam ba <0.06703 Ng/L 0.06703 0.01176 1 10/14/22 22:23 VIC L643610 Dichlorprop <0.09359 ug/L 0.09359 0.1176 1 10/14/22 22:23 VIC L643610 Dinoseb <0.03172 Ng/L 0.03172 0.1176 1 10/14/22 22:23 VIC L643610 MCPA <22.33 ug/L 22.33 58.82 1 10/14/22 22:23 VIC L643610 MCPP <13.82 Ng/L 13.82 58.82 1 10/14/22 22:23 VIC L643610 Picloram <0.05324 ug/L 0.05324 0.1176 1 10/14/22 22:23 VIC L643610 2,4,5-T <0.01178 Ng/L 0.01178 0.03529 1 10/14/22 22:23 VIC L643610 2,4,5-TP(Silvex) <0.01921 ug/L 0.01921 0.1176 1 10/14/22 22:23 VIC L643610 Surrogate: DCAA 61.20 Limits: 20-150% 1 10/14/22 22:23 L643610 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 49 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89903 Matrix: Aqueous Sample ID: SW-01-20221003 Sampled: 10/3/2022 13:15 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/11/22 01:24 MSA V24952 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/17/2219:43 ANG V25249 Acrolein <2.00 Ng/L 2.00 5.00 1 10/11/22 01:24 MSA V24952 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/11/22 01:24 MSA V24952 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/17/22 19:43 ANG V25249 Benzene <0.180 ug/L 0.180 0.500 1 10/11/22 01:24 MSA V24952 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/11/22 01:24 MSA V24952 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/11/22 01:24 MSA V24952 Bromoform <1.50 Ng/L 1.50 5.00 1 10/11/22 01:24 MSA V24952 Bromomethane <0.280 ug/L 0.280 1.00 1 10/11/22 01:24 MSA V24952 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/11/22 01:24 MSA V24952 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/11/22 01:24 MSA V24952 Chlorobenzene <0.190 Ng/L 0.190 0.500 1 10/11/22 01:24 MSA V24952 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/11/22 01:24 MSA V24952 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/11/22 01:24 MSA V24952 Chloroform <0.220 ug/L 0.220 0.500 1 10/11/22 01:24 MSA V24952 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/11/22 01:24 MSA V24952 Chloroprene <0.450 ug/L 0.450 10.0 1 10/17/2219:43 ANG V25249 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/11/22 01:24 MSA V24952 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/11/22 01:24 MSA V24952 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/11/22 01:24 MSA V24952 trans-1,4-Dichloro-2-butene <1.30 pg/L 1.30 10.0 1 10/11/22 01:24 MSA V24952 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 50 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89903 Matrix: Aqueous Sample ID: SW-01-20221003 Sampled: 10/3/2022 13:15 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene <0.220 Ng/L 0.220 0.500 1 10/11/22 01:24 MSA V24952 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/11/22 01:24 MSA V24952 1,4-Dichlorobenzene <0.210 Ng/L 0.210 0.500 1 10/11/22 01:24 MSA V24952 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/11/22 01:24 MSA V24952 1,1-Dichloroethane <0.240 Ng/L 0.240 0.500 1 10/11/22 01:24 MSA V24952 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/11/22 01:24 MSA V24952 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/11/22 01:24 MSA V24952 cis- 1,2-Dich loroethene <0.200 ug/L 0.200 0.500 1 10/11/22 01:24 MSA V24952 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/11/22 01:24 MSA V24952 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/11/22 01:24 MSA V24952 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/11/22 01:24 MSA V24952 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/11/22 01:24 MSA V24952 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/11/22 01:24 MSA V24952 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/11/22 01:24 MSA V24952 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/11/22 01:24 MSA V24952 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/17/22 19:43 ANG V25249 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/11/22 01:24 MSA V24952 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/11/22 01:24 MSA V24952 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/11/22 01:24 MSA V24952 Iodomethane <0.054 ug/L 0.054 0.500 1 10/11/22 01:24 MSA V24952 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/11/22 01:24 MSA V24952 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/17/2219:43 ANG V25249 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 51 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89903 Matrix: Aqueous Sample ID: SW-01-20221003 Sampled: 10/3/2022 13:15 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/11/22 01:24 MSA V24952 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/11/22 01:24 MSA V24952 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/11/22 01:24 MSA V24952 Propionitrile <23.7 ug/L 23.7 10.0 1 10/17/2219:43 ANG V25249 Styrene <0.220 Ng/L 0.220 0.500 1 10/11/22 01:24 MSA V24952 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 01:24 MSA V24952 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/11/22 01:24 MSA V24952 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/11/22 01:24 MSA V24952 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/11/22 01:24 MSA V24952 Toluene <0.220 ug/L 0.220 0.500 1 10/11/22 01:24 MSA V24952 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/11/22 01:24 MSA V24952 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 01:24 MSA V24952 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/11/22 01:24 MSA V24952 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/11/22 01:24 MSA V24952 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/11/22 01:24 MSA V24952 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/11/22 01:24 MSA V24952 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/11/22 01:24 MSA V24952 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/11/22 01:24 MSA V24952 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/11/22 01:24 MSA V24952 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/11/22 01:24 MSA V24952 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 52 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89903 Matrix: Aqueous Sample ID: SW-01-20221003 Sampled: 10/3/2022 13:15 Analytical Method: 8260D Prep Method: 5030E Test Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.21 Ng/L 0.210 0.500 98.6 Limits: 80-124% 98.2 Limits: 75-129% 93.2 Limits: 63-136% 96.6 Limits: 77-123% 99.2 Limits: 80-124% 97.2 Limits: 75-129% 97.0 Limits: 63-136% 99.8 Limits: 77-123% 1 10/11/22 01:24 V24952 1 10/11/22 01:24 MSA V24952 1 10/11/22 01:24 MSA V24952 1 10/11/22 01:24 MSA V24952 1 10/11/22 01:24 MSA V24952 1 10/17/22 19:43 ANG V25249 1 10/17/22 19:43 ANG V25249 1 10/17/22 19:43 ANG V25249 1 10/17/22 19:43 ANG V25249 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 53 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89904 Sample ID: SW-02-20221003 Matrix: Aqueous Sampled: 10/3/2022 14:40 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane <0.139 Ng/L 0.139 2.00 1 10/06/22 13:15 TBL 8260D SIM Sulfide 0.90 J mg/L 0.83 2.00 1 10/10/22 11:00 SLO 4500S2F-2011 Antimony <0.618 Ng/L 0.618 1.00 1 10/28/22 23:01 BKN 6020E Arsenic 0.4163 ug/L 0.297 1.00 1 11/01/22 17:01 CPW 6020B Barium 15.2 Ng/L 0.453 1.00 1 10/28/22 23:01 BKN 6020B Beryllium <0.102 ug/L 0.102 1.00 1 10/28/22 23:01 BKN 6020B Cadmium <0.350 Ng/L 0.350 1.00 1 10/28/22 23:01 BKN 6020B Chromium 0.638 J ug/L 0.346 1.00 1 10/28/22 23:01 BKN 6020B Cobalt 0.248 J Ng/L 0.060 1.00 1 10/28/22 23:01 BKN 6020B Copper 1.47 ug/L 0.489 1.00 1 10/28/22 23:01 BKN 6020B Lead 0.266 J Ng/L 0.264 1.00 1 10/28/22 23:01 BKN 6020B Mercury (Total) <0.0700 ug/L 0.0700 0.200 1 10/11/22 16:12 EDV 7470A Nickel 0.552 J Ng/L 0.182 1.00 1 10/28/22 23:01 BKN 6020B Selenium <0.703 ug/L 0.703 1.00 1 10/28/22 23:01 BKN 6020B Silver <0.0570 Ng/L 0.0570 1.00 1 10/28/22 23:01 BKN 6020B Tin <1.44 ug/L 1.44 5.00 1 10/28/22 23:01 BKN 6020B Thallium <0.0610 Ng/L 0.0610 1.00 1 10/28/22 23:01 BKN 6020B Vanadium <0.767 ug/L 0.767 5.00 1 10/28/22 23:01 BKN 6020B Zinc 13.9 Ng/L 4.67 10.0 1 10/28/22 23:01 BKN 6020B Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 54 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89904 Matrix: Aqueous Sample ID: SW-02-20221003 Sampled: 10/3/2022 14:40 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Aldrin <0.0023 H Ng/L 0.0023 0.0444 10 10/20/22 10:25 VIC L644344 alpha-BHC <0.0023 H ug/L 0.0023 0.0444 10 10/20/22 10:25 VIC L644344 beta-BHC <0.0023 H Ng/L 0.0023 0.0444 10 10/20/22 10:25 VIC L644344 delta-BHC <0.0017 H ug/L 0.0017 0.0444 10 10/20/22 10:25 VIC L644344 Chlordane <0.0245 H Ng/L 0.0245 0.222 10 10/20/22 10:25 VIC L644344 alpha -Chlordane <0.0023 H ug/L 0.0023 0.0444 10 10/20/22 10:25 VIC L644344 gamma -Chlordane <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 10:25 VIC L644344 4,4'-DDD <0.0023 H ug/L 0.0023 0.0444 10 10/20/22 10:25 VIC L644344 4,4'-DDE <0.0023 H Ng/L 0.0023 0.0444 10 10/20/22 10:25 VIC L644344 4,4'-DDT <0.0038 H ug/L 0.0038 0.0444 10 10/20/22 10:25 VIC L644344 Dieldrin <0.0017 H Ng/L 0.0017 0.0444 10 10/20/22 10:25 VIC L644344 EndosulfanI <0.0017 H ug/L 0.0017 0.0444 10 10/20/22 10:25 VIC L644344 EndosulfanII <0.0031 H Ng/L 0.0031 0.0444 10 10/20/22 10:25 VIC L644344 Endosulfan Sulfate <0.0016 H ug/L 0.0016 0.0444 10 10/20/22 10:25 VIC L644344 Endrin <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 10:25 VIC L644344 Endrin Aldehyde <0.0016 H ug/L 0.0016 0.0444 10 10/20/22 10:25 VIC L644344 Endrin Ketone <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 10:25 VIC L644344 gamma-BHC <0.0020 H ug/L 0.0020 0.0444 10 10/20/22 10:25 VIC L644344 Heptachlor <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 10:25 VIC L644344 Heptachlor Epoxide <0.0016 H ug/L 0.0016 0.0444 10 10/20/22 10:25 VIC L644344 Methoxychlor <0.0016 H Ng/L 0.0016 0.0444 10 10/20/22 10:25 VIC L644344 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 55 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 Lab No : 89904 Sample ID: SW-02-20221003 REPOR T OF A NA L YSIS Matrix: Aqueous Sampled: 10/3/2022 14:40 Analytical Method: 8081B Prep Batch(es): L644115 10/19/22 16:59 Prep Method: 3510C Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Toxaphene <0.0223 H Ng/L 0.0223 0.333 10 10/20/22 10:25 VIC L644344 Surrogate: Decachlorobiphenyl 96.6 Limits: 36-116% 10 10/20/22 10:25 L644344 Surrogate: Tetrachloro-m-xylene 75.9 Limits: 25-123% 10 10/20/22 10:25 L644344 Analytical Method: 8151A Prep Batch(es): L642283 10/10/22 17:03 Prep Method: 8151A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,4-D <0.2375 Pg/L 0.2375 0.2857 1 10/14/22 22:48 VIC L643610 Dalapon <0.5885 Ng/L 0.5885 0.6286 1 10/14/22 22:48 VIC L643610 2,4-DB <0.1559 ug/L 0.1559 0.2857 1 10/14/22 22:48 VIC L643610 Dicamba <0.06509 Ng/L 0.06509 0.01142 1 10/14/22 22:48 VIC L643610 Dichlorprop <0.09097 ug/L 0.09097 0.1143 1 10/14/22 22:48 VIC L643610 Dinoseb <0.03083 Ng/L 0.03083 0.1143 1 10/14/22 22:48 VIC L643610 MCPA <21.69 ug/L 21.69 57.14 1 10/14/22 22:48 VIC L643610 MCPP <13.43 Ng/L 13.43 57.14 1 10/14/22 22:48 VIC L643610 Picloram <0.05175 ug/L 0.05175 0.1143 1 10/14/22 22:48 VIC L643610 2,4,5-T <0.01144 Ng/L 0.01144 0.03428 1 10/14/22 22:48 VIC L643610 2,4,5-TP(Silvex) <0.01867 ug/L 0.01867 0.1143 1 10/14/22 22:48 VIC L643610 Surrogate: DCAA 68.01 Limits: 20-150% 1 10/14/22 22:48 L643610 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 56 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89904 Matrix: Aqueous Sample ID: SW-02-20221003 Sampled: 10/3/2022 14:40 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/11/22 01:51 MSA V24952 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/17/22 20:10 ANG V25249 Acrolein <2.00 Ng/L 2.00 5.00 1 10/11/22 01:51 MSA V24952 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/11/22 01:51 MSA V24952 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/17/22 20:10 ANG V25249 Benzene <0.180 ug/L 0.180 0.500 1 10/11/22 01:51 MSA V24952 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/11/22 01:51 MSA V24952 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/11/22 01:51 MSA V24952 Bromoform <1.50 Ng/L 1.50 5.00 1 10/11/22 01:51 MSA V24952 Bromomethane <0.280 ug/L 0.280 1.00 1 10/11/22 01:51 MSA V24952 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/11/22 01:51 MSA V24952 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/11/22 01:51 MSA V24952 Chlorobenzene <0.190 Ng/L 0.190 0.500 1 10/11/22 01:51 MSA V24952 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/11/22 01:51 MSA V24952 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/11/22 01:51 MSA V24952 Chloroform <0.220 ug/L 0.220 0.500 1 10/11/22 01:51 MSA V24952 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/11/22 01:51 MSA V24952 Chloroprene <0.450 ug/L 0.450 10.0 1 10/17/22 20:10 ANG V25249 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/11/22 01:51 MSA V24952 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/11/22 01:51 MSA V24952 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/11/22 01:51 MSA V24952 trans-1,4-Dichloro-2-butene <1.30 pg/L 1.30 10.0 1 10/11/22 01:51 MSA V24952 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 57 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPORT OF ANAL YSIS Lab No : 89904 Matrix: Aqueous Sample ID: SW-02-20221003 Sampled: 10/3/2022 14:40 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene <0.220 Ng/L 0.220 0.500 1 10/11/22 01:51 MSA V24952 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/11/22 01:51 MSA V24952 1,4-Dichlorobenzene <0.210 Ng/L 0.210 0.500 1 10/11/22 01:51 MSA V24952 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/11/22 01:51 MSA V24952 1,1-Dichloroethane <0.240 Ng/L 0.240 0.500 1 10/11/22 01:51 MSA V24952 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/11/22 01:51 MSA V24952 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/11/22 01:51 MSA V24952 cis- 1,2-Dich loroethene <0.200 ug/L 0.200 0.500 1 10/11/22 01:51 MSA V24952 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/11/22 01:51 MSA V24952 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/11/22 01:51 MSA V24952 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/11/22 01:51 MSA V24952 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/11/22 01:51 MSA V24952 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/11/22 01:51 MSA V24952 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/11/22 01:51 MSA V24952 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/11/22 01:51 MSA V24952 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/17/22 20:10 ANG V25249 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/11/22 01:51 MSA V24952 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/11/22 01:51 MSA V24952 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/11/22 01:51 MSA V24952 Iodomethane <0.054 ug/L 0.054 0.500 1 10/11/22 01:51 MSA V24952 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/11/22 01:51 MSA V24952 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/17/22 20:10 ANG V25249 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 58 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89904 Matrix: Aqueous Sample ID: SW-02-20221003 Sampled: 10/3/2022 14:40 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone <1.00 Ng/L 1.00 5.00 1 10/11/22 01:51 MSA V24952 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/11/22 01:51 MSA V24952 Naphthalene <0.470 Ng/L 0.470 1.00 1 10/11/22 01:51 MSA V24952 Propionitrile <23.7 ug/L 23.7 10.0 1 10/17/22 20:10 ANG V25249 Styrene <0.220 Ng/L 0.220 0.500 1 10/11/22 01:51 MSA V24952 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 01:51 MSA V24952 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/11/22 01:51 MSA V24952 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/11/22 01:51 MSA V24952 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/11/22 01:51 MSA V24952 Toluene <0.220 ug/L 0.220 0.500 1 10/11/22 01:51 MSA V24952 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/11/22 01:51 MSA V24952 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 01:51 MSA V24952 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/11/22 01:51 MSA V24952 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/11/22 01:51 MSA V24952 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/11/22 01:51 MSA V24952 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/11/22 01:51 MSA V24952 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/11/22 01:51 MSA V24952 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/11/22 01:51 MSA V24952 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/11/22 01:51 MSA V24952 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/11/22 01:51 MSA V24952 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 59 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89904 Matrix: Aqueous Sample ID: SW-02-20221003 Sampled: 10/3/2022 14:40 Analytical Method: 8260D Prep Method: 5030E Test Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0.21 Ng/L 0.210 0.500 98.0 Limits: 80-124% 95.6 Limits: 75-129% 92.6 Limits: 63-136% 97.2 Limits: 77-123% 99.6 Limits: 80-124% 98.0 Limits: 75-129% 98.2 Limits: 63-136% 101 Limits: 77-123% 1 10/11/22 01:51 V24952 1 10/11/22 01:51 MSA V24952 1 10/11/22 01:51 MSA V24952 1 10/11/22 01:51 MSA V24952 1 10/11/22 01:51 MSA V24952 1 10/17/22 20:10 ANG V25249 1 10/17/22 20:10 ANG V25249 1 10/17/22 20:10 ANG V25249 1 10/17/22 20:10 ANG V25249 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 60 of 123 WavDdibnto ANALYTICAL 01015 Anchor QEA of North Carolina, PLLC Chuck Pippin 231 Haywood Street Asheville , NC 28801 Report Number : 22-277-0040 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti ca Isom Project ID : Project Jackson County Information : C21480-01.01, WA-1 REPORT OF ANAL YSIS Report Date : 11/09/2022 Received : 10/04/2022 Lab No : 89905 Matrix: Aqueous Sample ID: LT-01-20221003 Sampled: 10/3/2022 16:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane 80.0 Ng/L 0.139 2.00 1 10/06/22 13:40 TBL 8260D SIM Antimony <3.40 ug/L 3.40 10.0 5 10/10/2219:45 EDV 6020B Dissolved Antimony <6.18 Ng/L 6.18 10.0 10 10/29/22 14:26 BKN 6020B Arsenic 85.7 pg/L 2.45 5.00 5 10/10/2219:45 EDV 6020B Dissolved Arsenic 12.3 Ng/L 2.97 10.0 10 10/29/22 14:26 BKN 6020B Barium 4460 ug/L 4.53 10.0 10 10/28/2211:05 BKN 6020B Dissolved Barium 410 Ng/L 4.53 10.0 10 10/29/22 14:26 BKN 6020E Beryllium 10.6 ug/L 1.20 5.00 5 10/10/2219:45 EDV 6020B Dissolved Beryllium <1.02 Ng/L 1.02 10.0 10 10/29/22 14:26 BKN 6020E Cadmium <0.750 ug/L 0.750 5.00 5 10/10/2219:45 EDV 6020B Dissolved Cadmium <3.50 Ng/L 3.50 10.0 10 10/29/22 14:26 BKN 6020E Chromium 476 ug/L 5.00 10.0 5 10/10/2219:45 EDV 6020B Dissolved Chromium 6.093 Ng/L 3.46 10.0 10 10/29/22 14:26 BKN 6020E Cobalt 151 ug/L 0.400 5.00 5 10/10/2219:45 EDV 6020B Dissolved Cobalt 9.563 Ng/L 0.600 10.0 10 10/29/22 14:26 BKN 6020E Copper 238 ug/L 4.45 10.0 5 10/11/22 17:02 EDV 6020B Dissolved Copper <4.89 Ng/L 4.89 10.0 10 10/29/22 14:26 BKN 6020E Lead 86.4 ug/L 2.50 5.00 5 10/10/22 19:45 EDV 6020B Dissolved Lead <2.64 Ng/L 2.64 10.0 10 10/29/22 14:26 BKN 6020E Mercury (Total) <0.300 ug/L 0.300 0.800 1 10/11/22 16:14 EDV 7470A Dissolved Mercury <0.0700 Ng/L 0.0700 0.200 1 10/24/22 15:35 EDV 7470A Dissolved Nickel 33.4 ug/L 1.82 10.0 10 10/29/22 14:26 BKN 6020B Nickel 232 Ng/L 3.60 10.0 5 10/10/2219:45 EDV 6020E Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 61 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89905 Sample ID: LT-01-20221003 Matrix: Aqueous Sampled: 10/3/2022 16:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium 125 Ng/L 11.5 25.0 5 10/10/22 19:45 EDV 6020B Dissolved Selenium <7.03 ug/L 7.03 10.0 10 10/29/22 14:26 BKN 6020B Silver <0.650 Ng/L 0.650 5.00 5 10/10/22 19:45 EDV 6020E Dissolved Silver <0.570 ug/L 0.570 10.0 10 10/29/22 14:26 BKN 6020B Tin 18.73 Ng/L 7.50 25.0 5 10/10/22 19:45 EDV 6020B Dissolved Tin <14.4 ug/L 14.4 50.0 10 10/29/22 14:26 BKN 6020B Thallium 2.983 Ng/L 1.40 10.0 5 10/10/22 19:45 EDV 6020B Dissolved Thallium <0.610 ug/L 0.610 10.0 10 10/29/22 14:26 BKN 6020B Vanadium 581 Ng/L 10.5 25.0 5 10/10/22 19:45 EDV 6020B Dissolved Vanadium <7.67 ug/L 7.67 50.0 10 10/29/22 14:26 BKN 6020B Zinc 764 Ng/L 19.5 100 5 10/10/22 19:45 EDV 6020B Dissolved Zinc <46.7 ug/L 46.7 100 10 10/29/22 14:26 BKN 6020B Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 62 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89905 Matrix: Aqueous Sample ID: LT-01-20221003 Sampled: 10/3/2022 16:00 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/11/22 02:18 MSA V24952 Acetonitrile <20.3 ug/L 20.3 10.0 1 10/17/22 20:37 ANG V25249 Acrolein <2.00 Ng/L 2.00 5.00 1 10/11/22 02:18 MSA V24952 Acrylonitrile <0.230 ug/L 0.230 5.00 1 10/11/22 02:18 MSA V24952 Allyl Chloride <0.579 Ng/L 0.579 10.0 1 10/17/22 20:37 ANG V25249 Benzene 0.568 ug/L 0.180 0.500 1 10/11/22 02:18 MSA V24952 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/11/22 02:18 MSA V24952 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/11/22 02:18 MSA V24952 Bromoform <1.50 Ng/L 1.50 5.00 1 10/11/22 02:18 MSA V24952 Bromomethane <0.280 ug/L 0.280 1.00 1 10/11/22 02:18 MSA V24952 Carbon Disulfide 0.6833 Ng/L 0.150 5.00 1 10/11/22 02:18 MSA V24952 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/11/22 02:18 MSA V24952 Chlorobenzene 1.39 Ng/L 0.190 0.500 1 10/11/22 02:18 MSA V24952 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/11/22 02:18 MSA V24952 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/11/22 02:18 MSA V24952 Chloroform <0.220 ug/L 0.220 0.500 1 10/11/22 02:18 MSA V24952 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/11/22 02:18 MSA V24952 Chloroprene <0.450 ug/L 0.450 10.0 1 10/17/22 20:37 ANG V25249 1,2-Dibromo-3-Chloropropane <1.10 Ng/L 1.10 2.00 1 10/11/22 02:18 MSA V24952 1,2-Dibromoethane <0.200 ug/L 0.200 0.500 1 10/11/22 02:18 MSA V24952 Dibromomethane <0.230 Ng/L 0.230 0.500 1 10/11/22 02:18 MSA V24952 trans-1,4-Dichloro-2-butene <1.30 ug/L 1.30 10.0 1 10/11/22 02:18 MSA V24952 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 63 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89905 Matrix: Aqueous Sample ID: LT-01-20221003 Sampled: 10/3/2022 16:00 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,2-Dichlorobenzene <0.220 Ng/L 0.220 0.500 1 10/11/22 02:18 MSA V24952 1,3-Dichlorobenzene <0.190 ug/L 0.190 0.500 1 10/11/22 02:18 MSA V24952 1,4-Dichlorobenzene 1.82 Ng/L 0.210 0.500 1 10/11/22 02:18 MSA V24952 Dichlorodifluoromethane <1.20 ug/L 1.20 5.00 1 10/11/22 02:18 MSA V24952 1,1-Dichloroethane <0.240 Ng/L 0.240 0.500 1 10/11/22 02:18 MSA V24952 1,2-Dichloroethane <0.150 ug/L 0.150 0.500 1 10/11/22 02:18 MSA V24952 1,1-Dichloroethene <0.150 Ng/L 0.150 0.500 1 10/11/22 02:18 MSA V24952 cis- 1,2-Dich loroethene <0.200 ug/L 0.200 0.500 1 10/11/22 02:18 MSA V24952 trans-1,2-Dichloroethene <0.180 Ng/L 0.180 0.500 1 10/11/22 02:18 MSA V24952 1,2-Dichloropropane <0.190 ug/L 0.190 0.500 1 10/11/22 02:18 MSA V24952 1,3-Dichloropropane <0.130 Ng/L 0.130 0.500 1 10/11/22 02:18 MSA V24952 2,2-Dichloropropane <0.210 ug/L 0.210 2.00 1 10/11/22 02:18 MSA V24952 1,1-Dichloropropene <0.200 Ng/L 0.200 0.500 1 10/11/22 02:18 MSA V24952 cis- 1,3-Dich loropropene <0.210 ug/L 0.210 0.500 1 10/11/22 02:18 MSA V24952 trans-1,3-Dichloropropene <0.150 Ng/L 0.150 0.500 1 10/11/22 02:18 MSA V24952 Ethyl Methacrylate <1.62 ug/L 1.62 10.0 1 10/17/22 20:37 ANG V25249 Ethylbenzene 0.2673 Ng/L 0.170 0.500 1 10/11/22 02:18 MSA V24952 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/11/22 02:18 MSA V24952 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/11/22 02:18 MSA V24952 Iodomethane <0.054 ug/L 0.054 0.500 1 10/11/22 02:18 MSA V24952 Methyl Ethyl Ketone (MEK) 2.363 Ng/L 0.710 5.00 1 10/11/22 02:18 MSA V24952 Methacrylonitrile <12.6 ug/L 12.6 10.0 1 10/17/22 20:37 ANG V25249 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 64 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89905 Matrix: Aqueous Sample ID: LT-01-20221003 Sampled: 10/3/2022 16:00 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 4-Methyl-2-Pentanone 1.123 Ng/L 1.00 5.00 1 10/11/22 02:18 MSA V24952 Methylene Chloride <0.330 ug/L 0.330 1.00 1 10/11/22 02:18 MSA V24952 Naphthalene 3.66 Ng/L 0.470 1.00 1 10/11/22 02:18 MSA V24952 Propionitrile <23.7 ug/L 23.7 10.0 1 10/17/22 20:37 ANG V25249 Styrene <0.220 Ng/L 0.220 0.500 1 10/11/22 02:18 MSA V24952 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 02:18 MSA V24952 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/11/22 02:18 MSA V24952 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/11/22 02:18 MSA V24952 Tetrahydrofuran 67.8 Ng/L 1.50 10.0 1 10/11/22 02:18 MSA V24952 Toluene 0.240 J ug/L 0.220 0.500 1 10/11/22 02:18 MSA V24952 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/11/22 02:18 MSA V24952 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/11/22 02:18 MSA V24952 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/11/22 02:18 MSA V24952 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/11/22 02:18 MSA V24952 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/11/22 02:18 MSA V24952 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/11/22 02:18 MSA V24952 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/11/22 02:18 MSA V24952 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/11/22 02:18 MSA V24952 o-Xylene 0.4653 Ng/L 0.210 0.500 1 10/11/22 02:18 MSA V24952 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/11/22 02:18 MSA V24952 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 65 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89905 Matrix: Aqueous Sample ID: LT-01-20221003 Sampled: 10/3/2022 16:00 Analytical Method: 8260D Prep Batch(es): V24951 10/07/22 14:00 V25248 10/17/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Xylene (Total) Surrogate: 4-Bromofl uorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane - d4 Surrogate: Toluene-d8 0.4653 Ng/L 0.210 0.500 99.4 Limits: 80-124% 98.0 Limits: 75-129% 93.8 Limits: 63-136% 95.4 Limits: 77-123% 99.6 Limits: 80-124% 98.0 Limits: 75-129% 99.0 Limits: 63-136% 100 Limits: 77-123% 1 10/11/22 02:18 KCC V24952 1 10/11/22 02:18 MSA V24952 1 10/11/22 02:18 MSA V24952 1 10/11/22 02:18 MSA V24952 1 10/11/22 02:18 MSA V24952 1 10/17/22 20:37 ANG V25249 1 10/17/22 20:37 ANG V25249 1 10/17/22 20:37 ANG V25249 1 10/17/22 20:37 ANG V25249 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 66 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89909 Matrix: Aqueous Sample ID : TB-20221003-2 Sampled: 10/3/2022 0:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method 1,4-Dioxane <0.139 Ng/L 0.139 2.00 1 10/06/22 14:06 TBL 8260D SIM Surrogate: 4-Bromofluorobenzene 134 * Limits: 70-130% 1 10/06/22 14:06 TBL V24810 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 67 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89909 Matrix: Aqueous Sample ID : TB-20221003-2 Sampled: 10/3/2022 0:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Acetone <1.80 Ng/L 1.80 5.00 1 10/10/22 13:42 ANG V24950 Acrolein <2.00 ug/L 2.00 5.00 1 10/10/22 13:42 ANG V24950 Acrylonitrile <0.230 Ng/L 0.230 5.00 1 10/10/22 13:42 ANG V24950 Benzene <0.180 ug/L 0.180 0.500 1 10/10/22 13:42 ANG V24950 Bromochloromethane <0.420 Ng/L 0.420 1.00 1 10/10/22 13:42 ANG V24950 Bromodichloromethane <0.160 ug/L 0.160 0.500 1 10/10/22 13:42 ANG V24950 Bromoform <1.50 Ng/L 1.50 5.00 1 10/10/22 13:42 ANG V24950 Bromomethane <0.280 ug/L 0.280 1.00 1 10/10/22 13:42 ANG V24950 Carbon Disulfide <0.150 Ng/L 0.150 5.00 1 10/10/22 13:42 ANG V24950 Carbon Tetrachloride <0.180 ug/L 0.180 0.500 1 10/10/22 13:42 ANG V24950 Chlorobenzene <0.190 Ng/L 0.190 0.500 1 10/10/22 13:42 ANG V24950 Chlorodibromomethane <0.190 ug/L 0.190 0.500 1 10/10/22 13:42 ANG V24950 Chloroethane <0.430 Ng/L 0.430 1.00 1 10/10/22 13:42 ANG V24950 Chloroform <0.220 ug/L 0.220 0.500 1 10/10/22 13:42 ANG V24950 Chloromethane <0.220 Ng/L 0.220 0.500 1 10/10/22 13:42 ANG V24950 1,2-Dibromo-3-Chloropropane <1.10 ug/L 1.10 2.00 1 10/10/22 13:42 ANG V24950 1,2-Dibromoethane <0.200 Ng/L 0.200 0.500 1 10/10/22 13:42 ANG V24950 Dibromomethane <0.230 ug/L 0.230 0.500 1 10/10/22 13:42 ANG V24950 trans-1,4-Dichloro-2-butene <1.30 Ng/L 1.30 10.0 1 10/10/22 13:42 ANG V24950 1,2-Dichlorobenzene <0.220 ug/L 0.220 0.500 1 10/10/22 13:42 ANG V24950 1,3-Dichlorobenzene <0.190 Ng/L 0.190 0.500 1 10/10/22 13:42 ANG V24950 1,4-Dichlorobenzene <0.210 ug/L 0.210 0.500 1 10/10/22 13:42 ANG V24950 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 68 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89909 Matrix: Aqueous Sample ID : TB-20221003-2 Sampled: 10/3/2022 0:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Dichlorodifluoromethane <1.20 Ng/L 1.20 5.00 1 10/10/22 13:42 ANG V24950 1,1-Dichloroethane <0.240 ug/L 0.240 0.500 1 10/10/22 13:42 ANG V24950 1,2-Dichloroethane <0.150 Ng/L 0.150 0.500 1 10/10/22 13:42 ANG V24950 1,1-Dichloroethene <0.150 ug/L 0.150 0.500 1 10/10/22 13:42 ANG V24950 cis- 1,2-Dich loroethene <0.200 Ng/L 0.200 0.500 1 10/10/22 13:42 ANG V24950 trans- 1.2-Dichloroethene <0.180 ug/L 0.180 0.500 1 10/10/22 13:42 ANG V24950 1,2-Dichloropropane <0.190 Ng/L 0.190 0.500 1 10/10/22 13:42 ANG V24950 1,3-Dichloropropane <0.130 ug/L 0.130 0.500 1 10/10/22 13:42 ANG V24950 2,2-Dichloropropane <0.210 Ng/L 0.210 2.00 1 10/10/22 13:42 ANG V24950 1,1-Dichloropropene <0.200 ug/L 0.200 0.500 1 10/10/22 13:42 ANG V24950 cis- 1,3-Dich loropropene <0.210 Ng/L 0.210 0.500 1 10/10/22 13:42 ANG V24950 trans-1,3-Dichloropropene <0.150 ug/L 0.150 0.500 1 10/10/22 13:42 ANG V24950 Ethylbenzene <0.170 Ng/L 0.170 0.500 1 10/10/22 13:42 ANG V24950 Hexachlorobutadiene <0.350 ug/L 0.350 2.00 1 10/10/22 13:42 ANG V24950 2-Hexanone <0.380 Ng/L 0.380 5.00 1 10/10/22 13:42 ANG V24950 Iodomethane <0.054 ug/L 0.054 0.500 1 10/10/22 13:42 ANG V24950 Methyl Ethyl Ketone (MEK) <0.710 Ng/L 0.710 5.00 1 10/10/22 13:42 ANG V24950 4-Methyl-2-Pentanone <1.00 ug/L 1.00 5.00 1 10/10/22 13:42 ANG V24950 Methylene Chloride 0.4113 Ng/L 0.330 1.00 1 10/10/22 13:42 ANG V24950 Naphthalene <0.470 ug/L 0.470 1.00 1 10/10/22 13:42 ANG V24950 Styrene <0.220 Ng/L 0.220 0.500 1 10/10/22 13:42 ANG V24950 1,1,1,2-Tetrachloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 13:42 ANG V24950 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 69 of 123 Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01015 Project ID Anchor QEA of North Carolina, PLLC Project Jackson County Chuck Pippin Report Date : 11/09/2022 231 Haywood Street Information : C21480-01.01, WA-1 Received : 10/04/2022 Asheville , NC 28801 Report Number : 22-277-0040 REPOR T OF A NA L YSIS Lab No : 89909 Matrix: Aqueous Sample ID : TB-20221003-2 Sampled: 10/3/2022 0:00 Analytical Method: 8260D Prep Batch(es): V24949 10/10/22 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 1,1,2,2-Tetrachloroethane <0.160 Ng/L 0.160 0.500 1 10/10/22 13:42 ANG V24950 Tetrachloroethene <0.220 ug/L 0.220 0.500 1 10/10/22 13:42 ANG V24950 Tetrahydrofuran <1.50 Ng/L 1.50 10.0 1 10/10/22 13:42 ANG V24950 Toluene <0.220 ug/L 0.220 0.500 1 10/10/22 13:42 ANG V24950 1,2,4-Trichlorobenzene <0.310 Ng/L 0.310 1.00 1 10/10/22 13:42 ANG V24950 1,1,1-Trichloroethane <0.160 ug/L 0.160 0.500 1 10/10/22 13:42 ANG V24950 1,1,2-Trichloroethane <0.096 Ng/L 0.096 0.500 1 10/10/22 13:42 ANG V24950 Trichloroethene <0.180 ug/L 0.180 0.500 1 10/10/22 13:42 ANG V24950 Trichlorofluoromethane <0.180 Ng/L 0.180 0.500 1 10/10/22 13:42 ANG V24950 1,2,3-Trichloropropane <0.270 ug/L 0.270 1.00 1 10/10/22 13:42 ANG V24950 Vinyl Acetate <1.00 Ng/L 1.00 2.00 1 10/10/22 13:42 ANG V24950 Vinyl Chloride <0.170 ug/L 0.170 0.500 1 10/10/22 13:42 ANG V24950 o-Xylene <0.210 Ng/L 0.210 0.500 1 10/10/22 13:42 ANG V24950 m,p-Xylene <0.420 ug/L 0.420 1.00 1 10/10/22 13:42 ANG V24950 Xylene (Total) <0.21 Ng/L 0.210 0.500 1 10/10/22 13:42 V24950 Surrogate:4-Bromofluorobenzene 98.4 Limits:80-124% 1 10/10/22 13:42 ANG V24950 Surrogate: Dibromofluoromethane 94.4 Limits: 75-129% 1 10/10/22 13:42 ANG V24950 Surrogate: 1,2-Dichloroethane - d4 93.4 Limits: 63-136% 1 10/10/22 13:42 ANG V24950 Surrogate: Toluene-d8 96.6 Limits: 77-123% 1 10/10/22 13:42 ANG V24950 Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions DF Dilution Factor H Beyond holding time J Estimated value M Minimum value MQL Method Quantitation Limit Page 70 of 123 lacioAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 October 10, 2022 Danyale Love Waypoint Analytical, LLC 449 Springbrook Rd Charlotte, NC 28217 RE: Project: 22-277-0040 Pace Project No.: 92629688 Dear Danyale Love: Enclosed are the analytical results for sample(s) received by the laboratory on October 06, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Angela Overcash, Waypoint Analytical V AtQ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, B ; without the written consent of Pace Analytical Services, LLC. Page 71 of 123 Page 1 of 12 a� _ ;a'ceAnalyfica( ff www.pacelabs.com I Project: 22-277-0040 Pace Project No.: 92629688 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 72 of 123 Page 2 of 12 lacioAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: 22-277-0040 Pace Project No.: 92629688 Lab ID Sample ID Matrix Date Collected Date Received 92629688001 DW-01-20221003 Drinking Water 10/03/22 17:45 10/06/22 09:34 92629688002 DW-02-20221003 Drinking Water 10/03/22 17:05 10/06/22 09:34 92629688003 TB-20221003-1 Drinking Water 10/03/22 00:00 10/06/22 09:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 Page 73 of 123 lacioAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: 22-277-0040 Pace Project No.: 92629688 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92629688001 DW-01-20221003 EPA 524.2 LMB 11 PASI-C 92629688002 DW-02-20221003 EPA 524.2 LMB 11 PASI-C 92629688003 TB-20221003-1 EPA 524.2 LMB 11 PASI-C PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 12 Page 74 of 123 lacioAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 22-277-0040 Pace Project No.: 92629688 Sample: DW-01-20221003 Lab ID: 92629688001 Collected: 10/03/22 17:45 Received: 10/06/22 09:34 Matrix: Drinking Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 524.2 MSV SC List Benzene 1,2-Dichloroethane Ethylbenzene Methyl -tert-butyl ether Naphthalene Toluene Xylene (Total) m&p-Xylene o-Xylene Surrogates 1,2-Dichlorobenzene-d4(S) 4-Bromofluorobenzene (S) Analytical Method: EPA 524.2 Pace Analytical Services - Charlotte ND mg/L 0.00050 0.00021 1 10/07/2212:51 71-43-2 ND mg/L 0.00050 0.00016 1 10/07/2212:51 107-06-2 ND mg/L 0.00050 0.00022 1 10/07/2212:51 100-41-4 ND mg/L 0.00050 0.00014 1 10/07/2212:51 1634-04-4 ND mg/L 0.00050 0.00035 1 10/07/2212:51 91-20-3 ND mg/L 0.00050 0.00020 1 10/07/2212:51 108-88-3 ND mg/L 0.00050 0.00022 1 10/07/2212:51 1330-20-7 ND mg/L 0.0010 0.00039 1 10/07/2212:51 179601-23-1 ND mg/L 0.00050 0.00022 1 10/07/2212:51 95-47-6 88 % 70-130 1 10/07/2212:51 2199-69-1 77 % 70-130 1 10/07/2212:51 460-00-4 Sample: DW-02-20221003 Lab ID: 92629688002 Collected: 10/03/22 17:05 Received: 10/06/22 09:34 Matrix: Drinking Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 524.2 MSV SC List Benzene 1,2-Dichloroethane Ethylbenzene Methyl -tert-butyl ether Naphthalene Toluene Xylene (Total) m&p-Xylene o-Xylene Surrogates 1,2-Dichlorobenzene-d4(S) 4-Bromofluorobenzene (S) Analytical Method: EPA 524.2 Pace Analytical Services - Charlotte ND mg/L 0.00050 0.00021 1 10/07/2212:24 71-43-2 ND mg/L 0.00050 0.00016 1 10/07/2212:24 107-06-2 ND mg/L 0.00050 0.00022 1 10/07/2212:24 100-41-4 ND mg/L 0.00050 0.00014 1 10/07/2212:24 1634-04-4 ND mg/L 0.00050 0.00035 1 10/07/2212:24 91-20-3 ND mg/L 0.00050 0.00020 1 10/07/2212:24 108-88-3 ND mg/L 0.00050 0.00022 1 10/07/2212:24 1330-20-7 ND mg/L 0.0010 0.00039 1 10/07/2212:24 179601-23-1 ND mg/L 0.00050 0.00022 1 10/07/2212:24 95-47-6 89 % 70-130 1 10/07/2212:24 2199-69-1 79 % 70-130 1 10/07/2212:24 460-00-4 Sample: TB-20221003-1 Lab ID: 92629688003 Collected: 10/03/22 00:00 Received: 10/06/22 09:34 Matrix: Drinking Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 524.2 MSV SC List Analytical Method: EPA 524.2 Pace Analytical Services - Charlotte Benzene ND mg/L 0.00050 0.00021 1 1,2-Dichloroethane ND mg/L 0.00050 0.00016 1 Ethylbenzene ND mg/L 0.00050 0.00022 1 Methyl -tert-butyl ether ND mg/L 0.00050 0.00014 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/10/2022 03:24 PM without the written consent of Pace Analytical Services, LLC. 10/07/22 11:32 71-43-2 10/07/22 11:32 107-06-2 10/07/22 11:32 100-41-4 10/07/22 11:32 1634-04-4 Page 5 of 12 Page 75 of 123 lacioAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 22-277-0040 Pace Project No.: 92629688 Sample: TB-20221003-1 Lab ID: 92629688003 Collected: 10/03/22 00:00 Received: 10/06/22 09:34 Matrix: Drinking Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 524.2 MSV SC List Analytical Method: EPA 524.2 Pace Analytical Services - Charlotte Naphthalene ND mg/L 0.00050 0.00035 1 10/07/22 11:32 91-20-3 Toluene ND mg/L 0.00050 0.00020 1 10/07/22 11:32 108-88-3 Xylene (Total) ND mg/L 0.00050 0.00022 1 10/07/22 11:32 1330-20-7 m&p-Xylene ND mg/L 0.0010 0.00039 1 10/07/22 11:32 179601-23-1 o-Xylene ND mg/L 0.00050 0.00022 1 10/07/22 11:32 95-47-6 Surrogates 1,2-Dichlorobenzene-d4 (S) 83 % 70-130 1 10/07/22 11:32 2199-69-1 4-Bromofluorobenzene (S) 73 % 70-130 1 10/07/22 11:32 460-00-4 Date: 10/10/2022 03:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 12 Page 76 of 123 lacioAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 22-277-0040 Pace Project No.: 92629688 QC Batch: 728567 Analysis Method: EPA 524.2 QC Batch Method: EPA 524.2 Analysis Description: 524.2 MSV Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92629688001, 92629688002, 92629688003 METHOD BLANK: 3794369 Matrix: Associated Lab Samples: 92629688001, 92629688002, 92629688003 Blank Parameter Units Result Water Reporting Limit 1,2-Dichloroethane mg/L ND 0.00050 Benzene mg/L ND 0.00050 Ethylbenzene mg/L ND 0.00050 m&p-Xylene mg/L ND 0.0010 Methyl -tert-butyl ether mg/L ND 0.00050 Naphthalene mg/L ND 0.00050 o-Xylene mg/L ND 0.00050 Toluene mg/L ND 0.00050 Xylene (Total) mg/L ND 0.00050 1,2-Dichlorobenzene-d4 (S) % 89 70-130 4-Bromofluorobenzene (S) % 79 70-130 MDL Analyzed LABORATORY CONTROL SAMPLE: Parameter 3794370 Units Spike Conc. LCS LCS Result % Rec 1,2-Dichloroethane mg/L 0.02 0.020 Benzene mg/L 0.02 0.019 Ethylbenzene mg/L 0.02 0.017 m&p-Xylene mg/L 0.04 0.035 Methyl -tert-butyl ether mg/L 0.02 0.021 Naphthalene mg/L 0.02 0.019 o-Xylene mg/L 0.02 0.017 Toluene mg/L 0.02 0.020 Xylene (Total) mg/L 0.06 0.052 1,2-Dichlorobenzene-d4 (S) % 4-Bromofluorobenzene (S) % 0.00016 10/07/22 08:55 0.00021 10/07/22 08:55 0.00022 10/07/22 08:55 0.00039 10/07/22 08:55 0.00014 10/07/22 08:55 0.00035 10/07/22 08:55 0.00022 10/07/22 08:55 0.00020 10/07/22 08:55 0.00022 10/07/22 08:55 10/07/22 08:55 10/07/22 08:55 % Rec Limits 99 70-130 96 70-130 85 70-130 89 70-130 106 70-130 96 70-130 84 70-130 98 70-130 87 104 70-130 106 70-130 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/10/2022 03:24 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 Page 77 of 123 a� _ ;a'ceAnalyfica( www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: 22-277-0040 Pace Project No.: 92629688 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/10/2022 03:24 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 Page 78 of 123 lacioAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: 22-277-0040 Pace Project No.: 92629688 Lab ID Sample ID QC Batch Method QC Batch 92629688001 DW-01-20221003 EPA 524.2 728567 92629688002 DW-02-20221003 EPA 524.2 728567 92629688003 TB-20221003-1 EPA 524.2 728567 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/10/2022 03:24 PM without the written consent of Pace Analytical Services, LLC. Analytical Analytical Method Batch Page 9 of 12 Page 79 of 123 DUO —Title: ENV-FRM-HUN1-0083 v01 — Sample Condition Upon Receipt qa e Effective Date: 05/121202205/12/2022 Laboratory receiving samples: Asheville ❑ Eden ❑ Greenwood ❑ Huntersvilleo Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersvillel—I SampleUpon Client Name; WOE# . 92'6296188 Receipt L" � Project { Courier: ❑Fe Ex UP ❑t15PS Client II IIII' IIII II I II II I III ❑ Commercial ❑Pace l ❑Other: 926291588 Custody Seat Present? ❑Yes [2No Seals Intact? ❑Yes No r Date/Initials Person Examining Conte ts; , Packing Material: ❑Bubble WrapBubble Bags g ❑None ❑ Other Biological Tissu,�e, �F °zen? � L- Thermometer: ( ❑Yes ❑No �N/A ❑ IRGuniD: , n "t Type of Ice: [Vet Correction Factor: y Cooler Temp: — S -_0 Add/Subtract (°C) Cooler Temp Corrected Val,11 USDA Regulated Soil ( N/A, water sample) l Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? nYes nNo ❑Blue ❑None Temp should be above freezing to 6"C ❑Samples out o€temp criteria. Samples on ice, coaling process has begun Did samples originate from a foreign source (internationally, including Hawaii and Puerto Rico)? ❑Yes ❑No Chain of Custody Present? LYCs ❑Nn ❑N/A 1. Samples Arrived within Hold Time? 9<7 [I No ❑N/A 2, Short Hold Time Analysis (c72 hr.)? ❑Yes E4 ❑N/A 3. Rush Turn Around Time Requested? ❑Yes DK ❑N/A Q. Sufficient Volume? EJYes ❑No ❑N/A 5. Correct Containers Used? Yes ❑No ❑N/A 6, -Pace Containers Used? 2rLs [_]No ❑N/A Containers Intact? Yes ❑No EIN/A, 7. Dissolved analysis: Samples Field Filtered? ❑Yes ❑No N/A S. Sample Labels Match COC? es [:]No ❑N/A 9. -Includes Date/Time/ID/Analysis Matrix: k ZUJ Headspace in VOA Vials (>5-6mm)? ❑Yes ZfNo ❑N/A 10. Trip Blank Present? []Yes ❑EIno ❑NIA 11. Trip Blank Custody Seals Present? ❑Yes [3<0 ❑N/A COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: }'rojecL Manager 5RF Review; - Lot ID of split containers: Date/Time; Date: Date: Field Data Required? ❑Yes ❑No Qualtrax ID: 69614 Page 80 of 123 Page 1 of 2 Page 10 of 12 _Titie: ENV-FRM-HUNI.0083 v01 Sample Condition Upon Receipt .iYace L)G# Effective Date: 05/121202205/12/2022 *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Did and Grease, DRO/8015 (water) DOC, Wig "Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine Project;WN : 92629688 PM: M14B Due Date: 10/13/22 CLIENT• : 92-Pr ism Q, K E w f a m m c u to ro a J Ln er e�. no v N a c u Vf ra a a r m n. m a d m c = V " ro a J o r t a com Q Z a tr1 a o. C `-'"i, " _m C1 m 7 a N v n �t O N V d J N -7 v a m N v a m Oz x V ro a J o NN.� Z m c. m o 06 m m Q N a J a 4 a m v n a = Oro z V �' ro rL J vEi rNi CA a a m m 7 .R ^ m l7 -0C v u o y 3 a a a a 0. v .G E a 4 m e-I 7 '+ e7 a v a S w E Q a rl 2 •y i7 a z v cJ a c E ¢ J o CJ 7 m i7 a v 2 n v 0 N `y a E ¢ ° vwF4 ri e� a v 0. a O rya S A E Q J of N M �7 ¢ Z u 2 z E Q of N ta31 0o ¢ 2 U = Q O > J E 4 M l7 z m � VS N Z Q O > E 61 c7 > _ v w y CI C Q O > E T 0 > d _ Z 1 0Y 2 Q Q �! E V Q1 o Q ? a Ln O y Qy`JaJ O > E Q T o b a ? X a N ° v L7 a Z ,N 4' W 4 N E rr'i N Ln Z �, !p a- Qi VJ J E O N a N� U ri a O = Z a J E N M a. m a Z aJ m C = ¢ J E O l7 a z m C ' Vl E = +n > H ro as h Q E Q E QV D 0 a 1 - z 3 ` 1 4 I 5 6 7 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt pate preservation adjusted Time preservation adjusted Amount of Preservative added Lot N Note:Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e.� Out of hold, incorrect preservative, out of temp, incorrect containers. Quaitrax ID: 69614 Page 2 of 2 Page 11 of 12 Page 81 of 123 a 0 , m U N 3 rD o � � -! a C CD CCD 0 Ln S a' w X x�p W � l�D m m .4Z N t� N N N N N N N ` C> D 0 o o03 y ro 00 N NNj v N N N N n G ro N-- �I 0 0 0 ( n o c c o w 0 w 0 w 3 coo SD 'T a Nj a o ID o v �• V o V I Ln 4 i_n oM NJ o , 0 N 3 0 G N W Y M O M O W 3 M z 0 is X o O �a N L11 91 O A A N � � N CL W A � N N Off T 1� > U z O 0 o co co 3 m o 0 avi 3 N o o a n n v � S 0 � w rt o N N N Q' z (� to Q n 0 O N � S o �' n CL o � Na a T n rt s O n n 0 CL m ID 3 mn fl} 'O �1 f* N °: N ti+ � C y rt ,� c�A n 01 00 �, ^° GCL J n a >> 5o W N p f/1 NJ 0 p N O < N w 0 tocn cn Page 82 of 123 Page 12 of 12 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Analytical Batch: V24885 Analysis Method: 4500S2F-2011 Analysis Description: Sulfide Lab Reagent Blank LRB Matrix: AQU Associated Lab Samples: 89898, 89901, 89902, 89903, 89904 Blank MDL MQL Analyzed Parameter Units Result Sulfide mg/L <0.83 0.83 2.00 10/10/2211:00 Laboratory Control Sample LCS Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Sulfide mg/L 10.0 11.0 110 70-122 Date: 11/09/2022 10:53 AM Page 83 of 123 Page 1 of 38 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L645234 QC Analytical Batch(es): L646059,L646579 QC Prep Batch Method: 3005A Analysis Method: 6020B Analysis Description: Metals Analyses Lab Reagent Blank LRB-1-645234 Matrix: AQU Associated Lab Samples: 89904, 89905 Parameter Units Blank Result MDL MQL Analyzed Antimony pg/L <0.618 0.618 1.00 10/28/22 21:47 Arsenic pg/L <0.297 0.297 1.00 10/28/22 21:47 Barium pg/L <0.453 0.453 1.00 10/28/22 21:47 Beryllium pg/L <0.102 0.102 1.00 10/28/22 21:47 Cadmium pg/L <0.350 0.350 1.00 10/28/22 21:47 Chromium pg/L <0.346 0.346 1.00 10/28/22 21:47 Cobalt pg/L <0.060 0.060 1.00 10/28/22 21:47 Copper pg/L <0.489 0.489 1.00 10/28/22 21:47 Lead pg/L <0.264 0.264 1.00 10/28/22 21:47 Nickel pg/L <0.182 0.182 1.00 10/28/22 21:47 Selenium pg/L <0.703 0.703 1.00 10/28/22 21:47 Silver pg/L <0.0570 0.0570 1.00 10/28/22 21:47 Tin pg/L <1.44 1.44 5.00 10/28/22 21:47 Thallium pg/L <0.0610 0.0610 1.00 10/28/22 21:47 Vanadium pg/L <0.767 0.767 5.00 10/28/22 21:47 Zinc pg/L <4.67 4.67 10.0 10/28/22 21:47 Laboratory Control Sample LCS-L645234 Parameter Units Spike Conc. LCS Result LCS %Rec % Rec Limits Antimony pg/L 100 102 102 80-120 Arsenic Ng/L 50.0 48.0 96.0 80-120 Barium pg/L 100 95.7 96.0 80-120 Beryllium Ng/L 50.0 49.6 99.0 80-120 Cadmium pg/L 10.0 9.40 94.0 80-120 Chromium pg/L 100 100 100 80-120 Cobalt pg/L 100 98.6 99.0 80-120 Date: 11/09/2022 10:53 AM Page 2 of 38 Page 84 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L645234 QC Analytical Batch(es): L646059,L646579 QC Prep Batch Method: 3005A Analysis Method: 6020B Analysis Description: Metals Analyses Laboratory Control Sample LCS-L645234 Parameter Units Spike Conc. LCS Result LCS %Rec % Rec Limits Copper pg/L 50.0 50.2 100 80-120 Lead pg/L 50.0 49.1 98.0 80-120 Nickel pg/L 50.0 49.3 99.0 80-120 Selenium pg/L 100 97.5 98.0 80-120 Silver pg/L 10.0 9.46 95.0 80-120 Tin pg/L 500 480 96.0 80-120 Thallium pg/L 10.0 9.68 97.0 80-120 Vanadium pg/L 500 497 99.0 80-120 Zinc pg/L 500 506 101 80-120 Matrix Spike & Matrix Spike Duplicate Parameter Units V 90260-MS-1-645234 MS Spike Result Conc. V 90260-MSD-L645234 MSD MS Result MSD Spike Result Conc. MS %Rec MSD %Rec %Rec Limits RPD Max RPD Antimony pg/L < 0.618 100 100 101 102 101 102 75-125 0.9 20.0 Arsenic pg/L < 0.297 50.0 50.0 50.0 53.9 100 108 75-125 7.5 20.0 Barium pg/L 55.9 100 100 148 151 92.0 95.0 75-125 2.0 20.0 Beryllium pg/L < 0.102 50.0 50.0 49.0 52.0 98.0 104 75-125 5.9 20.0 Cadmium pg/L < 0.350 10.0 10.0 9.59 9.46 96.0 95.0 75-125 1.3 20.0 Chromium pg/L 0.851 100 100 101 102 100 101 75-125 0.9 20.0 Cobalt pg/L 0.882 100 100 98.5 101 98.0 100 75-125 2.5 20.0 Copper pg/L 1.13 50.0 50.0 50.3 50.5 98.0 99.0 75-125 0.3 20.0 Lead pg/L < 0.264 50.0 50.0 49.7 50.4 99.0 101 75-125 1.3 20.0 Nickel pg/L 0.943 50.0 50.0 48.4 49.6 95.0 97.0 75-125 2.4 20.0 Selenium pg/L < 0.703 100 100 93.1 96.0 93.0 96.0 75-125 3.0 20.0 Silver pg/L < 0.0570 10.0 10.0 9.28 9.46 93.0 95.0 75-125 1.9 20.0 Tin pg/L < 1.44 500 500 477 482 95.0 96.0 75-125 1.0 20.0 Date: 11/09/2022 10:53 AM Page 3 of 38 Page 85 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L645234 QC Analytical Batch(es): L646059,L646579 QC Prep Batch Method: 3005A Analysis Method: 6020B Analysis Description: Metals Analyses Matrix Spike & Matrix Spike Duplicate V 90260-MS-1-645234 V 90260-MSD-L645234 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD Conc. Thallium pg/L 0.0638 10.0 10.0 9.83 10.0 98.0 99.0 75-125 1.7 20.0 Vanadium pg/L < 0.767 500 500 505 518 101 104 75-125 2.5 20.0 Zinc pg/L 14.0 500 500 512 520 100 101 75-125 1.5 20.0 Post Digestion Spike V 90260-PDS-L645234 PDS % Analyzed Parameter Units Result Recovery Antimony pg/L 50.6 101 10/28/22 23:55 Arsenic pg/L 49.5 198* 11/01/2218:03 Barium pg/L 77.3 99.0 10/28/22 23:55 Beryllium pg/L 25.5 102 10/28/22 23:55 Cadmium pg/L 4.91 98.0 10/28/22 23:55 Chromium pg/L 50.4 100 10/28/22 23:55 Cobalt pg/L 50.5 100 10/28/22 23:55 Copper pg/L 26.3 103 10/28/22 23:55 Lead pg/L 25.7 103 10/28/22 23:55 Nickel pg/L 24.9 98.0 10/28/22 23:55 Selenium pg/L 50.7 101 10/28/22 23:55 Silver pg/L 5.01 100 10/28/22 23:55 Tin pg/L 251 100 10/28/22 23:55 Thallium pg/L 5.19 103 10/28/22 23:55 Vanadium pg/L 252 101 10/28/22 23:55 Zinc pg/L 262 102 10/28/22 23:55 * QC Fail Date: 11/09/2022 10:53 AM Page 4 of 38 Page 86 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L645354 QC Analytical Batch(es): L646083 QC Prep Batch Method: 3005A Analysis Method: 6020B Analysis Description: Metals Analyses Lab Reagent Blank LRB-1-645354 Matrix: AQU Associated Lab Samples: 89898, 89901, 89905 Blank MDL MQL Analyzed Parameter Units Result Dissolved Antimony pg/L <0.618 0.618 1.00 10/29/22 13:55 Dissolved Arsenic pg/L <0.297 0.297 1.00 10/29/22 13:55 Dissolved Barium pg/L <0.453 0.453 1.00 10/29/22 13:55 Dissolved Beryllium pg/L <0.102 0.102 1.00 10/29/22 13:55 Dissolved Cadmium pg/L <0.350 0.350 1.00 10/29/22 13:55 Dissolved Chromium pg/L <0.346 0.346 1.00 10/29/22 13:55 Dissolved Cobalt pg/L <0.060 0.060 1.00 10/29/22 13:55 Dissolved Copper pg/L <0.489 0.489 1.00 10/29/22 13:55 Dissolved Lead pg/L <0.264 0.264 1.00 10/29/22 13:55 Dissolved Nickel pg/L <0.182 0.182 1.00 10/29/22 13:55 Dissolved Selenium pg/L <0.703 0.703 1.00 10/29/22 13:55 Dissolved Silver pg/L <0.0570 0.0570 1.00 10/29/22 13:55 Dissolved Tin pg/L <1.44 1.44 5.00 10/29/22 13:55 Dissolved Thallium pg/L <0.0610 0.0610 1.00 10/29/22 13:55 Dissolved Vanadium pg/L <0.767 0.767 5.00 10/29/22 13:55 Dissolved Zinc pg/L 5.66 4.67 10.0 10/29/22 13:55 Laboratory Control Sample & LCSD LCS-L645354 LCSD-L645354 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Dissolved Antimony pg/L 100 100 99.1 100 99.0 80-120 0.9 20.0 Dissolved Arsenic pg/L 50.0 48.1 48.3 96.0 97.0 80-120 0.4 20.0 Dissolved Barium pg/L 100 94.7 93.8 95.0 94.0 80-120 0.9 20.0 Dissolved Beryllium pg/L 50.0 48.7 48.6 97.0 97.0 80-120 0.2 20.0 Dissolved Cadmium pg/L 10.0 9.72 9.55 97.0 96.0 80-120 1.7 20.0 Dissolved Chromium pg/L 100 98.2 97.5 98.0 98.0 80-120 0.7 20.0 Date: 11/09/2022 10:53 AM Page 5 of 38 Page 87 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L645354 QC Analytical Batch(es): L646083 QC Prep Batch Method: 3005A Analysis Method: 6020B Analysis Description: Metals Analyses Laboratory Control Sample & LCSD LCS-L645354 LCSD-L645354 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Dissolved Cobalt pg/L 100 97.2 97.0 97.0 97.0 80-120 0.2 20.0 Dissolved Copper pg/L 50.0 47.9 47.3 96.0 95.0 80-120 1.2 20.0 Dissolved Lead pg/L 50.0 48.9 48.2 98.0 96.0 80-120 1.4 20.0 Dissolved Nickel pg/L 50.0 48.0 48.7 96.0 97.0 80-120 1.4 20.0 Dissolved Selenium pg/L 100 89.4 93.2 89.0 93.0 80-120 4.1 20.0 Dissolved Silver pg/L 10.0 9.33 9.07 93.0 91.0 80-120 2.8 20.0 Dissolved Tin pg/L 500 485 477 97.0 95.0 80-120 1.6 20.0 Dissolved Thallium pg/L 10.0 9.80 9.76 98.0 98.0 80-120 0.4 20.0 Dissolved Vanadium pg/L 500 489 495 98.0 99.0 80-120 1.2 20.0 Dissolved Zinc pg/L 500 495 492 99.0 98.0 80-120 0.6 20.0 Date: 11/09/2022 10:53 AM Page 6 of 38 Page 88 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24878 QC Prep Batch Method: 3005A QC Analytical Batch(es): V24932,V25023 Analysis Method: 6020B Analysis Description: Metals Analyses Lab Reagent Blank LRB-V24878 Matrix: AQU Associated Lab Samples: 89898, 89901, 89902, 89903, 89905 Blank MDL MQL Analyzed Parameter Units Result Antimony pg/L <0.680 0.680 2.00 10/10/22 18:31 Arsenic pg/L <0.490 0.490 1.00 10/10/22 18:31 Barium pg/L <3.40 3.40 10.0 10/10/22 18:31 Beryllium pg/L <0.240 0.240 1.00 10/10/22 18:31 Cadmium pg/L <0.150 0.150 1.00 10/10/22 18:31 Chromium pg/L <1.00 1.00 2.00 10/10/22 18:31 Cobalt pg/L <0.080 0.080 1.00 10/10/22 18:31 Copper pg/L <0.890 0.890 2.00 10/11/22 15:48 Lead pg/L <0.500 0.500 1.00 10/10/22 18:31 Nickel pg/L <0.720 0.720 2.00 10/10/22 18:31 Selenium pg/L <2.30 2.30 5.00 10/10/22 18:31 Silver pg/L <0.130 0.130 1.00 10/10/22 18:31 Tin pg/L <1.50 1.50 5.00 10/10/22 18:31 Thallium pg/L <0.280 0.280 2.00 10/10/22 18:31 Vanadium pg/L <2.10 2.10 5.00 10/10/22 18:31 Zinc pg/L <3.90 3.90 20.0 10/10/22 18:31 Laboratory Control Sample LCS-V24878 Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Antimony pg/L 100 99.7 100 80-120 Arsenic pg/L 100 93.7 94.0 80-120 Barium pg/L 100 96.5 97.0 80-120 Beryllium pg/L 100 94.1 94.0 80-120 Cadmium pg/L 100 94.0 94.0 80-120 Chromium pg/L 100 97.0 97.0 80-120 Cobalt pg/L 100 99.4 99.0 80-120 Date: 11/09/2022 10:53 AM Page 7 of 38 Page 89 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24878 QC Analytical Batch(es): V24932,V25023 QC Prep Batch Method: 3005A Analysis Method: 6020B Analysis Description: Metals Analyses Laboratory Control Sample LCS-V24878 Parameter Units Spike Conc. LCS Result LCS %Rec % Rec Limits Copper pg/L 100 98.0 98.0 80-120 Lead pg/L 100 99.6 100 80-120 Nickel pg/L 100 96.4 96.0 80-120 Selenium pg/L 100 97.6 98.0 80-120 Silver pg/L 100 98.7 99.0 80-120 Tin pg/L 100 99.2 99.0 80-120 Thallium pg/L 100 98.8 99.0 80-120 Vanadium pg/L 100 98.2 98.0 80-120 Zinc pg/L 100 98.2 98.0 80-120 Matrix Spike & Matrix Spike Duplicate Parameter Units V 89898-MS-V24878 MS Spike Result Conc. V 89898-MSD-V24878 MSD MS Result Spike Conc. MSD Result MS %Rec MSD %Rec %Rec Limits RPD Max RPD Antimony pg/L < 3.40 100 100 75.4 75.6 75.0 76.0 75-125 0.2 20.0 Arsenic pg/L 10.1 100 100 102 102 92.0 92.0 75-125 0.0 20.0 Barium pg/L 224 100 100 315 313 91.0 89.0 75-125 0.6 20.0 Beryllium pg/L < 1.20 100 100 92.9 95.0 93.0 95.0 75-125 2.2 20.0 Cadmium pg/L < 0.750 100 100 93.2 93.2 93.0 93.0 75-125 0.0 20.0 Chromium pg/L 42.2 100 100 140 141 98.0 99.0 75-125 0.7 20.0 Cobalt pg/L 40.7 100 100 141 142 100 101 75-125 0.7 20.0 Lead pg/L 9.82 100 100 110 111 100 101 75-125 0.9 20.0 Nickel pg/L 32.0 100 100 128 129 96.0 97.0 75-125 0.7 20.0 Selenium pg/L 36.2 100 100 131 124 95.0 88.0 75-125 5.4 20.0 Silver pg/L < 0.650 100 100 100 100 100 100 75-125 0.0 20.0 Tin pg/L < 7.50 100 100 98.4 101 98.0 101 75-125 2.6 20.0 Thallium pg/L < 1.40 100 100 101 102 101 102 75-125 0.9 20.0 Date: 11/09/2022 10:53 AM Page 8 of 38 Page 90 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24878 QC Analytical Batch(es): V24932,V25023 QC Prep Batch Method: 3005A Analysis Method: 6020B Analysis Description: Metals Analyses Matrix Spike & Matrix Spike Duplicate V 89898-MS-V24878 V 89898-MSD-V24878 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD Conc. Vanadium ug/L 52.3 100 100 150 152 98.0 100 75-125 1.3 20.0 Zinc ug/L 103 100 100 200 210 97.0 107 75-125 4.8 20.0 Post Digestion Spike V 89898-PDS-V24878 PDS % Analyzed Parameter Units Result Recovery Antimony ug/L 242 97.0 10/10/22 20:32 Arsenic ug/L 251 99.0 10/10/22 20:32 Barium ug/L 353 98.0 10/10/22 20:32 Beryllium ug/L 235 94.0 10/10/22 20:32 Cadmium ug/L 239 96.0 10/10/22 20:32 Chromium ug/L 267 98.0 10/10/22 20:32 Cobalt ug/L 272 101 10/10/22 20:32 Lead ug/L 256 101 10/10/22 20:32 Nickel ug/L 260 98.0 10/10/22 20:32 Selenium ug/L 266 99.0 10/10/22 20:32 Silver ug/L 251 100 10/10/22 20:32 Tin ug/L 250 100 10/10/22 20:32 Thallium ug/L 261 105 10/10/22 20:32 Vanadium ug/L 273 99.0 10/10/22 20:32 Zinc ug/L 293 97.0 10/10/22 20:32 Date: 11/09/2022 10:53 AM Page 9 of 38 Page 91 of 123 • Waypoint, 449 Springbrook Rd, Ch Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypoi ntana lytica l.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24941 QC Analytical Batch(es): V24994 QC Prep Batch Method: 7470A Analysis Method: 7470A Analysis Description: Total Aqueous Mercury Analysis - CVAA Lab Reagent Blank LRB-V24941 Matrix: AQU Associated Lab Samples: 89898, 89901, 89902, 89903, 89904, 89905 Blank MDL MQL Analyzed Parameter Units Result Mercury (Total) pg/L <0.0700 0.0700 0.200 10/11/22 15:15 Laboratory Control Sample LCS-V24941 Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Mercury (Total) pg/L 9.38 9.61 103 80-120 Matrix Spike & Matrix Spike Duplicate V 89834-MS-V24941 V 89834-MSD-V24941 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD Conc. Mercury (Total) pg/L <0.0700 9.38 9.38 8.39 8.74 89.0 93.0 80-120 4.0 20 Post Digestion Spike V 89834-PDS-V24941 PDS % Analyzed Parameter Units Result Recovery Mercury (Total) pg/L 4.53 97.0 10/11/22 15:39 Date: 11/09/2022 10:53 AM Page 10 of 38 Page 92 of 123 • Waypoint, 449 Springbrook Rd, Ch Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypoi ntana lytica l.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V25422 QC Analytical Batch(es): V25487 QC Prep Batch Method: 7470A Analysis Method: 7470A Analysis Description: Total Aqueous Mercury Analysis - CVAA Lab Reagent Blank LRB-V25422 Matrix: AQU Associated Lab Samples: 89898, 89901, 89905 Blank MDL MQL Analyzed Parameter Units Result Dissolved Mercury pg/L 0.000 0.000 0.200 10/24/22 15:17 Laboratory Control Sample LCS-V25422 Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits Dissolved Mercury pg/L 9.38 9.50 101 80-120 Matrix Spike & Matrix Spike Duplicate V 90496-V25365-MS-V25422 V 90496-V25365-MSD-V25422 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD Conc. Dissolved Mercury pg/L <0.0700 9.38 9.38 9.17 9.13 98.0 97.0 80-120 0.4 20 Post Digestion Spike V 90496-V25365-PDS-V25422 PDS % Analyzed Parameter Units Result Recovery Dissolved Mercury pg/L 4.55 97.0 10/24/22 15:53 Date: 11/09/2022 10:53 AM Page 11 of 38 Page 93 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L644115 QC Analytical Batch(es): L644344 QC Prep Batch Method: 3510C Analysis Method: 8081B Analysis Description: Organochlorine Pesticides by GC Lab Reagent Blank LRB-L644115 Matrix: AQU Associated Lab Samples: 89898, 89901, 89902, 89903, 89904 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Aldrin alpha-BHC beta-BHC delta-BHC Chlordane alpha -Chlordane gamma -Chlordane 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Endrin Ketone gamma-BHC Heptachlor Heptachlor Epoxide M ethoxychlor Toxaphene Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) pg/L <0.0021 pg/L <0.0021 pg/L <0.0020 pg/L <0.0015 pg/L <0.0221 pg/L <0.0021 pg/L <0.0014 pg/L <0.0021 pg/L <0.0021 pg/L <0.0035 pg/L <0.0015 pg/L <0.0015 pg/L <0.0028 pg/L <0.0015 pg/L <0.0015 pg/L <0.0015 pg/L <0.0015 pg/L 0.0378 pg/L <0.0014 pg/L <0.0014 pg/L <0.0014 pg/L <0.0201 0.0021 0.0021 0.0020 0.0015 0.0221 0.0021 0.0014 0.0021 0.0021 0.0035 0.0015 0.0015 0.0028 0.0015 0.0015 0.0015 0.0015 0.0018 0.0014 0.0014 0.0014 0.0201 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.200 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.0400 10/20/22 02:10 0.300 10/20/22 02:10 10/20/22 02:10 10/20/22 02:10 83.6 46.5 36-116 25-123 Date: 11/09/2022 10:53 AM Page 94 of 123 Page 12 of 38 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L644115 QC Analytical Batch(es): L644344 QC Prep Batch Method: 3510C Analysis Method: 8081B Analysis Description: Organochlorine Pesticides by GC Laboratory Control Sample & LCSD LCS-L644115 LCSD-L644115 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Aldrin pg/L 2.00 1.42 1.50 71.0 75.0 34-105 5.4 20.0 alpha-BHC pg/L 2.00 1.45 1.55 72.5 77.5 41-102 6.6 20.0 beta-BHC pg/L 2.00 1.55 1.62 77.5 81.0 26-151 4.4 20.0 delta-BHC pg/L 2.00 1.36 1.45 68.0 72.5 40-110 6.4 20.0 alpha -Chlordane pg/L 2.00 1.49 1.64 74.5 82.0 48-117 9.5 20.0 gamma -Chlordane pg/L 2.00 1.73 1.84 86.5 92.0 51-108 6.1 20.0 4,4'-DDD pg/L 2.00 1.69 1.86 84.5 93.0 30-110 9.5 20.0 4,4'-DDE pg/L 2.00 1.52 1.70 76.0 85.0 41-111 11.1 20.0 4,4'-DDT pg/L 2.00 1.52 1.76 76.0 88.0 39-123 14.6 20.0 Dieldrin pg/L 2.00 1.69 1.82 84.5 91.0 42-111 7.4 20.0 Endosulfan I pg/L 2.00 1.50 1.62 75.0 81.0 41-111 7.6 20.0 Endosulfan II pg/L 2.00 1.54 1.71 77.0 85.5 30-110 10.4 20.0 Endosulfan Sulfate pg/L 2.00 1.61 1.73 80.5 86.5 46-111 7.1 20.0 Endrin pg/L 2.00 1.59 1.75 79.5 87.5 45-117 9.5 20.0 Endrin Aldehyde pg/L 2.00 1.53 1.68 76.5 84.0 48-125 9.3 20.0 Endrin Ketone pg/L 2.00 1.61 1.75 80.5 87.5 51-112 8.3 20.0 gamma-BHC pg/L 2.00 1.62 1.76 81.0 88.0 41-102 8.2 20.0 Heptachlor pg/L 2.00 1.54 1.70 77.0 85.0 40-110 9.8 20.0 Heptachlor Epoxide pg/L 2.00 1.48 1.60 74.0 80.0 42-115 7.7 20.0 Methoxychlor pg/L 2.00 1.57 1.67 78.5 83.5 39-140 6.1 20.0 Decachlorobiphenyl (S) 56.0 102 36-116 Tetrachloro-m-xylene (S) 69.5 70.1 25-123 Date: 11/09/2022 10:53 AM Page 13 of 38 Page 95 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642283 QC Analytical Batch(es): L643610 QC Prep Batch Method: 8151A Analysis Method: 8151A Analysis Description: Phenoxy Acid Herbicides - GC/ECD Lab Reagent Blank LRB-L642283 Matrix: AQU Associated Lab Samples: 89898, 89901, 89902, 89903, 89904 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 2,4-D pg/L <0.2078 0.2078 0.2500 10/14/22 19:54 Dalapon pg/L <0.5149 0.5149 0.5500 10/14/22 19:54 2,4-DB pg/L <0.1364 0.1364 0.2500 10/14/22 19:54 Dicamba pg/L <0.05700 0.05700 0.01000 10/14/22 19:54 Dichlorprop pg/L <0.07959 0.07959 0.1000 10/14/22 19:54 Dinoseb pg/L <0.02698 0.02698 0.1000 10/14/22 19:54 MCPA pg/L <18.98 18.98 50.00 10/14/22 19:54 MCPP pg/L <11.75 11.75 50.00 10/14/22 19:54 Picloram pg/L <0.04528 0.04528 0.1000 10/14/22 19:54 2,4,5-T pg/L <0.01002 0.01002 0.03000 10/14/22 19:54 2,4,5-TP (Silvex) pg/L <0.01634 0.01634 0.1000 10/14/22 19:54 DCAA (S) 10/14/22 19:54 67.9 20-150 Laboratory Control Sample & LCSD LCS-L642283 LCSD-L642283 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD a/o Rec % Rec Limits RPD Max RPD 2,4-D pg/L 5.000 3.215 3.229 64.3 64.5 20-120 0.4 20.00 Dalapon pg/L 12.50 4.245 7.396 33.9 59.1 20-120 54.1* 20.00 2,4-DB pg/L 5.000 3.419 3.464 68.3 69.2 20-120 1.3 20.00 Dicamba pg/L 0.5000 0.3689 0.3626 73.7 72.5 20-120 1.7 20.00 Dichlorprop pg/L 5.000 3.582 3.547 71.6 70.9 20-120 0.9 20.00 Dinoseb pg/L 2.500 1.734 1.756 69.3 70.2 20-120 1.2 20.00 MCPA pg/L 500.0 350.4 351.3 70.0 70.2 20-120 0.2 20.00 MCPP pg/L 500.0 345.3 355.6 69.0 71.1 20-120 2.9 20.00 Picloram pg/L 1.250 0.5693 0.5792 45.5 46.3 20-120 1.7 20.00 2,4,5-T pg/L 0.5000 0.3792 0.3818 75.8 76.3 20-120 0.6 20.00 * QC Fail Date: 11/09/2022 10:53 AM Page 14 of 38 Page 96 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642283 QC Analytical Batch(es): L643610 QC Prep Batch Method: 8151A Analysis Method: 8151A Analysis Description: Phenoxy Acid Herbicides - GC/ECD Laboratory Control Sample & LCSD LCS-L642283 LCSD-L642283 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD 2,4,5-TP (Silvex) pg/L 0.5000 0.3748 0.3676 74.9 73.5 20-120 1.9 20.00 DCAA (S) 65.8 67.9 20-150 Date: 11/09/2022 10:53 AM Page 15 of 38 Page 97 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24809 QC Analytical Batch(es): V24810 QC Prep Batch Method: 5030B Analysis Method: 8260D SIM Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V24809 Matrix: AQU Associated Lab Samples: 89898, 89901, 89902, 89903, 89904, 89905, 89909 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 1,4-Dioxane pg/L <0.139 0.139 2.00 10/06/2211:10 4-Bromofluorobenzene (S) 10/06/22 11:10 129 70-130 Laboratory Control Sample LCS-V24809 Spike LCS LCS %Rec % Rec Parameter Units Conc. Result Limits 1,4-Dioxane pg/L 50.0 46.0 92.0 70-130 4-Bromofluorobenzene (S) 123 70-130 Matrix Spike & Matrix Spike Duplicate V 89909-MS-V24809 V 89909-MSD-V24809 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD Conc. 1,4-Dioxane pg/L < 0.139 50.0 50.0 48.7 50.4 97.4 101 70-130 4-Bromofluorobenzene (S) 139* 135* 70-130 * QC Fail Date: 11/09/2022 10:53 AM Page 16 of 38 Page 98 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24949 QC Prep Batch Method: 5030B Lab Reagent Blank LRB-V24949 Associated Lab Samples: 89898, 89901, 89902, 89909 QC Analytical Batch(es): V24950 Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Acetone pg/L <1.80 1.80 5.00 10/10/22 13:15 Acrolein pg/L <2.00 2.00 5.00 10/10/22 13:15 Acrylonitrile pg/L <0.230 0.230 5.00 10/10/22 13:15 Benzene pg/L <0.180 0.180 0.500 10/10/22 13:15 Bromochloromethane pg/L <0.420 0.420 1.00 10/10/22 13:15 Bromodichloromethane pg/L <0.160 0.160 0.500 10/10/22 13:15 Bromoform pg/L <1.50 1.50 5.00 10/10/22 13:15 Bromomethane pg/L <0.280 0.280 1.00 10/10/22 13:15 Carbon Disulfide pg/L <0.150 0.150 5.00 10/10/22 13:15 Carbon Tetrachloride pg/L <0.180 0.180 0.500 10/10/22 13:15 Chlorobenzene pg/L <0.190 0.190 0.500 10/10/22 13:15 Chlorodibromomethane pg/L <0.190 0.190 0.500 10/10/22 13:15 Chloroethane pg/L <0.430 0.430 1.00 10/10/22 13:15 Chloroform pg/L <0.220 0.220 0.500 10/10/22 13:15 Chloromethane pg/L <0.220 0.220 0.500 10/10/22 13:15 1,2-Dibromo-3-Chloropropane pg/L <1.10 1.10 2.00 10/10/22 13:15 1,2-Dibromoethane pg/L <0.200 0.200 0.500 10/10/22 13:15 Dibromomethane pg/L <0.230 0.230 0.500 10/10/22 13:15 trans-1,4-Dichloro-2-butene pg/L < 1.30 1.30 10.0 10/10/22 13:15 1,2-Dichlorobenzene pg/L <0.220 0.220 0.500 10/10/22 13:15 1,3-Dichlorobenzene pg/L <0.190 0.190 0.500 10/10/22 13:15 1,4-Dichlorobenzene pg/L <0.210 0.210 0.500 10/10/22 13:15 Dichlorodifluoromethane pg/L <1.20 1.20 5.00 10/10/22 13:15 1,1-Dichloroethane pg/L <0.240 0.240 0.500 10/10/22 13:15 1,2-Dichloroethane pg/L <0.150 0.150 0.500 10/10/22 13:15 1,1-Dichloroethene pg/L <0.150 0.150 0.500 10/10/22 13:15 cis-1,2-Dichloroethene pg/L <0.200 0.200 0.500 10/10/22 13:15 Date: 11/09/2022 10:53 AM Page 17 of 38 Page 99 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24949 QC Prep Batch Method: 5030B Lab Reagent Blank LRB-V24949 Associated Lab Samples: 89898, 89901, 89902, 89909 QC Analytical Batch(es): V24950 Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits trans-1,2-Dichloroethene pg/L <0.180 0.180 0.500 10/10/22 13:15 1,2-Dichloropropane pg/L <0.190 0.190 0.500 10/10/22 13:15 1,3-Dichloropropane pg/L <0.130 0.130 0.500 10/10/22 13:15 2,2-Dichloropropane pg/L <0.210 0.210 2.00 10/10/22 13:15 1,1-Dichloropropene pg/L <0.200 0.200 0.500 10/10/22 13:15 cis-1,3-Dichloropropene pg/L <0.210 0.210 0.500 10/10/22 13:15 trans-1,3-Dichloropropene pg/L <0.150 0.150 0.500 10/10/22 13:15 Ethylbenzene pg/L <0.170 0.170 0.500 10/10/22 13:15 Hexachlorobutadiene pg/L <0.350 0.350 2.00 10/10/22 13:15 2-Hexanone pg/L <0.380 0.380 5.00 10/10/22 13:15 Iodomethane pg/L <0.054 0.054 0.500 10/10/22 13:15 Methyl Ethyl Ketone (MEK) pg/L <0.710 0.710 5.00 10/10/22 13:15 4-Methyl-2-Pentanone pg/L <1.00 1.00 5.00 10/10/22 13:15 Methylene Chloride pg/L <0.330 0.330 1.00 10/10/22 13:15 Naphthalene pg/L <0.470 0.470 1.00 10/10/22 13:15 Styrene pg/L <0.220 0.220 0.500 10/10/22 13:15 1,1,1,2-Tetrachloroethane pg/L <0.160 0.160 0.500 10/10/22 13:15 1,1,2,2-Tetrachloroethane pg/L <0.160 0.160 0.500 10/10/22 13:15 Tetrachloroethene pg/L <0.220 0.220 0.500 10/10/22 13:15 Tetrahydrofuran pg/L <1.50 1.50 10.0 10/10/22 13:15 Toluene pg/L <0.220 0.220 0.500 10/10/22 13:15 1,2,4-Trichlorobenzene pg/L <0.310 0.310 1.00 10/10/22 13:15 1,1,1-Trichloroethane pg/L <0.160 0.160 0.500 10/10/22 13:15 1,1,2-Trichloroethane pg/L <0.096 0.096 0.500 10/10/22 13:15 Trichloroethene pg/L <0.180 0.180 0.500 10/10/22 13:15 Trichlorofluoromethane pg/L <0.180 0.180 0.500 10/10/22 13:15 1,2,3-Trichloropropane pg/L <0.270 0.270 1.00 10/10/22 13:15 Date: 11/09/2022 10:53 AM Page 18 of 38 Page 100 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24949 QC Analytical Batch(es): V24950 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V24949 Matrix: AQU Associated Lab Samples: 89898, 89901, 89902, 89909 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Vinyl Acetate pg/L <1.00 1.00 2.00 10/10/22 13:15 Vinyl Chloride pg/L <0.170 0.170 0.500 10/10/22 13:15 o-Xylene pg/L <0.210 0.210 0.500 10/10/22 13:15 m,p-Xylene pg/L <0.420 0.420 1.00 10/10/22 13:15 4-Bromofluorobenzene (S) 10/10/22 13:15 99.0 80-124 Dibromofluoromethane (S) 10/10/22 13:15 95.0 75-129 1,2-Dichloroethane - d4 (S) 10/10/22 13:15 92.8 63-136 Toluene-d8 (S) 10/10/22 13:15 96.0 77-123 Laboratory Control Sample & LCSD LCS-V24949 LCSD-V24949 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD a/o Rec % Rec Limits RPD Max RPD Acetone pg/L 40.0 40.4 40.7 101 102 40-166 0.7 20.0 Acrolein pg/L 40.0 45.9 46.7 115 117 70-130 1.7 20.0 Acrylonitrile pg/L 40.0 46.0 47.1 115 118 81-127 2.3 20.0 Benzene pg/L 20.0 20.8 20.3 104 102 77-128 2.4 20.0 Bromochloromethane pg/L 20.0 21.3 20.7 107 104 78-135 2.8 20.0 Bromodichloromethane pg/L 20.0 19.5 19.8 97.5 99.0 76-138 1.5 20.0 Bromoform pg/L 20.0 19.5 19.9 97.5 99.5 71-135 2.0 20.0 Bromomethane pg/L 20.0 17.0 16.4 85.0 82.0 41-168 3.5 20.0 Carbon Disulfide pg/L 20.0 21.7 20.9 109 105 59-135 3.7 20.0 Carbon Tetrachloride pg/L 20.0 23.3 19.1 117 95.5 72-142 19.8 20.0 Chlorobenzene pg/L 20.0 20.3 20.2 102 101 78-119 0.4 20.0 Chlorodibromomethane pg/L 20.0 20.5 20.7 103 104 75-134 0.9 20.0 Chloroethane pg/L 20.0 17.0 16.4 85.0 82.0 57-142 3.5 20.0 Chloroform pg/L 20.0 21.2 20.2 106 101 77-130 4.8 20.0 Date: 11/09/2022 10:53 AM Page 19 of 38 Page 101 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24949 QC Analytical Batch(es): V24950 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-V24949 LCSD-V24949 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Chloromethane pg/L 20.0 15.6 15.1 78.0 75.5 47-145 3.2 20.0 1,2-Dibromo-3-Chloropropane pg/L 20.0 16.6 17.7 83.0 88.5 63-134 6.4 20.0 1,2-Dibromoethane pg/L 20.0 21.3 21.5 107 108 77-135 0.9 20.0 Dibromomethane pg/L 20.0 20.8 20.8 104 104 76-138 0.0 20.0 trans-1,4-Dichloro-2-butene pg/L 20.0 19.3 19.2 96.5 96.0 70-130 0.5 20.0 1,2-Dichlorobenzene pg/L 20.0 20.0 19.7 100 98.5 78-128 1.5 20.0 1,3-Dichlorobenzene pg/L 20.0 20.7 20.8 104 104 77-125 0.4 20.0 1,4-Dichlorobenzene pg/L 20.0 20.5 20.1 103 101 75-126 1.9 20.0 Dichlorodifluoromethane pg/L 20.0 18.1 17.1 90.5 85.5 28-163 5.6 20.0 1,1-Dichloroethane pg/L 20.0 20.7 20.8 104 104 70-130 0.4 20.0 1,2-Dichloroethane pg/L 20.0 18.8 18.5 94.0 92.5 68-131 1.6 20.0 1,1-Dichloroethene pg/L 20.0 19.6 18.8 98.0 94.0 70-154 4.1 20.0 cis-1,2-Dichloroethene pg/L 20.0 20.0 19.8 100 99.0 76-141 1.0 20.0 trans-1,2-Dichloroethene pg/L 20.0 20.6 20.0 103 100 76-135 2.9 20.0 1,2-Dichloropropane pg/L 20.0 20.8 20.1 104 101 77-130 3.4 20.0 1,3-Dichloropropane pg/L 20.0 20.1 20.9 101 105 76-132 3.9 20.0 2,2-Dichloropropane pg/L 20.0 19.2 19.4 96.0 97.0 29-149 1.0 20.0 1,1-Dichloropropene pg/L 20.0 22.3 21.5 112 108 71-136 3.6 20.0 cis-1,3-Dichloropropene pg/L 20.0 21.1 20.7 106 104 65-140 1.9 20.0 trans-1,3-Dichloropropene pg/L 20.0 21.1 20.7 106 104 67-140 1.9 20.0 Ethylbenzene pg/L 20.0 19.0 19.0 95.0 95.0 80-127 0.0 20.0 Hexachlorobutadiene pg/L 20.0 19.2 19.5 96.0 97.5 61-134 1.5 20.0 2-Hexanone pg/L 20.0 18.6 18.4 93.0 92.0 64-137 1.0 20.0 Iodomethane pg/L 20.0 14.7 14.1 73.5 70.5 70-130 4.1 20.0 Methyl Ethyl Ketone (MEK) pg/L 20.0 19.3 19.3 96.5 96.5 71-134 0.0 20.0 4-Methyl-2-Pentanone pg/L 20.0 19.4 19.9 97.0 99.5 69-134 2.5 20.0 Date: 11/09/2022 10:53 AM Page 20 of 38 Page 102 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24949 QC Analytical Batch(es): V24950 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-V24949 LCSD-V24949 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Methylene Chloride pg/L 20.0 20.1 19.4 101 97.0 73-131 3.5 20.0 Naphthalene pg/L 20.0 17.4 18.1 87.0 90.5 64-136 3.9 20.0 Styrene pg/L 20.0 20.3 19.7 102 98.5 78-129 3.0 20.0 1,1,1,2-Tetrachloroethane pg/L 20.0 19.8 19.1 99.0 95.5 79-134 3.5 20.0 1,1,2,2-Tetrachloroethane pg/L 20.0 19.2 20.1 96.0 101 62-127 4.5 20.0 Tetrachloroethene pg/L 20.0 20.4 19.8 102 99.0 80-129 2.9 20.0 Tetrahydrofuran pg/L 20.0 20.8 20.8 104 104 70-130 0.0 20.0 Toluene pg/L 20.0 20.4 19.6 102 98.0 76-131 4.0 20.0 1,2,4-Trichlorobenzene pg/L 20.0 19.5 19.7 97.5 98.5 66-139 1.0 20.0 1,1,1-Trichloroethane pg/L 20.0 20.2 19.7 101 98.5 75-135 2.5 20.0 1,1,2-Trichloroethane pg/L 20.0 21.7 21.4 109 107 70-140 1.3 20.0 Trichloroethene pg/L 20.0 21.1 20.4 106 102 77-133 3.3 20.0 Trichlorofluoromethane pg/L 20.0 18.9 17.5 94.5 87.5 62-148 7.6 20.0 1,2,3-Trichloropropane pg/L 20.0 18.9 19.2 94.5 96.0 71-127 1.5 20.0 Vinyl Acetate pg/L 20.0 21.6 22.0 108 110 34-167 1.8 20.0 Vinyl Chloride pg/L 20.0 19.3 18.2 96.5 91.0 57-141 5.8 20.0 o-Xylene pg/L 20.0 19.2 18.8 96.0 94.0 78-128 2.1 20.0 m,p-Xylene pg/L 40.0 40.0 39.7 100 99.2 77-133 0.7 20.0 4-Bromofluorobenzene (S) 97.8 99.8 80-124 Dibromofluoromethane (S) 100 98.0 75-129 1,2-Dichloroethane - d4 (S) 93.6 93.6 63-136 Toluene-d8 (S) 96.2 96.6 77-123 Date: 11/09/2022 10:53 AM Page 21 of 38 Page 103 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24951 QC Prep Batch Method: 5030B Lab Reagent Blank LRB-V24951 Associated Lab Samples: 89903, 89904, 89905 QC Analytical Batch(es): V24952 Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Acetone pg/L <1.80 1.80 5.00 10/11/22 00:30 Acrolein pg/L <2.00 2.00 5.00 10/11/22 00:30 Acrylonitrile pg/L <0.230 0.230 5.00 10/11/22 00:30 Benzene pg/L <0.180 0.180 0.500 10/11/22 00:30 Bromochloromethane pg/L <0.420 0.420 1.00 10/11/22 00:30 Bromodichloromethane pg/L <0.160 0.160 0.500 10/11/22 00:30 Bromoform pg/L <1.50 1.50 5.00 10/11/22 00:30 Bromomethane pg/L <0.280 0.280 1.00 10/11/22 00:30 Carbon Disulfide pg/L <0.150 0.150 5.00 10/11/22 00:30 Carbon Tetrachloride pg/L <0.180 0.180 0.500 10/11/22 00:30 Chlorobenzene pg/L <0.190 0.190 0.500 10/11/22 00:30 Chlorodibromomethane pg/L <0.190 0.190 0.500 10/11/22 00:30 Chloroethane pg/L <0.430 0.430 1.00 10/11/22 00:30 Chloroform pg/L <0.220 0.220 0.500 10/11/22 00:30 Chloromethane pg/L <0.220 0.220 0.500 10/11/22 00:30 1,2-Dibromo-3-Chloropropane pg/L <1.10 1.10 2.00 10/11/22 00:30 1,2-Dibromoethane pg/L <0.200 0.200 0.500 10/11/22 00:30 Dibromomethane pg/L <0.230 0.230 0.500 10/11/22 00:30 trans-1,4-Dichloro-2-butene pg/L < 1.30 1.30 10.0 10/11/22 00:30 1,2-Dichlorobenzene pg/L <0.220 0.220 0.500 10/11/22 00:30 1,3-Dichlorobenzene pg/L <0.190 0.190 0.500 10/11/22 00:30 1,4-Dichlorobenzene pg/L <0.210 0.210 0.500 10/11/22 00:30 Dichlorodifluoromethane pg/L <1.20 1.20 5.00 10/11/22 00:30 1,1-Dichloroethane pg/L <0.240 0.240 0.500 10/11/22 00:30 1,2-Dichloroethane pg/L <0.150 0.150 0.500 10/11/22 00:30 1,1-Dichloroethene pg/L <0.150 0.150 0.500 10/11/22 00:30 cis-1,2-Dichloroethene pg/L <0.200 0.200 0.500 10/11/22 00:30 Date: 11/09/2022 10:53 AM Page 22 of 38 Page 104 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24951 QC Prep Batch Method: 5030B Lab Reagent Blank LRB-V24951 Associated Lab Samples: 89903, 89904, 89905 QC Analytical Batch(es): V24952 Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits trans-1,2-Dichloroethene pg/L <0.180 0.180 0.500 10/11/22 00:30 1,2-Dichloropropane pg/L <0.190 0.190 0.500 10/11/22 00:30 1,3-Dichloropropane pg/L <0.130 0.130 0.500 10/11/22 00:30 2,2-Dichloropropane pg/L <0.210 0.210 2.00 10/11/22 00:30 1,1-Dichloropropene pg/L <0.200 0.200 0.500 10/11/22 00:30 cis-1,3-Dichloropropene pg/L <0.210 0.210 0.500 10/11/22 00:30 trans-1,3-Dichloropropene pg/L <0.150 0.150 0.500 10/11/22 00:30 Ethylbenzene pg/L <0.170 0.170 0.500 10/11/22 00:30 Hexachlorobutadiene pg/L <0.350 0.350 2.00 10/11/22 00:30 2-Hexanone pg/L <0.380 0.380 5.00 10/11/22 00:30 Iodomethane pg/L <0.054 0.054 0.500 10/11/22 00:30 Methyl Ethyl Ketone (MEK) pg/L <0.710 0.710 5.00 10/11/22 00:30 4-Methyl-2-Pentanone pg/L <1.00 1.00 5.00 10/11/22 00:30 Methylene Chloride pg/L <0.330 0.330 1.00 10/11/22 00:30 Naphthalene pg/L <0.470 0.470 1.00 10/11/22 00:30 Styrene pg/L <0.220 0.220 0.500 10/11/22 00:30 1,1,1,2-Tetrachloroethane pg/L <0.160 0.160 0.500 10/11/22 00:30 1,1,2,2-Tetrachloroethane pg/L <0.160 0.160 0.500 10/11/22 00:30 Tetrachloroethene pg/L <0.220 0.220 0.500 10/11/22 00:30 Tetrahydrofuran pg/L <1.50 1.50 10.0 10/11/22 00:30 Toluene pg/L <0.220 0.220 0.500 10/11/22 00:30 1,2,4-Trichlorobenzene pg/L <0.310 0.310 1.00 10/11/22 00:30 1,1,1-Trichloroethane pg/L <0.160 0.160 0.500 10/11/22 00:30 1,1,2-Trichloroethane pg/L <0.096 0.096 0.500 10/11/22 00:30 Trichloroethene pg/L <0.180 0.180 0.500 10/11/22 00:30 Trichlorofluoromethane pg/L <0.180 0.180 0.500 10/11/22 00:30 1,2,3-Trichloropropane pg/L <0.270 0.270 1.00 10/11/22 00:30 Date: 11/09/2022 10:53 AM Page 23 of 38 Page 105 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24951 QC Analytical Batch(es): V24952 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V24951 Matrix: AQU Associated Lab Samples: 89903, 89904, 89905 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Vinyl Acetate pg/L <1.00 1.00 2.00 10/11/22 00:30 Vinyl Chloride pg/L <0.170 0.170 0.500 10/11/22 00:30 o-Xylene pg/L <0.210 0.210 0.500 10/11/22 00:30 m,p-Xylene pg/L <0.420 0.420 1.00 10/11/22 00:30 4-Bromofluorobenzene (S) 10/11/22 00:30 99.6 80-124 Dibromofluoromethane (S) 10/11/22 00:30 96.4 75-129 1,2-Dichloroethane - d4 (S) 10/11/22 00:30 93.4 63-136 Toluene-d8(S) 10/11/22 00:30 96.0 77-123 Laboratory Control Sample & LCSD LCS-V24951 LCSD-V24951 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD a/o Rec % Rec Limits RPD Max RPD Acetone pg/L 40.0 42.1 40.8 105 102 40-166 3.1 20.0 Acrolein pg/L 40.0 42.4 43.7 106 109 70-130 3.0 20.0 Acrylonitrile pg/L 40.0 44.6 47.5 112 119 81-127 6.2 20.0 Benzene pg/L 20.0 21.2 21.0 106 105 77-128 0.9 20.0 Bromochloromethane pg/L 20.0 20.7 19.9 104 99.5 78-135 3.9 20.0 Bromodichloromethane pg/L 20.0 19.8 19.5 99.0 97.5 76-138 1.5 20.0 Bromoform pg/L 20.0 20.3 20.8 102 104 71-135 2.4 20.0 Bromomethane pg/L 20.0 18.2 16.1 91.0 80.5 41-168 12.2 20.0 Carbon Disulfide pg/L 20.0 21.5 20.8 108 104 59-135 3.3 20.0 Carbon Tetrachloride pg/L 20.0 21.0 23.8 105 119 72-142 12.5 20.0 Chlorobenzene pg/L 20.0 20.3 19.7 102 98.5 78-119 3.0 20.0 Chlorodibromomethane pg/L 20.0 20.3 20.1 102 101 75-134 0.9 20.0 Chloroethane pg/L 20.0 17.6 16.9 88.0 84.5 57-142 4.0 20.0 Chloroform pg/L 20.0 21.1 21.2 106 106 77-130 0.4 20.0 Date: 11/09/2022 10:53 AM Page 24 of 38 Page 106 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24951 QC Analytical Batch(es): V24952 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-V24951 LCSD-V24951 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Chloromethane pg/L 20.0 16.8 16.6 84.0 83.0 47-145 1.1 20.0 1,2-Dibromo-3-Chloropropane pg/L 20.0 17.4 17.2 87.0 86.0 63-134 1.1 20.0 1,2-Dibromoethane pg/L 20.0 21.2 21.5 106 108 77-135 1.4 20.0 Dibromomethane pg/L 20.0 20.5 21.0 103 105 76-138 2.4 20.0 trans-1,4-Dichloro-2-butene pg/L 20.0 18.3 18.9 91.5 94.5 70-130 3.2 20.0 1,2-Dichlorobenzene pg/L 20.0 19.0 18.7 95.0 93.5 78-128 1.5 20.0 1,3-Dichlorobenzene pg/L 20.0 19.4 18.9 97.0 94.5 77-125 2.6 20.0 1,4-Dichlorobenzene pg/L 20.0 19.1 18.9 95.5 94.5 75-126 1.0 20.0 Dichlorodifluoromethane pg/L 20.0 18.5 18.3 92.5 91.5 28-163 1.0 20.0 1,1-Dichloroethane pg/L 20.0 21.6 21.4 108 107 70-130 0.9 20.0 1,2-Dichloroethane pg/L 20.0 18.4 18.5 92.0 92.5 68-131 0.5 20.0 1,1-Dichloroethene pg/L 20.0 20.7 19.7 104 98.5 70-154 4.9 20.0 cis-1,2-Dichloroethene pg/L 20.0 21.0 20.5 105 103 76-141 2.4 20.0 trans-1,2-Dichloroethene pg/L 20.0 21.5 20.4 108 102 76-135 5.2 20.0 1,2-Dichloropropane pg/L 20.0 21.0 20.2 105 101 77-130 3.8 20.0 1,3-Dichloropropane pg/L 20.0 19.6 19.9 98.0 99.5 76-132 1.5 20.0 2,2-Dichloropropane pg/L 20.0 18.5 17.8 92.5 89.0 29-149 3.8 20.0 1,1-Dichloropropene pg/L 20.0 23.0 22.7 115 114 71-136 1.3 20.0 cis-1,3-Dichloropropene pg/L 20.0 20.3 20.9 102 105 65-140 2.9 20.0 trans-1,3-Dichloropropene pg/L 20.0 20.3 20.9 102 105 67-140 2.9 20.0 Ethylbenzene pg/L 20.0 19.3 19.1 96.5 95.5 80-127 1.0 20.0 Hexachlorobutadiene pg/L 20.0 16.9 16.8 84.5 84.0 61-134 0.5 20.0 2-Hexanone pg/L 20.0 17.9 17.3 89.5 86.5 64-137 3.4 20.0 Iodomethane pg/L 20.0 15.7 15.6 78.5 78.0 70-130 0.6 20.0 Methyl Ethyl Ketone (MEK) pg/L 20.0 19.8 19.5 99.0 97.5 71-134 1.5 20.0 4-Methyl-2-Pentanone pg/L 20.0 19.3 19.8 96.5 99.0 69-134 2.5 20.0 Date: 11/09/2022 10:53 AM Page 25 of 38 Page 107 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V24951 QC Analytical Batch(es): V24952 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-V24951 LCSD-V24951 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits Methylene Chloride pg/L 20.0 20.3 20.2 102 101 73-131 Naphthalene pg/L 20.0 17.0 17.3 85.0 86.5 64-136 Styrene pg/L 20.0 19.9 20.3 99.5 102 78-129 1,1,1,2-Tetrachloroethane pg/L 20.0 19.7 19.3 98.5 96.5 79-134 1,1,2,2-Tetrachloroethane pg/L 20.0 18.9 19.8 94.5 99.0 62-127 Tetrachloroethene pg/L 20.0 20.9 19.8 105 99.0 80-129 Tetrahydrofuran pg/L 20.0 20.1 21.5 101 108 70-130 Toluene pg/L 20.0 20.9 20.2 105 101 76-131 1,2,4-Trichlorobenzene pg/L 20.0 17.8 16.9 89.0 84.5 66-139 1,1,1-Trichloroethane pg/L 20.0 20.9 21.0 105 105 75-135 1,1,2-Trichloroethane pg/L 20.0 22.0 21.7 110 109 70-140 Trichloroethene pg/L 20.0 22.1 20.8 111 104 77-133 Trichlorofluoromethane pg/L 20.0 19.7 18.4 98.5 92.0 62-148 1,2,3-Trichloropropane pg/L 20.0 18.9 19.9 94.5 99.5 71-127 Vinyl Acetate pg/L 20.0 17.7 20.7 88.5 104 34-167 Vinyl Chloride pg/L 20.0 19.8 19.2 99.0 96.0 57-141 o-Xylene pg/L 20.0 19.3 18.4 96.5 92.0 78-128 m,p-Xylene pg/L 40.0 40.3 39.1 101 97.7 77-133 4-Bromofluorobenzene (S) 99.8 101 80-124 Dibromofluoromethane (S) 100 101 75-129 1,2-Dichloroethane - d4 (S) 93.4 94.0 63-136 Toluene-d8 (S) 96.2 95.4 77-123 RPD 0.4 1.7 1.9 2.0 4.6 5.4 6.7 3.4 5.1 0.4 1.3 6.0 6.8 5.1 15.6 3.0 4.7 3.0 Max RPD 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 Date: 11/09/2022 10:53 AM Page 26 of 38 Page 108 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V25068 QC Analytical Batch(es): V25069 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V25068 Matrix: AQU Associated Lab Samples: 89898, 89902 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Acetonitrile pg/L <20.3 20.3 10.0 10/13/22 00:53 Allyl Chloride pg/L <0.579 0.579 10.0 10/13/22 00:53 Chloroprene pg/L <0.450 0.450 10.0 10/13/22 00:53 Ethyl Methacrylate pg/L < 1.62 1.62 10.0 10/13/22 00:53 Methacrylonitrile pg/L <12.6 12.6 10.0 10/13/22 00:53 Propionitrile pg/L <23.7 23.7 10.0 10/13/22 00:53 4-Bromofluorobenzene (S) 10/13/22 00:53 102 80-124 Dibromofluoromethane (S) 10/13/22 00:53 99.0 75-129 1,2-Dichloroethane - d4 (S) 10/13/22 00:53 96.6 63-136 Toluene-d8 (S) 10/13/22 00:53 97.8 77-123 Laboratory Control Sample & LCSD LCS-V25068 LCSD-V25068 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD Acetonitrile pg/L 20.0 21.1 <20.3 106 0.0* 40-160 3.8 20.0 Allyl Chloride pg/L 20.0 19.9 20.2 99.5 101 40-160 1.4 20.0 Chloroprene pg/L 20.0 21.2 21.8 106 109 40-160 2.7 20.0 Ethyl Methacrylate pg/L 20.0 19.9 19.5 99.5 97.5 40-160 2.0 20.0 Methacrylonitrile pg/L 20.0 20.1 20.1 101 101 40-160 0.0 20.0 Propionitrile pg/L 20.0 <23.7 <23.7 0.0* 0.0* 40-160 0.0 20.0 4-Bromofluorobenzene (S) 101 99.4 80-124 Dibromofluoromethane (S) 101 101 75-129 1,2-Dichloroethane - d4 (S) 96.2 97.0 63-136 Toluene-d8(S) 99.4 98.0 77-123 * QC Fail Date: 11/09/2022 10:53 AM Page 27 of 38 Page 109 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: V25248 QC Analytical Batch(es): V25249 QC Prep Batch Method: 5030B Analysis Method: 8260D Analysis Description: Volatile Organic Compounds - GC/MS Lab Reagent Blank LRB-V25248 Matrix: AQU Associated Lab Samples: 89901, 89903, 89904, 89905 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Acetonitrile pg/L <20.3 20.3 10.0 10/17/22 18:49 Allyl Chloride pg/L <0.579 0.579 10.0 10/17/22 18:49 Chloroprene pg/L <0.450 0.450 10.0 10/17/22 18:49 Ethyl Methacrylate pg/L < 1.62 1.62 10.0 10/17/22 18:49 Methacrylonitrile pg/L <12.6 12.6 10.0 10/17/22 18:49 Propionitrile pg/L <23.7 23.7 10.0 10/17/22 18:49 4-Bromofluorobenzene (S) 10/17/22 18:49 98.2 80-124 Dibromofluoromethane (S) 10/17/22 18:49 97.2 75-129 1,2-Dichloroethane - d4 (S) 10/17/22 18:49 97.0 63-136 Toluene-d8(S) 10/17/22 18:49 100 77-123 Laboratory Control Sample & LCSD LCS-V25248 LCSD-V25248 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD Acetonitrile pg/L 20.0 <20.3 <20.3 0.0* 0.0* 40-160 0.0 20.0 Allyl Chloride pg/L 20.0 20.5 20.7 103 104 40-160 0.9 20.0 Chloroprene pg/L 20.0 21.2 22.4 106 112 40-160 5.5 20.0 Ethyl Methacrylate pg/L 20.0 20.1 19.9 101 99.5 40-160 1.0 20.0 Methacrylonitrile pg/L 20.0 18.4 18.2 92.0 91.0 40-160 1.0 20.0 Propionitrile pg/L 20.0 <23.7 <23.7 0.0* 0.0* 40-160 0.0 20.0 4-Bromofluorobenzene (S) 101 99.2 80-124 Dibromofluoromethane (S) 102 102 75-129 1,2-Dichloroethane - d4 (S) 97.6 98.6 63-136 Toluene-d8(S) 101 101 77-123 * QC Fail Date: 11/09/2022 10:53 AM Page 28 of 38 Page 110 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642252 QC Prep Batch Method: 3510C Lab Reagent Blank LRB-L642252 Associated Lab Samples: 89898, 89901, 89902 Blank MDL Parameter Units Result Dimethoate pg/L <0.713 0.713 Disulfoton pg/L <0.466 0.466 Ethyl Parathion pg/L <0.568 0.568 Famphur pg/L <0.512 0.512 Methyl Parathion pg/L <0.805 0.805 Phorate pg/L <0.659 0.659 0,0,0-Triethyl Phosphorothioate pg/L <0.330 0.330 Tributyl phosphate (S) Triphenyl phosphate (S) QC Analytical Batch(es): L644472 Analysis Method: 8270C Analysis Description: Organophosphorus Pesticides by GC/MS Matrix: AQU MQL Analyzed 0/0 Recovery 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 1.00 10/24/22 13:52 10/24/22 13:52 68.5 10/24/22 13:52 72.5 Laboratory Control Sample & LCSD LCS-L642252 LCSD-L642252 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits Dimethoate pg/L 20.0 11.1 8.79 55.5 43.9 40-140 Disulfoton pg/L 20.0 12.4 10.2 62.0 51.0 40-140 Ethyl Parathion pg/L 20.0 12.4 9.83 62.0 49.1 40-140 Famphur pg/L 20.0 13.6 11.1 68.0 55.5 40-140 Methyl Parathion pg/L 20.0 14.0 11.1 70.0 55.5 40-140 Phorate pg/L 20.0 12.1 10.0 60.5 50.0 40-140 0,0,0-Triethyl Phosphorothioate pg/L 20.0 12.6 10.8 63.0 54.0 40-140 Tributyl phosphate (S) 64.0 60.5 50-150 Triphenyl phosphate (S) 68.0 63.5 50-150 Rec Limits 50-150 50-150 RPD Max RPD 23.2* 20.0 19.4 20.0 23.1* 20.0 20.2* 20.0 23.1* 20.0 19.0 20.0 15.3 20.0 * QC Fail Date: 11/09/2022 10:53 AM Page 111 of 123 Page 29 of 38 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642250 QC Prep Batch Method: 3510C Lab Reagent Blank LRB-1-642250 Associated Lab Samples: 89898, 89901, 89902 QC Analytical Batch(es): L644470 Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 1,3-Dinitrobenzene pg/L <0.904 0.904 10.0 10/20/22 19:45 Acenaphthene pg/L <0.422 0.422 2.00 10/20/22 19:45 Acenaphthylene pg/L <0.429 0.429 2.00 10/20/22 19:45 Acetophenone pg/L <0.686 0.686 5.00 10/20/22 19:45 Anthracene pg/L <0.467 0.467 2.00 10/20/22 19:45 Benzo(a)anthracene pg/L <0.427 0.427 2.00 10/20/22 19:45 Benzo(a)pyrene pg/L <1.00 1.00 2.00 10/20/22 19:45 Benzo(b)fluoranthene pg/L <0.941 0.941 2.00 10/20/22 19:45 Benzo(g,h,i)perylene pg/L <1.36 1.36 2.00 10/20/22 19:45 Benzo(k)fluoranthene pg/L <0.752 0.752 2.00 10/20/22 19:45 Benzyl alcohol pg/L <3.01 3.01 10.0 10/20/22 19:45 Bis(2-Chloroethoxy)methane pg/L <0.433 0.433 5.00 10/20/22 19:45 Bis(2-Chloroethyl)ether pg/L <0.447 0.447 5.00 10/20/22 19:45 Bis(2-Chloroisopropyl)ether pg/L <0.546 0.546 5.00 10/20/22 19:45 Bis(2-ethylhexyl)phthalate pg/L <3.66 3.66 5.00 10/20/22 19:45 4-Bromophenyl phenyl ether pg/L <0.500 0.500 5.00 10/20/22 19:45 Butyl benzyl phthalate pg/L <4.59 4.59 5.00 10/20/22 19:45 4-Chloro-3-methylphenol pg/L <0.503 0.503 5.00 10/20/22 19:45 4-Chloroaniline pg/L <0.526 0.526 5.00 10/20/22 19:45 Chlorobenzilate pg/L <1.90 1.90 5.00 10/20/22 19:45 2-Chloronaphthalene pg/L <0.476 0.476 5.00 10/20/22 19:45 2-Chlorophenol pg/L <0.736 0.736 5.00 10/20/22 19:45 4-Chlorophenyl phenyl ether pg/L <0.479 0.479 5.00 10/20/22 19:45 Chrysene pg/L <0.731 0.731 2.00 10/20/22 19:45 Dibenz(a,h)anthracene pg/L <0.252 0.252 2.00 10/20/22 19:45 Dibenzofuran pg/L <0.423 0.423 5.00 10/20/22 19:45 1,2-Dichlorobenzene pg/L <0.629 0.629 5.00 10/20/22 19:45 Date: 11/09/2022 10:53 AM Page 30 of 38 Page 112 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642250 QC Prep Batch Method: 3510C Lab Reagent Blank LRB-1-642250 Associated Lab Samples: 89898, 89901, 89902 QC Analytical Batch(es): L644470 Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Matrix: AQU Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 1,3-Dichlorobenzene pg/L <0.491 0.491 5.00 10/20/22 19:45 1,4-Dichlorobenzene pg/L <0.580 0.580 5.00 10/20/22 19:45 3,3'-Dichlorobenzidine pg/L <3.74 3.74 10.0 10/20/22 19:45 2,4-Dichlorophenol pg/L <1.52 1.52 5.00 10/20/22 19:45 2,6-Dichlorophenol pg/L <0.703 0.703 5.00 10/20/22 19:45 Diethyl phthalate pg/L <0.585 0.585 5.00 10/20/22 19:45 Dimethyl phthalate pg/L <0.510 0.510 5.00 10/20/22 19:45 3,3' Dimethylbenzidine pg/L <1.88 1.88 10.0 10/20/22 19:45 2,4-Dimethylphenol pg/L <0.674 0.674 5.00 10/20/22 19:45 Di-n-butyl phthalate pg/L <1.58 1.58 5.00 10/20/22 19:45 4,6- Din itro-2-methylphenol pg/L <3.47 3.47 10.0 10/20/22 19:45 2,4-Dinitrophenol pg/L <4.85 4.85 10.0 10/20/22 19:45 2,4-Dinitrotoluene pg/L <0.403 0.403 5.00 10/20/22 19:45 2,6-Dinitrotoluene pg/L <0.413 0.413 5.00 10/20/22 19:45 Di-n-Octyl Phthalate pg/L <1.72 1.72 5.00 10/20/22 19:45 Ethyl methanesulfonate pg/L <0.714 0.714 5.00 10/20/22 19:45 Fluoranthene pg/L <0.406 0.406 2.00 10/20/22 19:45 Fluorene pg/L <0.444 0.444 2.00 10/20/22 19:45 Hexachlorobenzene pg/L <2.57 2.57 5.00 10/20/22 19:45 Hexachlorobutadiene pg/L <0.405 0.405 5.00 10/20/22 19:45 Hexachlorocyclopentadiene pg/L <2.34 2.34 5.00 10/20/22 19:45 Hexachloroethane pg/L <0.277 0.277 5.00 10/20/22 19:45 Indeno(1,2,3-cd)pyrene pg/L <1.01 1.01 2.00 10/20/22 19:45 Isophorone pg/L <0.360 0.360 5.00 10/20/22 19:45 Methyl methanesulfonate pg/L <0.618 0.618 5.00 10/20/22 19:45 2-Methylnaphthalene pg/L <0.485 0.485 2.00 10/20/22 19:45 2-Methylphenol pg/L <0.721 0.721 5.00 10/20/22 19:45 Date: 11/09/2022 10:53 AM Page 31 of 38 Page 113 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642250 QC Analytical Batch(es): L644470 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Lab Reagent Blank LRB-1-642250 Matrix: AQU Associated Lab Samples: 89898, 89901, 89902 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits 3&4 Methylphenol pg/L <0.691 0.691 5.00 10/20/22 19:45 Naphthalene pg/L <0.484 0.484 2.00 10/20/22 19:45 2-Nitroaniline pg/L <0.574 0.574 5.00 10/20/22 19:45 3-Nitroaniline pg/L <1.53 1.53 10.0 10/20/22 19:45 4-Nitroaniline pg/L <0.740 0.740 5.00 10/20/22 19:45 Nitrobenzene pg/L <0.531 0.531 5.00 10/20/22 19:45 2-Nitrophenol pg/L <0.606 0.606 5.00 10/20/22 19:45 4-Nitrophenol pg/L <1.39 1.39 10.0 10/20/22 19:45 N-Nitrosodimethylamine pg/L <0.249 0.249 5.00 10/20/22 19:45 N-Nitrosodiphenylamine pg/L <0.783 0.783 10.0 10/20/22 19:45 N-Nitrosodiethylamine pg/L <0.400 0.400 5.00 10/20/22 19:45 N-Nitroso-di-n-butylamine pg/L <0.752 0.752 5.00 10/20/22 19:45 N-Nitroso-di-n-propylamine pg/L <0.334 0.334 5.00 10/20/22 19:45 Pentachloronitrobenzene pg/L <1.15 1.15 5.00 10/20/22 19:45 Pentachlorophenol pg/L <2.45 2.45 10.0 10/20/22 19:45 Phenacetin pg/L <1.28 1.28 5.00 10/20/22 19:45 Phenanthrene pg/L <0.464 0.464 2.00 10/20/22 19:45 Phenol pg/L <0.389 0.389 5.00 10/20/22 19:45 Pyrene pg/L <1.04 1.04 2.00 10/20/22 19:45 1,2,4,5-Tetrachlorobenzene pg/L <0.317 0.317 5.00 10/20/22 19:45 2,3,4,6-Tetrachlorophenol pg/L <0.355 0.355 5.00 10/20/22 19:45 1,2,4-Trichlorobenzene pg/L <0.482 0.482 5.00 10/20/22 19:45 2,4,5-Trichlorophenol pg/L <0.350 0.350 5.00 10/20/22 19:45 2,4,6-Trichlorophenol pg/L <0.344 0.344 5.00 10/20/22 19:45 2-Fluorobiphenyl(S) 10/20/22 19:45 54.3 24-93 2-Fluorophenol(S) 10/20/22 19:45 21.2 10-44 Nitrobenzene-d5 (S) 10/20/22 19:45 54.4 20-91 Date: 11/09/2022 10:53 AM Page 32 of 38 Page 114 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642250 QC Analytical Batch(es): L644470 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Lab Reagent Blank LRB-1-642250 Matrix: AQU Associated Lab Samples: 89898, 89901, 89902 Blank MDL MQL Analyzed % % Rec Parameter Units Result Recovery Limits Phenol-d6 (S) 10/20/22 19:45 13.6 7-32 4-Terphenyl-d14 (S) 10/20/22 19:45 63.6 35-126 2,4,6-Tribromophenol(S) 10/20/22 19:45 62.4 39-110 Laboratory Control Sample & LCSD LCS-L642250 LCSD-L642250 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD 1,3-Dinitrobenzene pg/L 50.0 48.6 43.3 97.2 86.6 45-135 11.5 20.0 Acenaphthene pg/L 50.0 30.2 26.1 60.4 52.2 38-117 14.5 20.0 Acenaphthylene pg/L 50.0 25.3 22.1 50.6 44.2 37-114 13.5 20.0 Acetophenone pg/L 50.0 29.1 25.1 58.2 50.2 25-108 14.7 20.0 Anthracene pg/L 50.0 29.2 25.7 58.4 51.4 34-128 12.7 20.0 Benzo(a)anthracene pg/L 50.0 31.7 27.4 63.4 54.8 36-127 14.5 20.0 Benzo(a)pyrene pg/L 50.0 30.1 26.2 60.2 52.4 34-131 13.8 20.0 Benzo(b)fluoranthene pg/L 50.0 32.2 26.4 64.4 52.8 36-131 19.7 20.0 Benzo(g,h,i)perylene pg/L 50.0 27.5 25.9 55.0 51.8 26-123 5.9 20.0 Benzo(k)fluoranthene pg/L 50.0 35.1 31.5 70.2 63.0 32-132 10.8 20.0 Benzyl alcohol pg/L 50.0 19.6 17.3 39.2 34.6 20-109 12.4 20.0 Bis(2-Chloroethoxy)methane pg/L 50.0 29.1 25.1 58.2 50.2 20-126 14.7 20.0 Bis(2-Chloroethyl)ether pg/L 50.0 26.0 22.3 52.0 44.6 16-122 15.3 20.0 Bis(2-Chloroisopropyl)ether pg/L 50.0 23.0 19.7 46.0 39.4 28-108 15.4 20.0 Bis(2-ethylhexyl)phthalate pg/L 50.0 33.0 29.6 66.0 59.2 21-162 10.8 20.0 4-Bromophenyl phenyl ether pg/L 50.0 32.8 28.6 65.6 57.2 31-124 13.6 20.0 Butyl benzyl phthalate pg/L 50.0 34.1 30.9 68.2 61.8 33-142 9.8 20.0 4-Chloro-3-methyl phenol pg/L 50.0 27.0 24.6 54.0 49.2 35-117 9.3 20.0 4-Chloroaniline pg/L 50.0 21.6 18.2 43.2 36.4 24-127 17.0 20.0 Date: 11/09/2022 10:53 AM Page 33 of 38 Page 115 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642250 QC Analytical Batch(es): L644470 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-L642250 LCSD-L642250 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Chlorobenzilate pg/L 50.0 35.1 31.7 70.2 63.4 35-118 10.1 20.0 2-Chloronaphthalene pg/L 50.0 28.4 24.3 56.8 48.6 29-137 15.5 20.0 2-Chlorophenol pg/L 50.0 22.9 20.2 45.8 40.4 27-102 12.5 20.0 4-Chlorophenyl phenyl ether pg/L 50.0 31.9 27.9 63.8 55.8 39-110 13.3 20.0 Chrysene pg/L 50.0 28.7 25.0 57.4 50.0 30-124 13.7 20.0 Dibenz(a,h)anthracene pg/L 50.0 30.5 28.4 61.0 56.8 27-124 7.1 20.0 Dibenzofuran pg/L 50.0 32.0 28.2 64.0 56.4 40-108 12.6 20.0 1,2-Dichlorobenzene pg/L 50.0 25.4 22.0 50.8 44.0 26-100 14.3 20.0 1,3-Dichlorobenzene pg/L 50.0 24.1 21.3 48.2 42.6 21-102 12.3 20.0 1,4-Dichlorobenzene pg/L 50.0 24.1 21.0 48.2 42.0 24-99 13.7 20.0 3,3'-Dichlorobenzidine pg/L 150 86.9 78.6 57.9 52.4 6-192 10.0 20.0 2,4-Dichlorophenol pg/L 50.0 30.6 27.6 61.2 55.2 32-110 10.3 20.0 2,6-Dichlorophenol pg/L 50.0 31.8 27.7 63.6 55.4 25-112 13.7 20.0 Diethyl phthalate pg/L 50.0 31.6 28.9 63.2 57.8 36-130 8.9 20.0 Dimethyl phthalate pg/L 50.0 29.8 27.8 59.6 55.6 34-123 6.9 20.0 3,3' Dimethylbenzidine pg/L 200 36.4 30.6 18.2 15.3 6-192 17.3 20.0 2,4-Dimethylphenol pg/L 50.0 9.67 10.4 19.3* 20.8* 34-105 7.2 20.0 Di-n-butyl phthalate pg/L 50.0 31.0 27.2 62.0 54.4 19-158 13.0 20.0 4,6- Din itro-2-methylphenol pg/L 50.0 38.0 33.5 76.0 67.0 27-128 12.5 20.0 2,4-Dinitrophenol pg/L 150 88.6 78.7 59.0 52.4 10-132 11.8 20.0 2,4-Dinitrotoluene pg/L 50.0 31.0 28.0 62.0 56.0 24-147 10.1 20.0 2,6-Dinitrotoluene pg/L 50.0 31.7 28.1 63.4 56.2 36-125 12.0 20.0 Di-n-Octyl Phthalate pg/L 50.0 34.4 31.6 68.8 63.2 29-136 8.4 20.0 Ethyl methanesulfonate pg/L 50.0 26.9 22.8 53.8 45.6 20-121 16.4 20.0 Fluoranthene pg/L 50.0 30.6 27.1 61.2 54.2 28-127 12.1 20.0 Fluorene pg/L 50.0 31.7 28.2 63.4 56.4 41-116 11.6 20.0 * QC Fail Date: 11/09/2022 10:53 AM Page 34 of 38 Page 116 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642250 QC Analytical Batch(es): L644470 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-L642250 LCSD-L642250 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD Hexachlorobenzene pg/L 50.0 32.9 29.0 65.8 58.0 18-136 12.6 20.0 Hexachlorobutadiene pg/L 50.0 28.0 23.9 56.0 47.8 22-109 15.7 20.0 Hexachlorocyclopentadiene pg/L 50.0 26.5 23.9 53.0 47.8 10-102 10.3 20.0 Hexachloroethane pg/L 50.0 24.5 21.6 49.0 43.2 16-107 12.5 20.0 Indeno(1,2,3-cd)pyrene pg/L 50.0 30.4 28.7 60.8 57.4 22-126 5.7 20.0 Isophorone pg/L 50.0 15.5 13.3 31.0 26.6* 31-116 15.2 20.0 Methyl methanesulfonate pg/L 50.0 18.2 15.5 36.4 31.0 15-82 16.0 20.0 2-Methylnaphthalene pg/L 50.0 30.4 26.5 60.8 53.0 34-108 13.7 20.0 2-Methylphenol pg/L 50.0 16.4 15.0 32.8 30.0 22-97 8.9 20.0 3&4 Methylphenol pg/L 50.0 17.0 15.8 34.0 31.6 21-96 7.3 20.0 Naphthalene pg/L 50.0 27.1 23.2 54.2 46.4 33-108 15.5 20.0 2-Nitroaniline pg/L 50.0 32.8 29.0 65.6 58.0 32-127 12.2 20.0 3-Nitroaniline pg/L 50.0 27.3 24.5 54.6 49.0 28-142 10.8 20.0 4-Nitroaniline pg/L 50.0 36.6 33.5 73.2 67.0 23-139 8.8 20.0 Nitrobenzene pg/L 50.0 27.2 23.4 54.4 46.8 27-117 15.0 20.0 2-Nitrophenol pg/L 50.0 30.6 26.0 61.2 52.0 25-114 16.2 20.0 4-Nitrophenol pg/L 50.0 7.40 6.71 14.8 13.4 1-76 9.7 20.0 N-Nitrosodimethylamine pg/L 50.0 13.5 11.4 27.0 22.8 14-84 16.8 20.0 N-Nitrosodiphenylamine pg/L 50.0 26.7 23.7 53.4 47.4 45-135 11.9 20.0 N-Nitrosodiethylamine pg/L 50.0 28.3 23.9 56.6 47.8 25-107 16.8 20.0 N-Nitroso-di-n-butylamine pg/L 50.0 29.8 26.1 59.6 52.2 25-126 13.2 20.0 N-Nitroso-di-n-propylamine pg/L 50.0 26.2 22.6 52.4 45.2 29-114 14.7 20.0 Pentachloronitrobenzene pg/L 50.0 36.2 32.9 72.4 65.8 34-135 9.5 20.0 Pentachlorophenol pg/L 50.0 16.7 11.7 33.4 23.4 17-142 35.2* 20.0 Phenacetin pg/L 50.0 30.1 27.3 60.2 54.6 29-141 9.7 20.0 Phenanthrene pg/L 50.0 28.2 24.9 56.4 49.8 40-120 12.4 20.0 * QC Fail Date: 11/09/2022 10:53 AM Page 35 of 38 Page 117 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642250 QC Analytical Batch(es): L644470 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS Laboratory Control Sample & LCSD LCS-L642250 LCSD-L642250 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD Phenol pg/L 50.0 7.87 7.37 15.7 14.7 11-55 6.5 20.0 Pyrene pg/L 50.0 33.5 30.4 67.0 60.8 20-154 9.7 20.0 1,2,4,5-Tetrachlorobenzene pg/L 50.0 29.9 25.7 59.8 51.4 28-110 15.1 20.0 2,3,4,6-Tetrachlorophenol pg/L 50.0 29.6 26.1 59.2 52.2 28-118 12.5 20.0 1,2,4-Trichlorobenzene pg/L 50.0 27.9 23.9 55.8 47.8 23-106 15.4 20.0 2,4,5-Trichlorophenol pg/L 50.0 31.3 27.0 62.6 54.0 26-118 14.7 20.0 2,4,6-Trichlorophenol pg/L 50.0 31.7 27.4 63.4 54.8 26-115 14.5 20.0 2-Fluorobiphenyl (S) 54.0 50.2 24-93 2-Fluorophenol (S) 20.6 19.8 10-44 Nitrobenzene-d5 (S) 54.0 49.4 20-91 Phenol-d6 (S) 13.7 13.1 7-32 4-Terphenyl-d14 (S) 65.3 63.3 35-126 2,4,6-Tribromophenol(S) 64.9 60.2 39-110 Date: 11/09/2022 10:53 AM Page 36 of 38 Page 118 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642251 QC Analytical Batch(es): L644471 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: 8270 Extended List Lab Reagent Blank LRB-1-642251 Matrix: AQU Associated Lab Samples: 89898, 89901, 89902 Blank MDL MQL Analyzed Parameter Units Result 1,3,5-Trinitrobenzene pg/L <10.0 10.0 10.0 10/20/2219:45 Isodrin pg/L <10.0 10.0 10.0 10/20/2219:45 Kepone pg/L <10.0 10.0 10.0 10/20/22 19:45 1,4-Naphthoquinone pg/L <10.0 10.0 10.0 10/20/2219:45 1-Naphthylamine pg/L <10.0 10.0 10.0 10/20/2219:45 2-Acetylaminofluorene pg/L <10.0 10.0 10.0 10/20/2219:45 2-Naphthylamine pg/L <10.0 10.0 10.0 10/20/2219:45 3-Methylcholanthrene pg/L <10.0 10.0 10.0 10/20/2219:45 4-Aminobiphenyl pg/L <10.0 10.0 10.0 10/20/2219:45 5-Nitro-o-toluidine pg/L <10.0 10.0 10.0 10/20/2219:45 7,12-Di methyl benz(a)anth racene pg/L <10.0 10.0 10.0 10/20/2219:45 Diallate pg/L <10.0 10.0 10.0 10/20/2219:45 Hexachloropropene pg/L <10.0 10.0 10.0 10/20/2219:45 Isosafrole pg/L <10.0 10.0 10.0 10/20/2219:45 Methapyrilene pg/L <10.0 10.0 20.0 10/20/2219:45 N-Nitrosomethylethylamine pg/L <10.0 10.0 10.0 10/20/2219:45 N-Nitrosomorpholine pg/L <10.0 10.0 10.0 10/20/2219:45 N-Nitrosopiperidine pg/L <10.0 10.0 10.0 10/20/2219:45 N-Nitrosopyrrolidine pg/L <10.0 10.0 10.0 10/20/2219:45 o-Toluidine pg/L <10.0 10.0 10.0 10/20/2219:45 p-Dimethylaminoazobenzene pg/L <10.0 10.0 10.0 10/20/2219:45 p-Phenylenediamine pg/L <10.0 10.0 10.0 10/20/2219:45 Pronamide pg/L <10.0 10.0 10.0 10/20/2219:45 Safrole pg/L <10.0 10.0 10.0 10/20/2219:45 Date: 11/09/2022 10:53 AM Page 37 of 38 Page 119 of 123 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Quality Control Data Client ID: Anchor QEA of North Carolina, PLLC Project Description: Jackson County Report No: 22-277-0040 QC Prep: L642251 QC Analytical Batch(es): L644471 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: 8270 Extended List Laboratory Control Sample & LCSD LCS-L642251 LCSD-L642251 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD 1,3,5-Trinitrobenzene pg/L 50.0 29.8 33.8 59.6 67.6 20-120 12.5 20.0 Isodrin pg/L 50.0 28.9 28.7 57.8 57.4 20-120 0.6 20.0 Kepone pg/L 50.0 27.4 30.3 54.8 60.6 20-120 10.0 20.0 1,4-Naphthoquinone pg/L 50.0 13.9 14.7 27.8 29.4 20-120 5.5 20.0 1-Naphthylamine pg/L 50.0 10.3 <10.0 20.6 0.0* 20-120 2.9 20.0 2-Acetylaminofluorene pg/L 50.0 29.7 31.5 59.4 63.0 20-120 5.8 20.0 2-Naphthylamine pg/L 50.0 23.8 20.1 47.6 40.2 20-120 16.8 20.0 3-Methylcholanthrene pg/L 50.0 24.7 23.8 49.4 47.6 20-120 3.7 20.0 4-Aminobiphenyl pg/L 50.0 25.7 21.8 51.4 43.6 20-120 16.4 20.0 5-Nitro-o-toluidine pg/L 50.0 28.6 30.7 57.2 61.4 20-120 7.0 20.0 7,12-Di methyl benz(a)anth racene pg/L 50.0 20.5 19.7 41.0 39.4 20-120 3.9 20.0 Diallate pg/L 50.0 27.7 27.2 55.4 54.4 20-120 1.8 20.0 Hexachloropropene pg/L 50.0 18.2 18.8 36.4 37.6 20-120 3.2 20.0 Isosafrole pg/L 50.0 20.5 22.7 41.0 45.4 20-120 10.1 20.0 Methapyrilene pg/L 50.0 27.6 20.5 55.2 41.0 20-120 29.5* 20.0 N-Nitrosomethylethylamine pg/L 50.0 21.0 20.1 42.0 40.2 20-120 4.3 20.0 N-Nitrosomorpholine pg/L 50.0 20.4 19.8 40.8 39.6 20-120 2.9 20.0 N-Nitrosopiperidine pg/L 50.0 23.2 24.0 46.4 48.0 20-120 3.3 20.0 N-Nitrosopyrrolidine pg/L 50.0 22.7 21.8 45.4 43.6 20-120 4.0 20.0 o-Toluidine pg/L 50.0 25.2 19.4 50.4 38.8 20-120 26.0* 20.0 p-Dimethylaminoazobenzene pg/L 50.0 28.9 28.0 57.8 56.0 20-120 3.1 20.0 p-Phenylenediamine pg/L 50.0 <10.0 <10.0 0.0* 0.0* 20-120 0.0 20.0 Pronamide pg/L 50.0 29.5 30.7 59.0 61.4 20-120 3.9 20.0 Safrole pg/L 50.0 24.1 24.8 48.2 49.6 20-120 2.8 20.0 * QC Fail Date: 11/09/2022 10:53 AM Page 38 of 38 Page 120 of 123 WayPAoint. NALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: 01015 Customer Name: Anchor QEA of North Carolina, PLLC Report Number: 22-277-0040 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client # Courier 0 Other: Thermometer ID: IRT-15 2.7C Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F Custody seals intact on shipping container/cooler? (*� Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample Iabel(s)? (0) Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? U Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? U Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. U Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No U N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F Low concentration EnCore samplers (48 hr) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: ngelo Norvell Date & Time: 10/04/2022 19:49:35 Page 121 of 123 1 An( Jac v CHAIN OF CUSTODY RECORDWaypoint•PAGE [ OF J— QUOTE N TOENSURE PROPER BILLING:__ Y NO NIA ANALYTICAL Protect Name: �� 1 Samples INTACT upon arrival? IN ICE? 449 Springbravk Road •Charlotte, NC 28217 Phone 7041529-6364 • Fax: 70V525-D409 Short Hold Analysis (Yes) U Project: (Yes) �) `Please ATTACH ;Received PROPER PRESERVATIVES indicated? C Received WITHIN HOLDING TIMES? ]� Company Name: r any project IC reporting (QC LEVEL 1 li I I Client provisions and/or QC R/e-quire n s CUSTODY SEALS INTACT? Report TolContact Name: � Invoice To: il� VOLATiLES rec'd WIOUT HEADSPACE7 Reporting Address: _� Address: PROPER CONTAI S used? _ -C TEMP: Therm ID Observed— 17 ICarrZ77-C TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Phone: Fax (Yes)(No): Purchase Order NoJBilling Reference Email Address: Requested Due Date Ll 1 Day Days J 3 Days J 4 Days J 5 Days Certification: NC � Sc EDD Type: PDF ExCBI Other Working Days" J 6-9 Day�tandard 10 days L] PreAppoust Be Site Location Name: Samples received after 15:OD will be processed next business day Other NIA Site Location Physicat Address: Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES NO Y�/ I� LJf i (SEE REVERSE FOR TERMS 3 CONDITIONS REGARDJNG SERVICES Samples Iced Upon Collec ion: YES,Ip_ RENDERED BY WAYPOINT ANALYTICAL. LLC TO CLIENT) CLIENT DATE TIME COLLECTED MATRIX (SOIL, SAMPLE CONTAINER PRESERVA- ANALYSIS REQUESTEDa KS 1D NO. SAMPLE DESCRIPTION COLLECTED MILITARY HOURS` WATER, OR SLUDGE) 'TYPE NO SIZE TIVES Cif :r SEE BELOW {; Mrs-0'2- U2-'KDv3 I b jb 2-022 10bQ w } i st vadez 1w+ru•b�-2oz21[ad3 �triA3j?b=t IS� ,}� w 43 - 2[7121ab3 119({� .Zb7Z 1 �fb sou- -�zlax [�falau YJ L.r 2012-1004 iD b3 -=1003Q X Z-1D I� lb r Sampler's Signature Sampled By (Print Name) _' r-6HTptise 1 ( LU Affiliation —1 LAB USE ONLY Upon relinquishing, this Chain of Custody is your authorization for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be SIOe Arrival Time: submitted in writing to the Waypoint Analytical Project Manager. There will be charges for any changes after analyses have been initializsd. Relin shed By: (Signatu Received By: (Signature) Dale MililarylHours Additional Comments: Site Departure Time: Lid Re inquish Hy- ( r, Lure) Recelved : (Signature) Da Field Tech Fee: Relinquis�hea By tSignalure) 6Mileage: Received For Wa nalyUcal By: fo'r.owp LIT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. Na If �� ii lil�i ills iiflil iill lliii lii�ii 111111111111 � UHT1L RECEIVED AT THE LABORATORY. �lii 01015 19:46-15 } Other , hot QEAof North Carolina PLLC 19 g6:15 WATER: SOLID WASTE: RCRA: BRWNFLD LANDFILL OTHER: Irson County C J NC ❑ SC I J NC J SC o NC J SC L i NC Zi Sc J NC LJ SC nR IC I1V et ass P = Plastic; TL = Teflon -Lined Cap VOA - Volatile Organics Analysis (Zero Head Space) L x L N L K ro m a 7 0 Kj n a =� r Q ❑ y > m v (Al cv) °a YA x C m m W rn �m v r m o n ❑ x z Cn x m M _ N m 22-277-0o4e Ar"`hor 4ER of North Carolina, PLLC 01015 Jackson COU.Iy 10-04-2022 9 46 15 (ninmm�i m m d 3 0 a� m m a 7 7 y z a Qp � 61 N � n k N z v m c o3 7 Rai m�am Q m ZQ m ❑ O C mAmm m m 4 m 0 a m T rr d m p J L L ° Cm� i A 7 O Z a y w m L yn��� 1 z G N ° a z y v O �VpI N C. r N D C W 0 n �mc CD i7 F'y7,� �r 0 F- in A icna��O m vn'i a 3 o L� a a� D c m 01 N In 03 r10 y m 3 Am � n p to m W o n 'L p o r = o fn a 4 m�4 Z n 0 e rA z n -i x a C fA r z L3 z D m Cl1 z Z m r n j y'[Ab y = aw j�.I o r ata]� 10 y w n'< at °c �-a 4 o C 0 m to`� C a . O w 0 c m n v � v 7 y �a W m r M< n o Z m� m r W ° v m ;a0 C r-0 C, f0.3 C m O m m� m x -irClcx cz. m m o umiw� z y 0 Y a N z m a r M c moo' i C) v N� m a ��I11111rr Page 123 of 123